NCG030145_MONITORING INFO_20190503

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V
DOC TYPE
El HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ D' 65o 3
YYYYMMDD

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No, NCG030000
Date submitted s �.,wq
CERTIFICATE OF COVERAGE NO. NCG030145
FACILITY NAME: Newton Instruments
COUNTY: Granville
PERSON COLLECTING SAMPLES: Geoffrey Murphrey RECEIVED
LABORATORY: Pace Analytical Lab Cert. #: 40 tf i
Comments on sample collection or analysis: Monthly saWplin Z019
SAMPLE COLLECTION YEAR: 2019
SAMPLE PERIOD[:] Jan -June❑ July -Dec
or®Monthly' April 2019
DISCHARGING TO CLASS❑ORW®HQW❑Trout❑PNA
❑Zero-flow❑Water Supply❑SA
❑Other
CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3-->
DWR SECTION
Part A: Stormwater Benchmarks and Monitoring Results
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended
Solids
PH,Non-Polar
Standard
units
Copper
Lead
Zinc
O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks ==_>
-
-
100 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
001
04/05/19
0.5
45.5 mg/L
7.1
0.0097 mg/L
<0.005 mg/L
0.0573 mg/L
<4.8 mg/L
0.0011 mg/L
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan mayso certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
Permit Date: 11/1/2017-10/31/2022 SWU-245, last revised 10/25/2012
Page 1 of 3

"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
Name (Print me)
Title (Prin 'tle)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report _Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month.
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =_->
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2017-10/31/2022 5WU-245, last revised 10/25/2012
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?YES ® NO
IF YES,HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE?YES ® NO
REGIONAL OFFICE CONTACT NAME: John Holley
Mail an original and one copy of this DMf% including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case o "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Perm
(Date)
Permit Date: 11/1/2017-10/31/2022
SWU-245, last revised 10/25/2012
Page 3 of 3

m
aceAnalyltical
www.pacelebs.com
April 22, 2019
Mr. Pete Dressel
Piedmont Geologic
6003 Chapel Hill Road
Suite 109
Raleigh, NC 27607
RE: Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Dressel:
Enclosed are the analytical results for sample(s) received by the laboratory on April 05, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jonathan Murphrey, Piedmont Geologic
Q pCCRFO
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pagel of 29

aceAnalytical�
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Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VrginiafVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 29

m
aceAnaVical
www.pacelabs.com
Project: Newton Instruments
Pace Project No.: 92424294
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92424294001 Outfall -001 Water 04/05/19 09:45 04/05/19 12:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 29

Pace Analytical Services, LLC
® 9800 Kincey Ave. Suite 100
acmnalXical Huntersville, NC 28078
WWWpacelab3 mm [phone]
SAMPLE ANALYTE COUNT
Project! Newton Instruments
Pace Project No.: 92424294
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92424294001 Outfall -001 EPA 16648
JMS
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
DS
12
PAST -A
EPA 245.1 Rev 3.0 1994
RDT
1
PASI-A
EPA625.1
BPJ
62
PASI-C
EPA624.1
DLK
32
PASI-C
SM 2540D-2011
MJP
1
PASI-A
EPA 420A Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2011
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 29

aceAnalytrcal
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments
Pace Project No.: 92424294
Sample: Outfall -001
Lab ID: 92424294001
Collected:
04/05/19 09:45
Received: 04/05119 1Z25 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Field Data
Analytical Method:
Collected By
G.
1
04/09/19 10:16
Mutphrey
Collected Date
04105/19
1
04/09/19 10A6
Collected Time
09:45
1
04/09/19 10:16
pH
7.1
Std. Units
0.10
1
04/09/19 10:16
HEM, Oil and Grease
Analytical
Method: EPA 1664B
Oil and Grease
NO
mg1L
4.8
1.2
1
04/18/19 06:48
608 PCB Pest RVE
Analytical
Method: EPA 608.3
Preparation Method:
EPA 608.3
Aldrin
NO
ug1L
0.050
0.022
1
04/10/19 07752
04/10/19 17:11
309-00-2
alpha-8HC
NO
ug1L
0.050
0.019
1
04/10119 07:52
04/10119 17:11
319-84-6
beta-BHC
NO
ug1L
0.050
0.014
1
04/10/19 07:52
04/10/19 17:11
319-85-7
delta-BHC
NO
ug1L
0.050
0.020
1
04/10/19 07:52
04/10/19 17:11
319-86-B
gamma-BHC (Lindane)
ND
ug/L
0,050
0.012
1
04/10/19 07:52
04/10119 17:11
58-89-9
Chlordane (Technical)
NO
uglL
0.50
0.20
1
04110/19 07:52
04/10/19 17:11
57-74-9
alpha -Chlordane
NO
uglL
0.050
0.0090
1
04/10/19 07:52
04/10/19 17:11
5103-71-9
gamma -Chlordane
NO
uglL
0.050
0,017
1
04/10/19 07:52
04110/19 17:11
5103-74-2
4.4'-DDD
NO
uglL
0.050
0,0069
1
04110/19 07:52
04110/19 17:11
72-54-8
4.4'-DDE
NO
uglL
0,050
0,0064
1
04110/19 07:52
04110/19 17:11
72-55-9
4,4'-DDT
NO
uglL
0.050
0.018
1
04110/19 07:52
04110/19 17:11
50-29-3
Dieldrin
NO
uglL
0.050
0.0073
1
04/10/19 07:52
04/10/19 17:11
60-57-1
Endosulfan I
NO
uglL
0.050
0.0094
1
04/10/19 07:52
04/10/19 17:11
959-98-8
Endosulfan II
NO
uglL
0.050
0.0065
1
04/10/19 07:52
04110/19 17:11
33213-65-9
Endosulfan sulfate
NO
uglL
0.050
0.0091
1
04/10/19 07:52
04110/19 17:11
1031-07-8
Endrin
NO
uglL
0.050
0,0089
1
04/10/19 07:52
04/10/19 17:11
72-20-8
Endrin aldehyde
ND
uglL
0.050
0.013
1
04/10/19 07:52
04/10/19 17:11
7421-93-4
Heptachlor
NO
uglL
0.050
0.016
1
04/10/19 07:52
04/10/19 17:11
76-44-8
Heptachlor epoxide
NO
ug1L
0.050
0,0097
1
04110/19 07:52
04110/19 17:11
1024-57-3
PCB-1016 (Aroclor 1016)
ND
uglL
0.50
0.50
1
04110/19 07:52
04/10/19 17:11
12674-11-2
PCB-1221 (Aroclor 1221)
ND
uglL
0.50
0.50
1
04110/19 07:52
04/10/19 17:11
11104-28-2
PCB-1232 (Aroclor 1232)
NO
uglL
0.50
0.50
1
04/10/19 07:52
04110/19 17:11
11141-16-5
PCB-1242 (Aroclor 1242)
NO
uglL
0.50
0.50
1
04/10/19 07:52
04/10/19 17:11
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug1L
0.50
0.50
1
04/10/19 07:52
04/10/19 17:11
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug1L
0.50
0.50
1
04/10/19 07:52
04/10/19 17:11
11097-69-1
PCB-1260 (Aroclor 1260)
NO
ug1L
0.50
0.50
1
04/10/19 07:52
04/10/19 17:11
11096-82-5
Toxaphene
ND
uglL
0.50
0.20
1
04/10/19 07:52
04/10/19 17:11
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
102
%
10-130
1
04/10/19 07:52
04/10/19 17:11
877-09-8
Decachlorobiphenyl (S)
50
%
10-130
1
04/10/19 07:52
04110/19 17:11
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Antimony
NO
ug/L
5.0
3.9
1
04/12/19 16:19
04/15/19 03:55
7440-36-0
Arsenic
ND
ug1L
10.0
5.0
1
04/12/19 16:19
04/15/19 03:55
7440-38-2
Beryllium
0.067J
ug1L
1.0
0.050
1
04/12/19 16:19
04/15/19 03:55
7440-41-7
Cadmium
ND
uglL
1.0
0.50
1
04/12/19 16:19
04/15/19 03:55
7440-43-9
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except
in full,
Date: 04122/2019 04:24 PM
without the written consent of Pace Analytical Services, LLC.
Page 5 of 29

