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HomeMy WebLinkAboutNC0024881_Compliance Evaluation Inspection_20191029ROY COOPER Governor MICHAEL S. REGAN Secretary LINDA CULPEPPER Director NORTH CAROLINA Environmental Quality October 29, 2019 CERTIFIED MAIL 7002 0860 0000 7978 3478 RETURN RECEIPT REQUESTED D Kelly Almond City of Reidsville 230 W Morehead St Reidsville, NC 27320 Subject: Notice of Violation — Compliance Evaluation Inspection NOV Tracking No. NOV-2019-PC-0714 NPDES Permit NCO024881 City of Reidsville WWTP, Rockingham County Dear Mr. Almond: On September 27, 2019, Paul DiMatteo and Mike Turner of the Division of Water Resources (Division), Winston-Salem Regional Office met with Ben Bani, Operator in Responsible Charge (ORC), to conduct a Compliance Evaluation Inspection of the above referenced wastewater treatment plant. This inspection consisted of (1) a review of the permit and accompanying documentation to determine compliance with permit conditions, and (2) an on -site inspection of several collection system components. The attached inspection form notes the areas that were evaluated for the inspection, with any observed violations as follows: Summary of Non -Compliance As noted during the previous inspection and reported in our letter dated 2/27/2018, the plant's generators do not have the capacity to power the effluent pumps. This results in a bypass to Little Troublesome Creek whenever power is interrupted. Little Troublesome Creek is not a permitted receiving stream for this facility. Part II. Section C.7 Power Failures states that "the Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 02H .0124) to prevent the discharge of untreated or inadequately treated wastes during electrical power failures either by means of alternate power sources, standby generators or retention of inadequately treated effluent." From January 1, 2018 through October 1, 2019, operators reported 9 such bypasses to this office, with an estimated total of 3.810 million gallons being released to Little Troublesome Creek (Class WS-V, NSW). Such bypasses are both not authorized by the NPDES permit, and the discharged water is inadequately treated for the receiving stream, in violation of this Condition. Please see the attached inspection form for other observations and concerns from the inspection. D North Carolina Department of Environmental Quality I Division of Water Resources EQ�p Winston-Salem Regional Office 1 450 West Hanes Mill Road, Suite 300 I Winston-Salem, North Carolina 27105 NORTH CAROLINA � o•o•°"•mme""°"^•"vin"•i� /� 336.776.9800 Requested Response Within 30 days of receipt of this report, please submit a written plan to address the violation noted above. If you have any questions concerning this report, please contact Paul DiMatteo at (336) 776- 9691 or me at (336) 776-9700. Sincerely, Docu Siiggned by: %_ 145B49E225C94EA... Lon T. Snider, Regional Supervisor Water Quality Regional Operations Section Winston-Salem Regional Office Division of Water Resources, NCDEQ Enclosures — Inspection Report, Regional Inspectors' Checklist for Field Parameters CC: WSRO Laserfiche Files DWR Laboratory Certification Branch (via e-mail) United States Environmental Protection Agency Form Approved. EPA Washington, D.C. 20460 OMB No. 2040-0057 Water Compliance Inspection Report Approval expires 8-31-98 Section A: National Data System Coding (i.e., PCS) Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type 1 IN I 2 IF I 3 I NCO024881 111 12 I 19/09/27 I17 18 I S J 19 L G] 201 I 211111 I I I I I I II I I I I I I I I I I I I I I I I I I I I I I I II I I I I I f6 Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA ---------------------- Reserved ------------------- 671 70 I I 71 I I 72 I r I 73 I I 174 751 I I I I I I I80 u I� I I i Section B: Facility Data Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include Entry Time/Date Permit Effective Date POTW name and NPDES oermit Number) 10:45AM 19/09/27 13/06/01 Reidsville WWTP 407 Broad St Exit Time/Date Permit Expiration Date Reidsville NC 27320 02:OOPM 19/09/27 16/04/30 Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s) Other Facility Data Name, Address of Responsible Official/Title/Phone and Fax Number Contacted D Kelly Almond,230 W Morehead St Reidsville NC 27320//336-349-1030/3363423649 No Section C: Areas Evaluated During Inspection (Check only those areas evaluated) Permit 0 Flow Measurement Operations & Maintenance Records/Reports Self -Monitoring Program 0 Facility Site Review Effluent/Receiving Waters Laboratory Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary) (See attachment summary) Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date Paul DiMatteo DWR/WSRO WQ/336-776-9691/ Signature of Management Q A Review Docusigned by: Agency/Office/Phone and Fax Numbers Date Luti '? Snider 10/29/2019 EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete. Page# NPDES yr/mo/day Inspection Type (Cont.) NCO024881 I11 121 19/09/27 117 18 JCJ Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary) Operator said they're in the process of upgrading next year for 3 stage BNR to lower TP and TN. Still in planning/engineering stages. Flow meter calibrations: 2/11/2019 Custom Controls Unlimited 2/16/2018 Carolina Technical Services 8/14/2019 Carolina Technical Services Other findings of note: 1. Influent & Effluent Composite Sampling. During the inspection, aliquot volume was measured at the effluent composite sampler. The sampler was programmed to take 190 ml, but barely 100 ml was collected. Operators went through the calibration process during the inspection, and the sampler was left properly taking the programmed volume. Please be sure to periodically check the aliquot volume with a graduated cylinder and calibrate the samplers as necessary. 2. Secondary Clarifiers. In Clarifier #1, the inspector noted that there were areas where the effluent appeared to be going under, rather than over, the weirs. This should be corrected so that the clarifiers operate as designed. 3. Effluent flow measurement. The inspector noted that the effluent ultrasonic sensor appeared to be closer to the Parshall flume's throat section than expected. Conditions observed on site appeared to indicate that the recorded flow was within acceptable tolerances at the time of inspection; however, having the sensor at this location may produce a systematic under -reporting of flow. SCADA readings should be compared with the in -situ staff gauge and discharge table at a variety of flow conditions to ensure that recorded flows are within 10% of actual flow for the entire expected flow range. Page# Permit: NCO024881 Owner - Facility: Reidsville WWTP Inspection Date: 09/27/2019 Inspection Type: Compliance Evaluation Operations & Maintenance Yes No NA NE Is the plant generally clean with acceptable housekeeping? 0 ❑ ❑ ❑ Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable ❑ ❑ ❑ Solids, pH, DO, Sludge Judge, and other that are applicable? Comment: Permit Yes No NA NE (If the present permit expires in 6 months or less). Has the permittee submitted a new 0 ❑ ❑ ❑ application? Is the facility as described in the permit? 0 ❑ ❑ ❑ # Are there any special conditions for the permit? ❑ 0 ❑ ❑ Is access to the plant site restricted to the general public? 0 ❑ ❑ ❑ Is the inspector granted access to all areas for inspection? 0 ❑ ❑ ❑ Comment: 7.5 mgd permitted flow. Expired 4/2016, in review. Record Keeping Yes No NA NE Are records kept and maintained as required by the permit? 0 ❑ ❑ ❑ Is all required information readily available, complete and current? 0 ❑ ❑ ❑ Are all records maintained for 3 years (lab. reg. required 5 years)? 0 ❑ ❑ ❑ Are analytical results consistent with data reported on DMRs? 0 ❑ ❑ ❑ Is the chain -of -custody complete? 0 ❑ ❑ ❑ Dates, times and location of sampling Name of individual performing the sampling Results of analysis and calibration Dates of analysis Name of person performing analyses Transported COCs Are DMRs complete: do they include all permit parameters? ❑ ❑ ❑ Has the facility submitted its annual compliance report to users and DWQ? ❑ ❑ ❑ (If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator ❑ ❑ ❑ on each shift? Is the ORC visitation log available and current? ❑ ❑ ❑ Is the ORC certified at grade equal to or higher than the facility classification? ❑ ❑ ❑ Is the backup operator certified at one grade less or greater than the facility classification? ❑ ❑ ❑ Is a copy of the current NPDES permit available on site? ❑ ❑ ❑ Page# 3 Permit: NCO024881 Owner - Facility: Reidsville WWTP Inspection Date: 09/27/2019 Inspection Type: Compliance Evaluation Record Keeping Yes No NA NE Facility has copy of previous year's Annual Report on file for review? 0 ❑ ❑ ❑ Comment: Flow Measurement - Influent Yes No NA NE # Is flow meter used for reporting? ❑ 0 ❑ ❑ Is flow meter calibrated annually? 0 ❑ ❑ ❑ Is the flow meter operational? 0 ❑ ❑ ❑ (If units are separated) Does the chart recorder match the flow meter? ❑ ❑ 0 ❑ Comment: Influent Sampling Yes No NA NE # Is composite sampling flow proportional? 0 ❑ ❑ ❑ Is sample collected above side streams? 0 ❑ ❑ ❑ Is proper volume collected? ❑ ❑ ❑ Is the tubing clean? 0 ❑ ❑ ❑ # Is proper temperature set for sample storage (kept at less than or equal to 6.0 degrees 0 ❑ ❑ ❑ Celsius)? Is sampling performed according to the permit? 0 ❑ ❑ ❑ Comment: Hach Siama SD900 Set for flow proportional sampling 150 ml every 105 counts (however, count volume unknown) Operators said they normally pull --10L/day Temperature checked and recorded on bench sheet daily, read 3C during inspection. Aliquot volume not verified during inspection. Pump Station - Influent Yes No NA NE Is the pump wet well free of bypass lines or structures? ❑ ❑ ❑ Is the wet well free of excessive grease? ❑ ❑ ❑ Are all pumps present? ❑ ❑ ❑ Are all pumps operable? ❑ ❑ ❑ Are float controls operable? ❑ ❑ ❑ Is SCADA telemetry available and operational? 0 ❑ ❑ ❑ Is audible and visual alarm available and operational? ❑ ❑ ❑ Page# 4 Permit: NCO024881 Inspection Date: 09/27/2019 Owner - Facility: Reidsville WWTP Inspection Type: Compliance Evaluation Pump Station - Influent Yes No NA NE Comment: "influent" pumps are after grit removal and pump water up the hill to the aeration basins. Then flows by gravity until it reaches the effluent pumps. During the inspection 1/4 pumps was completely down and 1 was having issues. Operator said they were working on the pump with issues and they would get a portable pump while the other one was down. We did not observe the actual wet well. Bar Screens Yes No NA NE Type of bar screen a.Manual b.Mechanical Are the bars adequately screening debris? 0 ❑ ❑ ❑ Is the screen free of excessive debris? 0 ❑ ❑ ❑ Is disposal of screening in compliance? 0 ❑ ❑ ❑ Is the unit in good condition? 0 ❑ ❑ ❑ Comment: Both mechanical and manual bar screens are in use. Grit Removal Yes No NA NE Type of grit removal a.Manual ❑ b.Mechanical Is the grit free of excessive organic matter? 0 ❑ ❑ ❑ Is the grit free of excessive odor? 0 ❑ ❑ ❑ # Is disposal of grit in compliance? 0 ❑ ❑ ❑ Comment: Aeration Basins Yes No NA NE Mode of operation Ext. Air Type of aeration system Diffused Is the basin free of dead spots? 0 ❑ ❑ ❑ Are surface aerators and mixers operational? ❑ ❑ 0 ❑ Are the diffusers operational? 0 ❑ ❑ ❑ Is the foam the proper color for the treatment process? 0 ❑ ❑ ❑ Does the foam cover less than 25% of the basin's surface? 0 ❑ ❑ ❑ Is the DO level acceptable? 0 ❑ ❑ ❑ Page# 5 Permit: NCO024881 Inspection Date: 09/27/2019 Aeration Basins Is the DO level acceptable?(1.0 to 3.0 mg/1) Owner - Facility: Reidsville WWTP Inspection Type: Compliance Evaluation Comment: Aeration basin DO as read by the oermanently installed Drobes Yes No NA NE ■ ❑ ❑ ❑ 0.8 mg/I 1 st 3rd 2.3 mg/I 2nd 3rd 3.8 mg/I last 3rd One of two aeration basins is in use. Per ORC, they're in the planning stapes of a BNR upgrade in both aeration basins, so they will be identical. Secondary Clarifier Is the clarifier free of black and odorous wastewater? Is the site free of excessive buildup of solids in center well of circular clarifier? Are weirs level? Is the site free of weir blockage? Is the site free of evidence of short-circuiting? Is scum removal adequate? Is the site free of excessive floating sludge? Is the drive unit operational? Is the return rate acceptable (low turbulence)? Is the overflow clear of excessive solids/pin floc? Is the sludge blanket level acceptable? (Approximately'/ of the sidewall depth) Yes No NA NE • ❑ ❑ ❑ • ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ❑ ■ ❑ ❑ • ❑ ❑ ❑ • ❑ ❑ ❑ • ❑ ❑ ❑ • ❑ ❑ ❑ • ❑ ❑ ❑ • ❑ ❑ ❑ Comment: Sludge blanket -2.5 feet (13 feet total depth). Measured in clarifier #1. There appeared to be an area where water was being discharged from under the clarifier weir rather than over it. This should be corrected. Filtration (High Rate Tertiary) Yes No NA NE Type of operation: Down flow Is the filter media present? ❑ ❑ ❑ Is the filter surface free of clogging? ❑ ❑ ❑ Is the filter free of growth? ❑ ❑ ❑ Is the air scour operational? ❑ ❑ ❑ Is the scouring acceptable? ❑ ❑ ❑ Is the clear well free of excessive solids and filter media? 0 ❑ ❑ ❑ Comment: Disinfection -Gas Yes No NA NE Are cylinders secured adequately? 0 ❑ ❑ ❑ Page# 6 Permit: NCO024881 Owner - Facility: Reidsville WWTP Inspection Date: 09/27/2019 Inspection Type: Compliance Evaluation Disinfection -Gas Yes No NA NE Are cylinders protected from direct sunlight? 0 ❑ ❑ ❑ Is there adequate reserve supply of disinfectant? 0 ❑ ❑ ❑ Is the level of chlorine residual acceptable? 0 ❑ ❑ ❑ Is the contact chamber free of growth, or sludge buildup? 0 ❑ ❑ ❑ Is there chlorine residual prior to de -chlorination? ❑ ❑ ❑ Does the Stationary Source have more than 2500 Ibs of Chlorine (CAS No. 7782-50-5)? ❑ 0 ❑ ❑ If yes, then is there a Risk Management Plan on site? ❑ ❑ 0 ❑ If yes, then what is the EPA twelve digit ID Number? (1000- - ) If yes, then when was the RMP last updated? Comment: Have 9 150 lb tanks. Operators said they get 5 tanks every 2 weeks. Chlorine is added both before and after the sand filter. De -chlorination Type of system ? Is the feed ratio proportional to chlorine amount (1 to 1)? Is storage appropriate for cylinders? # Is de -chlorination substance stored away from chlorine containers? Are the tablets the proper size and type? Comment: Stored in separate sheds across the plant from each other. Are tablet de -chlorinators operational? Number of tubes in use? Comment: Sulfur dioxide Standby Power Is automatically activated standby power available? Is the generator tested by interrupting primary power source? Is the generator tested under load? Was generator tested & operational during the inspection? Do the generator(s) have adequate capacity to operate the entire wastewater site? Is there an emergency agreement with a fuel vendor for extended run on back-up power? Is the generator fuel level monitored? Yes No NA NE Gas ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ Yes No NA NE ■ ❑ ❑ ❑ ❑ ■ ❑ ❑ ■ ❑ ❑ ❑ ❑ ❑ ❑ ■ ❑ ■ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ Page# 7 Permit: NCO024881 Inspection Date: 09/27/2019 Standby Power Comment: Yearlv maintenance. Owner - Facility: Reidsville WWTP Inspection Type: Compliance Evaluation Yes No NA NE Operators said it isn't necessarily tested regularly under load, but it sounds like it comes on fairly frequently due to power interruptions, including the morning of the inspection. The generators run the entire plant except for the effluent pumps, leading to a bypass of treated wastewater to Little Troublesome Creek during power outages. The operators have been in the process of having a dedicated generator installed, but it has taken some time to get funding approved. Pumps-RAS-WAS Are pumps in place? Are pumps operational? Are there adequate spare parts and supplies on site? Comment: Laboratory Are field parameters performed by certified personnel or laboratory? Are all other parameters(excluding field parameters) performed by a certified lab? # Is the facility using a contract lab? # Is proper temperature set for sample storage (kept at less than or equal to 6.0 degrees Celsius)? Incubator (Fecal Coliform) set to 44.5 degrees Celsius+/- 0.2 degrees? Incubator (BOD) set to 20.0 degrees Celsius +/- 1.0 degrees? Yes No NA NE ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ Yes No NA NE • ❑ ❑ ❑ • ❑ ❑ ❑ • ❑ ❑ ❑ • ❑ ❑ ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ Comment: Analyze TSS and field parameters at lab. Other samples are analyzed by Meritech. A Regional Inspector's Checklist for Field Parameters was completed during the inspection. The form is attached. Flow Measurement - Effluent # Is flow meter used for reporting? Is flow meter calibrated annually? Is the flow meter operational? (If units are separated) Does the chart recorder match the flow meter? Yes No NA NE ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ❑ ❑ ■ ❑ Comment: Flow readings are recorded on SCADA. 