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HomeMy WebLinkAboutAppendix G - Summary of Waste Rock and Process Tailings Geochemical AssessmentPiedmont Lithium Carolinas, Inc. I North Carolina Mining Permit Application Appendices PIEDMONT LITHIUM Appendix G: Summary of Waste Rock and Process Tailings Geochemical Assessment and Addendum Report: Results of Humidity Cell Leaching Tests \ Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont lithium Project August 2019 Prepared by Marshall Miller & Associates 582 Industrial Park Road Bluefield, Virginia 24605-9364 www.mmal.com Prepared for Piedmont Lithium, Inc. 32 North Main Street Ste 100 Belmont, North Carolina 28012 T :77 582 Industrial Park Road, Bluefield, VA 24605-9364 ■ Phone 276.322.5467 www.mmal.com ■ info@mmal.com August 5, 2019 Mr. Patrick Brindle Vice President Piedmont Lithium 32 North Main Street Ste 100 Belmont, NC 28012 Subject: Summary of Waste Rock and Process Tailings Geochemical Assessment — Piedmont Lithium Project Dear Patrick: The following report summarizes the results of assessment to determine the potential for adverse effects to the environment associated with proposed waste rock and process tailings materials to be produced from the proposed Piedmont Lithium mine project near Bessemer City, North Carolina. A preliminary summary of results, titled "PRELIMINARY —Acid Base Accounting (ABA) Results Summary - Piedmont Lithium Project", was submitted on January 25, 2019. The current report contains the results from the initial summary, in addition to various other results from subsequent testing. The geochemical assessment described below includes sampling of both drill core and pilot tailings materials, and laboratory testing including Acid Base Accounting (ABA), Whole Rock Elemental Analysis, and Toxicity Characteristic Leaching Procedure (TCLP). Additional Humidity Cell tests are currently underway. Sincerely, MARSHALL MILLER & ASSOCIATES, INC. Ronald H. Mullennex, CPG, CGWP Senior Principal Direct Line: 304-809-0705 ron.mullennex@mmal.com /drd Attachments File: Final-PLIT104 Summary Report-2019 08 05.docx Kevin Andrews, CPG Vice President/Supervisory Geologist Direct Line: 1 276 970 6065 Email: kevin.andrews@mmal.com ENERGY & MINERAL RESOURCES ■ HYDROGEOLOGY & GEOLOGY ■ GEOPHYSICAL LOGGING SERVICES CARBON MANAGEMENT ■ EXPERT WITNESS TESTIMONY ■ MINING ENGINEERING ■ PETROLEUM ENGINEERING Summary of Waste Rock and Process Tailings GeochemicaI Assessment Piedmont Lithium Project ► ► ' ► ► �� August 2019 Table of Contents 1 Introduction.........................................................................................................................1 2 Summary..............................................................................................................................1 3 Waste Rock Analysis............................................................................................................. 2 3.1 Acid Base Accounting (ABA)/Sulfur Fractionation for Waste Rock Samples.....................4 3.2 Elemental Analyses of Waste Rock Samples...................................................................... 7 3.2.1 Further Investigation of Chromium Presence..................................................................................8 3.3 Toxicity Characteristic Leaching Procedure (TCLP) for Waste Rock Samples .................... 8 3.4 Waste Rock - Summary.................................................................................................... 10 4 Tailings...............................................................................................................................11 4.1 Acid Base Accounting (ABA) for Tailings Samples............................................................ 11 4.2 Elemental Analyses for Tailings Samples......................................................................... 12 4.3 Toxicity Characteristic Leach Procedure (TCLP) for Tailings Samples .............................. 13 4.4 Tailings - Summary........................................................................................................... 14 5 Conclusions........................................................................................................................ 15 6 Ongoing Work— Humidity Cells........................................................................................... 15 Appendices A...................................................................................... ABA Lab Sheets for Waste Rock and Tailings B...............................................................................Sulfur Fractionation Results for Waste Rock Only C................................................................. Elemental Analysis Summary for Waste Rock and Tailings D.......................................................... Chromium Speciation Results For Select Waste Rock Samples E............................................................................................................TCLP — Waste Rock and Tailings MARSHALL MILLER & AssociATE5, INC. ;jHjkLLhNLLE ES ° 1 Introduction Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 Piedmont Lithium (Piedmont) tasked Marshall Miller & Associates (MM&A) with designing and implementing a geochemical sampling and analysis program to include both waste rock (overburden) and process tailings. The purpose of the assessment is to examine the potential for the waste rock and tailings generated from the proposed Piedmont Lithium Project to have adverse effects on the environment. With regard to the waste rock, the program included sampling and testing of 101 composited rock core samples from 13 different core holes distributed throughout the four main pit areas. Sampled hole locations and depth intervals in the holes were designed to provide an evenly distributed assessment of the proposed mine area. The core samples were collected by both MM&A and Piedmont Lithium geologists. The program also included 10 process tailings samples collected from pilot testing activities. Tailings sample collection was conducted by the Minerals Research Laboratory (MRL) at NC State University in Asheville, North Carolina. Analyses conducted on the waste rock and tailings samples included Acid Base Accounting (ABA), "whole rock" elemental determination, and Toxicity Characteristic Leaching Procedure (TCLP). Where applicable, the ABA analyses results were supplemented with sulfur fractionation (sulfur forms) analyses to better determine the distribution of sulfidic (pyritic) sulfur in selected samples. In addition, selected waste rock and tailings samples are currently being analyzed for leachability via humidity cell testing. 2 Summary The results of the waste rock analyses indicate no significant potential for the material to produce acidic conditions. Paste pH values for the samples are typically between 9 and 10, with only shallower samples of saprolitic rock exhibiting lower paste pH values in the 5-6 range. Total Sulfur for the waste rock samples is generally in the range of 0.01 to 0.3 percent, with only three of the 101 samples having a total sulfur content greater than 0.5 percent. Samples exhibiting a sulfur content greater than 0.2 percent were further analyzed using a sulfur fractionation procedure. Results of the sulfur fractionation analyses indicate that the total pyritic sulfur (acid -producing) present in the samples is very low. With consideration of the sulfur forms, results show that all waste rock samples exhibit an excess alkalinity condition. Similarly, ABA analyses for the tailings samples indicate very low Total Sulfur content (0.01 percent), high paste pH values (9.0-9.6), and excess neutralization potential (that is, greater acid - neutralizing potential than acid -generating potential) for all tailings samples. Waste rock and tailings samples were also analyzed to determine their overall elemental constituents, as a means for better understanding the "whole rock" components of the materials. The elemental MARSHALL MILLER & AssoclATES INC. ljlHUIL%NNLLE SOLI ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 analyses results were compared against relevant regulatory guidelines to screen for potentially problematic components. The ABA and elemental analyses results were used as a guide for selection of a representative set of waste rock and tailings samples for further testing via TCLP analysis. The TCLP procedure is a short- term but aggressive test for detecting contaminants that may leach from the samples. Results of the TCLP testing were compared against the EPA's "D" list, a list of regulatory levels for the "toxicity" characteristic as determined specifically from the TCLP test. The TCLP results indicate that all of the samples yielded results well below D list toxicity threshold levels. Overall, results of this assessment indicate that acidic drainage is not expected to be released from either the waste rock (overburden) or the process tailings. In addition, consideration of whole rock elemental and TCLP test results does not indicate the potential for leaching hazardous levels of contaminants, as defined by EPA's D list. While the testing done to date does not indicate the potential for adverse effects from the waste rock or tailings, additional humidity cell leach testing is currently underway. The humidity cell test results are expected to further confirm the current results. 3 Waste Rock Analysis Samples representative of waste rock were collected from exploration drill core in November 2018 by a team of geologists from both MM&A and Piedmont. In total, 101 composite core samples were collected from core holes stored in the Piedmont core storage building near Lincolnton, North Carolina. The following table summarizes the number of samples collected from each sampled hole. Hole NumberNumber of - 18-BD-205 . 13 17-BD-45 4 18-BD-140 6 17-BD-65A 8 18-BD-226 7 17-BD-112 6 18-BD-131 8 18-BD-183 8 18-BD-214 7 18-BD-207 9 18-BD-212 7 18-BD-197 7 18-BD-177 11 TOTAL 101 MARSHALL MILLER & ASSOc1ATES INC. 2 ljlHUIL%NNLLE SOCI ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 The figure below shows the distribution of the sampled holes. The smaller black dots are locations of other exploration holes that were not sampled. Figure 1: Distribution of Sampled Holes for Waste Rock Analysis 18-BD-197 North Pit a 18-BD.f77 17'BD 65A. _ 18-BD-131 �Ic' • 18-BD-226 ' West'Plt, • �� C 18- BD' 140 18-BD-212 17.- D 132 \ 1 HEPH ZIBAH Ct{IURCH R6 1 Q -BD-214 � • Soufh Pit ,,. r 18-BD'2o5 17 W _ •SNitheast Pit Splits of material from the 101 core samples were first analyzed for ABA and then packaged and shipped to SGS Laboratory for elemental analysis. MARSHALL MILLER & ASSOc1ATES INC. 3 ljlHUIL%NNLLE SOLI ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 3.1 Acid Base Accounting (ABA)/Sulfur Fractionation for Waste Rock Samples An important consideration in handling and disposing of waste rock is whether, and to what degree, the rock may generate acid drainage as it weathers upon exposure to oxygen and water. Generally, acidic, low -pH conditions (acid rock drainage, orARD) promote dissolution and leaching of metals from rock. The potential for acid generation is principally determined by the sulfidic sulfur content of the rock; and the degree of acid -neutralizing (alkaline) minerals that may also be present. The Acid -Base Account (ABA) test was developed to assess the acid -producing and acid -neutralizing potential of rock materials, and is a well -accepted, standard procedure for that purpose in the mining industry. As a conservative measure, the possible acid -producing character of each of the 101 samples was assessed on the basis of its total sulfur content. Only nine of the 101 samples exhibited a total sulfur content of 0.2 percent or greater (maximum value was 0.73 percent). The 92 samples with less than 0.2 percent total sulfur content have virtually no potential to generate significant acid. The nine samples with more than 0.2 percent total sulfur were considered to possibly have some mild acid -producing potential, depending upon the form of sulfur present and the presence or absence of acid -neutralizing minerals. Subsequent analyses of sulfur forms in those samples show that very little of the sulfur is in sulfidic form (maximum is only 0.06 percent), and thus the acid -producing potential is quite low to non-existent. Further, comparison of neutralizing potential to maximum -possible acid - generating potential (NP/MPA ratio) reveals that the neutralizing potential (NP) is in every instance several times the magnitude of the maximum potential acidity (MPA) (see Table 1 below, and laboratory test results in Appendix A [ABA] and Appendix B (sulfur fractionation]). In summary, results of the ABA and sulfur fractionation analyses show the planned waste rock material to have virtually no likelihood of generating acidic drainage, and therefore relatively low potential for leaching of most metals. Table 1: Waste Rock - Summary of ABA/Sulfur Fractionation Core Client Sample Id Interval (meters) Top I Bottom Desc Reaction to HCl Total Sulfur Total Pyritic Sulfur Paste pH [SU ) % Sulfur Max Pot Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio % Sulfur Max Pot Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio 17-BD-45 17-BD-45-1 0.00 7.92 SAP 0 0.01 0.28 0.75 0.47 2.64 5.1 17-BD-45-2 7.92 15.54 ROCK 0 0.01 0.31 2.50 2.19 8.00 5.7 17-BD-45-3 24.54 37.76 ROCK 0 0.05 1.43 10.00 8.57 6.98 6.4 17-BD-45-4 39.12 61.04 ROCK 0 0.01 0.26 7.00 6.74 26.51 8.9 17-BD-65A 17-BD-65A-1 0.00 8.30 SAP 0 0.01 0.31 0.75 0.44 2.40 6.3 17-BD-65A-2 8.30 13.60 ROCK 0 0.01 0.31 11.00 10.69 35.20 7.8 17-BD-65A-3 13.601 27.74 ROCK 0 0.11 3.56 6.50 2.94 1.82 9.7 17-BD-65A-4 27.74 41.58 ROCK 1 0.05 1.60 21.75 20.15 13.59 10.1 17-BD-65A-5 41.58 64.05 ROCK 0 0.13 4.03 6.75 2.72 1.67 10.0 17-BD-65A-6 64.05 80.24 ROCK 0 0.10 3.16 9.75 6.59 3.09 10.0 17-BD-65A-7 80.24 96.13 ROCK 0 0.04 1.20 12.50 11.30 10.44 10.0 17-BD-65A-8 114.59 134.041 ROCK 1 1 1 0.18 1 5.47 1 18.251 12.781 3.341 i i i i10.2 MARSHALL MILLER & ASsoc1ATES INC. 4 Summary of Waste Rock and Process Tailings GeochemicaI Assessment HKLLNNLLE SOLI ES` Piedmont Lithium Project August 2019 Core Client Sample Id Interval (meters) Top Bottom Desc Reaction to HCI Total Sulfur Total Pyritic Sulfur Paste pH (SU ) % Sulfur Max Pot Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio % Sulfur Max Pot Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio 17-BD-112 17-BD-112-1 0.00 23.08 SAP 0 0.01 0.31 4.25 3.94 13.60 5.6 17-BD-112-2 23.08 38.36 ROCK 0 0.11 3.38 10.50 7.13 3.11 9.9 17-BD-112-3 42.53 67.00 ROCK 0 0.08 2.45 11.00 8.55 4.50 10.0 17-BD-112-4 67.00 89.50 ROCK 0 0.10 3.09 9.25 6.16 3.00 9.5 17-BD-112-5 89.50 108.93 ROCK 0 0.07 2.14 9.00 6.86 4.21 9.7 17-BD-112-6 112.54 137.00 ROCK 0 0.04 1.29 8.50 7.21 6.57 1 9.7 18-BD-131 18-BD-131-1 78.95 84.88 ROCK 0 0.10 3.10 8.50 5.40 2.74 9.9 18-BD-131-2 90.50 93.32 ROCK 0 0.07 2.23 7.75 5.52 3.47 10.2 18-BD-131-3 98.75 113.10 ROCK 0 0.30 9.31 9.00 -0.31 0.97 0.01 0.31 9.00 8.69 28.80 9.9 18-BD-131-4 125.57 127.21 ROCK 0 0.12 1 3.75 7.251 3.50 1.93 10.0 18-BD-131-5 132.91 150.19 ROCK 0 0.08 2.56 5.75 3.19 2.24 9.7 18-BD-131-6 156.00 158.88 ROCK 0 0.23 7.13 6.75 -0.38 0.95 <0.01 0.31 6.75 6.44 21.60 9.2 18-BD-131-7 172.80 176.00 ROCK 0 0.11 3.31 7.75 4.44 2.34 9.7 18-BD-131-8 184.55 187.50 ROCK 0 0.05 1.43 10.25 8.83 7.19 9.5 18-BD-140 18-BD-140-1 65.00 87.88 ROCK 0 0.11 3.56 6.50 2.94 1.82 9.9 18-BD-140-2 87.88 101.30 ROCK 0 0.01 1 0.45 9.501 9.05 21.11 9.9 18-BD-140-3 110.50 136.70 ROCK 0 0.10 3.16 9.00 5.84 2.85 9.7 18-BD-140-4 136.70 156.55 ROCK 1 0.03 0.91 16.50 15.59 18.08 9.2 18-BD-140-5 164.28 202.50 ROCK 0 0.07 2.33 11.50 9.17 4.93 9.7 18-BD-140-6 202.50 mZ32.50 ROCK 0 0.10 2.97 9.25 6.281 3.12 9.7 18-BD-177 18-BD-177-1 0.00 3.00 OVB 0 0.02 0.59 2.75 2.16 4.66 5.6 18-BD-177-2 3.00 12.80 SAP 0 0.01 1 0.31 6.75 6.44 21.60 6.2 18-BD-177-3 12.80 18.53 ROCK 0 0.01 0.31 12.75 12.44 40.80 7.9 18-BD-177-4 18.53 47.36 ROCK 0 0.05 1.62 9.50 7.88 5.88 9.1 18-BD-177-5 56.601 73.00 ROCK 0 0.07 2.10 14.001 11.90 6.67 1 1 9.5 18-BD-177-6 75.971 80.43 ROCK 0 0.07 2.16 7.00 4.84 3.24 9.7 18-BD-177-7 81.91 90.32 ROCK 0 0.11 3.47 11.75 8.28 3.39 9.5 18-BD-177-8 91.15 94.25 ROCK 0 0.14 4.22 8.75 4.53 2.07 9.8 18-BD-177-9 102.97 105.39 ROCK 1 0 0.12 1 3.59 10.25 6.66 2.851 9.5 18-BD-177-10 107.93 127.80 ROCK 0 0.32 10.03 11.75 1.72 1.17 <0.01 0.31 11.75 11.44 37.60 8.9 18-BD-177-11 129.75 155.00 ROCK 0 0.03 1.01 1 10.75 9.74 10.64 1 1 9.7 18-BD-183 18-BD-183-1 0.00 3.02 OVB 0 0.01 0.45 1.25 0.80 2.78 5.5 18-BD-183-2 3.02 19.89 SAP 0 0.01 0.31 3.00 2.69 9.60 5.5 18-BD-183-3 19.89 27.51 ROCK 0 0.05 1.68 11.25 9.57 6.70 8.8 18-BD-183-4 47.35 71.94 ROCK 1 0 0.07 1 2.29 9.75 7.461 4.26 1 9.7 18-BD-183-5 71.94 90.23 ROCK 0 0.10 3.02 10.00 6.98 3.31 10.1 18-BD-183-6 90.23 111.56 ROCK 0 0.11 3.28 11.50 8.22 3.50 10.0 18-BD-183-7 111.56 132.82 ROCK 0 0.06 1.83 12.00 10.17 6.56 10.1 18-BD-183-8 132.821 150.67 ROCK 0 0.07 2.10 11.00 8.90 5.24 1 9.7 18-BD-183-8 132.82 150.67 ROCK 0 I 0.07 2.10 11.001 8.90 5.24 9.7 18-BD-197 18-BD-197-1 0.00 6.00 ROCK 0 0.01 0.31 7.50 7.19 24.00 5.5 18-BD-197-2 6.00 18.70 ROCK 0 0.10 3.22 11.00 7.78 3.42 5.5 18-BD-197-3 20.00 35.09 ROCK 0 0.08 2.40 10.75 8.35 4.47 8.8 18-BD-197-4 39.64 51.94 ROCK 0 0.01 0.25 56.50 56.25 222.39 9.7 18-BD-197-5 53.07 66.59 ROCK 0 0.16 5.00 12.50 7.50 2.50 10.1 18-BD-197-6 67.85 83.17 ROCK 0 0.12 3.66 7.75 4.09 2.121 10.0 18-BD-197-7 1 88.701 103.14 ROCK 2 1 0.04 1 1.24 1 26.251 25.011 21.111 1 1 1 1 1 10.1 MARSHALL MILLER & Assoc1ATE5, INC. Summary of Waste Rock and Process Tailings GeochemicaI Assessment HKLLNNLLE SOLI ES` Piedmont Lithium Project August 2019 Core Client Sample Id Interval (meters) Top I Bottom Desc Reaction to HCI Total Sulfur Total Pyritic Sulfur Paste pH (SU ) % Sulfur Max Pot Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio % Sulfur Max Pot I Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio 18-BD-205 18-BD-205-1 0.00 1.50 OVB 0 0.01 0.29 3.00 2.71 10.27 6.1 18-BD-205-2 1.50 2.50 ROCK 0 0.01 0.31 6.00 5.69 19.20 6.0 18-BD-205-3 2.50 25.00 ROCK 0 0.01 0.31 11.50 11.19 36.80 6.8 18-BD-205-4 25.00 45.00 ROCK 0 0.11 3.38 14.25 10.88 4.22 8.9 18-BD-205-5 45.00 65.00 ROCK 0 0.01 0.31 10.50 10.19 33.60 9.8 18-BD-205-6 65.001 82.15 ROCK 0 1 0.04 1.30 1 9.00 7.70 6.91 9.9 18-BD-205-7 84.201 101.40 ROCK 0 0.01 0.31 9.75 9.44 31.20 9.8 18-BD-205-8 112.47 130.55 ROCK 0 0.07 2.24 7.75 5.51 3.46 9.8 18-BD-205-9 132.56 139.86 ROCK 0 0.01 0.31 7.00 6.69 22.40 10.1 18-BD-205-10 139.86 142.00 ROCK 0 0.01 0.31 7.50 7.19 24.00 9.7 18-BD-205-11 142.00 153.00 ROCK 1 0.01 0.27 22.50 22.23 82.10 10.1 18-BD-205-12 153.00 165.00 ROCK 0 0.08 2.35 9.75 7.40 4.14 10.2 18-BD-205-13 165.001 173.00 ROCK 0 0.04 1.29 8.50 7.21 6.57 10.2 18-BD-207 18-BD-207-1 0.001 21.00 OVB 0 0.02 0.49 2.25 1.76 4.56 5.8 18-BD-207-2 21.00 25.00 SAP 0 0.06 1.93 9.75 7.83 5.06 6.5 18-BD-207-3 27.00 39.58 ROCK 0 0.32 10.13 8.50 -1.63 0.84 <0.01 0.31 8.50 8.19 27.20 9.2 18-BD-207-4 49.05 71.05 ROCK 1 0.14 4.23 22.25 18.02 5.25 9.8 18-BD-207-5 71.05 87.80 ROCK 0 0.51 15.90 7.50 -8.40 0.47 0.01 0.31 7.50 7.19 24.00 10.0 18-BD-207-6 102.37 129.02 ROCK 0 0.73 22.71 8.00 -14.71 0.35 0.06 1.86 8.00 6.14 4.30 9.9 18-BD-207-7 129.02 158.55 ROCK 0 0.66 20.68 4.75 -15.93 0.23 0.01 0.31 4.75 4.44 15.20 9.9 18-BD-207-8 162.361 193.28 ROCK 0 0.26 7.99 6.00 -1.99 0.75 0.03 0.86 6.00 5.14 6.98 10.2 18-BD-207-9 195.35 217.19 ROCK 0 0.06 1.77 18.25 16.48 10.30 10.2 18-BD-212 18-BD-212-1 0.00 5.05 SAP 0 0.01 0.31 1.00 0.69 3.20 5.7 18-BD-212-2 5.80 15.36 ROCK 0 0.01 0.31 6.25 5.94 20.00 7.4 18-BD-212-3 15.36 34.65 ROCK 0 0.07 1 2.33 7.251 4.92 3.111 4P 9.9 18-BD-212-4 34.65 55.00 ROCK 0 0.12 3.59 9.00 5.41 2.50 9.8 18-BD-212-5 55.00 79.72 ROCK 0 0.14 4.41 6.50 2.09 1.48 10.1 18-BD-212-6 95.681 105.39 ROCK 0 0.15 4.78 11.75 6.97 2.46 10.0 18-BD-212-7 105.39 136.37 ROCK 0 0.07 2.12 15.00 12.88 7.08 9.7 18-BD-214 18-BD-214-1 1.50 10.90 SAP 0 0.01 0.26 4.00 3.74 15.48 5.3 18-BD-214-2 10.90 22.601 SAP 0 1 0.01 0.31 1 2.501 2.19 8.001 1 6.6 18-BD-214-3 22.60 37.45 ROCK 2 0.14 4.44 26.25 21.81 5.92 9.4 18-BD-214-4 39.50 62.45 ROCK 0 0.28 8.69 10.75 2.06 1.24 0.03 0.94 10.75 9.81 11.47 9.5 18-BD-214-5 66.47 72.55 ROCK 2 0.08 2.52 82.50 79.98 32.71 9.6 18-BD-214-6 75.27 95.20 ROCK 0 0.12 3.81 15.25 11.44 4.00 9.5 18-BD-214-7 95.20 118.60 ROCK 0 0.21 6.50 11.00 4.50 1.69 0.05 1.56 11.00 9.441 7.04 9.6 18-BD-197 18-BD-197-1 0.00 6.00 ROCK 0 0.01 0.31 7.50 7.19 24.001 5.5 18-BD-197-2 6.00 18.70 ROCK 0 0.10 1 3.22 11.001 7.78 3.42 5.5 18-BD-197-3 20.00 35.09 ROCK 0 0.08 2.40 10.75 8.35 4.47 8.8 18-BD-197-4 39.64 51.94 ROCK 0 0.01 0.25 56.50 56.25 222.39 9.7 18-BD-197-5 53.07 66.59 ROCK 0 0.16 5.00 12.50 7.50 2.50 10.1 18-BD-197-6 67.851 83.17 ROCK 1 0 0.12 3.66 7.75 4.09 2.12 10.0 18-BD-197-7 88.70 103.14 ROCK 2 0.04 1.24 26.25 25.01 21.111 1 10.1 18-BD-205 18-BD-205-1 0.00 1.50 OVB 0 0.01 1 0.29 3.001 2.71 10.27 6.1 18-BD-205-2 1.50 2.50 ROCK 0 0.01 0.31 6.00 5.69 19.20 6.0 18-BD-205-3 2.50 25.00 ROCK 0 0.01 0.31 11.50 11.19 36.80 6.8 18-BD-205-4 25.00 45.00 ROCK 0 0.11 3.38 14.25 10.88 4.22 8.9 18-BD-205-5 45.00 65.00 ROCK 0 0.01 0.31 10.50 10.19 33.60 9.8 18-BD-205-6 65.00 82.15 ROCK 1 0 0.04 1.30 9.00 7.701 6.91 9.9 18-BD-205-7 84.20 101.40 ROCK 0 0.01 0.31 9.75 9.441 31.20 9.8 18-BD-205-8 112.47 130.55 ROCK 0 1 0.07 2.24 7.75 5.51 3.46 9.8 18-BD-205-9 132.56 139.86 ROCK 0 0.01 0.31 7.00 6.69 22.40 10.1 18-BD-205-10 139.86 142.00 ROCK 0 0.01 0.31 7.50 7.19 24.00 9.7 18-BD-205-11 1 142.001 153.00 ROCK 1 0.01 0.27 1 22.50 22.23 82.101 10.1 18-BD-205-12 1 153.001 165.00 ROCK 0 0.08 2.35 1 9.75 7.40 4.14 10.2 18-BD-205-13 1 165.001 173.001 ROCK 1 0 0.04 1 1.29 1 8.501 7.211 10.2 MARSHALL MILLER & Assoc1ATE5, INC. ;jHjkLLhNLLE ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 Core Client Sample Id Interval (meters) Top I Bottom Desc Reaction to HCl Total Sulfur Total Pyritic Sulfur Paste pH (SU ) % Sulfur Max Pot Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio % Sulfur Max Pot Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio 18-BD-207 18-BD-207-1 0.00 21.00 OVB 0 0.02 0.49 2.25 1.76 4.56 5.8 18-BD-207-2 21.00 25.00 SAP 0 0.06 1.93 9.75 7.83 5.06 6.5 18-BD-207-3 27.00 39.58 ROCK 0 0.32 10.13 8.50 -1.63 0.84 <0.01 0.31 8.50 8.19 27.20 9.2 18-BD-207-4 49.05 71.05 ROCK 1 0.14 4.23 22.25 18.02 5.25 9.8 18-BD-207-5 71.05 87.80 ROCK 0 0.51 15.90 7.50 -8.40 0.47 0.01 0.31 7.50 7.19 24.00 10.0 18-BD-207-6 102.37 129.02 ROCK 0 0.73 22.71 8.00 -14.71 0.35 0.06 1.861 8.00 6.14 4.30 9.9 18-BD-207-7 129.02 158.55 ROCK 0 0.66 20.68 4.75 -15.93 0.23 0.01 0.31 4.75 4.44 15.20 9.9 18-BD-207-8 162.36 193.28 ROCK 0 0.26 7.99 6.00 -1.99 0.75 0.03 0.86 6.00 5.14 6.98 10.2 18-BD-207-9 195.35 217.19 ROCK 0 1 0.06 1.77 18.25 16.48 10.301 10.2 18-BD-212 18-BD-212-1 0.00 5.05 SAP 0 0.01 0.31 1.00 0.69 3.20 5.7 18-BD-212-2 5.80 15.36 ROCK 0 0.01 0.31 6.25 5.94 20.00 7.4 18-BD-212-3 15.36 34.65 ROCK 0 0.07 2.33 7.25 4.92 3.11 1 9.9 18-BD-212-4 34.65 55.00 ROCK 0 0.12 3.59 9.00 5.41 2.50 9.8 18-BD-212-5 55.00 79.72 ROCK 0 0.14 4.41 6.50 2.09 1.48 10.1 18-BD-212-6 95.68 105.39 ROCK 0 0.15 4.78 11.75 6.97 2.46 10.0 18-BD-212-7 105.39 136.37 ROCK 0 1 0.07 2.12 15.00 12.881 7.08 1 9.7 18-BD-214 18-BD-214-1 1.50 10.90 SAP 0 0.01 0.26 4.00 3.74 15.481 5.3 18-BD-214-2 10.90 22.601 SAP 0 0.01 0.31 2.50 2.19 8.00 1 6.6 18-BD-214-3 22.60 37.45 ROCK 2 0.14 4.44 26.25 21.81 5.92 9.4 18-BD-214-4 39.50 62.45 ROCK 0 0.28 8.69 10.75 2.06 1.24 0.03 0.94 10.75 9.81 11.47 9.5 18-BD-214-5 66.47 72.55 ROCK 2 0.08 2.52 82.50 79.98 32.71 9.6 18-BD-214-6 75.27 95.20 ROCK 0 0.12 3.81 15.25 11.44 4.00 9.5 18-BD-214-7 95.20 118.60 ROCK 0 0.21 6.50 11.00 4.50 1.69 0.05 1.56 11.00 9.44 7.04 9.6 18-BD-226 18-BD-226-1 0.00 3.17 OVB 0 0.01 0.37 0.50 0.13 1.37 5.3 18-BD-226-2 3.17 18.60 SAP 0 0.01 0.31 6.50 6.19 20.80 6.3 18-BD-226-3 18.60 46.29 ROCK 0 0.06 1.77 8.25 6.48 4.67 8.6 18-BD-226-4 49.30 69.60 ROCK 0 0.07 2.26 6.50 4.24 2.88 9.2 18-BD-226-5 75.30 95.82 ROCK 0 0.11 3.34 6.75 3.41 2.02 9.6 18-BD-226-6 1 101.72 1 116.361 ROCK 1 0 1 0.10 1 3.19 1 8.001 4.811 2.511 1 9.5 18-BD-226-7 1 122.381 134.171 ROCK 1 0 1 0.13 1 3.91 1 8.501 4.591 2.181 1 1 19.7 3.2 Elemental Analyses of Waste Rock Samples A further investigative step involved elemental analyses of the 101 core samples by ICP-OES/MS (see results in Appendix C). Results of these analyses indicate the rock constituency, but do not indicate the propensity for leaching of constituents to the environment. The results afford a guide for use in assessing the need for further tests of leachability, and for what parameters. North Carolina has no regulatory standards specific to elemental concentrations in mine waste rock. For reference and screening purposes, the elemental analyses results were compared against North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals for industrial soils and protection of groundwater'. Results indicate that the rock contains manganese and lithium at concentrations that exceed the preliminary screening level goal for industrial soil; and that manganese, lithium, iron, cobalt, and thallium commonly occur at concentrations greater than the preliminary soil goal for protection of groundwater. While the subject waste rock is not soil and is 1 North Carolina Department of Environmental Quality, "Preliminary Soil Remediation Goals (PSRG)," February 2018 (based on November 2017 USEPA Screening Tables). MARSHALL MILLER & Assoc1ATES INC. 7 ;jHjkLLNNLLE ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 unlikely to leach contaminants as readily as industrial soil, the comparisons were used as a guide for further testing of leachability. A commonly -used leachability test is the Toxicity Characteristic Leaching Procedure (TCLP), which is designed to mimic the pH conditions in a municipal landfill (that is, a moderately acidic environment, which is unlikely to be found in disposal of the subject waste rock). The USEPA has established toxicity characteristic limits for leachability of eight metals (the RCRA 8 list) using the TCLP test. However, it should be noted that, because of dilution factors involved in the TCLP, a whole -rock elemental concentration of less than 20 times the RCRA TCLP limit could not exceed the regulatory TCLP limit, even if the entirety of that element were to leach out. Comparison of concentrations in the subject rock samples to 20X TCLP limit for the RCRA 8 metals shows that none of those metals except chromium could potentially exhibit toxic concentrations, and such levels of chromium occur only occasionally. The regulatory TCLP limit for chromium is based upon the hexavalent form of the element, which is potentially carcinogenic and therefore has a very low regulatory threshold of concern. Chromium in the more common trivalent form is not regarded as highly toxic, and is not readily mobile in the environment. 3.2.1 Further Investigation of Chromium Presence To further investigate the chromium concentrations in the waste rock, chromium speciation tests were conducted to differentiate trivalent chromium from hexavalent chromium in both solid waste rock material and from the results of the initial flush ("Time 0") of ongoing humidity cell testing. The speciation testing was conducted on samples 18-BD-205-7 and 18-BD-212-6. As expected, results of the speciation tests for both solid material and humidity cell effluent indicate that the chromium in the subject rock is principally or entirely in its reduced, trivalent form (in the mineral Chromite) which is not readily mobile nor strongly toxic. In sample 18-BD-205-7 (containing 45 µg/g of chromium as determined by ICP-OES/MS), the concentration of hexavalent chromium in the solid is below detection (DL = 0.2 µg/g) and the "Time 0" humidity cell effluent is also below the detection limit for both trivalent chromium (DL= 0.08 µg/L) and hexavalent chromium (DL= 0.2 jig/Q. In sample 18-BD-212-6 (containing 490 µg/g of total chromium as determined by ICP-OES/MS), the concentration of hexavalent chromium in the solid is below detection, while the first flush of leachable chromium from the humidity cell contained no detectable hexavalent chromium and only 0.09 µg/L of trivalent chromium. In short, the chromium present in these samples is essentially all in trivalent form and has very low leachability, even under the moderately aggressive conditions of the TCLP test (pH of 5, pulverized material). Laboratory results sheets for the chromium speciation testing for solid material and for the initial "Time 0" effluent from ongoing humidity cell testing are included in Appendix D. 3.3 Toxicity Characteristic Leaching Procedure (TCLP) for Waste Rock Samples The TCLP test is frequently used for assessing parameter leachability and for classification of waste material as hazardous or non -hazardous. As with most laboratory leach tests, the TCLP involves MARSHALL MILLER & ASSOc1ATES INC. 8 ljlHUIL%NNLLE SOLI ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 acceleration of the leaching process in a controlled environment. The TCLP test assumes that the leaching reaction of the waste rock occurs rapidly. In many ways, the TCLP test can be considered a "worst case" test, as testing involves pulverized material (increased surface area relative to generally larger particles that may be expected in the proposed waste disposal), significant agitation of the material, and use of a lower pH (5) water than is expected to occur in the waste disposal structures. The TCLP test results for the waste rock are summarized in the table below and laboratory data is included in Appendix E. Where applicable, the Toxicity Characteristic Limit is shown on the table (third column from left). The results are that leachate concentrations of elements for which a Toxicity Characterization Limit is established (including chromium) are all well below (by orders of magnitude) the respective toxicity threshold values reflected on the EPA D list of potentially hazardous waste elements. The prominent metal released by the TCLP is iron, at 18.7 to 61.5 mg/L in the TCLP leachate. The iron mobilization is strongly promoted by the TCLP conditions of pH 5 water and pulverized sample material. It is very unlikely that leaching conditions within the waste rock disposal structures will be that aggressive, and the TCLP result represents worst -case conditions that are unlikely to occur in the field. MARSHALL MILLER & ASSOCIATES INC. 9 HKLLNNLLE SOLI ES` Summary of Waste Rock and Process Tailings GeochemicaI Assessment Piedmont Lithium Project August 2019 Table 2: Waste Rock - Summary of TCLP Results (mg/Q Parameter DL Toxicity Character. Limit 18-BD- 205-7 17-DB- 45-3 17-BD- 65A-8 18-BD- 183-8 18-BD- 214-6 18-BD- 207-6 18-BD- 212-6 18-BD- 177-10 Sample weight (g) 100 100 100 100 100.0 100 100 100 Ext Fluid (#1 or #2) 1 1 1 1 1 1 1 1 Ext Volume (mQ 2000 2000 2000 2000 2000 2000 2000 2000 Final pH (no unit) 0.01 5.05 4.95 5.13 5.00 5.01 5.00 5.02 5.08 Hg 0.00001 0.2 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 Al 0.001 0.865 0.529 0.701 0.849 0.789 0.795 0.771 0.607 As 0.0002 5.0 0.0011 0.0009 0.0010 0.0014 0.0007 0.0009 0.0023 0.0015 Ag 0.00005 5.0 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 Ba 0.00002 100.0 0.181 0.194 0.156 0.246 0.203 0.125 0.228 0.298 Be 0.000007 0.000312 0.00119 0.00119 0.000984 0.000139 0.000438 0.00121 0.000202 B 0.002 0.112 0.242 0.161 0.070 0.071 0.060 0.061 0.051 Bi 0.000007 0.000010 < 0.000007 0.000014 < 0.000007 < 0.000007 < 0.000007 0.000113 0.000017 Ca 0.01 71.7 7.49 150 25.2 23.9 34.7 62.8 87.4 Cd 0.000003 1.0 0.000107 0.000122 0.000327 0.000085 0.000042 0.000062 0.000147 0.000393 Co 0.000004 0.00416 0.0538 0.00445 0.00442 0.00660 0.00417 0.0276 0.00532 Cr 0.00008 5.0 0.384 0.122 0.233 0.374 0.384 0.259 0.235 0.409 Cu 0.0002 0.0404 0.0175 0.0054 0.0261 0.0063 0.0024 0.0059 0.0022 Fe 0.007 53.0 18.7 38.5 54.1 61.5 40.9 40.3 55.6 K 0.009 6.48 6.79 7.70 9.61 4.86 4.18 12.4 9.52 Li 0.0001 0.128 0.156 0.150 0.161 0.118 0.119 0.166 0.169 Mg 0.001 1.18 1.75 3.39 1.25 1.16 1.02 2.27 1.01 Mn 0.00001 0.615 0.389 2.02 0.623 0.579 0.455 1.23 2.01 Mo 0.00004 0.0226 1 0.00382 0.0108 0.0267 0.0115 0.0170 0.0234 0.0544 Na 0.01 1290 1340 1250 1340 1370 1330 1350 1320 Ni 0.0001 0.0330 0.0435 0.0250 0.0326 0.0311 0.0234 0.0427 0.0303 P 0.003 0.014 0.010 0.010 0.008 0.010 0.007 0.016 0.014 Pb 0.00001 5.0 0.00164 0.00041 0.00273 0.00355 0.00210 0.00095 0.00240 0.00175 Sb 0.0009 0.0015 < 0.0009 < 0.0009 < 0.0009 < 0.0009 0.0011 0.0011 < 0.0009 Se 0.00004 1.0 0.00013 0.00011 0.00012 0.00013 0.00006 0.00007 0.00013 0.00013 Si 0.02 2.54 1.82 2.50 2.62 2.86 2.12 2.05 2.16 Sn 0.00006 0.00008 < 0.00006 0.00006 0.00013 0.00010 < 0.00006 < 0.00006 0.00010 Sr 0.00002 0.0478 0.0571 0.276 0.0887 0.0593 0.0368 0.101 0.0685 Th 0.0001 0.0002 0.0003 0.0004 0.0012 0.0002 0.0003 0.0003 0.0001 Ti 0.00005 0.00988 0.00117 0.00049 0.00082 0.00062 0.00072 0.00071 0.00147 TI 0.000005 0.000378 1 0.000931 0.000684 0.000409 0.000094 0.000471 0.000707 0.000441 U 0.000002 0.000997 0.00191 0.00120 0.00105 0.000187 0.00107 0.00134 0.000192 V 0.00001 0.00044 0.00019 0.00008 1 0.00019 1 0.00012 0.00028 0.00023 0.00121 W 0.00002 0.00004 0.00004 0.00004 0.00004 0.00003 < 0.00002 0.00003 0.00011 Y 0.000002 0.00155 0.00135 0.00582 0.00131 0.00126 0.00126 0.00339 0.00343 Zn 1 0.002 1 0.038 0.057 1 0.037 0.032 0.025 1 0.016 1 0.016 1 0.020 3.4 Waste Rock - Summary The results of the waste rock analyses indicate no significant potential for the material to produce acidic conditions. Paste pH values for the samples are typically between 9 and 10, with only shallower samples of saprolitic rock exhibiting lower paste pH values in the 5-6 range. Total Sulfur for the waste rock samples is generally in the range of 0.01 to 0.3 percent, with only three of the 101 samples having a total sulfur content greater than 0.5 percent. Samples exhibiting a sulfur content greater than 0.2 percent were further analyzed using a sulfur fractionation procedure. Results of the sulfur fractionation analyses indicate that the total pyritic (acid -producing) sulfur present in the samples is very low. On MARSHALL MILLER & AssociATE5, INC. 10 ;jHjkLLhNLLE ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 the basis of the sulfur forms and the alkalinity present, all waste rock samples exhibit an excess alkalinity condition and acidic conditions are not expected to develop. Comparison of elemental analyses results for the waste rock to a 20X TCLP limit suggests that none of the RCRA 8 metals except chromium could potentially exhibit toxic concentrations. However, results of chromium speciation testing (differentiating trivalent and hexavalent chromium) for both the solid material and humidity cell effluent indicate that the chromium in the subject rock is overwhelmingly or entirely in its reduced, trivalent form (in the mineral Chromite) which is not readily mobile nor strongly toxic. TCLP testing of the waste rock samples indicates that the leachate has no parameters that approach Toxicity Characteristic Limits as described by the EPA's D List. The TCLP testing is currently being followed up by longer -term humidity cell leach testing. Results of the humidity cell tests will be summarized following completion, and are expected to confirm the current conclusions from the ABA and TCLP tests. 4 Tailings In addition to the 101 core samples collected and analyzed, 10 tailings samples were collected and analyzed for ABA, elemental content, and TCLP. The tailings samples originated from processing work completed at the Minerals Research Laboratory (MRL) at NC State University in Asheville, North Carolina. Testing of the tailings samples was carried out in the same manner as the waste rock, with the exception that sulfur forms testing was not performed as none of the samples exhibited significant total sulfur contents. 4.1 Acid Base Accounting (ABA) for Tailings Samples The ABA results for the tailings samples are summarized in the table below and associated laboratory data are included in Appendix A. ABA analyses for the tailings samples indicate a very low Total Sulfur content (0.01 percent), above -neutral paste pH values (9.0-9.6), and excess neutralization potential for all samples. MARSHALL MILLER & Assoc1ATES INC. 11 ;jHjkLLhNLLE ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 Table 3: Tailings - Summary of ABA Analyses Client Sample ID Reaction to HCI Total % Sulfur Max Pot Acidity NP NET EXCESS /DEFIC NP/ MPA Ratio Paste pH ( SU ) T-1 0 0.01 0.31 5.50 5.19 17.74 9.0 T-2 0 0.01 0.31 2.50 2.19 8.06 9.5 T-3 0 0.01 0.31 2.25 1.94 7.26 9.6 T-4 0 0.01 0.31 1.75 1.44 5.65 9.5 T-5 0 0.01 0.31 1.25 0.94 4.03 9.4 T-6 0 0.01 0.31 2.50 2.19 8.06 9.3 T-7 0 0.01 0.31 2.75 2.44 8.87 9.2 T-8 0 0.01 0.31 2.50 2.19 8.06 9.2 T-9 0 0.01 0.31 4.00 3.69 12.9 9.3 T-10 0 0.01 0.31 3.25 2.94 10.48 9.3 T-11 1 0 1 0.01 1 0.31 2.251 1.941 7.261 9.4 Based on the test results, the tailings are not expected to yield acidic conditions. 4.2 Elemental Analyses for Tailings Samples Elemental analyses of the process tailings were conducted to determine the concentrations of individual elements in the material. A summary of the elemental analyses results is included in the table below, and laboratory data are included in Appendix C. While the results of the elemental analyses are not necessarily indicative of the potential for contamination to be released, the analyses help to characterize the material and guide the selection of samples for any further analyses in subsequent phases. Comparison of tailings element concentrations to that of the waste rock reveals that the tailings generally have lower concentrations of metals of concern than does the waste rock. MARSHALL MILLER & AsSOc1ATES INC. 12 HKLLNNLLE SOLI ES` Summary of Waste Rock and Process Tailings GeochemicaI Assessment Piedmont Lithium Project August 2019 Table 4: Tailings - Summary of Elemental Analyses (µg/g) Parameter Detection Limit Tailings 1 Tailings 2 Tailings 3 Tailings 4 Tailings 5 Tailings 6 Tailings 7 Tailings 8 Tailings 9 Tailings 10 Si (%) 33.2 33.4 34.5 35.3 36.0 35.5 36.3 35.9 36.1 35.4 Hg 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Ag 0.01 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Al 3 64000 57000 55000 65000 63000 67000 66000 62000 63000 64000 As 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 B 1 <1 <1 1.2 <1 <1 <1 <1 <1 <1 <1 Ba 0.01 19 20 19 22 22 25 21 21 20 22 Be 0.02 27 26 22 24 27 24 22 20 30 21 Bi 0.09 1.2 0.39 1.1 1.7 0.77 0.60 0.74 0.70 1.5 0.86 Ca 3 1000 880 920 1000 1100 1100 1100 1000 1100 1100 Cd 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 Cc 0.01 0.10 0.11 0.11 0.15 0.12 0.16 0.12 0.11 0.15 0.13 Cr 0.5 4.5 3.3 < 3 < 3 < 3 5.2 < 3 < 3 3.6 < 3 Cu 0.1 3.0 0.4 0.3 0.2 0.3 3.0 0.8 0.2 0.7 0.2 Fe 3 1200 1300 1300 1500 1300 1300 1400 1200 1400 1400 K 3 22000 21000 21000 23000 22000 23000 23000 22000 23000 23000 Li 2 290 260 270 260 250 260 300 220 340 260 Mg 3 143 147 157 183 169 160 173 153 182 175 Mn 0.1 94 91 95 95 93 93 96 89 104 92 Mo 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 Na 3 32000 32000 31000 31000 32000 34000 32000 33000 31000 32000 Ni 0.1 0.5 0.4 0.4 0.8 0.6 0.5 0.5 0.5 0.6 0.5 P 3 390 380 360 380 370 400 380 400 390 380 Pb 0.05 12 12 12 12 12 13 12 13 12 13 Sb 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Se 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Sn 6 47 48 49 56 51 47 53 45 54 52 Sr 0.02 19 17 17 19 19 21 20 18 20 19 Th 0.01 0.13 0.10 0.15 0.11 0.13 0.11 0.11 0.13 0.14 0.22 Ti 0.1 54 58 58 68 58 57 63 53 65 66 TI 0.02 5.1 5.1 4.9 5.2 5.2 5.3 5.3 5.0 5.3 5.2 U 0.002 1.2 0.92 2.6 1.2 0.93 1.9 1.3 1.4 1.3 6.4 V 1 1 1 1 1 1 1 1 1 1 1 W 0.04 0.74 0.71 0.73 0.84 0.74 0.74 0.76 0.64 0.76 0.76 Y 0.004 0.14 0.12 0.11 0.15 0.15 0.14 0.13 0.12 0.18 0.18 Zn 0.7 22 22 21 24 21 22 24 19 24 24 4.3 Toxicity Characteristic Leach Procedure (TCLP) for Tailings Samples The TCLP test results for the tailings samples are summarized in the table below and laboratory data are included in Appendix E. TCLP testing of the tailings samples was conducted in the same manner as testing of the waste rock samples. MARSHALL MILLER & AssociATE5, INC. 13 ;jHjkLLNNLLE ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 Table 5: Tailings - Summary of TCLP Analysis (mg/L) Parameter Detection Limit Toxicity Character. Limit Tailings Tailings10 Sample weight (g) 100 100 Ext Fluid (#1 or 42) 1 1 Ext Volume (mL) 2000 2000 Final pH (no unit) 0.01 4.93 4.93 Hg 0.00001 0.2 < 0.00001 < 0.00001 Al 0.001 0.149 0.151 As 0.0002 5.0 0.0007 0.0007 Ag 0.00005 5.0 < 0.00005 < 0.00005 Ba 0.00002 100.0 0.0780 0.0639 Be 0.000007 0.00215 0.00235 B 0.002 0.077 0.064 Bi 0.000007 0.000322 0.000336 Ca 0.01 4.47 4.60 Cd 0.000003 1.0 0.000119 0.000163 Co 0.000004 0.000130 0.000156 Cr 0.00008 1 5.0 0.00198 0.00201 Cu 0.0002 0.0045 0.0038 Fe 0.007 0.117 1 0.094 K 0.009 1.24 1.24 Li 0.0001 0.0478 0.0503 Mg 0.001 0.314 0.311 Mn 0.00001 0.467 0.483 Mo 0.00004 0.00077 0.00066 Na 0.01 1310 1310 Ni 0.0001 1 0.0017 0.0017 P 0.003 0.530 0.567 Pb 0.00001 5.0 0.00377 0.00406 Sb 0.0009 < 0.0009 < 0.0009 Se 0.00004 1.0 0.00007 0.00006 Si 0.02 0.53 0.48 Sn 0.00006 < 0.00006 < 0.00006 Sr 0.00002 1 0.0172 0.0176 Th 0.0001 < 0.0001 < 0.0001 Ti 0.00005 0.00019 0.00017 TI 0.000005 0.000164 0.000178 U 0.000002 0.00697 0.007466 V 0.00001 0.00020 0.00019 W 0.00002 0.00005 0.00005 Y 0.000002 0.000359 0.000389 Zn 0.002 0.045 1 0.039 As was the case for the waste rock samples, leachate concentrations of elements for which there is an established Toxicity Characteristic Limit are all several orders of magnitude below the respective toxicity threshold value. The potential for significant leaching of any parameters from the tailings, including iron, is indicated to be quite low. 4.4 Tailings - Summary The process tailings to be produced from the proposed project are not expected to produce acidic discharge. Additionally, TCLP results indicate that the material is not expected to produce discharge MARSHALL MILLER & AssociATES INC. 14 ;jHjkLLNNLLE ES ° Summary of Waste Rock and Process Tailings Geochemical Assessment Piedmont Lithium Project August 2019 with concentrations that exceed the Toxicity Characteristic Limit for materials on the EPA's D List; or that cause adverse environmental conditions. 5 Conclusions The results of this assessment indicate that acidic drainage is not expected to be released from either the waste rock (overburden) or the process tailings. In addition, whole rock elemental and TCLP test results do not indicate the potential for leaching of contaminants at hazardous levels, as defined by EPA's D list. Research of public records suggests that no significant environmental issues have been reported to be associated with the previous lithium pegmatite mining in the region; and results of this current testing program are consistent with that general indication. 6 Ongoing Work — Humidity Cells Additional laboratory testing, in the form of humidity cell tests, is ongoing as of the time of issuance of this report. Samples 18-BD-205-7, 18-BD-212-6, and Tailings 4 were selected for humidity cell testing. Humidity cell testing provides insight with regard to the potential for acid leachate generation and the primary rates of reaction under aerobic weathering conditions. The selected samples are also part of the TCLP test group, so that results from both tests can be compared. The humidity cell testing was initiated on May 24, 2019, and final results are not yet available. As previously discussed, chromium speciation analysis was conducted on the "Time 0" effluent for the waste rock samples (18-BD-205-7 and 18-BD-212-6) to determine that the chromium concentrations in the subject rock are of the trivalent form (and not in the hexavalent form). Humidity cell testing was part of the original sampling and analysis plan and the results from the testing are expected to further confirm the conclusions from the other portions of the plan. The duration of humidity cell testing is difficult to predict, as it is dependent upon each sample's individual mineralogical characteristics. Results of the humidity cell testing are expected to be reported on a monthly basis, with the testing expected to conclude after three months. MARSHALL MILLER & Assoc1ATES INC. 15 APPENDIX A ABA LAB SHEETS FOR WASTE ROCK & TAILINGS ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 17-BD-45 REIC Job #: 19010758 Completed: 1 /16/2019 Approved By-. T.A. Kccnc, cscarch Soil Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - aceAnalytical REIC Sample Number Client Sample Identification Sample Collection Date Interval ( Meters) • • c • • Thickness ( Meters) Description Munsell Soil Color Reaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material as e pH (SU ) Potential Acidity Neutralization Potential Net Neutralizers 01 17-BD-45-1 (B) 11/26/2018 0.00 7.92 7.92 SAP 10 YR 6/6 0 0.01 0.28 0.75 0.47 5.1 02 17-BD-45-2 (B) 11/26/2018 7.92 15.54 7.62 ROCK 10 YR 6/6 0 0.01 0.31 2.50 2.19 5.7 03 17-BD-45-3 (B) 11/26/2018 24.54 37.76 1 13.22 1 ROCK 1 10 YR 6/1 0 0.05 1.43 10.00 8.57 6.4 04 17-BD-45-4 (B) 11/26/2018 39.12 61.04 1 21.92 1 ROCK 1 2.5 YR 5/01 0 1 0.01 1 0.26 1 7.00 6.74 8.9 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 17-BD-65A REIC Job #: 19010902 Completed: 1 /16/2019 Approved By: T.A Keene Esear& Soil Scientist "As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - I REIC Sample Number Client Sample Identification Sample Collection Date Interval ( Meters) Thickness (Meters) Description Munsell Soil Color Heaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material Paste pH (SU) Potential Acidity Neutralization Potential Net Neutralizers 01 17-BD-65A-1 (B) 11/28/2018 0.00 8.30 8.30 SAP 10 YR 5/8 0 0.01 0.31 0.75 0.44 6.3 02 17-BD-65A-2 (B) 11/28/2018 8.30 13.60 5.30 ROCK 10 YR 6/1 0 0.01 0.31 11.00 10.69 7.8 03 17-BD-65A-3 (B) 11/28/2018 13.60 27.74 14.14 ROCK 2.5 YR 5/0 0 0.11 3.56 6.50 2.94 9.7 04 17-BD-65A-4 (B) 11/28/2018 27.74 41.58 13.84 ROCK 2.5 YR 5/0 1 0.05 1.60 21.75 20.15 10.1 05 17-BD-65A-5 (B) 11/28/2018 1 41.58 1 64.05 22.47 ROCK 2.5 YR 5/0 0 0.13 1 4.03 1 6.75 2.72 10.0 06 17-BD-65A-6 (B) 11/28/2018 64.05 80.24 16.19 ROCK 2.5 YR 5/0 0 0.10 3.16 9.75 6.59 10.0 07 17-BD-65A-7 (B) 11/28/2018 80.24 96.13 15.89 ROCK 2.5 YR 6/0 0 0.04 1.20 1 12.50 11.30 10.0 08 17-BD-65A-8 (B) 11/28/2018 114.59 134.04 19.45 ROCK 2.5 YR 6/0 1 0.18 5.47 1 18.25 12.78 10.2 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 17-BD-112 REIC Job #: 19010929 Completed: 1 /16/2019 Approved By: T.A. Keene os-arch Snil Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - Ana "i l f REIC Sample Number Client Sample Identification amp a Collection Date Interval ( Meters) Thickness (Meters) Description Munsell Soil Color Heaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons 11000 Tons of Material Paste pH Potential Acidity Neutralization Potential Net Neutralizers �gIIIII(SU) 01 17-BD-112-1 (B) 11/26/2018 0.00 23.08 23.08 SAP 10 YR 6/6 0 0.01 0.31 4.25 3.94 5.6 02 17-BD-112-2 B 11/26/2018 23.08 38.36 15.28 ROCK 2.5 YR 5/0 0 0.11 3.38 10.50 7.13 9.9 03 17-BD-112-3 (B) 11/26/2018 42.53 67.00 24.47 ROCK 1 2.5 YR 5/01 0 1 0.08 1 2.45 11.00 8.55 10.0 04 17-BD-112-4 B 11/26/2018 67.00 89.50 22.50 ROCK 1 2.5 YR 5/01 0 1 0.10 3.09 1 9.25 6.16 9.5 05 17-BD-112-5 (B) 11/26/2018 89.50 108.93 19.43 ROCK 1 2.5 YR 5/01 0 1 0.07 2.14 1 9.00 6.86 9.7 06 17-BD-112-6 B 11/26/20181 112.54 1 137.00 24.46 ROCK 1 2.5 YR 5/01 0 1 0.04 1.29 1 8.50 7.21 9.7 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-131 REIC .lob #: 19010930 Completed: 2/21 /2019 App�ovcd By: T.A. Kccnc cscarch Soil Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Labora ory Methods Applicable to Overburden and Minesoils - AC eAnalWical.. 1- I REIC Sample Number Client Sample Identification Sample Collection Date Interval ( Meters) • • c • • Thickness ( Meters) Description Munsell Soil Color Reaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material as e pH (SU ) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-131-1 (B) 11/28/2018 78.95 84.88 5.93 ROCK 2.5 YR 5/0 0 0.10 3.10 8.50 5.40 9.9 02 18-BD-131-2 B 11/28/2018 90.50 93.32 2.82 ROCK 2.5 YR 5/2 0 0.07 2.23 7.75 5.52 10.2 03 118-BD-131-3 B 11/28/2018 98.75 113.10 14.35 ROCK 2.5 YR 5/0 0 1 0.01 * 0.31 9.00 8.69 9.9 04 18-BD-131-4 B 11/28/2018 125.57 127.21 1.64 ROCK 2.5 YR 5/0 0 0.12 3.75 7.25 3.50 10.0 05 18-BD-131-5 B 11/28/2018 132.91 150.19 17.28 ROCK 2.5 YR 4/0 0 0.08 2.56 5.75 3.19 9.7 06 18-BD-131-6 B 11/28/2018 156.00 158.88 2.88 ROCK 2.5 YR 5/0 0 < 0.01 * 0.31 6.75 6.44 9.2 07 18-BD-131-7 B 11/28/2018 172.80 1 176.001 3.20 ROCK 2.5 YR 6/0 0 0.11 3.31 7.75 4.44 9.7 08 18-BD-131-8 B 11/28/2018 184.55 1 187.501 2.95 ROCK 12.5 YR 6/01 0 0.05 1 1.43 1 10.25 8.83 1 9.5 * Pyritic Sulfur Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.pacelabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-140 REIC Job #: 19010931 Completed: 1 /17/2019 Z Ay. T.A. Kccnc cscarch Soil Scicritist -As Referenced EPA Manual: EPA-600 / 2-78-054: Field and Laboratory Methods ADDlicable to Overburden and Minesoils - �FaceAnalytrcal REIC Sample Number lent Sample Identification 5ample Collection Date Interval ( Meters) .. :. . Thickness ( Meters) Description Munsell Soil Color Reaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material Paste pH ( SU) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-140-1 (B) 11/28/2018 65.00 87.88 22.88 ROCK 2.5 YR 5/0 0 0.11 3.56 6.50 2.94 9.9 02 18-BD-140-2 (B) 11/28/2018 87.88 101.30 13.42 ROCK 2.5 YR 5/0 0 0.01 0.45 9.50 9.05 9.9 03 18-BD-140-3 (B) 11/28/2018 110.50 136.70 26.20 ROCK 2.5 YR 5/0 0 0.10 3.16 9.00 5.84 9.7 04 18-BD-140-4 (B) 11/28/2018 136.70 156.55 19.85 ROCK 2.5 YR 6/0 1 0.03 0.91 16.50 15.59 9.2 05 18-BD-140-5 (B) 11/28/2018 164.28 202.50 38.22 ROCK 2.5 YR 5/0 0 0.07 2.33 11.50 9.17 9.7 06 18-BD-140-6 (B) 11/28/2018 202.50 232.50 30.00 ROCK 2.5 YR 5/0 0 0.10 2.97 9.25 6.28 9.7 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-177 REIC Job #. 19010932 Completed: 2/21 /2019 ApFiorcd B�: T.A. �Cvc;nc,• usc:�r�h Soil Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - eAnalyfical I REIC Sample Number wient Sample Identification Sample Collection Date Interval ( Meters) .. :. . Thickness (Meters) Description Munsell Soil Color Heaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons 11000 Tons of Material Paste pH (SU) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-177-1 (B) 11/28/2018 0.00 3.00 3.00 OVB 7.5 YR 5/8 0 0.02 0.59 2.75 2.16 5.6 02 18-BD-177-2 (B) 11/28/2018 3.00 12.80 9.80 SAP 10 YR 6/6 0 0.01 0.31 6.75 6.44 6.2 03 18-BD-177-3 B 11/28/2018 12.80 18.53 5.73 ROCK 2.5 YR 5/2 0 0.01 0.31 12.75 12.44 7.9 04 18-BD-177-4 (B) 11/28/2018 18.53 47.36 28.83 ROCK 10 YR 5/1 0 0.05 1.62 9.50 7.88 9.1 05 18-BD-177-5 B 11/28/2018 56.60 73.00 16.40 ROCK 10 YR 5/1 0 0.07 2.10 14.00 11.90 9.5 06 18-BD-177-6 (B) 11/28/2018 75.97 80.43 4.46 ROCK 10 YR 5/1 0 0.07 2.16 7.00 4.84 9.7 07 18-BD-177-7 B 11/28/2018 81.91 90.32 8.41 ROCK 10 YR 5/1 0 0.11 3.47 11.75 8.28 9.5 08 18-BD-177-8 (B) 11/28/2018 91.15 94.25 3.10 ROCK 10 YR 5/1 0 0.14 4.22 8.75 4.53 9.8 09 18-BD-177-9 B 11/28/2018 2.97 105.39 2.42 ROCK 10 YR 5/1 0 0.12 3.59 10.25 6.66 9.5 10 18-BD-177-10 (B) 11/28/20187.93 t129.75 127.80 19.87 ROCK 2.5 YR 4/0 0 < 0.01 0.31 11.75 11.44 8.9 11 18-BD-177-11 B 11/28/2018 155.00 25.25 ROCK 10 YR 5/8 0 0.03 1.01 10.75 9.74 9.7 Pyritic Sulfur Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.12acelabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-183 REIC .lob #: 19010933 Completed: 1 /17/2019 Approved By: T.A. Kccnc, Soil Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - aceAnalytical REIC Sample Number Client Sample Identification amp a Collection Date Interval ( Meters) • • c • • Thickness ( Meters) Description Munsell Soil Color Reaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material Paste pH (SU) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-183-1 (B) 11/28/2018 0.00 3.02 3.02 OVB 7.5 YR 5/8 0 0.01 0.45 1.25 0.80 5.5 02 18-BD-183-2 B 11/28/2018 3.02 19.89 16.87 SAP 10 YR 6/6 0 0.01 0.31 3.00 2.69 5.5 03 18-BD-183-3 B 11/28/2018 19.89 27.51 7.62 ROCK 5 YR 5/1 0 1 0.05 1.68 11.25 9.57 8.8 04 18-BD-183-4 B 11/28/2018 47.35 71.94 24.59 ROCK 5 YR 5/1 0 0.07 2.29 9.75 7.46 9.7 05 18-BD-183-5 B 11/28/2018 71.94 90.23 18.29 ROCK 5 YR 5/1 0 0.10 3.02 10.00 6.98 10.1 06 18-BD-183-6 B 11/28/2018 90.23 111.56 21.33 ROCK 5 YR 5/1 0 0.11 3.28 11.50 8.22 10.0 07 18-BD-183-7 B 11/28/2018 111.56 132.821 21.26 1 ROCK 5 YR 5/1 0 0.06 1.83 12.00 10.17 10.1 08 18-BD-183-8 B 11/28/2018 132.82 150.671 17.85 1 ROCK 1 5 YR 5/1 0 0.07 2.10 11.00 8.90 9.7 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-197 REIC Job #: 19010934 Completed: 1 /17/2019 Approved By: T.A. Keene esFarch Sni' Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - ace Ana lWi l f REIC Sample Number yen Sample Identification ample Collection Date Interval ( Meters) (Meters) Thickness4CK D Munsell Soil Color Reaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material Paste pH (Su) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-197-1 (B) 11/28/2018 0.00 6.00 6.00 5 YR 5/2 0 0.01 0.31 7.50 7.19 5.5 02 18-BD-197-2 B 11/28/2018 6.00 18.70 12.70 5 YR 5/1 0 0.10 3.22 11.00 7.78 5.5 03 18-BD-197-3 (B) 11/28/2018 20.00 35.09 15.09 2.5 YR 6/0 0 0.08 2.40 10.75 8.35 8.8 04 18-BD-197-4 B 11/28/2018 39.64 51.94 12.30 ROCK 2.5 YR 7/0 0 0.01 0.25 56.50 56.25 9.7 05 18-BD-197-5 (B) 11/28/2018 53.07 66.59 13.52 ROCK 2.5 YR 6/0 0 0.16 5.00 12.50 7.50 10.1 06 18-BD-197-6 B 11/28/2018 67.85 83.17 15.32 ROCK 2.5 YR 6/0 0 0.12 3.66 7.75 4.09 10.0 07 18-BD-197-7 (B) 11/28/2018 88.70 103.14 14.44 1 ROCK 12.5 YR 6/01 2 0.04 1.24 26.25 25.01 10.1 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-205 REIC Job #: 19010937 Completed: 1 /17/2019 Approw-,J By. T.A. Keene esearch Soil Scicntist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - Ll AnaV f caf n� I REIC Sample Number Client Sample Identification amp a Collection Date Interval ( Meters) •• =• • Thickness (Meters) Description Munsell Soil Color Reaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons 11000 Tons of Material Paste pH (Su) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-205-1 (B) 11/28/2018 0.00 1.50 1.50 OVB 7.5 YR 5/8 0 0.01 0.29 3.00 2.71 6.1 02 18-BD-205-2 (B) 11/28/2018 1.50 2.50 1.00 ROCK 10 YR 5/8 0 0.01 0.31 6.00 5.69 6.0 03 18-BD-205-3 (B) 11/28/2018 2.50 25.00 22.50 ROCK 2.5 YR 5/12 0 0.01 0.31 11.50 11.19 6.8 04 18-BD-205-4 (B) 11/28/2018 25.00 45.00 20.00 ROCK 2.5 YR 5/0 0 0.11 3.38 14.25 10.88 8.9 05 18-BD-205-5 (B) 11/28/2018 45.00 65.00 20.00 ROCK 2.5 YR 5/0 0 0.01 0.31 10.50 10.19 9.8 06 18-BD-205-6 (B) 11/28/2018 65.00 82.15 17.15 ROCK 2.5 YR 5/0 0 0.04 1.30 9.00 7.70 9.9 07 18-BD-205-7 (B) 11/28/2018 84.20 101.40 17.20 ROCK 2.5 YR 5/0 0 0.01 0.31 9.75 9.44 9.8 08 18-BD-205-8 (B) 11/28/2018 112.47 130.55 18.08 ROCK 2.5 YR 5/0 0 0.07 2.24 7.75 5.51 9.8 09 118-BD-205-9 (B) 11/28/2018 132.56 139.861 7.30 ROCK 2.5 YR 5/0 0 1 0.01 0.31 7.00 6.69 10.1 10 18-BD-205-10 (B) 11/28/2018 139.86 142.00 2.14 ROCK 2.5 YR 5/0 0 0.01 0.31 7.50 7.19 9.7 11 18-BD-205-11 (B) 11/28/2018 142.00 153.00 11.00 ROCK 2.5 YR 5/0 1 0.01 0.27 22.50 22.23 10.1 12 18-BD-205-12 (B) 11/28/2018 153.00 165.00 12.00 ROCK 2.5 YR 5/0 0 0.08 2.35 9.75 7.40 10.2 13 18-BD-205-13 (B) 11/28/2018 165.00 173.00 8.00 ROCK 2.5 YR 5/0 0 0.04 1.29 8.50 7.21 10.2 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-207 REIC Job #: 19010959 Completed: 2/21 /2019 (- Y __; eo_� Approved By: TA. KF:Fnv esearch Soi' Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - I REIC Sample Number Client Sample Identification Sample Collection Date Interval ( Meters) • • : • • Thickness ( Meters) Description Munsell Soil Color Heaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons 11000 Tons of Material Paste pH (SU) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-207-1 (B) 11/28/2018 0.00 21.00 21.00 OVB 7.5 YR 5/8 0 0.02 0.49 2.25 1.76 5.8 02 18-BD-207-2 B 11/28/2018 21.00 25.00 4.00 SAP 2.5 YR 6/4 0 0.06 1.93 9.75 7.83 6.5 03 18-BD-207-3 (B) 11/28/2018 27.00 39.58 12.58 ROCK 2.5 YR 5/0 0 1 < 0.01 * 0.31 8.50 8.19 9.2 04 18-BD-207-4 B 11/28/2018 49.05 71.05 22.00 ROCK 2.5 YR 5/0 1 0.14 4.23 22.25 18.02 9.8 05 18-BD-207-5 (B) 11/28/2018 71.05 87.80 16.75 ROCK 2.5 YR 5/0 0 0.01 * 0.31 7.50 7.19 10.0 06 18-BD-207-6 (B) 11/28/2018 102.37 129.02 26.65 ROCK 2.5 YR 5/0 0 0.06 * 1.86 8.00 6.14 9.9 07 18-BD-207-7 (B) 11/28/2018 129.02 158.55 29.53 ROCK 2.5 YR 5/0 0 0.01 * 0.31 4.75 4.44 9.9 08 18-BD-207-8 (B) 11/28/2018 162.36 193.28 30.92 ROCK 12.5 YR 5/0 0 0.03 * 0.86 6.00 5.14 10.2 09 18-BD-207-9 (B) 11/28/20181 195.35 1 217.191 21.84 1 ROCK 17.5 YR 5/0 0 1 0.06 1.77 18.25 16.48 10.2 * Pyritic Sulfur Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.12acelabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-212 Site ID: REIC ,lob #: 19010961 Completed: 1 /22/2019 Appeoocd By: T.A. Kcanc, asaarch Soil Scientist -As Referenced EPA Manual- EPA-6nn 12-7R-nSd- Field and Lahnrafnry Methnds Annlicahle to Overhurden and Minesnils - Z'D;a A na1W icaI.. 1 i REIC Sample Number Client Sample Identification amp a Collection Date Interval ( Meters) • • c • • Thickness ( Meters) Description Munsell Soil Color Heaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material 11asre pH (SU) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-212-1 (B) 11/28/2018 0.00 5.05 5.05 SAP 7.5 YR 5/8 0 0.01 0.31 1.00 0.69 5.7 02 18-BD-212-2 B 11 /28/2018 5.80 15.36 9.56 ROCK 5 YR 5/2 0 0.01 0.31 6.25 5.94 7.4 03 18-BD-212-3 B 11 /28/2018 15.36 34.65 19.29 ROCK 2.5 YR 5/0 0 1 0.07 2.33 7.25 4.92 9.9 04 18-BD-212-4 B 11 /28/2018 34.65 55.00 20.35 ROCK 2.5 YR 5/0 0 0.12 3.59 9.00 5.41 9.8 05 18-BD-212-5 B 11 /28/2018 55.00 79.72 24.72 ROCK 2.5 YR 5/0 0 0.14 4.41 6.50 2.09 10.1 06 18-BD-212-6 B 11/28/20181 95.68 1 105.39 9.71 ROCK 5 YR 5/2 0 0.15 4.78 11.75 6.97 10.0 07 18-BD-212-7 B 11/28/20181 105.39 1 136.37 30.98 ROCK 2.5 YR 5/0 0 0.07 2.12 15.00 12.88 9.7 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-214 REIC .lob #: 19010966 Completed: 2/21 /2019 App�ovcd By: T.A. Kccnc, a5Carcit Soil Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Labo tory Methods Applicable to Overburden and Minesoils - aceAnalytical REIC Sample Number Client Sample Identification Sample Collection Date Interval ( Meters) • • = • • Thickness ( Meters) Description Munsell Soil Color Reaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material as e pH (SU ) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-214-1 (B) 11/28/2018 1.50 10.90 9.40 SAP 7.5 YR 5/8 0 0.01 0.26 4.00 3.74 5.3 02 18-BD-214-2 B 11/28/2018 10.90 22.60 11.70 SAP 2.5 YR 6/4 0 0.01 0.31 2.50 2.19 6.6 03 118-BD-214-3 B 11/28/2018 22.60 37.45 14.85 ROCK 2.5 YR 5/0 2 1 0.14 4.44 26.25 21.81 9.4 04 18-BD-214-4 (B) 11/28/2018 39.50 62.45 22.95 ROCK 2.5 YR 5/0 0 0.03 * 0.94 10.75 9.81 9.5 05 18-BD-214-5 B 11/28/2018 66.47 72.55 6.08 ROCK 2.5 YR 5/0 2 0.08 2.52 82.50 79.98 9.6 06 18-BD-214-6 B 11/28/2018 75.27 95.20 19.93 ROCK 2.5 YR 5/0 0 0.12 3.81 15.25 11.44 9.5 07 18-BD-214-7 (B) 11/28/2018 95.20 1 118.60 23.40 ROCK 2.5 YR 5/0 0 0.05 * 1.56 11.00 9.44 9.6 * Pyritic Sulfur Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.pacelabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-226 REIC Job #: 19010968 Completed: 1 /22/2019 `' Approved By. T.A. Kccnc csc:arch Soil Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Labo tory Methods Applicable to Overburden and Minesoils - aceAnalytical REIC Sample Number Client Sample Identification amp a Collection Date Interval ( Meters) • • = • • Thickness ( Meters) Description Munsell Soil Color Reaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material Paste pH (SU ) Potential Acidity Neutralization Potential Net Neutralizers 01 18-BD-226-1 (B) 11/28/2018 0.00 3.17 3.17 OVB 2.5 YR 6/6 0 0.01 0.37 0.50 0.13 5.3 02 18-BD-226-2 B 11/28/2018 3.17 18.60 15.43 SAP 10 YR 5/0 0 0.01 0.31 6.50 6.19 6.3 03 118-BD-226-3 B 11/28/2018 18.60 46.29 27.69 ROCK 5 YR 5/0 0 1 0.06 1.77 8.25 6.48 8.6 04 18-BD-226-4 B 11/28/2018 49.30 69.60 20.30 ROCK 5 YR 5/0 0 0.07 2.26 6.50 4.24 9.2 05 18-BD-226-5 B 11/28/2018 75.30 95.82 20.52 ROCK 5 YR 5/0 0 0.11 3.34 6.75 3.41 9.6 06 18-BD-226-6 B 11/28/2018 101.72 116.36 14.64 ROCK 5 YR 5/0 0 0.10 3.19 8.00 4.81 9.5 07 18-BD-226-7 B 11/28/2018 122.38 134.171 11.79 ROCK 5 YR 6/0 0 0.13 3.91 8.50 4.59 9.7 Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 ACID -BASE ACCOUNTING ABA.Rev. 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: MP 30 PILOT PLANT RUN Site ID: SCAVENGER TAILINGS REIC Job #: 19020154 Completed: 2/4/2019 Approved By: T.A. Keene esearch Sui Scientist -As Referenced EPA Manual: EPA-600 / 2-78-054; Field and Laboratory Methods Applicable to Overburden and Minesoils - aceRnalytical f REIC Sample Number Client Sample Identification amp a Collection Date Description Munsell Soil Color Heaction to HCI Total % Sulfur Calcium Carbonate Equivalent in Tons / 1000 Tons of Material flaste pH Potential Acidity Neutralization Potentiallgaggm�gIIIII(SU) Net Neutralizers 01 T-1 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 7.5 YR 8/2 0 0.01 0.31 5.50 5.19 9.0 02 T-2 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 2.50 2.19 9.5 03 T-3 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 2.25 1.94 9.6 04 T-4 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 1.75 1.44 9.5 05 T-5 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 1.25 0.94 9.4 06 T-6 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 2.50 2.19 9.3 07 T-7 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 2.75 2.44 9.2 08 T-8 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 2.50 2.19 9.2 09 T-9 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 4.00 3.69 9.3 10 T-10 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 3.25 2.94 9.3 11 T-11 1/24/2019 QUARTZ, FELDSPAR, MICA < 60 MESH 2.5 YR 8/0 0 0.01 0.31 2.25 1.94 9.4 NOTE: Each 10 kg bag was subsampled by inserting a 35 mm ID plastic pipe vertically and extracting -250 grams, which was dried and pulverized to < 60 Mesh. Pace Analytical Services, LLC. P.O. Box 286, Beaver, WV 25813 800-999-0105 www.reiclabs.com Page 1 of 1 APPENDIX SULFUR FRACTIONATION RESULTS FOR WASTE ROCK ONLY SULFUR FRACTIONATION * SULFURFRACT.Rev 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-131 REIC Job a: 19010930 Completed: 2/19/2019 Apprcrvec Bv: T.A. 4eEpn es -arch Soil Sac,ntigt 2 aceAnalytical� REIC Client Sample Total Pyritic Sulfate Organic Pyritic Sulfur of Sulfate Sulfur of Sample Sample Collection Sulfur Sulfur Sulfur Sulfur Total Sulfur Total Sulfur Number Identification Date (%) (%) (%) (%) (%) (%) 03 18-BD-131-3 (B) 11/28/2018 0.30 0.01 0.25 0.05 2.7% 82.2% 06 18-BD-131-6 (B) 11/28/2018 0.23 <0.01 0.20 0.04 4.4% 89.1% * ASTM D2492-84 and EPA-600/ 2-78-054, Section 3.2.6 (Modified) Minimum Qualifying Limit (MQL) - 0.01 Pace P.O. Box 286, Beaver, WV 25813 800-999-0105 Page 1 of 1 SULFUR FRACTIONATION * SULFURFRACT.Rev 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-177 REic Job #: 19010932 Completed: 2/21 /2019 (7�� - .Approved By; TA. Keen esearch Soil Scientist aceAnalytical REIC Client Sample Total Pyritic Sulfate Organic Pyritic Sulfur of Sulfate Sulfur of Sample Sample Collection I Sulfur Sulfur Sulfur Sulfur Total Sulfur Total Sulfur Number Identification Date (%) (%) (%) (%) (%) (%) 10 18-BD-177-10 (B) 11/28/2018 0.32 <0.01 0.25 0.07 0.7% 1 78.9% * ASTM D2492-84 and EPA-600/ 2-78-054, Section 3.2.6 (Modified) Minimum Qualifying Limit (MQL) - 0.01 Pace P.O. Box 286, Beaver, WV 25813 800-999-0105 Page 1 of 1 SULFUR FRACTIONATION * SULFURFRACT.Rev 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-207 REIC Job #: 19010959 Completed: 2/21 /2019 Approved B;: TA Keene F.SoRr&i Sbll Scientist aceAnalytical REIC Sample Number Client Sample Identification Sample Collection Date Total Sulfur (%) Pyritic Sulfur (%) Sulfate Sulfur (%) Organic Sulfur (%) Pyritic Sulfur of Total Sulfur (%) Sulfate Sulfur of Total Sulfur (%) 03 18-BD-207-3 B 11/28/2018 0.32 <0.01 0.28 0.05 0.2% 85.6% 05 18-BD-207-5 (B) 11/28/2018 0.51 0.01 0.48 0.05 2.0% 94.8% 06 18-BD-207-6 B 11/28/2018 0.73 0.06 0.58 0.09 8.2% 79.2% 07 18-BD-207-7 (B) 11/28/20181 0.66 1 0.01 0.56 1 0.10 1.6% 84.0% 08 18-BD-207-8 (B) 11/28/20181 0.26 1 0.03 0.19 1 0.04 1 10.8% 73.3% * ASTM D2492-84 and EPA-600/ 2-78-054, Section 3.2.6 (Modified) Minimum Qualifying Limit (MQL) - 0.01 Pace P.O. Box 286, Beaver, WV 25813 800-999-0105 Page 1 of 1 SULFUR FRACTIONATION * SULFURFRACT.Rev 0, Date 08-23-2018 (Form 1 of 1) PIEDMONT LITHIUM, INC. Project ID: 18-BD-214 REIC Job #: 19010966 Completed: 2/21 /2019 Approved By: T.A. Keene esearch Soil Scientist (0'4.0"_ aceAnalytical "' REIC Client Sample Total Pyritic Sulfate Organic Pyritic Sulfur of Sulfate Sulfur of Sample Sample Collection Sulfur Sulfur Sulfur Sulfur Total Sulfur Total Sulfur Number Identification Date ( %) (%) (%) (%) (%) ( %) 04 18-BD-214-4 B 11/28/2018 0.28 0.03 0.19 0.05 12.0% 69.6% 07 18-BD-214-7 (B) 11/28/2018 0.21 0.05 0.11 0.04 26.3% 53.0% * ASTM D2492-84 and EPA-600 / 2-78-054, Section 3.2.6 (Modified) Minimum Qualifying Limit (MQL) - 0.01 Pace P.O. Box 286, Beaver, WV 25813 800-999-0105 Page 1 of 1 APPENDIX ELEMENTAL ANALYSIS SUMMARY FOR WASTE ROCK & TAILINGS 0 SGS- SGS Canada Inc. P.O. Box 4300 - 185 Concession St. Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 SGS Lakefield Environmental Met Attn : Barb Bowman Project : CA20M-00000-110-17234-01 21-February-2019 Date Rec. : LR Report: Reference: Copy: CERTIFICATE OF ANALYSIS Final Report 12 February 2019 CA14338-FEB19 17234-01-01 #1 Analysis 3: Analysis Completed Date 4: Analysis Completed Time 5: QC - Blank 6: QC - STD % Recovery 7: QC - DUP % RPD 9: 18-BD-205-1 10: 18-BD-205-2 11: 18-BD-205-3 12: 18-BD-205-4 13: 18-BD-205-5 Sample Date & Time N/A N/A N/A N/A N/A Silica [%] --- --- --- --- --- 21.1 17.7 23.3 21.9 21.9 Mercury [ug/g] 20-Feb-19 11:49 < 0.05 101 % 6% 0.06 < 0.05 < 0.05 < 0.05 < 0.05 Silver [lag/g] 19-Feb-19 10:17 < 0.01 100% 8% < 1 < 1 < 1 < 1 < 1 Aluminum [pg/g] 19-Feb-19 10:17 < 3 104% 1 % 96000 100000 83000 82000 87000 Arsenic [pg/g] 19-Feb-19 10:17 < 0.5 108% 2% 9.1 7.4 3.7 2.8 2.4 Boron [pg/g] 19-Feb-19 10:17 < 1 99% ND < 1 < 1 < 1 < 1 < 1 Barium [Ng/g] 19-Feb-19 10:17 < 0.01 109% 2% 170 190 320 270 210 Beryllium [Ng/g] 19-Feb-19 10:17 < 0.02 102% 3% 8.6 2.7 2.0 4.7 1.6 Bismuth [lag/g] 19-Feb-19 10:17 < 0.09 100% 6% 1.3 0.42 0.23 0.22 0.12 Calcium[pg/g] 19-Feb-19 10:17 <3 103% 1% 15000 33000 47000 53000 56000 Cadmium [Ng/g] 19-Feb-19 10:17 < 0.02 103% 15% 0.13 0.18 0.18 0.22 0.16 Cobalt [Ng/g] 19-Feb-19 10:17 < 0.01 107% 0% 18 29 18 18 22 Chromium [Ng/g] 19-Feb-19 10:17 < 0.5 106% 3% 65 25 39 35 40 Copper [lag/g] 19-Feb-19 10:17 < 0.1 106% 1 % 17 11 6.6 7.7 4.4 Iron [lag/g] 19-Feb-19 10:17 < 3 106% 2% 87000 110000 76000 79000 68000 Potassium [lag/g] 19-Feb-19 10:17 < 3 110% 3% 5000 5500 8700 7700 6700 Page 1 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 3: 4: 5: 6: 7: 9: 10: 11: 12: 13: Analysis Analysis QC - Blank QC - STD % QC - DUP % 18-BD-205-1 18-BD-205-2 18-BD-205-3 18-BD-205-4 18-BD-205-5 Completed Completed Recovery RPD Date Time Lithium [lag/g] 19-Feb-19 10:17 < 2 100% 3% 430 400 370 360 240 Magnesium [lag/g] 19-Feb-19 10:17 < 3 102% 1 % 9500 18000 17000 17000 22000 Manganese [lag/g] 19-Feb-19 10:17 < 0.1 109% 3% 1700 2000 1700 1700 1300 Molybdenum [pg/g] 19-Feb-19 10:17 < 0.1 103% 7% 1.3 0.6 0.7 2.2 2.5 Sodium [Ng/g] 19-Feb-19 10:17 < 3 102% 2% 3800 11000 20000 22000 19000 Nickel [Ng/g] 19-Feb-19 10:17 < 0.1 106% 2% 16 7.5 3.5 3.7 4.5 Phosphorus [Ng/g] 19-Feb-19 10:17 < 3 105% 1 % 670 2700 3300 3700 1200 Lead [lag/g] 19-Feb-19 10:17 < 0.05 104% 4% 16 11 9.7 8.8 8.0 Antimony [Ng/g] 19-Feb-19 10:17 < 0.8 103% ND < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [Ng/g] 19-Feb-19 10:17 < 0.7 108% 3% 0.8 < 0.7 < 0.7 < 0.7 < 0.7 Tin [fag/g] 19-Feb-19 10:17 < 6 109% 1 % 19 6 < 6 10 9 Strontium [Ng/g] 19-Feb-19 10:17 < 0.02 105% 2% 46 160 290 340 300 Thorium [Ng/g] 19-Feb-19 10:17 < 0.01 105% 3% 4.2 2.6 2.8 2.0 2.7 Titanium [Ng/g] 19-Feb-19 10:17 < 0.1 103% 3% 13000 15000 12000 12000 9900 Thallium [Ng/g] 19-Feb-19 10:17 < 0.02 106% 3% 0.78 0.29 0.41 0.39 0.25 Uranium [Ng/g] 19-Feb-19 10:17 < 0.002 100% 2% 2.6 1.4 1.4 1.1 1.2 Vanadium [Ng/g] 19-Feb-19 10:17 < 1 107% 1 % 230 240 160 150 300 Tungsten [Ng/g] 19-Feb-19 10:17 < 0.04 92% 0% 2.0 1.1 0.62 0.61 0.57 Yttrium [Ng/g] 19-Feb-19 10:17 < 0.004 105% 3% 37 37 46 47 25 Zinc [Ng/g] 19-Feb-19 10:17 < 0.7 105% 3% 100 140 130 130 91 Analysis 14: 15: 16: 17: 18: 19: 20: 21: 22: 23: 18-B D-205-6 18-B D-205-7 18-B D-205-8 18-B D-205-9 18-B D-205-10 18-B D-205-11 18-B D-205-12 18-B D-205-13 17-B D-45-1 17-B D-45-2 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 22.0 23.1 22.5 22.9 22.6 24.1 23.4 23.3 20.4 25.5 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [lag/g] 83000 81000 89000 87000 84000 79000 81000 83000 100000 90000 Arsenic [lag/g] 2.5 2.0 1.7 1.4 1.1 1.5 1.5 1.0 3.8 2.4 0 Page 2 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 0 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 14: 15: 16: 17: 18: 19: 20: 21: 22: 23: 18-B D-205-6 18-B D-205-7 18-B D-205-8 18-B D-205-9 18-B D-205-10 18-B D-205-11 18-B D-205-12 18-B D-205-13 17-BD-45-1 17-BD-45-2 Boron[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 1.2 Barium [pg/g] 230 240 240 200 200 200 350 280 420 420 Beryllium [pg/g] 1.6 2.5 1.9 5.5 3.0 22 5.2 7.3 16 14 Bismuth [pg/g] 0.13 0.10 0.13 0.16 0.13 0.31 0.17 0.13 0.22 0.42 Calcium [pg/g] 58000 53000 59000 58000 57000 46000 46000 50000 460 1500 Cadmium [pg/g] 0.19 0.13 0.12 0.13 0.17 0.11 0.23 0.19 0.17 0.14 Cobalt [pg/g] 22 22 25 26 22 21 14 19 64 53 Chromium [pg/g] 41 45 67 40 37 44 38 45 65 71 Copper [pg/g] 5.6 5.1 10 5.6 5.6 3.8 9.8 4.6 17 19 Iron[pg/g] 73000 66000 66000 75000 64000 59000 74000 65000 72000 57000 Potassium [pg/g] 7300 9200 7400 9100 7500 12000 11000 14000 10000 12000 Lithium [pg/g] 230 400 860 840 650 1000 670 740 710 700 Magnesium [pg/g] 23000 24000 26000 30000 24000 24000 15000 23000 11000 9400 Manganese[pg/g] 1500 1300 1200 1500 1200 1300 1800 1400 1500 1800 Molybdenum [pg/g] 2.3 2.7 3.2 1.4 2.1 1.6 2.2 1.5 0.5 0.7 Sodium [pg/g] 21000 18000 19000 16000 16000 17000 19000 17000 400 1500 Nickel [pg/g] 5.0 5.2 12 5.3 4.9 5.0 3.4 4.1 16 11 Phosphorus[pg/g] 1500 840 1000 580 670 1800 1900 1300 420 500 Lead [pg/g] 6.8 6.8 6.2 6.1 6.0 6.5 8.1 7.9 21 20 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [pg/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Tin [pg/g] 8 16 < 6 17 14 59 23 44 22 19 Strontium [pg/g] 280 270 340 280 290 240 300 240 5.48 12 Thorium [pg/g] 2.1 2.8 2.4 1.6 2.1 1.7 2.2 2.6 1.5 4.4 Titanium [pg/g] 11000 8700 8200 11000 9100 8100 8500 7000 6100 6200 Thallium [pg/g] 0.26 0.65 0.75 2.2 1.1 2.9 3.0 2.7 1.7 2.6 Uranium [pg/g] 0.94 0.97 0.81 0.75 0.64 1.8 1.1 1.0 2.3 2.8 Vanadium [pg/g] 290 270 250 350 300 270 110 150 160 110 Tungsten [pg/g] 1.5 0.71 0.61 0.42 0.42 0.62 0.43 0.46 2.8 27 Yttrium [pg/g] 29 22 24 20 19 18 39 32 12 20 Zinc [pg/g] 110 90 83 100 85 110 150 120 140 140 Page 3 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 24: 25: 26: 27: 28: 29: 30: 31: 32: 33: 17-B D-45-3 17-B D-45-4 18-B D-140-1 18-B D-140-2 18-B D-140-3 18-B D-140-4 18-B D-140-5 18-B D-140-6 17-B D-65A-1 17-B D-65A-2 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 21.6 21.7 22.2 23.5 22.8 22.8 23.9 23.3 18.4 23.6 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [pg/g] 85000 85000 84000 82000 84000 77000 79000 84000 110000 81000 Arsenic [pg/g] 2.8 1.1 1.7 2.8 1.2 1.1 1.3 1.0 3.6 1.6 Boron[pg/g] <1 <1 <1 <1 <1 <1 1.3 <1 <1 <1 Barium [pg/g] 200 180 160 180 290 340 340 350 290 160 Beryllium [pg/g] 3.6 2.5 3.1 25 3.6 8.6 3.3 20 9.4 23 Bismuth [pg/g] 0.18 0.16 0.14 0.70 0.16 0.21 0.14 0.19 0.68 13 Calcium [pg/g] 54000 61000 57000 49000 54000 46000 49000 47000 17000 50000 Cadmium [pg/g] 0.19 0.18 0.19 0.20 0.19 0.25 0.22 0.18 0.16 0.22 Cobalt [pg/g] 26 23 26 22 25 24 21 20 36 19 Chromium [pg/g] 68 55 54 58 59 62 62 90 140 130 Copper [pg/g] 13 8.4 9.4 8.0 9.3 6.6 7.9 6.7 8.8 5.9 Iron[pg/g] 73000 74000 67000 58000 65000 63000 64000 61000 93000 58000 Potassium [pg/g] 7700 6300 7400 12000 9100 12000 8400 12000 5700 7800 Lithium [pg/g] 940 550 480 700 480 820 430 450 580 330 Magnesium [pg/g] 26000 27000 29000 26000 29000 29000 23000 22000 21000 27000 Manganese[pg/g] 1700 1500 1300 1200 1300 1300 1300 1400 1900 1300 Molybdenum [pg/g] 2.0 2.9 3.1 2.6 3.9 2.5 3.4 3.1 0.9 0.8 Sodium [pg/g] 17000 16000 16000 16000 17000 13000 20000 23000 1800 20000 Nickel[pg/g] 26 6.5 9.8 9.6 10 9.8 8.2 8.7 7.2 6.3 Phosphorus[pg/g] 1300 730 740 790 760 660 980 1400 800 1500 Lead [pg/g] 7.7 6.5 7.0 6.5 7.8 9.9 8.9 10 10 8.3 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [pg/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Tin [pg/g] 11 9 < 6 43 9 29 9 130 34 10 Strontium [pg/g] 280 280 260 230 250 130 260 280 27 220 Thorium [pg/g] 0.99 1.7 1.7 1.3 1.9 2.0 2.6 2.0 2.2 1.3 Titanium [pg/g] 8900 12000 8700 6600 8200 6400 7200 7200 14000 6700 0 Page 4 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 0 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 24: 25: 26: 27: 28: 29: 30: 31: 32: 33: 17-B D-45-3 17-B D-45-4 18-B D-140-1 18-B D-140-2 18-B D-140-3 18-B D-140-4 18-B D-140-5 18-B D-140-6 17-B D-65A-1 17-B D-65A-2 Thallium [pg/g] 1.1 0.81 0.46 1.9 0.56 1.6 0.47 0.70 1.5 1.6 Uranium [pg/g] 0.52 0.84 0.88 1.4 1.0 1.3 1.4 1.7 1.4 1.3 Vanadium [pg/g] 230 500 250 190 190 180 180 160 450 220 Tungsten [pg/g] 0.83 0.55 0.51 0.78 0.46 0.51 0.42 0.53 1.9 0.68 Yttrium [pg/g] 25 20 62 48 42 43 40 34 39 43 Zinc [pg/g] 120 97 100 99 110 110 110 110 160 98 Analysis 34: 35: 36: 37: 38: 39: 40: 41: 42: 43: 17 -B D -65A-3 17-B D-65A-4 17-B D-65A-5 17-B D -65A-6 17-B D-65A-7 17 -B D -65A-8 18 -B D -226-1 18-B D-226-2 18 -B D -226-3 18-B D-226-4 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 21.2 22.5 24.1 23.0 27.9 22.3 21.0 22.7 22.3 23.6 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [pg/g] 83000 83000 79000 77000 76000 60000 110000 89000 83000 84000 Arsenic [pg/g] 2.1 1.4 1.5 1.2 1.3 1.1 7.7 2.5 11 1.6 Boron[pg/g] <1 <1 <1 <1 <1 1.2 <1 <1 <1 <1 Barium [pg/g] 160 220 160 260 280 230 190 260 240 240 Beryllium [pg/g] 3.1 2.0 14 4.6 21 6.4 10 6.1 2.8 2.3 Bismuth [pg/g] 0.55 0.23 0.39 0.20 0.31 0.28 1.5 0.18 0.14 0.15 Calcium [pg/g] 58000 57000 55000 60000 32000 45000 900 39000 62000 56000 Cadmium [pg/g] 0.22 0.19 0.24 0.19 0.19 0.17 0.04 0.24 0.21 0.22 Cobalt [pg/g] 26 25 23 28 14 44 26 24 31 22 Chromium [pg/g] 120 45 59 57 51 480 53 47 69 60 Copper [pg/g] 7.8 5.7 7.3 9.1 5.8 15 12 8.3 10 7.8 Iron[pg/g] 76000 72000 60000 63000 43000 68000 84000 70000 73000 64000 Potassium [pg/g] 7600 10000 7900 9900 14000 14000 4800 6800 7500 6500 Lithium [pg/g] 400 440 450 640 740 2400 260 260 430 390 Magnesium [pg/g] 30000 28000 25000 33000 15000 72000 3600 20000 35000 25000 Manganese[pg/g] 1500 1400 1100 1200 870 1300 1400 1400 1400 1300 Page 5 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 34: 35: 36: 37: 38: 39: 40: 41: 42: 43: 17-BD-65A-3 17-BD-65A-4 17-BD-65A-5 17-BD-65A-6 17-BD-65A-7 17-BD-65A-8 18-BD-226-1 18-BD-226-2 18-BD-226-3 18-BD-226-4 Molybdenum [pg/g] 3.1 1.8 2.5 5.2 2.0 3.3 1.0 0.3 2.7 3.4 Sodium [pg/g] 18000 15000 18000 11000 23000 6000 860 13000 17000 19000 Nickel[pg/g] 7.8 4.7 5.2 7.2 4.6 31 14 6.5 8.3 7.1 Phosphorus[pg/g] 770 770 580 290 630 280 720 1000 890 820 Lead [pg/g] 6.4 8.0 7.9 7.5 13 4.0 14 8.1 5.6 7.6 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [pg/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 0.8 < 0.7 < 0.7 < 0.7 Tin [pg/g] 8 13 17 16 14 28 17 9 10 9 Strontium [pg/g] 290 280 270 200 180 140 12 180 240 260 Thorium [pg/g] 1.5 2.1 2.0 2.1 4.1 2.1 3.2 2.3 0.92 1.5 Titanium [pg/g] 7100 8400 7500 6400 4200 3400 11000 7100 7600 8000 Thallium [pg/g] 0.48 1.3 0.79 1.3 1.2 2.1 1.0 0.62 0.60 0.56 Uranium [pg/g] 0.64 0.76 1.3 1.1 3.0 0.73 2.9 1.3 0.40 0.67 Vanadium [pg/g] 230 250 270 290 110 150 240 200 240 210 Tungsten [pg/g] 0.49 0.60 0.67 0.77 0.61 6.4 2.8 0.80 0.53 0.41 Yttrium [pg/g] 34 31 30 39 24 25 36 43 58 47 Zinc [pg/g] 120 110 95 84 90 96 100 120 110 110 Analysis 44: 18-BD-226-5 45: 18-BD-226-6 46: 18-BD-226-7 47: 17-BD-112-1 48: 17-BD-112-2 49: 17-BD-112-3 50: 17-BD-112-4 51: 17-BD-112-5 52: 17-BD-112-6 53: 18-BD-131-1 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 23.5 23.0 24.2 22.9 24.6 26.0 23.6 24.3 25.5 22.9 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [pg/g] 84000 84000 84000 100000 84000 89000 80000 72000 77000 79000 Arsenic [pg/g] 3.4 9.2 1.8 2.6 1.0 0.8 1.0 1.6 0.8 0.8 Boron[pg/g] <1 <1 1.3 <1 <1 <1 <1 <1 <1 1.2 Barium [pg/g] 170 240 330 520 450 240 220 280 380 120 Beryllium [pg/g] 9.8 7.4 4.7 9.0 2.9 23 2.6 4.8 3.4 5.9 0 Page 6 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. 0 SGS- SGS Canada Inc. P.O. Box 4300 - 185 Concession St. Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 18-B D-226-5 18 -B D -226-6 18-B D-226-7 17-BD-1 12-1 17-B D-112 -2 Project : CA20M-00000-110-17234-01 LR Report: CA14338-FEB19 49: 50: 51: 52: 53: 17-BD-1 12-3 17-BD-112-4 17-BD-1 12-5 17-BD-1 12-6 18-BD-131-1 Bismuth [pg/g] 0.43 0.22 0.13 0.45 0.16 0.21 0.21 0.15 0.12 0.19 Calcium [Ng/g] 58000 55000 50000 9100 43000 40000 42000 44000 39000 58000 Cadmium [Ng/g] 0.23 0.23 0.21 0.24 0.24 0.17 0.17 0.18 0.18 0.17 Cobalt [Ng/g] 25 24 19 17 15 13 17 18 15 32 Chromium [Ng/g] 71 62 68 45 51 46 56 66 54 88 Copper [Ng/g] 9.5 12 11 9.6 9.7 7.4 9.0 7.9 7.8 10 Iron[pg/g] 62000 71000 66000 74000 65000 59000 62000 56000 57000 60000 Potassium [pg/g] 6700 7400 8300 9700 10000 11000 11000 13000 12000 6600 Lithium [pg/g] 570 660 550 470 480 380 510 510 570 430 Magnesium [lag/g] 29000 27000 20000 9100 15000 14000 19000 22000 16000 35000 Manganese[pg/g] 1300 1500 1400 1600 1400 1300 1400 1200 1300 1100 Molybdenum [Ng/g] 2.7 10 3.8 0.6 3.3 2.4 3.0 2.9 3.5 2.1 Sodium [Ng/g] 19000 19000 23000 3900 25000 31000 20000 17000 21000 18000 Nickel[pg/g] 8.5 7.4 7.7 5.7 6.0 5.6 5.5 6.9 5.7 20 Phosphorus[pg/g] 820 1300 1200 840 1200 1200 970 670 870 870 Lead [lag/g] 5.7 7.1 8.9 17 11 10 10 11 12 5.3 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [Ng/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Tin [Ng/g] 18 33 15 8 7 23 8 13 10 16 Strontium [Ng/g] 250 270 300 60 290 270 240 170 260 200 Thorium [Ng/g] 0.81 0.94 1.3 3.4 2.4 2.5 3.5 6.0 3.3 0.80 Titanium [Ng/g] 7000 8600 8400 9300 7400 7400 7500 6000 6300 5800 Thallium [lag/g] 0.83 1.3 0.37 1.3 0.71 1.1 0.99 0.93 0.87 1.1 Uranium [lag/g] 1.2 0.79 0.56 2.0 0.92 2.4 1.6 1.9 1.1 1.7 Vanadium [Ng/g] 210 230 180 160 150 140 200 180 150 200 Tungsten [Ng/g] 0.41 0.43 0.38 1.6 0.43 0.56 0.66 0.80 0.52 0.42 Yttrium [Ng/g] 40 47 37 55 37 28 36 48 40 33 Zinc [lag/g] 100 130 120 160 120 110 100 110 100 89 Page 7 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. 0 SGS- SGS Canada Inc. P.O. Box 4300 - 185 Concession St. Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 18-BD-131-2 Project : CA20M-00000-110-17234-01 LR Report: CA14338-FEB19 55: 56: 57: 58: 59: 60: 61: 62: 63: 18-BD-131-3 18-BD-131-4 18-BD-131-5 18-BD-131-6 18-BD-131-7 18-BD-131-8 18-BD-183-1 18-BD-183-2 18-BD-183-3 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 25.4 23.2 21.5 22.6 20.3 20.6 21.3 17.2 20.8 23.6 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [pg/g] 79000 82000 88000 83000 83000 87000 76000 130000 100000 87000 Arsenic [pg/g] 1.0 0.8 0.9 0.5 1.0 1.1 4.7 5.6 3.4 1.6 Boron[pg/g] <1 <1 <1 <1 1.1 <1 <1 <1 <1 <1 Barium [pg/g] 370 250 140 120 160 160 120 110 590 330 Beryllium [pg/g] 2.2 3.6 1.8 9.6 3.7 2.4 6.4 132 19 3.4 Bismuth [pg/g] 0.11 0.37 0.16 0.11 0.27 0.20 0.43 0.82 0.84 0.20 Calcium [pg/g] 47000 52000 69000 60000 66000 65000 62000 1500 5500 47000 Cadmium [pg/g] 0.12 0.17 0.19 0.16 0.18 0.17 0.19 0.08 0.30 0.21 Cobalt [pg/g] 26 24 38 33 40 40 41 22 33 19 Chromium [pg/g] 63 94 100 76 42 35 41 39 39 36 Copper [pg/g] 11 18 15 11 16 13 14 13 15 7.5 Iron[pg/g] 55000 71000 71000 63000 80000 82000 83000 110000 89000 70000 Potassium [pg/g] 12000 8500 6100 6200 7600 8700 8700 2400 7900 7900 Lithium [pg/g] 360 420 470 420 620 720 760 340 970 1000 Magnesium [pg/g] 25000 26000 41000 36000 37000 38000 38000 3100 12000 18000 Manganese[pg/g] 1000 1400 1300 1200 1400 1400 1500 1200 2100 1500 Molybdenum [pg/g] 6.3 6.0 3.7 3.9 3.3 3.5 3.2 2.2 1.5 1.7 Sodium [pg/g] 17000 21000 18000 19000 9600 11000 9700 540 3300 22000 Nickel [pg/g] 9.9 12 23 24 10 11 9.5 9.6 8.9 6.3 Phosphorus[pg/g] 300 1000 610 610 290 460 690 780 1500 1400 Lead [pg/g] 17 7.5 4.5 4.8 5.5 6.4 5.6 15 13 9.8 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [pg/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 0.8 < 0.7 < 0.7 Tin [pg/g] 7 18 < 6 22 30 12 38 19 23 < 6 Strontium [pg/g] 210 270 260 230 230 240 150 9.58 27 310 Thorium [pg/g] 7.6 2.3 0.87 0.73 1.4 1.6 2.3 3.4 3.5 1.8 Titanium [pg/g] 4200 8000 8400 7000 8700 8800 8100 12000 10000 9800 Page 8 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. 0 SGS- SGS Canada Inc. P.O. Box 4300 - 185 Concession St. Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 18-BD-131-2 Project : CA20M-00000-110-17234-01 LR Report: CA14338-FEB19 55: 56: 57: 58: 59: 60: 61: 62: 63: 18-BD-131-3 18-BD-131-4 18-BD-131-5 18-BD-131-6 18-BD-131-7 18-BD-131-8 18-BD-183-1 18-BD-183-2 18-BD-183-3 Thallium [pg/g] 0.55 0.51 0.42 0.46 0.73 1.5 1.3 0.58 1.4 0.54 Uranium [pg/g] 1.6 0.91 0.35 0.80 0.97 0.61 1.2 1.8 2.6 0.83 Vanadium [pg/g] 170 200 240 200 370 370 350 320 200 220 Tungsten [pg/g] 0.53 0.51 0.33 0.55 0.57 0.52 0.57 2.0 4.5 0.69 Yttrium [pg/g] 24 36 41 32 48 60 64 17 59 38 Zinc [pg/g] 71 110 92 86 99 93 110 110 210 130 Analysis 64: 65: 66: 67: 68: 69: 70: 71: 72: 73: 18-B D-183-4 18-B D-183-5 18-B D-183-6 18-B D-183-7 18-B D-183-8 18-B D-214-1 18-B D-214-2 18-B D-214-3 18-B D-214-4 18-B D-214-5 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 26.1 25.6 25.0 25.7 25.3 23.7 26.4 23.0 22.5 26.2 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [pg/g] 82000 79000 80000 85000 79000 96000 94000 82000 31000 77000 Arsenic [pg/g] 1.4 1.2 1.5 0.9 1.2 2.1 1.2 1.5 2.1 0.9 Boron [pg/g] < 1 < 1 < 1 < 1 < 1 3.4 < 1 1.5 21 1.1 Barium [pg/g] 420 400 320 450 370 120 290 250 110 200 Beryllium [pg/g] 3.8 2.2 2.4 5.3 4.8 5.6 30 20 0.92 74 Bismuth [pg/g] 0.25 0.23 0.22 0.17 0.19 0.26 1.0 0.30 0.19 0.79 Calcium [pg/g] 36000 44000 50000 46000 43000 170 8100 48000 17000 33000 Cadmium [pg/g] 0.18 0.16 0.19 0.19 0.14 0.10 0.33 0.26 0.05 0.31 Cobalt [pg/g] 16 16 18 17 15 27 13 23 22 11 Chromium [pg/g] 47 53 52 58 49 57 32 64 37 63 Copper [pg/g] 7.2 7.2 8.8 7.2 8.3 12 11 16 23 8.7 Iron[pg/g] 57000 56000 61000 59000 56000 71000 44000 75000 39000 53000 Potassium [pg/g] 16000 14000 14000 16000 12000 2900 17000 8900 2900 7800 Lithium [pg/g] 640 270 180 270 510 320 580 590 400 2900 Magnesium [pg/g] 16000 19000 21000 20000 17000 4700 10000 23000 15000 12000 Manganese[pg/g] 1300 1200 1400 1300 1200 1500 1200 1900 430 1600 Page 9 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 64: 65: 66: 67: 68: 69: 70: 71: 72: 73: 18-B D-183-4 18-B D-183-5 18-B D-183-6 18-B D-183-7 18-B D-183-8 18-B D-214-1 18-B D-214-2 18-B D-214-3 18-B D-214-4 18-B D-214-5 Molybdenum [pg/g] 2.8 2.7 2.3 3.0 3.8 0.5 0.4 3.1 2.3 2.8 Sodium [pg/g] 22000 21000 20000 22000 19000 280 19000 21000 2300 22000 Nickel [pg/g] 5.6 4.7 4.6 5.3 5.4 20 8.8 15 18 7.1 Phosphorus[pg/g] 830 810 820 840 960 680 940 1500 790 1800 Lead [pg/g] 13 13 13 13 12 12 11 8.3 2.5 7.6 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [pg/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Tin [pg/g] 13 < 6 < 6 < 6 6 34 32 21 < 6 35 Strontium [pg/g] 230 230 210 240 240 2.34 46 260 63 250 Thorium [pg/g] 3.5 4.3 4.0 2.7 4.4 2.4 2.2 1.8 0.51 1.1 Titanium [pg/g] 6700 6100 6300 6300 6500 7100 3400 9500 1600 6600 Thallium [pg/g] 0.83 0.46 0.36 0.53 0.91 0.74 6.5 1.7 0.23 1.6 Uranium [pg/g] 2.0 2.1 1.3 1.5 1.5 1.7 3.0 0.92 0.33 1.5 Vanadium [pg/g] 150 150 180 170 150 140 110 280 76 97 Tungsten [pg/g] 0.82 1.8 0.77 0.61 0.84 2.2 1.1 0.62 0.068 0.57 Yttrium [pg/g] 38 39 43 42 32 27 18 29 8.6 19 Zinc [pg/g] 110 98 100 100 94 93 140 120 60 180 Analysis 74: 18-BD-214-6 75: 18-BD-214-7 76: 18-BD-207-1 77: 18-BD-207-2 78: 18-BD-207-3 79: 18-BD-207-4 80: 18-BD-207-5 81: 18-BD-207-6 82: 18-BD-207-7 83: 18-BD-207-8 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 23.4 25.4 26.1 23.0 23.6 24.2 24.2 23.4 23.3 25.5 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [pg/g] 84000 84000 91000 94000 26000 52000 83000 83000 87000 54000 Arsenic [pg/g] 1.6 1.0 6.6 2.1 0.7 1.0 0.9 1.2 0.9 1.2 Boron [pg/g] < 1 < 1 1.5 < 1 21 13 < 1 < 1 < 1 2.8 Barium [pg/g] 220 230 180 340 220 270 230 240 290 200 Beryllium [pg/g] 2.1 15 7.7 7.1 0.43 1.8 3.8 10 3.7 3.3 0 Page 10 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. 0 SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 74: 75: 76: 77: 78: 79: 80: 81: 82: 83: 18-BD-214-6 18-BD-214-7 18-BD-207-1 18-BD-207-2 18-BD-207-3 18-BD-207-4 18-BD-207-5 18-BD-207-6 18-BD-207-7 18-BD-207-8 Bismuth [pg/g] 0.19 0.14 0.72 0.41 0.09 0.20 0.26 0.27 0.26 0.22 Calcium [Ng/g] 54000 44000 800 21000 11000 28000 54000 51000 53000 35000 Cadmium [Ng/g] 0.21 0.28 0.16 0.52 0.05 0.15 0.18 0.12 0.16 0.14 Cobalt [Ng/g] 23 23 22 27 20 23 29 35 31 20 Chromium [Ng/g] 72 72 55 48 30 53 77 68 84 59 Copper [Ng/g] 15 15 17 14 18 16 23 26 29 15 Iron[pg/g] 80000 61000 66000 68000 37000 56000 75000 81000 83000 57000 Potassium [pg/g] 6600 8800 7300 12000 9000 11000 9200 9700 11000 8500 Lithium [pg/g] 390 380 240 420 400 570 690 820 570 410 Magnesium [fag/g] 25000 24000 4700 19000 15000 22000 24000 23000 24000 20000 Manganese[pg/g] 1800 1300 1200 1500 380 870 1400 1100 1300 1100 Molybdenum [Ng/g] 5.4 2.7 1.1 1.0 1.5 2.5 2.5 2.5 2.4 3.5 Sodium [Ng/g] 19000 20000 420 6500 1600 6400 15000 16000 16000 11000 Nickel [pg/g] 11 13 17 13 13 15 19 15 23 8.8 Phosphorus[pg/g] 2000 930 510 640 800 1200 870 770 560 670 Lead [fag/g] 6.7 7.5 17 11 1.6 3.9 7.3 8.4 9.3 6.8 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [Ng/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Tin [Ng/g] < 6 19 18 20 < 6 12 22 27 9 12 Strontium [Ng/g] 320 250 12 110 26 110 280 290 320 170 Thorium [Ng/g] 1.4 2.0 5.1 3.4 1.7 2.1 2.3 3.9 3.2 3.1 Titanium [Ng/g] 11000 7300 10000 6900 1500 2700 10000 11000 12000 3600 Thallium [pg/g] 0.48 0.69 1.1 2.1 0.49 1.2 1.1 1.3 0.74 0.44 Uranium [pg/g] 0.55 1.2 3.1 2.2 0.90 0.91 0.84 1.2 1.4 1.6 Vanadium [Ng/g] 230 190 180 170 69 170 330 440 430 190 Tungsten [Ng/g] 0.56 0.49 3.1 0.57 0.041 0.21 0.47 0.64 0.63 1.0 Yttrium [Ng/g] 32 16 20 26 7.2 18 22 17 23 27 Zinc [fag/g] 110 97 79 110 62 95 96 100 110 80 Page 11 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. 0 SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 84: 85: 86: 87: 88: 89: 90: 91: 92: 93: 18-B D-207-9 18-B D-212-1 18-B D-212-2 18-B D-212-3 18-B D-212-4 18-B D-212-5 18-B D-212-6 18-B D-212-7 18-B D-197-1 18-B D-197-2 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 26.3 23.3 26.4 26.1 26.2 24.0 22.8 24.6 24.3 25.2 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [pg/g] 21000 93000 71000 76000 76000 74000 70000 74000 77000 72000 Arsenic [pg/g] 1.0 15 2.2 2.2 1.6 1.9 2.7 4.9 2.6 2.2 Boron [pg/g] 24 < 1 < 1 < 1 < 1 2.2 1.2 1.2 < 1 < 1 Barium [pg/g] 220 370 450 510 490 300 420 400 510 470 Beryllium [pg/g] 0.88 5.8 3.1 3.4 5.2 2.2 7.0 5.8 3.2 3.2 Bismuth [pg/g] < 0.09 0.27 0.12 0.21 0.29 0.18 0.95 0.24 0.29 0.46 Calcium [pg/g] 11000 510 33000 38000 36000 50000 40000 40000 37000 43000 Cadmium [pg/g] 0.08 0.04 0.15 0.14 0.18 0.15 0.14 0.19 0.18 0.15 Cobalt [pg/g] 12 22 13 14 14 32 45 20 21 20 Chromium [pg/g] 39 35 52 56 54 190 490 120 37 40 Copper [pg/g] 18 11 5.2 7.3 8.1 20 26 17 12 13 Iron[pg/g] 35000 72000 51000 56000 56000 59000 64000 65000 72000 69000 Potassium [pg/g] 12000 9000 13000 15000 15000 13000 21000 14000 14000 14000 Lithium [pg/g] 500 870 480 310 390 440 1100 770 510 640 Magnesium [pg/g] 11000 9400 13000 15000 14000 36000 55000 22000 15000 15000 Manganese[pg/g] 580 1100 1100 1200 1400 1200 1200 1400 1400 1300 Molybdenum [pg/g] 1.1 1.4 0.8 2.6 2.6 1.9 1.3 2.9 1.2 2.0 Sodium [pg/g] 1100 480 21000 24000 23000 19000 13000 21000 18000 21000 Nickel [pg/g] 7.0 9.1 4.8 4.7 5.2 81 230 38 5.0 4.8 Phosphorus[pg/g] 1600 590 800 920 1000 540 2000 1200 1400 1500 Lead [pg/g] 2.4 19 14 15 14 9.4 8.9 12 13 13 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [pg/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Tin [pg/g] < 6 9 < 6 < 6 8 < 6 22 29 < 6 < 6 Strontium [pg/g] 17 5.08 210 230 230 270 210 240 230 270 Thorium [pg/g] 3.6 2.1 2.7 4.2 3.8 2.5 2.1 2.4 3.7 3.2 Titanium [pg/g] 1900 8200 5900 6300 6600 5900 5600 7200 10000 9700 Page 12 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. 0 SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 84: 85: 86: 87: 88: 89: 90: 91: 92: 93: 18-B D-207-9 18-B D-212-1 18-B D-212-2 18-B D-212-3 18-B D-212-4 18-B D-212-5 18-B D-212-6 18-B D-212-7 18-B D-197-1 18-B D-197-2 Thallium [pg/g] 1.4 1.6 0.57 0.64 0.71 0.55 2.0 1.2 0.71 0.85 Uranium [pg/g] 2.4 3.1 1.3 1.8 1.8 0.94 0.92 1.4 1.5 1.6 Vanadium [pg/g] 84 160 140 130 140 160 150 150 200 190 Tungsten [pg/g] 0.093 1.6 0.68 0.93 0.69 0.44 0.39 1.1 1.2 1.3 Yttrium [pg/g] 14 16 27 34 31 27 27 34 34 35 Zinc [pg/g] 61 130 100 110 110 82 93 120 120 120 Analysis 94: 95: 96: 97: 98: 99: 100: 101: 102: 103: 18-B D-197-3 18-B D-197-4 18-B D-197-5 18-B D-197-6 18-B D-197-7 18-B D-177-1 18-B D-177-2 18-B D-177-3 18-B D-177-4 18-B D-177-5 Sample Date & Time N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Silica [%] 27.4 33.4 25.4 25.2 25.6 25.0 21.4 24.5 24.9 23.7 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver[pg/g] <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Aluminum [pg/g] 72000 66000 73000 72000 70000 79000 94000 82000 78000 72000 Arsenic [pg/g] 1.5 1.5 2.0 1.4 4.2 6.5 3.3 2.5 1.5 1.5 Boron [pg/g] 1.1 1.2 1.2 < 1 < 1 1.9 1.6 1.1 < 1 1.2 Barium [pg/g] 330 590 460 420 330 230 500 400 400 340 Beryllium [pg/g] 32 5.2 2.5 2.5 18 12 7.8 4.3 2.9 5.2 Bismuth [pg/g] 0.87 0.23 0.37 0.31 1.2 1.1 0.24 0.35 0.34 0.60 Calcium [pg/g] 31000 11000 39000 44000 44000 740 11000 41000 49000 43000 Cadmium [pg/g] 0.21 0.05 0.16 0.14 0.21 0.05 0.22 0.20 0.26 0.17 Cobalt [pg/g] 13 2.7 16 21 19 27 27 21 21 17 Chromium [pg/g] 55 48 64 76 66 73 52 53 70 50 Copper [pg/g] 11 3.9 15 17 12 11 11 8.2 7.5 10 Iron[pg/g] 51000 14000 57000 57000 52000 60000 80000 63000 68000 64000 Potassium [pg/g] 16000 32000 15000 13000 13000 7200 8100 10000 10000 11000 Lithium [pg/g] 720 350 710 680 980 1100 520 430 410 900 Magnesium [pg/g] 10000 2700 15000 18000 16000 3800 14000 20000 22000 16000 Manganese[pg/g] 1100 210 1200 1200 1100 1100 1700 1400 1500 1300 Page 13 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 94: 95: 96: 97: 98: 99: 100: 101: 102: 103: 18-B D-197-3 18-B D-197-4 18-B D-197-5 18-B D-197-6 18-B D-197-7 18-B D-177-1 18-B D-177-2 18-B D-177-3 18-B D-177-4 18-B D-177-5 Molybdenum [pg/g] 4.8 3.3 4.7 3.2 3.6 1.0 0.7 0.6 3.8 4.0 Sodium [pg/g] 28000 25000 24000 20000 24000 3700 1700 19000 21000 21000 Nickel [pg/g] 4.8 4.2 6.9 12 12 15 8.1 6.0 7.3 6.8 Phosphorus[pg/g] 1100 290 920 800 920 500 910 1100 940 1100 Lead [pg/g] 14 28 13 12 12 15 12 9.7 11 10 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [pg/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Tin [pg/g] 11 < 6 < 6 6 13 20 < 6 7 < 6 11 Strontium [pg/g] 200 120 260 270 240 13 29 280 300 310 Thorium [pg/g] 3.8 16 3.3 3.8 1.9 2.4 2.2 2.4 2.5 1.3 Titanium [pg/g] 6500 1500 7000 6900 6200 9900 11000 8100 7900 7600 Thallium [pg/g] 1.4 0.90 0.82 0.61 1.6 1.6 1.6 1.1 0.59 1.6 Uranium [pg/g] 3.9 3.4 1.6 1.3 2.1 2.8 1.9 1.1 1.2 0.81 Vanadium [pg/g] 120 20 160 170 150 170 210 190 200 180 Tungsten [pg/g] 1.2 0.32 1.1 1.0 1.2 4.0 4.3 1.2 0.76 0.52 Yttrium [pg/g] 31 13 30 29 20 14 26 34 32 20 Zinc [pg/g] 100 37 94 95 100 84 140 110 110 110 Analysis 104: 105: 106: 107: 108: 109: 18-B D-177-6 18-B D-177-7 18-B D-177-8 18-B D-177-9 18-B D-177-10 18-B D-177-11 Sample Date & Time N/A N/A N/A N/A N/A N/A Silica [%] 24.1 23.9 26.0 25.0 24.3 27.1 Mercury [ug/g] < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Silver [pg/g] < 1 < 1 < 1 < 1 < 1 < 1 Aluminum [pg/g] 74000 82000 70000 76000 76000 79000 Arsenic [pg/g] 1.0 5.3 3.2 1.4 2.7 2.0 Boron [pg/g] < 1 1.5 3.4 1.2 < 1 < 1 Barium [pg/g] 340 470 310 380 340 290 Beryllium [pg/g] 3.0 2.7 10 3.2 3.0 19 Page 14 of 16 0 it N Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. 0 SGS- SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report: CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Analysis 104: 105: 106: 107: 108: 109: 18-B D-177-6 18-B D-177-7 18-B D-177-8 18-B D-177-9 18-B D-177-10 18-B D-177-11 Bismuth [pg/g] 0.45 0.24 0.61 0.21 0.59 0.33 Calcium [Ng/g] 44000 44000 40000 46000 47000 37000 Cadmium [Ng/g] 0.19 0.21 0.23 0.25 0.25 0.18 Cobalt [Ng/g] 18 18 15 16 18 13 Chromium [Ng/g] 46 54 46 56 52 73 Copper [Ng/g] 7.7 11 7.3 9.5 21 9.5 Iron [Ng/g] 66000 69000 57000 65000 69000 56000 Potassium [pg/g] 9700 14000 10000 9100 10000 9500 Lithium [pg/g] 1000 950 890 850 730 950 Magnesium [fag/g] 17000 18000 15000 18000 18000 14000 Manganese [pg/g] 1300 1300 1200 1400 1500 1200 Molybdenum [Ng/g] 3.0 3.9 2.9 3.1 2.6 6.5 Sodium [Ng/g] 21000 20000 22000 22000 21000 28000 Nickel [Ng/g] 7.0 8.0 4.1 5.2 5.5 5.6 Phosphorus [pg/g] 1200 1200 980 990 1000 1100 Lead [fag/g] 10 10 10 11 11 9.4 Antimony [pg/g] < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Selenium [Ng/g] < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Tin [Ng/g] < 6 < 6 8 7 6 23 Strontium [Ng/g] 330 350 270 290 290 240 Thorium [Ng/g] 1.4 2.2 1.8 2.0 2.1 1.9 Titanium [Ng/g] 8000 8000 7200 7800 8500 6300 Thallium [pg/g] 0.57 1.2 0.76 0.44 0.72 1.7 Uranium [pg/g] 0.71 0.97 1.7 0.90 0.88 3.1 Vanadium [Ng/g] 180 180 170 170 200 140 Tungsten [Ng/g] 0.44 0.63 0.57 0.58 0.56 0.61 Yttrium [Ng/g] 21 29 26 37 40 28 Zinc [fag/g] 120 120 100 120 120 110 Page 15 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. S r-, SGS Canada Inc. Project : CA20M-00000-110-17234-01 P.O. Box 4300 - 185 Concession St. LR Report : CA14338-FEB19 Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 r Patti Stark Project Specialist, Environment, Health & Safety Page 16 of 16 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_ and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt" is representative of the whole shipment and may not reflect the temperature of individual samples. SGS Elemental Analysis Tailings Tailings Samples from Mineral Research Lab Piedmont Lithium Project Phase 1 Characterization SGS Reference No.: CA20M-00000-110-17234-01 Parameter Unit DL Tailings 1 Tailings 2 Tailings 3 Tailings 4 Tailings 5 Tailings 6 Tailings 7 Tailings 8 Tailings 9 Tailings 10 LIMS 14494-FEB19 14494-FEB19 14494-FEB19 14494-FEB19 14494-FEB19 14494-FEB19 14494-FEB19 14494-FEB19 14494-FEB19 14494-FEB19 Si % 33.2 33.4 34.5 35.3 36.0 35.5 36.3 35.9 36.1 35.4 Hg pg/g 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 Ag pg/g 0.01 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Al pg/g 3 64000 57000 55000 65000 63000 67000 66000 62000 63000 64000 As pg/g 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 B pg/g 1 <1 <1 1.2 <1 <1 <1 <1 <1 <1 <1 Ba pg/g 0.01 19 20 19 22 22 25 21 21 20 22 Be pg/g 0.02 27 26 22 24 27 24 22 20 30 21 Bi pg/g 0.09 1.2 0.39 1.1 1.7 0.77 0.60 0.74 0.70 1.5 0.86 Ca pg/g 3 1000 880 920 1000 1100 1100 1100 1000 1100 1100 Cd pg/g 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 < 0.02 Co pg/g 0.01 0.10 0.11 0.11 0.15 0.12 0.16 0.12 0.11 0.15 0.13 Cr pg/g 0.5 4.5 3.3 < 3 < 3 < 3 5.2 < 3 < 3 3.6 < 3 Cu pg/g 0.1 3.0 0.4 0.3 0.2 0.3 3.0 0.8 0.2 0.7 0.2 Fe pg/g 3 1200 1300 1300 1500 1300 1300 1400 1200 1400 1400 K pg/g 3 22000 21000 21000 23000 22000 23000 23000 22000 23000 23000 Li pg/g 2 290 260 270 260 250 260 300 220 340 260 Mg pg/g 3 143 147 157 183 169 160 173 153 182 175 Mn pg/g 0.1 94 91 95 95 93 93 96 89 104 92 MO pg/g 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 Na pg/g 3 32000 32000 31000 31000 32000 34000 32000 33000 31000 32000 Ni pg/g 0.1 0.5 0.4 0.4 0.8 0.6 0.5 0.5 0.5 0.6 0.5 P pg/g 3 390 380 360 380 370 400 380 400 390 380 Pb pg/g 0.05 12 12 12 12 12 13 12 13 12 13 S b pg/g 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 < 0.8 Se pg/g 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 < 0.7 Sn pg/g 6 47 48 49 56 51 47 53 45 54 52 Sr pg/g 0.02 19 17 17 19 19 21 20 18 20 19 Th pg/g 0.01 0.13 0.10 0.15 0.11 0.13 0.11 0.11 0.13 0.14 0.22 Ti pg/g 0.1 54 58 58 68 58 57 63 53 65 66 TI pg/g 0.02 5.1 5.1 4.9 5.2 5.2 5.3 5.3 5.0 5.3 5.2 U pg/g 0.002 1.2 0.92 2.6 1.2 0.93 1.9 1.3 1.4 1.3 6.4 V pg/g 1 1 1 1 1 1 1 1 1 1 1 W pg/g 0.04 0.74 0.71 0.73 0.84 0.74 0.74 0.76 0.64 0.76 0.76 Y pg/g 0.004 0.14 0.12 0.11 0.15 0.15 0.14 0.13 0.12 0.18 0.18 Zn pg/g 0.7 22 22 21 24 21 22 24 19 24 24 SGS Minerals Services Tailings Phase 1 APPENDIX Fe J CHROMIUM SPECIATION RESULTS FOR SELECT WASTE ROCK SAMPLES Dl CHROMIUM VI DATA SUMMARY Z7keSWILWILLER SOCI ES° Waste RockTailings Samples from Mineral Research Lab Piedmont Lithium Project Phase 2 Characterization SGS Reference No.: CA20M-00000-110-17234-01 Chromium 6 Data Selected Waste Rock and Waste Rock Time 0 Humidity Cell Data Parameter Unit DL 18-BD-205-7 18-BD-212-6 LIMS 14338-FEB19 14338-FEB19 Cr Total pg/g 0.3 45 490 LIMS 14941-JUN19 14941-JUN19 Cr (VI) pg/g 0.2 <0.2 <0.2 LIMS 0.01 10458-J U N 19 10458-J U N 19 pH no unit 0.00001 8.01 7.77 Cr in Week 0 HCT pg/L 0.001 <0.08 0.09 Cr (VI) in Week 0 HCT pg/L 0.002 <0.2 <0.2 SGS Minerals Services Chrome 6 Data D2 ELEMENTAL WASTE ROCK RESULTS (SEE APPENDIX C - ELEMENTAL ANALYSIS SUMMARY FOR WASTE ROCK AND TAILINGS) 71�hASHULINkILLER SOCI ES° D3 CHROMIUM VI RESULTS FROM SOLID MATERIAL kRSHkLL ILLER SOCI ES° SGS Canada Inc. P.O. Box 4300 - 185 Concession St. Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 SGS Lakefield Environmental Met Attn : Barb Bowman Project: CA20M-00000-110-17234-01 03-July-2019 Date Rec.: 24 June 2019 LR Report: CA14941-JUN19 Reference: 17234-01-05 Copy: #1 CERTIFICATE OF ANALYSIS Final Report Analysis 3: 4: 5: 6: 7: 9: 10: Analysis Analysis QC - Blank QC - STD % QC - DUP % 18-BD-205-7 18-BD-212-6 Completed Date Completed Recovery RPD Time Sample Date & Time N/A N/A Chromium VI [Ng/g] 28-Jun-19 16:03 < 0.2 97% ND < 0.2 < 0.2 ND - Not Det ect ed Patti Stark Project Specialist, Environment, Health & Safety Page 1 of 1 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. D4 HUMIDITY CELL RESULTS, WEEK 0 71�MZSHULWILLER SOCI ES° SGS Canada Inc. P.O. Box 4300 - 185 Concession St. Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 SGS Lakefield Environmental Met Attn : Barb Bowman Project: 20M-00000-110-17234-01 27-June-2019 Date Rec.: 13 June 2019 LR Report: CA10458-JUN19 Reference: Wk# 0 Copy: #3 CERTIFICATE OF ANALYSIS Final Report - Revised Analysis 3: 4: 5: 6: 7: 8: 9: 10: 11: Analysis Analysis QC - Blank QC - STD % QC - DUP % QC - Spike 18-BD-205-7 18-BD-212-6 Tailings 4 Approval Approval Recovery RPD Rep Wk# 0 Wk# 0 Wk# 0 Date Time Sample Date & Time 13-Jun-19 13-Jun-19 13-Jun-19 Hum Cell Leachate Volume [mL] 13-Jun-19 13:06 812 788 612 pH [no unit] 19-Jun-19 11:33 NA 100% 1% NA 8.01 7.77 6.89 Acidity [mg/L as CaCO3] 19-Jun-19 11:33 < 2 100% ND NA < 2 < 2 < 2 Alkalinity [mg/L as CaCO3] 19-Jun-19 11:33 < 2 102% 0% NA 22 24 8 Conductivity [uS/cm] 19-Jun-19 11:33 < 2 98% 0% NA 44 82 28 Sulphate [mg/L] 14-Jun-19 14:45 < 0.2 92% NV NV 0.5 6.2 1.4 Chromium VI [ug/L] 25-Jun-19 11:25 < 0.2 109% 10% 94% < 0.2 < 0.2 < 0.2 Mercury [mg/L] 17-Jun-19 14:41 < 0.00001 118% 85% 110% < 0.00001 < 0.00001 < 0.00001 Silver [mg/L] 19-Jun-19 08:26 < 0.00005 96% ND 95% < 0.00005 < 0.00005 < 0.00005 Aluminum [mg/L] 19-Jun-19 08:26 < 0.001 96% 5% NV 0.111 0.063 0.055 Arsenic [mg/L] 19-Jun-19 08:26 < 0.0002 93% 3% NV 0.0002 0.0011 0.0010 Boron [mg/L] 19-Jun-19 08:26 < 0.002 93% 5% NV 0.003 0.002 0.005 Barium [mg/L] 19-Jun-19 08:26 < 0.00002 96% 4% NV 0.00070 0.00338 0.00025 Beryllium [mg/L] 19-Jun-19 08:26 < 0.000007 101% ND 86% < 0.000007 < 0.000007 0.000027 Bismuth [mg/L] 19-Jun-19 08:26 < 0.000007 99% ND 107% < 0.000007 < 0.000007 0.000017 Calcium [mg/L] 19-Jun-19 08:26 < 0.01 96% 3% 130% 4.30 6.08 0.44 Cadmium [mg/L] 19-Jun-19 08:26 < 0.000003 96% 3% 80% < 0.000003 < 0.000003 < 0.000003 Cobalt [mg/L] 19-Jun-19 08:26 < 0.000004 94% 1 % 98% 0.000018 0.000048 0.000027 Chromium [mg/L] 19-Jun-19 08:26 < 0.00008 94% ND 107% < 0.00008 0.00009 0.00015 Copper [mg/L] 19-Jun-19 08:26 < 0.0002 94% 6% 114% 0.0005 0.0004 0.0030 Iron [mg/L] 19-Jun-19 08:26 < 0.007 96% 5% NV 0.007 < 0.007 < 0.007 Potassium [mg/L] 19-Jun-19 08:26 < 0.009 98% 4% 120% 1.80 7.89 0.459 Lithium [mg/L] 19-Jun-19 08:26 < 0.0001 100% 2% 102% 0.317 0.589 0.0800 Magnesium [mg/L] 19-Jun-19 08:26 < 0.001 104% 4% 92% 0.177 0.766 0.050 Manganese [mg/L] 19-Jun-19 08:26 < 0.00001 95% 4% 124% 0.00110 0.00227 0.00277 Molybdenum[mg/L] 19-Jun-19 08:26 <0.00004 101% 3% 114% 0.00095 0.00161 0.00133 Sodium [mg/L] 19-Jun-19 08:26 < 0.01 92% 4% 127% 2.28 2.13 4.54 Nickel[mg/L] 19-Jun-19 08:26 <0.0001 95% 6% 101% 0.0001 0.0006 0.0003 Phosphorus [mg/L] 19-Jun-19 08:26 < 0.003 96% 0% NV 0.003 0.005 0.065 Lead [mg/L] 19-Jun-19 08:26 < 0.00001 92% 10% 90% 0.00004 0.00001 0.00010 Antimony [mg/L] 19-Jun-19 08:26 < 0.0009 97% ND 101% < 0.0009 < 0.0009 < 0.0009 Selenium [mg/L] 19-Jun-19 08:26 < 0.00004 104% 7% NV 0.00015 0.00042 0.00005 Silicon [mg/L] 19-Jun-19 08:26 < 0.02 99% 5% NV 0.47 0.65 0.47 Tin [mg/L] 19-Jun-19 08:26 < 0.00006 104% ND NV 0.00016 0.00016 0.00043 Strontium [mg/L] 19-Jun-19 08:26 < 0.00002 97% 3% 124% 0.00624 0.0157 0.00159 Page 1 of 2 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_ and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt" is representative of the whole shipment and may not reflect the temperature of individual samples. SGS Canada Inc. P.O. Box 4300 - 185 Concession St. Lakefield - Ontario - KOL 2HO Phone: 705-652-2000 FAX: 705-652-6365 Project: 20M-00000-110-17234-01 LR Report: CA10458-JUN19 Analysis S: 4: o: b: f: ts: a: lu: ll: Analysis Analysis QC - Blank QC - STD % QC - DUP % QC - Spike 18-BD-205-7 18-BD-212-6 Tailings 4 Approval Approval Recovery RPD Rep Wk# 0 Wk# 0 Wk# 0 Date Time Titanium [mg/L] 19-Jun-19 08:26 <0.00005 101% 19% NV 0.00024 0.00023 0.00010 Thorium [mg/L] 19-Jun-19 08:26 < 0.0001 101% ND NV < 0.0001 < 0.0001 < 0.0001 Thallium [mg/L] 19-Jun-19 08:26 < 0.000005 90% ND 83% 0.000023 0.000069 0.000012 Uranium [mg/L] 19-Jun-19 08:26 < 0.000002 94% 0% 80% 0.000031 0.000027 0.00545 Vanadium [mg/L] 19-Jun-19 08:26 < 0.00001 94% 10% 107% 0.00199 0.00059 0.00035 Tungsten [mg/L] 19-Jun-19 08:26 <0.00002 101% ND NV 0.00015 0.00010 0.00003 Yttrium [mg/L] 19-Jun-19 08:26 < 0.000002 98% 5% NV 0.000008 < 0.000002 0.000006 Zinc [mg/L] 19-Jun-19 08:26 < 0.002 97% 3% NV < 0.002 < 0.002 0.004 Zirconium [mg/L] 20-Jun-19 15:25 < 0.002 101% ND NV < 0.002 < 0.002 < 0.002 NA- Not appl i cabl ND- Not Detected NV - No Val ue Repor t r evi sed t o i ncl ude r esul t s f or Zi r coni um Repor t r evi sed t o add r esul t s f or Chr oni um VI as r equest ed by cl i ent . Patti Stark Project Specialist, Environment, Health & Safety 0 V O w Page 2 of 2 Data reported represents the sample submitted to SGS. Reproduction of this analytical report in full or in part is prohibited without prior written approval. Please refer to SGS General Conditions of Services located at http://www.sgs.com/terms_and_conditions_service.htm. (Printed copies are available upon request.) Test method information available upon request. "Temperature Upon Receipt' is representative of the whole shipment and may not reflect the temperature of individual samples. APPENDIX :9 TCLP-WASTE ROCK & TAILINGS Tailings Samples from Mineral Research Lab Piedmont Lithium Project Phase 2 Characterization SGS Reference No.: CA20M-00000-110-17234-01 EPA Method 1311 - TCLP Selected Waste Rock and Tailings Toxicity Parameter Unit DL Characteristic 18-BD-205-7 17-DB-45-3 17-BD-65A-8 18-BD-183-8 18-BD-214-6 18-BD-207-6 18-BD-212-6 18-BD-177-10 Tailings 4 Tailings 10 Limit LIMS 14243-APR19 14243-APR19 14243-APR19 14243-APR19 14243-APR19 14243-APR19 14243-APR19 14243-APR19 14243-APR19 14243-APR19 Sample weight g 100 100 100 100 100.0 100 100 100 100 100 Ext Fluid #1 or#2 1 1 1 1 1 1 1 1 1 1 Ext Volume mL 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 Final pH no unit 0.01 5.05 4.95 5.13 5.00 5.01 5.00 5.02 5.08 4.93 4.93 Hg mg/L 0.00001 0.2 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 Al mg/L 0.001 0.865 0.529 0.701 0.849 0.789 0.795 0.771 0.607 0.149 0.151 As mg/L 0.0002 5.0 0.0011 0.0009 0.0010 0.0014 0.0007 0.0009 0.0023 0.0015 0.0007 0.0007 Ag mg/L 0.00005 5.0 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 Ba mg/L 0.00002 100.0 0.181 0.194 0.156 0.246 0.203 0.125 0.228 0.298 0.0780 0.0639 Be mg/L 0.000007 0.000312 0.00119 0.00119 0.000984 0.000139 0.000438 0.00121 0.000202 0.00215 0.00235 B mg/L 0.002 0.112 0.242 0.161 0.070 0.071 0.060 0.061 0.051 0.077 0.064 Bi mg/L 0.000007 0.000010 < 0.000007 0.000014 < 0.000007 < 0.000007 < 0.000007 0.000113 0.000017 0.000322 0.000336 Ca mg/L 0.01 71.7 7.49 150 25.2 23.9 34.7 62.8 87.4 4.47 4.60 Cd mg/L 0.000003 1.0 0.000107 0.000122 0.000327 0.000085 0.000042 0.000062 0.000147 0.000393 0.000119 0.000163 Co mg/L 0.000004 0.00416 0.0538 0.00445 0.00442 0.00660 0.00417 0.0276 0.00532 0.000130 0.000156 Cr mg/L 0.00008 5.0 0.384 0.122 0.233 0.374 0.384 0.259 0.235 0.409 0.00198 0.00201 Cu mg/L 0.0002 0.0404 0.0175 0.0054 0.0261 0.0063 0.0024 0.0059 0.0022 0.0045 0.0038 Fe mg/L 0.007 53.0 18.7 38.5 54.1 61.5 40.9 40.3 55.6 0.117 0.094 K mg/L 0.009 6.48 6.79 7.70 9.61 4.86 4.18 12.4 9.52 1.24 1.24 Li mg/L 0.0001 0.128 0.156 0.150 0.161 0.118 0.119 0.166 0.169 0.0478 0.0503 Mg mg/L 0.001 1.18 1.75 3.39 1.25 1.16 1.02 2.27 1.01 0.314 0.311 Mn mg/L 0.00001 0.615 0.389 2.02 0.623 0.579 0.455 1.23 2.01 0.467 0.483 MO mg/L 0.00004 0.0226 0.00382 0.0108 0.0267 0.0115 0.0170 0.0234 0.0544 0.00077 0.00066 Na mg/L 0.01 1290 1340 1250 1340 1370 1330 1350 1320 1310 1310 Ni mg/L 0.0001 0.0330 0.0435 0.0250 0.0326 0.0311 0.0234 0.0427 0.0303 0.0017 0.0017 P mg/L 0.003 0.014 0.010 0.010 0.008 0.010 0.007 0.016 0.014 0.530 0.567 Pb mg/L 0.00001 5.0 0.00164 0.00041 0.00273 0.00355 0.00210 0.00095 0.00240 0.00175 0.00377 0.00406 Sb mg/L 0.0009 0.0015 < 0.0009 < 0.0009 < 0.0009 < 0.0009 0.0011 0.0011 < 0.0009 < 0.0009 < 0.0009 Se mg/L 0.00004 1.0 0.00013 0.00011 0.00012 0.00013 0.00006 0.00007 0.00013 0.00013 0.00007 0.00006 Si mg/L 0.02 2.54 1.82 2.50 2.62 2.86 2.12 2.05 2.16 0.53 0.48 Sn mg/L 0.00006 0.00008 < 0.00006 0.00006 0.00013 0.00010 < 0.00006 < 0.00006 0.00010 < 0.00006 < 0.00006 Sr mg/L 0.00002 0.0478 0.0571 0.276 0.0887 0.0593 0.0368 0.101 0.0685 0.0172 0.0176 Th mg/L 0.0001 0.0002 0.0003 0.0004 0.0012 0.0002 0.0003 0.0003 0.0001 < 0.0001 < 0.0001 Ti mg/L 0.00005 0.00988 0.00117 0.00049 0.00082 0.00062 0.00072 0.00071 0.00147 0.00019 0.00017 TI mg/L 0.000005 0.000378 0.000931 0.000684 0.000409 0.000094 0.000471 0.000707 0.000441 0.000164 0.000178 U mg/L 0.000002 0.000997 0.00191 0.00120 0.00105 0.000187 0.00107 0.00134 0.000192 0.00697 0.007466 V mg/L 0.00001 0.00044 0.00019 0.00008 0.00019 0.00012 0.00028 0.00023 0.00121 0.00020 0.00019 W mg/L 0.00002 0.00004 0.00004 0.00004 0.00004 0.00003 < 0.00002 0.00003 0.00011 0.00005 0.00005 Y mg/L 0.000002 0.00155 0.00135 0.00582 0.00131 0.00126 0.00126 0.00339 0.00343 0.000359 0.000389 Zn mg/L 0.002 0.038 0.057 0.037 0.032 0.025 0.016 0.016 0.020 0.045 0.039 SGS Minerals Services Waste Rock and Tailings Phase 2 0 Addendum Report: Results of Humidity Cell Leaching Tests, Piedmont Lithium Project December 2019 Prepared by Marshall Miller & Associates 582 Industrial Park Road Bluefield, Virginia 24605-9364 www.mmal.com Prepared for Piedmont Lithium, Inc. 32 North Main Street Ste 100 Belmont, North Carolina 28012 HALL LLE soa �s 582 Industrial Park Road, Bluefield, VA 24605-9364 ■ Phone 276.322.5467 www.mmal.com ■ info@mmal.com December 3, 2019 Mr. Patrick Brindle Vice President Piedmont Lithium 32 North Main Street Ste 100 Belmont, NC 28012 Subject: Addendum Report: Results of Humidity Cell Leaching Tests, Piedmont Lithium Project Dear Patrick: Enclosed is the report "Addendum Report: Results of Humidity Cell Leaching Tests, Piedmont Lithium Project". As was expected based on the previous testing results (elemental analyses, acid -base accounting, and Toxicity Characteristic Leaching Procedure), the humidity cell leaching program results continue to confirm that there is virtually no likelihood of acidic drainage to be generated by the subject site's waste rock or process tailings materials, over any timeframe; and that leaching of metals is very unlikely to reach concentrations of potential health or environmental concerns. We appreciate the opportunity to have assisted you in this important investigation. If you have any questions regarding any of the enclosed, please do not hesitate to contact us. Sincerely, MARSHALL MILLER & ASSOCIATES, INC. Ronald H. Mullennex, CPG, CGWP Senior Principal Associate Direct Line: 304-809-0705 ron.mullennex@mmal.com /drd Attachments File: PLIT108-Add Rpt Results Hum Cell Leaching Tests (rhm) 20191203.docx Kevin Andrews, PG Vice President/Supervisory Geologist Direct Line: 1 276 970 6065 Email: kevin.andrews@mmal.com ENERGY & MINERAL RESOURCES ■ HYDROGEOLOGY & GEOLOGY ■ GEOPHYSICAL LOGGING SERVICES CARBON MANAGEMENT ■ EXPERT WITNESS TESTIMONY ■ MINING ENGINEERING ■ PETROLEUM ENGINEERING ;jHALL LLE OCI ES° Table of Contents Addendum Report: Results of Humidity Cell Leaching Tests, Piedmont Lithium Project December 2019 1 Introduction.............................................................................................................................. 1 2 Humidity Cell Testing Program................................................................................................. 1 3 Testing Results.......................................................................................................................... 2 3.1 Potential for Acidic Drainage......................................................................................... 2 3.2 Potential for Significant Release of Metals..................................................................... 3 4 Summary and Conclusions........................................................................................................ 3 Tables 1 ......Summary of Acid -generating and Acid -neutralizing Depletion Rates over 20-Week Test Period 2 ......................... Summary of Humidity Cell Leaching Results Through Week 20, Waste Rock 205-7 3 ......................... Summary of Humidity Cell Leaching Results Through Week 20, Waste Rock 212-6 4 ........................ Summary of Humidity Cell Leaching Results Through Week 20, Tailings 4 Leachate Appendices A.................................................................................... Analyses of Weekly Humidity Cell Leachate A.1............................................................................................................................... Sample 205-7 A.2............................................................................................................................... Sample 212-6 A.3..........................................................................................................................Sample Tailings 4 MARSHALL MILLER & ASSOCIATES, mc. ;jHALL LLE OCI ES° 1 Introduction Addendum Report: Results of Humidity Cell Leaching Tests, Piedmont Lithium Project December 2019 In August 2019, Marshall Miller & Associates (MM&A) submitted to Piedmont Lithium a report summarizing our evaluation of the geochemical environmental impact potential of waste rock and process tailings that would result from the proposed Piedmont Lithium mine project near Bessemer City, North Carolina. That evaluation, based on laboratory test results including acid -base account (ABA), elemental analyses, and Toxicity Characteristic Leaching Procedure (TCLP) analyses of multiple samples representing waste rock and tailings materials, concluded that neither the waste rock nor the tailings would generate acidic drainage, and would not be expected to leach contaminants at hazardous levels. As of that August 2019 timeframe, additional testing of leaching potential was in progress, through a 20-week duration humidity cell leaching protocol. That humidity cell testing program is now complete. The results continue to support the indications from previous testing that no acidic or hazardous drainage is to be expected from on -site disposal of the subject materials. This report documents the humidity cell leaching test results and provides a brief summary discussion of characteristics and trends observed. 2 Humidity Cell Testing Program Two samples of potential waste rock material and one sample of the expected process tailings material were selected for humidity cell leaching tests, based on the completed ABA, elemental composition, and TCLP results. A 20-week leaching and testing program was initiated in mid -June 2019 and completed at the end of October 2019. One kilogram of each sample was crushed to pass a 0.25-inch screen and then placed in a four -inch diameter, eight -inch tall humidity cell. The initial leach at the beginning of the period is designated Week 0. Thereafter, each weekly cycle consisted of three days of dry air exposure passed through the cell from the bottom, three days of humid air exposure in the same manner, then a flush using one liter of deionized water added through the top of the cell and allowed to stand for one hour. Each weekly leachate sample was analyzed as to pH, acidity, alkalinity, electrical conductivity (EC), and sulfate. An extensive analysis suite of metals was performed weekly through Week 5, then every fifth week for the remainder of the program period. The initial leach (Week 0) was analyzed for hexavalent chromium (in addition to total chromium, which was included in the extensive metals analytical suite). The test program duration was intended to clearly define both the long-term acid generation potential and the long-term metals leaching potential, and that objective was satisfied by the 20-week program. As is discussed further below, the trends of relative weathering rates of acid -generating and acid - neutralizing sources point conclusively to there being no potential for significant acidic drainage from any of the tested materials, and the weathering release of metals is at a very low rate that diminished with time. MARSHALL MILLER & ASSOCIATES, mc. 1 MSOCIHALL LLE ES° 3 Testing Results Addendum Report: Results of Humidity Cell Leaching Tests, Piedmont Lithium Project December 2019 Two waste rock samples were selected for humidity cell testing, based on their geochemicaI differences in TCLP testing and ratio of acid neutralization potential to maximum potential acid generation (NP/MPA ratio). Sample 18-BD-205-7 (205-7) exhibits a NP/MPA ratio of 31.20, which is moderately high in comparison to most of the waste rock samples. Sample 18-BD-212-6 (212-6) has a NP/MPA ratio of 2.46, which is moderately low in comparison to most of the samples. The one tailings sample (Tailings 4) exhibits a NP/MPA ratio of 5.65, but is of very low potential reactivity in any regard (it has very low sulfide and very low neutralization potential). 3.1 Potential for Acidic Drainage While the NP of each sample exceeds its MPA in the unweathered state, the acid -generating and acid - neutralizing minerals may weather at unequal rates leading to depletion of one before the other. In the subject tests, however, results show that the weathering rate of sulfide (depletion rate) exceeds that of the neutralization potential, such that the potential for generation of acidic drainage, which is extremely low in the samples to begin with, diminishes even further as weathering progresses. Table 1: Summary of Acid -generating and Acid -neutralizing Depletion Rates over 20-Week Test Period (see Analytical Results, Appendix A) Total SulfurL % JMP tal 003 LN Sulfide Depletion Cumula- NP Depletion 1 CO3 NP Depletio SP* 212-6 .. :: 00 :• * NP and MPA in tons CaCO3 per 1000 tons of material, or parts per thousand. Note that in the two waste rock samples the rate of carbonate (CO3) NP depletion is lower than the rate of sulfide (MPA) depletion, but in the tailings sample only the total NP (not the carbonate NP) retains a lower rate of depletion than that of the sulfide. There is very little sulfide or carbonate in the tailings sample, and its NP is substantially from clays or other non -carbonate constituents. In any event, all three samples show the total NP to exceed the MPA before weathering, and the MPA to be depleted at a faster rate than the NP such that any potential for acidic drainage to result from any of these materials is essentially nil. The pH values of weekly leachates remained circum-neutral throughout the test period (6.98 — 8.01 in the waste rock samples, and 6.34 — 7.27 in the tailings sample). MARSHALL MILLER & ASSOCIATES, INC. 2 11�HKULIL"NNLLE SOCI ES° 3.2 Potential for Significant Release of Metals Addendum Report: Results of Humidity Cell Leaching Tests, Piedmont Lithium Project December 2019 During the humidity cell leaching program, no dissolved concentrations of any parameter exceeded (or even approached) an applicable regulatory groundwater standard (USEPA Drinking Water Standard or North Carolina Ground Water Standard), with the marginal and temporary exception of pH in the Tailings 4 leachate in Weeks 14, 15, and 20. The minimum pH value was 6.34, slightly below the 6.5 — 8.5 pH range targeted in those regulatory guidances. As is noted on Tables Z 3, and 4, the peak concentrations of most parameters generally occurred in the initial flush, and if not then, within the first three leaching events. The general trend for the great majority of parameters was a decline in concentration over time, with the lowest concentrations occurring at or near the end of the test period. The parameter phosphorus is the consistent exception to that trend, but its concentrations remain extremely low throughout. Because some regulatory standards for chromium are based upon the toxic and mobile hexavalent form, the valence state and mobility of chromium present in the samples was specifically evaluated. The humidity cell leaching test results confirm the earlier indications of low mobility and support the conclusion that the chromium present in these samples is essentially all in the trivalent form, and is of low toxicity and low leachability. 4 Summary and Conclusions As expected, the results of the humidity cell leaching program support and confirm the indications of earlier testing that neither the waste rock nor the process tailings material at the subject site are likely to generate significant hazardous leachings to groundwater. The potential for acidic drainage from these materials is essentially nil, and the dissolved constituents in the weekly leachate collections are all at levels far below any regulatory concern. As was noted in the August 2019 report on findings based on elemental, ABA, and TCLP analyses, research of public records suggests that no significant environmental issues have been reported to be associated with the previous lithium pegmatite mining in the region; and results of recent testing, including the humidity cell leaching program, are consistent with that indication. MARSHALL MILLER & ASSOCIATES, mc. 3 F"kk \\ •KNi., �� Piedmont Lithium Summary of Acid -generating and Acid -neutralizing Depletion Rates over 20-Week Test Period (see Analytical Results, Appendix A ) Table 1 * NP and MPA in tons CaCO 3 per 1000 tons of material, or parts per thousand. 71��k!IZSHIULMLLE SOCI ES° Piedmont Lithium Summary of Humidity Cell Leaching Results Through Week 20 Waste Rock 205-7 Table 2 Parameter USEPA Drinking Water Standard North Carolina Ground Water Standard Leachate Concentration Range Week of Peak Concentration Final Week Concentration (Units: µg/L) Hg 2 1 ND (<0.01) - 0.01 15 ND (<0.01) Ag 100* 20 ND (<0.05) µg/L throughout As 10 10 ND (<0.2) - 0.2 0 ND (<0.2) B 300 H.A. 700 ND (<2) - 4 1 ND (<2) Ba 2,000 700 0.22 - 0.7 0 0.22 Be 4 ND (<0.007) - 0.008 3 ND (<0.007) Bi ND (<0.007) µg/Lthroughout Cd 5 2 ND (<0.003) - 0.015 5 0.009 Co ND (<0.004) - 0.025 15 ND (<0.004) Cr 100 10 ND (<0.08) µg/L throughout Cu 1,300 A.L. 1,000 ND (<0.2) - 0.5 0 0.15 Mo 0.95 - 12.4 5 9.11 Ni 100 H.A. 100 ND (<0.1) - 0.2 1 0.1 Pb 15 A.L. 15 ND (<0.01) - 0.06 1 0.03 Sb 6 ND (<0.9) µg/Lthroughout Se 50 20 ND (<0.04) - 0.15 0 ND (<0.04) Sn ND (<0.06) - 0.25 0 ND (<0.06) Sr 25,000 H.A. 3.63 - 6.24 0 3.82 Ti ND (<0.05) - 0.24 0 0.20 Th ND (<0.1) - 0.9 1 ND (<0.1) TI 2 ND (<0.005) - 0.023 0 ND (<0.005) U 30 0.031 - 0.272 20 0.272 V 0.3 - 1.99 0 0.40 W ND (<0.02) - 0.19 0 ND (<0.02) y ND (<0.002) - 0.008 0 0.004 Zr ND (<2) µg/L throughout (Units: mg/L) Al 50 - 200* 0.057 - 0.111 0 0.067 Fe 0.3* 0.3 ND (<0.007) - 0.007 0 ND (<0.007) K 0.13 - 1.8 0 0.130 Li 0.0139 - 0.317 0 0.0095 Mg 0.177 - 0.242 15 0.190 Mn 0.05* 0.05 0.00110 - 0.00524 2 0.00340 Na 0.16 - 2.28 0 0.16 P ND (<0.003) - 0.016 20 0.016 Si 0.38 - 0.47 1 0.43 Zn 5* 1.00 ND (<0.002) mg/L throughout SO4 250* 250 ND (<0.2) - 0.5 1 0 ND (<0.2) Acidity ND (<2) mg/L throughout Alkalinity 9 - 22 0 11 (Units: pH in Standard Units, EC in MS/cm) pH 6.5-8.5 6.5-8.5 6.98 - 8.01 0 7.15 EC 20 - 44 1 0 22 * Secondary Standard H.A. Health Advisory A.L. Action Level 71��k!IZSHIULMLLE SOCI ES° Piedmont Lithium Summary of Humidity Cell Leaching Results Through Week 20 Waste Rock 212-6 Table 3 Parameter USEPA Drinking Water Standard North Carolina Ground Water Standard Leachate Concentration Range Week of Peak Concentration Final Week Concentration (Units: µg/L) Hg 2 1 ND (<0.01) µg/L throughout Ag 100* 20 ND (<0.05) µg/L throughout As 10 10 0.3 - 1.1 0 0.3 B 300 H.A. 700 ND (<2) - 4 1 ND (<2) Ba 2,000 700 0.61 - 3.38 0 0.61 Be 4 ND (<0.007) - 0.013 3 ND (<0.007) Bi ND (<0.007) - 0.008 1 ND (<0.007) Cd 5 2 ND (<0.003) - 0.010 3 ND (<0.003) Co 0.013 - 0.048 0 0.030 Cr 100 10 ND (<0.08) - 0.19 20 0.19 Cu 1,300 A.L. 1,000 ND (<0.2) - 2 15 ND (<0.2) Mo 1.61 - 20.5 3 5.36 Ni 100 H.A. 100 ND (<0.1) - 0.6 0 0.1 Pb 15 A.L. 15 ND (<0.01) - 0.13 1 0.01 Sb 6 ND (<0.9) µg/Lthroughout Se 50 20 ND (<0.04) - 0.42 0 ND (<0.04) Sn ND (<0.06) - 0.2 3 ND (<0.06) Sr 25,000 H.A. 8.32 - 15.7 0 9.27 Ti 0.08 - 0.38 1 0.08 Th ND (<0.1) - 0.3 2 ND (<0.1) TI 2 0.011 - 0.069 0 0.011 U 30 0.015 - 3.47 5 0.204 V 0.14 - 0.59 0 0.20 W ND (<0.02) - 0.19 1 ND (<0.02) y ND (<0.002) - 0.014 20 0.014 Zr ND (<2) µg/L throughout (Units: mg/L) Al 50 - 200* 0.059 - 0.094 10 0.061 Fe 0.3* 0.3 ND (<0.007) - 0.008 1 ND (<0.007) K 0.424 - 7.89 0 0.424 Li 0.0171 - 0.589 0 0.0171 Mg 0.422 - 0.784 5 0.422 Mn 0.05* 0.05 0.00227 - 0.00637 3 0.00321 Na 0.08 - 2.13 0 0.09 P ND (<0.003) - 0.012 20 0.012 Si 0.52 - 0.66 5 0.55 Zn 5* 1.00 ND (<0.002) mg/L throughout SO4 250* 250 1.9 - 6.2 1 0 2.4 Acidity ND (<2) mg/L throughout Alkalinity 10 - 24 0 11 (Units: pH in Standard Units, EC in MS/cm) pH 6.5-8.5 6.5-8.5 7.07 7.77 0 7.10 EC 27 82 1 0 31 * Secondary Standard H.A. Health Advisory A.L. Action Level 71��R�SHULWLLE SOCI ES° Piedmont Lithium Summary of Humidity Cell Leaching Results Through Week 20 Tailings 4 Leachate Table 4 Parameter USEPA Drinking Water Standard North Carolina Ground Water Standard Leachate Concentration Range Week of Peak Concentration Final Week Concentration (Units: µg/L) Hg 2 1 ND (<0.01) 0.01 5 ND (<0.01) Ag 100* 20 ND (<0.05) µg/L throughout As 10 10 0.4 - 1.3 1 0.4 B 300 H.A. 700 ND (<2) 9 1 ND (<2) Ba 2,000 700 0.25 - 2.76 3 0.92 Be 4 0.009 - 0.034 20 0.034 Bi ND (<0.007) - 0.017 0 ND (<0.007) Cd 5 2 ND (<0.003) - 0.032 1 0.009 Co ND (<0.004) 0.027 0 ND (<0.004) Cr 100 10 0.13 - 0.66 2 ND (<0.08) Cu 1,300 A.L. 1,000 ND (<0.2) - 3 0 ND (<0.2) Mo 0.24 - 26.5 5 0.31 Ni 100 H.A. 100 ND (<0.1) 0.3 0 ND (<0.1) Pb 15 A.L. 15 0.01 - 0.16 1 0.04 Sb 6 ND (<0.9) 1.1 2 ND (<0.9) Se 50 20 ND (<0.04) - 0.05 0 ND (<0.04) Sn 0.11 - 0.43 0 0.13 Sr 25,000 H.A. 1.59 11.9 2 2.03 Ti ND (<0.05) - 0.19 1 ND (<0.05) Th ND (<0.01) - 0.1 2 ND (<0.01) TI 2 0.012 0.048 1 0.006 U 30 0.083 - 12.2 1 0.046 V 0.16 - 0.47 1 0.16 W ND (<0.02) - 0.25 1 ND (<0.02) y ND (<0.002) - 0.011 5 0.003 Zr ND (<2) µg/L throughout (Units: mg/L) Al 50 - 200* 0.016 0.55 0 0.007 Fe 0.3* 0.3 ND (<0.007) mg/L throughout K 0.077 1.12 1 0.119 Li 0.0093 0.135 2 0.0118 Mg 0.043 0.448 2 0.043 Mn 0.05* 0.05 0.0005 0.0219 20 0.0219 Na 0.07 5.35 1 0.11 P 0.034 0.131 20 0.131 Si 0.47 1.76 2 0.68 Zn 5* 1 ND (<0.002) 0.004 0 0.003 SO4 250* 250 ND (<0.2) 1.4 0 ND (<0.2) Acidity ND (<2) 2 15 ND (<2) Alkalinity 2 21 2 2 (Units: pH in Standard Units, EC in MS/cm) pH 6.5-8.5 6.5-8.5 6.34 7.27 5 6.34 EC 4 - 42 1 1 1 5 * Secondary Standard H.A. Health Advisory A.L. Action Level APPENDIX A ANALYSES OF WEEKLY HUMIDITY CELL LEACHATE Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Test Specimen Sample Weight (g) 18-BD-205-7 1000 Analysis of Weekly Humidity Cell Leachate Parameter Units 0 1 2 3 4 5 6 7 8 9 10 Date 13-Jun-19 20-Jun-19 27-Jun-19 04-Jul-19 11-Jul-19 18-Jul-19 25-Jul-19 01-Aug-19 08-Aug-19 15-Aug-19 22-Aug-19 LIMS 10458-JUN19 10459-JUN19 10620-JUN19 10028-JUL19 10112-JUL19 10149-JUL19 10334-JUL19 10002-AUG19 10031-AUG19 10126-AUG19 10196-AUG19 Hum Cell Leachate Vol mL 812 970 961 993 977 976 992 956 988 960 949 pH no unit 8.01 7.26 7.24 7.21 7.34 7.45 7.24 7.41 7.51 7.56 7.51 Acidity mg/L as CaCO3 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 Alkalinity mg/L as CaCO3 22 12 11 13 11 11 10 10 10 11 9 Conductivity PS/CM 44 28 26 23 21 23 20 23 22 23 22 SOa mg/L 0.5 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 Cr(VI) mg/L < 0.2 --- --- --- --- --- --- --- --- --- --- Hg mg/L < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 --- --- --- --- < 0.00001 Ag mg/L < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 --- --- --- --- < 0.00005 Al mg/L 0.111 0.082 0.057 0.068 0.069 0.066 --- --- --- --- 0.069 As mg/L 0.0002 < 0.0002 < 0.0002 < 0.0002 < 0.0002 < 0.0002 --- --- --- --- < 0.0002 B mg/L 0.003 0.004 0.003 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 Ba mg/L 0.00070 0.00041 0.00048 0.00030 0.00025 0.00026 --- --- --- --- 0.00022 Be mg/L < 0.000007 < 0.000007 < 0.000007 0.000008 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 Bi mg/L < 0.000007 < 0.000007 < 0.000007 < 0.000007 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 Ca mg/L 4.30 2.95 3.12 3.31 3.51 3.46 --- --- --- --- 3.26 Cd mg/L < 0.000003 0.000004 < 0.000003 0.000014 0.000006 0.000015 --- --- --- --- < 0.000003 Co mg/L 0.000018 0.000012 0.000012 0.000015 < 0.000004 < 0.000004 --- --- --- --- < 0.000004 Cr mg/L < 0.00008 < 0.00008 < 0.00008 < 0.00008 < 0.00008 < 0.00008 --- --- --- --- < 0.00008 CU mg/L 0.0005 0.0003 < 0.0002 < 0.0002 0.0002 < 0.0002 --- --- --- --- 0.0002 Fe mg/L 0.007 < 0.007 < 0.007 < 0.007 < 0.007 < 0.007 --- --- --- --- < 0.007 K mg/L 1.80 1.09 0.795 0.609 0.493 0.404 --- --- --- --- 0.304 Li mg/L 0.317 0.173 0.153 0.0573 0.0395 0.0334 --- --- --- --- 0.0209 Mg mg/L 0.177 0.199 0.228 0.232 0.239 0.239 --- --- --- --- 0.220 Mn mg/L 0.00110 0.00437 0.00524 0.00494 0.00412 0.00454 --- --- --- --- 0.00418 Mo mg/L 0.00095 0.0102 0.00793 0.0122 0.0117 0.0124 --- --- --- --- 0.00700 Na mg/L 2.28 1.57 0.81 0.43 0.34 0.32 --- --- --- --- 0.35 Ni mg/L 0.0001 0.0002 < 0.0001 < 0.0001 < 0.0001 < 0.0001 --- --- --- --- < 0.0001 P mg/L 0.003 < 0.003 < 0.003 < 0.003 < 0.003 < 0.003 --- --- --- --- < 0.003 Pb mg/L 0.00004 0.00006 < 0.00001 < 0.00001 < 0.00001 < 0.00001 --- --- --- --- 0.00001 Sb mg/L < 0.0009 < 0.0009 < 0.0009 < 0.0009 < 0.0009 < 0.0009 --- --- --- --- < 0.0009 Se mg/L 0.00015 < 0.00004 < 0.00004 < 0.00004 < 0.00004 < 0.00004 --- --- --- --- < 0.00004 Si mg/L 0.47 0.46 0.42 0.43 0.45 0.44 --- --- --- --- 0.38 Sn mg/L 0.00016 0.00016 0.00025 0.00008 < 0.00006 < 0.00006 --- --- --- --- < 0.00006 Sr mg/L 0.00624 0.00435 0.00439 0.00417 0.00377 0.00455 --- --- --- --- 0.00363 Ti mg/L 0.00024 0.00007 < 0.00005 0.00009 0.00014 0.00022 --- --- --- --- 0.00019 Th mg/L < 0.0001 0.0009 0.0003 < 0.0001 < 0.0001 < 0.0001 --- --- --- --- < 0.0001 TI mg/L 0.000023 0.000013 0.000008 0.000010 0.000007 0.000009 --- --- --- --- 0.000006 U mg/L 0.000031 0.000107 0.000101 0.000172 0.000156 0.000253 --- --- --- --- 0.000155 V mg/L 0.00199 0.00045 0.00030 0.00032 0.00030 0.00031 --- --- --- --- 0.00033 W mg/L 0.00015 0.00019 0.00010 0.00008 0.00006 0.00003 --- --- --- --- < 0.00002 Y mg/L 0.000008 < 0.000002 0.000002 0.000005 0.000002 0.000002 --- --- --- --- < 0.000002 Zn mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 Zr mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Test Specimen Sample Weight (g) 18-BD-205-7 1000 Analysis of Weekly Humidity Cell Leachate Parameter Units 11 12 13 14 15 16 17 18 19 20 Date 29-Aug-19 05-Sep-19 12-Sep-19 19-Sep-19 26-Sep-19 03-Oct-19 10-Oct-19 17-Oct-19 24-Oct-19 31-Oct-19 LIMS 10286-AUG19 10026-SEP19 10052-SEP19 10154-SEP19 10279-SEP19 10026-OCT19 10103-OCT19 10190-OCT19 10329-OCT19 10380-OCT19 Hum Cell Leachate Vol mL 967 932 970 971 934 963 935 994 1015 979 pH no unit 7.67 7.37 7.25 7.46 6.98 7.08 7.44 7.48 7.57 7.15 Acidity mg/L as CaCO3 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 Alkalinity mg/L as CaCO3 10 9 10 13 10 10 9 10 11 11 Conductivity PS/Cm 27 20 20 24 21 24 20 24 23 22 SO4 mg/L < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 0.2 0.2 < 0.2 Cr(VI) mg/L --- --- --- --- --- -- Hg mg/L --- --- --- --- 0.00001 --- --- --- --- < 0.00001 Ag mg/L --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 Al mg/L --- --- --- --- 0.079 --- --- --- --- 0.067 As mg/L --- --- --- --- < 0.0002 --- --- --- --- < 0.0002 B mg/L --- --- --- --- < 0.002 --- --- --- --- < 0.002 Ba mg/L --- --- --- --- 0.00032 --- --- --- --- 0.00022 Be mg/L --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Bi mg/L --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Ca mg/L --- --- --- --- 3.63 --- --- --- --- 3.50 Cd mg/L --- --- --- --- 0.000006 --- --- --- --- 0.000009 Co mg/L --- --- --- --- 0.000025 --- --- --- --- < 0.000004 Cr mg/L --- --- --- --- < 0.00008 --- --- --- --- 0.00015 Cu mg/L --- --- --- --- < 0.0002 --- --- --- --- < 0.0002 Fe mg/L --- --- --- --- < 0.007 --- --- --- --- < 0.007 K mg/L --- --- --- --- 0.163 --- --- --- --- 0.130 Li mg/L --- --- --- --- 0.0139 --- --- --- --- 0.0095 Mg mg/L --- --- --- --- 0.242 --- --- --- --- 0.190 Mn mg/L --- --- --- --- 0.00399 --- --- --- --- 0.00340 MO mg/L --- --- --- --- 0.00795 --- --- --- --- 0.00911 Na mg/L --- --- --- --- 0.19 --- --- --- --- 0.16 Ni mg/L --- --- --- --- < 0.0001 --- --- --- --- 0.0001 P mg/L --- --- --- --- < 0.003 --- --- --- --- 0.016 Pb mg/L --- --- --- --- 0.00002 --- --- --- --- 0.00003 Sib mg/L --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 Se mg/L --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 Si mg/L --- --- --- --- 0.39 --- --- --- --- 0.43 Sn mg/L --- --- --- --- < 0.00006 --- --- --- --- 0.00011 Sr mg/L --- --- --- --- 0.00385 --- --- --- --- 0.00382 Ti mg/L --- --- --- --- 0.00012 --- --- --- --- 0.00020 Th mg/L --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 TI mg/L --- --- --- --- 0.000007 --- --- --- --- < 0.000005 U mg/L --- --- --- --- 0.000205 --- --- --- --- 0.000272 V mg/L --- --- --- --- 0.00041 --- --- --- --- 0.00040 W mg/L --- --- --- --- 0.00005 --- --- --- --- < 0.00002 Y mg/L --- --- --- --- 0.000004 --- --- --- --- 0.000004 Zn mg/L --- --- --- --- < 0.002 --- --- --- --- < 0.002 Zr mg/L --- --- --- --- < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. TEST REPORT Humidity Cell Test (ASTM D 5744-96) Test Specimen Summary of ABA Test Data Sample Weight (g) Parameter Units Ref No.: 14328-JUL19 18-BD-205-7 1000 Sulphur (S) % 0.009 Sulphide (S-) % <0.02 NP t CaCO3/10001 15.1 CO, NP t CaCO3/10001 3.49 Leachate Parameters Measured Acid Generation' Weekly Volume pH Acidity Alkalinity Conductivity SO4 SO4 Cumulative Weekly Cumulative Leach Collected Production SO4 S- S- CaCO3 eq. CaCO3 eq. Rate Production Depletion Depletion No. mL units PS/CM mg mg/L mg/L g/t/wk g/t % % 0 812 8.01 <2 22 44 0.5 0.4 0.4 0.07 0.07 1 970 7.26 <2 12 28 0.2 0.2 0.6 0.03 0.10 2 961 7.24 <2 11 26 <0.2 0.2 0.8 0.03 0.13 3 993 7.21 <2 13 23 <0.2 0.2 1.0 0.03 0.17 4 977 7.34 <2 11 21 <0.2 0.2 1.2 0.03 0.20 5 976 7.45 <2 11 23 <0.2 0.2 1.4 0.03 0.23 6 992 7.24 <2 10 20 <0.2 0.2 1.6 0.03 0.26 7 956 7.41 <2 10 23 <0.2 0.2 1.8 0.03 0.30 8 988 7.51 <2 10 22 <0.2 0.2 2.0 0.03 0.33 9 960 7.56 <2 11 23 <0.2 0.2 2.2 0.03 0.36 10 949 7.51 <2 9 22 <0.2 0.2 2.4 0.03 0.39 11 967 7.67 <2 10 27 <0.2 0.2 2.5 0.03 0.42 12 932 7.37 <2 9 20 <0.2 0.2 2.7 0.03 0.46 13 970 7.25 <2 10 20 <0.2 0.2 2.9 0.03 0.49 14 971 7.46 <2 13 24 <0.2 0.2 3.1 0.03 0.52 15 934 6.98 <2 10 21 <0.2 0.2 3.3 0.03 0.55 16 963 7.08 <2 10 24 <0.2 0.2 3.5 0.03 0.58 17 935 7.44 <2 9 20 <0.2 0.2 3.7 0.03 0.61 18 994 7.48 <2 10 24 0.2 0.2 3.9 0.03 0.65 19 1015 7.57 <2 11 23 0.2 0.2 4.1 0.03 0.68 20 979 7.15 <2 11 22 <0.2 0.2 4.3 0.03 0.71 Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Acid Neutralization' NP Cumulative Cumulative Consumption NP CO3 NP Depletion Depletion CaCO3, g/t/wk % % 0.42 0.00 0.01 0.20 0.00 0.02 0.20 0.01 0.02 0.21 0.01 0.03 0.20 0.01 0.04 0.20 0.01 0.04 0.21 0.01 0.05 0.20 0.01 0.05 0.21 0.01 0.06 0.20 0.01 0.06 0.20 0.02 0.07 0.20 0.02 0.08 0.19 0.02 0.08 0.20 0.02 0.09 0.20 0.02 0.09 0.19 0.02 0.10 0.20 0.02 0.10 0.19 0.03 0.11 0.21 0.03 0.12 0.21 0.03 0.12 0.20 0.03 0.13 * Initial Week 0 leachate may included soluble sulphate, and may not indicate oxidation of sulphide in the sample material has occurred. 'Calculated values Summary - Weeks 0 to 20 _ Maximum Value 8.01 2 22 44 0.5 0.4 0.07 0.4 Minimum Value 6.98 <2 9 20 <0.2 0.2 0.03 0.2 Average Value 7.34 2 11 24 0.2 0.2 0.03 0.21 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. 0 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Conductivity, Sulphate, and pH in Weekly Humidity Cell Leachate 18-BD-205-7 100 a> 90 E 80 OV 70 'i-■-■.a ■-i-■-r;-■-a ■-ir ti ■ ■ ■ ; ■ U c 60 R 50 i 40 30 20 3 10 0 U 0 Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 10 9 8 7 6 M 5 .E 3 4 = a 3 2 1 0 0 5 10 15 20 25 30 35 40 Time (weeks) Conductivity t Sulphate ... I--- pH Cumulative Sulphide and NP Depletion 18-BD-205-7 100 90 c w0 80 d a 70 d 0 y 60 m 50 3 E 40 30 m 20 10 U 0 5 4 3 2 1 0 0 10 20 30 40 0 5 10 15 20 25 30 35 40 Time (weeks) Sulphide Depletion NP Depletion 0 CO3 NP Depletion Note: NP depletion calculated based on sulphate assay. Note 2: Y-axis of inset graph reduced to 5% for ease of viewing. This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Selected Parameters in Weekly Humidity Cell Leachate 18-BD-205-7 50 45 40 rn E 35 c 0 30 m 25 m 20 0 U 15 10 5 ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ 0 0 5 10 15 20 25 30 35 40 Time (weeks) ❑ Ca o Mg o SO4 Carbonate (Ca + M9/SO4) and Anorthoclase (Ca/SO4) Molar Ratio: 18-BD-205-7 100 90 80 70 60 � 50 p 00 0 0 40 00❑❑❑ 0 El 30 20 10 0 _________________ 0 5 10 15 20 25 30 35 40 Time (weeks) ❑ Anorthoclase Molar Ratio (Ca/SO4) 0 Carbonate Molar Ratio (Ca + Mg/SO4) This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. 0 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Selected Parameters in Weekly Humidity Cell Leachate 18-BD-205-7 60 50 a 40 0 ° ❑ ❑ 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 0 5 10 15 20 25 30 35 40 Time (weeks) ❑ Alkalinity o Acidity n 0 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. OPO Test Specimen Sample Weight (g) 18-BD-205-7 1000 Analysis of Weekly Humidity Cell Leachate Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Parameter Units 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 Date 13-Jun-19 20-Jun-19 27-Jun-19 04-Jul-19 11-Jul-19 18-Jul-19 25-Jul-19 01-Aug-19 08-Aug-19 15-Aug-19 22-Aug-19 29-Aug-19 05-Sep-19 12-Sep-19 19-Sep-19 26-Sep-19 03-Oct-19 10-Oct-19 17-Oct-19 24-Oct-19 31-Oct-19 L I MS 10458-JUN 19 10459-JUN 19 10620-JUN 19 10028-JUL 19 10112-JUL 19 10149-JUL 19 10334-JUL 19 10002-AUG 19 10031-AUG 19 10126-AUG 19 10196-AUG 19 10286-AUG 19 10026-SEP 19 10052-SEP 19 10154-SEP 19 10279-SEP 19 10026-OCT19 10103-OCT19 10190-OCT19 10329-OCT19 10380-OCT19 Hum Cell Leachate Vol mL 812 970 961 993 977 976 992 956 988 960 949 967 932 970 971 934 963 935 994 1015 979 pH no unit 8.01 7.26 7.24 7.21 7.34 7.45 7.24 7.41 7.51 7.56 7.51 7.67 7.37 7.25 7.46 6.98 7.08 7.44 7.48 7.57 7.15 Acidity mg/LasCaCO3 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 Alkalinity mg/L as CaCO3 22 12 11 13 11 11 10 10 10 11 9 10 9 10 13 10 10 9 10 11 11 Conductivity PS/cm 44 28 26 23 21 23 20 23 22 23 22 27 20 20 24 21 24 20 24 23 22 SO4 mg/L 0.5 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 0.2 0.2 < 0.2 Cr(VI) mg/L <0.2 --- --- --- --- --- --- --- --- --- --- --- --- --- -- --- --- --- --- --- --- Hg mg/L < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 --- --- --- --- < 0.00001 --- --- --- --- 0.00001 --- --- --- --- < 0.00001 Ag mg/L < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 Al mg/L 0.111 0.082 0.057 0.068 0.069 0.066 --- --- --- --- 0.069 --- --- --- --- 0.079 --- --- --- --- 0.067 As mg/L 0.0002 < 0.0002 < 0.0002 < 0.0002 < 0.0002 < 0.0002 --- --- --- --- < 0.0002 --- --- --- --- < 0.0002 --- --- --- --- < 0.0002 B mg/L 0.003 0.004 0.003 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 Ba mg/L 0.00070 0.00041 0.00048 0.00030 0.00025 0.00026 --- --- --- --- 0.00022 --- --- --- --- 0.00032 --- --- --- --- 0.00022 Be mg/L < 0.000007 < 0.000007 < 0.000007 0.000008 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Bi mg/L < 0.000007 < 0.000007 < 0.000007 < 0.000007 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Ca mg/L 4.30 2.95 3.12 3.31 3.51 3.46 --- --- --- --- 3.26 --- --- --- --- 3.63 --- --- --- --- 3.50 Cd mg/L < 0.000003 0.000004 < 0.000003 0.000014 0.000006 0.000015 --- --- --- --- < 0.000003 --- --- --- --- 0.000006 --- --- --- --- 0.000009 Co mg/L 0.000018 0.000012 0.000012 0.000015 < 0.000004 < 0.000004 --- --- --- --- < 0.000004 --- --- --- --- 0.000025 --- --- --- --- < 0.000004 Cr mg/L < 0.00008 < 0.00008 < 0.00008 < 0.00008 < 0.00008 < 0.00008 --- --- --- --- < 0.00008 --- --- --- --- < 0.00008 --- --- --- --- 0.00015 Cu mg/L 0.0005 0.0003 < 0.0002 < 0.0002 0.0002 < 0.0002 --- --- --- --- 0.0002 --- --- --- --- < 0.0002 --- --- --- --- < 0.0002 Fe mg/L 0.007 < 0.007 < 0.007 < 0.007 < 0.007 < 0.007 --- --- --- --- < 0.007 --- --- --- --- < 0.007 --- --- --- --- < 0.007 K mg/L 1.80 1.09 0.795 0.609 0.493 0.404 --- --- --- --- 0.304 --- --- --- --- 0.163 --- --- --- --- 0.130 Li mg/L 0.317 0.173 0.153 0.0573 0.0395 0.0334 --- --- --- --- 0.0209 --- --- --- --- 0.0139 --- --- --- --- 0.0095 Mg mg/L 0.177 0.199 0.228 0.232 0.239 0.239 --- --- --- --- 0.220 --- --- --- --- 0.242 --- --- --- --- 0.190 Mn mg/L 0.00110 0.00437 0.00524 0.00494 0.00412 0.00454 --- --- --- --- 0.00418 --- --- --- --- 0.00399 --- --- --- --- 0.00340 Mo mg/L 0.00095 0.0102 0.00793 0.0122 0.0117 0.0124 --- --- --- --- 0.00700 --- --- --- --- 0.00795 --- --- --- --- 0.00911 Na mg/L 2.28 1.57 0.81 0.43 0.34 0.32 --- --- --- --- 0.35 --- --- --- --- 0.19 --- --- --- --- 0.16 Ni mg/L 0.0001 0.0002 < 0.0001 < 0.0001 < 0.0001 < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- 0.0001 P mg/L 0.003 < 0.003 < 0.003 < 0.003 < 0.003 < 0.003 --- --- --- --- < 0.003 --- --- --- --- < 0.003 --- --- --- --- 0.016 Pb mg/L 0.00004 0.00006 < 0.00001 < 0.00001 < 0.00001 < 0.00001 --- --- --- --- 0.00001 --- --- --- --- 0.00002 --- --- --- --- 0.00003 Sb mg/L < 0.0009 < 0.0009 < 0.0009 < 0.0009 < 0.0009 < 0.0009 --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 Se mg/L 0.00015 < 0.00004 < 0.00004 < 0.00004 < 0.00004 < 0.00004 --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 Si mg/L 0.47 0.46 0.42 0.43 0.45 0.44 --- --- --- --- 0.38 --- --- --- --- 0.39 --- --- --- --- 0.43 Sn mg/L 0.00016 0.00016 0.00025 0.00008 < 0.00006 < 0.00006 --- --- --- --- < 0.00006 --- --- --- --- < 0.00006 --- --- --- --- 0.00011 Sr mg/L 0.00624 0.00435 0.00439 0.00417 0.00377 0.00455 --- --- --- --- 0.00363 --- --- --- --- 0.00385 --- --- --- --- 0.00382 Ti mg/L 0.00024 0.00007 < 0.00005 0.00009 0.00014 0.00022 --- --- --- --- 0.00019 --- --- --- --- 0.00012 --- --- --- --- 0.00020 Th mg/L < 0.0001 0.0009 0.0003 < 0.0001 < 0.0001 < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 Ti mg/L 0.000023 0.000013 0.000008 0.000010 0.000007 0.000009 --- --- --- --- 0.000006 --- --- --- --- 0.000007 --- --- --- --- < 0.000005 J mg/L 0.000031 0.000107 0.000101 0.000172 0.000156 0.000253 --- --- --- --- 0.000155 --- --- --- --- 0.000205 --- --- --- --- 0.000272 V mg/L 0.00199 0.00045 0.00030 0.00032 0.00030 0.00031 --- --- --- --- 0.00033 --- --- --- --- 0.00041 --- --- --- --- 0.00040 W mg/L 0.00015 0.00019 0.00010 0.00008 0.00006 0.00003 --- --- --- --- < 0.00002 --- --- --- --- 0.00005 --- --- --- --- < 0.00002 Y mg/L 0.000008 < 0.000002 0.000002 0.000005 0.000002 0.000002 --- --- --- --- < 0.000002 --- --- --- --- 0.000004 --- --- --- --- 0.000004 Zn mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 Zr mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. APPENDIX ■ SAMPLE 212-6 Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Test Specimen Sample Weight (g) 18-BD-212-6 1000 Analysis of Weekly Humidity Cell Leachate Parameter Units 0 1 2 3 4 5 6 7 8 9 10 Date 13-Jun-19 20-Jun-19 27-Jun-19 04-Jul-19 11-Jul-19 18-Jul-19 25-Jul-19 01-Aug-19 08-Aug-19 15-Aug-19 22-Aug-19 LIMS 10458-JUN19 10459-JUN19 10620-JUN19 10028-JUL19 10112-JUL19 10149-JUL19 10334-JUL19 10002-AUG19 10031-AUG19 10126-AUG19 10196-AUG19 Hum Cell Leachate Vol mL 788 924 926 957 941 954 959 960 995 984 982 pH no unit 7.77 7.45 7.29 7.40 7.34 7.55 7.43 7.45 7.64 7.69 7.58 Acidity mg/L as CaCO3 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 Alkalinity mg/L as CaCO3 24 20 12 16 14 15 15 13 17 14 13 Conductivity PS/CM 82 46 42 42 38 38 35 36 36 35 34 SO4 mg/L 6.2 3.6 3.5 3.4 2.7 2.5 2.2 2.2 2.2 2.0 1.9 Cr(VI) mg/L < 0.2 --- --- --- --- --- --- --- --- --- --- Hg mg/L < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 --- --- --- --- < 0.00001 Ag mg/L < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 --- --- --- --- < 0.00005 Al mg/L 0.063 0.081 0.059 0.078 0.078 0.078 --- --- --- --- 0.094 As mg/L 0.0011 0.0003 0.0004 0.0003 0.0003 0.0003 --- --- --- --- 0.0003 B mg/L 0.002 0.004 0.003 0.002 0.002 0.003 --- --- --- --- < 0.002 Ba mg/L 0.00338 0.00151 0.00144 0.00131 0.00108 0.00107 --- --- --- --- 0.00070 Be mg/L < 0.000007 < 0.000007 < 0.000007 0.000013 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 Bi mg/L < 0.000007 0.000008 < 0.000007 < 0.000007 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 Ca mg/L 6.08 3.16 3.59 4.25 4.52 4.64 --- --- --- --- 4.56 Cd mg/L < 0.000003 0.000004 0.000003 0.000010 0.000010 0.000010 --- --- --- --- < 0.000003 Co mg/L 0.000048 0.000042 0.000043 0.000043 0.000024 0.000013 --- --- --- --- 0.000028 Cr mg/L 0.00009 < 0.00008 0.00008 < 0.00008 < 0.00008 < 0.00008 --- --- --- --- 0.00008 CU mg/L 0.0004 0.0005 0.0003 0.0003 < 0.0002 0.0002 --- --- --- --- 0.0004 Fe mg/L < 0.007 0.008 < 0.007 < 0.007 < 0.007 < 0.007 --- --- --- --- < 0.007 K mg/L 7.89 5.48 4.20 3.92 3.00 2.45 --- --- --- --- 0.941 Li mg/L 0.589 0.263 0.214 0.0977 0.0653 0.0515 --- --- --- --- 0.0301 Mg mg/L 0.766 0.550 0.632 0.732 0.758 0.784 --- --- --- --- 0.565 Mn mg/L 0.00227 0.00623 0.00578 0.00637 0.00512 0.00455 --- --- --- --- 0.00354 Mo mg/L 0.00161 0.0138 0.0152 0.0205 0.0196 0.0173 --- --- --- --- 0.0100 Na mg/L 2.13 1.10 0.52 0.27 0.20 0.19 --- --- --- --- 0.28 Ni mg/L 0.0006 0.0002 0.0002 < 0.0001 < 0.0001 0.0001 --- --- --- --- < 0.0001 P mg/L 0.005 0.004 < 0.003 < 0.003 < 0.003 < 0.003 --- --- --- --- < 0.003 Pb mg/L 0.00001 0.00013 0.00002 < 0.00001 0.00001 < 0.00001 --- --- --- --- < 0.00001 Sb mg/L < 0.0009 < 0.0009 < 0.0009 < 0.0009 < 0.0009 < 0.0009 --- --- --- --- < 0.0009 Se mg/L 0.00042 0.00005 0.00004 < 0.00004 < 0.00004 < 0.00004 --- --- --- --- < 0.00004 Si mg/L 0.65 0.52 0.52 0.58 0.58 0.66 --- --- --- --- 0.58 Sn mg/L 0.00016 0.00015 0.00009 0.00020 < 0.00006 < 0.00006 --- --- --- --- < 0.00006 Sr mg/L 0.0157 0.00832 0.00915 0.0102 0.00928 0.0108 --- --- --- --- 0.00906 Ti mg/L 0.00023 0.00038 0.00033 0.00027 0.00034 0.00024 --- --- --- --- 0.00009 Th mg/L < 0.0001 < 0.0001 0.0003 < 0.0001 < 0.0001 < 0.0001 --- --- --- --- < 0.0001 TI mg/L 0.000069 0.000046 0.000040 0.000040 0.000031 0.000030 --- --- --- --- 0.000020 U mg/L 0.000027 0.000015 0.000040 0.000077 0.000610 0.00347 --- --- --- --- 0.000074 V mg/L 0.00059 0.00018 0.00014 0.00016 0.00017 0.00016 --- --- --- --- 0.00019 W mg/L 0.00010 0.00019 0.00008 0.00006 0.00004 < 0.00002 --- --- --- --- 0.00003 Y mg/L < 0.000002 0.000006 0.000002 0.000006 0.000003 < 0.000002 --- --- --- --- < 0.000002 Zn mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 Zr mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Test Specimen Sample Weight (g) 18-BD-212-6 1000 Analysis of Weekly Humidity Cell Leachate Parameter Units 11 12 13 14 15 16 17 18 19 20 Date 29-Aug-19 05-Sep-19 12-Sep-19 19-Sep-19 26-Sep-19 03-Oct-19 10-Oct-19 17-Oct-19 24-Oct-19 31-Oct-19 LIMS 10286-AUG19 10026-SEP19 10052-SEP19 10154-SEP19 10279-SEP19 10026-OCT19 10103-OCT19 10190-OCT19 10329-OCT19 10380-OCT19 Hum Cell Leachate Vol mL 978 967 991 986 977 987 988 951 906 950 pH no unit 7.56 7.53 7.27 7.62 7.07 7.16 7.54 7.48 7.51 7.10 Acidity mg/L as CaCO3 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 Alkalinity mg/L as CaCO3 13 17 12 14 14 13 13 12 10 11 Conductivity PS/Cm 34 33 30 34 31 33 31 32 27 31 SO4 mg/L 2.0 1.9 1.9 1.9 2.0 1.9 2.0 2.1 2.1 2.4 Cr(VI) mg/L --- --- --- --- --- --- --- --- -- Hg mg/L --- --- --- --- < 0.00001 --- --- --- --- < 0.00001 Ag mg/L --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 Al mg/L --- --- --- --- 0.087 --- --- --- --- 0.061 As mg/L --- --- --- --- 0.0004 --- --- --- --- 0.0003 B mg/L --- --- --- --- < 0.002 --- --- --- --- < 0.002 Ba mg/L --- --- --- --- 0.00071 --- --- --- --- 0.00061 Be mg/L --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Bi mg/L --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Ca mg/L --- --- --- --- 4.77 --- --- --- --- 4.50 Cd mg/L --- --- --- --- 0.000009 --- --- --- --- < 0.000003 Co mg/L --- --- --- --- 0.000035 --- --- --- --- 0.000030 Cr mg/L --- --- --- --- 0.00013 --- --- --- --- 0.00019 Cu mg/L --- --- --- --- 0.0020 --- --- --- --- < 0.0002 Fe mg/L --- --- --- --- < 0.007 --- --- --- --- < 0.007 K mg/L --- --- --- --- 0.511 --- --- --- --- 0.424 Li mg/L --- --- --- --- 0.0176 --- --- --- --- 0.0171 Mg mg/L --- --- --- --- 0.479 --- --- --- --- 0.422 Mn mg/L --- --- --- --- 0.00312 --- --- --- --- 0.00321 MO mg/L --- --- --- --- 0.00725 --- --- --- --- 0.00536 Na mg/L --- --- --- --- 0.08 --- --- --- --- 0.09 Ni mg/L --- --- --- --- < 0.0001 --- --- --- --- 0.0001 P mg/L --- --- --- --- < 0.003 --- --- --- --- 0.012 Pb mg/L --- --- --- --- 0.00002 --- --- --- --- 0.00001 Sib mg/L --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 Se mg/L --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 Si mg/L --- --- --- --- 0.57 --- --- --- --- 0.55 Sn mg/L --- --- --- --- 0.00009 --- --- --- --- < 0.00006 Sr mg/L --- --- --- --- 0.00893 --- --- --- --- 0.00927 Ti mg/L --- --- --- --- 0.00014 --- --- --- --- 0.00008 Th mg/L --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 TI mg/L --- --- --- --- 0.000014 --- --- --- --- 0.000011 U mg/L --- --- --- --- 0.000137 --- --- --- --- 0.000204 V mg/L --- --- --- --- 0.00023 --- --- --- --- 0.00020 W mg/L --- --- --- --- 0.00005 --- --- --- --- < 0.00002 Y mg/L --- --- --- --- 0.000003 --- --- --- --- 0.000014 Zn mg/L --- --- --- --- < 0.002 --- --- --- --- < 0.002 Zr mg/L --- --- --- --- < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Test Specimen Summary of ABA Test Data Sample Weight (g) Parameter Units Ref No.: 14328-JUL19 18-BD-212-6 1000 Sulphur (S) % 0.166 Sulphide (S-) % 0.06 NP t CaCO3/10001 23.0 CO, NP t CaCO3/10001 2.74 Leachate Parameters Measured Acid Generation' Acid Neutralization' - Weekly Volume pH Acidity Alkalinity Conductivity SO4 SO4 Cumulative Weekly Cumulative NP Cumulative Cumulative Leach Collected Production SO4 S- S- Consumption NP CO, NP CaCO3 eq. CaCO3 eq. Rate Production Depletion Depletion Depletion Depletion No. mL units PS/CM mg/L m /L g m /L g g /t/wk g /t % ° /° CaCO3, g/t/wk ° /° ° /° 0 788 7.77 <2 24 82 6.2 4.9 4.9 0.27 0.27 5.09 0.02 0.19 1 924 7.45 <2 20 46 3.6 3.3 8.2 0.18 0.46 3.47 0.04 0.31 2 926 7.29 <2 12 42 3.5 3.2 11.5 0.18 0.64 3.38 0.05 0.44 3 957 7.40 <2 16 42 3.4 3.3 14.7 0.18 0.82 3.39 0.07 0.56 4 941 7.34 <2 14 38 2.7 2.5 17.2 0.14 0.96 2.65 0.08 0.66 5 954 7.55 <2 15 38 2.5 2.4 19.6 0.13 1.09 2.48 0.09 0.75 6 959 7.43 <2 15 35 2.2 2.1 21.7 0.12 1.21 2.20 0.10 0.83 7 960 7.45 <2 13 36 2.2 2.1 23.9 0.12 1.33 2.20 0.11 0.91 8 995 7.64 <2 17 36 2.2 2.2 26.0 0.12 1.45 2.28 0.12 0.99 9 984 7.69 <2 14 35 2.0 2.0 28.0 0.11 1.56 2.05 0.13 1.07 10 982 7.58 <2 13 34 1.9 1.9 29.9 0.10 1.66 1.94 0.14 1.14 11 978 7.56 <2 13 34 2.0 2.0 31.8 0.11 1.77 2.04 0.14 1.21 12 967 7.53 <2 17 33 1.9 1.8 33.7 0.10 1.87 1.91 0.15 1.28 13 991 7.27 <2 12 30 1.9 1.9 35.6 0.10 1.98 1.96 0.16 1.35 14 986 7.62 <2 14 34 1.9 1.9 37.4 0.10 2.08 1.95 0.17 1.42 15 977 7.07 <2 14 31 2.0 2.0 39.4 0.11 2.19 2.04 0.18 1.50 16 987 7.16 <2 13 33 1.9 1.9 41.3 0.10 2.29 1.95 0.19 1.57 17 988 7.54 <2 13 31 2.0 2.0 43.2 0.11 2.40 2.06 0.20 1.64 18 951 7.48 <2 12 32 2.1 2.0 45.2 0.11 2.51 2.08 0.20 1.72 19 906 7.51 <2 10 27 2.1 1.9 47.1 0.11 2.62 1.98 0.21 1.79 20 950 7.10 <2 11 31 2.4 2.3 49.4 0.13 2.75 2.38 0.22 1.88 * Initial Week 0 leachate may included soluble sulphate, and may not indicate oxidation of sulphide in the sample material has occurred. 'Calculated values Summary - Weeks 0 to 20 _ Maximum Value 7.77 2 24 82 6.2 4.9 0.27 5.1 Minimum Value 7.07 <2 10 27 1.9 1.8 0.10 1.9 Average Value 7.41 2 14 37 2.6 2.4 0.13 2.50 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. 0 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Conductivity, Sulphate, and pH in Weekly Humidity Cell Leachate 18-BD-212-6 100 a> 90 E 80 O 70 ■ • ■' ■-r t U c 60 R 50 i 40 30 20 3 10 0 U 0 Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 10 9 8 7 6 M 5 .E 3 4 = a 3 2 1 0 0 5 10 15 20 25 30 35 40 Time (weeks) Conductivity t Sulphate ...■--- pH Cumulative Sulphide and NP Depletion 18-BD-212-6 100 90 c w0 80 d a 70 d 0 y 60 m 50 3 E 40 30 m 20 10 U 0 5 4 3 2 1 0 0 10 20 30 40 0 5 10 15 20 25 30 35 40 Time (weeks) Sulphide Depletion NP Depletion 0 CO3 NP Depletion Note: NP depletion calculated based on sulphate assay. Note 2: Y-axis of inset graph reduced to 5% for ease of viewing. This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. 0 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Selected Parameters in Weekly Humidity Cell Leachate 18-BD-212-6 50 45 40 rn E 35 c 0 30 m 25 m 20 0 U 15 10 5 0 Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 0 5 10 15 20 25 30 35 40 Time (weeks) o Ca o Mg v SO4 Carbonate (Ca + M9/SO4) and Anorthoclase (Ca/SO4) Molar Ratio: 18-BD-212-6 100 90 80 70 60 50 40 30 20 10 0 0 0 =Q Q_Q 0=Q________________________________________________________________ 0 5 10 15 20 25 30 35 40 Time (weeks) ❑ Anorthoclase Molar Ratio (Ca/SO4) 0 Carbonate Molar Ratio (Ca + Mg/SO4) This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. 0 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Selected Parameters in Weekly Humidity Cell Leachate 18-BD-212-6 60 50 a 40 0 ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 0 5 10 15 20 25 30 35 40 Time (weeks) ❑ Alkalinity o Acidity n 0 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. OPO Test Specimen Sample Weight (g) 18-B D-212-6 1000 Analysis of Weekly Humidity Cell Leachate Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Parameter Units 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 Date 13-Jun-19 20-Jun-19 27-Jun-19 04-Jul-19 11-Jul-19 18-Jul-19 25-Jul-19 01-Aug-19 08-Aug-19 15-Aug-19 22-Aug-19 29-Aug-19 05-Sep-19 12-Sep-19 19-Sep-19 26-Sep-19 03-Oct-19 10-Oct-19 17-Oct-19 24-Oct-19 31-Oct-19 L I MS 10458-JUN 19 10459-JUN 19 10620-JUN 19 10028-JUL 19 10112-JUL 19 10149-JUL 19 10334-JUL 19 10002-AUG 19 10031-AUG 19 10126-AUG 19 10196-AUG 19 10286-AUG 19 10026-SEP 19 10052-SEP 19 10154-SEP 19 10279-SEP 19 10026-OCT19 10103-OCT19 10190-OCT19 10329-OCT19 10380-OCT19 Hum Cell Leachate Vol mL 788 924 926 957 941 954 959 960 995 984 982 978 967 991 986 977 987 988 951 906 950 pH no unit 7.77 7.45 7.29 7.40 7.34 7.55 7.43 7.45 7.64 7.69 7.58 7.56 7.53 7.27 7.62 7.07 7.16 7.54 7.48 7.51 7.10 Acidity mg/LasCaCO3 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 Alkalinity mg/L as CaCO3 24 20 12 16 14 15 15 13 17 14 13 13 17 12 14 14 13 13 12 10 11 Conductivity PS/cm 82 46 42 42 38 38 35 36 36 35 34 34 33 30 34 31 33 31 32 27 31 SO4 mg/L 6.2 3.6 3.5 3.4 2.7 2.5 2.2 2.2 2.2 2.0 1.9 2.0 1.9 1.9 1.9 2.0 1.9 2.0 2.1 2.1 2.4 Cr(VI) mg/L <0.2 --- --- --- --- --- --- --- --- --- --- --- --- --- -- --- --- --- --- --- --- Hg mg/L < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 --- --- --- --- < 0.00001 --- --- --- --- < 0.00001 --- --- --- --- < 0.00001 Ag mg/L < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 Al mg/L 0.063 0.081 0.059 0.078 0.078 0.078 --- --- --- --- 0.094 --- --- --- --- 0.087 --- --- --- --- 0.061 As mg/L 0.0011 0.0003 0.0004 0.0003 0.0003 0.0003 --- --- --- --- 0.0003 --- --- --- --- 0.0004 --- --- --- --- 0.0003 B mg/L 0.002 0.004 0.003 0.002 0.002 0.003 --- --- --- --- < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 Ba mg/L 0.00338 0.00151 0.00144 0.00131 0.00108 0.00107 --- --- --- --- 0.00070 --- --- --- --- 0.00071 --- --- --- --- 0.00061 Be mg/L < 0.000007 < 0.000007 < 0.000007 0.000013 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Bi mg/L < 0.000007 0.000008 < 0.000007 < 0.000007 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Ca mg/L 6.08 3.16 3.59 4.25 4.52 4.64 --- --- --- --- 4.56 --- --- --- --- 4.77 --- --- --- --- 4.50 Cd mg/L < 0.000003 0.000004 0.000003 0.000010 0.000010 0.000010 --- --- --- --- < 0.000003 --- --- --- --- 0.000009 --- --- --- --- < 0.000003 Co mg/L 0.000048 0.000042 0.000043 0.000043 0.000024 0.000013 --- --- --- --- 0.000028 --- --- --- --- 0.000035 --- --- --- --- 0.000030 Cr mg/L 0.00009 < 0.00008 0.00008 < 0.00008 < 0.00008 < 0.00008 --- --- --- --- 0.00008 --- --- --- --- 0.00013 --- --- --- --- 0.00019 Cu mg/L 0.0004 0.0005 0.0003 0.0003 < 0.0002 0.0002 --- --- --- --- 0.0004 --- --- --- --- 0.0020 --- --- --- --- < 0.0002 Fe mg/L < 0.007 0.008 < 0.007 < 0.007 < 0.007 < 0.007 --- --- --- --- < 0.007 --- --- --- --- < 0.007 --- --- --- --- < 0.007 K mg/L 7.89 5.48 4.20 3.92 3.00 2.45 --- --- --- --- 0.941 --- --- --- --- 0.511 --- --- --- --- 0.424 Li mg/L 0.589 0.263 0.214 0.0977 0.0653 0.0515 --- --- --- --- 0.0301 --- --- --- --- 0.0176 --- --- --- --- 0.0171 Mg mg/L 0.766 0.550 0.632 0.732 0.758 0.784 --- --- --- --- 0.565 --- --- --- --- 0.479 --- --- --- --- 0.422 Mn mg/L 0.00227 0.00623 0.00578 0.00637 0.00512 0.00455 --- --- --- --- 0.00354 --- --- --- --- 0.00312 --- --- --- --- 0.00321 Mo mg/L 0.00161 0.0138 0.0152 0.0205 0.0196 0.0173 --- --- --- --- 0.0100 --- --- --- --- 0.00725 --- --- --- --- 0.00536 Na mg/L 2.13 1.10 0.52 0.27 0.20 0.19 --- --- --- --- 0.28 --- --- --- --- 0.08 --- --- --- --- 0.09 Ni mg/L 0.0006 0.0002 0.0002 < 0.0001 < 0.0001 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- 0.0001 P mg/L 0.005 0.004 < 0.003 < 0.003 < 0.003 < 0.003 --- --- --- --- < 0.003 --- --- --- --- < 0.003 --- --- --- --- 0.012 Pb mg/L 0.00001 0.00013 0.00002 < 0.00001 0.00001 < 0.00001 --- --- --- --- < 0.00001 --- --- --- --- 0.00002 --- --- --- --- 0.00001 Sb mg/L < 0.0009 < 0.0009 < 0.0009 < 0.0009 < 0.0009 < 0.0009 --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 Se mg/L 0.00042 0.00005 0.00004 < 0.00004 < 0.00004 < 0.00004 --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 Si mg/L 0.65 0.52 0.52 0.58 0.58 0.66 --- --- --- --- 0.58 --- --- --- --- 0.57 --- --- --- --- 0.55 Sn mg/L 0.00016 0.00015 0.00009 0.00020 < 0.00006 < 0.00006 --- --- --- --- < 0.00006 --- --- --- --- 0.00009 --- --- --- --- < 0.00006 Sr mg/L 0.0157 0.00832 0.00915 0.0102 0.00928 0.0108 --- --- --- --- 0.00906 --- --- --- --- 0.00893 --- --- --- --- 0.00927 Ti mg/L 0.00023 0.00038 0.00033 0.00027 0.00034 0.00024 --- --- --- --- 0.00009 --- --- --- --- 0.00014 --- --- --- --- 0.00008 Th mg/L < 0.0001 < 0.0001 0.0003 < 0.0001 < 0.0001 < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 Ti mg/L 0.000069 0.000046 0.000040 0.000040 0.000031 0.000030 --- --- --- --- 0.000020 --- --- --- --- 0.000014 --- --- --- --- 0.000011 J mg/L 0.000027 0.000015 0.000040 0.000077 0.000610 0.00347 --- --- --- --- 0.000074 --- --- --- --- 0.000137 --- --- --- --- 0.000204 V mg/L 0.00059 0.00018 0.00014 0.00016 0.00017 0.00016 --- --- --- --- 0.00019 --- --- --- --- 0.00023 --- --- --- --- 0.00020 W mg/L 0.00010 0.00019 0.00008 0.00006 0.00004 < 0.00002 --- --- --- --- 0.00003 --- --- --- --- 0.00005 --- --- --- --- < 0.00002 Y mg/L < 0.000002 0.000006 0.000002 0.000006 0.000003 < 0.000002 --- --- --- --- < 0.000002 --- --- --- --- 0.000003 --- --- --- --- 0.000014 Zn mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 Zr mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Test Specimen Sample Weight (g) Tailings 4 1000 Analysis of Weekly Humidity Cell Leachate Parameter Units 0 1 2 3 4 5 6 7 8 9 10 Date 13-Jun-19 20-Jun-19 27-Jun-19 04-Jul-19 11-Jul-19 18-Jul-19 25-Jul-19 01-Aug-19 08-Aug-19 15-Aug-19 22-Aug-19 LIMS 10458-JUN19 10459-JUN19 10620-JUN19 10028-JUL19 10112-JUL19 10149-JUL19 10334-JUL19 10002-AUG19 10031-AUG19 10126-AUG19 10196-AUG19 Hum Cell Leachate Vol mL 612 932 918 936 929 948 934 950 1033 936 913 pH no unit 6.89 7.24 7.22 7.21 7.25 7.27 7.02 7.07 7.13 7.10 6.99 Acidity mg/L as CaCO3 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 Alkalinity mg/L as CaCO3 8 20 21 14 11 7 7 7 5 5 5 Conductivity PS/CM 28 42 40 27 20 17 13 13 12 10 8 SOa mg/L 1.4 0.8 0.4 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 Cr(VI) mg/L < 0.2 --- --- --- --- --- --- --- --- --- --- Hg mg/L < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 0.00001 --- --- --- --- < 0.00001 Ag mg/L < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 --- --- --- --- < 0.00005 Al mg/L 0.055 0.016 0.017 0.023 0.022 0.021 --- --- --- --- 0.019 As mg/L 0.0010 0.0013 0.0011 0.0008 0.0006 0.0005 --- --- --- --- 0.0004 B mg/L 0.005 0.009 0.007 < 0.002 < 0.002 0.002 --- --- --- --- < 0.002 Ba mg/L 0.00025 0.00112 0.00257 0.00276 0.00261 0.00271 --- --- --- --- 0.00172 Be mg/L 0.000027 0.000011 0.000011 0.000019 0.000011 0.000009 --- --- --- --- 0.000027 Bi mg/L 0.000017 0.000009 0.000008 < 0.000007 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 Ca mg/L 0.44 2.59 3.61 3.67 3.06 2.55 --- --- --- --- 1.09 Cd mg/L < 0.000003 0.000032 0.000006 < 0.000003 0.000005 0.000014 --- --- --- --- 0.000004 Co mg/L 0.000027 0.000024 0.000019 0.000018 < 0.000004 < 0.000004 --- --- --- --- < 0.000004 Cr mg/L 0.00015 0.00046 0.00066 0.00042 0.00029 0.00027 --- --- --- --- 0.00013 CU mg/L 0.0030 0.0020 0.0010 0.0006 0.0004 0.0007 --- --- --- --- < 0.0002 Fe mg/L < 0.007 < 0.007 < 0.007 < 0.007 < 0.007 < 0.007 --- --- --- --- < 0.007 K mg/L 0.459 1.12 0.948 0.614 0.402 0.321 --- --- --- --- 0.216 Li mg/L 0.0800 0.114 0.135 0.0499 0.0315 0.0253 --- --- --- --- 0.0144 Mg mg/L 0.050 0.357 0.448 0.385 0.302 0.242 --- --- --- --- 0.094 Mn mg/L 0.00277 0.00108 0.00060 0.00064 0.00053 0.00074 --- --- --- --- 0.00410 Mo mg/L 0.00133 0.00230 0.00156 0.00130 0.00082 0.0265 --- --- --- --- 0.00056 Na mg/L 4.54 5.35 2.97 0.96 0.43 0.28 --- --- --- --- 0.28 Ni mg/L 0.0003 0.0002 0.0001 < 0.0001 < 0.0001 0.0001 --- --- --- --- < 0.0001 P mg/L 0.065 0.066 0.064 0.044 0.034 0.045 --- --- --- --- 0.069 Pb mg/L 0.00010 0.00016 0.00006 0.00002 0.00003 0.00003 --- --- --- --- 0.00001 Sb mg/L < 0.0009 < 0.0009 0.0011 < 0.0009 < 0.0009 < 0.0009 --- --- --- --- < 0.0009 Se mg/L 0.00005 < 0.00004 < 0.00004 < 0.00004 < 0.00004 < 0.00004 --- --- --- --- < 0.00004 Si mg/L 0.47 1.39 1.76 1.55 1.45 1.29 --- --- --- --- 1.18 Sn mg/L 0.00043 0.00035 0.00039 0.00029 0.00023 0.00019 --- --- --- --- 0.00011 Sr mg/L 0.00159 0.00960 0.0119 0.00982 0.00671 0.00661 --- --- --- --- 0.00275 Ti mg/L 0.00010 0.00019 < 0.00005 < 0.00005 < 0.00005 0.00008 --- --- --- --- < 0.00005 Th mg/L < 0.0001 < 0.0001 0.0001 < 0.0001 < 0.0001 < 0.0001 --- --- --- --- < 0.0001 TI mg/L 0.000012 0.000044 0.000048 0.000034 0.000018 0.000020 --- --- --- --- 0.000017 U mg/L 0.00545 0.0122 0.00715 0.00241 0.000933 0.00534 --- --- --- --- 0.000083 V mg/L 0.00035 0.00047 0.00045 0.00038 0.00028 0.00043 --- --- --- --- 0.00021 W mg/L 0.00003 0.00025 0.00011 0.00003 < 0.00002 < 0.00002 --- --- --- --- < 0.00002 Y mg/L 0.000006 0.000008 0.000003 0.000003 0.000005 0.000011 --- --- --- --- < 0.000002 Zn mg/L 0.004 0.003 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- 0.004 Zr mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Test Specimen Sample Weight (g) Tailings 4 1000 Analysis of Weekly Humidity Cell Leachate Parameter Units 11 12 13 14 15 16 17 18 19 20 Date 29-Aug-19 05-Sep-19 12-Sep-19 19-Sep-19 26-Sep-19 03-Oct-19 10-Oct-19 17-Oct-19 24-Oct-19 31-Oct-19 LIMS 10286-AUG19 10026-SEP19 10052-SEP19 10154-SEP19 10279-SEP19 10026-OCT19 10103-OCT19 10190-OCT19 10329-OCT19 10380-OCT19 Hum Cell Leachate Vol mL 1018 896 899 997 832 978 912 957 809 922 pH no unit 6.93 6.88 6.67 6.49 6.43 6.59 6.73 6.58 6.68 6.34 Acidity mg/L as CaCO3 2 < 2 < 2 < 2 2 < 2 < 2 < 2 < 2 < 2 Alkalinity mg/L as CaCO3 3 2 3 4 3 3 2 2 2 2 Conductivity PS/Cm 7 6 4 6 4 7 5 5 5 5 SO4 mg/L < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 Cr(VI) mg/L --- --- --- --- --- -- --- -- Hg mg/L --- --- --- --- 0.00001 --- --- --- --- < 0.00001 Ag mg/L --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 Al mg/L --- --- --- --- 0.022 --- --- --- --- 0.007 As mg/L --- --- --- --- 0.0004 --- --- --- --- 0.0004 B mg/L --- --- --- --- < 0.002 --- --- --- --- < 0.002 Ba mg/L --- --- --- --- 0.00141 --- --- --- --- 0.00092 Be mg/L --- --- --- --- 0.000017 --- --- --- --- 0.000034 Bi mg/L --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Ca mg/L --- --- --- --- 0.64 --- --- --- --- 0.54 Cd mg/L --- --- --- --- 0.000009 --- --- --- --- 0.000009 Co mg/L --- --- --- --- 0.000018 --- --- --- --- < 0.000004 Cr mg/L --- --- --- --- 0.00013 --- --- --- --- < 0.00008 Cu mg/L --- --- --- --- 0.0004 --- --- --- --- < 0.0002 Fe mg/L --- --- --- --- < 0.007 --- --- --- --- < 0.007 K mg/L --- --- --- --- 0.077 --- --- --- --- 0.119 Li mg/L --- --- --- --- 0.0093 --- --- --- --- 0.0118 Mg mg/L --- --- --- --- 0.054 --- --- --- --- 0.043 Mn mg/L --- --- --- --- 0.00897 --- --- --- --- 0.0219 MO mg/L --- --- --- --- 0.00024 --- --- --- --- 0.00031 Na mg/L --- --- --- --- 0.07 --- --- --- --- 0.11 Ni mg/L --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 P mg/L --- --- --- --- 0.090 --- --- --- --- 0.131 Pb mg/L --- --- --- --- 0.00003 --- --- --- --- 0.00004 Sib mg/L --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 Se mg/L --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 Si mg/L --- --- --- --- 0.75 --- --- --- --- 0.68 Sn mg/L --- --- --- --- 0.00013 --- --- --- --- 0.00013 Sr mg/L --- --- --- --- 0.00186 --- --- --- --- 0.00203 Ti mg/L --- --- --- --- 0.00017 --- --- --- --- < 0.00005 Th mg/L --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 TI mg/L --- --- --- --- 0.000014 --- --- --- --- 0.000006 U mg/L --- --- --- --- 0.000109 --- --- --- --- 0.000046 V mg/L --- --- --- --- 0.00019 --- --- --- --- 0.00016 W mg/L --- --- --- --- 0.00003 --- --- --- --- < 0.00002 Y mg/L --- --- --- --- 0.000002 --- --- --- --- 0.000003 Zn mg/L --- --- --- --- 0.002 --- --- --- --- 0.003 Zr mg/L --- --- --- --- < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Test Specimen Summary of ABA Test Data Sample Weight (g) Parameter Units Ref No.: 14328-JUL19 Tailings 4 1000 Sulphur (S) % <0.005 Sulphide (S-) % <0.02 NP t CaCO3/10001 3.3 CO, NP t CaCO3/10001 <0.42 Leachate Parameters Measured Acid Generation' Acid Neutralization' Weekly Volume pH Acidity Alkalinity Conductivity SO4 SO4 Cumulative Weekly Cumulative NP Cumulative Cumulative Leach Collected Production SO4 S- S- Consumption NP CO, NP CaCO3 eq. CaCO3 eq. Rate Production Depletion Depletion Depletion Depletion No. mL units PS/CM mg/L m /L g m /L g g /t/wk g /t % ° /° CaCO3, g/t/wk ° /° ° /° 0 612 6.89 <2 8 28 1.4 0.9 0.9 0.14 0.14 0.89 0.03 0.22 1 932 7.24 <2 20 42 0.8 0.7 1.6 0.12 0.27 0.78 0.05 0.40 2 918 7.22 <2 21 40 0.4 0.4 2.0 0.06 0.33 0.38 0.06 0.49 3 936 7.21 <2 14 27 <0.2 0.2 2.2 0.03 0.36 0.20 0.07 0.54 4 929 7.25 <2 11 20 <0.2 0.2 2.3 0.03 0.39 0.19 0.07 0.59 5 948 7.27 <2 7 17 <0.2 0.2 2.5 0.03 0.42 0.20 0.08 0.64 6 934 7.02 <2 7 13 <0.2 0.2 2.7 0.03 0.45 0.19 0.09 0.68 7 950 7.07 <2 7 13 <0.2 0.2 2.9 0.03 0.48 0.20 0.09 0.73 8 1033 7.13 <2 5 12 <0.2 0.2 3.1 0.03 0.52 0.22 0.10 0.78 9 936 7.10 <2 5 10 <0.2 0.2 3.3 0.03 0.55 0.20 0.10 0.83 10 913 6.99 <2 5 8 <0.2 0.2 3.5 0.03 0.58 0.19 0.11 0.87 11 1018 6.93 2 3 7 <0.2 0.2 3.7 0.03 0.61 0.21 0.12 0.93 12 896 6.88 <2 2 6 <0.2 0.2 3.9 0.03 0.64 0.19 0.12 0.97 13 899 6.67 <2 3 4 <0.2 0.2 4.0 0.03 0.67 0.19 0.13 1.02 14 997 6.49 <2 4 6 <0.2 0.2 4.2 0.03 0.71 0.21 0.13 1.07 15 832 6.43 2 3 4 <0.2 0.2 4.4 0.03 0.74 0.17 0.14 1.11 16 978 6.59 <2 3 7 <0.2 0.2 4.6 0.03 0.77 0.20 0.15 1.16 17 912 6.73 <2 2 5 <0.2 0.2 4.8 0.03 0.80 0.19 0.15 1.20 18 957 6.58 <2 2 5 <0.2 0.2 5.0 0.03 0.83 0.20 0.16 1.25 19 809 6.68 <2 2 5 <0.2 0.2 5.1 0.03 0.86 0.17 0.16 1.29 20 922 6.34 <2 2 5 <0.2 0.2 5.3 0.03 0.89 0.19 0.17 1.34 * Initial Week 0 leachate may included soluble sulphate, and may not indicate oxidation of sulphide in the sample material has occurred. 'Calculated values Summary - Weeks 0 to 20 Maximum Value 7.27 2 21 42 1.4 0.9 0.14 0.9 Minimum Value 6.34 <2 2 4 <0.2 0.2 0.03 0.2 Average Value 6.79 2 6 14 0.3 0.3 0.04 0.28 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. 0 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Conductivity, Sulphate, and pH in Weekly Humidity Cell Leachate Tailings 4 100 a> 90 E 80 v Q 70 i_E_■ s ■ ti-■-ay ■ c 60 R 50 i 40 30 '5 20 3 10 0 U 0 Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 10 9 8 7 6 M 5 .E 3 4 = a 3 2 1 0 0 5 10 15 20 25 30 35 40 Time (weeks) Conductivity t Sulphate ...■--- pH Cumulative Sulphide and NP Depletion Tailings 4 100 90 c w0 80 d a 70 d 60 m 50 3 E 40 30 m 20 10 U 0 5 4 3 2 1 0 0 10 20 30 40 0 5 10 15 20 25 30 35 40 Time (weeks) Sulphide Depletion NP Depletion 0 CO3 NP Depletion Note: NP depletion calculated based on sulphate assay. Note 2: Y-axis of inset graph reduced to 5% for ease of viewing. This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Selected Parameters in Weekly Humidity Cell Leachate Tailings 4 50 45 40 rn E 35 c 0 30 m 25 m 20 0 U 15 10 5 ❑ ❑ ❑ ❑ ❑ 0 0 5 10 15 20 25 30 35 40 Time (weeks) ❑ Ca o Mg o SO4 Carbonate (Ca + M9/SO4) and Anorthoclase (Ca/SO4) Molar Ratio: Tailings 4 100 90 80 70 60 50 0 40 D0 ❑ 0 30 ❑ 0 20 10 8 0 0 0 0 5 10 15 20 25 30 35 40 Time (weeks) ❑ Anorthoclase Molar Ratio (Ca/SO4) 0 Carbonate Molar Ratio (Ca + Mg/SO4) This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. 0 TEST REPORT Humidity Cell Test (ASTM D 5744-96) Selected Parameters in Weekly Humidity Cell Leachate Tailings 4 60 50 40 a� E r- 30 0 y 20 ❑ ❑ c o ❑ U 10 0 0 ❑ ❑ ❑ ❑ ❑ ❑ 0 0 0 0 0 0 0 0 0 0 8 0 8 0 9 8 0❑❑ o Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 0 5 10 15 20 25 30 35 40 Time (weeks) ❑ Alkalinity 0 Acidity n 0 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method. OPO Test Specimen Sample Weight (g) Tailings 4 1000 Analysis of Weekly Humidity Cell Leachate Environmental Testing Piedmont Lithium SGS Reference No.: 17234-01 Parameter Units 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 Date 13-Jun-19 20-Jun-19 27-Jun-19 04-Jul-19 11-Jul-19 18-Jul-19 25-Jul-19 01-Aug-19 08-Aug-19 15-Aug-19 22-Aug-19 29-Aug-19 05-Sep-19 12-Sep-19 19-Sep-19 26-Sep-19 03-Oct-19 10-Oct-19 17-Oct-19 24-Oct-19 31-Oct-19 L I MS 10458-JUN 19 10459-JUN 19 10620-JUN 19 10028-JUL 19 10112-JUL 19 10149-JUL 19 10334-JUL 19 10002-AUG 19 10031-AUG 19 10126-AUG 19 10196-AUG 19 10286-AUG 19 10026-SEP 19 10052-SEP 19 10154-SEP 19 10279-SEP 19 10026-OCT19 10103-OCT19 10190-OCT19 10329-OCT19 10380-OCT19 Hum Cell Leachate Vol mL 612 932 918 936 929 948 934 950 1033 936 913 1018 896 899 997 832 978 912 957 809 922 pH no unit 6.89 7.24 7.22 7.21 7.25 7.27 7.02 7.07 7.13 7.10 6.99 6.93 6.88 6.67 6.49 6.43 6.59 6.73 6.58 6.68 6.34 Acidity mg/LasCaCO3 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 2 <2 <2 <2 2 <2 <2 <2 <2 <2 Alkalinity mg/L as CaCO3 8 20 21 14 11 7 7 7 5 5 5 3 2 3 4 3 3 2 2 2 2 Conductivity PS/cm 28 42 40 27 20 17 13 13 12 10 8 7 6 4 6 4 7 5 5 5 5 SO4 mg/L 1.4 0.8 0.4 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 < 0.2 Cr(VI) mg/L <0.2 --- --- --- --- --- --- --- --- --- --- --- --- --- -- --- --- --- --- --- --- Hg mg/L < 0.00001 < 0.00001 < 0.00001 < 0.00001 < 0.00001 0.00001 --- --- --- --- < 0.00001 --- --- --- --- 0.00001 --- --- --- --- < 0.00001 Ag mg/L < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 < 0.00005 --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 --- --- --- --- < 0.00005 Al mg/L 0.055 0.016 0.017 0.023 0.022 0.021 --- --- --- --- 0.019 --- --- --- --- 0.022 --- --- --- --- 0.007 As mg/L 0.0010 0.0013 0.0011 0.0008 0.0006 0.0005 --- --- --- --- 0.0004 --- --- --- --- 0.0004 --- --- --- --- 0.0004 B mg/L 0.005 0.009 0.007 < 0.002 < 0.002 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 Ba mg/L 0.00025 0.00112 0.00257 0.00276 0.00261 0.00271 --- --- --- --- 0.00172 --- --- --- --- 0.00141 --- --- --- --- 0.00092 Be mg/L 0.000027 0.000011 0.000011 0.000019 0.000011 0.000009 --- --- --- --- 0.000027 --- --- --- --- 0.000017 --- --- --- --- 0.000034 Bi mg/L 0.000017 0.000009 0.000008 < 0.000007 < 0.000007 < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 --- --- --- --- < 0.000007 Ca mg/L 0.44 2.59 3.61 3.67 3.06 2.55 --- --- --- --- 1.09 --- --- --- --- 0.64 --- --- --- --- 0.54 Cd mg/L < 0.000003 0.000032 0.000006 < 0.000003 0.000005 0.000014 --- --- --- --- 0.000004 --- --- --- --- 0.000009 --- --- --- --- 0.000009 Co mg/L 0.000027 0.000024 0.000019 0.000018 < 0.000004 < 0.000004 --- --- --- --- < 0.000004 --- --- --- --- 0.000018 --- --- --- --- < 0.000004 Cr mg/L 0.00015 0.00046 0.00066 0.00042 0.00029 0.00027 --- --- --- --- 0.00013 --- --- --- --- 0.00013 --- --- --- --- < 0.00008 Cu mg/L 0.0030 0.0020 0.0010 0.0006 0.0004 0.0007 --- --- --- --- < 0.0002 --- --- --- --- 0.0004 --- --- --- --- < 0.0002 Fe mg/L < 0.007 < 0.007 < 0.007 < 0.007 < 0.007 < 0.007 --- --- --- --- < 0.007 --- --- --- --- < 0.007 --- --- --- --- < 0.007 K mg/L 0.459 1.12 0.948 0.614 0.402 0.321 --- --- --- --- 0.216 --- --- --- --- 0.077 --- --- --- --- 0.119 Li mg/L 0.0800 0.114 0.135 0.0499 0.0315 0.0253 --- --- --- --- 0.0144 --- --- --- --- 0.0093 --- --- --- --- 0.0118 Mg mg/L 0.050 0.357 0.448 0.385 0.302 0.242 --- --- --- --- 0.094 --- --- --- --- 0.054 --- --- --- --- 0.043 Mn mg/L 0.00277 0.00108 0.00060 0.00064 0.00053 0.00074 --- --- --- --- 0.00410 --- --- --- --- 0.00897 --- --- --- --- 0.0219 Mo mg/L 0.00133 0.00230 0.00156 0.00130 0.00082 0.0265 --- --- --- --- 0.00056 --- --- --- --- 0.00024 --- --- --- --- 0.00031 Na mg/L 4.54 5.35 2.97 0.96 0.43 0.28 --- --- --- --- 0.28 --- --- --- --- 0.07 --- --- --- --- 0.11 Ni mg/L 0.0003 0.0002 0.0001 < 0.0001 < 0.0001 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 P mg/L 0.065 0.066 0.064 0.044 0.034 0.045 --- --- --- --- 0.069 --- --- --- --- 0.090 --- --- --- --- 0.131 Pb mg/L 0.00010 0.00016 0.00006 0.00002 0.00003 0.00003 --- --- --- --- 0.00001 --- --- --- --- 0.00003 --- --- --- --- 0.00004 Sb mg/L < 0.0009 < 0.0009 0.0011 < 0.0009 < 0.0009 < 0.0009 --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 --- --- --- --- < 0.0009 Se mg/L 0.00005 < 0.00004 < 0.00004 < 0.00004 < 0.00004 < 0.00004 --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 --- --- --- --- < 0.00004 Si mg/L 0.47 1.39 1.76 1.55 1.45 1.29 --- --- --- --- 1.18 --- --- --- --- 0.75 --- --- --- --- 0.68 Sn mg/L 0.00043 0.00035 0.00039 0.00029 0.00023 0.00019 --- --- --- --- 0.00011 --- --- --- --- 0.00013 --- --- --- --- 0.00013 Sr mg/L 0.00159 0.00960 0.0119 0.00982 0.00671 0.00661 --- --- --- --- 0.00275 --- --- --- --- 0.00186 --- --- --- --- 0.00203 Ti mg/L 0.00010 0.00019 < 0.00005 < 0.00005 < 0.00005 0.00008 --- --- --- --- < 0.00005 --- --- --- --- 0.00017 --- --- --- --- < 0.00005 Th mg/L < 0.0001 < 0.0001 0.0001 < 0.0001 < 0.0001 < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 --- --- --- --- < 0.0001 Ti mg/L 0.000012 0.000044 0.000048 0.000034 0.000018 0.000020 --- --- --- --- 0.000017 --- --- --- --- 0.000014 --- --- --- --- 0.000006 J mg/L 0.00545 0.0122 0.00715 0.00241 0.000933 0.00534 --- --- --- --- 0.000083 --- --- --- --- 0.000109 --- --- --- --- 0.000046 V mg/L 0.00035 0.00047 0.00045 0.00038 0.00028 0.00043 --- --- --- --- 0.00021 --- --- --- --- 0.00019 --- --- --- --- 0.00016 W mg/L 0.00003 0.00025 0.00011 0.00003 < 0.00002 < 0.00002 --- --- --- --- < 0.00002 --- --- --- --- 0.00003 --- --- --- --- < 0.00002 Y mg/L 0.000006 0.000008 0.000003 0.000003 0.000005 0.000011 --- --- --- --- < 0.000002 --- --- --- --- 0.000002 --- --- --- --- 0.000003 Zn mg/L 0.004 0.003 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- 0.004 --- --- --- --- 0.002 --- --- --- --- 0.003 Zr mg/L < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 --- --- --- --- < 0.002 This report refers to the samples as -received. SGS Minerals Services is not responsible for any use of this data beyond the result of this test method.