10153-AH-Chemical_Analysis-083019

1293 Graham Farm Road, PO Box 68
McClellanville, South Carolina 29458
[phone]
www.athenatechnologies.com

2 May 2018

Mr. Robert Neal
Moffatt & Nichol
272 N. Front Street, Suite 204
Wilmington, NC 28401

RE: Chemical Data Summary
Atlantic Harbor
Carteret County Navigation Project
North Carolina

Dear Mr. Neal,

Athena Technologies, Inc. is pleased to submit this Chemical Data Summary for
Atlantic Harbor. Should you have any questions or concerns regarding the attached data
summary, please don’t hesitate to contact me via the information below.

Respectfully,

J. Adam Freeze
Vice President / Geologist

1293 Graham Farm Road, PO Box 68
McClellanville, South Carolina 29458
[phone]
www.athenatechnologies.com

CHEMICAL DATA SUMMARY

ATLANTIC HARBOR
CARTERET COUNTY NAVIGATION PROJECT
NORTH CAROLINA

TABLE OF CONTENTS

Table 1: Summary of Analytical Detections – Volatile Organic
Compounds, Semivolatile Organic Compounds, and Petroleum
Hydrocarbons

Table 2: Summary of Analytical Detections – Metals and Pesticides

APPENDICES

Appendix A: Laboratory Analytical Reports – Chemical Analyses

P a g e | 1G1 G2 G3 C1 G1 G2 G3 C1 G1G1-DUPG2 G3 C1C1-DUPG1 G2 G3 C1 G1 G2 G3 C10.5 3.1 5.7 0 - 6.2 0.5 2.7 4.8 0 - 5.3 0.5 0.5 1.6 2.7 0 - 3.2 0 - 3.2 0.5 3.7 6.8 0 - 7.3 0.5 2.8 5.1 0 - 5.6GGGCGGGCGG / DUPGGCC / DUPGGGCGGGCAnalyte CAS No.EPA [1]NOAA TEL [2]NOAA ERL [3]UnitsAcetone 67-64-1 -- -- --ȝJNJND ND ND NA ND13ND NA27ND16ND NA NA ND ND ND NA ND ND ND NACarbon disulfide 75-15-0 131 -- --ȝJNJND ND ND NA ND ND ND NA11ND ND ND NA NA ND ND ND NA ND ND ND NAMethylene Chloride 75-09-2 667 -- --ȝJNJND ND ND NA7.5 7.1 5.6NA13 10 8.3 15NA NA ND ND ND NA ND ND ND NAToluene 108-88-3 568 -- --ȝJNJND ND3.6NA ND ND ND NA ND ND ND ND NA NA ND ND ND NA ND ND ND NAAcenaphthene 83-32-9 6.7 6.71 16ȝJNJNA NA NA ND NA NA NA14 JNA NA NA NA ND ND NANA NA ND NA NA NA NDAcenaphthylene 208-96-8 5.9 5.87 44ȝJNJNA NA NA ND NA NA NA32 JNA NA NA NA52 J 45 JNA NA NA ND NA NA NA NDAnthracene 120-12-7 47 46.9 85.3ȝJNJNA NA NA26NA NA NA50NA NA NA NA53 J 40 JNA NA NA ND NA NA NA NDBenzo[a]anthracene 56-55-3 75 74.8 261ȝJNJNA NA NA16 JNA NA NA150NA NA NA NA130 100NA NA NA1.7NA NA NA NDBenzo[a]pyrene 50-32-8 89 88.8 430ȝJNJNA NA NA16 JNA NA NA130NA NA NA NA150 110NA NA NA ND NA NA NA NDBenzo[b]fluoranthene 205-99-2 -- -- --ȝJNJNA NA NA32NA NA NA200NANA NA NA290 220NA NA NA2.5NA NA NA NDBenzo[g,h,i]perylene 191-24-2 310 -- --ȝJNJNA NA NA12 JNA NA NA79NA NA NA NA90 67NA NA NA ND NA NA NA NDBenzo[k]fluoranthene 207-08-9 -- -- --ȝJNJNA NA NA13 JNA NA NA68NA NA NA NA120 98NA NA NA ND NA NA NA NDChrysene 218-01-9 108 108 384ȝJNJNA NA NA28NA NA NA150NA NA NA NA120 110NA NA NA1.8NA NA NA NDDibenz(a,h)anthracene 53-70-3 6.2 6.22 63.4ȝJNJNA NA NA ND NA NA NA25 JNA NA NA NA23 J 16 JNA NA NA ND NA NA NA NDFluoranthene 206-44-0 113 113 600ȝJNJNA NA NA31NA NA NA400NA NA NA NA160 130NA NA NA ND NA NA NA NDFluorene 86-73-7 21 21.2 19ȝJNJNA NA NA ND NA NA NA15 JNA NA NA NA ND ND NA NA NA ND NA NA NA NDIndeno[1,2,3-cd]pyrene 193-39-5 340 -- --ȝJNJNA NA NA8.9 JNA NA NA74NA NA NA NA85 61NA NA NA ND NA NA NA NDPhenanthrene 85-01-8 87 86.7 240ȝJNJNA NA NA8.4 JNA NA NA60NA NA NA NA ND ND NA NA NA ND NA NA NA NDPyrene 129-00-0 153 153 665ȝJNJNA NA NA25NA NA NA310NA NA NA NA260 220NA NA NA1.9NA NA NA NDTPH - Residual68476-53-9 -- -- -- mg/kg NA NA NA ND NA NA NA310 JNA NA NA NA500 J 610 JNA NA NA ND NA NA NA NDC11-C22 Aromatics -- -- -- -- mg/kg NA NA NA ND NA NA NA12NA NA NA NA28 16NA NA NA ND NA NA NA NDC19-C36 Aliphatics -- -- -- -- mg/kg NA NA NA ND NA NA NA12NA NA NA NA ND ND NA NA NA ND NA NA NA NDC9-C18 Aliphatics -- -- -- -- mg/kg NA NA NA ND NA NA NA ND NA NA NA NA15ND NA NA NA ND NA NA NA NDNotesft bss = feet below sediment surfaceG= Grab sampleC = Composite sampleDUP = Field duplicate sampleCAS No. = Chemical Abstracts Service NumberEPA[1]= U.S. Environmental Protection Agency (USEPA), Region 4 Ecological Risk Assessment Supplemental Guidance, Sediment Screening Values for Hazardous Waste Sites, Marine/Estuarine Sediment, Ecological Screening Value (ESV) (USEPA 2018).NOAA TEL [2]= National Oceanic and Atmospheric Administration (NOAA), Screening Quick Reference Tables (SQuiRTs), Marine Sediment, Threshold Effects Levels (Buchman, M.F., 2008).NOAA ERL [3]= National Oceanic and Atmospheric Administration (NOAA), Screening Quick Reference Tables (SQuiRTs), Marine Sediment, Effects Range-Low (Buchman, M.F., 2008).-- = Screening criteria not establishedȝJNJ= micrograms per kilogramND = Analyte not detected above laboratory Method Detection Limit.NA = Not AnalyzedBold= Analyte detected above laboratory Method Detection Limit.Yellow Shading = Concentration exceeds respective screening criteria.J= Result is less that the Reporting Limit but greater than or equal to the Method Detection Limit and the concentration is an approximate value.mg/kg = milligrams per kilogramVolatile Petroleum Hydrcarbons (VPH)Not detected above laboratory method detection limit.AH-06-0318 AH-07-0318TABLE 1SUMMARY OF ANALYTICAL DETECTIONSVOLATILE ORGANIC COMPOUNDS, SEMIVOLATILE ORGANIC COMPOUNDS, AND PETROLEUM HYDROCARBONSATLANTIC HARBORVolatile Organic CompoundsSemivolatile Organic CompoundsAH-05-0318Boring ID:Sample ID:Sample Depth / Interval (ft bss):Sample Type:AH-02-0318 AH-04-0318Total Petroleum Hydrocarbons (TPH)Extractable Petroleum Hydrocarbons (EPH) 1293 Graham Farm Road, PO Box 68McClellanville, South Carolina 29458(843) 887-3800www.athenatechnologies.com
P a g e |2AH-02-0318 AH-04-0318AH-06-0318 AH-07-0318C1 C1 C1 C1-DUP C1 C10 - 6.2 0 - 5.3 0 - 3.2 0 - 3.2 0 - 7.3 0 - 5.6C C C C / DUP C CAnalyte CAS No.EPA [1]NOAATEL [2]NOAAERL [3]UnitsAntimony 7440-36-0 2 -- -- mg/kg ND0.075 JND0.13 JND NDArsenic 7440-38-2 7.24 7.24 8.2 mg/kg4.5 7.8 10 8.3 1.4 0.75Beryllium 7440-41-7 -- -- -- mg/kg0.37 0.58 0.69 0.62 0.0920.054 JCadmium 7440-43-9 0.68 0.68 1.2 mg/kg0.045 J0.13 0.33 0.29ND0.011 JChromium 7440-47-3 52.3 52.3 81 mg/kg19 30 38 32 4.8 3.1Copper 7440-50-8 18.7 18.7 34 mg/kg6.9 34 120 99 1.8 0.73Lead 7439-92-1 30.2 30.24 46.7 mg/kg12 23 34 27 1.8 1.5Manganese 7439-96-5 -- -- -- mg/kg110 150 160 140 14 9.5Nickel 7440-02-0 15.9 15.9 20.9 mg/kg81215122.31.2Selenium 7782-49-2 -- -- -- mg/kg0.44 J0.74 1.11 J 0.13 J 0.037 JSilver 7440-22-4 0.73 0.73 1 mg/kg0.024 J 0.055 J 0.069 J 0.051 JND NDThallium7440-28-0 -- -- -- mg/kg0.11 0.2 0.3 0.250.019 J 0.023 JZinc 7440-66-6 124 124 150 mg/kg31 80 170 150 6.3 2.9Mercury 7439-97-6 0.13 0.13 0.15 mg/kg0.03 0.059 0.11 0.099ND NDChromium, Trivalent 16065-83-1 -- -- -- mg/kg19 30 38 32 4.7 2.9Chromium, Hexavalent 18540-29-9 -- -- -- mg/kg ND ND ND ND0.19 J 0.19 J4,4'-DDD 72-54-8 1.2 1.22 2ȝJNJ0.11 J1.7 1.8 1.8ND F1 ND4,4'-DDE 72-55-9 2.1 2.07 2.2ȝJNJ0.23 J1.5 4.8 4.30.016 J F1ND4,4'-DDT 50-29-3 0.7 1.19 1ȝJNJND6.6ND ND ND NDEndrin aldehyde 7421-93-4 -- -- --ȝJNJND ND ND ND0.018 J F1NDoxy-Chlordane 27304-13-8 -- -- --ȝJNJND ND ND ND0.011 J p 0.012 J ptrans-Chlordane 5103-74-2 -- -- --ȝJNJND0.36 J 0.58 J 0.58 JND F1 NDNotesft bss = feet below sediment surfaceC= Composite sampleDUP = Field duplicate sampleCAS No. = Chemical Abstracts Service NumberEPA[1]= U.S. Environmental Protection Agency (USEPA), Region 4 Ecological Risk Assessment Supplemental Guidance, Sediment Screening Values for Hazardous Waste Sites, Marine/Estuarine Sediment, Ecological Screening Value (ESV) (USEPA 2018).NOAA TEL [2]= National Oceanic and Atmospheric Administration (NOAA), Screening Quick Reference Tables (SQuiRTs), Marine Sediment, Threshold Effects Levels (Buchman, M.F., 2008).NOAA ERL [3]= National Oceanic and Atmospheric Administration (NOAA), Screening Quick Reference Tables (SQuiRTs), Marine Sediment, Effects Range-Low (Buchman, M.F., 2008).-- = Screening criteria not establishedmg/kg= milligrams per kilogramND = Analyte not detected above laboratory Method Detection Limit.Bold= Analyte detected above laboratory Method Detection Limit.J= Result is less that the Reporting Limit but greater than or equal to the Method Detection Limit and the concentration is an approximate value.ȝJNJ= micrograms per kilogramF1= Matrix spike and/or matrix spike duplicate recovery is outside acceptance limits.p= The Relative Percent Difference between the primary and confirmation column/detector is greater than 40%. The lower value has been reported. PesticidesMetalsTABLE 2SUMMARY OF ANALYTICAL DETECTIONSMETALS AND PESTICIDESATLANTIC HARBORSample Type:Boring ID:Sample ID:Sample Depth / Interval (ft bss):AH-05-0318 1293 Graham Farm Road, PO Box 68McClellanville, South Carolina 29458(843) 887-3800www.athenatechnologies.com

1293 Graham Farm Road, PO Box 68
McClellanville, South Carolina 29458
[phone]
www.athenatechnologies.com
Appendix A:
Laboratory Analytical Reports – Chemical Analyses
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Pittsburgh
301 Alpha Drive
RIDC Park
Pittsburgh, PA 15238
Tel: [phone]
TestAmerica Job ID: 180-76196-1
Client Project/Site: North Carolina Sediment Project
For:
Athena Technologies, Inc
1293 Graham Farm Road
PO BOX 68
McClellanville, South Carolina 29458
Attn: Adam Freeze
Authorized for release by:
4/18/2018 1:31:35 PM
Carrie Gamber, Senior Project Manager
[phone]
[e-mail]
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 180-76196-1
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .58
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .87
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .95
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .104
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Case Narrative
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Job ID: 180-76196-1
Laboratory: TestAmerica Pittsburgh
Narrative
CASE NARRATIVE
Client: Athena Technologies, Inc
Project: North Carolina Sediment Project
Report Number: 180-76196-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 03/28/2018 and 03/28/2018; the samples arrived in good condition, properly preserved and on ice. The
temperatures of the 3 coolers at receipt time were 3.4º C, 4.8º C and 5.8º C.
The following samples were listed on the Chain of Custody (COC); however, no samples were received as there was a cooler delayed in
shipment. These samples were received on March 29, 2018 within temperature: AH-07-0318-G1 (180-76196-1), AH-07-0318-G2
(180-76196-2), AH-07-0318-G3 (180-76196-3), AH-07-0318-C (180-76196-4) and AH-06-0318-G1 (180-76196-5).
The container label for the following sample did not match the information listed on the Chain-of-Custody (COC): AH-04-0318-G3
(180-76196-15). The container labels list AH-04-0318-G2, while the COC lists AH-04-0318-G3. The id on the COC was used.
The Chain-of-Custody (COC) was incomplete as received and/or improperly completed. The COC lists three containers for the following
sample; however two were received.
The vials received for the TOC analysis were preserved at the laboratory per the notation on the COC: EB-02-0318 (180-76196-24)
The following samples were received outside of the holding time for freezing the volatile terracores. The terra core vials were frozen as
soon as possible after receipt. The samples have had the H qualifier applied: AH-07-0318-G1 (180-76196-1), AH-07-0318-G2
(180-76196-2), AH-07-0318-G3 (180-76196-3) and AH-07-0318-C (180-76196-4).
VOLATILES
Methylene Chloride was detected in method blank MB 180-240896/7 at a level that was above the method detection limit but below the
reporting limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the
MDL and/or RL, the result has been flagged.
Methylene Chloride was detected in method blank MB 180-241049/6 at a level that was above the method detection limit but below the
reporting limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the
MDL and/or RL, the result has been flagged.
The following analyte recovered outside control limits for the LCS associated with analytical batch 180-240736: Chloroethane. This is not
indicative of a systematic control problem because these were random marginal exceedances. Qualified results have been reported.
The continuing calibration verification (CCV) associated with batch 180-240660 recovered above the upper control limit for
Dichlorodifluoro-methane. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have
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Case Narrative
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Job ID: 180-76196-1 (Continued)
Laboratory: TestAmerica Pittsburgh (Continued)
been reported. The following sample is impacted: (CCVIS 180-240660/2).
The continuing calibration verification (CCV) associated with batch 180-240865 recovered above the upper control limit for Carbon
Tetrachloride. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
The following sample is impacted: (CCVIS 180-240865/2).
SEMIVOLATILES
An incorrect volume of surrogate spiking solution was inadvertently added the following samples: AH-02-0318-C (180-76196-12). Percent
recoveries are based on the amount spiked.
The following samples were diluted due to the nature of the sample matrix: AH-07-0318-C (180-76196-4), AH-06-0318-C (180-76196-8),
AH-02-0318-C (180-76196-12), AH-04-0318-C (180-76196-16), AH-05-0318-C (180-76196-21), AH-05-0318-C-DUP (180-76196-22),
(180-76196-A-4-B MS) and (180-76196-A-4-C MSD). Elevated reporting limits (RLs) are provided.
The continuing calibration verification (CCV) analyzed in batch 180-241401 was outside the method criteria for the following analyte:
Nitrobenzene-d5 (Surr) was >20% high. As indicated in the reference method, sample analysis may proceed; however, any detection for
the affected analyte is considered estimated.
PESTICIDES
The following samples were diluted due to the nature of the sample matrix: AH-02-0318-C (180-76196-12), AH-04-0318-C
(180-76196-16), AH-05-0318-C (180-76196-21) and AH-05-0318-C-DUP (180-76196-22). Elevated reporting limits (RLs) are provided.
The sample extracts were a medium yellow color after GPC clean-up.
Surrogate DCB Decachlorobiphenyl (Surr) recovery for the following sample was outside control limits on the confirmation column:
EB-02-0318 (180-76196-24). Evidence of matrix interference is present due to preceding sample analyzed; therefore, re-extraction and/or
re-analysis was not performed.
Surrogate recovery was outside acceptance limits for the following sample: (180-76196-A-8-I MSD). The parent sample and MS
surrogates recovery was within limits. The MSD sample has been qualified and reported.
Several analytes failed the recovery criteria low for the MS/MSD of sample AH-06-0318-C (180-76196-8) in batch 180-242257.
The continuing calibration verification (CCV) associated with batch 242257 recovered outside acceptance criteria, low biased, for
delta-BHC and Endosulfan sulfate. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the
associated samples were non-detect for this analyte, the data have been reported.
The continuing calibration verification (CCV) associated with batch 241080 recovered outside acceptance criteria, low biased, for
delta-BHC and Endosulfan sulfate on MR-1 column and Endosulfan sulfate and Endrin ketone on MR-2 column. A reporting limit (RL)
standard was analyzed, and the target analyte was detected. Since the associated samples were non-detect for this analyte, the data
have been reported. Detections of these compounds were taken from their passing column, where applicable.
METALS
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GENERAL CHEMSITRY
The sample post-digestion spike (PDS) recoveries were outside criteria. Acceptable laboratory control sample (LCS) soluble and
insoluble analysis data demonstrate that the analytical system was operating in control; therefore, this condition is most likely due to a
matrix effect.
The reporting limit for Lloyd Kahn TOC analysis is a nominal value and does not reflect adjustments in sample mass processed on an
individual basis.
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Definitions/Glossary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Qualifiers
GC/MS VOA
Qualifier Description
H Sample was prepped or analyzed beyond the specified holding time
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
*LCS or LCSD is outside acceptance limits.
GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
X Surrogate is outside control limits
F1 MS and/or MSD Recovery is outside acceptance limits.
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
General Chemistry
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Accreditation/Certification Summary
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Laboratory: TestAmerica Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)4344State Program 12-31-18
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but are not accredited/certified under this accreditation/certification:
Lloyd Kahn Sediment Total Organic Carbon - Duplicates
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
2540G Sediment Percent Moisture
2540G Sediment Percent Solids
Laboratory: TestAmerica Pensacola
The accreditations/certifications listed below are applicable to this report.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3144State Program 12-31-18
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Sample Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
180-76196-1 AH-07-0318-G1 Sediment 03/27/18 08:40 03/28/18 11:36
180-76196-2 AH-07-0318-G2 Sediment 03/27/18 08:42 03/28/18 11:36
180-76196-3 AH-07-0318-G3 Sediment 03/27/18 08:45 03/28/18 11:36
180-76196-4 AH-07-0318-C Sediment 03/27/18 08:50 03/28/18 11:36
180-76196-5 AH-06-0318-G1 Sediment 03/27/18 09:20 03/28/18 11:36
180-76196-6 AH-06-0318-G2 Sediment 03/27/18 09:22 03/28/18 11:36
180-76196-7 AH-06-0318-G3 Sediment 03/27/18 09:25 03/28/18 11:36
180-76196-8 AH-06-0318-C Sediment 03/27/18 09:30 03/28/18 11:36
180-76196-9 AH-02-0318-G1 Sediment 03/27/18 09:55 03/28/18 11:36
180-76196-10 AH-02-0318-G2 Sediment 03/27/18 09:57 03/28/18 11:36
180-76196-11 AH-02-0318-G3 Sediment 03/27/18 10:00 03/28/18 11:36
180-76196-12 AH-02-0318-C Sediment 03/27/18 10:05 03/28/18 11:36
180-76196-13 AH-04-0318-G1 Sediment 03/27/18 10:40 03/28/18 09:30
180-76196-14 AH-04-0318-G2 Sediment 03/27/18 10:42 03/28/18 09:30
180-76196-15 AH-04-0318-G3 Sediment 03/27/18 10:45 03/28/18 09:30
180-76196-16 AH-04-0318-C Sediment 03/27/18 10:50 03/28/18 09:30
180-76196-17 AH-05-0318-G1 Sediment 03/27/18 11:35 03/28/18 09:30
180-76196-18 AH-05-0318-G1-DUP Sediment 03/27/18 11:37 03/28/18 09:30
180-76196-19 AH-05-0318-G2 Sediment 03/27/18 11:40 03/28/18 09:30
180-76196-20 AH-05-0318-G3 Sediment 03/27/18 11:45 03/28/18 09:30
180-76196-21 AH-05-0318-C Sediment 03/27/18 11:55 03/28/18 09:30
180-76196-22 AH-05-0318-C-DUP Sediment 03/27/18 11:58 03/28/18 09:30
180-76196-23 TB-02-0318 Water 03/27/18 12:30 03/28/18 09:30
180-76196-24 EB-02-0318 Water 03/27/18 12:50 03/28/18 09:30
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Method Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method Method Description LaboratoryProtocol
SW846EPA 8260B Volatile Organic Compounds (GC/MS)TAL PIT
SW8468270D LL Semivolatile Organic Compounds by GC/MS - Low Level TAL PIT
SW846EPA 8270D LL Semivolatile Organic Compounds by GC/MS - Low Level TAL PIT
SW8468081B_LL Organochlorine Pesticides (GC)TAL PIT
SW846EPA 8081B LL Organochlorine Pesticides (GC)TAL PIT
SW8466020BMetals (ICP/MS)TAL PIT
SW8467471BMercury (CVAA)TAL PIT
SW846EPA 6020B Metals (ICP/MS)TAL PIT
SW846EPA 7470A Mercury (CVAA)TAL PIT
1664B1664BHEM and SGT-HEM TAL PEN
SM222540GSM 2540G TAL PIT
SW8467196AChromium, Trivalent (Colorimetric)TAL PIT
SW846EPA 7196A Chromium, Hexavalent TAL PIT
SW846EPA 9071B HEM and SGT-HEM TAL PIT
EPALloyd Kahn Organic Carbon, Total (TOC)TAL PIT
SMSM 5310C Total Organic Carbon TAL PIT
Protocol References:
1664B = 1664B
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater",
SM22 = SM22
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Pittsburgh
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-G1 Lab Sample ID: 180-76196-1
Matrix: SedimentDate Collected: 03/27/18 08:40
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-07-0318-G1 Lab Sample ID: 180-76196-1
Matrix: SedimentDate Collected: 03/27/18 08:40
Percent Solids: 77.6Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.1985 g 5 mL
Analysis EPA 8260B 1 240896 03/30/18 15:26 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-07-0318-G2 Lab Sample ID: 180-76196-2
Matrix: SedimentDate Collected: 03/27/18 08:42
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-07-0318-G2 Lab Sample ID: 180-76196-2
Matrix: SedimentDate Collected: 03/27/18 08:42
Percent Solids: 77.4Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.0621 g 5 mL
Analysis EPA 8260B 1 240896 03/30/18 17:23 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-07-0318-G3 Lab Sample ID: 180-76196-3
Matrix: SedimentDate Collected: 03/27/18 08:45
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-07-0318-G3 Lab Sample ID: 180-76196-3
Matrix: SedimentDate Collected: 03/27/18 08:45
Percent Solids: 83.8Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.1219 g 5 mL
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-G3 Lab Sample ID: 180-76196-3
Matrix: SedimentDate Collected: 03/27/18 08:45
Percent Solids: 83.8Date Received: 03/28/18 11:36
Analysis EPA 8260B KLG04/02/18 09:401 TAL PIT241049
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-07-0318-C Lab Sample ID: 180-76196-4
Matrix: SedimentDate Collected: 03/27/18 08:50
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Analysis 7196A 1 241989 04/12/18 11:38 MM1 TAL PITTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-07-0318-C Lab Sample ID: 180-76196-4
Matrix: SedimentDate Collected: 03/27/18 08:50
Percent Solids: 81.0Date Received: 03/28/18 11:36
Prep 3541 BAP04/02/18 03:39 TAL PIT241037
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.1 g 0.5 mL
Analysis 8270D LL 2 241401 04/05/18 15:20 DLF TAL PITTotal/NA 1 mL 1 mL
CH71Instrument ID:
Prep 3541 241038 04/02/18 03:41 BAP TAL PITTotal/NA 30.3 g 10.0 mL
Cleanup 3640A 241931 04/12/18 06:12 BAP TAL PITTotal/NA 5.0 mL 0.5 mL
Analysis 8081B_LL 1 242257 04/16/18 13:54 DFE TAL PITTotal/NA
CHGC15Instrument ID:
Prep 3050B 241695 04/09/18 16:04 KA TAL PITTotal/NA 2.00 g 100 mL
Analysis 6020B 1 241911 04/11/18 02:00 WTR TAL PITTotal/NA
MInstrument ID:
Prep 7471B 241273 04/04/18 08:35 RJR TAL PITTotal/NA 1.32 g 100 mL
Analysis 7471B 1 241400 04/05/18 09:30 RJR TAL PITTotal/NA
KInstrument ID:
Prep 3060A 240858 03/29/18 14:32 SES TAL PITTotal/NA 2.47 g 100 mL
Analysis EPA 7196A 1 240949 03/30/18 13:18 SES TAL PITTotal/NA 25 mL 25 mL
GENESYS10SInstrument ID:
Prep 9071B 241004 03/31/18 06:25 CBY TAL PITTotal/NA 30.0 g 30.0 g
Analysis EPA 9071B 1 241091 04/03/18 08:15 JAS TAL PITTotal/NA
NOEQUIPInstrument ID:
Analysis Lloyd Kahn 1 241158 04/02/18 14:55 JBF TAL PITTotal/NA
FLASHEAInstrument ID:
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-G1 Lab Sample ID: 180-76196-5
Matrix: SedimentDate Collected: 03/27/18 09:20
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-06-0318-G1 Lab Sample ID: 180-76196-5
Matrix: SedimentDate Collected: 03/27/18 09:20
Percent Solids: 78.9Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.3981 g 5 mL
Analysis EPA 8260B 1 240896 03/30/18 16:13 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-06-0318-G2 Lab Sample ID: 180-76196-6
Matrix: SedimentDate Collected: 03/27/18 09:22
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-06-0318-G2 Lab Sample ID: 180-76196-6
Matrix: SedimentDate Collected: 03/27/18 09:22
Percent Solids: 75.6Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.9669 g 5 mL
Analysis EPA 8260B 1 240896 03/30/18 16:36 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-06-0318-G3 Lab Sample ID: 180-76196-7
Matrix: SedimentDate Collected: 03/27/18 09:25
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-06-0318-G3 Lab Sample ID: 180-76196-7
Matrix: SedimentDate Collected: 03/27/18 09:25
Percent Solids: 79.3Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.9743 g 5 mL
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-06-0318-G3 Lab Sample ID: 180-76196-7
Matrix: SedimentDate Collected: 03/27/18 09:25
Percent Solids: 79.3Date Received: 03/28/18 11:36
Analysis EPA 8260B KLG03/30/18 17:001 TAL PIT240896
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-06-0318-C Lab Sample ID: 180-76196-8
Matrix: SedimentDate Collected: 03/27/18 09:30
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Analysis 7196A 1 241989 04/12/18 11:38 MM1 TAL PITTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-06-0318-C Lab Sample ID: 180-76196-8
Matrix: SedimentDate Collected: 03/27/18 09:30
Percent Solids: 81.5Date Received: 03/28/18 11:36
Prep 3541 BAP04/02/18 03:39 TAL PIT241037
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.3 g 0.5 mL
Analysis 8270D LL 2 241401 04/05/18 18:34 DLF TAL PITTotal/NA 1 mL 1 mL
CH71Instrument ID:
Prep 3541 241038 04/02/18 03:41 BAP TAL PITTotal/NA 30.4 g 10.0 mL
Cleanup 3640A 241931 04/12/18 06:12 BAP TAL PITTotal/NA 5.0 mL 0.5 mL
Analysis 8081B_LL 1 242257 04/16/18 14:10 DFE TAL PITTotal/NA
CHGC15Instrument ID:
Prep 3050B 241695 04/09/18 16:04 KA TAL PITTotal/NA 2.00 g 100 mL
Analysis 6020B 1 241911 04/11/18 02:05 WTR TAL PITTotal/NA
MInstrument ID:
Prep 7471B 241273 04/04/18 08:35 RJR TAL PITTotal/NA 1.28 g 100 mL
Analysis 7471B 1 241400 04/05/18 09:32 RJR TAL PITTotal/NA
KInstrument ID:
Prep 3060A 240858 03/29/18 14:32 SES TAL PITTotal/NA 2.53 g 100 mL
Analysis EPA 7196A 1 240949 03/30/18 13:19 SES TAL PITTotal/NA 25 mL 25 mL
GENESYS10SInstrument ID:
Prep 9071B 241004 03/31/18 06:25 CBY TAL PITTotal/NA 30.0 g 30.0 g
Analysis EPA 9071B 1 241091 04/03/18 08:15 JAS TAL PITTotal/NA
NOEQUIPInstrument ID:
Analysis Lloyd Kahn 1 241158 04/02/18 15:05 JBF TAL PITTotal/NA
FLASHEAInstrument ID:
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-G1 Lab Sample ID: 180-76196-9
Matrix: SedimentDate Collected: 03/27/18 09:55
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-02-0318-G1 Lab Sample ID: 180-76196-9
Matrix: SedimentDate Collected: 03/27/18 09:55
Percent Solids: 78.4Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.1779 g 5 mL
Analysis EPA 8260B 1 240896 03/30/18 17:47 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-02-0318-G2 Lab Sample ID: 180-76196-10
Matrix: SedimentDate Collected: 03/27/18 09:57
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-02-0318-G2 Lab Sample ID: 180-76196-10
Matrix: SedimentDate Collected: 03/27/18 09:57
Percent Solids: 59.7Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.3332 g 5 mL
Analysis EPA 8260B 1 240896 03/30/18 18:10 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-02-0318-G3 Lab Sample ID: 180-76196-11
Matrix: SedimentDate Collected: 03/27/18 10:00
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-02-0318-G3 Lab Sample ID: 180-76196-11
Matrix: SedimentDate Collected: 03/27/18 10:00
Percent Solids: 46.5Date Received: 03/28/18 11:36
Prep 5035 KLG03/29/18 09:21 TAL PIT240903
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.1891 g 5 mL
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-G3 Lab Sample ID: 180-76196-11
Matrix: SedimentDate Collected: 03/27/18 10:00
Percent Solids: 46.5Date Received: 03/28/18 11:36
Analysis EPA 8260B KLG04/02/18 10:271 TAL PIT241049
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-02-0318-C Lab Sample ID: 180-76196-12
Matrix: SedimentDate Collected: 03/27/18 10:05
Date Received: 03/28/18 11:36
Analysis 2540G CLL03/29/18 11:321 TAL PIT240823
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Analysis 7196A 1 241989 04/12/18 11:38 MM1 TAL PITTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-02-0318-C Lab Sample ID: 180-76196-12
Matrix: SedimentDate Collected: 03/27/18 10:05
Percent Solids: 57.2Date Received: 03/28/18 11:36
Prep 3541 BAP04/02/18 03:39 TAL PIT241037
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.2 g 0.5 mL
Analysis 8270D LL 4 241401 04/05/18 19:02 DLF TAL PITTotal/NA 1 mL 1 mL
CH71Instrument ID:
Prep 3541 241038 04/02/18 03:41 BAP TAL PITTotal/NA 30.1 g 10.0 mL
Cleanup 3640A 241931 04/12/18 06:12 BAP TAL PITTotal/NA 5.0 mL 0.5 mL
Analysis 8081B_LL 5 242257 04/16/18 14:56 DFE TAL PITTotal/NA
CHGC15Instrument ID:
Prep 3050B 241695 04/09/18 16:04 KA TAL PITTotal/NA 1.95 g 100 mL
Analysis 6020B 1 241911 04/11/18 02:09 WTR TAL PITTotal/NA
MInstrument ID:
Prep 7471B 241273 04/04/18 08:35 RJR TAL PITTotal/NA 1.31 g 100 mL
Analysis 7471B 1 241400 04/05/18 09:34 RJR TAL PITTotal/NA
KInstrument ID:
Prep 3060A 240858 03/29/18 14:32 SES TAL PITTotal/NA 2.55 g 100 mL
Analysis EPA 7196A 1 240949 03/30/18 13:23 SES TAL PITTotal/NA 25 mL 25 mL
GENESYS10SInstrument ID:
Prep 9071B 241004 03/31/18 06:25 CBY TAL PITTotal/NA 30.1 g 30.0 g
Analysis EPA 9071B 1 241091 04/03/18 08:15 JAS TAL PITTotal/NA
NOEQUIPInstrument ID:
Analysis Lloyd Kahn 1 241158 04/02/18 15:15 JBF TAL PITTotal/NA
FLASHEAInstrument ID:
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Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-04-0318-G1 Lab Sample ID: 180-76196-13
Matrix: SedimentDate Collected: 03/27/18 10:40
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-04-0318-G1 Lab Sample ID: 180-76196-13
Matrix: SedimentDate Collected: 03/27/18 10:40
Percent Solids: 39.2Date Received: 03/28/18 09:30
Prep 5035 KLG03/28/18 12:15 TAL PIT240706
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.0511 g 5 mL
Analysis EPA 8260B 1 240660 03/28/18 14:17 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-04-0318-G2 Lab Sample ID: 180-76196-14
Matrix: SedimentDate Collected: 03/27/18 10:42
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-04-0318-G2 Lab Sample ID: 180-76196-14
Matrix: SedimentDate Collected: 03/27/18 10:42
Percent Solids: 39.1Date Received: 03/28/18 09:30
Prep 5035 KLG03/28/18 12:15 TAL PIT240706
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.0915 g 5 mL
Analysis EPA 8260B 1 240660 03/28/18 14:41 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-04-0318-G3 Lab Sample ID: 180-76196-15
Matrix: SedimentDate Collected: 03/27/18 10:45
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-04-0318-G3 Lab Sample ID: 180-76196-15
Matrix: SedimentDate Collected: 03/27/18 10:45
Percent Solids: 46.9Date Received: 03/28/18 09:30
Prep 5035 KLG03/28/18 12:15 TAL PIT240706
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.0875 g 5 mL
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-04-0318-G3 Lab Sample ID: 180-76196-15
Matrix: SedimentDate Collected: 03/27/18 10:45
Percent Solids: 46.9Date Received: 03/28/18 09:30
Analysis EPA 8260B KLG03/28/18 15:041 TAL PIT240660
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-04-0318-C Lab Sample ID: 180-76196-16
Matrix: SedimentDate Collected: 03/27/18 10:50
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Analysis 7196A 1 241989 04/12/18 11:38 MM1 TAL PITTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-04-0318-C Lab Sample ID: 180-76196-16
Matrix: SedimentDate Collected: 03/27/18 10:50
Percent Solids: 41.2Date Received: 03/28/18 09:30
Prep 3541 BAP04/02/18 03:39 TAL PIT241037
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.2 g 0.5 mL
Analysis 8270D LL 5 241401 04/05/18 19:30 DLF TAL PITTotal/NA 1 mL 1 mL
CH71Instrument ID:
Prep 3541 241038 04/02/18 03:41 BAP TAL PITTotal/NA 30.1 g 10.0 mL
Cleanup 3640A 241931 04/12/18 06:12 BAP TAL PITTotal/NA 5.0 mL 0.5 mL
Analysis 8081B_LL 5 242257 04/16/18 15:11 DFE TAL PITTotal/NA
CHGC15Instrument ID:
Prep 3050B 241695 04/09/18 16:04 KA TAL PITTotal/NA 2.00 g 100 mL
Analysis 6020B 1 241911 04/11/18 02:14 WTR TAL PITTotal/NA
MInstrument ID:
Prep 7471B 241273 04/04/18 08:35 RJR TAL PITTotal/NA 1.33 g 100 mL
Analysis 7471B 1 241400 04/05/18 09:36 RJR TAL PITTotal/NA
KInstrument ID:
Prep 3060A 240858 03/29/18 14:32 SES TAL PITTotal/NA 2.53 g 100 mL
Analysis EPA 7196A 1 240949 03/30/18 13:24 SES TAL PITTotal/NA 25 mL 25 mL
GENESYS10SInstrument ID:
Prep 9071B 241004 03/31/18 06:25 CBY TAL PITTotal/NA 30.2 g 30.0 g
Analysis EPA 9071B 1 241091 04/03/18 08:15 JAS TAL PITTotal/NA
NOEQUIPInstrument ID:
Analysis Lloyd Kahn 1 240909 03/29/18 16:39 JBF TAL PITTotal/NA
FLASHEAInstrument ID:
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-G1 Lab Sample ID: 180-76196-17
Matrix: SedimentDate Collected: 03/27/18 11:35
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-05-0318-G1 Lab Sample ID: 180-76196-17
Matrix: SedimentDate Collected: 03/27/18 11:35
Percent Solids: 25.9Date Received: 03/28/18 09:30
Prep 5035 KLG03/28/18 12:15 TAL PIT240706
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.0808 g 5 mL
Analysis EPA 8260B 1 240660 03/28/18 15:28 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-05-0318-G1-DUP Lab Sample ID: 180-76196-18
Matrix: SedimentDate Collected: 03/27/18 11:37
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-05-0318-G1-DUP Lab Sample ID: 180-76196-18
Matrix: SedimentDate Collected: 03/27/18 11:37
Percent Solids: 24.2Date Received: 03/28/18 09:30
Prep 5035 KLG03/28/18 12:15 TAL PIT240706
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.4377 g 5 mL
Analysis EPA 8260B 1 240660 03/28/18 15:51 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-05-0318-G2 Lab Sample ID: 180-76196-19
Matrix: SedimentDate Collected: 03/27/18 11:40
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-05-0318-G2 Lab Sample ID: 180-76196-19
Matrix: SedimentDate Collected: 03/27/18 11:40
Percent Solids: 28.4Date Received: 03/28/18 09:30
Prep 5035 KLG03/28/18 12:15 TAL PIT240706
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.2324 g 5 mL
TestAmerica Pittsburgh
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-G2 Lab Sample ID: 180-76196-19
Matrix: SedimentDate Collected: 03/27/18 11:40
Percent Solids: 28.4Date Received: 03/28/18 09:30
Analysis EPA 8260B KLG03/28/18 16:141 TAL PIT240660
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-05-0318-G3 Lab Sample ID: 180-76196-20
Matrix: SedimentDate Collected: 03/27/18 11:45
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-05-0318-G3 Lab Sample ID: 180-76196-20
Matrix: SedimentDate Collected: 03/27/18 11:45
Percent Solids: 16.8Date Received: 03/28/18 09:30
Prep 5035 KLG03/28/18 12:15 TAL PIT240706
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.9811 g 5 mL
Analysis EPA 8260B 1 240660 03/28/18 16:38 KLG TAL PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: AH-05-0318-C Lab Sample ID: 180-76196-21
Matrix: SedimentDate Collected: 03/27/18 11:55
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Analysis 7196A 1 241989 04/12/18 11:38 MM1 TAL PITTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-05-0318-C Lab Sample ID: 180-76196-21
Matrix: SedimentDate Collected: 03/27/18 11:55
Percent Solids: 24.0Date Received: 03/28/18 09:30
Prep 3541 BAP04/02/18 03:39 TAL PIT241037
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.4 g 0.5 mL
Analysis 8270D LL 5 241401 04/05/18 19:58 DLF TAL PITTotal/NA 1 mL 1 mL
CH71Instrument ID:
Prep 3541 241038 04/02/18 03:41 BAP TAL PITTotal/NA 30.4 g 10.0 mL
Cleanup 3640A 241931 04/12/18 06:12 BAP TAL PITTotal/NA 5.0 mL 0.5 mL
Analysis 8081B_LL 5 242257 04/16/18 15:27 DFE TAL PITTotal/NA
CHGC15Instrument ID:
Prep 3050B 241695 04/09/18 16:04 KA TAL PITTotal/NA 2.04 g 100 mL
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C Lab Sample ID: 180-76196-21
Matrix: SedimentDate Collected: 03/27/18 11:55
Percent Solids: 24.0Date Received: 03/28/18 09:30
Analysis 6020B WTR04/11/18 02:191 TAL PIT241911
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
MInstrument ID:
Prep 7471B 241273 04/04/18 08:35 RJR TAL PITTotal/NA 1.21 g 100 mL
Analysis 7471B 1 241400 04/05/18 09:42 RJR TAL PITTotal/NA
KInstrument ID:
Prep 3060A 240858 03/29/18 14:32 SES TAL PITTotal/NA 2.55 g 100 mL
Analysis EPA 7196A 1 240949 03/30/18 13:30 SES TAL PITTotal/NA 25 mL 25 mL
GENESYS10SInstrument ID:
Prep 9071B 241004 03/31/18 06:25 CBY TAL PITTotal/NA 30.0 g 30.0 g
Analysis EPA 9071B 1 241091 04/03/18 08:15 JAS TAL PITTotal/NA
NOEQUIPInstrument ID:
Analysis Lloyd Kahn 1 240909 03/29/18 16:49 JBF TAL PITTotal/NA
FLASHEAInstrument ID:
Client Sample ID: AH-05-0318-C-DUP Lab Sample ID: 180-76196-22
Matrix: SedimentDate Collected: 03/27/18 11:58
Date Received: 03/28/18 09:30
Analysis 2540G CLL03/29/18 08:421 TAL PIT240793
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
NOEQUIPInstrument ID:
Analysis 7196A 1 241989 04/12/18 11:38 MM1 TAL PITTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: AH-05-0318-C-DUP Lab Sample ID: 180-76196-22
Matrix: SedimentDate Collected: 03/27/18 11:58
Percent Solids: 23.9Date Received: 03/28/18 09:30
Prep 3541 BAP04/02/18 03:39 TAL PIT241037
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.0 g 0.5 mL
Analysis 8270D LL 4 241401 04/05/18 20:26 DLF TAL PITTotal/NA 1 mL 1 mL
CH71Instrument ID:
Prep 3541 241038 04/02/18 03:41 BAP TAL PITTotal/NA 30.3 g 10.0 mL
Cleanup 3640A 241931 04/12/18 06:12 BAP TAL PITTotal/NA 5.0 mL 0.5 mL
Analysis 8081B_LL 5 242257 04/16/18 17:15 DFE TAL PITTotal/NA
CHGC15Instrument ID:
Prep 3050B 241695 04/09/18 16:04 KA TAL PITTotal/NA 1.95 g 100 mL
Analysis 6020B 1 241911 04/11/18 02:23 WTR TAL PITTotal/NA
MInstrument ID:
Prep 7471B 241273 04/04/18 08:35 RJR TAL PITTotal/NA 1.19 g 100 mL
Analysis 7471B 1 241400 04/05/18 09:44 RJR TAL PITTotal/NA
KInstrument ID:
Prep 3060A 240858 03/29/18 14:43 SES TAL PITTotal/NA 2.50 g 100 mL
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C-DUP Lab Sample ID: 180-76196-22
Matrix: SedimentDate Collected: 03/27/18 11:58
Percent Solids: 23.9Date Received: 03/28/18 09:30
Analysis EPA 7196A SES03/30/18 13:311 TAL PIT240949
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 25 mL 25 mL
GENESYS10SInstrument ID:
Prep 9071B 241004 03/31/18 06:25 CBY TAL PITTotal/NA 30.0 g 30.0 g
Analysis EPA 9071B 1 241091 04/03/18 08:15 JAS TAL PITTotal/NA
NOEQUIPInstrument ID:
Analysis Lloyd Kahn 1 240909 03/29/18 16:59 JBF TAL PITTotal/NA
FLASHEAInstrument ID:
Client Sample ID: TB-02-0318 Lab Sample ID: 180-76196-23
Matrix: WaterDate Collected: 03/27/18 12:30
Date Received: 03/28/18 09:30
Analysis EPA 8260B FBB03/28/18 21:151 TAL PIT240736
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CHHP5Instrument ID:
Client Sample ID: EB-02-0318 Lab Sample ID: 180-76196-24
Matrix: WaterDate Collected: 03/27/18 12:50
Date Received: 03/28/18 09:30
Analysis EPA 8260B KLG03/29/18 21:471 TAL PIT240865
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
CHHP6Instrument ID:
Prep 3520C 241088 04/02/18 11:29 BJT TAL PITTotal/NA 240 mL 250 uL
Analysis EPA 8270D LL 1 241375 04/06/18 00:27 VVP TAL PITTotal/NA 1 mL 1 mL
CH733Instrument ID:
Prep 3510C 240746 03/28/18 12:35 CBY TAL PITTotal/NA 980 mL 1.0 mL
Analysis EPA 8081B LL 1 241080 04/02/18 19:49 DFE TAL PITTotal/NA
CHGC15Instrument ID:
Prep 3005A 240953 03/30/18 13:04 KA TAL PITTotal Recoverable 50 mL 50 mL
Analysis EPA 6020B 1 241140 03/31/18 12:37 RSK TAL PITTotal Recoverable
AInstrument ID:
Prep 7470A 241732 04/10/18 11:20 RSK TAL PITTotal/NA 50.0 mL 50.0 mL
Analysis EPA 7470A 1 241904 04/11/18 11:08 RSK TAL PITTotal/NA
KInstrument ID:
Prep 1664B 392275 04/01/18 14:43 BAW TAL PENTotal/NA 986 mL 1000 mL
Analysis 1664B 1 392295 04/02/18 09:06 BAW TAL PENTotal/NA
SPEEDVAPInstrument ID:
Analysis 7196A 1 241989 04/12/18 11:38 MM1 TAL PITTotal/NA
NOEQUIPInstrument ID:
Analysis EPA 7196A 1 240705 03/28/18 12:08 SES TAL PITTotal/NA 25 mL 25 mL
GENESYS10SInstrument ID:
Analysis SM 5310C 1 241245 04/03/18 17:12 CLL TAL PITTotal/NA
TOC1030Instrument ID:
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 180-76196-1
Project/Site: North Carolina Sediment Project
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
Analyst References:
Lab: TAL PEN
Batch Type: Prep
BAW = Benjamin Whatley
Batch Type: Analysis
BAW = Benjamin Whatley
Lab: TAL PIT
Batch Type: Cleanup
BAP = Brian Pino
Batch Type: Prep
BAP = Brian Pino
BJT = Bill Trout
CBY = Charles Yushinski
KA = Kayla Kalamasz
KLG = Kathy Gordon
RJR = Ron Rosenbaum
RSK = Robert Kurtz
SES = Samantha Strauser
Batch Type: Analysis
CLL = Cheryl Loheyde
DFE = David Eppinger
DLF = Donald Ferguson
FBB = Frank Bungard
JAS = Joshua Schmidt
JBF = Joshua Fritsch
KLG = Kathy Gordon
MM1 = Mary Beth Miller
RJR = Ron Rosenbaum
RSK = Robert Kurtz
SES = Samantha Strauser
VVP = Vincent Piccolino
WTR = Bill Reinheimer
TestAmerica Pittsburgh
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-1Client Sample ID: AH-07-0318-G1
Matrix: SedimentDate Collected: 03/27/18 08:40
Percent Solids: 77.6Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND H 6.2 3.1 ug/Kg ☼03/29/18 09:21 03/30/18 15:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.2 3.7 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,1,2,2-Tetrachloroethane ND H
6.2 2.4 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND H
6.2 3.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,1,2-Trichloroethane ND H
6.2 2.2 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,1-Dichloroethane ND H
6.2 3.5 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,1-Dichloroethene ND H
6.2 2.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,2,4-Trichlorobenzene ND H
6.2 3.8 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,2-Dibromo-3-Chloropropane ND H
6.2 5.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,2-Dichlorobenzene ND H
6.2 1.8 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,2-Dichloroethane ND H
6.2 3.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,2-Dichloropropane ND H
6.2 2.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,3-Dichlorobenzene ND H
6.2 1.3 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,4-Dichlorobenzene ND H
6.2 3.6 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼2-Butanone (MEK)ND H
6.2 5.2 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼2-Hexanone ND H
6.2 2.3 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼4-Methyl-2-pentanone (MIBK)ND H
25 3.9 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Acetone ND H
6.2 2.4 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Benzene ND H
6.2 3.2 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Bromoform ND H
6.2 5.6 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Bromomethane ND H
6.2 3.7 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Carbon disulfide ND H
6.2 4.1 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Carbon tetrachloride ND H
6.2 2.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Chlorobenzene ND H
6.2 3.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Chlorodibromomethane ND H
6.2 2.6 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Chloroform ND H
6.2 4.8 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Chloromethane ND H
6.2 3.2 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Chloroethane ND H
6.2 2.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼cis-1,2-Dichloroethene ND H
6.2 2.0 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼cis-1,3-Dichloropropene ND H
6.2 1.5 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Cyclohexane ND H
6.2 2.9 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Dichlorobromomethane ND H
6.2 3.6 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Dichlorodifluoromethane ND H
6.2 2.7 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Ethylbenzene ND H
6.2 3.4 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼1,2-Dibromoethane ND H
6.2 2.9 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Isopropylbenzene ND H
31 7.3 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Methyl acetate ND H
6.2 4.6 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Methyl tert-butyl ether ND H
6.2 2.6 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Methylcyclohexane ND H
6.2 2.9 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Methylene Chloride ND H
6.2 1.7 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Styrene ND H
6.2 2.5 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Tetrachloroethene ND H
6.2 2.1 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Toluene ND H
6.2 3.1 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼trans-1,2-Dichloroethene ND H
6.2 2.1 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼trans-1,3-Dichloropropene ND H
6.2 1.9 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Trichloroethene ND H
6.2 1.8 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Trichlorofluoromethane ND H
12 5.3 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Xylenes, Total ND H
6.2 4.5 ug/Kg 03/29/18 09:21 03/30/18 15:26 1☼Vinyl chloride ND H
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-1Client Sample ID: AH-07-0318-G1
Matrix: SedimentDate Collected: 03/27/18 08:40
Percent Solids: 77.6Date Received: 03/28/18 11:36
1,2-Dichloroethane-d4 (Surr)92 62 -118 03/29/18 09:21 03/30/18 15:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 03/29/18 09:21 03/30/18 15:26 176-111
Dibromofluoromethane (Surr)95 03/29/18 09:21 03/30/18 15:26 172-116
Toluene-d8 (Surr)107 03/29/18 09:21 03/30/18 15:26 180-129
General Chemistry
RL MDL
Percent Moisture 22.4 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 77.6
Lab Sample ID: 180-76196-2Client Sample ID: AH-07-0318-G2
Matrix: SedimentDate Collected: 03/27/18 08:42
Percent Solids: 77.4Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND H 6.4 3.2 ug/Kg ☼03/29/18 09:21 03/30/18 17:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.4 3.8 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,1,2,2-Tetrachloroethane ND H
6.4 2.4 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND H
6.4 3.1 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,1,2-Trichloroethane ND H
6.4 2.3 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,1-Dichloroethane ND H
6.4 3.6 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,1-Dichloroethene ND H
6.4 2.1 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,2,4-Trichlorobenzene ND H
6.4 3.9 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,2-Dibromo-3-Chloropropane ND H
6.4 5.1 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,2-Dichlorobenzene ND H
6.4 1.9 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,2-Dichloroethane ND H
6.4 3.1 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,2-Dichloropropane ND H
6.4 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,3-Dichlorobenzene ND H
6.4 1.3 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,4-Dichlorobenzene ND H
6.4 3.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼2-Butanone (MEK)ND H
6.4 5.3 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼2-Hexanone ND H
6.4 2.4 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼4-Methyl-2-pentanone (MIBK)ND H
26 4.0 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Acetone ND H
6.4 2.5 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Benzene ND H
6.4 3.3 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Bromoform ND H
6.4 5.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Bromomethane ND H
6.4 3.8 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Carbon disulfide ND H
6.4 4.2 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Carbon tetrachloride ND H
6.4 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Chlorobenzene ND H
6.4 3.1 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Chlorodibromomethane ND H
6.4 2.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Chloroform ND H
6.4 4.9 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Chloromethane ND H
6.4 3.3 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Chloroethane ND H
6.4 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼cis-1,2-Dichloroethene ND H
6.4 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼cis-1,3-Dichloropropene ND H
6.4 1.6 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Cyclohexane ND H
6.4 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Dichlorobromomethane ND H
6.4 3.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Dichlorodifluoromethane ND H
6.4 2.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Ethylbenzene ND H
6.4 3.5 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼1,2-Dibromoethane ND H
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-2Client Sample ID: AH-07-0318-G2
Matrix: SedimentDate Collected: 03/27/18 08:42
Percent Solids: 77.4Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Isopropylbenzene ND H 6.4 3.0 ug/Kg ☼03/29/18 09:21 03/30/18 17:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
32 7.5 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Methyl acetate ND H
6.4 4.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Methyl tert-butyl ether ND H
6.4 2.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Methylcyclohexane ND H
6.4 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Methylene Chloride ND H
6.4 1.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Styrene ND H
6.4 2.6 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Tetrachloroethene ND H
6.4 2.2 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Toluene ND H
6.4 3.2 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼trans-1,2-Dichloroethene ND H
6.4 2.2 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼trans-1,3-Dichloropropene ND H
6.4 1.9 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Trichloroethene ND H
6.4 1.9 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Trichlorofluoromethane ND H
13 5.5 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Xylenes, Total ND H
6.4 4.7 ug/Kg 03/29/18 09:21 03/30/18 17:23 1☼Vinyl chloride ND H
