DEQp00021102

IEA
An Aquarion Company
ANNUAL POLLUTANT ANALYSIS MONITORING REQUIREMENT
Report -Form A
(Revised June 1990)
I. Facility Information:
Vul
Page 1 of 9
NPDES Permit No: G Oo S 3' Discharge (Pipe) No: OD2— Year: Z
s '
Facility Name: �t�/,//lass: County: /3ee✓
Person (s) Collecting Samples: Y S SOhnJSO i•/
Status of facility wastewater treatment operation on day of sampling:
typical: L Yes No
If no, explain briefly:
Analytical Laboratory: Industrial and Environmental Analysts, Inc.
II. Sampling:
24 hr composite for main sample/grab sample for purgeable fraction
Date Sampled: (composite sample) CorrespondinQ sample taken for toxicity testing:
Sampling begun (date, time) : ell f !L Z ___ X, Yes
Sampling finished (date, time) : Q/i q/ 9t— No
Date and time sampled (grab sample).

IEA
An Aquarion Company
Sample ID: 951-032-1 (001 Eff#081992)
A. Purgeable (Volatile Organic) Fraction, EPA'Method 8240
Number of chemicals detected in Fraction 0
Fraction STORET Number 84085
STORET
Compound Quantitation
Quantitation
Number
Limit
Targe,
Limit*
Pollutants to be analyzed for: (ug/L)
(ug/L)
}
34210
Acrolein
100
34215
Acrylonitrile
100
34030
Benzene
5
32101
Bromodichloromethane
5
32104
Bromoform
5
34413
Bromomethane
10
32102
Carbon tetrachloride
5
34301
Chlorobenzene
6
34311
Chloroethane
10
34576
2-Chloroethyl vinyl ether
10
32106
Chloroform
5
34418
Chloromethane
10
32105
Dibromochloromethane
5
34496
1,1-Dichloroethane
5
34531
1,2-Dichloroethane
5
34501
1,1-Dichloroethylene
5
34546
trans-1,2-Dichloroethylene
5
34541
1,2-Dichloropropane
6
34704
cis-1,3-Dichloropropane
5
34699
trans-1,3-Dichloropropene
5
34371
Ethylbenzene
8
34423
Methylene chloride
5
34516
1,1,2,2 -Tetrachloroethane
7
34475
Tetrachloroethylene
5
34010
Toluene
6
34506
1,1,1 -Trichloroethane
5
34511
1,1,2 -Trichloroethane
5
39180
Trichloroethylene
5
34488
Trichlorofluoromethane
10
39175
Vinyl chloride
10
*If different from quantitation limit target
Page 2 of 9
Concentration
Detected
(ug/L)
<100
<100
<5
<5
<5
<10
<5
<6
<10
<10
<5
<10
<5
<5
<5
<5
<5
<6
<5
<5
<8
<5
<7
<5
<6
<5
<5
<5
<10
<10
GC/MS
Confirmation?
Yes No
CENTRAL FILE COPY

Rr-E3b®elf. Estimated Library Match RetentionIdentification
CnfnpLind M®le§wler Ganrgntrgt1an Probability Time (RT)
Weight (ug/L Min
Basis
(Check all that enDiv)
Scan
Number
Library Manual
Match Interpretation RT
N R
N/R = Not Requested
Complete only if non—targeted compounds are present:
Retention
Internal Standard Time
Min
A
r
N
(n o [�
B0- Q�.
3 3" Q.
-0 (D oS.
Y Z 0
(D o
HC 3 >
a
m
D tQ
Q
LT
%.0 m
U1
H
1 n
0C
W "t3
N
I ct
�O
00
O
>r �
mto
--h :T
—h (D
# N
O ct
W
r�
\0 (D
\0 0)
N X'
N
LTi

IEA
An Aquarion Company
Sample I.D.:951-032-1 (001 Eff#081992)
B. Acid Extractable Fraction, EPA Method 625
Number of chemicals detected in Fraction 0
Fraction STORET Number 45582
STORET
Compound Quantitation
Number
Limit Target
Confirmation?
�1
Pollutants to be analyzed for:
(ug/:W
(ug/L)
(ug/L)
y
34452
4-Chloro-3-methylphenol
10
34586
2 -Chlorophenol
10.
34601
2,4-Dichlorophenol
10
34606
2,4 -Dimethylphenol
10
34616
214-Dinitrophenol
50
34657
2-Methyl-4,6-dinitrophenol
50
34591
2-Nitrophenol
10
34646
4-Nitrophenol
50
39032
Pentachlorophenol
50
34694
Phenol
10
34621
2,4,6 -Trichlorophenol
10
*If different from quantitation limit target
Page 4 of 9
Quantitation
Concentration
GC/MS
Limit*Detected
Confirmation?
(ug/L)
(ug/L)
Yes No
<10
X
<10
X
<10
X
<10
X
<50
X
<50
X
<10
X
<50
X
<50
X
<10
X
<10
X
CENTRAL FELE Copy
0

Compound
Probable
Molecular
Weight
Estimated
Concentration
u L
Library Match
Probability
%
Retention
Time (RT)
Min
Identification Basis
Check all that apply)
Scan
Number
Library
Match
Manual
Interpretation
RT
N R
3
H 0
n
ea
:.(D
k
C+
n
w
to c+
cnSD
�Cr
I Fr
o (D
wm
N
1
N sr
ro
O c+
00
M o
o N•
00 w
CD (D
tow
N f+
b
(D
P
x
C'1
n
O
J'
! "
Cgn
s'?s
L:TZ
N/R = Not Requested
Complete only if non—targeted compounds are present:
Retention
Internal Standard Time
Min
cn o
;
0 fi
b::Y,
n
�.
�n
;
b
m
3
H 0
n
ea
:.(D
k
C+
n
w
to c+
cnSD
�Cr
I Fr
o (D
wm
N
1
N sr
ro
O c+
00
M o
o N•
00 w
CD (D
tow
N f+
b
(D
P
x

IEA
An Aquarion Company
Sample
I.D.: 951-032-1 (001 Eff#081992)
C. Base/Neutral Fraction, EPA Method
625
Page 6 of 9
Number
of chemicals detected in Fraction
0
Fraction STORET Number 45583
STORET
Commpound Quantitation
Quantitation Concentration
GC/MS
Number
Limit Target
Limit* Detected
Confirmation?
Pollutants to be analyzed for:
(ug/L)
(ug/L) (ug/L)
Yes No
34205
Acenaphthene
10
<10
`'
X
34200
Acenaphthylene
101
<10
X
34220
Anthracene
10�
<10
X
39120
Benzidine
5.0
<50
X
34526
Benzo (a) anthracene
10
<10
X
34247
Benzo (a) pyrene
10
<10
X
34230
Benzo (b) fluoranthene
10
<10
X
34521
Benzo (ghi) perylene
10
<10
X
34242
Benzo (k) fluoranthene
10
<10
X
34278
Bis (2-chloroethoxy)methane
10
<10
X
34273
Bis(2-chloroethyl)ether
10
<10
X
34283
Bis(2-chloroisopropyl)ether
10
<10
X
39100
Bis(2-ethylhexyl)phthalate
10
<10
X
34636
4-Bromophenyl phenyl ether
10
<10
X
34292
Butyl benzyl phthalate
10
<10
X
34581
2-Chloronaphthalene
10
<10
X
34641
4-Chlorophenyl phenyl ether
10
<10
X
34320
Chrysene
10
<10
X
34556
Dibenzo(a,h) anthracene
10
<10
X
34536
1,2 -Dichlorobenzene
10
<10
X
34566
1,3 -Dichlorobenzene
10
<10
X
34571
1,4 -Dichlorobenzene
10
<10
X
34631
3,3-Dichlorobenzidine
20
<20
X
34336
Diethyl phthalate
10
<10
X
34341
Dimethyl phthalate
10
<10
X
39110
Di -n -butyl phthalate
10
<10
X
34611
2,4-Dinitrotoluene
10
<10
X
34626
2,6-Dinotrotoluene
10
<10
X
34596
Di-n-octyl phthalate
10
<10
X
34346
1,2-Diphenylhydrazine
10
<10
X
34376
Fluoranthene
10
<10
X
34381
Fluorene
10
<10
X
39700
Hexachlorobenzene
10
<10
X
34391
Hexachlorobutadiene
10
<10
X
34386
Hexachlorocyclopentadiene
10 <10
X
34396
Hexachloroethane
10�--
<10
X
34403
Indeno(1,2,3-cd)pyrene
10
<10
X
34408
Isophorone
10
<10
X
34696
Naphthalene
10
<10
X
34447
Nitrobenzene
10
CFN VPAL FILE COPY <10
X
34438
N-nitrosodimethylamine
10
<10
X
34428
N-nitroso-di-n-propylamine
10
<10
X
34433
N-nitrosodiphenylamine
10
<10
X
34461
Phenanthrene
10
<10
X
34469
Pyrene
10
<10
X
34551
1,2,4-Trichlorobenzene
10
<10
X
*If different from quantitation target

Compound
Ofebable Estimated. Library Match
Molecular Concentration Probability
Weight u L %
Retention
Time (RT)
Min
Identification Basis
Check all that apply)
Scan
Number
Library Manual
Match Interpretation
RT
N R
Comments:
N/R = Not Requested
Complete only if non --targeted compounds are present:
Retention
Internal Standard Time
Min
Cl)
r—
r=-
M
n
0
0
0

IEA.
An Aquarion Company
Sample ID: 951-032-1 (001 Eff#081992) Page 8 of 9
D. Organochlorine/Organophosphorus Pesticides and PCB's
Number of chemicals detected in Fraction N/R = Not Requested
Fraction STORET Number 00188
STORET Compound Quantitation Quantitation Concentration Confirmation?
Number Limit Target Limit* Detected Dual Column GC/MS
1.Pollutants to be analyzed for: (ug/L) (ug/L) (ug/L) Yes No Yes No
Organochlorine Pesticides/PCB's:
EPA Met �iod 8080
39330
Aldrin
0.05
39337
alpha -BHC
0.05 7
39338
Beta -BHC
0.05
34259
Delta -BHC
0.1
39340
Gamma -BHC (Lindane)
0.05
39350
Chlordane
0.2
39310
4,4' -DDD
0.1
39320
4,4' -DDE
0.1
39300
4,4' -DDT
0.1
39380
Dieldrin
0.02
34361
Endosulfan I (alpha)
0.1
34356
Endosulfan II (beta)
0.1
34351
Endosulfan sulfate
0.7
39390
Endrin
0.06
34366
Endrin aldehyde
0.2
39410
Heptachlor
0.05
39420
Heptachlor epoxide
0.8
39480
Methoxychlor
0.5
39755
Mirex
0.2
39400
Toxaphene
2.4
34671
PCB 1016
0.5
39488
PCB 1221
0.5
39492
PCB 1232
0.5
39496
PCB 1242
0.5
39500
PCB 1248
0.5
39504
PCB 1254
1.0
39508
PCB 1260
1.0
Organophosphorus Pesticides : EPA Method 8080
39560 Demeton 2.5
39540 Parathion (ethyl) 0.6
N/R X
N/R X
N/R x
N/R X
N/R X
N/R X
N/R X
N/R X
N/R X
N/R x
N/R x
N/R x
N/R x
N/R X
N/R x
N/R x
N/R X
N/R x
N/R x
N/R x
N/R x +'
N/R x
j4 �
U` N/R x
x
N/R x
N/R x
N/R x
E. Herbicides, EPA Method 8150
Number of chemicals detected in Fraction N/R = Not Requested
Fraction STORET Number 00148
STORET Compound
Quantitation Quantitation
Concentration
Confirmation?
Number
Limit Target Limit*
Detected
Dual Column
Pollutants to be analyzed for: (ug/L) (ug/L)
(ug/L)
Yes No
39730 2,4-D
12
N/R
x
39045 Silvex
2
N/R
x
39740 2,4,5-T
2
N/R
x
*If different from
quantitation limit target
x
x

IEA
An Aquarion Company
Organic Analytical Information: Page 9 of 9
Organic Fraction Method GC Operating Conditions Surrogates (Spikes)
Extraction Column Description Compound Recovery
Batch Continuous Length X ID, Film Thickness, %
Column Type, Carrier Gas & Flow
Rate, Temperature Program
Purgeable 8240
DB -6241 75 x .53 IDX3 u
1,2-DCE-d4
94
He - 10 ml/min, 35 Degrees C
TOL-d8
104
N/R
(5 min) to 155 Degrees C:
BFB
98
01027 Cadmium 2
sJ {
( 0 min) at 6 Degrees C/:ui rt
N/R
01034 Chromium 5
Acid Extractables 625
X 30m X 0.32mm, 0.54um, DB -5,625,
Phenol -d5
52
N/R
ti He, 30 cm/sec, 40 Degrees C
2-Fluorphenol
45
71900 Mercury 0.2
(4 min) -300 Degrees C,
2,4,6-
73
10 Degrees C/min
Tribromophenol
Base/Neutral 625
X 30m X 0.32mm, 0.54um, DB -5,625,
Nitrobenzene -d5
60
Extractable
He, 30 cm/sec, 40 Degrees C
2-Fluorobiphenyl
59
(4 min) -300 Degrees C,
Terphenyl-d14
36
N/R
10 Degrees C/min
N/R
GC/MS Library size (number of reference spectra): 55,000+
F. Metals and Other Chemicals
Number of Metals and Other Chemicals(as listed above) detected in Sample 0
Fraction STORET Number 78240 N/R = Not Requested
STORET Compound Quantitation Quantitation Concentration
Number Limit Target Limit* Detected
Pollutants to be analyzed for (ug/L) (ug/L) (ug/L)
01104 Aluminum 50
N/R
01097 Antimony 50
N/R
01002 Arsenic 10
N/R
01012 Beryllium 25
N/R
01027 Cadmium 2
N/R
01034 Chromium 5
N/R
01042 Copper 2
N/R
01051 Lead 10
N/R
71900 Mercury 0.2
N/R
01067 Nickel 10
N/R
01147 Selenium 5
N/R
01077 Silver 5
N/R
01092 Zinc 10
N/R
3ther Inorganics:
N/R
81007 Barium 500
N/R
30940 Chloride 1000
N/R
30720 Cyanide 20
N/R
30951 Fluoride 100
N/R
tIf different from quantitation limit target
lnalytical Laboratory Representative:
2'igned: {/% �i/� i Date:
9/aah1;Z_
Facility Operator in Responsible Charge (OCR):
[ certify that this report is accurate and complete
to the best of my
knowledge.
signed: Date: