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HomeMy WebLinkAboutWQ0001347_Residual Annual Report 2015_201601210 MillerCoors 863 E Meadow Road Eden, NC 27288-3636 January 15, 2016 CERTIFIED MAIL RETURN RECEIPT REQUESTED Mr. Ed Hardee NCDENR Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 RECEIVEDINCDEQIDWR JAN 2 1 2016 Non -Discharge Permitting Unit RF(,FI\IEQ JAN 21 2016 DWR SECTION INFORMATION PROCESSING UNIT RE: Annual Distribution and Marketing/Surface Disposal Certification and Summary Distribution of Process Residuals Permit Number WQ0001347 MillerCoors LLC, Eden, NC Dear Mr. Hardee: Please find enclosed the Annual Distribution and Marketing/Surface Disposal Certification and Summary for MillerCoors LLC located in Eden, Rockingham County, North Carolina. As discussed earlier this year, three additional samples were taken as a result of a communication error with our laboratory. Our lab did not get an updated list of parameters with our permit renewal. They were going off the old permit requirements, which did not require sampling for Arsenic, Mercury, Molybdenum, or Selenium. Per your request, additional samples were taken to ensure compliance and to make up for the missed analysis. Three copies of the following forms have been included: 1) Annual Distribution and Marketing/Surface Disposal Certification and Summary (Form DMSDF) 2) Annual Residual Sampling Summary Form (Form RSSF) 3) Annual Residual Sampling Summary Form (Form RSSF-B) 4) List of Recipient Information 5) 3 Copies of Lab Residual Analysis Results Please contact me if you should have any questions or comments at 336-627-2136 or via e-mail at eric.tillmanCaD_millercoors.com Sincerely, Eric Tillman Environmental & Sustainability Engineer cc: Audrey Templeton — Milwaukee, WI Jim Smith Mike Lozano Matt Toms ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM PERMIT #: WQ0001347 FACILITY NAME: MillerCoors LLC PHONE: 336-627-2100 COUNTY: Rockingham OPERATOR: MillerCoors LLC FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) 0 Distribution and Marketing (complete Parts A, B, and C) aiii-inn *ho nae* valendar vPar9 r❑ vec []No No If No skip parts A, B, C and certify form below VV IMa LAI%, la\.111 L,' ■u virvau . .b -- t.....--^-----"- J ---- - - - -- - - Part B*: Part A*: Volume (dry tons) Recipient Information Month Sources(s) (include NPDES # if applicable) Admendment/ Residual In Product Out Name(s) Volume d (ry Intended use(s) Bulking Agent tons) January NCO029980 4 163.71 167.71 See Attached Sheet February NCO029980 6.1 253.69 259.79 See Attached Sheet March NCO029980 4.7 192.96 197.66 See Attached Sheet April NCO029980 3.9 161.32 165.22 See Attached Sheet May NCO029980 1 41.98 42.98 See Attached Sheet June NCO029980 0.3 12.71 13.01 See Attached Sheet July NCO029980 0.6 24.34 24.94 See Attached Sheet August NCO029980 3 125.41 128.41 See Attached Sheet September NCO029980 3.4 139.37 142.77 See Attached Sheet October NCO029980 3.5 142.5 146 See Attached Sheet November NCO029980 3.2, 130.55 133.75 See Attached Sheet December NCO029980 1.7 68.46 1 70.16 - See Attached Sheet Totals: Annual (drytons): 35.4 1457 1492.4 .............. I ..... 0 Admendment s used: None Bulking Agent(s) used: Lime * If more space than given is required, please attach additional mtormation sheet(s). in Cnecx box it aaaitionai snec<<s) arc auaciicu Part C: Facility was compliant during calendar year 2015 with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Quality. R1 Yes ❑ No If No, please provide a written description why the facility was not. compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware tha there are significa t penalties for submitting false-informaiton, includi g the possi lity of fines and imprisonment for knowing violations." gnature of Permittee Date Signature of Pr arer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) -- DENR FORM DMSDF (5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001347 Laboratory: 1) Meritech, Inc Facility Name: NPDES # or WQ#: WWTP Name: MillerCoors LLC NCO029980 NA 2) 3) 4) 5) 1\GJ1llLLRl C111 R1 J1J Y Sample or 2/2/15 4/1/15 6/1/15 7/22/15 8/3/15 9/1/15 1011115 11/23/15 12/15/15 Composite Date Percent Solids 12.9 13 14.8 17.3 14 16.8 15.4 11.3 14.6 Arsenic NA NA 3.39 2.89 3.57 2.98 3.25 4.42 3.42 Cadmium 0.775 0.769 0.676 0.578 0.9 0.595 0.649 0.885 0.685 Chromium NA NA NA NA NA NA NA NA NA Copper 22.4 28.6 31.4 29 33.4 33.6 30.7 31.8 31 ?� Lead 3.88 4.98 3.38 3.35 3.57 3.11 3.25 23.3 12.1 Mercury NA NA NA 0.058 0.071 0.06 0.065 0.088 0.068 CD Molybdenum NA NA 2.14 2.46 3.34 2.66 3.4 2.21 2.53 y Nickel 6.27 6.72 5.97 5.33 6.08 4.57 5.53 7.76 5.6 Selenium NA NA 3.39 2.89 3.57 2.98 3.25 4.42 3.42 Zinc 196 205 211 176 231 259 250 250 286 Total Phosphorus 3,280 13,200 7,300 2,680 7,430 7,320 6820 8300 7470 TKN 3,970 3,980 6,950 36,200 18,900 10,300 7270 21000 38900 Ammonia -Nitrogen 1810 2570 6300 7790 9630 4,070 1160 12400 10000 Nitrate and Nitrite 77.5 76.9 67.6 57.8 71.4 59.5 64.9 88.5 68.5 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties fo submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature o Preparer Date DENR FORM RSSF (5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001347 Laboratory: 1) Meritech, Inc Facility Name: MillerCoors LLC 2) NPDES # or NCO029980 3) WQ#: 4) WWTP Name: NA 5) • T iXG3IUU[11 t11141 J1J L"L - Sample or 2/2/15 4/1/15 6/1/15 7/22/15 8/3/15 9/1/15 1011115 11/23/15 12/15/15 Composite Date pH 7.4 7.1 6.8 7.5 6.4 6.2 6.3 6.6 6.67 Nitrogen, Total 4,048 4,057 7,018 36,258 18,971 10,360 7,335 21,089 38,969 PAN 3,298 3,139 3,793 177,599 72,251 20,580 5762 86641 232032 Aluminum, Total 392 430 566 527 79 899 721 713 653 Calcium, Total 8,220 13,000 12,000 6,990 8,640 19,800 7660 38700 28200 Magnesium, Total 2,670 3,150 2,090 1,870 1,920 1,900 1910 2220 1970 Potassium, Total 3280 3,130 2340 2680 5860 2,760 3260 2550 3411 Sodium, Total 196 6,240 5000 4720 6,540 4,920 4050 4960 4880 SAR 4.74 4.58 7.3 5.37 6.18 3.66 4.2 2.23 2.89 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1 � Signature of Preparer Date DENR FORM RSSF-B (5/2003) FARM ON DISTRIBUTION 2015 NORTH CAROLINA 276 Rockingham 922.34 118.98 See Farm Recipient Tab for Locations 367 Rockingham 154.74 19.96 112 Rockingham 74.7 9.64 55 Rockingham 148.31 19.13 1300.09 167.71 367 55 Rockingham Rockingham 228.23 108.05 29.44 13.94 276 Guilford 936.06 120.75 279 Rockingham 91.17 11.76 340 Rockingham 650.40 83.90 2013.91 259.79 367 Rockingham 66.61 8.59 279 Rockingham 125.17 16.15 367 Rockingham 413.05 53.28 340 Rockingham 101.21 13.06 276 Rockingham 826.19 106.58 1532.23 197.66 367 Rockingham 887.84 115.42 112 Rockingham 97.36 12.66 326 Rockingham 285.75 37.15 1270.95 165.22 326 Rockingham 330.62 42.98 330.62 42.98 112 Rockingham 87.9 13.01 87.90 13.01 329 Rockingham 71.84 10.63 112 Rockingham 96.68 14.31 168.52 24.94 340 Rockingham 361.53 50.61 467 Rockingham 50.68 7.10 304 Rockingham 504.98 70.70 917.19 128.41 304 Rockingham 579.71 81.16 340 Rockingham 440.04 61.61 1019.75 142.77 777 Caswell 309.36 47.64 340 Rockingham 414.64 63.85 329 Rockingham 185.30 28.54 340 Rockingham 38.74 5.97 948.04 146.00 340 Rockingham 868.53 133.75 868.53 133.75 340 Rockingham 620.85 70.16 620.85 70.16 11078.581 1492.40 Dry Solids I Sample Date 12.9 1 2/23/2015 13 2 4/1/2015 14.8 3 6/3/2015 14.0 4 8/3/2015 15.4 5 10/1/2015 11.3 6 11/25/2015 13.6 Averaae Miller Breweries East, Inc Eden, NC LI.- Farm Recipients - NC MI Steve WiElPs.,,448 Bent Fram Road, Stoneville, NC 27048 11 1 Don Campbell, 14570 NC 87N, Eden, NC 27288 55 ISammy Manuel 575 Dairy Road, Reidsville, NC 27320 108 Barry James, 440 Estes Road, Ruffin, NC 27326 112 Harden Brown PO Box 243 Ruffin, NC 27326 169 Glen Hardin, 8177 Benaja Rd., Reidsville, NC 27320 186 Patience Englis Oakhaven Farm, 414 Piedmont Ave, Rocky Mount, NC 27803 189 1 Cecil Martin, 304 Woodrow Rd., Stoneville, NC 27048 194 David Burroughs, 2944 Garrett Rd., Stoneville, NC 27048 261 Arthur Edwards, 397 Fisherhill Rod, Eden, NC27288 276 Philip Faucette, 7725 Friendship Church Rd, Borwn Summit NC 27214 277 Russell Purdue, 352 Watts Farm Road, Reidsville, NC 27320 279 John edwards, 3465 Hwy 135, Stoneville, NC 27048 294 Dr. GH French, Jr, Sunny Home Farm, 11181 NC 770, Eden,NC 27288 300 Ralf Leaks, 508 Oregon Hill Rd Stoneville, NC 27048 304 Elmer French, 2843 Oregon Hill Road, Ruffin, NC 27326 311 IS.A. Fitts, PO Box 70, Cascade, VA 24069 312 Jim Anderson 600 Roberts Rd, Eden, NC 27288 317 Ruby S. Hinson 488 Memorial Baptist Church Road, Stoneville, NC 27048 318 Doug Stephanes, 1255 Guerant Springs Rd., Ruffin, NC 27326 321 NCSU, Upper Piedmon Research Stn. 1944 Wentworth st. Reidsville, NC 27320 326 Larry Shough, 362 Duggins Road, Stoneville, NC 27048 327 John Isley 2523 Iron Works Rd. Reidsville, NC 27320 329 Larry Shough 362 Duggins Rd. Stoneville, NC 27048 331 Steve Hopper, 101 Hwy 700, Eden, NC 27288 332 Bernie S. Pryor 3406 Ashland Rd. Reidsville, NC 27320 340 Robert M. Osborne, PO Box 1107, Eden, NC 27288 344 Claude Pryor Jr., 2013 Mayfield Road, Ruffin, NC 27326 345 lVirginia Rakestraw, 455 Eagle Falls Rd. Madison NC 27025 346 William M. London, 1768 Estes Rd., Ruffin, NC 27326 347 Jeremy Tyson, 742 Eagle Falls Road, Madison, NC 27025 350 James Smith, 919 Buck Road, Pelham, NC 27311 355 William S. Shreve, 390 Falcon Rd., Reidsville, NC 27320 443 Maynard Nance, 581 US 158, Ruffin, NC 27326 467 Tim Lilly, 6140, Hwy 770 Stoneville, NC 27048 367 Keith Adkins, 161 Taralin. Mayodan, NC 27027 367 Roger Long. 1281 Rhodes Rd., Eden, NC 27288 368 Freddie Harvey, 267 Heritage Rd, Eden, NC 27288 368 Charles Ratliffe, 464 Canteen Rd., Reidsville, NC 27320 777 Norris Williamson, 461 graves Road, Reidsville, NC 27320 North Carolina Land Application Month Total Lime In NC ProductOut VA Out Total Out %VA %NC Total Lime NC Tons Lime Jan 6.37 167.71 101.68 269.39 37.7% 62.3% 6.37 4.0 Feb 7.14 259.79 41.93 301.72 13.9% 86.1% 7.14 6.1 March 6.75 197.66 87.85 285.51 30.8% 69.2% 6.75 4.7 April 5.10 165.22 50.37 215.59 23.4% 76.6% 5.10 3.9 May 4.44 42.98 144.87 187.85 77.1% 22.9% 4.44 1.0 June 6.69 13.01 270 283.01 95.4% 4.6% 6.69 0.3 July 4.65 24.94 171.66 = 196.6 87.3% 12.7% 4.65 0.6 August 4.67 128.41 69.12 197.53 35.0% 65.0% 4.67 3.0 Sept 4.61 142.77 52.24 195.01 '26.8% 73.2% 4.61 3.4 Oct 6.75 146 139.62 285.62 48.9% 51.1% 6.75 3.5 Nov 5.19 133.75 85.81 219.56 39.1% 60.9% 5.19 3.2 Dec 4.64 70.16 126.11 196.27 64.3% 35.7% 4.64 1.7 Total 67.011 1492.41 1341.261 2833.66 47.3% 52.7%1 67.011 35.29 2015 Purchased Lime (lbs) Purchased Lime (tons) Total NC and VA Dry Tons Tons Lime/Ton Dry 134 220 67.01 2833.66 0.023647862 Plant Available Nitrogen Calculation 2015 Reporting Year mg/kg Feb-15 Apr-15 Jun-15 Jul-16 Aug-15 Sep-15 Oct-15 Nov-15 Dec-15 NH3-N 1810 2570 6300 7790 9630 4070 1160 12400 10000 NN 77.5 76.9 67.6 57.8 71.4 59.5 64.9 88.5 68.5 TKN 3970 3980 6950 36200 18900 10300 7270 21000 38900 Organic-N 2082.5 1333.1 582.4 28352.2 9198.6 6170.5 6045.1 8511.5 28831.5 Volatization Rate (V) 0.5 Per Derrick Denard - NCDENR on 6/30/11 Demineralization Factor (D) 0 Lime -Stabilized Mineralization Factor (K) 0.4 Per Derrick Denard - NCDENR on 6/30/11 PAN = [AN x(1-V/100) + NN + ON x (K/100)] x (1-D/100) X 0.002 Plant Available Nitrogen 3298 3139 3793 177599 72251 20580 5762 86641 232032 Sodium Absorption Ratio (SAR) 2015 Reporting Year Feb-15 Apr-15 Jun-15 Jul-16 Aug-15 Sep-15 Oct-15 Nov-15 Dec-15 Magnesium,mg/kg 2670 3150 2090 1870 1920 1900 1910 2220 1970 Calcium, mg/kg 8220 13000 1770 6990 8640 19800 7660 38700 28200 Sodium, mg/kg 5400 62401 5000 4720 6540 4920 4050 4960 4880 % Solids 12.9% 13.0% 14.8% 17.3% 14.0% 16.8% 15.4% 11.3% 14.6% Magnesium, mg/L 344.43 409.5 309.32 323.51 268.8 319.2 294.14 250.86 287.62 calcuim Mg/L 1060.4 1690 261.96 1209.3 1209.6 3326.4 1179.64 4373.1 4117.2 Sodium, Mg/L 696.6 811.2 740 816.56 915.6 826.56 623.7 560.48 712.48 Magnesium, meq 28.703 34.1251 25.777 26.959 22.4 26.6 24.51167 20.905 23.96833 Calcium, meq 53.019 84.5 13.098 60.464 60.48 166.32 58.982 218.655 205.86 Sodium, meq 30.287 35.27 32.174 35.503 39.809 35.93739 27.11739 24.3687 30.97739 SAR 1 4.74 4.58 7.30 5.37 6.18 3.66 4.20 2.23 2.89 S.A.R. _ (Cla2+ + l�c�' Eq. Weight Atomic Weight (AW) Valence (V) Na 23 22.9 1 Ca 20 40.08 2 Mg 12 1 24.31 2 Meritech, Inc. Environmental Laboratory •�, . ,,,�, Laboratory Certification No.165 Contact: Eric Tillman Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Report Date: 2/23/2015 NPDES #: NCO029980 Date Sample Rcvd: 2/2/2015 Meritech Work Order # 02021561 Sample: Farm On Grab 2/2/15 Parameters Result Analysis Date Reporting Limit Method %Total Solids 12.9 % 2/2/15 0-100 % SM 2540B Ammonia, Nitrogen 1810 mg/kg 2/9/15 10 mg/kg EPA 350.1 TKN 3,970 mg/kg 2/19/15 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <77.5 mg/kg 2/6/15 77.5 mg/kg EPA 353.2 Aluminum, total 392 mg/kg 2/19/15 5.00 mg/kg EPA 200.7 Cadmium, total <0.775 mg/kg 2/19/15 0.775 mg/kg EPA 200.7 Calcium, total 8,220 mg/kg 2/19/15 10.0 mg/kg EPA 200.7 Copper, total 22.4 mg/kg 2/19/15 10.0 mg/kg EPA 200.7 Lead, total <3.88 mg/kg 2/19/15 3.88 mg/kg EPA 200.7 Magnesium, total 2,670 mg/kg 2/19/15 10.0 mg/kg EPA 200.7 Nickel, total 6.27 mg/kg 2/19/15 2.0 mg/kg EPA 200.7 Phosphorous, total 1,620 mg/kg 2/19/15 2.00 mg/kg EPA 200.7 Potassium, total 3,280 mg/kg 2/19/15 20.0 mg/kg EPA 200.7 Sodium, total 5,400 mg/kg 2/19/15 20.0 mg/kg EPA 200.7 Zinc, total 196 mg/kg 2/19/15 10.0 mg/kg EPA 200.7 pH 7.40 S.U. 2/2/15 1.0-14.0 S.U. SM 4500-H B I hereby certify that I have reviewed and approve these data. (I. LJ)4�z Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC Client: MillerCoors T_. Address: 863 E. Meadow Road Eden, NC 27288 ! �✓ Attention: NPDES #: N00029980 Phone: 336-627-25y " �9���,�?