1,2-Dichloroethane-d4 (Surr)95 62 -118 03/29/18 09:21 03/30/18 17:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 03/29/18 09:21 03/30/18 17:23 176-111
Dibromofluoromethane (Surr)96 03/29/18 09:21 03/30/18 17:23 172-116
Toluene-d8 (Surr)110 03/29/18 09:21 03/30/18 17:23 180-129
General Chemistry
RL MDL
Percent Moisture 22.6 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 77.4
Lab Sample ID: 180-76196-3Client Sample ID: AH-07-0318-G3
Matrix: SedimentDate Collected: 03/27/18 08:45
Percent Solids: 83.8Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND H 5.8 2.9 ug/Kg ☼03/29/18 09:21 04/02/18 09:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.8 3.5 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,1,2,2-Tetrachloroethane ND H
5.8 2.2 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND H
5.8 2.8 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,1,2-Trichloroethane ND H
5.8 2.1 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,1-Dichloroethane ND H
5.8 3.3 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,1-Dichloroethene ND H
5.8 1.9 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,2,4-Trichlorobenzene ND H
5.8 3.6 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,2-Dibromo-3-Chloropropane ND H
5.8 4.7 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,2-Dichlorobenzene ND H
5.8 1.7 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,2-Dichloroethane ND H
5.8 2.9 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,2-Dichloropropane ND H
5.8 1.9 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,3-Dichlorobenzene ND H
5.8 1.2 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,4-Dichlorobenzene ND H
5.8 3.4 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼2-Butanone (MEK)ND H
5.8 4.9 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼2-Hexanone ND H
5.8 2.2 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼4-Methyl-2-pentanone (MIBK)ND H
23 3.7 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Acetone ND H
5.8 2.3 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Benzene ND H
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-3Client Sample ID: AH-07-0318-G3
Matrix: SedimentDate Collected: 03/27/18 08:45
Percent Solids: 83.8Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Bromoform ND H 5.8 3.0 ug/Kg ☼03/29/18 09:21 04/02/18 09:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.8 5.2 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Bromomethane ND H
5.8 3.5 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Carbon disulfide ND H
5.8 3.9 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Carbon tetrachloride ND H
5.8 1.8 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Chlorobenzene ND H
5.8 2.8 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Chlorodibromomethane ND H
5.8 2.5 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Chloroform ND H
5.8 4.5 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Chloromethane ND H
5.8 3.0 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Chloroethane ND H
5.8 1.8 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼cis-1,2-Dichloroethene ND H
5.8 1.9 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼cis-1,3-Dichloropropene ND H
5.8 1.4 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Cyclohexane ND H
5.8 2.7 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Dichlorobromomethane ND H
5.8 3.4 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Dichlorodifluoromethane ND H
5.8 2.5 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Ethylbenzene ND H
5.8 3.2 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼1,2-Dibromoethane ND H
5.8 2.7 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Isopropylbenzene ND H
29 6.9 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Methyl acetate ND H
5.8 4.3 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Methyl tert-butyl ether ND H
5.8 2.4 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Methylcyclohexane ND H
5.8 2.7 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Methylene Chloride ND H
5.8 1.6 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Styrene ND H
5.8 2.3 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Tetrachloroethene ND H
5.8 2.0 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Toluene ND H
5.8 3.0 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼trans-1,2-Dichloroethene ND H
5.8 2.0 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼trans-1,3-Dichloropropene ND H
5.8 1.7 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Trichloroethene ND H
5.8 1.7 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Trichlorofluoromethane ND H
12 5.0 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Xylenes, Total ND H
5.8 4.3 ug/Kg 03/29/18 09:21 04/02/18 09:40 1☼Vinyl chloride ND H
1,2-Dichloroethane-d4 (Surr)91 62 -118 03/29/18 09:21 04/02/18 09:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 03/29/18 09:21 04/02/18 09:40 176-111
Dibromofluoromethane (Surr)97 03/29/18 09:21 04/02/18 09:40 172-116
Toluene-d8 (Surr)109 03/29/18 09:21 04/02/18 09:40 180-129
General Chemistry
RL MDL
Percent Moisture 16.2 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 83.8
Lab Sample ID: 180-76196-4Client Sample ID: AH-07-0318-C
Matrix: SedimentDate Collected: 03/27/18 08:50
Percent Solids: 81.0Date Received: 03/28/18 11:36
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene ND 8.2 2.4 ug/Kg ☼04/02/18 03:39 04/05/18 15:20 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
8.2 1.8 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Acenaphthylene ND
TestAmerica Pittsburgh
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-4Client Sample ID: AH-07-0318-C
Matrix: SedimentDate Collected: 03/27/18 08:50
Percent Solids: 81.0Date Received: 03/28/18 11:36
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
RL MDL
Anthracene ND 8.2 2.1 ug/Kg ☼04/02/18 03:39 04/05/18 15:20 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
8.2 1.6 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Benzo[a]anthracene ND
8.2 1.8 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Benzo[a]pyrene ND
8.2 2.0 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Benzo[b]fluoranthene ND
8.2 1.8 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Benzo[g,h,i]perylene ND
8.2 1.6 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Chrysene ND
8.2 1.8 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Dibenz(a,h)anthracene ND
8.2 2.2 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Fluoranthene ND
8.2 1.6 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Fluorene ND
8.2 1.7 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Indeno[1,2,3-cd]pyrene ND
8.2 1.6 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Naphthalene ND
8.2 2.2 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Phenanthrene ND
8.2 1.9 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Pyrene ND
8.2 2.5 ug/Kg 04/02/18 03:39 04/05/18 15:20 2☼Benzo[k]fluoranthene ND
2-Fluorobiphenyl 84 34 -100 04/02/18 03:39 04/05/18 15:20 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)93 04/02/18 03:39 04/05/18 15:20 233-100
Terphenyl-d14 (Surr)76 04/02/18 03:39 04/05/18 15:20 230-100
Method: 8081B_LL - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 0.051 0.016 ug/Kg ☼04/02/18 03:41 04/16/18 13:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.051 0.013 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼alpha-BHC ND
0.051 0.013 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼cis-Chlordane ND
0.051 0.013 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼beta-BHC ND
0.51 0.22 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Chlordane (technical)ND
0.051 0.014 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼4,4'-DDD ND
0.051 0.010 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼4,4'-DDE ND
0.051 0.019 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼4,4'-DDT ND
0.051 0.016 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼delta-BHC ND
0.051 0.013 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Dieldrin ND
0.051 0.014 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Endosulfan I ND
0.051 0.011 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Endosulfan II ND
0.051 0.013 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Endosulfan sulfate ND
0.051 0.020 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Endrin ND
0.051 0.018 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Endrin aldehyde ND
0.051 0.018 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Endrin ketone ND
0.051 0.017 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼gamma-BHC (Lindane)ND
0.051 0.012 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼trans-Chlordane ND
0.051 0.016 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Heptachlor ND
0.051 0.013 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Heptachlor epoxide ND
0.051 0.020 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Methoxychlor ND
0.051 0.011 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼oxy-Chlordane 0.012 J p
2.0 1.4 ug/Kg 04/02/18 03:41 04/16/18 13:54 1☼Toxaphene ND
DCB Decachlorobiphenyl (Surr)62 33 -137 04/02/18 03:41 04/16/18 13:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr)62 04/02/18 03:41 04/16/18 13:54 133-137
Tetrachloro-m-xylene 59 04/02/18 03:41 04/16/18 13:54 126-120
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-4Client Sample ID: AH-07-0318-C
Matrix: SedimentDate Collected: 03/27/18 08:50
Percent Solids: 81.0Date Received: 03/28/18 11:36
Method: 8081B_LL - Organochlorine Pesticides (GC) (Continued)
Tetrachloro-m-xylene 66 26 -120 04/02/18 03:41 04/16/18 13:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony ND 0.12 0.038 mg/Kg ☼04/09/18 16:04 04/11/18 02:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.062 0.016 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Arsenic 0.75
0.062 0.0047 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Beryllium 0.054 J
0.062 0.010 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Cadmium 0.011 J
0.12 0.041 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Chromium 3.1
0.12 0.070 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Copper 0.73
0.062 0.022 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Lead 1.5
0.31 0.099 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Manganese 9.5
0.062 0.038 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Nickel 1.2
0.31 0.037 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Selenium 0.037 J
0.062 0.0086 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Silver ND
0.062 0.0080 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Thallium 0.023 J
0.31 0.21 mg/Kg 04/09/18 16:04 04/11/18 02:00 1☼Zinc 2.9
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.019 0.0041 mg/Kg ☼04/04/18 08:35 04/05/18 09:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Moisture 19.0 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 81.0
0.50 0.11 mg/Kg 04/12/18 11:38 1Cr (III)2.9
0.50 0.14 mg/Kg 03/29/18 14:32 03/30/18 13:18 1☼Cr (VI)0.19 J
210 100 mg/Kg 03/31/18 06:25 04/03/18 08:15 1☼Total Petroleum Hydrocarbons
(SGT-HEM)
ND
1200 920 mg/Kg 04/02/18 14:55 1☼Total Organic Carbon - Duplicates 2700
Lab Sample ID: 180-76196-5Client Sample ID: AH-06-0318-G1
Matrix: SedimentDate Collected: 03/27/18 09:20
Percent Solids: 78.9Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND H 5.9 2.9 ug/Kg ☼03/29/18 09:21 03/30/18 16:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.9 3.5 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,1,2,2-Tetrachloroethane ND H
5.9 2.2 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND H
5.9 2.8 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,1,2-Trichloroethane ND H
5.9 2.1 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,1-Dichloroethane ND H
5.9 3.3 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,1-Dichloroethene ND H
5.9 1.9 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,2,4-Trichlorobenzene ND H
5.9 3.6 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,2-Dibromo-3-Chloropropane ND H
5.9 4.7 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,2-Dichlorobenzene ND H
5.9 1.7 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,2-Dichloroethane ND H
5.9 2.9 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,2-Dichloropropane ND H
5.9 1.9 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,3-Dichlorobenzene ND H
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-5Client Sample ID: AH-06-0318-G1
Matrix: SedimentDate Collected: 03/27/18 09:20
Percent Solids: 78.9Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,4-Dichlorobenzene ND H 5.9 1.2 ug/Kg ☼03/29/18 09:21 03/30/18 16:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.9 3.4 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼2-Butanone (MEK)ND H
5.9 4.9 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼2-Hexanone ND H
5.9 2.2 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼4-Methyl-2-pentanone (MIBK)ND H
23 3.7 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Acetone ND H
5.9 2.3 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Benzene ND H
5.9 3.1 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Bromoform ND H
5.9 5.3 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Bromomethane ND H
5.9 3.5 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Carbon disulfide ND H
5.9 3.9 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Carbon tetrachloride ND H
5.9 1.8 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Chlorobenzene ND H
5.9 2.8 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Chlorodibromomethane ND H
5.9 2.5 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Chloroform ND H
5.9 4.5 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Chloromethane ND H
5.9 3.0 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Chloroethane ND H
5.9 1.8 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼cis-1,2-Dichloroethene ND H
5.9 1.9 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼cis-1,3-Dichloropropene ND H
5.9 1.4 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Cyclohexane ND H
5.9 2.8 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Dichlorobromomethane ND H
5.9 3.4 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Dichlorodifluoromethane ND H
5.9 2.5 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Ethylbenzene ND H
5.9 3.2 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼1,2-Dibromoethane ND H
5.9 2.7 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Isopropylbenzene ND H
29 6.9 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Methyl acetate ND H
5.9 4.3 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Methyl tert-butyl ether ND H
5.9 2.5 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Methylcyclohexane ND H
5.9 2.8 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Methylene Chloride ND H
5.9 1.6 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Styrene ND H
5.9 2.3 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Tetrachloroethene ND H
5.9 2.0 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Toluene ND H
5.9 3.0 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼trans-1,2-Dichloroethene ND H
5.9 2.0 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼trans-1,3-Dichloropropene ND H
5.9 1.8 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Trichloroethene ND H
5.9 1.7 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Trichlorofluoromethane ND H
12 5.1 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Xylenes, Total ND H
5.9 4.3 ug/Kg 03/29/18 09:21 03/30/18 16:13 1☼Vinyl chloride ND H
1,2-Dichloroethane-d4 (Surr)99 62 -118 03/29/18 09:21 03/30/18 16:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 03/29/18 09:21 03/30/18 16:13 176-111
Dibromofluoromethane (Surr)99 03/29/18 09:21 03/30/18 16:13 172-116
Toluene-d8 (Surr)110 03/29/18 09:21 03/30/18 16:13 180-129
General Chemistry
RL MDL
Percent Moisture 21.1 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 78.9
TestAmerica Pittsburgh
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-6Client Sample ID: AH-06-0318-G2
Matrix: SedimentDate Collected: 03/27/18 09:22
Percent Solids: 75.6Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 6.7 3.3 ug/Kg ☼03/29/18 09:21 03/30/18 16:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.7 4.0 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,1,2,2-Tetrachloroethane ND
6.7 2.5 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
6.7 3.2 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,1,2-Trichloroethane ND
6.7 2.4 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,1-Dichloroethane ND
6.7 3.8 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,1-Dichloroethene ND
6.7 2.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,2,4-Trichlorobenzene ND
6.7 4.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,2-Dibromo-3-Chloropropane ND
6.7 5.4 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,2-Dichlorobenzene ND
6.7 1.9 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,2-Dichloroethane ND
6.7 3.3 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,2-Dichloropropane ND
6.7 2.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,3-Dichlorobenzene ND
6.7 1.4 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,4-Dichlorobenzene ND
6.7 3.9 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼2-Butanone (MEK)ND
6.7 5.6 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼2-Hexanone ND
6.7 2.5 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼4-Methyl-2-pentanone (MIBK)ND
27 4.2 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Acetone ND
6.7 2.6 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Benzene ND
6.7 3.5 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Bromoform ND
6.7 6.0 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Bromomethane ND
6.7 4.0 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Carbon disulfide ND
6.7 4.4 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Carbon tetrachloride ND
6.7 2.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Chlorobenzene ND
6.7 3.2 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Chlorodibromomethane ND
6.7 2.8 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Chloroform ND
6.7 5.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Chloromethane ND
6.7 3.4 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Chloroethane ND
6.7 2.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼cis-1,2-Dichloroethene ND
6.7 2.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼cis-1,3-Dichloropropene ND
6.7 1.6 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Cyclohexane ND
6.7 3.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Dichlorobromomethane ND
6.7 3.9 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Dichlorodifluoromethane ND
6.7 2.9 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Ethylbenzene ND
6.7 3.6 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼1,2-Dibromoethane ND
6.7 3.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Isopropylbenzene ND
33 7.9 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Methyl acetate ND
6.7 4.9 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Methyl tert-butyl ether ND
6.7 2.8 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Methylcyclohexane ND
6.7 3.1 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Methylene Chloride ND
6.7 1.8 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Styrene ND
6.7 2.7 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Tetrachloroethene ND
6.7 2.2 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Toluene ND
6.7 3.4 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼trans-1,2-Dichloroethene ND
6.7 2.3 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼trans-1,3-Dichloropropene ND
6.7 2.0 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Trichloroethene ND
6.7 1.9 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Trichlorofluoromethane ND
13 5.7 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Xylenes, Total ND
6.7 4.9 ug/Kg 03/29/18 09:21 03/30/18 16:36 1☼Vinyl chloride ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-6Client Sample ID: AH-06-0318-G2
Matrix: SedimentDate Collected: 03/27/18 09:22
Percent Solids: 75.6Date Received: 03/28/18 11:36
1,2-Dichloroethane-d4 (Surr)94 62 -118 03/29/18 09:21 03/30/18 16:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 03/29/18 09:21 03/30/18 16:36 176-111
Dibromofluoromethane (Surr)98 03/29/18 09:21 03/30/18 16:36 172-116
Toluene-d8 (Surr)108 03/29/18 09:21 03/30/18 16:36 180-129
General Chemistry
RL MDL
Percent Moisture 24.4 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 75.6
Lab Sample ID: 180-76196-7Client Sample ID: AH-06-0318-G3
Matrix: SedimentDate Collected: 03/27/18 09:25
Percent Solids: 79.3Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 6.3 3.2 ug/Kg ☼03/29/18 09:21 03/30/18 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.3 3.8 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,1,2,2-Tetrachloroethane ND
6.3 2.4 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
6.3 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,1,2-Trichloroethane ND
6.3 2.3 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,1-Dichloroethane ND
6.3 3.6 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,1-Dichloroethene ND
6.3 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,2,4-Trichlorobenzene ND
6.3 3.9 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,2-Dibromo-3-Chloropropane ND
6.3 5.1 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,2-Dichlorobenzene ND
6.3 1.8 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,2-Dichloroethane ND
6.3 3.1 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,2-Dichloropropane ND
6.3 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,3-Dichlorobenzene ND
6.3 1.3 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,4-Dichlorobenzene ND
6.3 3.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼2-Butanone (MEK)ND
6.3 5.3 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼2-Hexanone ND
6.3 2.4 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼4-Methyl-2-pentanone (MIBK)ND
25 4.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Acetone ND
6.3 2.5 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Benzene ND
6.3 3.3 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Bromoform ND
6.3 5.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Bromomethane ND
6.3 3.8 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Carbon disulfide ND
6.3 4.2 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Carbon tetrachloride ND
6.3 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Chlorobenzene ND
6.3 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Chlorodibromomethane ND
6.3 2.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Chloroform ND
6.3 4.9 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Chloromethane ND
6.3 3.3 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Chloroethane ND
6.3 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼cis-1,2-Dichloroethene ND
6.3 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼cis-1,3-Dichloropropene ND
6.3 1.5 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Cyclohexane ND
6.3 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Dichlorobromomethane ND
6.3 3.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Dichlorodifluoromethane ND
6.3 2.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Ethylbenzene ND
6.3 3.5 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼1,2-Dibromoethane ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-7Client Sample ID: AH-06-0318-G3
Matrix: SedimentDate Collected: 03/27/18 09:25
Percent Solids: 79.3Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Isopropylbenzene ND 6.3 2.9 ug/Kg ☼03/29/18 09:21 03/30/18 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
32 7.5 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Methyl acetate ND
6.3 4.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Methyl tert-butyl ether ND
6.3 2.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Methylcyclohexane ND
6.3 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Methylene Chloride ND
6.3 1.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Styrene ND
6.3 2.5 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Tetrachloroethene ND
6.3 2.1 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Toluene ND
6.3 3.2 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼trans-1,2-Dichloroethene ND
6.3 2.2 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼trans-1,3-Dichloropropene ND
6.3 1.9 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Trichloroethene ND
6.3 1.8 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Trichlorofluoromethane ND
13 5.5 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Xylenes, Total ND
6.3 4.7 ug/Kg 03/29/18 09:21 03/30/18 17:00 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)94 62 -118 03/29/18 09:21 03/30/18 17:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 03/29/18 09:21 03/30/18 17:00 176-111
Dibromofluoromethane (Surr)95 03/29/18 09:21 03/30/18 17:00 172-116
Toluene-d8 (Surr)108 03/29/18 09:21 03/30/18 17:00 180-129
General Chemistry
RL MDL
Percent Moisture 20.7 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 79.3
Lab Sample ID: 180-76196-8Client Sample ID: AH-06-0318-C
Matrix: SedimentDate Collected: 03/27/18 09:30
Percent Solids: 81.5Date Received: 03/28/18 11:36
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene ND 8.1 2.3 ug/Kg ☼04/02/18 03:39 04/05/18 18:34 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
8.1 1.8 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Acenaphthylene ND
8.1 2.1 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Anthracene ND
8.1 1.5 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Benzo[a]anthracene 1.7 J
8.1 1.8 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Benzo[a]pyrene ND
8.1 2.0 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Benzo[b]fluoranthene 2.5 J
8.1 1.7 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Benzo[g,h,i]perylene ND
8.1 1.6 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Chrysene 1.8 J
8.1 1.8 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Dibenz(a,h)anthracene ND
8.1 2.1 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Fluoranthene ND
8.1 1.6 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Fluorene ND
8.1 1.6 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Indeno[1,2,3-cd]pyrene ND
8.1 1.6 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Naphthalene ND
8.1 2.2 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Phenanthrene ND
8.1 1.9 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Pyrene 1.9 J
8.1 2.4 ug/Kg 04/02/18 03:39 04/05/18 18:34 2☼Benzo[k]fluoranthene ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-8Client Sample ID: AH-06-0318-C
Matrix: SedimentDate Collected: 03/27/18 09:30
Percent Solids: 81.5Date Received: 03/28/18 11:36
2-Fluorobiphenyl 76 34 -100 04/02/18 03:39 04/05/18 18:34 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)82 04/02/18 03:39 04/05/18 18:34 233-100
Terphenyl-d14 (Surr)79 04/02/18 03:39 04/05/18 18:34 230-100
Method: 8081B_LL - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND F1 0.050 0.016 ug/Kg ☼04/02/18 03:41 04/16/18 14:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.050 0.012 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼alpha-BHC ND F1
0.050 0.013 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼cis-Chlordane ND F1
0.050 0.013 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼beta-BHC ND F1
0.50 0.22 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Chlordane (technical)ND
0.050 0.014 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼4,4'-DDD ND F1
0.050 0.010 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼4,4'-DDE 0.016 J F1
0.050 0.019 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼4,4'-DDT ND
0.050 0.016 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼delta-BHC ND
0.050 0.013 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Dieldrin ND F1
0.050 0.014 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Endosulfan I ND F1
0.050 0.011 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Endosulfan II ND F1
0.050 0.013 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Endosulfan sulfate ND F1
0.050 0.020 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Endrin ND F1
0.050 0.018 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Endrin aldehyde 0.018 J F1 p
0.050 0.018 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Endrin ketone ND F1
0.050 0.017 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼gamma-BHC (Lindane)ND F1
0.050 0.012 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼trans-Chlordane ND F1
0.050 0.016 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Heptachlor ND F1
0.050 0.013 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Heptachlor epoxide ND F1
0.050 0.020 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Methoxychlor ND
0.050 0.011 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼oxy-Chlordane 0.011 J p
2.0 1.4 ug/Kg 04/02/18 03:41 04/16/18 14:10 1☼Toxaphene ND
DCB Decachlorobiphenyl (Surr)60 33 -137 04/02/18 03:41 04/16/18 14:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr)62 04/02/18 03:41 04/16/18 14:10 133-137
Tetrachloro-m-xylene 61 04/02/18 03:41 04/16/18 14:10 126-120
Tetrachloro-m-xylene 69 04/02/18 03:41 04/16/18 14:10 126-120
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony ND 0.12 0.038 mg/Kg ☼04/09/18 16:04 04/11/18 02:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.061 0.016 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Arsenic 1.4
0.061 0.0047 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Beryllium 0.092
0.061 0.010 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Cadmium ND
0.12 0.040 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Chromium 4.8
0.12 0.070 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Copper 1.8
0.061 0.022 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Lead 1.8
0.31 0.098 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Manganese 14
0.061 0.038 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Nickel 2.3
0.31 0.037 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Selenium 0.13 J
0.061 0.0086 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Silver ND
0.061 0.0080 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Thallium 0.019 J
0.31 0.20 mg/Kg 04/09/18 16:04 04/11/18 02:05 1☼Zinc 6.3
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.019 0.0043 mg/Kg ☼04/04/18 08:35 04/05/18 09:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Moisture 18.5 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 81.5
0.50 0.11 mg/Kg 04/12/18 11:38 1Cr (III)4.7
0.48 0.14 mg/Kg 03/29/18 14:32 03/30/18 13:19 1☼Cr (VI)0.19 J
200 100 mg/Kg 03/31/18 06:25 04/03/18 08:15 1☼Total Petroleum Hydrocarbons
(SGT-HEM)
ND
1200 920 mg/Kg 04/02/18 15:05 1☼Total Organic Carbon - Duplicates 2100
Lab Sample ID: 180-76196-9Client Sample ID: AH-02-0318-G1
Matrix: SedimentDate Collected: 03/27/18 09:55
Percent Solids: 78.4Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 6.2 3.1 ug/Kg ☼03/29/18 09:21 03/30/18 17:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.2 3.7 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,1,2,2-Tetrachloroethane ND
6.2 2.4 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
6.2 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,1,2-Trichloroethane ND
6.2 2.2 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,1-Dichloroethane ND
6.2 3.5 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,1-Dichloroethene ND
6.2 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,2,4-Trichlorobenzene ND
6.2 3.8 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,2-Dibromo-3-Chloropropane ND
6.2 5.0 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,2-Dichlorobenzene ND
6.2 1.8 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,2-Dichloroethane ND
6.2 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,2-Dichloropropane ND
6.2 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,3-Dichlorobenzene ND
6.2 1.3 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,4-Dichlorobenzene ND
6.2 3.6 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼2-Butanone (MEK)ND
6.2 5.2 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼2-Hexanone ND
6.2 2.3 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼4-Methyl-2-pentanone (MIBK)ND
25 3.9 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Acetone ND
6.2 2.4 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Benzene ND
6.2 3.2 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Bromoform ND
6.2 5.5 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Bromomethane ND
6.2 3.7 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Carbon disulfide ND
6.2 4.1 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Carbon tetrachloride ND
6.2 1.9 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Chlorobenzene ND
6.2 3.0 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Chlorodibromomethane ND
6.2 2.6 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Chloroform ND
6.2 4.7 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Chloromethane ND
6.2 3.2 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Chloroethane ND
6.2 1.9 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼cis-1,2-Dichloroethene ND
6.2 2.0 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼cis-1,3-Dichloropropene ND
6.2 1.5 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Cyclohexane ND
6.2 2.9 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Dichlorobromomethane ND
6.2 3.6 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Dichlorodifluoromethane ND
6.2 2.7 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Ethylbenzene ND
6.2 3.4 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼1,2-Dibromoethane ND
6.2 2.9 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Isopropylbenzene ND
31 7.3 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Methyl acetate ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-9Client Sample ID: AH-02-0318-G1
Matrix: SedimentDate Collected: 03/27/18 09:55
Percent Solids: 78.4Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl tert-butyl ether ND 6.2 4.5 ug/Kg ☼03/29/18 09:21 03/30/18 17:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.2 2.6 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Methylcyclohexane ND
6.2 2.9 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Methylene Chloride ND
6.2 1.6 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Styrene ND
6.2 2.5 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Tetrachloroethene ND
6.2 2.1 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Toluene ND
6.2 3.1 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼trans-1,2-Dichloroethene ND
6.2 2.1 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼trans-1,3-Dichloropropene ND
6.2 1.9 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Trichloroethene ND
6.2 1.8 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Trichlorofluoromethane ND
12 5.3 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Xylenes, Total ND
6.2 4.5 ug/Kg 03/29/18 09:21 03/30/18 17:47 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)96 62 -118 03/29/18 09:21 03/30/18 17:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 03/29/18 09:21 03/30/18 17:47 176-111
Dibromofluoromethane (Surr)98 03/29/18 09:21 03/30/18 17:47 172-116
Toluene-d8 (Surr)111 03/29/18 09:21 03/30/18 17:47 180-129
General Chemistry
RL MDL
Percent Moisture 21.6 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 78.4
Lab Sample ID: 180-76196-10Client Sample ID: AH-02-0318-G2
Matrix: SedimentDate Collected: 03/27/18 09:57
Percent Solids: 59.7Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 7.9 3.9 ug/Kg ☼03/29/18 09:21 03/30/18 18:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.9 4.7 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,1,2,2-Tetrachloroethane ND
7.9 3.0 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
7.9 3.8 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,1,2-Trichloroethane ND
7.9 2.8 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,1-Dichloroethane ND
7.9 4.5 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,1-Dichloroethene ND
7.9 2.5 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,2,4-Trichlorobenzene ND
7.9 4.8 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,2-Dibromo-3-Chloropropane ND
7.9 6.3 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,2-Dichlorobenzene ND
7.9 2.3 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,2-Dichloroethane ND
7.9 3.9 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,2-Dichloropropane ND
7.9 2.5 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,3-Dichlorobenzene ND
7.9 1.6 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,4-Dichlorobenzene ND
7.9 4.6 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼2-Butanone (MEK)ND
7.9 6.6 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼2-Hexanone ND
7.9 2.9 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼4-Methyl-2-pentanone (MIBK)ND
31 4.9 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Acetone ND
7.9 3.1 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Benzene ND
7.9 4.1 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Bromoform ND
7.9 7.1 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Bromomethane ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-10Client Sample ID: AH-02-0318-G2
Matrix: SedimentDate Collected: 03/27/18 09:57
Percent Solids: 59.7Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Carbon disulfide ND 7.9 4.7 ug/Kg ☼03/29/18 09:21 03/30/18 18:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.9 5.2 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Carbon tetrachloride ND
7.9 2.5 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Chlorobenzene ND
7.9 3.8 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Chlorodibromomethane ND
7.9 3.3 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Chloroform ND
7.9 6.1 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Chloromethane ND
7.9 4.1 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Chloroethane ND
7.9 2.5 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼cis-1,2-Dichloroethene ND
7.9 2.5 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼cis-1,3-Dichloropropene ND
7.9 1.9 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Cyclohexane ND
7.9 3.7 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Dichlorobromomethane ND
7.9 4.6 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Dichlorodifluoromethane ND
7.9 3.4 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Ethylbenzene ND
7.9 4.3 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼1,2-Dibromoethane ND
7.9 3.6 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Isopropylbenzene ND
39 9.3 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Methyl acetate ND
7.9 5.8 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Methyl tert-butyl ether ND
7.9 3.3 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Methylcyclohexane ND
7.9 3.7 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Methylene Chloride ND
7.9 2.1 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Styrene ND
7.9 3.1 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Tetrachloroethene ND
7.9 2.6 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Toluene ND
7.9 4.0 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼trans-1,2-Dichloroethene ND
7.9 2.7 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼trans-1,3-Dichloropropene ND
7.9 2.4 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Trichloroethene ND
7.9 2.3 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Trichlorofluoromethane ND
16 6.8 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Xylenes, Total ND
7.9 5.8 ug/Kg 03/29/18 09:21 03/30/18 18:10 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)93 62 -118 03/29/18 09:21 03/30/18 18:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)91 03/29/18 09:21 03/30/18 18:10 176-111
Dibromofluoromethane (Surr)99 03/29/18 09:21 03/30/18 18:10 172-116
Toluene-d8 (Surr)116 03/29/18 09:21 03/30/18 18:10 180-129
General Chemistry
RL MDL
Percent Moisture 40.3 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 59.7
Lab Sample ID: 180-76196-11Client Sample ID: AH-02-0318-G3
Matrix: SedimentDate Collected: 03/27/18 10:00
Percent Solids: 46.5Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 10 5.2 ug/Kg ☼03/29/18 09:21 04/02/18 10:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 6.2 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,1,2,2-Tetrachloroethane ND
10 4.0 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
10 5.0 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,1,2-Trichloroethane ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-11Client Sample ID: AH-02-0318-G3
Matrix: SedimentDate Collected: 03/27/18 10:00
Percent Solids: 46.5Date Received: 03/28/18 11:36
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1-Dichloroethane ND 10 3.7 ug/Kg ☼03/29/18 09:21 04/02/18 10:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 5.9 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,1-Dichloroethene ND
10 3.3 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,2,4-Trichlorobenzene ND
10 6.4 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,2-Dibromo-3-Chloropropane ND
10 8.3 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,2-Dichlorobenzene ND
10 3.0 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,2-Dichloroethane ND
10 5.1 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,2-Dichloropropane ND
10 3.3 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,3-Dichlorobenzene ND
10 2.1 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,4-Dichlorobenzene ND
10 6.0 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼2-Butanone (MEK)ND
10 8.7 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼2-Hexanone ND
10 3.8 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼4-Methyl-2-pentanone (MIBK)ND
41 6.5 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Acetone ND
10 4.1 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Benzene ND
10 5.4 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Bromoform ND
10 9.3 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Bromomethane ND
10 6.2 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Carbon disulfide ND
10 6.9 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Carbon tetrachloride ND
10 3.3 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Chlorobenzene ND
10 5.0 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Chlorodibromomethane ND
10 4.4 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Chloroform ND
10 8.0 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Chloromethane ND
10 5.4 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Chloroethane ND
10 3.3 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼cis-1,2-Dichloroethene ND
10 3.3 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼cis-1,3-Dichloropropene ND
10 2.5 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Cyclohexane ND
10 4.9 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Dichlorobromomethane ND
10 6.0 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Dichlorodifluoromethane ND
10 4.5 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Ethylbenzene ND
10 5.7 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼1,2-Dibromoethane ND
10 4.8 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Isopropylbenzene ND
52 12 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Methyl acetate ND
10 7.6 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Methyl tert-butyl ether ND
10 4.4 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Methylcyclohexane ND
10 4.9 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Methylene Chloride ND
10 2.8 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Styrene ND
10 4.1 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Tetrachloroethene ND
10 3.5 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Toluene 3.6 J
10 5.3 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼trans-1,2-Dichloroethene ND
10 3.6 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼trans-1,3-Dichloropropene ND
10 3.1 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Trichloroethene ND
10 3.0 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Trichlorofluoromethane ND
21 8.9 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Xylenes, Total ND
10 7.6 ug/Kg 03/29/18 09:21 04/02/18 10:27 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)96 62 -118 03/29/18 09:21 04/02/18 10:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 03/29/18 09:21 04/02/18 10:27 176-111
Dibromofluoromethane (Surr)99 03/29/18 09:21 04/02/18 10:27 172-116
Toluene-d8 (Surr)106 03/29/18 09:21 04/02/18 10:27 180-129
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
General Chemistry
RL MDL
Percent Moisture 53.5 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 46.5
Lab Sample ID: 180-76196-12Client Sample ID: AH-02-0318-C
Matrix: SedimentDate Collected: 03/27/18 10:05
Percent Solids: 57.2Date Received: 03/28/18 11:36
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene ND 23 6.7 ug/Kg ☼04/02/18 03:39 04/05/18 19:02 4
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
23 5.1 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Acenaphthylene ND
23 6.0 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Anthracene 26
23 4.4 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Benzo[a]anthracene 16 J
23 5.0 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Benzo[a]pyrene 16 J
23 5.7 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Benzo[b]fluoranthene 32
23 5.0 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Benzo[g,h,i]perylene 12 J
23 4.5 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Chrysene 28
23 5.2 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Dibenz(a,h)anthracene ND
23 6.1 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Fluoranthene 31
23 4.5 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Fluorene ND
23 4.7 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Indeno[1,2,3-cd]pyrene 8.9 J
23 4.5 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Naphthalene ND
23 6.2 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Phenanthrene 8.4 J
23 5.5 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Pyrene 25
23 6.9 ug/Kg 04/02/18 03:39 04/05/18 19:02 4☼Benzo[k]fluoranthene 13 J
2-Fluorobiphenyl 59 34 -100 04/02/18 03:39 04/05/18 19:02 4
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)69 04/02/18 03:39 04/05/18 19:02 433-100
Terphenyl-d14 (Surr)58 04/02/18 03:39 04/05/18 19:02 430-100
Method: 8081B_LL - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 0.36 0.11 ug/Kg ☼04/02/18 03:41 04/16/18 14:56 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.36 0.089 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼alpha-BHC ND
0.36 0.091 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼cis-Chlordane ND
0.36 0.093 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼beta-BHC ND
3.6 1.6 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Chlordane (technical)ND
0.36 0.098 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼4,4'-DDD 0.11 J
0.36 0.074 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼4,4'-DDE 0.23 J
0.36 0.14 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼4,4'-DDT ND
0.36 0.11 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼delta-BHC ND
0.36 0.091 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Dieldrin ND
0.36 0.098 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Endosulfan I ND
0.36 0.080 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Endosulfan II ND
0.36 0.094 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Endosulfan sulfate ND
0.36 0.14 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Endrin ND
0.36 0.13 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Endrin aldehyde ND
0.36 0.13 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Endrin ketone ND
0.36 0.12 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼gamma-BHC (Lindane)ND
0.36 0.084 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼trans-Chlordane ND
0.36 0.11 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Heptachlor ND
0.36 0.093 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Heptachlor epoxide ND
0.36 0.14 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Methoxychlor ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-12Client Sample ID: AH-02-0318-C
Matrix: SedimentDate Collected: 03/27/18 10:05
Percent Solids: 57.2Date Received: 03/28/18 11:36
Method: 8081B_LL - Organochlorine Pesticides (GC) (Continued)
RL MDL
oxy-Chlordane ND 0.36 0.081 ug/Kg ☼04/02/18 03:41 04/16/18 14:56 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 9.8 ug/Kg 04/02/18 03:41 04/16/18 14:56 5☼Toxaphene ND
DCB Decachlorobiphenyl (Surr)65 33 -137 04/02/18 03:41 04/16/18 14:56 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr)63 04/02/18 03:41 04/16/18 14:56 533-137
Tetrachloro-m-xylene 56 04/02/18 03:41 04/16/18 14:56 526-120
Tetrachloro-m-xylene 52 04/02/18 03:41 04/16/18 14:56 526-120
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony ND 0.18 0.056 mg/Kg ☼04/09/18 16:04 04/11/18 02:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.090 0.023 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Arsenic 4.5
0.090 0.0068 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Beryllium 0.37
0.090 0.015 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Cadmium 0.045 J
0.18 0.059 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Chromium 19
0.18 0.10 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Copper 6.9
0.090 0.032 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Lead 12
0.45 0.14 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Manganese 110
0.090 0.056 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Nickel 8.0
0.45 0.054 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Selenium 0.44 J
0.090 0.013 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Silver 0.024 J
0.090 0.012 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Thallium 0.11
0.45 0.30 mg/Kg 04/09/18 16:04 04/11/18 02:09 1☼Zinc 31
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.030 0.026 0.0059 mg/Kg ☼04/04/18 08:35 04/05/18 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Moisture 42.8 0.1 0.1 %03/29/18 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 11:32 1Percent Solids 57.2
0.50 0.11 mg/Kg 04/12/18 11:38 1Cr (III)19
0.69 0.19 mg/Kg 03/29/18 14:32 03/30/18 13:23 1☼Cr (VI)ND
290 140 mg/Kg 03/31/18 06:25 04/03/18 08:15 1☼Total Petroleum Hydrocarbons
(SGT-HEM)
ND
1700 1300 mg/Kg 04/02/18 15:15 1☼Total Organic Carbon - Duplicates 14000
Lab Sample ID: 180-76196-13Client Sample ID: AH-04-0318-G1
Matrix: SedimentDate Collected: 03/27/18 10:40
Percent Solids: 39.2Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 13 6.3 ug/Kg ☼03/28/18 12:15 03/28/18 14:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
13 7.5 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,1,2,2-Tetrachloroethane ND
13 4.8 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
13 6.1 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,1,2-Trichloroethane ND
13 4.6 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,1-Dichloroethane ND
13 7.2 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,1-Dichloroethene ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-13Client Sample ID: AH-04-0318-G1
Matrix: SedimentDate Collected: 03/27/18 10:40
Percent Solids: 39.2Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2,4-Trichlorobenzene ND 13 4.1 ug/Kg ☼03/28/18 12:15 03/28/18 14:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
13 7.8 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,2-Dibromo-3-Chloropropane ND
13 10 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,2-Dichlorobenzene ND
13 3.7 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,2-Dichloroethane ND
13 6.2 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,2-Dichloropropane ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,3-Dichlorobenzene ND
13 2.6 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,4-Dichlorobenzene ND
13 7.3 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼2-Butanone (MEK)ND
13 11 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼2-Hexanone ND
13 4.7 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼4-Methyl-2-pentanone (MIBK)ND
51 8.0 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Acetone ND
13 5.0 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Benzene ND
13 6.6 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Bromoform ND
13 11 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Bromomethane ND
13 7.6 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Carbon disulfide ND
13 8.4 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Carbon tetrachloride ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Chlorobenzene ND
13 6.1 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Chlorodibromomethane ND
13 5.3 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Chloroform ND
13 9.7 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Chloromethane ND
13 6.5 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Chloroethane ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼cis-1,2-Dichloroethene ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼cis-1,3-Dichloropropene ND
13 3.1 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Cyclohexane ND
13 6.0 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Dichlorobromomethane ND
13 7.4 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Dichlorodifluoromethane ND
13 5.4 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Ethylbenzene ND
13 6.9 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼1,2-Dibromoethane ND
13 5.9 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Isopropylbenzene ND
63 15 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Methyl acetate ND
13 9.3 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Methyl tert-butyl ether ND
13 5.3 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Methylcyclohexane ND
13 6.0 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Methylene Chloride 7.5 J
13 3.4 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Styrene ND
13 5.1 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Tetrachloroethene ND
13 4.3 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Toluene ND
13 6.4 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼trans-1,2-Dichloroethene ND
13 4.4 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼trans-1,3-Dichloropropene ND
13 3.8 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Trichloroethene ND
13 3.7 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Trichlorofluoromethane ND
25 11 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Xylenes, Total ND
13 9.3 ug/Kg 03/28/18 12:15 03/28/18 14:17 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)93 62 -118 03/28/18 12:15 03/28/18 14:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 03/28/18 12:15 03/28/18 14:17 176-111
Dibromofluoromethane (Surr)99 03/28/18 12:15 03/28/18 14:17 172-116
Toluene-d8 (Surr)113 03/28/18 12:15 03/28/18 14:17 180-129
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-13Client Sample ID: AH-04-0318-G1
Matrix: SedimentDate Collected: 03/27/18 10:40
Percent Solids: 39.2Date Received: 03/28/18 09:30
General Chemistry
RL MDL
Percent Moisture 60.8 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 39.2
Lab Sample ID: 180-76196-14Client Sample ID: AH-04-0318-G2
Matrix: SedimentDate Collected: 03/27/18 10:42
Percent Solids: 39.1Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 13 6.3 ug/Kg ☼03/28/18 12:15 03/28/18 14:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
13 7.5 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,1,2,2-Tetrachloroethane ND
13 4.8 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
13 6.0 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,1,2-Trichloroethane ND
13 4.5 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,1-Dichloroethane ND
13 7.2 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,1-Dichloroethene ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,2,4-Trichlorobenzene ND
13 7.7 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,2-Dibromo-3-Chloropropane ND
13 10 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,2-Dichlorobenzene ND
13 3.6 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,2-Dichloroethane ND
13 6.2 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,2-Dichloropropane ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,3-Dichlorobenzene ND
13 2.6 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,4-Dichlorobenzene ND
13 7.3 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼2-Butanone (MEK)ND
13 11 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼2-Hexanone ND
13 4.7 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼4-Methyl-2-pentanone (MIBK)ND
50 7.9 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Acetone 13 J
13 4.9 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Benzene ND
13 6.6 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Bromoform ND
13 11 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Bromomethane ND
13 7.6 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Carbon disulfide ND
13 8.3 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Carbon tetrachloride ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Chlorobenzene ND
13 6.0 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Chlorodibromomethane ND
13 5.3 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Chloroform ND
13 9.7 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Chloromethane ND
13 6.5 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Chloroethane ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼cis-1,2-Dichloroethene ND
13 4.0 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼cis-1,3-Dichloropropene ND
13 3.1 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Cyclohexane ND
13 5.9 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Dichlorobromomethane ND
13 7.3 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Dichlorodifluoromethane ND
13 5.4 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Ethylbenzene ND
13 6.9 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼1,2-Dibromoethane ND
13 5.8 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Isopropylbenzene ND
63 15 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Methyl acetate ND
13 9.2 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Methyl tert-butyl ether ND
13 5.3 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Methylcyclohexane ND
13 5.9 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Methylene Chloride 7.1 J
13 3.3 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Styrene ND
13 5.0 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Tetrachloroethene ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-14Client Sample ID: AH-04-0318-G2
Matrix: SedimentDate Collected: 03/27/18 10:42
Percent Solids: 39.1Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Toluene ND 13 4.2 ug/Kg ☼03/28/18 12:15 03/28/18 14:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
13 6.4 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼trans-1,2-Dichloroethene ND
13 4.3 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼trans-1,3-Dichloropropene ND
13 3.8 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Trichloroethene ND
13 3.7 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Trichlorofluoromethane ND
25 11 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Xylenes, Total ND
13 9.2 ug/Kg 03/28/18 12:15 03/28/18 14:41 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)95 62 -118 03/28/18 12:15 03/28/18 14:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)90 03/28/18 12:15 03/28/18 14:41 176-111
Dibromofluoromethane (Surr)98 03/28/18 12:15 03/28/18 14:41 172-116
Toluene-d8 (Surr)112 03/28/18 12:15 03/28/18 14:41 180-129
General Chemistry
RL MDL
Percent Moisture 60.9 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 39.1
Lab Sample ID: 180-76196-15Client Sample ID: AH-04-0318-G3
Matrix: SedimentDate Collected: 03/27/18 10:45
Percent Solids: 46.9Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 10 5.3 ug/Kg ☼03/28/18 12:15 03/28/18 15:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 6.3 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,1,2,2-Tetrachloroethane ND
10 4.0 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
10 5.0 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,1,2-Trichloroethane ND
10 3.8 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,1-Dichloroethane ND
10 6.0 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,1-Dichloroethene ND
10 3.4 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,2,4-Trichlorobenzene ND
10 6.4 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,2-Dibromo-3-Chloropropane ND
10 8.4 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,2-Dichlorobenzene ND
10 3.0 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,2-Dichloroethane ND
10 5.1 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,2-Dichloropropane ND
10 3.3 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,3-Dichlorobenzene ND
10 2.1 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,4-Dichlorobenzene ND
10 6.1 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼2-Butanone (MEK)ND
10 8.8 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼2-Hexanone ND
10 3.9 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼4-Methyl-2-pentanone (MIBK)ND
42 6.6 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Acetone ND
10 4.1 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Benzene ND
10 5.5 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Bromoform ND
10 9.4 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Bromomethane ND
10 6.3 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Carbon disulfide ND
10 7.0 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Carbon tetrachloride ND
10 3.3 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Chlorobenzene ND
10 5.0 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Chlorodibromomethane ND
10 4.4 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Chloroform ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-15Client Sample ID: AH-04-0318-G3
Matrix: SedimentDate Collected: 03/27/18 10:45
Percent Solids: 46.9Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Chloromethane ND 10 8.1 ug/Kg ☼03/28/18 12:15 03/28/18 15:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 5.4 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Chloroethane ND
10 3.3 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼cis-1,2-Dichloroethene ND
10 3.3 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼cis-1,3-Dichloropropene ND
10 2.6 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Cyclohexane ND
10 4.9 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Dichlorobromomethane ND
10 6.1 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Dichlorodifluoromethane ND
10 4.5 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Ethylbenzene ND
10 5.7 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼1,2-Dibromoethane ND
10 4.9 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Isopropylbenzene ND
52 12 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Methyl acetate ND
10 7.7 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Methyl tert-butyl ether ND
10 4.4 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Methylcyclohexane ND
10 4.9 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Methylene Chloride 5.6 J
10 2.8 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Styrene ND
10 4.2 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Tetrachloroethene ND
10 3.5 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Toluene ND
10 5.3 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼trans-1,2-Dichloroethene ND
10 3.6 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼trans-1,3-Dichloropropene ND
10 3.1 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Trichloroethene ND
10 3.1 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Trichlorofluoromethane ND
21 9.0 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Xylenes, Total ND
10 7.7 ug/Kg 03/28/18 12:15 03/28/18 15:04 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)94 62 -118 03/28/18 12:15 03/28/18 15:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)88 03/28/18 12:15 03/28/18 15:04 176-111
Dibromofluoromethane (Surr)102 03/28/18 12:15 03/28/18 15:04 172-116
Toluene-d8 (Surr)114 03/28/18 12:15 03/28/18 15:04 180-129
General Chemistry
RL MDL
Percent Moisture 53.1 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 46.9
Lab Sample ID: 180-76196-16Client Sample ID: AH-04-0318-C
Matrix: SedimentDate Collected: 03/27/18 10:50
Percent Solids: 41.2Date Received: 03/28/18 09:30
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene 14 J 40 12 ug/Kg ☼04/02/18 03:39 04/05/18 19:30 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
40 8.8 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Acenaphthylene 32 J
40 10 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Anthracene 50
40 7.6 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Benzo[a]anthracene 150
40 8.7 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Benzo[a]pyrene 130
40 9.9 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Benzo[b]fluoranthene 200
40 8.7 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Benzo[g,h,i]perylene 79
40 7.9 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Chrysene 150
40 9.0 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Dibenz(a,h)anthracene 25 J
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-16Client Sample ID: AH-04-0318-C
Matrix: SedimentDate Collected: 03/27/18 10:50
Percent Solids: 41.2Date Received: 03/28/18 09:30
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
RL MDL
Fluoranthene 400 40 11 ug/Kg ☼04/02/18 03:39 04/05/18 19:30 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
40 7.9 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Fluorene 15 J
40 8.1 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Indeno[1,2,3-cd]pyrene 74
40 7.8 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Naphthalene ND
40 11 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Phenanthrene 60
40 9.5 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Pyrene 310
40 12 ug/Kg 04/02/18 03:39 04/05/18 19:30 5☼Benzo[k]fluoranthene 68
2-Fluorobiphenyl 69 34 -100 04/02/18 03:39 04/05/18 19:30 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)77 04/02/18 03:39 04/05/18 19:30 533-100
Terphenyl-d14 (Surr)69 04/02/18 03:39 04/05/18 19:30 530-100
Method: 8081B_LL - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 0.50 0.16 ug/Kg ☼04/02/18 03:41 04/16/18 15:11 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.12 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼alpha-BHC ND
0.50 0.13 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼cis-Chlordane ND
0.50 0.13 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼beta-BHC ND
5.0 2.2 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Chlordane (technical)ND
0.50 0.14 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼4,4'-DDD 1.7
0.50 0.10 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼4,4'-DDE 1.5
0.50 0.19 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼4,4'-DDT 6.6
0.50 0.16 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼delta-BHC ND
0.50 0.13 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Dieldrin ND
0.50 0.14 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Endosulfan I ND
0.50 0.11 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Endosulfan II ND
0.50 0.13 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Endosulfan sulfate ND
0.50 0.20 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Endrin ND
0.50 0.18 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Endrin aldehyde ND
0.50 0.18 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Endrin ketone ND
0.50 0.17 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼gamma-BHC (Lindane)ND
0.50 0.12 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼trans-Chlordane 0.36 J
0.50 0.16 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Heptachlor ND
0.50 0.13 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Heptachlor epoxide ND
0.50 0.20 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Methoxychlor ND
0.50 0.11 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼oxy-Chlordane ND
20 14 ug/Kg 04/02/18 03:41 04/16/18 15:11 5☼Toxaphene ND
DCB Decachlorobiphenyl (Surr)80 33 -137 04/02/18 03:41 04/16/18 15:11 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr)76 04/02/18 03:41 04/16/18 15:11 533-137
Tetrachloro-m-xylene 69 04/02/18 03:41 04/16/18 15:11 526-120
Tetrachloro-m-xylene 62 04/02/18 03:41 04/16/18 15:11 526-120
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 0.075 J 0.24 0.075 mg/Kg ☼04/09/18 16:04 04/11/18 02:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.12 0.032 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Arsenic 7.8
0.12 0.0092 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Beryllium 0.58
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-16Client Sample ID: AH-04-0318-C
Matrix: SedimentDate Collected: 03/27/18 10:50
Percent Solids: 41.2Date Received: 03/28/18 09:30
Method: 6020B - Metals (ICP/MS) (Continued)
RL MDL
Cadmium 0.13 0.12 0.021 mg/Kg ☼04/09/18 16:04 04/11/18 02:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.24 0.080 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Chromium 30
0.24 0.14 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Copper 34
0.12 0.044 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Lead 23
0.61 0.19 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Manganese 150
0.12 0.075 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Nickel 12
0.61 0.073 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Selenium 0.74
0.12 0.017 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Silver 0.055 J
0.12 0.016 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Thallium 0.20
0.61 0.41 mg/Kg 04/09/18 16:04 04/11/18 02:14 1☼Zinc 80
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.059 0.036 0.0081 mg/Kg ☼04/04/18 08:35 04/05/18 09:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Moisture 58.8 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 41.2
0.50 0.11 mg/Kg 04/12/18 11:38 1Cr (III)30
0.96 0.27 mg/Kg 03/29/18 14:32 03/30/18 13:24 1☼Cr (VI)ND
400 200 mg/Kg 03/31/18 06:25 04/03/18 08:15 1☼Total Petroleum Hydrocarbons
(SGT-HEM)
310 J
2400 1800 mg/Kg 03/29/18 16:39 1☼Total Organic Carbon - Duplicates 24000
Lab Sample ID: 180-76196-17Client Sample ID: AH-05-0318-G1
Matrix: SedimentDate Collected: 03/27/18 11:35
Percent Solids: 25.9Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 19 9.5 ug/Kg ☼03/28/18 12:15 03/28/18 15:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,1,2,2-Tetrachloroethane ND
19 7.3 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
19 9.1 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,1,2-Trichloroethane ND
19 6.9 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,1-Dichloroethane ND
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,1-Dichloroethene ND
19 6.1 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,2,4-Trichlorobenzene ND
19 12 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,2-Dibromo-3-Chloropropane ND
19 15 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,2-Dichlorobenzene ND
19 5.5 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,2-Dichloroethane ND
19 9.3 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,2-Dichloropropane ND
19 6.1 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,3-Dichlorobenzene ND
19 3.9 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,4-Dichlorobenzene ND
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼2-Butanone (MEK)ND
19 16 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼2-Hexanone ND
19 7.1 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼4-Methyl-2-pentanone (MIBK)ND
76 12 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Acetone 27 J
19 7.5 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Benzene ND
19 9.9 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Bromoform ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-17Client Sample ID: AH-05-0318-G1
Matrix: SedimentDate Collected: 03/27/18 11:35
Percent Solids: 25.9Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Bromomethane ND 19 17 ug/Kg ☼03/28/18 12:15 03/28/18 15:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Carbon disulfide 11 J
19 13 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Carbon tetrachloride ND
19 6.0 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Chlorobenzene ND
19 9.1 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Chlorodibromomethane ND
19 8.0 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Chloroform ND
19 15 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Chloromethane ND
19 9.8 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Chloroethane ND
19 6.0 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼cis-1,2-Dichloroethene ND
19 6.1 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼cis-1,3-Dichloropropene ND
19 4.6 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Cyclohexane ND
19 9.0 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Dichlorobromomethane ND
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Dichlorodifluoromethane ND
19 8.2 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Ethylbenzene ND
19 10 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼1,2-Dibromoethane ND
19 8.8 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Isopropylbenzene ND
95 22 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Methyl acetate ND
19 14 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Methyl tert-butyl ether ND
19 8.0 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Methylcyclohexane ND
19 9.0 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Methylene Chloride 13 J
19 5.1 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Styrene ND
19 7.6 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Tetrachloroethene ND
19 6.4 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Toluene ND
19 9.6 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼trans-1,2-Dichloroethene ND
19 6.6 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼trans-1,3-Dichloropropene ND
19 5.7 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Trichloroethene ND
19 5.5 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Trichlorofluoromethane ND
38 16 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Xylenes, Total ND
19 14 ug/Kg 03/28/18 12:15 03/28/18 15:28 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)93 62 -118 03/28/18 12:15 03/28/18 15:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)90 03/28/18 12:15 03/28/18 15:28 176-111
Dibromofluoromethane (Surr)102 03/28/18 12:15 03/28/18 15:28 172-116
Toluene-d8 (Surr)117 03/28/18 12:15 03/28/18 15:28 180-129
General Chemistry
RL MDL
Percent Moisture 74.1 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 25.9
Lab Sample ID: 180-76196-18Client Sample ID: AH-05-0318-G1-DUP
Matrix: SedimentDate Collected: 03/27/18 11:37
Percent Solids: 24.2Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 19 9.5 ug/Kg ☼03/28/18 12:15 03/28/18 15:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,1,2,2-Tetrachloroethane ND
19 7.2 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-18Client Sample ID: AH-05-0318-G1-DUP
Matrix: SedimentDate Collected: 03/27/18 11:37
Percent Solids: 24.2Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,2-Trichloroethane ND 19 9.1 ug/Kg ☼03/28/18 12:15 03/28/18 15:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
19 6.9 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,1-Dichloroethane ND
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,1-Dichloroethene ND
19 6.1 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,2,4-Trichlorobenzene ND
19 12 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,2-Dibromo-3-Chloropropane ND
19 15 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,2-Dichlorobenzene ND
19 5.5 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,2-Dichloroethane ND
19 9.3 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,2-Dichloropropane ND
19 6.0 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,3-Dichlorobenzene ND
19 3.9 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,4-Dichlorobenzene ND
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼2-Butanone (MEK)ND
19 16 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼2-Hexanone ND
19 7.0 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼4-Methyl-2-pentanone (MIBK)ND
76 12 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Acetone ND
19 7.4 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Benzene ND
19 9.9 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Bromoform ND
19 17 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Bromomethane ND
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Carbon disulfide ND
19 13 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Carbon tetrachloride ND
19 6.0 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Chlorobenzene ND
19 9.1 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Chlorodibromomethane ND
19 8.0 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Chloroform ND
19 15 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Chloromethane ND
19 9.8 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Chloroethane ND
19 6.0 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼cis-1,2-Dichloroethene ND
19 6.1 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼cis-1,3-Dichloropropene ND
19 4.6 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Cyclohexane ND
19 8.9 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Dichlorobromomethane ND
19 11 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Dichlorodifluoromethane ND
19 8.2 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Ethylbenzene ND
19 10 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼1,2-Dibromoethane ND
19 8.8 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Isopropylbenzene ND
95 22 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Methyl acetate ND
19 14 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Methyl tert-butyl ether ND
19 8.0 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Methylcyclohexane ND
19 9.0 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Methylene Chloride 10 J
19 5.1 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Styrene ND
19 7.6 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Tetrachloroethene ND
19 6.4 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Toluene ND
19 9.6 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼trans-1,2-Dichloroethene ND
19 6.6 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼trans-1,3-Dichloropropene ND
19 5.7 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Trichloroethene ND
19 5.5 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Trichlorofluoromethane ND
38 16 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Xylenes, Total ND
19 14 ug/Kg 03/28/18 12:15 03/28/18 15:51 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)93 62 -118 03/28/18 12:15 03/28/18 15:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)91 03/28/18 12:15 03/28/18 15:51 176-111
Dibromofluoromethane (Surr)99 03/28/18 12:15 03/28/18 15:51 172-116
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-18Client Sample ID: AH-05-0318-G1-DUP
Matrix: SedimentDate Collected: 03/27/18 11:37
Percent Solids: 24.2Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Toluene-d8 (Surr)114 80 -129 03/28/18 12:15 03/28/18 15:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL MDL
Percent Moisture 75.8 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 24.2
Lab Sample ID: 180-76196-19Client Sample ID: AH-05-0318-G2
Matrix: SedimentDate Collected: 03/27/18 11:40
Percent Solids: 28.4Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 17 8.4 ug/Kg ☼03/28/18 12:15 03/28/18 16:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
17 10 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,1,2,2-Tetrachloroethane ND
17 6.4 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
17 8.1 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,1,2-Trichloroethane ND
17 6.1 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,1-Dichloroethane ND
17 9.6 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,1-Dichloroethene ND
17 5.4 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,2,4-Trichlorobenzene ND
17 10 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,2-Dibromo-3-Chloropropane ND
17 14 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,2-Dichlorobenzene ND
17 4.9 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,2-Dichloroethane ND
17 8.2 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,2-Dichloropropane ND
17 5.4 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,3-Dichlorobenzene ND
17 3.4 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,4-Dichlorobenzene ND
17 9.7 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼2-Butanone (MEK)ND
17 14 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼2-Hexanone ND
17 6.2 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼4-Methyl-2-pentanone (MIBK)ND
67 11 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Acetone 16 J
17 6.6 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Benzene ND
17 8.8 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Bromoform ND
17 15 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Bromomethane ND
17 10 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Carbon disulfide ND
17 11 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Carbon tetrachloride ND
17 5.3 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Chlorobenzene ND
17 8.1 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Chlorodibromomethane ND
17 7.1 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Chloroform ND
17 13 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Chloromethane ND
17 8.7 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Chloroethane ND
17 5.3 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼cis-1,2-Dichloroethene ND
17 5.4 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼cis-1,3-Dichloropropene ND
17 4.1 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Cyclohexane ND
17 7.9 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Dichlorobromomethane ND
17 9.8 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Dichlorodifluoromethane ND
17 7.2 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Ethylbenzene ND
17 9.2 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼1,2-Dibromoethane ND
17 7.8 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Isopropylbenzene ND
84 20 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Methyl acetate ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-19Client Sample ID: AH-05-0318-G2
Matrix: SedimentDate Collected: 03/27/18 11:40
Percent Solids: 28.4Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl tert-butyl ether ND 17 12 ug/Kg ☼03/28/18 12:15 03/28/18 16:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
17 7.1 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Methylcyclohexane ND
17 7.9 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Methylene Chloride 8.3 J
17 4.5 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Styrene ND
17 6.7 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Tetrachloroethene ND
17 5.7 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Toluene ND
17 8.5 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼trans-1,2-Dichloroethene ND
17 5.8 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼trans-1,3-Dichloropropene ND
17 5.1 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Trichloroethene ND
17 4.9 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Trichlorofluoromethane ND
34 14 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Xylenes, Total ND
17 12 ug/Kg 03/28/18 12:15 03/28/18 16:14 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)93 62 -118 03/28/18 12:15 03/28/18 16:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)89 03/28/18 12:15 03/28/18 16:14 176-111
Dibromofluoromethane (Surr)97 03/28/18 12:15 03/28/18 16:14 172-116
Toluene-d8 (Surr)110 03/28/18 12:15 03/28/18 16:14 180-129
General Chemistry
RL MDL
Percent Moisture 71.6 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 28.4
Lab Sample ID: 180-76196-20Client Sample ID: AH-05-0318-G3
Matrix: SedimentDate Collected: 03/27/18 11:45
Percent Solids: 16.8Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 30 15 ug/Kg ☼03/28/18 12:15 03/28/18 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
30 18 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,1,2,2-Tetrachloroethane ND
30 11 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
30 14 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,1,2-Trichloroethane ND
30 11 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,1-Dichloroethane ND
30 17 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,1-Dichloroethene ND
30 9.7 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,2,4-Trichlorobenzene ND
30 18 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,2-Dibromo-3-Chloropropane ND
30 24 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,2-Dichlorobenzene ND
30 8.7 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,2-Dichloroethane ND
30 15 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,2-Dichloropropane ND
30 9.6 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,3-Dichlorobenzene ND
30 6.1 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,4-Dichlorobenzene ND
30 17 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼2-Butanone (MEK)ND
30 25 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼2-Hexanone ND
30 11 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼4-Methyl-2-pentanone (MIBK)ND
120 19 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Acetone ND
30 12 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Benzene ND
30 16 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Bromoform ND
30 27 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Bromomethane ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-20Client Sample ID: AH-05-0318-G3
Matrix: SedimentDate Collected: 03/27/18 11:45
Percent Solids: 16.8Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Carbon disulfide ND 30 18 ug/Kg ☼03/28/18 12:15 03/28/18 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
30 20 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Carbon tetrachloride ND
30 9.4 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Chlorobenzene ND
30 14 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Chlorodibromomethane ND
30 13 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Chloroform ND
30 23 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Chloromethane ND
30 15 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Chloroethane ND
30 9.4 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼cis-1,2-Dichloroethene ND
30 9.6 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼cis-1,3-Dichloropropene ND
30 7.3 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Cyclohexane ND
30 14 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Dichlorobromomethane ND
30 17 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Dichlorodifluoromethane ND
30 13 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Ethylbenzene ND
30 16 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼1,2-Dibromoethane ND
30 14 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Isopropylbenzene ND
150 35 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Methyl acetate ND
30 22 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Methyl tert-butyl ether ND
30 13 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Methylcyclohexane ND
30 14 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Methylene Chloride 15 J
30 8.0 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Styrene ND
30 12 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Tetrachloroethene ND
30 10 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Toluene ND
30 15 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼trans-1,2-Dichloroethene ND
30 10 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼trans-1,3-Dichloropropene ND
30 9.0 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Trichloroethene ND
30 8.7 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Trichlorofluoromethane ND
60 26 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Xylenes, Total ND
30 22 ug/Kg 03/28/18 12:15 03/28/18 16:38 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)94 62 -118 03/28/18 12:15 03/28/18 16:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)82 03/28/18 12:15 03/28/18 16:38 176-111
Dibromofluoromethane (Surr)103 03/28/18 12:15 03/28/18 16:38 172-116
Toluene-d8 (Surr)118 03/28/18 12:15 03/28/18 16:38 180-129
General Chemistry
RL MDL
Percent Moisture 83.2 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 16.8
Lab Sample ID: 180-76196-21Client Sample ID: AH-05-0318-C
Matrix: SedimentDate Collected: 03/27/18 11:55
Percent Solids: 24.0Date Received: 03/28/18 09:30
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene ND 69 20 ug/Kg ☼04/02/18 03:39 04/05/18 19:58 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
69 15 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Acenaphthylene 52 J
69 18 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Anthracene 53 J
69 13 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Benzo[a]anthracene 130
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-21Client Sample ID: AH-05-0318-C
Matrix: SedimentDate Collected: 03/27/18 11:55
Percent Solids: 24.0Date Received: 03/28/18 09:30
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
RL MDL
Benzo[a]pyrene 150 69 15 ug/Kg ☼04/02/18 03:39 04/05/18 19:58 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
69 17 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Benzo[b]fluoranthene 290
69 15 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Benzo[g,h,i]perylene 90
69 13 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Chrysene 120
69 15 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Dibenz(a,h)anthracene 23 J
69 18 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Fluoranthene 160
69 13 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Fluorene ND
69 14 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Indeno[1,2,3-cd]pyrene 85
69 13 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Naphthalene ND
69 18 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Phenanthrene ND
69 16 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Pyrene 260
69 21 ug/Kg 04/02/18 03:39 04/05/18 19:58 5☼Benzo[k]fluoranthene 120
2-Fluorobiphenyl 58 34 -100 04/02/18 03:39 04/05/18 19:58 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)65 04/02/18 03:39 04/05/18 19:58 533-100
Terphenyl-d14 (Surr)56 04/02/18 03:39 04/05/18 19:58 530-100
Method: 8081B_LL - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 0.86 0.27 ug/Kg ☼04/02/18 03:41 04/16/18 15:27 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.86 0.21 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼alpha-BHC ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼cis-Chlordane ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼beta-BHC ND
8.6 3.7 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Chlordane (technical)ND
0.86 0.23 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼4,4'-DDD 1.8
0.86 0.18 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼4,4'-DDE 4.8
0.86 0.33 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼4,4'-DDT ND
0.86 0.27 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼delta-BHC ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Dieldrin ND
0.86 0.23 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Endosulfan I ND
0.86 0.19 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Endosulfan II ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Endosulfan sulfate ND
0.86 0.33 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Endrin ND
0.86 0.31 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Endrin aldehyde ND
0.86 0.31 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Endrin ketone ND
0.86 0.29 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼gamma-BHC (Lindane)ND
0.86 0.20 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼trans-Chlordane 0.58 J
0.86 0.27 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Heptachlor ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Heptachlor epoxide ND
0.86 0.33 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Methoxychlor 1.2
0.86 0.19 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼oxy-Chlordane ND
34 23 ug/Kg 04/02/18 03:41 04/16/18 15:27 5☼Toxaphene ND
DCB Decachlorobiphenyl (Surr)88 33 -137 04/02/18 03:41 04/16/18 15:27 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr)84 04/02/18 03:41 04/16/18 15:27 533-137
Tetrachloro-m-xylene 69 04/02/18 03:41 04/16/18 15:27 526-120
Tetrachloro-m-xylene 67 04/02/18 03:41 04/16/18 15:27 526-120
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-21Client Sample ID: AH-05-0318-C
Matrix: SedimentDate Collected: 03/27/18 11:55
Percent Solids: 24.0Date Received: 03/28/18 09:30
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony ND 0.41 0.13 mg/Kg ☼04/09/18 16:04 04/11/18 02:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.053 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Arsenic 10
0.20 0.016 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Beryllium 0.69
0.20 0.035 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Cadmium 0.33
0.41 0.14 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Chromium 38
0.41 0.23 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Copper 120
0.20 0.074 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Lead 34
1.0 0.33 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Manganese 160
0.20 0.13 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Nickel 15
1.0 0.12 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Selenium 1.1
0.20 0.029 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Silver 0.069 J
0.20 0.027 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Thallium 0.30
1.0 0.68 mg/Kg 04/09/18 16:04 04/11/18 02:19 1☼Zinc 170
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.11 0.068 0.015 mg/Kg ☼04/04/18 08:35 04/05/18 09:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Moisture 76.0 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 24.0
0.50 0.11 mg/Kg 04/12/18 11:38 1Cr (III)38
1.6 0.46 mg/Kg 03/29/18 14:32 03/30/18 13:30 1☼Cr (VI)ND
700 350 mg/Kg 03/31/18 06:25 04/03/18 08:15 1☼Total Petroleum Hydrocarbons
(SGT-HEM)
500 J
4200 3100 mg/Kg 03/29/18 16:49 1☼Total Organic Carbon - Duplicates 83000
Lab Sample ID: 180-76196-22Client Sample ID: AH-05-0318-C-DUP
Matrix: SedimentDate Collected: 03/27/18 11:58
Percent Solids: 23.9Date Received: 03/28/18 09:30
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene ND 56 16 ug/Kg ☼04/02/18 03:39 04/05/18 20:26 4
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
56 12 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Acenaphthylene 45 J
56 15 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Anthracene 40 J
56 11 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Benzo[a]anthracene 100
56 12 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Benzo[a]pyrene 110
56 14 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Benzo[b]fluoranthene 220
56 12 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Benzo[g,h,i]perylene 67
56 11 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Chrysene 110
56 12 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Dibenz(a,h)anthracene 16 J
56 15 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Fluoranthene 130
56 11 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Fluorene ND
56 11 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Indeno[1,2,3-cd]pyrene 61
56 11 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Naphthalene ND
56 15 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Phenanthrene ND
56 13 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Pyrene 220
56 17 ug/Kg 04/02/18 03:39 04/05/18 20:26 4☼Benzo[k]fluoranthene 98
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-22Client Sample ID: AH-05-0318-C-DUP
Matrix: SedimentDate Collected: 03/27/18 11:58
Percent Solids: 23.9Date Received: 03/28/18 09:30
2-Fluorobiphenyl 48 34 -100 04/02/18 03:39 04/05/18 20:26 4
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)58 04/02/18 03:39 04/05/18 20:26 433-100
Terphenyl-d14 (Surr)46 04/02/18 03:39 04/05/18 20:26 430-100
Method: 8081B_LL - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 0.86 0.27 ug/Kg ☼04/02/18 03:41 04/16/18 17:15 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.86 0.21 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼alpha-BHC ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼cis-Chlordane ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼beta-BHC ND
8.6 3.7 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Chlordane (technical)ND
0.86 0.23 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼4,4'-DDD 1.8
0.86 0.18 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼4,4'-DDE 4.3
0.86 0.33 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼4,4'-DDT ND
0.86 0.27 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼delta-BHC ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Dieldrin ND
0.86 0.23 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Endosulfan I ND
0.86 0.19 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Endosulfan II ND
0.86 0.23 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Endosulfan sulfate ND
0.86 0.34 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Endrin ND
0.86 0.31 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Endrin aldehyde ND
0.86 0.31 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Endrin ketone ND
0.86 0.30 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼gamma-BHC (Lindane)ND
0.86 0.20 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼trans-Chlordane 0.58 J
0.86 0.27 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Heptachlor ND
0.86 0.22 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Heptachlor epoxide ND
0.86 0.34 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Methoxychlor ND
0.86 0.19 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼oxy-Chlordane ND
35 23 ug/Kg 04/02/18 03:41 04/16/18 17:15 5☼Toxaphene ND
DCB Decachlorobiphenyl (Surr)79 33 -137 04/02/18 03:41 04/16/18 17:15 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr)78 04/02/18 03:41 04/16/18 17:15 533-137
Tetrachloro-m-xylene 66 04/02/18 03:41 04/16/18 17:15 526-120
Tetrachloro-m-xylene 62 04/02/18 03:41 04/16/18 17:15 526-120
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 0.13 J 0.43 0.13 mg/Kg ☼04/09/18 16:04 04/11/18 02:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.21 0.056 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Arsenic 8.3
0.21 0.016 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Beryllium 0.62
0.21 0.037 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Cadmium 0.29
0.43 0.14 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Chromium 32
0.43 0.25 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Copper 99
0.21 0.077 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Lead 27
1.1 0.34 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Manganese 140
0.21 0.13 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Nickel 12
1.1 0.13 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Selenium 1.0 J
0.21 0.030 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Silver 0.051 J
0.21 0.028 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Thallium 0.25
1.1 0.72 mg/Kg 04/09/18 16:04 04/11/18 02:23 1☼Zinc 150
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.099 0.070 0.016 mg/Kg ☼04/04/18 08:35 04/05/18 09:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Percent Moisture 76.1 0.1 0.1 %03/29/18 08:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %03/29/18 08:42 1Percent Solids 23.9
0.50 0.11 mg/Kg 04/12/18 11:38 1Cr (III)32
1.7 0.48 mg/Kg 03/29/18 14:43 03/30/18 13:31 1☼Cr (VI)ND
700 350 mg/Kg 03/31/18 06:25 04/03/18 08:15 1☼Total Petroleum Hydrocarbons
(SGT-HEM)
610 J
4200 3100 mg/Kg 03/29/18 16:59 1☼Total Organic Carbon - Duplicates 77000
Lab Sample ID: 180-76196-23Client Sample ID: TB-02-0318
Matrix: WaterDate Collected: 03/27/18 12:30
Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 1.0 0.60 ug/L 03/28/18 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.60 ug/L 03/28/18 21:15 11,1,2,2-Tetrachloroethane ND
1.0 0.86 ug/L 03/28/18 21:15 11,1,2-Trichloro-1,2,2-trifluoroethane ND
1.0 0.45 ug/L 03/28/18 21:15 11,1,2-Trichloroethane ND
1.0 0.63 ug/L 03/28/18 21:15 11,1-Dichloroethane ND
1.0 0.55 ug/L 03/28/18 21:15 11,1-Dichloroethene ND
1.0 0.77 ug/L 03/28/18 21:15 11,2,4-Trichlorobenzene ND
1.0 0.89 ug/L 03/28/18 21:15 11,2-Dibromo-3-Chloropropane ND
1.0 0.36 ug/L 03/28/18 21:15 11,2-Dichlorobenzene ND
1.0 0.57 ug/L 03/28/18 21:15 11,2-Dichloroethane ND
1.0 0.66 ug/L 03/28/18 21:15 11,2-Dichloropropane ND
1.0 0.50 ug/L 03/28/18 21:15 11,3-Dichlorobenzene ND
1.0 0.54 ug/L 03/28/18 21:15 11,4-Dichlorobenzene ND
5.0 2.6 ug/L 03/28/18 21:15 12-Butanone (MEK)ND
5.0 3.3 ug/L 03/28/18 21:15 12-Hexanone ND
5.0 3.1 ug/L 03/28/18 21:15 14-Methyl-2-pentanone (MIBK)ND
5.0 3.4 ug/L 03/28/18 21:15 1Acetone6.2
1.0 0.60 ug/L 03/28/18 21:15 1BenzeneND
1.0 0.98 ug/L 03/28/18 21:15 1BromoformND
1.0 0.89 ug/L 03/28/18 21:15 1BromomethaneND
1.0 0.88 ug/L 03/28/18 21:15 1Carbon disulfide ND
1.0 0.88 ug/L 03/28/18 21:15 1Carbon tetrachloride ND
1.0 0.50 ug/L 03/28/18 21:15 1ChlorobenzeneND
1.0 0.84 ug/L 03/28/18 21:15 1ChlorodibromomethaneND
1.0 0.90 ug/L 03/28/18 21:15 1ChloroethaneND*
1.0 0.60 ug/L 03/28/18 21:15 1ChloroformND
1.0 0.90 ug/L 03/28/18 21:15 1ChloromethaneND
1.0 0.71 ug/L 03/28/18 21:15 1cis-1,2-Dichloroethene ND
1.0 0.59 ug/L 03/28/18 21:15 1cis-1,3-Dichloropropene ND
1.0 0.63 ug/L 03/28/18 21:15 1CyclohexaneND
1.0 0.64 ug/L 03/28/18 21:15 1DichlorobromomethaneND
1.0 0.83 ug/L 03/28/18 21:15 1DichlorodifluoromethaneND
1.0 0.51 ug/L 03/28/18 21:15 1EthylbenzeneND
1.0 0.50 ug/L 03/28/18 21:15 11,2-Dibromoethane ND
1.0 0.34 ug/L 03/28/18 21:15 1IsopropylbenzeneND
5.0 1.7 ug/L 03/28/18 21:15 1Methyl acetate ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-23Client Sample ID: TB-02-0318
Matrix: WaterDate Collected: 03/27/18 12:30
Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl tert-butyl ether ND 1.0 0.59 ug/L 03/28/18 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.61 ug/L 03/28/18 21:15 1MethylcyclohexaneND
1.0 0.36 ug/L 03/28/18 21:15 1Methylene Chloride ND
1.0 0.47 ug/L 03/28/18 21:15 1StyreneND
1.0 0.47 ug/L 03/28/18 21:15 1TetrachloroetheneND
1.0 0.46 ug/L 03/28/18 21:15 1TolueneND
1.0 0.67 ug/L 03/28/18 21:15 1trans-1,2-Dichloroethene ND
1.0 0.58 ug/L 03/28/18 21:15 1trans-1,3-Dichloropropene ND
1.0 0.69 ug/L 03/28/18 21:15 1TrichloroetheneND
1.0 0.87 ug/L 03/28/18 21:15 1TrichlorofluoromethaneND
1.0 0.88 ug/L 03/28/18 21:15 1Vinyl chloride ND
2.0 0.89 ug/L 03/28/18 21:15 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)109 65 -121 03/28/18 21:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)81 03/28/18 21:15 180-120
Dibromofluoromethane (Surr)107 03/28/18 21:15 173-120
Toluene-d8 (Surr)101 03/28/18 21:15 173-120
Lab Sample ID: 180-76196-24Client Sample ID: EB-02-0318
Matrix: WaterDate Collected: 03/27/18 12:50
Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1-Trichloroethane ND 1.0 0.60 ug/L 03/29/18 21:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.60 ug/L 03/29/18 21:47 11,1,2,2-Tetrachloroethane ND
1.0 0.86 ug/L 03/29/18 21:47 11,1,2-Trichloro-1,2,2-trifluoroethane ND
1.0 0.45 ug/L 03/29/18 21:47 11,1,2-Trichloroethane ND
1.0 0.63 ug/L 03/29/18 21:47 11,1-Dichloroethane ND
1.0 0.55 ug/L 03/29/18 21:47 11,1-Dichloroethene ND
1.0 0.77 ug/L 03/29/18 21:47 11,2,4-Trichlorobenzene ND
1.0 0.89 ug/L 03/29/18 21:47 11,2-Dibromo-3-Chloropropane ND
1.0 0.36 ug/L 03/29/18 21:47 11,2-Dichlorobenzene ND
1.0 0.57 ug/L 03/29/18 21:47 11,2-Dichloroethane ND
1.0 0.66 ug/L 03/29/18 21:47 11,2-Dichloropropane ND
1.0 0.50 ug/L 03/29/18 21:47 11,3-Dichlorobenzene ND
1.0 0.54 ug/L 03/29/18 21:47 11,4-Dichlorobenzene ND
5.0 2.6 ug/L 03/29/18 21:47 12-Butanone (MEK)ND
5.0 3.3 ug/L 03/29/18 21:47 12-Hexanone ND
5.0 3.1 ug/L 03/29/18 21:47 14-Methyl-2-pentanone (MIBK)ND
5.0 3.4 ug/L 03/29/18 21:47 1Acetone6.5
1.0 0.60 ug/L 03/29/18 21:47 1BenzeneND
1.0 0.98 ug/L 03/29/18 21:47 1BromoformND
1.0 0.89 ug/L 03/29/18 21:47 1BromomethaneND
1.0 0.88 ug/L 03/29/18 21:47 1Carbon disulfide ND
1.0 0.88 ug/L 03/29/18 21:47 1Carbon tetrachloride ND
1.0 0.50 ug/L 03/29/18 21:47 1ChlorobenzeneND
1.0 0.84 ug/L 03/29/18 21:47 1ChlorodibromomethaneND
1.0 0.90 ug/L 03/29/18 21:47 1ChloroethaneND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-24Client Sample ID: EB-02-0318
Matrix: WaterDate Collected: 03/27/18 12:50
Date Received: 03/28/18 09:30
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Chloroform ND 1.0 0.60 ug/L 03/29/18 21:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.90 ug/L 03/29/18 21:47 1ChloromethaneND
1.0 0.71 ug/L 03/29/18 21:47 1cis-1,2-Dichloroethene ND
1.0 0.59 ug/L 03/29/18 21:47 1cis-1,3-Dichloropropene ND
1.0 0.63 ug/L 03/29/18 21:47 1CyclohexaneND
1.0 0.64 ug/L 03/29/18 21:47 1DichlorobromomethaneND
1.0 0.83 ug/L 03/29/18 21:47 1DichlorodifluoromethaneND
1.0 0.51 ug/L 03/29/18 21:47 1EthylbenzeneND
1.0 0.50 ug/L 03/29/18 21:47 11,2-Dibromoethane ND
1.0 0.34 ug/L 03/29/18 21:47 1IsopropylbenzeneND
5.0 1.7 ug/L 03/29/18 21:47 1Methyl acetate ND
1.0 0.59 ug/L 03/29/18 21:47 1Methyl tert-butyl ether ND
1.0 0.61 ug/L 03/29/18 21:47 1MethylcyclohexaneND
1.0 0.36 ug/L 03/29/18 21:47 1Methylene Chloride ND
1.0 0.47 ug/L 03/29/18 21:47 1StyreneND
1.0 0.47 ug/L 03/29/18 21:47 1TetrachloroetheneND
1.0 0.46 ug/L 03/29/18 21:47 1TolueneND
1.0 0.67 ug/L 03/29/18 21:47 1trans-1,2-Dichloroethene ND
1.0 0.58 ug/L 03/29/18 21:47 1trans-1,3-Dichloropropene ND
1.0 0.69 ug/L 03/29/18 21:47 1TrichloroetheneND
1.0 0.87 ug/L 03/29/18 21:47 1TrichlorofluoromethaneND
1.0 0.88 ug/L 03/29/18 21:47 1Vinyl chloride ND
2.0 0.89 ug/L 03/29/18 21:47 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)88 65 -121 03/29/18 21:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)89 03/29/18 21:47 180-120
Dibromofluoromethane (Surr)85 03/29/18 21:47 173-120
Toluene-d8 (Surr)90 03/29/18 21:47 173-120
Method: EPA 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
RL MDL
Acenaphthene ND 0.20 0.068 ug/L 04/02/18 11:29 04/06/18 00:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.068 ug/L 04/02/18 11:29 04/06/18 00:27 1AcenaphthyleneND
0.20 0.051 ug/L 04/02/18 11:29 04/06/18 00:27 1AnthraceneND
0.20 0.078 ug/L 04/02/18 11:29 04/06/18 00:27 1Benzo[a]anthracene ND
0.20 0.10 ug/L 04/02/18 11:29 04/06/18 00:27 1Benzo[b]fluoranthene ND
0.20 0.072 ug/L 04/02/18 11:29 04/06/18 00:27 1Benzo[g,h,i]perylene ND
0.20 0.055 ug/L 04/02/18 11:29 04/06/18 00:27 1Benzo[a]pyrene ND
0.20 0.084 ug/L 04/02/18 11:29 04/06/18 00:27 1ChryseneND
0.20 0.075 ug/L 04/02/18 11:29 04/06/18 00:27 1Dibenz(a,h)anthracene ND
0.20 0.063 ug/L 04/02/18 11:29 04/06/18 00:27 1FluorantheneND
0.20 0.072 ug/L 04/02/18 11:29 04/06/18 00:27 1FluoreneND
0.20 0.089 ug/L 04/02/18 11:29 04/06/18 00:27 1Indeno[1,2,3-cd]pyrene ND
0.20 0.061 ug/L 04/02/18 11:29 04/06/18 00:27 1NaphthaleneND
0.20 0.057 ug/L 04/02/18 11:29 04/06/18 00:27 1PhenanthreneND
0.20 0.056 ug/L 04/02/18 11:29 04/06/18 00:27 1PyreneND
0.20 0.092 ug/L 04/02/18 11:29 04/06/18 00:27 1Benzo[k]fluoranthene ND
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 180-76196-24Client Sample ID: EB-02-0318
Matrix: WaterDate Collected: 03/27/18 12:50
Date Received: 03/28/18 09:30
2-Fluorobiphenyl 69 26 -103 04/02/18 11:29 04/06/18 00:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)71 04/02/18 11:29 04/06/18 00:27 130-101
Terphenyl-d14 (Surr)90 04/02/18 11:29 04/06/18 00:27 120-119
Method: EPA 8081B LL - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 0.0013 0.00012 ug/L 03/28/18 12:35 04/02/18 19:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0013 0.00012 ug/L 03/28/18 12:35 04/02/18 19:49 1alpha-BHC ND
0.0013 0.00016 ug/L 03/28/18 12:35 04/02/18 19:49 1beta-BHC ND
0.0013 0.00035 ug/L 03/28/18 12:35 04/02/18 19:49 1delta-BHC ND
0.0013 0.00012 ug/L 03/28/18 12:35 04/02/18 19:49 1gamma-BHC (Lindane)ND
0.0013 0.00014 ug/L 03/28/18 12:35 04/02/18 19:49 1cis-Chlordane ND
0.0013 0.00013 ug/L 03/28/18 12:35 04/02/18 19:49 1trans-Chlordane ND
0.017 0.00021 ug/L 03/28/18 12:35 04/02/18 19:49 1oxy-Chlordane ND
0.013 0.0015 ug/L 03/28/18 12:35 04/02/18 19:49 1Chlordane (technical)ND
0.0013 0.00021 ug/L 03/28/18 12:35 04/02/18 19:49 14,4'-DDD ND
0.0013 0.00011 ug/L 03/28/18 12:35 04/02/18 19:49 14,4'-DDE ND
0.0013 0.00030 ug/L 03/28/18 12:35 04/02/18 19:49 14,4'-DDT ND
0.0013 0.00013 ug/L 03/28/18 12:35 04/02/18 19:49 1DieldrinND
0.0013 0.00015 ug/L 03/28/18 12:35 04/02/18 19:49 1Endosulfan I ND
0.0013 0.00012 ug/L 03/28/18 12:35 04/02/18 19:49 1Endosulfan II ND
0.0013 0.00030 ug/L 03/28/18 12:35 04/02/18 19:49 1Endosulfan sulfate ND
0.0013 0.00023 ug/L 03/28/18 12:35 04/02/18 19:49 1EndrinND
0.0013 0.00025 ug/L 03/28/18 12:35 04/02/18 19:49 1Endrin aldehyde ND
0.0013 0.00017 ug/L 03/28/18 12:35 04/02/18 19:49 1Endrin ketone ND
0.0013 0.00046 ug/L 03/28/18 12:35 04/02/18 19:49 1HeptachlorND
0.0013 0.00014 ug/L 03/28/18 12:35 04/02/18 19:49 1Heptachlor epoxide ND
0.0013 0.00035 ug/L 03/28/18 12:35 04/02/18 19:49 1MethoxychlorND
0.10 0.012 ug/L 03/28/18 12:35 04/02/18 19:49 1ToxapheneND
Tetrachloro-m-xylene 69 41 -124 03/28/18 12:35 04/02/18 19:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 76 03/28/18 12:35 04/02/18 19:49 141-124
DCB Decachlorobiphenyl (Surr)78 p 03/28/18 12:35 04/02/18 19:49 164-126
DCB Decachlorobiphenyl (Surr)208 X 03/28/18 12:35 04/02/18 19:49 164-126
Method: EPA 6020B - Metals (ICP/MS) - Total Recoverable
RL MDL
Antimony ND 2.0 1.1 ug/L 03/30/18 13:04 03/31/18 12:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.32 ug/L 03/30/18 13:04 03/31/18 12:37 1ArsenicND
1.0 0.057 ug/L 03/30/18 13:04 03/31/18 12:37 1BerylliumND
1.0 0.13 ug/L 03/30/18 13:04 03/31/18 12:37 1CadmiumND
2.0 0.63 ug/L 03/30/18 13:04 03/31/18 12:37 1Chromium1.7 J
2.0 1.3 ug/L 03/30/18 13:04 03/31/18 12:37 1CopperND
1.0 0.094 ug/L 03/30/18 13:04 03/31/18 12:37 1LeadND
5.0 1.4 ug/L 03/30/18 13:04 03/31/18 12:37 1Manganese2.0 J
1.0 0.31 ug/L 03/30/18 13:04 03/31/18 12:37 1Nickel2.9
5.0 0.81 ug/L 03/30/18 13:04 03/31/18 12:37 1SeleniumND
1.0 0.12 ug/L 03/30/18 13:04 03/31/18 12:37 1SilverND
1.0 0.063 ug/L 03/30/18 13:04 03/31/18 12:37 1ThalliumND
5.0 2.4 ug/L 03/30/18 13:04 03/31/18 12:37 1Zinc3.2 J
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Client Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.20 0.065 ug/L 04/10/18 11:20 04/11/18 11:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Total Petroleum Hydrocarbons
(SGT-HEM)
ND 4.1 1.4 mg/L 04/01/18 14:43 04/02/18 09:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 3.2 ug/L 04/12/18 11:38 1Cr (III)ND
0.010 0.0032 mg/L 03/28/18 12:08 1Cr (VI)ND
1.0 0.51 mg/L 04/03/18 17:12 1Total Organic Carbon - Duplicates 0.55 J
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-240660/9
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240660
RL MDL
1,1,1-Trichloroethane ND 5.0 2.5 ug/Kg 03/28/18 09:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.05.0 ug/Kg 03/28/18 09:44 11,1,2,2-Tetrachloroethane
ND 1.95.0 ug/Kg 03/28/18 09:44 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 2.45.0 ug/Kg 03/28/18 09:44 11,1,2-Trichloroethane
ND 1.85.0 ug/Kg 03/28/18 09:44 11,1-Dichloroethane
ND 2.95.0 ug/Kg 03/28/18 09:44 11,1-Dichloroethene
ND 1.65.0 ug/Kg 03/28/18 09:44 11,2,4-Trichlorobenzene
ND 3.15.0 ug/Kg 03/28/18 09:44 11,2-Dibromo-3-Chloropropane
ND 4.05.0 ug/Kg 03/28/18 09:44 11,2-Dichlorobenzene
ND 1.55.0 ug/Kg 03/28/18 09:44 11,2-Dichloroethane
ND 2.55.0 ug/Kg 03/28/18 09:44 11,2-Dichloropropane
ND 1.65.0 ug/Kg 03/28/18 09:44 11,3-Dichlorobenzene
ND 1.05.0 ug/Kg 03/28/18 09:44 11,4-Dichlorobenzene
ND 2.95.0 ug/Kg 03/28/18 09:44 12-Butanone (MEK)
ND 4.25.0 ug/Kg 03/28/18 09:44 12-Hexanone
ND 1.95.0 ug/Kg 03/28/18 09:44 14-Methyl-2-pentanone (MIBK)
ND 3.220 ug/Kg 03/28/18 09:44 1Acetone
ND 2.05.0 ug/Kg 03/28/18 09:44 1Benzene
ND 2.65.0 ug/Kg 03/28/18 09:44 1Bromoform
ND 4.55.0 ug/Kg 03/28/18 09:44 1Bromomethane
ND 3.05.0 ug/Kg 03/28/18 09:44 1Carbon disulfide
ND 3.35.0 ug/Kg 03/28/18 09:44 1Carbon tetrachloride
ND 1.65.0 ug/Kg 03/28/18 09:44 1Chlorobenzene
ND 2.45.0 ug/Kg 03/28/18 09:44 1Chlorodibromomethane
ND 2.15.0 ug/Kg 03/28/18 09:44 1Chloroform
ND 3.95.0 ug/Kg 03/28/18 09:44 1Chloromethane
ND 2.65.0 ug/Kg 03/28/18 09:44 1Chloroethane
ND 1.65.0 ug/Kg 03/28/18 09:44 1cis-1,2-Dichloroethene
ND 1.65.0 ug/Kg 03/28/18 09:44 1cis-1,3-Dichloropropene
ND 1.25.0 ug/Kg 03/28/18 09:44 1Cyclohexane
ND 2.45.0 ug/Kg 03/28/18 09:44 1Dichlorobromomethane
ND 2.95.0 ug/Kg 03/28/18 09:44 1Dichlorodifluoromethane
ND 2.25.0 ug/Kg 03/28/18 09:44 1Ethylbenzene
ND 2.75.0 ug/Kg 03/28/18 09:44 11,2-Dibromoethane
ND 2.35.0 ug/Kg 03/28/18 09:44 1Isopropylbenzene
ND 5.925 ug/Kg 03/28/18 09:44 1Methyl acetate
ND 3.75.0 ug/Kg 03/28/18 09:44 1Methyl tert-butyl ether
ND 2.15.0 ug/Kg 03/28/18 09:44 1Methylcyclohexane
ND 2.45.0 ug/Kg 03/28/18 09:44 1Methylene Chloride
ND 1.35.0 ug/Kg 03/28/18 09:44 1Styrene
ND 2.05.0 ug/Kg 03/28/18 09:44 1Tetrachloroethene
ND 1.75.0 ug/Kg 03/28/18 09:44 1Toluene
ND 2.55.0 ug/Kg 03/28/18 09:44 1trans-1,2-Dichloroethene
ND 1.75.0 ug/Kg 03/28/18 09:44 1trans-1,3-Dichloropropene
ND 1.55.0 ug/Kg 03/28/18 09:44 1Trichloroethene
ND 1.55.0 ug/Kg 03/28/18 09:44 1Trichlorofluoromethane
ND 4.310 ug/Kg 03/28/18 09:44 1Xylenes, Total
ND 3.75.0 ug/Kg 03/28/18 09:44 1Vinyl chloride
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
1,2-Dichloroethane-d4 (Surr)99 62 -118 03/28/18 09:44 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
95 03/28/18 09:44 14-Bromofluorobenzene (Surr)76 -111
98 03/28/18 09:44 1Dibromofluoromethane (Surr)72 -116
107 03/28/18 09:44 1Toluene-d8 (Surr)80 -129
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240660/3
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240660
1,1,1-Trichloroethane 40.0 40.2 ug/Kg 100 69 -135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2,2-Tetrachloroethane 40.0 43.9 ug/Kg 110 71 -125
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 42.1 ug/Kg 105 61 -137
1,1,2-Trichloroethane 40.0 43.7 ug/Kg 109 78 -118
1,1-Dichloroethane 40.0 40.9 ug/Kg 102 67 -129
1,1-Dichloroethene 40.0 39.9 ug/Kg 100 59 -128
1,2,4-Trichlorobenzene 40.0 30.3 ug/Kg 76 65 -135
1,2-Dibromo-3-Chloropropane 40.0 37.4 ug/Kg 94 54 -129
1,2-Dichlorobenzene 40.0 39.1 ug/Kg 98 78 -118
1,2-Dichloroethane 40.0 41.9 ug/Kg 105 67 -123
1,2-Dichloropropane 40.0 39.9 ug/Kg 100 80 -121
1,3-Dichlorobenzene 40.0 40.6 ug/Kg 102 78 -118
1,4-Dichlorobenzene 40.0 39.7 ug/Kg 99 78 -118
2-Butanone (MEK)40.0 45.1 ug/Kg 113 30 -150
2-Hexanone 40.0 47.4 ug/Kg 118 36 -150
4-Methyl-2-pentanone (MIBK)40.0 42.7 ug/Kg 107 62 -145
Acetone 40.0 57.1 ug/Kg 143 36 -150
Benzene 40.0 42.1 ug/Kg 105 78 -118
Bromoform 40.0 35.8 ug/Kg 89 56 -150
Bromomethane 40.0 35.7 ug/Kg 89 34 -150
Carbon disulfide 40.0 35.6 ug/Kg 89 66 -128
Carbon tetrachloride 40.0 39.0 ug/Kg 98 60 -137
Chlorobenzene 40.0 41.6 ug/Kg 104 78 -118
Chlorodibromomethane 40.0 37.6 ug/Kg 94 58 -140
Chloroform 40.0 40.8 ug/Kg 102 68 -124
Chloromethane 40.0 35.9 ug/Kg 90 46 -150
Chloroethane 40.0 41.6 ug/Kg 104 37 -150
cis-1,2-Dichloroethene 40.0 43.0 ug/Kg 108 71 -120
cis-1,3-Dichloropropene 40.0 39.4 ug/Kg 99 70 -131
Cyclohexane 40.0 40.2 ug/Kg 100 70 -133
Dichlorobromomethane 40.0 38.3 ug/Kg 96 66 -136
Dichlorodifluoromethane 40.0 57.3 ug/Kg 143 16 -150
Ethylbenzene 40.0 41.0 ug/Kg 103 78 -118
1,2-Dibromoethane 40.0 43.4 ug/Kg 109 78 -118
Isopropylbenzene 40.0 39.7 ug/Kg 99 76 -123
Methyl acetate 80.0 93.8 ug/Kg 117 64 -140
Methyl tert-butyl ether 40.0 42.3 ug/Kg 106 73 -121
Methylcyclohexane 40.0 42.5 ug/Kg 106 75 -124
Methylene Chloride 40.0 40.1 ug/Kg 100 68 -120
m-Xylene & p-Xylene 40.0 40.9 ug/Kg 102 78 -118
o-Xylene 40.0 41.1 ug/Kg 103 78 -118
Styrene 40.0 39.7 ug/Kg 99 79 -119
Tetrachloroethene 40.0 41.6 ug/Kg 104 78 -118
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240660/3
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240660
Toluene 40.0 41.2 ug/Kg 103 79 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
trans-1,2-Dichloroethene 40.0 42.4 ug/Kg 106 71 -123
trans-1,3-Dichloropropene 40.0 37.7 ug/Kg 94 62 -133
Trichloroethene 40.0 42.6 ug/Kg 106 76 -120
Trichlorofluoromethane 40.0 38.6 ug/Kg 96 25 -150
Xylenes, Total 80.0 82.0 ug/Kg 103 78 -118
Vinyl chloride 40.0 39.7 ug/Kg 99 53 -148
1,2-Dichloroethane-d4 (Surr)62 -118
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)76 -111
103Dibromofluoromethane (Surr)72 -116
105Toluene-d8 (Surr)80 -129
Client Sample ID: Method BlankLab Sample ID: MB 180-240736/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240736
RL MDL
1,1,1-Trichloroethane ND 1.0 0.60 ug/L 03/28/18 18:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.601.0 ug/L 03/28/18 18:24 11,1,2,2-Tetrachloroethane
ND 0.861.0 ug/L 03/28/18 18:24 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.451.0 ug/L 03/28/18 18:24 11,1,2-Trichloroethane
ND 0.631.0 ug/L 03/28/18 18:24 11,1-Dichloroethane
ND 0.551.0 ug/L 03/28/18 18:24 11,1-Dichloroethene
ND 0.771.0 ug/L 03/28/18 18:24 11,2,4-Trichlorobenzene
ND 0.891.0 ug/L 03/28/18 18:24 11,2-Dibromo-3-Chloropropane
ND 0.361.0 ug/L 03/28/18 18:24 11,2-Dichlorobenzene
ND 0.571.0 ug/L 03/28/18 18:24 11,2-Dichloroethane
ND 0.661.0 ug/L 03/28/18 18:24 11,2-Dichloropropane
ND 0.501.0 ug/L 03/28/18 18:24 11,3-Dichlorobenzene
ND 0.541.0 ug/L 03/28/18 18:24 11,4-Dichlorobenzene
ND 2.65.0 ug/L 03/28/18 18:24 12-Butanone (MEK)
ND 3.35.0 ug/L 03/28/18 18:24 12-Hexanone
ND 3.15.0 ug/L 03/28/18 18:24 14-Methyl-2-pentanone (MIBK)
ND 3.45.0 ug/L 03/28/18 18:24 1Acetone
ND 0.601.0 ug/L 03/28/18 18:24 1Benzene
ND 0.981.0 ug/L 03/28/18 18:24 1Bromoform
ND 0.891.0 ug/L 03/28/18 18:24 1Bromomethane
ND 0.881.0 ug/L 03/28/18 18:24 1Carbon disulfide
ND 0.881.0 ug/L 03/28/18 18:24 1Carbon tetrachloride
ND 0.501.0 ug/L 03/28/18 18:24 1Chlorobenzene
ND 0.841.0 ug/L 03/28/18 18:24 1Chlorodibromomethane
ND 0.901.0 ug/L 03/28/18 18:24 1Chloroethane
ND 0.601.0 ug/L 03/28/18 18:24 1Chloroform
ND 0.901.0 ug/L 03/28/18 18:24 1Chloromethane
ND 0.711.0 ug/L 03/28/18 18:24 1cis-1,2-Dichloroethene
ND 0.591.0 ug/L 03/28/18 18:24 1cis-1,3-Dichloropropene
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-240736/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240736
RL MDL
Cyclohexane ND 1.0 0.63 ug/L 03/28/18 18:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.641.0 ug/L 03/28/18 18:24 1Dichlorobromomethane
ND 0.831.0 ug/L 03/28/18 18:24 1Dichlorodifluoromethane
ND 0.511.0 ug/L 03/28/18 18:24 1Ethylbenzene
ND 0.501.0 ug/L 03/28/18 18:24 11,2-Dibromoethane
ND 0.341.0 ug/L 03/28/18 18:24 1Isopropylbenzene
ND 1.75.0 ug/L 03/28/18 18:24 1Methyl acetate
ND 0.591.0 ug/L 03/28/18 18:24 1Methyl tert-butyl ether
ND 0.611.0 ug/L 03/28/18 18:24 1Methylcyclohexane
ND 0.361.0 ug/L 03/28/18 18:24 1Methylene Chloride
ND 0.471.0 ug/L 03/28/18 18:24 1Styrene
ND 0.471.0 ug/L 03/28/18 18:24 1Tetrachloroethene
ND 0.461.0 ug/L 03/28/18 18:24 1Toluene
ND 0.671.0 ug/L 03/28/18 18:24 1trans-1,2-Dichloroethene
ND 0.581.0 ug/L 03/28/18 18:24 1trans-1,3-Dichloropropene
ND 0.691.0 ug/L 03/28/18 18:24 1Trichloroethene
ND 0.871.0 ug/L 03/28/18 18:24 1Trichlorofluoromethane
ND 0.881.0 ug/L 03/28/18 18:24 1Vinyl chloride
ND 0.892.0 ug/L 03/28/18 18:24 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)102 65 -121 03/28/18 18:24 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
87 03/28/18 18:24 14-Bromofluorobenzene (Surr)80 -120
100 03/28/18 18:24 1Dibromofluoromethane (Surr)73 -120
99 03/28/18 18:24 1Toluene-d8 (Surr)73 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240736/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240736
1,1,1-Trichloroethane 10.0 10.5 ug/L 105 66 -129
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2,2-Tetrachloroethane 10.0 9.83 ug/L 98 72 -128
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
10.0 10.5 ug/L 105 55 -138
1,1,2-Trichloroethane 10.0 10.1 ug/L 101 74 -126
1,1-Dichloroethane 10.0 9.71 ug/L 97 66 -122
1,1-Dichloroethene 10.0 10.4 ug/L 104 64 -131
1,2,4-Trichlorobenzene 10.0 7.64 ug/L 76 39 -147
1,2-Dibromo-3-Chloropropane 10.0 7.10 ug/L 71 48 -132
1,2-Dichlorobenzene 10.0 9.36 ug/L 94 74 -121
1,2-Dichloroethane 10.0 9.46 ug/L 95 63 -130
1,2-Dichloropropane 10.0 9.44 ug/L 94 67 -119
1,3-Dichlorobenzene 10.0 9.33 ug/L 93 77 -119
1,4-Dichlorobenzene 10.0 9.36 ug/L 94 76 -118
2-Butanone (MEK)20.0 17.2 ug/L 86 37 -150
2-Hexanone 20.0 15.7 ug/L 79 37 -150
4-Methyl-2-pentanone (MIBK)20.0 15.1 ug/L 75 41 -135
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240736/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240736
Acetone 20.0 19.5 ug/L 98 24 -150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 10.0 10.1 ug/L 101 75 -123
Bromoform 10.0 8.85 ug/L 88 54 -136
Bromomethane 10.0 8.76 ug/L 88 37 -150
Carbon disulfide 10.0 9.27 ug/L 93 20 -150
Carbon tetrachloride 10.0 10.8 ug/L 108 58 -145
Chlorobenzene 10.0 10.8 ug/L 108 79 -124
Chlorodibromomethane 10.0 9.95 ug/L 100 63 -131
Chloroethane 10.0 14.2 *ug/L 142 44 -139
Chloroform 10.0 9.68 ug/L 97 72 -123
Chloromethane 10.0 7.47 ug/L 75 49 -135
cis-1,2-Dichloroethene 10.0 9.74 ug/L 97 73 -120
cis-1,3-Dichloropropene 10.0 8.69 ug/L 87 61 -127
Cyclohexane 10.0 9.15 ug/L 92 50 -133
Dichlorobromomethane 10.0 9.01 ug/L 90 62 -127
Dichlorodifluoromethane 10.0 6.37 ug/L 64 33 -150
Ethylbenzene 10.0 10.0 ug/L 100 77 -124
1,2-Dibromoethane 10.0 9.57 ug/L 96 76 -128
Isopropylbenzene 10.0 10.0 ug/L 100 74 -131
Methyl acetate 20.0 14.7 ug/L 74 49 -150
Methyl tert-butyl ether 10.0 9.08 ug/L 91 66 -130
Methylcyclohexane 10.0 9.38 ug/L 94 62 -129
Methylene Chloride 10.0 10.0 ug/L 100 66 -123
m-Xylene & p-Xylene 10.0 10.1 ug/L 101 77 -125
o-Xylene 10.0 9.82 ug/L 98 75 -124
Styrene 10.0 9.73 ug/L 97 80 -125
Tetrachloroethene 10.0 11.1 ug/L 111 76 -128
Toluene 10.0 11.4 ug/L 114 76 -129
trans-1,2-Dichloroethene 10.0 10.6 ug/L 106 70 -123
trans-1,3-Dichloropropene 10.0 10.0 ug/L 100 61 -136
Trichloroethene 10.0 9.46 ug/L 95 74 -121
Trichlorofluoromethane 10.0 12.8 ug/L 128 43 -150
Vinyl chloride 10.0 8.50 ug/L 85 52 -136
Xylenes, Total 20.0 19.9 ug/L 100 76 -124
1,2-Dichloroethane-d4 (Surr)65 -121
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
1024-Bromofluorobenzene (Surr)80 -120
102Dibromofluoromethane (Surr)73 -120
120Toluene-d8 (Surr)73 -120
Client Sample ID: Method BlankLab Sample ID: MB 180-240865/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240865
RL MDL
1,1,1-Trichloroethane ND 1.0 0.60 ug/L 03/29/18 19:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.601.0 ug/L 03/29/18 19:45 11,1,2,2-Tetrachloroethane
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-240865/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240865
RL MDL
1,1,2-Trichloro-1,2,2-trifluoroethane ND 1.0 0.86 ug/L 03/29/18 19:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.451.0 ug/L 03/29/18 19:45 11,1,2-Trichloroethane
ND 0.631.0 ug/L 03/29/18 19:45 11,1-Dichloroethane
ND 0.551.0 ug/L 03/29/18 19:45 11,1-Dichloroethene
ND 0.771.0 ug/L 03/29/18 19:45 11,2,4-Trichlorobenzene
ND 0.891.0 ug/L 03/29/18 19:45 11,2-Dibromo-3-Chloropropane
ND 0.361.0 ug/L 03/29/18 19:45 11,2-Dichlorobenzene
ND 0.571.0 ug/L 03/29/18 19:45 11,2-Dichloroethane
ND 0.661.0 ug/L 03/29/18 19:45 11,2-Dichloropropane
ND 0.501.0 ug/L 03/29/18 19:45 11,3-Dichlorobenzene
ND 0.541.0 ug/L 03/29/18 19:45 11,4-Dichlorobenzene
ND 2.65.0 ug/L 03/29/18 19:45 12-Butanone (MEK)
ND 3.35.0 ug/L 03/29/18 19:45 12-Hexanone
ND 3.15.0 ug/L 03/29/18 19:45 14-Methyl-2-pentanone (MIBK)
ND 3.45.0 ug/L 03/29/18 19:45 1Acetone
ND 0.601.0 ug/L 03/29/18 19:45 1Benzene
ND 0.981.0 ug/L 03/29/18 19:45 1Bromoform
ND 0.891.0 ug/L 03/29/18 19:45 1Bromomethane
ND 0.881.0 ug/L 03/29/18 19:45 1Carbon disulfide
ND 0.881.0 ug/L 03/29/18 19:45 1Carbon tetrachloride
ND 0.501.0 ug/L 03/29/18 19:45 1Chlorobenzene
ND 0.841.0 ug/L 03/29/18 19:45 1Chlorodibromomethane
ND 0.901.0 ug/L 03/29/18 19:45 1Chloroethane
ND 0.601.0 ug/L 03/29/18 19:45 1Chloroform
ND 0.901.0 ug/L 03/29/18 19:45 1Chloromethane
ND 0.711.0 ug/L 03/29/18 19:45 1cis-1,2-Dichloroethene
ND 0.591.0 ug/L 03/29/18 19:45 1cis-1,3-Dichloropropene
ND 0.631.0 ug/L 03/29/18 19:45 1Cyclohexane
ND 0.641.0 ug/L 03/29/18 19:45 1Dichlorobromomethane
ND 0.831.0 ug/L 03/29/18 19:45 1Dichlorodifluoromethane
ND 0.511.0 ug/L 03/29/18 19:45 1Ethylbenzene
ND 0.501.0 ug/L 03/29/18 19:45 11,2-Dibromoethane
ND 0.341.0 ug/L 03/29/18 19:45 1Isopropylbenzene
ND 1.75.0 ug/L 03/29/18 19:45 1Methyl acetate
ND 0.591.0 ug/L 03/29/18 19:45 1Methyl tert-butyl ether
ND 0.611.0 ug/L 03/29/18 19:45 1Methylcyclohexane
ND 0.361.0 ug/L 03/29/18 19:45 1Methylene Chloride
ND 0.471.0 ug/L 03/29/18 19:45 1Styrene
ND 0.471.0 ug/L 03/29/18 19:45 1Tetrachloroethene
ND 0.461.0 ug/L 03/29/18 19:45 1Toluene
ND 0.671.0 ug/L 03/29/18 19:45 1trans-1,2-Dichloroethene
ND 0.581.0 ug/L 03/29/18 19:45 1trans-1,3-Dichloropropene
ND 0.691.0 ug/L 03/29/18 19:45 1Trichloroethene
ND 0.871.0 ug/L 03/29/18 19:45 1Trichlorofluoromethane
ND 0.881.0 ug/L 03/29/18 19:45 1Vinyl chloride
ND 0.892.0 ug/L 03/29/18 19:45 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-240865/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240865
1,2-Dichloroethane-d4 (Surr)84 65 -121 03/29/18 19:45 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
89 03/29/18 19:45 14-Bromofluorobenzene (Surr)80 -120
84 03/29/18 19:45 1Dibromofluoromethane (Surr)73 -120
92 03/29/18 19:45 1Toluene-d8 (Surr)73 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240865/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240865
1,1,1-Trichloroethane 10.0 11.7 ug/L 117 66 -129
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2,2-Tetrachloroethane 10.0 8.26 ug/L 83 72 -128
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
10.0 10.9 ug/L 109 55 -138
1,1,2-Trichloroethane 10.0 10.4 ug/L 104 74 -126
1,1-Dichloroethane 10.0 9.81 ug/L 98 66 -122
1,1-Dichloroethene 10.0 9.99 ug/L 100 64 -131
1,2,4-Trichlorobenzene 10.0 6.21 ug/L 62 39 -147
1,2-Dibromo-3-Chloropropane 10.0 7.26 ug/L 73 48 -132
1,2-Dichlorobenzene 10.0 9.44 ug/L 94 74 -121
1,2-Dichloroethane 10.0 9.64 ug/L 96 63 -130
1,2-Dichloropropane 10.0 9.75 ug/L 98 67 -119
1,3-Dichlorobenzene 10.0 10.3 ug/L 103 77 -119
1,4-Dichlorobenzene 10.0 10.5 ug/L 105 76 -118
2-Butanone (MEK)20.0 18.1 ug/L 91 37 -150
2-Hexanone 20.0 19.6 ug/L 98 37 -150
4-Methyl-2-pentanone (MIBK)20.0 18.1 ug/L 91 41 -135
Acetone 20.0 19.2 ug/L 96 24 -150
Benzene 10.0 10.3 ug/L 103 75 -123
Bromoform 10.0 7.61 ug/L 76 54 -136
Bromomethane 10.0 12.2 ug/L 122 37 -150
Carbon disulfide 10.0 8.81 ug/L 88 20 -150
Carbon tetrachloride 10.0 12.4 ug/L 124 58 -145
Chlorobenzene 10.0 10.6 ug/L 106 79 -124
Chlorodibromomethane 10.0 10.1 ug/L 101 63 -131
Chloroethane 10.0 12.0 ug/L 120 44 -139
Chloroform 10.0 9.48 ug/L 95 72 -123
Chloromethane 10.0 9.35 ug/L 93 49 -135
cis-1,2-Dichloroethene 10.0 9.69 ug/L 97 73 -120
cis-1,3-Dichloropropene 10.0 10.7 ug/L 107 61 -127
Cyclohexane 10.0 10.3 ug/L 103 50 -133
Dichlorobromomethane 10.0 8.95 ug/L 89 62 -127
Dichlorodifluoromethane 10.0 11.1 ug/L 111 33 -150
Ethylbenzene 10.0 10.2 ug/L 102 77 -124
1,2-Dibromoethane 10.0 10.1 ug/L 101 76 -128
Isopropylbenzene 10.0 9.11 ug/L 91 74 -131
Methyl acetate 20.0 21.3 ug/L 106 49 -150
Methyl tert-butyl ether 10.0 8.96 ug/L 90 66 -130
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240865/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240865
Methylcyclohexane 10.0 9.87 ug/L 99 62 -129
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Methylene Chloride 10.0 9.95 ug/L 99 66 -123
m-Xylene & p-Xylene 10.0 10.4 ug/L 104 77 -125
o-Xylene 10.0 9.44 ug/L 94 75 -124
Styrene 10.0 9.66 ug/L 97 80 -125
Tetrachloroethene 10.0 11.3 ug/L 113 76 -128
Toluene 10.0 10.7 ug/L 107 76 -129
trans-1,2-Dichloroethene 10.0 10.4 ug/L 104 70 -123
trans-1,3-Dichloropropene 10.0 10.3 ug/L 103 61 -136
Trichloroethene 10.0 11.1 ug/L 111 74 -121
Trichlorofluoromethane 10.0 12.5 ug/L 125 43 -150
Vinyl chloride 10.0 9.99 ug/L 100 52 -136
Xylenes, Total 20.0 19.8 ug/L 99 76 -124
1,2-Dichloroethane-d4 (Surr)65 -121
Surrogate
93
LCS LCS
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr)80 -120
93Dibromofluoromethane (Surr)73 -120
114Toluene-d8 (Surr)73 -120
Client Sample ID: Method BlankLab Sample ID: MB 180-240896/7
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240896
RL MDL
1,1,1-Trichloroethane ND 5.0 2.5 ug/Kg 03/30/18 09:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.05.0 ug/Kg 03/30/18 09:51 11,1,2,2-Tetrachloroethane
ND 1.95.0 ug/Kg 03/30/18 09:51 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 2.45.0 ug/Kg 03/30/18 09:51 11,1,2-Trichloroethane
ND 1.85.0 ug/Kg 03/30/18 09:51 11,1-Dichloroethane
ND 2.95.0 ug/Kg 03/30/18 09:51 11,1-Dichloroethene
ND 1.65.0 ug/Kg 03/30/18 09:51 11,2,4-Trichlorobenzene
ND 3.15.0 ug/Kg 03/30/18 09:51 11,2-Dibromo-3-Chloropropane
ND 4.05.0 ug/Kg 03/30/18 09:51 11,2-Dichlorobenzene
ND 1.55.0 ug/Kg 03/30/18 09:51 11,2-Dichloroethane
ND 2.55.0 ug/Kg 03/30/18 09:51 11,2-Dichloropropane
ND 1.65.0 ug/Kg 03/30/18 09:51 11,3-Dichlorobenzene
ND 1.05.0 ug/Kg 03/30/18 09:51 11,4-Dichlorobenzene
ND 2.95.0 ug/Kg 03/30/18 09:51 12-Butanone (MEK)
ND 4.25.0 ug/Kg 03/30/18 09:51 12-Hexanone
ND 1.95.0 ug/Kg 03/30/18 09:51 14-Methyl-2-pentanone (MIBK)
ND 3.220 ug/Kg 03/30/18 09:51 1Acetone
ND 2.05.0 ug/Kg 03/30/18 09:51 1Benzene
ND 2.65.0 ug/Kg 03/30/18 09:51 1Bromoform
ND 4.55.0 ug/Kg 03/30/18 09:51 1Bromomethane
ND 3.05.0 ug/Kg 03/30/18 09:51 1Carbon disulfide
ND 3.35.0 ug/Kg 03/30/18 09:51 1Carbon tetrachloride
ND 1.65.0 ug/Kg 03/30/18 09:51 1Chlorobenzene
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-240896/7
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240896
RL MDL
Chlorodibromomethane ND 5.0 2.4 ug/Kg 03/30/18 09:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 2.15.0 ug/Kg 03/30/18 09:51 1Chloroform
ND 3.95.0 ug/Kg 03/30/18 09:51 1Chloromethane
ND 2.65.0 ug/Kg 03/30/18 09:51 1Chloroethane
ND 1.65.0 ug/Kg 03/30/18 09:51 1cis-1,2-Dichloroethene
ND 1.65.0 ug/Kg 03/30/18 09:51 1cis-1,3-Dichloropropene
ND 1.25.0 ug/Kg 03/30/18 09:51 1Cyclohexane
ND 2.45.0 ug/Kg 03/30/18 09:51 1Dichlorobromomethane
ND 2.95.0 ug/Kg 03/30/18 09:51 1Dichlorodifluoromethane
ND 2.25.0 ug/Kg 03/30/18 09:51 1Ethylbenzene
ND 2.75.0 ug/Kg 03/30/18 09:51 11,2-Dibromoethane
ND 2.35.0 ug/Kg 03/30/18 09:51 1Isopropylbenzene
ND 5.925 ug/Kg 03/30/18 09:51 1Methyl acetate
ND 3.75.0 ug/Kg 03/30/18 09:51 1Methyl tert-butyl ether
ND 2.15.0 ug/Kg 03/30/18 09:51 1Methylcyclohexane
2.54 J 2.45.0 ug/Kg 03/30/18 09:51 1Methylene Chloride
ND 1.35.0 ug/Kg 03/30/18 09:51 1Styrene
ND 2.05.0 ug/Kg 03/30/18 09:51 1Tetrachloroethene
ND 1.75.0 ug/Kg 03/30/18 09:51 1Toluene
ND 2.55.0 ug/Kg 03/30/18 09:51 1trans-1,2-Dichloroethene
ND 1.75.0 ug/Kg 03/30/18 09:51 1trans-1,3-Dichloropropene
ND 1.55.0 ug/Kg 03/30/18 09:51 1Trichloroethene
ND 1.55.0 ug/Kg 03/30/18 09:51 1Trichlorofluoromethane
ND 4.310 ug/Kg 03/30/18 09:51 1Xylenes, Total
ND 3.75.0 ug/Kg 03/30/18 09:51 1Vinyl chloride
1,2-Dichloroethane-d4 (Surr)92 62 -118 03/30/18 09:51 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
92 03/30/18 09:51 14-Bromofluorobenzene (Surr)76 -111
95 03/30/18 09:51 1Dibromofluoromethane (Surr)72 -116
106 03/30/18 09:51 1Toluene-d8 (Surr)80 -129
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240896/3
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240896
1,1,1-Trichloroethane 40.0 39.7 ug/Kg 99 69 -135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2,2-Tetrachloroethane 40.0 36.8 ug/Kg 92 71 -125
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 44.3 ug/Kg 111 61 -137
1,1,2-Trichloroethane 40.0 40.5 ug/Kg 101 78 -118
1,1-Dichloroethane 40.0 40.1 ug/Kg 100 67 -129
1,1-Dichloroethene 40.0 43.0 ug/Kg 108 59 -128
1,2,4-Trichlorobenzene 40.0 38.8 ug/Kg 97 65 -135
1,2-Dibromo-3-Chloropropane 40.0 26.9 ug/Kg 67 54 -129
1,2-Dichlorobenzene 40.0 40.4 ug/Kg 101 78 -118
1,2-Dichloroethane 40.0 37.4 ug/Kg 94 67 -123
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240896/3
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240896
1,2-Dichloropropane 40.0 39.5 ug/Kg 99 80 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,3-Dichlorobenzene 40.0 42.2 ug/Kg 105 78 -118
1,4-Dichlorobenzene 40.0 41.7 ug/Kg 104 78 -118
2-Butanone (MEK)40.0 30.9 ug/Kg 77 30 -150
2-Hexanone 40.0 33.9 ug/Kg 85 36 -150
4-Methyl-2-pentanone (MIBK)40.0 32.4 ug/Kg 81 62 -145
Acetone 40.0 41.2 ug/Kg 103 36 -150
Benzene 40.0 42.5 ug/Kg 106 78 -118
Bromoform 40.0 33.3 ug/Kg 83 56 -150
Bromomethane 40.0 32.1 ug/Kg 80 34 -150
Carbon disulfide 40.0 39.8 ug/Kg 99 66 -128
Carbon tetrachloride 40.0 39.1 ug/Kg 98 60 -137
Chlorobenzene 40.0 43.7 ug/Kg 109 78 -118
Chlorodibromomethane 40.0 36.6 ug/Kg 91 58 -140
Chloroform 40.0 39.6 ug/Kg 99 68 -124
Chloromethane 40.0 39.3 ug/Kg 98 46 -150
Chloroethane 40.0 37.9 ug/Kg 95 37 -150
cis-1,2-Dichloroethene 40.0 42.9 ug/Kg 107 71 -120
cis-1,3-Dichloropropene 40.0 37.6 ug/Kg 94 70 -131
Cyclohexane 40.0 41.3 ug/Kg 103 70 -133
Dichlorobromomethane 40.0 36.8 ug/Kg 92 66 -136
Dichlorodifluoromethane 40.0 56.0 ug/Kg 140 16 -150
Ethylbenzene 40.0 44.2 ug/Kg 110 78 -118
1,2-Dibromoethane 40.0 39.0 ug/Kg 98 78 -118
Isopropylbenzene 40.0 42.4 ug/Kg 106 76 -123
Methyl acetate 80.0 63.3 ug/Kg 79 64 -140
Methyl tert-butyl ether 40.0 36.4 ug/Kg 91 73 -121
Methylcyclohexane 40.0 44.2 ug/Kg 111 75 -124
Methylene Chloride 40.0 41.5 ug/Kg 104 68 -120
m-Xylene & p-Xylene 40.0 42.9 ug/Kg 107 78 -118
o-Xylene 40.0 42.9 ug/Kg 107 78 -118
Styrene 40.0 41.6 ug/Kg 104 79 -119
Tetrachloroethene 40.0 45.4 ug/Kg 113 78 -118
Toluene 40.0 43.5 ug/Kg 109 79 -121
trans-1,2-Dichloroethene 40.0 43.2 ug/Kg 108 71 -123
trans-1,3-Dichloropropene 40.0 36.1 ug/Kg 90 62 -133
Trichloroethene 40.0 43.2 ug/Kg 108 76 -120
Trichlorofluoromethane 40.0 42.4 ug/Kg 106 25 -150
Xylenes, Total 80.0 85.8 ug/Kg 107 78 -118
Vinyl chloride 40.0 40.4 ug/Kg 101 53 -148
1,2-Dichloroethane-d4 (Surr)62 -118
Surrogate
88
LCS LCS
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)76 -111
101Dibromofluoromethane (Surr)72 -116
107Toluene-d8 (Surr)80 -129
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-241049/6
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241049
RL MDL
1,1,1-Trichloroethane ND 5.0 2.5 ug/Kg 04/02/18 08:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.05.0 ug/Kg 04/02/18 08:53 11,1,2,2-Tetrachloroethane
ND 1.95.0 ug/Kg 04/02/18 08:53 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 2.45.0 ug/Kg 04/02/18 08:53 11,1,2-Trichloroethane
ND 1.85.0 ug/Kg 04/02/18 08:53 11,1-Dichloroethane
ND 2.95.0 ug/Kg 04/02/18 08:53 11,1-Dichloroethene
ND 1.65.0 ug/Kg 04/02/18 08:53 11,2,4-Trichlorobenzene
ND 3.15.0 ug/Kg 04/02/18 08:53 11,2-Dibromo-3-Chloropropane
ND 4.05.0 ug/Kg 04/02/18 08:53 11,2-Dichlorobenzene
ND 1.55.0 ug/Kg 04/02/18 08:53 11,2-Dichloroethane
ND 2.55.0 ug/Kg 04/02/18 08:53 11,2-Dichloropropane
ND 1.65.0 ug/Kg 04/02/18 08:53 11,3-Dichlorobenzene
ND 1.05.0 ug/Kg 04/02/18 08:53 11,4-Dichlorobenzene
ND 2.95.0 ug/Kg 04/02/18 08:53 12-Butanone (MEK)
ND 4.25.0 ug/Kg 04/02/18 08:53 12-Hexanone
ND 1.95.0 ug/Kg 04/02/18 08:53 14-Methyl-2-pentanone (MIBK)
ND 3.220 ug/Kg 04/02/18 08:53 1Acetone
ND 2.05.0 ug/Kg 04/02/18 08:53 1Benzene
ND 2.65.0 ug/Kg 04/02/18 08:53 1Bromoform
ND 4.55.0 ug/Kg 04/02/18 08:53 1Bromomethane
ND 3.05.0 ug/Kg 04/02/18 08:53 1Carbon disulfide
ND 3.35.0 ug/Kg 04/02/18 08:53 1Carbon tetrachloride
ND 1.65.0 ug/Kg 04/02/18 08:53 1Chlorobenzene
ND 2.45.0 ug/Kg 04/02/18 08:53 1Chlorodibromomethane
ND 2.15.0 ug/Kg 04/02/18 08:53 1Chloroform
ND 3.95.0 ug/Kg 04/02/18 08:53 1Chloromethane
ND 2.65.0 ug/Kg 04/02/18 08:53 1Chloroethane
ND 1.65.0 ug/Kg 04/02/18 08:53 1cis-1,2-Dichloroethene
ND 1.65.0 ug/Kg 04/02/18 08:53 1cis-1,3-Dichloropropene
ND 1.25.0 ug/Kg 04/02/18 08:53 1Cyclohexane
ND 2.45.0 ug/Kg 04/02/18 08:53 1Dichlorobromomethane
ND 2.95.0 ug/Kg 04/02/18 08:53 1Dichlorodifluoromethane
ND 2.25.0 ug/Kg 04/02/18 08:53 1Ethylbenzene
ND 2.75.0 ug/Kg 04/02/18 08:53 11,2-Dibromoethane
ND 2.35.0 ug/Kg 04/02/18 08:53 1Isopropylbenzene
ND 5.925 ug/Kg 04/02/18 08:53 1Methyl acetate
ND 3.75.0 ug/Kg 04/02/18 08:53 1Methyl tert-butyl ether
ND 2.15.0 ug/Kg 04/02/18 08:53 1Methylcyclohexane
2.45 J 2.45.0 ug/Kg 04/02/18 08:53 1Methylene Chloride
ND 1.35.0 ug/Kg 04/02/18 08:53 1Styrene
ND 2.05.0 ug/Kg 04/02/18 08:53 1Tetrachloroethene
ND 1.75.0 ug/Kg 04/02/18 08:53 1Toluene
ND 2.55.0 ug/Kg 04/02/18 08:53 1trans-1,2-Dichloroethene
ND 1.75.0 ug/Kg 04/02/18 08:53 1trans-1,3-Dichloropropene
ND 1.55.0 ug/Kg 04/02/18 08:53 1Trichloroethene
ND 1.55.0 ug/Kg 04/02/18 08:53 1Trichlorofluoromethane
ND 4.310 ug/Kg 04/02/18 08:53 1Xylenes, Total
ND 3.75.0 ug/Kg 04/02/18 08:53 1Vinyl chloride
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
1,2-Dichloroethane-d4 (Surr)94 62 -118 04/02/18 08:53 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 04/02/18 08:53 14-Bromofluorobenzene (Surr)76 -111
102 04/02/18 08:53 1Dibromofluoromethane (Surr)72 -116
114 04/02/18 08:53 1Toluene-d8 (Surr)80 -129
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241049/3
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241049
1,1,1-Trichloroethane 40.0 40.2 ug/Kg 101 69 -135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2,2-Tetrachloroethane 40.0 30.9 ug/Kg 77 71 -125
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 45.6 ug/Kg 114 61 -137
1,1,2-Trichloroethane 40.0 35.9 ug/Kg 90 78 -118
1,1-Dichloroethane 40.0 41.4 ug/Kg 103 67 -129
1,1-Dichloroethene 40.0 42.7 ug/Kg 107 59 -128
1,2,4-Trichlorobenzene 40.0 36.0 ug/Kg 90 65 -135
1,2-Dibromo-3-Chloropropane 40.0 23.5 ug/Kg 59 54 -129
1,2-Dichlorobenzene 40.0 38.3 ug/Kg 96 78 -118
1,2-Dichloroethane 40.0 35.9 ug/Kg 90 67 -123
1,2-Dichloropropane 40.0 38.8 ug/Kg 97 80 -121
1,3-Dichlorobenzene 40.0 41.0 ug/Kg 102 78 -118
1,4-Dichlorobenzene 40.0 39.8 ug/Kg 99 78 -118
2-Butanone (MEK)40.0 27.0 ug/Kg 67 30 -150
2-Hexanone 40.0 27.0 ug/Kg 68 36 -150
4-Methyl-2-pentanone (MIBK)40.0 26.5 ug/Kg 66 62 -145
Acetone 40.0 32.9 ug/Kg 82 36 -150
Benzene 40.0 42.8 ug/Kg 107 78 -118
Bromoform 40.0 28.6 ug/Kg 71 56 -150
Bromomethane 40.0 34.1 ug/Kg 85 34 -150
Carbon disulfide 40.0 38.4 ug/Kg 96 66 -128
Carbon tetrachloride 40.0 40.3 ug/Kg 101 60 -137
Chlorobenzene 40.0 41.7 ug/Kg 104 78 -118
Chlorodibromomethane 40.0 33.6 ug/Kg 84 58 -140
Chloroform 40.0 40.2 ug/Kg 101 68 -124
Chloromethane 40.0 37.8 ug/Kg 95 46 -150
Chloroethane 40.0 40.1 ug/Kg 100 37 -150
cis-1,2-Dichloroethene 40.0 43.0 ug/Kg 107 71 -120
cis-1,3-Dichloropropene 40.0 36.9 ug/Kg 92 70 -131
Cyclohexane 40.0 41.6 ug/Kg 104 70 -133
Dichlorobromomethane 40.0 35.8 ug/Kg 90 66 -136
Dichlorodifluoromethane 40.0 50.0 ug/Kg 125 16 -150
Ethylbenzene 40.0 41.7 ug/Kg 104 78 -118
1,2-Dibromoethane 40.0 34.1 ug/Kg 85 78 -118
Isopropylbenzene 40.0 40.8 ug/Kg 102 76 -123
Methyl acetate 80.0 56.0 ug/Kg 70 64 -140
Methyl tert-butyl ether 40.0 33.5 ug/Kg 84 73 -121
Methylcyclohexane 40.0 43.7 ug/Kg 109 75 -124
Methylene Chloride 40.0 40.1 ug/Kg 100 68 -120
m-Xylene & p-Xylene 40.0 40.9 ug/Kg 102 78 -118
o-Xylene 40.0 40.9 ug/Kg 102 78 -118
Styrene 40.0 39.1 ug/Kg 98 79 -119
Tetrachloroethene 40.0 43.8 ug/Kg 110 78 -118
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241049/3
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241049
Toluene 40.0 41.8 ug/Kg 104 79 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
trans-1,2-Dichloroethene 40.0 43.3 ug/Kg 108 71 -123
trans-1,3-Dichloropropene 40.0 32.6 ug/Kg 82 62 -133
Trichloroethene 40.0 44.4 ug/Kg 111 76 -120
Trichlorofluoromethane 40.0 46.6 ug/Kg 116 25 -150
Xylenes, Total 80.0 81.8 ug/Kg 102 78 -118
Vinyl chloride 40.0 41.0 ug/Kg 103 53 -148
1,2-Dichloroethane-d4 (Surr)62 -118
Surrogate
84
LCS LCS
Qualifier Limits%Recovery
894-Bromofluorobenzene (Surr)76 -111
97Dibromofluoromethane (Surr)72 -116
103Toluene-d8 (Surr)80 -129
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-241049/4
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241049
1,1,1-Trichloroethane 40.0 43.4 ug/Kg 108 69 -135 8 22
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 40.0 35.9 ug/Kg 90 71 -125 15 25
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 48.1 ug/Kg 120 61 -137 5 35
1,1,2-Trichloroethane 40.0 39.4 ug/Kg 99 78 -118 9 18
1,1-Dichloroethane 40.0 43.6 ug/Kg 109 67 -129 5 15
1,1-Dichloroethene 40.0 45.2 ug/Kg 113 59 -128 6 17
1,2,4-Trichlorobenzene 40.0 40.3 ug/Kg 101 65 -135 11 20
1,2-Dibromo-3-Chloropropane 40.0 27.6 ug/Kg 69 54 -129 16 20
1,2-Dichlorobenzene 40.0 41.6 ug/Kg 104 78 -118 8 15
1,2-Dichloroethane 40.0 38.7 ug/Kg 97 67 -123 8 15
1,2-Dichloropropane 40.0 41.8 ug/Kg 104 80 -121 7 15
1,3-Dichlorobenzene 40.0 43.7 ug/Kg 109 78 -118 6 15
1,4-Dichlorobenzene 40.0 43.0 ug/Kg 107 78 -118 8 15
2-Butanone (MEK)40.0 30.6 ug/Kg 76 30 -150 13 35
2-Hexanone 40.0 30.5 ug/Kg 76 36 -150 12 35
4-Methyl-2-pentanone (MIBK)40.0 30.4 ug/Kg 76 62 -145 14 27
Acetone 40.0 38.5 ug/Kg 96 36 -150 15 35
Benzene 40.0 46.0 ug/Kg 115 78 -118 7 15
Bromoform 40.0 31.5 ug/Kg 79 56 -150 10 16
Bromomethane 40.0 37.2 ug/Kg 93 34 -150 9 35
Carbon disulfide 40.0 42.0 ug/Kg 105 66 -128 9 27
Carbon tetrachloride 40.0 43.6 ug/Kg 109 60 -137 8 21
Chlorobenzene 40.0 44.2 ug/Kg 110 78 -118 6 15
Chlorodibromomethane 40.0 36.2 ug/Kg 90 58 -140 7 20
Chloroform 40.0 44.4 ug/Kg 111 68 -124 10 15
Chloromethane 40.0 38.9 ug/Kg 97 46 -150 3 35
Chloroethane 40.0 42.2 ug/Kg 105 37 -150 5 35
cis-1,2-Dichloroethene 40.0 45.4 ug/Kg 113 71 -120 5 15
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-241049/4
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241049
cis-1,3-Dichloropropene 40.0 40.0 ug/Kg 100 70 -131 8 21
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Cyclohexane 40.0 45.5 ug/Kg 114 70 -133 9 28
Dichlorobromomethane 40.0 39.7 ug/Kg 99 66 -136 10 15
Dichlorodifluoromethane 40.0 53.6 ug/Kg 134 16 -150 7 35
Ethylbenzene 40.0 45.1 ug/Kg 113 78 -118 8 15
1,2-Dibromoethane 40.0 38.2 ug/Kg 96 78 -118 11 15
Isopropylbenzene 40.0 43.6 ug/Kg 109 76 -123 7 19
Methyl acetate 80.0 63.5 ug/Kg 79 64 -140 13 24
Methyl tert-butyl ether 40.0 38.4 ug/Kg 96 73 -121 14 24
Methylcyclohexane 40.0 48.3 ug/Kg 121 75 -124 10 24
Methylene Chloride 40.0 42.5 ug/Kg 106 68 -120 6 19
m-Xylene & p-Xylene 40.0 43.3 ug/Kg 108 78 -118 6 16
o-Xylene 40.0 43.2 ug/Kg 108 78 -118 6 15
Styrene 40.0 41.6 ug/Kg 104 79 -119 6 15
Tetrachloroethene 40.0 46.0 ug/Kg 115 78 -118 5 20
Toluene 40.0 44.3 ug/Kg 111 79 -121 6 18
trans-1,2-Dichloroethene 40.0 47.5 ug/Kg 119 71 -123 9 15
trans-1,3-Dichloropropene 40.0 35.3 ug/Kg 88 62 -133 8 21
Trichloroethene 40.0 45.2 ug/Kg 113 76 -120 2 15
Trichlorofluoromethane 40.0 49.2 ug/Kg 123 25 -150 5 35
Xylenes, Total 80.0 86.5 ug/Kg 108 78 -118 6 15
Vinyl chloride 40.0 43.5 ug/Kg 109 53 -148 6 35
1,2-Dichloroethane-d4 (Surr)62 -118
Surrogate
92
LCSD LCSD
Qualifier Limits%Recovery
924-Bromofluorobenzene (Surr)76 -111
104Dibromofluoromethane (Surr)72 -116
105Toluene-d8 (Surr)80 -129
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
Client Sample ID: Method BlankLab Sample ID: MB 180-241037/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241401 Prep Batch: 241037
RL MDL
Acenaphthene ND 3.4 0.96 ug/Kg 04/02/18 03:39 04/05/18 14:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.733.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Acenaphthylene
ND 0.873.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Anthracene
ND 0.633.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Benzo[a]anthracene
ND 0.823.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Benzo[b]fluoranthene
ND 0.733.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Benzo[a]pyrene
ND 0.723.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Benzo[g,h,i]perylene
ND 0.663.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Chrysene
ND 0.753.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Dibenz(a,h)anthracene
ND 0.883.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Fluoranthene
ND 0.663.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Fluorene
ND 0.683.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Indeno[1,2,3-cd]pyrene
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-241037/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241401 Prep Batch: 241037
RL MDL
Naphthalene ND 3.4 0.65 ug/Kg 04/02/18 03:39 04/05/18 14:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.903.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Phenanthrene
ND 0.793.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Pyrene
ND 1.03.4 ug/Kg 04/02/18 03:39 04/05/18 14:24 1Benzo[k]fluoranthene
2-Fluorobiphenyl 78 34 -100 04/05/18 14:24 1
MB MB
Surrogate
04/02/18 03:39
Dil FacPreparedAnalyzedQualifierLimits%Recovery
90 04/02/18 03:39 04/05/18 14:24 1Nitrobenzene-d5 (Surr)33 -100
87 04/02/18 03:39 04/05/18 14:24 1Terphenyl-d14 (Surr)30 -100
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241037/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241401 Prep Batch: 241037
Acenaphthene 333 230 ug/Kg 69 43 -100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 333 251 ug/Kg 75 43 -100
Anthracene 333 246 ug/Kg 74 48 -100
Benzo[a]anthracene 333 254 ug/Kg 76 46 -100
Benzo[b]fluoranthene 333 250 ug/Kg 75 42 -100
Benzo[a]pyrene 333 275 ug/Kg 82 46 -100
Benzo[g,h,i]perylene 333 250 ug/Kg 75 45 -100
Chrysene 333 231 ug/Kg 69 47 -100
Dibenz(a,h)anthracene 333 258 ug/Kg 77 47 -100
Fluoranthene 333 257 ug/Kg 77 47 -100
Fluorene 333 237 ug/Kg 71 45 -100
Indeno[1,2,3-cd]pyrene 333 262 ug/Kg 79 46 -100
Naphthalene 333 213 ug/Kg 64 46 -100
Phenanthrene 333 237 ug/Kg 71 46 -100
Pyrene 333 233 ug/Kg 70 41 -100
Benzo[k]fluoranthene 333 255 ug/Kg 76 45 -100
2-Fluorobiphenyl 34 -100
Surrogate
71
LCS LCS
Qualifier Limits%Recovery
82Nitrobenzene-d5 (Surr)33 -100
87Terphenyl-d14 (Surr)30 -100
Client Sample ID: AH-07-0318-CLab Sample ID: 180-76196-4 MS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241401 Prep Batch: 241037
Acenaphthene ND 406 350 ug/Kg 86 43 -100☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene ND 406 366 ug/Kg 90 43 -100☼
Anthracene ND 406 346 ug/Kg 85 48 -100☼
Benzo[a]anthracene ND 406 368 ug/Kg 91 46 -100☼
Benzo[b]fluoranthene ND 406 355 ug/Kg 87 42 -100☼
Benzo[a]pyrene ND 406 366 ug/Kg 90 46 -100☼
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
Client Sample ID: AH-07-0318-CLab Sample ID: 180-76196-4 MS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241401 Prep Batch: 241037
Benzo[g,h,i]perylene ND 406 347 ug/Kg 86 45 -100☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Chrysene ND 406 335 ug/Kg 83 47 -100☼
Dibenz(a,h)anthracene ND 406 369 ug/Kg 91 47 -100☼
Fluoranthene ND 406 344 ug/Kg 85 47 -100☼
Fluorene ND 406 357 ug/Kg 88 45 -100☼
Indeno[1,2,3-cd]pyrene ND 406 389 ug/Kg 96 46 -100☼
Naphthalene ND 406 311 ug/Kg 76 46 -100☼
Phenanthrene ND 406 338 ug/Kg 83 46 -100☼
Pyrene ND 406 329 ug/Kg 81 41 -100☼
Benzo[k]fluoranthene ND 406 363 ug/Kg 89 45 -100☼
2-Fluorobiphenyl 34 -100
Surrogate
83
MS MS
Qualifier Limits%Recovery
94Nitrobenzene-d5 (Surr)33 -100
92Terphenyl-d14 (Surr)30 -100
Client Sample ID: AH-07-0318-CLab Sample ID: 180-76196-4 MSD
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241401 Prep Batch: 241037
Acenaphthene ND 410 331 ug/Kg 81 43 -100 5 27☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene ND 410 355 ug/Kg 86 43 -100 3 27☼
Anthracene ND 410 335 ug/Kg 82 48 -100 3 31☼
Benzo[a]anthracene ND 410 337 ug/Kg 82 46 -100 9 31☼
Benzo[b]fluoranthene ND 410 342 ug/Kg 83 42 -100 4 31☼
Benzo[a]pyrene ND 410 367 ug/Kg 89 46 -100 0 29☼
Benzo[g,h,i]perylene ND 410 352 ug/Kg 86 45 -100 1 38☼
Chrysene ND 410 316 ug/Kg 77 47 -100 6 31☼
Dibenz(a,h)anthracene ND 410 370 ug/Kg 90 47 -100 0 35☼
Fluoranthene ND 410 336 ug/Kg 82 47 -100 2 30☼
Fluorene ND 410 340 ug/Kg 83 45 -100 5 29☼
Indeno[1,2,3-cd]pyrene ND 410 378 ug/Kg 92 46 -100 3 35☼
Naphthalene ND 410 299 ug/Kg 73 46 -100 4 19☼
Phenanthrene ND 410 325 ug/Kg 79 46 -100 4 32☼
Pyrene ND 410 323 ug/Kg 79 41 -100 2 34☼
Benzo[k]fluoranthene ND 410 353 ug/Kg 86 45 -100 3 28☼
2-Fluorobiphenyl 34 -100
Surrogate
84
MSD MSD
Qualifier Limits%Recovery
97Nitrobenzene-d5 (Surr)33 -100
100Terphenyl-d14 (Surr)30 -100
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level
Client Sample ID: Method BlankLab Sample ID: MB 180-241088/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241375 Prep Batch: 241088
RL MDL
Acenaphthene ND 0.19 0.065 ug/L 04/02/18 11:28 04/05/18 14:33 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0650.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Acenaphthylene
ND 0.0490.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Anthracene
ND 0.0750.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Benzo[a]anthracene
ND 0.0970.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Benzo[b]fluoranthene
ND 0.0530.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Benzo[a]pyrene
ND 0.0690.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Benzo[g,h,i]perylene
ND 0.0810.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Chrysene
ND 0.0720.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Dibenz(a,h)anthracene
ND 0.0600.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Fluoranthene
ND 0.0690.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Fluorene
ND 0.0850.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Indeno[1,2,3-cd]pyrene
ND 0.0590.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Naphthalene
ND 0.0550.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Phenanthrene
ND 0.0540.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Pyrene
ND 0.0880.19 ug/L 04/02/18 11:28 04/05/18 14:33 1Benzo[k]fluoranthene
2-Fluorobiphenyl 71 26 -103 04/05/18 14:33 1
MB MB
Surrogate
04/02/18 11:28
Dil FacPreparedAnalyzedQualifierLimits%Recovery
73 04/02/18 11:28 04/05/18 14:33 1Nitrobenzene-d5 (Surr)30 -101
79 04/02/18 11:28 04/05/18 14:33 1Terphenyl-d14 (Surr)20 -119
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241088/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241375 Prep Batch: 241088
Acenaphthene 20.0 11.4 ug/L 57 49 -100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 20.0 12.1 ug/L 60 46 -100
Anthracene 20.0 11.4 ug/L 57 50 -100
Benzo[a]anthracene 20.0 12.0 ug/L 60 50 -100
Benzo[b]fluoranthene 20.0 12.2 ug/L 61 47 -100
Benzo[a]pyrene 20.0 12.4 ug/L 62 50 -100
Benzo[g,h,i]perylene 20.0 12.1 ug/L 60 48 -100
Chrysene 20.0 11.6 ug/L 58 49 -100
Dibenz(a,h)anthracene 20.0 11.8 ug/L 59 49 -100
Fluoranthene 20.0 13.3 ug/L 67 51 -100
Fluorene 20.0 12.0 ug/L 60 49 -100
Indeno[1,2,3-cd]pyrene 20.0 12.5 ug/L 62 49 -100
Naphthalene 20.0 11.9 ug/L 60 51 -100
Phenanthrene 20.0 11.4 ug/L 57 50 -100
Pyrene 20.0 12.8 ug/L 64 47 -100
Benzo[k]fluoranthene 20.0 12.1 ug/L 60 47 -100
2-Fluorobiphenyl 26 -103
Surrogate
60
LCS LCS
Qualifier Limits%Recovery
70Nitrobenzene-d5 (Surr)30 -101
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8270D LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241088/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241375 Prep Batch: 241088
Terphenyl-d14 (Surr)20 -119
Surrogate
71
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-241088/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241375 Prep Batch: 241088
Acenaphthene 20.0 11.9 ug/L 60 49 -100 4 15
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 20.0 12.7 ug/L 63 46 -100 5 15
Anthracene 20.0 12.0 ug/L 60 50 -100 5 15
Benzo[a]anthracene 20.0 11.8 ug/L 59 50 -100 2 15
Benzo[b]fluoranthene 20.0 12.3 ug/L 62 47 -100 1 16
Benzo[a]pyrene 20.0 12.6 ug/L 63 50 -100 1 15
Benzo[g,h,i]perylene 20.0 12.0 ug/L 60 48 -100 0 17
Chrysene 20.0 11.4 ug/L 57 49 -100 2 15
Dibenz(a,h)anthracene 20.0 12.3 ug/L 61 49 -100 4 17
Fluoranthene 20.0 13.7 ug/L 68 51 -100 2 15
Fluorene 20.0 12.3 ug/L 62 49 -100 3 17
Indeno[1,2,3-cd]pyrene 20.0 12.6 ug/L 63 49 -100 1 17
Naphthalene 20.0 12.2 ug/L 61 51 -100 2 15
Phenanthrene 20.0 12.0 ug/L 60 50 -100 5 15
Pyrene 20.0 12.5 ug/L 63 47 -100 3 18
Benzo[k]fluoranthene 20.0 12.3 ug/L 62 47 -100 2 16
2-Fluorobiphenyl 26 -103
Surrogate
62
LCSD LCSD
Qualifier Limits%Recovery
70Nitrobenzene-d5 (Surr)30 -101
69Terphenyl-d14 (Surr)20 -119
Method: 8081B_LL - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 180-241038/1-B
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 242257 Prep Batch: 241038
RL MDL
Aldrin ND 0.042 0.013 ug/Kg 04/02/18 03:41 04/16/18 13:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0100.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1alpha-BHC
ND 0.0110.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1beta-BHC
ND 0.0100.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1cis-Chlordane
ND 0.180.42 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Chlordane (technical)
ND 0.0110.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 14,4'-DDD
ND 0.0130.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1delta-BHC
ND 0.00850.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 14,4'-DDE
ND 0.0160.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 14,4'-DDT
ND 0.0100.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Dieldrin
ND 0.0110.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Endosulfan I
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 8081B_LL - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-241038/1-B
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 242257 Prep Batch: 241038
RL MDL
Endosulfan II ND 0.042 0.0092 ug/Kg 04/02/18 03:41 04/16/18 13:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0110.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Endosulfan sulfate
ND 0.0160.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Endrin
ND 0.0150.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Endrin aldehyde
ND 0.0140.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1gamma-BHC (Lindane)
ND 0.0150.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Endrin ketone
ND 0.00970.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1trans-Chlordane
ND 0.0130.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Heptachlor
ND 0.0110.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Heptachlor epoxide
ND 0.0160.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Methoxychlor
ND 0.00930.042 ug/Kg 04/02/18 03:41 04/16/18 13:39 1oxy-Chlordane
ND 1.11.7 ug/Kg 04/02/18 03:41 04/16/18 13:39 1Toxaphene
Tetrachloro-m-xylene 80 26 -120 04/16/18 13:39 1
MB MB
Surrogate
04/02/18 03:41
Dil FacPreparedAnalyzedQualifierLimits%Recovery
92 04/02/18 03:41 04/16/18 13:39 1Tetrachloro-m-xylene 26 -120
85 04/02/18 03:41 04/16/18 13:39 1DCB Decachlorobiphenyl (Surr)33 -137
83 04/02/18 03:41 04/16/18 13:39 1DCB Decachlorobiphenyl (Surr)33 -137
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241038/2-B
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 242257 Prep Batch: 241038
Aldrin 1.67 1.19 ug/Kg 71 37 -121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
alpha-BHC 1.67 1.10 ug/Kg 66 39 -114
beta-BHC 1.67 1.24 ug/Kg 74 37 -113
cis-Chlordane 1.67 1.23 ug/Kg 74 35 -121
4,4'-DDD 1.67 1.46 ug/Kg 87 48 -119
delta-BHC 1.67 0.592 ug/Kg 36 12 -100
4,4'-DDE 1.67 1.34 ug/Kg 80 47 -118
4,4'-DDT 1.67 1.34 ug/Kg 81 29 -123
Dieldrin 1.67 1.31 ug/Kg 79 46 -119
Endosulfan I 1.67 1.31 ug/Kg 78 36 -120
Endosulfan II 1.67 1.25 ug/Kg 75 46 -114
Endosulfan sulfate 1.67 0.906 ug/Kg 54 40 -104
Endrin 1.67 1.28 ug/Kg 77 45 -118
Endrin aldehyde 1.67 1.28 ug/Kg 77 39 -109
gamma-BHC (Lindane)1.67 1.11 ug/Kg 67 38 -115
Endrin ketone 1.67 1.32 ug/Kg 79 44 -114
trans-Chlordane 1.67 1.25 ug/Kg 75 36 -121
Heptachlor 1.67 1.26 ug/Kg 76 38 -122
Heptachlor epoxide 1.67 1.24 ug/Kg 74 36 -123
Methoxychlor 1.67 1.43 ug/Kg 86 34 -126
Tetrachloro-m-xylene 26 -120
Surrogate
79
LCS LCS
Qualifier Limits%Recovery
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 8081B_LL - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241038/2-B
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 242257 Prep Batch: 241038
Tetrachloro-m-xylene 26 -120
Surrogate
91
LCS LCS
Qualifier Limits%Recovery
85DCB Decachlorobiphenyl (Surr)33 -137
86DCB Decachlorobiphenyl (Surr)33 -137
Client Sample ID: AH-06-0318-CLab Sample ID: 180-76196-8 MS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 242257 Prep Batch: 241038
Aldrin ND F1 2.04 0.624 F1 ug/Kg 31 37 -121☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
alpha-BHC ND F1 2.04 0.572 F1 ug/Kg 28 39 -114☼
beta-BHC ND F1 2.04 0.652 F1 ug/Kg 32 37 -113☼
cis-Chlordane ND F1 2.04 0.659 F1 ug/Kg 32 35 -121☼
4,4'-DDD ND F1 2.04 0.738 F1 ug/Kg 36 48 -119☼
delta-BHC ND 2.04 0.352 ug/Kg 17 12 -100☼
4,4'-DDE 0.016 J F1 2.04 0.687 F1 ug/Kg 33 47 -118☼
4,4'-DDT ND 2.04 0.668 ug/Kg 33 29 -123☼
Dieldrin ND F1 2.04 0.667 F1 ug/Kg 33 46 -119☼
Endosulfan I ND F1 2.04 0.684 F1 ug/Kg 34 36 -120☼
Endosulfan II ND F1 2.04 0.653 F1 ug/Kg 32 46 -114☼
Endosulfan sulfate ND F1 2.04 0.550 F1 ug/Kg 27 40 -104☼
Endrin ND F1 2.04 0.637 F1 ug/Kg 31 45 -118☼
Endrin aldehyde 0.018 J F1 p 2.04 0.743 F1 ug/Kg 36 39 -109☼
gamma-BHC (Lindane)ND F1 2.04 0.595 F1 ug/Kg 29 38 -115☼
Endrin ketone ND F1 2.04 0.673 F1 ug/Kg 33 44 -114☼
trans-Chlordane ND F1 2.04 0.666 F1 ug/Kg 33 36 -121☼
Heptachlor ND F1 2.04 0.666 F1 ug/Kg 33 38 -122☼
Heptachlor epoxide ND F1 2.04 0.721 F1 ug/Kg 35 36 -123☼
Methoxychlor ND 2.04 0.693 ug/Kg 34 34 -126☼
Tetrachloro-m-xylene 26 -120
Surrogate
35
MS MS
Qualifier Limits%Recovery
38Tetrachloro-m-xylene 26 -120
38DCB Decachlorobiphenyl (Surr)33 -137
37DCB Decachlorobiphenyl (Surr)33 -137
Client Sample ID: AH-06-0318-CLab Sample ID: 180-76196-8 MSD
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 242257 Prep Batch: 241038
Aldrin ND F1 2.04 0.771 ug/Kg 38 37 -121 21 33☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
alpha-BHC ND F1 2.04 0.701 F1 ug/Kg 34 39 -114 20 38☼
beta-BHC ND F1 2.04 0.810 ug/Kg 40 37 -113 22 37☼
cis-Chlordane ND F1 2.04 0.787 ug/Kg 39 35 -121 18 36☼
4,4'-DDD ND F1 2.04 0.915 F1 ug/Kg 45 48 -119 21 32☼
delta-BHC ND 2.04 0.431 ug/Kg 21 12 -100 20 34☼
4,4'-DDE 0.016 J F1 2.04 0.839 F1 ug/Kg 40 47 -118 20 31☼
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 8081B_LL - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: AH-06-0318-CLab Sample ID: 180-76196-8 MSD
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 242257 Prep Batch: 241038
4,4'-DDT ND 2.04 0.805 ug/Kg 39 29 -123 19 38☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Dieldrin ND F1 2.04 0.804 F1 ug/Kg 39 46 -119 19 32☼
Endosulfan I ND F1 2.04 0.846 ug/Kg 41 36 -120 21 39☼
Endosulfan II ND F1 2.04 0.791 F1 ug/Kg 39 46 -114 19 29☼
Endosulfan sulfate ND F1 2.04 0.669 F1 ug/Kg 33 40 -104 19 34☼
Endrin ND F1 2.04 0.775 F1 ug/Kg 38 45 -118 20 31☼
Endrin aldehyde 0.018 J F1 p 2.04 0.888 ug/Kg 43 39 -109 18 37☼
gamma-BHC (Lindane)ND F1 2.04 0.724 F1 ug/Kg 35 38 -115 20 38☼
Endrin ketone ND F1 2.04 0.813 F1 ug/Kg 40 44 -114 19 34☼
trans-Chlordane ND F1 2.04 0.799 ug/Kg 39 36 -121 18 35☼
Heptachlor ND F1 2.04 0.817 ug/Kg 40 38 -122 20 38☼
Heptachlor epoxide ND F1 2.04 0.862 ug/Kg 42 36 -123 18 35☼
Methoxychlor ND 2.04 0.829 ug/Kg 41 34 -126 18 35☼
Tetrachloro-m-xylene X 26 -120
Surrogate
11
MSD MSD
Qualifier Limits%Recovery
12 XTetrachloro-m-xylene 26 -120
13 XDCB Decachlorobiphenyl (Surr)33 -137
12 XDCB Decachlorobiphenyl (Surr)33 -137
Method: EPA 8081B LL - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 180-240746/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241080 Prep Batch: 240746
RL MDL
Aldrin ND 0.0013 0.00012 ug/L 03/28/18 10:45 04/02/18 14:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.000120.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1alpha-BHC
ND 0.000150.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1beta-BHC
ND 0.000140.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1cis-Chlordane
ND 0.00150.013 ug/L 03/28/18 10:45 04/02/18 14:25 1Chlordane (technical)
ND 0.000210.0013 ug/L 03/28/18 10:45 04/02/18 14:25 14,4'-DDD
ND 0.000340.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1delta-BHC
ND 0.000110.0013 ug/L 03/28/18 10:45 04/02/18 14:25 14,4'-DDE
ND 0.000300.0013 ug/L 03/28/18 10:45 04/02/18 14:25 14,4'-DDT
ND 0.000130.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Dieldrin
ND 0.000150.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Endosulfan I
ND 0.000120.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Endosulfan II
ND 0.000290.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Endosulfan sulfate
ND 0.000230.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Endrin
ND 0.000240.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Endrin aldehyde
ND 0.000120.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1gamma-BHC (Lindane)
ND 0.000170.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Endrin ketone
ND 0.000120.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1trans-Chlordane
ND 0.000450.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Heptachlor
ND 0.000140.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Heptachlor epoxide
ND 0.000340.0013 ug/L 03/28/18 10:45 04/02/18 14:25 1Methoxychlor
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8081B LL - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-240746/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241080 Prep Batch: 240746
RL MDL
oxy-Chlordane ND 0.017 0.00021 ug/L 03/28/18 10:45 04/02/18 14:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0110.10 ug/L 03/28/18 10:45 04/02/18 14:25 1Toxaphene
Tetrachloro-m-xylene 79 41 -124 04/02/18 14:25 1
MB MB
Surrogate
03/28/18 10:45
Dil FacPreparedAnalyzedQualifierLimits%Recovery
86 03/28/18 10:45 04/02/18 14:25 1Tetrachloro-m-xylene 41 -124
86 03/28/18 10:45 04/02/18 14:25 1DCB Decachlorobiphenyl (Surr)64 -126
92 03/28/18 10:45 04/02/18 14:25 1DCB Decachlorobiphenyl (Surr)64 -126
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240746/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241080 Prep Batch: 240746
Aldrin 0.0250 0.0206 ug/L 83 50 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
alpha-BHC 0.0250 0.0182 ug/L 73 52 -110
beta-BHC 0.0250 0.0195 ug/L 78 50 -112
cis-Chlordane 0.0250 0.0214 ug/L 86 49 -118
4,4'-DDD 0.0250 0.0214 ug/L 86 64 -109
delta-BHC 0.0250 0.00864 ug/L 35 10 -100
4,4'-DDE 0.0250 0.0208 ug/L 83 59 -116
4,4'-DDT 0.0250 0.0200 ug/L 80 43 -114
Dieldrin 0.0250 0.0198 ug/L 79 61 -113
Endosulfan I 0.0250 0.0220 ug/L 88 49 -119
Endosulfan II 0.0250 0.0200 ug/L 80 61 -109
Endosulfan sulfate 0.0250 0.0153 ug/L 61 48 -100
Endrin 0.0250 0.0190 ug/L 76 61 -115
Endrin aldehyde 0.0250 0.0220 ug/L 88 50 -111
gamma-BHC (Lindane)0.0250 0.0190 ug/L 76 51 -112
Endrin ketone 0.0250 0.0199 ug/L 80 51 -117
trans-Chlordane 0.0250 0.0205 ug/L 82 49 -119
Heptachlor 0.0250 0.0216 ug/L 86 55 -118
Heptachlor epoxide 0.0250 0.0215 ug/L 86 50 -123
Methoxychlor 0.0250 0.0206 ug/L 82 49 -119
Tetrachloro-m-xylene 41 -124
Surrogate
82
LCS LCS
Qualifier Limits%Recovery
90Tetrachloro-m-xylene 41 -124
81DCB Decachlorobiphenyl (Surr)64 -126
85DCB Decachlorobiphenyl (Surr)64 -126
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-240746/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241080 Prep Batch: 240746
Aldrin 0.0250 0.0223 ug/L 89 50 -120 8 22
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
alpha-BHC 0.0250 0.0191 ug/L 76 52 -110 5 20
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 8081B LL - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-240746/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241080 Prep Batch: 240746
beta-BHC 0.0250 0.0200 ug/L 80 50 -112 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
cis-Chlordane 0.0250 0.0219 ug/L 87 49 -118 2 24
4,4'-DDD 0.0250 0.0236 ug/L 94 64 -109 10 19
delta-BHC 0.0250 0.00908 ug/L 36 10 -100 5 21
4,4'-DDE 0.0250 0.0224 ug/L 90 59 -116 7 20
4,4'-DDT 0.0250 0.0213 ug/L 85 43 -114 6 22
Dieldrin 0.0250 0.0212 ug/L 85 61 -113 7 20
Endosulfan I 0.0250 0.0224 ug/L 90 49 -119 2 22
Endosulfan II 0.0250 0.0216 ug/L 86 61 -109 8 19
Endosulfan sulfate 0.0250 0.0165 ug/L 66 48 -100 8 21
Endrin 0.0250 0.0207 ug/L 83 61 -115 9 20
Endrin aldehyde 0.0250 0.0243 ug/L 97 50 -111 10 21
gamma-BHC (Lindane)0.0250 0.0203 ug/L 81 51 -112 7 20
Endrin ketone 0.0250 0.0218 ug/L 87 51 -117 9 28
trans-Chlordane 0.0250 0.0216 ug/L 87 49 -119 5 25
Heptachlor 0.0250 0.0222 ug/L 89 55 -118 3 21
Heptachlor epoxide 0.0250 0.0224 ug/L 89 50 -123 4 22
Methoxychlor 0.0250 0.0218 ug/L 87 49 -119 6 22
Tetrachloro-m-xylene 41 -124
Surrogate
88
LCSD LCSD
Qualifier Limits%Recovery
96Tetrachloro-m-xylene 41 -124
90DCB Decachlorobiphenyl (Surr)64 -126
87DCB Decachlorobiphenyl (Surr)64 -126
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-241695/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241911 Prep Batch: 241695
RL MDL
Antimony ND 0.10 0.031 mg/Kg 04/09/18 16:04 04/11/18 00:56 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0130.050 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Arsenic
ND 0.00380.050 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Beryllium
ND 0.00850.050 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Cadmium
ND 0.0330.10 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Chromium
ND 0.0570.10 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Copper
ND 0.0180.050 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Lead
ND 0.0800.25 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Manganese
ND 0.0310.050 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Nickel
ND 0.0300.25 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Selenium
ND 0.00700.050 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Silver
ND 0.00650.050 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Thallium
ND 0.170.25 mg/Kg 04/09/18 16:04 04/11/18 00:56 1Zinc
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241695/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241911 Prep Batch: 241695
Antimony 25.0 22.6 mg/Kg 90 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 2.00 1.79 mg/Kg 90 80 -120
Beryllium 2.50 2.38 mg/Kg 95 80 -120
Cadmium 2.50 2.48 mg/Kg 99 80 -120
Chromium 10.0 11.1 mg/Kg 111 80 -120
Copper 12.5 11.7 mg/Kg 94 80 -120
Lead 1.00 1.01 mg/Kg 101 80 -120
Manganese 25.0 23.6 mg/Kg 94 80 -120
Nickel 25.0 23.1 mg/Kg 92 80 -120
Selenium 0.500 0.432 mg/Kg 86 80 -120
Silver 2.50 2.57 mg/Kg 103 80 -120
Thallium 2.50 2.52 mg/Kg 101 80 -120
Zinc 25.0 22.3 mg/Kg 89 80 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 180-241695/19-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241911 Prep Batch: 241695
Antimony 0.300 0.142 J mg/Kg 47
Analyte
LCSSRM LCSSRM
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 6.23 4.94 mg/Kg 79
Beryllium 1.00 0.323 mg/Kg 32
Cadmium 0.148 0.140 mg/Kg 94
Chromium 40.9 18.6 mg/Kg 45
Copper 10.0 8.82 mg/Kg 88
Lead 11.7 7.74 mg/Kg 66
Manganese 235 99.0 mg/Kg 42
Nickel 23.0 17.0 mg/Kg 74
Selenium 0.193 0.455 J mg/Kg 236
Silver 0.300 0.0348 J mg/Kg 12
Thallium 0.500 0.0838 J mg/Kg 17
Zinc 48.9 29.6 mg/Kg 60
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 180-241273/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241400 Prep Batch: 241273
RL MDL
Mercury ND 0.017 0.0037 mg/Kg 04/04/18 08:35 04/05/18 08:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241273/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241400 Prep Batch: 241273
Mercury 0.208 0.225 mg/Kg 108 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 7471B - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 180-241273/3-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241400 Prep Batch: 241273
Mercury 0.0400 0.0457 mg/Kg 114
Analyte
LCSSRM LCSSRM
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: EPA 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-240953/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 241140 Prep Batch: 240953
RL MDL
Antimony ND 2.0 1.1 ug/L 03/30/18 13:04 03/31/18 11:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.321.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Arsenic
ND 0.0571.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Beryllium
ND 0.131.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Cadmium
ND 0.632.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Chromium
ND 1.32.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Copper
ND 0.0941.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Lead
ND 1.45.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Manganese
ND 0.311.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Nickel
ND 0.815.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Selenium
ND 0.121.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Silver
ND 0.0631.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Thallium
ND 2.45.0 ug/L 03/30/18 13:04 03/31/18 11:51 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240953/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 241140 Prep Batch: 240953
Antimony 500 535 ug/L 107 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 40.0 47.0 ug/L 118 80 -120
Beryllium 50.0 51.6 ug/L 103 80 -120
Cadmium 50.0 53.2 ug/L 106 80 -120
Chromium 200 226 ug/L 113 80 -120
Copper 250 235 ug/L 94 80 -120
Lead 20.0 20.5 ug/L 103 80 -120
Manganese 500 546 ug/L 109 80 -120
Nickel 500 448 ug/L 90 80 -120
Selenium 10.0 10.6 ug/L 106 80 -120
Silver 50.0 50.5 ug/L 101 80 -120
Thallium 50.0 47.4 ug/L 95 80 -120
Zinc 500 438 ug/L 88 80 -120
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 180-241732/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241904 Prep Batch: 241732
RL MDL
Mercury ND 0.20 0.065 ug/L 04/10/18 11:20 04/11/18 10:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241732/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241904 Prep Batch: 241732
Mercury 2.50 2.76 ug/L 110 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: 1664B - HEM and SGT-HEM
Client Sample ID: Method BlankLab Sample ID: MB 400-392275/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392295 Prep Batch: 392275
RL MDL
Total Petroleum Hydrocarbons
(SGT-HEM)
ND 4.0 1.4 mg/L 04/01/18 14:43 04/02/18 09:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-392275/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392295 Prep Batch: 392275
Total Petroleum Hydrocarbons
(SGT-HEM)
20.0 15.80 mg/L 79 64 -132
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: 2540G - SM 2540G
Client Sample ID: AH-04-0318-CLab Sample ID: 180-76196-16 DU
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240793
Percent Moisture 58.8 58.0 %1 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 41.2 42.0 %2 20
Client Sample ID: AH-05-0318-C-DUPLab Sample ID: 180-76196-22 DU
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240793
Percent Moisture 76.1 75.9 %0.4 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 23.9 24.1 %1 20
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: 2540G - SM 2540G (Continued)
Client Sample ID: AH-07-0318-CLab Sample ID: 180-76196-4 DU
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240823
Percent Moisture 19.0 19.5 %2 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 81.0 80.5 %0.6 20
Client Sample ID: AH-02-0318-CLab Sample ID: 180-76196-12 DU
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240823
Percent Moisture 42.8 42.2 %1 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 57.2 57.8 %0.9 20
Method: EPA 7196A - Chromium, Hexavalent
Client Sample ID: Method BlankLab Sample ID: MB 180-240705/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240705
RL MDL
Cr (VI)ND 0.010 0.0032 mg/L 03/28/18 12:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240705/11
Matrix: Water Prep Type: Total/NA
Analysis Batch: 240705
Cr (VI)0.250 0.228 mg/L 91 85 -115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 180-240858/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240949 Prep Batch: 240858
RL MDL
Cr (VI)ND 0.40 0.11 mg/Kg 03/29/18 14:32 03/30/18 13:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 180-240858/3-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240949 Prep Batch: 240858
Cr (VI)708 605 mg/Kg 85 80 -120
Analyte
LCSI LCSI
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSS 180-240858/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240949 Prep Batch: 240858
Cr (VI)20.0 18.8 mg/Kg 94 80 -120
Analyte
LCSS LCSS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: EPA 7196A - Chromium, Hexavalent (Continued)
Client Sample ID: AH-04-0318-CLab Sample ID: 180-76196-16 MSI
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240949 Prep Batch: 240858
Cr (VI)ND 1680 1310 mg/Kg 78 75 -125☼
Analyte
MSI MSI
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: AH-04-0318-CLab Sample ID: 180-76196-16 MSS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240949 Prep Batch: 240858
Cr (VI)ND 47.6 39.4 mg/Kg 83 75 -125☼
Analyte
MSS MSS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: AH-04-0318-CLab Sample ID: 180-76196-16 DU
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240949 Prep Batch: 240858
Cr (VI)ND ND mg/Kg NC 20☼
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: EPA 9071B - HEM and SGT-HEM
Client Sample ID: Method BlankLab Sample ID: MB 180-241004/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241091 Prep Batch: 241004
RL MDL
Total Petroleum Hydrocarbons
(SGT-HEM)
ND 170 83 mg/Kg 03/31/18 06:25 04/03/18 08:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241004/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241091 Prep Batch: 241004
Total Petroleum Hydrocarbons
(SGT-HEM)
667 480 mg/Kg 72 64 -132
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-241004/3-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241091 Prep Batch: 241004
Total Petroleum Hydrocarbons
(SGT-HEM)
667 480 mg/Kg 72 64 -132 0 34
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: Lloyd Kahn - Organic Carbon, Total (TOC)
Client Sample ID: Method BlankLab Sample ID: MB 180-240909/3
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240909
RL MDL
Total Organic Carbon - Duplicates ND 1000 750 mg/Kg 03/29/18 13:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-240909/4
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 240909
Total Organic Carbon -
Duplicates
37800 31400 mg/Kg 83 75 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 180-241158/3
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241158
RL MDL
Total Organic Carbon - Duplicates ND 1000 750 mg/Kg 04/02/18 13:37 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241158/4
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 241158
Total Organic Carbon -
Duplicates
34500 34500 mg/Kg 100 75 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: SM 5310C - Total Organic Carbon
Client Sample ID: Method BlankLab Sample ID: MB 180-241245/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241245
RL MDL
Total Organic Carbon - Duplicates ND 1.0 0.51 mg/L 04/03/18 15:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-241245/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241245
Total Organic Carbon -
Duplicates
20.0 19.1 mg/L 96 85 -115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-241245/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 241245
Total Organic Carbon -
Duplicates
20.0 19.1 mg/L 96 85 -115 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC/MS VOA
Analysis Batch: 240660
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment EPA 8260B 240706180-76196-13 AH-04-0318-G1 Total/NA
Sediment EPA 8260B 240706180-76196-14 AH-04-0318-G2 Total/NA
Sediment EPA 8260B 240706180-76196-15 AH-04-0318-G3 Total/NA
Sediment EPA 8260B 240706180-76196-17 AH-05-0318-G1 Total/NA
Sediment EPA 8260B 240706180-76196-18 AH-05-0318-G1-DUP Total/NA
Sediment EPA 8260B 240706180-76196-19 AH-05-0318-G2 Total/NA
Sediment EPA 8260B 240706180-76196-20 AH-05-0318-G3 Total/NA
Sediment EPA 8260BMB 180-240660/9 Method Blank Total/NA
Sediment EPA 8260BLCS 180-240660/3 Lab Control Sample Total/NA
Prep Batch: 240706
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 5035180-76196-13 AH-04-0318-G1 Total/NA
Sediment 5035180-76196-14 AH-04-0318-G2 Total/NA
Sediment 5035180-76196-15 AH-04-0318-G3 Total/NA
Sediment 5035180-76196-17 AH-05-0318-G1 Total/NA
Sediment 5035180-76196-18 AH-05-0318-G1-DUP Total/NA
Sediment 5035180-76196-19 AH-05-0318-G2 Total/NA
Sediment 5035180-76196-20 AH-05-0318-G3 Total/NA
Analysis Batch: 240736
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water EPA 8260B180-76196-23 TB-02-0318 Total/NA
Water EPA 8260BMB 180-240736/5 Method Blank Total/NA
Water EPA 8260BLCS 180-240736/3 Lab Control Sample Total/NA
Analysis Batch: 240865
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water EPA 8260B180-76196-24 EB-02-0318 Total/NA
Water EPA 8260BMB 180-240865/6 Method Blank Total/NA
Water EPA 8260BLCS 180-240865/4 Lab Control Sample Total/NA
Analysis Batch: 240896
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment EPA 8260B 240903180-76196-1 AH-07-0318-G1 Total/NA
Sediment EPA 8260B 240903180-76196-2 AH-07-0318-G2 Total/NA
Sediment EPA 8260B 240903180-76196-5 AH-06-0318-G1 Total/NA
Sediment EPA 8260B 240903180-76196-6 AH-06-0318-G2 Total/NA
Sediment EPA 8260B 240903180-76196-7 AH-06-0318-G3 Total/NA
Sediment EPA 8260B 240903180-76196-9 AH-02-0318-G1 Total/NA
Sediment EPA 8260B 240903180-76196-10 AH-02-0318-G2 Total/NA
Sediment EPA 8260BMB 180-240896/7 Method Blank Total/NA
Sediment EPA 8260BLCS 180-240896/3 Lab Control Sample Total/NA
Prep Batch: 240903
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 5035180-76196-1 AH-07-0318-G1 Total/NA
Sediment 5035180-76196-2 AH-07-0318-G2 Total/NA
Sediment 5035180-76196-3 AH-07-0318-G3 Total/NA
Sediment 5035180-76196-5 AH-06-0318-G1 Total/NA
Sediment 5035180-76196-6 AH-06-0318-G2 Total/NA
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QC Association Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC/MS VOA (Continued)
Prep Batch: 240903 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 5035180-76196-7 AH-06-0318-G3 Total/NA
Sediment 5035180-76196-9 AH-02-0318-G1 Total/NA
Sediment 5035180-76196-10 AH-02-0318-G2 Total/NA
Sediment 5035180-76196-11 AH-02-0318-G3 Total/NA
Analysis Batch: 241049
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment EPA 8260B 240903180-76196-3 AH-07-0318-G3 Total/NA
Sediment EPA 8260B 240903180-76196-11 AH-02-0318-G3 Total/NA
Sediment EPA 8260BMB 180-241049/6 Method Blank Total/NA
Sediment EPA 8260BLCS 180-241049/3 Lab Control Sample Total/NA
Sediment EPA 8260BLCSD 180-241049/4 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 241037
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 3541180-76196-4 AH-07-0318-C Total/NA
Sediment 3541180-76196-8 AH-06-0318-C Total/NA
Sediment 3541180-76196-12 AH-02-0318-C Total/NA
Sediment 3541180-76196-16 AH-04-0318-C Total/NA
Sediment 3541180-76196-21 AH-05-0318-C Total/NA
Sediment 3541180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 3541MB 180-241037/1-A Method Blank Total/NA
Sediment 3541LCS 180-241037/2-A Lab Control Sample Total/NA
Sediment 3541180-76196-4 MS AH-07-0318-C Total/NA
Sediment 3541180-76196-4 MSD AH-07-0318-C Total/NA
Prep Batch: 241088
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520C180-76196-24 EB-02-0318 Total/NA
Water 3520CMB 180-241088/1-A Method Blank Total/NA
Water 3520CLCS 180-241088/2-A Lab Control Sample Total/NA
Water 3520CLCSD 180-241088/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 241375
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water EPA 8270D LL 241088180-76196-24 EB-02-0318 Total/NA
Water EPA 8270D LL 241088MB 180-241088/1-A Method Blank Total/NA
Water EPA 8270D LL 241088LCS 180-241088/2-A Lab Control Sample Total/NA
Water EPA 8270D LL 241088LCSD 180-241088/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 241401
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 8270D LL 241037180-76196-4 AH-07-0318-C Total/NA
Sediment 8270D LL 241037180-76196-8 AH-06-0318-C Total/NA
Sediment 8270D LL 241037180-76196-12 AH-02-0318-C Total/NA
Sediment 8270D LL 241037180-76196-16 AH-04-0318-C Total/NA
Sediment 8270D LL 241037180-76196-21 AH-05-0318-C Total/NA
Sediment 8270D LL 241037180-76196-22 AH-05-0318-C-DUP Total/NA
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QC Association Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC/MS Semi VOA (Continued)
Analysis Batch: 241401 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 8270D LL 241037MB 180-241037/1-A Method Blank Total/NA
Sediment 8270D LL 241037LCS 180-241037/2-A Lab Control Sample Total/NA
Sediment 8270D LL 241037180-76196-4 MS AH-07-0318-C Total/NA
Sediment 8270D LL 241037180-76196-4 MSD AH-07-0318-C Total/NA
GC Semi VOA
Prep Batch: 240746
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C180-76196-24 EB-02-0318 Total/NA
Water 3510CMB 180-240746/1-A Method Blank Total/NA
Water 3510CLCS 180-240746/2-A Lab Control Sample Total/NA
Water 3510CLCSD 180-240746/3-A Lab Control Sample Dup Total/NA
Prep Batch: 241038
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 3541180-76196-4 AH-07-0318-C Total/NA
Sediment 3541180-76196-8 AH-06-0318-C Total/NA
Sediment 3541180-76196-12 AH-02-0318-C Total/NA
Sediment 3541180-76196-16 AH-04-0318-C Total/NA
Sediment 3541180-76196-21 AH-05-0318-C Total/NA
Sediment 3541180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 3541MB 180-241038/1-B Method Blank Total/NA
Sediment 3541LCS 180-241038/2-B Lab Control Sample Total/NA
Sediment 3541180-76196-8 MS AH-06-0318-C Total/NA
Sediment 3541180-76196-8 MSD AH-06-0318-C Total/NA
Analysis Batch: 241080
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water EPA 8081B LL 240746180-76196-24 EB-02-0318 Total/NA
Water EPA 8081B LL 240746MB 180-240746/1-A Method Blank Total/NA
Water EPA 8081B LL 240746LCS 180-240746/2-A Lab Control Sample Total/NA
Water EPA 8081B LL 240746LCSD 180-240746/3-A Lab Control Sample Dup Total/NA
Cleanup Batch: 241931
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 3640A 241038180-76196-4 AH-07-0318-C Total/NA
Sediment 3640A 241038180-76196-8 AH-06-0318-C Total/NA
Sediment 3640A 241038180-76196-12 AH-02-0318-C Total/NA
Sediment 3640A 241038180-76196-16 AH-04-0318-C Total/NA
Sediment 3640A 241038180-76196-21 AH-05-0318-C Total/NA
Sediment 3640A 241038180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 3640A 241038MB 180-241038/1-B Method Blank Total/NA
Sediment 3640A 241038LCS 180-241038/2-B Lab Control Sample Total/NA
Sediment 3640A 241038180-76196-8 MS AH-06-0318-C Total/NA
Sediment 3640A 241038180-76196-8 MSD AH-06-0318-C Total/NA
Analysis Batch: 242257
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 8081B_LL 241931180-76196-4 AH-07-0318-C Total/NA
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QC Association Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC Semi VOA (Continued)
Analysis Batch: 242257 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 8081B_LL 241931180-76196-8 AH-06-0318-C Total/NA
Sediment 8081B_LL 241931180-76196-12 AH-02-0318-C Total/NA
Sediment 8081B_LL 241931180-76196-16 AH-04-0318-C Total/NA
Sediment 8081B_LL 241931180-76196-21 AH-05-0318-C Total/NA
Sediment 8081B_LL 241931180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 8081B_LL 241931MB 180-241038/1-B Method Blank Total/NA
Sediment 8081B_LL 241931LCS 180-241038/2-B Lab Control Sample Total/NA
Sediment 8081B_LL 241931180-76196-8 MS AH-06-0318-C Total/NA
Sediment 8081B_LL 241931180-76196-8 MSD AH-06-0318-C Total/NA
Metals
Prep Batch: 240953
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A180-76196-24 EB-02-0318 Total Recoverable
Water 3005AMB 180-240953/1-A Method Blank Total Recoverable
Water 3005ALCS 180-240953/2-A Lab Control Sample Total Recoverable
Analysis Batch: 241140
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water EPA 6020B 240953180-76196-24 EB-02-0318 Total Recoverable
Water EPA 6020B 240953MB 180-240953/1-A Method Blank Total Recoverable
Water EPA 6020B 240953LCS 180-240953/2-A Lab Control Sample Total Recoverable
Prep Batch: 241273
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 7471B180-76196-4 AH-07-0318-C Total/NA
Sediment 7471B180-76196-8 AH-06-0318-C Total/NA
Sediment 7471B180-76196-12 AH-02-0318-C Total/NA
Sediment 7471B180-76196-16 AH-04-0318-C Total/NA
Sediment 7471B180-76196-21 AH-05-0318-C Total/NA
Sediment 7471B180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 7471BMB 180-241273/1-A Method Blank Total/NA
Sediment 7471BLCS 180-241273/2-A Lab Control Sample Total/NA
Sediment 7471BLCSSRM 180-241273/3-A Lab Control Sample Total/NA
Analysis Batch: 241400
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 7471B 241273180-76196-4 AH-07-0318-C Total/NA
Sediment 7471B 241273180-76196-8 AH-06-0318-C Total/NA
Sediment 7471B 241273180-76196-12 AH-02-0318-C Total/NA
Sediment 7471B 241273180-76196-16 AH-04-0318-C Total/NA
Sediment 7471B 241273180-76196-21 AH-05-0318-C Total/NA
Sediment 7471B 241273180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 7471B 241273MB 180-241273/1-A Method Blank Total/NA
Sediment 7471B 241273LCS 180-241273/2-A Lab Control Sample Total/NA
Sediment 7471B 241273LCSSRM 180-241273/3-A Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Metals (Continued)
Prep Batch: 241695
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 3050B180-76196-4 AH-07-0318-C Total/NA
Sediment 3050B180-76196-8 AH-06-0318-C Total/NA
Sediment 3050B180-76196-12 AH-02-0318-C Total/NA
Sediment 3050B180-76196-16 AH-04-0318-C Total/NA
Sediment 3050B180-76196-21 AH-05-0318-C Total/NA
Sediment 3050B180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 3050BMB 180-241695/1-A Method Blank Total/NA
Sediment 3050BLCS 180-241695/2-A Lab Control Sample Total/NA
Sediment 3050BLCSSRM 180-241695/19-A Lab Control Sample Total/NA
Prep Batch: 241732
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A180-76196-24 EB-02-0318 Total/NA
Water 7470AMB 180-241732/1-A Method Blank Total/NA
Water 7470ALCS 180-241732/2-A Lab Control Sample Total/NA
Analysis Batch: 241904
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water EPA 7470A 241732180-76196-24 EB-02-0318 Total/NA
Water EPA 7470A 241732MB 180-241732/1-A Method Blank Total/NA
Water EPA 7470A 241732LCS 180-241732/2-A Lab Control Sample Total/NA
Analysis Batch: 241911
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 6020B 241695180-76196-4 AH-07-0318-C Total/NA
Sediment 6020B 241695180-76196-8 AH-06-0318-C Total/NA
Sediment 6020B 241695180-76196-12 AH-02-0318-C Total/NA
Sediment 6020B 241695180-76196-16 AH-04-0318-C Total/NA
Sediment 6020B 241695180-76196-21 AH-05-0318-C Total/NA
Sediment 6020B 241695180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 6020B 241695MB 180-241695/1-A Method Blank Total/NA
Sediment 6020B 241695LCS 180-241695/2-A Lab Control Sample Total/NA
Sediment 6020B 241695LCSSRM 180-241695/19-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 240705
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water EPA 7196A180-76196-24 EB-02-0318 Total/NA
Water EPA 7196AMB 180-240705/10 Method Blank Total/NA
Water EPA 7196ALCS 180-240705/11 Lab Control Sample Total/NA
Analysis Batch: 240793
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 2540G180-76196-13 AH-04-0318-G1 Total/NA
Sediment 2540G180-76196-14 AH-04-0318-G2 Total/NA
Sediment 2540G180-76196-15 AH-04-0318-G3 Total/NA
Sediment 2540G180-76196-16 AH-04-0318-C Total/NA
Sediment 2540G180-76196-17 AH-05-0318-G1 Total/NA
Sediment 2540G180-76196-18 AH-05-0318-G1-DUP Total/NA
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QC Association Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
General Chemistry (Continued)
Analysis Batch: 240793 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 2540G180-76196-19 AH-05-0318-G2 Total/NA
Sediment 2540G180-76196-20 AH-05-0318-G3 Total/NA
Sediment 2540G180-76196-21 AH-05-0318-C Total/NA
Sediment 2540G180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 2540G180-76196-16 DU AH-04-0318-C Total/NA
Sediment 2540G180-76196-22 DU AH-05-0318-C-DUP Total/NA
Analysis Batch: 240823
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 2540G180-76196-1 AH-07-0318-G1 Total/NA
Sediment 2540G180-76196-2 AH-07-0318-G2 Total/NA
Sediment 2540G180-76196-3 AH-07-0318-G3 Total/NA
Sediment 2540G180-76196-4 AH-07-0318-C Total/NA
Sediment 2540G180-76196-5 AH-06-0318-G1 Total/NA
Sediment 2540G180-76196-6 AH-06-0318-G2 Total/NA
Sediment 2540G180-76196-7 AH-06-0318-G3 Total/NA
Sediment 2540G180-76196-8 AH-06-0318-C Total/NA
Sediment 2540G180-76196-9 AH-02-0318-G1 Total/NA
Sediment 2540G180-76196-10 AH-02-0318-G2 Total/NA
Sediment 2540G180-76196-11 AH-02-0318-G3 Total/NA
Sediment 2540G180-76196-12 AH-02-0318-C Total/NA
Sediment 2540G180-76196-4 DU AH-07-0318-C Total/NA
Sediment 2540G180-76196-12 DU AH-02-0318-C Total/NA
Prep Batch: 240858
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 3060A180-76196-4 AH-07-0318-C Total/NA
Sediment 3060A180-76196-8 AH-06-0318-C Total/NA
Sediment 3060A180-76196-12 AH-02-0318-C Total/NA
Sediment 3060A180-76196-16 AH-04-0318-C Total/NA
Sediment 3060A180-76196-21 AH-05-0318-C Total/NA
Sediment 3060A180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 3060AMB 180-240858/1-A Method Blank Total/NA
Sediment 3060ALCSI 180-240858/3-A Lab Control Sample Total/NA
Sediment 3060ALCSS 180-240858/2-A Lab Control Sample Total/NA
Sediment 3060A180-76196-16 MSI AH-04-0318-C Total/NA
Sediment 3060A180-76196-16 MSS AH-04-0318-C Total/NA
Sediment 3060A180-76196-16 DU AH-04-0318-C Total/NA
Analysis Batch: 240909
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment Lloyd Kahn180-76196-16 AH-04-0318-C Total/NA
Sediment Lloyd Kahn180-76196-21 AH-05-0318-C Total/NA
Sediment Lloyd Kahn180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment Lloyd KahnMB 180-240909/3 Method Blank Total/NA
Sediment Lloyd KahnLCS 180-240909/4 Lab Control Sample Total/NA
Analysis Batch: 240949
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment EPA 7196A 240858180-76196-4 AH-07-0318-C Total/NA
Sediment EPA 7196A 240858180-76196-8 AH-06-0318-C Total/NA
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QC Association Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
General Chemistry (Continued)
Analysis Batch: 240949 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment EPA 7196A 240858180-76196-12 AH-02-0318-C Total/NA
Sediment EPA 7196A 240858180-76196-16 AH-04-0318-C Total/NA
Sediment EPA 7196A 240858180-76196-21 AH-05-0318-C Total/NA
Sediment EPA 7196A 240858180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment EPA 7196A 240858MB 180-240858/1-A Method Blank Total/NA
Sediment EPA 7196A 240858LCSI 180-240858/3-A Lab Control Sample Total/NA
Sediment EPA 7196A 240858LCSS 180-240858/2-A Lab Control Sample Total/NA
Sediment EPA 7196A 240858180-76196-16 MSI AH-04-0318-C Total/NA
Sediment EPA 7196A 240858180-76196-16 MSS AH-04-0318-C Total/NA
Sediment EPA 7196A 240858180-76196-16 DU AH-04-0318-C Total/NA
Prep Batch: 241004
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 9071B180-76196-4 AH-07-0318-C Total/NA
Sediment 9071B180-76196-8 AH-06-0318-C Total/NA
Sediment 9071B180-76196-12 AH-02-0318-C Total/NA
Sediment 9071B180-76196-16 AH-04-0318-C Total/NA
Sediment 9071B180-76196-21 AH-05-0318-C Total/NA
Sediment 9071B180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment 9071BMB 180-241004/1-A Method Blank Total/NA
Sediment 9071BLCS 180-241004/2-A Lab Control Sample Total/NA
Sediment 9071BLCSD 180-241004/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 241091
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment EPA 9071B 241004180-76196-4 AH-07-0318-C Total/NA
Sediment EPA 9071B 241004180-76196-8 AH-06-0318-C Total/NA
Sediment EPA 9071B 241004180-76196-12 AH-02-0318-C Total/NA
Sediment EPA 9071B 241004180-76196-16 AH-04-0318-C Total/NA
Sediment EPA 9071B 241004180-76196-21 AH-05-0318-C Total/NA
Sediment EPA 9071B 241004180-76196-22 AH-05-0318-C-DUP Total/NA
Sediment EPA 9071B 241004MB 180-241004/1-A Method Blank Total/NA
Sediment EPA 9071B 241004LCS 180-241004/2-A Lab Control Sample Total/NA
Sediment EPA 9071B 241004LCSD 180-241004/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 241158
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment Lloyd Kahn180-76196-4 AH-07-0318-C Total/NA
Sediment Lloyd Kahn180-76196-8 AH-06-0318-C Total/NA
Sediment Lloyd Kahn180-76196-12 AH-02-0318-C Total/NA
Sediment Lloyd KahnMB 180-241158/3 Method Blank Total/NA
Sediment Lloyd KahnLCS 180-241158/4 Lab Control Sample Total/NA
Analysis Batch: 241245
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 5310C180-76196-24 EB-02-0318 Total/NA
Water SM 5310CMB 180-241245/6 Method Blank Total/NA
Water SM 5310CLCS 180-241245/4 Lab Control Sample Total/NA
Water SM 5310CLCSD 180-241245/5 Lab Control Sample Dup Total/NA
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QC Association Summary
TestAmerica Job ID: 180-76196-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
General Chemistry (Continued)
Analysis Batch: 241989
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 7196A180-76196-4 AH-07-0318-C Total/NA
Sediment 7196A180-76196-8 AH-06-0318-C Total/NA
Sediment 7196A180-76196-12 AH-02-0318-C Total/NA
Sediment 7196A180-76196-16 AH-04-0318-C Total/NA
Sediment 7196A180-76196-21 AH-05-0318-C Total/NA
Sediment 7196A180-76196-22 AH-05-0318-C-DUP Total/NA
Water 7196A180-76196-24 EB-02-0318 Total/NA
Prep Batch: 392275
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 1664B180-76196-24 EB-02-0318 Total/NA
Water 1664BMB 400-392275/1-A Method Blank Total/NA
Water 1664BLCS 400-392275/2-A Lab Control Sample Total/NA
Analysis Batch: 392295
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 1664B 392275180-76196-24 EB-02-0318 Total/NA
Water 1664B 392275MB 400-392275/1-A Method Blank Total/NA
Water 1664B 392275LCS 400-392275/2-A Lab Control Sample Total/NA
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Login Sample Receipt Checklist
Client: Athena Technologies, Inc Job Number: 180-76196-1
Login Number: 76196
Question Answer Comment
Creator: Kovitch, Christina M
List Source: TestAmerica Pittsburgh
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC.
FalseSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Pittsburgh
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Login Sample Receipt Checklist
Client: Athena Technologies, Inc Job Number: 180-76196-1
Login Number: 76196
Question Answer Comment
Creator: Watson, Debbie
List Source: TestAmerica Pittsburgh
List Number: 2
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Pittsburgh
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Login Sample Receipt Checklist
Client: Athena Technologies, Inc Job Number: 180-76196-1
Login Number: 76196
Question Answer Comment
Creator: Conrady, Hank W
List Source: TestAmerica Pensacola
List Creation: 03/30/18 04:08 PMList Number: 3
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
FalseThe cooler's custody seal, if present, is intact.NO CUSTODY SEAL
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.3.4°C IR-7
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Pittsburgh
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
TestAmerica Job ID: 400-151454-1
Client Project/Site: North Carolina Sediment Project
For:
Athena Technologies, Inc
1293 Graham Farm Road
PO BOX 68
McClellanville, South Carolina 29458
Attn: Adam Freeze
Authorized for release by:
4/12/2018 12:52:45 PM
Carrie Gamber, Senior Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
TestAmerica Job ID: 400-151454-1
Page 2 of 37
TestAmerica Pensacola
4/12/2018
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37
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Case Narrative
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Job ID: 400-151454-1
Laboratory: TestAmerica Pensacola
Narrative
CASE NARRATIVE
Client: Athena Technologies, Inc
Project: North Carolina Sediment Project
Report Number: 400-151454-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 03/28/2018; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.0 C.
MAVPH
Several samples required dilution due to the sample matrix. Elevated reporting limits (RLs) were reported.
MAEPH
Four surrogates were used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria
without performing re-extraction/re-analysis. The following sample contained an allowable number of surrogate compounds outside
limits: EB-02-0318 (400-151454-7). These results have been reported and qualified.
Four surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria without
performing re-extraction/re-analysis. The following samples contained an allowable number of surrogate compounds outside limits:
(AH-06-0318-C (400-151454-2MS) and AH-02-0318-C (400-151454-3MS). These results have been reported and qualified.
C19-C36 Aliphatics failed the recovery criteria low for the MS of sample AH-06-0318-C (400-151454-2) in batch 400-392564.
C19-C36 Aliphatics, C9-C18 Aliphatics and C11-C22 Aromatics failed the recovery criteria low for the MS of sample AH-02-0318-C
(400-151454-3) in batch 400-393048. C9-C18 Aliphatics and C11-C22 Aromatics exceeded the RPD limit for the MSD of sample
AH-02-0318-C (400-151454-3) in batch 400-393048.
PERCENT SOLIDS
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Pensacola
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Detection Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-C Lab Sample ID: 400-151454-1
No Detections.
Client Sample ID: AH-06-0318-C Lab Sample ID: 400-151454-2
No Detections.
Client Sample ID: AH-02-0318-C Lab Sample ID: 400-151454-3
No Detections.
Client Sample ID: AH-04-0318-C Lab Sample ID: 400-151454-4
☼C11-C22 Aromatics
RL
7.8 mg/Kg
MDL
7.8
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA112MA-EPH
☼C19-C36 Aliphatics 7.8 mg/Kg7.8 Total/NA112MA-EPH
Client Sample ID: AH-05-0318-C Lab Sample ID: 400-151454-5
☼C11-C22 Aromatics
RL
13 mg/Kg
MDL
13
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA128MA-EPH
☼C9-C18 Aliphatics 13 mg/Kg13 Total/NA115MA-EPH
Client Sample ID: AH-05-0318-C-DUP Lab Sample ID: 400-151454-6
☼C11-C22 Aromatics
RL
12 mg/Kg
MDL
12
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA116MA-EPH
Client Sample ID: EB-02-0318 Lab Sample ID: 400-151454-7
No Detections.
TestAmerica Pensacola
This Detection Summary does not include radiochemical test results.
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Sample Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
400-151454-1 AH-07-0318-C Sediment 03/27/18 08:50 03/28/18 09:44
400-151454-2 AH-06-0318-C Sediment 03/27/18 09:30 03/28/18 09:44
400-151454-3 AH-02-0318-C Sediment 03/27/18 10:05 03/28/18 09:44
400-151454-4 AH-04-0318-C Sediment 03/27/18 10:50 03/28/18 09:44
400-151454-5 AH-05-0318-C Sediment 03/27/18 11:55 03/28/18 09:44
400-151454-6 AH-05-0318-C-DUP Sediment 03/27/18 11:58 03/28/18 09:44
400-151454-7 EB-02-0318 Water 03/27/18 12:50 03/28/18 09:44
TestAmerica Pensacola
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Client Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 400-151454-1Client Sample ID: AH-07-0318-C
Matrix: SedimentDate Collected: 03/27/18 08:50
Percent Solids: 80.8Date Received: 03/28/18 09:44
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics ND 7.9 7.9 mg/Kg ☼03/29/18 13:00 03/29/18 23:44 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.2 2.2 mg/Kg 03/29/18 13:00 03/29/18 23:44 50☼C9-C10 Aromatics ND
4.1 4.1 mg/Kg 03/29/18 13:00 03/29/18 23:44 50☼C9-C12 Aliphatics ND
a,a,a-Trifluorotoluene (fid)96 70 -130 03/29/18 13:00 03/29/18 23:44 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)95 03/29/18 13:00 03/29/18 23:44 5070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C11-C22 Aromatics ND 3.9 3.9 mg/Kg ☼03/29/18 12:30 04/04/18 02:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.9 3.9 mg/Kg 03/29/18 12:30 04/03/18 21:07 1☼C19-C36 Aliphatics ND
3.9 3.9 mg/Kg 03/29/18 12:30 04/03/18 21:07 1☼C9-C18 Aliphatics ND
1-Chlorooctadecane 46 40 -140 03/29/18 12:30 04/03/18 21:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Bromonaphthalene 50 03/29/18 12:30 04/04/18 02:06 140-140
2-Fluorobiphenyl 68 03/29/18 12:30 04/04/18 02:06 140-140
o-Terphenyl 50 03/29/18 12:30 04/04/18 02:06 140-140
General Chemistry
RL MDL
Percent Solids 80.8 0.01 0.01 %03/29/18 10:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %03/29/18 10:37 1Percent Moisture 19.2
TestAmerica Pensacola
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Client Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 400-151454-2Client Sample ID: AH-06-0318-C
Matrix: SedimentDate Collected: 03/27/18 09:30
Percent Solids: 81.0Date Received: 03/28/18 09:44
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics ND 9.6 9.6 mg/Kg ☼03/29/18 13:00 03/30/18 00:44 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.7 2.7 mg/Kg 03/29/18 13:00 03/30/18 00:44 50☼C9-C10 Aromatics ND
5.0 5.0 mg/Kg 03/29/18 13:00 03/30/18 00:44 50☼C9-C12 Aliphatics ND
a,a,a-Trifluorotoluene (fid)101 70 -130 03/29/18 13:00 03/30/18 00:44 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)100 03/29/18 13:00 03/30/18 00:44 5070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C11-C22 Aromatics ND 3.9 3.9 mg/Kg ☼03/29/18 12:30 04/04/18 01:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.9 3.9 mg/Kg 03/29/18 12:30 04/03/18 20:38 1☼C19-C36 Aliphatics ND F1
3.9 3.9 mg/Kg 03/29/18 12:30 04/03/18 20:38 1☼C9-C18 Aliphatics ND
1-Chlorooctadecane 49 40 -140 03/29/18 12:30 04/03/18 20:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Bromonaphthalene 59 03/29/18 12:30 04/04/18 01:38 140-140
2-Fluorobiphenyl 73 03/29/18 12:30 04/04/18 01:38 140-140
o-Terphenyl 53 03/29/18 12:30 04/04/18 01:38 140-140
General Chemistry
RL MDL
Percent Solids 81.0 0.01 0.01 %03/29/18 10:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %03/29/18 10:37 1Percent Moisture 19.0
TestAmerica Pensacola
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Client Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 400-151454-3Client Sample ID: AH-02-0318-C
Matrix: SedimentDate Collected: 03/27/18 10:05
Percent Solids: 61.6Date Received: 03/28/18 09:44
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics ND 18 18 mg/Kg ☼03/29/18 13:00 03/30/18 01:44 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.9 4.9 mg/Kg 03/29/18 13:00 03/30/18 01:44 50☼C9-C10 Aromatics ND
9.1 9.1 mg/Kg 03/29/18 13:00 03/30/18 01:44 50☼C9-C12 Aliphatics ND
a,a,a-Trifluorotoluene (fid)96 70 -130 03/29/18 13:00 03/30/18 01:44 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)95 03/29/18 13:00 03/30/18 01:44 5070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C11-C22 Aromatics ND F1 F2 5.1 5.1 mg/Kg ☼04/04/18 12:45 04/09/18 17:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.1 5.1 mg/Kg 04/04/18 12:45 04/09/18 12:16 1☼C19-C36 Aliphatics ND F1
5.1 5.1 mg/Kg 04/04/18 12:45 04/09/18 12:16 1☼C9-C18 Aliphatics ND F1 F2
1-Chlorooctadecane 54 40 -140 04/04/18 12:45 04/09/18 12:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Bromonaphthalene 55 04/04/18 12:45 04/09/18 17:28 140-140
2-Fluorobiphenyl 69 04/04/18 12:45 04/09/18 17:28 140-140
o-Terphenyl 54 04/04/18 12:45 04/09/18 17:28 140-140
General Chemistry
RL MDL
Percent Solids 61.6 0.01 0.01 %03/29/18 10:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %03/29/18 10:37 1Percent Moisture 38.5
TestAmerica Pensacola
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Client Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 400-151454-4Client Sample ID: AH-04-0318-C
Matrix: SedimentDate Collected: 03/27/18 10:50
Percent Solids: 40.2Date Received: 03/28/18 09:44
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics ND 24 24 mg/Kg ☼03/29/18 13:00 03/30/18 02:43 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.8 6.8 mg/Kg 03/29/18 13:00 03/30/18 02:43 50☼C9-C10 Aromatics ND
13 13 mg/Kg 03/29/18 13:00 03/30/18 02:43 50☼C9-C12 Aliphatics ND
a,a,a-Trifluorotoluene (fid)95 70 -130 03/29/18 13:00 03/30/18 02:43 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)94 03/29/18 13:00 03/30/18 02:43 5070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C11-C22 Aromatics 12 7.8 7.8 mg/Kg ☼03/29/18 12:30 04/04/18 02:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.8 7.8 mg/Kg 03/29/18 12:30 04/03/18 21:27 1☼C19-C36 Aliphatics 12
7.8 7.8 mg/Kg 03/29/18 12:30 04/03/18 21:27 1☼C9-C18 Aliphatics ND
1-Chlorooctadecane 54 40 -140 03/29/18 12:30 04/03/18 21:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Bromonaphthalene 52 03/29/18 12:30 04/04/18 02:26 140-140
2-Fluorobiphenyl 64 03/29/18 12:30 04/04/18 02:26 140-140
o-Terphenyl 51 03/29/18 12:30 04/04/18 02:26 140-140
General Chemistry
RL MDL
Percent Solids 40.3 0.01 0.01 %03/29/18 10:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %03/29/18 10:37 1Percent Moisture 59.8
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Client Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 400-151454-5Client Sample ID: AH-05-0318-C
Matrix: SedimentDate Collected: 03/27/18 11:55
Percent Solids: 24.7Date Received: 03/28/18 09:44
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics ND 76 76 mg/Kg ☼03/29/18 13:00 03/30/18 03:43 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
21 21 mg/Kg 03/29/18 13:00 03/30/18 03:43 50☼C9-C10 Aromatics ND
39 39 mg/Kg 03/29/18 13:00 03/30/18 03:43 50☼C9-C12 Aliphatics ND
a,a,a-Trifluorotoluene (fid)96 70 -130 03/29/18 13:00 03/30/18 03:43 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)95 03/29/18 13:00 03/30/18 03:43 5070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C11-C22 Aromatics 28 13 13 mg/Kg ☼03/29/18 12:30 04/04/18 02:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
13 13 mg/Kg 03/29/18 12:30 04/03/18 21:37 1☼C19-C36 Aliphatics ND
13 13 mg/Kg 03/29/18 12:30 04/03/18 21:37 1☼C9-C18 Aliphatics 15
1-Chlorooctadecane 50 40 -140 03/29/18 12:30 04/03/18 21:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Bromonaphthalene 52 03/29/18 12:30 04/04/18 02:36 140-140
2-Fluorobiphenyl 64 03/29/18 12:30 04/04/18 02:36 140-140
o-Terphenyl 48 03/29/18 12:30 04/04/18 02:36 140-140
General Chemistry
RL MDL
Percent Solids 24.7 0.01 0.01 %03/29/18 10:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %03/29/18 10:37 1Percent Moisture 75.3
TestAmerica Pensacola
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Client Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 400-151454-6Client Sample ID: AH-05-0318-C-DUP
Matrix: SedimentDate Collected: 03/27/18 11:58
Percent Solids: 25.3Date Received: 03/28/18 09:44
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics ND 100 100 mg/Kg ☼03/29/18 13:00 03/30/18 04:43 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
28 28 mg/Kg 03/29/18 13:00 03/30/18 04:43 50☼C9-C10 Aromatics ND
53 53 mg/Kg 03/29/18 13:00 03/30/18 04:43 50☼C9-C12 Aliphatics ND
a,a,a-Trifluorotoluene (fid)124 70 -130 03/29/18 13:00 03/30/18 04:43 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)123 03/29/18 13:00 03/30/18 04:43 5070-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C11-C22 Aromatics 16 12 12 mg/Kg ☼03/29/18 12:30 04/04/18 02:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
12 12 mg/Kg 03/29/18 12:30 04/03/18 21:47 1☼C19-C36 Aliphatics ND
12 12 mg/Kg 03/29/18 12:30 04/03/18 21:47 1☼C9-C18 Aliphatics ND
1-Chlorooctadecane 41 40 -140 03/29/18 12:30 04/03/18 21:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Bromonaphthalene 57 03/29/18 12:30 04/04/18 02:45 140-140
2-Fluorobiphenyl 71 03/29/18 12:30 04/04/18 02:45 140-140
o-Terphenyl 42 03/29/18 12:30 04/04/18 02:45 140-140
General Chemistry
RL MDL
Percent Solids 25.3 0.01 0.01 %03/29/18 10:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %03/29/18 10:37 1Percent Moisture 74.7
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Client Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Lab Sample ID: 400-151454-7Client Sample ID: EB-02-0318
Matrix: WaterDate Collected: 03/27/18 12:50
Date Received: 03/28/18 09:44
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics ND 26 26 ug/L 03/29/18 19:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
11 11 ug/L 03/29/18 19:46 1C9-C12 Aliphatics ND
7.0 7.0 ug/L 03/29/18 19:46 1C9-C10 Aromatics ND
a,a,a-Trifluorotoluene (fid)100 70 -130 03/29/18 19:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)100 03/29/18 19:46 170-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C9-C18 Aliphatics ND 0.054 0.054 mg/L 04/03/18 10:59 04/09/18 14:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.054 0.054 mg/L 04/03/18 10:59 04/09/18 14:33 1C19-C36 Aliphatics ND
0.054 0.054 mg/L 04/03/18 10:59 04/09/18 19:44 1C11-C22 Aromatics ND
1-Chlorooctadecane 73 40 -140 04/03/18 10:59 04/09/18 14:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 67 04/03/18 10:59 04/09/18 19:44 140-140
2-Fluorobiphenyl 68 04/03/18 10:59 04/09/18 19:44 140-140
2-Bromonaphthalene 26 X 04/03/18 10:59 04/09/18 19:44 140-140
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Definitions/Glossary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Qualifiers
GC Semi VOA
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
X Surrogate is outside control limits
F2 MS/MSD RPD exceeds control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Surrogate Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Sediment
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F2 TFT-P1
96 95400-151454-1
Percent Surrogate Recovery (Acceptance Limits)
AH-07-0318-C
101 100400-151454-2 AH-06-0318-C
96 95400-151454-3 AH-02-0318-C
95 94400-151454-4 AH-04-0318-C
96 95400-151454-5 AH-05-0318-C
124 123400-151454-6 AH-05-0318-C-DUP
96 95LCS 400-391552/2-A Lab Control Sample
93 92LCSD 400-391552/3-A Lab Control Sample Dup
93 93MB 400-391552/1-A Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-130)(70-130)
TFT-F2 TFT-P1
100 100400-151454-7
Percent Surrogate Recovery (Acceptance Limits)
EB-02-0318
100 100LCS 400-391983/4 Lab Control Sample
108 107LCSD 400-391983/13 Lab Control Sample Dup
101 102MB 400-391983/2 Method Blank
Surrogate Legend
TFT-F = a,a,a-Trifluorotoluene (fid)
TFT-P = a,a,a-Trifluorotoluene (pid)
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Sediment
Lab Sample ID Client Sample ID (40-140)
1COD1
46400-151454-1
Percent Surrogate Recovery (Acceptance Limits)
AH-07-0318-C
49400-151454-2 AH-06-0318-C
35 X400-151454-2 MS AH-06-0318-C
47400-151454-2 MSD AH-06-0318-C
54400-151454-3 AH-02-0318-C
19 X400-151454-3 MS AH-02-0318-C
58400-151454-3 MSD AH-02-0318-C
54400-151454-4 AH-04-0318-C
50400-151454-5 AH-05-0318-C
41400-151454-6 AH-05-0318-C-DUP
59LCS 400-391988/2-A Lab Control Sample
59LCS 400-392659/2-A Lab Control Sample
67MB 400-391988/1-A Method Blank
56MB 400-392659/1-A Method Blank
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Surrogate Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Surrogate Legend
1COD = 1-Chlorooctadecane
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Sediment
Lab Sample ID Client Sample ID (40-140)(40-140)(40-140)
2BN1 FBP1 OTPH1
50 68 50400-151454-1
Percent Surrogate Recovery (Acceptance Limits)
AH-07-0318-C
59 73 53400-151454-2 AH-06-0318-C
49 72 42400-151454-2 MS AH-06-0318-C
63 76 50400-151454-2 MSD AH-06-0318-C
55 69 54400-151454-3 AH-02-0318-C
55 68 21 X400-151454-3 MS AH-02-0318-C
56 70 51400-151454-3 MSD AH-02-0318-C
52 64 51400-151454-4 AH-04-0318-C
52 64 48400-151454-5 AH-05-0318-C
57 71 42400-151454-6 AH-05-0318-C-DUP
58 71 56LCS 400-391988/2-A Lab Control Sample
62 70 54LCS 400-392659/2-A Lab Control Sample
65 73 57MB 400-391988/1-A Method Blank
52 62 49MB 400-392659/1-A Method Blank
Surrogate Legend
2BN = 2-Bromonaphthalene
FBP = 2-Fluorobiphenyl
OTPH = o-Terphenyl
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-140)
1COD1
73400-151454-7
Percent Surrogate Recovery (Acceptance Limits)
EB-02-0318
74LCS 400-392483/2-A Lab Control Sample
69LCSD 400-392483/3-A Lab Control Sample Dup
75MB 400-392483/1-A Method Blank
Surrogate Legend
1COD = 1-Chlorooctadecane
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (40-140)(40-140)(40-140)
OTPH1 FBP1 2BN1
67 68 26 X400-151454-7
Percent Surrogate Recovery (Acceptance Limits)
EB-02-0318
72 74 66LCS 400-392483/2-A Lab Control Sample
59 65 58LCSD 400-392483/3-A Lab Control Sample Dup
66 66 61MB 400-392483/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl
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Surrogate Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
FBP = 2-Fluorobiphenyl
2BN = 2-Bromonaphthalene
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QC Association Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC VOA
Analysis Batch: 391473
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment MAVPH 391552400-151454-1 AH-07-0318-C Total/NA
Sediment MAVPH 391552400-151454-2 AH-06-0318-C Total/NA
Sediment MAVPH 391552400-151454-3 AH-02-0318-C Total/NA
Sediment MAVPH 391552400-151454-4 AH-04-0318-C Total/NA
Sediment MAVPH 391552400-151454-5 AH-05-0318-C Total/NA
Sediment MAVPH 391552400-151454-6 AH-05-0318-C-DUP Total/NA
Sediment MAVPH 391552MB 400-391552/1-A Method Blank Total/NA
Sediment MAVPH 391552LCS 400-391552/2-A Lab Control Sample Total/NA
Sediment MAVPH 391552LCSD 400-391552/3-A Lab Control Sample Dup Total/NA
Prep Batch: 391552
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 5035400-151454-1 AH-07-0318-C Total/NA
Sediment 5035400-151454-2 AH-06-0318-C Total/NA
Sediment 5035400-151454-3 AH-02-0318-C Total/NA
Sediment 5035400-151454-4 AH-04-0318-C Total/NA
Sediment 5035400-151454-5 AH-05-0318-C Total/NA
Sediment 5035400-151454-6 AH-05-0318-C-DUP Total/NA
Sediment 5035MB 400-391552/1-A Method Blank Total/NA
Sediment 5035LCS 400-391552/2-A Lab Control Sample Total/NA
Sediment 5035LCSD 400-391552/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 391983
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MAVPH400-151454-7 EB-02-0318 Total/NA
Water MAVPHMB 400-391983/2 Method Blank Total/NA
Water MAVPHLCS 400-391983/4 Lab Control Sample Total/NA
Water MAVPHLCSD 400-391983/13 Lab Control Sample Dup Total/NA
GC Semi VOA
Prep Batch: 391988
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 3546400-151454-1 AH-07-0318-C Total/NA
Sediment 3546400-151454-2 AH-06-0318-C Total/NA
Sediment 3546400-151454-4 AH-04-0318-C Total/NA
Sediment 3546400-151454-5 AH-05-0318-C Total/NA
Sediment 3546400-151454-6 AH-05-0318-C-DUP Total/NA
Sediment 3546MB 400-391988/1-A Method Blank Total/NA
Sediment 3546LCS 400-391988/2-A Lab Control Sample Total/NA
Sediment 3546400-151454-2 MS AH-06-0318-C Total/NA
Sediment 3546400-151454-2 MSD AH-06-0318-C Total/NA
Prep Batch: 392483
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520C400-151454-7 EB-02-0318 Total/NA
Water 3520CMB 400-392483/1-A Method Blank Total/NA
Water 3520CLCS 400-392483/2-A Lab Control Sample Total/NA
Water 3520CLCSD 400-392483/3-A Lab Control Sample Dup Total/NA
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QC Association Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC Semi VOA (Continued)
Analysis Batch: 392564
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment MA-EPH 391988400-151454-1 AH-07-0318-C Total/NA
Sediment MA-EPH 391988400-151454-2 AH-06-0318-C Total/NA
Sediment MA-EPH 391988400-151454-4 AH-04-0318-C Total/NA
Sediment MA-EPH 391988400-151454-5 AH-05-0318-C Total/NA
Sediment MA-EPH 391988400-151454-6 AH-05-0318-C-DUP Total/NA
Sediment MA-EPH 391988MB 400-391988/1-A Method Blank Total/NA
Sediment MA-EPH 391988LCS 400-391988/2-A Lab Control Sample Total/NA
Sediment MA-EPH 391988400-151454-2 MS AH-06-0318-C Total/NA
Sediment MA-EPH 391988400-151454-2 MSD AH-06-0318-C Total/NA
Analysis Batch: 392567
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment MA-EPH 391988400-151454-1 AH-07-0318-C Total/NA
Sediment MA-EPH 391988400-151454-2 AH-06-0318-C Total/NA
Sediment MA-EPH 391988400-151454-4 AH-04-0318-C Total/NA
Sediment MA-EPH 391988400-151454-5 AH-05-0318-C Total/NA
Sediment MA-EPH 391988400-151454-6 AH-05-0318-C-DUP Total/NA
Sediment MA-EPH 391988MB 400-391988/1-A Method Blank Total/NA
Sediment MA-EPH 391988LCS 400-391988/2-A Lab Control Sample Total/NA
Sediment MA-EPH 391988400-151454-2 MS AH-06-0318-C Total/NA
Sediment MA-EPH 391988400-151454-2 MSD AH-06-0318-C Total/NA
Prep Batch: 392659
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 3546400-151454-3 AH-02-0318-C Total/NA
Sediment 3546MB 400-392659/1-A Method Blank Total/NA
Sediment 3546LCS 400-392659/2-A Lab Control Sample Total/NA
Sediment 3546400-151454-3 MS AH-02-0318-C Total/NA
Sediment 3546400-151454-3 MSD AH-02-0318-C Total/NA
Analysis Batch: 393044
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment MA-EPH 392659400-151454-3 AH-02-0318-C Total/NA
Sediment MA-EPH 392659MB 400-392659/1-A Method Blank Total/NA
Sediment MA-EPH 392659LCS 400-392659/2-A Lab Control Sample Total/NA
Sediment MA-EPH 392659400-151454-3 MS AH-02-0318-C Total/NA
Sediment MA-EPH 392659400-151454-3 MSD AH-02-0318-C Total/NA
Analysis Batch: 393045
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 392483400-151454-7 EB-02-0318 Total/NA
Water MA-EPH 392483MB 400-392483/1-A Method Blank Total/NA
Water MA-EPH 392483LCS 400-392483/2-A Lab Control Sample Total/NA
Water MA-EPH 392483LCSD 400-392483/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 393048
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment MA-EPH 392659400-151454-3 AH-02-0318-C Total/NA
Sediment MA-EPH 392659MB 400-392659/1-A Method Blank Total/NA
Sediment MA-EPH 392659LCS 400-392659/2-A Lab Control Sample Total/NA
Sediment MA-EPH 392659400-151454-3 MS AH-02-0318-C Total/NA
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QC Association Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
GC Semi VOA (Continued)
Analysis Batch: 393048 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment MA-EPH 392659400-151454-3 MSD AH-02-0318-C Total/NA
Analysis Batch: 393049
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water MA-EPH 392483400-151454-7 EB-02-0318 Total/NA
Water MA-EPH 392483MB 400-392483/1-A Method Blank Total/NA
Water MA-EPH 392483LCS 400-392483/2-A Lab Control Sample Total/NA
Water MA-EPH 392483LCSD 400-392483/3-A Lab Control Sample Dup Total/NA
General Chemistry
Analysis Batch: 391941
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment Moisture400-151454-1 AH-07-0318-C Total/NA
Sediment Moisture400-151454-2 AH-06-0318-C Total/NA
Sediment Moisture400-151454-3 AH-02-0318-C Total/NA
Sediment Moisture400-151454-4 AH-04-0318-C Total/NA
Sediment Moisture400-151454-5 AH-05-0318-C Total/NA
Sediment Moisture400-151454-6 AH-05-0318-C-DUP Total/NA
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QC Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-391552/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 391473 Prep Batch: 391552
RL MDL
C5-C8 Aliphatics ND 2.7 2.7 mg/Kg 03/26/18 14:00 03/26/18 17:44 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.750.75 mg/Kg 03/26/18 14:00 03/26/18 17:44 50C9-C10 Aromatics
ND 1.41.4 mg/Kg 03/26/18 14:00 03/26/18 17:44 50C9-C12 Aliphatics
a,a,a-Trifluorotoluene (fid)93 70 -130 03/26/18 17:44 50
MB MB
Surrogate
03/26/18 14:00
Dil FacPreparedAnalyzedQualifierLimits%Recovery
93 03/26/18 14:00 03/26/18 17:44 50a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-391552/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 391473 Prep Batch: 391552
C5-C8 Aliphatics 15.0 13.9 mg/Kg 93 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C10 Aromatics 2.50 2.58 mg/Kg 103 70 -130
C9-C12 Aliphatics 17.5 17.9 mg/Kg 102 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
95a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-391552/3-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 391473 Prep Batch: 391552
C5-C8 Aliphatics 15.0 14.6 mg/Kg 98 70 -130 5 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C10 Aromatics 2.50 2.66 mg/Kg 106 70 -130 3 25
C9-C12 Aliphatics 17.5 19.1 mg/Kg 109 70 -130 7 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
93
LCSD LCSD
Qualifier Limits%Recovery
92a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 400-391983/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 391983
RL MDL
C5-C8 Aliphatics ND 26 26 ug/L 03/29/18 14:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 7.07.0 ug/L 03/29/18 14:16 1C9-C10 Aromatics
ND 1111 ug/L 03/29/18 14:16 1C9-C12 Aliphatics
a,a,a-Trifluorotoluene (fid)101 70 -130 03/29/18 14:16 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
102 03/29/18 14:16 1a,a,a-Trifluorotoluene (pid)70 -130
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QC Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-391983/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 391983
C5-C8 Aliphatics 300 297 ug/L 99 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C10 Aromatics 50.0 53.7 ug/L 107 70 -130
C9-C12 Aliphatics 350 375 ug/L 107 70 -130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
100a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-391983/13
Matrix: Water Prep Type: Total/NA
Analysis Batch: 391983
C5-C8 Aliphatics 300 301 ug/L 100 70 -130 1 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C10 Aromatics 50.0 48.6 ug/L 97 70 -130 10 25
C9-C12 Aliphatics 350 372 ug/L 106 70 -130 1 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
108
LCSD LCSD
Qualifier Limits%Recovery
107a,a,a-Trifluorotoluene (pid)70 -130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-391988/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392564 Prep Batch: 391988
RL MDL
C19-C36 Aliphatics ND 3.2 3.2 mg/Kg 03/29/18 12:30 04/03/18 20:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.23.2 mg/Kg 03/29/18 12:30 04/03/18 20:18 1C9-C18 Aliphatics
1-Chlorooctadecane 67 40 -140 04/03/18 20:18 1
MB MB
Surrogate
03/29/18 12:30
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 400-391988/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392567 Prep Batch: 391988
RL MDL
C11-C22 Aromatics ND 3.2 3.2 mg/Kg 03/29/18 12:30 04/04/18 01:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 57 40 -140 04/04/18 01:18 1
MB MB
Surrogate
03/29/18 12:30
Dil FacPreparedAnalyzedQualifierLimits%Recovery
73 03/29/18 12:30 04/04/18 01:18 12-Fluorobiphenyl 40 -140
65 03/29/18 12:30 04/04/18 01:18 12-Bromonaphthalene 40 -140
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QC Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-391988/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392564 Prep Batch: 391988
C19-C36 Aliphatics 26.7 13.7 mg/Kg 52 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C18 Aliphatics 20.0 11.8 mg/Kg 59 40 -140
1-Chlorooctadecane 40 -140
Surrogate
59
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-391988/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392567 Prep Batch: 391988
C11-C22 Aromatics 56.7 34.7 mg/Kg 61 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
56
LCS LCS
Qualifier Limits%Recovery
712-Fluorobiphenyl 40 -140
582-Bromonaphthalene 40 -140
Client Sample ID: AH-06-0318-CLab Sample ID: 400-151454-2 MS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392564 Prep Batch: 391988
C19-C36 Aliphatics ND F1 32.7 9.00 F1 mg/Kg 28 40 -140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
C9-C18 Aliphatics ND 24.5 10.0 mg/Kg 41 40 -140☼
1-Chlorooctadecane X 40 -140
Surrogate
35
MS MS
Qualifier Limits%Recovery
Client Sample ID: AH-06-0318-CLab Sample ID: 400-151454-2 MS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392567 Prep Batch: 391988
C11-C22 Aromatics ND 69.4 31.1 mg/Kg 45 40 -140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
42
MS MS
Qualifier Limits%Recovery
722-Fluorobiphenyl 40 -140
492-Bromonaphthalene 40 -140
Client Sample ID: AH-06-0318-CLab Sample ID: 400-151454-2 MSD
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392564 Prep Batch: 391988
C19-C36 Aliphatics ND F1 32.8 13.3 mg/Kg 41 40 -140 39 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: AH-06-0318-CLab Sample ID: 400-151454-2 MSD
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392564 Prep Batch: 391988
C9-C18 Aliphatics ND 24.6 13.6 mg/Kg 55 40 -140 30 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1-Chlorooctadecane 40 -140
Surrogate
47
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: AH-06-0318-CLab Sample ID: 400-151454-2 MSD
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 392567 Prep Batch: 391988
C11-C22 Aromatics ND 69.7 37.2 mg/Kg 53 40 -140 18 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
o-Terphenyl 40 -140
Surrogate
50
MSD MSD
Qualifier Limits%Recovery
762-Fluorobiphenyl 40 -140
632-Bromonaphthalene 40 -140
Client Sample ID: Method BlankLab Sample ID: MB 400-392483/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393045 Prep Batch: 392483
RL MDL
C19-C36 Aliphatics ND 0.050 0.050 mg/L 04/03/18 10:59 04/09/18 14:04 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0500.050 mg/L 04/03/18 10:59 04/09/18 14:04 1C9-C18 Aliphatics
1-Chlorooctadecane 75 40 -140 04/09/18 14:04 1
MB MB
Surrogate
04/03/18 10:59
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 400-392483/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393049 Prep Batch: 392483
RL MDL
C11-C22 Aromatics ND 0.050 0.050 mg/L 04/03/18 10:59 04/09/18 19:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 66 40 -140 04/09/18 19:14 1
MB MB
Surrogate
04/03/18 10:59
Dil FacPreparedAnalyzedQualifierLimits%Recovery
66 04/03/18 10:59 04/09/18 19:14 12-Fluorobiphenyl 40 -140
61 04/03/18 10:59 04/09/18 19:14 12-Bromonaphthalene 40 -140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-392483/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393045 Prep Batch: 392483
C19-C36 Aliphatics 0.400 0.221 mg/L 55 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C18 Aliphatics 0.300 0.135 mg/L 45 40 -140
TestAmerica Pensacola
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QC Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-392483/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393045 Prep Batch: 392483
1-Chlorooctadecane 40 -140
Surrogate
74
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-392483/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393049 Prep Batch: 392483
C11-C22 Aromatics 0.850 0.599 mg/L 70 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
72
LCS LCS
Qualifier Limits%Recovery
742-Fluorobiphenyl 40 -140
662-Bromonaphthalene 40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-392483/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393045 Prep Batch: 392483
C19-C36 Aliphatics 0.400 0.223 mg/L 56 40 -140 1 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C18 Aliphatics 0.300 0.135 mg/L 45 40 -140 0 50
1-Chlorooctadecane 40 -140
Surrogate
69
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-392483/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393049 Prep Batch: 392483
C11-C22 Aromatics 0.850 0.502 mg/L 59 40 -140 18 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
o-Terphenyl 40 -140
Surrogate
59
LCSD LCSD
Qualifier Limits%Recovery
652-Fluorobiphenyl 40 -140
582-Bromonaphthalene 40 -140
Client Sample ID: Method BlankLab Sample ID: MB 400-392659/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393044 Prep Batch: 392659
RL MDL
C19-C36 Aliphatics ND 3.2 3.2 mg/Kg 04/04/18 12:45 04/09/18 11:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.23.2 mg/Kg 04/04/18 12:45 04/09/18 11:38 1C9-C18 Aliphatics
1-Chlorooctadecane 56 40 -140 04/09/18 11:38 1
MB MB
Surrogate
04/04/18 12:45
Dil FacPreparedAnalyzedQualifierLimits%Recovery
TestAmerica Pensacola
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QC Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Client Sample ID: Method BlankLab Sample ID: MB 400-392659/1-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393048 Prep Batch: 392659
RL MDL
C11-C22 Aromatics ND 3.2 3.2 mg/Kg 04/04/18 12:45 04/09/18 16:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 49 40 -140 04/09/18 16:50 1
MB MB
Surrogate
04/04/18 12:45
Dil FacPreparedAnalyzedQualifierLimits%Recovery
62 04/04/18 12:45 04/09/18 16:50 12-Fluorobiphenyl 40 -140
52 04/04/18 12:45 04/09/18 16:50 12-Bromonaphthalene 40 -140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-392659/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393044 Prep Batch: 392659
C19-C36 Aliphatics 26.7 13.9 mg/Kg 52 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C18 Aliphatics 20.0 12.5 mg/Kg 62 40 -140
1-Chlorooctadecane 40 -140
Surrogate
59
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-392659/2-A
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393048 Prep Batch: 392659
C11-C22 Aromatics 56.7 35.3 mg/Kg 62 40 -140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
702-Fluorobiphenyl 40 -140
622-Bromonaphthalene 40 -140
Client Sample ID: AH-02-0318-CLab Sample ID: 400-151454-3 MS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393044 Prep Batch: 392659
C19-C36 Aliphatics ND F1 42.5 ND F1 mg/Kg 0 40 -140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
C9-C18 Aliphatics ND F1 F2 31.9 5.82 F1 mg/Kg 18 40 -140☼
1-Chlorooctadecane X 40 -140
Surrogate
19
MS MS
Qualifier Limits%Recovery
Client Sample ID: AH-02-0318-CLab Sample ID: 400-151454-3 MS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393048 Prep Batch: 392659
C11-C22 Aromatics ND F1 F2 90.3 8.90 F1 mg/Kg 10 40 -140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
TestAmerica Pensacola
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QC Sample Results
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: AH-02-0318-CLab Sample ID: 400-151454-3 MS
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393048 Prep Batch: 392659
o-Terphenyl X 40 -140
Surrogate
21
MS MS
Qualifier Limits%Recovery
682-Fluorobiphenyl 40 -140
552-Bromonaphthalene 40 -140
Client Sample ID: AH-02-0318-CLab Sample ID: 400-151454-3 MSD
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393044 Prep Batch: 392659
C19-C36 Aliphatics ND F1 42.6 21.6 mg/Kg 51 40 -140 NC 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
C9-C18 Aliphatics ND F1 F2 31.9 17.5 F2 mg/Kg 55 40 -140 100 50☼
1-Chlorooctadecane 40 -140
Surrogate
58
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: AH-02-0318-CLab Sample ID: 400-151454-3 MSD
Matrix: Sediment Prep Type: Total/NA
Analysis Batch: 393048 Prep Batch: 392659
C11-C22 Aromatics ND F1 F2 90.5 51.7 F2 mg/Kg 57 40 -140 141 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
o-Terphenyl 40 -140
Surrogate
51
MSD MSD
Qualifier Limits%Recovery
702-Fluorobiphenyl 40 -140
562-Bromonaphthalene 40 -140
TestAmerica Pensacola
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-07-0318-C Lab Sample ID: 400-151454-1
Matrix: SedimentDate Collected: 03/27/18 08:50
Date Received: 03/28/18 09:44
Analysis Moisture CAC03/29/18 10:371 TAL PEN391941
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: AH-07-0318-C Lab Sample ID: 400-151454-1
Matrix: SedimentDate Collected: 03/27/18 08:50
Percent Solids: 80.8Date Received: 03/28/18 09:44
Prep 5035 MKA03/29/18 13:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.318 g 15.00 mL
Analysis MAVPH 50 391473 03/29/18 23:44 MKA TAL PENTotal/NA 5 mL 5 mL
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.07 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 21:07 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.07 g 2.0 mL
Analysis MA-EPH 1 392567 04/04/18 02:06 TAJ TAL PENTotal/NA
Client Sample ID: AH-06-0318-C Lab Sample ID: 400-151454-2
Matrix: SedimentDate Collected: 03/27/18 09:30
Date Received: 03/28/18 09:44
Analysis Moisture CAC03/29/18 10:371 TAL PEN391941
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: AH-06-0318-C Lab Sample ID: 400-151454-2
Matrix: SedimentDate Collected: 03/27/18 09:30
Percent Solids: 81.0Date Received: 03/28/18 09:44
Prep 5035 MKA03/29/18 13:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.2 g 15.00 mL
Analysis MAVPH 50 391473 03/30/18 00:44 MKA TAL PENTotal/NA 5 mL 5 mL
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.09 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 20:38 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.09 g 2.0 mL
Analysis MA-EPH 1 392567 04/04/18 01:38 TAJ TAL PENTotal/NA
Client Sample ID: AH-02-0318-C Lab Sample ID: 400-151454-3
Matrix: SedimentDate Collected: 03/27/18 10:05
Date Received: 03/28/18 09:44
Analysis Moisture CAC03/29/18 10:371 TAL PEN391941
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
TestAmerica Pensacola
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-C Lab Sample ID: 400-151454-3
Matrix: SedimentDate Collected: 03/27/18 10:05
Percent Solids: 61.6Date Received: 03/28/18 09:44
Prep 5035 MKA03/29/18 13:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 3.756 g 15.00 mL
Analysis MAVPH 50 391473 03/30/18 01:44 MKA TAL PENTotal/NA 5 mL 5 mL
Prep 3546 392659 04/04/18 12:45 KLR TAL PENTotal/NA 15.19 g 2.0 mL
Analysis MA-EPH 1 393044 04/09/18 12:16 TAJ TAL PENTotal/NA
Prep 3546 392659 04/04/18 12:45 KLR TAL PENTotal/NA 15.19 g 2.0 mL
Analysis MA-EPH 1 393048 04/09/18 17:28 TAJ TAL PENTotal/NA
Client Sample ID: AH-04-0318-C Lab Sample ID: 400-151454-4
Matrix: SedimentDate Collected: 03/27/18 10:50
Date Received: 03/28/18 09:44
Analysis Moisture CAC03/29/18 10:371 TAL PEN391941
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: AH-04-0318-C Lab Sample ID: 400-151454-4
Matrix: SedimentDate Collected: 03/27/18 10:50
Percent Solids: 40.2Date Received: 03/28/18 09:44
Prep 5035 MKA03/29/18 13:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.138 g 15.00 mL
Analysis MAVPH 50 391473 03/30/18 02:43 MKA TAL PENTotal/NA 5 mL 5 mL
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.29 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 21:27 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.29 g 2.0 mL
Analysis MA-EPH 1 392567 04/04/18 02:26 TAJ TAL PENTotal/NA
Client Sample ID: AH-05-0318-C Lab Sample ID: 400-151454-5
Matrix: SedimentDate Collected: 03/27/18 11:55
Date Received: 03/28/18 09:44
Analysis Moisture CAC03/29/18 10:371 TAL PEN391941
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: AH-05-0318-C Lab Sample ID: 400-151454-5
Matrix: SedimentDate Collected: 03/27/18 11:55
Percent Solids: 24.7Date Received: 03/28/18 09:44
Prep 5035 MKA03/29/18 13:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.16 g 15.00 mL
Analysis MAVPH 50 391473 03/30/18 03:43 MKA TAL PENTotal/NA 5 mL 5 mL
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.26 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 21:37 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.26 g 2.0 mL
TestAmerica Pensacola
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-05-0318-C Lab Sample ID: 400-151454-5
Matrix: SedimentDate Collected: 03/27/18 11:55
Percent Solids: 24.7Date Received: 03/28/18 09:44
Analysis MA-EPH TAJ04/04/18 02:361 TAL PEN392567
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: AH-05-0318-C-DUP Lab Sample ID: 400-151454-6
Matrix: SedimentDate Collected: 03/27/18 11:58
Date Received: 03/28/18 09:44
Analysis Moisture CAC03/29/18 10:371 TAL PEN391941
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: AH-05-0318-C-DUP Lab Sample ID: 400-151454-6
Matrix: SedimentDate Collected: 03/27/18 11:58
Percent Solids: 25.3Date Received: 03/28/18 09:44
Prep 5035 MKA03/29/18 13:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.572 g 15.00 mL
Analysis MAVPH 50 391473 03/30/18 04:43 MKA TAL PENTotal/NA 5 mL 5 mL
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.25 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 21:47 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.25 g 2.0 mL
Analysis MA-EPH 1 392567 04/04/18 02:45 TAJ TAL PENTotal/NA
Client Sample ID: EB-02-0318 Lab Sample ID: 400-151454-7
Matrix: WaterDate Collected: 03/27/18 12:50
Date Received: 03/28/18 09:44
Analysis MAVPH MKA03/29/18 19:461 TAL PEN391983
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 392483 04/03/18 10:59 NTH TAL PENTotal/NA 931.2 mL 2.0 mL
Analysis MA-EPH 1 393045 04/09/18 14:33 TAJ TAL PENTotal/NA
Prep 3520C 392483 04/03/18 10:59 NTH TAL PENTotal/NA 931.2 mL 2.0 mL
Analysis MA-EPH 1 393049 04/09/18 19:44 TAJ TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-391552/1-A
Matrix: SedimentDate Collected: N/A
Date Received: N/A
Prep 5035 MKA03/26/18 14:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 15.00 mL
Analysis MAVPH 50 391473 03/26/18 17:44 MKA TAL PENTotal/NA 5 mL 5 mL
TestAmerica Pensacola
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: Method Blank Lab Sample ID: MB 400-391983/2
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis MAVPH MKA03/29/18 14:161 TAL PEN391983
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-391988/1-A
Matrix: SedimentDate Collected: N/A
Date Received: N/A
Prep 3546 KLR03/29/18 12:30 TAL PEN391988
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 20:18 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.00 g 2.0 mL
Analysis MA-EPH 1 392567 04/04/18 01:18 TAJ TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-392483/1-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3520C NTH04/03/18 10:59 TAL PEN392483
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1000 mL 2.0 mL
Analysis MA-EPH 1 393045 04/09/18 14:04 TAJ TAL PENTotal/NA
Prep 3520C 392483 04/03/18 10:59 NTH TAL PENTotal/NA 1000 mL 2.0 mL
Analysis MA-EPH 1 393049 04/09/18 19:14 TAJ TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-392659/1-A
Matrix: SedimentDate Collected: N/A
Date Received: N/A
Prep 3546 KLR04/04/18 12:45 TAL PEN392659
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 2.0 mL
Analysis MA-EPH 1 393044 04/09/18 11:38 TAJ TAL PENTotal/NA
Prep 3546 392659 04/04/18 12:45 KLR TAL PENTotal/NA 15.00 g 2.0 mL
Analysis MA-EPH 1 393048 04/09/18 16:50 TAJ TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-391552/2-A
Matrix: SedimentDate Collected: N/A
Date Received: N/A
Prep 5035 MKA03/26/18 14:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 15.00 mL
Analysis MAVPH 50 391473 03/26/18 18:44 MKA TAL PENTotal/NA 5 mL 5 mL
TestAmerica Pensacola
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-391983/4
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis MAVPH MKA03/29/18 17:461 TAL PEN391983
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-391988/2-A
Matrix: SedimentDate Collected: N/A
Date Received: N/A
Prep 3546 KLR03/29/18 12:30 TAL PEN391988
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 20:28 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.00 g 2.0 mL
Analysis MA-EPH 1 392567 04/04/18 01:28 TAJ TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-392483/2-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3520C NTH04/03/18 10:59 TAL PEN392483
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1000 mL 2.0 mL
Analysis MA-EPH 1 393045 04/09/18 14:14 TAJ TAL PENTotal/NA
Prep 3520C 392483 04/03/18 10:59 NTH TAL PENTotal/NA 1000 mL 2.0 mL
Analysis MA-EPH 1 393049 04/09/18 19:24 TAJ TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-392659/2-A
Matrix: SedimentDate Collected: N/A
Date Received: N/A
Prep 3546 KLR04/04/18 12:45 TAL PEN392659
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 2.0 mL
Analysis MA-EPH 1 393044 04/09/18 11:47 TAJ TAL PENTotal/NA
Prep 3546 392659 04/04/18 12:45 KLR TAL PENTotal/NA 15.00 g 2.0 mL
Analysis MA-EPH 1 393048 04/09/18 16:59 TAJ TAL PENTotal/NA
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-391552/3-A
Matrix: SedimentDate Collected: N/A
Date Received: N/A
Prep 5035 MKA03/26/18 14:00 TAL PEN391552
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.00 g 15.00 mL
Analysis MAVPH 50 391473 03/27/18 12:12 MKA TAL PENTotal/NA 5 mL 5 mL
TestAmerica Pensacola
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-391983/13
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis MAVPH MKA03/30/18 10:481 TAL PEN391983
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-392483/3-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 3520C NTH04/03/18 10:59 TAL PEN392483
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1000 mL 2.0 mL
Analysis MA-EPH 1 393045 04/09/18 14:24 TAJ TAL PENTotal/NA
Prep 3520C 392483 04/03/18 10:59 NTH TAL PENTotal/NA 1000 mL 2.0 mL
Analysis MA-EPH 1 393049 04/09/18 19:34 TAJ TAL PENTotal/NA
Client Sample ID: AH-06-0318-C Lab Sample ID: 400-151454-2 MS
Matrix: SedimentDate Collected: 03/27/18 09:30
Percent Solids: 81.0Date Received: 03/28/18 09:44
Prep 3546 KLR03/29/18 12:30 TAL PEN391988
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.11 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 20:47 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.11 g 2.0 mL
Analysis MA-EPH 1 392567 04/04/18 01:47 TAJ TAL PENTotal/NA
Client Sample ID: AH-06-0318-C Lab Sample ID: 400-151454-2 MSD
Matrix: SedimentDate Collected: 03/27/18 09:30
Percent Solids: 81.0Date Received: 03/28/18 09:44
Prep 3546 KLR03/29/18 12:30 TAL PEN391988
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.05 g 2.0 mL
Analysis MA-EPH 1 392564 04/03/18 20:57 TAJ TAL PENTotal/NA
Prep 3546 391988 03/29/18 12:30 KLR TAL PENTotal/NA 15.05 g 2.0 mL
Analysis MA-EPH 1 392567 04/04/18 01:57 TAJ TAL PENTotal/NA
Client Sample ID: AH-02-0318-C Lab Sample ID: 400-151454-3 MS
Matrix: SedimentDate Collected: 03/27/18 10:05
Percent Solids: 61.6Date Received: 03/28/18 09:44
Prep 3546 KLR04/04/18 12:45 TAL PEN392659
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.29 g 2.0 mL
Analysis MA-EPH 1 393044 04/09/18 11:57 TAJ TAL PENTotal/NA
Prep 3546 392659 04/04/18 12:45 KLR TAL PENTotal/NA 15.29 g 2.0 mL
Analysis MA-EPH 1 393048 04/09/18 17:09 TAJ TAL PENTotal/NA
TestAmerica Pensacola
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Lab Chronicle
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Client Sample ID: AH-02-0318-C Lab Sample ID: 400-151454-3 MSD
Matrix: SedimentDate Collected: 03/27/18 10:05
Percent Solids: 61.6Date Received: 03/28/18 09:44
Prep 3546 KLR04/04/18 12:45 TAL PEN392659
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.26 g 2.0 mL
Analysis MA-EPH 1 393044 04/09/18 12:06 TAJ TAL PENTotal/NA
Prep 3546 392659 04/04/18 12:45 KLR TAL PENTotal/NA 15.26 g 2.0 mL
Analysis MA-EPH 1 393048 04/09/18 17:18 TAJ TAL PENTotal/NA
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TestAmerica Pensacola
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Method Summary
TestAmerica Job ID: 400-151454-1Client: Athena Technologies, Inc
Project/Site: North Carolina Sediment Project
Method Method Description LaboratoryProtocol
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)TAL PEN
MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)TAL PEN
EPAMoisturePercent Moisture TAL PEN
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TestAmerica Pensacola
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Accreditation/Certification Summary
Client: Athena Technologies, Inc TestAmerica Job ID: 400-151454-1
Project/Site: North Carolina Sediment Project
Laboratory: TestAmerica Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3144State Program 12-31-18
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
Moisture Sediment Percent Moisture
Moisture Sediment Percent Solids
Laboratory: TestAmerica Pittsburgh
The accreditations/certifications listed below are applicable to this report.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)4344State Program 12-31-18
TestAmerica Pensacola
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Login Sample Receipt Checklist
Client: Athena Technologies, Inc Job Number: 400-151454-1
Login Number: 151454
Question Answer Comment
Creator: Perez, Trina M
List Source: TestAmerica Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.0.0°C IR-7
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Pensacola
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