WQ0034688_Residual Annual Report 2014_20150225

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NEUSE REGIONAL WATER AND SEWER AUTHORITY
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0034688
2014 ANNUAL REPORT
•
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• Neuse Regional Water and Sewer Authority, NC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual. Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses
•

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00034688 County Lenoir Year 2014
Facility Name (as shown on permit) Neuse Regional Water Treatment Plant NPDES No. NC0088111
• Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: N/A
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 389.63
Total number of acres utilized for land application during the year: 116.5
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 .
regulated facilities).
9.. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. ]
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Harold Herring, Executive Director
Permittee Name and Title (type or print) gignature of Perinittee 15ate
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
0

2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
NEUSE REGIONAL WASA, NC
&EUSE REGIONAL WASA, NC WTP LIQUID
MONTHNEAR
October 2014
YEARLY TOTAL
•
AMOUNT UNIT
2,938,188.00 G
2,938,188.00 G
DRY METRIC
DRY TONS UNIT TONS
389.63 D 353.37
389.63 D 353.37
2/17/2015

•
PROJECT:
FACILITY:
2014 ANNUAL REPORT
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
40
Neuse Regional Water and Sewer
Authority
Neuse Regional Water Treatment Plant
2811 Barrus Road
LaGrange, NC 28551
252-522-2567
NCO088111
Harold Herring, Executive Director
2811 Barrus Road
LaGrange, NC 28551
PO Box 6277
Kinston, NC 28501
252-522-3567
Charlie Colie
NRWASA Superintendent
2811 Barrus Road
LaGrange, NC 28551
252-522-2567
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

•
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0034688 Laboratory
Facility Name: NEUSE REGIONAL WASA, NC A&L Eastern Laboratories Inc.
NPDES# : NCO088111
or WQ# (residual only)
WWTP Name: NEUSE REGIONAL WASA WTP
Residuals Analysis Data
Product Type
WPL
WPL
WPL
WPL
WPL
Date Sampled (grab) or 08/19/14
09/17/14
10/06/14
10/09/14
10/21/14
Date Composited
Percent Solids
3.33
3.18
4.79
2.02
5.07
PARAMETERS (mg/kg dry weight)
Arsenic
9
9
10
15
8
Cadmium
<2
<2
<2
<2
<2
Mercury
<0.4
<0.4
<0.4
0.5
<0.4
Chromium
82
67
209
22
256
Copper
761
670
749
336
883
Lead
12
11
12
5
9
Molybdenum
<5
<5
<5
19
<5
Nickel
34
28
82
12
93
Selenium
<5
<5
<5
<5
<5
Zinc
95
84
90
161
75
Total Phosphorus
2150
2090
2640
2930
2140
TKN
10500
12600
11700
9900
6310
Ammonia -Nitrogen
4200
3770
1040
1980
394
Nitrate and Nitrite
18
<2
50.1
<2
<2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date��-
(SIGNATURE OF
•
DENR FORM RSSF (5/2003) Printed: Tuesday - February 17 2015 at 10:20:10 for: 1703 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0034688 Laboratory
Facility Name: NEUSE REGIONAL WASA, NC A&L Eastern Laboratories Inc.
NPDES# : NCO088111
or WQ# (residual only)
WWTP Name: NEUSE REGIONAL WASA WTP
Residuals Analysis Data
Product Type
WPL
WPL
WPL
WPL
WPL
Date Sampled (grab) or 08/19/14
09/17/14
10/06/14
10/09/14
10/21/14
Date Composited
Percent Solids
3.33
3.18
4.79
2.02
5.07
PARAMETERS (mg/kg dry weight)
Aluminum
128000
139000
104000
129000
117000
Calcium
4130
4790
1910
1480
1600
Magnesium
920
1030
786
1150
756
pH
6.91
7.02
6.52
5.35
6.63
Potassium
775
942
648
544
739
Sodium
543
626
539
758
522
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF REPARER)
NR - Data Not Reported or Data Not Required
Date ���
3
DENR FORM RSSF-B (7/2002) Printed: Tuesday - February 17, 2015 at 10:20:35 for: 1703 01

•
Page: 1 of 2
Report Number: 14-234-0203
Account Number: 00454 9
Submitted By: WILL VARNER www.aleastem.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALL PURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 57169
Sample Id : NRWASA
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: NRWASA
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 8/19/2014 13:30:00
Date Received: 08/22/2014 00:00
Date Reported: 08/28/2014
Total Solids *
3.33
33300
100.0
RD
08/22/2014 14:19
SM-2540G
Moisture *
96.67
100.0
RD
08/22/2014 14:19
SM-2540G
Total Kjeldahl Nitrogen
1.05
10500
10.0
JM
08/25/2014 08:24
SM-4500-NH3C-TKN
Total Phosphorus
0.22
2150
100
KM
08/28/2014 09:03
SW 6010C
Total Potassium
0.08
775
100
KM
08/28/2014 09:03
SW 6010C
Total Sulfur
0.91
9090
100
KM
08/28/2014 09:03
SW 6010C
Total Calcium
0.41
4130
100
KM
08/28/2014 09:03
SW 6010C
Total Magnesium
0.09
920
100
KM
08/28/2014 09:03
SW 6010C
Total Sodium
0.05
543
100
KM
08/28/2014 09:03
SW 6010C
Total Iron
27200
100
KM
08/28/2014 09:03
SW 6010C
Total Aluminum
128000
100
KM
08/28/2014 09:03
SW 6010C
Total Manganese
1090
5
KM
08/28/2014 09:03
SW 6010C
Total Copper
761
5
KM
08/28/2014 09:03
SW 6010C
Total Zinc
95
5
KM
08/28/2014 09:03
SW 6010C
Ammonia Nitrogen
0.42
4200
10.0
JM
08/25/2014 08:24
SM-4500-NH3C
Organic N
0.63
6300
10.0
08/25/2014 08:24
CALCULATION
Nitrate+Nitrite-N
18.0
2.00
JM
08/25/2014 08:25
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
08/28/2014 09:03
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9;6�1
9
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•

•
Page: 2 of 2
Report Number: 14-234-020399,
Account Number: 00454
Submitted By: WILL VARNER wwwaleastem.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALL PURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: NRWASA
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 8/19/2014 13:30:00
Lab Number: 57169 Date Received: 08/22/2014 00:00
Sample Id: NRWASA Date Reported: 08/28/2014
Total Chromium
82
5
KIVI
U6/Zt5lLU 14 Ua:w
0VV ov IUi.
Total Nickel
34
5
KM
08/28/2014 09:03
SW 6010C
Total Lead
12
5
KM
08/28/2014 09:03
SW 6010C
Total Arsenic
9.0
3.0
KM
08/28/2014 09:03
SW 6010C
Total Mercury
<0.4
0.4
KM
08/26/2014 12:45
SW-7471 B
Total Selenium
<5.0
5.0
KM
08/28/2014 09:03
SW 6010C
pH (Standard Units) `
6.91
2.00
JM
08/25/2014 08:24
SW-9045D
Total Molybdenum
<5
5
KM
08/28/2014 09:03
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX XPIKE WAS OUT OF LIMITS FOR "P", "Fe", AND "Cr", ALL OTHER QA/QC WAS WITHIN LIMITS.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

•
•
SAMi'I_tPJG LOG
CHAIN OF CUSTODY
CUSTOMER: SYNAGRO SOUTHEAST ` ����p���������plu���V�l�����1111���i�����l�� lll� 9� zo3 �E�QRD & ANALYSIS
os-zz-zoia RECORD
� SYNAGRO CENTRAL LLC7NEUSE REG WASH 1 L25'32
PROl�CT MANAGER: NRWASAVNC CERT9257 field sampling procedures
Phone: ( �j6 ) ;� T �G
collection of these samples.
ram -
SAMPLER
A & L CUSTOMER
LAB # SAMPLE J.D.
SAMPLING
LOCATION
SAMPLE
TYPE
# OF SAMPLING METHOD
CONTAINERS DATE TIME PRESERVED
METHOD
SHIPPED
Relinquis d by Sam
Relinqu e by:
d,,
Relinquished by:
SPECIAL INSTRUCTIONS:
For
monitoring purposes.
Date Time Recieved by:
D e Time
32-/ 1")
Date Time
Recieved
PO#:
REMARKS:
SAMPLE
ANALYSIS REQUEST
I.D.
=L1
L2
NH4N
NO3N
Organic
NCd
Cr
Ni
Pb
As
Hg
Se
pH
CacO
a uiv�
Volatile
Solids
I Mo
GI
NO2-N
too
Y
Poor
pot
pot
koo
Pot
Poll`
Y
k0or
k0of
ok
SL1: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
White —A & L Canary MANAGER COPY

Sodium Absorption Ratio Calculation (SAR)
0
Product Code Product Name Sample Date Report Range Ratio
1703-01-WPL-NC NEUSE REGIONAL WASA, NC WTP LIQUID 8/19/2014 / / - / / 0.3621
Na mg/I = (Na mg/kg x % Solids) = 100 = (543 x 3.3300) _ 100 = 18.0819
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (4130 x 3.3300) =100 = 137.529
Mg mg/I = (mg mg/kg x % Solids) = 100 = (920 x 3.3300) = 100 = 30.636
Na meq = Na mg/I _ Molec.Wgt.Na = 18.0819 _ 23 = 0.78617
Ca meq = Ca mg/I + Molec.Wgt.Ca = 137.529 = 20 = 6.87645
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 30.636 _ 12 = 2.553
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.78617 _ SgrRoot[0.5(6.87645+2.553)] = 0.362066
•
Printed: 2/17/2015
Page 1 10:21

