HomeMy WebLinkAboutAQ_F_1900104_20220128_CMPL_CompRpt 3M Industrial Minerals Product Division
3M 4191 Hwy 87 South
Moncure, NC 27559
January 28,2022
North Carolina Department of Environmental Quality
Division of Air Quality NC Dept of Environment-i Quality
Raleigh Regional Office
Ms. Taylor Hartsfield,Raleigh Regional Office Supervisor �A� 31 L J�
3800 Barrett Drive
Raleigh,NC 27609
Raleigh Regional Office
CERTIFIED MAIL: 7020 3160 00013479 2760
Re: 3M Company—Pittsboro,NC
Air Quality Permit Number: 09006T07
Facility ID: 1900104
3M Industrial Mineral Products,Moncure,NC,
July 1 to December 31,2021
Semiannual Title V Deviation Report and
Opacity Emissions Summary Report
Dear Ms. Taylor Hartsfield,
Enclosed please find the Semiannual Deviation Report for the 3M Pittsboro facility for the July 1
through December 31, 2021,reporting period.
The quarterly performance audits were performed in conformation with 40 CFR Part 60,
Appendix F, Procedure 3 and completed on 9/24/21 for the third quarter and on 12/16/21 for the
fourth quarter. The results of these audits are included.
The percent excess emissions(%EE)and percent monitor downtime(%MD)are less than the
target criteria of 6%for Quarter 3 and 4. Quarter 3 exceeded 3%downtime,which has been
attributed to the span motor reaching a hard stop during daily calibration and failing. Our third-
party contractor is working on the units to prevent the hard stop by installing switches. The
consecutive quarter,Q4, is below 3%therefore 3M Pittsboro is in compliance with good
operation and maintenance practices pursuant to NCAC 2D.0524,40 CFR 60.11(d),and 40 CFR
60.13.
Additionally,during the I half semiannual deviation report for the timeframe of January 1
through June 30,2021,the 3M Pittsboro facility disclosed more than 10 excursions for
differential pressure<2 inches of water. Since that time 3M Pittsboro has investigated the root
cause of the excursions,and found differential pressure was being continuously monitored while
the process was offline when maintenance was performed on the kilns and mixers.It has been
determined that no excursions occurred during the period.3M Pittsboro has since updated the
program logic related to the continuous monitoring of differential pressure to address this issue.
Please feel free to call me at(919)642-4010 with any questions or comments.
r—
Sincerely,
W., � - 44
Della Z. Hardy
3M Pittsboro EHS Engineer
Based on information and belief formed after reasonable inquiry,the undersigned certifies
under penalty of law that all information and statements in this document are true,
accurate,and com lete.
�x -
/ 2 Zz
(Signature of Responsible Official) (Date)
Name: Mr. Blake Arnett, Plant Director
Enclosures
cc: NCDAQ—Supervisor, Stationary Source Compliance
Andrew Miller, 3M Pittsboro EHS Supervisor
Blake Arnett, 3M Pittsboro Plant Director
Conner Doede, 3M IMPD EHS Engineer
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions 14C ept of Environmenll.i Quality
Source or Permit
Emission Source Control Condition Deviations? Records was Deviation a Determining
of •,� L��
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance/No) Dplianc St Comments AN
Number(s)
Number (Yes/No/NA) issue. (ves/No) Compliance Status
Crushing and
Screening Plant Review of monitoring,
aleigh Regional Office
Particulates from Comply with 15A recordkeeping and
sand,gravel, or NA 2.1.A.l.d NCAC 02D.0510 No Yes No reporting requirements per See comments below.
crushed stone permit conditions
operations
Method 22 (visual records
No visible fugitive performed monthly on one
Crushing and emissions greater page summary(normal All the required monitoring,
Screening Plant than 10% expected emissions= no record keeping,and reporting
Building HVAC and discharged from visible emissions). Each
NA No Yes No requirements are in compliance
other openings, 2.1.A.2.c.i.(A) any building visual is on a 6-minute with the applicable emissions
except baghouse (15A NCAC 2D timeframe. If visual standard(s).
stacks] .0524&40 CFR emissions are observed,
60.672) then Method 22 must be
repeated in same day.
Visible emissions Method 22(visual records
from any vent, performed monthly on one-
Crushing and stack,etc.shall page summary(normal
Screening Plant not exceed 7% expected emissions= no
Building "Vents" NA 2.1.A.2.c.ii Opacity No Yes No visible emissions).Each
[i.e. baghouse [15NCAC visual is on a 6-minute
stacks] 02D.0524&40 timeframe. If visual
CFR 60,Subpart emissions are observed,
00] then Method 9 shall be
repeated in same day.
Crushing and 0.05 g/dscm PM Methods 5&9, initial test All the required monitoring,
Screening Plant [15A NCAC 2D completed 8/5/2002 thru record keeping,and reporting
Building "Vents" NA No Yes No 8/8/2002. Method 5 and 9, requirements are in compliance
6067
[i.e. baghouse 21.A.2.c.iii(A) .0. &40 CFR initial testing for ES5155C with the applicable emissions
stacks] 672] conducted on 9/26/2007. standard(s).
Reporting Year 2021 Permit#:09006T07
Page 1 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
source or permit Records Was Deviation a Method(s)of
Emission Source Control Condition Deviations?
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Particulate
emissions from any
vent of any
building Method 22 (visual records
Crushing and constructed after performed monthly on one All the required monitoring,
Screening Plant April 22,2008, page summary(normal record keeping,and reporting
Building "Vents" NA 2.1.A.2.c.iii.(B) shall not be more No Yes No expected emissions= no requirements are in compliance
[i.e. baghouse than 0.032 grams visible emissions). Each with the applicable emissions
stacks] per dry standard visual is on a 6-minute standard(s).
cubic meter. timeframe.
[15A NCAC 2D
0.524&40 CFR
60.672]
Crushing and Conduct initial
Screening Plant compliance or any Methods 5&9, initial test All the required monitoring,
New Source required completed 8/5/2002 thru record keeping,and reporting
Performance NA 2.1.A.2.b subsequent No Yes No 8/8/2002. Method 5 and 9, requirements are in compliance
Standards additional testing initial testing for ES5155C with the applicable emissions
(Testing) [15A NCAC 02Q conducted on 9/26/2007. standard(s).
.0508(f)]
Crushing and Method 22 (visual records
Screening Plant Observe each performed monthly on one-All the required monitoring,
New Source building for visible page summary(normal record keeping,and reporting
Performance NA 2.1.A.2.d.i.(A) emissions. No Yes No expected emissions = no requirements are in compliance
Standards [15A NCAC visible emissions). Each with the applicable emissions
(Monitoring) 02Q.0508(f)] visual is on a 6-minute standard(s).
timeframe.
After corrective
action taken,
Crushing and Method 9 opacity
Screening Plant for stacks or All the required monitoring,
New Source Method 22 for Method 9 or 22 records record keeping,and reporting
NA 2.1.A.2.c.i.(B) No Yes No requirements are in compliance
Performance buildings to available.
Standards demonstrate with the applicable emissions
(Monitoring) compliance with 40 standard(s).
CFR 60.672(a)and
e.
Reporting Year 2021 Permit#:09006T07
Page 2 of 30 Jul-Dec Report Location ID#: 1900104
I E
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31, 2021
Terms&Conditions
Source or Permit Methods of
Emission Source Control Condition Deviations? Records Was Deviation e ( )
Condition Maintained? non-compliance Determining Comments
Description Device ID Number Summary (Yes/NoI (Yes/No/NA) Issue?(Yes/No) Compliance Status
Number(s)
Crushing and Method 22(visual records
Screening Plant Maintenance of performed monthly on one All the required monitoring,
New Source Monitoring Log- page summary(normal record keeping,and reporting
Performance NA 2.1.A.2.e.i Results No Yes No expected emissions= no requirements are in compliance
Standards 15A NCAC visible emissions).Each with the applicable emissions
(Recordkeeping) 2Q.0508(f) visual is on a 6-minute standard(s).
timeframe.
Crushing and Maintenance of Method 22(visual records
Screening Plant Monitoring Log- performed monthly on one All the required monitoring,
New Source Visible Emissions page summary(normal record keeping,and reporting
Performance
NA 2.1.A.2.e.ii Present(yes/no) No Yes No expected emissions=no requirements are in compliance
Standards 15A NCAC visible emissions).Each with the applicable emissions
(Recordkeeping) 2Q.0508(f) visual is on a 6-minute standard(s).
timeframe.
Crushing and Maintenance of Method 22(visual records
Screening Plant Monitoring Log-If performed monthly on one All the required monitoring,
New Source emissions present, page summary(normal record keeping,and reporting
Performance NA 2.1.A.2.e.iii corrective actions No Yes No expected emissions= no requirements are in compliance
Standards taken. visible emissions). Each with the applicable emissions
(Recordkeeping) 15A NCAC visual is on a 6-minute standard(s).
2Q.0508(f) timeframe.
Maintenance of Method 22(visual records
Crushing and Monitoring Log-If performed monthly on one All the required monitoring,
Screening Plant emissions present, page summary(normal record keeping,and reporting
New Source follow up
NA 2.1.A.2.e.iv No Yes No expected emissions= no requirements are in compliance
Performance observation
Standards reports. visible emissions).Each with the applicable emissions
visual is on a 6-minute standard(s).
(Recordkeeping) 15A NCAC
2Q.0508(f) timeframe.
Crushing and Reporting of any To our knowledge,all requests
Screening Plant changes.At the Monitor communications or inquiries from the NCDEQ
New Source NA 2.1.A.2.g.i request of the No Yes No from the NCDEQ DAQ for DAQ Administrator have been
Performance Administrator Standards [15A NCAC 2Q requests of change report. fulfilled in time and upon
(Reporting) .0508(f)] request.
Reporting Year 2021 Permit#:09006T07
Page 3 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1, 2021 through December 31,2021
Terms&Conditions
Source or permit Method(s)of
Emission Source Control, Condition Deviations? Records Was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue. (Yes/No) Compliance Status
Crushing and Submit Semiannual All the required monitoring,
Screening Plant Monitoring Report, Semiannual Monitoring record keeping,and reporting
New Source NA 2.1.A.2.g.ii due on 1/30 and No Yes No Reports submitted on or requirements are in compliance
Performance 7/30 15A NCAC before 1/30 and 7/30 with the applicable emissions
Standards .508(f) standard(s).
(Reporting)
If an exceedance is
determined to exist
by Method 9 or 22,
Crushing and submit report
Screening Plant identifying the All the required monitoring,
New Source exceedance, cause Results of Method 9 and record keeping,and reporting
Performance N/A 2.1.A.2.g.iii and corrective No Yes No 22 checks and reports on requirements are in compliance
Standards action taken,due same. with the applicable emissions
(Reporting) <_5 bus.days of standard(s).
non-compliant
observation
[15A NCAC
02Q.0508(f)]
Crushing and 2.3 lb SO2/MM Btu Based on AP-42 emissions No monitoring, recordkeeping,
ES1415 heat input factors and fuel usage, or reporting is required at this
Screening Plant (Dryer) 2.1.B.l.a [15A NCAC 02D No Yes No rate calc'd well under this time per 2.1.B.1.c of our
Dryer .0516] limit. permit.
Crushing and E51415, Meet NSPS UUU
Screening Plant CDC,,& 2.1.B.2.a No Yes No[40 CFR Part 60 detailed in next two rows
Dryer,Cyclone, & CDB3 sub UUU, including below
Baghouse sub A]
Crushing and E51415 0.057 gm/dscm PM
,
Screening Plant 15A NCAC 2D Methods 5&9, initial test
CDB3
Dryer,Cyclone,& CDC1, & 2.1.B.2.b .0524&40 CFR No Yes No completed 8/6/2002
Baghouse 60.732
Reporting Year 2021 Permit#:09006T07
Page 4 of 30 Jul-Dec Report Location ID#: 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1, 2021 through December 31, 2021
Terms&Conditions
Source or permit Method(s)of
Emission Source Control Condition Deviations? Records was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) Issue?(Yes/No) Compliance Status
All the required monitoring,
record keeping,and reporting
Crushing and 10%opacity(6 requirements are in compliance
ES1415, minute average) with the applicable emissions
Screening Plant CDC1,& 2.1.B.2.c [15A NCAC 2D No Yes No Continuous Opacity standard(s). There were no
Dryer,Cyclone,& CD83 .0524&40 CFR Monitoring System deviations from the monitoring
Baghouse 60.732] requirements of 40 CFR 60 sub
UUU and the relevant Subpart
A"General Provisions."
Conduct Initial All the required monitoring,
Crushing and NSPS UUU Test
ES1415, record keeping,and reporting
Screening Plant [PM and visible Methods 5&9,initial test
CDC1,& 2.1.B.2.d No Yes No requirements are in compliance
Dryer,Cyclone,& CDB3 emissions] completed 8/6/2002 with the applicable emissions
0.2601 Baghouse 2D standard(s).
.2
Install,calibrate, All the required monitoring,
Crushing and maintain,and Continuous Opacity
E51415, record keeping,and reporting
Screening Plant 2.1.B.2.e.i and operate a COMS Monitoring System.
Dryer,Cyclone,& 15A NCAC 2Q Preventative maintenance
CDCI,& No Yes No requirements are in compliance
ii
Baghouse CD133 .0508(f)&40 CFR procedures. with the applicable emissions
60.734, .735 standard(s).
Crushing and inspect for leaks All the required monitoring,
ES1415, 1/yr. [ Preventive maintenance record keeping,and reporting
Screening Plant CDCI,& 2.1.B.2.e.ii.(A) 15A NCAC 2Q No Yes No requirements are in compliance
Dryer,Cyclone,& CDB3 .0508(f)&40 CFR procedures. with the applicable emissions
Baghouse 60.734, .735] standard(s).
Inspect baghouse All the required monitoring,
Crushing and for structural
E51415, record keeping,and reporting
Screening Plant integrity 1/yr. Preventive maintenance
CDCi,& 2.1.B.2.e.ii.(B) No Yes No requirements are in compliance
Dryer,Cyclone,& CDB3 15A NCAC 2Q procedures. with the applicable emissions
Baghouse .0508(f)&40 CFR standard(s).
60.734, .735
Reporting Year 2021 Permit#:09006T07
Page 5 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31, 2021
Terms&Conditions
Source or permit Method(s)of
Emission Source control Condition Deviations? Records Was Deviation a
Description Device ID Condition Summary (Yes/No) Mainta issue?(Yes/No) Compliance Status
ined? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA)
Inspect cyclone for All the required monitoring,
Crushing and structural integrity
ES1415, record keeping,and reporting
Screening Plant 1/yr. Preventive maintenance., , CDC1, & 2.1.B.2.e.ii.(C) No Yes No requirements are in compliance
Drer, Cyclone,&
y y CDB3 [15A NCAC 2Q procedures with the applicable emissions
Baghouse .0508(f)&40 CFR standard(s).
60.734, .735)
Any work orders on
baghouses and cyclones
were reported into a
For each instance maintenance data tracking
of maintenance, system called CMMS.This
record date,time, system tracks all work
results performed and any
variances from
Crushing and
If any variance manufacturers All the required monitoring,
E51415, from manuf.'s record keeping,and reporting
Screening Plant CDC1, & 2.1.B.2.e.iii maintenance No Yes No maintenance procedures. requirements are in compliance
Dryer,Cyclone,& CDB3 recommend.,then CMMS builds the proper with the applicable emissions
Baghouse maintenance history
record corrections standard(s).
made required for such an
15A NCAC 2Q emissions handling
.0508(f)&40 CFR system.Quarterly PM
60.734, .735 records and other work
conducted by a third party
are maintained
electronically or hard
copies of work performed.
Crushing and Submit Semiannual All the required monitoring,
Screening Plant Monitoring Report, Semiannual Monitoring record keeping,and reporting
Dryer Baghouse& NA 2.1.B.2.f due on 1/30 and No Yes No Reports submitted on or requirements are in compliance
Cyclone 7/30 15A NCAC before 1/30 and 7/30 with the applicable emissions
.508(f) standard(s).
Reporting Year 2021 Permit#:09006T07
Page 6 of 30 Jul-Dec Report Location ID#: 1900104
01111
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or permit
Emission Source Control Condition Deviations? Records Was Deviation a Method(s)of
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Coloring Plant. Review of monitoring, All the required monitoring,
Particulates from record keeping,and reporting
0510
Comply with 15A recordkeeping and
sand,gravel, or N/A 2.1.C.l.d No Yes No requirements are in compliance
crushed stone NCAC 02D. reporting requirements per with the applicable emissions
operations permit conditions standard(s).
Visible Emissions
not to exceed 20% Method 22 (visual records
when averaged performed monthly on one
over a six minute page summary(normal
period,and may expected emissions= no
not occur more visible emissions). Each
Coloring Plant. then once in any visual is on a 6-minute No visible emissions exceeding
Control of Visible NA 2.1.C.2.a one hour period No Yes No timeframe. If visual 20%were observed or
Emissions and not more then emissions are observed, recorded.
four times per in then Method 22 must be
24 hour period. No repeated in same day.
event may exceed Continuous opacity
87%opacity. monitoring for Coloring
[15A NCAC 02D Dryers.
.05211
Establish "normal"
Coloring Plant level of visible All the required monitoring,
control of Visible emissions Completed-records on record keeping,and reporting
N/A 2.1.C.2.b No Yes No Method 22 checklist sheet-requirements are in compliance
emissions DUE: 2/14/2005
established normal as zero with the applicable emissions
(Testing) [permit effective
standard(s).
date+30d]
Method 22 (visual records
performed monthly on one
page summary(normal
Observe visible All the required monitoring,
Coloring Plant expected emissions= no
emissions once per record keeping,and reporting
Control of Visible NA 2.1.C.2.c month for above No Yes No visible emissions). Each requirements are in compliance
Emissions "normal"and visual is on a 6-minute with the applicable emissions
(Monitoring) timeframe. If visual
record. standard(s).
emissions are observed,
then Method 22 must be
repeated in same day.
Reporting Year 2021 Permit#:09006T07
Page 7 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or permit Records Was Deviation a Method(s)of
Emission Source Control Condition Deviations?
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (ves/No/Na) issue?(Yes/No) Compliance Status
If visible emissions
from a source are
observed to be All the required monitoring,
Coloring Plant above normal,take record keeping,and reporting
Control of Visible N/A 2.1.C.2.c.i appropriate action No Yes No Results of Method 9 and requirements are in compliance
Emissions to correct the issue 22 checks and reports. with the applicable emissions
(Monitoring) and record the
action taken. standard(s).
[15A NCAC 02Q
.0508(f)]
If visible emissions
from a source are
observed to be
above normal,and
after corrective
action is taken, All the required monitoring,
Coloring Plant demonstrate that record keeping,and reporting
Control of Visible the /o opacity is Results of Method 9 and
N/A 2.1.C.2.c.ii u No Yes No requirements are in compliance
Emissions below the 20/o 22 checks and reports. with the applicable emissions
(Monitoring) limit and at or
below the"normal" standard(s).
emissions for a
period of 12
minutes.
[15A NCAC 2Q
.0508(f)]
Reporting Year 2021 Permit#:09006T07
Page 8 of 30 Jul-Dec Report Location ID#:1900104
1 0 1 111
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or Per Method(s)of
Emission Source Control Condition Deviations? Records Was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)P Number Y (Yes/No/NA) issue?(Yes/No) Compliance Status
Method 22 (visual records
performed monthly on one
page summary (normal
Maintenance of All the required monitoring,
Coloring Plant expected emissions= no
Monitoring Log- record keeping, and reporting
Control of Visible NA 2.1.C.2.d.i Date and Time No Yes No visible emissions). Each requirements are in compliance
Emissions visual is on a 6-minute
(Recordkeeping) 2Q.0(15A NCAC visual
timeframe. If visual With the applicable emissions
Q.0 standard(s).
emissions are observed,
then Method 22 must be
repeated in same day.
Maintenance of Method 22 (visual records
Monitoring Log- performed monthly on one
page summary(normal
Results,Visible All the required monitoring,
Coloring Plant expected emissions= no
Emissions Present record keeping,and reporting
Control of Visible NA 2.1.C.2.d.ii (yes/no), No Yes No visible emissions). Each requirements are in compliance
Emissions Corrective Actions visual is on a 6-minute with the applicable emissions
(Recordkeeping) timeframe. If visual
Taken standard(s).
15A NCAC emissions are observed,
02Q.0508(f) then Method 22 must be
repeated in same day.
Maintenance of Method 22 (visual records
Monitoring Log -If performed monthly on one
emissions were Page summary(normal All the required monitoring,
Coloring Plant expected emissions= no
present,corrective record keeping,and reporting
Control of Visible NA 2.1.C.2.d.iii actions taken and No Yes No visible emissions). Each requirements are in compliance
Emissions results of action visual is on a 6-minute with the applicable emissions
(Recordkeeping) timeframe. If visual
taken. standard(s).
15A NCAC emissions are observed,
02Q.0508(f) then Method 22 must be
repeated in same day.
Reporting Year 2021 Permit#:09006T07
Page 9 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or Permit
of
Emission Source Control Condition Deviations? Records was Deviation Method(s)
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance
Determiningg
Comments
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Number(s)
Coloring Plant Submit Semiannual All the required monitoring,
Control of Visible Monitoring Report, Semiannual Monitoring record keeping,and reporting
Emissions NA 2.1.C.2.e due on 1/30 and No Yes No Reports submitted on or requirements are in compliance
(Reporting) 7/30 15A NCAC before 1/30 and 7/30 with the applicable emissions
.508(f) standard(s).
2.3 lb SO2/MM Btu No monitoring, recordkeeping,
Coloring Plant ESCPPHI heat input Based on AP-42 emissions or reporting is required at this
Dryers ESCPPH2 2.1.D.l.a 15A NCAC 02D No Yes No factors and fuel usage, time per 2.1.D.l.c of our
.0516 rate calc'd under limit permit. (ESCPPH3 referenced
in the permit not yet installed)
Coloring Plant ESCPPHI Meet NSPS UUU
ESCPPH2 [40 CFR Part 60 detailed in next two rows (ESCPPH3/CBD18 referenced
Dryers& CBD9 2.1.D.2.a sub UUU, including No Yes No below in the permit not yet installed)
Baghouses CBD10 sub A]
Methods 5&9, initial test
Coloring Plant ESCPPHI 0.057 gm/dscm PM completed 8/8/2002 and
ESCPPH2 [15A NCAC 2D 8/7/2002 for ESCPPHI/ (ESCPPH3/CBD18 referenced
Dryers& CBD9 2.1.D.2.b .0524&40 CFR No Yes No CBD9 and ESCPPH2/ in the permit not yet installed)
Baghouses CBD10 60.7321 CBD10.(ESCPPH3/
CBD18 not yet installed)
All the required monitoring,
record keeping,and reporting
requirements are in compliance
ESCPPHI 10%opacity(6 with the applicable emissions
Coloring Plant ESCPPH2 Continuous Opacity minute average) standard(s). There were no
I
Dryers& 2.1.D.2.c 15A NCAC 2D No Yes No deviations from the monitoring
Baghouses CBD9' .0524&40 CFR Monitoring System requirements of 40 CFR 60 sub
CBD10 60.732 UUU and the relevant Subpart
A"General Provisions."
(ESCPPH3/CBD18 referenced
in the permit not yet installed)
Reporting Year 2021 Permit#:090D6T07
P 9
Page 10 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1, 2021 through December 31, 2021
Terms&Conditions
Source or Permit
Emission Source Control Condition Deviations? Records was Deviation a Method(s)of
Condition Maintained? non-compliance Determining Comments
Number(s)Description Device ID Number Summary (yes/�) (yps/No/NA) issue?(yes/No) Compliance Status
Conduct Initial Methods 5&9,initial test All the required monitoring,
ESCPPHI NSPS UUU Test completed 8/8/2002 and record keeping,and reporting
Coloring Plant requirements are in compliance
ESCPPH2 [PM and visible 8/7/2002 for ESCPPHI/
Dryers& CBD9, 2.1.D.2.d emissions] No Yes No CBD9 and ESCPPH2/ with the applicable emissions
Baghouses standard(s).(ESCPPH3/
CBD10 15A NCAC 2D CBD10.(ESCPPH3/
0.2601 CBD18 not yet installed) CBD18 referenced in the
permit not yet installed)
install,calibrate,
Coloring Plant All the required monitoring,
Dryers& ESCPPHI maintain,and Continuous Opacity record keeping,and reporting
ESCPPH2 operate a COMS Monitoring System.
Baghouses 2.1.D.2.e.i No Yes No requirments are in compliance
CBD9, 15A NCAC 2Q Preventative maintenance
(Monitoring and CBD10 0508(f)&40 CFR procedures. with applicable emissions
.
Recordkeeping) standard(s).
60.734, .735
All the required monitoring,
Coloring Plant record keeping,and reporting
Dryers& ESCPPHI Inspect for leaks requirements are in compliance
CBD9, 2Q.0508(f)&40 procedures
ESCPPH2 1/yr. 15A NCAC Preventive maintenance
q
Baghouses 2.1.D.2.e.ii.(A) No Yes No with the applicable emissions
(Monitoring and
standa
Recordkeeping) CBD10 CFR 60.734, .735 CBD18 cedPn the
permit not yet installed)
Inspect for All the required monitoring,
Coloring Plant record keeping,and reporting
ESCPPHI structural integrity
Dryers& requirements are In compliance
ESCPPH2 1/yr. Preventive maintenance
Baghouses 2.S.D.2.e.ii.(B) No Yes No with the applicable emissions
CBD9, 15A NCAC 2Q procedures.
(Monitoring and CBD10 .05 standard(s).(ESCPPH3/
08{f)&40 CFR
Recordkeeping) 60.734,08(f .735 CBD18 referenced in the
permit not yet installed)
I
i
Reporting Year 2021 Permit#:09006T07
Page 11 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report _
For July 1,2021 through December 31,2021
Terms&Conditions
Source or Permit Method(s)of
Emission Source control Condition Deviations? Records was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? none?(Ye non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Any work orders on
baghouses are reported
into a maintenance data
For each instance tracking system called
of maintenance, CMMS.This system tracks
record date,time, all work performed and
results any variances from All the required monitoring,
Coloring Plant ESCPPHI If any variance manufacturers record keeping,and reporting
Dryers& ESCPPfrom manuf.'s maintenance procedures. requirements are in compliance
C
Baghouses BD9, 2 2.1.D.2.e.iii maintenance No Yes No CMMS builds the proper with the applicable emissions
BD
(Monitoring and recommend.,then maintenance history standard(s).(ESCPPH3/
Recordkeeping) CBD10 record corrections required for such an CBD18referenced in the permit
made emissions handling not yet installed)
15A NCAC 2Q system. Quarterly PM
.0508(f)&40 CFR records and other work
60.734, .735 conducted by a third party
are maintained
electronically or hard
copies of work performed.
Coloring Plant Submit Semiannual All the required monitoring,
Dryers& Monitoring Report, Semiannual Monitoring record keeping,and reporting
Baghouses N/A 2.1.D.2.f due on 1/30 and No Yes No Reports submitted on or requirements are in compliance
(Reporting) 7/30 15A NCAC before 1/30 and 7/30 with the applicable emissions
.508(f) standard(s).
Particulate
Emissions E=4.10 All the required monitoring,
06� Per NCAC 2D .0515 record keeping,and reporting
ColoringPlant ESCPKI x(P) for
ESCPK2 P<=30tph process weight rule Title V requirements are in compliance
Kilns&Baghouses CDB13, 2.1.E.i.a E=55.0 x(P)o.ri No Yes No calculation,we are in with the applicable emissions
(Particulates) compliance with this standard(s). (ESCPK3/CBD20
CDB14 40 for P>=30 tph requirement. referenced in the permit not
[15A NCAC 02D yet installed)
0515]
Reporting Year 2021 Permit#:09006T07
Page 12 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1, 2021 through December 31,2021
Terms&Conditions
Source or permit Method(s)of
Emission Source Control Condition Deviations? Records was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) Issue?(Yes/No) Compliance Status
If emissions testing
Coloring Plant ESCPKI is required,testing Perform testing per 15A No emissions testing is
ESCPK2 shall be performed NCAC 02D.2600 and currently required.(ESCPK3/
Kilns&Baghouses CDB13, 2.1.E.i.b in accordance with No Yes No General Condition JJ found CBD20 referenced in the
(Testing) CDB14 General Condition in Section 3 of the permit. permit not yet installed)
JJ.
All the required monitoring,
Coloring Plant ESCPKI Inspect for leaks record keeping,and reporting
Kilns&Baghouses ESCPK2 1/yr. 15A NCAC Preventive maintenance requirements are in compliance
(Monitoring and CDB13, 2Q.0508(f)&40 procedures
2.1.E.1.c.1 No Yes No with the applicable emissions Recordkeeping) CDB14 CFR 60.734, .735 standard(s).(ESCPK3/CBD20referenced in the permit not
yet installed)
Inspect for All the required monitoring,
Coloring Plant ESCPKI structural integrity record keeping,and reporting
Kilns&Baghouses ESCPK2 1/yr. Preventive maintenance requirements are in compliance
(Monitoring and CDB13, 2.1.E.l.c.ii 15A NCAC 2Q No Yes No procedures. with the applicable emissions
Recordkeeping) CDB14 .0508(f)&40 CFR standard(s).(ESCPK3/CBD20
60.734, .735 referenced in the permit not
yet installed)
Any work orders on
For each instance baghouses and were
of maintenance, reported into a
record date,time, maintenance data tracking
results system called CMMS.This All the required monitoring,
Coloring Plant ESCPKI If any variance system tracks all work record keeping,and reporting
Kilns&Baghouses ESCPK2 from variance
's performed and any requirements are in compliance
(Monitoring and CDB13, 2.1.E.l.d maintenance No Yes No variances from with the applicable emissions
(Monitoring
in CDB14 recommend.,then manufacturers standard(s). (ESCPK3/CBD20
Recordkeeping) maintenance procedures. referenced in the permit not
record corrections CMMS builds the proper yet installed)
made
15A NCAC 02Q maintenance history
.0508(f) required for such an
emissions handling
system.
Reporting Year 2021 Permit#:09006To7
Page 13 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
I
Semiannual Compliance Summary Report _
For July 1,2021 through December 31,2021
Terms&Conditions
source or Permit Methods)of
Emission Source Control Condition Deviations? Records was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s) Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Submit results of
any maintenance All the required monitoring,
ESCPKI performed on the record keeping,and reporting
Coloring Plant Preventive maintenance requirements are in compliance
Kilns&Ba houses ESCPK2 2.1.E.l.e bagfilters within 30 No Yes No 9 CDB13, day a request procedures and with the applicable emissions
of
(Reporting) CDB14 by D of recordkeeping standard(s). (ESCPK3/CBD20
[ NCAC 02Q. referenced in the permit not
0508(f)] yet installed)
Submit Semiannual All the required monitoring,
ESCPKI Monitoring Report, record keeping,and reporting
Coloring Plant Semiannual Monitoring requirements are in compliance
Kilns&Baghouses ESCPK2 2.1.E.1.f 7/30 due on 1/30 and No Yes No Reports submitted on or with the applicable emissions
(Reporting) CDB14 [15A NCAC 02Q. before 1/30 and 7/30 standard(s). (ESCPK3/
0508(f)] CBD20 referenced in the
permit not yet installed)
No monitoring, recordkeeping,
Coloring Plant ESCPKI 2.3 lb SC2/MM Btu or reporting is required at this
Kilns&Baghouses ESCPK2 heat input Based on AP-42 emissionstime per 2.1.E.2.c of our
(Sulfur Dioxide CDB13, 2.1.E.2 [15A NCAC No Yes No factors and fuel usage,
rate calc'd under limit Permit. (ESCPK3/CBD20
Emissions) CDB14 02D.0516] referenced in the permit not
yet installed)
Visible Emissions
not to exceed 20% Method 22 (visual records
when averaged
over a six minute performed monthly on one
period,and may page summary.Shall not
not occur more be more than 20 opacity No visible emissions exceeding
Coloring Plant ESCPKI then once in any when averaged over a six 20%were observed or
2.1.E.3.a one hour period No Yes No
Kilns&Baghouses ESCPK2 minute period. However,
(Control of Visible CDB13, six minute averaging recorded. (ESCPK3/CBD20
and not more then referenced in the permit not
Emissions) CDB14 four times per in periods may exceed 20 yet installed)
24 hour period. No not more than once in any
event may exceed hour and not more than 4
87%opacity. times in any 24 hour
15A NCAC 02D period.
.0521
Reporting Year 2021 Permit# 09006T07
Page 14 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or Permit
Emission Sour ce Control COndltlOn Deviations? Records Was Deviation a Method(s)of
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
If emissions testing
Coloring Plant ESCPKI is required,testing Perform testing per 15A No emissions testing is
ESCPK2 shall be performed NCAC 2D .2601 and currently required. (ESCPK3/
Kilns&Baghouses CDB13, 2.1.E.3.b in accordance with No Yes No General Condition JJ found CBD20 referenced in the
(Testing) CDB14 15A NCAC 2D in Section 3 of the permit. permit not yet installed)
.2601
Method 22(visual records
performed monthly on one
page summary(normal All the required monitoring,
Coloring Plant Observe visible record keeping,and reporting
ESCPKI expected emissions= no
Kilns&Baghouses emissions once per requirements are in compliance
ESCPK2 visible emissions). Each
Control of Visible 2.1.E.3.c month for above No Yes No with the applicable emissions
"
CDB13, visual is on a 6-minute
Emissions normal"and standard(s).(ESCPK3/CBD20
CDB14 timeframe. If visual
(Monitoring) record. referenced in the permit not
emissions are observed,
then Method 22 must be Yet installed)
repeated in same day.
If visible emissions
from a source are
observed to be All the required monitoring,
Coloring Plant record keeping,and reporting
ESCPKI above normal,take
Kilns&Baghouses requirements are in compliance
Control of Visible ESCPK2 2.1.E.3.c.i appropriate action No Yes No Results of Method 9 and with the applicable emissions
Emissions CDB13, to correct the issue 22 checks and reports. standard(s).(ESCPK3/CBD20
(Monitoring) CDB14 and record the referenced in the permit not
action taken.
[15A NCAC 2Q yet installed)
.0508(f)]
Reporting Year 2021 Permit#:09006T07
Page 15 of 30 Jul-Dec Report Location ID#: 1900104
110 - 11
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
i
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or Permit Method(s)of
Emission Source Control Condition Deviations? R
Description Device ID Condition Summary (Yes/No) Maintecords Was Deviation a ained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
If visible emissions
from a source are
observed to be
above normal,and
after corrective
action is taken All the required monitoring,
,
Coloring Plant record keeping,and reporting
ESCPKI demonstrate that
Kilns&Baghouses v requirements/o ESCPK2 the opacity is Results of Method 9 and
are in compliance
Control of Visible CD1313, 2.1.E.3.c.ii below the 20% No Yes No 22 checks and reports. with the applicable emissions
Emissions CDB14 limit and at or standard(s). (ESCPK3/CBD20
(Monitoring) below the"normal" referenced in the permit not
emissions for a yet installed)
period of 12
minutes.
[15A NCAC 2Q
.0508(f)]
Method 22(visual records
performed monthly on one
page summary(normal All the required monitoring,
Coloring Plant Maintenance of record keeping,and reporting
Kilns&Baghouses ESCPK2 expected emissions= no
Monitoring Log - requirements are in compliance
ESCPK2 visible emissions). Each
Control of Visible CDB13, 2.1.E.3.d.i Date and Time No Yes No visual is on a 6-minute with the applicable emissions
Emissions CDB14 timeframe.If visual 15A NCAC standard(s). (ESCPK3/CBD20
(Recordkeeping) 2Q.0508(f) emissions are observed, referenced in the permit not
then Method 22 must be yet installed)
repeated in same day.
Maintenance of Method 22 (visual records
Monitoring Log- performed monthly on one All the required monitoring,
page summary(normal
Results,Visible record keeping,and reporting
ESCPK2 expected emissions= no
Coloring Plant Emissions Present requirements are in compliance
ESCPK2 visible emissions).Each
Kilns&Baghouses 2.1.E.3.d.ii (yes/no), No Yes No with the applicable emissions
CDB13, visual is on a 6-minute
(Recordkeeping) CDB14 Corrective Actions timeframe. If visual standard(s).(ESCPK3/CBD20
Taken referenced in the permit not
15A NCAC emissions are observed, yet installed)
2Q.0508(f) then Method 22 must be
repeated in same day.
Reporting Year 2021 Permit#:09006T07
Page 16 of 30 Jul-Dec Report Location ID#. 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1, 2021 through December 31,2021
Terms&Conditions
Source or Permit Methods of
Emission Source Control Condition Deviations? Records Was Deviation a ( )
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) Issue. (Yes/No) Compliance Status
Maintenance of Method 22(visual records
Monitoring Log-If performed monthly on one All the required monitoring,
Coloring Plant emissions were page summary(normal record keeping,and reporting
ESCPKI expected emissions=no requirements are in compliance
Kilns&Baghouses present,corrective
ESCPK2 visible emissions).Each
Control of Visible CD813, 2.1.E.3.d.iii actions taken and No Yes No visual is on a 6-minute with the applicable emissions
Emissions results of action standard(s).(ESCPK3/CBD20
CDB14 timeframe.If visual
(Recordkeeping) taken. emissions are observed referenced in the permit not
,
15A NCAC yet installed)
2Q.0508(f) then Method 22 must be
repeated in same day.
Submit Semiannual All the required monitoring,
Coloring Plant record keeping,and reporting
Kilns&Baghouses ESCPKI Monitoring Report, Semiannual Monitoring requirements are in compliance
CDB13, 7/30
Control of Visible ESCPK2 2.1.E.3.e due on 1/30 and No Yes No Reports submitted on or with the applicable emissions
Emissiosns before 1/30 and 7/30 standard(s). (ESCPK3/
0508(f)]
(Reporting) CD814 [15A NCACO2Q CBD20 referenced in the
permit not yet installed)
Particulate
Emissions E=4.10
All the required monitoring,
Coloring Plant ESCPMI x(P) for
0 6� Per NCAC 2D.0515 record keeping,and reporting
Mixers& ESCPM2 P<=30tph process weight rule Title V requirements are in compliance
Baghouses CDBil, 2.1.F.l.a E=55.0 x(P)°11- No Yes No calculation,we are in with the applicable emissions
(Particulates) CDB12 40 for x(P)O"- compliance with this standard(s).(ESCPM3/CBD19
[15f NCAC 0 t requirement. referenced in the permit not
.0515] yet installed)
If emissions testing Perform testing,if
Coloring Plant ESCPMI is required,testing required,per 15A NCAC No emissions testing is
21.F.l.b
Mixers& ESCPM2 shall be performed currently required.(ESCPM3/
. No Yes No OZD.2600 and General
Baghouses CDB11, in accordance with CBD19 referenced in the
(Testing) CDB12 15A NCAC 2D Condition JJ found permit not yet installed)
.2601 Section 3 of the permit.
Reporting Year 2021 Permit#:09006T07
Page 17 of 30 Jul-Dec Report Location ID#:1900104
I =---
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or permit Records Was Deviation a Method(s)of
Emission Source Control Condition Deviations?
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
All the required monitoring,
Coloring Plant ESCPMI inspect for leaks record keeping,and reporting
Mixers& requirements are in compliance
ESCPM2 1/yr. Preventive maintenance
Baghouses CDB11, 2.1.1'.1.0 [15A NCAC 2Q No Yes No procedures with the applicable emissions
(Monitoring/ CDB12 .0508(f)] standard(s).(ESCPM3/CBD19
Recordkeeping) referenced in the permit not
yet installed)
inspect for All the required monitoring,
Coloring Plant record keeping,and reporting
ESCPMI structural integrity
Mixers& requirements are in compliance
ESCPM2 1/yr. Preventive maintenance
Baghouses 2.1.F.i.c.ii No Yes No with the applicable emissions
CDB11, 15A NCAC 2Q procedures.
(Monitoring/ 08(f)& standard(s). (ESCPK3/CBD20
CDB12 .05 40 CFR
Recordkeeping) 60.734,08(f . 4 referenced in the permit not
yet installed)
Any work orders on
baghouses and were
For each instance of maintenance, reported into amaintenance data tracking
record date,time,results system called CMMS.This All the required monitoring,
Coloring Plant system tracks all work record keeping,and reporting
Mixers& ESCPMI If any variance
ESCPM2 from manuf's performed and any requirements are in compliance
.
Baghouses 2.1.F.l.d No Yes No variances from with the applicable emissions
CDB11, maintenance
(Monitoring/ manufacturers standard(s).(ESCPM3/CBD19
Recordkeeping) CDB12 recommend.,then maintenance procedures. referenced in the permit not
record corrections CMMS builds the proper yet installed)
made
[15A NCAC 02Q maintenance history
.0508(f) ] required for such an
emissions handling
system.
Submit results of
any maintenance All the required monitoring,
Coloring Plant ESCPMI performed on the record keeping, and reporting
Mixers& ESCPM2 bagfilters within 30 Preventive maintenance requirements are in compliance
2.1.F.l.e No Yes No procedures and with the applicable emissions
Baghouses CDB11. day of a request
(Reporting) CDB12 by DAQ recordkeeping standreferenced
i (ESCPM3/CBD19
[15A NCAC referenced in the permit not
02Q.0508(f)] yet installed)
Reporting Year 2021 Permit#:09006T07
Page 18 of 30 Jul-Dec Report Location ID#: 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report _
For July 1,2021 through December 31, 2021
Terms&Conditions
Source or permit Method(s)of
Emission Source COnYrO1 Condition Deviations? Records Was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number (Yes/No/NA) issue. (Yes/No) Compliance Status
Number(s)
Submit Semiannual All the required monitoring,
Coloring Plant ESCPMI Monitoring Report, record keeping,and reporting
Mixers& ESCPM2 due on 1/30 and Semiannual Monitoring requirements are in compliance
Baghouses CDB11, 2.1.F.l.f 7/30 No Yes No Reports submitted on or with the applicable emissions
(Reporting) CDB12 [15A NCAC before 1/30 and 7/30 standard(s). (ESCPM3/
02Q.0508(f)] CBD19 referenced in the
permit not yet installed)
Visible Emissions
not to exceed 20% Method 22 (visual records
when averaged
over a six minute performed monthly on one-
period,and may page summary. Shall not
be more than 20%opacity
Coloring Plant ESCPM2 not occur more No visible emissions exceeding
ESCPM2
Mixers& then once in any when averaged over a six 20%were observed or
minute period. However,
Baghouses 2.1.F.2.a one hour period No Yes No recorded. (ESCPM3/CBD19
CDB11, six minute averaging
(Control of Visible CDB12 and not more then referenced in the permit not
Emissions) four times per in periods may exceed 20% yet installed)
24 hour period. No not more than once in any
event may exceed hour and not more than 4
87%opacity. times in any 24-hour
[15A NCAC 2D period.
.0521]
Coloring Plant If emissions testing
Control of Visible ESCPM2 is required,testing Perform testing per 15A No emissions testing is
Emissions ESCPM2 shall be performed NCAC 02D .2600 and currently required. (ESCPM3/
Mixers& CDB11, 2.1.F.2.b in accordance with No Yes No General Condition JJ found CBD19 referenced in the
Baghouses CDB12 15A NCAC 21D in Section 3 of the permit. permit not yet installed)
(Testing) .2601
Reporting Year 2021 Permit#.09006T07
Page 19 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31, 2021
Terms&Conditions
Source or permit Method(s)of
Emission Source Control Condition Deviations? Records Was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)p Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Method 22 (visual records
performed monthly on one All the required monitoring,
Coloring Plant page summary(normal
Observe visible record keeping,and reporting
Control of Visible ESCPMI emissions once per expected emissions= no
requirements are in compliance
Emissions ESCPM2 visible emissions).Each
2.1.F.2.c month for above No Yes No with the applicable emissions
Mixers& CDB11, visual is on a 6-minute
Baghouses CDB12 "normal"and timeframe.If visual referenced
(ESCPM3 i CBD19
(Monitoring) record. emissions are observed, referenced in the permit not
then Method 22 must be yet installed)
repeated in same day.
If visible emissions
from a source are
Coloring Plant observed to be All the required monitoring,
Control of Visible ESCPMI above normal,take record keeping,and reporting
Emissions ESCPM2 appropriate action Results of Method 9 and requirements are in compliance
Mixers& CDB11, 2.1.F.2.c.i to correct the issue No Yes No 22 checks and reports. standwith the applicable emissions
Baghouses CDB12 and record the referenced
i (ESCPM3 i CBD19
(Monitoring) action taken. referenced in the permit not
[15A NCAC 2Q yet installed)
.0508(f)]
Reporting Year 2021 Permit#i 09006T07
Page 20 of 30 Jul-Dec Report Location ID#: 1900104
111
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
_ Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or permit
Emission Source Control Condition Deviations? Records Was Deviation a Method(s)Of
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue. (Yes/No) Compliance Status
If visible emissions
from a source are
observed to be
above normal,and
after corrective
action is taken All the required monitoring,
,
Coloring Plant record keeping,and reporting
ESCPMI demonstrate that
Control of Visible o requirements are in compliance
/o
Emissions ESCPM2 2 1.F.2.c.ii the opacity o is No Yes No Results of Method 9 and with the applicable emissions
Kilns&Baghouses CDB11, below the 20/0 22 checks and reports. standard(s). (ESCPM3/CBD19
(Monitoring) CDB12 limit and at or referenced in the permit not
below the"normal"
e yet installed)
missions for
period of 12
minutes.
15A NCAC 2Q
.0508(f)
Method 22 (visual records
performed monthly on one All the required monitoring,
Coloring Plant page summary(normal
Maintenance of record keeping,and reporting
Control of Visible ESCPMI Monitoring expected emissions= no
Emissions ESCPM2
g Log visible emissions). Each requirements are in compliance
Mixers& CDB11, 2.1.F.2.d.i Date and Time No Yes No visual is on a 6-minute with the applicable emissions
Baghouses CDB12
[15A NCAC timeframe. If visual standard(s). (ESCPM3/CBD19
(Recordkeeping) 2Q.0508(f)] emissions are observed, referenced in the permit not
then Method 22 must be yet installed)
repeated in same day.
Maintenance of
Method 22 (visual records
Monitoring Log - performed monthly on one All the required monitoring,
page summary(normal
Results,Visible record keeping,and reporting
Coloring Plant ESCPMI expected emissions= no
Emissions Present requirements are in compliance
Mixers& ESCPM2 visible emissions).Each
2.1.F.2.d.ii (yes/no), No Yes No with the applicable emissions
Baghouses CDB11, visual is on a 6-minute
Corrective Actions standard(s). (ESCPM3/CBD19
(Recordkeeping) CDB12 timeframe. If visual
Taken referenced in the permit not
[15A NCAC emissions are observed, yet installed)
2Q.0508(f)] then Method 22 must be
repeated in same day.
Reporting Year 2021 Permit#:09006T07
Page 21 of 30 Jul-Dec Report Location ID#: 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1, 2021 through December 31,2021
Terms&Conditions
source or Permit Method(s)of
Emission Source Control Condition Deviations? Records was Deviation a
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Maintenance of Method 22 (visual records
performed monthly on one
Plant Monitoring Log- If All the required monitoring,
Coloring page summary(normal
emissions were record keeping,and reporting
Control of Visible ESCPMI expected emissions= no
present,corrective requirements are in compliance
Emissions ESCPM2 visible emissions). Each
Mixers& CDB11, 2.1.F.2.d.iii actions taken and No Yes No visual is on a 6-minute with the applicable emissions
Baghouses CDB12 results of action timeframe. If visual standard(s). (ESCPM3/CBD19
(Recordkeeping) taken. emissions are observed, referenced in the permit not
[15A NCAC then Method 22 must be yet installed)
2Q.0508(f)]
repeated in same day.
Coloring Plant Submit Semiannual All the required monitoring,
Control of Visible ESCPMI Monitoring Report, record keeping, and reporting
Emissions ESCPM2 due on 1/30 and Semiannual Monitoring requirements are in compliance
Mixers& CDB11, 2.1.F_2.e 7/30 No Yes No Reports submitted on or with the applicable emissions
Baghouses CDB12 [15A NCAC 02Q before 1/30 and 7/30 standard(s). (ESCPM3/
(Reporting) .0508(f)] CBD19 referenced in the
permit not yet installed)
Particulate
Emissions E=4.10 Methods 5&9, initial test All the required monitoring,
x( )P 061 for completed 8/5/2002 thru record keeping,and reporting
Coloring Plant 8/8/2002, Per NCAC 2D requirements are in compliance
ESCPCI P<=30tph
Coolers ESCPC2 2.1.G.l.a E=55.0 x (P)o.ii No Yes No .0515 process weight rule with the applicable emissions
(Particulates) Title V calculation,we are standard(s). (ESCPC3
40 for P>=30 tph in compliance with this referenced in the permit not
[15A NCAC 2D requirement. yet installed)
.0515]
Perform testing, if
If emissions testing required, per 15A NCAC
is required,testing 02D .2600 and General No additional emissions testing
Coloring Plant ESCPCI 2.1.G.1.b shall be performed No Yes No Condition JJ found in is currently required.(ESCPC3
Coolers(Testing) ESCPC2 in accordance with Section 3 of the permit. referenced in the permit not
15A NCAC 02D Methods 5&9, initial test yet installed)
.2600 completed 8/5/2002 thru
8/8/2002
Reporting Year 2021 Permit#:09006T07
Page 22 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or Per
Records Was Deviation a Method(s)of
Emission Source Control Condition Deviations?
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Maintain records
sufficient to All the required monitoring,
Coloring Plant record keeping,and reporting
demonstrate
Coolers Methods 5&9,initial test requirements are in compliance
(Monitoring/ ESCPCI 2.1.G.l.c compliance and No Yes No completed 8/5/2002 thru with the applicable emissions
ESCPC2 make these
Recordkeeping/ 8/8/2002 standard(s). (ESCPC3
Reporting) records available referenced in the permit not
to DAQ upon
yet installed)
request.
Visible Emissions
not to exceed 20%
when averaged Method 22 (visual records
over a six minute performed monthly on one
period,and may page summary. Shall not
/o
not occur more be more than 20 opacity
Coloring Plant then once in any when averaged over a six No visible emissions exceeding
ESCPCI minute period. However, 20%were observed or
Coolers(Control of ESCPC2 2.1.G.2.a one hour period No Yes No six minute averaging recorded. (ESCPC3 referenced
Visible Emissions) and not more then
periods may exceed 20% in the permit not yet installed)
four times per in
four
hour period. No not more than once in any
24 t may exceed hour and not more than 4
event
times in any 24-hour
opacity.
115A NCAC 2D period.
.0521(d)]
Coloring Plant If emissions testing
Control of Visible
s required,testing Methods 5&9,initial test No additional emissions testing
ESCPCI shall be performed is currently required. (ESCPC3
Emissions ESCPC2 2.1.G.2.b in accordance with No Yes No completed 8/5/2002 thru referenced in the permit not
Coolers 15A NCAC 2D 8/8/2002 yet installed)
(Testing) .2601
Reporting Year 2021 Permit#:09006T07
Page 23 of 30 Jul-Dec Report Location ID#: 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or Permit
Emission Source Control Condition Deviations? Records was Deviation a Method(s)of
Description Device ID Condition Summary (yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Method 22(visual records
performed monthly on one All the required monitoring,
Coloring Plant Observe visible page summary(normal record keeping,and reporting
Control of Visible emissions once per expected emissions=no requirements are in compliance �
ESCPCi visible emissions).Each
Emissions 2.1.G.2.c month for above No Yes No with the applicable emissions
ESCPC2 visual is on a 6-minute
Coolers "normal"and standard(s).(ESCPC3
(Monitoring) record. timeframe.If visualreferenced i)the permit not
emissions are observed,
then Method 22 must be yet installed)
repeated in same day.
If visible emissions
from a source are
observed to be All the required monitoring,
Coloring Plant record keeping,and reporting
take
Control of Visible above normal, requirements are in compliance
Emissions ESCPCI 2.1.G.2.c.i appropriate action No Yes No Results of Method 9 and with the applicable emissions
Coolers ESCPC2 to correct the issue 22 checks and reports. standard(s).(ESCPC3
(Monitoring) and record the referenced in the permit not
action taken. yet installed)
[15A NCAC 2Q
.0508(f)]
Reporting Year 2021 Permit#:09006T07
Page 24 of 30 Jul-Dec Report Location ID#:1900104
North Carolina Department of Environmental and Natural Resources _
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or Permit
Emission Source Control Condition Deviations? Records Was Deviation a Method(s)Of
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue. (Yes/No) Compliance Status
If visible emissions
from a source are
observed to be
above normal,and
after corrective
action is taken All the required monitoring,
,
Coloring Plant record keeping,and reporting
Control of Visible demonstrate thato requirements are in compliance
/o
Emissions ESCPCI 2.1.G.2c.ii the opacity is No Yes No Results of Method 9 and with the applicable emissions
Coolers ESCPC2 below the 20. /0 22 checks and reports. standard(s). (ESCPC3
(Monitoring) limit and at or referenced in the permit not
below the"normal"
e yet installed)
missions for
period of 12
minutes.
[15A NCAC 2Q
.O508(f)]
Method 22 (visual records
performed monthly on one
page summary(normal All the required monitoring,
o
Coloring Plant Maintenance of expected emissions = n record keeping,and reporting
Control of Visible Monitoring Log- requirements are in compliance
Each ESCPCI
Emissions Z.1.G.2.d.i Date and Time No Yes No visible emissions). with the applicable emissions
ESCPC2 visual is on a 6-minute
Coolers [15A NCAC standard(s). (ESCPC3
(Recordkeeping) 2Q.0508(f)] timeframe. If visualemissions are observed, referenced in the permit not
then Method 22 must be yet installed)
repeated in same day.
Maintenance of Method 22(visual records
Monitoring Log- performed monthly on one-All the required monitoring,
Coloring Plant Results,Visible page summary(normal o expected emissions= n record keeping,and reporting
Control of Visible Emissions Present requirements are in compliance
Emissions ESCPCI d 2 G 1 2. . . . .ii visible emissions). Each
ESCPC2 (Yes/no), No Yes No visual is on a 6-minute with the applicable emissions
Coolers Corrective Actions timeframe If visual standard(s).(ESCPC3
.
(Recordkeeping) Taken referenced in the permit not
15A NCAC emissions are observed, yet installed)
2Q.0508(f) then Method 22 must be
repeated in same day.
Reporting Year 2021 Permit#:09006T07
Page 25 of 30 Jul-Dec Report Location ID#: 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or permit
Emission Source Control Condition Deviations? MaiRecords was Deviation a Method(s)of
Description Device ID Condition Summary (Yes/No) ntained? non-compliance Determining Comments
Number(s) Number (Yes/No/NA) issue. (Yes/No) Compliance Status
Maintenance of Method 22(visual records
Monitoring Log-If performed monthly on one-All the required monitoring,
emissions were page summary(normal record keeping,and reporting
Coloring Plant present,corrective requirements are in compliance
Coolers ESCPC1 2,1.G.2.d.iii actions taken and No Yes No vi expected emissions = no sible emissions). Each with the applicable emissions
(Recordkeeping) ESCPC2 results of action visual is on a 6-minute standard(s).(ESCPC3
timeframe. If visual
taken. referenced in the permit not
[25A NCAC emissions are observed, yet installed)
2Q.0508(f)] then Method 22 must be
repeated in same day.
Coloring Plant Submit Semiannual record keeping,
All lyd required ll
Monitoring Report, ping'andreportin g
Control of Visible ESCPC2 Semiannual Monitoring requirements are in compliance
7/30
Emissions 2.1.G.2.e due on 1/30 and No Yes No Reports submitted on or with the applicable emissions
Coolers [15A NCAC ESCPC2 before 1/30 and 7/30 standard(s). (ESCPC3
02Q.0508(f)]
(Reporting) referenced in the permit not
2Q. 08(
yet installed)
Fugitive non-
Multiple process dust
Emission emissions: do not No Records of su No monitoring, recordkeeping,
Source bstantives) cause or contribute or reporting is required at this
NA substantive NA No complaints on fugitive
Non-process 2.2.A.l.b to"substantive complaints emissions if any time per 2.2.A.l.h of our
, .
Fugitive Dust complaints" permit.
Emission Sources 15A NCAC 02D
.0540
Within 30 days of
notice from
Director of second
Multiple substantive
Emission complaint in 12 No Records of substantive No monitoring, recordkeeping,
Source(s) substantive NA No complaints on fugitive NA 2.2.A.i.c.i month period, or reporting is required at this
Non-process submit description complaints emissions, if any. time per 2.2.A.l.h of our
Fugitive Dust of what has/will be permit.
Emission Sources done to reduce the
emissions
[15A NCAC
02D.0540]
Reporting Year 2021 Permit*09006T07
Page 26 of 30 Jul-Dec Report Location ID#: 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1, 2021 through December 31,2021
Terms&Conditions
Source or permit Records Was Deviation a Method(s)of
Emission Source Control Condition Deviations?
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
p Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Number(s)
Within 60 days of
notice from
Multiple Director of second
substantive
Emission No monitoring, recordkeeping,
complaint in 12- No Records of substantive
Source(s) or reporting is required at this
Non-process NA 2.2.A.l.c.ii month period, substantive NA No complaints on fugitive time per 2.2.A.l.h of our
submit to the complaints emissions, if any.
Fugitive Dust permit.
Emission Sources Director a Control
Plan
[15A NCAC
02D.0540]
Non-process within 30 days
Fugitive Dust after the Director No monitoring,recordkee
Emission Sources approves the plan, No Records of substantive pm
Particulates from NA 2.1.A.l.c.iii be in compliance substantive NA No complaints on fugitive time
reporting is required at this
s
fugitive non with the plan complaints emissions, if any. tme per 2.2.A.l.h of our
Process dust [15A NCAC permit.
emission sources 02D.0540]
ES1415
Facility-wide ESCPPHI Monthly monitoring This requirement was added in
affected ESCPPH2 of total HAP 3 with our new permit
emission sources ESCPKI emissions from anndd 010 the facility began meeting
Dryers, Kilns& ESCPK2 2.2.B.2.c facility wide Mass balance method the new requirements
Mixers&Coolers ESCPMI 2.2.B.2.d sources of HAP No Yes No utilized for monitoring of immediately after the permit
(HAP Emissions- ESCPM2 emissions. HAP emissions. was issued. M3,and
E
Monitoring& ESCPC1 Maintain records Eferenc d in the,and t not
Recordkeeping) ESCPC2 for 5 years on site. referenced in the permit not
yet installed)
Facility-wide
affected Submit Semiannual All the required monitoring,
emission sources Monitoring Report, Semiannual Monitoring record keeping,and reporting
Dryers, Kilns& NA 2.2.B.2.e due 1/30 and 7/30 No Yes No Reports submitted on 1/30 requirements are in compliance
Mixers&Coolers [15A NCAC 02Q. and 7/30 with the applicable emissions
(HAP Emissions- 0508(f)] standard(s).
Reporting)
Reporting Year 2021 Permit#:09006T07
Page 27 of 30 Jul-Dec Report Location ID#:1900104
E I- E -
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or permit
Emission Source Control Condition Deviations? Records Was Deviation a Method(s)of
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
ES1415
ESCPPHI
Facility-wide ESCPPH2 Permit limits not to
affected ESCPKI be exceeded: All the required monitoring,
emission sources ESCPK2 Arsenic&Compds Mass balance method record keeping,and reporting
2.2.B.3.a No Yes No utilized for monitoring of requirements are in compliance
Dryers, Kilns& ESCPMI 0.69 Ib/yr, TAP emissions. with the applicable emissions
Mixers&Coolers ESCPM2 Cadmium Metal
(HAP Emissions) ESCPCI 3.79 Ib/yr standard(s).
ESCPC2
ES1415
ESCPPHI
Facility-wide ESCPPH2
affected ESCPKI 15A NCAC 2Q All the required monitoring,
emission sources ESCPK2 .0711: Emissions Mass balance method record keeping,and reporting
2.2.B.4 No Yes No utilized for monitoring of requirements are in compliance
Dryers, Kilns& ESCPMI Rates Requiring a
Mixers&Coolers ESCPM2 Permit TAP emissions. with the applicable emissions
(TAP Emissions) ESCPCI standard(s).
ESCPC2
Compliance ESCPMI
Assurance ESCPM2 Pressure drop All the required monitoring,
Monitoring ESCPKI A continuous data
monitored record keeping,and reporting
Affected Sources ESCPK2 acquisition database
2.2.C.i.c.i. continuously and No Yes No requirements are in compliance
Kilns&Mixers& CDB11 daily averages monitors pressure drop on with the applicable emissions
Baghouses CDB12 our baghouses.
(Monitoring and CDB13 recorded daily standard(s).
Recordkeeping) CDB14
Compliance ESCPMI
Assurance ESCPM2 All the required monitoring,
Monitoring ESCPKI 2 >= P-drop A continuous data
record keeping,and reporting
Affected Sources ESCPK2 acquisition database
2.2.C.l.c.i.(B) across the bagfilter No Yes No requirements are in compliance
Kilns&Mixers& CDB11 <= 6 in H2O monitors pressure drop on with the applicable emissions
Baghouses CDB12 our baghouses.
(Monitoring and CDB13 standard(s).
Recordkeeping) CDB14
Reporting Year 2021 Permit#:09006T07
Page 28 of 30 Jul-Dec Report Location ID#: 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or permit Method(s)of
Emission Source Control Condition Deviations? Records Was Deviation a
Description Device ID Condition Summary (Yes/No) Main[ained? non-compliance Determining Comments
Number(s)
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
In the event of an
excursion
Permittee shall
take appropriate
action to correct as
Compliance ESCPMI soon as possible. All the required monitoring,
If a source or Monitor differential
Assurance ESCPM2 record keeping,and reporting
bagfilter operates pressure and operating
Monitoring ESCPKS with than ten conditions on a minimum requirements are in compliance
Affected Sources ESCPK2 with the applicable
2.2.C.1.c.ii excursi more ons in a No Yes No of a semi-annual basis to
Kilns&Mixers& CDB11 standard(s). (ESCPM3/CBD19
semiannual determine if Quality
Baghouses CDB12 andESCPK3/CBD20
reporting period, Improvement Plan is
(Monitoring and CDB13 then the permittee required referenced in the permit not
.
Recordkeeping) CDB14 yet installed)
shall develop a
Quality
Improvement
Plan(QIP) in
accordance with 40
CFR 64.8.
Preventative maintenance
procedures. Date and time
of reached recorded
Compliance ESCPMI Results of action, results of All the required monitoring,
Assurance ESCPM2 monitoring differential pressure and record keeping,and reporting
Monitoring ESCPKI inspections, emissions monitoring. requirements are in compliance
Affected Sources ESCPK2 maintenance, Results of any inspections with the applicable
Kilns&Mixers& CDB11 2.2.C.l.c.iii calibrations and No Yes No or maintenance performed standard(s). (ESCPM3/CBD19
Baghouses CDB12 corrections as on baghouse or differential and ESCPK3/CBD20
(Monitoring and CDB13 pursuant to pressure drop gauges.Any referenced in the permit not
recordkeeping) CDB14 sections above. variance from yet installed)
manufacturer's
recommendations, if any
corrections made.
Reporting Year 2021 Permit#:09006T07
Page 29 of 30 Jul-Dec Report Location ID#:1900104
North.Carolina Department of Environmental and Natural Resources
Division of Air Quality
Semiannual Compliance Summary Report
For July 1,2021 through December 31,2021
Terms&Conditions
Source or
Emission Source_ Control permit Condition Deviations? Records Was Deviation Methods
Description Device ID Condition Summary (Yes/No) Maintained? non-compliance
Determiningg
Comments
Number (Yes/No/NA) issue?(Yes/No) Compliance Status
Number(s)
Compliance ESCPMi All the required monitoring,
Assurance ESCPM2 record keeping,and reporting
ESCPKI requirements are in compliance
Monitoring Submit Semiannual Semiannual Monitoring
ESCPK2 with the applicable emissions
Affected Sources 2.2.C.i.d Monitoring Report, No Yes No Reports submitted by 1/30
Kilns&Mixers& CDBII due 1/30 and 7/30 and 7/30 standard(s).(ESCPM3/CBD19
Baghouses CDB12 and ESCPK3/CBD20
(Reporting) CDB13 referenced in the permit not
CDB14 yet installed)
Reporting Year 2021 Permit#:09006T07
Page 30 of 30 Jul-Dec Report Location ID#: 1900104
North Carolina Department of Environmental and Natural Resources
Division of Air Quality
_ Compliance Summary Report For General Conditions_
For 07/01/2021 through 12/31/2021
Terms &Conditions
Was Deviation
Permit Records a non- Method(s) of
Condition Condition Summary Deviations? Maintained? compliance Determining Comments
Number (Yes/No) (Yes/No/NA) issue?
Compliance Status
(Yes/No)
Review on a regular basis Modification of permitted
IA General Provisions Yes Yes Yes all changes made to the installation that is not
process that may affect consistant with terms of
permit conditions. permit.
Air Quality Permit
3.6 Permit available at facility No Yes No permit available at facility 09006T07 issued and on
site
2020 Annual Compliance
Report submitted to DAQ
Submissions of reports to regional
reports submitted to per requirements
3.D office and Stationary Source No Yes No
Compliance Office (COMS Only) regional office
Calendar Year 2021 Permit#:09006T07
Page 1 of 3 Jul-Dec Report Facility ID#: 1900104
Per compliance summary
report 1-1-21 thru 06-30
21: Crushing and
Screening opertions M
screen No. 1, No. 2, No.
3 blocked off from
associated baghouse
CD132 and M Screen No.
Review on a regular basis 4, 6 blanked off from
3.F Circumvention Yes NA Yes all changes made to the associated baghouse
process that may affect CDB4.
permit conditions.
Formal disclosure made
in Nov. 2021. Exhaust
flow to screening
baghouse No.1 and No.2
re-established
12/28/2021.
3.G Permit modifications No Yes No records maintained
3.H Changes Not Requiring Permit No Yes No No modifications needed NA
Modifications
Reporting requirements for excess No Excess Emissions or
3.I.A emissions and permit deviations No Yes No records maintained Permit Deviations
3.I.B Other Requirements under 15A NCAC No Yes No records maintained In compliance with
02D.0535 permit
Application for permit
3.K Permit renewal every 5 years No Yes No records maintained renewal submitted to NC
DEQ on 06/01/2020.
3.M Duty to submit any information No Yes No copies maintained and filed No request for any
requested by director information.
Follow up regarding
differential pressure
excursions disclosed
during semi-annual
Review of all reports and deviation report
3.N Duty to Supplement No Yes No data submitted for submitted 7/30/21 for
accuracy. 1/1/2021 through
6/30/2021 provided in
cover letter of this
submittal.
3.0 Retention of records No Yes No maintained in
Calendar Year 202'l documentation room
Page 2 of 3 Jul-Dec Report Facility ID#: 1900104
Annual Compliance
3.P Annual compliance certification No Yes No filing of annual compliance certification for 2020
certification submitted on 2/24/2021
3.Q Certification by responsible official No Yes No proper signature and
records certification
3.T Insignificant activities records No Yes No records in documentation
available at facility room
_ 3.V Inspection and Entry No Yes No N/A No known issues.
3.W Annual fee payment No Yes No receipt on file
2020 AEI sumbitted via
3.X Annual emissions inventory No Yes No inventory in file AERO on 6/29/2021 and
requirement backup data mailed the
same day.
3.Y Confidential Information No Yes No Nothing submitted
32 Construction and operation permits No Yes No permits on file
3.AA Standard Application Form and No Yes No records maintained
Required Information _
3.CC Refrigerant requirements No Yes No records maintained in
document room
The facility does not exceed
Prevention of accidental releases -
the thresholds of
3.DD Section 112® No Yes No substances that would
trigger filing a Section
112@ plan
Prevention of accidental releases - Facility takes steps to
3.EE "General Duty Clause" Section No Yes No manage any hazardous
1129(L) substances
3.II Ambient Air Quality Standards No Yes No NA
Emission testing and reporting testing results are on file in
3'J� requirements No Yes No documentation room
Reporting requirements for non-
3.LL No Yes No records on file
operating equipment
3.NN S ecific Permit Modifications No Yes No Irecords on file
3.00 Third Review fo
Party Participation and EPA Noj Ir
Yes No o modifications applied
Calendar Year 2021 Permit#: 09006T07
Page 3 of 3 Jul-Dec Report Facility ID#: 1900104
North Carolina Depar anent of Environmental and Natural Resources
Division of Air Quality
Deviation Summary Report
For 7/01/2021 through 12/31/2021
Source or Control
Emission Source Permit Condition Deviation Deviation Suspected Cause Corrective Action
Description Device ID Number Pollutant Deviation Description pates Du.atkm Of Deviation Taken
Number(s)
M screen No. CDB2&CDB4 3.A General Provisions PM Ductwork passthrough a 2019 approx. Holes created in Initial disclosure
du 1,3,4,5,6 process bin(ES340A& Novemberctwork by abrasive included in semi-annual
ES340-B),abrasive 2017- material causing deviation report
material from bin has 12/28/2021 material from submitted 7/30/21 for 1
caused holes in process bin to 1-21 thru 6/30/21.
ductwork.Ductwork has contaminate product Formal disclosure made
be sealed off from downstream. in Nov.2021.Control re-
process to prevent Ductwork was established 12/28/2021.
product contamination. disconnected from M
Fugitive emissions from Screens and blanked
source is contained in the off to prevent
building. product
contamination.
M screen No. CDB1&CDB4 3.F Circumvention PM Ductwork to CDBI& 2019 approx. Holes created in Initial disclosure
1,3,4,5,6 CDB4 sealed off from November ductwork by abrasive included in semi-annual
process to prevent 2017- material causing deviation report
product contamination. 12/28/2021 material from submitted 7130/21 for 1-
Fugitive emissions from process bin to 1-21 thru 6/30/21.
source is contained in the contaminate product Formal disclosure made
building. downstream. in Nov.2021.Control re
Ductwork was established 12/28/2021.
disconnected from M
Screens and blanked
off to prevent
product
contamination.
Calender Year 2019 Permit#:09006T06
Page 1 of 1 Jul-Dec Report Location ID#:1900104
SUMMARY REPORT - GASEOUS AND OPACITY EXCESS EMISSION
AND MONITORING SYSTEM PERFORMANCE
Pollutant(Circle One): S02 NOx TRS H2S CO Opacity
Reporting Period Dates: From: 7/1/2021 To: 9/30/2021
Company Name: 3M Company- Pittsboro IMP Division (Facility No.: 1900104)
AFS Number: 09006T04
Emissions Limitation: 10% Opacity
Monitor Manufacturer: Land 4500 Mkll
Date of Last CMS Certification or
Audit: 9/24/21
Process Unit Description: C&S: Gas Fired Dryer(Emissions Source ID No.: ES1415)
(Control Device ID No(s): CDC1 and CDB3)
Total Source Operating Time In
Reporting Period: 105,600 minutes
EMISSIONS DATA SUMMARY' CMS PERFORMANCE SUMMARY"
1. Reason for Excess Emissions: 1. Reason for CEM Downtime:
a.Startup/Shutdown: 0 min. a.Monitor Equipment Malfunction: 0 min.
b.Control Equipment Problem: 0 min. b.Non-Monitor Equipment Malfunction: 0 min.
c.Process Problems 0 min. c.Quality Assurance Calibration: 552 min.
d.Other Known Problem: 0 min. d.Other Known Causes: 0 min.(1)
e.Unknown Problems: 0 min. e.Unknown Causes: 510 min.
2. Total Excess Emissions 0 min. 2. Total CMS Downtime: 1,062 min.
3. Total Excess Emissions x(100)= 0.00% 3. Total CMS Downtime x(100)= 1.01%
Total Source Operation Time Total Source Operating Time
On a separate page,describe any changes asince the last reporting period in CMS,process,or controls.
I certify that the information in this report is true,accurate,and complete.
Name: Mr. Blake Arnett
Title: Plant Direct r
Signature:
6604
"FOR OPACITY,RECORD ALL TIMES IN MINUTES.FOR GASES,RECORD ALL TIMES IN HOURS
Notes:
(1)The time listed under"Other Known Causes"is actual time for Third Party Quarterly Calibration and Audit.
SUMMARY REPORT - GASEOUS AND OPACITY EXCESS EMISSION
AND MONITORING SYSTEM PERFORMANCE
Pollutant(Circle One): S02 NOx TRS H2S CO Opacity
Reporting Period Dates: From: 7/1/2021 To: 9/30/2021
Company Name: 3M Company- Pittsboro IMP Division (Facility No.: 1900104)
AFS Number: 09006T04
Emissions Limitation: 10% Opacity
Monitor Manufacturer: Land 4500 Mkll
Date of Last CMS Certification or
Audit: 9/24/21
Process Unit Description: Natural gas-fired dryer, line 1 (Emission Source ID No.: ESCPPH1)
(Control Device ID No.: CDB9)
Total Source Operating Time In
Reporting Period': 60,360 minutes
EMISSIONS DATA SUMMARY CMS PERFORMANCE SUMMARY
1. Reason for Excess Emissions: 1. Reason for CEM Downtime:
a.Startup!Shutdown: 0 min. a.Monitor Equipment Malfunction: 0 min.
b.Control Equipment Problem: 0 min. b.Non-Monitor Equipment Malfunction: 0 min.
c.Process Problems 0 min. c.Quality Assurance Calibration: 552 min.
d.Other Known Problem: 0 min. d.Other Known Causes: 30 min.(1)
e.Unknown Problems: 0 min. e.Unknown Causes: 1,914 min.
2. Total Excess Emissions 0 min. 2. Total CMS Downtime: 2,496 min.
3. Total Excess Emissions x(100)= 0.00% 3. Total CMS Downtime x(100)= 4.14%
Total Source Operation Time Total Source Operating Time
On a separate page,describe any changes asince the last reporting period in CMS,process,or controls.
I certify that the information in this report is true,accurate,and complete.
Name: Mr. Blake Arnett
Title: Plant Director '
0
Signature:
FOR OPACITY,RECORD ALL TIMES IN MINUTES.FOR GASES,RECORD ALL TIMES IN HOURS
Notes:
(1)The time listed under"Other Known Causes"is actual time for Third Party Quarterly Calibration and Audit.
SUMMARY REPORT - GASEOUS AND OPACITY EXCESS EMISSION
AND MONITORING SYSTEM PERFORMANCE
Pollutant(Circle One): S02 NOx TRS H2S CO Opacity
Reporting Period Dates: From: 7/1/2021 To: 9/30/2021
Company Name: 3M Company-Pittsboro IMP Division(Facility No.: 1900104)
AFS Number: 09006T04
Emissions Limitation: 10%Opacity
Monitor Manufacturer: Land 4500 Mkl I
Date of Last CMS Certification or
Audit: 9/24/21
Process Unit Description: Natural Gas Fired Dryer, line 2(Emission Source ID No. ESCPPH2)
(Control Device ID No.: CDB10)
Total Source Operating Time In
Reporting Period*: 59,460 minutes
EMISSIONS DATA SUMMARY CMS PERFORMANCE SUMMARY
1. Reason for Excess Emissions: 1. Reason for CEM Downtime:
a.Startup/Shutdown: 0 min. a.Monitor Equipment Malfunction: 0 min.
b.Control Equipment Problem: 0 min. b.Non-Monitor Equipment Malfunction: 0 min.
c.Process Problems 0 min. c.Quality Assurance Calibration: 552 min.
d.Other Known Problem: 0 min. d.Other Known Causes: 0 min.(1)
e.Unknown Problems: 0 min. e.Unknown Causes: 1,848 min.
2. Total Excess Emissions 0 min. 2. Total CMS Downtime: 2,400 min.
3. Total Excess Emissions x(100)= 0.00% 3. Total CMS Downtime x(100)= 4.04%
Total Source Operation Time Total Source Operating Time
On a separate page,describe any changes asince the last reporting period in CMS,process,or controls.
I certify that the information in this report is true,accurate,and complete.
Name: Mr. Blake Arnett
Title: Plant Director
Signature:
*FOR OPACITY,RECORD Al. TIMES IN MINUTES.FOR GASES,RECORD ALL TIMES IN HOURS
Notes:
(1)The time listed under"Other Known Causes"is actual time for Third Party Quarterly Calibration and Audit.
SUMMARY REPORT - GASEOUS AND OPACITY EXCESS EMISSION
AND MONITORING SYSTEM PERFORMANCE
Pollutant(Circle One): S02 NOx TRS H2S CO Opacity
Reporting Period Dates: From: 10/1/2021 To: 12/31/2021
Company Name: 3M Company- Pittsboro IMP Division (Facility No.: 1900104)
AFS Number: 09006T04
Emissions Limitation: 10% Opacity
Monitor Manufacturer: Land 4500 Mkll
Date of Last CMS Certification or
Audit: 12/16/21
Process Unit Description: C&S: Gas Fired Dryer(Emissions Source ID No.: ES1415)
(Control Device ID No(s): CDC1 and CDB3)
Total Source Operating Time In
Reporting Period*: 91,080 minutes
EMISSIONS DATA SUMMARY* CMS PERFORMANCE SUMMARY*
1. Reason for Excess Emissions: 1. Reason for CEM Downtime:
a.Startup/Shutdown: 0 min. a.Monitor Equipment Malfunction: 0 min.
b.Control Equipment Problem: 0 min. b. Non-Monitor Equipment Malfunction: 0 min.
c. Process Problems 0 min. c.Quality Assurance Calibration: 552 min.
d.Other Known Problem: 0 min. d.Other Known Causes: 217 min. (1)
e. Unknown Problems: 0 min, e. Unknown Causes: 0 min.
2. Total Excess Emissions 0 min. 2. Total CMS Downtime: 769 min.
3. Total Excess Emissions x(100)= 0.00% 3. Total CMS Downtime x(100)= 0.84%
Total Source Operation Time Total Source Operating Time
On a separate page,describe any changes since the last reporting period in CMS,process,or controls.
I certify that the information in this report is true,accurate,and complete.
Name: Mr. Blake Arnett
Title: Plant Director
Signature: /";19�11 �
*FOR OPACITY, RECORD ALL TIMES IN MINUTES. FOR GASES,RECORD ALL TIMES IN HOURS
Notes:
(1)Third Party Quarterly Calibration and Audit were performed when the plant was shut down.
SUMMARY REPORT - GASEOUS AND OPACITY EXCESS EMISSION
AND MONITORING SYSTEM PERFORMANCE
Pollutant(Circle One): S02 NOx TRS H2S CO Opacity
Reporting Period Dates: From: 10/1/2021 To: 12/31/2021
Company Name: 3M Company- Pittsboro IMP Division (Facility No.: 1900104)
AFS Number: 09006T04
Emissions Limitation: 10% Opacity
Monitor Manufacturer: Land 4500 Mkll
Date of Last CMS Certification or
Audit: 12/16/21
Process Unit Description: Natural gas-fired dryer, line 1 (Emission Source ID No.: ESCPPH1)
(Control Device ID No.: CDB9)
Total Source Operating Time In
Reporting Period*: 56,220 minutes
EMISSIONS DATA SUMMARY CMS PERFORMANCE SUMMARY
1. Reason for Excess Emissions: 1. Reason for CEM Downtime:
a.Startup/Shutdown: 0 min. a.Monitor Equipment Malfunction: 0 min.
b.Control Equipment Problem: 0 min. b.Non-Monitor Equipment Malfunction: 0 min.
c.Process Problems 0 min. c.Quality Assurance Calibration: 552 min.(2)
d.Other Known Problem: 0 min. d.Other Known Causes: 0 min.(1)
e.Unknown Problems: 0 min. e.Unknown Causes: 0 min.
2. Total Excess Emissions 0 min. 2. Total CMS Downtime: 552 min.
3. Total Excess Emissions x(100)= 0.00% 3. Total CMS Downtime x(100)= 0.98%
Total Source Operation Time Total Source Operating Time
On a separate page,describe any changes since the last reporting period in CMS,process,or controls.
I certify that the information in this report is true,accurate,and complete.
Name: Mr. Blake Arnett
Title: Plant Director
Signature: //40
*FOR OPACITY,RECORD ALL IMES IN MINUTES.FOR GASES,RECORD ALL TIMES IN HOURS
Notes:
(1)Third Party Quarterly Calibration and Audit were performed when the plant was shut down.
(2)10/28/20 Opacity Monitor missed scheduled daily calibration due to a power outage.The unit calibrated on
start-up and 1212 minutes of data were revalidated.
SUMMARY REPORT -GASEOUS AND OPACITY EXCESS EMISSION
AND MONITORING SYSTEM PERFORMANCE
Pollutant(Circle One): S02 NOx TRS H2S CO Opacity
Reporting Period Dates: From: 10/1/2021 To: 12/31/2021
Company Name: 3M Company-Pittsboro IMP Division (Facility No.: 1900104)
AFS Number: 09006T04
Emissions Limitation: 10%Opacity
Monitor Manufacturer: Land 4500 Mkll
Date of Last CMS Certification or
Audit: 12/16/21
Process Unit Description: Natural Gas Fired Dryer, line 2(Emission Source ID No. ESCPPH2)
(Control Device ID No.: CDB10)
Total Source Operating Time In
Reporting Period`: 50,220 minutes
EMISSIONS DATA SUMMARY CMS PERFORMANCE SUMMARY
1. Reason for Excess Emissions: 1. Reason for CEM Downtime:
a.Startup/Shutdown: 0 min. a.Monitor Equipment Malfunction: 0 min.
b.Control Equipment Problem: 0 min. b.Non-Monitor Equipment Malfunction: 0 min.
c.Process Problems 0 min. c.Quality Assurance Calibration: 552 min.
d.Other Known Problem: 0 min. d.Other Known Causes: 246 min.(1)
e.Unknown Problems: 0 min. e.Unknown Causes: 0 min.
2. Total Excess Emissions 0 min. 2. Total CMS Downtime: 798 min.
3. Total Excess Emissions x(100)= 0.00% 3. Total CMS Downtime x(100)= 1.59%
Total Source Operation Time Total Source Operating Time
On a separate page,describe any changes since the last reporting period in CMS,process,or controls.
I certify that the information in this report is true,accurate,and complete.
Name: Mr. Blake Arnett
Title: Plant Director.
Signature:
•FOR OPACITY,RECORD AA ES ES IN MINUTES.FOR GASES,RECORD ALL TIMES IN HOURS
Notes:
(1)Third Party Quarterly Calibration and Audit were performed when the plant was shut down.
TEC HN OC Ask ms
TM
Maintenance Records
and
Quality Assurance Test Results
Quarter 3 - 2021
for
OPACITY COMS
4191 NC 87 South
Moncure, NC 27559
by
TechnoCEMS
11139 Ragsdale Ct
New Port Richey, FL 34654
John Tsouris, Senior CEM Specialist
v
Table Of Contents
Page
1. Summary
2. Line 1 - Opacity Calibration Test Audit Results
6. Line 2 - Opacity Calibration Test Audit Results
10. Dryer - Opacity Calibration Test Audit Results
14. Optical Filter Certification Report
19. Maintenance Checklists
24. Appendix A - Opacity Formulas
I
Adak
During calendar Quarter 3 (Q3) 2021 , TechnoCEMS
personnel performed the required preventive maintenance
and quality assurance testing on the 3M Corp Continuous
Opacity Monitoring systems. The opacity monitor
maintenance activities and calibration filter audits were
performed in accordance with the regulatory and company
guidelines provided by 3M Corporation intended to meet the
Quality Assurance Requirements of 40 CFR 60 Appendix F,
Procedure 3. The results of this testing and a record of the
maintenance activities are included herein.
Page 1
Opacity Calibration Audit Results
Page 2
Calibration Audit . ea
AirVision Wonderware
Parameter - Opacity LOW: 0.1 0.2
MID: 0.1 0.0
HIGH: 0.1 0.1
ASS Pass/Fail: <3% Error
See appendices for test formula
Parameter - Zero Compensation Compensation at
Time of Audit:
Equivalent Opacity: 0.00%
ASS Pass/Fail: <4%Opacity
See appendices for test formula
Parameter - Optical Alignment
ASS
Pass/Fail: Indicator inside 2nd ring-
Defined by manufacturer as point at
which opacity reading changes 2%.
Page 3
CALIBRATION ERROR DETERMINATION - PREHEATER LINE 1
TESTER John Tsouris-TechnoCEMS Manufacturer LAND Combustion
COMPANY 3M Model 4500Mk3 Serial# 227691 72
LOCATION Pittsboro, NC
SOURCE Line 1
DATE September 24, 2021 Filter Value Corrected Required
Range
Filter 1 Value 15.5% 9.8% 1 5%-10%
Last Off-Stack Calibration(3 Year-calendar) 6/24/2020 Filter 2 Value 26.4% 17.1% 10%-20%
Cross-stack target within spec? YES Cross Stack Target Filter 3 Value 47.9% 32.9% 20%-40%
Off-stack zero as-found(2%max): 0.8% 10/o
o
(/
Off-stack zero post service: 0.0% Opacity Limit(+, / OPLR 0,305
Last cal-kit Calibration 9/24/21 Taper Ratio(2 X OPLR) 0.611
Cross-stack target within spec? YES Dirt Compensation During Cal Audit 0.00 (4%max)
Cal-kit zero as-found(2%max): 0.3% Cross-stack target within spec? YES
Cal-kit zero post service: 0.0%
Corrected ARITHMETIC DIFFERENCE
Target AIrVISIon Wonderware Wonderware Wonderware AirVision Wonderware AiMsion Filter Wondenvare
Run# Value Response Response AlMsion Zero Zero AirVislon Filter 1 Filter 1 Filler 2 Filter 2 3 Filter 3
Zero At Start 0.0 0.1 0.0 0.1 0.0 -------- -------- -------- -------- -------- --------
9.8 9.9 9.8 -------- -------- 0.1 0.0 -------- -------- -------- --------
Drop 1 17.1 17.2 17.1 -------- -------- -------- -------- 0.1 0.0 -------- --------
32.9 32.8 32.8 -------- -------- -------- -------- -------- -------- -0.1 -0.1
9.8 9.9 9.8 -------- -------- 0.1 0.0 -------- -------- -------- --------
Drop 2 17.1 17.2 17.1 -------- -------- -------- -------- 0.1 0.0 -------- --------
32.9 32.8 32.8 -------- -------- -------- -------- -------- -------- -0.1 -0.1
9.8 9.9 9.9 -------- -------- 0.1 0.1 -------- -------- -------- --------
Drop 3 17.1 17.2 17.1 -------- -------- -------- -------- 0.1 0.0 -------- --------
32.9 32.8 32.8 -------- -------- -------- -------- -------- -------- -0.1 -0.1
Zero At End 0.0 0.1 0.0 0.1 0.0 -------- -------- -------- -------- -------- --------
Arithmetic Mean X 0.100 0.000 0.100 0.033 0.100 0.000 j -0.100 -0.100
Confidence Coefficient CC -------- -------- 0.000 0.143 0.000 0,000 0.000 0.000
Calibration Error 1XI+ICCI -------- -------- 0.100 0.176 0.100 0.000 0,100 0.100
Calibration Error-Rounded 0.1 0.0 0.1 0.2 0.1 0.0 0.1 0.1
Pass=<1.0%-All Pass=<3.0%Error
Page 4
OpacityData Printout
te/Ti Line 1 -AirVision Line 1 - Date/Time Line 1 -AirVision Line 1 -Wonderware
OPACITY Value Wonderware OPACITY Value OPACITY Value
9/24/2112:10 0.1 0.0 9/24/2112:42 28.3 28.3
9/24/211211 8.4 8.4 9/24/2112:43 0.1 0.0
9/24/2112:12 9.9 9.8
9/24/2112:13 9.9 9.8
9/24/21 12:14 10.3 10.3
9/24/21 12.15 17.2 17.1
9/24/21 12:16 17.2 17.1
9/24/21 12:17 17.1 17.1
9/24/2112.18 29.7 29.7
9/24/2112:19 32.8 32.8
9/24/2112:20 32.8 32.8
9/24/2112.21 32.8 32.8
9/24/2112:22 32.8 32.8
9/24/21 12:2 3 14.4 14.1
9/24/2112:24 9.9 9.8
9/24/2112:25 9.9 9.9
9/24/21 12:26 14.2 14.2
9/24/21 12:27 17.2 17.1
9/24/21 12:2 8 17.2 17.1
9/24/2112:29 20.0 20.0
9/24/2112:30 32.8 32.8
9/24/2112:31 32.8 32.8
9/24/2112:32 29.6 29.6
9/24/2112:33 9.9 9.9
9/24/2112:34 9.9 9.9
9/24/21 12:35 10.6 10.5
9/24/21 12:36 17.2 17.1
9/24/21 12:37 17.2 17.1 Key
9/24/21 12:38 17.4 17.4 Zero
9/24/2112:39 32.8 32.8 Low
9/24/2112:40 32.8 32.8 Mid
9/24/2112:41 32.8 32.8 High
Page 5
Opacity Calibration Audit Results
LINE 2
Page 6
Calibration Audit Summary
AirVision Wonderware
Parameter - Opacity Low: 0.1 0.1
MID: 0.1 0.1
HIGH: 0.1 0.1
ASS Pass/Fail: < 3% Error
See appendices for test formula
Parameter - Zero Compensation Compensation at
Time of Audit:
Equivalent Opacity: 0.00%
ASS Pass/Fail: <4%Opacity
See appendices for test formula
Parameter - Optical Alignment
ASS
Pass/Fail: Indicator inside 2nd ring-
Defined by manufacturer as point at
which opacity reading changes 2%.
Page 7
CALIBRATION ERROR DETERMINATION - PREHEATER LINE 2
TESTER John Tsouris-TechnoCEMS Manufacturer LAND Combustion
COMPANY 3M Model 4500Mk3 Serial# 227480 72
LOCATION Pittsboro, NC
SOURCE Line 2
Filter Value Corrected Required
DATE September 24, 2021 Range
Filter 1 Value 15.5% 9.8% 5%-10%
Last Off-Stack Calibration(3 Year-calendar) 6/24/2020 Filter 2 Value 26.4% 17.1% 10%-20%
Cross-stack target within spec? YES Cross Stack Target Filter 3 Value 47.9% 32.9% 20%-40%
Off-stack zero as-found(2%max): 0.0% r-� Opacity Limit 10%
Off stack zero post service: 0.0% (^\ OPLR 0.305
Last cal-kit Calibration 9/24/21 �J Taper Ratio(2 X OPLR) 0.611
Cross-stack target within spec? YES Dirt Compensation During Cal Audit 0.00 (4%max)
Cal-kit zero as-found(2%max): 0.0% Cross-stack target within spec? YES
Cal-kit zero post service: 0.0%
Corrected ARITHMETIC DIFFERENCE
Target AirVision Wonderware Wonderware AiNtsion Filter Wonderware AirVision Wonderware AirVision Filter Wonderware
Run# Value Response Response AirVmjon Zero Zero 1 Filter 1 Filter 2 Flitter 2 3 Filter 3
Zero At Start 0.0 0.0 0.0 0.0 0.0 -------- -------- -------- -------- -------- --------
1 1
9.8 9.9 9.9 -------- -------- 0.1 0.1 -------- -------- -------- --------
Drop 1 17.1 17.2 17.2 -------- -------- -------- -------- 0.1 0.1 -------- --------
32.9 33.0 33.0 -------- -------- -------- -------- -------- -------- 0.1 0.1
9.8 9.9 9.9 -------- -------- 0.1 0.1 -------- -------- -------- --------
Drop 2 17.1 17.2 17.2 -------- -------- -------- -------- 0.1 0.1 -------- --------
32.9 33.0 33.0 -------- -------- -------- -------- -------- -------- 0.1 0.1
9.8 9.9 9.9 -------- -------- 0.1 0.1 -------- -------- -------- --------
Drop 3 17.1 17.2 17.2 -------- -------- -------- -------- 0.1 0.1 -------- --------
32.9 33.0 33.0 -------- -------- -------- -------- -------- -------- 0.1 0.1
Zero At End 0.0 0.1 0.1 0.1 0.1 -------- -------- -------- -------- -------- --------
Arithmetic Mean X 0.050 0.050 0.100 0.100 0.100 0.100 0.100 0.100
Confidence Coefficient CC --- -------- 0.000 0.000 0.000 0.000 0.000 0.000
Calibration Error 1XI+ICCI ------- -------- 0.100 0.100 0.100 0.100 0.100 0.100
Calibration Error-Rounded 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1
Pass=<1.0%-All Pass=<3.0°%Error
Page 8
Opacity Data Printout - Preheater Line 2
DateJTime Line 2-AirVision Line 2- Date/Time Line 2-AirVision Line 2-Wonderware
OPACITY Value Wonderware OPACITY Value OPACITY Value
9/24/2112:07 0.0 0.0 9/24/2112:39 0.1 0.1
9/24/2112:08 8.0 8.0
9/24/2112:09 9.9 9.9
9/24/21 12:10 11.0 11.0
9/24/21 12:11 17.2 17.2
9/24/21 12:12 17.2 17.2
9/24/21 12:13 17.2 17.2
9/24/2112:14 24.8 24.7
9/24/2112:15 33.0 33.0
9/24/2112:16 33.0 33.0
9/24/2112:17 28.8 28.7
9/24/2112:18 9.9 9.9
9/24/2112:19 9.9 9.9
9/24/2112:20 9.9 9.9
9/24/2112:21 9.9 9.9
9/24/21 12:22 10.3 10.4
9/24/21 12:2 3 17.2 17.2
9/24/21 12:24 17.2 17.2
9/24/21 12:2 5 17.2 17.2
9/24/2112:26 32.2 32.3
9/24/2112:27 33.0 33.0
9/24/2112:28 33.0 33.0
9/24/2112:29 20.1 20.2
9/24/2112:30 9.9 9.9
9/24/2112:31 9.9 9.9
9/24/21 12:32 13.2 13.2
9/24/21 12:33 17.2 17.2
9/24/21 12:34 17.2 17.2 Key
9/24/2112:35 22.8 22.7 Zero
9/24/2112:36 33.0 33.0 Low
9/24/2112:37 33.0 33.0 Mid
9/24/2112:38 20.4 20.8 High
Page 9
Opacity Calibration Audit Results
COMMON - DRYER
Page 10
Calibration Audit
AirVision Wonderware
Parameter - Opacity LOW: 0.4 0.4
MID: 0.4 0.4
HIGH: 0.2 0.2
ASS Pass/Fail: <3% Error
See appendices for test formula
Parameter - Zero Compensation Compensation at
Time of Audit:
Equivalent Opacity: 0.00%
ASS Pass/Fail: <4%Opacity
See appendices for test formula
Parameter - Optical Alignment
of
ASS
Pass/Fail: Indicator inside 2nd ring-
Defined by manufacturer as point at
which opacity reading changes 2%.
Page 11
CALIBRATION ERROR DETERMINATION - COMMON - DRYER
TESTER John Tsouris-TechnoCEMS Manufacturer LAND Combustion
COMPANY 3M Model 4500Mk3 Serial# 227696 72
LOCATION Pittsboro, NC
SOURCE Common
DATE September 24, 2021 Filter Value Corrected Required
Range
Filter 1 Value 15.5% 7.4% 5%-10%
Last Off-Stack Calibration(3 Year-calendar) 6/24/2020 Filter 2 Value 26.4% 13.1% 10%-20%
Cross-stack target within spec? YES Cross Stack Target Filter 3 Value 47.9% 25.9% 20%-40%
Off-stack zero as-found(2%max): -0.2% Opacity Limit 10%
Off-stack zero post service: 0.0% OPLR 0.230
Last cal-kit Calibration 9/24/21
Taper Ratio(2 X OPLR) 0.460
Cross-stack target within spec? YES Dirt Compensation During Cal Audit 0.00 (4%max)
Cal-kit zero as-found(2%max): 0.3% Cross-stack target within spec? YES
Cal-kit zero post service: 0.0%
Corrected ARITHMETIC DIFFERENCE
Target AIrVision Wonderware Wonderware AirVision Wonderware AirVlsion Wonde"re AirVision Filter Wonderware
Run# Value Response Response AirVision Zero Zero Filter 1 Fitter 1 Filter 2 Filter 3 Filter 3
Zero At Start 0.0 0.1 0.1 0.1 0.1 -------- -------- -------- -------- ------- --------
7.4 7.6 7.6 -------- -------- 0.2 0.2 -------- -------- -------- --------
Drop 1 13.1 13.3 13.3 -------- -------- -------- -------- 0.2 0.2 -------- --------
25.9 26.1 26.1 ------- -------- -------- -------- -------- -------- 0.2 0.2
7.4 7.6 7.6 -------- -------- 0.2 0.2 -------- -------- -------- --------
Drop 2 13.1 13.3 13.3 -------- -------- -------- -------- 0.2 0.2 -------- --------
25.9 26.1 26.1 -------- -------- -------- -------- -------- -------- 0.2 0.2
7.4 7.7 7.7 -------- -------- 0.3 0.3 -------- -------- -------- --------
Drop 3 13.1 13.4 13.4 -------- -------- -------- -------- 0.3 0.3 -------- --------
25.9 26.1 26.1 -------- -------- -------- -------- -------- -------- 0.2 0.2
Zero At End 0.0 0.1 0.1 0.1 0.1 ------- -------- -------- -------- -------- --------
Arithmetic Mean X 0.100 0.100 0.233 0.233 0.233 0.233 0.200 0.200
Confidence Coefficient CC -- -------- 0.143 0.143 0.143 0.143 0.000 0.000
Calibration Error 1XI+ICCI -------- -------- 0.376 0.376 0.376 0.376 0.200 0.200
Calibration Error-Rounded 0.1 0.1 0.4 0.4 0.4 0A 0.2 0.2
Pass=<1.0%-All Pass=<3.0%Error
Page 12
Opacity Data • Common - Dryer
Common-AirVision Common- Common-AirVision Common-
Date/Time OPACITY Value Wonderware Date/Time OPACITY Value Wonderware
OPACITY Value OPACITY Value
9/24/2113:37 0.1 0.1
9/24/21 13:38 1.6 1.5
9/24/211339 7.6 7.6
9/24/2113:40 7.6 7.6
9/24/21 13:41 9.7 9.5
9/24/21 13:42 13.3 13.3
9/24/21 1143 13.3 13.3
9/24/211144 24.1 23.9
9/24/2113:45 26.1 26.1
9/24/2113:46 20.4 21.2
9/24/2113:47 7.6 7.6
9/24/2113:48 7.6 7.7
9/24/2113:49 7.6 7.6
9/24/2113:50 7.6 7.7
9/24/21 13:51 11.4 11.2
9/24/21 13:52 13.3 13,3
9/24/21 1153 14.8 14.4
9/24/2113:54 26.1 26.1
9/24/2113:55 26.1 26.1
9/24/2113:56 19.2 20.1
9/24/211157 7.7 7.7
9/24/2113:58 7.7 7.7
9/24/21 13:59 12.1 12.0
9/24/21 14:00 13.4 13.4
9/24/21 14:01 17.3 17.2
9/24/2114:02 26.1 26.1
9/24/2114:03 26.1 26.1
9/24/21 14:04 10.2 10.9 Key
9/24/2114:05 0.4 0.6 Zero
9/24/2114:06 0.1 0.1 Low
Mid
High
Page 13
Optical Filter CertificationReport
Page 14
Opacity Certification Services, LLC 8600 Harbor Drive
Raleigh,Nnrth Carolina 27615
A Proud Veteran-Owned Business Phone 919.215.9384
Fax 919.946.6041
Web:www.oDacitvicert.com
Results of NIST-Traceable Opacity Filter
(Audit Attenuators) Certification
Customer: I 3M Pittsboro
Date of Certification: Ma 26 2021
Date of Expiration: May 25,2022 Document Number: USZ6Z1-U3
This data is generaled for the following Opacity Monitor and may not apply to other monitors.
Opacity Monitor Make/Model: AMETEK-Land 4500 Mk III series
Monitor Light Source: L.E.D. Specific L.E.D.Peak Spectral Response: 520am
Optical
Opacity @ Transmittance Density Previous opacity( Opacity Ca)Serial No: PLCF= @ PLCF—1.000 @PLCF— Opacity a Opacity PLCF= PLCF=
1.000 1000 0.6100 0.4600
B14B 15.52% 84.48% 0.0732 15.77% -0.25 9.78% 7.46%
Y27A 1 26.36% 73.64% 1 0.1329 26.58% 1 -0.22 1 17.02% 1 13.13%
Y28A 47.86% 52.14% 0.2829 47.88% -0.02 32.79% 25.89%
Spectrophotometer Information
Make/Model:A ilent Cary 60 UV-Via I Serial Number:MY20179221
Maximum Accuracy:f 0.250 Absolute Opacity Laboratory Temperature:72°F t 3°/22°C t 1°
NIST Standard Reference Material SRM Information
SRM Type:NIST 2031b series I Serial Number Blank;709-10;772-30.709-90
SRM Date of Certification:29 April 2021 1 SRM Date of Expiration:30 April 2023
Signature of Spectrophotometer Operator
Al Siffer
I'ago I'i
Opacity Certification Services, LLC 8600 Harbor Drive
Raleigh,North Carolina 27615
A Proud Veteran-Owned Business Phone 919.215.9384
Fax 919.846.6041
Web:www.ot)acitvicert.com
Customer: 3M Pittsboro
Date of Certification: 26-Ma -2021
Recertification Due: 25-May-2022 Serial No
Monitor: Land 4500 Mk III B14B
A Scan Data Weighting Weighted Opacity(%)
(L.E.D. Scan 1 Scan 2 Ave. Factors Transmittance 15.52
Specific)
570 84.487 84.476 84.482 5 422.41 0.011
560 84.561 84.568 84.565 50 4228.23 0.007 Transmission(%)
550 84.610 84.619 84.615 210 17769.05 0.009 84.48
540 84.645 84.660 84.653 890 75340.73 0.015
530 M.585 84.579 84.582 1850 156476.70 0.006
520 84.504 84.492 84.498 3990 337147.02 0.012
510 84.415 84.402 84.409 1850 156155.73 0.013 Optical Density:
500 84.238 84.232 84.235 890 74969.15 0.006 O.O 2
490 84.135 84.130 84.133 210 17667.83 0.005
480 84.183 84.169 84.176 50 4208.80 0.014
470 84.211 84.194 84.203 5 421.01 0.017 Previous Opacity(%
Sum 10000 844806.64 Sum 1
84.48 5.77
PLCF's 0.6100 0.4600 Change in Opacity
Correcte 9.78 7.46 -0.25
Opacity
90.000
80.000
70.000
60.000
a
50.000
40.000
r=
30.000
20.000
10.000
0.000 •
570 S60 550 540 530 S20 S10 S00 490 480 470
Wavelength
Page 16
Opacity Certification Services, LLC 8600 Harbor Drive
Raleigh,North Carolina 27615
A Proud Veteran-Owned Business Phone 919.215.9384
Fax 919.846.6041
Web:www.oi)acitvicert.com
Customer: 3M Pittsboro
Date of Certification: 26-Ma -2021
Recertification Due: 25-May-2022 Serial No
Monitor: Land 4500 Mk ill I Y27A
A Scan Data Weighting Weighted Opacity(%)
(L.E.13. Scan 1 Scan 2 Ave. Factors Transmittance 26.36
Specific)
570 73.750 73.731 73.741 5 368.70 0.019
560 73.985 74.001 73.993 50 3699.65 0.016 Transmission(%)
550 74,003 74.016 74.010 210 15542.00 0.013 73.64
540 74.051 74.039 74.045 890 65900.05 0.012
530 73.923 73.910 73.917 1850 136745.53 0.013
520 73.683 1 73.682 73.683 3990 293993.18 0.001
510 73.428 73.415 73.422 1850 135829.78 0.013 Optical Density:
500 73.080 73.082 73.081 890 65042.09 0.002 0 1329
490 72.849 72.856 72.853 210 15299.03 0.007
480 72.879 72.867 72.873 50 3643.65 0.012
470 72.946 72.948 72.947 51 364.74 0.002 Previous Opacity(%
Sum 10000 736428.37 Sum 2
73.64 6.58
PLCF's 0.6100 1 0.4600J Change in Opacity
Corrected 17.02 1 13.13 -Q 22
Opacity
somo
70.000
60.000
50.000
E 40.000
a0.000
20.000
10.000
0.000 •
570 560 550 540 530 520 530 500 490 480 470
Wavelength
,Compliant
Page 17
Opacity Certification Services, LLC 8600 Harbor Drive
Raleigh,North Carolina 27615
A Proud Veteran-Owned Business Phone 919.215.9384
Fax 919.846.6041
Web:www.oDacitvicert.com
Customer: 3M Pittsboro
Date of Certification: 26-Ma -2021
Recertification Due: 25-May-2022 Serial No
Monitor: Land 4500 Mk III Y28A
A Scan Data Weighting Weighted Opacity(%)
(L.E.D. Scan 1 Scan 2 Ave. Factors Transmittance 47.86
Specific)
570 51.762 51.768 51.765 5 258.83 0.006
560 52.721 52.729 52.725 50 2636.25 0.008 Transmission(%)
550 53.196 53.206 53.201 210 11172.11 0.009 C . 4
540 53.149 53.150 53.150 890 47303.06 0.001 7 2
530 52.590 52.586 52.588 1850 97287.8U 0.004
520 51.976 51.984 51.980 3990 207400.20 0.008
510 51.667 51.656 51.662 1850 95573.78 0.011 Optical Density:
500 51.623 51.613 51.618 890 45940.02 0.010 0.�O029
490 51.892 51.889 51.891 210 10897.01 0.003
480 52.526 52.512 52.519 50 2625.95 0.014
470 53.224 53.216 53.220 5 266.10 0.008 Previous Opacity(%
Sum 10000 521361.09 Sum A O0
52.14 4 o0
PLCF's 0.6100 0.4600 Change in Opacity
Carrecte4 32.79 25.89 1 -0.02
Opacity
60.000
S0.000
40.000
E 30.000
h
20.000
10.000
0.000
S70 560 $50 540 $30 520 510 Soo 490 480 470
Wavelength
Ne%% and Existing 011,1JIN and 24-48 1 lour Set-%ice PS-1.Procedure 3.Appendix F&
Fage 1B
Maintenance Checklists - Recorded Values
ALL UNITS
Page 19
Quarterly Service Checklist
Client 3M Site Pittsboro, NC Unit# 's 1,2,Common
Instrument Physical
Description F req. Date Performed
lean Instruments Q 9/24/2021
Inspect Instrument Blowers U 9/24/2021
Inspect Blower Tubing 9/24/2021
Blowers
Description req• ate Performed
Change Blower Filters As needed 9/24/2021
Monitor
Description F req. Date Performed
Check for Faults 9/24/2021
Clean Optics 9/24/2021
Check Target Alignments 9/24/2021
Clean Optics/ Reflectors Q 9/24/2021
Calibration Error Determination Q 9/24/2021
1 Off-Stack Calibration 3A 6/24/2020
2 Off-Stack Calibration 3A 6/24/2020
Comm Off-Stack Calibration 3A 6/24/2020
Technician John Tsouris Date 9/24/2021
Page 20
Opacity LAND 4500Mk3 Quarterly Recorded Values
Serial Number: 227691 72 Unit Line 1
Diagnostics Menu
Parameter Description Value Nominal Value
153 W- Dirty Window Correction-Pre Maintenance -0.20% 0%-4%
Cal Kit Cal Kit Reading-Pre Maintenance 0.29% 0%-2%
121 Sm - Signal Measurement 11432 n/a
122 Rm - Reference Measurement 54644 n/a
123 SF - Signal Flood Value 47062 n/a
124 Rf- Reference Flood Value 52166 n/a
125 So- Signal Offset 57 n/a
126 Ro -Reference Offset 100 n/a
127 Calculated Opacity -0.03 n/a
137 PLCF 0.611 0.611
140 C -Calibration Sloe 4.858 —4.7
141 X - Calibration Offset 0.121 —.125
142 B - Calibration Balance Factor 0.904 —1.0
149 W-Dirty Window Correction- Post Maintenance 1.00 n/a
153 Op0 -Zero Compensation 0.00% 0
154 Opz -Cal Check Last Zero 0.00% 0
155 O c- Cal Check Last Upscale 17.28% —17.2%
Cal Kit Cal Kit Reading- Post Maintenance 0.00% 0%-2%
Alarms
All OK OK ON/OFF OFF
Technician John Tsouris Date 9/24/2021
Page 21
Opacity LAND 4500Mk3 Quarterly Recorded Values
Serial Number: 227480 72 Unit Line 2
Diagnostics Menu
Parameter Description Value Nominal Value
153 W-Dirty Window Correction - Pre Maintenance 0.18% 0%-4%
Cal Kit Cal Kit Reading-Pre Maintenance 0.00% 0%-2%
121 Sm - Signal Measurement 12769 n/a
122 Rm - Reference Measurement 54326 n/a
123 SF - Signal Flood Value 48917 n/a
124 Rf- Reference Flood Value 52243 n/a
125 So - Signal Offset 113 n/a
126 Ro -Reference Offset 62 n/a
127 Calculated Opacity 0.01 n/a
137 PLCF 0.611 0.611
140 C -Calibration Slope 4.272 -V4.50
141 X - Calibration Offset 0.106 —.110
142 B - Calibration Balance Factor 0.879 —1.0
149 W-Dirty Window Correction - Post Maintenance 1.00 n/a
153 OpO - Zero Compensation 0.00% 0
154 O z -Cal Check Last Zero 0.00% 0
155 Opc- Cal Check Last Upscale 16.93% —16.5%
Cal Kit Cal Kit Reading - Post Maintenance 0.00% 0%-2%
Alarms
All OK OK ON/OFF OFF
Technician John Tsouris Date 9/24/2021
Page 22
Opacity LAND 4500Mk3 Quarterly Recorded Values
Serial Number: 227696 72 Unit Common
Diagnostics Menu
Parameter Description Value Nominal Value
153 W- Dirty Window Correction - Pre Maintenance -0.11% 0%-4%
Cal Kit Cal Kit Reading-Pre Maintenance 0.30% 0%-2%
121 Sm - Signal Measurement 15553 n/a
122 Rm - Reference Measurement 54101 n/a
123 SF - Signai Flood Value 51880 n/a
124 Rf- Reference Flood Value 55831 n/a
125 So - Signal Offset 154 n/a
126 Ro -Reference Offset 124 n/a
127 Calculated Opacity 0.04 n/a
137 PLCF 0.460 0.460
140 C -Calibration Slope 3.543 n/a
141 X - Calibration Offset 0.092 n/a
142 B - Calibration Balance Factor 0.884 --1.0
149 W- Dirty Window Correction- Post Maintenance 1.00 n/a
153 Op0 - Zero Compensation 0.00% 0
154 Opz- Cal Check Last Zero 0.00% 0
155 Opc- Cal Check Last Upscale 13.20% —13%
Cal Kit Cal Kit Reading - Post Maintenance 0.00% 0%-2%
Alarms
All OK OK ON/OFF OFF
Technician John Tsouris Date 9/24/2021
Page 23
TE HNa S) MSTM
Maintenance Records
and
Quality Assurance Test Results
Quarter 4 - 2021
for
OPACITY COMS----
3M
4191 NC 87 South
Moncure, NC 27559
by
TechnoCEMS
8131 Lamella Ln
Tampa, FL 33647
John Tsouris, Senior CEM Specialist
Table 01' Contents
Page
1. Summary
2. Line 1 - Opacity Calibration Test Audit Results
6. Line 2 - Opacity Calibration Test Audit Results
10. Dryer - Opacity Calibration Test Audit Results
14. Optical Filter Certification Report
19. Maintenance Checklists
24. Appendix A - Opacity Formulas
Summary
During calendar Quarter 4 (Q4) 2021 , TechnoCEMS
personnel performed the required preventive maintenance
and quality assurance testing on the 3M Corp Continuous
Opacity Monitoring systems. The opacity monitor
maintenance activities and calibration filter audits were
performed in accordance with the regulatory and company
guidelines provided by 3M Corporation intended to meet the
Quality Assurance Requirements of 40 CFR 60 Appendix F,
Procedure 3. The results of this testing and a record of the
maintenance activities are included herein.
Page 1
Opacity Calibration Audit Results
Page 2
• . • AuditSummaryPre heater
AirVision Wonderware
Parameter - Opacity LOW: 0.1 0.1
MID: 0.1 0.1
HIGH: 0.0 0.0
ASS Pass/Fail: <3% Error
See appendices for test formula
Parameter - Zero Compensation Compensation at
Time of Audit:
Equivalent Opacity: 0.00%
ASS Pass/Fail: <4%Opacity
See appendices for test formula
Parameter - Optical Alignment �\
0
ASS
Pass/Fail: Indicator inside 2nd ring-
Defined by manufacturer as point at
which opacity reading changes 2%.
Page 3
CALIBRATION ERROR DETERMINATION - PREHEATER LINE 1
TESTER John Tsouris-TechnoCEMS Manufacturer LAND Combustion
COMPANY 3M Model 4500Mk3 Serial# 227691 72
LOCATION Pittsboro, NC
SOURCE Line 1
Filter Value Corrected Required
DATE December 16,2021 Range
Filter 1 Value 15.5% 9.8% 5%-10%
Last Off-Stack Calibration(3 Year-calendar) 6/24/2020 Filter 2 Value 26.4% 17.1% 10%-20%
Cross-stack target within spec? YES Cross Stack Target Filter 3 Value 47.9% 32.9% 20%-40%
Off-stack zero as-found(2%max): 0.8% Opacity Limit 10%
Off-stack zero post service: 0.0% O OPLR 0.305
Last cal-kit Calibration 12/16/21 Taper Ratio(2 X OPLR) 0.611
Cross-stack target within spec? YES Dirt Compensation During Cal Audit 0.00 (4%max)
Cal-kit zero as-found(2%max): 0.0% Cross-stack target within spec? YES
Cal-kit zero post service: 0.0%
Corrected ARITHMETIC DIFFERENCE
Target AirVision Wonderware Wonderware Wonderware AirVlston Wonderware AlrVfsion Filter Wonderware
Run# Value Response Response AirVisior zero zero AiMsion Filter Fitter Filter Filter 3 Filter-
3-Zero At Start 0.0 0.1 0.0 0.1 0.0 -------- -------- -------- -------- -------- --------
9.8 9.9 9.9 -------- -------- 0.1 0.1 -------- -------- -------- --------
Drop 1 17.1 17.2 17.2 ------- -------- -------- -------- 0.1 0.1 ------- --------
32.9 32.9 32.9 -------- -------- -------- -------- -------- -------- 0.0 0.0
9.8 9.9 9.9 -------- -------- 0.1 0.1 -------- -------- -------- --------
Drop 2 17.1 17.2 17.2 -------- -------- -------- -------- 0.1 0.1 -------- --------
32.9 32.9 32.9 -------- -------- -------- -------- -------- -------- 0.0 0.0
9.8 9.9 9.9 -------- -------- 0.1 0.1 -------- -------- -------- --------
Drop 3 17.1 17.2 17.2 -------- -------- -------- -------- 0.1 0.1 -------- --------
32.9 32.9 32.9 -------- -------- -------- -------- -------- -------- 0.0 0.0
Zero At End 0.0 0.1 0.0 0.1 0.0 --- ---- -------- -------- -------- -------- --------
Arithmetic Mean X 0.100 0,000 0.100 0.100 0.100 0.100 0.000 0.000
Confidence Coefficient CC -------- -------- 0.000 0.000 0.000 0.000 0.000 0.000
Calibration Error 1XI+1CCI -------- ------- 0.100 0.100 0.100 0.100 0.000 0.000
Calibration Error-Rounded 0.1 0.0 0.1 0.1 0.1 0.1 0.0 0.0
Pass=<1.0%-All Pass=<3.0%Error
Page 4
Opacity Data Printout - Preheater Line 1
Line 1 -AirVision Line 1 - Line 1 -AirVision Line 1 -Wonderware
Date/Time OPACITY Value Wonderware Date/Time OPACITY Value OPACITY Value
OPACITY Value
12/16/2110.-52 0.1 0.0
12/16/2110:53 1.0 0.7
12/16/2110:54 9.9 9.9
12/16/2110:55 9.9 9.9
12/16/2110.-56 9.9 9.9
12/16/21 10:57 14.3 14.0
12/16/21 10:58 17.2 17.2
12/16/21 10:59 17.2 17.2
12/16/2111:00 26.3 25.9
12/16/2111:01 32.9 32.9
12/16/2111:02 32.9 32.9
12/16/21 11:03 17.6 18.2
12/16/2111:04 9.9 9.9
12/16/2111:05 9.9 9.9
12/16/2111:06 9.9 9.9
12/16/2111:07 9.9 9.9
12/16/21 11:08 17.0 16.7
12/16/21 11:09 17.2 17.2
12/16/21 11:10 17.2 17.2
12/16/21 11:11 24.1 23.6
12/16/2111:12 32.9 32.9
12/16/2111:13 32.9 32.9
12/16/2111:14 19.3 20.0
12/16/2111:15 9.9 9.9
12/16/2111:16 9.9 9.9
12/16/21 11:17 15.4 15.1
12/16/21 11:18 17.2 17.2
12/16/21 11:19 17.3 17.2 Key
12/16/2111:20 32.6 32.0 Zero
12/16/2111:21 32.9 32.9 Low
12/16/2111:22 20.2 21.2 Mid
12/16/21 11:23 0.1 0.0 High
Page 5
Opacity Calibration Audit Results
Page 6
• ' . 'Calibration
AirVision Wonderware
Parameter - Opacity Low: 0.3 0.2
MID: 0.2 0.2
HIGH: 0.1 0.1
ASS Pass/Fail: < 3%Error
See appendices for test formula
Parameter - Zero Compensation Compensation at
Time of Audit:
Equivalent Opacity: 0.00%
ASS Pass/Fail: <4%Opacity
See appendices for test formula
Parameter - Optical Alignment �\
CO)
ASS
Pass/Fail: Indicator inside 2nd ring-
Defined by manufacturer as point at
which opacity reading changes 2%.
Page 7
CALIBRATION ERROR DETERMINATION - PREHEATER LINE 2
TESTER John Tsouris-TechnoCEMS Manufacturer LAND Combustion
COMPANY 3M Model 4500Mk3 Serial# 227480 72
LOCATION Pittsboro, NC
SOURCE Line 2
Required
DATE December 16, 2021 Filter Value Corrected Range
Filter 1 Value 15.5% 9.8% 1 5%-10%
Last Off-Stack Calibration(3 Year-calendar) 6/24/2020 Filter 2 Value 26.4% 17.1% 100-20%
Cross-stack target within spec? YES Cross Stack Target Filter 3 Value 47.9% 32.9% 20%-40%
Off-stack zero as-found(2%max): 0.0% Opacity Limit 10%
Off-stack zero post service: 0.0% O OPLR 0.305
Last cal-kit Calibration 12/16/21 Taper Ratio(2 X OPLR) 0.611
Cross-stack target within spec? YES Dirt Compensation During Cal Audit 0.00 (4%max)
Cal-kit zero as-found(2%max): 0.1% Cross-stack target within spec? YES
Cal-kit zero post service: 0.0%
Corrected ARITHMETIC DIFFERENCE
Target AirVision Wonderware Wonderware AirVision Filter Wonderware AirVision Wonderware AirVision FillerWonderware
Run# Value Response Response AirVision Zero zero 1 Filter Filter Filler 3 Filler
Zero At Start 0.0 0.0 0.0 0.0 0.0 -------- -------- -------- -------- -------- ------
9.8 9.9 10.0 -------- -------- 0.1 0.2 -------- -------- -------- --------
Drop 1 17.1 17.3 17.3 -------- -------- -------- -------- 0.2 0.2 -------- --------
32.9 33.0 33.0 -------- -------- -------- -------- -------- -------- 0.1 0.1
9.8 9.9 10.0 -------- -------- 0.1 0.2 -------- -------- -------- --------
Drop 2 17.1 17.3 17.3 -------- -------- -------- -------- 0.2 0.2 -------- --------
32.9 33.0 33.0 -------- -------- -------- ------- -------- -------- 0.1 0.1
9.8 10.0 10.0 -------- -------- 0.2 0.2 -------- -------- -------- --------
Drop 3 17.1 17.3 17.3 -------- -------- -------- -------- 0.2 0.2 -------- --------
32.9 33.0 33.0 -------- -------- -------- -------- -------- -------- 0.1 0.1
Zero At End 0.0 0.1 0.1 0.1 0.1 -------- -------- -------- -------- -------- --------
Arithmetic Mean X 0.050 0.050 0.133 0.200 0.200 0.200 0.100 0.100
Confidence Coefficient CC -------- -------- 0.143 0.000 0.000 0.000 0.000 0.000
Calibration Error 1XI + ICCI ------- -------- 0.276 0.200 0.200 0.200 0.100 0.100
Calibration Error- Rounded 0.1 0.1 0.3 0.2 0.2 0.2 0.1 0.1
Pass=<1.0%-All Pass=<3 0%Error
Page 8
14 Opacity Data Printout - Preheater Line 2
Line 2-AirVision Line 2- Line 2-AirVision Line 2-Wonderware
Date/Time OPACITY Value Wonderware Date/Time alue OPACITY Value OPACITY Value
OPACITY V
12/16/2110:48 0.0 0.0 12/16/2111:20 0.1 0.1
12/16/2110:49 2.6 2.4
12/16/2110:50 0.2 0.0
12/16/21 10:51 9.9 9.7
12/16/2110:52 9.9 10.0
12/16/21 10:53 13.2 12.9
12/16/21 10:54 17.3 17.3
12/16/21 10:55 17.3 17.3
12/16/21 10:56 17.4 17.3
12/16/2110:57 32.7 32.2
12/16/2110:58 33.0 33.0
12/16/2110:59 33.0 33.0
12/16/21 11:00 11.8 12.5
12/16/21 11:01 9.9 10.0
12/16/2111:02 9.9 10.0
12/16/21 11:03 16.8 16.5
12/16/21 11:04 17.3 17.3
12/16/21 11:05 17.3 17.3
12/16/21 11:06 17.3 17.3
12/16/2111:07 21.0 20.6
12/16/2111:08 33.0 33.0
12/16/2111:09 33.0 33.0
12/16/2111:10 33.0 33.0
12/16/21 11:11 15.8 16.4
12/16/21 11:12 10.0 10.0
12/16/21 11:13 10.0 10.0
12/16/21 11:14 16.0 15.8
12/16/21 11:15 17.3 17.3 Key
12/16/21 11:16 17.1 17.1 Zero
12/16/2111:17 33.0 32.8 Low
12/16/2111:18 33.0 33.0 Mid
12/16/21 11:19 24.0 24.9 High
Page 9
Opacity Calibration Audit Results
COMMON - DRYER
Page 10
Calib.-rati,on • • • • Dryer
AirVision Wonderware
Parameter - Opacity Low: 0.5 0.5
MID: 0.8 0.8
HIGH: 1.0 1.1
ASS Pass/Fail: < 3%Error
See appendices for test formula
Parameter - Zero Compensation Compensation at
Time of Audit:
Equivalent Opacity: 0.00%
ASS Pass/Fail: < 4%Opacity
See appendices for test formula
Parameter - Optical Alignment
CCII
ASS �76)
Pass/Fail: Indicator inside 2nd ring-
Defined by manufacturer as point at
which opacity reading changes 2%.
Page 11
CALIBRATION ERROR DETERMINATION - COMMON - DRYER
1.41
TESTER John Tsouris-TechnoCEMS Manufacturer LAND Combustion
COMPANY 3M Model 4500Mk3 Serial# 227696 72
LOCATION Pittsboro, NC
SOURCE Common
Required
Filter Value Corrected
DATE December 16, 2021 Ran e
Filter 1 Value 15.5% 7.4% 5%-10%
Last Off-Stack Calibration(3 Year-calendar) 6/24/2020 Filter 2 Value 26.4% 13.1% 10%-20%
Cross-stack target within spec? YES Cross Stack Target Filter 3 Value 47.9% 25.9% 20%-40%
Off-stack zero as-found(2%max): -0.2% Opacity Limit 10%
Off-stack zero post service: 0.0% Ice) OPLR 0.230
Last cal-kit Calibration 12/16/21 Taper Ratio(2 X OPLR) 0.460
Cross-stack target within spec? YES Dirt Compensation During Cal Audit 0.00 (4%max)
Cal-kit zero as-found(2%max): 0.2% Cross-stack target within spec? YES
Cal-kit zero post service: 0.0%
Corrected ARITHMETIC DIFFERENCE
Target AirVision Wonderware Wonderware AirVlsion Wonderware AirVision Wonderware AirVision Filter Wonderware
Run# Value Response Response AirVlsion Zero Zero Filter 1 Filter 1 Filter 2 Filter 2 3 Filter 3
Zero At Start 0.0 0.1 0.1 0.1 0.1 -------- -------- -------- ------- -------- --------
7.4 7.7 7.7 -------- -------- 0.3 0.3 -------- -------- -------- --------
Drop 1 13.1 13.5 13.5 -------- -------- -------- -------- 0.4 0.4 -------- --------
25.9 26.2 26.3 ------- -------- -------- -------- -------- -------- 0.3 0.4
7.4 7.7 7.7 -------- -------- 0.3 0.3 -------- -------- -------- --------
Drop 2 13.1 13.5 13.5 -------- -------- -------- -------- 0.4 0.4 -------- --------
25.9 26.4 26.4 -------- -------- -------- -------- -------- -------- 0.5 0.5
7.4 7.8 7.8 -------- -------- 0.4 0.4 -------- -------- -------- --------
Drop 3 13.1 13A 13.1 -------- -------- -------- -------- 0.0 0.0 -------- --------
25.9 25.8 25.8 -------- -------- -------- -------- -------- -------- -0.1 -0.1
Zero At End 0 0 0.0 0.0 0.0 0.0 -------- -------- ------- ------- -------- --------
Arithmetic Mean X 0.050 0.050 0.333 0,333 0.267 0.267 0.233 0.267
Confidence Coefficient CC -------- ------- 0.143 0.143 0.574 0.574 0.759 0.799
Calibration Error 1XI+ICCI -------- -------- 0.476 0.476 0.841 0.841 0.992 1.066
Calibration Error-Rounded 0.1 0.1 0.5 0.5 0.8 0.8 1.0 1.1
Pass=<1.0%-All Pass=<3.0%Error
Page 12
OpacityData Printout - Common - Dryer
Common-AirVision Common- Common-AirVision Common-
Date/Time OPACITY Value Wonderware Date/Time OPACITY Value Wonderware
OPACITY Value L OPACITY Value
12/16/2113:52 0.1 0.1
12/16/2113:53 5.7 5.6
12/16/2113:54 7.7 7.7
12/16/2113:55 8.7 8.7
12/16/21 13:56 13.5 13.5
12/16/21 1157 13.5 13.6
12/16/2113:58 23.4 23.3
12/16/2113:59 26.2 26.3
12/16/21 14:00 14.8 15.1
12/16/21 14:01 5.5 5.3
12/16/2114:02 7.7 7.7
12/16/2114:03 8.6 8.5
12/16/2114:04 6.5 6.2
12/16/21 14:05 13.4 13.4
12/16/21 14:06 13.5 13.5
12/16/21 14:07 16.6 16.2
12/16/2114:08 26.3 26.3
12/16/2114:09 26.4 26.4
12/16/2114-10 26.4 26.4
12/16/21 14:11 21.2 21.3
12/16/2114:12 3.4 2.6
12/16/2114:13 7.8 7.8
12/16/2114:14 7.9 7.9
12/16/21 14:15 5.1 6.5
12/16/21 14:16 10.7 10.6
12/16/21 14:17 13.1 13.1
12/16/21 14:18 12.7 12.1
12/16/2114:19 25.7 25.8 Key
12/16/2114:20 25.8 25.8 Zero
12/16/2114.21 25.8 25.8 Low
12/16/21 14:22 15.9 16.5 Mid
12/16/21 14:23 0.0 0.0 High
Page 13
Optical Filter CertificationReport
Page 14
Opacity Certification Services, LLC 8600 Harbor Drive
Raleigh,North Carolina 27615
A Proud Veteran-Owned Business Phone 919.215.9384
Fax 919.846.6041
Web:www.opacitvccrt.com
Results of NIST-Traceable Opacity Filter
(Audit Attenuators) Certification
Customer: I 3M Pittsboro
Date of Certification: May 26,2021 Document Number: 052621-03
Date of Expiration: May 25,2022
This data is generatedfor theJbIlowing Opacity Monitor and may not apply to other monitors.
Opacity Monitor Make/Model: AMETEK-Land 4500 Mk III series
Monitor Light Source: L.E.D. Specific L.E.D. Peak Spectral Response: 520nm
Optical
Opacity @ Opacity(a, Opacity(a;
Transmittance Density Previous
Serial No: PLCF= A Opacity PLCF= PLCF
1.000 L PLCF=1.000 LPLCF= Opacity 1.000 0.6100 0.4600
B14B 15.52% 84.48% 0.0732 15.77% -0.25 9.78% 7.46%
Y27A 26.36% 1 73.64% 1 0.1329 26.59% -0.22 17.02% 1 13.13%
Y28A 47.86% 1 52.14% 1 0.2829 1 47.88% 1 -0.02 132.79% 125.89%
Spectrophotometer Information
Make/Model:A 'lent Cary 60 UV-VIs Serial Number:MY20179221
Maximum Accuracy:f 0.250 Absolute Opacity Laboratory Temperature:72°F t 3°/22°C t 1°
NIST Standard Reference Material SRM Information
SRM Type:NIST 2031b series Serial Number:Blank;709-10.772-30.709-90
SRM Date of Certification:29 April 2021 SRM Date of Expiration:30 April 2023
Signature of Spectrophotorneter Operator
Al Siffer
Page 15
Opacity Certification Services, LLC 8600 Harbor Drive
kizRaleigh,North Carolina 27615
A Proud Veteran-Owned Business Phone 919.215.9384
Fax 919.846.6041
Web:www.ovaeltvicert.com
Customer: 3M Pittsboro
Date of Certification: 26-Ma -2021
Recertification Due: 25-May-2022 Serial No
Monitor: Land 4500 Mk III B14B
A Scan Data Weighting Weighted Opacity(%)
(L.E.D. Scan 1 Scan 2 Ave. Factors Transmittance 15C
Specific) •7
570 84.487 84.476 84.482 5 422.41 0.011
560 84.561 84.568 84.565 50 4228.23 0.007 Transmission(%)
550 84.610 84.619 84.615 210 17769.05 0.009 84.48
540 84.645 84.660 84.653 890 75340.73 0.015
530 84.585 84.579 84.582 1850 156476.70 0.006
520 84.504 84.492 84.498 3990 337147.02 0.012
510 84.415 84.402 84.409 1850 156155.73 0.013 Optical Density:
500 84.238 84.232 84.235 890 74969.15 0.006 O.O
490 84.135 84.130 84.133 210 17667.83 0.005
732
480 84.183 84.169 84.176 50 4208.80 0.014
470 84.211 84.194 84.203 51 421.01 0.017 Previous Opacity(%
Sum 10000 844806.64 Sum 1
84.48 5.77
PLCF's 0.6100 0.46"1 Change in Opacity
Correctedl 9.78 1 7.46 -0.25
Opacity
90.000
80.000
70.000
60.000
..� 50.000
E
1 40.000
i`-
30.000
20.000
10.000
0.000 •
570 560 550 540 530 520 510 500 490 480 470
Wavelength
New and Existing OpacitN;and 24-48 I-lour Service PS-1, Procedure 3, Appendix F&
Page 16
Opacity Certification Services, LLC 8600 Harbor Drive
Raleigh,North Carolina 27615
A Proud Veteran-Owned Business Phone 919.215.9384
Fax 919.846.6041
Web:www.opacitvicert.com
Customer: 3M Pittsboro
Date of Certification: 26-Ma -2021
Recertification Due: 25-May-2022 Serial No
Monitor: Land 4500 Mk III Y27A
A Scan Data Weighting Weighted Opacity(90)
(L.E.D. Scan 1 Scan 2 Ave. Factors Transmittance 26.36
Specific)
570 73.750 73.731 73.741 5 368.70 0.019
560 73.985 74.001 73.993 50 3699.65 0.016 Transmission(90)
550 74.003 74.016 74.010 210 15542.00 0.013 73.64
540 74.051 74.039 74.045 890 65900.05 0.012
530 73.923 73.910 73.917 1850 136745.53 0.013
520 73.683 73.682 73.683 3990 293993.18 0.001
510 73.428 73.415 73.422 1850 135829.78 0.013 Optical Density:
500 73.080 73.082 73.081 890 65042.09 0.002 0�1329
490 72.849 72.856 72.853 210 15299.03 0.007
480 72.879 72.867 72.873 50 3643.65 0.012
470 72.946 72.948 72.947 5 364.74 0.002 Previous Opacity(%
Sum 10000 736428.37 Sum 2
73.64 6.5$
PLCF's 0.6100 0.4600 Change in Opacity
Corrected 17.02 1 13.13
Opacity -0.22
80.000
70.000
60.000
50.000
E 40.000
f= 30.000
20.000
10.000
0.000 •
570 560 550 540 530 520 510 S00 490 480 470
Wavelength
Appendix
Page 17
Opacity Certification Services, LLC 8600 Harbor Drive
Raleigh,North Carolina 27615
A Proud Veteran-Owned Business Phone 919.215.9384
Fax 919.846.6041
Web:www.opacitvicert.com
Customer: 3M Pittsboro
Date of Certification: 26-Ma -2021
Recertification Due: 25-May-2022 Serial No
Monitor: Land 4500 Mk III Y28A
A Scan Data Weighting Weighted Opacity(%)
(L.E.D. Scan 1 Scan 2 Ave. Factors Transmittance 47.86
Specific) Ov
570 51.762 51.768 51.765 5 258.83 0.006
560 52.721 52.729 52.725 50 2636.25 0.008 Transmission(%)
550 53.196 53.205 53.201 210 11172.11 0.009 52.14
540 53.149 53.150 53.150 890 47303.06 0.001
530 52.590 52.586 52.588 1850 97287.80 0.004
520 51,976 51.984 51.980 39MI 207400.20 0.008
510 51.667 51.656 51.662 1850 95573.78 0.011 Optical Density:
500 51.623 51.613 51.618 890 45940.02 0.010 O
490 51.892 51.889 51.891 210 10897.01 0.003 0.2829
. O 7A
480 52.526 52.512 52.519 50 2625.95 0.014
470 53.224 53.216 53.220 5 266.10 0.008 Previous Opacity(%
Sum 10000 521361.09 Sum 4
52.14 7•88
PLCF's 0.6100 0.4600 Change in Opacity
Corrected! 32.79 25.89 -0.02
Opacity
60.000
50.000
40.000
E 30.000
t=
20.000
10.000
0.000
570 560 550 540 530 520 510 500 490 480 470
Wavelength
Appendix
Pege 18
Maintenance Checklists - Recorded Values
ALL UNITS
Page 19
Quarterly Service Checklist
Client 3M Site Pittsboro, NC Unit# 's 1,2,Common
Instrument Physical
Description Freq. Date Performed
Clean Instruments 12/16/2021
Inspect Instrument Blowers Q 12/16/2021
Inspect Blower Tubing 12/16/2021
Blowers
Description Freq. Date Performed
Change Blower Filters As needed 12/16/2021
Monitor
Description Freq. Date Performed
Check for Faults Q 12/16/2021
Clean Optics Q 12/16/2021
Check Target Alignments Q 12/16/2021
Clean Optics/ Reflectors Q 12/16/2021
Calibration Error Determination Q 12/16/2021
1 Off-Stack Calibration 3A 6/24/2020
2 Off-Stack Calibration 3A 6/24/2020
Comm Off-Stack Calibration 3A 6/24/2020
Technician John Tsouris Date 12/16/2021
Page 20
Opacity LAND 4500Mk3 Quarterly Recorded Values
Serial Number: 227691 72 Unit Line 1
Diagnostics Menu
Parameter Description Value Nominal Value
153 W-Dirty Window Correction - Pre Maintenance 0.33% 0%-4%
Cal Kit Cal Kit Reading-Pre Maintenance 0.00% 0%-2%
121 Sm - Signal Measurement 11651 n/a
122 Rm - Reference Measurement 55743 n/a
123 SF - Signal Flood Value 47442 n/a
124 Rf- Reference Flood Value 52612 n/a
125 So - Si nal Offset 58 n/a
126 Ro -Reference Offset 100 n/a
137 PLCF 0.611 0.611
140 C - Calibration Slope 4.849 —4.7
141 X - Calibration Offset 0.121 —.125
142 B - Calibration Balance Factor 0.904 —1.0
149 W- Dirty Window Correction - Post Maintenance 1.00 n/a
153 Op0 - Zero Compensation 0.00% 0
154 Opz - Cal Check Last Zero 0.00% 0
155 Opc - Cal Check Last Upscale 17.28% —17.2%
Cal Kit lCal Kit Reading-Post Maintenance 1 0.00% 0%-2%
Alarms
All OK OK ON/OFF OFF
Technician John Tsouris Date 12/16/2021
Page 21
f
Opacity LAND 4500Mk3 QuarterlV Recorded Values
Serial Number: 227480 72 Unit Line 2
Diagnostics Menu
Parameter Description Value Nominal Value
153 W- Dirty Window Correction - Pre Maintenance 0.69% 0%-4%
Cal Kit Cal Kit Reading -Pre Maintenance 0.10% 0%-2%
121 Sm - Signal Measurement 12578 n/a
122 Rm - Reference Measurement 54213 n/a
123 SF - Signal Flood Value 49194 n/a
124 Rf- Reference Flood Value 54719 n/a
125 So - Signal Offset 114 n/a
126 Ro -Reference Offset 62 n/a
137 PLCF 0.611 0.611
140 C -Calibration Slope 4.339 —4.50
141 X - Calibration Offset 0.111 —.110
142 B - Calibration Balance Factor 0.879 —1.0
149 W- Dirty Window Correction -Post Maintenance 1.00 n/a
153 Op0 -Zero Compensation 0.00% 0
154 Opz - Cal Check Last Zero 0.00% 0
155 Opc- Cal Check Last Upscale 17.04% —16.5%
Cal Kit ICal Kit Reading - Post Maintenance 0.00% 0%-2%
Alarms
All OK I OK ON/OFF OFF
Technician John Tsouris Date 12/16/2021
Page 22
Opacity LAND 4500Mk3 Quarterly Recorded Values
Serial Number: 227696 72 Unit Common
Diagnostics Menu
Parameter Description Value Nominal Value
153 W-Dirty Window Correction -Pre Maintenance 0.13% 0%-4%
Cal Kit Cal Kit Reading-Pre Maintenance 0.20% 0%-2%
121 Sm - Signal Measurement 15528 n/a
122 Rm - Reference Measurement 54349 n/a
123 SF - Si a nal Flood Value 52539 n/a
124 Rf- Reference Flood Value 56431 n/a
125 So- Signal Offset 133 n/a
126 Ro -Reference Offset 126 n/a
137 PLCF 0.460 0.460
140 C -Calibration Slope 3.561 n/a
141 X - Calibration Offset 0.091 n/a
142 B - Calibration Balance Factor 0.883 —1.0
149 W-Dirty Window Correction-Post Maintenance 1.00 n/a
153 Op0 - Zero Compensation 0.00% 0
154 O z - Cal Check Last Zero 0.00% 0
155 Opc- Cal Check Last Upscale 13.24% -V13%
Cal Kit Cal Kit Reading-Post Maintenance 0.00% 0%-2%
Alarms
All OK OK ON/OFF OFF
Technician John Tsouris Date 12/16/2021
Page 23