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Home My WebLink AboutWQ0036723_Residual Annual Report 2019_20200210Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submital an application?* r Yes r No Annual Report 2019 Year* Date Paper Copy 2/3/2020 Received:* Project Number* WQ0036723 Email Notifications ................................................................................................... Does this need O Yes review by the a No hydrogeologist? * Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by NJB Staff regarding electronic submittal, confirmation of receipt, and other issues. .................................................................................................................................................................................................................................................................................................................................................................................................... Name * Jamie Levis Email Address* jlevis@mooresvillenc.gov Project Information Submittal Type* f New Permit Application r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0036723 Applicant\Permittee * Town of Mooresville Phone Number* 704-662-8341To Facility Name * Rocky River Wastewater Treatment Facility r Modification (Major or Minor) r Additional Information r Other r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) CLASS A ANNUAL REPORT STATE. pdf 28.57MB Upload only 1 RJF document. Multiple documents rust be corrbined into one RJF file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contact the reviewer or Tessa Monday. If a paper application is required, be advised, applications accepted for pre -review until both the paper and electronic copies have been received. The paper copy shall include the following: o Application Form o All relevant attachments (caIcs, soils report, specs, etc,} o one full-size engineering plan set o One 11x17" engineering plan set 0 one extra set of specifications o Fee (if required} Mailine address: Division of Water Resources Division of Water Resources Non -Discharge Branch I Non -Discharge Branch ---- --- - --- - --- ------------ ------------------------------------i---------------------------------------------------------------------------- 1617 Mail -service Center Att: Nathaniel Thomburv, 9"' Floor, Office #942W ---- -NC �-- - -------------------------------------------- ------------------------------------------------ Raleih, 7699-1617 512 N. SaVisbury St For questions or problems contact Tessa Monday at tessa.monday@ncdenr.Qov or 919.707.3660. * W By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature C'��uFcc� �ct Submission Date 1/28/2020 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 Town of Mooresville FAX (704) 662-8473 NORTH CAROLINA POST OFFICE BOX 878 MOORESVILLE, NC 28115 Annual Class A Report, W'0036723 Rocky River Wastewater Treatment Facility Mooresville, N.C. 28115 Town of Mooresville NORTH CAROLINA NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 01/28/20 Subject: 2019 Annual Sludge Report, WQ0036723 Distribution of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone: 704-663-2840 2) Responsible official and facility contact — Larry Hendren, Bio-solids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone:704-799-4063 3) Class "A" dried biosolids were distributed under Town of Mooresville permit # WQ0036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2019 were transported to, Joe Hampton in Mt. Ulla, NC, Doug Carrigan in Mooresville, NC, Chad Swim in Mooresville, Rob Bailey in Mooresville, and Scott Goodman in Kannapolis. Total = 656.09 dry metric tons (See Attached Hauling Summary Sheets). Laboratory data from quarterly TCLP analyses have been included in this report. 5) (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: Larry Hendren, Bio-solids Coordinator Reviewed by: Jamie Levis, W WTP Plant Manaeer Signature 1 -Zg-ZO Date c !� Signature: ZZ p �ZO Date Town of Mooresville 2019 Hauling Summary Sheet DATE TONS TRANSPORTER DESTINATION COMMENTS 3/19/2019 47.8 Town of Mooresville Carrigan Farms- 8 Loads Mooresville 3/20/2019 45.5 Town of Mooresville Carrigan Farms- 7 Loads Mooresville 3/24/2019 21.5 Garin Klutz Farm Mt. Ulla 2 Loads 3/28/2019 15.0 Town of Mooresville Carrigan Farms- 3 Loads Mooresville 3/31/2019 10.4 Garin Klutz Farm Mt. Ulla 1 Load 4/17/2019 11.3 Town of Mooresville Carrigan Farms- 2 Loads Mooresville 4/29/2019 29.0 Town of Mooresville Carrigan Farms- 5 Loads Mooresville 4/30/2019 32.2 Town of Mooresville Carrigan arms- F 5 Loads Mooresville 5/8/2019 18.4 Town of Mooresville Carrigan Farms- 3 Loads Mooresville 5/16/2019 21.8 Town of Mooresville Carrigan Farms- 3 Loads Mooresville 6/20/2019 30.0 Town of Mooresville Carrigan Farms- 5 Loads Mooresville 6/24/2019 38.1 Town of Mooresville Carrigan Farms- 6 Loads Mooresville 6/26/2019 30.9 Town of Mooresville Carrigan Farms- 5 Loads Mooresville 7/3/2019 19.8 Town of Mooresville Carrigan Farms- 3 Loads Mooresville 7/10/2019 28.6 Town of Mooresville Carrigan Farms- 5 Loads Mooresville 7/11/2019 17.9 Town of Mooresville Carrigan Farms- 3 Loads Mooresville 7/15/2019 13.7 Town of Mooresville Carrigan Farms- 2 Loads Mooresville 7/22/2019 28.7 Town of Mooresville Carrigan Farms- 5 Loads Mooresville 8/14/2019 5.7 Chad Swim Mooresville 2 Loads 8/19/2019 24.4 Town of Mooresville AFH Farm 4 Loads Mooresville 8/20/2019 6.1 Town of Mooresville AFH Farm 1 Load Mooresville 8/26/2019 19.1 Town of Mooresville Carrigan Farms- 3 Loads Mooresville 9/4/2019 19.7 Town of Mooresville AFH Farm3 Loads Mooresville 9/4/2019 12.4 Town of Mooresville Carrigan Farms- 2 Loads Mooresville 9/10/2019 19.9 Town of Mooresville Carrigan Farms- 3 Loads Mooresville 9/10/2019 5.7 Town of Mooresville AFH Farm 1 Load Mooresville 9/18/2019 12.6 Town of Mooresville Carrigan Farms- 2 Loads Mooresville 9/18/2019 12.8 Town of Mooresville AFH Farm 2 Loads Mooresville 9/25/2019 6.8 Town of Mooresville Carrigan Farms- 1 Load Mooresville 9/25/2019 6.7 Town of Mooresville AFH Farm 1 Load Mooresville 9/26/2019 6.8 Town of Mooresville Carrigan Farms- 1 Load Mooresville 10/1/2019 4.2 Chad Swim Mooresville 1 Load 10/9/2019 6.4 Town of Mooresville AFH Farm 1 Load Mooresville 10/9/2019 6.7 Town of Mooresville Carrigan Farms- 1 Load Mooresville 10/15/2019 12.1 Town of Mooresville Carrigan Farms- 2 Loads Mooresville 10/15/2019 17.4 Town of Mooresville AFH Farm 3 Loads Mooresville 10/24/2019 12.0 Town of Mooresville Carrigan Farms- 2 Loads Mooresville 10/28/2019 23.3 Town of Mooresville Carrigan Farms- 4 Loads Mooresville 11/19/2019 17.9 Town of Mooresville Carrigan Farms- 3 Loads Mooresville 11/20/2019 21.7 Town of Mooresville Carrigan Farms- 4 Loads Mooresville 12/12/2019 11.8 Melton Hauling Scott Goodman 2 Loads Kannapolis Total tons 752.80 Avg. %solids 0.96 Drytons 723.21 Conversion factor 0.907184 Metric tons 682.93 Dry metric tons 656.09 Calculation: Dry metric tons= total tons * avg.%solids* conversion factor NC Certification No. 402 Case Narrative PR I S M Full -Service Analytical & NC Drinking Water Cart No. 3773502/28/2019 Environmental Solutions SC Certification No. 99012A9 WOME$ WG Town of Mooresville/RR WWWTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 02/11/2019 Prism Work Order. 9020168 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Analysis note for SAR: SAR =[Na]/SORT {([Ca]+[Mg])/2} SAR = [ 79.5/23 ] / SORT { ( [142/20] + [87.5/12.2]) / 2 } Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate —Nitrite PAN = 0.3 * (21000 — 1400) + 0.5 * (1400) + 8.7 PAN = 6700 Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Terri W. Cole Project Manager Reviewed By Terri W. Cole Project Manager This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1.900/529-6364- Fax: 7WS26-0409 Page 1 of 15 Data Qualifiers Key Reference BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB. SE Surrogate recovery outside the QC limits due to emulsion. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.D. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041629.6364-Toll Free Number: 1-800/529-6364-Fax: 704162"409 Page 2 of 1 1 ISM A Full -Service Analytical a % ' V' Environmental Solutions uww.ros,ea,xc Sample Receipt Summary 02/28/2019 Prism Work Order: 9020168 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received Class 9020168-01 Solid 02/11/19 7:03 02/11/19 13:30 Samples were received in good condition at 3.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 apringbrook Road -P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364-Toll Free Number: 1-800/62M364 - Fax: 7041628-0409 Page 3 0f 15 /' P R ISM I Full -Service Analytical Solutions Environmental tical& ,.eox�.oAies,xc Town of Mooresville/RR W W'rP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 0212812019 Client Sample ID: Class A Prism Sample ID: 9020168-01 Prism Work Order: 9020168 Time Collected: 02/11/19 07:03 Time Submitted: 02/11/19 13:30 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst DaterPme Batch ID General Chemistry Parameters Plant Available Nitrogen 6700 mg/kg dry 1600 460 10 "Calculation 2MS/19 11:63 CLB [CALL] % Solids 96.8 % by 0.100 0.100 1 `SM2540 G 2121/19 9:90 KBS P9130364 Weight Ammonia as N 1400 mg/kg dry 9.7 2A 1 'SM4600-NH3 C 2114119 16:31 ISMS PSB0236 Nitrate/Nitrde as N 8.7 mg/kg dry 5.2 1.4 1 `SM4600-NO3 F 2115119 11:63 CLB PSB0262 pH 6.3 pH Units 1 "9046D 2/16/19 17:00 CBM PSB0328 Phosphorus -Total 12000 mglkg dry 260 68 100 'SM4500-P F 2/21/19 8:29 CLB PSB0298 Total Meldahl Nitrogen 21000 mg/kg dry 6200 1600 10 •361.2 2113/19 9:06 CLB PSB0196 Microbiological Parameters Fecal Coliforms BRL MPN/g dry 0.2 1 `SM9221 E 2/11119 13:39 BMS P9B0205 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 `1311 2/13/19 7:20 MMR P9130208 TCLP Extraction Complete N/A 1 *1311 ZHE 2119119 9:50 TBL P9130322 TCLP Metals Mercury BRL mg/L 0.010 0.000030 1 '7470A 2113/19 13:44 MMR P9BD213 Arsenic BRL mg/L 0.10 0.016 1 '6010D 2/13/19 15:14 JAB P9130217 Barium BRL mg/L 5.1) 0.0040 1 `6010D 2113/19 15:14 JAB P9130217 Cadmium BRL mg/L 0.025 0.D0075 1 '6010D 2113119 1514 JAB PDB0217 Chromium BRL mg/L 0.25 0.0018 1 '6010D 2/13119 15:14 JAB PSB0217 Lead BRL mg/L 0.060 0.0040 1 '6010D 2113/19 15:14 JAB P980217 Selenium BRL mg/L 0.10 0.028 1 '6010D 2/13/19 15:14 JAB P9130217 Silver BRL mg/L 0.25 0.0020 1 `6010D 2113119 15:14 JAB P9130217 TCLP Organochlorine Pesticides by GC/ECD Chlordane BRL mg/L 0.0025 0.00086 1 '8081B 2/21/19 21:09 ZRC P980295 Dieldrin BRL mg/L 0.00050 0.000070 1 '8081B 2/21/19 21:09 ZRC P980295 Endrin BRL mg/L 0.00050 0.000075 1 '8081B 2121/19 21:09 ZRC POB0295 gamma-BHC BRL mg/L 0.00050 0.000065 1 '8081B 2121119 21:09 ZRC P9130295 Heptachlor BRL mg/L 0.00050 0.000085 1 `8081B 2/21119 21:09 ZRC P9130295 Heptachlor Epoxide BRL mg/L 0.00050 0.000065 1 *8081B 2/21119 21:09 ZRC P980295 Methoxychlor BRL mg/L 0.00050 0.00020 1 '8081B 2/21/19 21:09 ZRC P9130295 Toxaphene BRL mg/L 0.025 0.00037 1 '8081B 2/21119 21:09 ZRC P9130295 Surrogate Recovery Control Limits Decachloroblphenyl 15 % 13-186 Tetrachloro-m-xylene 14 % 40-134 SE TCLP Semivolatile Organic Compounds by GC/MS 2,4,5-Tdchlorophenol BRL mg/L 0.25 0.0016 1 '8270D 2113/19 20:58 JMV PGB0223 2,4,6-Tdchlorophenol BRL mg/L 0.10 0.0018 1 '8270D 2/13/19 20:58 JMV P9130223 2,4-Dinftrotoluene BRL mg/L 0.050 0.0014 1 '8270D 2113119 20:58 JMV P980223 2-Methylphenol BRL mg/L 0.050 0.0018 1 '8270D 2/13119 20:58 JMV P9130223 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041629.6364-Toll Free Number: 1.800/629.6364-Fax: 7041625-0409 Page4of 15 Laboratory Report &GAIR GSM I Full-6erviceAnalytical a Environmental Solutions uMa GR,s;,Ne 02128/2019 Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Prism Sample ID: 9020168-01 P. 0. Box 878 Prism Work Order: 9020168 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 02/11/19 07:03 Time Submitted: 02/11/19 13:30 Parameter Result units Report MOIL Limit Dilution Factor Method Analysis Date/Time Analyst Batch ID 3/4-Methylphenol BRL mg/L 0.050 0.0015 1 '8270D 2/13/19 20:58 JMV P9130223 Hexachlorobenzens BRL mg/L 0.050 0.0013 1 '8270D 2/13/19 20:58 JMV P9B0223 Hexachlorobutadiene BRL mg/L 0.050 0.0021 1 '827013 2/13119 20:58 JMV P960223 Hexachloroemane BRL mg/L 0.050 0.0017 1 '8270D 2/13119 20:58 JMV P9130223 Nitrobenzene BRL mg/L 0.050 0.0026 1 '8270D 2113/19 20:58 JMV P9B0223 Pentachlorophenol BRL mg/L 0.25 0.0012 1 '8270D 2/13119 20:58 JMV P9130223 Pyndine BRL mg/L 0.25 0.0010 1 '8270D 2/13/19 20:58 JMV P960223 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 20 % 43-140 SE 2-Fluorobiphenyl 20 % 44-119 SE 2-Fluorophenol 24 % 19-119 Nitrobenzene-05 19 % 44-120 SE Phenol-d5 19 % 11-52 Terphenyl-d14 22 % 50-134 SE TCLP Volatile Organic Compounds by GUMS 1,1-Dichioroethylene BRL mg/L 0.035 0.00083 1 '8260B 2/19/19 20:45 KDM P960356 1,2-Dichloroethane BRL mg/L 0.025 0.00066 1 '82608 2/19119 20:45 KDM P9130356 14-Dichlorobenzene BRL mg/L 0.38 0.00050 1 '8260B 2119/19 20:45 KDM P9130356 Benzene BRL mg/L 0.025 0.00048 1 '8260B 2119119 20:45 KDM P9130356 Carbon Tetrachloride BRL mg/L 0.025 0.0011 1 '8260B 2119/19 20:45 KDM P9130356 Chlorobenzene BRL mg/L 5.0 0.00062 1 '8260B 2119/19 20:45 KDM P9150356 Carbon disuMde BRL mg/L 0.050 0.00075 1 "82608 2/19119 20:45 KDM P980356 Chloroform BRL mg/L 0.30 0.00076 1 '8260B 2119119 20:45 KDM P9130356 Methyl Ethyl Ketone (2-Butanons) BRL mg/L 10 0.0024 1 '8260B 2/19/19 20.45 KDM P9B0356 Tetrachloroethylene BRL mg/L 0.035 0.00098 1 '8260B 2/19/19 20:45 KDM P9130356 Trichloroethylene BRL mg/L 0.025 0.00078 1 '8260B 2119119 20:45 KDM P980356 Vinyl chloride BRL mg/L 0.020 0.00097 1 '82608 2119119 20:45 KDM P9B0356 Surrogate Recovery Control Limits 4-Bromofluorobenzene 92 % 80-124 Dibromolluoromethane 85 % 75-129 Toluene-d8 98 % 77-123 Total Metals Aluminum 9600 mg/kg dry 5.2 0.76 1 -0010D 2118119 16:40 JAB P9130293 Mercury 0.22 mg/kg dry 0.062 0.0059 3 '74718 2121119 15:11 MMR P960366 SAR Soil Preparation Complete 9 1 '2-78-054 2119/19 8:50 MMR P9B0294 SAR Percent Moisture 88.4 % by 0.100 0.100 1 '2-78-064 2120/19 9:00 MMR P9B0321 Weight Arsenic 1.6 mg/kg dry 1.0 0.063 2 `6010D 2/20119 21:28 JAB PSB0293 Sodium Absorption Ratio 1.3 [blank) 0.30 0.016 1 `2.78-054 2120119 22:21 JAB PSB0320 Cadmium 0.30 mg/kg dry 0.26 0.0069 1 •6010D 2118119 16:40 JAB PSB0293 Calcium 8900 mg/kg dry 10 0.24 1 '6010D 2/18/19 16:40 JAB PSB0293 