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HomeMy WebLinkAboutDEQp00020267w /�_, hemours f• The Chemours Company 910-483-46810 Fluoroproducts chemours com 22828 NC Highway 87 W Fayetteville, NC 28306-7332 CERTIFIED MAIL ARTICLE NUMBER 7002 0860 0006 9104 7828 RETURN RECEIPT REQUESTED Ms. Wren Thedford NCDEQ Division of Water Resources NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 SUBJECT: NPDES Permit Renewal Application NPDES Permit No. NC0003573 Dear Ms. Thedford: April 27, 2016 RECEIVED/NCDEQ/DWR MAY 0'8 2016 Water Quality Permitting Section The Chemours Company — Fayetteville Works is requesting renewal of NPDES Wastewater Discharge Permit No. NC0003573. Since the issuance of the last permit, the ownership of this facility changed from the DuPont Company to The Chemours Company FC, LLC. Also, two separate companies, Kuraray America Inc. and the DuPont Company, are operating manufacturing units and are treating and discharging their wastewaters under the Chemours' NPDES Permit. Enclosed are the original and two copies of the General Information Form 1 (Form 3510-1), Wastewater Discharge Information Form 2C (Form 3510-2C), and additional required supporting documentation for renewal of the subject permit by the NC Division of Water Resources. Included in the permit application are the following supplemental information documents: Sludge Management Plan, Current Facility Wastewater Management, Current Facility Operating Conditions, Alternate Application Schedule for §316(b) of the Clean Water Act, Elimination of Monitoring Requirement for PFOA, and the non -reporting of bis(chloromethyl) ether. If you have any questions or need additional information, please contact me at (910) 678-1155. Enclosures I „ 'PleAe print or type in the unshaded areas only Foran Approved OMB No 2040-0086 FORM U S. ENVIRONMENTAL PROTECTION AGENCY I EPA I D NUMBER 1 GENERAL INFORMATION \0-/ EPA Consolidated Permits Program s F NCD 047 368 642 p GENERAL (Read the "General Instructions" before starting) , 2 13 14 1s GENERAL INSTRUCTIONS LABEL ITEMS If a prepnnted law has been provided, affix it in the • PLEASE PLACE LABEL IN THIS SPACE designated space Review the information carefully, if any of it Incorrect, cross through it and enter the correct data in the appropnate, rAMn area below Also, if any of the preprinted data is absent (the area to the left of the label space hats the information that should appear), please provide it in the proper I. EPA I D NUMBERis III. FACILITY NAME fill-in areas) below If the label is complete and conect, you need not complete Items 1, III, V, and A (except VI -B which must be completed regardless) Complete all items If no label V. FACILITY MAILING ADDRESS has been provided Refer to the instructions for detailed nem descriptions and for the legal authorizations under which this data is collected VI FACILITY LOCATION If POLLUTANT CHARACTERISTICS INSTRUCTIONS Complete A through J to determine whether.you need to submit any permit application forms to the EPA If you answer "yes" to any questions, you must submit this form and the supplemental form listed in the parenthesis following the question Mark "X" in the box in the third column if the supplemental form is attached If you answer "no" to each question, you need not submit any of these forms. You may answer 'no* If your activity is excluded from permit requirements, see Section C of the instructions See also, Seebon D of the instructions for definitions of bold-faced terms Mwk"x Mark SPECIFIC QUESTIONS SPECIFIC QUESTIONS res No FORM ATTACHED Yes NO FORM ATTACHED A Is this facility a publicly owned treatment works which U.S.? 2A) Xinclude B Does or will this facility (either existing or proposed) a concentrated animal feeding operation or results in a discharge to waters of the (FORM aquatic animal production facility which results in a 1e 12 is 19 20 z1 discharge to waters of the U.S.? (FORM 2B) C Is this a facility which currently results in discharges toD X Is this a proposed facility (other than those described in A X waters of the U.S. other than those described in A or B above? (FORM 2C) 22 23 24 the U.S.? (FORM 2D) 25 2e 22 E Does or will this facility treat, store, or dispose of F Do you or will you inject at this facility industrial or hazardous wastes? (FORM 3) X municipal effluent below the lowermost stratum X containing, within one quarter mile of the well bore, 2e 26 30 underground sources of drinking water? (FORM 4) 31 32 33 G Do you or will you inject at this facility any produced water H Do you or will you inject at this facility fluids for special or other fluids which are brought to the surface in X processes such as mining of sulfur by the Frasch process, solution mining of minerals, in situ combustion of fossil X connection with conventional oil or natural gas production, inject fluids used for enhanced recovery of oil or natural fuel, or recovery of geothermal energy? (FORM 4) gas, or inject fluids for storage of liquid hydrocarbons? (FORM 4) 34 35 35 37 3e I Is this facility a proposed stationary source which is one J Is this facility a proposed stationary source which is of the 28 industrial categories listed in the instructions and�/ X NOT one of the 28 industrial categories listed in the X which will potentially emit 100 tons per year of any air instructions and which will potentially emit 250 tons per pollutant regulated under the Clean Air Act and may affect year of any air pollutant regulated under the Clean Air Act 40 Al 42 43 µ 45 or be located in an attainment area? (FORM 5) and may affect or be located in an attainment area? (FORM 5) III NAME OF FACILITY SKIPC emours Company - Fayetteville Works ms to - 26 30 IV FACILITY CONTACT A NAME & TITLE (laet, first, d title) B PHONE (area code it, no) ch 2 Johnson, iael, nvironmenta Manager ( 1) 6 8-1 5 15 16 45 40 ae I a 51 52- 55 V,FACILTY MAILING ADDRESS A STREET OR P O BOX J3 22828 NC Highway 87 W ms 1e 4s B CITY OR TOWN IC STATE D ZIP CODE q Fayettevi le C 2113 6 15 ,s IM 1 41 42 47 Sl VI. FACILITY LOCATION A STREET, ROUTE NO OR OTHER SPECIFIC IDENTIFIER c 5 2 18 1 8 NC ighway 8 15 to 45 B COUNTY NAME Bladen 40 ro C CITY OR TOWN D STATE I E ZIP CODE F COUNTY CODE (ifknosm) s F y t e i i l C I 2 3 6 1340 7 15 1s 4.J 41 42 47 51 52 .54 EPA Forth 3510-1 (8-90) CONTINUE ON REVERSE i COt7TINUED FROM THt FKUN+ VII SIC CODES 4 -di it, in order of rfon B SECOND A FIRST c (Spec) INDUSTRIAL ORGANIC CHEMICALS 7 (speer) LAMINATED PLASTICS PLATE, SHEET, AND PROFILE SHAPES 3083 72869 IS 16 19 " 1e 79 D FOURTH C THIRD C(dpeCt11"UNSUPPORTED PLASTICS Fn M AND SHEET c (spear) PLASTIC MATERIALS AND RESINS 7 310811, NOTE Kuraray Butaclte ButaciteO and SentryGlasO sheeting 7 2821, NOTE: DuPont PVF resin process units is 18 to process units is 1e m Vill OPERATOR INFORMATION A NAME JB.Is the name listed in Item VIII -A also the owner? c TAhe Chemours Company FC, LLC O YES 13 NO A 55 15 18 C. STATUS OF OPERATOR (linter the appropriate tetter into the answer bac if "Other, " speetjy) D PHONE (area code & no) =FEDERAL M = PUBLIC (other than federal or state) F (specify)F AJ(302) 773-1000 S = STATE O =OTHER (specify) - 18 19 21 72 26 P = PRIVATE E STREET OR P O BOX 1 0 arket treet 55 za F CITY OR TOWN I G STATE I H ZIP CODE IX INDIAN LAND Is the facility located on Indian lands? �BWilmington DE 19898 ❑ YES © NO sx t0141 _16TO 42147 51 X EXISTING ENVIRONMENTAL PERMITS - A NPDES IJischo estoSurjacelYoter D PSD Airrmisuonsfrom Pro osedSources C T i e T, NC0003573 g P NC Title V Permit 03735 y N 15 is 17 to 30 ,s 1s 17 Ila >D B UIC Under roundlnect+ono%Fluids EOF_ s ce 7THER C-17 T c T W 0 3 431 (.vpeCljy)Land Application Permit 9 U NSA 9 30 15 19 /7 18 30 15 i6 17 IB C RCRA Hazardous Wastes E OTHER s cr T , c r i (specify) 9 Tc R NCD047368642 g is 1s tt ,5 30 15 ,e n ,e 3D XI MAP Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground Include all springs, rivers, and other surface water bodies in the map area. See instructions for precise requirements XII. NATURE OF BUSINESS (provide a bnefdescn hon) The Chemours Company - Fayetteville Works (formerly the DuPont Company - Fayetteville Works) is a fluorinated chemicals manufacturer situated on'a 2,200 -acre property in northwestern Bladen County, NC. The Chemours' products produced at the facility include fluorinated monomers and fluorinated vinyl ethers, Nafion' membranes and dispersion, and fluoropolymer processing aids. Chemours operates two natural gas / fuel oil -fired boilers, which provides steam for the entire facility. Also located at this facility are two tenant companies: Kuraray America Inc. and the DuPont Company. Kuraray thermoplastic sheet and resin manufacturing unit and the operates the Butacite® polyvinyl butyral (PVB) tonoplast interlayer manufacturing unit. DuPont operates two polyvinyl fluoride (PVF) resin SentryGlasO manufacturing units. Chemours receives and treats all of the Kuraray and DuPont process wastewater, sanitary wastewater, and contact stormwater in the Chemours' owned and operated wastewater treatment plant, and discharges that treated Wastewater Discharge Permit (Permit No. N00003573). wastewater through Outfall 001 under the Chemours' NPDES The Kuraray and DuPont non -contact cooling waters and stormwaters are discharged through Outfall 002 under the Chemours' NPDES Wastewater Discharge Permit. XIIi CERTIFICATION (see instructions) I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in the applicaho i believe that the information is true, accurate, and complete I for false information, including the possib,hty of fr and imprisonment am aware that there are significant penalties submitting A. NAME & OFFICIAL TiTLE (type orprint)BSI ATURV SIGNED CC DATEE-z Ellis H. MCGaughy - Plant Manager �V �1 -1 G% COMMENTS FOR OFFICIAL USE ONLY c C 's le EPA Form 3510-1 (8-90) DUAR'T QUADRANGLE STATE OF NORTH CAROLINA UNITED STATESNORTH CAROLINA DEPARTMENT OF NATURALaREs6L)kcI DEPARTMENT OF THE INTERIOR AND COMMUNITY DEVELOPMEN7� iyat 7.5 MINUTE SERIES (TOPOGRAPHIC) RALEIGH, N. C. GEOLOGICAL SURVEY SEA SA PALRIS 15'WA­AY so,�JO !CEDAR CREEK/ 30" 195 E 197 !' -. 7 —_ S i 7 gy r- .'� �. _ .% MIfI J..- t�r�ek Ila\ � _ -b--/,,/I/- t �.- I t f • :/ rr 17 All J_ - 6'4: . --. -�-' _ - •Tanks �,,,� 11. ----\ ` i r.>> FACILITY LEGAL--^\.,_-(ppp� .LoCk- Husks larka�DamNo3 �1 �r �-U,_1 I -55 n� ake -- -.� - laa� V�. r'� •k _ ,T�.a,� J Boat - Ypl- SCALE 1-24000 0 1000. .��...a I.WO.� 2000 IWO_ 6W0 fi0 I.Waa' 9.x_0 9000 _ IO�Q00 I! \`\ FEET- `; ` 1000 0 --= MFRS tom _,... —z000 lJ \\ v < - CONTOUR INTERVAL 5 FEET • • - _ NATIONAI. GEODETIC VERTICAL IIATUN OF 1929 DWK � [\ 1\ _ Roads do \� f Boorw art — �52 Tif15 MAP COT.:PIaES WIT" NATIONAL MAP ACCURACY STANDARDS am� 47'30" r r FOR SALE BY U. S. GEOLOGICAL SURVEY, DENVER, COLORADO 80225, OR RESTON, VIRGINIA 22092 :f ', A FOLDER DESCRIBING TOPOGRAPHIC MAPS AND SYMBOLS IS AVAILABLE ON REQUEST } CHEMOURS COMPANY - FAYETTEVILLE WORKS LOCATIONS OF INTAKE AND DISCHARGE STRUCTURES CHEMOURS COMPANY - FAYETTEVILLE WORKS LOCATIONS OF HAZARDOUS WASTE MANAGEMENT FACILITIES \ • �1 moi' � �. - lr PV a �.. t-_ 1- ' '9� � 3` �t`•11 vw- •• Cw.P. fir/• �' C �� - V �AQ5A1 EPA I.D. NUMBER (vopi finnn tarn /q/ Fo w, 1) Form Approved, OMB No. 2040-0086. NCD 047 368 642 Aooroval expires 3-31-98. urease print or type In the unst,a— alwaa FORM U.S. ENVIRONMENTAL PROTECTION AGENCY FOR PERMIT TO DISCHARGE WASTEWATER 2c ,EPA EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS Consolidated Permits Program NPDES I. OUTFALL LOCATION For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. A. OUTFALL NUMBER B. LATITUDE C. LONGITUDE D. RECEIVING WATER (name) 1 DEG 2. MIN. 3 SEC- 1. DEG 2. MIN 3 SEC. (h,f) 50.00 22.93 -78.00 50.00 11.47 Cape Fear River 001 34.00 50.00 21.58 -78.00 49.00 25.70 Cape Fear River 002 34.00 II. FLOWS. SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent. and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations. treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities). provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff; (2) The average flow contributed by each operation: and (3) The treatment received by the wastewater. Continue on additional sheets if necessary. 1 OUT- 2, OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT FALL b AVERAGE FLOW b. LIST CODES FROM NO. (hw) a. OPERATION (hst) (nichide row') a. DESCRIPTION TABLE 2C-1 BIOLOGICAL WASTEWATER TREATMENT' P;,AST 001 C:remours N.ant;far-tiring Processes 159,361 .-.1 /day cram R;tacite Mfq Process fl) Influent Sant " Y 5.7,55'; gal!day 1`• Nc:'aray SentryGlas N._o Frocess/day 121 £qua ization witn mrxino and aeracaoa 1-C 3 E 0 gal '.31 Emergenry Re.e nti,n Tank.. 1 _C. uu77- rvF v..`. Pracesses gallday - 211,ES4 Cemin Water Nea:_i-alized Renena_ate'•1! pre-Eioester Taut. 75;OGG ..I/day °`' (S) Activated Sludge Ae_•a`ion 'rank I A Sanitary Sewer10, GGo gal/nay i5) Clarifi_a:ion i:= clarifiers in parallel) 1 ,� rr^cess Areas S-orm:wa-ei - _ 94,215 ga 1;'day ITT'AL INFLUENT TO WWT1 1,205,628 yalidey vaporatioo from wwir Operations gnl/d2IGt-4�'•1Ci::. SC.UDGE '.SG_ICSi N.A[vA.=. c:¢'. c'a' - -50, 0G0 ay Evaporation frgm. Sludoe Drying 19,943 gal/day 111 Dissolved Air Flotation ` Water C.,,:.ent of iand`_ill.d Sludge (2) Rotary Filer S C - 2,493 y-1!day OIITFA!,I ,'l - TOTA:, EFFLUENT gal/day i3) 91Ldge Filter Pre -1 L o 1,133,452 i4) Sludo. Steam Weaoed Pryr_ F: i57 ti.r—1 a- off--t:—A!_t11 S 002 ;utfall on1 Treated Eflluen- 1,133,45^ ua Uday Non-Cnntacr riven -waver 2.1,051,845 gal!day Non eontacr. filtered water 1,92-5.128 gal/day _^rmaatei211,,0? ❑al/bay Sediment Re¢ovwl S0, 0G0 nal/'lay =oiler Con,iensaze alowdowa 3^a, 00t1 gal/�aY 07ITFAL' 002 , T'OTA' EFFLiEN"t.- Disrharge to surface water (Cape Fear Ricer} A. .5,813,133 galldaY OFFICIAL USE ONLY (efilurnlxradelin: , sah-r 1 g,,rh-,) EPA Form 3510-2C (8-90) PAGE 1 of 4 GUN I INUt UN KtVtKSt CONTINUED FRUM I Ht rRUN I C Except for storm runoff. leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal? Fj YES (­nt+plete the (ll-, mt: table) W1 NO.(;cn n, C.•, tun l//) 3 FREQUENCY 4 FLOW a DAYS PER a FLOW RATE (u+n?c,/) B TOTAL VOLUME (�pra lr,rnh+annl 1 OUTFALL 2 OPERATION(s) CONTRIBUTING FLOW WEEK (,r-th b MONTHS PER YEAR C DURATION 1 LONG TERM 2 MAXIMUM 1 LONGTERM 2 MAXIMUM NUMBER fhq) (h•,) (+1^`'tb AVERAGE DAILY AVERAGE DAILY III PRODUCTION A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility? W] YES (—Inplrrr hem 1/l -R) ❑ NO (e„ rt. A'r. vron /I ) B Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)? YES hese /l1-(') 0 NO (e,, w c,1wn /I) C. If you answered 'yes" to Item III -B. list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outfalls 1. AVERAGE DAILY PRODUCTION 2 AFFECTED OUTFALLS c OPERATION. PRODUCT MATERIAL. ETC- (h.rrnrtl<rllnunrh n) a. QUANTITY PER DAY b. UNITS OF MEASURE IV. IMPROVEMENTS A Are you now required by any Federal. State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater the discharges described in this application? This includes, but is not limited to, treatment equipment or practices or any other environmental programs which may affect loan conditions, administrative or enforcement orders, enforcement compliance schedule letters. stipulations, court orders, and grant or conditions permit 0 YES (—mphtr rhe A,//,nru?c /, J,/r) © NO (.,, e, lwm 11 -1f) 1. IDENTIFICATION OF CONDITION, 2. AFFECTED OUTFALLS 3 BRIEF DESCRIPTION OF PROJECT 4 FINAL COMPLIANCE DATE AGREEMENT, ETC. a NO b SOURCE OF DISCHARGE a REQUIRED b PROJECTED B OPTIONAL You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your discharges) you now have underway or which you plan Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for construction MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510-2C (8-90) PAGE 2 of 4 uuN I muc vN rt,vc a EPA I.D. NUMBER (' / r lawn brut / n/l w•m 1) rnnir�nu icn canoe ovr_c � NCD 047 368 642 EPA Form 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE V INTAKE AND EFFLUENT CHARACTERISTICS 713, 8 C See instructions before proceeding - Complete one set of tables for each outfall - Annotate the outfall number in the space provided. NOTE. Tables V-A, V -B. and V -C are included on separate sheets numbered V-1 through V-9. D Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged from any outfall. For every pollutant you list. briefly describe the reasons you believe it to be present and report any analytical data in your possession 1 POLLUTANT 2 SOURCE 1 POLLUTANT 2. SOURCE None of the pollutants listed in Table 2C-3 are believed to be present in the wastewater JEscharye from .r,i site. or final product or byproduct? VI POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS or a component of a substance which you currently use or manufacture as an intermediate Is any pollutant listed in Item V -C a substance W1 YES (Iru nll stn h polka r a, Ar/nu) ❑ NO (fin r„ hou I Fent i mono Benzene 1,2-dichloroethane Methylene chloride ^oluene EPA Form 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE C,UN ilNutV rmvrvr ,nc -- VII, BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? © YES (0,wrti, the th.•rr p w -p— , b,l... NO (en w.ie,tion 11/1) The "North Carolina Ceriodaphnia Chronic Effluent Bioassay Pruc•edure" is performed each quarter in accordance With the requirement of condition A(4) of the facility's NPDES Permit. The NCDEQ Division of Water Resources has copies of the Farm AT -1 test results that were submitted with the Discharge Monitoring Reports during the period from February 2012 through February 2016. The quarterly chronic test performed during February 2012, failed for the ceriodaphnia dubia reproduction. The required monthly chronic tests performed in March and April 2012 both passed. No other toxicity test failures occurred during the five-year term of the current permit. VIII. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? ® YES (h,r the mune adh--, ural tr/q,ln,ne rr,unArr o1, unJ/,,,//ut,rnA arv.rlc,a/ h,. ❑ NO (tro /,, eenon LQ r„ch se, h lahnralors orlirnr h.•lon } C TELEPHONE D. POLLUTANTS ANALYZED A NAME B ADDRESS („reu rod, ,t uo) (list) TPL 2401 West 51th Stieet 51 C,-'t3E-67°0 Chemical Oxygen Remand Lumberton, M," 283',P (COD); Total Organic Carbon (TCC); Tota1 SusDended Solid=_ (TSS); Ammonia (as N); Color; Fecal Coliform; Fluoride; nitrate -Nitrite las 17); Nitrogen; Total Organic ias N); Oil and Grease; Total Phosphorus (as P); Sulfate (as SO4); Surfactants; Total Aluminum; Total Iron; Total Magrnesium; Total Manganese; Part C Metals, Cyanide, and Total Phenols; Fart c GC/MS - ilglatile. Compounds; Part C GC/MS - Acid Compounds; Part C GClteS - Base/tIeutral Compounds; Part C GC/h.s Fraction - Pesticides IX CERTIFICATION I certify under penalty of lacy that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information: the information submitted is, to the best of my knowledge and belief, true. accurate, and complete I am aware that there are significant penalties for submitting false information. including the possibility of fine and 'imprisonment for knowing violations. A NAME & OFFICIAL TITLE (nlw or/nw,r) B PHONE NO (arca,,, h Ellis H. Mc:Gauq_hy - Plant Man ,er (410) 675-1224 C SIGN URE ; D DATE SIGNED � EPA Form 3510-2C (8-90) ` (J V PAGE 4 of 4 FDRM X MA: INA: U E DRAWING MES PEWRD BAL APPLICATIM CN=fsCompany •Fayeri dkWore WATER BALANCE (ReM 091.2016) MES Pem it No, NC000M Flow Units: Gallons per Day Basis: (1) All ManufacGrdng Units operating (2) Maximum 304y average of measured flows (2013.2016) ~ Cape Fear River URCNASED KURARAYAMERlCAS KURARAYAMERICAS 'DUPONT DUPONT POTABLE 0,000 CRENOURS BUTACe SENTRYGLASW FOLYWNYL POL"IM WATER 1,000 FLUORDPRODUCT POLYVKBUTYRAI LAMINATE FLUORIDE FLUORIDE MANUFACTURING MANUFACTURING MANUFACTURING 1 Rai REM SANITARY PROCESSES PROCESS PROCESS FR OCESSA PRDCESS12 _� FACILmES BOA. r 1 1 r i Evapaalm it sl +I 60,000 1 324000 .1 it � Erapatlri 1 i � suoske 5 S ACTIVATED CLARIFE ALL c° c° SLOE CATION, 001 o U U 19,943 BIOSW + z z° DEWATERI 1,133,492 26,813,133 f�--- NaDCI 3, poo MEMO Fibred W*r 50000 FILTERED $x,000 WATERSYSTEY soxcarracr NOVA eo MWATM 1,060,000 k1ha Ka.a Demineral¢ed --1 W*r URCNASED KURARAYAMERlCAS KURARAYAMERICAS 'DUPONT DUPONT POTABLE 0,000 CRENOURS BUTACe SENTRYGLASW FOLYWNYL POL"IM WATER 1,000 FLUORDPRODUCT POLYVKBUTYRAI LAMINATE FLUORIDE FLUORIDE MANUFACTURING MANUFACTURING MANUFACTURING 1 Rai REM SANITARY PROCESSES PROCESS PROCESS FR OCESSA PRDCESS12 _� FACILmES BOA. r 1 1 r i Evapaalm it sl +I 60,000 1 324000 .1 it � Erapatlri 1 i � suoske 5 S ACTIVATED CLARIFE ALL c° c° SLOE CATION, 001 o U U 19,943 BIOSW + z z° DEWATERI 1,133,492 26,813,133 OUTFALL 001 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY, You may report some or ail of this mformabon EPA LD NUMBER (copvfrom Item 1 of maim 1) on separate steels (use the same format) instead of completing these pages NCD 04 7 3 68 642 SEE INSTRUCTIONS, OUTFAII N0. V, INTAKE AND EFFLUENT CHARACTERISTICS (coftedfrom page 3 of Form 2-C) oa PART A —You must provide the results 0 at least one analysis for every pollutant in this table. Complete one table for each outfall, See instructions for additional details. 3, UNITS 4. INTAKE 2. EFFLUENT (specr(v rf blank) (npannaQ b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. VALUE a, LONG TERM a MAXIMUM DAILY VALUE (rf mm1lable) (jmvdable) AVERAGE, VALUE d. NOOF a, CONCEN NO. OF (1) (1) 1. POLLUTANT CONCENTRATION (2) MASS CONCENTRATION (2) MASS (1) CONCENTRATION q) MASS ANALYSES TRATION b. MASS (1)b. CONCENTRATION (2) MASS ANALYSES a. Biochemical Oxygen 71,0 67519 26,8 207,1 5.8 37,8 465 mg/L lb. n/a n/a n/a Demand (1101)) b, Chemical Oxygen 32.1 313.2 1 mg/L lb. n/a n/a n/a Demand (CDD) c. Total Organic Carbon (Ton 84.9 828.4 1 mg/L lb, n/a n/a n/a d, Total Suspended Solids (R 44,0 387.8 22,0 177.0 9.8 54.6 465 mg/L 1b, n/a n/a n/a e.Ammonia (ae11) 0,414 4.0 1 mg/L 1b. n/a n/a n/a VALUE VALUE VALUE VALUE f, Flow 1.627 1,133 0,907 1095 MGD MGD n/a n/a g Temperature VALUE VALUE VALUE VALUE (winter) 26.0 22,2 18.4 118 °C n/a n/a h, Temperature VALUE VALUE VALUE VALUE (summer) 32,0 30,6 29,0 118 °C n/a n/a MINIMUMMAXIMUM MINIMUM MAXI UM i PH 6.37 8.47 n/a n%a 374 STANDARD UNITS PART B — Mark "X° m column 2-a for each pollutant you know or have reason to believe is present Mark °X° in column 2-b for each pollutant you believe to be absent, If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an etRuem limitations guideline, you must provide the results of at least one analysis for that pollutant For other pollutants for which you mark column 2a, you must provide quantitative data oran explanation of their presence in your dacharge. Complete one table for each outfall. Seethe instructions foradddional details and requirements, 2. MARK `)° 3. EFFLUENT 4, UNITS 5, INTAKE (opnowa I. POLLUTANT b. MAXIMUM 30 DAY VALUE c LONG TERM AVRG. VALUE a, LONG TERM AVERAGE AND a b a. MAXIMUM DAILY VALUE (/available) (rrm�arlable) VALUE CAS NO, BELIEVED BELIEVED d. NO. OF a. CONCEN• b NO, OF (1) (1) (i) (1) (Java)lable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b, MASS CONCENTRATION (2) MASS ANALYSES a, Bromide �/ (2495961.9) X Chlonre,Total %/ 0.03 0,3 1 mg/L lb. n/a n/a n/a Residua c, Cow 10 n/a 1 PCU n/a n/a n/a n/a d, FedCddorm ��X X est. 2 n/a 1 col/dL n/a n/a n/a n/a e,FluardeX (1698448.8) /� 170 1659 1 mg/L lb. n/a n/a n/a If, Nitrate-Nimte (as M V A 0,065 0.6 1 mg/L lb, n/a n/a I n/a EPA Form 3510.2C (8.90) PAGE V•1 CONTINUE ON REVERSE OUTFALL 001 ITFM V.R (.ONTINIIFD FRn1A FRONT EPA Forth 3510.20 (8,90) PAGE V•2 CONTINUE ON PAGE V-3 2. MARK "X' 3. EFFLUENT 4, UNITS 5. INTAKE (opnowo 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c, LONGTERM AVRG. VALUE a. LONG TERM AND a b e, MAXIMUM DAILY VALUE (fm kble) (fmarlable) AVERAGEVALUE CAS NO, BELIEVED BELIEVED d, NO, OF a, CONCEN. b, NO. OF 11) (�) (1) 0) (f mailable) PRESENT ABSENT CONCENTRATION (2}MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES g. Nitrogen, TotalOrgank(arX 1.016 9.9 1 mgiL lb. n/a n/a n/a M h. 04 and�/ x <5.6 <50.0 5.2 42.5 0.26 1.87 36 mg/L lb, n/a n/a n/a Grease I Phosphorus (es P),Tofal x— 12.4 121.0 1 mg/L lb. nJa n/a n/a 0723.10) J. Rad*ad* (1)Alpha,Total X (2) Beta, Tohal X /�/` (3) Radium, x Total (4) Radium 226, �/ Total n k, Sulfate (MSWX 1083 10568 1 mg/L lb. n/a n/a n/a (14808 H) I. Sulfide �/ (m bi x m. (asiNo) (14265.453) 0.Surtadants X 3.07 30.0 1 mg/L 1b. n/a n/a n/a o.Abrmanum, Total�( 0.19 1,9 1 mg/L lb, n/a n/a n/a (7429945) / ` p. Banum, Total (7440.393) q, Boron, Total g44042-8) r, Cobalt, Total �/ x nom) s.Iron, TOWV x 0.28 2.7 1 mg/L lb, n/a n/a n/a (7439896) I, Magnesium, Total X 2.26 22.1 1 mg/L lb, n/a n/a n/a (1439954) u, Molybdenum, Total X (743 998 T) Y. Manganese, Total <0.005 <0.049 1 mg/L lb. n/a n/a n/a (74399& � w. Tin, Total x Q44431v� /� x, Tdanium, Total p44432 6) EPA Forth 3510.20 (8,90) PAGE V•2 CONTINUE ON PAGE V-3 OUTFALL 001 EPA I.D. NUMBER (copy fmm Item l of Form I) OUTFALL NUMBER NCD 047 368 642 001 VMY I nuru rRVVF VV,Im L -V PART C - 0 you are a primary industry and this outfall contains process wastewater, refer to Table 20.2 m the instructions to determine which of the GC1MS fractions you must test for. Mark'X' m column 2a for all such GC1MS fractions that apply to your industry and for ALL taxi metals, cyanides, and total phenols. 0 you are not required to mark column 2a (secondary industries, nonprocess wastewater o hits, and nonrequired GGMS hdons), mat 'X! in column 2-b for each pollutant you know or have reason to believe is present Mark'X' in column 2-c for each pollutant you believe is absent If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 1D ppb or greater. If you mark column 2b for acrolem, acrygondde, 2,4 dindrophend, or 2-metho, 6 drndropherrol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Othennse, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part, please review each carefully Complete one table (all T pages) for each 001111 See Instructions for additional detalls and requirements, 2, MARK'X' 3. EFFLUENT 4. UNITS 5, INTAKE (op iowm 1. POLLUTANT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG, a. LONG TERM AND a b c, a. MAXIMUM DAILY VALUE (f mailable) VALUE (f mwdable)AVERAGE d. NO a. CONCEN VALUE b NO, OF (11 (t) (1) (1) CONCENTRAT{ON (2)MASS CAS NUMBER TESTING BELIEVED BELIEVED .OF ANALYSES TRATION b MASS NALYSES (f ovodable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS METALS, CYANIDE, AND TOTAL PHENOLS 1M.Antimony, Total X <0.002 <0.020 1 mg/L lb. n/a n/a n/a (7440.364) /� 2M. Arsenic, Total V <0.005 <0.049 1 mg/L lb, n/a n/a n/a (t44D"39.2) !` 3M Beryllium, Total (0.001 (0.010 1 mg/L lb, n/a n/a n/a' (7440-01.7) 4M.Cadmium, Total V <0.002 <0.020 1 ni lb, n/a n/a n/a Q440.43.9) 5M,Chromum,V 0.010 0.070 0.010 0.070 0.004 0.034 4 mg/L lb. n/a n/a n/a Total (!44941.3) /� 6M. Copper, Tota!�/ x 0.007 0.050 0.007 0.050 0.0055 0.047 4 mg/L lb. n/a n/a n/a U440-59) 1M. Lead, Total<0.003 X <0,029 1 mg/L lb. n/a n/a n/a (7439 92.1) /` BM Mercury, Total V <0.0002 <0,002 1 mg/L lb. n/a n/a n/a (143957.6) 9M. Nickel, Total0.012 X x 0.090 0.012 0,090 0.0083 0.065 4 mg/L lb. n/a n/a n/a (!440.02.0) lom'Selenium, V <D.005 <0.049 1 mg/L lb, n/a n/a n/a Total (7192.492) /\ I I M Silver, Total V (0.002 <0.020 1 mg/L lb, n/a n/a n/a (7440.224) 12M Thallium, V <0.005 <0.049 1 mg/L lb. n/a n/a n/a Total (7440.19-0) /\ 13M,Zinc, Total�/ x 0.042 0.390 0.042 0.390 0.0343 0.286 4 mg/L lb. n/a n/a n/a U440�66�) 14M,Cyanide,�/ x <0,005 <0.049 1 mg/L lb. n/a n/a n/a Total (57-12.5) 15M.Phenols,�/ x <0.0400 <0.390 1 mg/L lb. n/a n/a n/a Total DIOXIN 2,3,7,8Teha- DESCRIBE RESULTS aoc applicable chlorodibenzo•P- X Dioxin (1164416) EPA Form 3510.2C (8.90) PAGE V-3 CONTINUE ON REVERSE 11 � OUTFALL 001 MkIT I inn oenu Tuo conur EPA Form 3510.2C (890) PAGE V4 CONTINUE ON PAGE V4 2, MARK'X' 3 EFFLUENT 4, UNITS 5. INTAKE (oprrota4 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a b I c a, MAXIMUM DAILY VALUE (rf tradable) VALUE (+f mmlable) AVERAGE VALUE CAS NUMBER TESTING BEUEVED BELIEVED d. NO.OF a. CONCEN b. NO OF ANALYSES (1) (1) (1) (1) (f mmlable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCEPATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS GCIMS FRACTION -VOLATILE COMPOUNDS 1V,A=&m<0.0500 X x <0.48B 1 mg/L lb. n/a n/a n/a (107-02.8) 2V.AayloftV x <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (107.13.1) 3V. BenzeneV x <0.00100 (0,10 1 mg/L lb, n/a n/a n/a (]1.43 1) 4V. &s (CMoro- mciM Ether X Not Req ired per NCDWR NPDES Permitt' g Unit (542.881) 5V,BM=formV x <0,00100 <0,10 1 mg/L lb, n/a n/a n/a W5•2) 6V Calu TehftxleX <0.00100 <0.10 1 mg/L lb. n/a n/a n/a (56.23 5) 7V.Chlorobenzm V (0.00100 <0.10 1 mg/L lb. n/a n/a n/a (10890.7) BV. ChW bmmometh�e x <0.00100 <0.10 1 mg/L lb, n/a I n/a n/a (124481) I W.ChbroethaaeV x <0.00500 <0.049 1 mg/L lb, n/a n/a n/a 95-00.3) 10V, 2 -Chloro- emyl gEmer <0.0500 <0.488 1 mg/L lb. n/a n/a n/a (110.750 11V. Chloroform�/ (0.00500 (0.049 1 mg/L lb. n/a n/a n/a (67.683) /� 12V. Drdtlora bmmornethane (0.00100 <0.10 1 mg/L lb, n/a n/a n/a 95.27.4) 13V. Dichloro- d6vama'hane X <0.00500 <0.049 1 mg/L lb, n/a n/a n/a (75.718) 14V.1,1acMoro- X <0.00100 <0.10 1 mg/L lb. n/a n/a n/a ethane (]534.3) /� 15V.1,2 -Moro- V <0.00100 <0.10 1 mg/L lb. n/a n/a n/a ethane (107-082) A 16V,1,1-DicNo*V <0,00100 <0.10 1 mg/L lb. n/a n/a n/a ethylene 9m)x 17V.1,2-DKND*V x <0.00100 <0.10 1 mg/L lb. n/a n/a n/a 98 87.5) 18V.1,3Dworo- Pmpy4eneX <0.00100 <0.10 1 mg/L lb. n/a n/a n/a (542.756) // �\ 19V Ethybeozene�/ <0.00100 <0.10 1 mg/L lb. n/a n/a n/a (100414) /� 20V WN x <0.00500 <0.049 1 mg/L lb, n/a n/a n/a Bromide 94-039) 1 21V,MeN v L <0.00250 <0.024 1 mg/L lb. n/a n/a n/a Chlonde 94.87-3) A EPA Form 3510.2C (890) PAGE V4 CONTINUE ON PAGE V4 OUTFALL 001 H/UfTlMl Irl\ r5nif 15A/±[ VI A VVI\ 111\ULU 111VRI I !.V L Y� 2. MARK \X" 3. EFFLUENT 4. UNITS 5. INTAKE (oplrnmr() 1 POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG, a. LONG TERM AND a b c a MAXIMUM DAILY VALUE (f avodable) VALUE (f available) d. NO. OF a CONCEN- AVERAGE VALUE b. NO. OF (1) CONCENTRATION (2)MASS (1) CONCENTRATION (7)MO (1) CONCENTRATION (2)MASS (1) CONCE NTR. CAS NUMBER (fmiable) TESTING REQUIRED BELIEVED PRESENT BELIEVED ABSENT ANALYSES TRAT{ON b MASS ANALYSES GCIMS FRACTION -VOLATILE COMPOUNDS (rmanmied) 22V,meweneX x <0.00500 <0.049 1 mg/L lb. n/a n/a n/a Chbdde (75-09.2) 23V, 4,1212- Tetrachlomelhane X <0.00100 (0.010 1 mg/L lb. n/a n/a n/a 9345 24V.Tetmchloro- X <0.00100 <0.010 1 mg/L lb, n/a n/a n/a ethylene (127.18.4) /\ 25V Toluene<0.00500 X <0.049 1 mg/L lb. n/a n/a n/a (108.88.3) / 26V.1,2 -Trans• DdloroethYlene X <0.00100 (0.010 1 mg/L lb. n/a n/a n/a 155695 27V.1,1,1-Trdb* V <0.00100 (0.010 1 mg/L lb. n/a n/a n/a ethane (11.556) 28V 1,12-Tnchloro- <0.00100 <0.010 1 mg/L lb. n/a n/a n/a ethane (790x5) 29VT01oro- X <0.00100 <0.010 1 mg/L lb. n/a n/a n/a ettAtene(1901.6) /� 30V, TneNoro- >luoromethaneX (0.00500 <0.049 1 mg/L 1b. n/a n/a n/a 569 4 31V.VinylChIDrWe V (0.00100 (0. 010 1 1mg/L lb, n/a n/a n/a (15.01.4} /� GC/MS FRACTION -ACID COMPOUNDS IA2-Chlorophenol <0.0100 <0.098 1 mg/L lb, n/a n/a n/a (95.57.8) 2A.2,4DchIo*�( x (0.0100 (0.098 1 mg/L lb, n/a n/a n/a phead (120.83.2) 3A,2,4Dimethyl- <0.0100 <0.098 1 mg/L lb. n/a n/a n/a phenol(1667-9) /\ 4A.4,6.Dm *O. <0.0100 <0.098 1 mg/L lb. n/a n/a n/a Crew! (6W2.1) A 5A.2,4Dndro.X <0.0100 <0.098 1 mg/L lb, n/a n/a n/a phend (51.28.5) 6A.2-N4rophend Y <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (89755) '\ 7A.4-N4rophend <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (100-02-T) BA.P-Chlo*M- X <0.0100 (0.098 1 mg/L lb. n/a n/a n/a Ctesol(59-W) /\ 9A Pentachloro-�( <0.0100 (0.098 1 mg/L lb. n/a n/a n/a phend (87.86.5) / 10A.Phend <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (108.95.2) llA.2,4,6-Tdddoro- <0.0100 <0.098 1. mg/L lb, n/a n/a n/a phenol (88-052) /� EPA Form 3510.2C (8.90) PAGE V-5 CONTINUE ON REVERSE I OUTFALL 001 e,.wlAII11:D mny TNF FRrWT EPA Form 3510.2C (8.90) PAGE V-6 CONTINUE ON PAGE V-7 2. MARK'X" 3. EFFLUENT 4. UNITS 5. INTAKE(opionalI 1 POLLUTANT b, MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONGTERM AND a b 0 a MAXIMUM DAILY VALUE (f mailable) VALUE (f anarlable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED d. N0, OF ANALYSES a. CQNCEN TRATION b.MASS b N0, OF ANALYSES (1) (1) (1) (1) (rfoulabte) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ��RATION R)� GCIMS FRACTION- BASEINEUTRAL COMPOUNDS 1B.Acenaphthert V (0.00100 <0.01 1 mg/L lb. n/a n/a n/a (83.32.9) /� 2B.kenaphtyteneV (0.00100 <0.01 1 mg/L lb. n/a n/a n/a (208.96.8) j� 3B. Anthracene \! (0.00100 (0.01 1 mg/L lb. n/a n/a n/a (120.12.7) /� 4B.Benadme�/ x (0.0100 <0.098 1 mg/L lb. n/a n/a n/a (9281-5) 58, Benzo (a) Aelhracene�( <0.00100 (0,01 1 mg/L lb, n/a n/a n/a (W /� 6BBenm(a)�( x <0.00100 <0,01 1 mg/L lb, n/a n/a n/a Pyrene (M-8) 7B, 3,4 -Benzo - flu ne (0.00100 <0.01 1 mg/L lb. n/a n/a n/a (205.99.2) 8B, Benzolphl)V x <0.00100 <0.01 1 mg/L lb. n/a n/a n/a Perylene (191-24.2) 9B Benzo (k) FluorantheneX <0.00100 (0.01 1 mg/L lb. n/a n/a n/a (2074&9) 10B. Bis (2-Cldoo ethoy) Methane�( <0, 0100 <0.098 1 mg/L 1b. n/a n/a n/a (111.91.1) ! \ 11B. &s (201oro• erhi7}Ether�( x <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (111.444) 12B. &s (2• ChloronopropA�( <0.0100 (0.098 1 mg/L lb. n/a n/a n/a Ether (102.80.1) / � 13B, Bis (2•Edml- luOPhthaMte <0.00300 <0.029 1 mg/L 1b. n/a n/a n/a (1 17-8i-7) 148 4&omophenyl PWI0 EM <0,0100 <0.098 1 mg/L lb. n/a n/a n/a (101.55.3) 15B.BOBanqI X <0.00300 <0.029 1 mg/L lb, n/a n/a n/a Phthalate (8568 7) 1612 -Chloro. ` nopl'thaweX <0.00100 (0,01 1 mg/L lb, n/a n/a n/a (91.58 7) 17B, 4•ChWo- phenylPheny Ether<0.0100 X x <0.098 1 mg/L lb, n/a n/a n/a {1005.12.3) 18B Chrysene <0.00100 <0.01 1 mg/L lb. n/a n/a n/a (218-01.9) 19B Dibenzo (a,b) Atr, e X <0.00100 <0,01 1 mg/L lb. n/a n/a n/a (53.10 3) 2DB.1,2•addoro-V x <0.00100 <0,01 1 mg/L lb, n/a n/a n/a benzene (95-50-1) 21B.1,�Ddlor0• V <0 00100 <0.01 1 mg/L lb. n/a n/a :n:/a] bomene(541.73.1) A . EPA Form 3510.2C (8.90) PAGE V-6 CONTINUE ON PAGE V-7 OUTFALL 001 n"IY - - -A.A 1 A AL 11 C VVI\111\VLV 11\Vml n4� •-� 2, MARK "X" 3 EFFLUENT 4. UNITS 5 INTAKE (opnowo 1. POLLUTANT b, MAXIMUM 30 DAY VALUE c, LONG TERM AVRG. a. LONG TERM AND a, b. c a. MAXIMUM DAILY VALUE (rf mwrlable) VALUE (f mildNe) AVERAGE VALUE b. NO CONCENTRATION (2)MASS CONCE(NIRATION (2)MASS CONCE(NFRATION (2)MASS CONCENTRATION (2)MA55 CAS NUMBER (fmadaWe) TESTING REQUIRED BELIEVED PRESENT BELIEVED ABSENT d. NO. OF ANALYSES a, CONCEN- TRATION b, MASS ANALYSES GCIMS FRACTION -BASEINEUTRAL COMPOUNDS (continued) 226.1,4-Dichloro-X V <0.00100 <0.001 1 mg/L lb. n/a n/a n/a benzene (10646.7) 238,3,3-Dehloro- v <0.0100 (0.098 1 mg/L lb, n/a n/a n/a benzidine (91.94.1) /\ 24B.Diethpl X <0.0030D <O.D29 1 mg/L lb. n/a n/a n/a Phlhalale (84.662) /� 258. Dimethyl Phthalate <0.00300 <0.029 1 mg/L lb, n/a n/a n/a (131.11.3) 26B.D-N-Bulgy V <0.00300 <0.029 1 mg/L lb. n/a n/a n/a Phthalale (8474.2) 27B.24Dndro- X <0.0100 <0.098 1 mg/L lb, n/a n/a n/a toluene(121.142) /\ 28B.2,60nitro- v <0.0100 <0.098 1 mg/L lb. n/a n/a n/a toh w (60620.2) A 298.DFN-0cM v <0.00300 (6.029 1 mg/L 1b. n/a n/a n/a Phthalate (117.840) 306.1,2 -Diphenyl hydrazine (as Azo- <0.0100 <0.098 1 mg/L lb. n/a n/a n/a benzene) (122.667) 31B Fluoranlhene v <0.00100 <0.001 1 mg/L lb. n/a n/a n/a (M44-0) A 328.Fluorenex V <0.00100 <0.001 1 mg/L lb, n/a n/a n/a (88.73-7) 33B.Hexachloro- v <0.00100 <0.001 1 mg/L lb, n/a n/a n/a benzene (1%744) A 34B.Hexaddoro-X <0.0100 (0.096 1 mg/L lb, n/a n/a n/a butadiene (87.68-3) 358. Hexachloro- cydopentadiene x <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (77.47.4) I 36BHexachlorD.�/ x <0.0100 <0.098 1 mg/L lb. n/a n/a n/a ethane (67.72.1) 37B. Indeno (1,2,3.uopyrene <0.00100 <0.001 1 mg/L lb. n/a n/a n/a (193.39.5) 388Isophorone x I (0.0100 <0,098 1 mg/L lb, n/a n/a n/a p8.59.1} I I I 39B,NaphtWene v <0.00100 <0.001 1 mg/L lb. n/a n/a n/a (91.203) 40B.libobenzeneX <0.0100 <0.098 1 mg/L lb, n/a n/a n/a (96953) 416. N Nino- sodimelhylarmne (0.0100 40.098 1 mg/L lb. n/a n/a n/a (62-75.9) 42B. N.Ndrosodl Oropome X <0.0100 <0 All 1 mg/L lb, n/a n/a n/a (621. 4- EPA Form 3510.2C (8-90) PAGE V-7 CONTINUE ON REVERSE OUTFALL 001 MOM IFr1 FROM THF MAT EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 2 MARK `)C 3 EFFLUENT 4, UNITS 5 INTAKE (opnow4 1, POLLUTANT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND b c a, MAXIMUM DAILY VALUE (f wadable) VALUE (f a�ndaNe) AVERAGE VALUE CAS NUMBER :REQ]LqRED BEUIEVED BEUIEVED d, NO. a, CONCEN b. NO (1) (1) (t} (1) (favadabie) PRESENT ABSENT CONCEN1ItATION (2) MASS CONCENTRATION (2}MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS LYSES GC/MS FRACTION- BASEINEUTRAL COMPOUNDS (commw4 43B. N t -o- sodiphenylamineX <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (86.306) 44B Phenanmrenev x <0.00100 <0.001 1 mg/L lb. n/a n/a n/a (85-01.8) 45B.Pyrene�/ (IN") x <0.00100 <0.001 1 mg/L lb. n/a n/a n/a 468.1,2,4-TrF chlorobewe X <0.0100 <0.098 1 mg/L lb. n/a n/a n/a (120.82.1) GCIMS FRACTION - PESTICIDES 1P.Aldnn�! x <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a ( 2) 2P.a-BHC\! x <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (319.84.6) Y'�BHC<0.000050 X x <5e-4 1 mg/L lb. n/a n/a n/a MUM 4Py-BHCV <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (58-&9.9) /� 5P,b-BHCX <0.000050 <5e-4 1 mg/L lb, n/a n/a n/a (31"") 6P.ChImImeV <0.000050 <0.005 1 mg/L lb. n/a n/a n/a (57.74.9) /� 7P.4,01)T<0,000050 X <5e-4 1 mg/L lb. n/a n/a n/a (5429.3) /\ 8P.4,4-DDEV x <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (72.549) OP,4,4'-DDDV x <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a P2-54.6) lop, Dieldrm�/ <0.000050 <5e-4 1 mg/L 1b. n/a n/a n/a (6457.1) /� 11P.aEwAsn�/ x <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (115.29.7) 115.29. dosuMan �/ <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (115.29.7) /� 13P Endosulfan SuBale <0.000050 <5e-4 1 mg/L lb, n/a n/a n/a (1031-07.8) 14P Endno<0,000050 X X <5e-4 1 mg/L lb. n/a n/a n/a (72.249) 1 15P, Endnn AldehydeX <0,000050 <5e-4 1 mg/L lb. n/a n/a n/a (7421.93.4) 16P.HeplacNor X <0.000050 c5e-4T 1 mg/L lb. n/a n/a n/a Pte) !� EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 OUTFAll001 EPA 10, NUMBER (copy from ltem l of Fom l) OUTFALL NUMBER NCD 047 368 642 001 nnuriw irn rnnu n.nr "i e vwnnrvw nwm rnv6 `2 MARK'X' 3. EFFLUENT 4 UNITS 5.INTAKE (opaona� 1, POLLUTANT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG, a, LONG TERM AND a, b. c a. MAXIMUM DAILY VALUE (f mailable) VALUE (rf available) AVERAGE VALUE b. NO. OF 111 (t) 11) (1) CAS NUMBER TESTING BELIEVED BELIEVED d, NO, OF ANALYSES a. CONCEN• TRATION b. MASS ANALYSES (f mmlable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATIONLMASS GCNS FRACTION- PESTICIDES (contmsed/ 17P. Heptachlor Epo)ode <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a (102457.3) 18P. PCB -1242 X 40.000500 <0.005 1 mg/L lb. n/a n/a n/a (5346&21.9) 19P.PM1254 <0.000500 <0.005 1 mg/L lb. n/a n/a n/a (11097.69.1) A 20P. PCB -1221 V <0.000500 <0,005 1 mg/L lb. n/a n/a n/a (11109.26-2) A 21P.PCM232�j x <0.000500 <0.005 1 mg/L lb. n/a n/a n/a (11141.16-5) 22P. PCB -1248<0.000500 x <0,000500 <0.005 1 mg/L lb, n/a n/a n/a (12072.29.6) x <0.000500 40.005 1 mg/L lb, n/a n/a n/a (110W 2.2 (1109682.5) f � 24P, PCB -1018 40.000500 40.005 1 mg/L lb. n/a n/a n/a (1267411.1) 25P,Tozaphere�/ x <0.000500 (0.005 1 mg/L lb, n/a (8001.352) EPA Form 3510.2C (6-90) PAGE V-9 OUTFALL 002 - PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this irdormabon EPA I,D, NUMBER (corvfrom Item 1 of Form I ) on separate sheets (use ft son bmit8o instead of completing these pages. NCD 047 368642 SEE INSTRUCTIONS. OUTFALL N0. V, INTAKE AND EFFLUENT CHARACTERISTICS (cortinuedfmrn page 3 ofForm 2•C) of PART A -You must prowde the resub of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details, 3. UNITS 4.INTAKE 2, EFFLUENT (specrfvf6lank) (oprmrwo b, MAXIMUM 3D DAY VALUE c LONGTERM AVRG, VALUE a. LONGTERM a, MAXIMUM DAILY VALUE (f mailable) (if awdable) AVERAGE VALUE d, NO OF a. CONCEN• b. NO, OF 1 1. POLLUTANT CONCENTRATION (2) MASS CONCENTRATION (2) MASS (t) CONCENTRATION j2) MASS ANALYSES TRATION b, MASS CANCENTRATION (2) ANALYSES a.BtochemdOxygen 3.9 762.1 3.9 762.1 1.4 185.7 12 mg/L lb. n/a n/a n/a Demand (80D) b.ChemdOxygen 33.7 4698 33.7 4898 4.37 458.6 12 mg/L lb. n/a n/a n/a Demand (COD) c.Total OrgaNcCarbon 12.8 1135 1 mg/L lb. n/a n/a n/a (TOC) d• Total Suspended 10.6 939.7 1 mg/L lb • n/a n/a n/a Solids (M e, Ammonia (as M 0,410 36.3 1 mg/L lb. n/a n/a n/a I. Flaw VALUE 34.791 VALUE 26.813 VALUE 14,556 1095 MGD MGD VALUE n/a n/a g. Temperature VALUE 22.0 VALUE 18.6 VALUE 14.1 188 a C VALUE n/a n/a (winter) h Temperature VALUE 33. D VALUE 31.1 VALUE 30.0 190 C VALUE n/a n/a (summer) MINIMUM MAXIMUM MINIMUM MAXIMUM i. pH 6.11 8.16 n/a n/a 647 STANDARD UNITS PART B - Mark'X' in column 2-a for each pollutant you know or have reason to believe is present Mark'X' m column 2•b for each pollutant you believe to be absent 9 you mark column 2a for any pollutant whd is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that polutant For other pollutants for which you mark column 20, you must provide quantitative data or an explanation of their presence in your decharge, Complete one table for each outfall. See the instructions for additional detalls and requirements, 2 MARK'X' 3. EFFLUENT 4. UNITS S. INTAKE (opnonat) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG VALUE a, LONG TERM AVERAGE AND a b a. MAXIMUM DAILY VALUE (f"flable) (f mailable) VALUE CAS NO. BELIEVED BELIEVED d. NO, OF a. CONCEN• b, NO, OF f fmiloble) PRESENT ABSEM CONCENTRATION (2►MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATION (2)MASS ANALYSES a, Bromide �/ X (249W7.9) b•Chlorme,Total v 0.14 12.4 1 mg/L lb. n/a n/a n/a ReWuaf A c. Cola 27 n/a 1 PCU n/a n/a n/a n/a orm d Fecal Coliform �X X / \V est. 2 n/a 1 col/dL n/a n/a n/a n/a a, Fluoride (tss /� 35.1 4110 35.1 4110 17.3 1783 12 mg/L lb. n/a n/a n/a f•Nitrate•Ndnte V 2.4 442.9 2.4 442.9 1.04 127.5 36 mg/L lb. n/a n/a n/a (as M I EPA Form 3510.2C (8.90) PAGE V-1 CONTINUE ON REVERSE e OUTFALL 002 I I CM v-6 vv1v I nrvrU rnvffl r nvn i 2. MARK °X" 3, EFFLUENT 4. UNITS 5, INTAKE (opnonaQ 1. POLLUTANT b, MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. VALUE a. LONG TERM AND 7BELIEVED b. a. MAXIMUM DAILY VALUE (+f avadabte) (f mariable) d NO.OF a. CONCEN AVERAGE VALUE b, N0, OF (11 CONCEMRATION (2) MASS (�) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS CAS N0, (favoilable) IEVED SENT ANALYSES TRATION b. MASS ANALYSES 9. Nt"en, TOW Orp ic(m / X 0.362 32.1 1 mg/L lb. n/a n/a n/a M h. Oil and6.76 X x <422 1 mg/L lb. n/a n/a n/a Grease 1. Phosphorus (as P), Toth X 1.2 154 1.2 154 0.8 85.8 36 mg/L lb. n/a n/a n/a (7723.14.0) 1. Radioactivity (1)Alpha,TOW X (2) Beta, Total X (3) Radium, Total (4) Radium 226, Total k. (M SW Supate X 105 9309 1 mg/L lb. n/a nJa n/a (1480&79.6) I. Suffde �/ x (a $l m, Suite (as SQ') (1426545.3) n.Sudadanls X 0,552 48.9 1 mg/L lb, n/a n/a n/a o. Alummum, Total�( 1.27 112.6 1 mg/L lb. n/a n/a n/a (1429.90.5) `\ p. Banum, Total (7440.39.3) q Boron, Total x(744042.8) r. Cobalt, Total �/ x (1440-08.4) sIron, TotalV x 1.15 102,0 1 mg/L lb. n/a n/a n/a (1439.896) I. Magnesium, Taalx 2.26 200.4 1 mg/L 1b. n/a n/a n/a (7439.954) u, Motybdortum, Total 643998 7) v. Manganese, Total�( 0.069 6.12 1 mg/L lb. n/a n/a n/a U43a96.5) ( ` w, Tin, Total �/ (!440.31.5) n x. Titanium, TOW (744432.6) EPA Form 3510-2C (8.90) PAGE V-2 CONTINUE ON PAGE V-3 OUTFALL 002 EPA I.D. NUMBER (copy jmm hem I ofFmm 1) OUTFALL NUMBER 11MITRn lCh Conu oer`C a rT r'nau')r NCD 047 368 642 1002 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Tet>le 2o-2 in the instructions to determine which of the GCIMS kacbons you must test for, MaA'X' in column 2-a for all such GCIMS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. B you are not required to mark column 2-a (secondary industries, nonprocess wastewater ouBafls, and nonregrared GWS fractions), mark 'X' in odumn 2-b for each pollutant you know or have reason to believe is present Mark 'V in column 2-c for each pollutant you believe is absent If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant If you mark cdumn 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to Wee d well be discharged in concentrations of 10 ppb or greater If you mark cdumn 2b for acrolem, acrylonmtle, 2,4 dinrtrophend, or 2-methyk, 6 dindrophenol, you must provide the results of at taast one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged Note that there are 7 pages to this park please review each carefully Complete one table (all 7 pages) for each outfdl. See instmdrons for additional details and requirements. 2, MARK'X' 3. EFFLUENT 4. UNITS 5. INTAKE (op 10 1. POLLUTANT b, MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. • a. LONG TERM AND ea, MAXIMUM DAILY VALUE (Jawmtable) VALUE (javarlable) AVERAGE VALUE CASNUMBER TTES'�NGBEuEvED BELIEVED d, NO.OF ANALYSES a. CONCEN• TRATION b MASS b NO OF (�) (1) (1) (�)7(�MAM (f avmlable) ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATIONANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1M, Antimony, Totd V <0,002 <0,177 1 mg/L lb. n/a n/a n/a (7440.360) I \ 2M Arses, Total X <0.005 <0.443 1 mg/L lb. n/a n/a n/a (1440.362) 3M.Baryhum,Total V (0.001 <0.099 1 mg/L lb. n/a n/a n/a p44041-7) 1 4M Cadmium, TotalV <0.002 <0.177 1 mg/L lb. n/a n/a n/a R"9)X SM, Chromim,\/ X <0.005 <0.433 1 mg/L lb. n/a n/a n/a Total (7440x47.3) 6M. Capper, TotalV 0.005 0.443 1 mg/L 1b. n/a n/a n/a (7440.5x8) /� 7M. Lead, Told X <0,003 <0.266 1 m9/L lb. n/a Na n/a (7439.92.1) 8M Mercury, Told V <0.0002 <0.018 1 mg/L lb, n/a n/a n/a (!439.97.6) 9M, Nickel, Total X <0,005 <0.433 1 mg/L lb. n/a n/a n/a (1440-02-0) /\ 10M.Selenium, <0.005 <0,433 1 mg/L lb, n/a n/a n/a Told 678249-2) /1 11 M. Silver, Total V <0.002 <0.177 1 mg/L lb, n/a n/a n/a (1440.224) f 12M.Thaurum,�/ X <0.005 <0,433 1 mg/L lb, n/a n/a n/a Total (7440.28-0) 13M. bric, Total V 0.008 0.709 1 mg/L 1b. n/a n/a n/a (744x666) A 14M. Cyanide, V <0.005 <0,433 1 mg/L lb, n/a n/a n/a Total (57.12-5) /\\ 15M. Phenofs,V X 0.0433 3.64 1 mg/L lb, n/a n/a n/a Total DIOXIN 2,3,7,8 -Tetra -D ESCRIBE RESULTS amt applicable chlorodrbenzo-P• (Amon (1764-01.6) EPA Form 3510.2C (8.90) PAGE V-3 CONTINUE ON REVERSE OUTFALL 002 rl1AITIMI ICn CMAU TWC ConMT EPA Form 3510.2C (8.90) PAGE V4 CONTINUE ON PAGE V-5 2 MARK'X' 3. EFFLUENT 4 UNITS 5, INTAKE (opwnu4 1 POLLUTANT b. MAXIMUM 30 DAY VALUE c, LONG TERM AVRG, a. LONG TERM AND a b c a MAXIMUM DAILY VALUE (i(avarlable) VALUE (rf wdable) dNOOF aCONCEN AVERAGE VALUE b NO. OF (1) CONCENTRATION (2) MASS 0) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS CAS NUMBER (�avadable) TESTING REQUIRED BELIEVED PRESENT BELIEVED ABSENT , ., ANALYSES TRATION b. MASS ANALYSES GC/MS FRACTION -VOLATILE COMPOUNDS 1V.Accrolmn <0,0500 <4.433 1 mg/L lb. n/a n/a n/a (107-02-8) 2V,Acrylondnie<0,0100 X x <0.887 1 mg/L lb. n/a n/a n/a (107.13.1) 3V. Benzene�I x <0,00100 <0.089 1 mg/L lb, n/a n/a n/a 61.43.2) 4V, Bis (Chlw- ` / me,114Ether x Not Req ired per NCDWR NPDES Permitt'g Unit (542.88.1) / ` 5V BromdormV x <0,00100 <0,089 1 mg/L lb. n/a n/a n/a (15.25.2) 6V, Carbon Tetrachloride X <0,00100 <0,089 1 mg/L lb. n/a n/a n/a (56 235) 7V. Chlordhenzene �/ (0.00100 <0.089 1 mg/L lb, n/a n/a n/a BV. Chloro& bromomethane X (0.00100 <0.089 1 mg/L lb. n/a n/a n/a (12448.1) Bv,ChlomethaneV x <0.00500 <0,443 1 mg/L lb, n/a n/a n/a (15.0.3) 10V, 2 -Chloro e1 owylEtherX <0.0500 <4.433 1 mg/L lb, n/a n/a n/a (110.75.6) llV, Chloroform�/ x 0 0248 2,199 1 mg/L lb, n/a n/a n/a (67.66.3) , 12V. Dichloro bromomethme 0.00422 0.374 1 mg/L lb. n/a n/a n/a 05.274) 13V. Dichbto dMuoromet" X <0,00500 <0.443 1 mg/L lb, n/a n/a n/a 65.11.8) 14V.1,1-DichloroX <0,00100 <0,089 1 mg/L lb, n/a n/a n/a elhane65.343) /\ W,1,2'Dkhb* V (0.00100 (0,089 1 mg/L lb. n/a n/a n/a ethane(107-06.2] A 16v.1,1-Dft* <0.00100 <0.089 1 mg/L lb. n/a n/a n/a ethylene 65.35.4] 17V.1,2-DirdboX x <0.00100 <0,089 1 mg/L lb, n/a n/a n/a propane 68.8744 18V.1,3•Ddbro• proPlleneX <0,00100 <0,089 1 mg/L lb. n/a n/a n/a (542.756) 19V.Ethpanzene V <0.00100 <0.089 1 mg/L lb. n/a n/a n/a (1001.4) 20V MethylX (0.00500 (0.443 1 mg/L lb. n/a n/a n/a Brormde 64.83.9) 21V.MeChhte <0.00250 <0,222 1 mg/L lb. n/a n/a n/a 6481.3) EPA Form 3510.2C (8.90) PAGE V4 CONTINUE ON PAGE V-5 OUTFALL 002 nnuriunen eon" nen[ if i EPA Form 35I(W (8.90) PAGE V•5 CONTINUE ON REVERSE 2, MARK W 3. EFFLUENT 4. UNITS 5 INTAKE (oprronal) 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c, LONG TERM AVRG, a. LONG TERM AND a b, a a. MAXIMUM DAILY VALUE (r( abble) VALUE (Javada6le) AVERAGE VALUE b, NO OF (1) CONCENTRATION (2) BASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS CAS NUMBER (iiavilahle) TESTING REQUIRED BELIEVED PRESENT BELIEVED ABSENT 0. ANALYSES a. CONCEN TRATION b. MASS ANALYSES GCIMS FRACTION -VOLATILE COMPOUNDS (caaraare4 22V,Metone x X <0.00500 <0.443 1 mg/L lb. n/a n/a n/a ChW6 p5-09.2) 23V.1,1,2,2- Te7achbroethane X <0.00100 <0.089 1 mg/L lb. n/a n/a n/a a 24V.Tebachlo* X <0.00100 (0.089 1 mg/L lb. n/a n/a n/a e8iylene (127.1&4) 25V,Tolma X <0.00500 (0.443 1 mg/L lb. n/a n/a n/a (ism) W. 1,2-Tre - mIoroe(hylene X <0.00100 <0.089 1 mg/L lb, n/a n/a n/a 156.6D5 27v.1,1,1•Trwh * V <0.00100 <0.089 1 mg/L lb. n/a n/a n/a ethane {71.556) A 28V,1,12-Tnchbra X (0.00100 <0.089 1 mg/L lb. n/a n/a n/a ethane (79 DO S) 2WTrdbv- X <0.00100 <0.089 1 mg/L lb. n/a n/a n/a etlrylene (79-016) 30V, Tnft* ilAwthane X <0.00500 (0.443 1 mg/L lb. n/a n/a n/a 5694 31V,Vinyl Chloide x X <0.00100 <0.089 1 mg/L lb. n/a n/a n/a URI -4) GCIMS FRACTION -ACID COMPOUNDS 1A.2 -Chlorophenol X <0.0100 <0.887 1 mg/L lb. n/a- n/a n/a (9557.8} /\ 2A 2,4.DdbD. X x <0.0100 <0.887 1 mg/L lb. n/a n/a n/a phenol (12H3.2) 3A.2,4•Dmet# X (0.0100 <0.887 1 mg/L lb. n/a n/a n/a phenol (10567-s) 4A.4,6•Din 0v X <0,0100 <0.887 1 mg/L lb. n/a n/a n/a Cresol (534.52.1) 5A.2,44)aidr . X <0.0100 <0.887 1 mg/L lb. n/a n/a n/a phenol (51.28-5) &k2-Ndrophenol X <0.0100 <0.887' 1 mg/L lb. n/a n/a n/a ISM 7A4.Nft heW X x <0.0100 <0.887 1 mg/L lb. n/a n/a n/a (107) 0-02. 6AP-CMoro.M• X <0.0100 <0.887 1 mg/L lb. n/a n/a n/a Cresol (59.50.7) 9A Pe"m X <0.0100 <0.887 1 mg/L lb. n/a n/a n/a phenol (87.86.5) IDA Phenol X <0.0100 <0.887 1 mg/L lb, n/a n/a n/a (108.95.2) 11A.2,4,6-TdchIo* V x <0.0100 <0.887 1 mg/L lb. n/a n/a n/a phenol(88*2) EPA Form 35I(W (8.90) PAGE V•5 CONTINUE ON REVERSE OUTFALL 002 WNIINUtUMM incrnvni 2. MARK'X7 3. EFFLUENT 4. UNITS 5 INTAKE(optionaf) 1, POLLUTANT b, MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a' b C. a. MAXIMUM DAILY VALUE (f oadable) VALUE (f aeadahle) d.NO.OF a.CONCEN AVERAGE VALUE b NO.OF (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2}MASS CAS NUMBER (fovadable) TESTING REQUIRED BELIEVED PRESENT BELIEVED ABSENT ANALYSES TRATION b MASS NALYSES GCIMS FRACTION - BASEINEUTRAL COMPOUNDS IB.Acenaphthene v <0.00100 <0.089 1 mg/L lb. n/a n/a n/a (83.32.9) / N 2B,AcenaphtAm�! x 40.00100 <0.089 1 mg/L lb, n/a n/a n/a (2D6.90) 3B, AnthraceneV x <0.00100 <0.089 1 mg/L lb. n/a n/a n/a (12012-n 48.Bmwine V <0.0100 40.887 1 mg/L lb. n/a n/a n/a (92.87.5) /� 5B. Benzo (a) AnthraceneX <0.00100 40,089 1 mg/L lb. n/a n/a n/a (56.E) BB Benzo (a)<0.00100 x <0.00100 <0,089 1 mg/L lb. n/a n/a n/a Pyrene (50.32.8) 76.3,4-Benzo- 8uorantheneX (0.00100 <0.089 1 mg/L lb. n/a n/a n/a (205.99.2) BB, Be"20�ln) X <0.00100 <0,089 1 mg/L lb, n/a n/a n/a Perylene (191.24.2) 9B. Benzo(k) Noranthene�( x <0.00100 <0,089 1 mg/L lb. n/a n/a n/a (207-06.9) (2-CIlIO/a- eUmxy)Methane�( x <0.0100 <0.887 1 mg/L lb, n/a n/a n/a (111.91.1) 11B Bis(Mllloro• erhvllEther�( <0,0100 <0.887 1 mg/L lb. n/a n/a n/a (I 1144-4) / � 12B,6o(2• Cbloroiraprorv� X 40.0100 40.887 1 mg/L lb, n/a n/a n/a Ether (102-8D.1) 138. Brs (2.lin0- bcgQPhthalete�( 40,00300 <0.266 1 mg/L lb. n/a n/a n/a (117-817) 148.4-Bromaphenyl Phenyl Ether�( <0,0100 <0,887 1 mg/L lb. n/a n/a n/a (101-55.3) / � 15B BUY Bew V <0.00300 <0.266 1 mg/L lb.n/a n/a n/a Phthalate(85�68.7) /\ 1613, 2 -Chloro - naphthalene X 40.00100 <0.089 1 mg/L lb. n/a n/a n/a (91.58.7) 178.4 Chloro- phony►Phenyl Ether X <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a (7005.72.3) /\ 18B.ChryseneV x (0.00100 <0.089 1 mg/L lb. n/a n/a n/a (218-01.9) 19B. abenzo (a,h) Anthracene�( (0.00100 <0.089 1 mg/L lb. n/a n/a n/a (53.70.3) / \ 208,1,2-Dchloro- v <0.00100 <0.089 1 mg/L lb. n/a n/a n/a benzene (9550.1) J\ 216,1,3-D4Imo. V 40.00100 <O.Q89 1 mg/L lb, n/a n/a n/a benzene (541.73.1) A EPA Form 3510.2C (8.90) PAGE V-6 WN i iNUt un rHL)t v -r OUTFALL 002 MIAITIAII ICA [DA11 DA!`_C \It EPA Form 3510-2C (8.9D) PAGE V-7 CONTINUE ON REVERSE 2. MARK *V 3 EFFLUENT 4. UNITS 5 INTAKE (oprrona() 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c, LONG TERM AVRG. a. LONG TERM AND a b a a. MAXIMUM DAILY VALUE (f available) VALUE (f milable) AVERAGE VALUE CAS NUMBER (f avmlable) TESTING REQUIRED BELIEVED PRESENT BELIEVED ABSENT d NO OF ANALYSES a. CONCEN• TRATION b, MASS b N0.OF ANALYSES (1) CONCENTRATION (2) MASS (t) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GCIMS FRACTION - BASEINEUTRAL COMPOUNDS (cononrred) 228,1,4.DkNoro-X <0.00100 <0.069 1 mg/L lb. n/a n/a n/a bemene (10646 7) 236.3,3oro-X <0.0100 <0.887 1 mg/L lb. n/a n/a n/a bemidine (91.94.1) 248( x <0.00300 <0.226 1 mg/L lb. n/a n/a n/a Phthalatelate(84.6G2) /� 258, Oanelhyl Phlhabte X <0.00300 <0.226 1 mg/L lb. n/a n/a n/a (131.11.3) 26B.Dr-N-Buh4 <0.00300 <0.226 1 mg/L lb. n/a n/a n/a Phthalate (84.74.2) 276.2,4-andro-V x <0.0100 <0.887 1 mg/L lb. n/a n/a n/a loluerre (121-14.2) 28B.2,6•Dmdro• V <0.0100 <0.887 1 mg/L lb, n/a n/a n/a toluene (606.2x2) J\ 29B. N" <0.00300 <0.226 1 mg/L lb. n/a n/a n/a Phlhabte (117.84-0) 30B 1,2-Qrphenyl- hydrazine(as Azo. <0,0100 <0.887 1 mg/L lb. n/a n/a n/a benzene) (122.66.7) 31B,FIuoranthene v <0.00100 <0.089 1 mg/L lb, n/a n/a n/a (2sw) A 32B.Fluorene�/ x <0.00100 <0,089 1 mg/L lb, n/a n/a n/a (86.737) 33B.Hexachloro- v <0.00100 <0.089 1 mg/L lb, n/a n/a n/a berizene (118.74.1) A 34B.ftachtaro- V <0.0100 <0.887 1 mg/L lb, n/a n/a n/a bu dene (87.68.3) 358. Hexachbro- cyclDpentadiene X <0.0100 <0,887 1 mg/L lb, n/a n/a n/a (474) 36BHexuNoro-V x <0.0100 <0,887 1 mg/L lb. n/a n/a n/a emane(67.72.1) d�ro (t2,3�Pyrene I.Z3. X <0.00100 <0.089 1 mg/L lb. n/a n/a n/a (193395) 388.IsophoroneV x <0.0100 <0.887 1 mg/L lb, n/a n/a n/a 08.59 1) 39B.Naphthalene X <0.00100 <0.089 1 mg/L lb. n/a n/a n/a (91-20-3) 40B.ti'ifrabenzene v <0.0100 <0.687 1 1 mg/L lb. n/a n/a n/a (9995.3) A 416 Ntlioa sodxnedrl4amine X <0.0100 <0.887 1 mg/L lb, n/a n/a n/a (62-75.9) 42B. N-Nbsodi- N�Propyamine X <0.0100 <0.887 1 mg/L]lb, n/a n/a n/a (62i46 EPA Form 3510-2C (8.9D) PAGE V-7 CONTINUE ON REVERSE - OUTFALL 002 n 1-1Irn -A,. rur rnAllr VVIY I IRUCV rnV1Yl II IL I nVly I 2. MARK'X' 3 EFFLUENT 4. UNITS 5. INTAKE (opuona� I.POLLUTANT AND CAS NUMBER (Ja�rilable) a TESTING REQUIRED b. BELIEVED PRESENT c BELIEVED ABSENT a MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE(ifamilable) d. NO OF ANALYSES a CONCEN TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO OF LYSES 11i CONCENTRATlDN (2) MASS fll CONCENTRATKNJ (2) MASS f1f CONCENTRATION (2) MASS (11 CONCENTRATION (2) MASS GCIMS FRACTION -BASEINEUTRAL COMPOUNDS (conomreO 43B. t0f* sodi0e*We�( <0.0100 <0.887 1 mg/L lb. n/a n/a n/a (66.30.6) 44B Phenanthrene�/ (85-01.8} x <0.00100 <0.089 1 mg/L lb. n/a n/a n/a 45B.PyremX (129-000) <0.00100 <0.089 1 mg/L lb, n/a n/a n/a 466.1,2,4 -Tri chlorowme (12082.1) X <0.0100 <0.887 1 mg/L lb. n/a n/a n/a GC/MS FRACTION - PESTICIDES 1P,AIddn<0.000050 (3al *2) X /` <0.005 1 mg/L lb. n/a n/a n/a (3 19646) X <0.000050 <0.005 1 mg/L lb. nta n/a n/a 3P.�BHCV (319.85.7) x <0.000050 <0.005 1 mg/L lb, n/a n/a n/a (58t89H X <0.000050 <0.005 1 mg/L lb. n/a n/a n/a 5P, i&BHC (318.868) x <0.000050 <0.005 1 mg/L lb. n/a n/a n/a 6P.CNordaneV (57-749) x <0.000050 <0.044 1 mg/L lb. n/a n/a n/a 7P.4,4'•DOT�( (5028 3) <0.000050 <0.005 1 mg/L lb. n/a n/a n/a 8P.4,4'-DDEx Q2.55.9} V (0.000050 <0.005 1 mg/L lb. n/a n/a n/a 9P,4,RADDV (12.54.6) x <0.000050 <0.005 1 mg/L lb, n/a n/a n/a 10P.Didddn�/ (6057.1) x <0,000050 <0.005 1 mg/L lb. n/a n/a n/a 11P.a-EnosWan (115.2!}7) v A <0.000050 <0.005 1 mg/L lb. n/a n/a n/a 12P.pEndosWan (115.284) V A <0.000050 <0.005 1 mg/L lb. n/a n/a n/a 13P. Endosu6an Surate�( <0.000050 <0.005 1 mg/L lb, n/a n/a n/a (1031-07-8) `\ 14P EndnnV (12.20 8) x <0.000050 <0.005 1 mg/L l -b. n/a n/a n/a 15P. Endrin AldehydeX <0.000050 <0.005 1 mg/L lb, n/a n/a n/a (7421.634) 16P.Hepfachla nom) �/ n (0.000050 <0.005 1 mg/L lb. n/a n/a n/a EPA Form 35102C (6.90) PAGE V•8 CON i INUE ON PAUL V-9 OUTFALL 002 EPA I.D. NUMBER (copy from Item I of Fom 1) OUTFALL NUMBER NCD 047 368 642 002 Wnunyw, i�vm, nv� ry 2. MARK'?(' 3 EFFLUENT 4. UNITS 5, INTAKE (opaona() 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND a b c a. MAXIMUM DAILY VALUE (i(ovadahle) VALUE (+f mmilahle) d. NO. CONCEN AVERAGE VALUE b N0.OF (11 CONCENTRATION (2) MASS (1) CONCWRATION (2)MA55 it) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS CAS NUMBER (�f aeodahle) TESTING REQUIRED BELIEVED PRESENT BELIEVED ABSENT ANALYSES TRATION b. MASS ANALYSE GCIMS FRACTION - PESTICIDES (continued) LIP IieplacMa ��� x <0.000050 <0.005 1 mg/L lb. n/a n/a n/a (102457.3) 18P.PCB-1242 V <0.000500 <0.044 1 mg/L lb. n/a n/a n/a (53469.21.9) A 19P PCB -1254 V <0.000500 <0.044 1 mg/L lb. n/a n/a n/a (11D97.59.1) A 1 20P PCB -1221V x <0.000500 <0.044 1 mg/L lb. n/a n/a n/a 0428 (111 2) 21P.PCB•1232�/ x <0.000500 <0.044 1 mg/L 1b. n/a n/a n/a (11141.165) 22P.PCB•1248�/ x <0.000500 <0.044 1 mg/L lb. n/a n/a n/a (12672.29 6•1260 (11096 82A (liW x �/ <0.000500 <0.044 1 mg/L lb, n/a n/a n/a 1<0.0005001 <0.044 1 mg/L lb. n/a n/a n/a (1267411.2) (126P-11.2)6 /� 25P. Toxaphene v<0.000500 <0.044 1 mg /L lb. n/a n/a n/a (8001.352) A EPA Form 3510-2C (8.90) PAGE V-9 Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Sludge Management Plan The Chemours Company — Fayetteville Works operates a Class 3 Wastewater Treatment Plant which is comprised of a single -stage activated sludge biological system. Excess sludge is removed from the system by diverting part of the Recycled Activated Sludge (at approximately 0.6% solids) from the clarifiers to a Dissolved Air Floatation ("DAF") unit for initial thickening. The sludge from the DAF (at approximately 3% solids) is transferred to a Mix Tank where polymer agents are added to enhance the dewatering process. The semi -thickened sludge is transferred from the Mix Tank to a Rotary Filter for final thickening, whereby the sludge is thickened to 6% solids. The thickened sludge is then transferred to a Screw Press where it is dewatered to a concentration of 9-20% solids. Following the Screw Press, the sludge is typically dried in steam heated dryers to a concentration of 40-55% solids. The dried sludge, or on occasion the dewatered sludge, is transported off-site to a commercial Subtitle D landfill. This sludge is currently being disposed of at the Waste Industries "Sampson County" Landfill near Roseboro, NC. In 2015, the average weekly quantity of generated wasted sludge was approximately 35,000 Ib. r Chemours Company — Fayetteville Works NPDES Permit No. NCO003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Current Facility Wastewater Management Process wastewater and stormwater from the various manufacturing areas are collected in the respective area sumps and ultimately conveyed via a gravity flow underground process sewer pipe to the facility's central wastewater treatment plant ("WWTP"). Sanitary sewage is conveyed via a separate underground sewer system to the WWTP. The permitted flowrate of the WWTP is 2.0 MGD, with an actual average flowrate of approximately 1.2 MGD. This untreated process wastewater is commingled in the WWTP Influent Sump where it is pumped to an 850,000 -gallon Equalization Basin. The Equalization Basin is mixed with two floating submerged mixers. Three floating surface aerators in the basin cool and aerate the incoming wastewater. A 175,000 -gallon Emergency Retention Tank is available for temporary storage of untreated wastewater which may need additional treatment or acclimation in the WWTP activated sludge process at a controlled rate that allows for proper biological treatment. Untreated wastewater from the Equalization Basin is normally pumped to a 250,000 -gallon Predigester Tank in which initial biological activity with the WWTP activated sludge begins. The Predigester Tank is aerated. The partially treated wastewater from the Predigester Tank is pumped to a 1,700,000 -gallon Aeration Tank. The Aeration Tank is the unit where the majority of the biological activity occurs. The Aeration Tank is aerated primarily by a diffused air system located in the bottom of the tank. The tank can have supplemental aeration via one or two floating Biomixers® that injects air through submerged rotors. The biologically treated wastewater is then sent to one of two in -ground clarifiers (119,000 gallons and 168,000 gallons respectively) or an above -ground 679,000 -gallon clarifier; with all clarifiers being operated in parallel. The clarified treated effluent is discharged to and through Outfall 001. The wasted activated sludge is sent to a Dissolved Air Floatation (DAF) unit, then to a 47,000 gallon Sludge Storage Tank, and finally to a Rotary Filter for thickening. The thickened sludge is dewatered in a Sludge Press, and can be dried in a steam -heated dryer for additional moisture removal. The dewatered sludge or dewatered/dried sludge is transported off-site to a commercial Subtitle D landfill. Non -contact process cooling water and non -process stormwater are conveyed via surface ditches. In addition, excess riverwater flow and Outfall 001 effluent are discharged directly to a surface ditch. The combined, total flow of water from the site is discharged through and monitored at Outfall 002. The discharged treated wastewater is conveyed via an underground pipe to the Cape Fear River, where it enters the river at a point approximately 1,500 feet upstream of the William O. Huske Lock & Dam (aka Lock & Dam No. 3). ✓ (if Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application - April 27, 2016 Current Facility Operating Conditions Chemours Fluoromonomers/Nafion® Membrane Manufacturing Area: The Chemours Company — Fayetteville Works' Fluoromonomers / Nafion® Membrane �t manufacturing area produces several final products. ChemoursTM Nafion® Membrane is a plastic 1 h al fu 1 cells ChemoursTM Nafion(& film used in the chloroalkali industry and in a ectroc emic e Polymer Dispersions are used in the fabrication of thin films and coating formulations for fuel cells membranes, catalyst coatings, sensors, and a variety of electrochemical applications. The HFPO monomer and the Vinyl Ether monomers are used to manufacture various fluorochemical products such as ChemoursTM Teflong. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. Chemours Polymer Processing Aid ("PPA" Manufacturing Area: The Chemours Company — Fayetteville Works' PPA manufacturing area produces a polymer processing aid. The processing aid produced in this unit is used in the manufacturing of '\fluoropolymers and fluorinated telomers,,but none of the produced processing aid is used at the k Fayetteville Works site. All process wastewater generated from this manufacturing facility is collected and shipped off-site for disposal. No process wastewater from this manufacturing facility 10 is discharged to the Chemours' wastewater treatment plant or to the Cape Fear River. Kuraray Butacite® Manufacturing Area: The Kuraray America Inc. — Fayetteville Plant's Butacite® manufacturing area produces two final products. KurarayTM Butacite® Interlayer plastic sheeting is the final product used in safety glass such as automobile windshields. Polyvinyl butyral resin is shipped off -.site as a transfer to other Kuraray locations for final processing. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. Kuraray SentryGlas® Manufacturing Area: The Kuraray America Inc. — Fayetteville Plant's SentryGlas@ manufacturing area produces �C?" KurarayTM SentryGlas® ionoplast interlayer laminate. SentryGlas(& interlayer is used for laminated safety glass in side, rear, and overhead automobile windows. It is also used in architectural applications desiring safety glass. There is no contact process wastewater generated from this manufacturing facility, therefore only sanitary waste from this area is treated in the Chemours' wastewater treatment plant. This manufacturing facility does discharge non -contact cooling water to a surface ditch and ultimately to Outfall 002. t DuPont Polyvinyl Fluoride ("PVF") Manufacturing Area: S� The DuPont Company — Fayetteville Works' PVF manufacturing area produces polyvinyl fluoride resin that is used in the electronics industry as a backing for photovoltaic cells, as well as many other uses. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. 0. Chemours Company — Fayetteville Works NPDES Permit No. NCO003573 ' Supplemental Information — Permit Renewal Application — April 27, 2016 Alternate Application Schedule for §316(b) of the Clean Water Act Final regulations implementing §316(b) of the Clean Water Act, which establish requirements for cooling water intake structures at existing facilities, were published in the Federal Register on August 15, 2014 with an effective date of October 14, 2014. The Chemours Company — Fayetteville Works ("Chemours") operates a cooling water intake structure on the Cape Fear River that is subject to this new Federal Cooling Water Intake Structure Rule ("the Rule") as codified in 40 CFR Part 125. The Rule requires' the owner or operator of a facility subject to Subpart J whose currently effective permit expires after July 14, 2018, to submit to the Director the information required in the applicable provisions of 40 CFR 122.21(r) when applying for a subsequent permit. Pursuant to 40 CFR 125.95(a)(2), the owner or operator of a facility subject to Part 125 Subpart J, "Requirements Applicable to Cooling Water Intake Structures for Existing Facilities Under Section 316(b) of the Clean Water Act", whose currently effective permit expires prior to July 14, 2018, may request the Director to establish an alternate schedule for the submission of the information required in 40 CFR 122.21(r) when applying for a subsequent (renewed) permit. On October 20, 2015, a letter was sent from Michael E. Johnson, Environmental Manager, Chemours Company — Fayetteville Works, to Dr. Sergei Chernikov, NCDEQ Division of Water Resources' NPDES Complex Permitting Unit, requesting an alternate schedule whereby all the materials required by the Rule will be submitted with the 2021 renewal application. On February 26, 2016, a letter was sent from S. Jay Zimmerman, Director, NCDEQ Division of Water Resources, to Michael E. Johnson, Environmental Manager, Chemours Company — Fayetteville Works, wherein the requested alternate schedule for submission of required CWIS information with the next permit renewal in 2021 was approved. A copy of Mr. Zimmerman's letter is attached to this application package. WaterResources ENVIRONMENTAL QUALITY February 26, 2016 Mr. Michael E. Johnson, P.E. Environmental Manager Chemours Company 22828 NC Highway 87 West Fayetteville, North Carolina 28306-7332 PAT MCCRORY Goremor DONALD R. VAN DER VAART Secretary S. JAY ZIMMERMAN Subject: Alternate CWA 316(b) Application Schedule NPDES Permit NC0003573 Fayetteville Works Bladen County Dear Mr. Johnson: Director The Clean Water Act Section 316(b) Cooling Water Intake Structure (CWIS) Final Rule outlines regulations and standards for the design and operation of cooling water intake structures under the NPDES program. Your current permit expires October 31, 2016, with renewal application due by May 4, 2016. Since your permit expires prior to July 14, 2018, under 40 CFR 125.95(a)(2), you have requested an alternative schedule for submission of CWIS permit application information required in 40 CFR Part 122.21( r). Based on Division review, an alternate schedule for submission of required CWIS information with the next permit renewal in 2021 is approved. This schedule date will be established in the 2016 permit renewal as well. Please note that facilities should begin to adapt their systems to comply with CWA Section 316(b) requirements. If you have any questions, please contact Tom Belnick with the NPDES Permitting Unit at 919-807-6390 or via email: tom.beinick@ncdenr.gov Sin c ely, -� S. Jay Zimmerman, P.G. Director, Division of Water Resources Cc: NPDES File Central File Ec: US EPA Region 4 US FWS NC WRC NC DWR/Fayetteville Region State of North Carolina I Environmental Quality I Water Resources 1617 Mail Service Center I Raleigh, Borth Carolina 27699-1617 919 707 9000 Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Elimination of Monitoring Requirement for PFOA In December 2002, the DuPont Company — Fayetteville Works began production of,ammonium perfluorooctanoate ("APFO"), which is the ammonium salt of perfluorooctanoic acid ("PFOA"). The renewed NPDES Permit No. NCO003573 that became effective on July 1, 2007, included a requirement for monthly monitoring of PFOA at Outfall 002. In 2006 the North Carolina Division of Water Quality ("DWQ"), in consultation with the North Carolina Division of Waste Management and the North Carolina Department of Health and Human Services, established an Interim Maximum Allowable Concentration ("IMAC") of 2 gg/L for PFOA, which was intended for the protection of groundwater as a source of drinking water. Following the issuance of this temporary health -based level, DWQ requested the assistance of the North Carolina Secretary's Science Advisory Board on Toxic Air Pollutants C NCSAB") in reviewing the toxicological literature on PFOA and recommending to DWQ an update of the IMAC for PFOA in groundwater. On August 10, 2012, the NCSAB, issued their recommendation to DWQ that the IMAC for PFOA in groundwater be reduced to 1 gg/L. During the 3 -year period from 2013 to 2015, the average monthly concentration of the final effluent discharge at Outfall 002 was 0.027 µg2 PFOA, with a maximum concentration of 0.088 gg/L PFOA. During the same period, the average monthly concentration of the incoming water from the Cape Fear River to the site, which is 99% of the effluent flow at Outfall 002, was 0.012 µg/L PFOA, with a maximum concentration of 0.031 gg/L PFOA. The production of APFO at this facility ceased in April 2013. The Chemours Company — Fayetteville Works (formerly the DuPont Company — FayetteviIle Works) is requesting that the monthly monitoring requirement for PFOA at Outfall 002 be eliminated in the renewed NPDES Permit No. NCO003573 for the following reasons: • APFO is no longer manufactured at this facility and has not been produced at the facility since April 2013; • APFO is not and has never been used as a process aid or a raw material at this facility; • The 3 -year average concentration at Outfall 002 was 0.027 gg/L PFOA, versus the current NC-DWR IMAC of 2 gg/L PFOA and the NCSAB recommended 1 gg/L PFOA; and • PFOA is present at low concentrations throughout the Cape Fear River basin, and that background level of PFOA in the Cape Fear River water contributes to the concentration measured at Outfall 002. �* Chemou s -Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Form 2C Permit Application — Bis(chloromethyl) ether Bis(chloromethyl) ether (CAS No. 542-88-1) was not analyzed for, and consequently was not reported on Page V4 of Form 2C for both Outfall 001 and Outfall 002. On November 28, 2014, the State of Oregon's Department of Environmental Quality ("ODEQ") issued a memorandum ('0' ') addressing the issue of analyzing for bis(chloromethyl) ether ("BCME"). In this memorandum, ODEQ states: " Based on the chemical's rapid hydrolysis in water, there are no analytical methods to measure BCME in water samples. Currently, the only analytical techniques available for this compound are for air samples. Region 10 EPA staff queried its Manchester Environmental Lab in Port Orchard, WA about potential, analytical methods for BCME. Staff at the lab confirmed that there is no EPA method for BCME because of its rapid degradation in water." Because of the lack of an'EPA approved analytical method for bis(chloromethyl) ether in a water matrix, ODEQ concluded: "Given its rapid hydrolysis in water, there are no recommended analytical methods for BCME in water samples. Because BCME is not quantifiable in wastewater, DEQ will not require permit holders to monitor or conduct reasonable potential analyses for this toxic pollutant." In an April 13, 2106, email from Tom Belnick, Supervisor of the NCDEQ Division of Water Resources' NPDES Complex Permitting Unit, to Michael Johnson, Environmental Manager, Chemours Company — Fayetteville Works, Mr. Belnick stated: "I checked with our DWR analytical lab, and they concur with Oregon's position and are not aware of any labs using even R&D methods for this analyte. Therefore, you can omit this parameter from your application renewal." Note l: http://www.deq.state.or.us/wq/standards/docs/toxics/BisChloromethylMemo.pdf