WQ0039053_Residual Annual Report 2019_20200131

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submital an
application?*
r Yes r No
Annual Report 2019
Year*
Date Paper Copy 1/29/2020
Received:*
Project Number* WQ0039053
Email Notifications
...................................................................................................
Does this need O Yes
review by the a No
hydrogeologist? *
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NJB Staff regarding electronic submittal, confirmation of receipt, and other issues.
....................................................................................................................................................................................................................................................................................................................................................................................................
Name * Martin Mabe
Email Address*
[e-mail]
Project Information
........................................................................................................................................................................
Submittal Type* f New Permit Application
r Renewal
r Annual Report
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0039053
Applicant\Permittee * Vaughn Stevenson
Facility Name * Bio-Nomic Services, Inc.
Phone Number*
336-312-1396
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Bio-Nomic Services, Inc. DCAR WQ0039053 - 2019 Annual Report
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Annual Report WQ0039053.pdf 36.53MB
upload only 1 RJF document. Maniple documents rust be combined into one RJF file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contact the reviewer or Tessa Monday. If a paper application is required,
be advised, applications accepted for pre -review until both the paper and electronic copies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (caIcs, soils report, specs, etc.
0 one full-size engineering plan set
0 One 11x17" engineering plan set
0 0ne extra set of specifications
o Fee (if required}
Mailine address:
Division of Water Resources Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
---- --- - --- - --- ------------ ------------------------------------i----------------------------------------------------------------------------
1617 Mail -service Center Att: Nathaniel Thornburg, 9"' Floor, Office #942W
---- -NC �-- - -------------------------------------------- ------------------------------------------------
Raleih, 7699-1617 512 N. SaVisbury St
For questions or problems contact Tessa Monday at [e-mail] or 919.707.3660.

* W By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 1/28/2020

2019 ANNUAL REPORT
LAND APPLICATION PROGRAM
BIO-NOMIC SERVICES, INC.
PERMIT #WQ0039053
Prepared For:
Bio-Nomic Services
530 Woodlawn St
Belmont, NC 28012
Compiled By:
Willcox & Mahe Soil Solutions, PLLC
723113 Summerfield Road
Summerfield, North Carolina 27358
January 2020

s
Willcox&mate
SOIL SOLUTIONS
January 28, 2020
NCDEQ-DWR Non -Discharge Branch
512 North Salisbury Street
01 Floor, Office #942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
Reference: 2019 LAND APPLICATION ANNUAL REPORT
Bio-Nomic Services, Inc.
Permit No. WQ0039053
WMSS Project No. 15-18 Ph: 09
Non -Discharge Permitting Unit
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Bio-Nomic Services,
Inc. (Bio-Nomics) for the above referenced permit. WMSS compiled this report using data
gathered during the compliance year by Bio-Nomics. This data includes: 1) Class A Annual
Distribution and Marketing / Surface Disposal Certification and Summary Form(s)
(DMSDF), 2) Annual Residual Sampling Summary Form(s) (ARSS), 3) Annual Pathogen
and Vector Attraction Reduction Form (2T), and 4) Analytical Data.
Bio-Nomics distributed a total of 3,645.52 Dry Tons of residual solids during the 2019
calendar year.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact the Bio-Nomic Services, Inc. or WMSS for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mahe
NC Land Application/Residuals Operator
#22753
Enclosures
SharedlWMSS ProjectM2015%15-18 Elio-Nomics\Phase 09 - Class A Permit12018 Annual Reporl\2018 ANNUAL REPORT.doc
Willcox & Mabe Sol Solutions, PLLC 17231 B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or Martin
336.312.1396 / www.willcownabesoil.com

Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
NC PERMIT # WQ0039053
Vaughn "Buck" Stevenson, Vice President
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmond, NC 28012
2019 Greenville Utilities WTP (NC0082139) Dry Tons 1,356.3
2019 McCall Farms WWTP (WQ0003823) Dry Tons 2,289.22
2019 Total Dry Tons 3,645.52
Total Dry Metric Tons 3,306.49

TABLE OF CONTENTS
SECTION NO. TITLE
DMSDF
II RSSF
III PVRF (271)
IV Analytical Data

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PVRF 2T

Greenville Utilities WTP is not required by permit to perform Pathogen Reduction or Vector Attraction
Reduction Monitoring, therefore no PVRF 2T Form has been included in this report.
McCall Farms W WTP falls into the bi-monthly (or 6 times per year) sampling frequency. This project
was performed in accordance with a lagoon closure plan in order to close out all lagoons at the facility.
The residual solids were removed from the lagoons, co -mingled, and stockpiled on site prior to land
application activities beginning. The project only lasted for approximately three months. Therefore all
six pathogen reduction samples (six sets of 7 fecal coliform samples) were collected during the three
month window of actual land application activities from the stockpiles to best represent the actual
material being land applied. On the attached PVRF 2T forms the monitoring period is listed as the
actual date of each set of 7 fecal coliform samples and was not listed as a time period such as January 1,
2019 through February 28, 2019. This approach is the best representation of the actual analytical data
collected.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
W WTP Name:
Bio-Nomic Services, Inc.
McCall Farms WWTP
Monitoring Period: From
2/26/2019 To
WQ Permit Number: W00039053
NPDES Number: W00003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thetmophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class
JAIL (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
1 Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
" '
If applicable to alternative performed (Class A or Class B) complete the following monitoring data.
Parameter
Allowable Level
in Sludge
g
Pathogen Density
g �'
Number o
Excee-
deuces
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
41
49
77
MPN/g
0
6 x Year
Grab
Stet 9221 c
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative nerformed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
JAR. 3 (30-day bench) ❑
I Alt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
jAlt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
lAft. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
I Alt. 10 (Incorporation)
El
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn "Buck" Stevenson, Vice President
Preparer Name and Title (type or print)
�� LY
Signature of Preparer* D to
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
02/26/19
42
1.6232
02/26/19
41
1.6128
02/26/19
48
1.6812
02/26/19
59
1.7709
02/26/19
41
1.6128
02/26/19
77
1 1.8865
02/26/19
42
1 1.6232
Total 11.8107
Average 1.6872
Geometric Mean 49 `€ ! Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results
3TATESVILLE
ANALYTICAL
Bio-Nomic
Service, INC
530 Woodlawn Street
Belmont, NC 28012
Receive Date:
02/26/2019
Reported:
03/15/2019
For:
McCall Farms Group #2
Comments:
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
190226-15-01
Fecal Coliforms
MF2-1
<42
MPN/g
SM92210E-2008
02/26/2019
WC
190226-15-01
Percent Solids
MF2-1
47.3
%
sm2 6-011
02/26/2019
WC
190226-15-02
Fecal Coliforms
MF2-2
<41
MPN/g
smm10E-2006
02/26/2019
WC
190226-15-02
Percent Solids
MF2-2
49
/,
W2WB-2011
02/26/2019
WC
190226-15-03
Fecal Coliforms
MF2-3
<48
MPN/g
SWWCE4006
02/26/2019
WC
190226-15-03
Percent Solids
MF2-3
42
%
sm2 a-2o11
02/26/2019
WC
190226-15.04
Fecal Coliforms
MF2-4
<59
MPN/g
SM02210E-2006
02/26/2019
WC
190226-15-04
Percent Solids
MF2-4
34
%
SM2640e-2011
02/26/2019
WC
190226-15-05
Fecal Coliforms
MF2-5
<41
MPN/g
sM92210E-200B
02/26/2019
WC
190226-15-05
Percent Solids
MF2-5
49
%
SM040B-2611
02/26/2019
WC
190226-15-06
Fecal Coliforms
MF2-6
<77
MPN/g
SM9 ICE-2006
02/26/2019
WC
190226-15-06
Percent Solids
MF2-6
26
%
SM2s40B-2o11
02/26/2019
WC
190226-15-07
Fecal Coliforms
MF2-7
<42
MPN/g
sM92210E-2006
02/26/2019
WC
190226-15-07
Percent Solids
MF2-7
47.4
%
SM2WB-2011
02/26/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cart#37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190226-15-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-06 Temp on Arrival: 3.2
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc.
WWTP Name: McCall Farms WWTP
Monitoring Period: From 2/26/2019 To
WQ Permit Number: WQ0039053
NPDES Number: WO0003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
i
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed. (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
PathogenDensity
ty
Number o
Excce-
denccs
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
32
47
77
MPN/g
0
6 x Year
Grab
SM 9221 c
Salmonella bacteria.
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC U2T .1107) - Please indicate alternative Derformed:
Alt.1 (VS reduction)
❑
JAR. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
JA1 6 (Alk. Stabilization
❑
Alt 7 (Drying -Stable) ❑
JAIt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
jAlt. 10 (Incorporation)
El
INo vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met.' (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn "Buck" Stevenson, Vice President
Preparer m ae and itle (type or print)
Z9 &
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
W00039053
McCall Farms
:::::::::::::::. .............
et. ram........:....:...............:...:.:
02/26/19
38
1.5798
02/26/19
54
1.7324
02/26/19
41
1.6128
02/26/19
32
1.5051
02/26/19
77
1.8865
02/26/19
38.5
1.5855
02/26/19
67
1.8261
Total 11.7281
Average 1.6754
Geometric MeanI Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results
Bio-Nomic Service, INC .vf
530 Woodlawn Street
Belmont, NC 28012
Receive Date: 02/26/2019
Reported: 03/15/2019
For: McCall Farms Group #1
Comments:
Sample Number parameter Sample ID Result Unit Method Analyzed Analyst
190226-16-01
Fecal Coliforms
MF-1-1
<38
MPN/g
SM92210E.2006
02/26/2019
WC
190226-16-01
Percent Solids
MF-1-1
53
%
SM2540B-2011
02/26/2019
WC
190226-16-02
Fecal Coliforms
MF1-2
<54
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-02
Percent Solids
MF1-2
37.3
q
SM2WB-2011
02/26/2019
WC
190226-16-03
Fecal Coliforms
MF1-3
<41
MPN/g
SWMCE-M06
02/26/2019
WC
190226-16-03
Percent Solids
MF1-3
49
%
SM25405-2011
02/26/2019
WC
190226-16-04
Fecal Coliforms
MF1-4
<32
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-04
Percent Solids
MF1-4
62.3
%
SM2540B-2011
02/26/2019
WC
190226-16-05
Fecal Coliforms
MF1-5
<77
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-05
Percent Solids
MF1-5
26
%
SWWB-2011
02/26/2019
WC
190226-16.06
Fecal Coliforms
MF1-6
<38.5
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-06
Percent Solids
MF1-6
52
%
SM2540B.2011
02/26/2019
WC
190226-16-07
Fecal Coliforms
MF1-7
<67
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-07
Percent Solids
MF1-7
30
%
SM2540B-2011
02/26/2019
WC
Respectfully submitted,
Dena Myers
NC Cent #440,
NCDW Cart #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190226-16-01 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-16-02 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-16-03 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-16-04 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-16-05 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-16-06 Temp on Arrival: 3.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-16-07 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc.
WWTPName: McCall Farms WWTP
Monitoring Period: From 3/4/2019 To
WQ Permit Number: WO0039053
NPDES Number: WO0003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerfnrmed-
Class A:
Alt. A (time/temp) ❑
( P)
Alt B Alk Treatment
( ) ❑
Alt. C (Prior Testing) ❑
"'''''"'
::..........
........
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
"
If applicable to alternative performed (Class A or Class B) complete the following monitoring data
Parameter
Allowable Level
in Sludge
Pathogen Density
g �'
Number o
Excee-
dences
Frequency
of Analysis
y
Sample
yp
Type
Analytical
Tech-ni que
Minimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
37
46
61
MPN/g
0
6 x Year
Grab
Stet 9221 C
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative Derformed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
jAlt. 10 (Incorporation)
1]
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
i7 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn "Buck" Stevenson, Vice President
Preparer Na a and Title (type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
03/04/19
48
1.6812
03/04/19
51.3
1.7101
03/04/19
43
1.6335
03/04/19
39
1.5911
03/04/19
�2
�1 6454
03/04/19
61
1.7853
03/04/19
37
1.5682
Total 11.6148
Average 1.6593
Geometric Mean Fecal Coliform NIPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction
requirement.

Analytical Results xr
Bio-Nomic Service, INC
530 Woodlawn Street
Belmont, NC 28012
Receive Date: 03/04/2019
Reported: 03/15/2019
For: McCall Farms Sample #3
Comments: Geometric Mean <46 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190304-12-01
Fecal Coliforms
1
<48
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-01
Percent Solids
1
42
%
SM25QB-2011
03/04/2019
WC
190304.12-02
Fecal Coliforms
2
<51.3
MPN/g
SM92210E-20M
03/04/2019
WC
190304-12-02
Percent Solids
2
39
%
SM WB-2011
03/04/2019
WC
190304-12-03
Fecal Coliforms
3
<43
MPN/g
sM92210E-2006
03/04/2019
WC
190304-12-03
Percent Solids
3
47
%
SM2540B-2011
03/04/2019
WC
190304-12-04
Fecal Coliforms
4
<39
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-04
Percent Solids
4
51.4
%
SM25406.2011
03/04/2019
WC
190304-12-05
Fecal Coliforms
5
<44.2
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-05
Percent Solids
5
45.2
%
SWWB-2011
03/04/2019
WC
190304-12-06
Fecal Coliforms
6
<61
MPN/g
SM92210E-20%
03/04/2019
WC
190304-12-06
Percent Solids
6
33
/
SM25QB-2011
03/04/2019
WC -
190304-12.07
Fecal Coliforms
7
<37
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12.07
Percent Solids
7
54
%
SWWB-2011
03/04/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cart #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190304-12-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-06 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc.
WWTPName: McCall Farms WWTP
Monitoring Period: From 3/4/2019 To
WQ Permit Number: W00039053
NPDES Number: W00003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
AIt.D (No Prior Test) ❑
Process to Farther Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatrent ❑ Thermoplulic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
I Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Mimmu
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
38
50
74
MPN/g
0
6 x Year
Grab
SM 9221 C
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
AIt. I (VS reduction)
❑
jAlt. 2 (40-day bench)
❑
Alt. 3 (30-day bench)
JAIT 4 (Spec. O, uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
JAR. 6 (Alk. Stabilization
jAlt 7 (Drying - Stable) ❑
1Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
JAIL 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn "Buck" Stevenson, Vice President
Preparer Na e and Title (type or print)
1 ) q -2,6
Signature of Preparer* ' Dke
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
Dafe
Fecal Lollforin
dog
03/04/19
55
1.7404
03/04/19
49
1.6902
03/04/19
51
1.7076
03/04/19
74
1.8692
03/04/19
38
1.5798
03/04/19
45
1.6532
03/04/19
42
1.6232
Total 11.8636
Average 1.6948
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction
requirement.

Analytical Results
Bio-Nomic Service, INC
530 Woodlawn Street
Belmont, NC 28012
Receive Date:
03/04/2019
Reported:
03/15/2019
For:
McCall Farms Sample #4
Comments:
Geometric Mean <50 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190304-13-01
Fecal Coliforms
1
<55
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-01
Percent Solids
1
36.3
%
SM2540B-2011
03/04/2019
WC
190304-13-02
Fecal Coliforms
2
<49
MPN/g
SM9221C&2006
03/04/2019
WC
190304-13-02
Percent Solids
2
41
%
SM2MOB-2011
03/04/2019
WC
190304-13-03
Fecal Coliforms
3
<51
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13.03
Percent Solids
3
39
%
SM2540B-2011
03/04/2019
WC
190304-13-04
Fecal Coliforms
4
<74
MPN/g
SM92210E-20M
03/04/2019
WC
190304-13-04
Percent Solids
4
27
4/
SM254OB-2011
03/04/2019
WC
190304-13-05
Fecal Coliforms
5
<38
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-05
Percent Solids
5
53
%
SM2540B"2011
03/04/2019
WC
190304-13-06
Fecal Coliforms
6
<45
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-06
Percent Solids
6
44
q
SM25408-2011
03/04/2019
WC
190304-13-07
Fecal Coliforms
7
<42
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13.07
Percent Solids
7
48
%
SM2540B-2011
03/04/2019
WC
Respectfully submitted,
Or -v✓Ul.J'Y)7tI
Dena Myers
NC Cert #440,
NCDW Cart #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190304-13-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-06 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers. lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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0
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0.1
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aC a: a: ¢ C.)I— F F H

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc.
WWTPName: McCall Farms WWTP
Monitoring Period: From 3/5/2019 To
WQ Permit Number: W00039053
NPDES Number: W00003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed -
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thennoplulic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑ ..................:....
Class B:
JAIL(l) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
.. ..
If applicable to alternative performed (Class A or Class B) complete the following monitoring data
Parameter
Allowable Level
in Sludge
PathogenDensity
ty
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimu
Geo. Mean
Maximu
Units
Fecal Colifotm
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
31
47
65
MPN/g
0
6 x Year
Grab
SM 9221 c
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAU 02T .1107) - Please indicate alternative Derformed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑Alt.
4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
JAlt. 6 (Alk. Stabilization
❑
JAIt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
jAlt. 10 (Incorporation)
e❑
INo vector attraction reduction alternatives were performed
❑
CEKFIk1CATI0N STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn "Buck" Stevenson, Vice President
Preparer Name and Title (type or print)
7/� zy za
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
Rafe
Fd64C-
03/05/19
53
1.7243
03/05/19
33
1.5185
03/05/19
63
1.7993
03/05/19
45
1.6532
03/05/19
51.3
1.7101
03/05/19
31
1.4914
03/05/19
65
1.8129
Total 11.7097
Average 1.6728
Geometric Mean4T siI Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction
requirement.

Analytical Results
Bio-Nomic Service, INC
530 Woodlawn Street
Belmont, NC 28012
Receive Date:
03/05/2019
Reported:
03/15/2019
For:
McCall Farm
Comments:
Geometric Mean: <47 MPN/g
STATESVILLE
ANALYTICAL
Sample Number parameter Sample ID Result Unit Method Analyzed Analyst
190305-33-01
Fecal Coliforms
1
<53
MPN/g
SM9221cE.2006
03/05/2019
CL
190305-33-01
Percent Solids
1
38
%
SWMOB.2011
03/05/2019
CL
190305-33-02
Fecal Coliforms
2
<33
MPN/g
SM92210E-20M
03/05/2019
CL
190305-33-02
Percent Solids
2
61.3
%
SM25QB-e011
03/05/2019
CL
190305-33.03
Fecal Coliforms
3
<63
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33.03
Percent Solids
3
32
%
SM25QB-2011
03/05/2019
CL
190305-33-04
Fecal Coliforms
4
<45
MPWg.
SM92210E-200B
03/05/2019
CL
190305-33-04
Percent Solids
4
44
"fie
SM25QB2011
03/05/2019
CL
190305-33-05
Fecal Coliforms
5
<51.3
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-05
Percent Solids
5
39
%
SM2590B-2011
03/05/2019
CL
190305-33-06
Fecal Coliforms
6
<31
MPN/g
SM9M10E-2W6
03/05/2019
CL
190305-33-06
Percent Solids
6
65
%
SM2Wa 2011
03/O6/2019
CL
190305-33-07
Fecal Coliforms
7
<65
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-07
Percent Solids
7
31
%
SMOWB-2011
03/05/2019
CL
Respectfully submitted,
'OP 'YJW v I ,!t I
Dena Myers
NC Cert #440,
NCDW Cart #37755,
EPA #NC00909
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190305-33-01 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-02 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-03 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-04 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-05 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-06 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-07 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 or 4

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Q Q Q

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
W WTP Name:
Bio-Nomic Services, Inc.
McCall Farms WWTP
Monitoring Period: From
3/5/2019 To
WQ Permit Number: W00039053
NPDES Number: W00003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
:....
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
is Digestion
........... .,.
.Anaero
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �'
Number o
dencExcee-
deuces
Frequency
of Analysis
y
Sample
yp
Type
Analytical
Tech-ni ue
q
Minimu
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
NIPN
CFU
1000 mpn per gram
of total solid (dry
weight)
27
32
36
MPN/g
0
6 x Year
Grab
SM9221 C
Salmonella bacteria
(in lieu of fecal
coliform)
3 NWN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
It. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
JAIt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
jAlt. 6 (Alk. Stabilization
❑
jAlt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
JAIt. 10 (Incorporation)
0
INo vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
l7 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn "Buck" Stevenson, Vice President
Prep�a'reerr Name and Title (type or print)
Signature of Preparer*
20
Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
...:.........:..... .
03/05/19
32
1.5051
03/05/19
27
1.4314
03/05/19
32
1.5051
03/05/19
36
1.5563
03/05/19
31
1.4914
03/05/19
34
1.5315
03/05/19
33
1.5185
Total 10.5393
Average 1.5056
Geometric Mean 32 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results
Bio-Nomic Service, INC
530 Woodlawn Street
Belmont, NC 28012
Receive Date: 03/05/2019
Reported: 03/15/2019
For:
Comments: Geometric Mean: <32 MPN/g
dANALT'fiL AL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190305-34-01
Fecal Coliforms
1
<32
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-01
Percent Solids
1
62
%
sm2we-w11
03/05/2019
CL
190305-34.02
Fecal Coliforms
2
<27
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-02
Percent Solids
2
74
%
sw5QB-2011
03/05/2019
CL
190305-34-03
Fecal Coliforms
3
<32
MPN/g
SMMlCE-20M
03/05/2019
CL
190305-34-03
Percent Solids
3
63
%
SM254OB-2011
03/05/2019
CL
190305-34-04
Fecal Coliforms
4
<36
MPN/g
sM92210E-w06
03/05/2019
CL
190305-34-04
Percent Solids
4
55.3
e/
SM2MB-2011
03/05/2019
CL
190305-34-05
Fecal Coliforms
5
<31
MPN/g
sM92210E-2005
03/05/2019
CL
190305-34-05
Percent Solids
5
65
%
SM2540&w11
03/05/2019
CL
190305-34-06
Fecal Coliforms
6
<34
MPN/g
SM9 10E-w06
03/05/2019
CL
190305-34.06
Percent Solids
6
59
%
SM2540B-2011
03/05/2019
CL
190305-34-07
Fecal Coliforms
7
<33
MPN/g
sM9221oE-20w
03/05/2019
CL
190305-34-07
Percent Solids
7
61
%
SMZQB-2011
03/05/2019
CL
Respectfully submitted,
rUD --'V�J'f7t i
Dena Myers
NC Cart #440,
NCDW Cart #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190305-34-01 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190305-34-02 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190305-34-03 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190305-34-04 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190305.34-05 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190305-34-06 Temp on Arrival: 3.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190305-34-07 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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ANALYTICAL DATA

Greenville Utilities WTP is an ongoing dredge and dewatering project at the alum lagoon at the
respective plant. The project actually began in June of 2019. The sampling frequency is bi-monthly (or
6 times per year) which is determined by the amount of dry tons distributed in 2019. Six sets of nutrient
and metal analyses were performed during 2019 to satisfy the permit condition outlined in Attachment
A. One TCLP analysis has also been included.
McCall Farms W WTP falls into the bi-monthly (or 6 times per year) sampling frequency. This project
was performed in accordance with a lagoon closure plan in order to close out all lagoons at the facility.
The residual solids were removed from the lagoons and stockpiled on site prior to land application
activities beginning. The project only lasted for approximately three months. Therefore all six nutrient
and metal analyses were collected during the three month window of actual land application activities
from the stockpiles to best represent the actual material being land applied. One TCLP analysis has also
been included.

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: May 6, 2019
Greenville Utility Commision #1 Permit No. W00039053
8.84 % Solids
6.7 nH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
1 (Mg/Kg x 0.002)
Nitrogen(TKN)
1.110
11,100.000
F 22.200
Phosphorus
0.209
2,090.000
4.180
Potassium
0.037
368.000
0.736
PAN (injected)*
0.230
3,869.500
7.739
PAN surface'
0.225
3777.000
7.554
AmmoniaNitrogen
0.010
100.000
0.200
Calcium
0.106
1,060.000
2.120
Calcium Carbonate E .
40.200
116,000.000
232.000
Magnesium
0.049
487.000
0,974
Sodium
0.025
250.000
0.500
Sulfur
4,830.000
9.660
Nitrate N / Nitrite N
--
4.760
0.010
Barium
---
---
SAR
Chloride
---
537.000
1.074
0.47
Iron
---
31700.000
63.400
Ceiling Concen.
Aluminum
---
117,000.00
234.000
(mg/Kg)
Arsenic
9.06
0.018
75
Cadmium
---
1.000
0.002
85
Chromium
---
23.900
0.048
--
Copper
---
247.00
0.494
4,300
Lead
---
15.70
0.031
840
Mercury
0,3040
0.001
57
Molybdenum
2.50
0.005
75
Nickel
9.41
0.019
420
Selenium
5.00
0.010
100
Zinc
---
53.10
0.106
7500
Waypoint Analytical 19-127-0214
"Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
E
wiIICOX&mabe
Prepared By: SOIL SOLUTIONS

a
Way po41nt .
ANALYTICAL
5/15/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-127-0214
Project Description: GUC #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-W6
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/7/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P'� P7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

QiWaypont
7621 ain 80i-7 Road, Richmond, 27 -6446 Main 804-743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-127-0214
Client Project Description: GUC #1
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66255
GUC
#1
Dewatered
Solids
05/06/2019
15:30
05/07/2019
WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354
SM-2540G
WiN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WrN
6010D
WiN
SM-4500-NH3C
WTN
9045D
WiN
AOAC 955.01
WrN
Page 2 of 6

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Wa FYI \ /�®� ��--� 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-127-0214
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Fr
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
r 1
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0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
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0 Yes
0 No
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0 Yes
0 No
COC properly completed
9 Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on Ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
N/A
Water- VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No
N/A
F— High concentration container (48 hr)
F— High concentration pre -weighed (methanol -14 d)
F— Low concentration EnCore samplers (48 hr)
F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: iBrandi Watson Date & Time: 05/07/2019 14:56:07
Page 5 of 6

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BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: May 6, 2019
Greenville Utility Commision #2 Permit No. W00039053
9.23 % Solids
6.1 nH
Parameter
%
Mg/KgDryWeightJ
0%9 x 10,OOQ)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
0.739
7,390.000
14.780
Phos horns
0.229
2,290.000
4.580
Potassium
0.029
292.000
0.584
PAN (injected)*
0.156
3,869.500
7.739
PAN (surface)*
0.151
3,777.000
7.554
Ammonia Nitrogen
0.010
100.000
0,200
Calcium
0.178
1,780.000
3.560
Calcium Carbonate E .
40.200
145.000.000
290.000
Magnesium
0.042
417.000
0.834
Sodium
0.027
273.000
0.546
Sulfur
5,890.000
11.780
Nitrate N /Nitrite N
---
4.700
0.009
Barium
--
---
---
SAR
Chloride
---
606.000
1.212
0.46
Iron
---
31600.000
63.200
Ceiling Concen.
Aluminum
137,000.00
274.000
4 /K
Arsenic
11.10
0.022
75
Cadmium
---
1.000
0.002
85
Chromium
---
43.700
0.087
---
Copper
293.00
0.586
4,300
Lead
---
15.10
0.030
840
Mercury
0.4390
0.001
57
Molybdenum
2.50
0.005
75
11.40
0.023
420
Selenium
5.00
0.010
100
1Nickel
Zmc
---
55.50
0.111
7 500
Waypoint Analytical 19-127-0215
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By: SOIL SOLUTIONS

0
Waypoint.
ANALYTICAL
5/15/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-127-0215
Project Description: GUC #2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/7/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
?':. r&-r
Pauric McGroary
Agronomist
Laboratory's liability In any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

0Waypoint
7621 ain 80i-7 Road, Richmond, 27 -6446 Main 804-743-9401 0Fax [phone]
ANALYTICAL www.waypDintanalytical.com
Sample Summary Table
Report Number: 19-127-0215
Client Project Description: GUC #2
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
66256
GUC
#2
Dewatered
Solids
OS/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
450ONO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
Page 2 of 6

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Wayp®int..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytfcal.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Service Inc
Report Number: 19-127-0215
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
�-
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
le Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
is Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
19 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No
N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
[— Low concentration EnCore samplers (48 hr)
[— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: lBrandi Watson Date & Time: .05/07/2019 15:00:29
Page 5 of 6

I Ti
I
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a

RIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: July 10, 2019
Greenville Utilitv Commision #3 Permit No. W00039053
20.00 % Solids
6.2 pH
Parameter
%
Mg/Kg Dry Weight
(°/a x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x Oc_0,02)
Nitrogen (TKN)
4.690
46,900.000
93.800
Phosphorus
0.239
2,390.000
4.780
Potassium
0.035
352.000
0.704
PAN (injected)*
0.947
3,869.500
7.739
PAN (surface)*
0.942
3,777.000
7.554
Ammonia Nitrogen
0,010
100.000
0.200
Calcium
0,148
1,480.000
2.960
Calcium Carbonate E .
40.200
27,000.000
54.000
Magnesium
0.050
501.000
1.002
Sodium
0.025
250.000
0.500
Sulfur
6,470.000
12.940
Nitrate N / Nitrite N
---
5.000
0.010
Barium
- -
--
---
SAR
Chloride
---
1190.000
2.380
0.64
Iron
-
29800.000
59.600
Ceiling Concen.
Aluminum
---
149,000.00
298.000
M li
Arsenic
-
11.30
0.023
75
Cadmium
---
1.000
0.002
85
Chromium
-
40.200
0.080
-
Copper
353.00
0.706
4 00
Lead
--
19.20
0.038
840
Mere
0.2520
0.001
57
Molybdenum
2.50
0.005
75
Nickel
13.30
0.027
420
Selenium
5.00
0.010
100
Zinc
61.60
0.123
7 00
Waypoint Analytical 19-192-0007
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N+ Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
willcox&mate
Prepared By: SOIL SOLUTIONS

WaypAoan ­ G.
NALYTICAL
7/19/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-192-0007 weµ
Project Description: GUC4-3
7621 whitepine Road, Richmond, VA 23237
Main 904-743-9401 ° Fax [phone]
w wmaypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 711112019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed In accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
? M v°.y'
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 8

0
Waypoin.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Bio-Nomic Servics Inc CASE NARRATIVE
Project: GUC-*3 PlKe*K 7-;!a-111
Lab Report Number: 19-192-0007
Date: 7/19/2019
Metals Analysis Method 6010D
Sample 67321
Analyte: Aluminum
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Calcium
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Sulfur
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Selenium
Page 2 of 8

WaypAANALintro G.
YTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 8

0.
Waypoi nt„ 7621 ain 80 -7 Road, Richmond, 27 -6446
Main 804-743-9401 0Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-192-0007
Client Project Description: GUC-4- 3 "4tEK't- 7-Xi-19
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
67317
GUC-3
Solids
67317
GUC-3
Solids
67317
GUC-3
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67317
GUC-3
Solids
67317
GUC-3
Solids
67317
GUC-3
Solids
67317
GUC-3
Solids
67317
GUC-3
Solids
67317
GUC-3
Solids
WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354
07/10/2019
11:47
07/11/2019
07/10/2019
11:47
07/11/2019
07/10/2019
11:47
07/11/2019
07/10/2019
11:47
07/11/2019
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07/11/2019
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07/11/2019
07/10/2019
11:47
07/11/2019
07/10/2019
11:47
07/11/2019
SM-2540G
WTN
SW-7471B
WFN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WrN
9045D
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AOAC 955.01
WTN
Page 4 of 8

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Way po nt . 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
ANALYTICAL www.waypolntanalytl al.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-192-0007
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: F-
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
r 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No I. Not Required
Custody seals intact on sample bottles?
0 Yes
0 No Not Required
Chain of Custody (CDC) present?
0 Yes
0 No
CDC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water- Sample containers properly preserved
0 Yes
0 No N/A
Water- VOA vials free of headspace
0 Yes
0 No N/A
Trip Blanks received with VOAs
0 Yes
0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration Encore samplers (48 hr)
F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Brandi Watson Date & Time: 7/11/2019 10:18:14
Page 7 of 8

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BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 28, 2019
Greenville Utility Commision #4 Permit No. W00039053
39.40 % Solids
5.9 pH
Parameter
%.
Mg/Kg Dry. Weight
(% x 10,000)
Pounds/UryTon
(Mg/K x 0.002)
Nitrogen(TKN)
0.513
5,130.000
1 10.260
Phosphorus
0.184
1,840.000
3.680
Potassium
0.068
680.000
1.360
PAN (injected)*
0.127
3,869.500
7.739
PAN (surface)*
0.112
3,777.000
7.554
Ammonia Nitrogen
0.031
305.000
0.610
Calcium
0.191
1,910.000
3.820
Calcium Carbonate E .
0.100
1,000.000
2.000
Magnesium
0.096
961.000
1.922
Sodium
0.025
250.000
0.500
Sulfur
4,070.000
8.140
Nitrate N / Nitrite N
-
4.560
0.009
Barium
---
-
SAR
Chloride
---
16.200
0.032
0.73
Iron
---
25 300.00
50.600
Ceiling Concert.
Aluminum
---
79,700.00
159.400
M /K
Arsenic
9.31
0.019
75
Cadmium
---
1.000
0.002
85
Chromium
---
102.000
0.204
--
Copper
127.00
0.254
4,300
Lead
---
20.70
0.041
840
Mercury
0.1170
0,000
57
Molybdenum
2.50
0.005
75
Nickel
38.10
0.076
420
Selenium
5.00
0.010
100
Zinc
---
50.20
0.100
7 500
Waypoint Analytical 19-241-0008
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.
Willcox&mabe
Prepared By: SOIL SOLUTIONS

Way ; --
a
ANALYTICAL
9/9/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-241-0008
Project Description: GUC-4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/29/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
F'" W67-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
W o
Page 1 of 6

0
W��■ ■�u 7621 W hitepine Road, Richmond, VA 23237
NMain 804-743-9401 ° Fax [phone]
pOI
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-241-0008
Client Project Description: GUC-4
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
67998
GUC4
Solids
67998
GUC4
Solids
67998
GUC4
Solids
67998
GUC4
Solids
67998
GUC4
Solids
67998
GUC4
Solids
67998
GUC4
Solids
67998
GUC4
Solids
67998
GUC4
Solids
67998
GUC4
Solids
WFN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
SM-254OG
WTN
SW-7471B
WTN
SM4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM4500-NH3C
WTN
9045D
WTN
9056A
WTN
AOAC 955.01
WFN
Page 2 of 6

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Wayl? iNALYnt.
ATICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nslytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servies Inc
Report Number: 19-241.0008
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
�—
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
40 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
41 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No
N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: lBrandi Watson Date & Time: 8/29/2019 14:18:16
Page 5 of 6

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BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 7, 2019
Greenville Utility Commision 95 Permit No. W00039053
19.60 % Solids
6.1 vH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0,002)
Nitrogen (TKN)
1.230
12,300.000
24.600
Phosphorus
0.291
2,910.000
5.820
Potassium
0.039
391.000
0.782
PAN (injected)*
0.289
3,869.500
7.739
PAN surface)*
0.264
3,777.000
7.554
Ammonia Nitrogen
0.051
510.000
1.020
Calcium
0.239
2,390.000
4.780
Calcium Carbonate E .
7.400
74,000.000
148.000
Mapnesium
0.061
607.000
1.214
Sodium
0.128
1280.000
2.560
Sulfur
5,970,000
11.940
Nitrate N / Nitrite N
---
25.000
0.050
Barium
---
- -
---
SAR
Chloride
---
53.600
0.107
2.67
Iron
---
32,200.00
64.400
Ceiling Concen.
Aluminum
---
128,000.00
256.000
M /K
Arsenic
25.50
0.051
75
Cadmium
---
5.100
0.010
85
Chromium
---
63.800
0.128
-
Copper
391.00
0.782
4,300
Lead
---
20.50
0.041
840
Mercury
0.5610
0.001
57
Molybdenum
12.80
0.026
75
Nickel
13.80
0.028
420
Selenium
25.50
0.051
100
Zinc
---
70.90
0.142
7,500
Waypoint Analytical 19-281-0002
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0;5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
sue, t
W11cox&mabe
Prepared By: SOIL SOLUTIONS

WaypAo0n ­ 0.
NALYTICAL
10/17/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number:19-281-0002
Project Description: GUC-5
7521 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 *Fax [phone]
www.waypointana"cal.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis In question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

0
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypolntanalytical.com
Client: Bio-Nomic Servics Inc CASE NARRATIVE
Project: GUC-5
Lab Report Number: 19-281-0002
Date: 10/16/2019
Metals Analysis Method 6010D
Sample 68529
Analyte: Aluminum
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Calcium
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Potassium
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Sulfur
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L458430
Page 2 of 8

WaypAoint�0.
NALYTICAL.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypo intanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 8

0.
Waypoint..
7621 Road, Richmond,
-6446
Main
ain
80.7
Sh4.743-9401 0Fax
27
804-271-6446
ANALYTICAL
w .waypointanalytical.com
Sample
Summary Table
Report
Number: 19-281-0002
Client
Project Description: GUC-5
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
SM-254GG
WTN
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
SW-7471B
WTN
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
SM-4500-NH3C-TKN
WrN
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
4506NO3F-2011
WTN
68526
GUC-5
Solids
10/07/2G19
14:11
10/08/2019
6010D
WTN
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
SM-4500-11113C
WTN
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
9045D
WTN
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
9056A
WTN
68526
GUC-5
Solids
10/07/2019
14:11
10/08/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
Page 4 of 8

Waypoint,.
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Ccert
530 Woodlawn St
Belmont, NC 28012
Report Number : 19-281-0002
Lab No: 68526
Sample ID: GUC-5
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9461 ° Fax [phone]
www.waypointana lytical.com
Project GUC-5
Information :
REPORTOPANALVSIS
Report Date: 10/17/2019
Received : 10/08/2019
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 10/ 7/ 2019 14:11
Moisture
80.4 H
%
0.010
1 10/15/19 16:30
ADM
SM-2540G
Selenium
<25.5
mg/Kg - dry
25.5
10 10/10/19 23:00
BKN
6010D
Total Solids
19.6 H
%
0.010
1 10/15/19 16:30
ADM
SM-2540G
Total Kjeldahl Nitrogen
1.23
% - dry
0.127
1 10/15/19 09:00
JPJ
;M-4500-NH3C-TKf
Phosphorus
2910
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Potassium
391
mg/Kg - dry
255
30 10/10/19 23:00
BKN
6010D
Sulfur
5970
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Calcium
2390
mg/Kg - dry
1280
10 10/10/19 23:00
BKN
6010D
Magnesium
607
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Iron
32200
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Manganese
857
mg/Kg - dry
25.5
10 10/10/19 23:00
BKN
6010D
Copper
391
mg/Kg - dry
12.8
10 10/10/19 23:00
BKN
6010D
Organic N
1.23
% - dry
0.127
1 10/15/19 09:00
CALCULATION
Nitrate+Nitrite-N
<25.0
mg/Kg - dry
25.0
1 10/11/19 15:28
ZBD
4500NO3F-2011
Nickel
13.6
mg/Kg - dry
12.8
10 10/10/19 23:00
BKN
6010D
Mercury
0.561
mg/Kg - dry
0.0785
1 10/11/19 12:17
TJS
SW-7471B
PH
6.1
S.U.
1 10/14/19 08:04
JSL
9045D
Calcium Carbonate Equivalent
7.4
%
0.1
1 10/15/19 14:55
DXT
AOAC 955.01
Total Volatile Solids
38.0 H
%
0.010
1 10/15/19 16:30
ADM
SM-254OG
Qualifiers/
*
Outside QC Limit
B
Analyte detected in blank
Definitions
C
GCMS Confirmation Analysis
E
Result above cal range
g
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter.
Page 5 of 8

(2)
Waypoimy
7621
-7 Road, Richmond,27 -6446
ain 80
Main 804-743-9401 0Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Joel Coert
Project
GUC-5
Report Date : 10/17/2019
530 Woodlawn St
Information :
Received: 10/08/2019
Belmont, NC 28012
me ow
Pam« 4
Report Number :19-281-0002
REPORTOFANALYSIS
Pauric McGroary
Agronomist
Lab No : 68526
Matrix:
Solids
Sample ID: GUC-5
Sampled:
10/7/2019 14:11
Test
Results
Units
MQL
DF Date ITime
By Analytical
Analyzed
Method
Ammonia Nitrogen
<0.051
% - dry
0.051
1 10/15/1913:00
JPJ SM-4500-NH3C
Chloride
53.6
mg/Kg - dry
20.4
1 10/14/19 17:23
CCR 9056A
Aluminum
128000
mg/Kg - dry
255
10 10/10/19 23:00
BKN 6010D
Arsenic
<25.5
mg/Kg - dry
25.5
10 10/10/19 23:00
BKN 6010D
Cadmium
<5.10
mg/Kg - dry
5.10
10 10/10/19 23:00
BKN 6010D
Chromium
63.8
mg/Kg - dry
12.8
10 10/10/19 23:00
BKN 6010D
Lead
20.5
mg/Kg - dry
15.3
10 10/10/19 23:00
BKN 6010D
Molybdenum
<12.8
mg/Kg - dry
12.8
10 10/10/19 23:00
BKN 6010D
Sodium <1280 mg/Kg - dry 1280 10 10/10/19 23:00 BKN 6010D
Zinc 70.9 mg/Kg - dry 63.8 10 10/10/19 23:00 BKN 6010D
Qualifiers/ B Analyte detected in blank
Definitions
H Beyond holding time
Page 6 of 8

Way p )Int.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanaiytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-281.0002
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other: �-
Thermometer ID: F—
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No 0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No 0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
IID Yes
0 No
CoolerlSamples arrived at the laboratory on ice.
ID Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No N/A
Water - VOA vials free of headspace
0 Yes
0 No 0 N/A
Trip Blanks received with VOAs
0 Yes
0 No 0 N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A
High concentration container (48 hr) F- Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Brandi Watson Date & Time: 10/08/2019 14:25:54
Page 7 of 8

w
0
v
ro
a

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 11, 2019
Greenville Utility Commision 96 Permit No. W00039053
16.50 % Solids
6.5 pH
Parameter
%
Mg/Kg Dry Weight
x 10,000
Pounds/Dry Ton
M x 0.002)
Nitrogen (TKN)
1.620
16,200.000
32.400
phosphorus
0.316
3,160.000
6.320
Potassium
0.046
458.000
0.916
PAN injected)*
0.376
3,755,100
7510
PAN surface)*
0.345
3,452.100
6.904
Ammonia Nitrogen
0.061
606.000
1.212
Calcium
0.192
1,920.000
3.840
Calcium Carbonate E .
8.400
84,000.000
168.000
Magnesium
0.056
559.000
1.118
Sodium
0.033
332.000
0.664
Sulfur
5,480.000
10.960
Nitrate N / Nitrite N
---
30.300
0.061
Barium
---
-
--
SAR
Chloride
---
89.700
0.179
0.69
Iron
---
35,400.00
70.800
Ceiling Concen.
Aluminum
---
139,000.00
278.000
(Mg/Kg)
Arsenic
---
16.40
0.033
75
Cadmium
---
0.606
0.001
85
Chromium
---
60.400
0.121
-
Copper
368.00
0.736
4,300
Lead
23.40
0.047
840
Mercury
---
0.5100
0.001
57
Molybdenum
---
1.96
0.004
75
Nickel
---
12.40
0.025
420
Selenium
---
419
0.008
100
Zinc
---
6I..80
0.124
7,500
Waypoint Analytical 19-346-0005
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:.
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
♦ E
WHICOx&mabe
Prepared By: SOIL SOLUTIONS

Waypointo
ANALYTICAL
12/20/2019
Bio-Nomic Service Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-346-0005
Project Description: GUC-6
7621 Whitepine Road, Ricbmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 12/12/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
&. Mc.7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

0Wy
ayP-oint7621 ain 80 -7 Road,Richmond,27 -6446 {rMain 804-743-9401 -Fax [phone]
ANALYTICAL www.waypointanalyticahcom
Sample Summary Table
Report Number: 19-346-0005
Client Project Description: GUC-6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
WTN: Waypoint Analytical - TN, Memphis, TN
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
SM-254OG
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
9056A
WTN
AOAC 955.01
WTN
Page 2 of 7

(D
Waypoint.,
ANALYTICAL
45671
Bic-Nomic Servics Inc
Joel Ccert
530 Wcodlawn St
Belmont, NC 28012
Report Number:19-346-0005
Lab No : 69881
Sample ID: GUC-6
Project GUC-6
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9461 ° Fax [phone]
www.waypoi ntanalytical.com
REPORTOFANALYSTS
Report Date : 12/20/2019
Received: 12/12/2019
PW« me (fawr
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 12/11/2019 7:44
Test
Results Units MQL DF Date/Time
By
Analytical
Analyzed
Method
Moisture
83.5 % 0.010 1 12116/1918:11
ADM
SM-2540G
Calcium Carbonate Equivalent
8.4 % - dry 0.1 1 12/17/19 09:33
DXT
AOAC 955.01
Test Results, Units MQL DF Date l Time By Analytical
Analyzed Method
Ammonia Nitrogen
<606
mg/Kg - dry
606
1
12/18/19 09:00
JPJ
SM-4500-NH3C
Chloride
89.7
mg/Kg - dry
24.2
1
12/18/19 17:47
OCR
9056A
Nitrate+Nitrite-N
<30.3
mg/Kg - dry
30.3
1
12/17/19 15:06
ZBD
4500NO3F-2011
Organic N
16200
mg/Kg - dry
1520
1
12/16/19 09:00
CALCULATION
pH
6.5
S.U.
1
12/16/19 07:16
JSL
9045D
Total Solids
16.5
%
0.010
1
12/16/19 18:11
ADM
SM-2540G
Total Volatile Solids
45.5
%
0.010
1
12/16/19 18:11
ADM
SM-2540G
Total Kjeldahl Nitrogen
16200
mg/Kg - dry
1520
1
12/16/19 09:00
JPJ
i11-4500-NH3C-TKP
Phosphorus
3160
mg/Kg - dry
30.3
1
12/17/19 01:37
BKN
6010D
Aluminum
139000
mg/Kg - dry
303
10
12/17/19 13:49
KKM
6010D
Arsenic
16.4
mg/Kg - dry
3.03
1
12/17/19 01:37
BKN
6010D
Calcium
1920
mg/Kg - dry
152
1
12/17/19 01:37
BKN
6010D
Cadmium
<0.606
mg/Kg - dry
0.606
1
12/17/19 01:37
BKN
6010D
Chromium
60.4
mg/Kg - dry
1.52
1
12/17/19 01:37
BKN
6010D
Copper
368
mg/Kg - dry
1.52
1
12/17/19 01:37
BKN
6010D
Iron
35400
mg/Kg - dry
30.3
1
12/17/19 01:37
KKM
6010D
Qualifiers/ B
Analyte detected in blank
OF
Dilution Factor
Definitions L
Limit Exceeded
MQL
Method Quantitation
Limit
Page 3 of 7

Waypoint.,
ANALYTICAL
45671
Bio-Nomic Service Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Report Number:19-346-0005
Lab No: 69881
Sample ID: GUC-6
7621 W hitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project GUC-6
Information :
REPORTOFANALYSIS
Report Date: 12/20/2019
Received : 12/12/2019
Pw« m° 60bwr
Paudc McGtoary
Agronomist
Matrix: Solids
Sampled: 12/11/2019 7:44
Test
Results
Units
MQL
DF
Date I Time
Analyzed
By
Analytical
Method
Lead
23.4
mg/Kg - dry
1.82
1
12/17/19 01:37
BKN
6010D
Magnesium
559
mg/Kg - dry
30.3
1
12/17/19 01:37
BKN
6010D
Manganese
812
mg/Kg - dry
3.03
1
12/17/19 01:37
KKM
6010D
Mercury
0.510
mg/Kg - dry
0.0806
1
12/17/19 15:54
TJS
SW-7471B
Molybdenum
1.96
mg/Kg - dry
1.52
1
12/17/19 01:37
BKN
6010D
Nickel
12.4
mg/Kg - dry
1.52
1
12/17/19 01:37
BKN
6010D
Potassium
458 B
mg/Kg - dry
30.3
1
12/17/19 19:47
KKM
6010D
Selenium
4.19
mg/Kg - dry
3.03
1
12/17/19 01:37
BKN
6010D
Sodium
332
mg/Kg - dry
152
1
12/17/19 01:37
BKN
6010D
Zinc
61.8
mg/Kg - dry
7.56
1
12/19/1914:51
KKM
6010D
Sulfur
5480
mg/Kg - dry
30.3
1
12/17/19 01:37
BKN
6010D
Qualifiers/ B Analyte detected in blank
Definitions
OF Dilution Factor
Page 4 of 7

Waypo0 -
G)
ANALYTICAL
Client: Bio-Nomic Servics Inc
Project: GUC-6
Lab Report Number: 19-346-0005
Date: 12119/2019
7621 WhItepine Road, Richmond, VA 23237
Main 804-743-94010Fax [phone]
www.waypointanaly6ca I.com
CASE NARRATIVE
Metals Analysis Method 601OD
Sample 69881 (GUC-6)
Analyte: Potassium
QC Batch No: 1-46939211-468801
Target analyte(s) was identified in the method blank associated with this project. Per laboratory protocol any
associated affected sample result is flagged "B" to indicate that it was detected in the method blank.
Page 5 of 7

Wayp®int.
ANALYTICAL
7621 Whltepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-346-0005
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS Q Client 0 Courier
0 Other:
Thermometer ID:
�-
F_
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
1'
Custody seals intact on shipping container/cooler?
O Yes
0 No
Not Present
Custody seals intact on sample bottles?
O Yes
O No
Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
O No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
O No
All samples received within holding time?
0 Yes
O No
Cooler temperature in compliance?
0 Yes
O No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
Q No
Water - Sample containers properly preserved
Q Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
O No
N/A
Trip Blanks received with VOAs
0 Yes
O No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No
N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
[_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: jBrandi Watson Date & Time: 12/12/2019 14:20:19
Page 6 of 7

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--Testhkmerica
,
THE LEADER IN ENVIRONMENTAL_ TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
- Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-168891-1
Client Project/Site: Greenville WTP
Revision: 2
\ For:
Bio-Nomics Services., Inc.
— -- 530 Woodlawn Street
Belmont, North Carolina 28012
............. LINKS ............
Review your project
results through
TotaiAccess
Have a Question?
j-� As k
The
Ex ert
Visit us at:
www.testamericainc.coni -
Attn: Vaughn Stevenson
Authorized for release by:
3/19/2019 12:40:16 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
2
Sample Summary .........................................
3
Case Narrative ...........................................
4
Definitions ...............................................
5
Client Sample Results ......................................
6
QC Sample Results ........................................
8
QC Association ...........................................
20
Chronicle ................................................
24
Method Summary .........................................
25
Certification Summary ......................................
26
Chain of Custody ..........................................
27
Receipt Checklists .........................................
30
Page 2 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)

Sample Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Lab Sample 1D Client Sample ID
490-168891-1 GUC
Matrix
Sludge
TestAmerica Job ID: 490-168891-1
Collected Received
02/19/19 12:00 02/21/19 08:55
TestAmerica Nashville
Page 3 of 30
3/19/2019 (Rev. 2)

Case Narrative
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Job ID: 490-168891-1 _ __..
Laboratory: TestAmerica Nashville
Narrative
TestAmerica Job ID: 490-168891-1
92
Job Narrative
490-168891.1
REVISED REPORT: Revised to report Cyanide, Sulfide, and PCBs without dry weight conversion. This report replaces the one generated
on 03/08/19 @ 1653.
Comments
While TA Pittsburgh carries South Carolina certification for 8260D and 8270E, the referenced matrix "Sludge", is causing the report to
indicate the lab as not certified for these.
No additional comments.
Receipt
The sample was received on 2/21/2019 8:55 AM; the sample arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 3.00 C.
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-271299 was outside the method criteria for the
following analyte: 2-Butanone. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is
considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
GCIMS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 101 OA: Method 1010A is applicable only to liquid matrix. This method has been modified to incorporate soil/ solid matrices of the
following sample: GUC (490-168891-1).
Method 9034 Calc: Sample GUC (490-168891-1) was analyzed for Sulfide. Sulfide as. 1-12S level is calculated at 1303.8 mg/Kg.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Geotechnical
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
Method 351 OC: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271365.
Method 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271367.
Method 8151A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and.180-271391.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
TestAmerica Nashville
Page 4 of 30 3/19/2019 (Rev. 2)

Definitions/Glossary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Qualifiers
GC/MS Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL sntl the concentration is an approximate value _
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratoryat clients request. - - -
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFI_ Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
L00 Limit of Quantitation (DOD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NO Not Calculated
NO Not Detected at the reporting limit (or MOIL or EDL if shown)
PQL Practical Quanthation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
011
Page 5 of 30 3/19/2019 (Rev. 2)

Client Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Client Sample ID: GUC Lab Sample ID: 490-168891-1
Date Collected: 02/19/19 12:00 Matrix: Sludge
Date Received: 02/21/19 08:55
Method: EPA 8260D - Volatile Organic Compounds by GCIMS - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
oil Fac
1,1-DiDichloroethene
ND
0200 _
mg/L
0228/1909:23
1
1,2-Dichloroethane
ND
0.200
mg/L
02/2611909:23
1 -
2-Butanone (MEK)
ND
0.200
mg/L
02/26/19 09:23
1 -
Benzene
ND
0.200
mg/L
02/26/19 09:23
1
Carbon tetrachloride
ND
0.200
mg/L
02/26/19 09:23
1
Chlorobenzene
ND
0200
mg/L
02/26/19 09:23
1
Chloroform
ND
0.200
mg1L
02/26/19 09:23
1
Tetrachloroethene
ND
0.200
mg/L
02126/1909:23
1
Trichlomethene
ND
0.200
mg1L
02/26/19 09:23
1
Vinyl chloride
ND
0.200
mg/L
02126119 09:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
DU Fac
1,2-Dichlooethane-d4(Sun)
89
73_143_
022611909:23
1
4-Bromofluombemene (Surf)
81
61.123
0226/19 09.23
1
Dibromofluoromethane(Sun)
106
68-128
0212611909.23
1
Toluene-d6 (Surr)
100
75-124
02/26/19 09:23
1
Method: 8270E - Semivolatile Organic Compounds (GCIMS) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
oil Fac
1,4-Dichlorobenzene
ND
0.0500
mg/L
02126/1912:10
0227/1917:24
1
2,4,5-Trichlorophenol
NO
0.0500
mg/L
02/26/1912:10
02127/1917:24
1
2,4,6-Trichlorophenol
ND
0.0500
mg1L
02/2611912:10
02127/1917:24
1
2,4-Dinitrololuene
ND
0.0500
mg1L
02126119 12:10
02127/1917:24
1
Hexachlorobenzene
ND
0.0500
mg1L
02I26/1912:10
022711917:24
1
Hexachlorobuladiene
ND
0.0500
mg/L
02/26/19 12:10
02127119 17:24
1
Hexachloroethane
ND
0.0500
mg/L
02/26/19 12:10
02127/19 17:24
1
Nitrobenzene
ND
0.0500
mg/L
02/261191210
0212711917:24
1
Pentachlorophenol
ND
0.250
mg/L
02/26/1912:10
02/27/1917:24
1
I Pyridine
ND
0.100
mg/L
02126/1912:10
0212711917:24
1
Cresols
ND
0.100
mg/L
0212611912:10
0212711917,24
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tdtiromopheno1(Sure)
76
25_192
022611912:10
022711917:24
1
2-Fluorophenol (Surr)
91
61.105
0226119 12:10
0227119 17:24
1
2-Fluorobiphenyl
93
62-105
022611912.10
022711917:24
1
Nitrobenzene-d5(Surr)
94
64-105
022611912:10
022711917,24
1
Phenol-d5(Sun)
85
47-105
0P26/1912:10
0227/1917:24
1
''. Terpheny/d14(Sufr)
84
45-130
022611912:10
022711917:24
1
Method: EPA 8081 B - Organochlodne
Pesticides
(GC) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
oil Fac
Chlordane (technical).
ND
0.00500
mg/L
6026/19 11:00
02/27/19 16:03
- 1
Endrin
ND
0.000500
mg1L
02/26119 11:00
02/27/19 16:03
1
gamma-BHC (Lindane)
ND
0.000600
mglL
M26/19 11:00
0227/19 16:03
1
Heptachlor
ND
0.000500
mg/L
0212611911:00
022711916:03
1
Heptachlor epoxide
ND
0.000500
mg1L
02/26/1911:00
0227/1916:03
1
Methoxychlor
ND
0.000500
mg/L
02/26/1911:00
02/27/1916:03
1
Toxaphene
ND
0.0400
mg/L
02126/1911:00
02/2711916:03
1
TestAmerica Nashville
Page 6 of 30 3/19/2019 (Rev. 2)

Client Sample Results
Client; Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Client Sample ID: GUC
Lab Sample ID: 490-1688-91-1
Date Collected: 02119/19 12:00
Matrix: Sludge
Date Received: 02/21/19 08:55
Surrogate %Recovery Qualifier Limits
Prepared Analyzed Dil Fac
j DCB Decachlorobiphenyl (Sufi) 95 - 62-150
0226/19 11:00 022711 116:03 1
Tetrachloro-m-xylene 91 54-139
0212611911:00 02/27/1916:03 I
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Analyte
Result Qualifier
RL
MDL Unit
_
D Prepared
Analyzed
oil Fac
PCB-1016
ND
6 4
ug/Kg
02127/1 009:52
02/28/1 115:46
1
PCB-1221
ND
16.4
ug/Kg
0227/19 09:52
02/28119 15A6
1
PCB-1232
ND
16.4
uglKg
02/27/19 09:52
02/28/19 15:46
1
PCB-1242
ND
16.4
ug/K9
02/27/19 09:52
02/28/19 15:46
1
PCB-1248
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB-1254
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB-1260
ND
16.4
u91Kg
02/27/19 09:52
02/2811915:46
1
I Surrogate %Recovery Qualifier
Tetrachloro-m-xylene (Sure) Bf51
DCB Decachlorobiphenyl (Surf) 87
Method: EPA 8151A - Herbicides (GC) - TCLP
! Analyte Result Qualifier
-
Limits
_ 176
44-116
RL
MDL
Unit
D
Prepared
0227P19 09:52
02/27/19 09:52
Prepared
Analyzed
0228/19 15:46
0228119 15:48
Analyzed
Dil Fac
1
1
oil Fac
2,4-D
ND
0.0400
m91L
62/26/19 14:30
0226/19 01:14
20
Silvex (2,4,5-TP)
ND
0.0100
mg/L
02/26/19 14:30
02/28/19 01:14
20
2,4,5-T
ND
0.0100
mg/L
02/2611914:30
02/2811901:14
20
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
fill Fac
2,4Dlchlorophenylacetic aacid
_ - - 73
20-105
621611914:30
0228/190114
20
Method: EPA 601 OD - Metals
(ICP) - TCLP
j Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
Arsenic -
ND
0.500
mg/L
-
62/26/19 1220
02/27119 09:13
1
Barium
ND
2.00
mglL
02126/191220
02127/1909:13
1
Cadmium
ND
0.500
mg/L
0226/19 12:20
02/27/19 09:13
1
j Chromium
ND
0.500
mg/L
02126/1912:20
02127/1909:13
1
Lead
ND
0.500
mg/L
02126/191220
=27/1909:13
1
Selenium
ND
0.500
mg/L
02/26/19 12:20
02/271190913
1
Silver
ND
0.500
mg/L
02/26/19 12:20
02/27/19 09:13
1
Method: EPA 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
Mercury
ND
0.000200
mg/L
0226I7911:05
02/2611916:17
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
Cyanide, Total _
ND
0.505
mglKg
03/01/19 12:40
63101/1919.32
1
Total Sulfide
31.7
30.0
mg/Kg
0226119 09:35
02/26/19 11:20
1
Analyte
Result Qualifier
RL
RL
Unit
D
Prepared
Analyzed
oil Fac
Flashpoint
->200
1.00
Degrees F
-
0-301119 17:29
1
Percent Moisture
97.4
0.1
%
02127119 08:43
1
Percent Solids
2.6
0.1
%
02/27/19 08:43
1
PH
6.6 HF
0.1
SU
02127/1912:00
1
TestAmerica Nashville
C
Page 7 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA mob - Volatile Organic Compounds by GC/MS
Lab Sample ID: LCS 180-271299/3 Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271299
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
t,1-Dichloroethene - _
0.0400
0.04011
mg/L
Too
57- 335
1,2-Dichloroethane
0.0400
0.03331
mg/L
83
69-127
2-Butanone(MEK)
0.0400
0.02829
mg/L
71
_
36-150
Benzene
0.0460
0.04064
mg/L
102
66-124
Carbon tetrachloride
0.0400
0.04205
mg/L
105
69-130
Chlorobenzene
0.0400
0.04443
mg/L
Ill
72-122
Chloroform
0.0400
0.03950
mg/L
99
69-119
Tetmchloroelhene
0.0400
0.04642
mg/L
116
73-129
Trichloroelhene
0.0400
0.04744
mg/L
119
75-122
Vinyl chloride
0.0400
0.03919
mg/L
98
57 -132
LCS LCS
Surrogate %Recovery Qualifier
1,2-Dichloroethane-d4 (Sun) 80
4-Bromotluombenzene (Sum) 97
Dibromofluoromethane (Surr) 105
Toluene-0 (Surr) 103
Lab Sample ID: LB 180-27131211-A
Matrix: Solid
Analysis Batch: 271299
Limits
73-143
61-123
68-128
75-124
Client Sample ID: Method Blank
Prep Type: TCLP
LB LB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
oil Fac
1,1-Dichloroethene
ND
0.0500
mglL
02/26/19 09:01
1
1,2-Dichloroethane
NO
0.0500
mg/L
02/26/19 09:01
1
2-Butanone(MEK)
NO
0,0500
mg/L
02/26/19 09:01
1
Benzene
NO
0.0500
mg/L
02/2611909:01
1
Carbon tetrachloride
NO
0.0500
mg/L
02/2611909:01
1
Chlorobenzene
NO
0.0500
mg/L
02/26/19 09:01
1
Chloroform
NO
0.0500
mg/L
02/26119 09:01
1
Telrachlomethene
NO
0.0500
mg/L
02/26/19 09:01
1
Tdchloroethene
NO
0.0500
mg/L
02126/19 09:01
1
Vinyl chloride
NO
0.0500
mg/L
02/26/19 09:01
1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
DU Fac
1,2-Dichloroethane-d4(Surr)
--- 85
73-143
-
02r26/1909:01
I
4-Bromotluorobenzene (Surr)
82
61-123
02/26/19 09:01
f
Dibromofluoromethane(Sum)
102
68-128
0212611909:01
1
Toluene-0 (Surr)
104
75-124
02/26/19 09:01
1
Lab Sample ID: 490-168891-1
MS
Client
Sample ID: GUC
Matrix: Sludge
Prep Type:
TCLP
Analysis Batch: 271299
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
1,1-Dichloroethene
ND
1.80
1.556
mg/L
97
57-135
1,2-Dichloroethane
NO
1.60
1.409
mg/L
88
69-127
2-Butanone(MEK)
NO
1.60
0,8771
mglL
55
38-150
TestAmerica Nashville
Page 8 of 30
3/1912019 (Rev. 2)