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543 Phone: 7041629.6364-Toll Free Number..l-800/629.6364-Fax: 7041626-0409 Page 5 of 15 Laboratory Report I Fulbserviea s /PRISM ,.ao,aarawiez we Environmental Solutions al Solutions 02/28/2019 Town of Mooresville/RR VWUTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Prism Sample ID: 9020168-01 P. O. Box 878 Prism Work Order: 9020168 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 02/11/19 07:03 Time Submitted: 02/11/19 13:30 Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch Limit Factor DateRme ID Calcium, BAR 140 ni 6.0 0.60 60 '6010D 2/20/19 22:21 JAB P9B0320 Copper 120 mglkg dry 0.52 0.047 1 '6010D 2118119 16:40 JAB P980293 Lead 6.6 mg/kg dry 0.26 0.048 1 '6010D 2118119 16:40 JAB P9B0293 Magnesium 2100 mg/kg dry 2.6 0.24 1 '60101) 2118/19 16:40 JAB PSB0293 Magnesium, BAR 88 mg/L 6.0 0.43 50 •6010D 2120/19 22:21 JAB P9B0320 Molybdenum 8.4 mglkg dry 0.62 0.016 1 •6010D 2/18/19 16:40 JAB P9B0293 Nickel 7.3 mg/kg dry 0.62 0.019 1 '6010D 2118119 16:40 JAB P980293 Potailstum 2900 Sit mg/kg dry 13 0.46 1 '6010D 2/18/19 16:40 JAB P980293 Selenium 2.2 mill dry 0.62 0.12 1 '6010D 2118119 18:40 JAB P980293 Sodium 760 mg1kg dry 31 1.0 2 '6010D 2120119 21:28 JAB P9B0293 Sodium, BAR 80 mg/L 25 0.90 50 '6010D 2120119 22:21 JAB P9190320 Zinc 280 mg/kg dry 26 0.92 10 '6010D 2119/19 17:06 JAB P980293 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road -P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 7041629-6364- Toil Free Number: 1-800/629-6364 - Fax: 704/625-0409 Page 6 of 15 Sample Extraction Data Prep Method: 351.2 Lab Number Batch Initial Final Date/Time 9020168-01 P9B0195 0.05 g 25 mL 02/12/19 12:00 Prep Method: SM4600-NH3 B Lab Number Batch Initial Final Date/Time 9020168-01 P9130236 1.07 g 50 mL 02/14/19 9:06 Prep Method: SM4600-PBS Lab Number Batch Initial Final Date/Time 9020168-01 POB0298 1 g 50 mL 02/18/19 10:39 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 9020168-01 P980208 100 9 2000 mL 02/12/19 14:50 9020168-01 P9130322 12.5 g 250 mL 02/18/19 15:45 Prep Method: 3010A Lab Number Batch Initial Final Datemime 9020168-01 P9B0217 10 mL 50 mL 02/13/19 9:20 Prep Method: 7470A Lab Number Batch Initial Final Datamime 9020168-01 P9B0213 20 mL 30 mL 02/13119 8:40 Prep Method: 3510C GC Lab Number Batch Initial Final DataRme 9020168-01 P9B0295 200 mL 10 mL 02/18/19 9:20 Prep Method: 3610C MS Lab Number Batch Initial Final Date/rime 9020168-01 P9130223 200 mL 1 mL 02/13/19 11:52 Prep Method: 5030B Lab Number Batch Initial Final Date/Time 9020168-01 P9130356 1 mL 10 mL 02/19/19 12:13 Prep Method: 3010A Lab Number Batch Initial Final Datemime 9020168-01 P9130320 50 mL 50 mL 02/19/19 8:50 9020168-01 P9130320 50 mL 50 mL 02/19/19 8:50 Prep Method: 3050B Lab Number Batch Initial Final Date/Time 9020168-01 P9B0293 2 g 50 mL 02/18/19 8:20 9020168-01 P9B0293 2 g 50 mL 02/18/19 8:20 9020168-01 P9B0293 2 g 50 mL 02/18/19 8:2D 9020168-01 P9BD293 2 g 50 mL 02/18/19 8:20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number..1-800/629-6364- Fax: 704/625.0409 Page 7 of 15 Sample Extraction Data Prep Method: 7471E Lab Number Batch Initial Final Date/Time 9020168-01 P9B0366 0.6 g 50 mL 02/21/19 9:10 Prep Method: SAR 2-78-064 Lab Number Batch Initial Final DateTime 9020168-01 PSB0294 250 g 250 g 02/18/19 8:20 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 902016"1 Herbicides TCLP (Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629.6364-Tall Free Number l-8001529-6364-Fax: 7041626-MB Page 8 of 15 PRISM I Full -Service Analytical ,y Environmental Solutions ..WQR1ES ING 449 Springbrook Road • Charlotte, NC 2821T Phone 7041529-6364 • Fax: 704/525-0409 Client Company Name: D ih&"� �It.. Report To/Contact Name: tA. W— Reporting Address: D C 9 0 OlCbyt 4 , MC, ills - CHAIN OF CUSTODY RECORD PAGE OF -2-- QUOTE a TO ENSURE PROPER BILLING: Project Name: _l a" _ Pr (()t 1 eA 's Short HOW Analysis: `tes (NO) UST ProjecN es) 10 'Please ATTACH any pro et specific reporting (QC LEV I I III IV) provisions and/or OC Requiremen�tsA Invoice To: OWA _ /vlaonelN)ly— Address: YES NO NIP M Samples INTACT upon arrival? _ Received ON WET ICE? O PROPER PRESERVATIVES indicated? "- — co ReCOlved WITHIN HOLDING TIMES?al r CUSTODY SEALS INTACT? n- VOLATILES reed W/OUT HEADSPACE? _ PROPER CONTAINERS used? s TEMP: Therm ID: 'r - r Observed: 2 -'IoC / Con: 2.r-, °C rn.,Iw;q Tl ax(Tes)jNoi: Email Address- tAXAW1 Purchase Order No./Billing Reference (btQYYUatf'tdM It. nc.. oV ❑ a Days ❑ 5 Days a4— Requested rue Date 13 1 Day ❑ 2 rays ❑ a Days day, EDD Type: PDF_Excel_Other "Working Days" ❑ 6-9 Days>a'Standam 10 days ❑Rush Work Must Be Site Location Name: Pre -Approved Samples received after 14:00 will be processed next business day. Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS a CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Certification: NELAC DoD_ FL— NC — SC_ OTHER N/A Water Chlorinated: YES NO1_ Sample Iced Upon Collection: YES_NO_ CLIENT SAMPLE DESCRIPTION DATE COLLECTED _ TIME MATRIX COLLECTED (SOIL, MILITARY ! WATER OR HOURS '�, SLUDGE) SAMPLE CONTAINER i PRESERVA- I TIYES pN�p}LVSISREQUESTED V J, •\� REMARKS - p ,^�. O�j y�' V •N RISM ID NO. �.___ `tYPE SEE BELOW NO' 8WE a�sPr a-11-19 I,;o3 "sD11 -- C o� � I I I i I " ' 1 Sampled By (P12.4 .. .- Sampler's Signature `�`-+-.�..(Print Name) L.Af� �4ncQ I Affiliation TtAA.0 Upon relinquishing, this Chain oftustody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charg for any changes after analyses have been Inrdj d. 1 '( enalure Rem By 19ealom) Im aws 2 t S Additional Comm/ants: SBeArtival Time: Relinquisneo ey:( re) N By: Iemnxe) 71�1 Vol /stMt Site Departure Time: Iingata ay: pnaluroL_ Remived PorPdsm Laborelad y �I Dy rv, llln Field Tech Fee: Z l /� ` : a73D- D ��fr;C� OS Mileage: Ipmarrc NOTE: A SAMPLE COO SH LO eE T PEO SHUT WITH CUSTOO SEALB FOR NSPOR ATION TO LABORATORY. C C G up Na. O �i.p SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVEOAT ELABORATOR". O Fed E< O UPS O Hrx4divered aelPriam Raid Servim ❑ Other 0 ��201b^ ❑ NC El SC Cl NC ❑ SC ❑ NCU ❑ SCTER: O NC 1❑l SCNC ❑ SC WASTE: ❑ NC O SC ❑ANC ❑ SC ❑ NC LANDFILL SC ❑ NC ❑ SC - ' ' •' -CVKIAINtKITPt:CVVES: A=Amber C=Clear G=Glass P=Plastic, TL=Teflon-tined Cap VOA= Volatile Organics Analysis (Zero Head Space) ORIGINAL Vr V1J51VUT Kt%iVKD i LAB USE ONLY YES NO NIAr Full -Service Analytical 8 PRISM�nwiin Environmental Solutions PAGE P-OF QUOTE a To rNSUR ROPER BILLING. .� 1 ORATORIES INC /] tI�� QSS R' R tgr S�tt ryl.pc. Samples INTACT upon arrival? / _ Project Name: li� 449 Springbrook Road • Charlotte, NC 28217 1 Received ON WET ICE? •G O Phone 7041529.6364 • Fax: 7041525-0409 Short Hold Analysis: as (NO) UST PrOJect: (Yes) So PROPER PRESERVATIVES indicated? .G Client Company Name: I ONM. 7�('psu�� `Please ATTACH any pro specific reporting (QC LEVEEel III IV) Received WITHIN HOLDING TIMES? ` m provisions and/or QC Requirements Report To/Contact Name: 1MfaC- CUSTODY SEALS INTACT? m -- -- d Invoice To: 'iatw. or- /Xno0PBh11�! VOLATILES reed WIOUT HEADSPACE7 Reporting Address:P.1bab.i. Moo vffiA 11 I - 2.3 Address: _ PROPER CONTAINERS used? _ _ TEMP: Therm iD: /4- / Observed: II �—°C / Con:.-0 IC: Phone:'{--Idab-3286 Fax (Yes) (No): Purchase Order No./Billing Reference Emall Address: 110ra etx4 1111`4000A4IN oil TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Requested Due Date ❑ El 1 Day 2 Days ❑ 3 Days Q 4 Days 5 Days EDD Type: PDF ✓ ExCei—Other Certification: NELAC— DoD— FL_ NC_ "Working Days" ❑ 6-9 Day�Standard 10 days ❑ Rush Mdust Be Site Location Name: Samples received after 14:00 will be processed next business day. SC OTHER NIA Site Location Physical Address: Turnaround time Is based on business days, excluding weekends and holidays. Water Chlorinated: YES NO (SEE REVERSEREGALISERVICES RENDEREDBY PRISM U190RATORIES, CONDITIONS . TO CLIENT) Sample Iced Upon Collection: YES_ NO TIME MATRIX SAMPLE CONTAINER I ANALYSIS REQUESTED PRISM CLIENT SAMPLE DESCRIPTION DATE COLLECTED COLLECTED MILITARY HOURS (SOIL, WATER OR SLUDGE)• PRESERVA• ` TNES -Mae �.r REMARKS ` 1 �:' sTj� d �` . �J_ ;4 air LAB ID NO. d� SE BELOW Cr NO. I SIZE i Sampler's Signature Sampled BY (Print Name) l.,4=NcrAffiliation Two. .. .• Upon relinquishing, this Chain of Custody is your authorization for Priam to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. Re q e Sgw ) Race" ignawre 2 MAE oursrAdftonal Comments: She Arrival Time: Rehn9uis a By: i9 Wre) d By: (Signature) ei . v"'u �(� Site Departure Time: ,� Reltn IGI ay' iSignmu@J Racevsd Fr Prism Labors pare Ul""'��Fieltl Teth Fea: J3.3c�a,tNA) ;�UL=BETAO Mileage: Shipment SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED ATTE: ALL SAMPLE COOLER a. E LABORATORY. N TO LABORATORY, /'�` +•� ��i ) () O Fad E. ❑ UPS ❑ Handdelivered dam Feld Service O Oth y vy/ Ar) NPDES: UST. GROUNDWATER: DRINKING WATER: j.391-ID E. RCRA:❑ N P❑ ❑NCOSC ❑NC ❑SC ❑NC ❑SC ❑NC El SIC O SC NC ❑ SC ❑ANC ❑ SC ❑ SC ❑ NC O SC "CONTAINER TYPE CODES: A=Amber C=Clear G=Glass P=Plastic; TL=Teflon-tined Cap VOA= Volatile Organics Analysis (Zero Head Space) GRiull l 0 ACCESS ANALYTICAL, INC. ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W. Cole PROJECT ID 9020168 LABORATORY REPORT NUMBER 19021308 DATE February 18, 2019 Primary Data Review By Secondary Data Review By Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick@axs-inc.com PLEASE NOTE: Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory 8 98016, NCDENR certified lab # 562, GA certified lab 8 FL-E87582, NELAP certified laboratory # E87582 - AIHA-LAP,LLC Laboratory IDA 00671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. - Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative oFAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your loco] Access Analytical representative at 803.781.4243 or toll fee at 893.315 4243 Page rPage 11 of 15 P R I S I V 1 I Fun -Service Analytical 6 j�{�_ Environmental Solutions -_:... _ �nuoruomciacc i �02&r6 SUBCONTRACT ORDER Cerlfflc=lot • NiLAC US'ACE _ Prism Laboratories, Inc. NCSC_ Other 9020168 N/A_ SENDING LABORATORY: RECEIVING LABORATORY: Prism Laboratories, Inc. Analytical Environmental Services, Inc. P. O. Box 240543 3080 Presidential Parkway Charlotte, NC 28224-0543 Atlanta, GA30340 Phone: 800-529.6364 Phone :(770) 457-8177 Fax: 704-525-0409 Fax: NA Project Manager,. Terri W. Cole Analysis Doe Expires Laboratory ID Comments Sample 1D: 9020168-01 Solid Sampled:02l13119 07:03 C l A s' f ' Herbicides TCLP (Sub) 02118A 9 07:03 UNM �4d x umc 2-13-1q lt�-01 Released By Datc Rcccived By Date Rcleasal By Date Reccivxi By Datc Page 1 of I Page Page 12 of 15 Analytical Environmental Services, Inc Date: IB-Feb-I9 Client: Prism Laboratories Client Sample 1D: CLASS A Lab Order 1902B08 Tag Number: 902016M1 Project Name: 9020168 Collection Date: 2/11/2019 7:03:00 AM Lab ID: 190211108-001A Matrix: Solid Analyses Result Reporting y Qual MDL Limit Units BatchlD DF Date Analyzed Analyst HERBICH)ES,TCLP SW1311/8151A 2,4,5-TP (Silvex) BRL 2,4-D BRL Surr: DCAA 62.9 Qmlinnr. • Vatua esceeds ntasnnum eoaaan.aal level BRL Not Dawvd at MDL H Holding Liam rorpmpamtioa or analysis exceeded N Mwlpenn NELAC certified D Aaalym detmad is the..attmd m hhpd blank (SW3510C) 0030 020 ing/L 274527 1 02/15/201917:35 HB 0.051 020 mg& 274527 1 0211520191735 HB 0 494-120 %REC 274527 1 02/15201917:35 HB E at, mued wlueabace gaanmaa... mngd S Sptke Recmcry Laxidc lnnns due to mains > Gmawr ihm Remh vnitrc r Esmnated wine &.e td Imlaw Ra,,m, Limn Lev than R,,att ca-ue Page Page 13 of 15 IAxata-rtent. gRtaNStRNMAL AES .StOB'IC3ffi.Ivr. 1. Client Name: Access Analytical, Inc. 2, Carrier: FedEv C UPS ❑ USPS ❑ Client[—] Courier❑ 3. 4, 5. 6. 7. 8. 9. 10. 31. 12. SAMPLE/COOLER RECEIPT CHECKLIST AES Work Order Number: 1902BOS vne Nn Mra Clear Save as Shipping container/cooler received in good condition? • damaged ❑ leaking ❑ other❑ Custody seals present on shipping container? Custody seals intact on shipping container? # # Temperature blanks present? Cooler temperature(s) within limits of G-VC? [See item 13 and 14 for temperature recordings.] O O O Cooling initiated for recently collected samples / ice present ❑ Chain of Custody (CDC) present? Chain of Custody signed,dated, and timed when relinquished and received? Sampler name and/or signature on CDC? Were all samples received within holding time? TAT marked on the CDC? • If no TAT indicated, pmceeded with standard TAT per Terms & Conditions. 13, Cooler 1 Temperature d0 oC Cooler 2 Temperature 14. Cooler 5 Temperature °C Cooler 6 Temperature 15 Comments: 16. 17 18. 19. 20. 21 22 23. 24. 25. 26. oC Cooler371emperature °C Cooler 4 Temperature °C °C Cooler71emperature °C Cooler 8 Temperature °C I certify that I have completed sections 1-15 (dated initials). AP 2/13119 Y.e Mn N/a nrdle Were sample containers intact upon receipt? ......_...- Custody seals present on sample containers? Custody seals Intact on sample containers? Do sample container labels match the CDC? O Incomplete Info Illegible no label ❑ other ❑ Are analyses requested indicated on the CDC? Were all of the samples listed on the CDC received? ®• Q © samples received but not listed on CDC samples listed on CDC not received n a Was the sample collection date/time noted? Did we receive sufficient sample volume for indicated analyses? Were samples received in appropriate containers? Were VOA samples received without headspace, (< 1/4" bubble)? Were trip blanks submitted? • listed on CDC not isted on COC❑ 27. Comments: This sacgon only applies to samples where PH can be charked at Ramnle RanoiM I certify that I have completed sections 16-27 (dated initials). HB 2/13/2019 --_-- ---- -- -- yes No N/A Details Comments 28. Have containers needing chemical preservation been checked? 29. Containers meet preservation guidelines? u? N 30. LMS pH adjusted at Sample Receipt? m ' Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCS and Oil & Greasa/IPH. A I certlfy Mat I have completed sections 28,30 (dated Initials). Checklist 6.9.17 Rev 2 Lacked kn HB 2/13/2019 Page 4 of 5 Analytical Environmental Services, Inc Client: Prism Laboratories Project Name: 9020168 Workorder, 1902B08 Date: 18-Feb-19 ANALYTICAL QC SUMMARY REPORT BatchlD: 274527 Sample ID: NIB-274527 Client ID: Units: mg/L Prep Dale: 02/15M19 Run No: 391204 SampleType: MBLK TestCode; HEkWCmE&TCLP SWI311/9151A BetchlD: 274527 Analysis Date: 02/1547019 Seq No: 8754609 Analyte Result RPT Limit SPK value SPK Re£Val %REC Low Limit High Limit RPD, Ref Val %RPD RPD Limit Qual 2.4,5-TP(Silvex) BRL 0.20 ? 4-D BRL 0.20 Sum: DCAA 0,3190 0 0.5000 63.8 49.4 120 Sample ID: LCS-274527 Client ID, Units: mg/L Prep Date: OV15/2019 Run No: 391204 SampleType: LCS TestCode: HERmCIDE&TCLP SWI31119151A Batch1D: 274527 Analysis Date: 02/15/2019 Seq No: 8754610 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 4,0-1 P (Sdvex) 03618 0.20 0.5000 72.4 49 120 2.4-D 03924 0.20 0.5000 76.5 509 120 Sum: DCAA 0 3595 0 0.5000 719 494 120 Sample ID: 1902862-002BhIS Client ID: Units: mg/L Prep Date: 02/15/2019 Run No: 391204 SampleType: MS TestCode: HERBICIDE&TCLP SW1311/d151A BatchID: 274527 Analysis Date: 02/15/2019 Seq No: 87546I3 Analyte Result RPT Limit SPK value SPK RefVal %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2A.5-TP(Silvex) 03537 020 0.5000 70.7 48.2 120 2.4-D 03570 0.20 0.5000 714 45 130 Surr: DCAA 03639 0 0.5000 728 49.4 120 p Quelirmrst > �Iorµan Result value < bees µan Result value B Andymd.tedodinl6emouaNdme"Wouk � BRL aelow rtponmg bmn E Evimmed (vilut above qumdmlian route) H HeI&n g nmexfw mepvmtim or analysis exeeWW (r I W.'W value daeard bclnv. R<poning Limit N Amym lnot NEWCcenified R RPD ovtcdelimits duo romeMx Rm Um ReWning Llniil S Spikn Retovmy outside limits due ro m x N Page 5 of 6 NC Certification No. 402 Case Narrative P R I S M Full -Service Analytical & NC Drinking Water Cent No, 37735 5/8/19 16:29 Environmental Solutions SC Certification No. 99012 I BORATOR Town of Mooresville/RR WAVTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 04/22/2019 Prism Work Order: 9040345 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Analysis note for SAR: SAR =[Na]/SQRT{([Ca]+[Mg])/2} SAR = [ 100/23 ] ! SORT { ( [240/201 + [150/12.2]) ! 2 ) SAR = 1.3 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate —Nitrite PAN = 0.3 * (25000 — 1900) + 0.5 * (1900) + 2.6 PAN = 7900 mg/kg Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 aprin9brook Road -P.O. Box 240543 - Charlotte, NC 28224.OW Phone: 704/629.6364-Toll Free Number: 1.800/629-6364 - Fax: 7041626-0409 Page 1 of 15 Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. WWM�4MWWJ Terri W. Cole Project Manager Data Qualifiers Key Reference DM Sample diluted and RL increased due to the matrix. SE Surrogate recovery outside the QC limits due to emulsion. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Reviewed By Terri W. Cole Project Manager Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in Its entirety, without the written consent of prism Laboratories, Inc. 449 Spring brook Road -P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 704/629-6364-Toll Free Number.1-800/52gE364- Fax: 704/625.0409 Page 2 of 15 LAIRUR I S M I Full -Service Analytical Environmental Solutions aacW.m.,sa$xe Sample Receipt Summary 05/08/2019 Prism Work Order: 9040345 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received Class A 9040345-01 Solid 04/22/19 8:42 04/22/19 11:33 Samples were received in good condition at 3.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: l-8001529.6364-Fax: 704/526-0409 Page 3 of 15 PRISM I Fun -Service Analytical 9 Environmental Solutions ueonnroaiEg,xc Town of Mooresville/RR WWTP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 05/08/2019 Client Sample ID: Class A Prism Sample ID: 9040345-01 Prism Work Order: 9040345 Time Collected: 04/22/19 08:42 Time Submitted: 04/22/19 11:33 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID General Chemistry Parameters Plant Available Nitrogen 7900 mg/kg dry 70 30 20 "Calculation 517M9 9:26 CLB ICALCI Solids 95.9 % by 0.100 0.100 1 `SM2640 G 6/1/19 16:19 KBS P9E0019 Weight Ammonia as N 1900 mglkg dry 10 2.6 1 'SM4500-NH3 C 512119 16:16 BMS PSE0026 Nitrate/Nhrke as N BRL mg/kg dry 5.2 1.4 1 'SM4500-NO3 F 4128119 9:02 CLB P9D0467 pH 6.2 pH Units 1 '9045D 4/24119 16:36 CBM P9D0461 Phosphorus -Total 12000 mg/kg dry 520 160 100 'SM4600-P F 4126119 8:20 CLB POD0424 Total Kjeldahl Nitrogen 25000 mglkg dry 210 94 20 •351.2 617119 9:26 CLB P9D0642 Microbiological Parameters Fecal Colifonns BRL MPN/g dry 0.2 1 'SM9221 E 4/22/19 12:45 BMS P9D0398 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 `1311 4/23119 7:10 MMR P9D0386 TCLP Extraction Complete N/A 1 `1311 ZHE 4/24/19 9:00 TBL P9130410 TCLP Metals Mercury BRL mg/L 0.010 0.00016 1 '7470A 4/23/19 15:26 MMR P9D0386 Arsenic BRL mg/L 0.10 0.030 1 '6010D 4/23119 22:59 JAB P9D0388 Barium BRL mg/L 5.0 0.010 1 '6010D 4/23/19 22:59 JAB P9D0388 Cadmium BRL mg/L 0.025 0.0020 1 '6010D 4123/19 22:59 JAB P9D0388 Chromium BRL mg/L 0.25 0.015 1 '6010D 4/23/19 22:59 JAB P9D0388 Lead BRL mg/L 0.050 0.020 1 '6010D 4123119 22:59 JAB P9D0388 Selenium BRL mg/L 0.15 0.063 1 `6010D 4/23/19 22:59 JAB P9D0388 Silver BRL mg/L 0.25 0.0045 1 '6010D 4/23119 22:59 JAB P9D0388 TCLP Organochlorine Pesticides by GC/ECD Chlordane BRL mg/L 0.0025 0.00090 1 `8081B 4/25/19 13:33 ZRC P9D0417 Dieldrin BRL mg/L 0.00050 0.000068 1 `80818 4/25/19 13:33 ZRC P9D0417 Enddn BRL mg/L 0.00050 0.000068 1 '8081B 4/25/19 13:33 ZRC PgD0417 gamma-BHC BRL mg/L 0.00050 0.000030 1 *8081B 4/25/19 13:33 ZRC PSD0417 Heptachlor BRL mg/L 0.00050 0.000065 1 `8081B 4/25119 13:33 ZRC P9130417 Heptachlor Epoxide BRL mg/L 0.00050 0.00011 1 '8081B 4125/19 13:33 ZRC P9D0417 Msthoxychlor BRL mg/L 0.00050 0.000090 1 '8081B 4125119 13:33 ZRC P9D0417 Toxaphene BRL mg/L 0.025 0.0018 1 '808113 4/25/19 13:33 ZRC PSD0417 Surrogate Recovery Control Limits Decachlorobiphenyl 12 % 13-186 SE Tetrachloro-m-xylene 11 % 40-134 SE TCLP Semivolatile Organic Compounds by GC/MS 2,4,5-Trichlorophenol BRL mg/L 0.25 0.0040 1 '8270D 4126119 14:04 JMV P9D0433 2,4,6-Tdchlorophenol BRL mall- 0.10 0.0044 1 `8270D 4/25/19 14:04 JMV P9130433 2,4-Dinitrotoluene BRL mg/L 0.012 0.0032 1 "8270D 4/25/19 14:04 JMV P9D0433 2-Methylphenol BRL mg/L 0.050 0.0019 1 `8270D 4/25/19 14:04 JMV P9D0433 This report should not be reproduced, except in its entirety, withoutthe written consent of Prism Laboratories, Inc. 449 Sprogbrook Road -P.O. Box 240M -Charlotte, NC 28224-OW Phone: 7041629.6364-Toll Free Number: 1-800/529.6364-Fax: 704/626-0409 Page 4 of 15 Laboratory Report ram] O I `- I� �1 Fun -Service Anaiyncal a r n J' V' Environmental Sowtlons �ow..ow,sa vw 05/08/2019 Town of Mooresville/RR WN/TP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Prism Sample ID: 9040345-01 P. 0. Box 878 Prism Work Order: 9040345 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 04/22/19 08:42 Time Submitted: 04/22/19 11:33 Parameter Result Units Report MDL Limit Dilution Factor Method Analysis Analyst DateTme Batch ID 3/4-Methylphenol BRL mg/L 0.050 0.0025 1 `8270D 4125/19 14:04 JMV P9D0433 Hexachlorobenzene BRL mg/L 0.020 0.0041 1 `8270D 4125/19 14:04 JMV P9D0433 Hexachlorobutadiene BRL mg/L 0.050 0.0028 1 `8270D 4/25/19 14:04 JMV P900433 Hexachloroethane BRL mg/L 0.050 0.0023 1 `82701) 4/25119 14:04 JMV P9D0433 Nitrobenzene BRL mg/L 0.050 0.0024 1 `8270D 4/25119 14:04 JMV PSD0433 Pentachlorophenol BRL mg/L 0.25 0.0033 1 '8270D 4125/19 14:04 JMV PgD0433 Pyridine BRL mg/L 0.25 0.0023 1 '82701) 4/25119 14:04 JMV P900433 Surrogate Recovery Control Limits 2,4,8-Tribromophenol 33 % 43-140 SE 2-Fluorobiphenyl 33 % 44-119 SE 2-Fluorophenol 39 % 19-119 Nitrobenzene-d5 31 % 44-120 SE Phenold5 28 % 11-52 Terphenyl-d14 35 % 50-134 SE TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRL mg/L 0.035 0.00083 1 '8260B 4/24119 23:13 KDM P9D0439 12-Dlchloroethane BRL mg/L 0.025 0.00066 1 "8260B 4/24119 23:13 KDM P91)0439 1,4-Dichlombenzene BRL mg/L 0.38 0.00050 1 '8260B 4/24/19 23:13 KDM P91)0439 Benzene BRL mg/L 0.025 0.00048 1 '8260B 4124/19 23:13 KDM PSD0439 Carbon Tetrachloride BRL mg/L 0.025 0.0011 1 '828013 4/24/19 23:13 KDM POD0439 Chlorobenzene BRL mg/L 5.0 0.00062 1 `8260B 4124119 23:13 KDM P9D0439 Chloroform BRL mg/L 0.30 0.00076 1 '8260B 4/24/19 23:13 KDM P9D0439 Methyl Ethyl Ketone (2-Butanone) BRL mg/L 10 0.0024 1 '8260B 4/24119 23:13 KDM P9D0439 Tetrachloroethylene BRL mg/L 0.035 0.00098 1 '8260B 4124119 23:13 KDM P9D0439 Trichloroethylene BRL mg/L 0.025 0.00078 1 '8260B 4/24119 23:13 KDM P9D0439 Vinyl chloride BRL mg/L 0.020 0.00097 1 '8260B 4124119 23:13 KDM P9D0439 Total Metals Aluminum 11000 mg/kg dry Mercury 0.59 DM mg/kg dry SAR Soil Preparation Complete g SAR Percent Moisture 81.6 %by Weight Arsenic 1.4 mg/kg dry Sodium Absorption Ratio 1.3 [blank] Cadmium BRL mg/kg dry Calcium 9900 mg/kg dry Calcium, SAR 240 mg/L Surrogate Recovery Control Limits 4-Bromanuorobenzene 95 % 80-124 Dibromolluoromethane 101 % 75-129 Toluene -de 95 % 77-123 26 6.7 1 '6010D 4/26M9 15:36 JAB PSD0478 0.62 0.18 10 '7471B 511/19 16;32 MMR PSE0006 1 '2-78-054 4/26119 10:00 MMR P00462 0.100 0.100 1 '2-78-064 4/29119 10:06 MMR P9D0494 1.0 0.14 1 '6010D 4/26119 15:36 JAB P9D0478 0.30 0.016 1 -2.78-064 4/26/19 16:43 JAB P9D0479 0.52 0.035 1 '6010D 4/26119 15:36 JAB P91)0478 100 27 1 "6010D 4126/19 16:36 JAB P91)0478 0.10 0.010 1 "6010D 4126/19 16:43 JAB PSD0479 This report should not be reproduced, except in As entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 704/629-6364-Toll Free Number: 1-8001629-6364-Fax: 704/525-0409 Page 5 of 15 /PRISM I Fun -Service Anaryu Environmental Solutions ,ss—saIES.I.Q Town of Mooresville/RR WWiP Attn: Whitney Munroe P. 0. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 05/08/2019 Client Sample ID: Class A Prism Sample ID: 9040345-01 Prism Work Order: 9040345 Time Collected: 04/22/19 08:42 Time Submitted: 04/22/19 11:33 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Copper 140 mglkg dry 26 3.6 10 Lead 6.0 mglkg dry 1.0 0.17 1 Magnesium 2200 mg/kg dry 26 2A 1 Magnesium, SAR 160 ni 0.10 0.0086 1 Molybdenum 6.6 mglkg dry 1.0 0.13 1 Nickel 8.7 mglkg dry 1.0 0.31 1 Potassium 2700 mg/kg dry 100 11 1 Selenium 2.1 mg/kg dry 1.0 0.29 1 Sodium 510 mglkg dry 100 14 1 Sodium, SAR 100 mg/L 0.60 0.018 1 Zinc 250 ni dry 100 16 10 '6010D 4/3011912:16 JAB P9130478 '60101) 412SM9 16:36 JAB PSD0478 -6011:11) 4/26M9 16:36 JAB P9D0478 '6010D 4126/19 16:43 JAB PSD0479 -6010D 4/26119 16:36 JAB P9D0478 '6010D 4126119 15:36 JAB PSD0478 '6010D 4126119 15:36 JAB PBD0478 '6010D 4126119 15:36 JAB P9D0478 •6010D 4/2611915:36 JAB P9130478 '6010D 4126119 16:43 JAB PSD0479 '6010D 4/30/19 12:16 JAB P9D0478 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.C. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/629-6364-ToUFree Number: l-8001629-6364- Fax: 704/626-0409 Page 6 of 15 Sample Extraction Data Prep Method: 361.2 Lab Number Batch Initial Final Date/Time 9040345-01 P9D0542 0.05 g 25 mL 04/30/19 9:45 Prep Method: SM4600-NH3 B Lab Number Batch Initial Final DateTme 9040345-01 P9E0026 1.01 9 50 mL 05/02/19 8:56 Prep Method: SM4600-PBS Lab Number Batch Initial Final Date/Time 9040345-01 P9D0424 1 g 50 mL 04/24/19 10:27 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final DateTme 9040345-01 PSE0019 30 g 30 g 05/01/19 16:19 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 9040345-01 PSD0410 12.5 g 250 mL 04/23/19 15:25 9040345-01 P9D0368 100 g 2000 mL 04/22/19 14:35 Prop Method: 3010A Lab Number Batch Initial Final DateTme 9040345-01 PSD0388 10 mL 50 mL 04/23/19 10:35 Prep Method: 7470A Lab Number Batch Initial Final DateTme 9040345-01 P91)0386 20 mL 30 mL 04/23/19 9:05 Prep Method: 3510C OC Lab Number Batch Initial Final Datarnime 9040345-01 P9D0417 200 mL 10 mL 04/24/19 9:15 Prep Method: 3510C MS Lab Number Batch Initial Final Date/rime 9040345-01 P9D0433 200 mL 1 mL 04/25/19 8:43 Prep Method: 5030E Lab Number Batch Initial Final Daternme 9040345-01 P9D0439 1 mL 10 mL 04/24/19 7:46 Prep Method: 3010A Lab Number Batch Initial Final DateTme 9040345-01 P9D0479 50 mL 50 mL 04/26/19 10:05 9040345-01 P9D0479 50 mL 50 mL 04/26/19 10:05 Prep Method: 3050E Lab Number Batch Initial Final DateTme 9040345-01 P9D0478 2 g 50 mL 04/26/19 8:10 9040345-01 P9D0478 2 g 50 mL 04/26/19 8:10 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-OW Phone: 7041629-6364-Toll Free Number: l-800/629.6364-Fax: 7041626-0409 Page 7 Of 15 Sample Extraction Data Prep Method: 74718 Lab Number Batch Initial Final Date/Time 9040345-01 P9E0005 0.6 g 50 mL 05/01/19 8.55 Prep Method: BAR 248-054 Lab Number Batch Initial Final Date/Time 9040345-01 P9D0462 250 g 250 9 04/25/19 10:00 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 9040345-01 Herbicides TCLP (Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - charlotte, NC 28224-OM Phone: 704/629.6364• Toll Free Number: l-800/62M364- Fax: 7041526-0409 Page 8 of 15 /PRISM I Full -Service Analytical & Environmental Solutions LnaenATenm m0. 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6364 • Fax: 704IS25-0409 Client Company Name: t1v,^- e�6lP Report To/Contact Name: Ullfit- Reporting Address: N G CHAIN( OF CUSTODY RECORD PAGE—L OF!/tQUOTE a TO Ensw PROPER BIWNG, Project Name: Gas O S1 c Short Hold Analysis: as (No) UST Project: (Yes) `Please ATTACH any project specific reporting (QC LEVE,)�j ll ill provisions and/or QC Requirements v Invoice To: MeoCtdN�� Address: YES NO N/A In Samples INTACT upon arrival? tea_ _ Received ON WET ICE7 e O PROPER PRESERVATIVES Indicated? ��Or)Received WITHIN HOLDING TIMES? \�•1.— O m CUSTODY SEALS INTACT? d VOLATILES reed WtOUT HEADSPACE?-�, 17 enone: -r"-rpuv-ya W Fax(Yes) (No): Purchase Order No./Billing Reference Email Address:tA)WtM2 Tvulft_dVl(� _ e� Requested Due Date 0 l Da 02D y ays ❑ 3 Days ❑ a Days Q 5 Deys EDD Type: PDF Excel_Other "Working Days" ❑ 6-9 Days�tandard 10 days O Rusp Work Must Be Site Location Name: Samples received after 14:00 will be processed next business daayyp� Site Location Physical Address: Turnaround time Is based on business days. excluding weekends and holidays. (SEE REVERSE RENDERED BYFPRSM� BORATORIES INC. TO CLIENT)IONS REGARDING TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEy Certification: NELAC DOD FL NC 1/ SC_ OTHER--7— NIA Water Chlorinated: YES_ NO ✓ /SERVICES Sample Iced Upon Collection: YES `/ NO CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRESERVA- TIMES AN is QUEST D ` ' _ DLO \ REMARKS a �Y ati PRISM LAB ID NO. `TYPE SEE BELOW NO. SIZE class �1-09. boil o D 1 i �,A � 4kt,- �2f r . . . Sampler's Signature Sampled By (Pent Name) 1' `A. � Affillatton Te Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be , submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized. e N oa B� sgn ure eeery By: 9lgnalure) ` DMilltaryfliours Additional Comments: Site Arrival Time: c- Z2 / ,S p 1 Ral hedI .