��� Fax: Email:(tb' Project: PO#: MERITECH INC. Environmental Laboratories nA Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab(2bellsouth.net Web Site: www.meritech-labs.com� Turn Around Time* Std (10 days) 3 - 5 Day I 24 - 48 Hr Sample LocationllD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #of Conts. Tests Required q On 1CO 1/ * pH OK? C12OK? Date Time Date Time Farm Onrf'i+ .,t 4 s'-�llm Grab ,F Cadmium, Copper, Lead, Nickel, Zinc, ; Ammonia -Nitrogen, Calcium, Magnesium, Nitrate -Nitrite -Nitrogen, pH, Phosphorus, % Total Solids, Plant Available Nitrogen (by calculation) Potassium, Sodium, TKN, Aluminum Method of Shipment: Comments: Express results as mglkg (Dry weight basis) UPS [] Fed Ex [� Hand Delivery ❑Other Will these results be used for regulatory purposes? Yes Yes No *RUSH wor Lust be approved prior to submitting samples. Reiinqutshed by: Date: Tim R at y: % e: ..Time: Re i ed b Date: Time: 2 ?J GSr i 2.. 2 Received by: Dat : Time: Rel nq- hed by: Date: Time: Received at la y: k, Date: Time: Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Hassan Nunn Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Report Date: 5/4/2015 NPDES #: NCO029980 Date Sample Rcvd: 4/1/2015 Meritech Work Order # 04011530 Sample: Farm On Grab 4/1/15 Parameters Result Analysis Date Reporting Limit Method % Total Solids 13.0 % 4/6/15 0-100 % SM 2540B Ammonia, Nitrogen 2,570 mg/kg 4/7/15 10 mg/kg EPA 350.1 TKN 3,980 mg/kg 4/8/15 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <76.9 mg/kg 4/6/15 76.9 mg/kg EPA 353.2 Aluminum, total 430 mg/kg 4/3/15 5.00 mg/kg EPA 200.7 Cadmium, total <0.769 mg/kg 4/3/15 0.769 mg/kg EPA 200.7 Calcium, total 13,000 mg/kg 5/2/15 10.0 mg/kg EPA 200.7 Copper, total 28.6 mg/kg 4/3/15 10.0 mg/kg EPA 200.7 Lead, total 4.98 mg/kg 5/2/15 3.88 mg/kg EPA 200.7 Magnesium, total 3,150 mg/kg 5/2/15 10.0 mg/kg EPA 200.7 Nickel, total 6.72 mg/kg 4/3/15 2.0 mg/kg EPA 200.7 Phosphorous, total 13,200 mg/kg 5/2/15 2.00 mg/kg EPA 200.7 Potassium, total 3,130 mg/kg 5/2/15 20.0 mg/kg EPA 200.7 Sodium, total 6,240 mg/kg 5/2/15 20.0 mg/kg EPA 200.7 Zinc, total 205 mg/kg 4/3/15 10.0 mg/kg EPA 200.7 pH 7.1 S.U. 4/8/15 1.0-14.0 S.U. SM 4500-H B z1-1 - I hereby certify that 1 have reviewed and approve these data. 11, 4V Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC Client: MillerCoors Address: 863 E. Meadow Road Eden, NC 27288 _J_ Attention: Hassan Nunn NPDES #: NCO029980 Phone: 336-627-2592 Fax: Email: nunn.hassan millercoors.com Project: PO MERI'TECH INC. Environmental Laboratories A Alvision of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtc[ab(afbellsouth.net Web Site: www.ineritech-labs.com Turn Around Time* Std (10 days) �-J 3 - 5 DaT—('i �— 24 -48 Hr Sample Location/ID # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? of Conts. Tests Re uired q On Ice? ;_. pH OK? C120K? Date Time Date Time Farm On A111 Grab f Cadmium, Copper, Lead, Nickel, Zinc, i ..,-.____ Ammonia -Nitrogen, Calcium, Magnesium, _ Nitrate-Nitrit6-Nitrogen, pl-I, Phosphorus, % Total Solids, Plant Available Nitrogen (by calculation) Potassium, Sodium, TKN, Aluminum _ Method of Shipment: Comments: Express results as mglkg (Dry weight basis) UPS [� Fed Ex [� Hand Delivery []Other _ �_,_ Will these results be used for regulatory purposes? Y Yes No *RUSH work must be approved prior to submitting samples. Relin ed Dale: / Time• -- t "�/ �G �© Recei ed�D Date: Time: ' r^ Relinquishe Date: Time: Received by: Dat Time: Reiinqulshed b : Date: Time: R at b D te: { Time: `� Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Eric Tillman Report Date: 7/16/2015 Client: MiIlerCoors NPDES #: NC0029980 863 East Meadow Road Eden, NC 27288 Date Sample Rcvd: 6/1/2015 Meritech Work Order # 06011505 Sample: Farm On Grab 6/1/15 Parameters Result Analysis Date Reporting Limit Method % Total Solids 14.8 % 6/3/15 0-100 % SM 2540E Ammonia, Nitrogen 6,300 mg/kg 6/30/15 10 mg/kg EPA 350.1 TKN 6,950 mg/kg 6/9/15 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen 67.6 mg/kg 6/25/15 10 mg/kg EPA 353.2 Aluminum, total 566 mg/kg 6/10/15 5.00 mg/kg EPA 200.7 Arsenic, total <3.39 mg/kg 6/10/15 3.39 mg/kg EPA 200.7 Cadmium, total <0.676 mg/kg 6/10/15 0.676 mg/kg EPA 200.7 Calcium, total 12,000 mg/kg 7/14/15 10.0 mg/kg EPA 200.7 Copper, total 31.4 mg/kg 6/10/15 10.0 mg/kg EPA 200.7 Lead, total <3.38 mg/kg 6/10/15 3.38 mg/kg EPA 200.7 Magnesium, total 2,090 mg/kg 6/10/15 10.0 mg/kg EPA 200.7 Molybdenum, total 2.14 mg/kg 6/10/15 0.500 mg/kg EPA 200.7 Nickel, total 5.97 mg/kg 6/10/15 2.0 mg/kg EPA 200.7 Phosphorous, total 7,300 mg/kg 6/10/15 2.00 mg/kg EPA 200.7 Potassium, total 2,340 mg/kg 6/10/15 20.0 mg/kg EPA 200.7 Selenium, total <3.39 mg/kg 6/10/15 3.39 mg/kg EPA 200.7 Sodium, total 5,000 mg/kg 6/10/15 20.0 mg/kg EPA 200.7 Zinc, total 211 mg/kg 6/10/15 10.0 mg/kg EPA 200.7 pH 6.8 S.U. 6/3/15 1.0-14.0 S.U. SM 4500-H B SAR 11.1 - - - - 1 hereby certify that 1 have reviewed and approve these data. (L- AI -a Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC NPDES#: NCO029980 Client: MillerCoors Phone: 336-627-2592 Fax: Address: _863 E. Meadow Road Email: augri.h?ssan@tlillprcoors.com Ed_e_n, NC 27288 — Project: Po #: Turn Around Time* Attention: Std (10 days) 3 - 5 Day 24 -48 Hr p4le, '0, O E_ r� Person Taking Sample (Signature): Lab Use Only MERI'T'ECH INC. - x Environmental Laboratories A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab(aDbellsouth.net Web Site: www.meritech-labs.com Sample Location/lD # Sampling Dates & Times START END Comp? Grab? Contonts. Tests Required Oil Ice? pH DO CUOK? Date Time Date Time Farm On /!r/r<�+ /S ' Grab Cadmium, Copper, Lead, Nickel, Zinc, �. Ammonia -Nitrogen, Calcium, Magnesium, Nitrate-NitritbI-Nitrogen, 1)4, Phosphorus, _ % Tota1"Solids, Plant Available Nitrogen (by calculation) Potassium, Sodium, TKN, Aluminum Method of Shipment: Comments: Express results as mglkg (Dry weight basis) UPS Fed Ex Hand Delivery [�Othcr Will these results be used for regulatory purposes? Yes IYes No *RUSH work must be approved prior to submitting samples. RelirlI ished by: //++Date: Time: � 'C-'� 4''�%/f' �j Received Oa Time: '� Relinquished by: Date: Time: Received by: Date: Time: Relinquished Date: ` R ed ab Dat 1_ Tim it v Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Eric Tillman Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Report Date: 8/14/2015 NPDES #: NCO029980 Date Sample Rcvd: 7/22/2015 Meritech Work Order # 072215109 Sample: Farm On Grab 7/22/15 Parameters Result Analysis Date Reporting Limit Method % Total Solids 17.3 % 8/10/15 0-100 % SM 2540B Ammonia, Nitrogen 7,790 mg/kg 8/6/15 10 mg/kg EPA 350.1 TKN 36,200 mg/kg 8/4/15 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <57.8 mg/kg 8/7/15 57.8 mg/kg EPA 353.2 Aluminum, total 527 mg/kg 8/10/15 5.00 mg/kg EPA 200.7 Arsenic, total <2.89 mg/kg 8/10/15 2.89 mg/kg EPA 200.7 Cadmium, total <0.578 mg/kg 8/10/15 0.578 rng/kg EPA 200.7 Calcium, total 6,990 mg/kg 8/10/15 10.0 mg/kg EPA 200.7 Copper, total 29.0 mg/kg 8/10/15 10.0 mg/kg EPA 200.7 Lead, total 3.35 mg/kg 8/10/15 2.0 mg/kg EPA 200.7 Magnesium, total 1,870 rng/kg 8/10/15 10.0 mg/kg EPA 200.7 Mercury, total <0.058 mg/kg 7/28/15 0.058 mg/kg EPA 245.1 Molybdenum, total 2.46 mg/kg 8/10/15 0.500 mg/kg EPA 200.7 Nickel, total 5.33 mg/kg 8/10/15 2.0 mg/kg EPA 200.7 Phosphorous, total 6,180 mg/kg 8/10/15 2.00 mg/kg EPA 200.7 Potassium, total 2,680 mg/kg 8/10/15 20.0 mg/kg EPA 200.7 Selenium, total <2.89 mg/kg 8/10/15 2.89 mg/kg EPA 200.7 Sodium, total 4,720 mg/kg 8/10/15 20.0 mg/kg EPA 200.7 Zinc, total 176 mg/kg 8/10/15 10.0 mg/kg EPA 200.7 pH 7.5 S.U. 8/3/15 1.0-14.0 S.U. SM 4500-H B CCE <1 % 8/12/15 1.0 % AOAC 955.01 1 herebycertify that I have reviewed and approve these data. fY pP Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC Client: MillerCoors Address: 863 E. Meadow Road Eden NC 27288 Attention: Eric Tillman NPDES #: NCO029980 Phone: 336-627-2592 Fax: Email: eric.tillman(a)_millercoors.com Project: Po #: MERITECH INC. Environmental Laboratories r A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab(&Wlsouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 days) 3 - 5 Day 24 -48 Hr Sample Location/ID # Sampling Dates & Times A I ,, Person Taking Sample (Signature): /ydr+4'J' Lab Use Only START END Comp? Grab? Contont s. Tests Required On Ice? j J pH OK? C 2OK? Date Time Date Time Farm On ,V 7-0r//`" 2 1 %U Grab TW24 Aluminum, Ammon a -Nitrogen, Arsenic,,' I Cadmium, Calcium, Copper, Lead, Magnesium, Mercury, Molybdenum, Nickel, Nitrate -Nitrite Nitrogen, Percent Total Solids, pH, Phosphorus, Sodium, Potassium; Selen�m, TKN, Zinc C O'l IM5 Method of Shipment: Comments: Express results as mg/kg (Dry weight basis) UPS Fed Ex Hand Delivery Other Will these results be used for regulatory purposes? Yes IYes No *RUSH work must be approved prior to submitting samples. Relinquished by: Date: Time: M I=r ram. 12-1 / ! Received Date: Tim Reli qu' ed by Date: Time: n ' ; _ ...: .? Received by: Date: Time: Relinquished by: Date: Time: rved at b -- r W l 5--- Tea Meritech, Inc. Environmental Laboratory 10 AW Laboratory Certification No.165 Contact: Eric Tillman Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Report Date: NPDES #: Date Sample Rcvd: 8/24/2015 NC0029980 8/5/2015 Meritech Work Order # 08051578 Sample: Farm On Grab 8/3/15 Parameters Result Analysis Date Reporting Limit Method % Total Solids 14.0 % 8/6/15 0-100 % SM 2540B Ammonia, Nitrogen 9,630 mg/kg 8/6/15 10 mg/kg EPA 350.1 TKN 18,900 mg/kg 8/18/15 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <71.4 mg/kg 8/7/15 71.4 mg/kg EPA 353.2 Aluminum, total 79.3 mg/kg 8/19/15 5.00 mg/kg EPA 200.7 Arsenic, total <3.57 mg/kg 8/19/15 3.57 mg/kg EPA 200.7 Cadmium, total 0.900 mg/kg 8/19/15 0.500 mg/kg EPA 200.7 Calcium, total 8,640 mg/kg 8/19/15 10.0 mg/kg EPA 200.7 Copper, total 33.4 mg/kg 8/19/15 10.0 mg/kg EPA 200.7 Lead, total <3.57 mg/kg 8/19/15 3.57 mg/kg EPA 200.7 Magnesium, total 1,920 mg/kg 8/19/15 10.0 mg/kg EPA 200.7 Mercury, total <0.071 mg/kg 8/11/15 0.071 mg/kg EPA 245.1 Molybdenum, total 3.34 mg/kg 8/19/15 0.500 mg/kg EPA 200.7 Nickel, total 6.08 mg/kg 8/19/15 2.0 mg/kg EPA 200.7 Phosphorous, total 7,430 mg/kg 8/19/15 2.00 mg/kg EPA 200.7 Potassium, total 5,860 mg/kg 8/19/15 20.0 mg/kg EPA 200.7 Selenium, total <3.57 mg/kg 8/19/15 3.57 mg/kg EPA 200.7 Sodium, total 6,540 mg/kg 8/19/15 20.0 mg/kg EPA 200.7 Zinc, total 231 mg/kg 8/19/15 10.0 mg/kg EPA 200.7 pH 6.4 S.U. 8/17/15 1.0-14.0 S.U. SM 4500-H B 1 hereby certify that I have reviewed and approve these data. � . Azag Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC Client: MillerCoors Address: 863 E. Meadow Road Eden, NC 27288 Attention: Eric Tillman NPDES #: NCO029980 Phone: 336-627-2592 Fax: Email: edc.tillman an millercoors.com Project: Po #: MERI'TECH INC. a Environmental Laboratories ` A Division of Water Technology and control, Inc. 642 Tamco Rd Phone 1-336.342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtciab(@bellsouth.net Web Site: www.meritech-labs.com Turn Around Time Std (10 days) I E� 3 - 5 Day I—_ 24 - 48 Hr Sample Location/ID # Sampling Dates & Times Person Taking sample (Signature)-.O i.A41 Lab Use Only START END Comp? Grab? #ot Conts. Tests Required On Ice? pH OK? C12 OK? Date Time Date Time Farm On jUrPin ais' : VS' Grab VeO Alumint7fii, Ammonia -Nitrogen, Arsenic, Cadmi6m, Calcium, Copper, Lead, IEEE Ma nesitim, Mercury, Molybdenum, Nickel, Nitrate -Nitrite Nitrogen, Percent Total Solids, p , Phosphdrus, 86dium, Potassium, Sel6nium, TKN, Zinc Method of Shipment: Comments: Express results as mglkg (Dry weight basis) UPS Fed Ex Hand Delivery' [Other Will these results be used for regulatory purposes? Yes IYes No RU work must be approved prior to submitting samples. ate:Tim/e: Reft:ja C� Recet d by: Data: Time: 5, 15 R Ilnqu he by L) te: Tlme: Received by: Date: Time: Relinquished by: Date: Time: JRw9T i by: Dat j ^t 115" 7l )Time* Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Eric Tillman Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Report Date: 9/15/2015 NPDES #: NCO029980 Date Sample Rcvd: 9/2/2015 Meritech Work Order # 09021528 Sample: Farm On Grab 9/1/15 Parameters Result Analysis Date Reporting Limit Method % Total Solids 16.8 % 9/3/15 0-100 % SM 2540B Ammonia, Nitrogen 4,070 mg/kg 9/3/15 10 mg/kg EPA 350.1 TKN 10,300 mg/kg 9/9/15 - 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <59.5 mg/kg 9/4/15 59.5 mg/kg EPA 353.2 Aluminum, total 899 mg/kg 9/14/15 5.00 mg/kg EPA 200.7 Arsenic, total <2.98 mg/kg 9/14/15 2.98 mg/kg EPA 200.7 Cadmium, total <0.595 mg/kg 9/14/15 0.595 mg/kg EPA 200.7 Calcium, total 19,800 - mg/kg 9/14/15 10.0 mg/kg EPA 200.7 Copper, total 33.6 mg/kg 9/14/15 10.0 mg/kg EPA 200.7 Lead, total 3.11 mg/kg 9/14/15 3.57 mg/kg EPA 200.7 Magnesium, total 1,900 mg/kg 9/14/15 10.0 mg/kg EPA 200.7 Mercury, total <0.060 mg/kg - 9/14/15 0.060 mg/kg EPA 245.1 Molybdenum, total 2.66 mg/kg 9/14/15 0.500 mg/kg EPA 200.7 Nickel, total 4.57 mg/kg 9/14/15 2.0 mg/kg EPA 200.7 Phosphorous, total 7,320 nig/kg 9/14/15 2.00 mg/kg EPA 200.7 Potassium, total 2,760 mg/kg 9/14/15 20.0 mg/kg EPA 200.7 Selenium, total <2.98 mg/kg 9/14/15 2.98 mg/kg EPA 200.7 Sodium, total 4,920 mg/kg 9/14/15 20.0 mg/kg EPA 200.7 Zinc, total 259 mg/kg 9/14/15 10.0 mg/kg EPA 200.7 pH 6.2 S.U. 9/9/15 1.0,-14.0 S.U. SM 4500-H B 1 hereby certify that I have reviewed and approve these data. LaboratotyRepres ntative 642 Tamco Road, Reidsville, North Carolina 27320 tei.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC Client: MillerCoors Address: 863 E. Meadow Road Eden NC 27288 Attention: Eric Tillman NPDES#: NCO029980 Phone: 336-627-2592 Fax: Email: eric.tillman(wmillercoors.com Project: Po #: MERITECH INC. Environmental Laboratories r _ ^ A pivisioa of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab(MbelIsouth.net Web Site: www.meritech-labs.com Sample Sampling Dates & Times p 9 START END Location/lD # Date Time Date Time Turn Around Time* std (ao days) 3 -S Day 24 -48 Hr Person Taking Sample (Signature): /.�� Lab use only Comp? Grab? #of Cents. Tests Re aired On fee? pH OK? C720K? Farm On 5%d0 Grab �o`� Aluminium, Amm6nia-Nitrogen, A4enic, Cadmiu>°ii, Calcium., Copper, Lead, Magnegium, Mefcury, Molybdenum, Nickel, Nitrate -Nitrite Nitrogen, Percent i Total Solids, pl-I, PhosKiorus, Sodium, Potassium, Selenium, TKN, Zinc Comments: Express results as mg/kg (Dry weight basis) Method of Shipment: ❑UPS [] Fed Ex ❑ Hand Delivery ❑Other Will these results be used for regulatory purposes? Yes IYes No *RUSH work must be approved prior to submitting samples. ' Relinquished by: Date: M a--KX - -( /z! Ij' Re' ish b : /1 Date: Time: I Rece' y: Date: Time: --�� Received by: Date: Time: Relinquished by: Date: Time: clued at lab D e fi TT� C.., A Contact: Eric Tillman Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Meritech, Inc, Environmental Laboratory Laboratory Certification No.165 Report Date: 10/14/2015 NPDES #: NCO029980 Date Sample Rcvd: 10/2/2015 Meritech Work Order # 10021505 Sample: Farm On Grab 10/1/15 Parameters Result Analysis Date Reporting Limit Method %Total Solids 15.4 % 10/6/15 0-100 % SM 2540B Ammonia, Nitrogen 1,160 mg/kg 10/5/15 10 mg/kg EPA 350.1 TKN 7,270 mg/kg 10/8/15 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <64.9 mg/kg 10/7/15 64.9 mg/kg EPA 353.2 Aluminum, total 721 rng/kg 10/7/15 5.00 mg/kg EPA 200.7 Arsenic, total <3.25 mg/kg 10/7/15 3.25 mg/kg EPA 200.7 Cadmium, total <0.649 mg/kg 10/7/15 0.649 mg/kg EPA 200.7 Calcium, total 7,660 mg/kg 10/7/15 10.0 mg/kg EPA 200.7 Copper, total 30.7 mg/kg 10/7/15 10.0 mg/kg EPA 200.7 Lead, total <3.25 mg/kg 10/7/15 3.25 mg/kg EPA 200.7 Magnesium, total 1,910 mg/kg 10,/7/15 10.0 mg/kg EPA 200.7 Mercury, total <0.065 mg/kg 10/5/15 0.065 mg/kg EPA 245.1 Molybdenum, total 3.40 rng/kg, 10/7/15 0.500 mg/kg EPA 200.7 Nickel, total 5.53 mg/kg 10/7/15 2.0 mg/kg EPA 200.7 Phosphorous, total 6,820 nig/kg 10/7/15 2.00 mg/kg EPA 200.7 Potassium, total 3,260 mg/kg 10/7/15 20.0 mg/kg EPA 200.7 Selenium, total <3.25 mg/kg 10/7/15 3.25 mg/kg EPA 200.7 Sodium, total 4,050 mg/kg 10/7/15 20.0 mg/kg EPA 200.7 Zinc, total 250 mg/kg 10/7/15 10.0 mg/kg EPA 200.7 PH 6.3 S.U. 10/8/15 1.0-14.0 S.U: SM 4500-H B I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342.4748 fax.(910)342-1522 Chain of Custody Record COC Client: MillerCoors Address: 863 E. Meadow Road Eden NC 27288 Attention: Eric Tillman NPDES#: N60029980 Phone: 336-627-2592 Fax: Email: eric.bllman(arnillercoors.com Project: PO #: MERITECH INC. Environmental Laboratories A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Pax: 1-336-342-1522 27320 Email: wtclab(@bellsouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 days) r` I 3-5 Day o 24 -48 Hr Sample Location/ID # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #of Conts. Tests Required uired - On Ice? I , j pH OK? C12 OK? Date Time Date Time Farm On / -7•;3U/ ' i a'- Grab Aluminum, Ammonia -Nitrogen, Arsenic, i- Cadmium, Calcium, Copper, Lead, Magnesium, Mercury, Molybdenum, Nickel Nitrate Nitrite Nitrogen, Percent Total Solids, pH, Phosphorus, Sodium, Potassidm, Selenium, Ti N, Zinc Method of Shipment: Comments: Express results as mg/kg (Dry weight basis) EJ UPS Fed Ex Hand Delivery ❑Other Will these results be used for regulatory purposes? Yes Fye—s----1 No *RUSH work must be approved prior to submitting samples. Relinquished by: Date: _ Time: "�� �, t Gf Z /' �� Received b Date: Time: Inf�� ICi/z/ f j '1 >� Relinquished /ate: _ �,Tlme: W e !!//�/ / � VJJ Received by: Date: Time: Relinquished by: Date: Time: Received lab y: Date: Time: r Contact: Eric Tillman Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Meritech Work Order # 11251507 Parameters %Total Solids Ammonia, Nitrogen TKN Nitrate/Nitrite, Nitrogen Aluminum, total Arsenic, total Cadmium, total Calcium, total Copper, total Lead, total Magnesium, total Mercury, total Molybdenum, total Nickel, total , Phosphorous, total Potassium, total Selenium, total Sodium, total Zinc, total PH Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Result Sample: Farm On Grab 11.3 12,400 mg/kg 21,000 mg/kg < 88.5 mg/kg 713 mg/kg < 4.42 .mg/kg < 0.885 mg/kg 38,700 mg/kg 31.8 mg/kg 23.3 mg/kg 2,220 mg/kg < 0.088 mg/kg < 2.21 nig/kg 7.76 mg/kg 8,300 mg/kg 2,550 mg/kg < 4.42 mg/kg 4,960 mg/kg 250 mg/kg 6.6 SM. Analysis Date 11/3/15 12/9/15 12/8/15 12/10/15 12/2/15 12/2/15 12/2/15 12/2/15 12/2/15 12/2/15 12/2/15 11/30/15 12/2/15 12/2/15 12/2/15 12/2/15 12/2/15 12/2/15 12/2/15 12/9/15 Report Date: 12/14/2015 NPDES #: NCO029980 Date Sample Rcvd: 11/25/2015 Reporting Limit 0-100 10 mg/kg 20 mg/kg 88.5 mg/kg 5.00 mg/kg 4.42 mg/kg 0.885 mg/kg 10.0 mg/kg 10.0 mg/kg 3.25 mg/kg 10.0 mg/kg 0.088 mg/kg 2.21 mg/kg 2.0 mg/kg 2.00 mg/kg 20.0 mg/kg 4.42 mg/kg 20.0 mg/kg 10.0 mg/kg 1.0-14.0 S.U. 11/23/15 Method SM 2540B EPA 350.1 EPA 351.1 EPA 353.2 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA200.7 EPA 200.7 EPA 245.1 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 SM 4500-H B I hereby certify that I have reviewed and approve these data. r/, az__e Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC Client: _ MillerCoors Address: 863 E. Meadow Road Eden NC 27288 Attention: Eric Tillman NPDES #: NCO029980 Phone: 336-627-2592 Fax: Email` eric.tillman @millercoors.com Project: PO#: MERI'TECH INC. Environmental Laboratories A Division of Water Techaologp and Control, Inc 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1622 27320 Email: wtclab(cDbellsouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (90 days) 3 - 6 Day t� 24 -48 Fir r--= Person Taking Sample (Signature): � °X"�`'j' Lab Use Only Sample LocationllD # Sampling Dates & Times START END Comp? Grab? #of coats. Tests Required On Ice? pH OK? C120K? Date Time Date Time Farm On av �3 �' �' rab G' t Aluminum, Ammonia -Nitrogen, Arsenic l Cadmium, Calcium, Copper, Lead, Magnesium, Mercury, Molybdenum, Nickel, Nitrate -Nitrite Nitrogen, Percent Total Solids, pH, Phosphorus, Sodium, Potassium, Selenium, TKN, Zinc Method of Shipment: Comments: Express results as mglkg (Dry weight basis) UPS i] Fed Ex Hand Delivery []Other Will these results be used for regulatory purposes? Yes Yes No *RUSH work st be appr ved prior to submitting samples. Relinquished by: � Date: Time: �'�- � 2_s � is Relinquished by Date }Time: J- ° ` Received by: Date Time: Received by: Date: Time: Relinquished by: Date: Time: ed at y ( Dates ime: Meritech, Inc. Environmental Laboratory Laboratory Certification No.169 Contact: Eric Tillman Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Report Date: 12/30/2015 NPDES #: NC0029980 Date Sample Rcvd: 12/16/2015 Meritech Work Order # 12161526 Sample: Farm On Grab 12/15/15 Parameters Result . Analysis Date Reporting Limit Method %Total Solids 14.6 % 12/16/15 0-100 % SM 2540B Ammonia, Nitrogen 10,000 mg/kg 12/29/15 10 mg/kg EPA 350.1 TKN 38,900 mg/kg 12/23/15 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <68.5 mg/kg 12/18/15 68.5 mg/kg EPA 353.2 Aluminum, total 653 mg/kg, 12/21/15 5.00 mg/kg EPA 200.7 Arsenic, total <3.42 mg/kg 12/21/15 3.42 mg/kg EPA 200.7 Cadmium, total <0.685 mg/kg 12/21/15 0.685 mg/kg EPA 200.7 Calcium, total 28,200 mg/kg 12/21/15 10.0 mg/kg EPA 200.7 Copper, total 31.0 mg/kg 12/21/15 10.0 mg/kg EPA 200.7 Lead, total 12.1 mg/kg 12/21/15 3.25 mg/kg EPA 200.7 Magnesium, total 1,970 mg/kg 12/21/15 10.0 mg/kg EPA 200.7 Mercury, total <0.068 mg/kg 12/22/15 0.068 mg/kg EPA 245.1 Molybdenum, total 2.53 mg/kg 12/21/15 2.21 mg/kg EPA 200.7 Nickel, total 5.60 mg/kg 12/21/15 2.0 mg/kg EPA 200.7 Phosphorous, total 7,470 mg/kg 12/21/15 2.00 mg/kg EPA 200.7 Potassium, total 3,411 mg/kg 12/21/15 20.0 mg/kg EPA 200.7 Selenium, total <3.42 mg/kg 12/21/15 3.42 mg/kg EPA 200.7 Sodium, total 4,880 mg/kg 12/21/15 20.0 mg/kg EPA 200.7 Zinc, total 286 mg/kg 12/21/15 10.0 mg/kg EPA 200.7 pH 6.67 S.U. 12/30/15 1.0-14.0 S.U. SM 4500-H B n, I hereby certify that I have reviewed and approve these data. Laboratoty Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC Client: MillerCoors Address: 863 E. Meadow Road Eden, NC 27288 Attention: Eric Tillman NPDES#: NCO029980 Phone: 336-627-2592 Fax: Email: eric.tiflman(a-millercoors.com Project: PO#- MERITECH INC. t; Environmental Laboratories r ~" A Division of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab(&bellsouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 days) o 3 -5 Day o 24-48 Hr Sample Location/lD # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #of Conts. Tests Required On lee? pH OK? C12 OK? Date Time Date Time Farm On Grab `�, Aluminum, Ammonia -Nitrogen, Arsenic, :i t. i •`t Cadmium, Calcium, Copper, Lead, Magnesium, Mercury, Molybdenum, Nickel, Nitrate -Nitrite Nitrogen, Percent Total Solids, pH, Phosphorus, Sodium, Potassium, Selenium, TKN, Zinc Method of Shipment: Comments: Express results as mg/kg (Dry weight basis) UPS Fed Ex Hand Delivery Other Will these results be used for regulatory purposes? Yes Yes No RUSH work �t iust be app ed prior to submitting samples. Relinquished b • 'T ` Date: Time: M ` ✓`/' % /J �';C/o Receive �'= � ,,,r Date: � Time: -" � _ - t - a/l/�r✓f ��;i/v Relinquishy;'` ✓� ;r Date: 1 Time: y� •.� ^'' . / �;' �'� i l,� (i':1,� Received by: Date: Time: RelinquTs'Tied by: Date: Time: Rimed at I y:� Date: Time;