m
ace Analytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvilie, NC 28078
[phone]
Project: Newton Instruments
Pace Project No.: 92424294
Sample: Outfall -001 Lab ID: 92424294001 Collected: 04/05/19 09:45 Received: 04/05/19 12:25 Matrix; Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Chromium
ND
ug/L
5.0
2.5
1
04/12/19 16:19
04/15119 0155 7440-47-3
Copper
9.7
ug1L
5.0
2.5
1
04/12/19 16:19
04/15119 03:55 7440-50-8
Lead
ND
ug/L
5.0
2.5
1
04/12/19 16:19
04/15/19 03:55 7439.92.1
Nickel
3.6.11
ug1L
5.0
2.5
1
04/12/19 16A9
04/15/19 03:55 7440-02-0
Selenium
ND
ug1L
10.0
5.0
1
04/12/19 16:19
04/15/19 03:55 7782-49-2
Silver
ND
ug1L
5.0
2.5
1
04/12/19 16:19
04/15/19 03:55 7440.22-4
Thallium
ND
ug1L
10.0
5.0
1
04/12/19 16:19
04/15119 03:55 7440-28-0
Zinc
57.3
ug1L
10.0
2.5
1
04/12119 16:19
04/15/19 03:55 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Mercury
ND
ug/L
0.20
0.10
1
04/1911908:30
04/19/1912;58
7439-97-6 M1
625 MSSV
Analytical Method: EPA625.1
Preparation Method: EPA625A
Acenaphthene
ND
ug/L
5.0
0.25
1
04/09/19 20:34
04/11/19 23:00
83-32-9
Acenaphthylene
ND
ug/L
5.0
0.21
1
04/09/19 20:34
04/11/19 23:00
208-96-8
Anthracene
ND
ug1L
5.0
0.14
1
04/09119 20:34
04/11/19 23:00
120-12-7
Benzidine
ND
ug/L
50.0
5.1
1
04/09/19 20:34
04/11/19 23:00
92-87-5 L2
Benzo(a)anth race ne
ND
ug/L
5.0
0.33
1
04/09/19 20:34
04/11/19 23:00
56-55-3
Benzo(a)pyrene
ND
ug1L
5.0
0.30
1
04/09/19 20:34
04/11/19 23:00
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
0.28
1
04/09119 20:34
04/11/19 23:00
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
0.38
1
04/09/19 20734
04/11/19 23:00
191-24-2
Benzo(k)fluoranthene
ND
ug1L
5.0
0.43
1
04/09/19 20:34
04/11/19 23:00
207-08-9
4-Bromophenylphenyl ether
ND
ug1L
5.0
0.82
1
04/09/19 20:34
04/11/19 23:00
101-55-3
Sutylbenzylphthalate
ND
ug1L
5.0
0.79
1
04/09119 20:34
04/11/19 23:00
85-68-7
4-Chloro-3-methylphenol
ND
ug1L
5.0
3.7
1
04/09/19 20:34
04/11/19 23:00
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
0.92
1
04/09119 20:34
04/11/19 23:00
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.0
1
04/09119 20:34
04/11119 23:00
111-44-4
2-Chloronaphlhalene
ND
ug1L
5.0
0.98
1
04/09/19 20:34
04/11/19 23:00
91-58-7
2-Chlorophenol
ND
ug1L
5.0
1.3
1
04/09/19 20:34
04/11/19 23:00
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
0.87
1
04/09119 20734
04/11/19 23:00
7005-72-3
Chrysene
ND
ug/L
5.0
0.21
1
04/09119 20:34
04/11/19 23:00
218-01-9
Dibenz(a,h)anth race ne
ND
ug1L
5.0
0.55
1
04/09/19 20:34
04/11/19 23:00
53-70-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.88
1
04/09119 20:34
04/11/19 23:00
95-50-1
1,3-Dichlorobenzene
ND
ug/L
5.0
0.81
1
04/09/19 20:34
04/11/19 23:00
541-73-1
1,4-Dichlorobenzene
1.1J
ug1L
5.0
0.95
1
04/09/19 20:34
04/11/19 23:00
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
25.0
2.1
1
04/09/19 20:34
04/11/19 23:00
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.7
1
04/09/19 20:34
04/11/19 23:00
120.83-2
Diethylphthalate
ND
ug/L
5.0
0.58
1
04/09/19 20:34
04/11/19 23:00
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1.2
1
04/09/19 20:34
04/11/19 23:00
105-67-9
Dimethylphthalate
ND
ug/L
5.0
0.76
1
04/09/19 20:34
04/11/19 23:00
131-11-3
Di-n-butylphthalate
ND
ug1L
5.0
0.75
1
04/09/19 20:34
04/11/19 23:00
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
2.6
1
04/09/19 20:34
04/11/19 23:00
534-52-1
2,4-Dinitrophenol
ND
ug1L
50.0
9.0
1
04/09/19 20i34
04/11/19 23:00
51-28-5
2,4-Dinitratoluene
ND
ug/L
5.0
0.90
1
04/09/19 20:34
04/11/19 23:00
121-14-2
2,6-Dinitratoluene
ND
ug/L
5.0
0.98
1
04/09/19 20:34
04/11/19 23:00
606-20-2
❑i-n-octylphthalate
ND
ug1L
5.0
0.66
1
04/09/19 20:34
04/11/19 23:00
117-84-0
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except
in fuli,
Date: 04/22/2019 04:24 PM
without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments
Pace Project No.: 92424294
Sample: Outfall -001
Lab ID: 92424294001
Collected:
04/05/19 09:45
Received: 04/05/19 12:25 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
625 MSSV
Analytical
Method: EPA 625.1 Preparation Method:
EPA 625.1
1,2-Diphenylhydrazine
ND
ug/L
5.0
0.90
1
04/09/19 20:34
04/11/19 23:00
122-66-7
bis(2-Ethyl hexyl)phtha late
ND
ug1L
5.0
0.79
1
04/09/19 20:34
04/11/19 23:00
117-81-7
Fluoranthene
ND
ug/L
5.0
0.21
1
04/09/19 20:34
04/11/19 23:00
206-44-0
Fluorene
ND
ug/L
5.0
0.21
1
04/09/19 20:34
04/11/19 23:00
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
0.94
1
04/09/19 20:34
04/11/19 23:00
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
0.72
1
04/09/19 20:34
04111/19 23:00
118-74.1
Hexachlorocyclopentadiene
ND
ug/L
10.0
0.88
1
04/09/19 20:34
04111/19 23:00
77-47-4
Hexachloroethane
ND
ug/L
5.0
1.1
1
04/09/19 20:34
04/11/19 23:00
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
0.29
1
0410911920:34
0411111923:00
193-39-5
Isophorone
ND
ug/L
10.0
0.89
1
04109/19 20:34
04111/19 23:00
78-59-1
Naphthalene
ND
uglL
5.0
0.34
1
04/09/19 20:34
04/11119 23:00
91-20-3
Nitrobenzene
ND
ug/L
5.0
1.1
1
04/09/19 20:34
04/11119 23:00
98-95-3
2-Nitrophenoli
ND
ug/L
5.0
0.91
1
04/09/19 20:34
04/11/19 23:00
88-75.5
4-Nitrophenol
ND
ug1L
50.0
4.1
1
04/09/19 20:34
04111/19 23:00
100-02-7
N-Nitrosodimethylamine
ND
ug1L
5.0
0.91
1
04/09/19 20:34
04111/19 23:00
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
0.99
1
04/09/19 20:34
04/11/19 23:00
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1.0
1
04/09/19 20:34
04/11/19 23:00
86-30-6
Pentachlorophenol
ND
ug/L
10.0
4.6
1
04/09/19 20:34
04111/19 23:00
87-86-5
Phenanthrene
ND
ug/L
5.0
0.22
1
04/09/19 20:34
04111/19 23:00
85-01-8
Phenol
ND
uglL
5.0
1.9
1
04109/19 20:34
04111/19 23:00
108-95-2
Pyrene
ND
ug/L
5.0
0.19
1
04/09/19 20:34
04111/19 23:00
129-00-0
1,2,4-Trichlorobe nzene
ND
uglL
5.0
0.98
1
04109/1920:34
04111/19 23:00
120-82-1
2,4,6-Trichlorophenol
ND
uglL
10.0
1.3
1
04/09/19 20:34
04/11/19 23:00
88.06-2
Surrogates
Nitrobenzene-d5 (S)
78
%
10-120
1
04/09/19 20:34
04111/19 23:00
4165-60-0
2-Fluorobiphenyl (S)
70
%
15-120
1
04/09/19 20:34
04111/19 23:00
321-60-8
Terphenyl-d14 (S)
70
%
11-131
1
04109/19 20:34
04/11/19 23:00
1718-51-0
Phenol-d6 (S)
20
%
10-120
1
04/09/19 20:34
04/11/19 23:00
13127-88-3
2-Fluorophenol (S)
32
%
10-120
1
04/09/19 20:34
04/11/19 23:00
367-12-4
2,4,6-Tribromophenol (S)
89
%
10-137
1
04/09/19 20:34
04/11/19 23:00
118-79-6
624 Volatile Organics
Analytical Method: EPA 624.1
Acrolein
ND
ug/L
5.0
2.7
1
04109/1919:34
107-02-8
Acrytonitrile
ND
ug/L
50.0
0.90
1
04/09/19 19:34
107-13-1
Benzene
ND
ug/L
1.0
0.15
1
04/09/19 19:34
71-43-2
Bromodichloromethane
ND
ug/L
2.0
0.26
1
04/09/19 19:34
75-27-4
Bromoform
ND
ug/L
2.0
0.62
1
04109/1919:34
75-25-2
Bromomethane
ND
ug/L
2.0
0.62
1
04109/1919:34
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
0.22
1
04/09/19 19:34
56-23-5
Chlorobenzene
ND
ug/L
2.0
0.23
1
04109/1919:34
108-90-7
Chloroethane
ND
ug/L
2A
0.49
1
04/0911919:34
75.00-3
2-Chloroethylvinyl ether
ND
ug/L
10.0
6.9
1
04109/19 19:34
110-75-8 c2
Chloroform
ND
ug/L
5.0
2.3
1
04/09/1919:34
67-66-3
Chloromethane
ND
ug/L
2.0
0.39
1
04109/1919:34
74-87-3
Dibromochloromethane
ND
ug/L
2.0
0.41
1
04/09/19 19:34
124-48-1
1,1-Dichloroethane
ND
ug/L
2.0
0.27
1
04109/1919:34
75-34-3
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except
in full,
Date: 04/22/2019 04:24 PM
without the written
consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall -001 Lab lD: 92424294001 Collected: 04105/19 09:45 Received: 04/05/19 12:25 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis- 1, 3-Dich loropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1, 2, 2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Thch loroetha ne
1,1, 2-Trish lorootha ne
Trichloroethene
Vinyl chloride
Surrogates
4-Bromafluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
420.4 Phenolics, Total
Phenol
450OCNE Cyanide, Total
Cyanide
Date: 04/22/2019 04:24 PM
Analytical Method: EPA 624.1
ND
ug1L
2.0
0.34
1
04109/1919:34
107-06-2
ND
ug/L
2.0
0.24
1
04/09/1919:34
75-35-4
ND
ug/L
2.0
0.25
1
0410911919:34
156-60-5
ND
ug/L
2.0
0.19
1
04/09/1919:34
78-87-5
ND
ug/L
2.0
0.30
1
04/09/1919:34
10061-01-5
ND
uq/L
2.0
0.31
1
04/09/1919:34
10061-02-6
ND
ug/1-
1.0
0.26
1
04109/1919:34
100-41-4
ND
ug/L
5.0
3.7
1
0410911919:34
75-09-2
ND
ug/L
20
0.22
1
04/09/1919:34
79-34-5
ND
ug/L
2.0
0.16
1
04/09/1919:34
127-18-4
ND
ug/L
1.0
0.24
1
04/09/1919:34
108-88-3
ND
ug/L
2.0
0.18
1
04109/1919:34
71-55-6
ND
ug/L
2.0
0.24
1
04/09/1919:34
79-00-5
ND
ug/L
2.0
0.22
1
04/0911919:34
79-01-6
ND
ug/L
2.0
0.24
1
04/0911919:34
75-01-4
102
%
70-130
1
04/09/19 19:34
460-00-4
117
%
70-130
1
04109/1919:34
2037-26-5
95
%
70-130
1
04/09/1919:34
17060.07-0
Analytical Method: SM 254OD-2011
45.5 mg1L 6.2 6.2 1 04109/1911:35
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
ND mg/L 0,020 0.0050 1 04/09/19 07:35 04/10/19 09:25 108-95-2
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
ND mg/L 0.0080 0,0060 1 04/10119 13:40 04/11/19 09:50 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 29

>o
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www.pecelabs.cnm
QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 470147 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92424294001
METHOD BLANK: 2552605 Matrix: Water
Associated Lab Samples: 92424294001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Oil and Grease mg1L ND 4.8 1,2 04/18/19 06:45
LABORATORY CONTROL SAMPLE:
2552606
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg1L
38.5 36.9
96
78-114
MATRIX SPIKE SAMPLE;
2552607
35460867002 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
5.7 38.5
43.5
98 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/2212019 04:24 PM without the written consent of Pace Analytical services, LLC. Page 9 of 29

m
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Project: Newton Instruments
Pace Project No.: 92424294
QC Batch: 470254
QC Batch Method: EPA 245.1 Rev 3.0 1994
Associated Lab Samples: 92424294001
METHOD BLANK: 2553164
Associated Lab Samples: 92424294001
Parameter
Mercury
QUALITY CONTROL DATA
Analysis Method: EPA 245.1 Rev 3.0 1994
Analysis Description: 245.1 Mercury
Matrix: Water
Blank Reporting
Units Result Limit
ug/L ND 0.20
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MDL Analyzed Qualifiers
0.10 04/19/19 12:47
LABORATORY CONTROL SAMPLE: 2553165
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 102 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2553166 2553167
MS MSD
92424268001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug1L ND 2.5 2.5 2.0 2.0 79 82 70-130 3 20
Results presented on this page are In the units indicated by the "Units- column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
QC Batch: 469120 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92424294001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HunlersvBle, NC 28078
[phone]
METHOD BLANK: 2547776
Associated Lab Samples: 92424294001
Parameter
Units
Matrix:
Blank
Result
water
Reporting
Limit
MDL
Analyzed Qualifiers
Antimony
uglL
ND
5.0
3.9
04/15/19 02:25
Arsenic
uglL
ND
10.0
5.0
04/15/19 02:25
Beryllium
uglL
ND
1.0
0.050
04/15/19 02:25
Cadmium
uglL
ND
1,0
0.50
04/15/19 02:25
Chromium
uglL
ND
5.0
2.5
04/15/19 02:25
Copper
uglL
ND
5.0
2.5
04/15/19 02:25
Lead
ug1L
ND
5.0
2.5
04/15/19 02:25
Nickel
uglL
ND
5.0
2.5
04/15/19 02:25
Selenium
uglL
ND
10.0
5.0
04/15/19 02:25
Silver
ug1L
ND
5.0
2.5
04/1,9119 02:25
Thallium
uglL
ND
10.0
5.0
04/15/19 02:25
Zinc
ug1L
ND
10.0
2.5
04/15/19 02:25
LABORATORY CONTROL SAMPLE:
Parameter
2547777
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug1L
500
504
101
85-115
Arsenic
ug1L
500
458
92
85.115
Beryllium
ug1L
500
498
100
85-115
Cadmium
ug1L
500
489
98
85-115
Chromium
uglL
500
485
97
85-115
Copper
uglL
500
494
99
85-115
Lead
ug1L
500
489
98
85-115
Nickel
uglL
500
486
97
85-115
Selenium
ug1L
500
498
100
85-115
Silver
ug1L
250
237
95
85-115
Thallium
ug1L
500
472
94
85-115
Zinc
ug1L
500
510
102
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2547778
2547779
MS
MSD
92424014001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
uglL
ND
500
500
525
519
104
103
70-130
1
20
Arsenic
uglL
ND
500
500
485
478
97
95
70-130
1
20
Beryllium
uglL
ND
500
500
508
498
102
99
70-130
2
20
Cadmium
uglL
ND
500
500
510
500
102
100
70-130
2
20
Chromium
uglL
14.2
500
500
506
496
98
96
70-130
2
20
Results presented on this page are in the units indicated by the -Units" column except whore an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 04122/2019 04:24 PM without the written consent of Pace Analytical Services, I.I.C.
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QUALITY CONTROL DATA
Pace Analyticai Services, LLC
980D Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Project: Newton Instruments
Pace Project No.: 924242,34
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2547778
2547779
MS
MSD
92424014001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Copper
ug/L
9.0
500
500
507
502
100
99
70-130
1
20
Lead
ug/L
ND
500
500
494
484
99
97
70-130
2
20
Nickel
ug/L
37.0
500
500
530
520
99
97
70-130
2
20
Selenium
ug/L
ND
500
500
539
533
107
106
70-130
1
20
Silver
ug/L
ND
250
250
236
234
94
93
70-130
1
20
Thallium
ug/L
ND
500
500
469
462
94
92
70-130
2
20
Zinc
ug/L
69.7
500
500
609
594
108
105
70-130
2
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2547780
2547781
MS
MSD
92424309006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
16.0
500
500
539
540
105
105
70-130
0
20
Arsenic
ug/L
ND
500
500
473
480
95
96
70-130
1
20
Beryllium
ug/L
ND
500
500
498
502
100
100
70-130
1
20
Cadmium
ug/L
ND
500
500
510
511
102
102
70.130
0
20
Chromium
ug1L
ND
500
500
484
490
97
98
70-130
1
20
Copper
ug/L
10.5
500
500
508
514
100
101
70-130
1
20
Lead
ug/L
9.6
500
500
510
511
100
100
70-130
0
20
Nickel
ugIL
ND
500
500
493
496
98
99
70-130
0
20
Selenium
ug/L
ND
500
500
547
546
109
109
70.130
0
20
Silver
ug/L
ND
250
250
236
240
94
96
70-130
2
20
Thallium
ug/L
ND
500
500
484
487
97
97
70-130
1
20
Zinc
ug/L
152
500
5o0
674
669
104
103
70-130
1
20
Results presented on this page are in the units indicated by the "Units" column except where an altamata unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04122/2019 04:24 PM without the written consent of Pace Analyticai Services, LLC.
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QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
QC Batch: 468196 Analysis Method: EPA624.1
QC Batch Method: EPA624.1 Analysis Description: 624 MSV
Associated Lab Samples: 92424294001
METHOD BLANK: 2543439
Associated Lab Samples: 92424294001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1-Trichloroethane
uglL
ND
2.0
0.18
04/09/1915:25
1,1,2,2-Tetrachloroethane
uglL
ND
2.0
0.22
04/09119 15:25
1,1,2-Trichloroethane
uglL
ND
2.0
0.24
04109/1915:25
1,1-Dichloroethane
uglL
ND
2.0
0.27
0410911915:25
1,1-Dichloroethene
ug1L
ND
2.0•
0.24
04109/1915:25
1,2-Dichloroethane
uglL
ND
2.0
0.34
04109/1915:25
1,2-Dichloropropane
ug1L
ND
2.0
0.19
04/09/1915:25
2-Chloroethylvinyl ether
uglL
ND
10.0
6.9
04109/19 15:25
Acrolein
uglL
ND
5.0
2.7
04/09/1915:25
Acrylonitrile
uglL
ND
50.0
0.90
04/09/1915:25
Benzene
uglL
ND
1.0
0.15
04/09119 15:25
Bromodichloromethane
ug1L
ND
2.0
0.26
04/09/1915:25
Bromoform
ug1L
ND
2.0
0.62
04/09/1915:25
Bromomelhane
uglL
ND
2.0
0.62
04109/1915:25
Carbon tetrachloride
uglL
NO
2.0
0.22
04/09/19 15:25
Chlorobenzene
ug1L
ND
2.0
0.23
04tO9/1915:25
Chloroethane
uglL
ND
2.0
0.49
04109/1915:25
Chloroform
ug1L
ND
5.0
2.3
0410911915:25
Chloromethane
ug1L
ND
2.0
0.39
04109/1915:25
cis-1,3-Dichloropropene
ug1L
ND
2.0
0.30
04/09/1915:25
Dibromochloromethane
ug1L
ND
2.0
0.41
04109/1915:25
Ethylbenzene
ug1L
ND
1.0
0.26
04109/1915:25
Methylene Chloride
ug1L
ND
5.0
3.7
04/09/19 15:25
Tetrachloroethene
ug1L
ND
2.0
0.16
0410911915:25
Toluene
ug1L
ND
1.0
0.24
04109/1915:25
trans-1,2-Dichtoroethene
ug1L
ND
2.0
0.25
04109/1915:25
trans-1,3-Dichloropropene
ug1L
ND
2.0
0.31
0410911915:25
Trichloroethene
ug1L
ND
2.0
0.22
04/09/1915:25
Vinyl chloride
ug1L
ND
2.0
0.24
04/09/19 15:25
1,2-Dichloroethane-d4 (S)
%
94
70-130
04/09119 15:25
4-Bromoftuorobenzene (S)
%
102
70-130
04109119 15:25
Toluene-d8 (S)
%
118
70-130
04/09119 15:25
Pace Analytical Services, LLC
9800 Kincey Ave- Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE:
2543440
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
uglL
20
21.9
110
70-130
1,1,2,2-Tetrachloroethane
ug1L
20
18.7
93
60-140
1,12-Trichloroethane
uglL
20
20.8
104
70-130
1,1-Dichloroethane
uglL
20
21.9
110
70-130
Results presented an this page are In the units Indicated by the "Units- column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
LABORATORY CONTROL SAMPLE: 2543440
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1-Dichloroothene
uglL
20
23.2
116
50-150
1,2-Dichloroethane
uglL
20
20.7
104
49-155
1,2-Dichloropropane
ug1L
20
22.2
111
35-165
2-Chloroethylvinyl ether
uglL
40
37.6
94
1-225
Acrolein
ug1L
100
110
110
60-140
Acrylonitrile
ug1L
100
106
106
60-140
Benzene
ug1L
20
21.7
109
65-135
Bromodichloromethane
uglL
20
22.4
112
65-135
Bromoform
uglL
20
15.9
80
70-130
Bromomethane
uglL
20
20.2
101
15-185
Carbon tetrachloride
uglL
20
21.7
109
70-130
Chlorobenzene
ug1L
20
19.2
96
65-135
Chloroethane
uglL
20
21.6
108
40-160
Chloroform
uglL
20
20.9
104
70-135
Chioromethane
ug1L
20
18.2
91
1-205
cis-1,3-Dichloropropene
ug1L
20
20.9
104
25-175
Dibromochloromethane
uglL
20
18.1
91
70-135
Ethylbenzene
uglL
20
19.4
97
60-140
Methylene Chloride
uglL
20
23.1
115
60-140
Tetrachloroethene
uglL
20
17.4
87
70-130
Toluene
uglL
20
19.6
98
70-130
trans- 1, 2-D ichloroethene
uglL
20
21.5
108
70-130
trans-1,3-Dichloropropene
uglL
20
20.4
102
50-150
Trichloroethene
uglL
20
19.9
100
65-135
Vinyl chloride
uglL
20
21.5
108
5-195
1,2-Dichloroethane-d4 (S)
%
104
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2543441
2543442
MS
MSD
92424535001
Spike
Spike
MS
MSD
M$ MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
1. 1, 1 -Trichloroethane
uglL
ND
20
20
20.1
21.1
101
106
52-162
5
36
1,12,2-Tetrachloroethane
uglL
ND
20
20
19.6
19.3
98
97
46-157
1
61
1,1,2-Trichloroethane
uglL
ND
20
20
19.6
20A
98
102
52-150
4
45
1,1-Dichloroethane
uglL
ND
20
20
22.0
22.0
110
110
59-155
0
40
1,1-Dichloroethene
uglL
ND
20
20
21.5
22.6
107
113
1-234
5
32
1,2-Dichloroethane
uglL
ND
20
20
20.6
22.0
103
110
49-155
6
49
1,2-Dichloropropane
uglL
ND
20
20
19.8
20.4
99
102
1-210
3
55
2-Chloroethylvinyl ether
uglL
NO
40
40
NO
NO
0
0
1-305
71 M1
Acrolein
uglL
NO
100
100
90.9
92.5
91
92
40-160
2
60
Acrylonitrile
uglL
NO
100
100
104
109
104
109
40-160
5
60
Benzene
uglL
ND
20
20
20.5
21.6
102
108
37-151
6
61
Bromodichloromethane
uglL
ND
20
20
20.7
21.8
103
109
35-155
5
56
Results presented on this page are in the units indicated by the -units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical services, LLC.
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntefsville, NC 28078
[phone]
Project: Newton Instruments
Pace Project No.: 92424294
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2543441
2543442
MS
MSD
92424535001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc,
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Bromoform
ug1L
NO
20
20
16.4
17.4
82
87
45-169
6
42
Bromomethane
ug1L
NO
20
20
12.2
14.1
61
70
1-242
15
61
Carbon tetrachloride
ug1L
NO
20
20
21.2
21.9
106
110
70-140
4
41
Chlorobenzene
ug1L
NO
20
20
19.5
20.3
98
102
37-160
4
53
Chloroethane
ug1L
NO
20
20
16.9
18.5
84
94
14-230
11
78
Chloroform
ug1L
ND
20
20
17.6
19.8
88
99
51-138
12
54
Chtoromethane
ug1L
NO
20
20
10.6
11.1
53
56
1-273
5
60
cis-1,3-Dichloropropene
ug/L
NO
20
20
15.8
16.5
79
83
1-227
5
58
Dibromochloromethane
ug1L
NO
20
20
15.9
16.8
79
84
53-149
6
50
Ethylbenzene
ug1L
ND
20
20
20.4
21.1
102
105
37-162
4
63
Methylene Chloride
ug1L
NO
20
20
21.6
22.9
108
114
1-221
6
28
Tetrachloroethene
ug1L
NO
20
20
18.5
18.9
93
95
64-148
2
39
Toluene
ug1L
NO
20
20
20.9
21.4
104
107
47-150
3
41
trans-1,2-Dichloroethene
ug/L
ND
20
20
217
23.0
10B
115
54-156
6
45
trans-1,3-Dichloropropene
ug1L
NO
20
20
15.9
16.8
80
84
17-183
6
86
Trichloroethene
ug1L
NO
20
20
17.0
17.7
85
89
70-157
5
48
Vinyl chloride
ug1L
NO
20
20
15.8
17.1
79
85
1-251
8
66
1,2-Dichloroethane-d4 (S)
%
106
106
70-130
4-Bromolluorobenzene (S)
%
105
105
70-130
Toluene-d8 (S)
%
104
106
70-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall nct be reproduced, except in full,
Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
QC Batch: 468174 Analysis Method: EPA 608.3
QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol
Associated Lab Samples: 92424294001
METHOD BLANK: 2543312
Associated Lab Samples: 92424294001
Parameter
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
alpha -Chlordane
beta-BHC
Chlordane (Technical)
delta-BHC
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
gamma -Chlordane
Heptachlor
Heptachlor epoxide
PCB- 1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Toxaphene
Decachlorobiphenyl (S)
Teirachloro-m-xylene (S)
Matrix: Water
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
uglL
ND
0.050
0.0069
0410911917:59
uglL
ND
0.050
0.0064
04/0911917:59
uglL
ND
0.050
0.018
0410911917:59
uglL
ND
0.050
0.022
04/09/1917:59
ug1L
ND
0.050
0.019
04/09/1917:59
uglL
NO
0,050
0,0090
04/09/1917:59
uglL
ND
0.050
0.014
04/09/1917:59
uglL
ND
0.50
0.20
04/09/1917:59
uglL
ND
0.050
0.020
04/0911917759
uglL
NO
0,050
0,0073
04/09/1917759
uglL
ND
0.050
0.0094
04/09/1917:59
uglL
NO
0.050
0.0065
04/0911917:59
uglL
NO
0.050
0.0091
04/0911917:59
uglL
NO
0.050
0.0089
04/0911917:59
uglL
NO
0.050
0.013
04/09/1917:59
uglL
NO
0.050
0.012
04/0911917:59
uglL
NO
0.050
0.017
04/0911917:59
uglL
NO
0.050
0.016
04/09/1917:59
uglL
NO
0.050
0.0097
04/09/1917:59
uglL
NO
0.50
0.50
04/09/1917:59
uglL
NO
0.50
0.50
04/09/1917:59
uglL
NO
0.50
0.50
04/09/1917:59
uglL
NO
0.50
0.50
04/09/1917:59
uglL
NO
0.50
0.50
04/09/1917:59
uglL
NO
0.50
0.50
04/09/1917:59
uglL
NO
0.50
0.50
04/09/1917:59
uglL
NO
0.50
0.20
04/09/1917:59
%
66
10-130
04/09/ 19 17:59
%
84
10-130
04/09/19 17:59
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunter5ville, NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2543313
units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4,4'-DDD
uglL
0.25
0,24
98
31-141
4,4'-DDE
uglL
0.25
0.22
87
30-145
4,4'-DDT
uglL
0.25
0.25
101
25-160
Aldrin
ugi
0.25
0.20
81
42-140
alpha-BHC
uglL
0,25
0.23
91
37-140
alpha -Chlordane
uglL
0.25
0.22
88
45-140
beta-BHC
uglL
0.25
0.25
101
17-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC.
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Project: Newton instruments
Pace Project No.: 92424294
LABORATORY CONTROL SAMPLE: 2543313
Parameter Units
delta-BHC
uglL
Dieldrin
ug1L
Endosulfan I
ug/L
Endosulfan II
ug/L
Endosulfan sulfate
ug1L
Endrin
ug/L
Endrin aldehyde
ug/L
gamma-BHC (Lindane)
ug/L
gamma -Chlordane
ug/L
Heptachlor
ug/L
Heptachlor epoxide
ug/L
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
QUALITY CONTROL DATA
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
0.25
0.24
95
19-140
0.25
0.24
96
36-146
0.25
0.24
98
45-153
0.25
0.25
102
1-202
0.25
0.25
98
26-144
0.25
0.25
99
30-147
0.25
0.26
104
50-150
0.25
0.23
93
32.140
0.25
0.26
103
45-140
0.25
0.24
96
34-140
0,25
0.23
94
37-142
81
10-130
104
10-130
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented an this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
QC Batch: 468296 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92424294001
METHOD BLANK: 2543874
Matrix:
Water
Associated Lab Samples: 92424294001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug1L
ND
5.0
0.98
04110/1910:57
1,2-Dichlorobenzene
ug1L
ND
5.0
0.88
0411011910:57
1,2-Diphenylhydrazine
ug1L
ND
5.0
0.90
04110/1910:57
1,3-Dichlorobenzene
ug/L
ND
5.0
0.81
04/10/19 10:57
1,4-Dichlorobenzene
ug1L
ND
5,0
0.95
0411011910:57
2,4,6-Trichlorophenol
uglL
ND
10.0
1.3
04110/1910:57
2,4-Dichlorophenol
ug1L
ND
5.0
1.7
04110/1910:57
2,4-Di methyl phenol
ug1L
ND
10.0
1.2
0411011910:57
2,4-Dinitrophenol
ug/L
ND
50.0
9.0
04110/1910:57
2,4-Dinitrotoluene
ug/L
ND
5.0
0.90
0411011910:57
2,6-Dinitrotoluene
ug/L
ND
5.0
0.98
04110/1910:57
2-Chloronaphthalene
uglL
ND
5.0
0.98
04/10/1910:57
2-Chlorophenol
ug1L
ND
5.0
1.3
04110/1910:57
2-Nitrophenot
ug1L
ND
5.0
0.91
04/1011910:57
3,3'-Dichlorobenzidine
ug1L
ND
25.0
2.1
04/1011910:57
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
2.6
0411011910:57
4-Bromophenylphenyl ether
ug1L
ND
5.0
0.82
04/10/19 10:57
4-Chloro-3-methylphenol
ug1L
ND
5.0
3.7
04/1011910:57
4-Chlorophenylphenyl ether
ug1L
ND
5.0
0.87
04/10119 10:57
4-Nitrophenol
ug1L
ND
50.0
4.1
04/10/1910:57
Acenaphthene
ug/L
ND
5.0
0.25
04110/1910:57
Acenaphthylene
ug1L
ND
5.0
0.21
04110/1910:57
Anthracene
ug1L
ND
5.0
0.14
04/10/19 10:57
Benzidine
ug/L
ND
50.0
5.1
0411011910:57
Benzo(a)anthracene
ug/L
N❑
5.0
0.33
0411011910:57
Benzo(a)pyrene
ug/L
ND
5.0
0.30
04/10/19 10:57
Benzo(b)iluoranihene
ug1L
ND
5.0
0.28
04/10/1910:57
Benzo(g,h,i)perylene
ug/L
ND
5.0
0.38
0411011910:57
Benzo(k)Fluoranthene
ug/L
ND
5.0
0.43
04/1011910:57
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
0.92
04/10/1910:57
bis(2-Chtaroethyl) ether
ug1L
ND
5.0
1.0
04/10/19 10:57
bis(2-Ethylhexyl)phthalate
ug1L
ND
5.0
0.79
04/1011910:57
Butylbenzyl phtha late
ug1L
ND
5.0
0.79
0411011910:57
Chrysene
ug1L
ND
5.0
0.21
04110/1910:57
Di-n-butylphthalate
ug/L
ND
5.0
0.75
0411011910:57
Di-n-octylphthalate
ug1L
ND
5.0
0.66
0411011910:57
Dibenz(a,h)anthracene
ug/L
ND
5.0
0.55
04/10/19 10:57
Diethyl phthalate
ug/L
ND
5.0
0.58
04/1011910:57
Dimethylphthalate
ug/L
ND
5.0
0.76
0411011910:57
Fluoranthene
ug/L
ND
5.0
0.21
04/10/1910:57
Fluorene
ug/L
ND
5.0
0.21
04/10/19 10:57
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated try the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/22/2019 04:24 PM wkthout the written consent of Pace Analytical Services, L.L.C. Page 18 of 29

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QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
METHOD BLANK: 2543874
Associated Lab Samples: 92424294001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Hexachloro-1,3-butadiene
uglL
ND
5.0
0.94
04/1011910:57
Hexachlorobenzene
uglL
ND
5.0
0.72
04110/1910:57
Hexachlorocyclopentadiene
uglL
ND
10.0
0-88
04110/1910:57
Hexachloroethane
uglL
ND
5.0
1.1
04110/1910:57
Indeno(1,2,3-cd)pyrene
uglL
ND
5.0
0.29
04/10/1910:57
Isophorone
uglL
ND
10.0
0,89
04110/1910:57
N-Nitroso-di-n-propylamine
ug1L
ND
5.0
0.99
04110/1910:57
N-Nitrosodimethylamine
ug1L
ND
5.0
0.91
04110/1910:57
N-Nitrosodiphenylamine
uglL
ND
10.0
1-0
04/10/1910:57
Naphthalene
uglL
ND
5.0
0.34
04110/1910:57
Nitrobenzene
ug1L
ND
5.0
1A
04110/1910:57
Pentachlorophenol
ug1L
ND
10.0
4.6
04110/1910:57
Phenanthrene
uglL
ND
5.0
0.22
04/10/1910:57
Phenol
uglL
ND
5.0
1.9
04/1011910:57
Pyrene
uglL
ND
5.0
0.19
04110/1910:57
2,4,6-Tribromophenol (S)
%
66
10-137
04/10/19 10:57
2-Fluorobiphenyl (S)
%
52
15-120
04/10/19 10:57
2-Fluorophenol (S)
%
30
10-120
04/10/19 10:57
Nitrobenzene-d5 (S)
%
51
10-120
04/10/19 10:57
Phenol-d6 (S)
%
20
10-120
04110/19 10:57
Terphenyl-d14 (S)
%
75
11-131
04/10/19 10:57
LABORATORY CONTROL SAMPLE:
Parameter
2543875
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
uglL
50
30.9
62
44-142
1,2-Dichlorobenzene
uglL
50
30.6
61
32-129
1,2-Diphenylhydrazine
uglL
50
39.7
79
25-150
1,3-Dichlorobenzene
uglL
50
29.5
59
1-172
1,4-Dichlorobenzene
ug1L
50
32.6
65
20-124
2,4,6-Trichlorophenol
uglL
50
40.5
81
37-144
2,4-Dichlorophenol
ug1L
50
35.6
71
39-135
2,4-Dimethylphenol
ug1L
50
36.2
72
32-120
2,4-Dinitrophenol
ug1L
250
222
89
1-191
2,4-Dinitrotoluene
uglL
50
42.8
86
39-139
2,6-Dinitrotoluene
ug1L
50
42.8
86
50-158
2-Chloronaphthalene
uglL
50
35.6
71
60-120
2-Chlorophenol
uglL
50
33.1
66
23-134
2-Nilrophenol
uglL
50
34.4
69
29-181
3,3'-Dichlorobenzidine
uglL
100
75.1
75
1-262
4,6-Dinitro-2-methylphenol
uglL
100
91.7
92
1-181
4-Bromophenylphenyl ether
uglL
50
43.5
87
53-127
4-Chloro-3-methylphenol
uglL
100
73.9
74
22-147
4-Chlorophenylphenyl ether
uglL
50
40.9
82
25-158
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the -Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 29

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QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2543875
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4-Nitrophenol
ug/L
250
90.0
36
1-132
Acenaphthene
ug/L
50
42.8
86
47-145
Acenaphthylene
ug/L
50
44.8
90
33-145
Anthracene
ug/L
50
46.4
93
27-133
Benzidine
ug/L
100
14.3J
14
25-150 L2
Benzo(a)anthracene
ug/L
50
46.9
94
33-143
Benzo(a)pyrene
ug/L
50
46.8
94
17-163
Benzo(b)fluoranthene
ug/L
50
45.8
92
24-159
Benzo(g,h,i)perylene
ug/L
50
44.4
89
1-219
Benzo(k)fluoranthene
uglL
50
45.8
92
11-162
bis(2-Chlo roethoxy)m ethane
ug/L
50
34.3
69
33-184
bis(2-Chtoroethyl) ether
ug1L
50
32.4
65
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
42.6
85
8-158
Butylbenzylphthalate
ug1L
50
41.9
84
1-152
Chrysene
ug1L
50
46.7
93
17-168
Di-n-butylphthalate
ug1L
50
43.0
86
1-120
Di-n-octylphthalate
ug1L
50
43.3
87
4-146
Dibenz(a,h)anth racene
ug1L
50
44.5
89
1-227
Diethylphthalate
ug1L
50
41.6
83
1-120
D imethyl phtha late
ug1L
50
42.2
84
1-120
Fluoranthene
ug/L
50
47.6
95
26-137
Fluorene
ug1L
50
44.7
89
59-121
Hexachloro-1,3-butadiene
ug/L
50
29.9
60
24-120
Hexachlorobenzene
ug1L
50
43.1
86
1-152
Hexachlo rocyclo pentad iene
ug1L
50
28.6
57
25-150
Hexachloroethane
ug1L
50
27.8
56
40-120
Indeno(1,2,3-cd)pyrene
ug1L
50
45.3
91
1-171
tsophorone
ug1L
50
35.8
72
21-196
N-Nitroso-di-n-propylamine
ug1L
50
35.4
71
1-230
N-Nitrosodimethylamine
uglL
50
20.8
42
25-150
N-Nitrosodiphenylamine
ug1L
50
42.7
85
25-150
Naphthalene
uglL
50
36.9
74
21-133
Nitrobenzene
ug1L
50
33.3
67
35-180
Pentachlorophenol
ug1L
100
88.5
88
14-176
Phenanthrene
uglL
50
46.3
93
54-120
Phenol
uglL
50
14.3
29
5-120
Pyrene
uglL
50
46.8
94
52-120
2,4,6-Tribromophenol (S)
%
96
10-137
2-Fluorobiphenyl (S)
%
76
15-120
2-Fluorophenol (S)
%
42
10-120
Nitrobenzene-d5 (S)
%
71
10-120
Phenol-d6 (S)
%
28
10-120
Terphenyl-d14 (S)
%
88
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in futl,
Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC,
Page 20 of 29

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2a078
[phone]
Project: Newton Instruments
Pace Project No.: 92424294
MATRIX SPIKE SAMPLE: 2543876
2616916001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trcchlorobenzene
ug/t_
ND
49.5
19.0
38
44-142 M1
1,2-Dichlorobenzene
ug/L
ND
49.5
19.2
39
32-129
1,2-Diphenylhydrazine
ug/L
ND
49.5
21.9
44
25-150
1,3-Dichlorobenzene
ug/L
ND
49.5
18.6
38
1-172
1,4-Dichlorobenzene
ug/L
ND
49.5
19.9
38
20-124
2,4,6-Trichlorophenol
ug/L
ND
49.5
22.9
46
37-144
2,4-Dichlorophenol
ug/L
ND
49.5
22.1
45
39-135
2,4-Dimethylphenol
ug/L
ND
49.5
21,8
44
32-120
2,4-Dinitrophenol
ug/L
ND
248
111
45
1-191
2,4-Dinitrotoluene
ug/L
ND
49.5
24.8
50
39-139
2,6-Dinitrotoluene
ug/L
ND
49.5
24.4
49
50-158 M1
2-Chloronaphthalene
uglL
ND
49.5
21.0
42
60.120 M1
2-Chlorophenol
ug/L
ND
49.5
22.6
46
23-134
2-Nitrophenol
ug/L
ND
49.5
20.9
42
29-182
3,3'-Dichlorobenzidine
ug/L
ND
99
38.5
39
1-262
4,6-Dinitro-2-methylphenol
ug/L
ND
99
54.0
54
1-181
4-Bromophenylphenyl ether
ug/L
ND
49.5
24,5
50
53.127 M1
4-Chloro-3-methylphenol
uglL
ND
99
45.6
46
22-147
4-Chlorophenylphenyl ether
uglL
ND
49.5
22.7
46
25-158
4-Nitrophenol
uglL
ND
248
63.4
26
1-132
Acenaphthene
uglL
ND
49.5
23.0
47
47-145
Acenaphthylene
ug1L
ND
49.5
24.9
50
33-145
Anthracene
uglL
ND
49.5
27.6
56
27-133
Benzidine
ug1L
ND
99
18.2.1
18
25-150 MO
Benzo(a)anthracene
uglL
ND
49.5
28.7
58
33-143
Benzo(a)pyrene
uglL
ND
49.5
28.8
58
17-163
Benzo(b)iluoranthene
ug1L
ND
49.5
28.1
57
24-159
Benzo(g,h,i)perylene
uglL
ND
49.5
27.1
55
1-219
Benzo(k)ftuoranthene
ug/L
ND
49.5
28.5
58
11-162
bis(2-Chloroethoxy)methane
uglL
ND
49.5
20.2
41
33-184
bis(2-Chloroethyl) ether
ug1L
ND
49.5
20.7
42
12-158
bis(2- Ethyl hexyl)phthalate
ug1L
ND
49.5
25.8
52
8-158
Butylbenzylphthalate
uglL
ND
49.5
24.5
49
1-152
Chrysene
ug1L
ND
49.5
28.3
57
17-168
Di-n-butylphthalate
ug1L
ND
49.5
24.7
50
1-120
Di-n-octylphthalate
ug/L
ND
49.5
25.2
51
4-146
Dibenz(a,h)anthracene
ug/L
ND
49.5
26.6
54
1-227
Diethylphthalate
ug/L
ND
49,5
23.9
48
1-120
Dimethylphthalate
ug/L
ND
49.5
23.7
48
1-120
Fluoranthene
ug/L
ND
49.5
28.3
57
26-137
Fluorene
ug/L
ND
49.5
24.7
50
59-121 M1
Hexachloro-1,3-butadiene
ug/L
ND
49.5
19.1
39
24.120
Hexachlorobenzene
ug/L
ND
49.5
25.9
52
1-152
Hexachlorocyclopentad iene
ug/L
ND
49.5
15.8
32
25-150
Hexachloroethane
ug/L
ND
49.5
17.0
34
40-120 M1
Indeno(1,2,3-cd)pyrene
ug/L
ND
49.5
27.4
55
1-171
Isophorone
ug/L
ND
49.5
20.5
41
21-196
Results presented on this page
are in the units indicated
by the -Units" column except where an altemate unit is
presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 29

m
aceAnalytical
wwwpacelabs.com
QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services, 1-LC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
2543876
Units
2616916001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
N-Nitroso-di-n-propylamine
uglL
ND
49.5
20.5
41
1-230
N-Nitrosodimethylamine
uglL
NO
49.5
14.9
30
25-150
N-Nitrosodiphenylamine
uglL
ND
49.5
24.8
50
25-150
Naphthalene
uglL
ND
49.5
22.9
46
21-133
Nitrobenzene
uglL
ND
49.5
21.7
44
35-180
Pentachtorophenol
uglL
ND
99
50,0
51
14-176
Phenanthrene
uglL
ND
49.5
27.8
56
54-120
Phenol
uglL
ND
49.5
10.3
21
5-120
Pyrene
uglL
NO
49.5
28.7
58
52.120
2,4,6-Tribromophenol (S)
%
59
10-137
2-Fluorobiphenyl (S)
%
43
15-120
2-Fluorophenol (S)
%
30
10-120
Nitrobenzene-d5 (S)
%
44
10-120
Phenol-d6 (S)
%
21
10-120
Terphenyl-d14 (S)
%
58
11-131
SAMPLE DUPLICATE: 2544007
Parameter
Units
2616906001
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
uglL
NO
NO
30
1,2-Dichlorobenzene
ug1L
NO
NO
30
1,2-Diphenylhydrazine
ug/L
NO
NO
30
1,3-Dichlorobenzene
uglL
NO
NO
30
1,4-Dichlorobenzene
uglL
NO
NO
30
2,4,6-Trichlorophenol
uglL
NO
NO
30
2,4-Dichlorophenol
uglL
NO
NO
30
2,4-Dimethylphenot
ug1L
NO
NO
30
2,4-Dinitrophenol
uglL
NO
NO
30
2,4-Dinitrotoluene
uglL
NO
NO
30
2,6-Dinitrotoluene
uglL
NO
NO
30
2-Chloronaphthatene
ug1L
NO
NO
30
2-Chlorophenol
ug/L
NO
NO
30
2-Nitrophenol
uglL
NO
NO
30
3,3'-Dichlorobenzidine
ug1L
NO
ND
30
4,6-Dinitro-2-methylphenol
ug1L
NO
ND
30
4-Bromophenylphenyl ether
uglL
ND
ND
30
4-Chloro-3-methylphenol
uglL
NO
ND
30
4-Chlorophenylphenyl ether
uglL
NO
N❑
30
4-Nitrophenat
ug1L
NO
ND
30
Acenaphthene
ug1L
NO
NO
30
Acenaphthylene
ug1L
ND
ND
30
Anthracene
uglL
NO
NO
30
Benzidine
ug1L
NO
ND
30
Benzo(a)anthracene
ug1L
NO
NO
30
Benzo(a)pyrene
ug1L
NO
NO
30
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 29

aceAnalytical®
www.pacelabs.oam
Project: Newton Instruments
Pace Project No.: 92424294
SAMPLE DUPLICATE: 2544007
Parameter
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2- Ethyl hexyl) phtha late
Butylbenzyl phthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthatate
Dibenz(a, h )an thracene
Diethyl phthalate
Dimethytphthalate
Fluoranthene
Fluorene
Hex achloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenoi (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
2616906001 Dup
Result Result
ug/L
ND
ug/L
ND
ug/L
ND
uglL
ND
ug/L
ND
ug/L
ND
ug/L
ND
uglL
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
uglL
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
uglL
ND
ug/L
ND
ug/L
ND
ug/L
ND
ugll-
ND
ug/L
ND
ug/L
ND
%
71
52
%
31
%
54
%
21
%
65
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
78
50
27
48
18
44
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)675-9092
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/22/2019 04;24 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 29

acmnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments
Pace Project No.: 92424294
QC Batch: 468187
Analysis Method: SM 254OD-2011
QC Batch Method: SM 2540D-2011
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92424294001
METHOD BLANK: 2543383
Matrix: Water
Associated Lab Samples: 92424294001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 2.5
04/09119 11:33
LABORATORY CONTROL SAMPLE: 2543384
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 246 98
90-110
SAMPLE DUPLICATE: 2543385
92424332001 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Suspended Solids
mg1L
7230 6930 4
5
SAMPLE DUPLICATE: 2543386
92424256001 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Suspended Solids
mg1L
13100 12900 1
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0412212019 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 29

0
aceAnalytical
www pacelabs. tarn
QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersviile, NC 28078
[phone]
QC Batch: 457973
Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA 420.4 Rev 1.0 1993
Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92424294001
METHOD BLANK: 2542622
Matrix: Water
Associated Lab Samples: 92424294001
Blank
Reporting
Parameter Units
Result
Limit
MIDI- Analyzed
Qualifiers
Phenol mg/L
ND 0.020
0,0050 04/10119 09:04
LABORATORY CONTROL SAMPLE: 2542623
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Phenol mg/L
0.05
0.052
104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2542624
2542625
MS
MSD
92423830001
Spike
Spike MS
MSD MS MSD
% Rec
Max
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD RPD Qual
Phenol mglL 0.039
0.05
0.05 0.079
0.074 81 70
90-110
7 10 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2542626
2542627
MS
MSD
92423832001
Spike
Spike MS
MSD MS MSD
% Rec
Max
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD RPD Qual
Phenol mglL ND
0.05
0.05 0.055
0.056 106 108
90-110
2 10
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 29

aceAnalytical
www pacelahs wm
QUALITY CONTROL DATA
Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 468450 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total
Associated Lab Samples: 92424294001
METHOD BLANK: 2544454 Matrix: Water
Associated Lab Samples: 92424294001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide mg1L ND 0.0080 0.0060 04/11/19 09:29
LABORATORY CONTROL SAMPLE: 2544455
Parameter Units
Cyanide mg/L
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0A 0.098 98 80.120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2544456 2544457
MS MSD
92424456001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1 0.1 0.10 0.095 102 94 80-120 8 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2544458 2544459
MS MSD
92424337003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1 0.1 0.081 0.091 81 90 80-120 11 10 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 29

aceAnalytical
~p=1abs.=
QUALIFIERS
Project: Newton Instruments
Pace Project No.: 92424294
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Qua ntitation Limit.
Pace Analytical Services, LLC
9BOD Kinrey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below OC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether.
1a=U*L'�i612W_1:1101:T-A��7:Z7_\►It1A 31,9
This report shall not be reproduced, except in full,
Date: 04/22/2019 04:24 PM without the written consent of Pace Analytical Services, I.I.C. Page 27 of 29

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Project: Newton Instruments
Pace Project No.: 92424294
Pace Analytical Services. LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical
Method
Analytical
Batch
92424294001
Outfall -001
92424294001
Outfall -001
EPA 1664B
470147
92424294001
Outfall -001
EPA 608.3
468174
EPA 60B.3
468413
92424294001
Outfall -001
EPA 200.7 Rev 4.4 1994
469120
EPA 200.7
Rev 4.4 1994
469174
92424294001
Outfall -001
EPA 245.1 Rev 3.0 1994
470254
EPA 245.1
Rev 3.0 1994
470464
92424294001
Outfall -001
EPA 625.1
468296
EPA 625.1
468479
92424294001
Outfall -001
EPA 624,1
468196
92424294001
Outfall -001
SM 2540D-2011
468187
92424294001
Outfall -001
EPA 420.4 Rev 1.0 1993
467973
EPA 420.4
Rev 1.0 1993
468129
92424294001
Outfall -001
SM 4500-CN-E-2011
468450
SM 4500-CN-E-2011
468543
Date: 04/22/2019 04:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall net be reproduced, except in full,
without the written consent or Pace Analytical Services LLC,
Page 28 of 29

CHAIN -OF -CUSTODY Analytical Request Document
aceAnalytical
Chain -of -Custody is a LEGAL pUCUMENT • Complete all rekevert fields
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Company:
Piedmont Geologic
Billing Information.,
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Address: 6W3-145 Chapel Hill Rd, Raleigh, NC 27607
Report To: Jonathan Mur )'ire
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Email To:
jmurphrey@piedmontgeoic�gic.com
" PruervailveTypes:ll) nitric acid, (2) sulfuric acid, (3) hydrochWic acid, 141 sodium hydroxide, (5) zinc acetate,
16) methanol, (7) sodium Nsulfate, (9) sodium thiasulfate, 191 hexane, {A) ascorbic acid. {9) ammonium svliate,
tt) ammonium hydroxide, In) T5P, 1U) unpreserved, (0) other
Copy To:
Site Collection Info/Address:
Analyses
lab Profile/Une:.
Customer Project Name/Number:Stott@:
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collector Signature Prescnt . N-NA ,
90CClesYntact N'NA '
Correct.Bottivi .N NA, -
'Sufficient Volun. :
Samples Received an Ice Y N y.
.. VCA -, trandapace ACsepcable Y N A
USaA Regulated Soils Y NdD
Semplas in Holding Time t4�s
Residual Chlorine present Y N A
Cl Strips:
Sample PH. Acceptable Y N NA
prl Strips: -
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Sulfide Pres enc Y. N
Lead ACCtate SLzipa: 4�
LAB USE ONLY! -
-,Lab Sample $,'/ r•-•^�••-^ts:
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Phone• [919]$54-970G
Email: jmsrrorrey*'aidtrnmugeologc.ram
Site/Facility ID 9:
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I INobd:
Rush:
[ } Same Day ( ) Next Day
[) 2 Ddy 113 Day I j 4 Day ( 1 5 Day
{Expedite Charges Apply)
field Filtered (if applicable]:
[ ]Yes I j No
Analysis;
• Matrix Codes (insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL}, Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay {g}, Vapor (V), Other (QT)
Customer Sample ID
Matrix'
Comp/
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Composite End
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Date
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Outtall-001
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Customer Remarks /Special Conditions/ Possible Hazards:
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Type of lee Used: '.we[ ' .. Blue:... f]ry,
SHORT HOLDS PRESENT (02 hours): .Y' -N N/A
Lab Sample Temperalure info:
Temp Blank Re ivOU- NA
Therm I T S
Cooler 1 Temp Upgrr Receipt: oC
Coder 1 Therm Corr. Factor: oC '
Cooler 1 Corrected Temp: I 3,50C
Comments:6ei
Packing Material Used
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Samples received via .,'
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R i uishe Company: (Signature)
Date/Time:
Received by/Company: (Sign7a'
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Date/Time:
Non Cdnformance(s):
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