•
Page: 1 of 2
Report Number: 14-261-0211
Account Number: 00454 @D,
Submitted By: WILL VARNER wwwaleastem.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALLPURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 57654
Sample Id : NRWASA
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: NRWASA
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 9/17/2014 11:00:00
Date Received: 09/18/2014 00:00
Date Reported: 09/24/2014
Total Solids *
3.18
31800
100.0
RD
09/18/2014 14:19
SM-2540G
Moisture *
96.82
100.0
RD
09/18/2014 14:19
SM-2540G
Total Kjeldahl Nitrogen
1.26
12600
10.0
JM
09/19/2014 09:00
SM-4500-NH3C-TKN
Total Phosphorus
0.21
2090
100
KM
09/22/2014 13:39
SW 6010C
Total Potassium
0.09
942
100
KM
09/22/2014 13:39
SW 6010C
Total Sulfur
0.87
8740
100
KM
09/22/2014 13:39
SW 6010C
Total Calcium
0.48
4790
100
KM
09/22/2014 13:39
SW 6010C
Total Magnesium
0.10
1030
100
KM
09/22/2014 13:39
SW 6010C
Total Sodium
0.06
626
100
KM
09/22/2014 13:39
SW 6010C
Total Iron
28900
100
KM
09/22/2014 13:39
SW 6010C
Total Aluminum
139000
100
KM
09/22/2014 13:39
SW 6010C
Total Manganese
1210
5
KM
09/22/2014 13:39
SW 6010C
Total Copper
670
5
KM
09/22/2014 13:39
SW 6010C
Total Zinc
84
5
KM
09/22/2014 13:39
SW 6010C
Ammonia Nitrogen
0.38
3770
10.0
JM
09/19/2014 08:30
SM-4500-NH3C
Organic N
0.88
8830
10.0
09/19/2014 08:30
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
09/22/2014 08:25
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
09/22/2014 13:39
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•

•
Page: 2 of 2
Report Number: 14-261-0211
Account Number: 00454
Submitted By: WILL VARNER www.aleastem.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALLPURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 57654
Sample Id : NRWASA
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: NRWASA
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 9/17/2014 11:00:00
Date Received: 09/18/2014 00:00
Date Reported: 09/24/2014
Total Chromium
67
5
KM
09/22/2014 13:39
SW 6010C
Total Nickel
28
5
KM
09/22/2014 13:39
SW 6010C
Total Lead
11
5
KM
09/22/2014 13:39
SW 6010C
Total Arsenic
9.0
3.0
KM
09/22/2014 13:39
SW 6010C
Total Mercury
<0.4
0.4
KM
09/22/2014 10:10
SW-7471 B
Total Selenium
<5.0
5.0
KM
09/22/2014 13:39
SW 6010C
pH (Standard Units) "
7.02
2.00
JM
09/19/2014 08:30
SW-9045D
Total Molybdenum
<5
5
KM
09/22/2014 13:39
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work the results; or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
0
Product Code Product Name Sample Date Report Range Ratio
1703-01-WPL-NC NEUSE REGIONAL WASA, NC WTP LIQUID 9/17/2014 10/1/2014-10/31/2014 0.3805
Na mg/I = (Na mg/kg x % Solids) _ 100 = (626 x 3.1800) = 100 = 19.9068
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (4790 x 3.1800) =100 = 152.322
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1030 x 3.1800) + 100 = 32.754
Na meq = Na mg/I = Molec.Wgt.Na = 19.9068 _ 23 = 0.865513
Ca meq = Ca mg/I = Molec.Wgt.Ca = 152.322 + 20 = 7.6161
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 32.754 + 12 = 2.7295
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.865513 _ SgrRoot[0.5(7.6161+2.7295)] = 0.380549
is
Printed: 2/17/2015
Page 1 10:21

•
Page: 1 of 2
Report Number: 14-281-0205Y■�[(�(
Account Number: 00454
m
Submitted By: WILL VARNER wwwaleastem.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALLPURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 58007
Sample Id: NRWASA
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271.W6
Project: NRWASA
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 10/6/2014 17:00:00
Date Received: 10/08/2014 00:00
Date Reported: 10/17/2014
Total Solids *
4.79
47900
100.0
JM
10/08/2014 13:45
SM-2540G
Moisture *
95.21
100.0
JM
10/08/2014 13:45
SM-2540G
Total Kjeldahl Nitrogen
1.17
11700
10.0
JM
10/09/2014 08:19
SM-4500-NH3C-TKN
Total Phosphorus
0.26
2640
100
KM
10/17/2014 08:39
SW 6010C
Total Potassium
0.06
648
100
KM
10/17/2014 08:39
SW 6010C
Total Sulfur
0.61
6060
100
KM
10/17/2014 08:39
SW 6010C
Total Calcium
0.19
1910
100
KM
10/17/2014 08:39
SW 6010C
Total Magnesium
0.08
786
100
KM
10/17/2014 08:39
SW 6010C
Total Sodium
0.05
539
100
KM
10/17/2014 08:39
SW 6010C
Total Iron
26200
100
KM
10/17/2014 08:39
SW 6010C
Total Aluminum
104000
100
KM
10/17/2014 08:39
SW 6010C
Total Manganese
1280
5
KM
10/17/2014 08:39
SW 6010C
Total Copper
749
5
KM
10/17/2014 08:39
SW 6010C
Total Zinc
90
5
KM
10/17/2014 08:39
SW 6010C
Ammonia Nitrogen
0.10
1040
10.0
JM
10/09/2014 08:19
SM-4500-NH3C
Organic N
1.07
10660
10.0
10/09/2014 08:19
CALCULATION
Nitrate+Nitrite-N
50.1
2.00
JM
10/09/2014 08:20
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
10/17/2014 08:39
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•
_J

•
Page: 2 of 2
Report Number: 14-281-0205�,f(
Account Number: 00454
Submitted By: WILL VARNER
www.aleastem.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG
WASA
MARSHALL PURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 58007
Sample Id : NRWASA
•
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: NRWASA
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 10/6/2014 17:00:00
Date Received: 10/08/2014 00:00
Date Reported: 10/17/2014
Total Chromium
209
5
KM
10/17/2014 08:39
SW 6010C
Total Nickel
82
5
KM
10/17/2014 08:39
SW 6010C
Total Lead
12
5
KM
10/17/2014 08:39
SW 6010C
Total Arsenic
10.0
3.0
KM
10/17/2014 08:39
SW 6010C
Total Mercury
<0.4
0.4
KM
10/09/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/17/2014 08:39
SW 6010C
pH (Standard Units) *
6.52
2.00
JM
10/09/2014 08:19
SW-9045D
Total Molybdenum
<5
5
KM
10/17/2014 08:39
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Mn", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
40
Product Code Product Name Sample Date Report Range Ratio
1703-01-WPL-NC NEUSE REGIONAL WASA, NC WTP LIQUID 10/6/2014 / / - / / 0.5717
Na mg/I = (Na mg/kg x % Solids) + 100 = (539 x 4.7900) + 100 = 25.8181
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (1910 x 4.7900) + 100 = 91.489
Mg mg/I = (mg mg/kg x % Solids) + 100 = (786 x 4.7900) + 100 = 37.6494
Na meq = Na mg/I + Molec.Wgt.Na = 25.8181 + 23 = 1.12253
Ca meq = Ca mg/I + Molec.Wgt.Ca = 91.489 + 20 = 4.57445
Mg meq = Mg mg/I + Molec.Wgt.Mg = 37.6494 + 12 = 3.13745
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.12253 + SgrRoot[0.5(4.57445+3.13745)] = 0.571651
is
Printed: 2/17/2015
Page 1 10:21

•
Page: 1 of 2
Report Number: 14-289-0206 99.
Account Number: 00454
Submitted By: WILL VARNER wwwaleastem.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALLPURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 58187
Sample Id: NRWASA
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 7434401 Fax [phone]
Project: NRWASA LAGOON
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 10/9/2014 15:00:00
Date Received: 10/16/2014 00:00
Date Reported: 10/23/2014
Total Solids *
2.02
20200
100.0
BW
10/16/2014 14:39
SM-2540G
Moisture *
97.98
100.0
BW
10/16/2014 14:39
SM-2540G
Total Kjeldahl Nitrogen
0.99
9900
10.0
JM
10/17/2014 09:20
SM-4500-NH3C-TKN
Total Phosphorus
0.29
2930
100
KM
10/20/2014 12:46
SW 6010C
Total Potassium
0.05
544
100
KM
10/20/2014 12:46
SW 6010C
Total Sulfur
1.56
15600
100
KM
10/20/2014 12:46
SW 6010C
Total Calcium
0.15
1480
100
KM
10/20/2014 12:46
SW 6010C
Total Magnesium
0.12
1150
100
KM
10/20/2014 12:46
SW 6010C
Total Sodium
0.08
758
100
KM
10/20/2014 12:46
SW 6010C
Total Iron
15000
100
KM
10/20/2014 12:46
SW 6010C
Total Aluminum
129000
100
KM
10/20/2014 12:46
SW 6010C
Total Manganese
1510
5
KM
10/20/2014 12:46
SW 6010C
Total Copper
336
5
KM
10/20/2014 12:46
SW 6010C
Total Zinc
161
5
KM
10/20/2014 12:46
SW 6010C
Ammonia Nitrogen
0.20
1980
10.0
JM
10/17/2014 09:20
SM-4500-NH3C
Organic N
0.79
7920
10.0
10/17/2014 09:20
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
10/22/2014 08:20
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
10/20/2014 12:46
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•

•
Page: 2 of 2
Report Number: 14-289-0206
Account Number: 00454 @D,
Submitted By: WILL VARNER wwwaleastern.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALL PURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 58187
Sample Id : NRWASA
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: NRWASA LAGOON
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 10/9/2014 15:00:00
Date Received: 10/16/2014 00:00
Date Reported: 10/23/2014
Total Chromium
22
5
KM
10/20/2014 12:46
SW 6010C
Total Nickel
12
5
KM
10/20/2014 12:46
SW 6010C
Total Lead
5
5
KM
10/20/2014 12:46
SW 6010C
Total Arsenic
15.0
3.0
KM
10/20/2014 12:46
SW 6010C
Total Mercury
0.5
0.4
KM
10/17/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/20/2014 12:46
SW 6010C
pH (Standard Units) *
5.35
2.00
JM
10/17/2014 09:20
SW-9045D
Total Molybdenum
19
5
KM
10/20/2014 12:46
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Fe", "P", "Se", "S", "NH4-N". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining ourprior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
40
Product Code Product Name Sample Date ReportRange Ratio
1703-01-WPL-NC NEUSE REGIONAL WASA, NC WTP LIQUID 10/9/2014 / / - / / 0.5083
Na mg/I = (Na mg/kg x % Solids) _ 100 = (758 x 2.0200) = 100 = 15.3116
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (1480 x 2.0200) =100 = 29.896
Mg mg/I = (mg mg/kg x % Solids) + 100 = (1150 x 2.0200) -100 = 23.23
Na meq = Na mg/I = Molec.Wgt.Na = 15.3116 _ 23 = 0.665722
Ca meq = Ca mg/I = Molec.Wgt.Ca = 29.896 _ 20 = 1.4948
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 23.23 _ 12 = 1.93583
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.665722 _ SgrRoot[0.5(1.4948+1.93583)] = 0.508301
•
Printed: 2/17/2015
Page 1 10:21

•
Page: 1 of 2
Report Number: 14-304-0204 Account Number: 00454
Submitted By: WILL VARNER www.aleastern.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALLPURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 58445
Sample Id : NRWASA
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: NRWASA
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 10/21/2014 14:00:00
Date Received: 10/31/2014 00:00
Date Reported: 11/06/2014
Total Solids *
5.07
50700
100.0
JM
10/31/2014 15:00
SM-2540G
Moisture *
94.93
100.0
JM
10/31/2014 15:00
SM-2540G
Total Kjeldahl Nitrogen
0.63
6310
10.0
JM
11/03/2014 08:24
SM-4500-NH3C-TKN
Total Phosphorus
0.21
2140
100
KM
11/03/2014 11:22
SW 6010C
Total Potassium
0.07
739
100
KM
11/03/2014 11:22
SW 6010C
Total Sulfur
0.75
7480
100
KM
11/03/2014 11:22
SW 6010C
Total Calcium
0.16
1600
100
KM
11/03/2014 11:22
SW 6010C
Total Magnesium
0.08
756
100
KM
11/03/2014 11:22
SW 6010C
Total Sodium
0.05
522
100
KM
11/03/2014 11:22
SW 6010C
Total Iron
23100
100
KM
11/03/2014 11:22
SW 6010C
Total Aluminum
117000
100
KM
11/03/2014 11:22
SW 6010C
Total Manganese
911
5
KM
11/03/2014 11:22
SW 6010C
Total Copper
883
5
KM
11/03/2014 11:22
SW 6010C
Total Zinc
75
5
KM
11/03/2014 11:22
SW 6010C
Ammonia Nitrogen
0.04
394
10.0
JM
11/03/2014 08:24
SM-4500-NH3C
Organic N
0.59
5916
10.0
11/03/2014 08:24
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
11/03/2014 07:55
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
11/03/2014 11:22
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or art nor may an reference be made
P Y P P, Y Y
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
•

•
Page: 2 of 2
Report Number: 14-304-0204 go.
Account Number: 00454
Submitted By: WILL VARNER www.aleastern.com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG WASA
MARSHALLPURYEAR
284 BOGER RD
STE 204
MOCKSVILLE , NC 27028
Lab Number: 58445
Sample Id: NRWASA
•
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: NRWASA
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 10/21/2014 14:00:00
Date Received: 10/31/2014 00:00
Date Reported: 11/06/2014
Total Chromium
256
5
KM
11/03/2014 11:22
SW 6010C
Total Nickel
93
5
KM
11/03/2014 11:22
SW 6010C
Total Lead
9
5
KM
11/03/2014 11:22
SW 6010C
Total Arsenic
8.0
3.0
KM
11/03/2014 11:22
SW 6010C
Total Mercury
<0.4
0.4
KM
11/03/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
11/03/2014 11:22
SW 6010C
pH (Standard Units) "
6.63
2.00
JM
11/03/2014 08:24
SW-9045D
Total Molybdenum
<5
5
KM
11/03/2014 11:22
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
1703-01-WPL-NC NEUSE REGIONAL WASA, NC WTP LIQUID 10/21/2014 / / - / / 0.6044
Na mg/I = (Na mg/kg x % Solids) _ 100 = (522 x 5.0700) _ 100 = 26.4654
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (1600 x 5.0700) t-100 = 81.12
Mg mg/1 = (mg mg/kg x % Solids) _ 100 = (756 x 5.0700) _ 100 = 38.3292
Na meq = Na mg/I t- Molec.Wgt.Na = 26.4654 _ 23 = 1.15067
Ca meq = Ca mg/I = Molec.Wgt.Ca = 81.12 _ 20 = 4.056
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 38.3292 = 12 = 3.1941
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.15067 _ SgrRoot[0.5(4.056+3.1941)] = 0.604357
•
Printed: 2/17/2015
Page 1 10:21

•
FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: NEUSE REGIONAL
SITE #: NC LN OOOX5 FIELD# : LN OOOX5 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: KALMIA
PERMIT #: WQ0034688 ANNUAL DRY TONS APPLIED: 72.67
OPERATOR: NEUSE REGIONAL CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 31.70 ACRES PERMITTED: 31.70
Page : 1
Lime Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/17/14
325,000.00 (G)
10252.366
3.18
1.360
NRWASA\
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
I BERMUDAGRASS
10/18/14
87,500.00 (G)
2760.252
3.18
0.366
NRWASA\
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
I BERMUDAGRASS
10/20/14
135,542.00 (G)
4275.773
3.18
0.567
NRWASA\
DRY
0-<1/2"
SUR
0.5
0.40
12,600.p
3,770.00 p
2.00 p
5419
BERMUDAGRASS
Oct-14
548,042.00 (G)
17,288.391
Total Gallons/Ac: 17,288.39
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
0.041
0.009
0.307
3.072
0.050
0.002
0.023
0.128
0.023
0.385 9.58
25
Cumulative lbs/acre
0.321
0.031
2.270
31.906
0.307
0.009
0.113
0.358
0.072
1.860�
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
.°,230
"
-
ra=k4 Ry
ad
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
TO
1339.0
267.9
15.0
�'
375.0
89.0
2500.0 �� �"�"
u
� _r
b.r
NRWASAWPL = NEUSE REGIONAL WASH, NC WTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

L
FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: NEUSE REGIONAL
SITE #: NC LN 000X5 FIELD# : LN 00OX5 0002
o Oo TTAT QnT TUnR/Q\•* Qan i;et at hnttnm of rP.nort
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: KALMIA
PERMIT #: W00034688 ANNUAL DRY TONS APPLIED: 27.55
OPERATOR: NEUSE REGIONAL CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 12.40 ACRES PERMITTED: 12.40
•
Page : 1
Lune Applied ***
Date
Lbs/Ac
o
��
Solids
o
��
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
nation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Total
Per Acre
3.18
3.18
1.331
0.890
NRWASAN
NRWASAN
I DRY
DRY
0-<1/2"
0-<1/2"
SUR
SUR
0.5
0.5
0.40
0.40
12,600. p
12,600. p
3,770.00 p
3,770.00 p
2.00 p
2.00 p
5419
1419
I BERMUDAGRASS
1 BERMUDAGRASS
10/9/14
10/10/14
Oct-14
124,477.00 (G)
83,250.00 (G)
207,727.00 (G)
10038.468
6713.710
16,752.178
Total Gallons/Ac: 16,752.18
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
24
Annuallbs/acre
0.040
0.009
0.298
2.977
0.049
0.002
0.022
0.124
0.022
0.373
9.29
0.058
1.505
Cumulativelbs/acre
0.249
0.022
1.855
33.797
0.255
0.007
0.088
0.281
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
"
�-
°H.,s' ✓fif",§;.s
ask-� c
'e<¢,zr„z
��''
? zs .%" „
,. ll
r.El= &,
r"�,r3 r�,
�. .^' to
,, et1,�4r
,
-�
a . aoF wn
y 'a ;Pik , hx'Lt. m
�' r�-• a- v 'tick.+�
ww. <<
iw r�;a:t `''€.#,�,°^;"
AN
BN
k "IMIWO
i, T" �'s y�,,,-
r"
a N
230
36.6
34.8EA
1339.0
267.9
15.0 , : 375.0
ri ..s.w
89.0 2500.0 1 ;t;; ,
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

•
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: NEUSE REGIONAL WASA, NC PREDOMINANT SOIL SERIES: KALMIA
OWNER: NEUSE REGIONAL PERMIT #: WQ0034688 ANNUAL DRY TONS APPLIED: 23.21
SITE #: NC LN OOOX5 FIELD# : LN OOOX5 0003 OPERATOR: NEUSE REGIONAL CATION EXCHANGE CAPACITY (NON ACRES UTILIZED: 9:40 ACRES PERMITTED:
MITTED: 9.40
RESIDUAL SOURCE(S):* See list at bottom of report
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
App1i-
Vola-
Miner -
or Wet Tons (WT) (specify)
o
��
Tons
Cond.
Precip.
cation
tili-
ali-
DATE or
Per Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
MONTH
Total Per Acre
Solids
10/18/14
75,000.00 (G) 7978.723
3.18
1.058 NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
10/20/14
100,000.00 (G) 10638.298
3.18
1.411 NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
Oct-14
175,000.00 (G) 18,617.021
Total Gallons/Ac: 18,617.02
As Cd Cr Cu Pb Hg
TOTALS:
Annuallbs/acre 0.044 0.010 0.331 3.308 0.054 0.002
Cumulative lbs/acre 0.379 1 0.033 1 2.778 47.793 1 0.377 0.011
Ammonia Nitrate
Nitrogen and
3,770.00 p 2.00 p
3,770.00 p 2.00 p
Mo Ni
0.025 0.138
0.131 0.397
•
Page: 1
Lime Applied
***
Date
Lbs/Ac
PAN
(Pprn) Crop
5419 I BERMUDAGRASS
5419 BERMUDAGRASS
Se Zn P PAN
27
0.025 0.415 10.32
0.082 2.213 ire;" ;, „ v;::ty '°
1st Crop/2nd Crop
k,
:-
��.
230
Permit PAN Limit (lbs/acre)
r
Loading Rate Limit (lbs/acre)
36.6
34.8re
1339.0
267.9
15.0 375.0
89.0
2500.0
#�06� i
FD Cumulative Pollutant
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