(Signs ) caW Y' ) m ��( v'01 t Site Departure Time: i �rn�s /~Roefad eaByDIaataRe n9uhad (gntuo) Field Tech Fee: p a(� �!�L.. �� Mileage: ALLSAMPLE COOLERS LD eE TAPED SH Y ORT/1TION T(1 TH LABORATORY. C O�rP SAMPLES ARE NOTACCEPTEDAND VERIFIED AGAINST CDC UNTIL RE IED AT THE LABORATORY. ❑ Fed Ex ❑ UPS D Hand -delivered rdsm Held Service O Olher IL NPDFS: LISTGROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA j LANDFILL OTHER: iI�NC❑ SC El ❑ SC ❑ NC ❑ SC ❑ NC ❑ SCF1C ❑ SC ❑ NC ❑ SC El NC ❑ SC j ❑ NC ❑ SC ❑ NC ❑ SC "CONTAINER TYPE CODES: A=Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (Zero Head Space) ORIGINAL PRISM 190PRTOWE4IN4 Full -Service Analytical & Environmental Solutions 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6364 - Fax: 7041525-0409 Client Company Name: TOt o br't6vtlle.,, Report To/Contact Name: I1JWAVuUA MUr%W__ Reporting Address: .J? ore6viltt , AIG sd I IS CHAIN OF CUSTODY RECORD PAGE � OF _0ZQUOTE # TO ENSURE PROP3B BILLING: 1 Project Name: .SS ff 6S f Short Hold Analysis: ( as (No) UST Project: ear O 'Please ATTACH any pro ect specific reporting (QC L 11 111 provisions and/or QC Requirements s 14 Invoice To:c� �DOI'�W Address: YES NO Samples INTACT upon arrival? \ V = Received ON WET ICE? PROPER PRESERVATIVES indlatad? _ Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOtATILES reed W/OUT HEADSPACE?�.__ _ PROPER CONTAINERS used? TEMP; Therm 14 b7E) Z Observed:3_L°C / Con; s O _ _. r - r- vv . max t,esi Iro/: Purchase Order No./Billing Reference Email Address: lhM'WW1CoLC1� (� r1C.• OV TO BE FILLED IN SY CLIENTISAMPLING PERSONNEL Requested Due Date Ol Day 020ays 03Days04Days 05Days EDD Type: PDP Excel Other yP Cordfrcation: NELAC_ DOD— FL_ NC ry "Working Days" O0-9 Days�SYandard l0 days OPrues-Apporrnrtied�� Site Location Name: Samples received after 14:00 will be processed next business day. SC_ OTHER NIA Site Location Physical Address: Turnaround time Is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO (SEE _ RENDEEEDByPRSMRLABORATORIES, INC. TOCLIENT)SERVICES Sample Iced Upon Collection:YES1/�NO_ TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED CLIENT DATE COLLECTED ( SOIL, PRESERVA- r r PRISM TYPE SEE BELOW NO. SIZE SAMPLE DESCRIPTION COLLECTED MILITARY HOURS WATER OR SLUDGE) TNES L /r ram' REMARKS �/ `- LAS ID NO. ass i4 N q 8='ice Eb1l ns i Samplers SI nature4wo Sampled BY (Print Name) 'Eud. Affiliation •-T-Q � r a Upon relinquishing, this Chain of Custody is your authorized for Priam to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be char for any changes after analyses have been initialized. r m Y: (R.7 y ignslare felt• r b e Additional Comments: Site nmval Time: Re ngvy Y 19 Nrv) I y: vlurel Dy Site Departure Time: Ralinqul.t!",:, Slgnelure)� / ive yr nc ns r.s By: p Field Tech Fee: ) —z a 'i n Mileage: tl nl:' 1E: C P COOL ULO 6E TAPE SHUT TRANSPORTATION TO THE LABORATORY. Gn, - SAMPLESARENOTACCEPTEDANDVERIFlEDAGAINSTCOCUNTI AT THE LABORATORY. GtV O Fed Ex O UPS O Hend4ernered dsm Field Service ❑ Other N1r GROUNDWADRINKINGIDWAST LC FO NC NC SCATER: ❑ NC ❑ SC ❑ NC ❑ SC I ZINC ❑ SCTER. ❑ NC ❑ SCE O❑ O SC O❑ NC ❑ SC ❑ NC SC OO NC CSC ❑ ❑ ❑ ❑ 'CONTAINER TYPE CODES: A=Amber C = Clear G= Glass P = Plastic; TL =Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL ACCESS ANALYTICAL, INC. ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W. Cole PROJECTID 9040345 LABORATORY REPORT NUMBER 1904N72 DATE April30,2019 Primary Data Review By Secondary Data Review By Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick@axs-inc.com PLEASE NOTE: Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, POW Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air). and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical; Inc Access Analytical is a representative ofAES serving client in the SC/NC/GA areas_ All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883 315 4243 Page Page 11 of 15 nEe8-Sevice Analytical PRISM IEnvironmental Solutions SENDING LABORATORY: Priam Laboratories, Inc. P. O. Box 240543 Charlotte, NC 28224-0543 Phone: 800-529-6364 Fax: 704-525-0409 Project Manager: Terri W. Cole IRoNwfg' SUBCONTRACT ORDER Cerlilicilljoly. NELAC USACE_ Prism Laboratories, Inc. N X SC,^ Other 9040345 N!A RECEIVING LABORATORY: Analytical Environmental Services, Inc. 3080 Presidential Parkway Atlanta, GA30340 Phone :(770) 457-8177 Fax: NA Analysis Due Expires 1 i ID Comments Semple ID: 9040345-01.. Solid Snmpled:04/22/1908:42 /Laboratory Cjli •(J7 r Herbicides TCLP (Sub) 04/29/19 08:42 t 'onramers Sapplied.- N 149- u�P- IVA 0 �/� Vila: X'? 9'vrogh Released By Date Received By Date Rcicoecl By 0alc Rcceivcd By Date Page I of 1 i Page Page 12 of 15 Analytical Environmental Services, Inc Date: 30-Apr-19 Client: Prism Laboratories Client Sample ID: CLASS Lab Order 1904N72 Tag Number: 9040345-01 Project Name: 9040345 Collection Date: 4222019 8:42:00 AM Lab ID: 1904N72-001A Matrix: Solid Analyses y Result QDaI MDL Reporting Units BatchlD DF Date Analyzed Analyst Limit HERBICIDES, TCLP SW1311/8151A (SW3510C) 2,45-TP (Silvex) BRL 0.030 0.20 -&L 278276 1 0429201917:39 RB 2,4-D BRL 0.051 0.20 nWL 278276 1 0429201917:39 BB Surr. DCAA 54.9 0 49A.120 %REC 278276 1 04292019 17:39 HB Qualifiers Value eecceds maximum conmminent level 80.L Not Delemed ut MDL H Hol&ny limes far pngomtion orvmlysls sac HN N Annlvie Mt NELAC ceniMd a Amilvte dmeeted in the p cmiA mmhad blmik E Esummed value abuse quaninmt.. mnye S Spike R..vi,, mnv&bmq dueu, mvam ereaterdmn Resue.mae J EsnmmA knue dmmmd below Repniny Limit < Less shim Rosult 4m, Page Page 13 of 15 VJsv I.MjoNF1r [CTn1. AIRS �S'a ICPS.ItsT. 1.0ent Name: Access Analytical, Inc. SAMPLE/COOLER RECEIPT CHECKLIST 2. Carder: FedEX Q UPS ❑ USPS❑ Client Courier❑ Othei v°< N.. W. 3. 4, 5 6. 7. 8. 9. lo. 11 12 Clear Save as AES Work Order Number: 1904N72 Shipping container/cooler received in good condition? • _. damaged [] leaking ❑ other❑ _......... Custody seals present on shipping container? Custody seals intact on shipping container? Temperature blanks present? Cooler temperature(s) within limits of 0-19"C? [See Item 13 and 14 for temperature recordings.] Q ® ® Cooling Initiated for recently collected samples / Ice present ❑ Chain of Custody (CDC) present? Chain of Custody signed, dated, and timed when relinquished and received? • SIGNATURE & DATE ONLY Sampler name and/or signature on COC? Were all samples received within holding time? TA7 marked on the COC1 • I If no TAT indicated, proceeded with standard TAT per Terims &Conditions. 13. Cooler l Temperature 4.8 °C Cooler 2 Temperature 14, Cooler S Temperature °C Cooler 6 Temperature 15, Comments; 16. 17 18. 19. 20 21. 22. 23. 24. 25, 26. 27. Comments. This section only appllas to samples where pH can be rFnrLnA .mot Onfnrl ' b..r.. w ro °C Cooler 3 Temperature °C Cooler 4 Temperature °C °C Cooler 7 Temperature °C Cooler 8 Temperature °C I certify that l have completed sections 2-15(dated initials). M14/23/19 Yes No N/A 0etaas Were sample containers intact upon receipt? Custody seals present on sample containers? •.in Custody seals intact on sample containers? Do sample container labels match the COC? 14VA.",® ® incomplete Info Illegible no label ❑ other ❑ Are analyses requested indicated on the COC? Were all of the samples listed on the CDC received? E) ® ® samples received but not listed on COC El samples listed on COC not received ❑ Was the sample collection date/time noted? Old we receive sufficient sample volume for indicated analyses? Were samples received in appropriate containers? Were VOAsamples received without headspace (<1/4" bubble)? 01 in Were trip blanks submitted? listed on CDC ❑ not listed on COC ❑ certify that I have completed sections 16-27 (dated Initials). EW 4/23/19 iwte. Vol tunI aoaiyses require cnemical preservation out must oe eneclteo in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/rPH. ? 1 certify that 1 have completed sections 28-30 (dated initials). Lyy 4/23/19 O Checklist 6.9.17 Rev 2 Locked Page 4 of 5 Analytical Environmental Services, Inc Client: Prism Laboratories Project Name: 9040345 Workorder: 1904N72 Date: 30-Apr-19 ANALYTICAL QC SUMMARY REPORT BatchID: 278276 Sample ID: MB-278276 Client ID: Units: mg/L Prep Date: 04/29/2019 Run No: 397006 SampleType: MBLK TestCode: HERBICIDES, TCLP SWIMISISLL BatchID: 278276 Analysis Date: 0429/2019 Seq No: 8892500 Analyte Result RPT Limit SPK valve SPK Ref Val 0/.REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-1 P(SiIVCX) BRL 0.20 2,4-D BRL 0.20 Surr: DCAA 0.2532 0 0.5000 50.6 49.4 120 Sample ID: LCS-278276 Client iD: Units: mg/L Prep Date: 04292019 Run No: 397006 SampleType: LCS TestCode: RERBICm6.S,TCLP SW131USISIA BatchID: 278276 Analysis Date: 04292019 Seq No: 8892501 Analyte Result RPT Limit SPK value SPK Ref Val 0/.REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qua] 2.4,5-TP(Silvcx) 0.2692 0.20 0.5000 53.8 49 120 2.4-D 02681 0.20 0.5000 53.6 50.9 120 Sum DCAA 02668 0 0.5000 53.4 494 120 Sample lD: 1904N72-001AMS ClienllD CLASSA Units: mg/L Prep Date: 04(292019 Run No: 397006 SampleType: MS TestCode IIERBICIDE%TCLP SWI31118151A BatchID: 278276 Analysis Date: 04/292019 Seq No: 8892503 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4.5-TP(Silvex) 02807 0.20 0.5000 561 48.2 120 2,4-D 0.2704 0.20 0.5000 54.1 45 130 Surr: DCAA 0.2613 0 0.5000 52.3 49.4 120 Qndlrcra a Qualerlb..Resullvelue [ Leasihm Reaultwlue 9 Analyledo1.udin1heas°i d.1h.dblmk (- a BRL aeluo; p..in°hmn E leimmed(w1w above gwnlitalion mV) H Nolen limes for b prtparali°n or analyse [xceeded 1 Eamaled wtue del[vled W. R,.,dne Limit N Anp1yhro1XELACeer6led R RPD omsid.limi�s dues mmrix O Rol Lim RepuAk,Luuk 5 spite uftu DuRide limits du[ 10 maldx n Page 5 of 5 NC Certification No. 402 Case Narrative / PRISM Full -Service Analytical & NC Drinking Water Cart No. 37735 7/29/19 13:59 Environmental Solutions SC Certification No. 99012 ` L EORATORIES INa Town of Mooresville/RR VW TP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 07/08/2019 Prism Work Order. 9070083 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Analysis note for SAR: SAR =[Na]/SQRT(([Ca]+[Mg])/2} SAR = [ 180/23 ] / SORT (( [280/201 + [100/12.2]) / 2 ) SAR = 2.4 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate —Nitrite PAN = 0.3 * (13000 — 1700) + 0.5 * (1700) + 5.6 PAN = 4296 mg/kg Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (D.3) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc, 449 apringbrook Road - P.O. Box 240943 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number. 1.8001629.6364 - Fax: 7041626-0409 Page 1 of 16 Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Terri W. Cole Project Manager Data Qualifiers Key Reference Reviewed By Terri W. Cole Project Manager DM Sample diluted and RL increased due to the matrix. SE Surrogate recovery outside the QC limits due to emulsion. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "a Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364-Toll Free Number: 1400/629-6364 - Fax: 7041626.0409 Page 2 of 16 Fue-Service AnalyticalPRISM I Evironmental Solutions �RIES,„o Sample Receipt Summary 07/29/2019 Prism Work Order: 9070083 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received Class A 9070083-01 Solid 07/08/19 8:31 07/08/19 12:50 Samples were received in good condition at 0.5 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224A643 Phone: 7041629-6364 - Toll Free Number: l-600/629.6364-Fax: 704/62"409 Page 3 of 16 Fun -Service uRISM I Environmental Solutions u�I.Q Town of Mooresville/RRWWTP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 07/29/2019 Client Sample ID: Class A Prism Sample ID: 9070083-01 Prism Work Order: 9070083 Time Collected: 07/08/19 08:31 Time Submitted: 07/08/19 12:50 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Daterrime Batch ID General Chemistry Parameters Plant Available Nitrogen 4200 mglkg dry 1600 710 10 -Calculation 7/26119 8:26 BMS [CALC] %Solids 96.7 %by 0.100 0.100 1 'SM2540G 7/12M9 14:30 HBS P9G0186 Weight Ammonia as N 1700 mg/kg dry 10 2.6 1 *SM4500.NH3 C 7126/19 8:26 BMS P9G0380 Nitrate/Nitrite as N 5.6 mglkg dry 5.2 1A 1 *SM4500-NO3 F 7122/19 10:16 CLB P9G0324 PH 6.8 pH Units 1 '9045D 7/9/19 12:34 CBM P9G0138 Phosphorus -Total 14000 mg/kg dry 1000 320 200 'SM4500-P F 7124/19 10:24 CLB P9G0216 Total IQeldahl Nitrogen 13000 mg/kg dry 6200 2400 10 *351.2 7119119 14:06 BMS P9G0213 Microbiological Parameters Fecal Coliforms 52 MPN/g dry 0.2 1 'SM9221 E 718119 13:06 BMS P930166 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 *1311 ZHE 7111/19 715 TBL P9G0154 TCLP Extraction Complete N/A 1 *1311 7117119 7:30 MMR P9G0245 TCLP Metals Mercury BRL mg/L 0.010 0.00016 1 *7470A 7118/19 14:21 MMR P9G0276 Arsenic BRL mg/L 0.10 0.030 1 *6010D 7117119 12:45 JAB P9G0249 Barium BRL mg/L 5.0 0.010 1 '6010D 7117/19 12:45 JAB P9G0249 Cadmium BRL mg/L 0.025 0.0020 1 '6010D 7117/19 12:45 JAB P9G0249 Chromium BRL mg/L 0.25 0.015 1 *6010D 7/17119 12:45 JAB P9G0249 Lead BRL mg/L 0.050 0.020 1 '6010D 7/17119 12:45 JAB P9130249 Selenium BRL mg/L 0.15 0.063 1 *6010D 7/17/19 12:45 JAB P9G0249 Silver BRL mg/L 0.25 0.0045 1 '6010D 7/17/19 12:45 JAB P9130249 TCLP Organochlorine Pesticides by GC/ECD Chlordane BRL mg/L 0.0025 0.00090 1 *8081B 7123119 18:25 ZRC P9G0347 Dieldrin BRL mg/L 0.00050 0.000068 1 *80816 7/23119 18:25 ZRC P9G0347 Endrin BRL mg/L 0.00050 0.000068 1 *8081B 7/23/19 18:25 ZRC P9130347 gamma-BHC BRL mg/L 0.00050 0.000030 1 *80818 7123/19 18:25 ZRC P9G0347 Heptachlor BRL mg/L 0.00050 0.000065 1 *8081B 7123/19 18:25 ZRC PgG0347 Heptachlor Epoxide BRL mg/L 0.00050 0.00011 1 *8081B 7/23119 18:25 ZRC P9G0347 Methoxychlor BRL mg/L 0.00050 0.000090 1 *8081B 7/23119 18:25 ZRC P9G0347 Toxaphene BRL mg/L 0.025 0.0018 1 *8081B 7123/19 18:25 ZRC P9G0347 Surrogate Recovery Control Limits Deoachlorobiphenyl 23 % 13-186 Tetrachloro-m-xylens 35 % 40-134 SE TCLP Semivolatile Organic Compounds by GC/MS 2,4,5-Trichlorophenol BRL mg/L 0.25 0.0036 1 *8270E 7/17119 16:24 JMV P9G0254 2,4,6-Trichlorophenol BRL mg/L 0.10 0.0045 1 *8270E 7/17119 16:24 JMV P9G0254 2,4-Dinkrotoluens BRL mg/L 0.012 0.0042 1 *8270E 7117/19 16:24 JMV P9G0254 2-Methylphenol BRL mg/L 0.050 0.0024 1 *8270E 7/17/19 16:24 JMV P9G0254 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratones, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number..1-8001529-6364- Fax; 704/625-04g9 Page4of16 /,�,r,�SM Full -Service Analytical a Laboratory Report ✓r S Environmental Solutions 07/29/2019 umwroniea,xc Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Prism Sample ID: 9070083-01 P. O. Box 878 Prism Work Order: 9070083 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 07/08/19 08:31 Time Submitted: 07/08/19 12:50 Parameter Result Units Report MDL Limit Dilubon Factor Method Analysis Analyst Date/11me Batch ID 3/4-Methylphenol BRL mg/L 0.050 0.0025 1 '8270E 7/17/19 16:24 JMV P9G0254 Hexachlorobenzene BRL mg/L 0.020 0.0039 1 '8270E 7/17119 18:24 JMV P9G0254 Hexachlorobutad]ene BRL mg/L 0.050 0.0045 1 '8270E 7117/19 16:24 JMV P9G0254 Hexachlamethane BRL mg/L 0.050 0.0037 1 '8270E 7/17119 18:24 JMV PeG0254 Nitrobenzene BRL mg/L 0.050 0.0038 1 '8270E 7/17119 16:24 JMV P9G0254 Pentachlorophenol BRL mg/L 0.25 0.011 1 '8270E 7/17/19 16:24 JMV P9G0254 Pyridine BRL mg/L 0.25 0.0016 1 '8270E 7117/19 16:24 JMV PgG0254 Surrogate Recovery Control Limits 2,4,6-Tdbromaphenol 54 % 43-140 2-Fluorobiphenyl 51 % 44-119 2-Fluorophenol 50 % 19-119 Nitrobenzen"S 43 % 44-120 SR Phenol-d5 38 % 11-52 Terphanyl-d14 51 % 50-134 TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRL mg/L O.D35 0.0035 1 '8260D 7/12119 22:10 KDM PSGO179 1,2-Dichloroethane BRL mg/L 0.025 0.0041 1 '826013 7112119 22:10 KDM P9G0179 1,4-Dichlorobenzene BRL mg/L 0.38 0.0042 1 '8260D 7112119 22:10 KDM PSG0179 Benzene BRL mg/L 0.025 0.0034 1 '82600 7112119 2210 KDM P9G0179 Carbon Tetrachloride BRL mg/L 0.025 0.0055 1 '8260D 7112M922:10 KDM P9130179 Chlorobenzene BRL mg/L 5.0 0,0034 1 '82601) 7112/19 22:10 KDM P9130179 Chloroform BRL mg/L 0.30 0.0048 1 '82601) 7/12/19 22:10 KDM P9G0179 Methyl Ethyl Ketone (2-Butanone) BRL mg/L 10 0.0078 1 '82601) 7/12/19 22:10 KDM P9G0179 Tetrachloroethylene BRL mg/L 0.035 0.0031 1 '82601) 7/12/19 22:10 KDM P9G0179 Tdchloroethylene BRL mg/L 0.025 0.0046 1 '82601) 7/12119 22:10 KDM P9G0179 Vinyl chloride BRL mg/L 0.010 0.0041 1 '8260D 7112119 22:10 KDM P9G0179 Surrogate Recovery Control Limits Total Metals Aluminum 220oa mg/kg dry Mercury 0.41 DM mg/kg dry SAR Sol] Preparation Complete g SAR Percent Moisture 77.3 %by Weight Arsenic 3.5 mg/kg dry Sodium Absorption Ratio 2.4 [blank] Cadmium BRL mgft dry Calcium 13000 mg/kg dry Calcium, SAR 280 mg/L 4-Bromoguorobenzene 102 % 80-124 Dibromo0uoromethane 108 % 75-129 Toluene-d8 102 % 77-123 270 68 10 '6010D 7MS/1912:19 JAB P9G0166 0.26 0.090 5 '7471B 7/1611911:22 MMR P9G0232 1 '2-7M54 7/16119 13:00 MMR PSG0225 0.100 0.100 1 '2.78464 7117/1913:16 MMR P9130239 1.1 0.14 1 '60101D 7111/1914:48 JAB PSG0166 0.30 0.016 1 -2.78-064 7126119 8:36 JAB P9G0238 0.53 0.036 1 `6010D 7111/19 14:48 JAB P9G0165 110 28 1 '6010D 7116MI) 12:27 JAB P9G0165 10 0.10 10 '6010D 7126119 8:36 JAB P9G0238 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc, 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/629-6364-Toll Free Number: l-800/629-6364- Fax: 7041626-0409 Page 5 of 16 Jlg2R uISM a�Es�wc I Full -Service Analytical Environmental Solutions ��ro Town of Mooresville/RR W WTP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 07/29/2019 Client Sample ID: Class A Prism Sample ID: 9070083-01 Prism Work Order: 9070083 Time Collected: 07/08/19 08:31 Time Submitted: 07/08/19 12:50 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis DateMme Analyst Batch ID Copper 190 mg/kg dry 27 3.6 10 `6010D 7/16119 12:19 JAB PSGO165 Lead 8.6 mg/kg dry 1.1 0.18 1 '60101) 7111/19 14:48 JAB P9G0165 Magnesium 2100 mg/kg dry 27 2.4 1 •6010D 7/11119 14:48 JAB P9G0165 Magnesium, BAR 100 mg/L 1.0 0.086 10 '6010D 7126/19 8:36 JAB P9G0238 Molybdenum 11 mglkg dry 1.1 0.13 1 '6010D 7111119 14:48 JAB P9G0165 Nickel 11 mg/kg dry 1.1 0.32 1 '6010D 7/11/19 14:48 JAB P9G0165 Potassium 2000 mg/kg dry 110 11 1 •60101) 7/11/19 14:48 JAB P9G0165 Selenium 3.2 mg/kg dry 1.1 0.29 1 •6010D 7/11/19 14:48 JAB P9G0166 Sodium 750 mg/kg dry 110 14 1 `60101) 7116119 12:27 JAB P9G0165 Sodium, BAR 180 mg/L 6.0 0.18 10 '6010D 7126/19 8:36 JAB PDG0238 Zinc 330 mg/kg dry 110 16 10 `6010D 7/16119 12:19 JAB 11,91310165 This report should not be reproduced, except in Its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240643 -Charlotte, INC 28224-0643 Phone: 704/629.6364-Toll Free Number: l-8001629-6364- Fax: 704/526-0409 Page 6 of 16 as Full -Service Analytical a I S M I Environmental Solutions ueowroeres, ixc Town of Mooresville/RR WVVTP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 07/29/2019 Client Sample ID: Class A Prism Sample ID: 9070083-01RE1 Prism Work Order: 9070083 Time Collected: 07/08/19 08:31 Time Submitted: 07/08/19 12:50 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 *1311 7123119 7:50 MMR P9G0342 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "a Springbrook Road - P.O. Box 240943 - Charlotte, NC 28224-0643 Phone: 7041529.6364-Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 7 of 16 Sample Extraction Data Prep Method: 361.2 Lab Number Batch Initial Final Date/Time 9070083-01 P9130213 0.06 g 25 mL 07/15/19 11:17 Prep Method: SM4500-NH3 B Lab Number Batch Initial Final Daternme 9070083-01 P9G0380 1.02 g 50 mL 07/24/19 9:54 Prep Method: SM4600-PBS Lab Number Batch Initial Final Date/Time 9070083-01 P9G0216 1 g 50 mL 07/15/19 10:10 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final DateTme 9070083-01 P9G0186 30 g 30 g 07/12/19 9:00 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 9070083-01 P9G0154 12.5 g 250 mL 07110/19 13:00 9070083-01 P9G0245 100 g 2000 mL 07/16/19 14:20 9070083-01RE1 P9G0342 100 g 2000 mL 07/22/19 15:20 Prep Method: 3010A Lab Number Batch Initial Final DateMms 9070083.01 P9G0249 10 mL 50 mL 07/17/19 9:20 Prep Method: 7470A Lab Number Batch Initial Final Date/Time 9070083-01 P9G0276 20 mL 30 mL 07/18/19 8:40 Prep Method: 3610C GC Lab Number Batch Initial Final Date/Time 9070083-01 P9G0347 200 mL 10 mL 07/23/19 10:10 Prep Method: 3610C MS Lab Number Batch Initial Final DateTime 9070083-01 P9G0254 200 mL 1 mL 07/17/19 9:30 Prep Method: 5030E Lab Number Batch Initial Final Daternme 9070083-01 P9G0179 1 mL 10 mL 07/12/19 10:36 Prep Method: 3010A Lab Number Batch Initial Final Date?me 9070083-01 P9G0238 50 mL 50 mL 07/16/19 13:05 9070083-01 P9G0238 50 mL 50 mL 07/16/19 13:05 Prep Method: 3060B Lab Number Batch Initial Final Date/Time 9070083-01 P9G0165 1.96 g 50 mL 07111/19 8:55 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240643 -Charlotte, NC 28224-OW Phone: 704/529-6364-Toll Free Number.lAgO/629-6364-Fax:704/525-0409 Page 8 of 16 Sample Extraction Data Prep Method: 3050E Lab Number Batch Initial Final Date/Time 9070083-01 P9G0165 1.96 g 50 mL 07111/19 8:55 9070083-01 P9G0165 1.96 g 50 mL 07/11/19 8:55 Prep Method: 7471 B Lab Number Batch Initial Final Date/Time 9070083-01 P9G0232 0.6 9 50 mL 07/16/19 8:30 Prep Method: SAR 2-78-064 Lab Number Batch Initial Final Date/Time 9070083-01 P9G0225 250 g 250 g 07/15119 12:55 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 9070083-01 Herbicides TCLP(Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529.6364-Toll Free Number.l-8001629.6364-Fax: 7041626-0409 Page 9 of 16 PRISM I Full -Service Analytical Environmental Solutions as LaeOeAVRAS, mQ 449 Springbrook Road • Charlotte, NC 28217 Phone 7041629-836644 • Fax: 7041525-0409 Client Company Naml0 u� Report To/Corttaet Nae: -me: Reporting Address: Mbilt NL �8115 CHAIN] OF CUSTODY RECORD PAGE.. OF aS QUOTE # To ENSURE P OPEN BILLING: Project Name: Li Short Hold Analysis: `Please ATTACH any 1 provisions and/or -OTC Invoice To: o Address: Pr ri r5 la (No) UST Proje specific reporting (QC L Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES reed W/OUT HEADSPACE? PROPER CONTAINERS used? YES NO N/A ), °C / Cun! Phone:-7W —Id#0 3U(Fax (Yes) (No): Email Address: 1,1PyD8 y"tem L1 f_ EDD Type: PDF Exeel_Othar Site Location Name: Site Location Physical Address: Purchase Order No./Billing Reference e / Requested Due Date D 1 Day ❑ 2 Days ❑ 3 Days D 4 Days o 5 Days "Working Daya" O 6-0 Daysstandard 10 days 0 Bu h Work Must Be Samples received after 14:00 will be processed next business day. Turnamund time is based on business days, excluding weekends and holidays. (SEE TERMS & CONDITIONS SERVICES FPRISM TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Certification: NELAC_ DoD_ FL_ NC ✓ SC_ OTHER ✓ N/A Water Chlorinated: YES_ NO LABORATORIES, INC.REGARDINGR RENDERED BYTO CUEENT) Sample Iced Upon Collection: YES— NO_ CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATEROR SLUDGE) SAMPLE CONTAINER PRESERVA- TIMES - b� ANAL��NQUESTEDaQ p�r. r .aTTGG . ,/ REMARKS � •S�y�aT. PRISM LAB ID NO. -.-- -TYPE SEE BELOW __.._ NO. .. SIZE ASS A � �8 OX3� Soil _ =CE _._ bl f Sampler's Signature t• !/ — Sampled By (Print Name) 1 "'atVT `�'^' k 4L/�1. Affiliation I 0 WAi Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be a submitted in writing to the Prism Project Manager. There will be charges for angel after analyses have been initialized. Ro meur.5etl :(m9nalun, RTTe gals ey,fSVl u Rolnwis Sigrq ) ewiwd. ISlgnmure) D2ate RecNvetl ow ) Data ®N r rlsrn Latxxebrks onp INyaleum AdditionalComments: Site Arrive[ Time: Dd(Site Departure Time: b� y1'k••i ' ` S Field Tech Fee: 8:1-14, Mileage: hod d 5h nY • A SAMPLE CO SHOULD BE TAPED SHU US100Y OR T SPORTATION TO THE LABORATOB. O Group No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY. O Fed Fx ❑UPS O Handtlell ed dam Field Servke O Olhor (Al U I D NPDES: UST: GROUNDWATER: DRINKING WATER: 50 'C FO r, ❑NCOSC ❑ NC OSC ONC OSC ❑NC ❑SC ❑ SCE 0 NC O SC O�NC ❑ SC ❑ NC SC ❑ NC O SC n '. n n n o o ' n 13 o 'CONTAINER TYPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL �P R I S M I Full -Service Analytical S Environmental Solutions IASORAMAIES, INC, 449 Springbrook Road • Charlotte, NC 28217 Phone 704/529-6364 • Fax: 70f1 4�1625-0409 Client Company Name: -OIAAn ey- �v IaOrt4l[L Report To/Contact Name: lL)) MuYtTL e- Reporting Address: P.0 •-%6X. tW r r r Moer - al4t NC, z6llS CHrAI^N OF CUSTODY RECORD PAGE OF% QUOTE a TO ENSUI%FR0P9R BILLING: Project Name: t•46l Q EN 610 Short Hold Analysis: (1Tes (No) UST Proj 'Please ATTACH any project specific reporting (QC provisions and/or QC Requirements ,, Invoice To: —! bIAA'I oF- M Dolre4k Address: YES NO N/A m Samples INTACT upon arrival? Received ON WET ICE? O PROPER PRESERVATIVES Indicated? Received WITHIN HOLDING TIMES? _ N CUSTODY SEALS INTACT? d VOLATILES reed W/OUT HEADSPACE? PROPER CONTAINERS ue _ TEMP: Therm ID ObservedD, µ °C r Con.�°C -' _- — ` aA I'='/ Ir"' " Purchase Order No./Billing Reference Email Address: �41WIUTVrot a Wwdrr56a 1L11C_ OV o y Requested Due Date ❑ 1 Day ��2 pp/aays ❑ 3 Days O 4 Days ❑ 5 Days EDD Type: PDF✓ Excel Other "Working Days" ❑ S-9 DaysAstandard 10 days ORushwork Must Be Pro- pproved Site Location Name: Samples received after 14:00 will be processed next business day. Site Location Physical Address: Turnaround lime B based an business days, excluding weekends and holtdays. (SEE REVERSE FOR TERMS 6 CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Certification: NELAC — DOD FL� NC — SC_ OTHER N/A Water Chlorinated: YES NO Sample Iced Upon Collection: YES ✓O_ SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR I SLUDGE) SAMPLE CONTAINER PRESERVA_ TIMES ANALYSIS REQUESTED % .� a rr / REMARKS j �f Q %��• C PRISM LAB ID NO. 'TYPE SEE BELOW NO. SIZE oA AAS Ili- � 8 (� m$3� 5et� 'LCE 61 i i I Sampler's Signature Sampled By (Print Name) MV\ Affiliation - uK-, Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There wig be charges fo changes after analyses have been Initialized. _ a4nqulsa y: ( gnOwns) ece a . Signs ) Data ry ours Addidon-all'Coitmments: Site Arrival Time - Relinquished By Wre) ReceNed By. gnaw.) De ' �I G' / V 1 �%�7�$ � Site Departure Time: Rallnquiz vd ure) w or m eborernnes ey �� at P1 1 As) lsh (�I �2Vt ( Field Tech Fee: r�I Alto( � AlQf Mileage: Z1 Shlp SAMPLES ARE NOT ACCEPTEDAND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY OTE; ALL SAMPLE COOLERS a... ntilt�`m I rrocra I UUT VON rFUIkR1ITORY CDO Group v D l O Fed Ex D UPS D Hand -delivered Prism Reld Service ❑ Other V n 1/ J NPOES: UST: G UNDWATER: I DRINKING WATER: S ID WASTE: RCRA: CERCLA LANDFILL OTHER: ❑NC❑SC ❑NC CI SC ❑ C ❑SC ❑NC ❑SC I, NLC ❑SC ❑NC13 ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ' *CONTAINER TYPE CODES: A=Amber C=Clear Gin Glass P=Plastic; TL=Teflon-Lined Cap VOA= Volaflle Organics Analysis (Zero Head Space) ORIGINAL Access ANALYTICAL, INC. ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W. Cole PROJECT ID 9070083 LABORATORY REPORT NUMBER 1907820 DATE July 15, 2019 Primary Data Review By Secondary Data Review By Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick@axs-inc.com PLEASE NOTE: - Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. - AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab H FL-E87582, NELAP certified laboratory # E87582 - AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Grevimetrie), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination, Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803,781.4243 or toll fee at 883.315.4243 Page Page 12 of 16 Full -Service Analytical 8 Q7 a !, f 0 C7 _ Environmental Solutions i" i�oonraomet,xa SUBCONTRACT ORDER Certification: NELAC_ USACE Prism Laboratories, Inc. NC SC_ Other 9070083 N/ _ SENDING LABORATORY: RECEIVING LABORATORY: Prism Laboratories, Inc. Analytical Environmental Services, Inc. P. O. Box 240543 3080 Prcaidential Parkway Charlotte, NC 28224-0543 Atlanta, GA30340 Phone: 800-529-6364 Phone :(770) 457-8177 Fax: 704-525-0409 Fax: NA Project Managar. Terri W. Cole Analysis Due Expires Laboratory ID Comments Sample ID: 9070083-01 Solid Samplcd:07108/1908:31 clan -1 Herbicides TCLP (Sub) 07/15/19 08:31 Re eamM By Date Rectived By Dale Released By Dew Received By Date Pngc I of 1 Pall Page 13 of 16 Analytical Environmental Services, Inc Date•. 15-1ul-19 Client: Prism Laboratories Client Sample ID: CLASS Lab Order 1907820 Tag Number: 9070083-01 Project Name: 9070083 Collation Date: 7/812019 8:31:00 AM Lab ID- 1907820-001A Matrix: Solid Analyses Result Reporting y Qoal MDL Limit Units BatchlD DF DateAnalyzed Analyst HERBICIDES, TCLP SW1311/8151A 2,4,5 TP (Silvex) BRL 2,4-D BRL Surr. DCAA 58.9 Qp Mr.: v V.I., eated,un.ha on mmamimm. level M Nor Daema m MDL H Holding lima for prepemrion or ondyvs maded N Arelyre nal NELAC cenifsd a A..M. deramed loth. awcimed method blank (SW3510C) 0.030 0.20 nWL 281962 1 07/12=1920:07 HB 0.051 0.20 nre/L 281962 1 07/1=01920:07 HB 0 49.4-120 %AEC 281862 1 07/12l201920:07 HB E Es:imaad,mlueobove'umlrmlon rem, S Spike Recovery outside limie due to ret o Greater han Rauh value I Eslimaai value dI bdmv, Reem-not Limit Les Wen Rauh slue Page Page 14 of 16 '�NAL1TiCAt- F.NFTRONatrn'LV. AES SERI'1M 1. C. SAMPLE/COOLER RECEIPT CHECKLIST 1. Client Name: Access Analytical, Inc. 2. Carrier. FeclEx ❑� UPS ❑ USPS❑ Client❑ Courier❑ Othel Yes N. N/A 3. 4. S, 6. 7. 8. 9. 10. 11. 12. AES Work Order Number: 1907820 neon. Clear Save as Shipping container/cooler received in good condition? • 0 damaged ❑ leaking ❑ other❑ Custody seals present on shipping container? Custody seals Intact an shipping container? Temperature blanks present? Cooler temperatures) within limits of 0-6PC7[See item 13 and 14 for temperature recordings.) 0 ® © Cooling initiated for recently collected samples/ice present ❑ Chain of Custody (COC) present? Chain of Custodysigned, dated, and timed when relinquished and received? Sampler name and/or signature on COC? Were all samples recehred within holding time? TAT marked on the COC?CO)If no TAT Indicated, proceeded with standard TAT per Terms & Conditionx Li 13. Cooler l Temperature 2.1 °C 14, Cooler 5 Temperature °C 15. Comments: 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. Cooler 2 Temperature °C Cooler 3 Temperature °C Cooler 4 Temperature °C Cooler 6 Temperature °C Cooler 7 Temperature °C Cooler 8 Temperature °C 1 certify that I have completed sections 1.15 (dated initials). RAJ 7/10/19 Yes Nn N/A nefea. Were sample containers intact upon receipt? .• Custody seals present on sample containers? Custody seals Intact on sample containers? 0• Do sample container labels match the COC? 2) ® ® incomplete Info ❑ illegible no label F_i other (_J Are analyses requested Indicated on the COC? Were all of the samples listed on the CDC received? Q ® Q samples received but not listed an CDC El samples listed on CDC not received ❑ Was the sample collection date/time noted? Did we receive sufficient sample volume for indicated analyses? Weresamples received In appropriate containers? Were VOA samples received without headspace I< 114" bubble)? Were trip blanks submitted? •I listed on CDC ❑ not listed on COC ❑ 27. Comments: This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initlals). checked at Sample Receipt. Yes No N/A Details Comments 28 Have containers needing chemical preservati 29. Container .at rQ 30. W ' Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH. N I certify that I have completed sections 2S-30 (dated initials). Checklist 6.9.17 Rev 2 Locked m AP 7/10/19 on been checked? preservation guidelines? * • ♦ Was pH adjusted at Sample Receipt? AP 7/10/19 Page 4 of 5 AP 7/10/19 Page 4 of 5 Analytical Environmental Services, Inc Client: Prism Laboratories Project Name; 9070083 Worlaorderl 1907820 Date: 15-Jul-19 ANALYTICAL QC SUMMARY REPORT BatchlD: 281862 Su nplc ID: MB-281862 Client ID: Units: mg/L Prep Date: 07/1112019 Run No: 402616 Samryle type: MBLK TCSICOde: HERBICIDES, TCLP SWI311/8151A BalchlD: 281862 Analysis Date: 07/12/2019 Seq No: 9037028 Analyle Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val p/oRPD RPD Limit Qua] 2,4,5-TP (Silvex) BRL 0.20 24-D BRL 0.20 Surr: DCAA 03287 0 0.5000 657 49.4 120 Sample ID: LCS-28/862 Client ID: Units: mg/L Prep Date: 07/11/2019 Run No: 402616 SampleType: LCS TestCode: nERRICIDES.TCLP SW)31118151A BetchlD: 281862 Analysis Date: 07/12/2019 Seq No: 9037029 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP(Silvex) 0.3438 0.20 0.5000 68.8 49 120 2.4-D 0.3778 0.20 0.5000 75.6 50.9 120 Surr: DCAA 0.3687 0 0.5000 73.7 49.4 120 Sample ID: 1907665-OOIBMS Client lD: Units: mg/L Prep Date: 07/11/2019 Run No: 402616 SamplcType: MS TestCode: BERBICIDES,TCLP SWI311/9151A BatchlD: 281962 Analysis Date: 07/12/2019 Seq No: 9037030 Analyle Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val 8/.RPD RPD Limit Qual 2.4.5-1'P (Silvex) 02964 020 0.5000 59.3 482 120 2.4-1) 03277 0.20 0.5000 655 45 130 Surr: DCAA 03017 0 0.5000 603 494 120 o. D1 Qnlirre'.. Giealcnhan Result vaInc fD BRL ad. repo...... him. � I EglmaleJ vmine JgegeJ helm. Repmning Lim,. 0 up, Lim Reporting Lim, < Lae lhm, Result Wue E Eslimaid(vm1w above glnmilmimn mnge) N Anmlyk wl NELAC ceniaed S Spike Recavery mmi& limits due nnnulx a Anelyte dmaled in the neeclated mghmd blank H Holdina times Rv prepmalpn°r enmlyshe caeaeded R RPn mind, Heine due m mane Page 5 of 5 NC Certification No.402 Case Narrative PRISMFull Service Analytical & NC Drinking Water Cart No. 37735 10/23/19 15:25 Environmental Solutions SC Certffication No. 99012 L 130MTORIEe, INC Town of Mooresville/RR WVVTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 10/07/2019 Prism Work Order: 9100089 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Analysis note for SAR: SAR = [ Na ] / SORT { ([Ca] + [Mg]) / 2) SAR = [ 115123 ] / SORT {( [298/20] + [68/12.2] ) / 2 ) SAR = 1.6 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SORT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate —Nitrite PAN = 0.3 * (22000 — 1400) + 0.5 * (1400) + 2.6 PAN = 6700 mg/kg Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) This report should not he reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "a Springbrook Road - P.O. Box 240M -Charlotte, NC 28224-OW Phone: 704/629-6364 - Toll Free Number..1-800/629-6364- Fax: 7041626-0409 Page 1 of 16 Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. ��vu:re�C�� Terri W. Cole Project Manager Data Qualifiers Key Reference: 47"'-cep Reviewed By Terri W. Cole Project Manager DM Sample diluted and RL increased due to the matrix. ECV Ending CCV above the QC limit. Analyte not detected down to the MDL. No further action taken. SE Surrogate recovery outside the QC limits due to emulsion. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 epringbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0645 Phone: 7041629.6364-Toll Free Number: 1-8001529-6364-Fax:7041626-0409 Page2of16 PRISM I Fa ironmce al Solutions s Environmental Solutions Sample Receipt Summary 10/23/2019 Prism Work Order: 9100089 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received Class A 9100089-01 Solid 10/07/19 9:14 10/07/19 12:50 Samples were received in good condition at 2.5 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224.OW Phone: 704/626-6364-Toll Free Number: l-800/629-6364- Fax: 704/62"409 Page 3 of 16 ey I [� n I Full -Service Analytical & 'v' Environmental Solutions Town of Mooresville/RR W WiP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 10/23/2019 Client Sample ID: Class A Prism Sample ID: 9100089-01 Prism Work Order: 9100089 Time Collected: 10/07/19 09:14 Time Submitted: 10/07/19 12:50 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datei ID General Chemistry Parameters Plant Available Nitrogen 6700 mg/kg dry 790 420 10 'Calculation 10/18/19 16:10 CLB [CALL] % Solids 95.9 % by 0.100 0.100 1 'SM2640 G 10/10/19 12:19 EDV P9J0157 Weight Ammonia as N 1400 mg/kg dry 9.6 2A 1 'SM4600-NH3 C 1OM8119 16:10 BMS PsJ0299 Nitrate/NitrBe as N BRL mg/kg dry 5.2 1.4 1 `SM4500-NO3F 10/11/19 9:24 CLB P9J0161 pH 6.2 pH Units 1 *9046D 1018119 16:23 CBM P9J0134 Phosphorus -Total 14000 mg/kg dry 620 160 100 'SM4500-P F 10/16119 9:24 CLB P9J0242 Total Kleldahl Nitrogen 22000 mg/flg dry 2600 1400 10 •361.2 1019119 7:57 CLB PSJ0116 Temperature 21.1 pH Units 1 '9045D 10/8/19 16:23 CBM P9J0134 Microbiological Parameters Fecal Colifonns 390 MPN/g dry 0.2 1 'SM9221 E 1017119 13:10 BMS P9J0130 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 '1311 ZHE 1019119 6:52 TBL P9J0120 TCLP Extraction Complete N/A 1 `1311 10/9119 7:20 EDV P9J0127 TCLP Metals Mercury BRL ni 0.010 0.000034 1 '7470A 10/9119 13:03 mmr P9J0145 Arsenic BRL mg/L 0.10 0.030 1 •5010D 10/11/19 20:53 JAB P9J0180 Barium BRL mg/L 5.0 0.010 1 `6010D 10/11/19 20:53 JAB P9J0180 Cadmium BRL mg/L 0.025 0.0020 1 '6010D 10/11/19 20:53 JAB P9J0180 Chromium BRL mg/L 0.25 0.015 1 '60101) 10/11/19 20:53 JAB P9J0180 Lead BRL mg/L 0.050 0.020 1 `6010D 10/11/19 20:53 JAB P9J0180 Selenium BRL mg/L 0.15 0.063 1 '6010D 10/11/19 20:53 JAB POJ0180 Silver BRL mg/L 0.25 0.0045 1 '6010D 10/11/19 20:53 JAB P9J0180 TCLP Organochlorine Pesticides by GC/ECD Chlordane BRL mg/L 0.0025 0.00090 1 '8081B 10/11/19 18:34 NMB P9J0187 Daldrin BRL mg/L 0.00050 0.000068 1 '8081B 10/11/19 18:34 NMB P9J0187 Endrin BRLECV mg/L 0.00050 0,000068 1 '8081B 10/11/19 18:34 NMB P9J0187 gamma-BHC BRL mg/L 0.00050 0.000030 1 '8081B 10/11/19 18:34 NMB PSJ0187 Heptachlor BRL ni 0.00050 0.000065 1 '80818 10/11/19 18:34 NMB P9J0187 Heptachlor Epoxide BRL mg/L 0.00050 0.00011 1 '8081B 10/11/19 18:34 NMB P9J0187 Methoxychlor BRLECV mg/L 0.00050 0.000090 1 '8081B 10/11/19 18:34 NMB P9J0187 Toxaphene BRL mg/L 0.025 0.0018 1 '8081B 10/11/19 18:34 NMB P9J0187 Surrogate Recovery Control Limits Decachlorobiphenyl 74 % 13-186 Tetrachloro-mxylene 60 % 40-134 TCLP Semivolatile Organic Compounds by GC/MS 2,4,5-Trichlorophenol BRL mg/L 0.25 0.0036 1 '8270E 10/10/19 17:45 JMV P9J0162 2,4,6-Trichlorophenol BRL mg/L 0.10 0.0045 1 `8270E 10/10/19 17:45 JMV P9J0162 2,4-Dinlbotoluene BRL mg/L 0,012 0.0042 1 '8270E 10/10/19 17:45 JMV P9J0162 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224.OW Phone: 7041529-6364 - Toll Free Number: l-800/629-6364-Fax: 704/52"409 Page 4 of 16 AAGSM Full-SemiceAnalytical& Laboratory Report Environmental Solutions 10/23/2019 woaama,sc [xc Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Prism Sample ID: 9100089-01 P. 0. Box 878 Prism Work Order: 9100089 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 10/07/19 09:14 Time Submitted: 10/07/19 12:50 Parameter Result Units Report MOIL Limit Dilution Factor Method Analysis Analyst Date/Time Batch ID 2-Methylphenol BRL mg/L 0.050 0.0024 1 '8270E 10/10/19 17:45 JMV PSJ0162 3/4-Methylphenol BRL mg/L 0.050 0.0025 1 '8270E 10/10/19 17:45 JMV P9J0162 Hexachlorobenzene BRL mg/L 0.020 0,0039 1 '8270E 10/10/19 WAS JMV P9J0162 Hexachlorobutadiene BRL mg/L 0.050 0.0045 1 '8270E 10/10/19 17:45 JMV P9J0162 Hexachloroethane BRL mg/L 0.050 0.0037 1 '8270E 10/10/19 17:45 JMV P9JD162 Nitrobenzene BRL mg/L 0.050 0.0038 1 '8270E 10/10/19 17:45 JMV P9J0162 Pentachlorophenol BRL mg/L 0.25 0.011 1 '8270E 10/10/19 17:45 JMV P9J0162 Pyridine BRL mg/L 0.25 0.0016 1 '8270E 10/10/19 17:45 JMV P9J0162 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 46 % 43-140 2-Fluorobiphenyl 43 % 44-119 SE 2-Fluorophenol 48 % 19-119 Nitrobenzene-d5 40 % 44-120 SE Phenol-d5 34 % 11-52 Terpher l-d14 47 % 50-134 SE TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRL mg/L 0.035 0.0035 1 `8260D 10/11/19 13:52 KDM P9J0158 1,2-Dichloroethane BRL mg/L 0.026 0.0041 1 `8260D 10/11/19 13:52 KDM P9J0158 1,4-Dichlorobenzene BRL mg/L 0.38 0.0042 1 '8260D 10/11/19 13:52 KDM P9J0158 Benzene BRL mg/L 0.025 0.0034 1 '8260D 10/11/19 13:52 KDM PSJ0158 Carbon Tetrachloride BRL mg/L 0.025 0.0055 1 `8260D 10/11/19 13:52 KDM P9J0158 Chlorobenzene BRL mg/L 5.0 0.0034 1 `8260D 10/11/19 13:52 KDM P9J0158 Chloroform BRL mg/L 0.30 0.0048 1 '8260D 10/11/19 13:62 KDM P9J0158 Methyl Ethyl Ketone (2-Butanone) BRL mg/L 10 0.0078 1 `8260D 10/11/19 13:52 KDM P9J0158 Tetmchloroethylene BRL mg/L 0.035 0.0031 1 `8260D 10/11/19 13:52 KDM PBJO158 Tdchloroethylene BRL mg/L 0.026 0.0046 1 `8260D 10/11/19 13:52 KDM PSJO158 Vinyl chloride BRL mg/L 0.010 0.0041 1 •8260D 10/11/19 13:52 KDM P9J0158 Surrogate Recovery Control Limits Total Metals Aluminum 28000 mglkg dry Mercury 0.78 DM mg/kg dry BAR Soil Preparation Complete 9 BAR Percent Moisture 67.6 %by Weight Arsenic 3.8 mglkg dry Sodium Absorption Ratio 1.6 [blank] Cadmium BRL mg/kg dry Calcium 22000 mg/kg dry 4-Bmmofluorobenzene 107 % 80-124 Dibromofluoromethene 99 % 75-129 Toluene-d8 100 % 77-123 260 57 10 `6010D 10/16/19 14:54 JAB P9J0176 0.16 0.064 3 •7471B 10/10/19 13:20 moor P9J0166 1 '2-78-054 10/10/19 14:50 MMR P9J0146 0.100 0.1DO 1 '2-78-064 10/11/19 14:50 MMR P9J0178 1.0 0.14 1 •601 Do 10/14/19 16:17 JAB P9J0176 0.30 0.016 1 •2.78-064 10/22/19 8:42 JAB PSJ0177 0.52 0.035 1 '6010D 10/14/19 15:17 JAB P9JD176 1000 270 10 '6010D 10/16/19 14:64 JAB 1`900176 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240643 -Charlotte, NC 28224OW Phone: 704/629.6364-Toll Free Number...1-8001529-6364- Fax: 704/626-0409 Page 5 of 16 Laboratory Report m ISM Full -Service Analytical a % n ea ,xc Environmental Solutions 10/23/2019 Town of Mooresville/RR W WTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Prism Sample ID: 9100089-01 P. 0. Box 878 Prism Work Order: 9100089 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 10/07/19 09:14 Time Submitted: 10/07/19 12:50 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Calcium, SAR 300 mg/L 10 0.10 10 *60101) 10/16/19 8:46 JAB P9J0177 Copper 270 mg/kg dry 26 3.6 10 *60101) 10116119 14:64 JAB P9J0176 Lead 8.4 mg/kg dry 1.0 0.17 1 *60100 10/14119 16:17 JAB P9J0176 Magnesium 2000 rrl dry 26 2A 1 *6010D 10/14/19 16:17 JAB P9J0176 Magnesium, SAR 68 mg/L 1.0 0.086 10 *6010D 10/16/19 8:46 JAB P9J0177 Molybdenum 8.5 mglkg dry 1.0 0.13 1 *60101) 10/14/19 16:17 JAB PSJ0176 Nickel 11 mg/kg dry 1.0 0.31 1 *6010D 10M4/19 16:17 JAB P9J0176 Potassium 2500 mg/kg dry 100 11 1 *6010D 10/14/19 16:17 JAB P9.10176 Selenium 4.7 mg/kg dry 1.0 0.29 1 *6010D 10/14/19 16:17 JAB P9J0176 Sodium 940 mg/kg dry 100 14 1 *6010D 10/16/19 16:02 JAB P9J0176 Sodium, SAR 110 mg/L 1.0 0,038 2 *6010D 10/21/19 23:14 JAB P9J0177 Zinc 510 mg/kg dry 100 16 10 *6010D 10116/19 14:64 JAB P9J0176 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spring brook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364- Toll Free Number. 1A001529.6364-Fax: 704/52"409 Page 6 of 16 Sample Extraction Data Prep Method: 361.2 Lab Number Batch Initial Final Date/Time 9100089-01 P9J0116 0.05 g 25 mL 10/08/19 9:50 Prep Method: SM4500-NH3 B Lab Number Batch Initial Final Date/11me 9100089-01 P9J0299 1.09 g 50 mL 10/18/19 8:47 Prep Method: SM4500-PBS Lab Number Batch Initial Final Date/Time 9100089-01 P9J0242 1 g 50 mL 10/15/19 11:20 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final DateTme 9100089-01 P9J0157 30 g 30 9 10/09/19 14:22 Prep Method: 1311 Lab Number Batch Initial Final DatelTlme 9100089-01 P9J0127 100 g 2000 mL 10/08/19 14:35 9100089-01 P9J0120 12.5 g 250 mL 10/08/19 12:00 Prep Method: 3010A Lab Number Batch Initial Final DatelTme 9100089-01 P9Jc180 10 mL 50 mL 10/11/19 10:40 Prep Method: 7470A Lab Number Batch Initial Final Date/Tlms 9100089-01 P9J0145 20 mL 30 mL 10/09/19 8:40 Prep Method: 3610C GC Lab Number Batch Initial Final DateTime 9100089-01 PSJ0187 200 mL 10 mL 10/11/19 8:41 Prep Method: 3610C MS Lab Number Batch Initial Final Date/lime 9100089-01 PSJ0162 200 mL 1 mL 10/10/19 8:27 Prep Method: 6030B Lab Number Batch Initial Final Date/Time 9100089-01 P9J0158 1 mL 10 mL 10/11/19 9:29 Prep Method: 3010A Lab Number Batch Initial Final DateTme 9100089-01 P9J0177 50 mL 50 mL 10/10/19 14:50 9100D89-01 P9J0177 50 mL 50 mL 10/10/19 14:50 9100089-01 PGJ0177 50 mL 50 mL 10/10/19 14:50 Prep Method: 3050E Lab Number Batch Initial Final Date7rime 910D089-01 P9J0176 2 g 50 mL 10/10/19 8:11 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364-Fax: 704/626-0409 Page 7 of 16 Sample Extraction Data Prep Method: 3050E Lab Number Batch Initial Final DateTme 9100089-01 P9J0176 2 g 50 mL 10/10/19 8:11 9100089-01 P9J0176 2 g 50 mL 10/10/19 8111 Prep Method: 7471 B Lab Number Batch Initial Final Date/Time 9100089-01 P9J0166 0.6 g 50 mL 10/10/19 9:43 Prep Method: SAR 2-78-054 Lab Number Batch Initial Final DateTime 9100089-01 P9J0146 250 g 250 g 10109/19 14:50 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 9190089-01 Herbicides TCLP (Sub) This report should not be reproduced, except In Its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 7041529.6364-Toll Free Number: l-800/629-6364-Fax: 7041526-0409 Page 8 of 16 j P R I S M I Full -Service Analytical Environmental Solutions �e LAannrtTOmE$�NC 449 Spdngbrook Road • Charlotte, NO 28217 Phone 7041629-6364 • Fax: 704/525.0409 Client Company Name: DRqn .(,-A kIY6,alei Report To/Contact Name: L fLUAn-e_ Reporting Address: P. n.'S MCOM40tt t n)c� a$Ils CHAIN OF CUSTODY RECORD Yr/ NO PAGE—L OF !L- QUOTE R TO ENSURE PROPER 1RILL/j11�NGr I� AAS ft �YT4Y ardvel? Samples INTACT WET Received ON WET ICE? _ Project Name: t�)14LV T Short Hold Analysis: (No) UST P ject: s) b PROPER PRESERVATIVES indicated? _ -Please ATTACH any project specific reporting (QC LEV�I III IV) Received WITHIN HOLDING TIMES? T _ provisions endlor qTC RegUlremeDts CUSTODY SEALS INTACT? Invoice To: IM.I1E7{�-iV�DUll2�iA`�C� VOLATILES redd W/OUT HEADSPACE? PROPER CONTAINERS u�seYd7 _ TEMP: Therm Ott_ 1, Observed: L, -c 1 Com Address: rnone: •mT—utru—s ca_y Fax (Yes) (No): Purchase Order NoJBilling Reference Email Address: WM rNe cresillE nC- d�/ TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL i �--- Requested Due Date O 1 Day ❑` 2 Days O 3 Days ❑ 4 D 5 Days EDD Type: PDF ✓ Excel-- Other Certification: NELAC_ DOD_ FL_ NC t/ RD�ayhs "working Days" ❑ BA Days g5lantlare 10 days O Pre-Appmved Be Site Location Name: Samples received after 14:00 will be processed next business day. SC_ OTHER NIA Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO_ (SEE REVERSE FOR TERMS a CONDITIONS REGARDING SERVICES RENDERED By PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES_ NO_ CLIENT DATE TIME COLLECTED MATRD( (SOIL, SAMPLE CONTAINER PRESERVA- r�i 4 . AN�AyLYs�a Rp�yQUESTED,�fr \ b 5 iti - PRISM SAMPLE DESCRIPTION COLLECTED MILITARY HOURS WATER OR SLUDGE) 1 *TYPE TIVES SEE BELOW NO. SIZE R},�T ,4-4'L"�4P r�`�,• REMARKS /�Q1 '�r, �i; a� S., , LAe ID NO. {} )U 7-I ©919 i =eE el Sampler's Signature, Annf�'Sampled 8y(Print Name)_I••r�iT"Q"� .?lMW� Alflnati0n 'Town. Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted In writing to the Prism Project Manager. There will be c as for any changes after analyses have been initialbad. RelNqulsneT y: Si9rNwre) D le MillivyNnum �[Addiitblo)n(all Corrnm nts: Site Anival Time: 1,�_ I',stMl : n re rvetl BY: (Signature) Dare • ""• r v Site Departure Time: Ra etl By1(i D b� met oc4i "ligpHibed By: (3 ONtpr Re.rew.d F.r P,le. Lad vauvies ay. pars Q�L / �� (� y Field Tech Fee: wo 6dFYN 16^Z•TIl Mileage: S 6EEDA 9HUTC CUS R S A I T H LA ORA RY. COG Group No. Malhpdp S Ipmenl: NAMPLE ARENOECOOLERS SAMPLEBARE NOTACCEPTEO AND VERIFIEDAGAINBT CDC UNTIL RECENEO AT THE LAeO TORV. RECEIVED DAT THE O Fed fix ❑ UPS O Hendderrveretl Pfism Field Servke O one e DES: UST. DRINKNGWATER: DWASCE. N❑ F❑ IC El SC ❑ NC ❑ SC ❑ NC SCAR. ❑ NC I SCNC ❑ ❑ NC ❑ SC ❑ENC ❑ SC ❑ NC SC I ❑TNC ❑ SC 1 ITAINER TYPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (Zero Head Space) ORIGINAL GIIAIN OF GUSTODY RECORDLAB USE ONLY Y@B NO NIA PRISMI Full -Service Analytical a Environmental SOIUtIODS PAGE OF QUOTE a TO ENSURE PROPER BILLING: L490PATOFIES INC d, S Samples INTACT upon anival? Received V _ � O 449 Project Name: Road -Charlotte, ON WET ICE? - o oneSpr70brook 25 0409 Phone 704/529.636a Fax: 704/525-0409 Short Hold Analysis: (Yes (No) UST Project: (Yes) ( O PROPER PRESERVATIVES Indicated? E/'- Client Company Name: �4u& eF MOorid7n11L 'Please ATTACH any project specific reporting (QC LEVE I 1 III Received WITHIN HOLDING TIMES? m ro Report To/Contact Name:_�ti )'li+'rl+c't j'y',u4'1 Y>•-C— Provisions and/or OC Requirements ,1 CUSTODY SEALS INTACT? _I o_ Invoice To: �µNl oT- A I D�YCGvi (4- Reporting Address: �• D."13 a'�ri VOLATILES mc'd WIOUT HPADSPACE? c`F Address: PROPER CONTAINS zed? N,O�Ij�/ A� .�) /� _ TEMP: Therm I17. - t'"� Observed:2.,K °C / Com1 � -. 'C Phone:-4e4—LLD -3J-A Fax (Yes) (NG): Purchase Order No./Billing Reference Email Address: Wrl^ r►egf—mer�ll.t-ne -c�! TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL _ Requested Due Date ❑ 1 Day ❑ 2 Days o a Days 04 Days ❑ 5 Days EDD Type: PDF_Excel_Other "Working Days" ❑ 6-B Days�ndard 10 days Rushh Be Certification: NELAC— DOD— FL_ NC ❑ poor must Site Location Name: Samples received after 14:00 will be processed next business day. Sc OTHER N/A Site Location Physical Address: Turnaround time Is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO_(SEE REVERSE FOR RAODnREGARDING SERVICES RENDERS Y PRISM .OIET) Sample Iced Upon Collection: YES_ NO TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED CLIENT SAMPLE DESCRIPTION DATE COLLECTED COLLECTED MILITARY (SOIL, WATER OR PRESERVA- ' / /�`�� /Q x, � PRISM LAB "TYPE NO. SIZE TIVES :' �`�: ty, /REMARKS ( �� ID NO. HOURS SLUDGE) SEE BELOW j huts Pr la1^I� 0AIL4 Soi I I/FT I/ oI I ' —jam' r e Sampler's Signature geL," Sampled A04ti9k1j 4ig By (Print Name) feLt Affiliation Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized. rpuf heAB. (Signature)Re D n�40 7� ii Wey Additional Comments: site Arrival Time: Rallnqu" Y t83 re Re Y: (Si9namm) Gas,� 4 ti��+� Site Departure Time: Rellnqua :(Signelure) Recehed For Prism Labarelodas y: - Oele I �/ �' Field Tech Fee: r(N n �M Me of Shipment NOTE: ALL SAMPLE B ON TO THE LABORgTORT. CDC p, �`� i/' ") Al MA, DaFTDAGAINSTCDC Mileage: ACCEPTED D RECEIVED ATTHTHANSPO p SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABO r UN UC 1� IV ' VVD� ❑ Fed Ex O UPS ❑ Handdelivared darn Feld Service ❑ Other NPDES: LIST NDWAI DRINNLID WASTE• F ❑ NC ❑ SC ❑ NC O SC ❑ NC ❑ SCTER: I ❑ NC ❑ CATER. QNC ❑ SIC ❑ NBC ❑ SC O�NC ❑CLA SC ❑ NC SC ❑ NC ❑ SC 1 ❑ ❑ ❑ ❑ _._. ❑ ❑ ❑ 71 n — `CONTAINER TYPE CODES: A=Amber C = Clear G= Glass P = Plastic; TL=Teflon-Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL ACCESS ANALYTICAL, INC. ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W. Cole PROJECTID 9100089 LABORATORY REPORT NUMBER 1910899 DATE October 15, 2019 Primary Data Review By Secondary Data Review By Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick@axs-ine.com PLEASE NOTE: Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. .AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, CA certified lab # FL-E87582, NELAP certified laboratory # E87582 AIHA-LAP,LLC Laboratory IDA00671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc, Access Analytical is a representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883315.4243 Page Page 11 of 16 [�} n n I Pull -Service Analytical & - -J v J Erl*tmmental Solutions • R VRNc�enf.nl: IC icowq1� SUBCONTRACT ORDER Cerlificatim: NELAC_ USACL- Prism Laboratories, Inc. NC SC_ Other 9100089 NIA-. .. SENDING LABORATORY: RECEIVING LABORATORY: Prism Laboratories, Inc. Analytical Environmental Services, Inc. P. O. Box 240543 3080 Presidential Parkway Charlotte, NC 29224-0543 Atlanta, GA 303,10 Phone:800-529-6364 Phone:(770)457.SI77 Fax: 704-525-0409 Fax: NA Project Manager. Terri W. Cole Analysis Due Expires Laboratory ID Comments a1 C':��155 Sample ID! 910008941 Solid Sampled: 10/D4h909:14 Herbicides TCLP (Sub) 10/18/19 09:14 L Released @v 1)am Received By [)me Released By Dmo Received 11% Date Paee I of 1 Pogo Page 12 Df 16 Analytical Environmental Services, Inc Date: 15-Oct-19 Client: Prism Laboratories Project: 9100089 Case Narrative Lab ID: 1910899 Sample Receiving Non-conformance: Sample information, on the Chain of Custody (COC), did not match that on the container label. On the COC, collection date is listed as 10/07/19 whereas, on the label, it is 10/O4/19. Sample logged in according to the COC. Page Page 13 of 16 Analytical Environmental Services, Inc Date: 15-Oct-I9 Client: Prins Laboratories Client Sample ID: CLASS Lab Order 1910899 Tag Number. 9300089-01 ProjectName: 9100089 Collection Date: 10/7/2019 9:14:00 AM Lab 1D: 1910899-OOIA Matrix: Solid Analyses Result Qua[ MDL Reporting Units Bil lD DF Date Analyzed Analyst Limit HERBICIDES,TCLP SW1311/8151A 2,4,5-7P (Silvex) BRL 2,4-D BRL Surr: DCAA 79.9 Quaaaersa a value eaemda maximum contaminant level BRL Nal De¢nedu MDL H Holdinadmasrorprepanauon.ranalysisaace N Analyle not NELAC ceniRed 3 Acolyte delemed In the oswdaled mnhad blank (SW3510C) 0.030 0,20 MVL 286382 1 10/15201913:24 HB 0.051 0.20 myL 286382 1 10115201913:24 HB 0 49.4-120 %REC 286382 1 10/15201913:24 HB E Enima¢d valueabore Ruunulmia. mnse S Spike Reeo,nry outside limds dun. mans s Gswmahan Result value J Enimmed value deemed below Rerun Limit Len than Reaue s.Ae Pago Page 14 of 16 ARnt,rncnt. aRS SttRt�cas.Ixr.N SAMPLE/COOLER RECEIPT CHECKLIST 1, OlentName: Access Analytical, Inc. 2. Cartier: Fed Ex ❑ts UPS ❑ USPS❑ Client❑ Courier❑ Othel 3. 4, S. 5, 7. 8. 9. 10. 1L 12 AES Work Order Number. 1910899 Ye[ N. N/A nmeile Clear Save as Shipping container/cooler received in good condition? • damaged 0 leaking other❑ -........... - Custody seals present on shipping container? Custody seals Intact on shipping container? Temperature blanks present? Cooler temperature(s) within limits of 0-6°C? (See Rem 13 and 14 for temperature recordings.) ® ® Cooling initiated for recently collected samples / ice present ❑ Chain of Custody (COC) present? Chain of Custody signed, dated, and timed when relinquished and received? Sampler nam.. nd/or signature an CDC? Were all samples received within holding time? TAT marked on the COC? • If no TAT indicated, proceeded with standard TAT per Terms&Conditions. 13 Cooler 1 Temperature 0.4 14, Cooler 5 Temperature 15 Comments: 16. 17 is 19. 20. 21, 22. 23. 24. 25. 26. °C Cooler 2 Temperature °C Cooler 3 Temperature °C Cooler 4 Temperature °C °C Cooler 6 Temperature °C Cooler 7 Temperature °C Cooler 8 Temperature °C 1 certify that I have completed sections 1-15 (dated initials). MOP 10/9/19 vex N.. corn Were sample containers intact upon receipt? • .� Custody seals present on sample containers? Custody seals intact on sample containers? Do sample container labels match the CDC? ©• ® © incomplete Info ❑ Illegible ❑ no label ❑ other ❑ Are analyses requested indicated on the CDC? Were all of the samples listed on the CDC received? ®• © ® samples received but not listed on CDC samples listed on CDC not received ❑ Was the sample collection date/time noted? Did we receive sufficient sample volume for indicated analyses? Were samples received in appropriate containers? Were VOA samples received without headspace (° 1/4" bubble)? Were trip blanks submitted? • listedon COC ❑ not listed on COC❑ 27. Comments. This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initials). MDP 1019119 checked at Sample Receipt. Yes No N/A Details Comments 28 Have containers needing chemical preservation been checked? 29. Containers meet preservation guidelines? g 30.1 Was pH adjusted at Sample Receipt? N ' Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Colifonns, VOCs and Oil & Graase/rPH. I certify that I have completed sections 29-30 (dated initials). MDP 10/9/19 Checklist 6.9.17 Rev 2 Locked rn Page 5 of 6 Analytical Environmental Services, Inc Client: Prism Laboratories Projeaa Name: 9100089 Workmder: 1910899 Date: 15-Oct-19 ANALYTICAL QC SUMMARY REPORT BatchlD: 286382 Sample ID: MB-286382 Client ID: Units: mg/L Prep Date: 10/14/2019 Run No: 409240 SalnplinType: MBLK TestCode: HERINCIDES,TCLP SW131118151A BatehID: 286382 Analysis Date: 10/15/2019 Sell No: 9206470 Analyte Result RPT Limit SPK value SPK Ref Val p/.REC Low Limit High Limit RPD WWI %RPD RPD Limit Qual G,4.0-I r (JIIVex) HILL 0.20 2,4-D BRL 0.20 Surr: DCAA 0.3725 0 0.5000 745 49.4 120 Sample ID: LCS-286382 Client ID: Units: mg/L Prep Date: 10/14/2019 Run No: 409240 SampleTypc: LCS TestCode: HERBICIDES,TCLP SWI311/8151A BatchlD: 286382 Analysis Date. 10/1512019 Seq No: 9206472 Analyte Result RPTLimit SPKvalue SPKRerval GKREC Low Limit High Limit RPD Ref Val %RPD RPDLimit Qual {4.D-IV(WIVCX) 03549 0.20 0.5000 71.0 49 120 2A-D 03745 020 0.5000 749 509 170 Surr: DCAA 03807 0 0.5000 76 1 494 120 SamplclD: 1910899.001AMS ClientlD: CLASSA Units: mg/L Prep Date: 10/14/2019 Run No: 409240 Samplcfype: MS TestCode: HERBICIDES,TCLP SWI31118151A BBtchID: 286382 Analysis Date: 10/15/2019 Seq No: 9206479 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual z,4,3- I r lm lvex) 04017 020 0.5000 80.3 482 120 2.4-D 04140 0.20 0.5000 82.8 45 130 Surr: DCAA 04053 0 0.5000 81.1 494 120 WQuaafiels > Gramm lhmt Reauli wlue rp BRC Belowrxpmmta hmil WI Euimaiml value deemed below Rimmma Limit 01 am Gm ft witind Limit < Ccs Nan Rmull value E l:aimmed (value above quantilaian aanae) N AWymnutNELACtimiied S $pike Aecoveryouldde limi¢due to matdz B Anaytedelmadiulheaz oaledmeUodblanb H Holdina Umu forpr[paraion or anaysis exceeded ft Rpp outsidelimitsdua to moWx JPage 6 of 6 TOWN OF MOORESVILLE CLASS A BIOSOLID PELLETS UTILIZATION AGREEMENT DISTRIBUTED UNDER NC DWQ PERMIT # WQ0036723 I. CONTACT INFORMATION THIRD PARTY r�fGp/ TOWN OF MOORESVILE FO TIQj,V%�� 7 LLB INFORMATION Name l� i� A Lamy Hendren 6 Ad X� (Permitree Designee) Mailing Address P.O. Box 878, Mooresville NC 28115 `�✓r �` C a �� 704-799-4063 Phone Number Email �S;, )i.,ngA4 - et'i'SL� di+� 1i4WY lhendren@mooresvillenc.gov II . DESCRIPTION Grp• This is pelletized material produced from the heat treatment of residuals from municipal wastewater. This product meets the standards for a Class A biosolid product according to the EPA's 40 CFR Part 503 regulations. III. RESTRICTIONS Residual land application is prohibited except in accordance with the instructions on this Utilization Agreement: L If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat 2. If the application causes prolonged nuisance conditions 3. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards 4. If the land is flooded, frozen, or snow -coveted, or is otherwise in a condition such that runoff of the residuals would occur 5. Within the 100 year flood elevation, unless the bulk residuals are injected or incorporated within a 24- hour period following a residuals land application event 6. During a measurable precipitation event (.e. greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period 7. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the pH of the soil, residuals and lime m;m„p is suitable for the specified crop 8. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event 9. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot 10. If the vertical separation of bedrock and the depth of residuals application is less than one foot 11. Biological Residuals shall not be stockpiled for more than 30 days prior to distribution 12. The Third Party accepting the residuals shall provide the Pennittee with all other nutrient applications (i.e. organic and/or inorganic fertilizers) 13. A copy of this Utilization Agreement shall be maintained at the site when bulk residuals are being applied 14. The residuals shall be prevented from entering any public or private water supply source (including wells) and any surface waters (e.g. streams, lake, river, wetland) 15. Residuals should be land applied at agronomic rates 0 2016 Town of Mooresville 16. Submission of Soil Samples prior to distribution of product 17. The Pertnittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the condition of the signed Utilization Agreement IV, SETBACKS Applicable setbacks in accordance with 15A NCAC 02T .1108(b): Description of Setback Setback by type of application (feet) Cake Residuals Private or public water supply 100 Surface Waters (streams — intermittent and perennial, perennial watetbodies, and wetlands) 25 Surface water diversions(ephemeral streams, waterwa s, ditches 0 Groundwater lowering ditches (where the bottom of the ditch intersects the S 0 Wells with ex ce tion to monitoring wells 100 Bedrock outcrops 0 V. APPLICATION RATES Application Rates should not exceed the calculated nitrogen requirements based on the Realistic Yield Expectation for a particular crop and the predominant soil series within the application area. This product has a North Carolina Fertilizer label of 5% Nitrogen — 1% Phosphorus — 0% Potassium ratio, but given that it is generated from aerobically digested residual biosolids it is assumed that a 30% mineralization rate (Organic Nitrogen to Plant Available Nitrogen) is used to calculated the Plant Available Nitrogen (PAN). The PAN listed below should be used along with other nutrient application to determine agronomic rates. NUTRIENT RANGES Percent Solids: 9498% Total Nitrogen: 22-1001bs/ton Ammonia Nitrogen: 0.4-6 lbs/ton Nittate/Nitrite Nitrogen: 0 - 0.01 lbs/ton PAN: 7-401bs/ton Total Phosphorus: Total Potassium: V.AGREEMENT 20-281bs/ton (2s P>O� 0-8 lbs/ton (as K20) $-AL{-n Larry Hen en Town of Mooresville Date Approximate Density:15 - 261bs/ft' &,4e Thin Par (P ' .ted Name) Tbard arty (Signature) Date C 2016 Town of Mooresville TOWN OF MOORESVILLE CLASS A BIOSOLID PELLETS UTILIZATION AGREEMENT DISTRIBUTED UNDER NC DWQ PERMIT # W00036723 I. CONTACT INFORMATION THIRD PARTY TOWN OF MOORESVILE INFF01 fPTJON INFORMATION Name ` Larry Hendren �. rPJ'nl (PemutteeDesignee) � Mailing Address ,7 "r4ar fM.n gu P.O. Box 878, Mooresville NC 28115 ;?JJ/S` 704-799-4063 Phone Number 704-1oT1J Email /'',ri G.» n�,, A lhendren@mooresvillenc.gov II . DESCRIPTION This is pelletized material produced from the heat treatment of residuals from municipal wastewater. This product meets the standards for a Class A biosolid product according to the EPA's 40 CFR Part 503 regulations. III. RESTRICTIONS Residual land application is prohibited except in accordance with the instructions on this Utilization Agreement: 1. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat 2. If the application causes prolonged nuisance conditions 3. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards 4. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur 5. Within the 100 year flood elevation, unless the bulk residuals are injected or incorporated within a 24- hour period following a residuals land application event 6. During a measurable precipitation event (i.e. greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period 7. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the pH of the soil, residuals and lime mixtute is suitable for the specified crop 8. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event 9. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot 10. If the vertical separation of bedrock and the depth of residuals application is less than one foot 11. Biological Residuals shall not be stockpiled for more than 30 days prior to distribution 12. The Third Party, accepting the residuals shall provide the Permittee with all other nutrient applications (Le. organic and/or inorganic fertilizers) 13. A copy of this Utilization Agreement shall be maintained at the site when bulk residuals are being applied 14. The residuals shall be prevented from entering any public or private water supply source (including wells) and any surface waters (e.g. streams, lake, river, wetland) 15. Residuals should be land applied at agronomic rates 0 2016 Town of Mooresville 16. Submission of Soil Samples prior to distribution of product 17. The Peruuttee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the condition of the signed Utilization Agreement IV. SETBACKS Applicable setbacks in accordance with 15A NCAC 02T .1108(b): Description of Setback Setback by type of application (feet) Cake Residuals Private or public water supply 100 Surface Waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 25 Surface water diversions (ephemeral streams waterways, ditches 0 Groundwater lowering ditches (where the bottom of the ditch intersects the S 0 Wells with exception to monitoting wells 100 Bedrock outcrops 0 V. APPLICATION RATES Application Rates should not exceed the calculated nitrogen requirements based on the Realistic Yield Expectation for a particular crop and the predominant soil series within the application area. This product has a North Carolina Fertilizer label of 5% Nitrogen —1 % Phosphorus — 0% Potassium ratio, but given that it is generated from aerobically digested residual biosolids it is assumed that a 30% mineralization rate (Organic Nitrogen to Plant Available Nitrogen) is used to calculated the Plant Available Nitrogen (PAN). The PAN listed below should be used along with other nutrient application to determine agronomic rates. NUTRIENT RANGES Percent Solids: 98% Total Nitrogen: 22-100 lbs/ton Ammonia Nitrogen: 0.4-6 lbs /ton Nitrate/Nitrite Nitrogen: 0 - 0.01 lbs/ton PAN: 7-40 lbs/ton Total Phosphorus: 20-281bs/ton (as P,O.I Total Potassium: V.AGREEMENT 0-81bs/ton as Larry Hend en)Town of Mooresville Date Approximate Density:15 - 20lbs/ft AjirS4;�®y Third Party (Printed Name) Third Pax i ignature) Date 0 2016 Town of Mooresville TOWN OF MOORESVILLE CLASS A BIOSOLID PELLETS UTILIZATION AGREEMENT DISTRIBUTED UNDER NC DWQ PERMIT # W00036723 I. CONTACT INFORMATION THIRD INF9]1YfATION� Name 5 Mailing Address //d a✓ e n u S .S 1- o%.G. ZPOP Phone Number o - - .3S-7 Email TOWN OF MOORESVILE INFORMATION Larry Hendren (Permittee Designee) P.O. Box 878, Mooresville NC 28115 704-799-4063 Ihendren@mooresvillenc.gov II . DESCRIPTION This is pelletized material produced from the heat treatment of residuals from municipal wastewater. This product meets the standards for. a Class A biosolid product according to the EPA's 40 CFR Part 503 regulations. III. RESTRICTIONS Residual land application is prohibited except in accordance with the instructions on this Utilization Agreement: 1. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat 2. If the application causes prolonged nuisance conditions 3. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards 4. If the Iand is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur 5. Within the 100 year flood elevation, unless the bulk residuals are injected or incorporated within a 24- hour period following a residuals land application event 6. During a measurable precipitation event (i.e. greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period 7. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop 8. If the land does not have an established vegetative cover unless the residuals ate incorporated or injected within a 24-hour period following a residuals land application event 9. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot 10. If the vertical separation of bedrock and the depth of residuals application is less than one foot 11. Biological Residuals shall not be stockpiled for more than 30 days prior to distribution 12. The Third Party accepting the residuals shall provide the Permittee with all other nutrient applications (i.e. organic and/or inorganic fertilizers) 13. A copy of this Utilization Agreement shall be maintained at the site when bulk residuals are being applied 14. The residuals shall be prevented from entering any public or private water supply source (including wells) and any surface waters (e.g. streams, lake, river, wetland) 15. Residuals should be land applied at agronomic rates 0 2016 Town of Mooresville 16. Submission of Soil Samples prior to distribution of product 17. The Petmittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the condition of the signed Utilization Agreement IV SETBACKS Applicable setbacks in accordance with 15A NCAC 02T .1108(b): Description of Setback Setback by type of application (feet) Cake Residuals Private or public water supply 100 Surface Waters (streams - intermittent and perennial, perennial waterbodies, and wetlands) 25 Surface water diversions(ephemeral streams, waterways, ditches 0 Groundwater lowering ditches (where the bottom of the ditch intersects the S 0 Wells with exception to monitoring wells 100 Bedrock outcrops 0 V. APPLICATION RATES Application Rates should not exceed the calculated nitrogen requirements based on the Realistic Yield Expectation for a particular crop and the predominant soil series within the application area This product has a North Carolina Fertilizer label of 5% Nitrogen -1 % Phosphorus - 0% Potassium ratio, but given that it is generated from aerobically digested residual biosolids it is assumed that a 30% mineralization rate (Organic Nitrogen to Plant Available Nitrogen) is used to calculated the Plant Available Nitrogen (PAN). The PAN listed below should be used along with other nutrient application to detennine agronomic rates. NUTRIENT RANGES Percent Solids: 4-9 ° o Total Nitrogen: 22-100 lbs/ton Ammonia Nitrogen: 0.4-6Is/ton Nitrate/Nitrite Nitrogen: 0 - 0.01 lbs/ton PAN: 7-40 lbs/ton Total Phosphorus: Total Potassium: V.AGREEMENT 20-28 lbs/ton (as P,Qj , 0-8lbs/ton (m K,0) Larry .t ooresville Date Approximate Density.15 - 20 lbs/fe Third Party (Printed Name) '; �>� w /L /L-/p Third Party (Signature) Date C 2016 Town of Mooresville YEAR Daily Dryer Log Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec YEAR�( �_ Daily D, Ver Log Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec Ol�Tis='�1►.ri�i��T�iiRrZ'I��i�� +�-.7�,�!!!��..l:�fA� m '��■r��:%�i�►� rr • "��i' �i a '.f��% I : ++ '1��y / y�� jap4/I jt3°i5f,f4 j m 1-Dv I ZT I 2106 YEARZa161 Jan Feb Mar Apr Daily Dryer Log May Jun Jul Aug Sept Oct Nov Dec Date Feed rate 8AM 4PM 12AM Ibs/hr Time Temp %DS Initials Time Temp %DS Initials Time Temp %DS Initials 1 Bypass f3 pass Syr ass [3 �s5 ISY L103 198 q ISY 00// /Yo 9 z o 00 q i'/ Wsf� 3 )a1152 -I' a 9I ° :s0 M 9 q •/. 11 52 1 q -1 9 q bi s Y 4 :/v 14� o AAA q01 po� '3 ° I2CiZ Iq �/ "/0 1Sj� s a05-o 08Iy q °� � L la m l� ��°r° 14,H S 9�°0 6 too C, C,k°G 4:os I9-1 99/• k •f-, 00 6 19�, 0 L✓Is 7 c�1Z5 ff. /S 05 17 44 ov l g q 5g � l ' aRm rqb R4`� 8 V150 ofj,zo 1q-1 q . 02 jC1$ '7/o I5Y / :0 ` ny 9 D erl3 I q'. :oY 9 / S 71aC/9% 15 10 r $� gc 00 1'71 9'f Z17 '105 B "5 6y®as 1Sy I c2 ' • 11 ar sc) 1c . ro 19 '•7 S 9 z 1-4 4'00 . 96 5a / f4� 1152 tq-7 q912 zz 2� : q s t 9 1( `3 .l in JRT : �i'13 ZZ19O 8 ; 10 10 V 9i L 9 / S IPO M4q '• TI 14 eRS Z,S' g : 00 194) S`i Z 14 -S1: o o t g ) 7 n 4-.,44 /a1 %oelAm )qg qq' 1 15 2Z75 8"06 19q 4q'/° r Sy 315 -7 9 5 9f% by 000� 14q 99 Y- 71N 16 7; rA 1 4i4'• T 3y /9s3 q % I y 1/ I G C %. /sY 17 d( � 11 1 1 CIR IN° m4fi, 5AM qq TkT 120 r16f q 9�4 1 18 als-o 6POM h q� 1Cf I 198 qq/o Isr 19 V100 q S s ,�r lq ' q 4, 20 a111 o 13l la 'G l M s03 9 21 a17� f;ro !9`X 97�� L6� 6a30 f 9 7 w17L 22 2 9'7 °, 3:55 104 987. 12oi !qq 99 °0 1sJ' 23 2 o o If'. / S / 9: 5 9 LEI o 1 7 /. 'S L 1 1 5 9 1 q 9 To /s 24 ° '� '~ ° ' . S 12 05 r q `d 2 aU eic, 1 151 Z o 1 °99o1 Sy 26 o�a :! 0 / 9 i g +7 y I P 1 9 °I °(o I �oZITT v a�� _ l a a 3: S °I V q� 1� S 28 Baas Cv.Zo `i 4;C 9,9 4-44 3:57 m (v g/1 S a'. 29 Zz 7 /% 9.5 La} -35 07 Cfq'/ ISi 121CP 196 qq% 15Y 30 2Z3; o7.90 a q`. AF• ti:�S Iq �' 115g j G `t "e rsy 31 S Cng19 0.(I oti r10 q:od .„ Iq5 aq'l. Arr 1203 19Li �q°° !Si 13rlia YEAR aU ( / Jan Feb Mar Apr Daily Dyer Log May Jun Jul Aug Sept Oct Nov Dec Date Feed rate 8AM 4PM 12AM Ibs/hr Time Temp %DS Initials Time Temp %DS Initials Time Temp %DS Initials 1 zaZcb %',vJ l`1(. 0,a'i L�l ° •j, M 1148 Iq/a q% /SY 2 �(o o �°r 3 g, 4 y;ee /9f� S9% Z,i1 115 % /S 5 zrzso T-L'o Pglk q`i°l= (-14 35G 19-7 9q°/. 07' 1202 Z049 qq 6 Zz6o of* 1'" i•rx �� y;v3p,,, y 9`1� `7'S 1151 I�Is '° iS 7 A;Z3 19 7 1 —7�5 5! S-Voft 1 1Z0-7 Iq(V 8 °M14 3: ss lei fZ /0 l q-7 qj 1ST' 9 IqP# 110 k Ia ° °a9 ql. 10 2Z3o V z,Q 111i AT It q / ic?00qq 'i 11 .2300 -(t 0S- /7 Y 179 'Lir ! 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