2' Parshall Flume with ultrasonic sensor. The sensor appeared to be slightly too close to the Flume's throat section. On 10/18/2019 1 was at the plant again for an unrelated reason and checked the flow meters again. At approximately 10:15 am, the staff gauge in the proper location in the flume read approximately 0.78 feet. SCADA at that time reported approximately 3.248 mqd; table value is 3.518 mqd. This is an error of 7.7%, which is acceptable. However, multiple flow rates should be evaluated to ensure that 10% accuracy is maintained throughout the range of expected flow. Page# 8 Permit: NCO024881 Inspection Date: 09/27/2019 Owner - Facility: Reidsville WWTP Inspection Type: Compliance Evaluation Effluent Sampling Is composite sampling flow proportional? Is sample collected below all treatment units? Is proper volume collected? Is the tubing clean? # Is proper temperature set for sample storage (kept at less than or equal to 6.0 degrees Celsius)? Is the facility sampling performed as required by the permit (frequency, sampling type representative)? Yes No NA NE ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ❑ ❑ ❑ ■ ■ ❑ ❑ ❑ Comment: Effluent sannDler is a HACH AS950. set to take 190 ml every 24.000 aal. Amount Dulled in a graduated cylinder was slightly under 100 ml. We went through the calibration process during the inspection so the pulled volume was as expected. Operators should check the calibration of their sampler periodically using a graduated cylinder. Refrigerator temperature approximately 3C. Pump Station - Effluent Yes No NA NE Is the pump wet well free of bypass lines or structures? ❑ 0 ❑ ❑ Are all pumps present? 0 ❑ ❑ ❑ Are all pumps operable? 0 ❑ ❑ ❑ Are float controls operable? 0 ❑ ❑ ❑ Is SCADA telemetry available and operational? 0 ❑ ❑ ❑ Is audible and visual alarm available and operational? 0 ❑ ❑ ❑ Comment: As mentioned Dreviouslv the outfall to Little Troublesome Creek is still available and used when the effluent pumps are offline due to power failures. Effluent Pipe Yes No NA NE Is right of way to the outfall properly maintained? 0 ❑ ❑ ❑ Are the receiving water free of foam other than trace amounts and other debris? 0 ❑ ❑ ❑ If effluent (diffuser pipes are required) are they operating properly? ❑ ❑ 0 ❑ Comment: Outfall is located on the Haw River near the bridge at NC 150. There appeared to be some color in the discharaed water. but it also aDDeared clearer than the stream water. Page# 9 Regional Inspectors' Checklist for Field Parameters DS [This checklist is to be completed during regional plant inspections for Field Laboratories, denoted by certification numbers in the 5000s.] `?MA Facility Name: Reidsville WWTP Regional Plant Inspector: Paul DiMatteo Permit #: NC0024881 Regional Inspector Contact #: 336-776-9691 Field Lab Certification #: 179 Region: Winston Salem Lab Contact: Larry Date: 9/27/2019 I. Check the parameter(s) performed at this site for reporting purposes. ® Total Residual Chlorine (TRC) ® Temperature (TEMP) ® Specific Conductance (SC) ® pH ® Dissolved Oxygen (DO) ❑ Settleable Residue (SETT) II. General Laboratory (note any exceptions in section XI) Are instruments, meters, probes, photometric cells, etc. maintained in good condition? ® Yes ❑ No Are standards, reagents and consumables used within manufacturer expiration dates? [TRC gel standard is exempt.] ® Yes ❑ No Are the following items documented ( where applicable): Item TRC pH TEMP DO SC SETT Date of sample collection* N/A Time of sample collection* N/A Sample collector's initials or signature N/A Date of sample analysis* N/A Time of sample analysis* N/A N/A Analyst initials or signature N/A Sample site i.e., facility name, location, ID, etc. N/A Instrument ID N/A Parameter N/A Data qualifiers, when required N/A *Date and time of sample collection and analysis may be the same for in situ or on -site measurements. III. Total Residual Chlorine — reference method: SM 2400 CI G-2011 Total Residual Chlorine meter make and model: Thermofisher Scientific S pectro photometer Is a check standard analyzed each day of use? (Circle one: gel or liquid standard) ® Yes ❑ No Does the check standard recover within ±10% of the known value? ® Yes ❑ No What is the assigned/observed value of the daily check standard? 50ug/I Is a 5-standard calibration verification performed? Note date of last verification: ® Yes ❑ No Alternatively, does the lab construct a linear regression, using 5 standards, to calculate results? Note date of last calibration curve constructed: ® Yes ❑ No True values: ® pg/L ❑ mg/L 20 30 50 100 300 Obtained values: ® lag/L ❑ mg/L 24 28 52 96 301 What program are samples analyzed on? N/E Are results reported in proper units? Check one: ❑ lag/L ❑ mg/L ® Yes ❑ No Are results reported between the facility's permit limit and the compliance limit of 50 lag/L? ® Yes ❑ No Are results less than the low standard reported as "<x", where x=low standard conc.? ® Yes ❑ No Is DPD/buffer added within 15 minutes of collection? ® Yes ❑ No Is a post -analysis check standard analyzed if samples are analyzed at multiple sites? ® Yes ❑ No IV. pH — reference method: SM 2500 H+ B-2011 pH meter manufacturer and model: Thermo Orion Star A211 Is the pH meter calibrated with at least 2 buffers per mfg's instructions each day of use? Note buffers used: ®Yes ❑ No Is the pH meter calibration checked with an additional buffer prior to sample analysis? Note check buffer used: ® Yes ❑ No Does the check buffer read within ±0.1 S.U. of the known value? ® Yes ❑ No Are the following items documented: Meter calibration? ® Yes ❑ No Check buffer readin s)? ® Yes ❑ No Are samples analyzed within 15 minutes of collection? ® Yes ❑ No Are sample results reported to 0.1 pH units on the eDMR? ® Yes ❑ No Is a post -analysis check buffer analyzed if samples are analyzed at multiple sites? N/A ❑ Yes 0 No V. Temperature — reference method: What instrument(s) is used to measure temperature? Check all that apply: ❑ pH meter ❑ DO meter ❑ Conductivity meter ❑ Digital thermometer ❑ Glass thermometer Is the instrument/thermometer calibration checked at least annually against a NIST traceable thermometer? ® Yes ❑ No Is NIST traceability documentation maintained on site? ® Yes ❑ No Are samples measured within 15 minutes? ® Yes ❑ No Are sample results reported in degrees C? ® Yes ❑ No VI. Dissolved Oxygen — reference method: SM 4500-OG 2011 DO meter make and model: YSI Pro Plus Is the air calibration of the DO meter performed each day of use? ® Yes ❑ No Is meter calibration documented? ® Yes ❑ No Are samples analyzed within 15 minutes of collection? ® Yes ❑ No Are results reported in m /L? ® Yes ❑ No If samples are analyzed at multiple sites, is the meter recalibrated at each site or a post- analysis calibration verification performed? N/A ❑ Yes ❑ No Does the post -analysis verification theoretical value agree within 0.5 mg/L of the meter calibration reading? N/A ❑ Yes ❑ No VII. Conductivity — reference method: Conductivity meter make and model: SensION EC 71 Is the meter calibrated daily according to the manufacturer's instructions? Note standard used this is generally a one -point calibration): 1400 ® Yes ❑ No Is a daily check standard analyzed? Note value: 718, 147 ® Yes ❑ No Is meter calibration documented? ® Yes ❑ No Are samples analyzed within 28 days of collection? ® Yes ❑ No Is a post -analysis check standard analyzed if multiple samples are analyzed? N/A Are results reported in pmhos/cm some meters display equivalent pS/cm units)? ® Yes ❑ No Vill. Settleable Residue — reference method: N/A Does the laboratory have an Imhoff Cone in good condition? ❑ Yes ❑ No Is the sample settled for 1 hour? ❑ Yes ❑ No Is the sample aitated after 45 minutes? ❑ Yes ❑ No Are the following items documented: Volume of sample analyzed? Note volume analyzed must use 1 L : ❑ Yes ❑ No Date and time of sample analysis (settling start time)? ❑ Yes ❑ No Time of agitation after 45 minutes of settling? ❑ Yes ❑ No Sample analysis completion (settling end time)? ❑ Yes ❑ No Are samples analyzed within 48 hours of collection? ❑ Yes ❑ No Are results reported in ml/L? ❑ Yes ❑ No IX. Was a paper trail (comparing contract lab and on -site data to DMRs) performed? If so, list months reviewed: 8/2018, 1/2019 ® Yes ❑ No X. Is follow-up by the Laboratory Certification program recommended? ❑ Yes ® No XI. Additional comments: Please submit a copy of this completed form to the Laboratory Certification program at: DWR Lab Certification, Water Sciences Section, 1623 Mail Service Center, Raleigh NC, 27699-1623 Electronic copies may be emailed to dana.satterwhite(a)-ncdenr.gov. Revision 4/2018