•
FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: J. W. ROBERTS
SITE #: NC LN 00OX7 FIELD# : LN 00OX7 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LUMBEE
PERMIT #: WQ0034688 ANNUAL DRY TONS APPLIED: 266.20
OPERATOR: J. W. ROBERTS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 63.00 ACRES PERMITTED: 63.00
•
Page : I
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/6/14
122,591.00 (G)
1945.889
3.18
0.258
NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
I WHEAT
10/7/14
377,382.00 (G)
5990.190
3.18
0.794
NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
1419
WHEAT
10/8/14
354,946.00 (G)
5634.063
3.18
0.747
NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
WHEAT
10/10/14
240,000.00 (G)
3809.524
3.18
0.505
NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
I WHEAT
10/11/14
270,000.00 (G)
4285.714
3.18
0.568
NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
I WHEAT
10/13/14
260,000.00 (G)
4126.984
3.18
0.547
NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
I WHEAT
10/14/14
292,500.00 (G)
4642.857
3.18
0.616
NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
WHEAT
10/15/14
90,000.00 (G)
1428.571
3.18
0.189
NRWASAN
DRY
0-<1/2"
SUR
0.5
0.40
12,600. p
3,770.00 p
2.00 p
5419
WHEAT
Oct-14
2,007,419.00 (G) 1
31,863.792

•
FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: J. W. ROBERTS
SITE #: NC LN 00OX7 FIELD# : LN 00OX7 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LUMBEE
PERMIT #: W00034688 ANNUAL DRY TONS APPLIED: 266.20
OPERATOR: J. W. ROBERTS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 63.00 ACRES PERMITTED: 63.00
0
Page : 2
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Gallons/Ac: 31,863.79
As
Cd
Cr
Cu
Pb
Hg
Mo,
Ni
Se
Zn P
PAN
TOTALS:
Amoral Ibs/acre
46
0.076
0.017
0.566
5.662
0.093
0.003
0.042
0.237
0.042
0.710 17.66
Cumulative Ibs/acre
0.218
0.034
2.025
32.100
0.251
0.008
0.099
0.361
0.089
1.562 [17�. w :V "s.
01
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
)
_
Mom.
&+fie �6�
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0-°� 375.0
89.0
2500.0
"Sri
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

Summit Environmental Technologies. Inc.
Summmrv- 3310 Win St.
P3VIR 3tdtll 1ai%L3E01:NC1L G4c`5, Mr, Cuyahoga Falls, Ohio 44223
rtl€tCrr/crpae#r7ts TEL: [phone] FAX. • [phone]
Website: ho.-Ilivww.settek.com
September 10, 2014
Will Varner
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: NRWasa
Dear Will Varner:
Order No.: 14082276
Summit Environmental Technologies, Inc. received 1 sample(s) on 8/22/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank)
3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099,
New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma
9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5,
Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West
Virginia 248 and 9957C and E87688, Wisconsin 399013010
Page 1 of 6
0

01VlRiCSPlMEWAL'YEC4Mtal13Glc.aS, INC.
tt.r alyticW
CLIENT: Synagro
Project: NRWasa
Lab SampleID Client Sample ID
14082276-001 NRWasa
C7
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX. [phone]
Wehsite: hW.1Avwiv.settelccon:
Tag No Date Collected
8/19/2014 1:30:00 PM
Workorder
Sample Summary
WO#: 14082276
Date Received
8/22/2014 10:00:00 AM
10-Sep-14
Matrix
Sludge
Page 2 of 6

y, Summit Environmental Technologies, Inc.
3310 Win St.
SUM&ANT Case Narrative
FP4tfIi{OtIfdGt4'r.ALT C14?40LOGIIES, MG- Cuyahoga Falls, Ohio 44223 WO#: 14082276
A;Talkti sl Laiwatode a TEL: [phone] FAX.- [phone]
Website: http://www.settek.com Date: 9/10/2014
CLIENT: Synagro
Project: NRWasa
This report in its entirety consists of the documents listed below. All documents contain the Summit
Envirorunental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
isOriginal
Page 3 of 6

Summit Environmental Technologies, Inc. WO#: 14082276
'm naw n 3310 Win St.
Ei3VIRONPAE14i'ALTi=CHtJOLOGIES,3I2C Cuyahoga Falls, Ohio44223 Date Reported: 9/10/2014
i Amilyticsl Laboratories TEL: [phone] FAX.- [phone] Company: Synagro
Website: htto:/Avww.settek.com Address: 284 Boger Rd.
Mocksville NC 27028
Received: 8/22/2014
Project#: NRWasa
TCLP Metals Analysis (6010)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
NRWasa
001
8/19/2014 TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
9/2/2014
WK
NRWasa
001
8/19/2014 TCLP Barium(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
9/2/2014
WK
NRWasa
001
8/19/2014 TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
9/2/2014
WK
NRWasa
001
8/19/2014 TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
9/2/2014
WK
NRWasa
001
8/19/2014 TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
9/2/2014
WK
NRWasa
001
8/19/2014 TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
9/2/2014
WK
NRWasa
001
8/19/2014 TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
9/2/2014
WK
TCLP Mercury Analysis (1311n470)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
NRWasa
001
8/19/2014 TCLP Mercury
0.0020
ND mg/L
Sludge
EPA 7470 A
1
0.20
9/2/2014
ALJ
SVOC
SW-846: 8081-TCLP
Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
NRWasa
001
8/19/2014 Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
9/2/2014
JBN
NRWasa
001
8/19/2014 Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
9/2/2014
JBN
NRWasa
001
8/19/2014 Enddn
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
9/2/2014
JBN
NRWasa
001
8/19/2014 gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
9/2/2014
JBN
NRWasa
001
8/19/2014 Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
9/2/2014
JBN
NRWasa
001
8/19/2014 Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
9/2/2014
JBN
NRWasa
001
8/19/2014 Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
9/2/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
NRWasa
001
8/19/2014 1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
8/27/2014
MES
NRWasa
001
8/19/2014 1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
8/27/2014
MES
NRWasa
001
8/19/2014 Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
8/27/2014
MES
NRWasa
001
8/19/2014 Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
8/27/2014
MES
NRWasa
001
8/19/2014 Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
8/27/2014
MES
NRWasa
001
8/19/2014 Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
8/27/2014
MES
NRWasa
001
8/19/2014 Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
8/27/2014
MES
NRWasa
001
8/19/2014 Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
8/27/2014
MES
NRWasa
001
8/19/2014 Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
8/27/2014
MES
NRWasa
001
8/19/2014 MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
8/27/2014
MES
Page 4 of 6

Summit Environmental Technologies, Inc. WO#: 14082276
3310 Win St.
ENVIRONMENTALTECHOOLO"e1y5; INC Cuyahoga Falls, Ohio 44223 Date Reported: 9/10/2014
n-aartical 1,abor orfe TEL: [phone] FAX.- [phone] Company: Synagro
Website: htto://Wwiv.settek.com
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 8/22/2014
Project#: NRWasa
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
NRWasa
001
8/19/2014 1,4.Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
9/4/2014
AKE
NRWasa
001
8/19/2014 2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
9/4/2014
AKE
NRWasa
001
8/19/2014 2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
9/4/2014
AKE
NRWasa
001
8/19/20,14 2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
9/4/2014
AKE
NRWasa
001
8/19/2014 Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
9/4/2014
AKE
NRWasa
001
8/19/2014 Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
9/4/2014
AKE
butadiene
NRWasa
001
8/19/2014 Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
9/4/2014
AKE
NRWasa
001
8/19/2014 Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
9/4/2014
AKE
NRWasa
001
8/19/2014 Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
9/4/2014
AKE
NRWasa
001
8/19/2014 Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
9/4/2014
AKE
NRWasa
001
8/19/2014 Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
9/4/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lint Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
NRWasa
001 8/19/2014 2,4-D
5.0 ND mg/L
Sludge
EPA 8321 A
1
10
9/9/2014
AMZ
NRWasa
001 8/19/2014 2,4,5-TP
0.50 ND mg/L
Sludge
EPA 8321 A
1
1.0
9/9/2014
AMZ
•
Page 5 of 6

i Summit Environmental Technologies, WO#• 14082276
. ,� �G 3310 Win St.
C aho a Falls, Ohio 44223 Date Reported: 9/10/2014
i E�131i't0�1FdEt�3ifii'3�Ct�Pdi�L+�t?i�S, INCu1' S
A ral rfrwt Lafio atodes TEL: [phone] FAX [phone] Company: Synagro
Website: http://ivlvw.settek.com
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 8/22/2014
Project#: NRWasa
Client ID#
Lab ID# Collected Analyte
Result Units
Matrix
Method
DF
RL Run
Analyst
NRWasa
001
8/19/2014
Flashpoint (140°F)
>200 °F
Sludge
EPA 1010
1
8/23/2014
TAH
NRWasa
001
8/19/2014
Cyanide, Reactive
ND ppm
Sludge
EPA 9014
1
0.50 8/26/2014
TIR
NRWasa
001
8/19/2014
pH
6.4 s.u.
Sludge
EPA 9045 D
1
8/23/2014
AYS
NRWasa
001
8/19/2014
Sulfide, Reactive
ND ppm
Sludge
EPA 9034
1
25 8/26/2014
TIR
is
Page 6 of 6

•
r
Summit
�nvpi.r.oialliental `FLehnololes, Inc.
33 3U di-wAnalysis C Lf% dlll r
Cif ixstotl�

•
Rev. 12
Date: 07/27/13
Sutftmit EnVironmental Technologies, Ific.
Cooler Receipt Forme
Initials, Of.Person inspecting cooler and samples.
Client, ' Order Number;
Date Rece;ved; •z Tlnifi ,Received. Date coolers) opened and samples inspected:
Number of CoolersBoxes: ( hI/A
Shipper: FED UPS, DHL Airborne US Postal Walk-in Pickup Other:
Packaging: Peanuts• , ubblelNrap Paper Foam None Other:
Tape on cooler/box: N NIA
Custody Seals Intact N WA
C-O-C in plastic N
NIA
Ice BIUe lee prey�kl/ absent / melted WA
Sample Temperature IR Gun #1 20 g CF 0 C 7 �c N/A
Rad{ological Tesfipg, instruinent,sei3ai a3. 5127 Y N
(see page:2; for scan: results)
•'Use 1,sheet.pecsariipl©'for,Ri- ogieatTesting. if sample, is HOT, the Radiologfeat Safety Officer must be notified
immirdlately.
C-O-C filled'out property, N WA
Samples in separate bags • N N/A
Sample oontainers`intact` N NIA
'If no, list broken_san*le(s):
Sample lab9l(s),c6mPlete-(Ib; date,4(4c;}
Label(s) agree with";C-O-C
Correct containers used
Suffic{erit sample received
Bubbles -Absent from 40 hit_, vials—
Y
Sampl+ s.wlth bubbles <gmm ar"acceptabto. Indicate bubble size if >6mm.
Was client contacted about "samples Y N
Will client send new samples Y N
Client contact:
Datemme:
Logged in by:
N
N
N
N
N
NIA
N/A
NIA
NIA
• G_ OC SHARED1Document Control Templates - Tracking\Cooler receipt form Rev. 12 07-27-13.doc Page 1 of 2

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Neuse Regional Water and Sewer Authority WQ Permit Number: WQ0034688
• WWTP Name: Neuse Regional Water Treatment Plant NPDES Number: NCO088111
Monitoring Period: From 01/01/14 To 3/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class A:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the followine monitorine data:
Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo. Mean Maximum Units dences Analysis
Fecal 2x10 to the 6` MPN MPN/g
Coliform power per gram
of total solids
No Land Application Occurred during this
monitoring period
Salmonella 3 MPN per 4 grams total
bacteria (in solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
Harold Herring, Executive Director NRWASA
Preparer Name and it type or print)
d d5r—
Signature of Preparer* 0 Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Neuse Regional Water and Sewer Authority WQ Permit Number: WQ0034688
WWTP Name: Neuse Regional Water Treatment Plant NPDES Number: NCO088111
isMonitoring Period: From 04/01/14 To 6/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class A:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If auplicable to alternative performed (Class A or Class B) comnlete the following monitorinn data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 1h
MPN
MPN/g
Coliform
power per gram
of total solids
No Land Application Occurred During this Monitoring
Period.
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Mt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Harold Herring,Executive Director NRWASA
• Preparer Na e and Titl (ty e r print)
Signature of Preparer* aD to
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Neuse Regional Water and Sewer Authority WQ Permit Number: WQ0034688
• WWTP Name: Neuse Regional Water Treatment Plant NPDES Number: NCO088111
Monitoring,Period: From 07/01/14 To 9/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class A:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization . Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6h
MPN
MPN/g
Coliform
power per gram
of total solids
No Land Application Occurred During this Monitoring
Period.
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) _
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Harold Herrine. Executive Director NRWASA
• Prepar ame and i (type or print) Land Applier Name and Title (if applicable) (type or print)
Si re of Preparer* aD tc Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

aceAnalytical
www.pacefabs.com
•
September 04, 2014
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: NRWASA
Pace Project No.: 92213999
Dear Marshall Puryear:
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Y
Jon D Bradley
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

aceAnalytical
4mw✓.pacelabs.com
Project: NRWASA
Pace Project No.: 92213999
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
•
CERTIFICATIONS
North Carolina Bioassay Certification M 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 11

aceAnalytical
www.pacelabs.com
•
Project: NRWASA
Pace Project No.: 92213999
Lab ID Sample ID
92213999001 NRWASA 1
92213999002 NRWASA 2
C7
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 11

aceAnalytical
www.pacelabs.com
•
Project: NRWASA
Pace Project No.: 92213999
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: NRWASA 1 Lab ID: 92213999001 Collected: 08/19/14 13:30 Received: 08/19/14 17:00 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 98.0 % 0.10 1 08/25/14 13:25
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 9.0 MPN/g 0.018 1 08/20/14 09:36 1g
•
Date: 09/04/2014 09:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 11

aceAnalytical
www.pacelabs.com
•
Project: NRWASA
Pace Project No.: 92213999
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NRWASA 2 Lab ID: 92213999002 Collected: 08/19/14 13:30 Received: 08/19/14 17:00 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.4 % 0.10 1 08/25/14 13:26
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 6.9 MPN/g 0.018 1 08/20/14 09:36 1g
•
Date: 09/04/2014 09:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 11

aceAnalytical0
www.pacelabs.com
QUALITY CONTROL DATA
Project: NRWASA
Pace Project No.: 92213999
QC Batch: PMST/6960 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92213999001, 92213999002
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE DUPLICATE: 1270837
92214091001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 26.1 25.0 4
SAMPLE DUPLICATE: 1270838
92214330001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 18.1 18.7 4
• Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/04/2014 09:31 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 11

aceAnalydcal
www.pacefabs.com
•
Project: NRWASA
Pace Project No.: 92213999
QUALITY CONTROL DATA
QC Batch: RBIO/4346 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92213999001, 92213999002
METHOD BLANK: 1268826 Matrix: Solid
Associated Lab Samples: 92213999001, 92213999002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 08/20/14 09:36
SAMPLE DUPLICATE: 1268826
92213999002 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 6.9 6.9 0 1g
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result.
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/04/2014 09:31 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 11

aceAnalytical
www.pacelaba.com
•
Project: NRWASA
Pace Project No.: 92213999
DEFINITIONS
QUALIFIERS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U _ Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/04/2014 09:31 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

acanalj4ical
www.pacelabs.c=
•
Project: NRWASA
Pace Project No.: 92213999
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92213999001
NRWASA 1
ASTM D2974-87
PMST/6960
92213999002
NRWASA 2
ASTM D2974-87
PMST/6960
92213999001
NRWASA 1
SM9221C E (MPN) 503
RBI0/4346
92213999002
NRWASA 2
SM9221 C E (MPN) 503
RBI0/4346
•
Date: 09/04/2014 09:31 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 11

•
�. Document Name: Sample Condition Upon Document Revised: April 04, 2u1S
Receipt SCUR Pa e 1 of2
/. ZwAnalytical' issuingAtlthorities:
Document No.: Pace Asheville Quality Office
F-RAL-CS-001-rev.02
Client Name: AA)
❑ Asheville Eden
Where Received: rsville Ashevlam( Raleigh
❑ Hunte_ ❑ Y
Courier (circle): • Fed Ex UPS USPS I(ent - Commercial Pace .Other
Custody Seal on Cooler/Box Present: ❑ yes Z no Seals intact 4 YQ5 ❑ no
Packing material: ❑ Bubble Wrap�1220!65387�y�
s gags None Other_` ss has begun
Circle Thermometer Used: IR Gun
of Ice: Wet Blue None ❑ Samples on Ice. cooling Prone
IR Gun eac 1�ps �' Date and lnttiels of pen on euamining
Temp Correction Factor: Add ! btract (� ` con P es ig° ,, +
cj C Biological Tissue is Frozen: Yas NA ehaelc "L i
Corrected CoolerTern Comments:
Temp. should be above freezing to e'C
Chain of Cnslo Present -----------------
ves ❑No ' C7wa 1.
Chain of CustodyFilled Out: Yes ❑No ❑NIA 2.
Chain of Custod Relinquished: Yea ❑No ❑NIA 3.
Sampler Name & Si nature on COG: Yes ON. ❑N1A 4.
Samples Arrived Vthin Hold Time: Yas ON.. Owa 5.
jpYOs ❑Iw ❑NIA 6. Ai
Containers Used: Aver ON. OwA
i
votume.received for Dissolved tests
Dyes ENO
WA 11.
Bred
Yes ONo
❑NIA 12.
triple labels match COC: .
Includes dateltimatID/Analysis Matrix:
containers needing preservation have been checked.
KY. ❑No
❑NrA 13.
containers needing preservation are found to be in
NYes ONO
///��_
❑WA
npiiance with EPA recernmendation.
epdana: VOA. Coidorm, TOC, DSG, 4VI-0RO (water}
Yes ONO
checked for dechlorination:
Yes ❑No
❑wA 14•
tmples
;adspace in VOA Vials (>6mm):
❑Yes ONs
NIA 15.
Oyes ON.
tvA 16.
ip Blank Present:
'
❑Yes 0N0
AwA
'ID Blank Custody Seals Present
Paco Tdp Blank Lot # (if purchased):
Field Data Required? Y / N
Client Notification/ Resolution: Date/Time:
Person Contacted:-
Commentsl Resolution:
Place label here
SCURF /SRF
Review:: OR ll
Nota: Whenever there is a discrepancy affecting North Carolina compliance Handwrite protenumber
COPY samples, a py of this form wr tempill be sent to the North Caro%na DEHmp protect number
no label available)
Certification Office (i,o out of hold. incorrect preservative, out o,
incorrect containers)
0
O
O

CHAIN -OF -CUSTODY I Analytical Request Document
ThnChahw-of-Cus" Is a LEGAL DOCUMENT. All ralovanifiolds must be cornplaiedacwratoy.
Section A Section B Section C
Page: of
Roquims! Client Informlion: Required PfO1001 Information: Invoice inllow
Company: Regan T.:J�A)) If Attention:
1838217
I L/a'#f C
Copy
To:
C—Pany N.M: REGO
' " ORCY
LATO;ky �,9
Address: r
NPDEs F GROUNDWATER f— DRINKING WATER
f— RCRA i OTHER
P—h—
Order No --
Were —UST
Project
Name.
pmF.Just
maeg.
"J"
Ieatjbn
Nctunfed DueDateaff; Project
Number.Sv
Section D MalftCodvs
R.Q.1.dCQW1.b—hM MATIux I coDP
COLLECTED
Pr9serveMs
vdml,.§ Water Dw
Water WT
ftst. Water
P'. 'p
SDIUSWd St.
Oil OL
:4;:
SAMPLE 10
VAN wp
Uj
(A-Z. "I.-) Air AR
9
.1
SOM0 Ns MUST BE UNIQUE Time TS
ON, OT
z
2
0 0-"
M1 Y
DATE
TIME
DATE
TIME
36M
'ZZ
3:
se
2
L
rr
Pace Project NoJ Lab I.D.
i.
nni
0 Z-
6.
4E;*
SAMPLE CONDITIONS
per/NY
14a&
RN."SAMPLER SIGNATURE',
I .
I .
ORIGINAL
PRWN—cfSAMPLIEF1c Well
DATE Signed
E
SIGNATURE of SAMPLER: �75S?? 1 2r2:�� M_L
I (MDDNY): _/9 //
'1r`TM2" N-1 RY NOPLIP �. Is -re me —Pwg Pe' . I NET 30 dbY p.y-1 wne,a and Bgretinj w loto chs" or 1.6% w r—In fo—y wdses = =:d %Mlft 30 days. F-ALL-Q-D20r0v.O7. 15-May-2U131

aceAnalytical
wmpacelabs.c=
I
•
September 23, 2014
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: NRWASA 9/17
Pace Project No.: 92217843
Dear Marshall Puryear:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 17, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Y
Jon D Bradley
[e-mail]
Project Manager
Enclosures
• a��AC�F
9e�RA.lp�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

aceAnalj6cal
www.paceWs.com
I
•
L
Project: NRWASA 9117
Pace Project No.: 92217843
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification M 12
South Carolina Certification #: 99006001
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 11

(:�;a'neAnalyficale
www.pacelabs.com
•
Project: NRWASA 9/17
Pace Project No.: 92217843
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92217843001 NRWASA1 ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92217843002 NRWASA2 ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 11

(�IacieAnalyfica(
www.pacelabs.com
•
Project: NRWASA 9/17
Pace Project No.: 92217843
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: NRWASA1 Lab ID: 92217843001 Collected: 09/17/14 11:00 Received: 09/17/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.0 % 0.10 1 09/23/14 13:55
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 7.4 MPN/g 0.018 1 09/18/14 08:31 1g
•
Date: 09/23/2014 10:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 11

(�IacieAnalXical"
www.pacelabs.com
•
Project: NRWASA 9/17
Pace Project No.: 92217843
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: NRWASA2 Lab ID: 92217843002 Collected: 09/17/14 11:00 Received: 09/17/14 15:05 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 97.0 % 0.10 1 09/23/14 13:55
92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 7.4 MPN/g 0.018 1 09/18/14 08:31 1g
•
Date: 09/23/2014 10:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 11

acmnalytical
www.pacelabs.com
•
Project: NRWASA 9/17
Pace Project No.: 92217843
QC Batch: PMST/7048
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92217843001, 92217843002
SAMPLE DUPLICATE: 1290178
Parameter Units
Percent Moisture %
SAMPLE DUPLICATE: 1290179
Parameter Units
Percent Moisture %
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92217472001 Dup
Result Result RPD Qualifiers
79.7 79.3 1
92217886001 Dup
Result Result RPD Qualifiers
73.1 73.4 0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/23/2014 10:24 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 11

aceAnalytical
www.pacelabs.com
•
Project: NRWASA9/17
Pace Project No.: 92217843
QUALITY CONTROL DATA
QC Batch: RBIO/4419 Analysis Method: SM9221 C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92217843001, 92217843002
METHOD BLANK: 1287976 Matrix: Solid
Associated Lab Samples: 92217843001, 92217843002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 09/18/14 08:31
SAMPLE DUPLICATE: 1287977
92217843002 Dup
Parameter Units Result Result
Fecal Coliforms, MPN MPN/g 7.4 7.4
RPD Qualifiers
0 1g
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/23/2014 10:24 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 11

aceAnalXical
www.pacefabs.com
•
Project: NRWASA 9/17
Pace Project No.: 92217843
DEFINITIONS
QUALIFIERS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/23/2014 10:24 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

aceAnalj&al
www.pacelabs.com
•
Project: NRWASA 9117
Pace Project No.: 92217843
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92217843001
NRWASA1
ASTM D2974-87
PMST/7048
92217843002
NRWASA2
ASTM D2974-87
PMST/7048
92217843001
NRWASA7
SM9221C E (MPN) 503
R121I0/4419
92217843002
NRWASA2
SM9221C E (MPN) 503
RBI0/4419
;7
Date: 09/23/2014 10:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 9 of 11

•
Document Name: Sample Condition Upon Document Revised: April 04, 2013
Receipt SCUR Pa e 1 of 2
aC8r4r1aiytTcal fssuing Auihor+>ies:
z a Document No,:
F-RAL-CS-001-rev.02 Pace Asheville Qua[it Office
Client dame:_grro
Where Received: [j Huntersville ❑ Ashe ' ❑ Eden Raleigh
courier (Circle): Fed Ex UPS, LISPS lie Commercial Pace . Other
Custody Seaton CooledBox Present: [] yes no Seats intact: �YeS ❑ no
Packing Material: ❑ Bubble Wrap ❑ Bubble gs None Other
Clrcio Thermometer used: IR Gun SN:12206 3�8�7% ff o"`f ice: Blue None ❑ $amptes on ice, cooling prooesshas begun
IR Gun Bee SN:122-lIWT1
� Date ancttials iniai parson examining
Temp Correction FaQtor: Add 1 S t content 1 P ery
Corrected CaalerTemp.: C Biological Tissue Is Frozen; Yes tb Nt check: `t
��.
Temp.should be above trOwng.ro o,Ll
-
Chdln of Custody Present:
OYes ONO
ONiA
1.
Chain of Custod Filled Out
Yes ONO,
ONIA
2. '
Chain of Custody Relinquished:
Yes Ciro
OritA
3.
Sampler Name & Si nature on COC:
Yes LINO
OwA
C .
Samples Arrived within Hold Time:
UfYea ONO
ONIA
S.
Short Hold Tune Artai sis 472hr :
Yes ONO
ONIA
B. L`a
Rush Turn Aroundl7lme Requested-.
OYes
OWA
7.
Sufftolent Volume:
Yes ONO
OIViA
8.
Corract Containers UserL'
Yes ONc
ON►A
g.
-Pace Containers Used:
Yes ONO
QVA
Containers Intact
es ONO
❑NA
in
Flitered votume•recelved for Dissolved tests
17Yes ONO
gWA
11,
Sample Labels match CAC:
,PJYes ORO
ONiA.
12.
-includes dateAlme1lD/Ariai sis Matrix
All Gontalners needing preservation heVa been checked.
[3No
ONIA
13.
AiI contahters needing preservation are found to be In
veS QNo
011
compliance with EPAreoammendation.
!�
empMns: VOA, roefama, TOO, OM WI•DRO weber
AY —Gs ONO
Sampler. checked for dechtorination:
OYw ONO
Mile
14.
Heads a in VOA Vlals ?6mm :
CIYss ON*
NiA
15.
Trip Blank Present:
Mee ONO Ia,.
i6.
OYes ONo NlA
Trip Blank Custody Seals Present
Face Trip Blank Lot# if purchased
Client Notificatloaf Resolution: Field Data R qu[red? Y I N
Person Contacted: Daterrime: -
Commentsl Resolution:
SCURF ISRF ��, Date:
Review::
Note: Whenever there is a discrepancy affecting North Carolina compliance
• samples, a copy of this form will be sent to the North Carolina DEHNR
Cartiftoation•Office f [.e out of hold, incorrect preservative, out of temp,
incorrect containers)
Page 10 of 11

C ` J
"Analytical
E701 Conference Drive, Raleigh, NC 27607
ph: [phone], fax: (918) SM-SW
NCWW'CerW7, NCDW Cert#37731
Report Results To:
Company:
Address:
Chain of Custody
Attn: J;( 11,zle4 ir"
Phonef:37.C— 519 9,1, 7
Fax: lea i'neriis �de�Pr�
Sampled by (signature):
Bill To:
W.O. #
Project Reference: / ' ` L/" I,
Project Number:
Purchase Order #:
❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
**Aueh proleCm are subteotto priorapprovat by
the laboratory
Requested Due Date:
Reiette by (s► tuns)
R by (signature)
Date
Time
Relinquished by (signature)
RMidbyAri0of
Daze
Time
Relinquished by (signature)
Received by (signature)
Date
Time
Receipt Conditions (Lab Use Only)
❑ 4*00 ❑ Temp: °C
Res- Chlorine:
❑ Absent ❑ Present ❑ Na
Acid preserv. c2?
❑ Yes 0 No ❑ n1a
Base preserv. >12? '
❑ Yes ❑ No ❑ nla
Page 11 of 11

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Neuse Regional Water and Sewer Authority WQ Permit Number: WQ0034688
• WWTP Name: Neuse Regional Water Treatment Plant NPDES Number: NCO088111
Monitoring Period: From 10/01/14 To 12/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class A:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
U annlienhle to alternative nerfnrmed !f lacc A nr Clacc Rl rmmn1a4a *hn fnllnwina mnnitnrina dla4a-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6b
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
4.3
4.3
4.3
MPN/g
0
Quarterly
Grab
SM9221C
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement In 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Harold Herring, Executive Director NRWASA _
• Prepare ame Ti (type or print)
Signature of Preparer* batj
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

aceAnalytical
www.pacelabs.corn
October 10, 2014
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: NR Wasa 10/6
Pace Project No.: 92220161
Dear Marshall Puryear:
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 07, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

acmnalytical
www.pacefabscom
I
•
Project: NR Wasa 10/6
Pace Project No.: 92220161
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
•
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification M 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 11

,(�Iace
Analytical"
www.pacelabs.com
Project: NR Wasa 1016
Pace Project No.: 92220161
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92220161001 NRWASA1
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92220161002 NRWASA2
ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 11

Pace Analytical Services, Inc.
aceAnalyiical ® 9800 Kincey Ave. Suite100
Huntersville, NC 26078078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: NR Wasa 10/6
Pace Project No.: 92220161
Sample: NRWASA1 Lab ID: 92220161001 Collected: 10/06/14 17:00 Received: 10/07/14 09:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 94.5 % 0.10 1 10/10/14 13:19
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 3.3 MPN/g 0.018 1 10/07/14 10:07 1g
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/10/2014 06:23 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11

aceaAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: NR Wasa 10/6
Pace Project No.: 92220161
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NRWASA2 Lab ID: 92220161002 Collected: 10/06/14 17:00 Received: 10/07/14 09:40 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 95.2 % 0.10 1 10/10/14 13:19
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 3.7 MPN/g 0.018 1 10/07/14 10:07 1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/10/2014 06:23 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11

amAnalytical
www.pacalabs.c=
f
•
Project: NR Wasa 10/6
Pace Project No.: 92220161
QC Batch: PMST/7113
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92220161001, 92220161002
SAMPLE DUPLICATE: 1303658
Parameter Units
Percent Moisture %
SAMPLE DUPLICATE: 1303659
Parameter Units
Percent Moisture %
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92220129002 Dup
Result Result RPD Qualifiers
5.5 4.7 15
92220550002 Dup
Result Result
93.1 93.1
RPD Qualifiers
0
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/10/2014 06:23 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 11

5ceAna1j&a1
www.pacelabs.com
•
Project: NR Wasa 10/6
Pace Project No.: 92220161
QUALITY CONTROL DATA
QC Batch: RBIO/4436 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92220161001, 92220161002
METHOD BLANK: 1301868 Matrix: Solid
Associated Lab Samples: 92220161001, 92220161002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 10/07/14 10:07
SAMPLE DUPLICATE: 1301869
Parameter
Fecal Coliforms, MPN
92220161002 Dup
Units Result Result
MPN/g 3.7 3.7
RPD Qualifiers
0 1g
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/10/2014 06:23 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 11

Pace Analytical Services, Inc.
Kincey Ave.
acte 100
eAnalytical ® 9800Huntersv le, NC128078
www.pacelabs.com
[phone]
I
• QUALIFIERS
Project: NR Wasa 10/6
Pace Project No.: 92220161
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
is
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/10/2014 06:23 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

(�IacieAnalytical
www.pacelabs.com
•
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
NR Wasa 10/6
92220161
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92220161001
NRWASA1
ASTM D2974-87
PMST/7113
92220161002
NRWASA2
ASTM D2974-87
PMST/7113
92220161001
NRWASA1
SM9221C E (MPN) 503
RBI0/4436
92220161002
NRWASA2
SM9221C E (MPN) 503
RBI0/4436
•
Date: 10/10/2014 06:23 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9of11

aceAnalytical
ujww.pace labs.rom
6701 Conference Drive, Raleigh, NC 27607
ph: (919) 8344984, fax: (919) 83 -M7
NCWW CedM7. NCDW Cert#37731
Report Results To:
Company: '��e4 ;j e5:a
Address:
Chain of Custody
Bill To:
W.O. #
Project Reference: `r' eI/,-`�e,
Attn: U!
Phone: 3A S tl ro
Fax
Sampled by (signature):
^�,
/
p,
Project Number: GI_�?�, f •.
Purchase Order #:
0 Standard Report Delivery
D Rush Report Delivery (w/surcharge)
"Rush projects are subject to prior approval by
the laboratory
Requested Due Date:
I.i_ �,i
(/l/
G----------------
Retinqu b (Signatur
Relinquished by (signature)
Relinquished by (signature)
Received by re)
Revived by (signature
Received by (signature)
pg� T�e Receipt Conditions ( Use
'� ( ❑ 4t2'C D Temp:
t)a<e Tune Res. Chlorine:
D Absent p Present p n
Acid presery <2?
Date Tirrte D Yes ❑ No D n!a
68SB preserv.>i2?
Yes DR pn/a
Page 10 of 11

r�
I',,�CeAnalY C81 '
a V-1. nco[OOs eom
Document Name:
Document No,:
Document
1 of 2
Issuing Authorities:
AthAY111A Mallty Office
Client Name:
Where Received: ❑ Huntersvilie ❑ Asheville E] I Eden Raleigh
Courier (Circle): - Fed Ex UPS USPS Hent Commercial Pece . Other
Custody Seal on CooleriSox Present: 0 yes no Seals intact: 0 yes ❑ no
Packing Material• ❑ Bubble Wrap ❑ Bubble Bags F) None Other_-
Circle Thermometer Used: IR Gun 220653t)7T a of Ice. we Blue None [] Samples an toe, cooling process has begun
te and Inttlals of person exam n ng
Temp Correction Factor: Add! btract
C
cc t ff s Paso rat o
Corrected Cooler Temp.: C
Biological Tissue
is Frozen: Yes hb NIA
[:.check:
Temp should be above freezing to VG
Comments:
Chain of Custody Present:
Yes ONO
13WA 1.
Chain of Custody Filled Out
Ayes ONO
QNIA
2.
Chain of Custody Relinquished:
Aye. ❑No
❑MA
3.
Sampler Name & Signature on COG:
Yes ONO
❑wA
4.
Samples Arrived within Hold Time:
byes ONO
OwA
5.
short Hold Time Analysls' <72hr :
Yes DNo
❑NIA
6.
Rush Turn Around Time fie nested:
Dyes VNo
t'NIA
7.
Sufficient Volume:
Yes DNo
❑NIA
8.
Correct Containers Used:
oyes ONO
❑wA
8. '
-Pace Containers Used:
s ❑No
❑NIA
Containers Intact:
Yes ONO
❑NIA
10.
Filtered volume-recelved for Dissolved tests
Oves ONO
A
11.
Sample Labels match COC:
plas NO
0MA
12.
-Includes dateltimbilDlAnalysis Matrix:
Ail oontainers needing preservation have been checked.
11yes DNo
OWA
13.
All Containers needing preservation are found to be in
�es ONO
CINIA
compliance with EPA recommendation.
exceptlorm VOA, conform, TOG, oaq, WI.ORO (water)
�i es ONO
Samples checked for dechtorination:
6ye4 ONO
❑WA
14.
Heads ace in VOA Vials (>6mm):
Dyes OM
NIA
15.
Trip Blank Present:
Oyes ONO
VWA
16.
Trip Blank Custody Seats Present
Oyes ONO
I�NIA
f(
Pacs Trip_Blank Lot # If purchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted; DatelTime:
Comments! Resolution:
SCURF-1811F Date; L2/n_/1
y
Review::
Note: Whenever there Is a discrepancy affeoling North Carolina complianCO
• samples, a copy of this form will be sent to the North Carolina DEHNR
Certification•Office (i.e outof hold, incorrect preservative, out of temp,
incorrect containers)
Page 11 of 11

acmna/Xical
www.pacetabs.com
•
October 24, 2014
Marshall Puryear
Synagro Technologies, Inc.
284 Boger Rd
Mocksville, NC 27028
RE: Project: NR WASA 10/20
Pace Project No.: 92222179
Dear Marshall Puryear:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
G� - -
Chris Derouen
[e-mail]
Project Manager
Enclosures
• SRC.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

axAnalytical
www.pacelabscom
Project: NR WASA 10/20
Pace Project No.: 92222179
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
.7
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification M 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification M 84
West Virginia Certification M 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 11

aceAnalXical
www.pacefabs.com
•
Project: NR WASA 10/20
Pace Project No.: 92222179
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92222179001 NRWASA 1 ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
92222179002 NRWASA 2 ASTM D2974-87
ACS
1
PASI-C
SM9221C E (MPN) 503
JW1
1
PASI-R
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 11

acmnalytical
www.pacelabs.com
•
Project: NR WASA 10/20
Pace Project No.: 92222179
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NRWASA 1 Lab ID: 92222179001 Collected: 10/20/14 16:30 Received: 10/21/14 11:55 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 95.8 % 0.10 1 10/24/14 13:05
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 4.3 MPN/g 0.018 1 10/20/14 12:41 1g
•
Date: 10/24/2014 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 11

aceAnalytical
www.pacelabs.com
•
Project: NR WASA 10/20
Pace Project No.: 92222179
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NRWASA 2 Lab ID: 92222179002 Collected: 10/20/14 16:20 Received: 10/21/14 11:55 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 95.8 % 0.10 1 10/24/14 13:05
92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503
Fecal Coliforms, MPN 4.3 MPN/g 0.018 1 10/20/14 12:41 1g
C,
Date: 10/24/2014 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 11

(�IacieAnalyticalo
www.pacelabs.com
•
Project: NR WASA 10/20
Pace Project No.: 92222179
QUALITY CONTROL DATA
QC Batch: PMST/7161 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92222179001, 92222179002
SAMPLE DUPLICATE: 1313713
92222341001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 28.6 27.9 3
SAMPLE DUPLICATE: 1313714
92222502001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 22.8 22.9 0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2014 05:47 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 11

aceAnalytical
www.pacefabs.com
•
Project: NR WASA 10/20
Pace Project No.: 92222179
QUALITY CONTROL DATA
QC Batch: RBIO/4471 Analysis Method: SM9221C E (MPN) 503
QC Batch Method: SM9221C E (MPN) 503 Analysis Description: 92210E Fecal Coliform, MPN Solid
Associated Lab Samples: 92222179001, 92222179002
METHOD BLANK: 1311621 Matrix: Solid
Associated Lab Samples: 92222179001, 92222179002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms, MPN MPN/g ND 0.018 10/20/14 12:41
SAMPLE DUPLICATE: 1311622
92222179001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms, MPN MPN/g 4.3 4.3 0 1g
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the resu
• lt
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2014 05:47 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 11

Pace Analytical Services, Inc.
(�Iacmn
9800 Kincey Ave. Suite 100
alytical Huntersville, NC 28078
www.pacelabs.com [phone]
• QUALIFIERS
Project: NR WASA 10/20
Pace Project No.: 92222179
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value.
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2014 05:47 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

aceAnalytical
www.pacelabs.com
•
Project: NR WASA 10/20
Pace Project No.: 92222179
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92222179001
NRWASA 1
ASTM D2974-87
PMST/7161
92222179002
NRWASA 2
ASTM D2974-87
PMST/7161
92222179001
NRWASA 1
SM9221C E (MPN) 503
RBI0/4471
92222179002
NRWASA 2
SM9221C E (MPN) 503
RBIO/4471
Date: 10/24/2014 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 9 of 11

an
eAnalj4 cal
www.pacefabs.com
6701 Conference Drive, Raleigh, NC 27607
ph: [phone], fax: (919) 834-sw
NCWW Ced#67, fQCOWQq"p.77,31 .... .
Report Results To:
Company: TS/a4 i/-0
Address:
Phone: _'_1_yL�
Fax: E.% U� Y-,eJ0,
Sampled by (signature}: ��
Chain of Custody
W.O. #
Sill To:
Project Reference:
Project Number:
Purchase Order #:
❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
"Rush projects are subject to prior approval by
the laboratory
Requested Due Date:
Reli ish by signature)
Relinquished by (signature)
'Relinquished
R by (signa
Date
Tune
ived n ure)
Date
Time
by (signature)
Received by (signature)
Date
Time
Receipt Conditions (Lan use vnry)
❑ 4t290 ❑ Temp: °C
Res. Chlorine:
❑ Absent ❑ Present ❑ We
Acid preserv. <2?
❑Yes ❑No ❑rda
Base preserv.>12?
❑Yes ❑No ❑Na
Page 10 of 11

•
Document Name: Sample Condition Upon Document Revised: April 04; 2013
Rept SCUR Page 1 of 2
PaceRnalyiicalN Issuing Authorities:
i'y ,.pacotnnw com Document No.:
i F-RAL-CS-001-rev.02 Pace Asheville Qualit Office
Client Name:_ •
Where Received: - E] Huntersville E]
Ashevil a
Eden. Raleigh- -... ... . -- .-
Courier (Circle): Fed Ex UPS USPS
G
Commercial Pam . Other _
Custody Seal on Cooler/Box Present: [] yes
0
Ss Intact: [yes (] no
Seals
" Packing Material: E] Babble Wrap eubbl s None F1 Other
Circle Thermometer Used: III Gun SN:1220(i 87 a of Ice: et Blue None J [] Samples on lce, cooling process has begun
IRGunwo SN:1220 371
tr n C
Add 1 S ty
Date and initials of person examining
I P servati����
Temp Correction Factor:
� contents
Tissue is Frozen: Yes No N1
Corrected CoolerTemp: _ �y� C
Biological
check:
Temp should be above freezing to VC
Comments:
Chain of Custody Present:
Yes EiNo
❑NIA 1. - -
Chain of Custod Filled Out
0yes ❑Na
❑NIA 2.
Chain of Custody Relingltished:
es ❑Nd
OwA 3.
Sampler Name & Signature on CDC:
yes ON.
❑wA 4.
samples Arrived within Hold Time:
6yes ❑No
❑wA 5.
Short Hold Time Analysls-(Q2hr):
yes ONO
❑NlA 6. A -
Rush Turn Around Time Requested:
❑Yes No
OwA 7.
Sufficient Volume:
es ONO
❑NIA 8.
Correct Containers Used:
Ayes ONO
❑NIA 9.
-Pace Containers Used:
oYes ONO
❑wA
Containers Intact:
es ONo
OwA. 10,
Filtered volume -received for -Dissolved tests
Oyes ONO
a 11
Sample Labels match COG:
Yes Onto
11wA 12.
-includes dateltimellDlAnalysis Matrix:
Z_
All containers needing preservation have been checked.
ONO
❑wA 13.
All containers needing preservation are found to be in
Afss ONO
'�
❑wA
compliance with EPA recommendation.
l
exceptions: O k, oo,ifornt, TOC, O&G, WIARO (water)
es ❑No
'
Samples checked for dechlorination:
Cayes ❑No
wA 44.
Heads ace In VOA Vlats >6mm :
Dyes ONO
NIA 15.
❑Yes ONO
C4WA 1ti.
Trip Blank Present
Trip Blank Custody Seals Present Oyes ❑NoNiA
Pace Ap Bienk Lot # (If purchased):
Field Data Required? y I N
Client Notification? Resolution:
Person Contacted:, Dateffime:
Comments! Resolution:
SCURF ISRF C Date: �/O�Iki+►>ii'to�!�utG�OG�r:.`.rir��w► g �;. ,,;=:x- ; t- 7fry".,
Review:: ;.+:,=:,,s`
T''.z£'ri'a=w�yiM1'•j
Note: Whenever there is a discrepancy affecting North Carol(na cornpilance:_}___ • , t ,.,.;. ,;
samples, a copy of this form will be sent to the North Camilna DEHNR �d)i 3 n i='
,.
x V
Certification Office ( i.e out of hold, incorrect preservative, out of temp.321
incorrect containers)_ --
Page 11 of 11

Agricultural Lime Application Log
Year: 2014
Project: Neuse Regional WASA
Field IE:Soil
(state -county -site -field)
NC-LN-5-1
pH
6.2
Lime Requirement
(tons/acre)
0.0
Tons/Acre
Applied
0.0
Date Applied
NC-LN-5-2
6.4
0.0
0.0
NC-LN-5-3
5.8
0.8
NC-LN-7-1
6.0
0.0
0.0
*Lime will be spread when field conditions improve

Page 1 of �
Report Num er: 14-316-0684 99
Account Number: 00454
Send To: SYNAGRO CENTRAL LLC/NEUSE REGnieastern.com
MARSHALLPURYEAR
284 BOGER RD
STE 204
MOCKSVILLE NC 27028
Date Received: 11/12/2014 Date Of Analysis: 11/13/2014
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower:
NEUSE REG WASA
SOIL ANALYSIS REPORT
Date Of Report: 11/13/2014
Submitted By: WILLVARNER
Farm ID:
Analytical Method(s):
Mehlich 3
a.-
Orga_ n(c-Matter"
Phosphorus
^„ .Y `:
, .
;:Potassium
Magnesium;
`
" Caict6iri'
, "
. .Sodium
pH -
Acidity
C.E."C
Sample ID
ID
Lab
Number
ENR
M®Mich 3
Reseore
K
M g
Na
Soil
Buffer
H .
Field
% Rate
itis%A "
ppm" Rate
RateK
ppm Rate
"Rpm
Rafe
,.
;ppm Rate
PH
Index
megt1t14g
megl1,OOg
.ppm A
"pPm
•,:Rate.="
LN-7-1
14772
2.3 L 90
162 VH
150 VH
97
H
456
M
15
VL
6.0
0.6
4.2
NC=135
NC=77
LN-5-1
14773
5.2 H 145
110 VH
111 M
118
H
825
M
17
VL
6.2
0.8
E
NC=92
NC=57
LN-5-2
14774
3.1 M 103
88 H
106 M
196
M
1961
H
118
VL
6.4
1
0.6
6.5
NC=73
NC=54
LN-5-3
14775
3.6 M 116
114 H
88 M
184
H
497
M
115
VL
5.8
6.85
0.8
4.3
NC=70
NC=45
Percent
Base Saturation
Nitrate
Sulfur".
Zinc
Manganese
Iron
Copper
Boron
Soluble
Salts,
Chloride
Aluminum
Sample iD
K
Mg
Ca
Na
H
NQ3N
S
Zn
Mn
Fe
i Cu
B
SS
Cl
AI
Field ID
%
%
%
%
%
ppm Rate
ppm Rate:
�pprri Rate
ppm Rate
ppm Rate,
ppm Rate
"ppm
Rate
ms/cm Rate
ppm Rate
ppm
LN-7-1
23 M
4.0 H
12 M
147 VH
8.1 VH
0.2
VL
0.12
VL
9.2
19.2
54.3
1.6
15.3
NC=48
NC=100.0
NC=75
NC=405.0
LN-5-1
36 VH
5.1 H
M
202 VH
19.9 VH
0.3
VL
0.08
VL
4.6
15.9
66.5
1.2
12.2
NC = 75
NC = 127.5
118
NC = 113
NC = 995.0
LN-5-2
M
L
15 M
150 VH
VH
VL
0.11
VL
4.2
12.3
73.9
1.2
9.0
121NC=44
12.1
NC=52.5
NC=94
17.0
NC=350.0
10.2
LN-5-3
VH
M
16 M
VH
12.9 VH
VL
VL
5.2
16.3
57.8
1.5
19.0
137
NC = 77
13.4
NC = 85.0
NC = 100
1182
NC = 645.0
10.2
10.07
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing, by: Pam•« or 60wr
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

Page 2 of 0
Report Number: 14-316-0684
Rk
Account Number: 00454
0
wivwaleastern,com
Send To: SYNAGRO CENTRAL LLC/NEUSE REG'
MARSHALLPURYEAR
284 BOGER RD
STE 204
MOCKSVILLE NC 27028
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 (804) 743.Ml Fax (804) 271.W6
Grower:
NEUSE REG WASA
Date Received: 11/12/2014
r% 4-- Af Deng+• 41l11V9n1A SOIL FERTILITY RECOMMENDATIONS
Submitted By: WILL VARNER
Farm ID:
a-
1
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crap performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1�O
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary