DEQp00021121

1,2/23/91 10.18 �'$ IBA,CIRI
GC/MS BASE/NEUTRAL E%TRACTABLES
EPA 625 COMPOUND LIST
IEA sample Number: 951-018-1 Date Reoeived: 11/19/91
Client Name2 E.Y. duPont Date Sampled: 11/19/91
Client Project ID: Quarterly NPDES Date Extracted: 11/22/91
Sample Identification: Outfall #001 Date Analyzed: 12/07/91
Xatrix: Water Analysis By: Gregory
DLIUtion Factor:l
t
Quantitation Results
Limit Concentration
Humber Ccuupauud (ug/L) (ug/L)
1 Acenaphthene 10 BQL
2 Acenaphthylene 10 BQL
3 Anthracene 10 BQL
4 Benzo(a)anthracene 10 RQL
5 Benzo(a)pyrene 10 BQIL
6 Benzo(b)fluoranthene 10 ROL
7 Benzo(g,h,i)perylene 10 BQL
8 Benzo(k)fluoranthene 10 ROL
9 bLe(2-0hloroethoxy)methane 10 SQL
10 bi8(2-Chloroethyl)ether 10 SQL
11 bis(2-ChloroLs0pr0pyl)ether 10 BQL
12 bis(2-Sthylhexyl)phthalate 10 ROL
13 4-Sromophenyl phenyl ether 10 SQL
14 Benzyl butyl phthalate 10 BQL
15 2-Chloronaphthalene 10 BQL
16 4-Chlorophenyl phenyl ether 10 SQL
17 Chrysene 10 BOL
18 Dibenzo(a,h)anthracene 10 SQL
19 1,2 -Dichlorobenzene 10 BOL
20 1,3 -Dichlorobenzene 10 SQL
21 1,4-Dich1orobenzene 10 BOL
22 3,31-Dichlorobenzidima 10 SQL
23 Diethyl phthalate 10 BQL
24 Dimethyl phthalate 10 BOL
25 Di-n-butylphthalate 10 SQL
26 2, 4-Diaitrotoluene 10 -BQL
27 2,6-Diaitrotoluene 10 BOL
28 Di.-n-octylphthalate 10 BOL
29 FluoraAthane 10 BQL
30 Fluorene 10 RQL
31 Sexachlorobenzene 10 BQL
32 Sexachlorobutadione 10 SQL
33 Hexachlorocyclopeatadisne 10_ - ;_ gam,
34 Sexachloroethane
35 Indeno(1,2,3-cd)pyrene
36 Isophorone 10 DEC,
37 Naphthalene 10 '991 SQL
FORM 625B (1) Rev. 101091
A
00ti

12'/23/91 10: 18 '$ IEA, CART Z004
ISA sample Number:
Client Name:
client Project ID:
Sample Identitication:
matrix:
GC/MS BASE/NEUTRAL EXTRACTABLE$
EPA 625 COMPOUND LIST
Number ,compound
951-018-1
S.I. duPont
Quarterly NPDEs
Outtall #001
Water
y
Date Received: 11/19/91
Date sampled: 1.1/19/91
Date Extracted: 11/22/91
Date Analyzed: 12/07/91
Analysis By: Gregory
Dilvition Factor:].
Quantitation Results
Limit concentration
(u8/I+) (ug/L )
36
Nitrobenzene
10
BQL
39
N-Nitroso-di-n-PxoPylamine
10
BQL
' 40
N-Nitrosodiphenylamine
10
BQL
41
Phenanthrene
10
BQL
42
Pyrene
10
BQL
43
1,2,4-TrichlorobenzeAe
10
HQL
44
Benzidine
45
N-Nitrosodimethylamine
10
BQL
comments:
*This compound is no longer provided as a normal target deliverable for
Method 625. Please contact your account representative for further
information.
Sample specific quantitation limits may be calculated by multiplying
the quantitation limit by the dilution factor.
BQL = Below Quantitation Limit
D'PC Ing,
FORM 625E (2) Rev. 101091 L��R411Rr,A-1 Fids (;�FY

12:23,'A1 10:1A $' IEA,CARI zoo
GC/HS ACID
EXTItACTABLES
EPA 625 COMPOUND LIST
IEA Sample Number: 951-018-1
Date Received:
11/19/91
Client Name: E.I. duPont
Date Sampled:
11/19/91
Client Project ID: Quarterly HPDES Date Extracted:
3-1/22/91
Sample Identification: Outfall #001
Date Analyzed:
12/07/91
Matrix: Water
Analysis By:
Gregory
Dilution Factor;l
yt/
F'.
Quantitation.
Results
Limit Concentration
Humber Compound
(ug/L)
(u5/L)
1. 4 -Chloro -3 methylphenol
10
BQL
2 2 -Chlorophenol
10
BQL
3 2,4-Dichlorophenol
10
BQL
4 2,4 -Dimethylphenol
10
BQL
5 2,4-Dinitrophenol
50
BQL
6 2--Methyl-4,6-dinitrophenol
5o
BQL
7 2-Nitrophenol
10
SQL
8 4-Nitrophenol
5o
SQL
9 Pentachlorophenol
So
B9L
10 Phenol
3,0
BQL
it 2,4,6 -Trichlorophenol
10
BQL
Comments:
Sample specific quantitation limits may be calculated by multiplying
the quantitation limit by the dilution factor.
DQL = Below Quantitation Limit
FORM 625A Rev. 101091 (��y
`•'[r7r r N C �iff Y
" c i

12/23/91 10:19 '$ IEA,CARI 01006
CC/MS SASE/NEUTRAL EXTRACTABLES
EPA 625 COMPOUND LIST
IEA sample Number: 951-018 Date Receive : N/A
Client Names E.I. duPo t Date Sampled X/A
Client Project ID: Quarterly DES Date Extri d! 11/22/91
Sample Identification: Qc Blank ( 512 ftte Analyz d: 11/27/91
Matrix: pater Analysis Scheer
sr` Dil MIAMI F ctor:l
Quantits.ti Reaults
Limit CozicQntratioA
Number Compound (u9/L) (u9/1" )
1 Acenaphthene 10 Ba
2 Acenaphthylene 10 SQL
3 Anthracene r 10 BQL4 Sent (a)anthra e 1 SQL
S Senzo )pyrene ` 1'
6 \Benzo(b luoran e 8 0 SQL
�Mzo(9,h i)Pe?yl /10 BQL
BQL
6 enzo )fl ranthe e
9 a{f-C oro boxy) hane j 10 SQL
10 b a'(2 -Ch1 root r ;' 10 SQL
11 bi(z-Chl oisal)ether 10 SQL
12bis(2-8thy yl) thalate % 10 SQL
13 8romophen phenyl ether ,' 10 BQL
14 zyl butyl hthalate 10 BQL
15 2 loronapht alone 10 BQL
16 4- ropheny phenyl ether t 10 BQL
17 Chry ne t` 10 HQL
18 Dibenzo(,a,h)ant scene 10 SQL
19 1,2-Dichioroben ne ' 10 SOL
20 1,3--Dichlorobenz a 10 BQL
21 1,4 -Dichlorobenzene 10 BQL
22 3,31-Diehlorobenzidizze 11 10 %X
23 Diethyl phthalate 10 SQL
24 Dimethyl phthalate 10 BQL
25 Di-n-butylphthalate 10 RQL
26 2,4-Dinitrotoluene 10 SQL
27 2,6-Dinitrotoluene 10 BQL
28 Di--n--octylphthalate 10 SQL
29 Fluoranthene 10 Rot+
30 Fluorene 10 SQL
31 Hexachlorobenzene 10 RQL
32 sexachlorobutadiene 10 SQL
33 Hexachlorocyclopentadiene 110 $QL
34 Hexachloroethane .10 SQL
35 Indeno(1,2,3-cd)pyrene 10 34L
36 Isophorone 10 ° SQL
37 Naphthalene 10 BQL
FORM 625E (1.) Rev, 101091

12,,,231;91 10:20 '$ IEA; CARP
GC1XS BASE/NBUTRAL EXTRACTABLES
BPA 625 COMPOUND LIST
ISA Sample Number: 951-018 Date Received: N/A
Client Name: E_I- duPont Date Sampled: N'/A
Client Project ID: Quarterly NPDES ate Fxtracted 11/22/91
sample Identification: QC Blank (SVB512) ate Analyzed: 11/27/91
Matrix: Water clysis By: Schemmer
s! ti ilu`tion Sant r:1
Quantitation Results
Limit concentration
Number C =pound ? - h SI L) ( uta/L )
38 Nitrobenzenei 10 BQL
39 N Nitroeo-di-n- opY1 10 BOL
40 N-Nitroeo .phenyl ins 'E: 10SOL
41 Phenanti� 6 , 10 ML
42 Pyre 10
43 1,2,4 Tic}slorobeuaene 10 BOL
44 BQnzid a
45 N -Nitro di tby7:�uine 10 SQL
Comments:
*This Compound is no longer provided as a norma
Method 625. Please contact your account repres
information.
sample specific quantitation limits may be ca
the quantitation limit by the dilution facto .
BQL = Below Quantitation Limit
N/A = Not Applicable
Corresponding Samples: 951-018-1
FORM 625E (2) Rev. 101091
target deliverable for
tative for further
by multiplying
DEC 310 199i
GCr �/
S<(1,A FILE COP
007

12/23'91 10:'20 $ IEA, CART' Z006
OrMM nts:
Sample specific quantitation limi maybe Qalculated by multiplying
the quantitation limit by the dilution f or.
SQL = Below Quantitation Limit t
N/A - Not Applicable
Corresponding Samples: 951-018-1
FORM 625A Rev. 101092
GC/MS ACID RXTRACTABLES
EPA 525 COMPOUND LIST
ZEA Sample
Number: 551-018,
Date
Received: N/A
Client Name: M. 1. duPont
Date
Sampled: N/A
Client Project ID: Quarterly NPD
Date
Extracted: 11/22/91
Sample Identification: QC Blank (SVBS
2) D e Analyzed: 11/27/91
alysia By: i Sabammer
xatrix:
Water
D lution FactoO l
let
Quanti
atfQn
Ro�ulte
Limi
Concentration
Number
Compound
i �•
1
4-Chloro-3-methylphenol
4L
/3130L
2
2 -Chlorophenol
10�\,
3
2,4-MLchlorophenol
_; 10
SQL
4
2, 4-Dith phenol
10
SQL
5
2,4 -Divi ro enol ; '
Rhyl 'r J
S0
5o
SQL
SQL
6
2- 4,6- ophenol
7
2 -Nig op enol °
10
SQL
8
9
,•
4 -Ni op enol ��'� ''
Penta hl opt enol'',-,
50
50
SOL
BQL
10
Phenol ',
10
BOL
11
2,4,6-T 'ghlorophen�l`
10
RQI+
OrMM nts:
Sample specific quantitation limi maybe Qalculated by multiplying
the quantitation limit by the dilution f or.
SQL = Below Quantitation Limit t
N/A - Not Applicable
Corresponding Samples: 951-018-1
FORM 625A Rev. 101092

12;20"'91 17:40 '$ IEA,CARI X005
dw
ACROLEIN / ACRYLONITRILE
EPA 603 COMPOUND LIST
IEA Sample Number:
951-017-1
Date Received:
11/13/91
Client Name:
E.I. duPont
Date Sampled:
11/13/91
Client Project Y.D.:
Quarterly NBDES
Date Analysed:
11/27/91
Sample identification:
Outfall, #002
Analysis By;;,
Smith
Matrix:
dater.
Dilution Factor:
1
Quantitation Results
Limit Concentration
Number Compound (ug/L) (ug/L)
1 Acrolein 5 SQL -
2 Acrylonitrile 5 BQL
Comments:
Sample specific quantitation limits may be calculated by multiplying
the quantitation limit by the dilution factor.
BQL - Below Quantitation Limit
FORM 603 Rev. 101091
=�Lll 3�i 1�lna
r} 1 �T
i RA F1L6 (;C)Py

12.20,91 17:40 ''$ IEA,CARI �I
Comments
Sample specifio quantitation limits may be calculated byy-,.
the quantitation limit by the dilution factor. 1
SOL - Below Quantitation Limit
appy
FORK 624 Rev. 101091
00`
GC/XS PURGEsABLES
EPA 624 COMPOUND LIST
IgA Sample Number: 951-017-1
Date Received:
11/13/91
Client
Name: P4,. 1. duPont
Date sampled:
11/13/91
Client
Project ID: Quarterly NMRS
Date Analyzed:
11/27/91
Sample
Identification: Outfall #001
Analysis By:
Harris
Matrix:
Water
Dilution Factor:l
Quantitation
Results
t
Limit
Concentration
Number
Compound
(ug/L)
(ug/L)
1
Benzene
5
BQL
2
Bromodichloromethane
5
SQL
3
Bromoform
5
BQL
4
BromomethaaQ
10
SQL
5
Carbon tetrachloride
5
BQL
6
Chlorobenzene
5
B9L
7
Chloroethane
20
SQL
8
2-Chloroet-hylvinyl ether
5
DOL
9
Chloroform
5
DOL
10
Chloromethane
10
BQL
11
Dibromochloromethane
5
BQL
12
1,2 -Dichlorobenzene
5
SOL
13
1,3 -Dichlorobenzene
5
BQL
14
1,4 -Dichlorobenzene
5
BQL
15
1,1-Dichloroethane
5
BQL
16
1,2--Dichloroothane
5
BOL
17
1,1-Dichloroethene
5
BQL
18
1,2-Dichloroethe a (total)
5
BQL
19
1,2-niahloropropane,
5
BOL
20
cis-1,3--Dichloropropene
5
BOL
21
trans-1,3-Dichloropropere
5
BQL
22
Ethylbenzene
5
BQL
23
Methylene chloride
5
BQL
24
1,1,2,2 -Tetrachloroethane
5
BQL
25
Tetrachloroethene
5
BOL
26
Toluene
5
BQL
27
1,1,3. -Trichloroethane
5
BQL
2S
1,1,2-Trichloroetha a
5
BQL
29
Trichloroethene
5
SQL
30
Trichlorofluoromethane
5
BQL
31
Vinyl Chloride
10
SQL
Comments
Sample specifio quantitation limits may be calculated byy-,.
the quantitation limit by the dilution factor. 1
SOL - Below Quantitation Limit
appy
FORK 624 Rev. 101091
00`

GG/MS MGZABLES
SPA 624 COMPOUND LIST
IEA Sample Number:
951-017
Date Receivedr
N/A
Client name: '
E.S_ duPont
Date Sampled;
N/A
client Project ID:
Quarterly NPDES
Date Analysed:
11/27/91
Sample Identification:
QC Blank (VBLR7N)
Analysis By:
Harris
Matrix:
Water
Dilution Factor:l
Number
1
2
3
4
5
fi
7
8
9
10
11
12
13
14
15
16
17
is
19
20
21
22
23
24
25
26
27
28
29
30
31
Compound
(ug/L)
Benzene 5
Brom dichloromethane 5
Bromoform S
Bromomethane 10
Results
094L)
SQL
iL
L
.L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
Coa ments:
Sample specific quantitation limits may Lie calculated by multiplying
the quantitation limit by the dilution factor, r,;, _,„''lf;J - nca�
EM = Below Quantitation Limit
N/A - Not Applicable (�
Filename .= 1127702
7%JP
Corresponding samples: 951-017-1
FORM 624 Rev. 101091
copy