WQ0000783_Residual Annual Report 2015_20160303

P.O. Box 8
Bolivia, NC 28422
1-910-253-4689
February 26, 2016
N.C. Dept of Environment and Natural Resources
Division of Water Resources
Water Quality Permit Section
Non -Discharge Permitting Unit
512 N. Salisbury St.
Raleigh, NC 27604
Dear Sir/Madam
_DEUI®119
't�IaR — 3
tAon-D\sr' ui ��,
P e .ek'09
r
FCI®
MAR 0, 3 2016
DWR SECTION
INFORMATION PROCESSING UNIT
S&B Maintenance, LLC is sending in the required forms for our DWQ permit for this past
year. This report is for the land application of residuals for the reporting year of 2014. If
you have questions "or need more information you can reach the office at the provided
phone number.
Since ely,
Sammy P Carteret

ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0000783 County: Brunswick Year: 2015
Facility Name (as. shown on permit): S&B Maintenance
Land Application Operator: Sammy P Carteret Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calendar year?
® Yes ® No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Part B:
Facility was compliant during calendar year 2015 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Resources.0 Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1.Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Resources.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations "
Sammy P Carteret/operator 6
Permittee Name WATitle (type or print) Signature of Permittee Date .
Signature01-R-parer'�Date Signature of Land Applier Date
(if differefrom Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part.503.9 (r)
nFNR FORM ACF (5/20031

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000783 Laboratory:
Facility Name:
NPDES # or
WQ#:
S&B Maintenance
NC0007064
WWTP Name: Duke Energy
Residual Analvsis Data
1) Envirochem Chemist
2)
3)
4)
5)
.. Sample 'D , -
-n-m------m-Total
Phosphorus
"I certify, under penalty of -law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant pens ' s or sZ-26--111,ubmitting false information, including the possibiliityof fines and imprisonment for knowing violations."
Signatur reparer Date
DENR FORM RSSF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed:than those required to be summarized on this form.,
Permit Number: WQ0000783 Laboratory:
Facility Name: S&B Maintenance
NPDES # or WQ0005790
- WQ#:
WWTP Name: Oak Island WWTP
Residual AnAvsis Data
1) Envirochem Chemist
2)
3)
4)
5)
Sample or
Composite Date
MOW
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties r s bmitting false information, including the possibility of fines and imprisonment for knowing violations."
*C,0;4 c) _.y/=`6
Signature reparer Date
DENR FORM RSSF (5/2003)

ANNUAL MKFALa FIELD LOADIAG SUMMARY JKORWr
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
S&B Maintenance
Total Dry Tons Applied (Annual):
Permit #: WQ0000783 Cation Exchange Capacity (non 503 only):
Operator: Sammy P Carteret Owner: Sammy P Carteret
Acres Used: 17.2 Acres Permitted: 17.2 Site #: Field #: 1A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
0.848595
Sample
or Com-
posite
ate
1
1/6/15
2
1/6/15
3
1/6/15
4
116115
5
116115
6
7
8
_.9f
101
11
12
% Solids
0.74
0.74
0.74
0.74
0.74
Arsenic
13
13
13
13
13
Cadmium
13
13
13
13
13
Chromium
0
0
0
0
0
Copper
124
124
124
124
124
Lead
13
13
13
13
13
Mercury
2
2
2
2
2
Molyb-
damim
13
13
13
13
13
Nickel
13
13
13
13
13
Selenium
13
13
13
13
13
Zinc
651
651
651
651
651
Total
Phos-
horus
13600
13600
13600
13600
13600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
0
1
2
3
4
5
6
7
8
9
10
11
12
c ty
c
0.009
o
0.009-,0.009
0.009
0.009
Arsenic
0.0002
0.0002
0.0002
0.0002
0.0002
0
0
0
0
0
0
0
10.0012
Cadmium
0.0002
0.0002
0.0002
0.0002
0.0002
0
0
0
0
0
0
0
0.0012
Chromiurr
0
0
0
0
0
0
0
0
0
0
0
0
0
Copper
.0.0022
0.0022
0.0022
0.0022
0.0022
0
0
0
0
0
0
0
0.0112
Lead
0.0002
0.0002
0.0002
0.0002
0.0002
0
0.
0
0
0
0
0
0.0012
Mercury
4E-05
AE-05
4E-05
4E-05
4E-05
0
0
0.
0
0
0
0
0.0002
Molyb-
demirn
0.0002
0.0002
0.0002
0.0002
0.0002
0
0
0
0
0
0
0
0.0012
Nickel
0.0002
0.0002
0002
0.0002
0.0002
0
0
0
0
0
0
0
0.0012
Selenium
0.0002
0.0002
0.0002
0.0002
0.0002
0,
0
0
0
0
0
0
0.0012
Zinc
0.0117
0.0117
0.0117
0.0111
0.0117
0
0
0
0
0
0
0
0.0586
Total
Phos-
0.2448
0.2448
0.2448
0.2448
0.2448
0
0
0
0
0
0
0
1.224
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I a aware that there are significant penalties for submitting false information,
includin the possibili o fines and imprisonment for knowing violations"
Signature of Land Applier Date
* See bottqm of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: S&B Maintenance Total Dry Tons Applied (Annual): 0.509157
Permit #: WQ0000783 Cation Exchange Capacity (non 503 only):
Operator: Sammy P Carteret Owner: Sammy P Carteret
Acres Used: 10.07 Acres Permitted: 10.07 Site #: Field #: 2A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
1
1/6/15
2
1/6/15
3
1/6/15
4
5
6
7
8
91
10
11
12
% Solids
0.74'
0.74
0.74
Arsenic
13
13
13
Cadmium
13
13
13
Chromium
0
0
0
Copper
124
124
124
Lead
13
13
13
Mercury
2
2
2
Molyb-
13
13
13
Nickel
13
13
13
Selenium
13
13
13
Zinc
651
651
65.1
Total
Phos-
horns
13600
13600
13600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
c
1
2
3
4
5
8
7
8
9
10
11
12
ri
c d
0.016
p y
4
o
0.016
0.016
Arsenic
0.0004
0.0004
0.0004
0
0
0
0
0
0
0
0
0
0.0012
Cadmium
0.0004
0.0004
0.0004
0
0
0
0
0
0
0
0
0
0.0012
Chromiun
0
0
0
0
0
0
0
0
0
0
0
0
0
Copper
0.004
0.004
0.004
0
0
0
0
0
0
0
0
0
0.0119
Lead
0.0004
0.0004
0.0004
0
0
0
0
0
0
0
0
0
0.0012
Mercury
6E-05
6E-05
6E-05
0
0
0
0
0
0
0
.0
0
6.6002
Molyb-
denurn
0.0004
0.0004
0.0004
0
0
0
0
0
0
0
0
0
0.0012
Nickel
0.0004
0.0004
0.0004
0
0
0
0
0
0
0
0
0
0.0012
Selenium
0.00041
0.0004
0.0004
0
0
0_
0
0
0
1 0
0
0
0.0012
Zinc -
0.0208
0.0208
0.0208
0
0
0
0
0
0
0
0
0
0.0625
Total
Phos-
0.4352
0.4352
0.4352
0
0
0
0
0
0
0
0
0
1.3056
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includi the possib' ' o fines and imprisonment for knowing .violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this N[FLSF Form and the mathematically linked FSF Form
nFNR FnRM MFI .RF (5/9nn i1

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: S&B Maintenance Total Dry Tons Applied (Annual): 5.121594
Permit #: WQ0000783 Cation Exchange Capacity (non 503 only):
Operator: Sammy P Carteret Owner:
Acres Used: 19.8 Acres Permitted: 19.8 Site #:
Sammy P Carteret
Field #: 1D
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
phorus
WO
MENEENEENE_
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
0
1J
2
3
4
5
6
7
8
9
10
11
12
e d
0.008
o
0.25
Arsenic
0.002
0.0002
0
0
0
0
0
0
0
0
0
0
0.0022
Cadmium
0.002
0.0002
0
0
0
0
0
0
0
0
0
0
0.0022
Chromiwl
0.0082
0
0
0
0
0
0
0
0
0
0
0
0.0082
Copper
0.171
0.002
0
0
0
0
0.
0
0
0
0
0
0.173
Lead
0.0065
0.0002
0
0
0
0
0
0
0
0
0
0
0.0067
Mercury
0.0019
3E-05
0
0
0
0
0
0
0
0
0.
0
0.002
Molyb-
0.002
0.0002
0
0
0
0
0
0
0
0
0
0
0.0022
Nickel
0.0079
0.0002
0
0
0
0
0
0
0
0
0
0
0.0081
Selenium
0.004
0.0002
0
0
0
0
0
0
0
0
0
0
0.0042
Zinc
0.399
0.0104
0
0
0
0
0
0
0
0
0
0
0.4094
Total
Phos-
18.4
01176
0
0
0
0
0
0
0
0
0
0
18.618
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includiiW the possibEJ4 of fines and imprisonment for knowing violations"
45A�� p 02-1� �r-A
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this A FLSF Form and the mathematically linked FSF Form
ni=mp Pr)PU MFI SF /.ri/,?nn i)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOREACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: S&B Maintenance Permit #: WQ0000783 Annual Dry Tons Applied:
Owner: Sammy P Carteret Operator: Sammy P Carteret Cation Exchange Capacity (non 503):
Site #:
Field #: lA Acres Utilized: 17.2
0.848595
Acres Permitted: 17.2
o ��
o
A
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Inches
Preci
past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
.Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
�
�
Gal.
T =
Report
Totals
in Gal.
Crop 1
_Crop 2
2=5-15
5,500
319.77
0.74
0.009867384
NC0007064
Dry
0
S
0.5
0.3
45,900
2190
122
0.2828
0.2828
1
2-21-15
5,500
319.77
0.74
0.009867384
NC0007064
Dry
0
S
0.5
0.3
45,900
2190
122
0.2828
0.2828
2
3-22-15
5,500
319.77
0.74
0.009867384
NC0007064
Dry
0
S
0.5
0.3
45,900
1 2190
122
0.2828
0.2828
3
1-23-1
5,500
319.77
0.74
0.009867384
NC0007064
Dry
0
S
0.5
0.3
45,900
2190
122
0.2828
0.2828
141
2-28-1
5,500
319.771
0.74
0.009867384
NC0007064
Dry
0
S
0.5
0.3
45,900
2190
1 122
0.2828
0.2828
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
1 0
0
1
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
rOTALS:
1599
• ` r m
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
knnual lbs/acre
0.00117
0.00117
0
0.01116
0.00117
0.00018
0.00117
0.00117
0.00117
0.05859
1.224
1 1.414
1.414
Date
lbs/ac
ry
�urrent Cumulative lbs/ac
0.79517
10.87517
0
128.3232114.4522
0.05618
1.29717
2.93117
0.46817
57.0496
'rior Years Cumulative lbs/ac
'ermitted C. P. L. R.***
0.794
36
1 0.874
34
0
NA
128.312
1 1338
14.4.51
267
0.056
15
1.296
NA
2.93
374
0.467
1 89
rmit PAN Limit 1 st/2nd Crop-
-
- Yip' - :Y'i-a�
ry, -
.-
.'S- - .3, -
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
lesigned to assure that qualif d personnel properly gathered and evaluated the information submitted. I am aware that there are
,ignificant pe allies for s 'tting false information, including the possibility of fines and imprisonment for knowing violations."
/ o *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Vnlatilization Rate: Surface - 0.5. fin iectinn/Tnearnoration - 1.0
***C'_P_L_R_: Cumulative Pollutant T,nadinu Rate
k * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name:
Owner:
Site #:
S&B Maintenance
Sammy P Carteret
Field #:
Operator:
2A
Permit #: WQ0000783
Sammy P Carteret
Acres Utilized: 10.07
Annual Dry Tons Applied: 0.509157
Cation Exchange Capacity (non 503):
Acres Permitted: 10.07
c
C
A
s eci
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre'
Residual
Sources
(Summarize)
Site
Cond.
D
Wet,
Inches.
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen.
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
2
Gal.
Cu.Yd.
'-
``
01
Report
Totals
in Gal.
Crop I
Crop 2
6-12-15
5,500
546.18
0.74
0.016853923
NC0007064.
Dry
0
S
0.5
0.3
45;900
1 2190
122 10.48303
0.48303
1
7-16-15
5,500
546.18
0.74
0.016853923
NC0007064
Dry
0
S
0.5
0.3
45,900
2190
122
0,48303
0.48303
2
8-28-15
5,500
546.18
0.74
0.016853923
NC0007064
Dry
0
S
0.5
0.3
45,900
2190
122
0.48303
0.48303
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
17
0
0
0
0
8
a
0
0
0
9
0
0
0
0
1
10
0
0
0
0
11
0
0
0
0
12
TOTALS:
1639
t= t
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
t=`
Annual lbs/acre
Current Cumulative lbs/ac
0.001248
0.226248
0.00125
0.14725
0
0
0.0119
4.8559-
0.00125
14.6952
0.00019
0.02019
0.00125
0.12025
0.00125
0.45925
0.458
374
0.00125
0.08025
0.079
89
0.0625
13.4405
13.378=
2498
1.3056 1.4491 1.4491
Date
lbs/ac
r
Prior Years Cumulative lbs/ac
1 0.225
0.146
0
4.844
1 14.694
0.02
0.119
Permitted C. P. L. R.
36
34
NA
1 1338
267
15
NA
Permit PAN Limit 1s/2nd Crop
- -
=
-
300
50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that 99alified personnel properly gathered and, evaluated the information submitted. I am aware that there are
significa t penalties bmitting false information, including the possibility of -fines and imprisonment for knowing violations."
^C =C*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Vnlatilization Rate: Surface - 0.5. Tniectinn/inearnnration - 1.0
***C.P1,_R_: 0imulative Pallutnut T,nadinu Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1'to MFLSF column # 1.
DENR FORM FSF (6/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: S&B Maintenance
Owner:
Site #:
Annual Dry Tons Applied: 5.121594
Sammy P Carteret Operator: Sammy P Carteret Cation Exchange Capacity (non 503):
Field #: 1D Acres Utilized: 19.8 -Acres Permitted: 19.8
Permit #: WQ0000783
oGal
N 0
o
A
Specify
Totals
Per
Acre
o
/o
Solid
s
Dry Tons Per
Acre'
Residual
Sources
(Summarize)
Site
Cond.
D
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate* *
Miner-
ali-
zation
Rate
TKN -
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
yd
-
= Report
x Totals
in Gal.
Crop 1
Crop 2
3-18-15
95,000
4798
1.25
0.250094697
WQ0005790
Dry
0
S
0.5
0.3
120000
57.6
2760
19.3931.
19.3931
1
10-15-1
5,500
277.78
0.74
0.008571667
NC0007064
Dry
0
S
0.5
0.3
45,900
2190
122
0.24566.
0.24566
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
1 0
0
1.
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
TOTALS:
5076
As
Cd
Cr
Cu
Pb
H
Mo
Ni,
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annual lbs/acre
0.002208
0.00221
0.0082
0.17298 '
0.00671
0.00196
0.00221
0.00811
0.00425
0.46942
18.6176
19.6388
19.6388
Date
lbs/ac
` ,
Current Cumulative lbs/ac
0.785208
1.08321
0.0202
32.611
27.7467
0.11796
-1.25321
4.59711
0:59325
62.6544
`:}." "= <;;;
-50
Prior Years Cumulative lbs/ac
0.783
1.081
0.012
32.438
27.74
0.116
1.251
4.589
0.589
62:245
Permitted C. P. L. R.***
36
34
1 NA
1 1338
267
15
NA
374
89
2498-71
P Permit P 1 2 0
e rt AN Limit st/ nd Cr
.j u _ f:. =:_< -
� =fix � - "=:y- � .
- - - :��
- - = N-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qu lified personnel properly gathered and evaluated the information submitted. I am aware that there are
Sig nifican enalties for witting -false information, including the possibility of fines and imprisonment for knowing violations."
,C *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Vnlatilization Rate: Surface - 0.5. Tnieelhon/fnearnaration - 1.0
***C'_P.T,_R_: 0imnlative Pollntnnt Laadinu Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered.ol° the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the Identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

Sewage Analysis for 2015
iple 01/06/2015 Envirochem report ## 2015-00238
Sewage Sludge Analysis Results Converted from ug/L to mgfL
version Formula (ug/L) X (1 mg/ 1000 ug) = mg/L
nple Conversion: (4980 ug/L) X (1 M911000 ug) = 4.98 mg/L
g/kg = 1 pprn 1 % = 10,00o ppm (used to convert Mg kg to %)
Performed Results
urninurn
1020
mg/kg
Organic Nitrogen
43710
irrt onia-N (dry -weight)
2190
mg/kg
'senic
<13.4
mglkg
MH4 %
0.219
idmiurn
<13.4
mg/kg
ilcium;
12200
mg(kg
k
0-5
ipper
124
mg/kg
.ad
<13.4
mglkg
M03 %
0.0122
agnesiurn
2120
mg/kg
ercurV (dry weight]
<2-43
mg/kg
Organic Nitrogen %
4.371.
olybdenum
<13.4
mg/kg
ckel
<13-4
mg/kg
f
0.2
trate-MitFite (dry weight)
122
mg/kg
i SOS'%Solution
6.95
S_U.
tosphorus, Testa[ (dry weight)
13600
mg(kg
PAN
19.918
itassiurn
7160
mglkg
leniurn
<13.4
mg/kg
diurn
27300
mg/kg
[Cjeldahl Nitrogen (dry tent)
45900
mg/kg
tc
651
mg/kg
rcent Dry Weight
0.74
%
Available Nitrogen 19.918 lbs/dry ton

Environmental Chemists, Inc.
envirochem 6602 Wmdmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL & CONSULTING [phone]
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Town of Oak Island Date of Report: Feb 18, 2015
4601 East Oak Island Drive Customer PO #:
Oak Island NC 28465 Customer ID: 11100035
Attention_ David Kelly, 11 Report #: 2015-00515
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
15-01247 Site: Fish Factory WNtTP 1/14/2015 10:30 AM Solid/Sludge sunny Wright
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA200.7
4950 mg/kg
01/30/2015
Arsenic
EPA200.7
<4.80mg/kg
02/02/2015
Cadmium
EPA200.7
<4.80 mg/kg
02/02/2016
Calcium
EPA200.7
39200mg/kg
01122/2015
Chromium
EPA200.7
16.4mg/kg
02/02/2015
Copper
EPA200.7
342 mgikg
02/02/2015
Lead
EPA200.7
13.0 mg/kg
02/02/2015
Magnesium,
EPA200.7
2420 mg/kg
01=2015
Molybdenum
EPA200.7
<4.80mg/kg
02/02/2015
Nickel
EPA200.7
15.8 mg/kg
02/02/2015
Potassium
EPA200.7
4460 mgikg
01/22/2015
Selenium
EPA200.7
8.08 mgikg
02/02/2015
Sodium
EPA200.7
4610 mg/kg
01/2312015
Zinc
EPA200.7
798 mg/kg
01130/2015
Ammonia Nitrogen
EPA350.1
57.6 mg/kg
01/15/2015
Total Kjeldahl Nitrogen (TKN)
EPA 3512
120000 mg/kg
01/16/2015
Nitrate+Nitrite-Nitrogen
EPA353.2
2760 mg/kg
01/1512015
Total Solids (%)
sM 2W B
1.25 %
01/1512015
pH
SM4500 H B
6.91 units
01/22/2015
Total Phosphorus
SM4500 P F
36800 mg/kg
01/1612015
Mercury
SW8467471B
3.85 mg/kg
02/13/2015
Comment Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed
Report#:: 2015-00575 Pagel of 1

ArfalYliCal & Consulting Chemists
CLIENT;, Town of Oak Island
ADDRESS- 4601 East Oak Island Drive
Oak island, NC 28466
ENVIRONMENTAL CHEMISTS9 INC
NCDENM DWQ CERTIFICATION 0 94 NCDHHS:'DLS CERTIFICATION 9 37729.
�AWIAEEMW.lm
PROJECT NAME: Fish,Factory
CONTACT NAME: David Kelly
REPORT TO. Tray_Bivins
Permit # W00006790 ,
6602 Windmill Way WilmingtOn, NC 28406
OFFICE: 910-392-0223 FAX [phone]
REPORT NO:
PO NO:
PHONEIFAX: 201.80411278.7438
Sampled. By: z4z��� SAMPLE
TYPE: i=jntluent,
it htnuem, vv =Vvell, at = ULF - 111j'Q%J--7w11j
0611ectlo
'U C'
CL
to
A
0 e
Ea 49
0
0
C
rc- 1-i
PRESERVATION
ANALYSIS REQUESTED
Sample Identification
Date I
-Time
Temp--
6
xi
x
X.1
w
EffluentG
Effluent
2/111Onii Ar-October
11monih Nov -March
C
P
G
G
G
C
G
P
G
G
Feb/June/October
C
P
x1XI
TDS, TOC, Chloride,
G
C
G
P
G
G-
C
L
C
G
P
G
G
C-
P
G
G
C
P
L
G.
—G
LIMITS, (daily): SOD 15 mg1L, NH3 6 mg1L, TSS 10 mgft, Fecal 26colonles1100 ml :1
Transfer RelinquisM By: Date/Time Received By: Date/Time
1.677/
Y-7 /5
2.
Temperature When KoCetVeCl:- Accepteci:
Delivered By: Re6eived By:
116pla
ate: ' Time:
TU I IN HARD N D:
—
I

Annual Pathogen and Vector Attraction Reduction Form
Facility Name S & B Maintenance Permit Number W00000783
WVVTP Name Duke Energy NPDES # NC0007064
Monitoring Period: From _1_/01_/ 15_ To _12 / 31 / 15_
Pathogen Reduction (40 CFR 503.39) - Please indicate level achieved and alternative performed.
Class A
Alternative 1 Alternative 2 Alternative 3
Alternative 4 Alternative 5 Alternative 6
Class B
Alternative 1 Alternative 2 _x_ Alternative 3
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce
Pathogens":
Aerobic Digestion Air Drying Anaerobic Digestion
Composting _x_ Lime Stabilization
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
Pathogen Density
Number of
Frequency of
Sample
Analytical
in Sludge
Minimum Average Maximum Units
Exceedence
Analysis
Type
Techniqu
s
e
Fecal
2 x 10P MPN
Coliform
per gram of
total solids or 2
x 106 CFU per
gram of total
solids
1000 MPN per
gram of total
solid (dry
weight)
Salmonell
3 MPN per 4
a bacteria
grams total
(in lieu of
solid (dry
fecal
weight)
coliform
Vector Attraction Reduction (40 CFR 503.33) - Please indicate.option performed
Option 1 Option 2 Option 3 Option 4
Option 5 Option 6 _x_ Option 7 Option 8
Option 9 . Option 10
No vector attraction reduction options were performed
Certification Statement (please check the appropriate statement)
—x_ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement
attach an explanation why you have not met one or both of the requirements.")
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
x C,*/a/A4-4'3 4 M.E'45orl 09c-
Preparer Name and Title (type or print) Land Ap Ier Name
x 1-2 /&
Signature of Preparer Date Signature of Land
Title (if applicable) (type or print)
applicable) Date

Annual Pathogen and Vector Attraction Redaction Form
Facility Name S&B Maintenance Permit Number WQ0000783_
W WTP Name Town of Oak Island NPDES # WQ0005793_
Monitoring Period: From _1 / 1 /15_ To _12 /31 /I S
Pathogen Reduction (40 CFR 50332) - Please indicate level achieved and alternative performed.
Class A
Alternative 1 Alternative 2 Alternative 3
Alternative 4 Alternative 5 Alternative 6
Class B a
Alternative 1 Alternative 2 x Alternative 3
If applicable to altemative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Aerobic Digestion Air Drying Anaerobic Digestion
Composting x Lime Stabilization
If applicable to alternative performed (Class A or Class B) complete the following monitoring data
Parameter
Allowable Level
Pathogen Density
Number of
Frequency of
Sample
Analytical
in Sludge
Minimum Average Maximum
Exceedences
Analysis
Type
Technique
Units
Fecal
2 x 1 WN
'
Coliform
per gram of total
solids or 2 x 100
CFU per gram
oftotal solids
1000 MPN per
gram oftotal
solid (dry
weight)
Salmonella
3 h 4PN per 4
bacteria (in
grams total solid
lieu of fecal
(dry weight)
cwliform
Vector Attraction Reduction (40 CM 503M) - Please indicate option performed
Option 1 Option 2 Option 3 Option 4
Option 5 Option 6 a Option 7 Option 8
Option 9 Option 10
No vector attraction reduction options were performed
Certification Statement (please check the appropriate statement)
x "I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332 and the vector attraction reduction requirement
in 40 CFR 50333 have been met:"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332 and the vector attraction reduction requitement in 40
CFR 503.33 have not been meL" (Please note if you check this statement attach an explanation why you have not met one or both ofthe
requirements.")
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and -evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification" cluding fine and imprisonment"
No ►-o ►CL(-y Y A. 1056�1( .Sdm . r
Preparer Name and Title (type or print) Land per Name a Syiapplicable) (type or print)
81 goature of Preparer . Dale " "Signature of Land pher (if applicable) Date

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY16-SL023542
Heavy Metals
Soil Report Mehlich-3 Extraction
1
Client: Sam Carteret Advisor:
S & B Maintenance, Inc.
3865 Bus 17 East
Bolivia, NC 28422
Sampled County: Brunswick
Sampled: 12/10/2015 Received: 01/27/2016 completed: 02/02/2016
Farts: 1473 Links to Helpful Information
Agronomist's Comments:
This report contains both routine soil test information as well as heavy metals data in a section labeled as Heavy Metals under soil test lab results. Using Mehlich 3 as a soil test
extractant, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic (As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium (Cr)- 0.2 ppm, lead (Pb)-
4.2 ppm, nickel (Ni)- 0.8 ppm, & selenium (Se)- 0.2 ppm (FY2005-2007).Although the above
note where elevated above background levels. Where soil test phosphorus (P) is very high (P-1
metals here are not believed to pose a concern for plant growth, continue to monitor these and
> 100), crops will not respond to additional P applied. Note any lime and fertilizer
recommendations. Tissue te ting is advised where soil PH is high and is of concern as in samples here. Ja athi Kamalakanthan 2/2/2016
Sample ID: 1A
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6
K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.0 180-220 0
2 -Small Grain (SG) 0.0 80-100 0
210 0 0 pH$ 0 0 0
110 0 0 $pH 0 0 0
Note: 12 Note:
Note: 3 Note:
Test Results [units - WN in g/cm3; CEC and Na in megM00 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn Al2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N
1.37 1.32 50.0 100 0.0 7.7 324 14 98 2
62 66 31 24 730 730 519 0.2 0
Heavy Metals (parts per million): Arsenic, 0.2 Cadmium, 0.0
Nickel, 1.1 Chromium, 0.2 Lead, 2.2 Selenium, 0.0
Sample ID: 2A
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6
K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.0 180-220 10
2 -Small Grain (SG) 0.0 80-100 10
230 0 0 $ 0 0 0
130 0 0 $pH 0 0 0
Note: 12 Note:
Note: 3 Note:
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drift
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS4 NO3-N
0.46 1.47 30.9 100 0.0 8.1 58 7 98 2
36 53 17 10 80 80 55 0.1 0
Heavy Metals (parts per million): Arsenic, 0.1 Cadmium, 0.0
Nickel, 0.8 Chromium, 0.1 Lead, 0.9 Selenium, 0.1
North Carolina
Yt�t+ac�+r Tru,i l'iu::i t:+hnrn�.suan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Trox

s
NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomU
ReportNo.
FY16-SL023542
Sam Carteret
Page 2 of 3
Sample ID: 1D
Recommendations: Lime
Nutrients (lb/acre)
More
Lime History:
Crop (tons/acre) N P2O6
1 -Bermuda hay/past., M 0.0 180-220 0
2 -Small Grain (SG) 0.0 80-100 0
K2O
220
130
Mg S
0 0
0 0
Mn
pH$
pH$
Zn
0
0
Cu B
0 0
0 0
Information
Note: 12 Note:
Note: 3 Note:
Test Results [units - WN in g/cO; CEC and Na in meq/100 cm3;
NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1
K-1 Ca% Mg%
S-1 Mn-1
Mn-All Mn-AI2
Zn-1
Zn-Al
Cu-I Na ESP SS-1 NO3-N
0.60 1.31 51.0 100 0.0 7.8 176
9 98 2
84 104
52 45
541
541
368 0.1
0
Heavy Metals (parts per million): Arsenic, 0.2
Cadmium, 0.0
Nickel, 0.6
Chromium, 0.2
Lead,
1.5 Selenium, 0.2

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY16-SLO23542
Sam Carteret
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit ivww.ncaprpoy/aClronomilobAart4.htmiMsflnd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS4
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncapraov/aaronomi/uyrst.htm

v S, 5[ to.✓ a %SM t o/ �e s
ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit # NC 0007064
Approximate Total Gallons
57106
NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units (S.U.).
Tank Identification # 1 Digester # 2 Digester #2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(CO)
S.U.
pH prior to
Lime Addition
a'zz''S
1(26
pH after initial
Lime addition
7•�s
llH 6
II Sa
JZ'G 6
2S.1�—
pH z 2 Hours
after Lime
2-
Lit, '-I
12.35
2ti.9
12.3S'
Addition
pH z 24 Hours
after Lime
�2-23-�y
/23Z
173-7
12-2z
2�', I
►2.2't
i�
Addition
Tank Identification # 1 Digester # 2 Digester #2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(CO)
S.U.
pH prior to
Lime Addition
12- 77.1S
I c t 3
112-6
-4,-9;
2 4,
�L
pH after initial
Lime Addition
/L' z Z^5
11ft
1tN 6
12.3 6
Z L4. $
12.36
pH z 2 Hours
after Lime
)l-iz-�5'
/k��
too I
j2. 3 2
24. S
12.32
5--�-
Addition
pH z 24 Hours
after Lime
IT -23 ��
/y3 2
Iz3 z
12./ 6
2 �' i
/2 . 16
Addition
OE&RC-3241 Rev. 14 Page 35 of 40

ATTACHMENT 9
Page 1 of I
Sewage Sludge pH Adjustment:
Sludge Soule BSF WVVTP ,`NPDES Permit #NC 0007064
6 Approximate Total Gallons SLt g!
NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart QE&RC-3224).
NOT, All pH measurements are in Standard Units (S•U.).
Tank Identification # 4 Digester # 2 Digester #2 Glarif€er (Circle One)
Date
Sample
Time
Analysis
Time
pH
(S.U.)
Temperature
(C°}
Calculated
pH
Operator
S U
pH prior to
Lime Addition
- E��
7, 3 3
f
y Q'�
PH after initial
Lime addition
e2 --3—I.?
I FJ7�.
I` j-j-4
f � � 3o
�j`
17. (
# .1 1
Gtfr._
pH >- 2 Hours
after Lime
- -Q
U �
q
4 SZ/
�r /
t k�7
12-- G
Addition
PH �t 24 Hours
after Lime
'+�
6 ti
I 17
/ 2-.17
2- Y
i i� to
Gte,--
Addition
Tank Identification # 1 Digester # 2 Digester Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
°
Calculated
pH
Operator
Time
Tune
(S_U.)
(�)
s u
pH prior to
Lime Addition
Z-3- ff—
1 r -76
7- 31
1
7, t
pH after initial
Lime Addition
-3 l �-
���4
if-0
1 d4t
,
2-`t 7
r
PH2t2Hours
after Lime
t
a. �11
'ii
f E�
i �
2—t o
Addition
PH >_ 24 Hours
after Lime
'`�'i
6 fy�
f
6 E
t f,
1, Y2-
Addition
aE&RC-3241 I Rear. 14 1 Page 35 of 40

(� ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit # NC 0007064
Approximate Total Gallons
NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units (S.U.).
Tank Identification # 1 Digester # 2 Digester #2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
PH
Operator
Time
Time
(S.U.)
(C°)
S.U.
PH prior to
7•q'r
Lime Addition
2_t5_I,r
Offs-'
old L
.23,
7, gZ
c=�t
s-v
PH after initial
Lime addition
_2-tti'0—
O qS7
/op b
l
�2 Li, 7—
pH z 2 Hours
after Lime
T-C
a
,3J
Addition
PH z 24 Hours
after Lime
��. if
jolt
1 p 2 Z
11. 0
a. 1 7
G it w
Addition
Tank Identification # 1 Digester 2 Digester #2 Clarifier (Circle One)
Date
Sample
Analysis
PH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(CO)
S.U.
PH prior to
Lime Addition
.2- I1-0'
pbS
0101
6,36
.2 Lt.f
/
(� +�
PH after initial
Lime Addition
0153
tool
/2. `a
A.3, 3
1 ,� ..7 %
PH z 2 Hours
after Lime
�5,
12;L0
f���
1.2•K�
C�
2 �- 1
��, l�(�
Gt� �'
Addition
PH z 24 Hours
after Lime
.1_2u-lr
1 U24
1a.24
S- 7
Q I6
crl�lk
Addition
OE&RC-3241 Rev. 14 Page 35 of 40

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit # NC 0007064
Approximate Total Gallons
NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units (S.U.).
Tank Identification # 1 Digester # 2 Digeste #2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(CO)
S.U.
PH prior to
Lime Addition
1 y is
0 0 7
10
S" ��
w
PH after initial
Lime addition
3, y. T
1036
i v3
2. ss
J 7.41
12,31w-f14.�
PH Z 2 Hours
after Lime
Addition
*g
12S7
i3U1
L-S�
120
2,32-
pH �: 24 Hours
after Lime
3-1D-Ij
l 1 d
II y
��•�
�S
1 �, I
C �... /J•.✓
Addition
Tank Identification # 1 Digester # 2 Digester #2 Clarifi (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(C°)
S.U.
PH prior to
Lime Addition
3li-IJ
o syi
laesC
r,,R
Z K,S�
�,f�•�✓
PH after initial
Lime Addition
M
Z• ��
`�
G
�.(J
�,����
pH z 2 Hours
after Lime
Addition
3.151
IZ,2
IJOS
12.61C,�v
,
,�/��'t
PH z 24 Hours
after Lime
11ov
1103
(,j.53
(S.7
��,�(o
G //'w.IJaw
Addition
OE&RC-3241 I Rev. 14 I Page 35 of 40

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit # NC 0007064
Approximate Total Gallons S Y Uy
NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units (S.U.).
Tank Identification # 1 Digester # 2 Digester V2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(Co)
S.U.
PH prior to
Lime Addition
((.2,1-ii
6 731
0 7 `l y
7. *2Z
Q
7, 72
Gt
PH after initial
Lime addition
j �'��'�
�Y�2'
1.2. 3
PH z 2 Hours
after Lime
/
Addition
PH >_ 24 Hours
after Lime
j �.1Lr�J
0 7
3/
2 s• �"
(Z 3
Addition
i 0
Tank Identification # 1 Digester (S;er #2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
PH
Operator
Time
Time
(S.U.)
(CO)
S.U.
PH prior to
Lime Addition
V-Aklf-
0739
O 7 Yr
'7. 9 /
,J
2 s-. !
7- y2
PH after initial
Lime Addition
J 1•2/•
O Y3Z
O Y39
1.1.2 6
2 S. 2-
/ 2.2
PH >_ 2 Hours
after Lime
�1'�I"
tt���
��fl
t?,2y
23' i
+
1���q
CtC�v
Addition
I
PH z 24 Hours
after Lime
�(,2?/t
toei7
L 00'
82.Z
��•
�2, '�-
C
Addition
OE&RC-3241 Rev. 14 Page 35 of 40

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit # NC 0007064
Approximate Total Gallons 6 , 60 6,i( g
LZ
NOTE: PH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units (S.U.).
Tank Identification # 1 Digester # 2 Digester #2 Clarifier (Circle One)
tia� I
Date
Sample
Analysis
PH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(C°)
S.U.
PH prior to
L meAddition
40"'i's
0" 5
0,'112
pH after initial
Lime addition
l0-t H
K
(0 Z5
12.52
PH z 2 Hours
after Lime
1230
q 3 s'
Addition
PH >_ 24 Hours
after Lime
lG-�•�5
It��
2�z
12.3 1
Addition
Tank Identification # 1 Digester # 2 Digester #2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
PH
Operator
Time
Time
(S.U.)
(C°)
S.U.
PH prior to
Lime Addition
10.1q_is
c)go
Oql
-7. 3 2
2 io
PH after initial
Lime Addition
a, 30
PH z 2 Hours
/
after Lime
� �—
Addition
pH z 24 Hours
IV
after Lime
HIS ,IS
115 t
�2 0 2
12.11
25. 3
S
Addition
14 etcc�rvod@, WZ L
OE&RC-3241 I Rev. 14 1 Page 35 of 40 1

P►,oe-&;� v-0
ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit #x NC 0007064
Approximate Total Gallons Lf "
NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units (S.U.).
Tank Identification # 1 Digester # 2 Digester 2 Llarifid (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
PH
Operator
Time
Time
(S.U.)
(C°)
S.U.
PH prior to
Lime Addition
6` !`�'rf
O tl �tY
0 `(Y y
6. �
.� �0
� �
�-
PH after initial
Lime addition
&CO-f1'
Cl�2d
vS1)
I �.3
2S. 6
I rS 2
r,4
pH >_ 2 Hours
after Lime
Addition
6_ cy-r
a U
% g
o l y
I2_ t'S�
d 2.3"r3''
GtF
PH >_ 24 Hours
after Lime
6-11-11r
l A.
Addition
Tank Identification # 1 Digester # 2 Digester #2 Clarifier (Circle One)
Date
Sample
Time
Analysis
Time
pH
(S.U.)
Temperature
(C°)
Calculated
PH
Operator
S.U.
PH prior to
Lime Addition
6 _ `u-IT
0YJJV
0 -69
S,3 2,
2_r o
S
PH after initial
Lime Addition
6 lu-`f,
V s d 2
of 2- ti
Lim
6 -Cw6f
pH >_ 2 Hours
after Lime
!ill
`a��
(0('6
I2-1
.Jr,
12..J^
Ct�
Addition
PH >_ 24 Hours
after Lime
6 - W ']**"
of
a5g0
1 a, y6
Addition
0E&RC-3241 I Rev. 14 1 Page 35 of 40

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit # NC 0007064
Approximate Total Gallons ✓ L "
NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units (S.U.).
Tank Identification�y # 1 Digester # 2 Digester 2 Clarifie (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(Co)
S.U.
PH prior to
Lime Addition
7-
r
130
7 70
PH after initial
Lime addition
?,./Y-if
O 32Z
132 y
12. U
2 5.7
2• ��
G
PH >_ 2 Hours
after Lime
7- /f'I S
15'Sr t
fo
C �
Addition
PH >_ 24 Hours
after Lime
7 cT-��
j'7W
1 `(u3
I� k9
�a
!2, drl
Addition
Tank Identification # 1 Digester 2 Digester #2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
Operator
Time
Time
(S.U.)
(C°)
S.U.
PH prior to
Lime Addition
%� t y-�
12,fr
1301.
G —
f' 3 If
PH after initial
Lime Addition
7r/ Y �r
/3�Z
4
��
21. 5
PH >_ 2 Hours
after Lime
7 �¢'/S
!TIL/
ITf 3
M, 31
28,0
/ 2 •*
C -
Addition
PH >_ 24 Hours
after Lime
7-15-'Y
y
I . f y
r�
3v o /
B Z, 71
C t
Addition
OE&RC-3241 Rev. 14 Page 35 of 40

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit # NC 0007064
Approximate Total Gallons 5t1u-o
NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units (S.U.).
Tank Identification # 1 Digester # 2 Digester #2 Clarifier (Circle One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
Operator
q
Time
Time
(S.U.)
(Co)
pH prior to
Lime Addition
a-2i-lf
GSIL
UTI`/
7 j-7
Z•S-1
7.3-7
G 4.
pH after initial
Lime addition
k)
v f4{r
/ 2. '10
(, 1
12. ILI
pH >_ 2 Hours
after Lime
�_Z(=1r
o qqr
o i q7
12.30
-2 - 7
Addition
pH >_ 24 Hours
after Lime
�:b6-[I
J�
lz.K7
2�S. %
!.Z•
CK
Addition
Tank Identification # 1 Digester Digester #2 Clarifier (Circle'One)
Date
Sample
Analysis
pH
Temperature
Calculated
pH
OperatorS.U.
Time
Time
(S.U.)
(CI)
pH prior to
Lime Addition
�(-ZJ=i,t'
oSl Z
D,r)!'
S y
S
S� I ,-q
-cX w�
pH after initial
Lime Addition
3
Bf-,fr
12.SN
o2 f. 7
/2.F6
c 4.t
pH >_ 2 Hours
after Lime
K Lf'11
v �Hf
d � Y �
/ :2.
P
/
c (c A,,-jt
Addition
pH z 24 Hours
after Lime
g -L`��
©,Fdy
`z_�V
�� j
L
C r� �+�.J�
Addition
V
OE&RC-3241 I Rev. 14 . I Page 35 of 40

Lime Stabilization pH Test Results
Town of Oak Island
S & B Maintenance: Hauler
Sludge Source: Fish Factory Rd WWTP Permit #: WQ0005790
Approx. Gallons:
Initial pH Test
Date:Time: 711 Operator:
pH Temp. �� (� °c
Converted pH to 25°c pH
Conversion Factor (cf) = (Temp reading'c - 25°c) x 0.03. (/°c - 257c) x 0.03
Converted pH = measured pH +/- the Correction Factor. _ j2 XpH (+/-) (cf) = j,�Z.pH
2 Hour pH Test
.Date: /&! ` S Time: "��� Operator: �✓
a
kJpH `,Z, f�
7� Temp• 1 7P3' °c : Y
Converted pH to 25 c //1 ' y pH
Conversion Factor (cf) = (Temp reading°c - 25°c) x 0.03. ((% Y 'c - 25°c) x-0.03 = _(cf)
Converted pH = measured pH +/- the Correction Factor. f z. /s H (+/_) r (cfl = pH
24 Hour pH Test
Dater
y ve/ Time: '� � �' ,�� Operator: 5-6,1 g t"
pH Temp. c
Converted pH to 25°c pH
Conversion Factor (cf) = (Temp reading°c - 25°c) x 0.03. (lL�c - 25°c) x 0.03 = �� (cf)
Converted pH = measured pH +/- the Correction Factor. /2_pH (+/-) , / (dfl = f �, pH
iiimai ana z dour test must be above a converted pH of 12 and the 24 Hour test must be above a converted pH of 11.5
Operator Signature for release: Date/Time
Hauler Signature of Acceptance: ���� �� Date/Time
dekii5/2/12

3868 Business 17
P.O. Box 8
Bolivia, NC 28422
1-910-253-4689
February 26, 2016
N.C. Dept of Environment and Natural Resources
Division of Water Resources
Water Quality Permit Section
Non -Discharge Permitting Unit
512 N. Salisbury St.
Raleigh, NC 27604
Dear Sir/Madam
S&B Maintenance, LLC is sending in the required forms for our DWQ permit for this past
year. This report is for the land application of residuals for the reporting year of 2014. If
you have questions or need more information you can reach the office at the provided
phone number.
Since ely,
Sammy P Carteret