WQ0036706_Residual Annual Report 2014_20150302

TOWN OF AHOSKIE
2014 ANNUAL LAND APPLICATION OF
RESIDUAL BIO-SOLIDS REPORT
CLASS B PROGRAM
WQ0036706
Submitted by:
Soil Plus
208 Williams Street
Greenville, North Carolina 27858
February 17, 2014
S -V? 1", U S
RECEVEDIDENDWR
MAR — 2 zo15
&Tauafiw
perming Section

s * �. �.j���� rUS
February 17, 2015
NCDENR-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2014 LAND APPLICATION ANNUAL REPORT
Town of Ahoskie "Class B" Program
NC Permit No.: WQ0036706
Soil Plus Project No. 200802.A10
Information Processing Unit:;
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Town of Ahoskie on behalf of Granville
Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year.
This data includes (1) certification form, (2) residual sampling, (3) field loading calculations,
(44) pathogen and vector attraction reduction, -documentation, (5) standard soil fertility
nutrient analysis.
The Town of Ahoskie conducted application events on permitted fields in Hertford
The Town of Ahoskie conducted application events on permitted fields in Hertford
County during 2014. A total of 136.86 Dry Tons or 1,094,000 gallons of permitted residual
bio-solids were land applied to the Town of Ahoskie's permitted fields. A total of 93.51
Dry Tons or 747,500 gallons of permitted residual bio-solids were land applied to Granville
Farms' permitted fields in Edgecombe and Martin Counties.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact me or the Town of Ahoskie (252-332-3840) for further
assistance.
Respectfully,
C. Scott Carpenter, L.S.S.
North Carolina Nutrient Management Planner
Stewart White, Town of Ahoskie
Jason Smith, Granville Farms
208 Williams St.
Greenville, NC 27858
t [phone]
f [phone]
7
- www.soilplus.net

Town of Ahoskie
2014 Annual Land
Application of
Residual Bio-Soilds
Report
WQ0036706
Ahoskie, NC
aAVERY' READY INDEX` 600083

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0036706 Town of Ahoskie Jason Smith Hertford [phone]
Year: 2014
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 4
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 136.86
Total number of acres utilizes for land application during the year: 28.75
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality W ❑
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (f required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilit
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilitie
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviatibn, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as speed in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations."
Permittee Name d Title a or print):
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Friday, February 13, 2015
Signature of Permittee
02-13-2-2015 La
Signature of Land Applier Date
(if different from Permittee)

Source Summary Report
Ahoskie \AVrP 1,094,000 136.86
Total 1,094,000 136.86
11
r Friday, February 13, 2015 Page 1 of 1

Site# TA
YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop I PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
1 10.24
422,500
52.85
127.82
45.27
2 4.5
152,000
19.02
93.23
48.48
3 4.69
296,000
37.03
218.26
46.51
4 9.32
223,500
27.96
55.59
45.01
Total
1,094,000
136.86
Common
151
84.7%
Fescue Hay
50
90.5%
Bermudagrass Hay
Common
172
54.2%
Fescue Hay
50
97.0%
Bermudagrass Hay
Common
230
94.9%
Fescue Hay
50
93.0%
Bermudagrass Hay
Fescue Hay
151
36.8%
Common
50
90.0%
Bermudagrass Hay
Friday, February 13, 2015 Page 1 of 1

N
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0036706 Facility Name Town of Ahoskic Source Pemrit No. NCO089561 Source Name Ahoskie W WTP
Laboratory 1 A&L Eastern
Labs, Inc
Laboratory 2
Sample or CompositeDate
Parameter (mg/Kg) Class A Clan B
Aluminum
N/A
N/A
30,400
Ammonia Nitrogen
N/A
N/A
6,670
Arsenic
41
75
4
Cadmium
39
85
2
Calcium
N/A
N/A
16,900
Copper
1,500
4,300
442
Lead
300
840
37
4,500
Magnesium
N/A
N/A
Mercury
17
57
0.8
Molybden
N/A
75
10
Nickel
Nitrate -Nitrite Nitrogen
420
N/A
420
N/A
24
43
Percent Solids
N/A
N/A
3.00
PH (no units)
N/A
N/A
7.16
Phosphorus
N/A
N/A
25,100
Potassium
N/A
N/A
4,960
PAN (Inj./Ina)
N/A
N/A
20,102
PAN (Surface)
N/A
N/A
16,767
Selenium
Sodium
100
100
5
N/A
N/A
5,690
SAR
N/A
N/A
1.73
Totat Nitrogen
N/A
N/A
51,300
Zinc
2,800
7,500
1050
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing azolations."
/ (0 / 15-
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

AGMAN FIELD LOADING ESTIMATES
Facility Ahoskie WWI?
Sampling Date
% Solids 3
Mineralization Rate 0.30
Gallons per DT 7,993.61
PH 7.16
Sodium Absorpotion 1.73 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 51,300 lbs./1,000 gal 12.84
Ammonia Nitrogen (rng/Kg) 6,670.00 lbs./1,000 gal 1.67
Nitrate -Nitrite (mg/Kg) 43.30 lbs./1,000 gal 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 16,767 lbs./1,000 gal 4.20
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 20,102 lbs./1,000 gal 5.03
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
41300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
Potassium lbs./1,000 gal
1.24
Phosphorus lbs./1,000 gal
6.28
Calcium lbs./1,000 gal
4.23
Calcium lbs./1,000 gal
1.13
Manganese lbs./1,000 gal
0.08
Sulfur lbs./1,000 gal
2.01
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
4.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
442.00
Copper lbs./1,000 gal
0.11
Lead (mg/Kg)
37.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.80
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
24.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
1050.00
Zinc lbs./1,000 gal
0.26
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
51,300
16,767
33.53
34,533
51,300
20,102 40.20
31,198
34,533
5,180
10.36
29,353
31,198
4,680 9.36
26,518
29,353
2,201
4.40
27,151
26,518
1,989 3.98
24,529
27,151
1,018
2.04
261-133
24,529
920 1.84
23,609
26,133
490
0.98
25,643
23,609
443 0.89
23,167
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x N143)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
l
1ota1 z5,657 51.31
Total 28,133 56.27

Page: 1 of 2
Report Number: 14-087-0206
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
Lab Number: 98641
Sample Id : TA032514
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (B04) 743-9401 Fax [phone]
www.aleastem.com
Project: 201201.A10-AHOSKIE WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/25/2014 12:30:00
Date Received: 03/28/2014 00:00
Date Reported: 04/03/2014
Total Solids *
3.00
30000
100.0
JM
03/28/2014 13:59
SM-254OG
Moisture *
97.00
100.0
JM
03/28/2014 13:59
SM-2540G
Total Kjeldahl Nitrogen
5.13
51300
10.0
JM
03/31/2014 09:00
SM-4500-NH3C-TKN
Total Phosphorus
2.51
25100
100
KM
03/31/2014 13:30
SW 6010C
Total Potassium
0.50
4960
100
KM
03/31/2014 13:30
SW 6010C
Total Sulfur
0.80
8030
100
KM
03/31/2014 13:30
SW 6010C
Total Calcium
1.69
16900
100
KM
03/31/2014 13:30
SW 6010C
Total Magnesium
0.45
4500
100
KM
03/31/2014 13:30
SW 6010C
Total Sodium
0.57
5690
100
KM
03/31/2014 13:30
SW 6010C
Total Iron
15000
100
KM
03/31/2014 13:30
SW 6010C
Total Aluminum
30400
100
KM
03/31/2014 13:30
SW 6010C
Total Manganese
313
5
KM
03/31/2014 13:30
SW 6010C
Total Copper
442
5
KM
03/31/2014 13:30
SW 6010C
Total Zinc
1050
5
KM
03/31/2014 13:30
SW 6010C
Ammonia Nitrogen
0.67
6670
10.0
JM
03/31/2014 09:00
SM-4500-NI3C
Organic N
4.46
44630
10.0
03/31/2014 09:00
CALCULATION
Nitrate+Nitrite-N
43.3
2.00
JM
03/31/2014 09:00
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
03/31/2014 13:30
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-087-0206
Account Number: 04596
Submitted By: SCOTT CARPENTER
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD, NC 27565
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271.WS
wwrw.aleastem.com
Project: 201201.A10-AHOSKIE WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/25/2014 12:30:00
Lab Number: 98641 Date Received: 03/28/2014 00:00
Sample Id : TA032514 Date Reported: 04/03/2014
Total Chromium
52
5
KM
03/31/2014 13:30
SW 6010C
Total Nickel
24
5
KM
03/31/2014 13:30
SW 6010C
Total Lead
37
5
KM
03/31/2014 13:30
SW 6010C
Total Arsenic
4.0
3.0
KM
03/31/2014 13:30
SW 6010C
Total Mercury
0.8
0.4
KM
03/31/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
03/31/2014 13:30
SW 6010C
pH (Standard Units) *
7.16
2.00
JM
03/31/2014 09:00
SW-9045D
Total Molybdenum
10
5
KM
03/31/2014 13:30
SW 6010C
Soluble Phosphorus
0.11 1100
100
JM
04/01/2014 10:39
SOLUBLE P IN MANURE
Comments:
WATER SOLUBLE P, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Microbaci
Microbac Laboratories, Inc. - Wilson Division
3809 Airport Drive NW
Wilson, NC 27896
Tel: [phone]
certificate of Analrrsis Report Date: 29-Apr-2014
SCOTT CARPENTER
SOIL PLUS
208 WILLIAMS ST
GREENVILLE NC 27858
USA
Work Order:
2014-03-31-003
Date Received:
28-Mar-2014
Quote:
23-20140328-14
Sample Description.
Biosolids
Collection
SIDN
Client Marks
Analysis
Method
Date/Time:
Result
AA46175
Town of
Flash Point,Liqulds
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
pH (Corrosivity)
Subcontracted
3/27/14
10:30
*See Attached
• Williamston TW .
032714
AA46175
Town of
Reactive Cyanide
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
Reactive Sulfide
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
032714
AA46175
Town of
TCLP,Full (Metals,
Subcontracted
3/27/14
10:30
*See Attached
Williamston TW
VOC SVOC Pest @
032714
Herb)
AA46176
Town of Ahoskie A
Flash Point,Liquids
Subcontracted
3127/14
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
pH (Corrosivity)
Subcontracted
3/27114
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
Reactive Cyanide
Subcontracted
3/27/14
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
Reactive Sulfide
Subcontracted
3/27/14
13:30
*See Attached
032714
AA46176
Town of Ahoskie A
TCLP,Full (Metals,
Subcontracted
3/27/14
13:30
*See Attached
032714
VOC SVOC Pest @
Herb)
Reviewed and Approved b : `!/.! P� / 9 air
PP Y Date: ,r, y
Kim Hesse
i
For any feedback concerning our services, please contact James Nokes, Senior Vice President, at [e-mail]
or Trevor Boyce, President, at [e-mail]
Chemical and Microbiological Analysis: Environmental — Agrochemical — Food — Pharmaceuticals
Page 1 of 1

Microbac Laboratories, Inc.
Knoxville Division
®®A 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
TH-Cities, TN 423.926.6385 1 Nashville, TN 615.242,1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES - FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. -Wilson Date Received: 4/1/2014
3809 Airport Drive Cust#., R9024
Wilson, NC 27896 Po#:
Workorder: 1406051 Project: Soil Sampling
Analyte Result Units Dil Qualifier ReportingLimit Analyst Analyzed Method
AA46176 Williamston Sampled: 03/27/2014 00:00
1406061-01 (Solid)
GCMS Volatiles
Analvzed Bv: Microbac Laboratories, Inc. - Chico og land
1, 1 -Dichloroethene
ND
mg/L
10
H
0.050
jin
04125/201413:34
1311/8280B
1,2-Dichloroethane
ND
mg/L
10
H
0.050
jin
04125/201413:34
1311/8260B
2-Butanone
ND
mg/L
10
H
0.10
jin
04/25/201413:34
1311/8260B
Benzene
ND
mg/L
10
H
0.050
jin
04/25/201413:34
1311/8260B
Carbon tetrachloride
ND
mg/L
10
H
0.050
jin
04/25/201413:34
1311/8260B
Chlorobenzene
ND
mg1L
10
H
0.050
jin
04/25/201413:34
1311/92608
Chloroform
ND
mg/L
10
H
0.050
jin
04/25/201413:34
1311/8260B
Tetrachloroethene
ND
mg/L
10
H
0.050
jin
04125/201413:34
131118260E
Tdchloroethene
ND
mg/L
10
H
0.050
jln
04/25/201413:34
1311/8280B
Vinyl chloride
ND
mg/L
10
H
0.020
jin
04/25/2014 13:34
1311/8260B
1,4-Dichlorobenzene
ND
mg/L
10
H
0.10
jin
04/25/201413:34
1311/8260B
Surrogate: 1,2-Dichloroethane-d4
74.5-132
H
106 %
04/251201413:34
131118260B
Surrogate: 4-Bromotluombenzene
80-120
H
93.8 %
04/251201413:34
131118260B
Surrogate: Dibromofluoromethane
80-120
H
101 %
04/25/201413:34
131118260B
Surrogate: Toluene-d8
80-120
H
101 %
04/25/201413:34
131118260B
Wet Chemistry
f Analyzed BY: Microbac Laboratories, Inc. - Chicagoland
r Reactive Cyanide ND mg/Kg 1 H 2.0 AGRIE 04/16/201413:00 Chapter?/9014
Reactive Sulfide ND mg/Kg 1 H 2.0 EB 04115/201409:15 Chapter?/9034
AA46175 Williamston Sampled: 03/27/2014 00:00
1406061-01RE7 (Solid)
TCLP Metals by 600017000 Series Methods
Analyzed By: Microbac Knoxville Division
Silver ND mg/L 1 0.00100 JNB 04/16/2014 21:31 SW846 6010E
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406051-02 (Solid)
Wet Chemistry
The data and Information on this, and other accompanying documents, represent any the somple(s) analyzed and Is rendered upon condition MEMBER
that It Is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory.
USDA-EPA-NIOSH Testing Food Sanitegon Consulting Chemlcal and Microbiological Analyses and Research
Page 3 of 9
www.microbac.com [e-mail]

c�
Microbac Laboratories, Inc.
Knoxville Division
®� 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUT)CALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Data Received: 4/1/2014
3809 Airport Drive oust #: R9024
Wilson, NC 27896 Po#:
Workorder: 1406051 Project: Soil Sampling
Analyte Result Units Oil Qualifier Reporting Analyst Analyzed Method
Limit
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406061-02 (Solid)
Wet Chemistry
Analyzed By: Microbac Knoxville Division
pH (Corrosivity) 7.3 pH Units 1 H4 SLN 04/091201416:00 SW846 9045D
General Chemistry
Analyzed By: Microbac Knoxville Division
Flash Point 121 °F 1 01 65 SDF 04/161201417:27 SW846 1010
TCLP Extraction Fluid 1 1 Ha JNB 04/11/2014 11:57 SW846 1311
TCLP Metals by 6000/7000 Series Methods
Analyzed By: Microbac Knoxville Division
Arsenic
0.0431
mg1L
1
0.0150
JNB
04/11/2014 20:24
SW846 6010B
Barium
0.151
mg/L
1
0.00400
JNB
04/11/2014 20:24
SW846 6010B
Cadmium
ND
mg/L
1
0.00750
JNB
04/11/2014 20:24
SW846 6010E
Chromium
ND
mg/L
1
0.00760
JNB
04/11/2014 20:24
SW846 6010B
Lead
ND
mg/L
1
0.0200
JNB
04/11/2014 20:24
SW846 601DB
Mercury
ND
mg/L
1
0.000200
JNB
04/15/201416:38
SW846 7470A
Selenium
0.0419
mg/L
1
0.0200
JNB
04/11/2014 20:24
SW846 6010E
TCLP Semivolatiles by EPA Method 131118270C
Analyzed By: Microbac Knoxville Division
o-Cresol
ND
mg1L
1
0.0385
SLH
04/16/201417:58
SW846 8270C
Pyridine
ND
mg/L
1
0.0192
SLH
04116/201417:58
8W846 8270C
meta/para-Cresol
ND
mg/L
1
0.0385
SLH
04/16/201417:58
SW846 8270C
Hexachloroethane
ND
mg/L
1
0.0192
SLH
04/16/201417:58
SW846 8270C
Nitrobenzene
ND
mg/L
1
0.0192
SLH
04/16/201417:58
SW846 82706
Hexachlorobutadiene
ND
mg/L
1
0.0192
SLH
04/16/201417:58
SW846 8270C
2,4,6-Trichlorophenol.
ND
mg/L
1
0.0192
SLH
04/161201417:58
SW846 8270C
2,4,5-Trichlorophenol
ND
mg1L
1
0.0192
SLH
041161201417:58
SW846 8270C
2,4-Dinitrotoluene
ND
mg/L
1
0.0192
SLH
04/1e/201417:58
SW846 8270C
Hexachlorobenzene
ND
mg/L
1
0.0192
SLH
04/161201417:58
SW846 8270C
Pentachlorophenol
ND
mg/L
1
0.154
SLH
04/161201417:58
SW846 8270C
1,4-Dichlorobenzene
ND
mg/L
1
0.0192
SLH
04/16/201417:58
SW846 8270C
Surrogate: 2-Fluorob/phenyl
10-108
59.0 %
04/161201417:58
SW846 8270C
The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condlllon MEMBER
that It is not to be reproduced wholly or in pad for advertising or other purposes without approval from the laboratory.
USDA-EPA-NIOSH Tesgng Food Sanhellon Consulting Chemical and Mlcrobiotogical Analyses and Research ril:i.t�
www.microbac.com [e-mail]
Page 4 of 9

Microbac Laboratories, Inc.
Snoxville Division
®®a 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY • MICROBIOLOGY - FOOD SAFETY • CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD - PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. -Wilson Date Received: 4/1/2014
3809 Airport Drive oust #: R9024
Wilson, NC 27896 Po#:
Workorder: 1406061 Project: Soil Sampling
Analyte Result Units DII Qualifier Reporting Analyst Analyzed Method
Limit
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406061-02 (Solid)
TCLP Semivolatiles by EPA Method 131118270C
Surrogate.,2-Fluorophenol
10.89.8
31.9%
04116/201417:58
SW846 8270C
Surrogate: Nitrobenzene-d5
10-107
64.3 %
041161201417:58
SW846 8270C
Surrogate: Phenol-0
10-86.9
29.8 %
041161201417:58
SW846 8270C
Surrogate: Terphenyl-04
10-111
74.3 %
04/16/201417:58
SW8466270C
Surrogate: 2,4,6-Tribromophenol
10-126
31.1 %
04/16/2014 17:58
SW846 82700
TCLP HERBICIDES
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
2,4-D
NO
ug/L
1
U, H1•
20.0
ECL
04/171201420:00
SW8151A
2,4,5 TP (Silvex)
NO
ug/L
1
U, H1
2.00
ECL
04/17/2014 20:00
SW8151A
Surrogate: 2,4-Dich/orophenylacetic acid
20-144
56.9 %
04/17/2014 20:00
SW8151A
TCLP Pesticides
Analyzed By: Microbac Laboratories, Inc. - Ohio Valley
Endrin
ND
ug/L
1
U, H1
0.500
ECL
04/171201422:57
SWa081A
Lindane
ND
ug/L
1
U, H1
0.500
ECL
04/17/2014 22:57
SW8081A
Methoxychior
NO
ug/L
1
U, H1
0.500
ECL
04/17/2014 22:57
SW8081A
Toxaphene
NO
ug/L
1
U, H1
10.0
ECL
04/171201422:57
SW8081A
Chlordane
NO
ug/L
1
U, H1
10.0
ECL
04/17/2014 22:57
SWB081A
Heptachlor
NO
ug/L
1
U, H1
0.500
ECL
04/171201422:57
SW8081A
Heptachlor Epoxide
NO
ug/L
1
U, H1
0.500
ECL
04/17/2014 22:57
SWB081A
alpha Chlordane
NO
ug/L
1
U, H1
0.600
ECL
04/17/2014 22:57
SW8081A
gamma Chlordane
NO
ug/L
1
U, H1
0.500
ECL
04/17/2014 22:57
SWB081A
Surrogate: 2,4,5,6-Tetrach/oro-m-xylene
20-180
35.1 %
04117/201422:57
SW8081A
Surrogate: Decach/orobipheny/
25-140
28.5 %
04/17/2014 22:57
SW8081A
GCMS Volatiles
Analyzed By: Microbac Laboratories, Inc. - Chicacloland
_
1,1-Dichloroethene
NO
mg/L
10
H
0.050
jin
04/24/201413:13
1311/8260B
1,2-Dichloroethane
NO
mg/L
10
H
0.050
jin
04124/201413:13
1311/8260B
2-Butanone
0.22
mg/L
10
H
0.10
jin
04/24/201413:13
1311/8260B
Benzene
ND
mg/L
10
H
0.050
jin
04/24/201413:13
1311/8260B
Carbon tetrachloride
ND
mg/L
10
H
0.050
jin
04/24/201413:13
1311/8260B
The data and Information on this, and other accompanying documents, represent only the sample(s) analyzed and Is rendered upon condition MEMBER
that it Is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory.
USDA•EPA•NIOSH Testing ,Food Sanitation Consulting Chemical and Microbiological Analyses and Research
Page 5 of 9
www.microbac.com [e-mail]

n
Microbac Laboratories, Inc.
]Knoxville Division
®® 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY CONSUMER PRODUCTS -WATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac laboratories, Inc. - Wilson Date Received: 4/112014
3809 Airport Drive Cust #: R9024
Wilson, NC 27896 Po#:
Workorder:- 1406061 Project: Soil Sampling
Analyte Result Units Dil Qualifier Reporting Analyst Analyzed Method
Limit
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406061-02 (Solid)
GCMS Volatiles
Chlorobenzene
ND
mg/L
10
H
0.050
jin
04/24/201413:13
1311/8260B
Chloroform
ND
mg/L
10
H
0.050
jin
04/24/201413:13
1311/8260B
Tetrachloroethene
ND
mg/L
10
H
0.050
jin
0412412014 13:13
1311/6260B
Trichloroethene
ND
mg/L
10
H
0.050
jin
04/24/201413:13
1311/8260B
Vinyl chloride
ND
mg/L
10
H
0.020
jln
04/24/201413:13
1311/6260B
1,4-Dichlorobenzene
ND
mg/L
10
H
0.10
jin
04/24/201413:13
1311/8260B
Surrogate: 1,2-Dich/oroethane-d4
74.5-132
H
104 %
o4/24/201413:13
131118260B
Surrogate: 4-Bromofluorobenzene
80-120
H
95.2 %
o4/24/201413:13
131118260B
Surrogate: Dibromofluoromethane
80-120
H
102 %
o4/24/201413:13
131118260E
Surrogate: Toluene-d8
80-120'
H
100 %
04/24/201413:13
131118260E
Wet Chemistry
Analyzed BY: Microbac Laboratories, Inc. - Chicagoland
Reactive Cyanide ND mglKg 1 H 2.0 AGRIE 04/161201413:06 Chapter7/9014
Reactive Sulfide ND mg/Kg 1 H 2.0 EB 04/15/201409:15 Chapter7/9034
AA46176 Ahoskie Sampled: 03/27/2014 00:00
1406051-02RE1 (Solid)
TCLP Metals by 6000/7000 Series Methods
Analyzed By: Microbac Knoxville Division
Silver ND mg/L 1 0.00100 JNB 04/16/2014 21:37 SW846 6010B
j
The data and Information on this, and other accompanying documents, represent any the sample(s) analyzed and Is rendered upon candltlon MEMBER
that It 4s riot to be reproduced wholly or In pan for advertising or other purposes without approval from the laboratory.
USDA•EPA•NICSH Testing Food Sanitation Consulting Chemical and MlcroblaloglcalAnalyses and Research
Page 6 of 9
www.microbac.com [e-mail]
�I
t'

Microbac Laboratories, Inc.
Knoxville Division
®©® 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTS •WATER • AIR • WASTES FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. -Wilson Date Received: 4/1/2014
3809 Airport Drive Cost #: R9024
Wilson, NC 27896 PO#:
Workorder: 1406051 Project: Soil Sampling
Certifications
Code
Description
Number
Expires
A21LA
A21LA ISO/IEC 17025 Env. DoD Testing
3045.02
09/30/2014
A2LA
A2lA ISO/IEC 17025 Biological Testing
3045.01
09/30/2014
A2LAB-KNX
ISO 17025 KNX food
3131.01
05131/2015
A2LAB-NSH
ISO 17025 NSH food
3131.02
06/30/2014
FL
State of Florida NELAC
E87966
06/30/2014
GA
Georgia Dept Natural Resources
980
04113/2014
ILDPH
Illinois DOPH Micro analysis of drinking water
1755266
12131/2016
ILEPA
Illinois EPA wastewater and solid waste analysis
200064
04/01/2015
INDEM
Indiana DEM support lab wastewater and solid waste
A305-9-292
12/31/2013
INDH
Indiana SDH Micro analysis of drinking water
M-45-8
12/31/2016
INSDH
Indiana SDH chemical analysis of drinking water
C-46-03
08/14/2016
KSDOH
Kansas Dept Health & Env. NELAP
E-10397
01/31/2016
KYEPP
Kentucky EPPC analysis Underground Storage Tanks
75
01/31/2015
NCEW
NC Environmental
678
12/31/2013
NYDOH
New York State Department of Health Wadsworth
49179
04/01/2016
NYDOH-1
New York State Department of Health Wadsworth
49386
04/01/2015
PADEP
Pennsylvania Department of Environmental Protect
68-04863
07/31/2014
PEDEP
Pennsylvania DEP Registration forAir analysis
68-04863
TN_DW
North Carolina DENR NPDES effluent, surface water
TNNC597
12/31/2014
TN_DW
State of Tennessee
TN02017
04/30/2014
USDA
US Department of Agriculture
11/30/2013
USDAS
USDA Permit To Receive Soil
P330-12-00174
06/20/2015
WADOE
Washington State Department of Ecology
C992
10/22/2014
WSDNR
Wisconsin DRN chemical analysis wastewater, solids
998036710
08/31/2014
The data and Information an this, and other accompanying documents, represent onty the sompla(s) analyzed and is rendered upon condition MEMBER
that it Is not labs reproduced wholly or In part for advertising or other purpases wilhout approval from the laboratory.
USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and MleroblologlcalAnetyses and Research
Page 7 of 9
www.microbac.com [e-mail]

Microbac Laboratories, Inc.
Knoxville Division
® 505 E. Broadway Avenue Maryville, TN 37804 865.977.1200 Fax:[phone]
Tri-Cities, TN 423.926.6385 1 Nashville, TN 615.242.1480
www.microbac.com
[e-mail]
CHEMISTRY MICROBIOLOGY FOOD SAFETY CONSUMER PRODUCTS •WATER • AIR - WASTES - FOOD • PHARMACEUTICALS • NUTRACEUTICALS
CERTIFICATE OF ANALYSIS
Kimberly Hesse
Microbac Laboratories, Inc. - Wilson
3809 Airport Drive
Wilson, NC 27896
Workorder: 1406051 Project: Soil Sampling
Notes and Definitions
Date Reported: 4/29/2014
Date Received: 4/1/2014
Cust #: R9024
PO#:
U Not detected at or above adjusted sample detection limit
R1 Duplicate RPD is outside of acceptance limits.
01 Flashpoint temperature went up with each of the four tests. Even with vigorous shaking it appears volitile portion lessened
each time.
M5 Post digestion spike is outside of acceptance limits.
M3 Matrix spike recovery is outside of acceptance limits. The post digestion spike recovery is acceptable. .
M2 Matrix spike recovery is outside of acceptance limits, biased low.
Ha Sample was analyzed past holding time.
H4 The test was performed outside of the EPA recommended holding time of 15 minutes.
H1 [Undefined]
H Analyte was prepared and/or analyzed outside of the analytical method holding time
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a dry weight basis
RPD Relative Percent Difference
The data and information on this. and other accompanying documents, represent only the sampiets) analyzed and Is rendered upon condition MEMBER
that It Is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory.
USDA-EPA•NIOSH Testing Food Sanitation Consulting Chemical and MlcroblologicalAnsysas and Research
A
Page 8 of 9
www.mir-robac.com [e-mail]

CERTIFICATE OF ANALYSIS
Kimberly Hesse Date Reported: 4/29/2014
Microbac Laboratories, Inc. - Wilson Date Received: 4/1/2014
3809 Airport Drive cust #: R9024
Wilson, NC 27896 Po#:
Workorder: 1406051 Project: Soil Sampling
Microbac Laboratories, Inc. - Knoxville
Maraea Branner, Project Manager
Thank you for your business. For any feedback, please contact Ashley Morris, at ashley,[e-mail]. You may also contact 7Yevor Boyce,
i President [e-mail].
t
As regulatory limits change frequently, Microbac advises the recipient ofthis report to confirm such limits with the appropriate Federal, state, or local
I authorities before acting in reliance on the regulatory limits provided.
The data and Information on this, and other accompanying documents, represent only the sample(s) analyzed and Is rendered upon condition MEMBER
that It Is not to be reproduced wholly or In pert for advertising or other purposes without approval from the laboratory.
USDA-EPA-NIOSH Testing Food sanitation Consulting Chemical and Microbiological Analyses and Research
Page 9 of 9
www.microbac.com [e-mail]

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0036706
Site# TA
County Hertford
Crop 1 Common Bermudagrass Hay
Facility Name Town of Ahoskie
Field Name 1
Soi6Series Rains
Crop 1 Pan 151
LandOwner Town of Ahoskie
Acres Permited 10.24
Soil Abbrevation: Ra
Crop 2 Fescue Hay
Operator
Crop 2 Pan 50
Volume
Acres Dry
Soil Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids Used DT/Ac. Tons
Source Condition Precip Method P Volatilization
Mineralization TKN Ammonia Nitrite PAN
PAN Crop
05/12/2014 Gallons 60,000 3.00
10.24 0.73 7.51
Ahoskie WWTP Dry 0 Surface 36.80
0.50 0.30 51,300 6,670.00 43.30 24.58
Crop 1
05/13/2014 Gallons 92,000 3.00
10.24 1.12 11.51
Ahoskie WWTP Dry 0 Surface 56.42
0.50 0.30 51,300 6,670.00 43.30 37.69
Crop 1
05/14/2014 Gallons 72,000 3.00
10.24 0.88 9.01
Ahoskie WWTP Dry 0 Surface 44.16
0.50 0.30 51,300 6,670.00 43.30 29.50
Crop 1
05/24/2014 Gallons 52,000 3.00
10.24 0.64 6.51
Ahoskie WWTP Dry 0 Surface 31.89
0.50 0.30 51,300 6,670.00 43.30 21.30
Crop 1
05/27/2014 Gallons 36,000 3.00
10.24 0.44 4.50
Ahoskie WWTP Dry 0 Surface 22.08
0.50 0.30 51,300 6,670.00 43.30 14.75
Crop 1
11/13/2014 Gallons 39,000 3.00
10.24 0.48 4.88
Ahoskie WW IP Moist 0 Surface 23.92
0.50 0.30 51,300 6,670.00 43.30
15.98 Crop 2
11/14/2014 Gallons 71,500 3.00
10.24 0.87 8.94
Ahoskie WWTP Moist 0 Surface 43.85
0.50 0.30 51,300 6,670.00 43.30
29.29 Crop 2
Total Volume Applied 422,500
Total Dry Tons 52.85
Sum Total P 259.11
Total 127.82
45.27 Total
Reported in Gallons Arsenic Cadmium
Copper Chromium
Lead Mercury Molybdenum Nickel Selenium
zinc Crop 1
Crop 2
PAN
PAN
Current Year 0.041 0.021
4.563 0.537
0.382 0.008 0.103 0.248 0.052
10.839 (lbs./Ac.)
Lime (T/Ac.) Date
(lbs./Ac.)
Prior Year 6.025 4.010
11.891 10.224
20.170 0.803 10.035 10.080 10.025
34.724
Cumulative Total 6.066 4.031
16.453 10.761
20.552 0.811 10.138 10.328 10.077
45.563
Permitted CPLR 36 34
1338
267 15 374 89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
2-13-2015
****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier
Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0036706 Site# TA County Hertford Crop 1 Common Bermudagrass Hay
Facility Name Town of Ahoskie Field Name 2 SoilSeries Lynchburg Crop 1 Pan 172
Landowner Town of Ahoskie Acres Permited 4.50 Soil Abbrevation: Ly Crop 2 Fescue Hay
Operator Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization TKN Ammonia Nitrite PAN
PAN Crop
05/15/2014 Gallons
100,000 3.00
4.50
2.78 12.51
Ahoskie WWTP
Dry 0
Surface
139.56
0.50
0.30 51,300
6,670.00 43.30 93.23
Crop 1
11/13/2014 Gallons
52,000 3.00
4.50
1.45 6.51
Ahoskie WWTP
Moist 0
Surface
72.57
0.50
0.30 51,300
6,670.00 43.30
48.48 Crop 2
Total Volume Applied
152,000
Total Dry Tons 19.02
Sum Total P
212.13
Total 93.23
48.48 Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.034 0.017
3.735
0.439
0.313
0.007
0.085
0.203
0.042
8.874
Lime (T/Ac.) Date
(ibs./Ac.)
(lbs./Ac.)
Prior Year
6.027 4.011
12.039
10.242
14.183
0.803
10.038
10.086
10.027
21.095
Cumulative Total
6.061 4.028
15.774
10.682
14.496
0.810
10.122
10.289
10.069
29.969
Permitted CPLR
36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
.�� **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested-0.3,raw sludge -0.4
2-13-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0036706 Site# TA County Hertford Crop 1 Common Bermudagrass Hay
Facility Name Town of Ahoskie Field Name 3 SoilSeries Goldsboro Crop 1 Pan 230
LandOwner Town of Ahoskie Acres Permited 4.69 Soil Abbrevation: GoA Crop 2 Fescue Hay
Operator Crop 2 Pan 50
Volume
I
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TEN
Ammonia Nitrite
PAN
PAN Crop
05/19/2014
Gallons
100,000
3.00
4.69
2.67
12.51
Ahoskie WWTP
Dry
0
Surface
133.90
0.50
0.30
51,300
6,670.00
43.30
89.45
Crop 1
05/21/2014
Gallons
84,000
3.00
4.69
2.24
10.51
Ahoskie WWTP
Dry
0
Surface
112.48
0.50
0.30
51,300
6,670.00
43.30
75.14
Crop 1
05/23/2014
Gallons
60,000
3.00
4.69
1.60
7.51
Ahoskie WWTP
Dry
0
Surface
80.34
0.50
0.30
51,300
6,670.00
43.30
53.67
Crop 1
11/12/2014
Gallons
52,000
3.00
4.69
1.39
6.51
Ahoskie WWTP
Moist
0
Surface
69.63
0.50
0.30
51,300
6,670.00
43.30
46.51 Crop 2
Total Volume Applied
296,000
Total Dry Tons 37.03
Sum Total P 396.35
Total 218.26
46.51 Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.063
0.032
6.980 0.821
0.584
0.013
0.158
0.379
0.079
16.580
(lbs./Ac.)
(lbs./Ac.)
Lime /Ac. Date
Prior Year
6.041
4.016
13.074 10.365
16.276
0.805
10.057
10.130
10.041
27.682
Cumulative Total
6.104
4.048
20.054 11.186
16.860
0.817
10.215
10.509
10.120
44.262
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
VJWX &4-4:L
- - -
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
****C.P.LR.: Cumulative Pollutant Loading Rate
Signature of Land Applies Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0036706 Site# TA County Hertford Crop 1 Fescue Hay
Facility Name Town of Ahoskie Field Name 4 SoilSeries Caroline Crop 1 Pan 151
LandOwner Town of Ahoskie Acres Permited 9.32 Soil Abbrevation: CaA Crop 2 Common Bermudagrass Hay
Operator Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
05/20/2014
Gallons
100,000
3.00
9.32
1.34
12.51
Ahoskie WWTP
Dry
0
Surface
67.38
0.50
0.30
51,300
6,670.00
43.30
45.01 Crop 2
10/29/2014
Gallons
19,500
3.00
9.32
0.26
2.44
Ahoskie WWTP
Dry
0
Surface
13.14
0.50
0.30
51,300
6,670.00
43.30
8.78
Crop 1
11/10/2014
Gallons
39,000
3.00
9.32
0.52
4.88
Ahoskie WWTP
Moist
0
Surface
26.28
0.50
0.30
51,300
6,670.00
43.30
17.55
Crop 1
11/11/2014
Gallons
52,000
3.00
9.32
0.70
6.51
Ahoskie WWTP
Moist
0
Surface
35.04
0.50
0.30
51,300
6,670.00
43.30
23.41
Crop 1
11/12/2014
Gallons
13,000
3.00
9.32
0.17
1.63
Ahoskie WWTP
Moist
0
Surface
8.76
0.50
0.30
51,300
6,670.00
43.30
5.85
Crop 1
Total Volume Applied
223,500
Total Dry Tons 27.96
Sum Total P 150.60
Total 55.59
45.01 Total
Reported in Gallons
genic Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop I
Crop 2
PAN
PAN
Current Year
0.024
0.012
2.652
0.312
0.222
0.005
0.060
0.144
0.030
6.300
(Ibs./Ac.)
(Ibs./Ac.)
Lime (T/Ac.) Date
Prior Year
6.031
4.012
12.321
10.276
20.208
0.804
10.043
10.098
10.031
23.799
Cumulative Total
6.055
4.024
14.973
10.588
20.430
0.808
10.103
10.242
10.061
30.098
Permitted CPLR
36
34
1338
267
15
374
89
2498
KI certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-13-2015 ***L. *C.P.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
I Facility Name: Town of Ahoskie WQ Permit Number: WQ0036706
WWTP Name: Ahoskie W IT NPEDS Number: NCO088561
Monitoring Period: 01/01/2014 to 12/31/2014
r
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed(" Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 22,949 27,400 29,410 0 1 Grab Samples
Weight)
Analytical Technique SM 9221 E
VectorAttraetion Reduction Performed (15A NCAC 02T .1107). ,Alt. 3 (30-day bench)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Stewart White, ORC Jason Smith VP
Preparer Name and Title (type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
jWX 02-13-2015
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Friday, February 13, 2015
--------------------

Am
P
PROM PT•ACCU RATE• RELIA9 LE
LABORATORIES, INC
WWR:PARLABS.CON1
REPORT OF ANALYSES
Attn: SCOTT CARPENTER
SOIL PLUS
208 WILLIAMS STREET
GREENVILLE, NC 27858-
PROJECT NAME: MAR 14
DATE: 05/07/14
SAMPLE NUMBER-
113320
SAMPLE ID- TA032514
SAMPLE MATRIX- SO
DATE SAMPLED-
03/25/14
TIME SAMPLED- 1230
DATE RECEIVED-
03/28/14
SAMPLER- SC
RECEIVED BY- RE
TIME RECEIVED-
1000
DELIVERED BY- UPS
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD
DATE
TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST
VAR
03/31/14
RE ATTACHED
FECAL COLIFORM
(GEOM. MEAN) SM 9221 E
03/31/14
RE 27,400 MPN/g
LABORATORY DIRECTOR
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]

PAR
PROMPT•ACCURATC-R`fr .,ACI_E
LABORA.'I'ORIES, 1XC
WWW. PARLASS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
Start: End:
TS
0.2295
0.2609
TS%
1.91%
1.91%
VS
0.1481
0.1626
VS%
64.53%
62.32%
IN
0.004578
OUT
0,004003
FSVR Mass Balance)
12.56%
FSVR Van Kleeck
9.08%
FSVR Mass Balance) <15%
YES
FSVR (Van Kieeck) <15%
YES
P.O. Box 411483 • Chariotte, NC 28241 1483
Phone: (704) i88.8131eFax: (704) 588.811i

PI)LF;Z
PROMFIX•ACCURATE-14CLA ,03 C
L,kBORA-1-ORIESx INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 201 SC Cert # 99003001
CLIENT NAME: •
SAMPLE ID:
SAMPLE DATE:
ANALYSIS: 11111111111900M,• • - •
ANALYSIS METHOD: •
7 s�
113320
1
Coliform
776
3.23%
24,030.86
2
936
3.20%
29,244.65
3
661
2.88%
22,949.25
4
929
3.16%
29,410.38
5
897
3.07%
29,223.79
6
936
3,19%
29,339.35
7
918
3.22%
28,510.33
Fecal Coliform
Geometric Mean= • 11

Page 1 of 1
Report Number: 14-356-0759
✓ p ,
Account Number: 04596
U
wwwaleastem.com
Send To: SOIL PLUS, LLC
SCOTT CARPENTER
P.O. BOX 1396
OXFORD NC 27565
Date Received: 12/22/2014 Date Of Analvsis: 12/23/2014
A&L Eastern Laboratories - Carolinas
2850 Daisy Lane Wilson, North Carolina 27896 [phone] Fax [phone]
Grower:
TOWN OFAHOSKIE
SOIL ANALYSIS REPORT
Date Of Report: 12/23/2014
Submitted By: SCOTT CARPENTER
Farm ID: TA
Analytical Method(s):
Mehlich 3
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
o ENR
/o Rate
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
. lbs/A
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm
Rate
p H
Index
meq/100g
meq/100g
1
15094
2.8 M 96
126 VH
38 VL
163
H
971
M
61
L
6.5
0.5
7.1
NC=105
NC=19
2
119 VH
45 VL
H
876
M
L
15095
1.7 L 75
1151
156
6.5
0.5
6.5
NC=99
NC=23
3
15096
0.9 VL 59
164 VH
69 L
1175
H
823
M
141
L
6.6
0.4
6.3
NC=137
NC=35
4
148 VH
97 M
148
H
773
M
52
L
15098
0.9 VL 59
1
6.2
0.8
6.3
NC=123
NC=50
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
CI
Al
Fed ID
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm
Rate
ms/cm Rate
ppm Rate
ppm
1
18 M
6.5 H
7 L
240
VH
2.1 H
0.9
M
1.4
19.1
68.4
3.7
7.4
NC=37
NC=162.5
NC=44
NC=105.0
2
L
6.9 H
5 L
185
VH
2.1 H
M
1.8
19.4
67.4
3.7
7.4
�13
11.1
NC=27
NC=172.5
NC=31
NC=105.0
3
M
8.4 VH
5 L
VH
H
M
2.8
23.1
65.3
2.8
5.9
�23
�189
12.1
11.1
NC=48
NC=210.0
NC=31
NC=105.0
4
19 M
9.3 VH
7 L
211
VH
2.5 H
H
3.9
19.6
61.3
3.6
12.2
11.3
NC=40
NC=232.5
NC=44
NC=125.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: ?Wz. IV
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary