WQ0032618_Residual Annual Report 2014_20150302

AJINOMOTO
2014 ANNUAL LAND APPLICATION OF
RESIDUAL BIO-SOLIDS REPORT
"CLASS A" RESIDUALS PROGRAM
WQ0032618
Submitted by:
Soil Plus
208 Williams Street
Greenville, North Carolina 27858
February 1, 2015
RECEIVEDiDENDIfiR
MAR r % 2015
�Ngteraudletv
p®PFfiifing $®C$@®n

S co At ;ems
-.
t..
208 Williams Street
Greenville, NC 27858
t [phone]
f [phone]
www.soilplus.net
February 1, 2015
NCDENR-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2014 LAND APPLICATION ANNUAL REPORT
Ajinomoto "Class A" Residuals Management Program
NC Permit No.: WQ0032618
Soil Plus Project No. 200902.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for Ajinomoto Amino Science, LLC (Ajinomoto).
Soil Plus compiled this report using data gathered during the compliance year. This data
includes (1) a certification form, (2) distribution & marketing summary form, & (3) residual
sampling summary.
Ajinomoto prepared and land applied approximately. 788,625 gallons or 368.36 dry tons of
"Class A" Residual Bio-solids (Cell Cream) during 2014. The residual bio-solids were
distributed to farms in Nash, Wake, and Johnston Counties for agricultural uses.
Approximately 5,727 wet tons or approximately 859 dry tons of Residual Bio-solids
produced from Ajinomoto's Wastewater Treatment Plant were taken to 'a private
composting facility for further processing.
If there is any further information required or questions regarding this annualreport please
do not hesitate to contact me or the Ajinomoto (252-723-2141) for further assistance.
Respectfully,
C. Scott Carpenter, L.S.S.
North Carolina Nutrient Management Planner
Kevin Adams, Ajinomoto
Jason Smith, Granville Farms

Ajinomoto 2014
Annual "Class A"
Residuals
Management
Report
WQ0032618
Raleigh, NC
ANNUAL LAND
APPLICATION
CERTIFICATION FORM
AJINOMOTO CAKE
ANNUAL RESIUDAL
SAMPILING SUMMARY
FORM
Nutrients
503 Metals
TCLP
AJINOMOTO CELL CREAM
ANNUAL RESIUDAL
SAMPILING SUMMARY
FORM
Nutrients
503 Metals
TCLP
DISTRIBUTION AND
MARKETING SUMMARY
FORM

APPENDIX 'I
CERTIFICATION FORM
SUMMARY FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0032618 Ajinomoto Amino Science, LLC Kevin Adams Wake [phone]
Year: 2014
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the 0
residuals were handled.
Part A -Residuals Application Summary:
Total number of application fields in the permit: NA
Total number of fields utilized for land application during the year: NA
Total amount of dry tons applied during the year for all application sites: 370.92
Total number of acres utilizes for land application during the year: NA
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality❑ ❑O
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
'5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
zertified laboratory results are attached
5.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated
;Facilities).
3. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated
kacilities).
). All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
nclude appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
'Part C - Certification:
'I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
mprisonment for knowing violations."
. nermitt , e nd Title (type or print):
Z
3igna re of Preparer* Date
;if different from Permittee)
Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Signature of Permittee
Signature of Land Applier Date
(if different from Permittee)
Friday, January 30, 2015

Source Summary Report
WWIP� VolumeApplied Measurement Total Dry _Tons
Ajinomoto Cell Cream- 778,625 Gallons 368.36 _
Total
368.36
Monday, February 2, 2015
Page 1 of 1

APPENDIX II
CAKE RESIDUAL SAMPLING SUMMARY FORM
ANALYTICAL

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0032618 Facility Name Ajinomoto Amino Science, LLC Source Permit No. AJIN
Laboratory 1
Laboratory 2
Laboratory 3
Sample Date Class A Clas B
A&L Eastern Labs,
A&L Eastern Labs,
A&L Eastern Labs,
A&L Eastern Labs,
3/13/2014
6/13/2014
9/4/2014
12/10/2014
Aluminum
N/A
N/A
1,300
200
1,100
500
Ammonia Nitrogen
N/A
N/A
3,570
3,560
3,110
3,990
Arsenic
41
75
3
3
3
3
Cadmium
39
85
2
2
2
2
Calcium
N/A
N/A
2,560
3,160
3,140
3,070
Copper
1,500
4,300
9
33
59
17
Lead
300
840
5
5
5
5
Magnesium
N/A
N/A
2,270
1,870
1,890
1,090
Mercury
17
57
0.4
0.4
0.4
0.4
Molybdenum
N/A
75
5
5
5
5
Nickel
420
420
5
6
5
5
Nitrate -Nitrite Nitrogen
N/A
N/A
9
24
2
15
Percent Solids
N/A
N/A
12.33
13.49
14.45
13.29
pH (no units)
N/A
N/A
7.63
7.77
8.21
7.60
Phosphorus
N/A
N/A
13,400
10,700
10,700
8,000
Potassium
N/A
N/A
9,230
8,930
6,860
8,450
PAN (Inj./Inc.)
N/A
N/A
29,748
28,526
28,339
29,898
PAN (Surface)
N/A
N/A
27,963
26,746
26,784
27,903
Selenium
100
100
5
5
5
5
Sodium
N/A
N/A
12,100
14,700
10,500
11,200
SAR
N/A
N/A
14.67
18.74
13.84
16.06
Total Nitrogen
N/A
N/A
90,800
86,700
87,200
90,300
Zinc
2,800
7,500
44
59
45
40
Source Name Ajinomoto Cake
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submit ' lsinformation, including the possibility of fines and imprisonment for knowing violations."
iig Ature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

y AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cake
Sampling Date 3/13/2014
% Solids 12.33
Mineralization Rate 0.3
Wet Tonsper DT 8.11
pH 7.63
Sodium Absorpotion 14.67 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 90,800
lbs./WT 22.39
Ammonia Nitrogen (mg/Kg) 3,570.00
lbs./WT 0.88
Nitrate -Nitrite (mg/Kg) 8.92
lbs./WT 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
i
PAN (mg/Kg) 27,963
lbs./WT 6.90
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 29,748
lbs./WT 7.34
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
1 st Year
2nd Year
3rd Year
_ 4th Year
�.. 5th Year
T
1
NUTRIENT APPLICATION
K20lbs./WT
2.73
P205lbs./WT
7.57
Calcium lbs./WT
0.63
Magnesium lbs./WT
0.56
Manganese lbs./WT
0.02
Sulfur lbs./WT
2.41
Molybdenum lbs./WT
0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
3.00
Arsenic lbs./WT
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./WT
0.00
Copper (mg/Kg)
9.00
Copper lbs./WT
0.00
Lead (mg/Kg)
5.00
Lead lbs./WT
0.00
Mercury (mg/Kg)
0.40
Mercury lbs./WT
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./WT
0.00
Selenium (mg/Kg)
5.00
. Selenium lbs./WT
0.00
Zinc (mg/Kg)
44.00
Zinc lbs./WT
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
TKN
PAN PAN
Nitrogen
TKN
PAN PAN
Nitrogen
(mg/kg) (lbs/DT)
(mg/Y)
(mg/kg) (lbs/DT)
(mg/Kg)
90,800
27,963 55.93
62,837
90,800'
29,148 59.50
61,052
62,837
9,426 18.85
53,412
61,052
9,158 18.32
51,894
53,412
4,006 8.01
49,406
51,894
3,892 7.78
48,002
49,406
1,853 3.71
47,553
48,002
1,800 3.60
46,202
47,553
892 1.78
46,661
46,202
866 1.73
45,336
l otal 44,139 88.28
Total 45,464 90.93
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

j ;
Page: 1 of 2
Report Number: 14-077-0214
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 98423
Sample Id: SLUDGE
A&L Eastern Laboratories, Inc.
ADL�
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www aleastern.xom
Project: SLUDGE/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/13/2014 09:30:00
Date Received: 03/18/2014 00:00
Date Reported: 03/21/2014
Total Solids " .
12.33
123300
100.0
JM
03/18/2014 15:15
SM-2540G
Moisture *
87.67
100.0
JM
03/18/2014 15:15
SM-2540G
Total Kjeldahl Nitrogen
9.08
90800
10.0
JM
03/20/2014 09:49
SM-4500-NH3C-TKN
Total Phosphorus
1.34
13400
100
KM
03/19/2014 14:57
SW 6010C
Total Potassium
0.92
9230
100
KM
03/19/2014 14:57
SW 6010C
Total Sulfur
0.98
9780
100
KM
03/19/2014 14:57
SW 6010C
Total Calcium
0.26
2560
100
KM
03/19/2014 14:57
SW 6010C
Total Magnesium
0.23
2270
100
KM
03/19/2014 14:57
SW 6010C
Total Sodium
1.21
12100
100
KM
03/19/2014 14:57
SW 6010C
Total Iron
909
100
KM
03/19/2014 14:57
SW 6010C
Total Aluminum
1300
100
KM
03/19/2014 14:57
SW 6010C
Total Manganese
74
5
KM
03/19/2014 14:57
SW 6010C
Total Copper
9
5
KM
03/19/2014 14:57
SW 6010C
Total Zinc
44
5
KM
03/19/2014 14:57
SW 6010C
Ammonia Nitrogen
0.36
3570
10.0
JM
03/20/2014 09:49
SM-4500-NI3C
Organic N
8.72
87230
10.0
03/20/2014 09:49
CALCULATION
Nitrate+Nitrite-N
8.92
2.00
jm
03/19/2014 09:00
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
03/19/2014 14:57
SW 6010C
All. values are on a dry weight
basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may
any reference be made
to the work, the results; or the company in any advertising, news release, or other
public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-077-0214
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 98423
Sample Id: SLUDGE
AFL A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
0
WWwaleastern.com
Project: SLUDGE/NC CERT#257
REPORT OF ANALYSIS
Total Chromium
8
5
KM
Total Nickel
5
5
KM
Total Lead
<5
5
KM
Total Arsenic
<3.0
3.0
KM
Total Mercury
<0.4
0.4
KM
Total Selenium
<5.0
5.0
KM
pH (Standard Units)7.63
2.00
JM
Total Molybdenum
<5
5
KM
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Date Sampled: 3/13/2014 09:30:00
Date Received: 03/18/2014 00:00
Date Reported: 03/21/2014
03/19/2014 14:57
SW 6010C
03/19/2014 14:57
SW 6010C
03/19/2014 14:57
SW 6010C
03/19/2014 14:57
SW 6010C
03/19/2014 09:00
SW-7471 B
03/19/2014 14:57
SW 6010C
03/19/2014 09:00
SW-9045D
03/19/2014 14:57
SW 6010C
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results; or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

-, AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cake
Sampling Date 6/13/2014
% Solids 13.49
Mineralization Rate 0.3
f per DT 7.41
pH 7.77
Sodium Absorpotion 18.74 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
=
TKN (mg/Kg) 86,700
lbs./WT 23.39
Ammonia Nitrogen (mg/Kg) 3,560.00
lbs./WT 0.96
Nitrate -Nitrite (mg/Kg) 23.70
lbs./WT 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 26,746
lbs./WT 7.22
- ,
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 28,526
lbs./WT 7.70
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
r� 1 st Year
*. ., 2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
K20lbs./WT
2.89
P205lbs./WT
6.61
Calcium lbs./WT
0.85
Magnesium lbs./WT
0.50
Manganese lbs./WT
0.02
Sulfur lbs./WT
3.13
Molybdenum lbs./WT
0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
3.00
Arsenic lbs./WT
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./WT
0.00
Copper (mg/Kg)
33.00
Copper lbs./WT
0.01
Lead (mg/Kg)
5.00
Lead lbs./WT
0.00
Mercury (mg/Kg)
0.40
Mercury lbs./WT
0.00
Nickel (mg/Kg)
6.00
Nickel lbs./WT
0.00
Selenium.(mg/Kg)
5.00
Selenium lbs./WT
0.00
Zinc (mg/Kg)
59.00
Zinc lbs./WT
0.02
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
TKN
PAN
PAN
Nitrogen
TKN
PAN PAN
Nitrogen
(mg/kg) (lbs/DT)
(mg/Kg)
(mg/kg) (lbs/DT)
(mg/Kg)
86,700
26,746
53.4.9
59,954
86,700
28,526 57.05
58,174
59,954
8,993
17.99
50,961
58,174
8,726 17.45
49,448
50,961
3,822
7.64
47,139
49,448
3,709 7.42
45,740
47,139
1,768
3.54
45,371
45,740
1,715 3.43
44,024
45,371
851
1.70
44,521
44,024
825 1.65
43,199
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 42,179 84.36
Total 43,501 87.00

Page: 1 of 2
ReportNumber: 14-168-0210 9� A&L Eastern Laboratories, Inc.
Account Number: 46974 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (e04) 271-6446
0
Submitted By: ALLEN WEATHINGTON www'aleastern.com
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 55977
Sample Id : SLUDGE CAKE
Project: AJINOMOTO-NORTH AMERICA
NC CERT#257
REPORT OF ANALYSIS
Total Solids *
13.49
134900
100.0
JM
Moisture "
86.51
100.0
JM
Total Kjeldahl Nitrogen
8.67
86700
10.0
JM
Total Phosphorus
1.07
10700
100
KM
Total Potassium
0.89
8930
100
KM
Total Sulfur
1.16
11600
100
KM
Total Calcium
0.32
3160
100
KM
Total Magnesium
0.19
1870
100
KM
Total Sodium
1.47
14700
100
KM
Total Iron
813
100
KM
Total Aluminum
200
100
KM
Total Manganese
80
5
KM
Total Copper
33
5
KM
Total Zinc
59
5
KM
Ammonia Nitrogen
0.36
3560
10.0
JM
Organic N
8.31
83140
10.0
Nitrate+Nitrite-N
23.7
2.00
JM
Total Cadmium
<2.0
2.0
KM
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Date Sampled: 6/13/2014 11:30:00
Date Received: 06/17/2014 00:00
Date Reported: 06/20/2014
06/17/2014 15:00
06/17/2014 15:00
06/19/2014 07:45
06/18/2014 13:27
06/18/2014 13:27
06/18/2014 13:27
06/18/2014 13:27
06/18/2014 13:27
06/18/2014 13:27
06/18/2014 13:27
06/18/2014 13:27
06/18/2014 13:27
06/18/2014 13:27
06/18/20.14 13:27
06/18/2014 07:59
06/18/2014 07:59
06/18/2014 08:00
06/18/2014 13:27
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NI3C
CALCULATION
SM-450ONO3F
SW 6010C

Page: 2 of 2
Report Number: 14-168-0210 A&L Eastern Laboratories, Inc.
Account Number: 46974� 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Submitted By: ALLEN WEATHINGTON www.aleastern.com
Send To: AJINOMOTO NORTH AMERICA INC Project: AJINOMOTO NORTH AMERICA
4020 AJINOMOTO DR NC CERT#257
RALEIGH , NC 27610
REPORT OF ANALYSIS
Lab Number: 55977
Sample Id : SLUDGE CAKE
Date Sampled: 6/13/2014 11:30:00
Date Received: 06/17/2014 00:00
Date Reported: 06/20/2014
Total Chromium
9
5
KM
06/18/2014 13:27
SW 6010C
Total Nickel
6
5
KM
06/18/2014 13:27
SW 6010C
Total Lead
<5
5
KM
06/18/2014 13:27
SW 6010C
Total Arsenic
<3.0
10
KM
06/18/2014 13:27
SW 6010C
Total Mercury
<0.4
0.4
KM
06/19/2014 00:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
06/18/2014 13:27
SW 6010C
pH (Standard Units) " 7.77
2.00
JM
06/18/2014 07:59
SW-9045D
Total Molybdenum
<5
'5
KM
06/18/2014 13:27
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Fe",
"P", AND "S".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ,
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cake
` Sampling Date 9/4/2014
y % Solids 14.45
Mineralization Rate 0.3
r Wet Tonsper DT 6.92
pH 8.21
Sodium Absorpotion 13.84 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 87,200 lbs./WT 25.20 K20 lbs./WT 2.38
Ammonia Nitrogen (mg/Kg) 3,110.00 lbs./WT 0.90 P2051bs./WT 7.08
Nitrate -Nitrite (mg/Kg) 2.08 lbs./WT 0.00 Calcium lbs./WT 0.91
r�
f
PLANT AVAILABLE NITROGEN SURFACE APPLIED Magnesium lbs./WT 0.55
PAN (mg/Kg) 26,784 lbs./WT 7.74 Manganese lbs./WT 0.03
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./WT 2.36
PAN (mg/Kg) 28,339 lbs./WT 8.19 Molybdenum lbs./WT 0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
71500
1st Year
,'2nd Year
' 3rd Year
1-\
"4th Year
5th Year
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
3.00
Arsenic lbs./WT
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./WT
0.00
Copper (mg/Kg)
59.00
Copper lbs./WT
0.02
Lead (mg/Kg)
5.00
Lead lbs./WT
0.00
Mercury (mg/Kg)
0.40
Mercury lbs./WT
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./WT
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./WT
0.00
Zinc (mg/Kg)
45.00
Zinc lbs./WT
0.01
RESIDUALNITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining,
Organic
Organic
PAN PAN
Nivogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(�/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
87,200
26,784 53.57 '
60,416
87,200
28,339 56.68
58,861
60,416
9,062 18.12
51,354
58,861
8,829 17.66
50,032
51,354
3,852 7.70
47,502
50,032
3,752 7.50
46,279
• 47,502
1,781 3.56
45,721
46,279
1,735 3.47
44,544
45,721
857 1.71
44,863
44,544
835 1.67
43,709
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd-Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
1 otal 42,337 84.67
Total 43,491 86.98

Page: 1 of 2
Report Number: 14-253-0212 AILAccount Number: 46974
Submitted By: ALLEN WEATHINGTON wwwaleastern.com
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 57509
Sample Id : SLUDGE CAKE
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-W6
Project: SLUDGE CAKE
NC CERT#257
REPORT OF ANALYSIS
Total Solids *
14.45
144500
100.0
JM
Moisture '
85.55
100.0
JM
Total Kjeldahl Nitrogen
8.72
87200
10.0
JM
Total Phosphorus
1.07
10700
100
KM
Total Potassium
0.69
6860
100
KM
Total Sulfur
0.82
8150
100
KM
Total Calcium
0.31
3140
100
KM
Total Magnesium
0.19
1890
100
KM
Total Sodium
1.05
10500
100
KM
Total Iron
1430
100
KM
Total Aluminum
1100
100
KM
Total Manganese
87
5
KM
Total Copper
59
5
KM
Total Zinc
45
5
KM
Ammonia Nitrogen
0.31
3110
10.0
JM
Organic N
8.41
84090
10.0
Nitrate+Nitrite-N
2.08
2.00
JM
Total Cadmium
<2.0
2.0
KM
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Date Sampled: 9/4/2014 15:00:00
Date Received: 06/10/2014 00:00
Date Reported: 09/15/2014
09/10/2014 13:59
09/10/2014 13:59
09/11/2014 10:00
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 12:39
09/11/2014 09:04
09/11/2014 09:04
09/11/2014 09:05
09/11/2014 12:39
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SM-450ONO3F
SW 6010C

Page: 2 of 2
Report Number: 14-253-0212
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 57509
Sample Id: SLUDGE CAKE
A&L Eastern Laboratories, Inc.
ILA 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: SLUDGE CAKE
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 9/4/2014 15:00:00
Date Received: 09/10/2014 00:00
Date Reported: 09/15/2014
Total Chromium
10
5
KM
09/11/2014 12:39
SW 6010C
Total Nickel
<5
5
KM
09/11/2014 12:39
SW 6010C
Total Lead
<5
5
KM
09/11/2014 12:39
SW 6010C
Total Arsenic
<3.0
3.0
KM
09/11/2014 12:39
SW 6010C
Total Mercury
<0.4
0.4
KM
09/11/2014 15:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
09/11/2014 12:39
SW 6010C
pH (Standard Units) " 8.21
2.00
JM
09/11/2014 09:04
SW-9045D
Total Molybdenum
<5
5 .
KM
09/11/2014 12:39
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE
PURPOSES.
QUALIFIER: THE LCS WAS OUT OF LIMITS FOR "Mn'.
THE MATRIX SPIKE WAS
OUT OF LIMITS FOR "Ca".
THE MSD WAS OUT OF LIMITS
FOR "SE".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as .noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results; or the company in any advertising. news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

AGMAN FIELD LOADING ESTIMATES
y
Facility Ajinomoto Cake
Sampling Date 12/10/2014
'
% Solids 13.29
'.
Mineralization Rate 0.3
'
Wet Tonsper DT 7.52
'.
pH 7.6
Sodium Absorpotion 16.06 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not
Land Apply
"
Ratio
=`
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 90,300 lbs./WT 24.00
K20lbs./WT
2.70
Ammonia Nitrogen (mg/Kg) 3,990.00 lbs./WT 1.06
P205 lbs./WT
4.87
Nitrate -Nitrite (mg/Kg) 15.05 lbs./WT 0.00
Calcium lbs./WT
0.82
• 1
PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./WT
0.29
PAN (mg/Kg) 27,903 lbs./WT 7.42
Manganese lbs./WT
0.01
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./WT .
2.19
PAN (mg/Kg) 29,898 lbs./WT 7.95
Molybdenum lbs./WT
0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
i
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,306
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
' 4th Year
5th Year
1 J
t
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
3.00
Arsenic lbs./WT
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./WT
0.00
Copper (mg/Kg)
17.00
Copper lbs./WT
0.00
Lead (mg/Kg)
5.00
, Lead lbs./WT
0.00
Mercury (mg/Kg)
0.40
Mercury lbs./WT
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./WT
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./WT
0.00
Zinc (mg/Kg)
40.00
Zinc lbs./WT
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN.
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TIN
(mg/kg) (lbs/DT)
(mg/Kg)
90,300
27,903
55.81
62,397
90,300
29,898 59.80
60,402
62,397
9,360
18.72
53,037
60,402
9,660 18.12
51,342
53,037
3,978
7.96
49,060
51,342
3,851 7.70
47,491
49,060
1,840
3.68
47,220
47,491
1,781 3.56
45,710
47,220
885
1.77
46,334
1 45,710
857 1.71
44,853
Total 43,966 87.93
Total 45,447 90.89
Equations
1st Yr. PAN (mg/Kg)=(MR x (IYN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

A 1. � � I r - ✓
Page: 1 of 2
Report Number: 14-345-0217
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
AIL
wwwaleastem.com
A&L Eastern Laboratories, Inc.
7621 Whitepine Road_ Richmond, Virginia 23237 [phone] Fax [phone]
Project: SLUDGE CAKE
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 12/10/2014 00:00:00
Lab Number: 59207 Date Received: 12/11/2014 00:00
Sample Id: SLUDGE CAKE Date Reported: 12/19/2014
Total Solids *
13.29
132900
100.0
DH
12/12/2014 13:59
SM-2540G
Moisture *
86.71
100.0
DH
12/12/2014 13:59
SM-2540G
Total Kjeldahl Nitrogen
9.03
90300
10.0
JM
12/17/2014 08:10
SM-4500-NH3C-TKN
Total Phosphorus
0.80
8000
100
KM
12/12/2014 12:36
SW 6010C
Total Potassium
0.85
8450-
100
KM
12/12/2014 12:36
SW 6010C
Total Sulfur
0.82
8230
100
KM
12/12/2014 12:36
SW 6010C
Total Calcium
0.31
3070
100
KM
12/12/2014 12:36
SW 6010C
Total Magnesium
0.11
1090
100
KM
12/12/2014 12:36
SW 6010C
Total Sodium
1.12
11200
100
KM
12/12/2014 12:36
SW 6010C
Total Iron.
639
100
KM
12/12/2014 12:36
SW 6010C
Total Aluminum
500
100
KM
12/12/2014 12:36
SW 6010C
Total Manganese
36
5
KM
12/12/2014 12:36
SW 6010C
Total Copper
17
5
KM
12/12/2014 12:36
SW 6010C
Total Zinc
40
5
KM
12/12/2014 12:36
SW 6010C
Ammonia Nitrogen
0.40
3990
10.0
JM
12/15/2014 09:04
SM-4500-NH3C
Organic N
8.63
86310
10.0
12/15/2014 09:04
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
12/12/2014 09:05
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
12/12/2014 12:36
SW.6010C
All values are on a dry weight basis except as noted
by asterisk. Detection limit on all N series is on a wet basis.
,
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-345-0217
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 59207
Sample Id SLUDGE CAKE
L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com
Project: SLUDGE CAKE
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 12/10/2014 00:00:00
Date Received: 12/11 /2014 00:00
Date Reported: 12/19/2014
Total Chromium
9
5
KM
12/12/2014 12:36
SW 6010C
Total Nickel
<5
5
KM
12/12/2014 12:36
SW 6010C
Total Lead
<5
5
KM
12/12/2014 12:36
SW 6010C
Total Arsenic
<3.0
3.0
KM
12/12/2014 12:36
SW 6010C
Total Mercury
<0.4
0.4
KM
12/12/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
12/12/2014 12:36
SW 6010C
pH (Standard Units) " 7.60
2.00
JM
12/12/2014 09:04
SW-9045D
Total Molybdenum
<5
5
KM
12/12/2014 12:36
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn".
THE MSD WAS OUT OF
LIMITS FOR "Se".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

1
aceAnalyiical
`. www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: TCLP 12/10
Pace Project No.: 92229377
Sample: TRP CELLCREAN Lab ID:
92229377001 Collected: 12/10/14 11:30
Results, reported on a "dry -weight" basis
Parameters Results
Units Report Limit
DF Qualifiers
1,2-Dichloroethane-d4 (S)
101 % 70-130
25 D3
Toluene-d8 (S)
96 % 67-135
25
4-Bromofluorobenzene (S)
89 % 70-130
25
Sample: SLUDGE Lab ID:
92229377002
Results reported on a "dry -weight" basis
Parameters Results Units
gamma-BHC (Lindane)
ND ug/L
Chlordane (Technical)
ND ug/L
Endrin
ND ug/L
Heptachlor epoxide
ND ug/L
Methoxychlor
ND ug/L
Toxaphene
ND ug/L
Decachlorobiphenyl (S)
66 %
Tetrachloro-m-xylene (S)
66 %
2,4-D
ND mg/L
2,4,5-TP (Silvex)
ND mg/L
2,4-DCAA (S)
77 %
Arsenic
ND mg/L
C
Barium
ND mg/L
Cadmium
ND mg/L
Chromium
ND mg/L
Lead
ND mg/L
Selenium
ND mg/L
Silver
ND mg/L
Mercury
ND ug/L
=
1,4-Dichlorobenzene
ND ug/L
2,4-Dinitrotoluene
ND ug/L
Hexachloro-1,3-butadiene
ND ug/L
Hexachlorobenzene
ND ug/L
Hexachloroethane
ND ug/L
2-Methylphenol(o-Cresol)
ND ug/L
3&4-Methylphenol(m&p Cresol)
ND ug/L
Nitrobenzene
ND ug/L
Pentachlorophenol
ND ug/L
Pyridine
ND ug/L
2,4,5-Trichlorophenol
ND ug/L
(
2,4,6-Trichlorophenol
ND ug/L
Nitrobenzene-d5 (S)
0 %
i
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
Benzene
Collected: 12/10/14 11:30
Report Limit DF Qualifiers
0.50
1
3.0
1
0.50
1
0.50-
1
1000
1
3:0
1
10-138
1
10-110
1
0.010
1
0.010
1"
42-142
1
0.050
1
0.25
1
0.0050
1
0.025
1
0.025
1
0.10
1
0.025
1
0.20
1
10000
10
10000
10
10000
10
10000
10
10000
10
10000
10
-10000
10
10000
10,
20000
10
10000
10
10000
10
10000
10
12-102
10 D3,
H5,
P3,
S4
0 %
13-107
10
0 %
21-132
10
'0 %
10A10
10
0 %
10-110
10
0 %
27-108
10
ND ug/L
192
38.5
REPORT OF LABORATORY ANALYSIS
Date: 01/02/2015 04:30 PM
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 9

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: TCLP 12/10
Pace Project No.: 92229377
--
Sample: SLUDGE Lab ID: 92229377002
`
Results reported on a "dry -weight' basis
Parameters
Results Units
2-Butanone (MEK)
ND ug/L
Carbon tetrachloride
ND ug/L
Chlorobenzene
ND ug/L
=
Chloroform
ND ug/L
1,4-Dichlorobenzene
ND ug/L
1,2-Dichloroethane
ND ug/L
'�--'
1,1-Dichloroethene
ND ug/L
r'
Tetrachloroethene
ND ug/L
Trichloroethene
ND ug/L
Vinyl chloride
ND ug/L
1,2-Dichloroethane-d4 (S)
85 %
Toluene-d8 (S)
100 %
{
4-13romofluorobenzene (S)
98 %
•
1
r
i
Date: 01/02/2015 04:30 PM
I ,
Collected: 12/10/14 11:30
Report Limit
DF Qualifiers
385
38.5
192
38.5
192
38.5
192
38.5
192
38.5
192
38.5
192
38.5
192
38.5
192
38.5
192
38.5
70-130
38.5 1 g
67-135 .
38.5
70-130
38.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 9

i Pace Analytical Services, Inc.
' y ® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: TCLP 12/10
Pace Project No.: 92229377
DEFINITIONS
' DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. '
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
/ SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LABORATORIES
r �
PASI-A Pace Analytical Services -Asheville
r PASI-C Pace Analytical Services - Charlotte
PASI-O Pace Analytical Services - Ormond Beach
i ANALYTE QUALIFIERS
1 g 8260 results are from a total analysis which show that analytes are not present or that they are present but at such low
levels that the appropriate regulatory levels could not possibly be exceeded, per Section 1.2 of Method 1311.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
H5 Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.
i
-_ P3 Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
�- S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
REPORT OF LABORATORY ANALYSIS
Date: 01 /02/2015 04:30 PM
1
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 9

zAnaly�lcal
` � "" wvrw.paeelabs.cam
'01 Conference Drive, Raleigh, NC 27607
^ r [phone], fax: [phone]
'WW Cert#67, NCDW Cert#37731
s - aport Results To:
Chain. of Custody w.O.#
_>>mpany:
_-,dress:
>to(at4k
NAG altda
in: ..8,eu;
r> ad gr. 5
_ . tone:
- �72�- ! �f
4/`L�
! f
' 2-V 1 -
_Ix:
,Impled by (signature):'
BUM:
Project Reference:
Project Number:
Purchase Order #:
,42-Standard Report Delivery
❑ Rush Report Delivery'(w/surcharge)
"Rush projects are subject to prior approval by
the laboratory
Requested Due Date:
--relinquished by (sig ature)
Rece ed by (signature)
Date
Time
in ished by (signature)
R ' ed by (si atu
Date
Time
$
efinquished by (s Itature)
Recelved by (signature)
Date
Time
Receipt Conditions (LUsg Qnly)
O 4t2°C ❑ Temp:`-" ' (� °C
Res. Chlorine:
❑ Absent ❑ Present ❑ rVa
Acid preserv. <2?
❑ Yes ❑ No ❑ rVa
Base preserv. >12?
❑ Yes ❑ No ❑ We
Page 8 of 9

0
Document Name: Sample Condition Upon
Document Revised: April 04, 2073
'
Receipt SCU.R
Page 1 of 2
" a eAlla1 /TI
I` ' w.,,w.pnaofpbF aa,n
'
Document No,:
issuing Authorities:
Pace Asheville QualitV Office
F-RAL-CS-001-rev.02
Client Name: I "LALA-_i2
Where Received: [] Huntersville Asheville (] Eden ee Raleigh.
Courier (Circle): Fed Ex UPS USPS Client Commercial Pace - Other -
Custody Seal on CooleriBox Present; Ej yes 0 no Seals intact: U yes E] no
Packing Material: [3 bubble Wrap Bubble 13800 None_q Other
Circle Thermometer Used: IR Gun S :12209 of Ice • We Blue None [] Samples on Ice, cooling process has begun
e t�
Temp Correction Factor: Add I ubtrac�y_ �` C
Corrected Cooler Temp.: .19 C Biological Tissue,is Frozen: Yos No
Date and initials of person ex a Inin
co t 1 Presery Ion
check: Ll
Temp. should be above freezing to M
Comments:
Chain of Custody Present:
es ONO
❑WA
4.
Chain of Custody-Fllled Out:
Qs [IN.
13wA'
2. '
Chain of Custody Relin wished:
s ONO
C7WA
3.
sampler Name R Signature on COC:
dYes ON.
OWA
4.
Samples Arrived within -Hold Time:
Yes ONo
❑wA
5.
Short Hold Time Analysts (<72hr):
Dyes 4No
❑NIA
6.
Rush Turn Around Time Requested:
t7Yes_ QINo'
ONiA
7..
Sufficient Volume:
Yes ONO
OWA
8.
Correct Containers Used:
P4ea ONO
DITA
9. '
-Pace Containers Used:
es ONo
❑NIA
Containers Intact:
Yes ONO
E]WA
10.
Filtered volume -received for Dissolved tests
DYes E]No
NIA
1l.
Sample Labels match COG:
Yes DNo
❑WA
12.
-Includes dateltime/lb/Ana[ sls Matrix:
13,
All containers needing -preservation have been chocked. Yes DNo OWA
All containers needing preservation are found to be in
(Yes ONO
OWA
compliance with EPA recommendation.
ONO
exceptions: VOA, gollform, TOO, O&G, WI•DRO (water)
es
Samples checked for dechlorination:
Yes DNo
ONIA
14,
Heads ace in VOA Vials >6mm :
Dyes ONo
ONIA
15.
Trip Blank Present:
Dyes ONo
OYes ONO
ONIA
�JN/A
16.
Trip Blank Custody Seals Present
Pace Trip Blank Lot # if purchased):,
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Datelfime:
Comments/ Resolution:
SCURF/SRF Date: /2 WO# : 92229377 - -
Review:: I - rx l
Note: Whenever there, Is a discrepancy affecting North Carolina compliance IIII IIIII IIIIII II III
samples, a copy of this form will be sent to the North Carolina DEHNR g2229377
Certification -Office ( i.a out of hold, incorrect preservative, out of temp.
Incorrect containers)
Page 9 of 9

APPENDIX III
CELL CREAM RESIDUAL SAMPLING SUMMARY
FORM
ANALYTICAL ,

WQ Permit No.
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ0032618 Facility Name Ajinomoto Amino Science, LLC Source Permit No. WQ0032618
Laboratory 1
Laboratory 2
Laboratory 3
Sample Date Class A Clas B
A&L Eastcm Labs,
Inc.
A&L Eastem L bs,
Inc.
A&L Eastern Labs,
Inc
A&L Eastern Labs,
Inc
3/13/2014
6/13/2014
9/4/2014
12/10/2014
Aluminum
N/A
N/A
200
100•
200
100
Ammonia Nitrogen
N/A
N/A
10,900
7,240
5,390
5,840
Arsenic
41
75
3
3
3
3
Cadmium
39
85
2
2
2
2
Calcium
N/A
N/A
152
316
205
412
Copper
1,500
4,300
5
7
7
6
Lead
300
840
5
5
5
5
Magnesium
N/A
N/A
100
127
100
110
Mercury
17
57
0.4
0.4
0.4
0.4
Molybdenum
N/A
75
5
5
5
5
Nickel
420
420
5
5
5
5
Nitrate -Nitrite Nitrogen
N/A
N/A
3
6
10
17
Percent Solids
N/A
N/A
13.87
10.77
8.90
11.65
PH (no units)
N/A
N/A
2.72
4.07
3.58
3.51
Phosphorus
N/A
N/A
10,500
9,290
7,960
8,680
Potassium
N/A
N/A
1,100
1,990
1,530
1,810
PAN (Ini./Inc.)
N/A
N/A
47,833
48,874
46,383
45,205
PAN (Surface)
N/A
N/A
42,383
45,254
43,688
42,285
Selenium
100
100
5
5
5
5
Sodium
N/A
N/A
374
340
436
0 446
SAR
N/A
N/A
2.15
1.34
1.86
1.72
Total Nitrogen
N/A
N/A
134,000
146,000
142,000
137,000
Zinc
2,800
7,500
5
6
5
5
Source Name. Ajinomoto Cell Cream
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submittin alse information, including the possibility of fines and imprisonment for knowing violations."
—z
ligature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

16 A
FIELD LOADING ESTIMATES
Facility Ajinomoto Cell Cream
Sampling Date 3/13/2014
% Solids 13.87
Mineralization Rate 0.3
Gallons per DT 1,728.97
pH 2.72
Sodium Absorpotion 2.15 <5.0 Safe 5.0 - 10.0 Careful Management
Ratio
NITROGEN APPLICATION
>15.0 Do Not Land Apply
TKN (mg/Kg) 134,000 lbs./1,000 gal 155.01
Ammonia Nitrogen (mg/Kg) 10,900.00 lbs./1,000 gal 12.61
Nitrate -Nitrite (mg/Kg) 2.88 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 42,383 lbs./1,000 gal 49.03
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 47,833 lbs./1,000 gal 55.33
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
NUTRIENT APPLICATION
K20 lbs./1,000 gal
1.53
P205 lbs./1,000 gal
27.81
Calcium lbs./1,000 gal
0.18
Magnesium lbs./1,000 gal
0.12
Manganese lbs./1,000 gal
0.01
Sulfur lbs./1,000 gal
18.62
Molybdenum lbs./1,000 gal
0.01
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
HEAVY METAL CONCENTRATION
HEAVY METAL LOADING
41
75
Arsenic (mg/Kg)
3.00
Arsenic lbs./1,000 gal
0.00
39
85
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
1,500
4,300
Copper (mg/Kg)
5.00
Copper lbs./1,000 gal
0.01
300
840
Lead (mg/Kg)
5.00
Lead lbs./1,000 gal
0.01
17
57
Mercury (mg/Kg)
0.40
Mercury lbs./1,000 gal
0.00
420
420
Nickel (mg/Kg)
5.00'
Nickel lbs./1,000 gal
0.01
100
1,00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.01
2,800 11
7,500
Zinc (mg/Kg)
5.00
Zinc lbs./1,000 gal
0.01
-
,RESIDUAL NITROGEN CALCULATION
1 st Year
2nd Year
-'3rd Year
- 4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/D'I)
(mg/Kg)
134,000
42,383 84.77
91,617
134,000
47,833 95.67
86,167
91,617
13,743 27.49
77,875
86;167
12,925 25.85
73,242
77,875
5,841 11.68
72,034
73,242
5,493 10.99
67,749
72,034
2,701 5.40
69,333
67,749
2,541 5.08
65,208
69,333
1,300 2.60
68,033
65,208
1,223 2.45
63,986
r
Equations
1stYr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOX
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 65,967 131.93
Total 70,014 140.03

Page: 1 of 2
Report Number: 14-077-0215
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 98424
Sample Id: CELL CREAM
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
0
wwwaleastem.com
Project: TRY P CELL CREAM
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 3/13/2014 00:00:00
Date Received: 03/18/2014 00:00
Date Reported: 03/21/2014
Total Solids
13.87
138700
100.0
JM
03/18/2014 15:15
Moisture *
86.13
100.0
JM
03/18/2014 15:15
Total Kjeldahl Nitrogen
13.40
134000
10.0
JM
03/19/2014 07:59
Total Phosphorus
1.05
10500
100
KM
03/19/2014 14:57
Total Potassium
0.11
1100
100
KM
03/19/2014 14:57
Total Sulfur
1.61
16100
100
KM
03/19/2014 14:57
Total Calcium
0.02
152
100
KM
03/19/2014 14:57
Total Magnesium
<0.01
<100
100
KM
03/19/2014 14:57
Total Sodium
0.04
37,4
100
KM
03/19/2014 14:57
Total Iron
<100
100
KM
03/19/2014 14:57
Total Aluminum
200
100
KM
03/19/2014 14:57
Total Manganese
7
5
KM
03/19/2014 14:57
Total Copper
<5
5
KM
03/19/2014 14:57
Total Zinc
<5
5
KM
03/19/2014 14:57
Ammonia Nitrogen
1.09
10900
10.0
JM
03/19/2014 11:30
Organic N
12.31
123100
10.0
03/19/2014 07:59
Nitrate+Nitrite-N
2.88
2.00
jm
03/19/2014 09:00
Total Cadmium
<2.0
2.0
KM
03/19/2014 14:57
All values are on a d
wei ht ba i t t d b t` k D t f 1` W. II N
4-b
SM-2540G
SM-2540G
SM-4500-N H3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NI
CALCULATION
SM-450ONO3F
SW 6010C
ry g s s excep as no e y as ens a ec ion imi on a series is on a we asis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results: or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
,Debbie Holt

Page: 2 of 2
Report Number: 10215
A&L Eastem Laboratories, ,Inc.
Account Number: 46974
6974
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Submitted By: ALLEN WEATHINGTON
www.aleastem.com
Send To: AJINOMOTO NORTH AMERICA INC
Project: TRY P CELL CREAM
4020 AJINOMOTO DR
NC CERT#257
RALEIGH , NC 27610
REPORT OF ANALYSIS Date Sampled: 3/13/2014 00:00:00
Lab Number: 98424
Date Received: 03/18/2014 00:00
Sample Id: CELL CREAM
Date Reported: 03/21/2014
PARAMETER RESULT
RESULT
QUANTITATION
.•
•.
Total Chromium
<5
5 KM 03/19/2014 14:57
SW 6010C
Total Nickel
<5
5 KM 03/19/2014 14:57
SW 6010C
Total Lead
<5
5 KM 03/19/2014 14:57
SW 6010C
Total Arsenic
<3.0
3.0 KM 03/19/2014 14:57
SW 6010C
Total Mercury
<0.4
0.4 KM 03/19/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0 KM 03/19/2014 14:57 _
SW 6010C
pH (Standard Units) * 2.72
2.00 JM 03/19/2014 09:00
SW-9045D
Total Molybdenum
<5
5 KM 03/19/2014 14:57
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results: or the company in any advertising, negvs release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

OIL
AGMANJ FIELD LOADING ESTIMATES
Facility Ajinomoto Cell Cream
Sampling Date 6/13/2014
% Solids 10.77
Mineralization Rate 0.3
Gallons per DT 2,226.63
pH 4.07
Sodium Absorpotion 1.34 <5.0 Safe 5.0 - 10.0 Careful Management
Ratio
'NITROGEN APPLICATION
>15.0 Do Not Land Apply
TKN (mg/Kg) 146,000 lbs./1,000 gal 131.14
Ammonia Nitrogen (mg/Kg) 7,240.00 lbs./1,000 gal 6.50
Nitrate -Nitrite (mg/Kg) 5.57 lbs./1,000 gal 0.01 -
-PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 45,254 lbs./1,000 gal 40.65
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 48,874 lbs./1,000 gal 43.90
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
K20 lbs./1,000 gal
2.14
P205 lbs./1,000 gal
19.11
Calcium lbs./1,000 gal
0.28
Magnesium lbs./1,000 gal
0.11
Manganese lbs./1,000 gal
0.01
Sulfur lbs./1,000 gal
15.90
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
3.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
7.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
5.00
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.40
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
6.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TEN
(mg/kg) Obs/DT)
(mg/Kg)
TKN
(lbs/DT)
(mg/Kg)
146,000
45,254 90.51
100,746
146,000
48,874 97.75
97,126
100,746
15,112 30.22
85,634
97,126
14,569 29.14
82,557
85,634
6,423 12.85
79,212
82,557
6,192 12.38
76,366
79,212
2,970 5.94
76,241
76,366.
2,864 5.73
73,502
76,241
1,430 2.86
74,'812
73,502
1,378 2.76
72,124
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 71,188 142.38
Total 73,876 147.75

Page: 1 of 2
Report Number: 14-168-0211
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 65978
Sample Id : HIS CELL CREAM
L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastem.com
Project: AJINOMOTO NORTH AMERICA/CELL CREAM
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/13/2014 11:30:00
Date Received: 06/17/2014 00:00
Date Reported: 06/20/2014
Total Solids '
t'
10.77
107700
100.0
JM
06/17/2014 15:00
Moisture "
89.23
100.0
JM
06/17/2014 15:00
Total Kjeldahl Nitrogen
14.60
146000
10.0
JM
06/19/2014 07:45
Total Phosphorus
0.93
9290
100
KM
06/18/2014 13:27
Total Potassium
0.20
1990
100
KM
06/18/2014 13:27
Total Sulfur
1.77
17700
100
KM
06/18/2014 13:27
Total Calcium
0.03
316
100
KM
06/18/2014 13:27
Total Magnesium
0.01
127
100
KM
06/18/2014 13:27
Total Sodium
0.03
340
100
KM
06/18/2014 13:27
Total Iron
140
100
KM
06/18/2014 13:27
Total Aluminum
<100
100
KM
06/18/2014 13:27
Total Manganese
10
5
KM
06/18/2014 13:27
Total Copper
7
5
KM
06/18/2014 13:27
Total Zinc
6
5
KM
06/18/2014 13:27
Ammonia Nitrogen
0.72
7240
10.0
JM
06/18/2014 07:59
Organic N
13.88
138760
10.0
06/18/2014 07:59
Nitrate+Nitrite-N
5.57
2.00
JM
06/18/2014 08:00
Total Cadmium
<2.0
2.0
KM
06/18/2014 13:27
All I d
ht b t t d
b 1. D 1' 't II N
t b
SM-254OG
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C.
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SM-450ONO3F
SW 6010C
Va ues are on a ry weig asis excep as no e y as ens . etection imi on a serves is on a we asis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2 tt,
Report Number: 14-168-0211 AL A&L Eastern Laboratories, Inc.
Account Number: 46974 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Submitted By: ALLEN WEATHINGTON wwwaleastem.com
Send To: AJINOMOTO NORTH AMERICA INC Project: AJINOMOTO NORTH AMERICA/CELL CREAM
4020 AJINOMOTO DR NC CERT#257
RALEIGH , NC 27610
REPORT OF ANALYSIS -Date Sampled: 6/13/2014 11:30:00
Lab Number: 55078 Date Received: 06/17/2014 00:00
Sample Id : HIS CELL CREAM Date Reported: 06/20/2014
Total Chromium
<5
5
KM
06/18/2014 13:27
SW 6010C
Total Nickel
<5
5
KM
06/18/2014 13:27
SW 6010C
Total Lead
<5
5
KM
06/18/2014 13:27
SW 6010C
Total Arsenic
<3.0
3.0
KM
06/18/2014 13:27
SW 6010C
Total Mercury
<0.4
0.4
KM
06/19/2014 00:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
06/18/2014 13:27
SW 6010C
pH (Standard Units) *
4.07
2.00
JM
06/18/2014 07:59
SW-9045D
Total Molybdenum
<5
5
KM
06/18/2014 13:27
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Na". THE MATRIX SPIKE WAS OUT OF LIMITS
FOR "Fe", "P",
AND "S". ALL OTHER QC DATA IS
ACCEPTABLE.
n
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without.obtaining our prior written authorization.
Debbie Holt

t
AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cell Cream
Sampling Date 9/4/2014
% Solids 8.9
Mineralization Rate 0.3
Gallons per DT 2,694.47
pH 3.58
Sodium Absorpotion 1.86 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
" Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 142,000 lbs./1,000 gal 105.40
Ammonia Nitrogen (mg/Kg) 5,390.00 lbs./1,000 gal 4.00
Nitrate -Nitrite (mg/Kg) 10.10 lbs./1,000 gal 0.01
r PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 43,688 lbs./1,000 gal 32.43
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 46,383 . lbs./1,000 gal 34.43
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
1st Year
l 12nd Year
3rd Year
4th Year
r-
5th Year
NUTRIENT APPLICATION
K2 lbs./1,000 gal
1.36
P205 lbs./1,000 gal
13.53 .
Calcium lbs./1,000 gal
0.15,
Magnesium lbs./1,000 gal
0.07
Manganese lbs./1,000 gal
0.02
Sulfur lbs./1,000 gal
13.29
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
3.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
7.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
5.00
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.40
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
5.00
Zinc lbs./1,000 gal
0.00
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
142,000
43,688 87.38
98,312
142,000
46,383 92.77
95,617 _
98,312
14,747 29.49
83,565
95,617
14,343 28.69
81,274
83,565
6,267 12.53
77,298
81,274
6,096 12.19
75,179
77,298
2,899 5.80
74,399
75,179
2,819 5.64
72,360
74,399
1,395 2.79
73,004
72,360
1,357 , 2.71
71,003
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 68,996 137.99
Total 70,997 141.99

Page: 1 of 2
Report Number: 14-253-0213
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 57510
Sample Id : SKK HIS CELL CREAM
A&L Eastern Laboratories, Inc®
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com
Project: SKK HIS CELL CREAM
NC CERT#257
REPORT OF ANALYSIS
Total Solids *
8.90
89000
100.0
JM
Moisture *
91.10
100.0
JM
Total Kjeldahl Nitrogen
14.20
142000
10.0
JM
Total Phosphorus
0.80
7960
100
KM
Total Potassium
0.15
1530
100
KM
Total Sulfur
1.79
17900
100
KM
` Total Calcium
0.02
205
•100
KM
Total Magnesium
<0.01
<100
100
KM
Total Sodium
0.04
436
100
KM
Total Iron
188
100
KM
Total Aluminum
200
100
KM
Total Manganese
26
5
KM
Total Copper
7
5
KM
Total Zinc
<5
5
KM
Ammonia Nitrogen
0.54
5390
10.0
JM
Organic N
13.66
136610
10.0
Nitrate+Nitrite-N
10.1
2.00
JM
Total Cadmium
<2.0
2.0
KM
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Date Sampled: 9/4/2014 15:00:00
Date Received: 09/10/2014 00:00
Date Reported: 09/15/2014
09/10/2014 13:59
09/10/2014 13:59
09/11/2014 10:00
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/12/2014 11:05
09/11/2014 09:04
09/11/2014 09:04
09/11/2014 09:05
09/12/2014 11:05
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SM-450ONO3F
SW 6010C

r
Page: 2 of 2
Report Number: 14-253-0213
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 57510
Sample Id : SKK HIS CELL CREAM
90 A&L Eastern Laboratories, Inc.
7621 Whitepme Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleasterh.com
Project: SKK HIS CELL CREAM
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 9/4/2014 15:00:00
Date Received: 09/10/2014 00:00
Date Reported: 09/15/2014
Total Chromium
<5
5
KM
09/12/2014 11:05
SW 6010C
Total Nickel
<5
5
KM
09/12/2014 11:05
SW 6010C
Total Lead
<5
5
KM
09/12/2014 11:05
SW 6010C
Total Arsenic
<3.0
3.0
KM
09/12/2014 11:05
SW 6010C
Total Mercury
<0.4
0.4
KM
09/11/2014 15:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
09/12/2014 11:05
SW 6010C
pH (Standard Units) * 3.58
2.00
JM
09/11/2014 09:04
SW-9045D
Total Molybdenum
<5
5
KM
09/12/2014 11:05
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "B" AND "Mn".
THE MSD WAS
OUT OF LIMITS FOR "SE". ALL
OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results; or the company in any advertising, news release, or other public announcements Without obtaining our prior written authorization.
Debbie Holt

. AGMAN FIELD LOADING ESTIMATES
Facility Ajinomoto Cell Cream
Sampling Date 12/10/2014
0/6 Solids 11.65
Mineralization Rate 0.3
Gallons per DT 2,058.44
pH 3.51
Sodium Absorpotion 1.72 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 137,000 lbs./1,000 gal 133.11
K20 lbs./1,000 gal
2.11
`-' Ammonia Nitrogen (mg/Kg) 5,840.00 lbs./1,000 gal 5.67
P205 lbs./1,000 gal
19.31
Nitrate -Nitrite (mg/Kg) 17.17 lbs./1,000 gal 0.02
Calcium lbs./1,000 gal
0.40
PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./1,000 gal
0.11
PAN (mg/Kg) 42,285 lbs./1,000 gal 41.08
Manganese lbs./1,000 gal
0.01
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
17.97
PAN (mg/Kg) 45,205 lbs./1,000 gal 43.92
Molybdenum lbs./1,000 gal
0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
HEAVY METAL CONCENTRATION
HEAVY METAL LOADING
41
75
Arsenic (mg/Kg)
3.00
Arsenic lbs./1,000 gal
0.00
39
85
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
1,500
4,300
Copper (mg/Kg)
6.00
Copper lbs./1,000 gal
0.01
300
840
Lead (mg/Kg)
5.00
Lead lbs./1,000 gal
0.00
17
57
Mercury (mg/Kg)
0.40
Mercury lbs./1,000 gal
0.00
420
420
Nickel (mg/Kg)
5.00
Nickel lbs./.1,000 gal
0.00
100
100
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
2,800
.7,500
Zinc (mg/Kg)
5.00
Zinc lbs./1,000 gal
0.00
RESIDUAL NITROGEN CALCULATION
1 st Year
2nd Year
3rd Year
4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)'
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
137,000
42,285 84.57
94,715
137,000
45,205 90.41
91,795
94,715
14,207 28.41
80,508
91,795
178,026
13,769 27.54
78,026
80,508
- 6,038 12.08
74,470
5,852 11.70
72,174
74,470
2,793 5.59
71,677
72,174
2,707 5.41
69,467
71,677
1,344 2.69
70,333
69,467
1,303 2.61
68,165
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 66,667 133.33 Total 68,835 137.67

Page: 1 of 2
Report Number: 14-345-0218
Account Number: 46974
Submitted By: ALLEN WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJINOMOTO DR
RALEIGH , NC 27610
Lab Number: 59208
Sample Id : TRP CELL CREAM
A&L Eastern Laboratories, Inc.
AL
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastem.com
Project: TRP CELL CREAM
NC CERT#257
REPORT OF ANALYSIS
Total Solids *
11.65
116500
100.0
RD 1
Moisture "
88.35
100.0
RD 1
Total Kjeldahl Nitrogen
13.70
137000
10.0
JM 1
Total Phosphorus
0.87
8680
100
KM 1
Total Potassium
0.18
1810
100
KM 1
Total Sulfur
1.85
18500
100
KM 1
Total Calcium
0.04
412
100
KM 1
Total Magnesium
0.01
110
100
KM 1
Total Sodium
0.04
446
100
KM 1
Total Iron
178
100
KM 1
Total Aluminum
100
100
KM 1
Total Manganese
9
5
KM 1
Total Copper
6
5
KM 1
Total Zinc
<5
5
KM 1
Ammonia.Nitrogen
0.58
5840
10.0
JM 1
Organic N
13.12
131160
10.0
1
Nitrate+Nitrite-N
<2.00
2.00
JM 1
Total Cadmium
<2.0
2.0
KM 1
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Date Sampled: 12/10/2014 00:00:00
Date Received: 12/11 /2014 00:00
Date Reported: 12/19/2014
2/11/2014 15:15
2/11/2014 15:15
2/17/2014 08:10
2/12/2014 12:36
2/12/2014 12:36.
2/12/2014 12:36
2/12/2014 12:36
2/12/2014 12:36
2/12/2014 12:36
2/12/2014 12:36
2/12/2014 12:36
2/12/2014 12:36
2/12/2014 12:36
2/12/2014 12:36
2/15/2014 09:04
2/15/2014 09:04
2/12/2014 09:05
2/12/2014 12:36
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SM-450ONO3F
SW 6010C
Debbie Holt

Page: 2 of 2
Report Number: 14-345-0218
Account Number: 46974
Submitted By: ALLEN.WEATHINGTON
Send To: AJINOMOTO NORTH AMERICA INC
4020 AJ I NOMOTO. D R
RALEIGH , NC 27610
Lab Number: 59208
Sample Id : TRP CELL CREAM
AFL A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com
Project: TRP CELL CREAM
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 12/10/2014 00:00:00
Date Received: 12/11/2014 00:00
Date Reported: 12/19/2014
Total Chromium
<5
5
KM
12/12/2014 12:36
SW 6010C
Total Nickel
<5
5
KM
12/12/2014 12:36
SW 6010C
Total Lead
<5
5
KM
12/12/2014 12:36
SW 6010C
Total Arsenic
<3.0
3.0
KM
12/12/2014 12:36
SW 6010C
Total Mercury
<0.4
0.4
KM
12/12/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
12/12/2014 12:36
SW 6010C
pH (Standard Units) " 3.51
2.00
JM
12/12/2014 09:04
SW-9045D
Total Molybdenum
<5
5
KM
12/12/2014 12:36
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE
PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MSD WAS OUT OF
LIMITS FOR "Se".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

aceAnalytical
www.pacelabs.com
- i
January 02, 2015
Kevin Adams
Ajinomoto AminoScience LLC
4020 Ajinomoto Drive
Raleigh, NC 27610
RE: Project: TCLP 12/10
Pace Project No.: 92229377
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Kevin Adams:
Enclosed are the analytical results for sample(s) received by the laboratory on December 11, 2014.
This report is a summary of the results based upon our understanding of your data quality objectives.
Please contact us if itemized quality control results are needed. These results relate only to the
samples included in this report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Accounts Payable, Ajinomoto AminoScience LLC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 9

aceAnalj cal
www.pacelabs.com
i
Project: TCLP 12/10
Pace Project No.: 92229377
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Arizona Certification #: AZ0735
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification * FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification M 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M! NC030
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Montana Certification #: Cent 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL765
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Washington Certification #: C955
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS.
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 9

' /Analj6cale
- www.pacelabs.com
Project: TCLP 12/10
Pace Project No.: 92229377
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
8800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92229377001 TRP CELLCREAN
EPA 8081
RES
8 PASI-C
EPA 8151
LJM
3 PASI-O
EPA 6010
JMW
7 PASI-A
EPA 7470
HVK
1 PASI-A
EPA 8270
RES
18 PASI-C
EPA 8260
GAW
14 PASI-C
92229377002 SLUDGE
EPA 8081
RES
8 PASI-C
EPA 8151
LJM
3 PASI-O
EPA 6010
JMW
7 PASI-A
EPA 7470
HVK
1 PASI-A
EPA 8270
RES
18 PASI-C
EPA 8260
DLK
14 PASI-C
t
r�.
r—.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 9

axAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: TCLP 12/10
Pace Project No.: 92229377
Sample: TRP CELLCREAN Lab ID: 92229377001 Collected: 12/10/14 11:30
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF
gamma-BHC (Lindane)
ND ug/L
0.50
1
Chlordane (Technical)
ND ug/L
3.0
1
Endrin
ND ug/L
0.50
1
Heptachlor epoxide
ND ug/L
0.50
1
Methoxychlor
ND ug/L
1000
1
Toxaphene
ND ug/L
3.0
1
- Decachlorobiphenyl (S)
0 %
10-138
1 S5
Tetrachloro-m-xylene (S)
0 %
10-110
1 S5
w` 2,4-D
ND mg/L
0.010
1
2,4,5-TP (Silvex)
ND mg/L
0.010
1
2,4-DCAA (S)
79 %
42-142
1
's= Arsenic
`
ND mg/L
0.1050
1
lv Barium
ND mg/L
0.25
1
Cadmium
ND mg/L
0.0050
1
Chromium
ND mg/L
0.025
1
Lead
ND mg/L
0.025
1
Selenium
ND mg/L
0.10
1
Silver
ND mg/L
0.025
1
Mercury
ND ug/L
0.20
1
1,4-Dichlorobenzene
ND ug/L
50.0
1
2,4-Dinitrotoluene
ND ug/L
50.0
1
Hexachloro-1,3-butadiene
ND ug/L
50.0
1
Hexachlorobenzene
ND ug/L
50.0
1
Hexachloroethane
ND ug/L
50.0
1
2-Methylphenol(o-Cresol)
ND ug/L
50.0
1
3&4-Methylphenol(m&p Cresol)
ND ug/L
50.0
1
Nitrobenzene
ND ug/L
50.0
1
Pentachlorophenol
ND ug/L
100
1
Pyridine
ND ug/L
50.0
1
2,4,5-Trichlorophenol
ND ug/L
50.0
1
" 2,4,6-Trichlorophenol
ND ug/L
50.0
1
Nitrobenzene-d5 (S)
38 %
12-102
1 H5
2-Fluorobiphenyl (S)
37 %
13-107
1
- Terphenyl-d14 (S)
35 %
21-132
1
Phenol-d6 (S)
14 %
10-110
1
2-Fluorophenol (S)
20 %
10-110
1
2,4,6-Tribromophenol (S)
39 %
27-108
1
Benzene
ND ug/L
125
25
2-Butanone (MEK)
ND ug/L
250
25
Carbon tetrachloride
ND ug/L
125
25
' Chlorobenzene
ND ug/L
125
25
Chloroform
ND ug/L
125
25
1,4-Dichlorobenzene
ND ug/L
125
25
1,2-Dichloroethane
ND ug/L
125
25
1,1-Dichloroethene .
ND ug/L
125.
25
Tetrachloroethene
ND ug/L
125
25
Trichloroethene
ND ug/L
125
25
Vinyl chloride
ND ug/L
125
25
REPORT OF LABORATORY ANALYSIS
'
This report shall not be reproduced, except in full,
Date: 01 /02/2015 04:30 PM
without the written consent of Pace Analytical Services, Inc..
Qualifiers
I9
Page 4 of 9

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: TCLP 12110
Pace Project No.: 92229377
Sample: TRP CELLCREAN Lab ID: 92229377001 Collected: 12/10/14 11:30
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Qualifiers
1,2-Dichloroethane-d4 (S) 101 % 70-130 25 D3
Toluene-d8 (S) 96 % 67-135 25
4-Bromofluorobenzene (S) 89 % 70-130 25
Sample: SLUDGE Lab ID:
Results reported on a "dry -weight" basis
Parameters Results
92229377002
Units
Collected: 12/10/14 11:30
Report Limit DF
Qualifiers
gamma-BHC (Lindane)
ND ug/L
0.50
1
Chlordane (Technical)
ND ug/L
3.0
1
Endrin
ND ug/L'
0.50
1
Heptachlor epoxide
ND ug/L
0.50
1
Methoxychlor
ND ug/L
1000
1
Toxaphene
ND ug/L
3.0
1
Decachlorobiphenyl (S)
66 %
10-138
1
Tetrachloro-m-xylene (S)
66 %
10-110
1
' 2,4-D
ND mg/L
0.010
11
2,4,5-TP (Silvex)
ND mg/L
0.010
1
2,4-DCAA (S)
77 %
42-142
1,
Arsenic
ND mg/L
0.050
1'
Barium
ND mg/L
0.25
1
Cadmium
ND mg/L
0..0050
1
Chromium
ND mg/L
0.025
1
Lead
ND mg/L
0.025
1
Selenium
ND mg/L
0.10
1
Silver
ND mg/L
0.025
1
Mercury
ND ug/L
0.20
1
1,4-Dichlorobenzene
ND ug/L
10000
10
2,4-Dinitrotoluene
ND ug/L
10000
10
Hexachloro-1,3-butadiene
ND ug/L
10000
10
Hexachlorobenzene
ND ug/L
10000
10
Hexachloroethane
ND ug/L
10000
10
2-Methylphenol(o-Cresol)
ND ug/L
10000
10
3&4-Methylphenol(m&p Cresol)
ND ug/L
10000
10
Nitrobenzene
ND ug/L
10000
10
Pentachlorophenol
ND ug/L
20000
10
Pyridine
ND ug/L
10000
10
2,4,5-Trichlorophenol
ND ug/L
10000
10
2,4,6-Trichlorophenol
ND ug/L
10000
10
Nitrobenzene=d5 (S)
0 %
12-102
10
D3, H5,
'
P3,
S4
' 2-Fluorobiphenyl (S)
0 %
13-107
10
Terphenyl-d14(5)
0 %
21-132
10
'Phenol-d6 (S)
0 %
10-110
10
2-Fluorophenol (S)
0 %
10-110
10
2,4,6-Tribromophenol (S)
0 %
27-108
10
Benzene IND
ug/L
192
38.5
Date: 01 /02/2015 04:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 9

APPENDIX IV
DISTRIBUTION AND MARKETING/SURFACE
DISPOSAL CERTIFICATION

ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Permit Number: WQ0032618 Facility Name: Ajinomoto Amino Science, LLC
Phone: [phone] County: Wake Operator: Kevin Adams
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
W Distribution and Marketing (complete Parts A, B, and.C)
the facility in operation during the past calendar year? ❑d Yes ❑ No If No skip parts A, B, C and certify form below
PART A *: PART B *:
Month Sources & NPDES
January
February
March
April
May
June
July
August
September
October
November
December
Ajinomoto Cell Cream
Ajinomoto Cell Cream
Ajinomoto Cell Cream
WQ0032618
WQ0032618
WQ0032618
Volume (Dry Tons)
Recipient Information
Amendment/Bulking Agent In Residual In
Product Out
Name(s)
Volume (Dry Tons)
Intended Use(s)
0.00 35.69,
35.69
Levern Sykes
35.69
Fescue Pasture
0.00 42.34
42.34
Levern Sykes
42.34
Fescue Pasture
0.00 39.52
39.52
Levern Sykes
39.52
Fescue Pasture
n--f rr--h
11 cc
17-- V-fi a
Ajinomoto Cell Cream
WQ0032618
0.00
27.55
27.55
Ajinomoto Cell Cream
WQ0032618
0.00
25.06
25.06
Ajinomoto Cell Cream
WQ0032618
0.00
23.53
23.53
Ajinomoto Cell Cream
WQ0032618
0.00
23.27
23.27
Ajinomoto Cell Cream
WQ0032618
0.00
27.01
27.01
Ajinomoto Cell Cream
WQ0032618
0.00
22.51
22.51
Ajinomoto Cell Cream
WQ0032618 "
0.00
37.38
37.38
Ajinomoto Cell Cream
WQ0032618
0.00
24.48
24.48
Ajinomoto Cell Cream
WQ0032618
0.00
40.03
40.03
TOTAL ANNUAL DRY TONS
0.00
368.36
368.36
Brent Creech
25.06
Fescue Pasture
Brent Creech
23.53
Fescue Pasture
Jack Carpenter
23.27
Fescue Pasture
Jack Carpenter
27.01
Fescue Pasture
Jack Carpenter
22.51
Fescue Pasture
Jack Carpenter
37.38
Fescue Pasture
Jack Carpenter
24.48
Fescue Pasture
Levern Sykes
40.03
Fescue Pasture
368.36
t C:
lity was compliant during the past calendar year with all conditions of the land application permit ❑d Yes
uding but not limited to items 1-3 below) issued by the Division of Water Quality: © No
11 monitoring was. done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
.11 operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
o contravention of Ground Water Quality Standards occurred at a monitoring well.
xtify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are
ificant penalties for submitting false infor on, including the possibility of fines and imprison ent for knowing violations."
tature ofPermittee Date Sig tore of Preparer**
(if different from Permittee)
reparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Total Number of DMSDF Forms 1
Date