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Purgeable (Volatile Organic) Fraction r Number of chemicals detected in Fraction 0 Fraction STORET Number 84085 STORET Compound Detection Number L�mit Target Pollutants to be analyzed for: } (ug/L) Concentration Detected (ug/L) Page 2 of 6 GC/MS Confirmation Yes/No 34210 Acrolein 100 N/R N/R 34215 Acrylonitrile 100 <100 Yes 34030 Benzene 5 <5 Yes 32101 Bromodichloromethane 5 N/R N/R 32104 Bromoform 5 N/R N/R 34413 Bromomethane 10 N/R N/R 32102 Carbon tetrachloride 5 <5 Yes 34301 Chlorobenzene 6 <6 Yes 34311 Chloroethane 10 <10 Yes 34576 2-Chloroethyl vinyl ether 10 N/R N/R 32106 Chloroform 5 <5 Yes 34481 Chloromethane 10 <10 Yes 32105 Dibromochloromethane 5 N/R N/R 34496 1,1-Dichloroethane 5 <5 Yes 34531 1,2-Dichloroethane 5 <5 Yes 34501 1,1-Dichloroethylene 5 <5 Yes 34546 trans-1,2-Dichloroethylene 5 <5 Yes 34541 1,2-Dichloropropane 6 <6 Yes 34704 cis-1,3-Dichloropropane 5 N/R N/R 34699 trans-1,3-Dichloropropene 5 <5 Yes 34371 Ethylbenzene 8 <8 Yes 34423 Methylene chloride 5 <5 Yes 34516 1,1,2,2 -Tetrachloroethane 7 N/R N/R 34475 Tetrachloroethylene 5 <5 Yes 34010 Toluene 6 <6 Yes 34506 1,1,1 -Trichloroethane 5 <5 Yes 34511 1,1,2 -Trichloroethane 5 <5 Yes 39180 Trichloroethylene 5 <5 Yes 34488 Trichlorofluoromethane 10 N/R N/R 39175 Vinyl chloride 10 <10 Yes Other purgeables (up to 10 highest peaks: N/A compound name conc agV,21 JUN 28 1990 CENTRAD FILE COPY B. Acid Extractable Fraction t (ug/L) Page 3 of 6 Number of chemicals detected in Fraction 0 <10 34200 Fraction STORET Number 45582 <10 34220 Anthracene STORET Compound Detection Concentration GC/MS Confirmation NumberLmit Target Detected Yes/No 10 <10 34247 Benzo (a) pyrene 10 Pollutants to be analyzed for: (ug/L) (ug/L) N/R 34521 Benzene (ghi) perylene 10 N/R 34242 34452 4-Chloro-3-methylphenol 10 N/R N/R 34586 2 -Chlorophenol; 10 <10 Yes 34601 2,4-Dichlorophenol 10 <10 Yes 34606 2,4 -Dimethylphenol 10 <10 Yes 34616 2,4-Dinitrophenol 50 <50 Yes 34657 2-Methyl-4,6-dinitrophenol 24 <24 Yes 34591 2-Nitrophenol 10 <10 Yes 34646 4-Nitrophenol 50 <50 Yes 39032 Pentachlorophenol 50 N/R N/R 34694 Phenol 10 <10 Yes 34621 2,4,6 -Trichlorophenol 10 N/R N/R other acid extractables (up to 10 highest peaks: N/A compound game conc C. Base/Neutral Fraction Number of chemicals detected in Fraction 0 Fraction STORET Number 45583 STORET Compound Detection Concentration Number Limit Target Detected Pollutants to be analyzed for: (ug/L) (ug/L) 34205 Acenaphthene 10 <10 34200 Acenaphthylene 10 <10 34220 Anthracene 10 <10 39120 Benzidine 44 N/R 34526 Benzo (a) anthracene 10 <10 34247 Benzo (a) pyrene 10 <10 34230 Benzo (b) €luoranthene 10 N/R 34521 Benzene (ghi) perylene 10 N/R 34242 Benzo (k) fluoranthene 10 <10 34278 Bis (2-chloroethoxy)methane 10 N/R GC/MS Confirmation Yes/No Yes /;�j fes °j JUN 28 s CENTRAL FILENDoPY Yes N/R C. Base/Neutral Fraction (Continued from page 3) Page 4 of 6 Fraction STORET Number 45583 f STORET Compound Detection Concentration GC/MS Confirmation Number Limit Target Detected Yes/No Pollutants to be analyzed for: (ug/L) (ug/L) 34273 Bis (2-chloroethyl) ether 10 N/R N/R 34283 Bis(2-chloroisopropyl)ether 10 <10 Yes 39100 Bis(2-ethylhexyl)phthalat}e 10 <10 Yes 34636 4-Bromophenyl'phenyl ether 10 N/R N/R 34292 Butyl benzyl phthalate 10 N/R N/R 34581 2-Chloronaphthalene 10 N/R N/R 34641 4-Chlorophenyl phenyl ether 10 N/R N/R 34320 Chrysene 10 <10 Yes 34556 Dibenzo(a,h) anthracene -10 N/R N/R 34536 1,2 -Dichlorobenzene 10 <10 Yes 34566 1,3 -Dichlorobenzene 10 <10 Yes 34571 1,4 -Dichlorobenzene 10 <10 Yes 34631 3,3-Dichlorobenzidine 20 N/R N/R 34336 Diethyl phthalate 10 <10 Yes 34341 Dimethyl phthalate 10 <10 Yes 39110 Di -n -butyl phthalate 10 <10 Yes 34611 2,4-Dinitrotoluene 10 <10 Yes 34626 2,6-Dinotrotoluene 10 <10 Yes 34596 Di-n-octyl phthalate 10 N/R N/R 34346 1,2-Diphenylhydrazine 10 N/R N/R 34376 Fluoranthene 10 <10 Yes 34381 Fluorene 10 <10 Yes 39700 Hexachlorobenzene 10 <10 Yes 34391 Hexachlorobutadiene 10 <10 Yes 34386 Hexachlorocyclopentadiene 10 N/R N/R 34396 Hexachloroethane 10 <10 Yes 34403 Indeno(1,2,3-cd)pyrene 10 N/R Yes 34408 Isophorone 10 N/R N/R 34696 Naphthalene 10 <10 N/R 34447 Nitrobenzene 10 <10 Yes 34438 N-nitrosodimethylamine 10 N/R N/R 34428 N-nitroso-di-n-propylamine 10 N/R N/R 34433 N-nitrosodiphenylamine 10 N/R N/R 34461 Phenanthrene 10 <10 Yes 34469 Pyrene 10 <10 Yes 34551 1,2,4-Trichlorobenzene 10 <10 Yes Other Base/Neutrals (up to 10 highest peaks: N/A D compound name conc JUN 28 1990 CENTRAL FILE COPY D.. Organochloride Pesticides and PCB's Number of chemicals detected in Fraction NOT REQUESTED BY CLIENT Page 5 of 6 Fraction STORET Number 00188 STORET Compound Detection Concentration GC/MS Confirmation Number Limit Target Detected Yes/No Pollutants to be analyzed for: (ug/L) (ug/T.) tom, 39330 Aldrin 0.05 N/R 39337 alpha -BHC 0.05 N/R 39338 Beta -BHC 0.05 N/R 34259 Delta -BHC 0.05 N/R 39340 Gamma -BHC (Lindane) 0.05 N/R 39350 Chlordane 0.5 N/R 39310 4,4' -DDA 0.1 N/R 39320 4,4' -DDE 0.1 N/R 39300 4,4' -DDT 0.1 N/R 39560 Demeton 0.1 N/R 39380 Di-eldrin 0.01 N/R 34361 Endosulfan I (alpha) 0.05 N/R 34356 Endosulfan II (beta) 0.1 N/R 34351 Endosulfan sulfate 0.1 N/R 39390 Endrin 0.01 N/R 34366 Endrin aldehyde 0.01 N/R 39410 Heptachlor 0.05 N/R 39420 Heptachlor epoxide 0.05 N/R 39480 Methoxychlor 0.5 N/R 39755 Mirex 0.06 N/R 39540 Parathion (ethyl) 0.6 N/R 39400 Toxaphene 1.0 N/R 34871 PCB 1016: 0.5 N/R 39488 PCB 1221 0.5 N/R 39492 PCB 1232 0.5 N/R 39496 PCB 1242 0.5 N/R 39500 PCB 1248 0.5 N/R 39504 PCB 1254 1.0 N/R 39508 PCB 1260 1.0 N/R Other Pesticides (up to 10 highest peaks: None JUN 28 f9 90 CENTRAL FILE Copy E. .Herbicides Number of chemicals detected in Fraction NOT -REQUESTED BY CLIENT Fraction STORET Number 00148 STORET Compound Detection Concentration Number Limit Target Detected Pollutants to be analyzed for: yy, (ug/L) (ug/L) 39730 2,4-D 50 N/R 39045 Silvex } 50 N/R 39740 2,4,5-T 5 N/R other Herbicides (up to 10 highest peaks: None Page 6 of 6 GC/MS Confirmation Yes/No F. Metals and Other Chemicals Number of chemicals detected in Fraction NOT REQUESTED BY CLIENT Fraction STORET Number 45583 STORET Compound Detection GC/MS Concentration Number Limit Target Detected Pollutants to be analyzed for: (ug/L) (ug/L) 01104 Aluminium 50 N/R 01097 Antimony 50 N/R 01002 Arsenic 10 N/R 01012 Beryllium 25 N/R 01027 Cadmium 2 N/R 01034 Chromium 5 N/R 01042 Copper 2 N/R 01051 Lead 10 N/R 01900 Mercury 0.2 N/R 01067 Nickel 10 N/R 01147 Selenium 5 N/R 01077 Silver 5 N/R 01092 Zinc 10 N/R Other Inorganics: 01007 Barium 500 N/R 00940 Chloride 1000 N/R 00720 Cyanide 20 N/R 00951 Fluoride 100 N/R Analytical Laboratory Representative: 1 Signed: Date: �o g .1�,�1V ', ?n-r�.t._ ,.?� �® 8 1990 Facility Operator in Responsible Charge (OCR) : CENTRAL FILE COPY I certify that this report is accurate and complete to the best of my knowledge. Signed: Date: