NCG020330_COMPLETE FILE - HISTORICAL_20161007

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/v C& bJ b 33
DOC TYPE
�, HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ J C)Ilp / DD
YYYYMMDD

acmnalyticale
WM pecelabs aom
September 27, 2016
Mr. Jim Zieglmeier
3M Corporation
4191 Highway 87 South
Moncure, NC 27559
RE: Project: Outfall Sample
Pace Project No.: 92312954
NC(,b )03L-30
OCT 07 Nib
CENTRAL FILES
DWR SECTION
Paco Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr, Zieglmeier:
Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
a., qq .
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc: Mr. Stanley Carter, 3M Corporation
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page t of 15

` aceAnalytical o
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Pace A naiytical Services, Inc,
9800 Kincey Ave. Suite 100
Huntersville, 128078
[phone]
CERTIFICATIONS
Project: C utfall Sample
Pace Project No.. 92312954
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Ftorida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
Eden Certification Ili
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 2 of 15

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SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincay Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Outfall Sample
Pace Project No.: 92312954
Analytes
Lab ID Sample ID Method Analysts Reported laboratory
92312954001 O F-002A B C
92312954002 OF-003BCD
92312954003 OF-004ABC
92312954004 OF-005ABC
92312964005 OF-006BCDEF
SM 2130B
DWJ
1
PASI-E
SM 2540D
KCE
1
PASI-E
SM 254OF
DWJ
1
PASI-E
SM 2130B
DWJ
1
PASI-E
SM 25401)
KCE
1
PASI-E
SM 254OF
DWJ
1
PASI-E
SM 2130B
DWJ
1
PASI-E
SM 2540D
KCE
1
PASI-E
SM 254OF
DWJ
1
PASI-E
SM 2130B
DWJ
1
PASI-E
SM 2540D
DWJ
1
PASI-E
SM 254OF
DWJ
1
PASI-E
SM 2130B
DWJ
1
PASI-E
SM 2540D
DWJ
1
PASI-E
SM 254OF
DWJ
1
PASI-E
EPA 1664B
JMS
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 15

aceAnalytical®
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ANALYTICAL RESULTS
Project: Outfall Sample
Pace Project No.: 92312954
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
huntersville, NC 28078
[phone]
Sample: OF-002ABC
Lab tD: 92312964001 Collected: 09/19/16 11:20
Received:
09/20/16 11:35 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
21308 Turbidity EDN
Analytical Method: SM 2130B
Turbidity
13.6 NTU
0.50
1
09/21/16 08:31
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
21.0 mglL
2.5
1
09/21/16 09:30
264OF Total Settleable Solids
Analytical Method: SM 254OF
Total Settleable Solids
ND mLlUhr
0.10
1
09/21/16 08:30
Sample: OF-003BCD
Lab ID: 92312954002 Collected: 09/19/16 11:15
Received:
09120116 11:35 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
2130B Turbidity EDN
Analytical Method: SM 2130B
Turbidity
2.7 NTU
0,50
1
09121/1608:31
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
7A mg/L
2.6
1
09/21/16 09:30
254OF Total Settleable Solids
Analytical Method: SM 2540F
Total Settleable Solids
ND mUUhr
0.10
1
09/21/16 08:30
Sample: OF-004ABC
Lab ID: 92312954003 Collected: 09/19/16 10:30
Received:
09/20/16 11:35 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
2130E Turbidity EDN
Analytical Method: SM 2130B
Turbidity
4.4 NTU
0.50
1
09/21116 08:31
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
28.9 mg1L
4.0
1
09/21/16 09:31
2540E Total Settleable Solids
Analytical Method: SM 254OF
Total Settleable Solids
ND mUUhr
0.10
1
09/21/16 08:30
Sample: OF-005ABC Lab ID: 92312954004 Collected: 09/19/16 09:50 Received: 09/20/16 11:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual
2130E Turbidity EDN Analytical Method: SM 21306
Turbidity 2.1 NTU 0.50 1 09/21/1608:31
Date: 09127/2016 02:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„
Page 4 of 15

e
aceAnalytical
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ANALYTICAL RESULTS
Project: Outfall Sample
Pace Project No.: 92312954
Pace Analytical Services, Inc.
9800 Kincay Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OF-005ABC Lab ID: 92312954004 Collected: 09/19/16 09:50 Received: 09/20/16 11:35 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 4.3 mg1L 3.3 1 09/22116 09:24
254OF Total Settleable Solids Analytical Method: SM 254OF
Total Settleable Solids NO rt1L11.1hr 0.10 1 09/21/16 08:30
Sample: OF-006BCDEF Lab ID: 92312954005 Collected: 09119/16 11:00 Received: 09/20/16 11:35 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
2130E Turbidity EDN
Analytical Method: SM 2130E
Turbidity
3.3 NTU
0.50 1
09/21/16 08:31
2540D Total Suspended Sollds
Analytical Method: SM 25400
Total Suspended Solids
6.4 mglL
2.5 1
09122/16 09:24
264OF Total Settleable Solids
Analytical Method: SM 254OF
Total Settleable Solids
NO mLlLJhr
0.10 1
09/21/16 08:30
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mglL
5.0 1
09/27/16 08:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2016 02:34 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 15

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QUALITY CONTROL DATA
Project: Outfall Sample
Pace Project No.: 92312954
QC Batch: 329571 Analysis Method: SM 2130B
QC Batch Method: SM 2130B Analysis Description: 2130B Turbidity EDN
Associated Lab Samples: 92312954001, 92312954002, 92312954003, 92312954004, 92312954005
METHOD BLANK: 1826199 Matrix: Water
Associated Lab Samples: 92312954001, 92312954002, 92312954003, 92312954004, 92312954005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 0.50 09/21116 08:31
SAMPLE DUPLICATE: 1826200
92312954004 Dup
Parameter Units Result Result RPD Qualifiers
Turbidity NTU 2.1 2.1 0
Pace Analytical services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in NO,
Date: 09/27/2016 02:34 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 15

aceAnalytical
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QUALITY CONTROL DATA
Project: Outfali Sample
Pace Project No.: 92312954
QC Batch: 329568 Analysis Method: SM 25400
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92312954001, 92312954002, 92312954003
METHOD BLANK: 1826189 Matrix: Water
Associated Lab Samples: 92312954001, 92312954002, 92312954003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 09/21/16 09:21
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1826190
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 252 101 90-110
SAMPLE DUPLICATE: 1826191
92312787001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 131 113 15 D6
SAMPLE DUPLICATE: 1826192
92312945003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 141 146 3
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2016 02:34 PM without the wntten consent of Pace Analytical Services, Inc.. Page 7 of 15

aceAnalytical.
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QUALITY CONTROL DATA
Project: Outfall Sample
Pace Project No.: 92312954
QC Batch: 329790 Analysis Method: SM 2540D
QC Batch Method: SM 25400 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92312954004, 92312954005
METHOD BLANK: 1827361
Associated Lab Samples: 92312954004, 92312954005
Parameter
Units
Total Suspended Solids
mglL
LABORATORY CONTROL SAMPLE:
1827362
Parameter
Units
Total Suspended Solids
mg1L
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suiie 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 09/22/16 09:22
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 25B 103 90-110
SAMPLE DUPLICATE: 1827363
92312999002 Dup
Parameter Units Result Result
Total Suspended Solids mg1L 18.0 16.8
SAMPLE DUPLICATE: 1827364
92312975001 Dup
Parameter Units Result Result
Total Suspended Solids mg1L 162 131
RPD Qualifiers
7 D6
RPD Qualifiers
22 D6
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2016 02:34 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 15

aceAnalytical
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QUALITY CONTROL DATA
Project: Outfall Sample
Pace Project No.: 92312954
QC Batch: 329561 Analysis Method: SM 2540F
QC Batch Method: SM 254OF Analysis Description: 254OF Total Settable Solids
Associated Lab Samples: 92312954001, 92312954002, 92312954003, 92312954004, 92312954005
METHOD BLANK; 1826164 Matrix: Water
Associated Lab Samples: 92312954001, 92312954002, 92312954003, 92312954004, 92312954005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Settleable Solids mL/Llhr ND 0.10 09/21116 08:30
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the unite indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09127/2016 02:34 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 15

acmnalytrcal
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Project: Outfail Sample
Pace Project No.: 92312954
QC Batch: 330460
QC Batch Method: EPA 1664E
Associated lab Samples: 92312954005
METHOD BLANK: 1830841
Associated Lab Samples: 92312954005
Parameter
Total Petroleum Hydrocarbons
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 SGT-HEM, TPH
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg1L NO 5.0 09/27/16 07:50
LABORATORY CONTROL SAMPLE: 1830842
Spike LCS
Parameter Units Conc. Result
Total Petroleum Hydrocarbons mg1L 20 17.5
LCS % Rec
% Rec Limits
88 64-132
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvi e, NC 28078
(704)B75-9092
Qualifiers
MATRIX SPIKE SAMPLE: 1830843
92313011001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L ND 20 16.1 80 64-132
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09127/2016 02:34 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15

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QUALIFIERS
Project: Outfall Sample
Pace Project No.: 92312954
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute,
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
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Date: 09/27/2016 02:34 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 15

acmnalyticalo
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Outfall Sample
Pace Project No.: 92312954
I_ab ID Sample ID QC Batch Method QC Batch
92312954001
OF-002ABC
SM
2130B
329571
92312964002
OF-003BCD
SM
2130B
329571
92312954003
OF-004ABC
SM
2130B
329571
92312954004
OF-005ABC
SM
2130B
329571
92312964006
OF-006BCDEF
SM
2130B
329571
92312954001
OF-002ABC
SM
2540D
329568
92312954002
OF-003BCD
SM
2540D
329568
92312954003
OF-004ABC
SM
2540D
329568
92312964004
OF-006ABC
SM
2540D
329790
92312WO05
OF-006BCDEF
SM
2540D
329790
92312954001
OF-002ABC
SM
254OF
329561
92312964002
OF-003BCD
SM
2540F
329561
92312954003
OF-004ABC
SM
2540F
329561
92312964004
OF-005ABC
SM
2540F
329561
92312954005
OF-006BCDEF
SM
254OF
329561
Y��iY��_i�I�I�a1�C�I�I�7=i�3�lx �'L•�i[:I�: icI�L•�:Ir',
Date: 09/27/2016 02:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical Method
Analytical
Batch
Page 12 of 15

� mAnalytfca(
uur:umenc Name:
Document No,:
F-RAL-CS-001-Rev.04
Client Name:
WProject It:
Courier. DFed Ex UP5 USPS [-]Client
❑ Commercial ®Pace ❑Other: —
Document Revised: May 24, 2016
Page I of 2
Issuing Authority:
Pace Ralels;h Quality Office
w0# Page 2 of 2 for internal Use ONLY
�92312954
92312934
Custody Seal Present? Des ?o Seals Intact? []Yes f'' ONo
[ate/lnhfals Pesaart t?xamintng Gtntan4r/Vft' w/
[]Bubble Material: Bubble Wrap ❑Bubble Bags VNane ❑Other. 11
Thermometer. T1505 Type of ioe: ;iiat ❑elue ❑None ❑samples on ice, cooling processqNIA
begun
Correction Factor: 0.0'C Cooler Temp Corrected ('C): _ n, Biological Tissue Frozen? ❑Yes []No
Temp should be above fr ezing to 6'C
USDA Regulated Soil ( N/A, water sample)
Did sample rlginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Inter tlonaiiy,
[] Yes No lnctuding Hawall and Puerto Rico)? ❑Yes No
CommenVIDIscrepanty
Chain of Custody Present?
yes
❑No
N A
1.
Sample5 Arrived within Hold Time?
Yes
No
❑N/A
2.
Short Hold Time Ana sfs 02 hr.)?Etas
No
NIA
3,
Rush Turn Around Time Re uesled?
Yes
No
NIA
4,
Sufficient Volume?
IAY.s
01111
❑NIA
5.
Correct Containers Used?
es
[]No
[]N/A
6.
-Pace Containers Used?
(Cafes
No
N A
Containers Intact?
es
oNo
NIA
7.
Samples Field Filtered?
❑Yes
QNo
JdxJA
8. Note if sediment Is visible in the dissolved container
Sample Labels Match COC?
Yes
[]NO
ON/A
9.
-includes Date/Time ID/Analysis Matrix:
All containers needing add/base preservation have been
checked?
©Y
❑No
❑N/A
All containers needing preservation are Found to be In
xaPnx
compliance with EPA recommendation? ,
(/
esm.,kr
(HNO& HISOA, HCk2; NaOH >9 Sulfide, NaOH>12 Cyanide)
(]�es
❑No
❑NIA
N4(mp*u
inceptions: VOA, Collform, TOC, Gil and Grease,
DRO/801S (water) DO(-LLHg
es
ONo
N/A
""MJ`O"p1°'
Sam fes checked for dechlorination?
es
No
N/A
11.
Heads ace in VOA Vlals (>5-6mm)?
thy.
No
12,
Trip Blank Present?
❑Yes
©No13.
T
Trip Blank Custody Seals Present?
❑Yes
[]NO
Pace Trip Blank Lotp if purchased):
CUEW INOTIFICATIONIRE50LUnON
Person Contacted: Date/rime:
Comments/Sample
Discrepancy:
Field data Required? (]Yes ❑No
Project Manager SCURF Review: 4_ jf�]J,�� Date: p� b-1(0 T —
Project Manager 5RF Review: _ _ t'j r_�_ I _ _ _ Date"
Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form w1l be sent to the North Carolina DEHNR Cerdficatlon Clttice li.e.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Page 13 of 15

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Outfall Drainage Area and Flow 1 Rainfall Calculation Spreadsheet
E. Funk-12/0712010
Instructions:
Insert the rainfall amount into the "Rainfall (inches) column and the remainder of the values
will be cacluated. The output of 'Volume (MG)" is to be recorded on the DMR
Conversions
1 acre =
43,560 sqft
1 foot =
12 inches
1 cf =
7.48 gallons
Rainfall = 1.11 inches For rainfall on 09-19-2016
Outfall
Number
Drainage
Area (acre
Drainage
Area (sgft)
Rainfall
(inches)
Rainfall
(feet)
Volume
(cub. Feet)
Volume
(gallons)
Volume
(MG)
001
63.2
2,752,992
1.11
0.0925
254,652
1,904,795
1.905
002
41.8
1,820,808
1.11
0.0925
168,425
1,259,817
1.260
004'
7.9
344,124
1.11
0.0925
31,831
238.099
0.238
005
47.7
2,077,812
1.11
0.0925
192,198
1,437,638
1.438
006
1 1.81
78,4081
1.111
0,09251
7.253
54,250
0.054
008
1 46.512,025,5401
1.111
M9251
187,362
1,401,471
1.401
" Outfall 004 listed drainage area includes Outfall 003 drainage area as outfall 003 discharges into Outfall 004
Outfall 003 is for mine dewatering basin and flowmeters are used for reporting dischange on a quarterly basis
Outfall 007. is the instream outfall and is not calcuated due to the fact that water outside of the property flows past through this outfall