QC Sample Results
Client: Bic-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: 490-168891-1 MS
Client Sample ID:
GUC
Matrix: Sludge
Prep Type:
TCLP
Analysis Batch: 271299
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit D
%Rec
Limits
� Benzene
ND
1.60
1.613
mgg/L - - -
101
66-124
Carbon tetrachloride
ND
1.60
1.711
mg/L
107
69-130
-
Chlorobenzene
ND
1.60
1.768
mg/L
111
72-122
Chloroform
ND
1.60
1.638
mg/L
102
69-119-
1 Tetrachloroelhene
ND
1.60
1.815
mg/L
113
73-129
Trichloroethene
ND
1.60
1M9
mg/L
117
75-122
Vinyl chloride
ND
1.60
1.383
mg/L
66
57-132
MS MS
Surrogate
%Recovery Qualifier
Limits
, 1,2-Dichloroef6ane-d4 (Surr)
85 _
73-143
4-Bromofluorobenzene (Surr)
96
61-123
Dibromofluoromethane (Surr)
104
68-128
Toluene-d8 (Surr)
101
75 -124
Lab Sample ID: 490-168891-1 MSD
Client Sample ID:
GUC
Matrix: Sludge
Prep Type:
TCLP
Analysis Batch: 271299
Sample Sample
Spike
MSD MSD
%Rec.
RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit D
%Rec
Limits RPD
Limit
1,1-Dichloroethene -
ND
- 1.60
-- 1702 - -
mglL
106
57-135 9
35
1,2-Dichioroethane
ND
1.60
1.434
mg/L
90
69-127 2
16
2-Butanone(MEK)
ND
1.60
0,9013
mg/L
56
36-150 3
35
Benzene
ND
1.60
1.638
mg/L
102
66-124 2
16
Carbon tetrachloride
ND
1.60
1.689
mg/L
106
69-130 1
17
Chlorobenzene
ND
1.60
1.798
mg/L
112
72-122 2
15
Chloroform
ND
1.60
1.639
mg/L
102
69-119 0
16
Tetrachloroethene
ND
1.60
1.882
mg/L
118
73-129 4
15
Trichloroethene
ND
1.60
1.879
mg/L
117
75-122 1
15
Vinyl chloride
ND
1.60
1.558
mg/L
97
57-132 12
21
MSD MSD
Surrogate
%Recovery Qualifier
Limits
1,2-Dichioroethane-d4 (Surr)
87
- 73. 143
4-Bromofluorobenzene (Surr)
99
61-123
Dibromofluoromethane (Sum)
106
68 -128
Toluene-d8 (Surr)
105
75-124
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 180-271367/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
I'
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed oil Fac
1,4-Dichlorobenzene
ND
0.0500
mg/L
0026iff 12,10 02127119 09:11 1
2,4,5-Trichlorophenol
ND
0.0500
mg/L
02/26/19 12:10 02/27/19 09:11 1
2,4,6-Trichlorophenol
ND
0.0500
mg/L
02/26/19 12:10 02/27/19 09:11 1
2,4-Dinitrotoluene
ND
0.0500
mg/L
02/26/19 12:10 02/27/19 09:11 1
TestAmerica Nashville
Page 9 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 180-271367/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed Oil Fac
Hexachlorobenzene
ND
0.0500
mglL
- -
02/26l19 12:10
6201190911 1
Hexachlorobutadiene
ND
0.0500
mg/L
02/26/1912:10
02/27/1909,11 1
Hexachloroelhane
ND
0.0500
mg/L
02/2611912:10
0212711909:11 1
Nitrobenzene
ND
0.0500
mg/L
02126/1912:10
02/27/1909:11 1
Pentachlorophenol
ND
0.250
mg/L
02126/1912:10
02/27/1909:11 1
Pyridine
ND
0.100
mg/L
02/26/19 12:10
02/27/19 09:11 1
Cresols
ND
0.100
mg/L
02126/1912:10
02/2711909:11 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4,6-Tribromophenol(Surr) -- --
63 -
---25-112-
02/26/1912:10
02YY27/1909: 17 1
2-Fluorophenol (Sun)
67
61-105
02/26/19 12:10
02/27/19 09:11 1
2-Fluorobiphenyl
83
62-105
0212611912:10
022711909:11 1
Nitrobenzene-d5(Surr)
63
64-105
0212611912: 10
02/27/1909,11 1
Phenol-d5(Surr)
66
47-105
0212611912:10
02/27/1909:11 1
Terphenyl-d14(Sum)
75
45-130
02/26/1912: 10
0212711909:11 1
Lab Sample ID: LCS 180-271367/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
Spike
LCS LCS
/Rea.
Analyte
Added
Result Qualifier
Unit
D %Rea
Limits
1,4-Dichlorobenzene
0.250
0.2277
mg/L
- 91
-57--100
2,4,5-Trichlorophenol
0.250
0.2157
mg/L
86
58-100
2,4,6-Trichlorophenol
0.250
0.2096
mg/L
84
57-100
2,4-Dinitrotoluene
0.250
0.2023
mg/L
81
40-100
Hexachlorobenzene
0.250
0.1527
mg/L
61
38-100
Hexachlorobutadiene
0.250
0.2146
mg/L
86
53-105
Hexachloroethane
0.250
0,2352
mg/L
94
57-100
Nitrobenzene
0.250
0.2299
mg/L
92
56-103
Pentachlorophenol
0.250
0.1630 J
mg/L
65
16-100
Pyridine
0.250
0.2391
mg/L
96
51 -107
Cresols
0.750
0.6754
mg/L
90
54 -103
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
2,4,6-Tribromophenol(Surr) 66
25-112
2-Fluorophenol (Surr) 90
61-105
2-Fluorobiphenyl 66
62-105
Nitrobenzene-d5 (Surr) 90
64-105
Phenol-d5 (Surr) 90
47-105
Terphenyl-d14 (Surr) 69
45-130
Lab Sample ID: LCSD 180-27136713-A
Matrix: Solid
Analysis Batch: 271438
Analyte
1,4-Dichlarobenzene
2,4,5-Trichlorophenol
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 271367
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rea Limits RPD Limit
- - 0.250 0.2220 - mgf- 89 57- 100 3 16
0.250 0.2095 mg/L 84 58-100 3 16
TestAmerica Nashville
Page 10 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method _8noE - SemIvolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 180-271367/3-A
Client Sample ID:
Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier Unit D %Rec
Limits RPD Limit
2,4,6-Trichlorophenol
0.250
0,2135
mg/L
85
57-100 2 15
2,4-Dinitrotoluene
0.250
0.1977
mg/L
79
40-100 2 15
Hexachlombenzene
0250
0.1553
mg/L
62
38-100 2 16
Hemchlorobutadiene
0.250
0.2085
mg1L
83
53.105 3 15
Hexachloroethane
0.250
0.2259
mg/L
90
57-100 4 18
Nitrobenzene
0.250
0.2141
mglL
86
56-103 7 15
Pentachlorophenol
0.250
0.1462 J
mg/L
58
16-100 11 24
Pyddine
0250
0.2257
mg1L
90
51-107 6 18
Cresols
0.750
0.6719
mg/L
90
54-103 1 17
Surrogate
LCSD LCSD
%Recovery Qualifier
2,4,6-Tnhromophenol (Sun)
86
2-Fluorophenol (Surr)
66
2-Fluorobipheny/
86
Nitrobenzene-d5 (Surr)
84
PhenoW5 (Sun)
Be
TerphenyW14 (Sun)
68
Limits
25-112
61-105
62-105
64-105
47-105
45-130
1 Lab Sample ID: LB 180-271274/1-D Client Sample ID: Method Blank
Matrix: Solid Prep Type: TCLP
Analysis Batch: 271438 Prep Batch: 271367
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
oil Fac
`1,4-Dichlorobenzene
- NO
0.0500
_ mg%L
02/26/19 12:10
02127/19 11:33
1
2,4,5-Trichlorophenol
NO
0.0500
mg/L
02126/1912:10
0212711911:33
1
2,4,6-Trichlorophenol
NO
0.0500
mg/L
02/26/19 12:10
02/27/19 11:33
1
2,4-Dinitrotoluene
NO
0-0500
mg/L
02/26/19 12:10
02/27/19 11:33
1
Hemchlorobenzene
NO
0.0500
mg1L
02/26/19 12:10
02t27/19 11:33
1
Hexachlorobutadiene
NO
0.0500
mg/L
02/20/19 12:10
02127/19 11:33
1
Hexachloroethane
NO
0.0500
mg/L
02/26/19 12:10
0212711911:33
1
Nitrobenzene
NO
0.0500
mg1L
0212611912:10
02127/1911:33
1
Pentachlorophenol
NO
0.250
mg/L
02/26/19 12:10
02127/19 11:33
1
Pyridine
NO
0.100
mg1L
02/26/19 12:10
02/27/19 11,33
1
Cresols
NO
0.100
mg/L
02/26/19 12:10
02/27/19 11:33
1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tnbrom6phenol(Sun)
88
25-112
0226/1912:10
52 71711911r33
1
2-Fluorophenol (Surr)
85
61-105
02,26/19 12:10
02/27/19 11:33
1
2-Fluorobiphenyl
85
62-105
02/2611912:10
0212711911:33
1
Nitrobenzene-d5 (Sun)
87
64-105
02/26/19 12:10
02/27/19 1133
1
Phenol-d5 (Suq)
87
47-105
0226119 12:10
02127119 11:33
1
Terphenyl414 (Sun)
74
45-130
0226119 12:10
0227119 11:33
1
TestAmerica Nashville
Page 11 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Analyte
Chlordane (technical) -
Enddn
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogate
DCB Decachlorobiphenyl (Surf)
Tetrach/om-m xylene
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 8081 B - Organochlorine Pesticides (GC)
Lab Sample ID: MIS 180-271365/1-A
Matrix: Solid
Analysis Batch: 271475
MB its
Result Qualifier
ND
ND
ND
ND
ND
ND
ND
RL
0.00500
0.000500
0.000500
0.000500
0.000500
0.000500
0.0400
Me MB
%Recovery Qualifier Limits
94 62-150
91 54 -138
Lab Sample ID: LCS 180-271365/2-A
Matrix: Solid
Analysis Batch: 271475
Analyte
Enddn
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
TestAmerica Job ID: 490-168891-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271365
MDL Unit
D Prepared
Analyzed
Dil Fac
_ mg/L
02/26/1911-:00
02127/1913:14
1
mg/L
022611911:00
021271191314
1
mg/L
0226/1911!00
02/2711913:14
1
mg/L
02126/1911:00
02/2711913:14
1
mg/L
0226/1911:00
02/27/1913:14
1
mg/L
0226/1911:00
02/27/1913:14
1
mg/L
02/26/1911:00
02/27/1913:14
1
Prepared
Analyzed
Dil Fac
02126119 11:56
0227/1913.14
1
0212611911:00
022711913:14
1
Spike
LCS LCS
Added
Result Qualifier
0.0100
0.009 224
0.0100
0.008481
0.0100
0.009290
0.0100
0.008870
0.0100
0.01001
LCS LCS
Surrogate %Recovery Qualifier Limits
! DCB Decachlorobiphenyl r§w 95 62-150
Tetrachlom-m-xylene 96 54-138
Lab Sample ID: LCSD 180-271365/3-A
Matrix: Solid
Analysis Batch: 271475
Spike
LCSD LCSD
Analyte
Added
Result Qualifier
Enddn
_
0.0100
- 0.009900
gamma-BHC (Lindane)
0.0100
0.008743
Heptachlor
0.0100
0.009428
Heptachlor epoxide
0.0100
0.008791
Methoxychlor
0.0100
0.009889
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
DCB Decachloroblphenyl (Surf)
95
62-150
Tetmchloro-m-xylene
93
54-138
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271365
%Rec.
Unit
D %Rec
Limits
m9/L
99
71 _ 134
mglL
85
66-127
mg/L
93
66-134
mg/L
89
65-141
mg/L
100
59-131
Client Sample ID:
Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 271365
%Rec. RPD
Unit D %Rec
Limits RPD Limit
mg%L -- --- -- --
99
71 -134- -- 0 18
mg/L
87
66 -127 3 15
mg/L
94
66 -134 1 15
mg/L
88
65-141 1 15
mglL
99
59-131 1 28
TestAmerica Nashville
Page 12 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA 8081 B - rganochlorine Pesticides (GC) (Continued)
Lab Sample ID: LB 180-271274/16-E
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271475
Prep Batch: 271365
LB LB
Analyte
Result Qualifier
RL
MDL Unit
_ -
D Prepared
Analyzed oil Fac
Chlordane (technical)
ND
0 M500
mg/L
02126119 11 W
02/21/19 1415 - 1
Enddn
NO
0.000500
mg/L
02/26/1911:00
02/27/191415 1
gamma-BHC (Lindane)
ND
0.000500
mg/L
02126/19 11:00
02/27119 14:15 1 _
Heptachlor
ND
0.000500
mg/L
02126/19 11:00
0212711914:15 1
Heptachlor epoxide
No
0.000500
mg/L
02126/19 11:00
02/27/19 14:15 1
Methoxychlor
ND
0.000500
mg/L
02/26/19 11:00
02127119 14:15 1
Toxaphene
NO
0.0400
mg/L
02/26/19 11:00
02/27119 14:15 1
LS LB
Surrogate
%Recovery Qualifter
Limits
Prepared
Analyzed oil Fac
DCBDecachlorobiphenyl(Sun)
98
62-150
50W19 11.00
6212711914:15 1
Tetrachlom-m-xylene
92
54_138
022611911:00
02,2711914:15 1
Method: EPA 80$2A - Polychlorinated Biphenyis (PCBs) by Gas Chromatography
Lab Sample ID: MB 180-271476/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271567
Prep Batch: 271476
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed oil Far
PCB-1016 _
NO
66.7
------
uglKg
62/27/19 09:52
0228/19 13:54 1
PCB-1221
ND
16.7
ug/Kg
02/27/1909:52
02/2811913:54 1
1 PCB-1232
ND
16.7
ug/Kg
0212711909:52
02/2811913:54 1
PCB-1242
ND
18.7
ug/Kg
02/27/19 09:52
02128/19 13:54 1
PCB-1248
NO
16.7
ug/Kg
02/27/19 09t52
02/28119 13:54 1
PCB-1254
NO
16.7
ug/Kg
02/2.7/19 09:52
02128/19 13:54 1
PCB-1260
ND
16.7
ug/Kg
0227/19 09;52
02/28/19 13:54 1
MB MB
Surrogate
%,Recovery Qualifier
Limits
Prepared
Analyzed OR Fac
Tetrachloro-m-xylene (Surr)
91
51-116
0&27119 09:52
0228119 33:54 1
l DCB Decachlorobiphenyl (Sun)
94
44-116
0227119 09:52
0212W913.54 1
Lab Sample ID: LCS 180-271476/2-A
Client Sample ID:
Lab Control Sample
Matrix; Solid
Prep Type: Total/NA
Analysis Batch: 271567
Prep Batch: 271476
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier Unit
D %Rec
Limits
PCB-1016 -- -----
- _ - -
1330
1090 -- uglk6
82
57-114 — - -
I PCB-1260
1330
1059 ug/Kg
79
55-112
LCS LCS
Surrogate %Recovery Qualifier
Limits
Tetmchloro--m-xylene (Surr)
85
51-116
DCB Decachlorobiphenyl (Surf)
67
44-116
TestAmerica Nashville
Page 13 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Lab Sample ID: 490-168890-B-1-J MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271567
Prep Batch: 271476
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
PCBd016 ND
1330
908.3 uglKg
68 57_114
PCB-1260 ND
1330
933.1 ug/Kg
70 55-112
MS MS
Surrogate %Recovery Qualifier
Tetrachloro-m-xylene (Suer)- 66
DCB Decach/orobiphenyl (Sun) 72
Lab Sample ID: 490-168890-B-1-K MSD
Matrix: Solid
Analysis Batch: 271567
Sample Sample
Analyte
Result Qualifier
PCB-1016 _ — - - ---
-- --ND - -- —
PCB-1260
ND
MSD MSD
Surrogate %Recovery Qualifier
Tefrachloro-m-xylene (Surrj 64
DCB Decachlorobiphenyl (Sun) 71
Method: EPA 8151A - Herbicides (GC)
Lab Sample ID: MB 180-271391/1-A
Matrix: Solid
Analysis Batch: 271555
Analyte
2,4 D
Silvex (2,4,5-TP)
2,4,5-T
Surrogate
2,4-Dichlorophenylacefic acid
Limits
51-116
44 - 116
Client Sample ID:
Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 271476
Spike
MSD MSD
%Rec. RPD
Added
Result Qualifier
Unit D %Rec
Limits RPD Limit
1290
.. __
in"
ug/Kg 64
57. 114 9 34
1290
837.2
ug/Kg 65
55-112 11 16
Limits
51-116
44-116
MB MB
Result Qualifier
RL
MDL Unit
ND
0.6400
- mg/L
ND
0.0100
mg/L
ND
0.0100
mg/L
MS MB
%Recovery Qualifier
Limits
--- 71
20-105
Lab Sample ID: LCS 180-271391/2-A
Matrix: Solid
Analysis Batch: 271555
Analyte
Silvex (2,4,5-TP)
2,4,5-T
LCS LCS
Surrogate %Recovery Qualifier
2,4-Dichlorophenylacefic acid 67
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch:271391
D Prepared Analyzed Dil Fac
02126/19 14:36 62/27119 20:57 20
02/26/19 14:30 02/27/19 20:57 20
02/26/19 14:30 02/27/19 20:57 20
Prepared Analyzed Dil Fac
02/26/19 14:30 62r27/19 20:57 20
Client Sample ID:
Lab Control Sample
Prep Type: Total/NA
Prep Batch:271391
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
0.200
0.1340
mg/L
- 67
10-100
0.0500
0.03454
mg/L
69
23 -109
0.0500
0.02981
mg/L
60
11 -101
Limits
20-105
TestAmerica Nashville
Page 14 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCSD 180-27139113-A
Matrix: Solid
Analysis Batch: 271555
Analyte
2,4-D
Silvex (2,4,5-TP)
2,4,5-T
Surrogate
2A-Dichlorophenylacetic acid
Spike
Added
---
0.200
0.0500
0.0500
LCSD LCSD
%Recovery Qualifer
Limits
M ---- --
-- 20-105
Lab Sample ID: LB 180-271274116-G
Matrix: Solid
Analysis Batch: 271555
LB LB
Analyte
Result Qualifier
RL
2,4-D
ND -
0.0400
Silvex (2,4,5-TP)
ND
0.0100
2,4,5-T
ND
0.0100
LB LB
Surrogate
%Recovery Qualifier
Limits
2,4-Dichlorophenylacetic acid
- 60
--20_705
Method: EPA 6010D - Metals (ICP)
TestAmerica Job ID: 490-168891-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch:271391
LCSD LCSD
%Rec. RPD
Result Qualifier Unit
D %Rec
Limits RPD Limit
0.1578
mglL _
- 79
10.700 16 35
0.04003
mg/L
80
23.109 15 35 -
0.03558
mg/L
71
11 -101 18 35 '
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch:271391
MDL Unit
D Prepared
Analyzed
Dil Fac
- — mg/L - - -
- - 02/26/19 t4:30
02 wls 22:24
20
mg/L
02/26/19 14:30
02/27/19 22:24
20
mg/L
02/26/19 14:30
02/27/19 22:24
20
Prepared
Analyzed
Dil Fac
02/2019 14:30
02727/19 22:24
20
Lab Sample ID:
MB 180-27135511-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch:
271499
Prep Batch: 271355
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Arsenic _
- - - -
ND
0.0500
-
mg/L
62/26/1912:20
02/27/19075_0 1
Barium
ND
0.200
mg/L
02/26/19 12:20
02/27/19 07:50 1
Cadmium
ND
0.0500
mg/L
02/26/19 12:20
02/27/19 07:50 1
Chromium
ND
0.0500
mg/L
02/26/19 12:20
02/27/19 07:50 1
Lead
ND
0.0500
mg/L
02/26/19 12:20
02/27/19 07:50 1
Selenium
ND
0.0500
mg/L
02/26/19 12:20
02/27/19 07:50 1
Silver
ND
0.0500
mg/L
02/26119 12:20
02/27/19 07:50 1
Lab Sample ID:
LCS 180-271355/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch:
271499
Prep Batch: 271355
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Arsenic_ -—
-�— -� ��
--0.500
-- -
0.5281
mglL
106
80-120
Barium
2.00
2.051
mg/L
103
80-120
Cadmium
0.0500
0.05449
mg/L
109
80-120
Chromium
0.200
0.2054
mg/L
103
80-120
Lead
0.500
0.5102
mg/L
102
80.120
Selenium
0.500
0,5558
mg/L
Ill
80-120
Silver
0.0500
0.05381
mg/L
108
80.120
TestAmerica Nashville
Page 15 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 6010D - Metals (ICP) (Continued)
Lab Sample ID: LB 180-27127411-C
Matrix: Solid
Analysis Batch: 271499
LB LB
Analyte
Result Qualifier
RL
MDL Unit
Arsenic - -
ND
- 0.506
mg%L
Barium
ND
2.00
mg/L
Cadmium
ND
0.500
mg/L
Chromium
ND
0.500
mg/L
Lead
ND
0.500
mg/L
Selenium
ND
0.500
mg/L
j Silver
ND
0.500
mg/L
Method: EPA 7470A - Mercury
(CVAA)
Lab Sample ID: MB 180-271342/1-A
Matrix: Solid
Analysis Batch: 271395
TestAmerica Job ID: 490-168891-1
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch:271355
D Prepared
Analyzed
Dil Fac
-- 02/26/19 12:26
02/27/19
08:00
1
02/26/19 12:20
02/27/19
08:00
1
02/26/19 12:20
02/27/19
08:00
1
L.'.
02/26/19 12:20
02/27/19
08:00
1
02/26/19 12:20
02/27/19
08:00
1
02/26/19 12:20
02/27/19
08:00
1
02/26/19 12:20
02/27/19
08:00
1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271342
MB MB
Analyte Result Qualifier
RL MDL Unit D Prepared Analyzed oil Fac
Mercury - - _- ND -
- 0.000200 mg/L 02/26/19 11:05 02/26/1916:00 - 1
Lab Sample ID: LCS 180-271342/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271395
Prep Batch: 271342
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
Mercury
0.00250
0.902606 _ mg%L --- 104 60-120-
Lab Sample ID: LB 180-271274/1-B
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
LB LB
Analyte Result Qualifier
RL MDL Unit D Prepared Analyzed Dil Fac
Mercury - _ - ND -
- o.b00200 rn / - - 02/26/19 11:05 62/26/19 16:02 1
Lab Sample ID: 180-86915-A-1-1 MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample Sample
Spike
MS MS %Rec.
I Analyte Result Qualifier
Added
Result Qualifier Unit D %Rec Limits
Mercury ND --
0.065 00
0.005020 mg/L 100 75-125
Lab Sample ID: 180-86915-A-1-J MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample Sample
Spike
MSD MSD %Rec. RPD
Analyte Result Qualifier
Added
Result Qualifier Unit D %Rec Limits RPD Limit
- -_ _ __
Mercury ND —
0.00300
_ ___ ___ __
- 0.005026 - mg/L__ vol 75-125_ ____ _ 0 -20
TestAmerica Nashville
Page 16 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: 1010A - Ignitability, Pensky-Martens Closed -Cup -Method
Lab Sample ID: MB 490-578372/1 Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 578372
Analyte
Flashpoint
MB MB
Result Qualifier
_ .i200
Lab Sample ID: LCS 490-578372/2
Matrix: Solid
Analysis Batch: 578372
RL RL Unit D Prepared Analyzed Dil Fac
1.00 Degrees - 03/01 /1917:29 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
'i Flashpoint - -
81.0
81.20
Degrees F
100 94 -106
Lab Sample ID: LCSD 490-578372114
Client
Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
Spike
LCSD LCSD
%Rec. RPD
1 Analyte
Added
Result Qualifier
Unit
D %Rec Limits RPD Limit
Flashpoint _
_ 81.0
83.40
Degrees F
_ 103 94�108 3 20
1 Lab Sample ID: 280-120182-A-1 DU
Client Sample ID: Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
Sample Sample
DU DU
RPD
Analyte Result Qualifier
Result Qualifier
Unit
D RPD Limit
Flashpoint - _- - - 128
- -
- 134.3
Degrees F
5 10
Method: 254OG - SM 2540G
Lab Sample ID: 180-86358-B-20 DU
Client Sample ID: Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271450
Sample Sample
DU DU
RPD
Analyte Result Qualifier
Result Qualifier
Unit
D RPD Limit
P—ercentMoist-ure—- 28.5
--__.-
28.2
%
- 6 10
Percent Solids 73.5
71.8
%
2 10
Method: EPA 9012B - Cyanide, Total andor Amenable
Lab Sample ID: MB 180-271760/4-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
MB MB
Analyte Result Qualifier
RL
MDL Unit
D
Prepared Analyzed Dil Fac
Cyanide, Total ND
- 0.500
mg/Kg
03/01/191240 03/01/1919:23 1
Lab Sample ID: HLCS 180-27176012-A
Client
Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Spike
HLCS HLCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
Cyanide, Total
0.250
0.2479 _ -
mg/Kg --
- 99 90-110
TestAmerica Nashville
Page 17 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 901213- Cyanide, Total andor Amenable (Continued)
TestAmerica Job ID: 490-168891-1
Lab Sample ID:
LCS 180-271760/3-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch:
271809
Prep Batch: 271760
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Cyanide, Total
.-
---190 ---
-174.2 -_---- -
mg/Kg -- - _-- 60 26-139
Lab Sample ID:
LLCS 180-27176011-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch:
271809
Prep Batch: 271760
Spike
LLCS LLCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Cyanide, Total
-
0.0500
- 0.04970
mg/Kg 99 90 -110
Lab Sample ID:
180-87076-D-1-B MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: Total/NA
Analysis Batch:
271809
Prep Batch: 271760
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits
Cyanide, Total
0.655
5.05
.--- 5.182 -
mg/Kg .90 75-125
Lab Sample ID:
180-87076-D-1-C MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch:
271809
Prep Batch: 271760
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Cyanitle, Total
0.659
5.05
5.263
mg/Kg - _ 91 _75-125 2 20
Method: EPA
9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID:
MB 180-271319/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch:
271334
Prep Batch: 271319
MB MB
Analyte Result Qualifier
Total Sulfide -_-- -ND
Lab Sample ID: LCS 180-271319/2-A
Matrix: Solid
Analysis Batch: 271334
Analyte
Total Sulfide
Lab Sample ID: 490-168890-B-1-C MS
Matrix: Solid
Analysis Batch: 271334
Sample Sample
Analyte Result Qualifier
Total Sulfide - 57.0
RL MDL Unit D Prepared Analyzed oil Fac
30.0 616% 02/26/19 09:35 02/26/19 11:15 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271319
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
150
144.3 ---
mg/Kg
-- 97
Client Sample
ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 271319
Spike
MS MS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
150
223.2 -
mg/Kg
17
75 -125
TestAmerica Nashville
Page 18 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA 9034 -Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: 490-168890-B-1-D MSD Client Sample ID: Matrix Spike Duplicate
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271334 Prep Batch: 271319
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Tolal Sulfde -- - 57.0 -149 209.1 mg/Kg 102 15-125 7 26
Method: EPA 9045D - pH
Lab Sample ID: LCS 180-271506/1 Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271506
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
__ -
PH 7.00 7.0 SU -- 101 99-101
Lab Sample ID: 180-86977-J-1 DU Client Sample ID: Duplicate
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271506
Sample Sample DU DU
Analyte Result Qualifier Result Qualifier Unit D
I pH - 3.6 736 SU
RPD
RPD Limit
0 2
TestAmerica Nashville
Page 19 of 30 3/19/2019 (Rev. 2)

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
GC/Ms-VOA
TestAmerica Job ID:490-168891-1
Analysis Batch: 271299
j Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
1 490-168891-1
GUC
-- TCLP
Sludge
EPA 8260D
271312
LB 180-27131211-A
Method Blank
TCLP
Solid
EPA 8260D
271312
LCS 180-271299/3
Lab Control Sample
TotaVNA
Solid
EPA 8260D
490-168891-1 MS
GUC
TCLP
Sludge
EPA 8260D
271312
490-158891-1 MSD
GUC
TCLP
Sludge
EPA 8260D
271312
Leach Batch: 271312
Lab Sample ID
Client Sample ID
490-168891-1
GUC
LB 180-27131211-A
Method Blank
490-168891-1 MS
GUC
490-168891-1 MSD
GUC
GCINNS Semi VOA
Leach Batch: 271274
Lab Sample ID
490-168891-1
LB 180-271274/1-D
L
Prep Batch: 271367
r
Lab Sample ID
Client Sample ID
GUC
Method Blank
Client Sample ID
490-168891-1
GUC ------
LS 180-27127411-D
Method Blank
MB 180-271367/1-A
Method Blank
LCS 180-27136712-A
Lab Control Sample
LCSD 180-27136713-A
Lab Control Sample Dup
Analysis Batch: 271438
Lab Sample ID
Client Sample ID
490-168891-1
GUC
LB 180-271274/1-0
Method Blank
MB 180-271367/1-A
Method Blank
LCS 180-271367/2-A
Lab Control Sample
LCSD 180-271367/3-A
Lab Control Sample Dup
GC Semi VOA
Leach Batch: 271274
Lab Sample ID
---- _
Client Sample ID
—
490-168891-1
----
GUC
li LB 180-271274/16-E
Method Blank
LB 180-271274/16-G
Method Blank
Prep Batch: 271365
Lab Sample ID
Client Sample ID
490-168891-1
GUC __ --
LB 180-271274116-E
Method Blank
MB 180-271365/1-A
Method Blank
:. LCS 180-2713652-A
Lab Control Sample
Prep Type Matrix Method Prep Batch a
TCLP
Sludge
EPA 1311
TCLP
Solid
EPA 1311
TCLP
Sludge
EPA 1311
TCLP
Sludge
EPA 1311
Prep Type
Matrix
Method Prep Batch
TCLP
Sludge
EPA 1311
TCLP
Solid
EPA 1311
Prep Type
Matrix
Method
Prep Batch
TCLP
Sludge
3510C
271274
TCLP
Solid
3510C
271274
TotaVNA
Solid
3510C
TotaVNA
Solid
3510C
Total/NA
Solid
3510C
Prep Type
Matrix
Method
Prep Batch
TCLP
Sludge
8270E
271367
TCLP
Solid
8270E
271367
Total/NA
Solid
8270E
271367
TotaVNA
Solid
8270E
271367
Total/NA
Solid
6270E
271367
Prep Type
Matrix
Method
Prep Batch
TCLP _-
Sludge --
EPA1311
TCLP
Solid
EPA 1311
TCLP
Solid
EPA 1311
Prep Type
Matrix
Method
Prep Batch
TCLP
Sludge
3570C-----�
---271274
TCLP
Solid
3510C
271274
Total/NA
Solid
3510C
TotaVNA
Solid
3510C
TestAmerica Nashville
Page 20 of 30
3/19/2019 (Rev. 2)

QC Association Summary
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
GC Semi VOA (Continued)
Prep Batch: 271365 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
[--LCSD 180-271365/3-A
Lab Control Sample Dup
Totel/NA
Solid
3510C
Prep Batch: 271391
Lab Sample lD __
Client Sample to
Prep Type
Matrix_
Method
Prep Batch
490-168891-1
GUC- -
TCLP
Sludge
- 8151A
271274
LB 100-271274/16-G
Method Blank
TCLP
Solid
8151A
271274
MB 180-27139111-A
Method Blank
TotaVNA
Solid
8151A
LCS 180-2713912-A
Lab Control Sample
Total/NA
Solid
8151A
L LCSD 180-27139113-A
Lab Control Sample Dup
TotaVNA
Solid
8151A
Analysis Batch:271475
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
EPA 8081B
271365
LB 180-271274/16-E
Method Blank
TCLP
Solid
EPA 8081B
271365
MB 180-271365/1-A
Method Blank
TotaVNA
Solid
EPA 8081B
271365
LCS 180-2713652-A
Lab Control Sample
Total/NA
Solid
EPA 8081B
271365
LCSD 180-27136513-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8081 B
271365
Prep Batch: 271476
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490.168891-1
GUC -
Total/NA
Sludge
3541
MB 180-271476/1-A
Method Blank
Total/NA
Solid
3541
LCS 180-271476/2-A
Lab Control Sample
TotaVNA
Solid
3541
490-168890-B-1-J MS
Matrix Spike
TotaVNA
Solid
3541
490-168890-B-1-K MSD
Matrix Spike Duplicate
Total/NA
Solid
3541
Analysis Batch:271555
Lab Sample ID _ _
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
_
Sludge
EPAB151A
271391
LB 180-271274/16-G
Method Blank
TCLP
Solid
EPA 8151A
271391
MB 180-27139111-A
Method Blank
Total/NA
Solid
EPA 8151A
271391
LCS 180-2713912-A
Lab Control Sample
TotaVNA
Solid
EPA 8151A
271391
LCSD 180-271391/3-A
Lab Control Sample Dup
TotaVNA
Solid
EPA 8151A
271391
Analysis Batch: 271567
Lab Sample ID
-
Client Sample to
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
Total/NA
Sludge
EPA 6082A
271476
MB 180-271476/1-A
Method Blank
Total/NA
Solid
EPA 8082A
271476
LCS 180-271476/2-A
Lab Control Sample
Total/NA
Solid
EPA 8082A
271476
490-168890-B-1-J MS
Matrix Spike
Total/NA
Solid
EPA 8082A
271476
j 490-168890-8-1-K MSD
Matrix Spike Duplicate
TotaVNA
Solid
EPA 8082A
271476
Metals
- -
Leach Batch: 271274
Lab Sample ID
-----
Client Sample ID
Prep Type.
Matrix
Method
Prep Batch
490-168891-7
GUC---------
TCLP - _--
Sludge—
------ EPA1311 -
-----
LB 180-271274/1-B
Method Blank
TCLP
Solid
EPA 1311
LB 180-27127411-C
Method Blank
TCLP
Solid
EPA 1311
180-86915-A-1-1 MS
Matrix Spike
TCLP
Solid
EPA 1311
TestAmerica Nashville
a
Page 21 of 30 3/19/2019 (Rev. 2)

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Metals (Continued)
Leach Batch: 271274 (Continued)
Sample ID
Client Sample ID
�Lab
180-86915-A-W MSD
Matrix Spike Duplicate
Prep Batch: 271342
rLab Sample ID
Client Sample 10
490-168891-1 -
GUC
LB 180-271274/1-B
Method Blank
MB 180-27134211-A
Method Blank
LCS 180-271342/2-A
Lab Control Sample
180-86915-A-1-1 MS
Matra Spike
180-86915-A-1-J MSD Matrix Spike Duplicate
Prep Batch: 271355
Lab Sample ID
Client Sample ID
490-168891-1
GUC
LB 180-27127411-C
Method Blank
MB 180-27135511-A
Method Blank
LCS 180-27135512-A
Lab Control Sample
Analysis Batch: 271395
Lab Sample to
Client Sample lD
490-168891-1
GUC
. LB 180-271274/1-B
Method Blank
MB 180-271342/1-A
Method Blank
LCS 180-271342/2-A
Lab Control Sample
180-86915-A-1-1 MS
Matrix Spike
180-86915-A-1-J MSD Matrix Spike Duplicate
Analysis Batch: 271499
Lab Sample ID
Client Sample ID
490-168891-1
GUC--- —
LB 180-271274/1-C
Method Blank
MB 180-271355/1-A
Method Blank
LCS 180-27135512-A
Lab Control Sample
General Chemistry
Prep Batch: 271319
Lab Sample 10
Client Sample ID
490-168891-1 _
GUC
MB 180-271319/1-A
Method Blank
LCS I BD-27131912-A
Lab Control Sample
490-168890-BA-C MS
Matrix Spike
490-168890-13-1-D MSD
Matrix Spike Duplicate
Analysis Batch: 271334
Lab Sample lD
Client Sample lD
490-168891-1
GUC
MB 180-271319/1-A
Method Blank
LCS 180-271319/2-A
Lab Control Sample
490-168890-B-1-C MS Matrix Spike
TestAmerica Job ID: 490-168891-1
Prep Type
Matrix
Method
Prep Batch
TCLP
Solid
EPA 1311
Prep Type
Matrix
Method
Prep Batch
TCLP
Sludge
7470A
271274
TCLP
Solid
7470A
271274
TotaVNA
Solid
7470A
TotaVNA
Solid
7470A
'
TCLP
Solid
7470A
271274
TCLP
Solid
7470A
271274
Prep Type
Matrix
Method
Prep Batch
TCLP
Sludge
3010A
271274
TCLP
Solid
3010A
271274
Total/NA
Solid
3010A
TotaVNA
Solid
3010A
Prep Type
Matrix
Method
Prep Batch
TCLP
Sludge
EPA 7470A
_ 271342
TCLP
Solid
EPA 7470A
271342
Total/NA
Solid
EPA 7470A
271342
TotaVNA
Solid
EPA 7470A
271342
TCLP
Solid
EPA 7470A
271342
TCLP
Solid
EPA 7470A
271342
Prep Type
Matrix
Method
Prep Batch
TCLP
Sludge
EPA 6010D
271355
TCLP
Solid
EPA 69100
271355
TotaVNA
Solid
EPA 6010D
271355
Total/NA
Solid
EPA 6010D
271355
Prep Type
Matrix
Method
Prep Batch
ToteVNA
Sludge
_
90308
TotaVNA
Solid
9030B
Total/NA
Solid
9030E
Total/NA
Solid
9030B
Total/NA
Solid
9030B
Prep Type
Matrix
Method
Prep Batch
Total/NA
Sludge
EPA 90134
277319
Total/NA
Solid
EPA 9034
271319
TotaVNA
Solid
EPA 9034
271319
Tota9NA
Solid
EPA 9034
271319
TestAmerica Nashville
Page 22 of 30
3/19/2019 (Rev. 2)

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
General Chemistry (Continued)
Analysis Batch: 271334 (Continued)
TestAmerica Job ID: 490-168891-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
j 490-16168890-BAD MSD
Matrix Spike Duplicate -- -
- -- - Total/NA
- Solid
- EPA 9034
271319
Analysis Batch: 271450
j Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TotaVNA
sludge
254OG
180-86358-B-20 DU
Duplicate
Total/NA
Solid
254OG
Analysis Batch: 271506
Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
1Lab
490-168891-1
GUC
TotaVNA
Sludge
EPA 9045D
LCS 180-271506/1
Lab Control Sample
TotaVNA
Solid
EPA 90451)
180-86977-J-1 DU
Duplicate
TotaVNA
Solid
EPA 9045D
Prep Batch: 271760
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168891-1
GUC
_ fot—al/KA
Sludge
9012E
MB 180-27176014-A
Method Blank
TotaVNA
Solid
9012B
HLCS 180-271760/2-A
Lab Control Sample
Total/NA
Solid
9012B
LCS 180-27176013-A
Lab Control Sample
Tota9NA
Solid
90123
LLCS 180-27176011-A
Lab Control Sample
TotaVNA
Solid
9012E
180-87076-0-1-B MS
Matrix Spike
TolaVNA
Solid
9012E
180-87076-D-1-C MSD
Matra Spike Duplicate
Total/NA
Solid
9012E
Analysis Batch: 271809
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC -
TotaVNA
Sludge
EPA 9012B
271760
MB 180-271760/4-A
Method Blank
TotaVNA
Solid
EPA 9012B
271760
HLCS 180-271760/2-A
Lab Control Sample
Total/NA
Solid
EPA 9012E
271760
LCS 180-271760/3-A
Lab Control Sample
TotaVNA
Solid
EPA 9012B
271760
LLCS 180-27176011-A
Lab Control Sample
Total/NA
Solid
EPA 90128
271760
180-87076-D-1-B MS
Matrix Spike
Total/NA
Solid
EPA 9012E
271760
180-87076-D-1-C MSD
Matra Spike Duplicate
TotaVNA
Solid
EPA 9012B
271760
Analysis Batch: 578372
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168891-1
GUC
Total/NA
Sludge
1010A
MB 490-578372/1
Method Blank
Total/NA
Solid
1010A
LCS 490-578372/2
Lab Control Sample
TotaVNA
Solid
1010A
LCSD 490-578372/14
Lab Control Sample Dup
Total/NA
Solid
1010A
280-120182-A-1 DU
Duplicate
Total/NA
Solid
1010A
TestAmerica Nashville
a
Page 23 of 30 3/19/2019 (Rev. 2)

Lab Chronicle
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Client Sample ID: GUC
Date Collected: 02/19/19 12:00
Date Received: 02/21/19 08:55
Batch Batch
Prep Type Type Method Run
TCLP
Leach
EPA 1311
TCLP
Analysis
EPA 8260D
TCLP
Leach
EPA 1311
TCLP
Prep
3510C
TCLP
Analysis
8270E
TCLP
Leach
EPA 1311
TCLP
Prep
3510C
TCLP
Analysis
EPA 8081E
Total/NA
Prep
3541
Total/NA
Analysis
EPA 8082A
TCLP
Leach
EPA 1311
TCLP
Prep
8151A
TCLP
Analysis
EPA 8151A
TCLP
Leach
EPA 1311
TCLP
Prep
3010A
TCLP
Analysis
EPA 601 OD
TCLP
Leach
EPA 1311
TCLP
Prep
7470A
TCLP
Analysis
EPA 7470A
Total/NA
Analysis
1010A
Total/NA
Analysis
254OG
Total/NA
Prep
9012E
Total/NA
Analysis
EPA 9012E
Total/NA
Prep
9030B
Total/NA
Analysis
EPA 9034
TotayNA
Analysis
EPA 9045D
Lab Sample ID: 490-168891-1
Matrix: Sludge
oil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
25 g
500 mL
271312
02/26/19 08:16
TAH
TAL PIT
1
0.125 mL
5 mL
271299
02/26/19 09:23
KLG
TAL PIT
100 g
2000 mL
271274
02125/19 16:00
MTT
TAL PIT
200 mL
10.0 mL
271367
02/26/19 12:10
CBY
TAL PIT
1
1 mL
1 mL
271438
02127/19 17:24
VVP
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
100 mL
40.0 mL
271365
02/26/19 11:00
CBY
TAL PIT
1
271475
02/27/19 16:03
DFE
TAL PIT
15.2.g
20.0 mL
271476
02/27/19 09:52
BAP
TAL PIT
1
271567
02/28/19 15:46
JMO
TAL PR
100 g
2000 mL
271274
02125/19 16:00
MITT
TAL PIT
100 mL
10.0 mL
271391
02/26119 14:30
CBY
TAL PIT
20
271555
02128/19 01:14
JBF
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MITT
TAL PIT
5 mL
50 mL
271355
02126/19 12:20
NAM
TAL PIT
1
271499
02/27/19 09:13
RJG
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
50 mL
50 mL
271342
02126N9 11:05
RJR
TAL PIT
1
271395
02/26/19 16:17
KAK
TAL PIT
1
578372
03/0111917:29
VRP
TAL NSH
1
271450
02/27119 08:43
JMS
TAL PIT
0.99 g
50 mL
271760
03/01/19 12:40
BSH
TAL PIT
1
271809
03/01/19 19:32
JAS
TAL PIT
5.00 g
50 mL
271319
02/26/19 09:35
SES
TAL PIT
1
271334
02/26/19 11:20
SES
TAL PIT
1
20 mL
20 mL
271506
02/27/19 12:00
JMS
TAL PIT
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmedca Pittsburgh, 301 Alpha Ddve, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
Page 24 of 30
3/19/2019 (Rev. 2)

Method Summary
Client: Bio-Nomics Services., Inc.
TestAnlerica Job ID: 490-168891-1
Project/Site:
Greenville WTP
Method
Method Description
Protocol
Laboratory
EPA 82600
_
Volatile Organic Compounds by GC/MS - -- - -
- - - SW846
TAL PIT
8270E
Semivolatile Organic Compounds (GC/MS)
SW846
TAL PIT
EPA 8081B
Organachlorine Pesticides (GC)
SW846
TAL PIT
EPA 8082A
Polychlarinated Biphenyls (PCBs) by Gas Chromatography
SW846
TAL PIT
EPA 8151A
Herbicides (GC)
SW846
TAL PIT
EPA 60100
Metals (ICP)
SW846
TAL PIT
EPA 7470A
Mercury (CVAA)
SW846
TAL PIT
1010A
Ignitability, Pensky-Martens Closed -Cup Method
SW846
TAL NSH
254OG
SM 254OG
SM22
TAL PIT
EPA 9012B
Cyanide, Total andor Amenable
SW846
TAL PIT
EPA 9034
Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL PIT
EPA 9045D
pH
SW846
TAL PIT
3010A
Preparation, Total Metals
SW846
TAL PIT
3510C
Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL PIT
3541
Automated Soxhlet Extraction
SW846
TAL PIT --
5030C
Purge and Trap
SW846
TAL PIT
7470A
Preparation, Mercury
SW846
TAL PIT
8151A
Extraction (Herbicides)
SW846
TAL PIT
9012B
Cyanide, Total and/or Amenable, Distillation
SW846
TAL PIT
9030E
Sulfide, Distillation (Acid Soluble and Insoluble)
SW846
TAL PIT
EPA 1311
TCLP Extraction
SW846
TAL PIT
Protocol References:
SM22 = Standard Methods For The Examination Of WaterAnd Wastewater, 22nd Edition
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Faster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAnnerica Nashville
Page 25 of 30 3/19/2019 (Rev. 2)

Accreditation/Certification Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Laboratory: TestAmerica Nashville
The accredilations/certifications listed below are applicable to this report
TestAmerica Job ID: 490-168891-1
Authority
Program
EPA Region Identification Number
Expiration Date
South Carolina
State Program
4 84009 (001)
62-28-19'
Laboratory: TestAmerica Pittsburgh
Unless otherwise noted, all
analytes for this laboratory were covered under each accreditation/certification below.
Authority
Program
EPA Region Identification Number
Expiration Date
South Camlina
Stale Program
4 89014
04-30-19
The following analytes are included in this report, but
the laboratory
is not certified by the governing authority. This
list may include analytes for which
the agency does not offer certification.
Analysis Method
Prep Method
Matrix
Analyte
254OG
- _
_
Sludge
_
Percent Moisture
2540E
Sludge
Percent Solids
8270E
3510C
Sludge
1,4-Dichlorobenzene
8270E
3510C
Sludge
2,4,5-Trtchlorophenol
8270E
3510C
Sludge
2,4,6-Tnchlorophenol
8270E
3510C
Sludge
2,4-Dinitrotoluene
, 8270E
3510C
Sludge
Cresols
8270E
3510C
Sludge
Hexachlorobenzene
8270E
3510C
Sludge
Hexachlorobutediene
8270E
3510C
Sludge
Hexachloroethane
8270E
3510C
Sludge
Nitrobenzene
8270E
3510C
Sludge
Pentachlorophenol
8270E
3510C
Sludge
Pyridine
EPA8151A
8151A
Sludge
2;4,5-T
EPA 8151A
8151A
Sludge
2,4-D
EPA 8151A
8151A
Sludge
Silvex (2,4,5-TP)
EPA 8260D
Sludge
1,1-Dichloroethene
EPA 8260D
Sludge
1,2-Dichloroethane
EPA 8260D
Sludge
2-Butanone (MEK)
EPA 8260D
Sludge
Benzene
EPA 8260D
Sludge
Carbon tetrachloride
EPA 8260D
Sludge
Chlorobenzene
EPA 8260D
Sludge
Chloroform
EPA 8260D
Sludge
Tetrachlomethene
EPA 8260D
Sludge
Tdchloroethene
EPA 8260D
Sludge
Vinyl chloride
EPA 9012E
9012E
Sludge
Cyanide, Total
Accreditation/Certification renewal pending - accreditation/certification considered valid.
TestAmerica Nashville
Page 26 of 30 3/19/2019 (Rev. 2)

f'"_ Al 4i
TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN
COOLER RECEIPT FORM
490-168891 Chain of Custody
Cooler RecelvedlOpened On 2/2112019 @ 9:55
Time Samples Removed From Cooler( • �yi Time Samples Placed In Storage <( (2 Hour Window)
1. Tracking# 63 (last 4 digits, FedEx) Courier: FedEx
IR Gun ID 17960358 pH Ship Lot Chlorine Strip Lot lo
2. Temperature of rep. sample or temp blank when opened: J sa Degrees Celsius
3. If Item #2 temperature Is 0"C or less, was the representative sample or temp blank frozen?
4. Were custody seals on outside of cooler? y,
If yes, how many and where: A `
YES NO.. lA�
&... NO ... NA
S. Were the seals intact signed, and dated correctly?
Rh ... NO ... NA
6. Were custody papers inside cooler?
,.NO ... NA
I certify that I opened the cooler and answered questions 1.6 fintlall
7. Were custody seals on containers: YES
NO
and Intact YES ... NO...NA
Were these signed and dated correctly?
YES ... NO
8. Packing mat'I used? ubblewra Plastic bag
Peanuts
Vermiculite Foam Insert Paper Other None
9. Coaling process: Ice
Ice -pack
Ice (direct contact) DryIce Other None
10. Did all containers arrive In good condition (unbroken)?
S ..NO...NA
11. Were all container labels complete (#, date, signed, pres., etc)?
12. Did all container labels and tags agree with custody papers?
13a. Were VOA vials received?
b. Was there any observable headspace present in any VOA vial?
• « Larger than this.
14. Was them a Trip Blank In this cooler? YES. NO.. NA
I certify thatl unloaded the cooler and answered Questions 7-141 RUM
ES ..NO...NA
NO...NA
YES.`NO, .NA
YES...NO..( AAA
If multiple coolers, sequence #
15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level?
YES ... NO. NA
b. Did the battle labels Indicate that the correct preservatives were used
DES ..NO...NA
16. Was residual chlorine present?
YES ... NO..NN
I certify that I checked for chlorine and pH as per SOP and answered questions 15.16 (Intial)
�
17. Were custody papers properlyfilled out (Ink, signed, etc)?
D... NO ... NA
18. Did you sign the custody papers in the appropriate place?
.OE ... NO ... NA
19. Were correct containers used for the analysis requested?
YE ... NO ... NA
20. Was sufficient amount of sample sent In each container?
YE ...NO...NA
I certify that I entered this prolect into LIMB and answered questions 17.20 (Intial)
I certify that I attached a label with the unique LIMS numbertoeach container (Intiall
21. Were there Non -Conformance issues at login YE . .(Ian Was a NCM generated? S ..NO...#
h
BIS = Broken in shipment
Ccolef Rcccipt Ponn.doc
LF-I
End of Fonn
Page 27 of 30
I
Revised 823117
I
3/19/2019 (Rev. 2)

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Page 29 of 30 3/19/2019 (Rev. 2)

Login Sample Receipt Checklist
Client: Bio-Nomics Services- Inc.
Job Number: 490-168891-1
SDG Number.
Login Number: 168891
List Source: TestAmerica Pittsburgh
List Number: 2
List Creation: 02/23/19 11:33 AM
Creator: Say, Thomas C
Question
Answer_
Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COG is present.
True
COG is filled out in ink and legible.
True
COG is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COG.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses; incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4').
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Nashville
Page 30 of 30 3/19/2019 (Rev. 2)

BIO-NOMIC SERVICES, INC. - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: Most Restrictive Result of all samples
McCall Permit No. W00003823
Mineralization Rate 0.20
Parameter
Carbonate
N / Nitrite N
45.80 %Solids
8.4 pH
/u Mg/Kg Dry Weight
(% x 10,000)
1.740 17,400.000
0.306 3,060,000
0.293 2.930.000
91
18.000
309.000
18,900.00
5.000
1.000
182.000
95.70
23.90
0.063
2.740
75.30
5.000
356.00
x u.uuz)
34.800
6,120
5.860
9.036
4.860
57.000
182.000
9.500
0.738
7.740
0.618
24.400
37.800
0.010
0.002
0.364
0.191
0.048
0.000
0.005
0.151
0.010
0.712
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.36
Ceiling Concen.
(M /Kg)
75
85
4,300
840
57
75
420
100
7,500

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 20, 2019
McCall Farms #1 Permit No. W00003823
Mineralization Rate 0.20 32.10 % Solids
8.4 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen TKN)
1.740
17,400.000
34.800
Phosphorus
0.306
3,060,000
6.120
Potassium
0.293
2,930.000
5.860
PAN (incor orated)*iisi;iit:[:it:'P'z':'>::
P
i) 6QD
::::.:::::.:::::::.:.:.:::::::.::1:1 Ri(:
PAN (surface)*
0.429
4,292.800
8.586
Ammonia. Nitrogen
0.243
2,430.000
4.860
Calcium
1.690
16,900.000
33.800
Calcium Carbonate Eq.
3.500
35,000,000
70.000
Magnesium
---
4,750.000
9.500
Sodium
369,000
0.738
Sulfur
---
3,870.000
7.740
Nitrate N / Nitrite N
---
83.800
0.168
Barium
Chloride
---
---
---
---
--
---
SAR
0.36
Iron
---
11,700.000
23.400
Ceiling Concen.
Aluminum
17,600.00
35.200
(Mg/K )
Arsenic
---
5.000
0.010
75
Cadmium
1.000
0.002
85
Chromium
---
182.000
0.364
-
Copper
---
95.70
0.191
4,300
Lead
---
23.90
0.048
840
Mercury
---
0.042
0.000
57
Molybdenum
---
2.740
0.005
75
Nickel
---
75.30
0.151
420
Selenium
---
5.000
0.010
100
Zinc
---
356.00
0.712
7,500
Waypoint Analytical 19-052-0206
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = %PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits.
for calculation purposes.

Waypo11
ANALYTICAL
3/1/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-052-0206
Project Description: McFar #1
7621 Whitepine Road, Richmond, VA 23237
Main 804.743-9401 o Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/21/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 Pennsylvania 68-03109 Virginia 460014
South Carolina 93007
New Jersey VA011
Florida E871087
North Carolina 257
Page 1 of 6

Wa� /�O' �� 7622 W hitepine Road, Richmond, VA 23237
./Y Main 804-743-94010 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-052-0206
Client Project Description: McFar #1
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
64890
McFar#1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
61890
McFar#1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
64890
McFar#1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354
02/20/2019
07:30
02/2112019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
0730
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
SM-254OG
WTN
SW-74718
WTN
SM4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
Page 2 of 6

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Waypoi nt
7621 Whitepine Road, Richmond, VA 23237
.
ANALYTICAL
Main 504-743-9401° Fax [phone]
www.waypolntanalydcal.com
Y Ytiol.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-052-0206
Shipping Method
Fed Ex Q US Postal 0 Lab
0 Other: F-
0 UPS O Client Q Courier
Thermometer ID: �—
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers received
I 1
Custody seals intact on shipping container/cooler?
Q Yes
0 No 0 Not Required
Custody seals intact on sample bottles?
Q Yes
0 No 0 Not Required
Chain of Custody (CDC) present?
0 Yes
0 No
CDC agrees with sample label(s)?
Yes
Q No
COC properly completed
Yes
Q No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
Q No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance? Yes
Q No
Cooler/Samples arrived at the laboratory on ice. Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved O Yes
Q No N/A
Water- VOA vials free of headspace 0 Yes
0 No N/A
Trip Blanks received with VOAs 0 Yes
0 No N/A
Soil VOA method 5035 — compliance criteria met Q Yes
0 No N/A
High concentration container (48 hr)
F Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d)
(— Low
conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes
No
Comments:
Signature: Brandi Watson Date & Time: 2/21/2019 14:09:52
Page 5 of 6

E

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 20, 2019
McCall Farms #2 Permit No. WO0003823
Minemliration Rate 0.20 42.50 % Solids
8.4 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen TKN)
0.998
9,980.000
19.960
Phosphorus
0.240
2,400.000
4.800
Potassium
0.260
2,600.000
5.200
PAN (incorporated)*
PAN (surface)*
0.247
2,468.200
4.936
Ammonia Nitrogen
0.153
1,530.000
3.060
Calcium
2.850
28,500.000
57.000
Calcium Carbonate Eq.
0.100
1,000.000
2.000
Magnesium
---
4,270.000
8.540
Sodium
323.000
0.646
Sulfur
2,930.000
5.860
Nitrate N / Nitrite N
---
13.200
0.026
Barium
Chloride
--_
___
Iron
---
I1,500.000
23.000
Aluminum
---
17,100.00
34.200
Arsenic
---
5.000
0.010
Cadmium
---
1.000
0.002
Chromium
---
161.000
0.322
Copper
71.70
0.143
Lead
---
20.30
0.041
Mercury
0.060
0.000
Molybdenum
---
2.500
0.005
Nickel
67.50
O.I35
Selenium
---
5.000
0.010
Zinc
---
971 nn
n 9A9
II I I I
Waypoint Analytical 19-052-0207
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia. N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
0.31
Ceiling Concen.
(MP,/Kg)
75
85
4,300
840
57
75
420
100
7,500

(2)
Waypoint
ANALYTICAL
3/1/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-052-0207
Project Description: McFar #2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica I.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/21/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
F.. va`!i
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZO629 Pennsylvania 68-03109 Virginia 450014
South Carolina 93007
Newlersey VA011
Florida E871087
North Carolina 257
Page 1 oF6

Wayp A t.
ANALYTICAL
Report Number: 19-052-0207
Client Project Description: McFar #2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyrical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
SM-254OG
W rN
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
SW-7471B
WiN
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
SM-4500-NH3C-TKN
WiN
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
4500NO3F-2011
WiN
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
6010D
WFN
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
SM-4500-NH3C
WiN
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
9045D
WiN
64891
McFar #2
Solids
02/20/2019
07:45
02/21/2019
AOAC 955.01
WTN
WrN: Waypoint Analytical- TN, Memphis, TN, Certification: #1354
Page 2 of 6

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WaY�®' ii� \7621 Whitepine Road, Richmond, VA 23237
e Main 804-743-9401 -Fax [phone]
ANALYTICAL . W.waypointanalydcal.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-052-0207
Shipping Method
Fed Ex O US Postal O Lab 0 Other: F
O UPS 0 Client O Courier Thermometer ID:
Shipping container/cooler uncompromised? 0 Yes O No
Number of coolers received r 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No ID Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Not Required
Chain of Custody (CDC) present? 0 Yes Q No
CDC agrees with sample label(s)? 0 Yes O No
COG properly completed 19 Yes 0 No
Samples in proper containers? 0 Yes O No
Sample containers intact? Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes O No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs Q Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 40 No
Comments:
Signature: Brandi Watson Date & Time: 2/21/2019 14:27:12
Page 5 of 6

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 1, 2019
McCall Farms #3 Permit No. W00003823
Mineralization Rate 0.20 43.10 % Solids
7.9 pH
Parameter
%
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(M x 0.002)
Nitrogen (TKN)
1.100
11,000.000
22.000
Phosphorus
0.174
1,740.000
3.480
Potassium
0.197
1,970.000
3.940
Carbonate
N / Nitrite N
2,7IT800
5.436
696.000
1.392
17,000.000
34.000
91,000.000
182.000
2,950.000
5.900
250.000
0.500
2,060.000
4.120
309.000
0.618
12,200.000
24.400
18,900.00
37.800
5.000
1.000
24.000
50.50
15.20
0.051
2.500
50.00
5.000
189.00
0.002
0.248
0.101
0.030
0.010
0.378
W aypoint Analytical 19-092-0211
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
0.30
Ceiling Concen.
(Mg/K )
75
85
4,300
840
57
75
420
100
7,500

0
Waypoint.
ANALYTICAL
4/10/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-092-0211
Project Description: Biosolid 3
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/2/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any Feld parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P.a ks l-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZO629 Pennsylvania 68-03109 Virginia 460014
South Carolina 93007
New Jersey
VA011
Florida E871087
North Carolina
257
Page 1 of 8

O
Waypoint_ .r.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Bio-Nomic Servics Inc CASE NARRATIVE
Project: Biosolid 3
Lab Report Number: 19-092-0211
Date: 4/10/2019
Metals Analysis Method 6010D
Sample 65680 (3)
Analyte: Aluminum
QC Batch No: L429733IL429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix Interference is suspected.
Analyte: Potassium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Sodium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate. (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Phosphorus
Page 2 of 8

0
Waypoint_
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyticai.com
QC Batch No: L429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Lead
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L429733IL429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 3 of 8

s
epine Road,
Waypoi nt . 7621Ma nt804-743-940110 F chmondx 804 271-6446
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-092-0211
Client Project Description: Biosolid 3
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65680
3
Solids
65680
3
Solids
65680
3
Solids
65680
3
Solids
65680
3
Solids
65680
3
Solids
65680
3
Solids
65680
3
Solids
65680
3
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
04/01/2019
09:00
04/02/2019
04/01/2019
09:00
04/02/2019
04/01/2019
09:00
04/02/2019
04/01/2019
09:00
04/02/2019
04/01/2019
09:00
04/02/2019
04/01/2019
09:00
04/02/2019
04/01/2019
09:00
04/02/2019
04/01/2019
09:00
04/02/2019
04/01/2019
09:00
04/02/2019
SM-2540G
WFN
SW-7471B
WFN
SM-4500-NH3C-TKN
WFN
4500NO3F-2011
WFN
6010D
WTN
SM-4500-NH3C
WTN
9045D
'ArrN
AOAC 955.01
WiN
Page 4 of 8

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Waypoint,-
ANALYTICAL
7621 Whitepine Road, Richmond, VA Z3237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-092-0211
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
F-
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
—71
r
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No
N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
[— Low concentration EnCore samplers (48 hr)
F- Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: lBrandi Watson Date & Time: 4/02I2019 13:55:40
Page 7 of 8

N

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 1, 2019
McCall Farms #4
Mineralization Rate 0.20
Parameter
44.80 % Solids
8.2 pH
'o 1 Mg/Kg Dry Weight
Permit No. W00003823
x
IlPhosphorus 1 0.1691 1,690.000 1 3.380 11
Carbonate
N / Nitrite N
0.158 1,580.000
1.270 12,700.000
7.100 71,000.000
--- 2,830.000
--- 250.000
--- 2,030,000
--- 36.400
--- 9,950.000
--- 15,200.00
--- 5.000
--- 1.000
--- 120.000
--- 54.10
-- 16.20
-- 0.063
--- 2.500
--- 48.70
5.000
196.00
3.160
25.400
142.000
5.660
0.500
4.060
0.073
19.900
30.400
0.010
0.002
0.240
0.108
0.005
0.097
0.010
0.392
p I I I
W aypoint Analytical 19-092-0212
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
0.35
Ceiling Concert.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

0
Waypoint.,
ANALYTICAL
4/10/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number:19-092-0212
Project Description: Biosolid 4
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/2/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P. Xrpi
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZO629 Pennsylvania 68-03109 Virginia 460014
South Carolina 93007
Newlersey
VA011
Florida E871087
North Carolina
257
Page 1 of 6

* 0
Way p Ant..
ANALYTICAL
Report Number: 19-092-0212
Client Project Description: Biosolid 4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
65681
4
Solids
04/01/2019 09:10
04/02/2019
65681
4
Solids
04/01/2019 09:10
04/02/2019
SM-2540G
WTN
65681
4
Solids
04/01/2019 09:10
04/02/2019
SW-7471B
WTN
65681
4
Solids
04/01/2019 09:10
04/02/2019
SM-4500-NH3C-TKN
WTN
65661
4
Solids
04/01/2019 09:10
04/02/2019
4500NO3F2011
WTN
65681
4
Solids
04/01/2019 09:10
04/02/2019
6010D
WrN
65681
4
Solids
04/01/2019 09:10
- 04/02/2019
SM4500-NH3C
WTN
65681
4
Solids
04/01/2019 09:10
04/02/2019
9045D
WiN
65681
4
Solids
04/01/2019 09:10
04/02/2019
AOAC 955.01
WTN
WTN: Waypoint Analydmi- TN, Memphis, TN, Certification: #1354
Page 2 or 6

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'P;p
Waypoint,.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-092-0212
Shipping Method
le Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
�-
�—
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
r 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (CDC) present?
0 Yes
0 No
CDC agrees with sample label(s)?
0 Yes
0 No
CDC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
4P Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
40 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No
N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
F— Low concentration EnCore samplers (48 hr)
[— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: lBrandi Watson Date & Time: 4/021201914:01:25
Page 5 of 6

BIO-NONIIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 1, 2019
McCall Farms #5 Permit No. W00003823
Mineralization Rate 0.20 32.10 % Solids
7.7 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
Mg/ICg x 0.002)
Nitrogen (TKN)
1.700
17,000.000
34.000
Phosphorus
0.221
2,210.000
4.420
Potassium
0.247
2,470.000
4.940
PAN(incorporated)*
PAN (surface)*
0.389
3,891.000
7.782
Ammonia Nitrogen
0.118
1,180.000
2.360
Calcium
1.620
16,200.000
32.400
Calcium Carbonate Eq.
8.600
86,000.000
172.000
Magnesium
---
3,960.000
7.920
Sodium
289.000
0.578
Sulfur
---
3,130.000
6.260
Nitrate N / Nitrite N
-
137.000
0.274
Barium
Chloride
--
-
---
---
---
SAR
0.30
Iron
---
9,870.000
19.740
Ceiling Concen.
Aluminum
---
15,500.00
31.000
(Mg/Kg)
Arsenic
---
5.000
0.010
75
Cadmium
---
1.000
0.002
85
Chromium
--
125.000
0.250
---
Copper
---
70.70
0.141
4,300
Lead
---
19.60
0.039
840
Mercury
---
0.037
0.000
57
Molybdenum
---
2.500
0.005
75
Nickel
---
50.90
0.102
420
Selenium
---
5.000
0.010
100
Zinc
--
263.00
0.526
7,500
Waypoint Analytical 19-092-0213
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

0
Waypoint.
ANALYTICAL
4/10/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-092-0213
Project Description: Biosolid 5
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/2/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P_, 06 7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZO629 Pennsylvania 68-03109 Virginia 460014
South Carolina 93007
New Jersey VA031
Florida E871087
North Carolina 257
Page 1 of 6

a
Waypoint 7621 ain 804-7 Road, Richmond, 27 -6446
Main 804-743-9401 0Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-092-0213
Client Project Description: Biosolid 5
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
SM-2540G
W-FN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
W-FN
SM-4500-NH3C
WTN
9045D
WrN
AOAC 955.01
WFN
Page 2 of 6

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Waypoint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401- Fax [phone]
www.waypointa nalyti ca I. co m
Cooler Receipt Form
Customer Number:45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19.092-0213
Shipping Method
IS Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
�-
�—
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers received
r-1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
9 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (CDC) present?
40 Yes
0 No
CDC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
40 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water- VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No
N/A
F— High concentration container (48 hr)
F— High concentration pre -weighed (methanol -14 d)
F— Low concentration EnCore samplers (48 hr)
F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes
0 No
Comments:
Signature: Brand! Watson Date & Time: 4/02/2019 14:03:21
Page 5 of 6

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&!

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 1, 2019
McCall Farms #6 Permit No. WQ0003823
Mineralization Rate 0.20 45.80 % Solids
8.2 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.330
13,300.000
26.600
Phosphorus
0.162
1,620.000
3.240
Potassium
0.205
2,050.000
4.100
PAN (incorporated)*
PAN surface)*
0.304
3,038.200
6.076
Ammonia Nitrogen
0.120
1,200.000
2.400
Calcium
1.400
14,000.000
28.000
Calcium Carbonate Eq.
9.000
90,000.000
180.000
Magnesium
---
2,910.000
5.820
Sodium
---
250.000
0.500
Sulfur
---
2,090.000
4.180
Nitrate N / Nitrite N
---
18.200
0.036
Barium
---
---
--
SAR
Chloride
---
---
---
0.34
Iron
---
10,900.000
21.800
Ceiling Concen.
Aluminum
---
16,100.00
32.200
(M g)
Arsenic
---
5.000
0.010
75
Cadmium
---
1.000
1 0.002
85
Chromium
---
122.000
0.244
---
Copper
---
50.50
0.101
4,300
Lead
---
15.40
0.031
840
Mercury
---
0.045
0.000
57
Molybdenum
---
2.500
0.005
1 75
Nickel
---
49.60
0.099
420
Selenium
---
5.000
0.010
100
Zinc
---
184.00
0.368
7,500
Waypoint Analytical 19-092-0214
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

0
Waypoint.
ANALYTICAL
4/10/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-092-0214
Project Description: Biosolid 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waVloointanaly-tical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/2/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
p,,,;. a'6.7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZO629 Pennsylvania 68-03109 Virginia 460014
South Carolina 93007
New Jersey VA012
Florida E871087
North Carolina 257
Page 1 of 5

0
aypoi nt . 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
W
Sample Summary Table
Report Number: 19-092-0214
Client Project Description: Biosolid 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65683
6
Solids
65683
6
Solids
65683
6
Solids
65683
6
Solids
65683
6
Solids
65683
6
Solids
65683
6
Solids
65683
6
Solids
65683
6
Solids
WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354
04/01/2019
09:20
04/02/2019
04/01/2019
09:20
04/02/2019
04/01/2019
09:20
04/02/2019
04/01/2019
09:20
04/02/2019
04/01/2019
09:20
04/02/2019
04/01/2019
09:20
04/02/2019
04/01/2019
09:20
04/02/2019
04/01/2019
09:20
04/02/2019
04/01/2019
09:20
04/02/2019
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WFN
4500NO3F2011
WrN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
Page 2 or 6

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oint.-��1J Wayp
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypoi ntanalytica I mom
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-092-0214
Shipping Method
10 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID: I
F_
_.
Shipping container/cooler uncompromised?
10 Yes
0 No
Number of coolers received
r 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals Intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (CDC) present?
4D Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
JR Yes
0 No
Sample containers intact?
ID Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water- Sample containers properly preserved
0 Yes
0 No
N/A
Water- VOAvials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
0 No
N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
[_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: lBrandi Watson Date & Time: 4/02/2019 14:04:45
Page 5 of 6

1❑
i esTAmenca
YTICAL REPORT
TestAmerica Laboratories,
TestAmerica Nashville
2960 Foster Creighton Drip
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-168890-1
Client Project/Site: McCall Farms
For:
Bio-Nomics Services., Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Vaughn Stevenson
Authorized for release by:
31612019 1:53:59 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI
parameters, exceptions are noted in this report. This report may r
and with written approval from the labomtory. For questions pleas
at the e-mail address or telephone number listed on this page.
foraccredited
;ed except in full,
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.

Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
2
Sample Summary .........................................
3
Case Narrative ...........................................
4
Definitions ...............................................
5
Client Sample Results ......................................
6
QC Sample Results ........................................
9
QC Association ...........................................
21
Chronicle ................................................
25
Method Summary .........................................
26
Certification Summary ......................................
27
Chain of Custody ..........................................
28
Receipt Checklists .........................................
31
Page 2 of 31
TestAmerica Nashville
3/6/2019
21

Sample Summary
Client: Bio-Nomics Services., Inc. TestAmenca Job ID: 490-168890-1
ProjecUSte: McCall Farms
Lab Sample ID. Client Sample ID Matrix Collected Received
490-168890-1 McCall Farms Sludge 02/19/19 10:00 0221/19 D8:55
TestAmerica Nashville
Page 3 of 31 3/6/2019

Case Narrative
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Job ID: 490-168890-1
Laboratory: TestAmerica Nashville
Narrative
490-168890-1
Comments
While TA Pittsburgh carries South Carolina certification for 8260D and 8270E, the referenced matrix "Sludge", is causing the report to
indicate the lab as not certified for these.
No additional comments.
Receipt
The sample was received on 2/21/2019 8:55 AM; the sample arrived in good condition, properly preserved and, where required, on Ice.
The temperature of the cooler at receipt was 3.0" C.
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-271299 was outside the method criteria for the
following analyte: 2-Butanone. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is
considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
GCIMS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 1010A: Method 1010A is applicable only to liquid matrix. This method has been modified to incorporate soil) solid matrices of the
following sample: McCall Farms (490-168890.1).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Geotechnical
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
Method 351OC: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271365.
Method 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271367.
Method 8151A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271391.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
Page 4 of 31 TestAmerica 3/6/2019

Definitions/Glossary
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Qualifiers
GC/MS Semi VOA
Qualifier Qualifier Description
TestAmerica Job ID: 490-168890-1
J Result is less than the RL but greater than or equal to the MDL antl the wncentrabon Is an approximate value.
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report
,: Listed under the "D" wlumn to designate that the result is reported on a dry weight hasis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fee Dilution Factor
OIL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 31 3/6/2019

Client Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Client Sample ID: McCall Farms
Date Collected: 02119/19 10:00
Date Received: 02/21/19 08:55
Method: EPA 8260D - Volatile Organic Compounds by GC/MS - TCLP
TestAmerica Job ID: 490-168890-1
Lab Sample ID: 490468890 7
Matrix: Sludge
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Oil Fac
1,1-Dichlor6ithene
ND
0.200
mg/L
02/2611910:29
t
1,2-Dichloroethane
NO
0.200
mg/L
02126/1910:29
1
®.
2-Butanone (MEK)
NO
0.200
mg/L
D226/1910:29
1
Benzene
NO
0.200
mg/L
02/26/1910:29
1
Carbon tetrachloride
NO
0.200
mg/L
02126119 10:29
1
Chlorobenzene
NO
0.200
mglL
02/2611910:29
1
Chloroform
NO
0.200
mg/L
02/26/1910:29
1
Tetrachloroethene
NO
0.200
mg/L
02/26/1910:29
1
Tdchloroethene
NO
0.200
mg/L
02/2611910:29
1
Vinyl chloride
NO
0.200
mg/L
02/26/19 10:29
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Oil Fac
1,2-Dichloroethane-d4 (Surr)
B9
73-143
022fi/19 f0:19
1
4-Bromofluorobenzene (Surr)
83
61-123
02/26/19 10.29
1
Dibromof/uoromethane (Surr)
105
68-128
02,26/19 10:29
1
Toluen"8 (Surr)
100
75-124
02,26119 10:29
1
Method: 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Oil Fac
1,4-Dichlorobenzene
ND
0.0500
mglL
02/2fi/1912.10
02/27/1916:57
1
2,4,5-Tdchlorophenol
NO
0.0500
mg/L
02126119 12:10
02/2711916:57
1
2,4,6-Tdchlorophenol
NO
0.0500
mg/L
02/26/1912:10
02/2711916:57
1
2,4-Dinitrotoluene
NO
0.0500
mg/L
02/26/1912:10
0212711916:57
1
Hexachlorobenzene
NO
0.0500
mg1L
0226/1912:10
02127/1916:57
1
Hexachlorobutadiene
NO
0.0500
mg/L
02/26/1912:10
0227/1916:57
1
Hexachloroethane
NO
0.0500
mglL
0226/1912:10
02/27/1916:57
1
Nitrobenzene
NO
0.0500
mg/L
02/26/1912:10
02/27/1916:57
1
Pentachlorophenol
NO
0.250
mg/L
02126/1912:10
022711916:57
1
Pyddine
NO
0.100
mg/L
0226/1912:10
022711916:57
1
Cresols
NO
0.100
mg/L
022611912:10
0227/1916:57
1
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol(Sua)
74
25-112
2-Fluomphenol (Surr)
89
61-105
2-Fluorobiphenyl
90
62-105
Nitrobenzene-d5 (Surr)
86
64 -105
Phenol-d5 (Surr)
86
47-105
Terphenyl-d14 (Surr)
79
45-130
Method: EPA 8081B - Organochlorine Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
Chlordane (technical)
NO
0.00500
Endrin
NO
0.000500
gamma-BHC (Lindane)
NO
0.000500
Heptachlor
NO
0.000500
Heptachlor epoxide
NO
0.000500
Methoxychlor
NO
0.000500
Toxaphene
NO
0.D400
Prepared
Analyzed
Dil Fac
OZ26/1912:10
OZ27/1916:57
1
022611912:10
OZ27/1916:57
1
022611912:10
0227/1916.57
1
022611912:10
022711916:57
1
0226/1912:10
OW711916:57
1
0226/1912:10
022711916:57
1
MDL Unit
0 Prepared
Analyzed
Oil Fac
mglL
0126/19 11:00
0227/1915:48
1
mg/L
022611911:00
0212711915:48
1
mg/L
0226/1911:00
0212711915:48
1
mg/L
0226/1911:00
02127/1915:48
1
mg/L
D2126/1911:00
022711915:48
1
mg/L
0212611911:00
0227/1915:48
1
mg/L
02126/1911:00
02/27/1915:48
1
TestAmerica Nashville
Page 6 of 31 3/6/2019

Client Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Client Sample ID: McCall Farms
Date Collected: 0211911910:00
Date Received: 02/21/19 08:55
Surrogate %,Recovery Qualifier Limits
DCB Decachlorobiphenyl (Surf) 93 62-150
Tetrachloro-m-xy/ene 97 54-138
Method: EPA 8151A - Herbicides (GC) - TCLP
TestAmerica Job ID: 490-168890-1
Lab Sample ID: 490-168890-1
Matrix: Sludge
Prepared Analyzed Dif Fac
622611 11100 0217/1915:48 1
0226/1911:00 0227/1915:48 1
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
oil Fac
2A-D
ND
0.0400
mg/L
022611914:30
UMB/190053
20
Silvex(2,4,5-TP)
ND
0.0100
mg/L
0226/1914:30
02/2811900:53
20
2,4,5-T
ND
0.0100
mg/L
0226/1914:30
0228/1900:53
20
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
oil Fac
2.4-Dichlorophenylecetic acid
64
20- 005
022611914:30
0228/1900.53
20
Method: EPA 6010D - Metals
(ICP) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
oil Fac
Arsenic
ND
0.500
mg/L
02126/1912:20
02/27/1 009:08
1
Barium
ND
2.00
mg/L
02126/19122D
0212711909:08
1
Cadmium
ND
0.500
mg1L
0226/1912:20
0227/1909:08
1
Chromium
ND
0.500
mg/L
0226/1912:20
02127/1909:08
1
Lead
ND
0.500
mg/L
0226/19 12:20
0227/19 09:08
1
Selenium
ND
0.500
mg/L
0226/1912:20
0227/1909:08
1
Silver
ND
0.500
mglL
02/26/19. 12:20
022711909:08
1
EPA 7470A - Mercury (CVAA) - TCLP
IMethod:
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
oil Fac
Mercury
ND
0.000200
69/L
—
62126/1911:05
02126/1916:16
1
General Chemistry
Analyte
Result Qualifier
RL
RL Unit
D
Prepared
Analyzed
oil Fac
Fiashpoint
>200
1.00
Degrees F
03101/1917:29
1
Percent Moisture
48.8
0.1
%
0227/1908:43
1
Percent Solids
51.2
0.1
%
02/27/1908;43
1
pH
8.6 HF
0.1
SU
0227/1912:00
1
TestAmerica Nashville
Page 7 of 31 3/6/2019

Client Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Client Sample ID: McCall Farms Lab Sample ID: 490-168890-1
Date Collected: 02/1911910:00
Matrix: Sludge
Date Received: 02/21/19 08:56
Percent Solids: 61.2
Method: EPA 8082A - Polychlorinated
Biphenyls (PCBs) by Gas
Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
PCB-1016
ND
32.4
ug/Kg
P
02/27/19 09:52
0228119 14:50
1
PCB-1221
ND
32.4
uglKg
*
02/27/19 09:52
0228119 14,50
1
PCB-1232
ND
32.4
ug/Kg
*
02/27/19 09:52
02/28/1914:50
1
PCB-1242
ND
32.4
ug/Kg
C
02127/1909:52
0228/1914:50
1
PCB-1248
ND
32.4
ug/Kg
t1
022711909:52
02/28/1914:50
1
PCB-1254
ND
32.4
u9/K9
q
02/27/19 09:52
0228119 14:50
1
PCB-1260
ND
32.4
u9/K9
C
02/27/19 09:52
0228/19 14:50
1
Surrogate %Recovery Qualifier Limits
Tetrachloro-m xylene (Sur) 83 51-116
DCB Decach/orobiphenyl (Sun) 90 44-116
Prepared Analyzed Dil Fac
0227119 09:52 02/28/19 14:50 1
02/27/19 09:52 0228119 14:50 1
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Cyanide, Total ND 0.940 mg/Kg u 03/01/19— 03/01/191930 1
Sulfide ill 58.3 mg/Kg C 02126/1909:35 02/2611911:22 1
TestAmerica Nashville
Page 8 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
FLab Sample ID: LCS 180-271299/3 Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271299
Analyte
1,1-Dichlomethene
1,2-Dichloroethane
2-Butanone (MEK)
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Spike
LCS LCS
Added
Result Qualifier
0.0400
0.04011
0.0400
0.03331
0.0400
0.02829
0.0400
0.04064
0.0400
0.04205
0.0400
0.04443
0.0400
0.03950
0.0400
0.D4642
0.0400
0.04744
0.0400
0.03919
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4(Sum)
60
73-1 33
4-Bromofiuorobenzene (Surf)
97
61-123
Dibromo6uoromethane(Surf)
105
68-128
Toluene-d8 (Sum)
103
75-124
%Rec.
Unit
D %Rec
Limits
mglL
100
57-135
mg/L
83
69 -127
mg/L
71
36 -150
mg/L
102
66-124
mg/L
105
69-130
mg1L
111
72-122
mg/L
99
69-119
mg/L
116
73-129
mg/L
119
75-122
mglL
98
57-132
Lab Sample ID: LB 180-27131211-A
Matrix: Solid
Analysis Batch: 271299
Analyte
LB LB
Result Qualifier
RL
MDL Unit
Client Sample ID: Method Blank
Prep Type: TCLP
D Prepared Analyzed Oil Fee
1,1-Dichloroethene
ND
0.0500
mglL
0226R909.01
1
1,2-Dichloroethane
NO
0,0500
mglL
02126/1909:01
1
2-Butanone (MEK)
NO
0,0500
mg/L
02126119 09:01
1
Benzene
NO
0.0500
mg/L
02/26119 09:01
1
Carbon tebachlonde
NO
0.0500
mg/L
02/26/19 09:01
1
Chlorobenzene
NO
0.0500
mg/L
02/26/1909:01
1
Chloroform
NO
0.0500
mglI-
02/26/19 09:01
1
Tetrachlomethene
NO
0.0500
mg/L
02/26/19 09:01
1
Tdchloroethene
NO
0.0500
mg/L
02/26/19 09:01
1
Vinyl chloride
NO
0.0500
mg/L
02126/1909:01
1
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed
Dif Fac
1,2-Dichloroethane-d4(Suv)
B5
73-143
022611909:01
1
4-Bmmofluorobenzene (Surr)
82
61-123
0226/19 09:01
1
Dibromofluoromethane (Surr)
102
68- 128
0226119 09:01
1
Toluene-d8 (Surr)
104
75-124
0226/19 09.01
1
Lab Sample ID: 490-168891-A-1-B MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271299
Sample Sample
Spike
MS Ms
%Rec.
Anayte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
1,1-Dichloroethene
ND
7.60
1.556
mg/L
97
57-135
1,2-Dichloroethane
NO
160
1.409
mg/L
88
69-127
2-Butanone (MEK)
NO
1.60
0.8771
mg/L
55
36-150
TestAmerica Nashville
Page 9 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: 490-168891-A-1-B MS Client Sample ID: Matrix Spike
Matrix: Solid Prep Type: TCLP
Analysis Batch: 271299
Sample Sample
Analyte
Result Qualifier
Benzene
ND
Carbon tetrachloride
NO
Chlorobenzene
NO
Chloroform
NO
Tetrachloroethene
NO
Trichloroethene
NO
Vinyl chloride
NO
Spike
MS MS
Added
Result Qualifier
1.60
1.613
1.60
1.711
1.60
1.768
1.60
1.638
1.60
1.815
1.60
1.869
1.60
1.383
MS MS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4(Surr)
85
73-143
4-Bromofluorobanzene (Surr)
96
61-123
Dibromo6uoromethane (Surr)
104
68-128
Toluene -dB (Sun)
101
75-124
FLab Sample ID: 490-168891-A-1-C MSD
Matrix: Solid
Analysis Batch:271299
Sample Sample
Analyte
Result Qualifier
1,1-Dichloroethene
ND
1,2-Dichloroethane
NO
2-Butanone (MEK)
NO
Benzene
NO
Carbon tetrachloride
NO
Chlorobenzene
NO
Chloroform
ND
Tetrachloroethene
NO
Trichloroethene
NO
Vinyl chloride
NO
Spike
MSD MSD
Added
Result Qualifier
1.60
1.702
1.60
1.434
1.60
0.9013
1.60
1.638
1.60
1.689
1.60
1.798
1.60
1.639
1.60
1.882
1.60
1.879
1.60
lMll
MSD MSD
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4(Surr)
87
73-143
4-Bromofluorobenzene (Surr)
99
61-123
DibromoNuoromethane (Surr)
106
68-128
Toluene-as(Surr)105
75-124
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 180-271367/1-A
Matrix: Solid
Analysis Batch: 271438
MB MB
Analyte
Result Qualifier
RL
1,4-Dichlorobenzene
ND
0.0500
2,4,5-Tdchlorophenol
NO
0.0500
2,4,6-Tdchlorophenol
NO
0.0500
2,4-Dinitrotoluene
NO
0.0500
%Rec.
Unit
D %Rec
Limits
mg/L
101
66-124
mg/L
107
69-130
mg/L
Ill
72 -122
mg/L
102
69 -119
mg/L
113
73-129
mg/L
117
75-122
mg/L
86
57-132
Client Sample ID: Matrix Spike Duplicate
Prep Type: TCLP
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
mg/L
106
57-135
9
35
mg/L
90
69 -127
2
16
mg/L
56
36 -150
3
35
mg/L
102
66 -124
2
16
mg/L
106
69-130
1
17
mg/L
112
72-122
2
15
mg/L
102
69-119
0
16
mg/L
118
73-129
4
15
mg/L
117
75-122
1
15
mg/L
97
57-132
12
21
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch:271367
MDL Unit
D Prepared
Analyzed
Oil Fac
mg/L
02/26/1912: 10
02/2711 009:11
1
mg/L
02/26/19 12:10
02/27/19 09:11
1
mg1L
02/26/19 12:10
02/27/19 09:11
1
mg/L
02/26/19 12:10
02/27/19 09:11
1
TestAmerica Nashville
Page 10 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 180-27136711-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch:
271367
MB M8
Analyte
Result Qualifier
RE.
Mot. Unit D
Prepared
Analyzed
Dil Fac
Hexachlorobenzene
ND
00500
mg/L
02/2611912; 10
0227/190911
1
Hexachlorobutediene
Hexachloroethane
ND
ND
0.0500
0.0500
mg/L
mg/L
02/26/19 12 10
02126/19 12:10
02127/1909:11
02/27/19 09:11
1
1
Nitrobenzene
ND
0,0500
mg/L
02/2611912:10
02/2711909,11
1
Pentachlorophenol
ND
0.250
mg/L
02J26I1912:10
02/2711909:11
1
Pyridine
ND
0.100
mg/L
02126/1912:10
02127/1909:11
1
Cresols
ND
0.100
mg/L
02126/1912:10
0227/1909:11
1
MB MB
Surrogate
%,Recovery Qualifier
Limits
Prepared
Analyzed
oil Fac
2,4,6-77dbromophenol (Sum)
83
25- 1 22
022611912: 10
0227/196-9 11
1
2-F/uorophenol (Surr)
87
61- 105
0226/19 12:10
0227/19 09:11
1
2-Fluorobiphen)d
63
62-105
OZ26/19 12:10
0227/19 09:11
1
Nitrobenzene-d5(Sum)
63
64-105
0226/1912:10
022711909:11
1
Phenol-d5 (Sum)
86
47-105
02/26r19 1210
0227119 09:11
1
Terphenyl-d14 (Sum)
75
45-130
02/26/19 12:10
0227/19 09. 11
1
Lab Sample ID: LCS 180-27136712-A
Matrix: Solid
Analysis Batch: 271438
Analyte
1,4-Dichlorobemene
2,4,5-Trichlorophenol
2,4,6-Trchlorophenol
2,4-131nitrotoluene
Hexachlorobenzene
Henchlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Cresols
LCS LCS
Surrogate
%Recovery Qualifier
2,4,6-Tribromophenol(Sum)
88
2-F/uorophenol(Sum)
90
2-F/uorobiphenyl
86
Nitrobenzene-d5(Surr)
90
Phenol-d5 (Sum)
90
Terphenyl-d14 (Sum)
69
Lab Sample ID: LCSD 180-27136713-A
Matrix: Solid
Analysis Batch: 271438
Analyte
1,4-Dichlorobenzene
2,4,5-Tnchlorophenol
Spike
LCS LCS
Added
Result Qualifier
0.250
0.2277
0.250
02157
0.250
0.2096
0.250
0.2023
0.250
0.1527
0.250
0.2146
D.250
0.2352
0.250
0.2299
0.250
0,1630 J
0.250
0.2391
0,750
0.6754
Limits
25-112
61-105
62-105
64-105
47-105
45-130
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271367
%Rea.
Unit
D %Rec
Limits
m9/L
91
57-190
mg/L
86
58-100
mg/L
84
57-100
mg/L
81
40-100
mg/L
61
38-100
mg/L
86
53-105
mg/L
94
57-100
mg/L
92
56-103
mg/L
65
16-100
mg/L
96
51 -107
mg/L
90
54-103
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 271367
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0.250 0.2220 mg/L 89 57-10o '3 16
0.250 0.2095 mg/L 54 58-100 3 16
TestAmerica Nashville
Page 11 of 31
3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 180-271367/3-A
Client Sample ID:
Lab Control Sample
Dup
Matrix: Solid
Prep Type:
Total/NA
Analysis Batch: 271438
Prep Batch:
271367
Spike
LCSD LCSD
%Rec.
RPD
Analyte
Added
Result Qualifier Unit D %Rec
Limits
RPD
Limit
2,4,6-Trichlorophenol
0.250
0.2135
mg/L
85
57-100
2
15
2,4-Dinitrotoluene
0.250
0,1977
mg/L
79
40-100
2
15
Hexachlorobenzene
0.250
0.1553
mg/L
62
38-100
2
16
Hexachlorobutadiene
0,250
0.2085
mg/L
83
53-105
3
15
Hexachloroethane
0.250
0.2259
mg/L
90
57-100
4
18
Nitrobenzene
0.250
0.2141
mg/L
86
56-103
7
15
Pentachlorophenol
0.250
0.1462 J
mg/L
58
16-100
11
24
Pyridine
0250
0.2257
mg/L
90
51-107
6
18
Cresols
0.750
0.6719
mg/L
90
54-103
1
17
Surrogate
LCSD LCSD
%Recovery Qualifier
Limits
2,4.6-Tribromophenol(Surr)
86
25-112
2-F/uorophenol (Sure)
86
61-105
2-Fluombipheny/
86
62-105
Nitrobenzene-d5 (Sun)
84
64-105
Phenol-d5 (Surr)
86
47-105
TerphenX-dl4(Surr)
68
45-130
Lab Sample ID: LB 180-27127411-D
Matrix: Solid
Analysis Batch: 271438
Analyte
LB LB
Result Qualifier
RL
MDL Unit
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 271367
D Prepared Analyzed DII Fac
1,4-Dichlorobenzene
ND
0.0500
mg/L
0212611912:10
0212711911:33
1
2,4,5-Tdchlorophenol
ND
0.0500
mg/L
02126/1912:10
02127/1911:33
1
2,4,6-Tdchlorophenol
ND
0.0500
mg/L
02/26/1912:10
02127/1911:33
1
2.4-Dinitrotoluene
ND
0.0500
mg/L
02/26/1912:10
02/2711911:33.
1
Hexachlorobenzene
ND
0.0500
mg/L
0212611912:10
02127/1911:33
1
Hexachlorobutadiene
ND
0.0500
mg/L
0212611912:10
0227/1911:33
1
Hexachlomethane
ND
0.0500
mg/L
02126119 12:10
0212711911:33
1
Nitrobenzene
ND
0.0500
mg/L
0226/1912:10
0227/1911:33
1
Pentachlorophenol
ND
0.250
mg/L
0226/1912:10
022711911:33
1
Pyddine
ND
0.100
mg/L
0226/1912:10
0227/1911:33
1
Cresols
ND
0.100
mg/L
02126/1912:10
02127/1911:33
1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2, 4, 6-Tribromophenol(Surr)
88
25-112
0226/1912:10
0227/1911:33
1
2-Fluorophenol (Surr)
85
61-105
0226(19 12. 10
0227/19 11:33
1
2-Fluorobiphenyl
85
62-105
0226/1912:10
0212711911:33
1
Nitrobenzene-d5 (Surr)
87
64 -105
02/26/19 12:10
0227/19 11:33
1
Phenol-d5 (Sun)
87
47-105
0226119 12;10
0227/19 11:33
1
Terphenyl-d14(Sum)
74
45-130
022611912;10
022711911:33
1
TestAmerica Nashville
L
Page 12 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Method: EPA 8081 B - Organochlorine Pesticides (GC)
Lab Sample ID: MB 180-27136611-A
Matrix: Solid
Analysis Batch: 271475
Analyte
NIB MB
Result Qualifier
RL
Chlordane (technical)
ND
0.00500
Endrin
ND
0.000500
gamma-BHC (Lindane)
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500
Toxaphene
ND
0.0400
MB MS
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surf)
94
62 -150
Tehachlom-m-xylene
91
54-138
Lab Sample ID: LCS 180-271365/2-A
Matrix: Solid
Analysis Batch: 271475
Analyte
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
TestAmerica Job ID: 490-168890-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271365
MDL Unit
D Prepared
Analyzed
Dil Fee
m91L
0226119 11:00
02127/19 13:14
1
mg/L
02/26M911:00
02127/1013:14
1
mg/L
02/26/1911;00
0212711913,14
1
mg/L
02/26/19 11:00
02/27119 13:14
1
mg/L
02126/1911:00
02127/1913:14
1
mg1L
0212611911:00
02/27/1913:14
1
mg/L
02/26/1911:00
0212711913:14
1
Prepared
Analyzed
Dil Fac
02126/1911:00
0212711913: 14
1
02261191100
0212711913: 14
1
Spike
Added
LCS LCS
Result Qualifier
0.0100
0009924
0.0100
0.008481
0.0100
0.009290
0.0100
0.008870
0.0100
0.01001
LCS LCS
Surrogate %Recovery Qualifier Limits
DCB Decachlombiphenyl (Surf) 95 62-150
Tetrachlor m-xylene 96 54-138
Lab Sample ID: LCSD 180-27136513-A
Matrix: Solid
Analysis Batch: 271475
Analyte
Endrin
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Client Sample ID:
Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271365
%Rec.
Unit
D %Rec
Limits
mg/L
99
71 -134
mg/L
85
66 -127
mg/L
93
66.134
mg/L
89
65-141
mglL
100
59-131
Client Sample ID:
Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 271365
Spike
LCSD LCSD
%Rec. RPD
Added
Result Qualifier
Unit D %Rec
Limits RPD Limit
0.0101)
0.009900
mg/L
99
71 134 -0 18
0.0100
0.008743
mg/L
87
66-127 3 15
0.0100
0.009428
mg/L
94
66-134 1 15
0.0100
0.008791
mg/L
88
65-141 1 15
0.0100
0.009889
mg/L
99
59-131 1 28
LCSD LCSD
Surrogate %,Recovery Qualifier Limits
DCB Decach/orobipheny/(Surd 95 62-150
Tetmchloro-m-xylene 93 54-138
TestAmerica Nashville
Page 13 of 31
3/6/2019

QC Sample Results
Client: Bio-NOmics Services., Inc.
Project/Site: McCall Farms
Method: EPA 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LB 180-271274116-E
Matrix: Solid
Analysis Batch: 271475
Analyte
LB LB
Result Qualifier
RL
Chlordane (technical)
NO
0.0050o
Enddn
NO
0.000500
gamma-BHC (Undane)
NO
0.000500
Heptachlor
NO
0.000500
Heptachlor epoxide
NO
0-000500
Methoxychlor
NO
0.000500
Toxephene
NO
0.0400
LB LB
Surrogate
%Recovery Qualifier
Limits
DCB Decachlombiphenyl (Surf)
98
62. 150
Tehachlom-m-xylene
92
54-130
TestAmerica Job ID: 490-168890-1
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch:271365
MDL Unit
D Prepared
Analyzed
oil Fac
m9/L
522611 11100
0212711 114:15
1
mg/L
02126/1911:00
0227/1914:15
1
mg/L
02/26/1911:00
0227/1914:15
1
mg/L
02/26/1911:00
0227/191415
1
mg/L
02126/1911:00
0227/1914:15
1
mg/L
0212611911;00
0227/1914:15
1
mg/L
02/26/1911:00
02/27/1914:15
1
Prepared
Analyzed
Oil Fac
0226/1911.00
0227/1914: 15
1
0226/1911:00
0227/1914:15
1
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: MB 180-27147611-A
Matrix: Solid
Analysis Batch:271567
Analyte
MB MB
Result Qualifier
RL
PCB-1016
ND
16.7
PCB-1221
NO
16.7
PCB-1232
NO
16.7
PCB-1242
NO
16.7
PCB-1248
NO
16.7
PCB-1254
NO
16.7
PCB-1260
NO
16.7
MB MB
Surrogate
%Recovery Qualifier
Limits
Tehachlor m-xylene (Sur)
91
51- 1 66
DCB Decachlombiphenyl (Sun)
94
44 - 116
Lab Sample ID: LCS 180-27147612-A
Matrix: Solid
Analysis Batch:271567
Analyte
PCB-1016
PCB-1260
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch:271476
MDL Unit
D Prepared
Analyzed
Oil Fac
ug/Kg
0227/1 009:52
0212811 113:54
1
ug/Kg
0227119 09:52
02/28/1913:54
1
ug/Kg
0227119 09:52
0228/19 13:54
1
ug/Kg
0227/19 09:52
0228119 13:54
1
ug/Kg
0227/19 09:52
02/26/19 13:54
1
ug/Kg
02/27/19 09:52
02/2811913:54
1
ug/Kg
02/27/19 09:52
02/28/19 13:54
1
Prepared
Analyzed
Oil Fac
0227119 09: 52
0228/19 13:54
1
022711909:52
0228/1913:54
1
Spike
LCS LCS
Added
Result Qualifier
1330
1090
1330
1059
LCS LCS
Surrogate %Recovery Qualifier Limits
Tetrech/om- xylene (Sum) 85 51- 116
DCB Decachlorobiphenyl (Sun) 87 44 -116
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch:271476
%Rec.
Unit D %Rec Limits
ug/Kg 82 57- 114
ug/Kg 79 55-112
TestAmerica Nashville
Page 14 of 31
3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Lab Sample ID: 490-168890-1 MS
Matrix: Sludge
Analysis Batch: 271567
Sample Sample
Spike
MS MS
Analyte
Result Qualifier
Added
Result Qualifier
PCB-1016
ND
2610
1775
PCB-1260
ND
2610
1824
MS MS
Surrogate
%Recovery QualMer Limits
Tetrachloro-m-zylene (Sun)
66 5l - 116
DCB Decachlorobiphenyl(Sum)
72 44-116
Lab Sample ID: 490-168890-1 MSD
Matrix: Sludge
Analysis Batch:271567
Sample Sample
Spike
MSD MSD
Analyte
Result Qualifier
Added
Result Qualifier
PCB-1016
ND
2520
1626
PCB-1260
ND
2520
1636
MSD MSD
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene (Sum) 64 51-116
DCB Decach/orobiphenyl (Sun) 71 44 -116
Method: EPA 8151A - Herbicides (GC)
Lab Sample ID:
MB 180-271391/1-A
Matrix: Solid
Analysis Batch:
271565
MB MB
Analyte
Result Qualifier
RL
2,4-D
ND
O.D400
Silvex (2,4,5-TP)
ND
0.0100
2,4,5-T
ND
0.0100
MB MB
Surrogate %Recovery Qualifier Limits
24-Dich/omphenylamb'c acid 77 —20-TO-5-
Client Sample ID: McCall Farms
Prep Type: Total/NA
Prep Batch:271476
%Rec.
Unit D %Rec Limits
uglKg v 68 57_114
uglKg ❑ 70 55-112
Client Sample ID: McCall Farms
Prep Type: Total/NA
Prep Batch:271476
%Rec. RPD
Unit D %Rec Limits RPD Limit
ug/Kg 64 57_114 9 34
ug/Kg # 65 55-112 11 16
Client Sample ID: Method Blank
Prep Type: TotalINA
Prep Batch: 271391
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02126/19 14:30
02/27/19 20:57
20
mg/L
02/26/19 14:30
02/27/19 20:57
20
mg/L
02/26119 14:30
02/27/19 20:57
20
Prepared
Analyzed
Dil Fac
02126119 14:30
02/27/19 20:57
20
Lab Sample ID: LCS 180-271391/2-A
Matrix: Solid
Analysis Batch: 271555
Spike
LCS LCS
Analyte
Added
Result Qualifier
2,4-D
0.200
0.1340
Silvex(2,4,5-TP)
0.0500
0.03454
2,4,5-T
0.0500
0.02981
LCS LCS
Surrogate %Recovery Qualfier
Limits
2,4-Dichlorophenylacetic acid 67
20-105
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271391
%Rec.
Unit D %Rec Limits
mg/L 67 10-100
mg/L 69 23-109
mg/L 60 11 -101
TestAmerica Nashville
Page 15 of 31 3/6/2019

QC Sample Results
Client: Bic-Nomics Services., Inc.
TeStAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: EPA M51A - Herbicides (GC) (Continued)
Lab Sample ID: LCSD 180-271391/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271555
Prep Batch: 271391
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
2,4-D
0.200
0.1578
mg/L 79 10-100 16 35
Silvex (2,4,5-TP)
0.0500
0.04003
mg/L 80 23. 109 15 35
2,4,5-T
0.0500
0,03558
mg/L 71 11-101 18 35
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
L2,4-Dichlomphenylacefic acid 78
20-105
Lab Sample ID: LB 180-271274/16-G
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271555
Prep Batch:271391
LB LB
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
2.4-D ND
0.0400
mg/L
02/26/1914:30 02127/1922:24 20
Silvex(2,4,5-TP) ND
0.0100
mg/L
02/2611914:30 0212711922:24 20
2,4,5-T ND
0,0100
mg/L
02/2611914:30 02/27/1922:24 20
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
2,4-Dichlomphenylacetic acid 60
20-105
OM6119 14:30 0227/19 22:24 20
Method: EPA 6010D - Metals (ICP)
Lab Sample ID: MB 180-271365/1-A
Client Sample ID: Method Blank
L--
Matrix: Solid
Prep Type: Total/NA
Analysis Batch:271499
Prep Batch:271355
i MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed oil Fac
Arsenic ND
0.0500
mg/L
02126/1912:20 0212711907*50 1
Barium ND
0.200
mg/L
02/2611912:20 02/27/1907:50 1
Cadmium ND
0.0500
mg/L
02/26/1912:20 02127/1907:50 1
Chromium ND
0.0500
mg/L
02/26/1912:20 02127/1907:50 1
Lead ND
0.0500
mg/L
02126/1912:20 02127/1907:50 1
Selenium ND
0.0500
mg/L
02/26/19 12:20 02/27/19 07:50 1
Silver ND
0.0500
mg/L
02/2611912:20 02/27/1907:50 1
[Lab Sample ID: LCS 180-27135512-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271499
Prep Batch:271355
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Arsenic
0.500
0.5281
mg/L 106 80-120
Barium
2.00
1051
mg/L 103 80-120
Cadmium
0.0500 0.05449
mg/L 109 80.120
Chromium
0.200
0.2054
mg/L 103 80.120
Lead
0.500
0.5102
mg/L 102 80-120
Selenium
0.500
0.5558
mg/L Ill 80-120
Silver
0.0500 0.05381
mg/L 108 80-120
TestAmerica Nashville
Page 16 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Method: EPA 6010D -Metals (ICP) (Continued)
Lab Sample ID: LB 180-271274/1-C
Matrix: Solid
Analysis Batch: 271499
LB LB
Analyte
Result Qualifier
Arsenic
ND
Barium
ND
Cadmium
ND
Chromium
NO
Lead
ND
Selenium
ND
Silver
ND
Method: EPA 7470A - Mercury (CVAA)
TestAmerica Job ID: 490-168890-1
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch:271355
RL
MDL Unit
D Prepared
Analyzed oil Fac
0.500
mg/L
0-2 26/19 1220
62/27/19 08:00 1
2.00
mg/L
02/26/19 12:20
02/27/19 08:00 1
0.500
mg/L
02/26/19 12:20
02/27/19 08:00 1`'
0,500
mg/L
02/261191220
L
02/27/1908:00 1
0.500
mg/L
02/26119 12:20
02/27/19 08:00 1
0.500
mg/L
02/26119 12:20
02/27/19 08:00 1
0.500
mg/L
02/26/1912:20
0212711908:00 1
Lab Sample ID: MB 180-271342/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271395
Prep Batch: 271342
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed oil Fac
Mercury ND
0.000200 mg/L
02/2611911:05 02/26/1916:00 1
Lab Sample ID: LCS 180-27134212-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271395
Prep Batch: 271342
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Mercury
0.00250
0.002605
mg/L 104 80-120
Lab Sample ID: LB 180-27127411-B
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
LB LB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed oil Fac
Mercury ND
0.000200 mg/L
02/26/1 11105 02/26/t91602 1
Lab Sample ID: 180-86915-A-1-1 MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits
Mercury ND
0.00500
0.005020
mg/L 100 75-125
Lab Sample ID: 180-86915-A-1.1 MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Mercury ND
0.0 5500
0.00 0026
mg/L --1W 75- 225 0 20
TestAmerica Nashville
Page 17 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Method: 1010A - Ignitability, Pensky-Martens Closed -Cup Method
Lab Sample ID: MB 490-578372/1
Matrix: Solid
Analysis Batch: 578372
MB MB
Analyte Result Qualifier RL
Flashpoint >200 1.00
Lab Sample ID: LCS 490-57837212
Matrix: Solid
Analysis Batch: 578372
TestAmerica Job ID: 490-168890-1
Client Sample ID: Method Blank
Prep Type: Total/NA
RL Unit D Prepared Analyzed Dil Fee
Degrees F 03/01/19 1729 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Flashpoint
81.0
81.20
Degrees F
100
94 -106
Lab Sample ID: LCSD 490-578372114
Matrix: Solid
Analysis Batch: 578372
Client Sample
ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Flashpoint
81.0
83.40
Degrees F
103
94.106 3 20
Lab Sample ID: 280-120182-A-1 DU
Matrix: Solid
Analysis Batch: 578372
Sample Sample
Analyte Result Qualifier
Flashpoint 128
Method: 2540G - SM 2540G
Lab Sample ID: 180-86358-B-20 DU
Matrix: Solid
Analysis Batch: 271460
Sample Sample
Analyte Result Qualifier
Percent Moisture 26.5
Percent Solids 73.5
DU DU
Result Qualifier Unit D
134.3 Degrees F
Client Sample ID: Duplicate
Prep Type: Total/NA
RPD
RPD Limit
5 10
Client Sample ID: Duplicate
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
28.2 °/ 6 0
71.8 % 2 10
Method: EPA 9012B - Cyanider Total andor Amenable
Lab Sample ID: MB 180-271760/4-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271809 Prep Batch: 271760
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fee
Cyanide, Total ND a500 mg/Kg 03/01/19 12:40 03/01/1919:23 1
Lab Sample ID: HLCS 180-271760/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: Prep Batch:271760
Spike HLCS HLCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Cyanide, Total 0.250 0.2479 mg/Kg 99 90-110
TestAmerica Nashville
Page 18 of 31
3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
ProjecttSite: McCall Farms
Method: EPA 90128 - Cyanide, Total andor Amenable (Continued)
Lab Sample ID: LCS 180-271760/3-A
Matrix: Solid
Analysis Batch: 271809
Analyte
Cyanide, Total
FLab Sample ID: LLCS 180-27176011-A
Matrix: Solid
Analysis Batch: 271809
Analyte
Cyanide, Total
Lab Sample ID: 180-87076-D-1-B MS
Matrix: Solid
Analysis Batch: 271809
Sample Sample
Analyte Result Qualifier
Cyanide, Total 2.35
Lab Sample ID: 180-87076-D-1-C MSD
Matrix: Solid
Analysis Batch: 271809
Sample Sample
Analyte Result Qualifier
Cyanide, Total 2.35
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch:271760
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
190 114.2 mg/Kg 60 26 -139
Client Sample ID: Lab Control Sample''
Prep Type: Total/NA
Prep Batch:271760
Spike LLCS LLCS %Rec.
Added Result Qualifier Unit D %Rec Limits
0,0500 0.04970 mg/Kg 99 90 -110
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch:271760
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
18.1 18.61 mg/Kg 8 90 75 -125
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 271760
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
18.1 18.92 mg/Kg 0 91 75 -125 2 20
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 180-27131911-A
Matrix: Solid
Analysis Batch:271334
MIS MB
Analyte Result Qualifier RL
Sulfide ND 30.0
Lab Sample ID: LCS 180-27131912-A
Matrix: Solid
Analysis Batch:271334
Analyte
Sulfide
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch:271319
MDL Unit D Prepared Analyzed Dil Fee
mg/Kg 62/26/1 009:35 02/2611 111:15 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271319
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
150 144.3 mg/Kg 97 85-115
Lab Sample ID: 490-168890-1 MS Client Sample ID: McCall Farms
Matrix: Sludge Prep Type: Total/NA
Analysis Batch:271334 Prep Batch:271319
Sample Sample Spike MS MS %Rec.
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits
Sulfide 111 293 436.2 mg/Kg a 111 75-125
TestAmerica Nashville
Page 19 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID:490-168890-1
Project/Site: McCall Farms
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: 490-168890-1 MSD Client Sample ID: McCall Farms
Matrix: Sludge Prep Type: Total/NA
Analysis Batch: 271334 Prep Batch: 271319
Sample Sample Spike MSD MSD %Rec. RPD
LAnalyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Sulida 111 292 408.7 mg/Kg 102 75-125 7 20
Method: EPA 9045D - pH
Lab Sample ID: LCS 180-271506/1 Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch:271506
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
PH 7.00 7.0 SU 101 99-101
Lab Sample ID: 180-86977.J-1 DU Client Sample ID: Duplicate
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271506
Sample Sample DU DU RPD
Analyte Result Qualifier Result Qualifier Unit D RPD Limit
LpH 3.6 3.6 SU 0 2
TestAmerica Nashville
Page 20 of 31 3/6/2019

QC Association Summary
Client: Bic-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
GC/MS VOA
Analysis Batch: 271299
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 8260D
271312
LB 180-271312/1-A
Method Blank
TCLP
Solid
EPA 8260D
271312
LCS 180-27129913
Lab Control Sample
Total/NA
Solid
EPA B260D
490-168891-A-1-B MS
Matrix Spike
TCLP
Solid
EPA 8260D
271312
490-168891-A-1-C MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 8260D
271312
Leach Batch: 271312
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 13 11
LB 180-271312/1-A
Method Blank
TCLP
Solid
EPA 1311
490-168891-A-1-B MS
Matrix Spike
TCLP
Solid
EPA 1311
490-168891-A-1-C MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 1311
Semi VOA
Leach Batch: 271274
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168690-1
McCall Farms
TCLP
Sludge
EPA 1311
LB 180-27127411-D
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 271367
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
3510C
271274
LB 180-271274/1-D
Method Blank
TCLP
Solid
3510C
271274
MB 180-271367/1-A
Method Blank
Total/NA
Solid
3510C
LCS 180-271367/2-A
Lab Control Sample
Total/NA
Solid
3510C
LCSD 180-27136713-A
Lab Control Sample Dup
Total/NA
Solid
351 OC
Analysis Batch: 271438
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Fans
TCLP
Sludge
6270E
271367
LB 180-271274/1-0
Method Blank
TCLP
Solid
8270E
271367
MB 180-271367/1-A
Method Blank
Total/NA
Solid
8270E
271367
LCS 180-271367/2-A
Lab Control Sample
Total/NA
Solid
8270E
271367
LCSD 180-27136713-A
Lab Control Sample Dup
Total/NA
Solid
8270E
271367
VOA
Leach Batch: 271274
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Fans
TCLP
Sludge
EPA 13 11
LB 180-271274/16-E
Method Blank
TCLP
Solid
EPA 1311
LB 180-271274116-G
Method Blank
TCLP
Solid
EPA 1311
Prep Batch:271365
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
3510C
271274
LB 180-271274/16-E
Method Blank
TCLP
Solid
351 CC
271274
MB 180-271365/1-A
Method Blank
Total/NA
Solid
3510C
LCS 180-271365/2-A
Lab Control Sample
Total/NA
Solid
3510C
TestAmerica Nashville
Page21 of'31 3/6/2019

QC Association Summary
Client: Bio-Nomics Services., Inc. TestAmenca Job ID: 490-168890-1
Project/Site: McCall Farms
GC Semi VOA (Continued)
Prep Batch: 271366 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LCSD 180-271365/3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Prep Batch: 271391
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
8151A
271274
LB 180-271274116-G
Method Blank
TCLP
Solid
8151A
271274
MB 180-271391/1-A
Method Blank
Total/NA
Solid
8151A
LCS 180-271391/2-A
Lab Control Sample
Total/NA
Solid
8151A
'
LCSD 180-27139113-A
Lab Control Sample Dup
Total/NA
Solid
8151A
Analysis Batch: 271475
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 808 BB
271365
LB 180-271274/16-E
Method Blank
TCLP
Solid
EPA 8081 B
271365
MB 180-271365/1-A
Method Blank
Total/NA
Solid
EPA8081B
271365
LCS 180-271365/2-A
Lab Control Sample
Total/NA
Solid
EPA 80818
271365
LCSD 100-271365/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8081B
271365
Prep Batch: 271476
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
3541
MB 180-27147611-A
Method Blank
Total/NA
Solid
3541
LCS 180-271476/2-A
Lab Control Sample
Total/NA
Solid
3541
490-168890-1 MS
McCall Farms
Total/NA
Sludge
3541
490-168890-1 MSD
McCall Farms
Total/NA
Sludge
3541
Analysis Batch: 271565
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-16a890-1
McCall Farms
TCLP
Sludge
EPA 8151A
271391
LB 180-271274/16-G
Method Blank
TCLP
Solid
EPA 8151A
271391
MB 180-271391/1-A
Method Blank
Total/NA
Solid
EPA 8151A
271391
LCS 180-271391/2-A
Lab Control Sample
Total/NA
Solid
EPA 8151A
271391
LCSD 180-271391/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8151A
271391
Analysis Batch: 271567
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
EPA 8082A
271476
MB 180-271476/1-A
Method Blank
Total/NA
Solid
EPA 8082A
271476
LCS 180-27147612-A
Lab Control Sample
Total/NA
Solid
EPA 8082A
271476
490-168890-1 MS
McCall Farms
Total/NA
Sludge
EPA 8082A
271476
490-168890-1 MSD
McCall Farms
Total/NA
Sludge
EPA 8082A
271476
Metals
Leach Batch: 271274
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 13 11
LB 180-27127411-B
Method Blank
TCLP
Solid
EPA 1311
LB 180-271274/1-C
Method Blank
TCLP
Solid
EPA 1311
180-86915-A-1-1 MS
Matrix Spike
TCLP
Solid
EPA 1311
TestAmerica Nashville
Page 22 of 31 3/6/2019

QC Association Summary
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Metals (Continued)
Leach Batch: 271274 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-86915-A-1-J MSD Matrix Spike Duplicate
TCLP
Solid
EPA 1311
Prep Batch: 271342
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1 McCall Farms
TCLP
Sludge
7470A
271274
LB 180-27127411-B Method Blank
TCLP
Solid
7470A
271274
MB 180-27134211-A Method Blank
Total/NA
Solid
7470A
LCS 180-27134212-A Lab Control Sample
Total/NA
Solid
7470A
'
180-86915-A-1-1 MS Matrix Spike
TCLP
Solid
7470A
271274
180-86915-A-1-J MSD Matrix Spike Duplicate
TCLP
Solid
7470A
271274
Prep Batch: 271355
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
3010A
271274
LB 180-27127411-C
Method Blank
TCLP
Solid
3010A
271274
MB 180-27135511-A
Method Blank
Total/NA
Solid
3010A
LCS 180-2713552-A
Lab Control Sample
Total/NA
Solid
301 DA
Analysis Batch:271396
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 7470A
271342
LB 180-27127411-B
Method Blank
TCLP
Solid
EPA 7470A
271342
MB 180-271342/1-A
Method Blank
Total/NA
Solid
EPA 7470A
271342
LCS 180-2713422-A
Lab Control Sample
Total/NA
Solid
EPA 7470A
271342
180-86915-A-1-1 MS
Matrix Spike
TCLP
Solid
EPA 7470A
271342
180-86915-A-1-J MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 7470A
271342
Analysis Batch: 271499
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 6010D
271355
LB 180-271274/1-C
Method Blank
TCLP
Solid
EPA 6010D
271355
MB 180-271355/1-A
Method Blank
Total/NA
Solid
EPA 601 OD
271355
LCS 180-27135512-A
Lab Control Sample
Total/NA
Solid
EPA 6010D
271355
General Chemistry
Prep Batch: 271319
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-16BB90-1
McCall Farms
Total/NA
Sludge
9030B
MB 180-27131911-A
Method Blank
Total/NA
Solid
9030E
LCS 180-2713192-A
Lab Control Sample
Total/NA
Solid
9030B
490-168890-1 MS
McCall Farms
Total/NA
Sludge
9030E
490-168890-1 MSD
McCall Farms
Total/NA
Sludge
9030E
Analysis Batch: 271334
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
EPA 9034
271319
MB 180-27131911-A
Method Blank
Total/NA
Solid
EPA 9034
271319
LCS 180-27131912-A
Lab Control Sample
Total/NA
Solid
EPA 9034
271319
490-168890-1 MS
McCall Farms
Total/NA
Sludge
EPA 9034
271319
TestAmenca Nashville
Page 23 of 31 3/6/2019

QC Association Summary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
General Chemistry (Continued)
Analysis Batch: 271334 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1 MSD
McCall Farms
Total/NA
Sludge
EPA 9034
271319
Analysis Batch: 271450
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
2540G
180-86358-B-20 DU
Duplicate
Total(NA
Solid
254OG
Analysis Batch: 271506
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
EPA 9045D
LCS 180-271506/1
Lab Control Sample
Total/NA
Solid
EPA 9045D
180-86977-J-1 DU
Duplicate
Total/NA
Solid
EPA 9045D
Prep Batch: 271760
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168890-1
McCall Fans
Total/NA
Sludge
9012B
MB 180-27176014-A
Method Blank
Total/NA
Solid
9012E
HLCS 180-2717602-A
Lab Control Sample
Total/NA
Solid
9012B
LCS 180-271760/3-A
Lab Control Sample
Total/NA
Solid
90128
LLCS 180-27176011-A
Lab Control Sample
Total/NA
Solid
9012E
180-87076-D-1-8 MS
Matrix Spike
Total/NA
Solid
9012B
180-87076-D-1-C MSD
Matrix Spike Duplicate
Total/NA
Solid
9012E
Analysis Batch: 271809
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
EPA 9012B
271760
MB 180-271760/4-A
Method Blank
Total/NA
Solid
EPA 9012E
271760
HLCS 180-2717602-A
Lab Control Sample
Total/NA
Solid
EPA 9012B
271760
LCS 180-27176013-A
Lab Control Sample
Total/NA
Solid
EPA 9012E
271760
LLCS 180-27176011-A
Lab Control Sample
Total/NA
Solid
EPA 9012B
271760
180-87076-D-1-B MS
Matrix Spike
Total/NA
Solid
EPA 9012E
271760
180-87076-D-1-C MSD
Matrix Spike Duplicate
Total/NA
Solid
EPA 9012E
271760
Analysis Batch:578372
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
1010A
MB 490-57837211
Method Blank
Total/NA
Solid
1010A
LCS 490-5783722
Lab Control Sample
Total/NA
Solid
1010A
LCSD 490578372/14
Lab Control Sample Dup
Total/NA
Solid
1010A
280.120182-A-1 DU
Duplicate
Total/NA
Solid
1010A
TestAmerica Nashville
Page 24 of 31 3/6/2019

Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Client Sample ID: McCall Farms
Date Collected: 02/1911910:00
Date Received: 02/21/19 08:55
Batch
Batch
Prep Type
Type
Method Run
TCLP
Leach
EPA 1311
TCLP
Analysis
EPA 8260D
TCLP
Leach
EPA 1311
TCLP
Prep
3510C
TCLP
Analysis
827DE
TCLP
Leach
EPA 1311
TCLP
Prep
3510C
TCLP
Analysis
EPA8081B
TCLP
Leach
EPA 1311
TCLP
Prep
8151A
TCLP
Analysis
EPA8151A
TCLP
Leach
EPA 1311
TCLP
Prep
3010A
TCLP
Analysis
EPA 601 OD
TCLP
Leach
EPA 1311
TCLP
Prep
7470A
TCLP
Analysis
EPA 7470A
Total/NA
Analysis
1010A
Total/NA
Analysis
254OG
Total/NA
Analysis
EPA 9045D
Lab Chronicle
TestAmerica Job ID: 490-168890-1
Lab Sample ID: 490-168890-1
Matrix: Sludge
oil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
259
500 mL
271312
02/26/19 08:16
TAH
TAL PIT
1
0.125 mL
5 mL
271299
02/26/19 10:29
KLG
TAL PIT
100 g
2000 mL
271274
02/25119 16:00
MTT
TAL PIT
200 mL
10.0 mL
271367
02/26/19 12:10
CBY
TAL PIT
1
1 mL
1 mL
271438
02/27/1916:57
WP
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
10D mL
40.0 mL
271365
02/26/19 11:00
CBY
TAL PIT
1
271475
02127/19 15:48
DFE
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
100 mL
10.0 mL
271391
02/26/19 14:30
CBY
TAL PIT
20
271555
02128/1900:53
JBF
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
5 mL
50 mL
271355
02/26/19 12:20
NAM
TAL PIT
1
271499
02/27/19 09:08
RJG
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
50 mL
50 mL
271342
02/26/1911:05
RJR
TAL PIT
1
271395
02/26/19 16:16
KA
TAL PIT
1
578372
03/01/19 17:29
VRP
TAL NSH
1
271450
02/27/19 08:43
JMS
TAL PIT
1
20.05 g
20 mL
271506
02/27/19 12:00
JMS
TAL PIT
Client Sample ID: McCall Farms Lab Sample ID: 490-168890-1
Date Collected: 02/19/1910:00 Matrix: Sludge
Date Received: 02/21/19 08:55 Percent Solids: 51.2
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Prep
3541
Total/NA
Analysis
EPA 8082A
Total/NA
Prep
9012E
Total/NA
Analysis
EPA 9012B
Total/NA
Prep
9030E
Total/NA
Analysis
EPA 9034
oil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
15.1 g
20.0 mL
271476
02127119 09:52
BAP
TAL PIT
1
271567
02/28/19 14:50
JMO
TAL PIT
1.04 g
50 mL
271760
03/01/19 12:40
BSH
TAL PIT
1
271809
03/01/19 19:30
JAB
TAL PIT
5.03 g
50 mL
271319
02126/19 09:35
SES
TAL PIT
1
271334
02/26/19 11:22
SES
TAL PIT
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
Page 25 of 31
3/6/2019

Method Summary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method
Method Description
Protocol
Laboratory
EPA 8260D
Volatile Organic Compounds by GC/MS
SW846
TAL PIT
8270E
Semivolatile Organic Compounds (GC/MS)
SW846
TAL PIT
EPA 8081 B
Organochlorine Pesticides (GC)
SW846
TAL PIT
EPA 8082A
Polychlorinated Biphenyls (PCBs) by Gas Chromatography
SW846
TAL PIT
EPA 8151A
Herbicides (GC)
SW846
TAL PIT
EPA 6010D
Metals (ICP)
SW846
TAL PIT
EPA 7470A
Mercury (CVAA)
SW846
TAL PIT
1010A
Ignitability, Pensky-Martens Closed -Cup Method
SW846
TAL NSH
2540G
SM 2540G
SM22
TAL PIT
EPA 9012B
Cyanide, Total andor Amenable
SW846
TAL PIT
EPA 9034
Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL PIT
EPA 9045D
pH
SW846
TAL PIT
3010A
Preparation, Total Metals
SW846
TAL PIT
3510C
Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL PIT
m
3541
Automated Soxhlet Extraction
SW846
TAL PIT
5030C
Purge and Trap
SW846
TAL PIT
7470A
Preparation, Mercury
SW846
TAL PIT
8151A
Extraction (Herbicides)
SW846
TAL PIT
9012B
Cyanide, Total and/or Amenable, Distillation
SW846
TAL PIT
9030E
Sulfide, Distillation (Acid Soluble and Insoluble)
SW846
TAL PIT
EPA 1311
TCLP Extraction
SW846
TAL PIT
Protocol References:
SM22 = Standard Methods For The Examination Of Water And Wastewater, 22nd Edition
SW846 ='Test Methods For Evaluating Solid Waste, Physical/Chemical Methods', Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
Page 26 of 31 3/6/2019

Accreditation/Certification Summary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project(Site: McCall Farms
Laboratory: TestAmerica Nashville
The accreditations/cerdfications listed below are applicable to this report.
LAuthority Program EPA Region Identification Number Expiration Date
South Carolina State Program 4 84009 [phone]
Laboratory: TestAmerica Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
South Carolina State Program 4 69014 04-30-19
The following analytes are included In this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method
Prep Method
Matrix
Analyte
254OG
Sludge
Percent Moisture
2540G
Sludge
Percent Solids
8270E
3510C
Sludge
1,4-Dichlombenzene
8270E
3510C
Sludge
2,4,5-Trichlorophenol
8270E
3510C
Sludge
2,4,6-Trichlorophenol
8270E
3510C
Sludge
2,4-Dinitrotoluene
8270E
3510C
Sludge
Cresols
8270E
3510C
Sludge
Hexachlorobenzene
6270E
3510C
Sludge
Hexachlorobutadiene
8270E
3510C
Sludge
Hexachloroethane
8270E
3510C
Sludge
Nitrobenzene
8270E
3510C
Sludge
Pentachlorophenol
8270E
3510C
Sludge
Pyridine
EPA8151A
8151A
Sludge
2,4,5-T
EPA8151A
8151A
Sludge
2,4-D
EPAS151A
8151A
Sludge
Silvex(2,4,5-TP)
EPA 8260D
Sludge
1,1-Dichlomethene
EPA 8260D
Sludge
1,2-Dichloroethane
EPA 8260D
Sludge
2-Butanone (MEK)
EPA 8260D
Sludge
Benzene
EPA 8260D
Sludge
Carbon tetrachloride
EPA 8260D
Sludge
Chlorobenzene
EPA 8260D
Sludge
Chloroform
EPA 8260D
Sludge
Tetrachloroethene
EPA 8260D
Sludge
Trchloroethene
EPA 8260D
Sludge
Vinyl chloride
EPA 9012E
9012B
Sludge
Cyanide, Total
Accreditation/Certification renewal pending - accreditation/certification considered valid.
TestAmerica Nashville
Page 27 of 31 3/6/2019

t
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN COOLER RECEIPT FORM
41910-11
Cooler Received/Opened Ort2/2112019 8:55
Time Samples Removed F omCCooler �r O Time Samples Placed In Storage f 5 �(� (2 Hour Window)
1. Tracking # 443. (last 4 digits, FeclEx) Courier: FeclEx
IR Gun to 17950358 pH Strip Lot Chlorine Strip Lot
2. Temperature of rep. sample or temp blank when opened: � Degries Ce/sfus
3. If Item #2 temperature is 0°C or less, was the representative sample or temp blank frozen? YES NO..CA)
4. Were custody seals on outside of cooler? X/�%% y, /Eg... NO.:NA
If yes, how many and where: l./
5. Were the seals Intact, signed, and dated correctly? '
�...NO...NA
6. Were custody papers Inside cooler?
C9 ...
NO ... NA
i
I certify that I opened the cooler and answered questions 1.6(intial)
7. Were custody seals an containers: YES N)
and Intact YES ...
NO...NA
Were these signed and dated correctly?
YES
NO..
...
8. Packing mat'I used? Bubblewrap Plastic bag Peanuts Vermiculite Foam Insert Paper Other None
'
9. Cooling process: Ic Ice -pack
Ice (direct contact) Dry ice Other
None
10—Did all containers arrive In good -condition (unbroken)? —
-- -- .. _. — _>•YFS...NO...NA
11. Were all container labels complete (#, date, signed, pres., etc)?
GE ...
NO ... NA
12. Did all container labels and tags agree with custody papers?
IE ...
NO ... NA
.
13a. Were VOA vials received?
r YES.5..NA
b. Was there any observable headspace present in any VOA vlal?
YES ...
s
NO... A
\J
19
Larger than this.
14. Was there a Trip Blank In this cooler? YES.(Na..NA If multiple coolers, sequence # I
I certify that I unloaded the cooler and answered oues0ons 7.14 lintial
15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level? YES ... N0..tf1A1
JJ
b. Did the bottle labels Indicate that the correct preservatives were used CVESI..NO... NA
16. Was resir{val chlorine present? _YES
..... NO..urA
I certify that I checked for chlorine and off as Per SOP and answered Questions 15-1611nt'all ������,d•
17. Were custody � apers properly 611ed out (ink, signed, etc)? ---
NO ... NA
18. Did you sign this custody'papers in the appropriate place? Y ...NO...NA
19. Were cpfrect containers usedYor the analysis requested? YE ...NO...NA I
20. Was sufficient amour of sample sent in each container? YE ..NO ... NA )
i 1 certify thrift entered this prolect into LIMS and answered au stlo 17-20 fintial) i
• I certify that I attached a label With the unique LIMB number to each container II gal)
21. Were ere.Non-Conformance Issues at login? YES...NO Was a NCM generated? YES., ...# ,
BIS a Broken it shipmliii(
Cooler Receipt Fonn.doc LF-I Revised 5/23117 I
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Page 30 of 31 3/6/2019

Login Sample Receipt Checklist
Client: Bio-Nomics Services- Inc. Job Number: 490-168890-1
SDG Number:
Login Number: 168890 List Source: TestAmerica Pittsburgh
List Number: 2 List Creation: 02/23119 11:33 AM
Creator: Say, Thomas C
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC7
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, ind. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked,
N/A
TestAmerica Nashville
Page 31 of 31 3/6/2019