DEQp00021150

Sample ID: 951-002-1
A. Purgeable (Volatile Organic) Fraction ,
Number of chemicals detected in Fraction 0
Fraction STORET Number 84085
STORET Compound Detection
Number Limit Target
Other purgeables (up to 10 highest peaks): N/R
compound same
NR - Not Requested
e_ 1
Concentration
Detected
(ug/L)
conc
N/R
<100
<5
N/R
N/R
N/R
<5
<6
<10
N/R
<5
<10
N/R
<5
<5
<5
<5
<6
N/R
<5
<8
<5
N/R
<5
<6
<5
<5
<5
N/R
<10
Page 2 of 6
GC/MS Confirmation
Yes/No
N/R
Yes
Yes
N/R
N/R
N/R
Yes
Yes
Yes
N/R
Yes
Yes
N/R
Yes
Yes
Yes
Yes
Yes
N/R
Yes
Yes
Yes
N/R
Yes
Yes
Yes
Yes
Yes
N/R
Yes
r
Pollutants
to be analyzed for:
(ug/L)
y
34210
Acrolein
100
34215
Acrylonitrile
100
34030
Benzene
5
32101
Bromodichloromethane
5
32104
Bromoform
5
34413
Bromomethane
10
32102
Carbon tetrachloride
5
34301
Chlorobenzene
6
34311
Chloroethane
10
34576
2-Chloroethyl vinyl ether
10
32106
Chloroform
5
34481
Chloromethane
10
32105
Dibromochloromethane
5
34496
1,1-Dichloroethane
5
34531
1,2-Dichloroethane
5
34501
1,1-Dichloroethylene
5
34546
trans-1,2-Dichloroethylene
5
34541
1,2-Dichloropropane
6
34704
cis-1,3-Dichloropropane
5
34699
trans-l,3-Dichloropropene
5
34371
Ethylbenzene
8
34423
Methylene chloride
5
34516
1,1,2,2 -Tetrachloroethane
7
34475
Tetrachloroethylene
5
34010
Toluene
6
34506
1,1,1 -Trichloroethane
5
34511
1,1,2 -Trichloroethane
5
39180
Trichloroethylene
5
34488
Trichlorofluoromethane
10
39175
Vinyl chloride
10
Other purgeables (up to 10 highest peaks): N/R
compound same
NR - Not Requested
e_ 1
Concentration
Detected
(ug/L)
conc
N/R
<100
<5
N/R
N/R
N/R
<5
<6
<10
N/R
<5
<10
N/R
<5
<5
<5
<5
<6
N/R
<5
<8
<5
N/R
<5
<6
<5
<5
<5
N/R
<10
Page 2 of 6
GC/MS Confirmation
Yes/No
N/R
Yes
Yes
N/R
N/R
N/R
Yes
Yes
Yes
N/R
Yes
Yes
N/R
Yes
Yes
Yes
Yes
Yes
N/R
Yes
Yes
Yes
N/R
Yes
Yes
Yes
Yes
Yes
N/R
Yes

2=0
Sample ID: 951-002-1
B. Acid Extractable Fraction
r
Number of chemicals detected in Fraction 0
Fraction STORET Number 45582
STORET
Compound
Detection
Concentration
Number
Fraction STORET
LAmit Target
Detected
STORET
Compound Detection
Pollutants
to be analyzed for:
(ug/L)
(ug/L)
Detected
Yes/No
4
to be analyzed for:
34452
4-Chloro-3-methylphenol
10
N/R
34586
2 -Chlorophenol-
10
<10
34601
2,4-Dichlorop.henol
10
<10
34606
2,4 -Dimethylphenol
10
<10
34616
2,4-Dinitrophenol
50
<50
34657
2-Methyl-4,6-dinitrophenol 24
<24
34591
2-Nitrophenol
.10
<10
34646
4-Nitrophenol
50
<50
39032
Pentachlorophenol
50
N/R
34694
Phenol
10
<10
34621
2,4,6 -Trichlorophenol
10
N/R
Other acid
extractables (up to 10 highest
peaks): N/R
<10
Yes
compound name
conc
10
NR = Not Requested
C. Base/Neutral Fraction
Page 3 of 6
GC/MS Confirmation
Yes/No
N/R
Yes
Yes
Yes
Yes
Yes
Yes
Yes
N/R
Yes
N/R
Number of
chemicals detected in Fraction
0
Fraction STORET
Number 45583
STORET
Compound Detection
Concentration
GC/MS Confirmation
Number
Limit Target
Detected
Yes/No
Pollutants
to be analyzed for:
(ug/L)
(ug/L)
34205
Acenaphthene
10
<10
Yes
34200
Acenaphthylene
10
<10
Yes
34220
Anthracene
10
<10
Yes
39120
Benzidine
44
N/R
N/R
34526
Benzo (a) anthracene
10
<10
Yes
34247
Benzo (a) pyrene
10
<10
Yes
34230
Benzo (b) fluoranthene
10
N/R
N/R
34521
Benzene (ghi) perylene
10
N/R
N/R
34242
Benzo (k) fluoranthene
10
<10
Yes
34278
Bis (2-chloroethoxy)methane
10
N/R
N/R

Sample ID: 951-002-1
C. Base/Neutral Fraction (Continued from page 3) Page 4 of 6
Fraction STORET Number 45583 N
STORET Compound Detection Concentration GC/MS Confirmation
Number Limit Target Detected Yes/No
Pollutants to be analyzed for: (ug/L) (ug/L)
34273 Bis(2-chloroethyl)ether �' 10 N/R N/R
34283 Bis(2-chloroisopropyl)ettier 10 <10 Yes
39100 Bis(2-ethylhexyl)phthalate 10 <10 Yes
34636 4-Bromophenyl phenyl ether 10 N/R N/R
34292 Butyl benzyl phthalate 10 N/R N/R
34581 2-Chloronaphthalene 10 N/R N/R
34641 4-Chlorophenyl phenyl ether 10 N/R N/R
34320 Chrysene 10 <10 Yes
34556 Dibenzo(a,h) anthracene 10 N/R N/R
34536 1,2 -Dichlorobenzene 10 <10 Yes
34566 1,3 -Dichlorobenzene 10 <10 Yes
34571 1,4 -Dichlorobenzene 10 <10 Yes
34631 3,3-Dichlorobenzidine 20 N/R N/R
34336 Diethyl phthalate 10 <10 Yes
34341 Dimethyl phthalate 10 <10 Yes
39110 Di -n -butyl phthalate 10 <10 Yes
34611 2,4-Dinitrotoluene 10 <10 Yes
34626 2,6-Dinotrotoluene 10 <10 Yes
34596 Di-n-octyl phthalate 10 N/R N/R
34346 1,2-Diphenylhydrazine 10 N/R N/R
34376 Fluoranthene 10 <10 Yes
34381 Fluorene 10 <10 Yes
39700 Hexachlorobenzene 10 <10 Yes
34391 Hexachlorobutadiene 10 <10 Yes
34386 Hexachlorocyclopentadiene 10 N/R N/R
34396 Hexachloroethane 10 <10 Yes
34403 Indeno(1,2,3-cd)pyrene 10 N/R N/R
34408 Isophorone 10 N/R N/R
34696 Naphthalene 10 <10 Yes
34447 Nitrobenzene 10 <10 Yes
34438 N-nitrosodimethylamine 10 N/R N/R
34428 N-nitroso-di-n-propylamine 10 N/R N/R
34433 N-nitrosodiphenylamine 10 N/R N/R
34461 Phenanthrene 10 <10 Yes
34469 Pyrene 10 <10 Yes
34551 1,2,4-Trichlorobenzene 10 <10 Yes
Other Base/Neutrals (up to 10 highest peaks): N/R
l»
compound name conc
NR Not Requested
jj

dib•
Sample ID: 951-002-1
D. Organochloride Pesticides and PCB's
Number of chemicals detected in Fraction NOT REQUESTED BY CLIENT Page 5 of 6
Fraction STORET Number 00188
STORET Compound Detection Concentration GC/KS Confirmation
Number Limit Target Detected Yes/No
.Pollutants
to be analyzed for:
(ug/L)
(ug/L)
39330
Aldrin
0.05
N/R
N/R
N/R
N/R
39337
alpha -BHC
0.05
N/R
N/R
39338
Beta -BHC
0.05
N/R
N/R
34259
Delta -BHC
0.05
N/R
N/R
39340
Gamma -BHC (Lindane)
0.05
N/R
N/R
39350
Chlordane
0.5
N/R
N/R
39310
4,4' -DDD
0.1
0.1
N/R
N/R
39320
4,4' -DDE
0.1
N/R
N/R
39300
4,4' -DDT
emeton
0.1
N/R
N/R
39560
39380
Dieldrin
0.01
N/R
N/R
N/R
34361
Endosulfan I (alpha)
0.05
N/R
N/R
N/R
34356
Endosulfan II (beta)
0.1
N/R
N/R
34351
Endosulfan sulfate
0.1
N/R
N/R
39390
Endrin
0.01
N/R
N/R
34366
Endrin aldehyde
0.01
N/R
N/R
39410
Heptachlor
0.05
N/R
N/R
39420
Hept oxide
0.05
N/R
N/R
39480
0
0.5
0.06
N/R
N/R
39755ixe
39540th=ten
-----�
(ethyl�j
0.6
N/R
N/R
N/R
39400
Toxaphene
1.0
N/R
N/R
N/R
34871
PCB 1016
0.5
0.5
N/R
N/R
39488
PCB 1221
0.5
N/R
N/R
39492
39496
PCB 1232
PCB 1242
0.5
N/R
N/R
39500
PCB 1248
0.5
N/R
N/R
N/R
N/R
39504
PCB 1254
1.0
1.0
N/R
N/R
39508
PCB 1260
Other Pesticides (up to 10 highest peaks):
None

Sample ID: 951-002-1
E. Herbicides
Number of chemicals detected in Fraction NOT,REQUESTED BY CLIENT
Fraction STORET Number 00148
STORET Compound Detection Concentration
Number Limit Target Detected
Pollutants to be analyzed for:
39730 2,4-D
39045 Silvex
39740 2,4,5-T
(ug/L) (ug/L)
r
50 N/R
y 50 NIR
5 NIR
Other Herbicides (up to 10 highest peaks):
None
Page 6 of 6
GC/MS Confirmation
Yes/No
F. Metals and Other Chemicals
Number of chemicals detected in Fraction NOT REQUESTED BY CLIENT
Fraction STORET Number 45583,
STORET Compound Detection GC/MS Concentration
Number Limit Target I Detected
Pollutants to be analyzed for:
(ug/L)
(ug/L)
01104
Aluminium
50
N/R
01097
Antimony
50
NIR
01002
Arsenic
10
N/R
01012
Beryllium
25
N/R
01027
Cadmium
2
N/R
01034
Chromium
5
N/R
01042
Copper
2
N/R
01051
Lead
10
N/R
01900
Mercury
0.2
N/R
01067
Nickel
10
N/R
01147
Selenium
5
N/R
01077
Silver
5
N/R
01092
Zinc
10
N/R
Other
Inorganics:
01007
Barium
500
N/R
00940
Chloride
1000
N/R
00720
Cyanide
20
N/R
009.51
Fluoride
100
N/R
Analytical Laboratory Representative:
N/R
N/R
N/R
N/R
N/R
N/R
N/R
NIR
N/R
N/R
NIR
N/R
N/R
N/R
N/R
NIR
NIR
N/R
NIR
NIR
N/R
Signed: Date: �q I Z. ( c(0)
}
I J IN t
Facility Operator in Responsible Charge (OCR):
I certify that this report is accurate and complete to the best of my.knowle�
Signed: Date: irt!L
ti