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HomeMy WebLinkAbout5. 2016 renewal applicationri !w 1%: Chemours The Chemours Company 910483-46810 Fiuoroproducts chemours com 22828 NC Highway 87 W Fayetteville, NC 28306-7332 CERTIFIED MAIL ARTICLE NUMBER 7002 0860 0006 9104 7828 RETURN RECEIPT REQUESTED Ms. Wren Thedford NCDEQ Division of Water Resources NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 276994617 SUBJECT: NPDES Permit Renewal Application NPDES Permit No. NC0003573 Dear Ms. Thedford: April 27, 2016 RECEIVED/NCDE6l/DWR MAY 0'8 1016 Water duality Permitting Section The Chemours Company —Fayetteville Works is requesting renewal of NPDES Wastewater Discharge Permit No. NC0003573. Since the issuance of the last permit, the ownership of this facility changed from the DuPont Company to The Chemours Company FC, LLC. Also, two separate companies, Kuraray America Inc. and the DuPont Company, are operating manufacturing units and are treating and discharging their wastewaters under the Chemours' NPDES Permit. Enclosed are the original and two copies of the General Information Form 1 (Form 3510-1), Wastewater Discharge Information Form 4%. (Form 3510-2C), and additional required supporting documentation for renewal of the subject permit by the NC Division of Water Resources. Included in the permit application are the following supplemental information documents: Sludge Management Plan, Current Facility Wastewater Management, Current Facility Operating Conditions, Alternate Application Schedule for §316(b) of the Clean Water Act, Elimination of Monitoring Requirement for PFOA, and the non -reporting of bis(chloromethyl) ether. If you have any questions or need additional information, please contact me at (910) 678-1155. Enclosures Rincerely please print or type in the unshaded areas only Form Approved OMB No 2040-0086 FORM EPA Form 3510-1 (8 U S. ENVIRONMENTAL PROTECTION AGENCY I EPA I D NUMBER 1 EPA GENERAL INFORMATION I T,,, I C Consolidated Permits Program F NCD 047 368 642 D GENERAL (Read the "General Instructions " before starling) 1 2 u 14 m LABEL ITEMSGENERAL INSTRUCTIONS If a preprinted label has been provided, affix it in the • designated space Review the information carefully, d any of 1t I. EPA I D NUMBER is incorrect, cross through it and enter the correct data in the appropriate fill -In area below Also, if any of the preprinted data is absent (the area to the left of the label space lists the III. FACILITY NAME PLEASE PLACE LABEL IN THIS SPACE informahon that should appear), please provide it in the proper fill-in area(s) below If the label is complete and correct, you V. FACILITY MAILING need not complete Items I, III, V, and VI (except VI -B which ADDRESS must be completed regardless) Complete all items d no label has been provided Refer to the instructions for detailed item VI FACILITY LOCATION descriptions and for the legal authorizations under which this data is collected II POLLUTANT CHARACTERISTICS INSTRUCTIONS Complete A through J to determine whether.you need to submit any permit application forms to the EPA If you answer yes" to any questions, you must submit this form and the supplemental form listed in the parenthesis following the question Mark OXO in the box in the third column if the supplemental form is attached If you answer'no' to each question, you need not submit any of these forms, You may answer "no' if your activity is excluded from permit requirements, see Section C of the Instructions See also, Section D of the Instructions for definitions of bold-faced terms Mark 4X' Mark •X' SPECIFIC QUESTIONS NO ATTACHED SPECIFIC QUESTIONS YES NO FORM ATTACHED A Is this facility a publicly owned treatment works which B Does or will this facility (either existing or proposed) results in a discharge to waters of the U.S? (FORM 2A) X include a concentrated animal feeding operation or X aquatic animal production facility which results in a 1e 17 1e discharge to waters of the U.S? (FORM 213) 19 20 21 C Is this a facility which currently results In discharges to�/ X �/ X D Is this a proposed facility (other than those described in A waters of the U.S, other than those described in A or B or B above) which will result in a discharge to waters of X above? (FORM 2C) the U.S.? (FORM 2D) 2z 23 24 25 1 le 1 27 E Does or will this facility treat, store, or dispose of F Do you or will you inject at this facility Industrial or hazardous wastes? (FORM 3) X municipal effluent below the lowermost stratum X containing, within one quarter mile of the well bore, underground sources of drinking water? (FORM 4) 2e 29 m 71 G Do you or will you inject at this facility any produced water H Do you or will you inject at this facility fluids for special or other fluids which are brought to the surface In processes such as mining of sulfur by the Frasch process, connection with conventional oil or natural gas production, X solution mining of minerals, In sliu combustion of fossil X inject fluids used for enhanced recovery of oil or natural fuel, or recovery of geothermal energy? (FORM 4) gas, or inject fluids for storage of liquid hydrocarbons? (FORM 4) s, 21 3a 39 I Is this facility a proposed stationary source which is one J Is this facility a proposed stationary source which is of the 28 industrial categories listed In the instructions and�/ which will emit 100 tons of any X NOT one of the 28 industrial categories listed In the X potentially per year air instructions and which will potentially emit 250 tons per pollutant regulated under the Clean Air Act and may affect I year of any air pollutant regulated under the Clean Air Act w 41 42 or be located in an attainment area? (FORM 5) and may affect or be located In an attainment area? 43 .. 45 (FORM 5) III NAME OF FACILITY ffSKIP C emours Company - Fayetteville Works - 1s - N 30 IV FACILITY CONTACT A NAME 8 TITLE (last, first, & title) B PHONE (area code 8r no) c Johnson, ichael, nvironmenta anager ( 1) 6 8-1 5 2 15 to 45 40 48 49 51 1 52. 55 V. FACILTY MAILING ADDRESS A STREET OR P O BOX c 3 22828 NC Highway 87 m 1e 45 B CITY OR TOWN C STATE D ZIP CODE c Fayetteville' C 2 3 6 q 15 IB b 41 42 47 51 VI. FACILITY LOCATION A STREET, ROUTE NO OR OTHER SPECIFIC IDENTIFIER c 218 8 NC ighway 8 5 15 1e l5 B COUNTY NAME Bladen 40 C CITY OR TOWN D STATE E ZIP CODE F COUNTY CODE (i%knoHn} F y t e i l C 2 3 6 3( Jc 6 15 18 40 41 421 47 51 57 154 -90) CONTINUE ON REVERSE COt7TINUED FROM THE FRONT Ur1 r01 m 3510-i VII SIC CODES (4 -digit, to order of rion A FIRST B SECOND 86 9 (spec) INDUSTRIAL ORGANIC CHEMICALS ; (1pect&) LAMINATED PLASTICS PLATE, SHEET, AND PROFILE SHAPES Ji72 3083 J19 10 IB 15 18 C THIRD D FOURTH c (Jpeco)UNSUPPORTED PLASTICS FILM AND SHEET c (1pec) PLASTIC MATERIALS AND RESINS 3 0 8 1 NOTE Kuraray Butaclte Butac>_teO and SentryGlaso sheeting 7 2 8 2 1 NOTE: DuPont PVF resin process units process units ' 1s 15 ,e 1s ,e 19 VIII OPERATOR INFORMATION A NAME B. Is the name listed In Item c s The Chemours Company FC, LLC VIII -A also the owner? 121 YES ❑ NO 5 +e ss 68 C. STATUS OF OPERATOR ('inner the appropriate letter into the anmiler box if "Otter, "spect(y) D PHONE (arra code R no ) F = FEDERAL (specify) S = STATE M = PUBLIC (other thanfederol or state) p 0=OTHER(specrfy) A (302) 773-1000 P=PRIVATE 5e +s s IS 19 ]i a 26 E STREET OR P O BOX 1 0 arket treet 35 55 F CITY OR TOWN IX INDIAN LAND I G STATE H ZIP CODE c B Wilmington Is thefaalitylocatedanlands� DE 19898 ❑ YES � NO 21NO is Ila n _ sl u X EXISTING ENVIRONMENTAL PERMITS A NPDES Dtscho estoSur%ace{Vaner D PSD (Air rfisvonsfromPro osedSources C T t T I 7 =NCO003573 g N y p INC Title V Permit 03735 15 1 16 1 17 lie ao +5 le1 17 lie 3 B UIC Under rotmdGr ecaon o%Fhads E OTHER s ea c T N/1 A T 1 W 0 3 431 (.rpeclfy) Land Application Permit g U I 9 15 15 1T Ie 00 15 1 18 1 +T 19 C RCRA Ha>ardots Was res E OTHER s ect c T I NCD047368642 C I T I I I I I I (Spec !&) s R 9 15 1 1s n Jim ao 15 le n le 301 XI MAP Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground Include all springs, rivers, and other surface water bodies in the map area. See instructions for precise requirements XII. NATURE OF BUSINESS (provide a brief description) The Chemours Company - Fayetteville Works (formerly the DuPont Company - Fayetteville Works) is a fluorinated chemicals manufacturer situated on'a 2,200 -acre property in northwestern Bladen County, NC. The Chemours' products produced at the facility include fluorinated monomers and fluorinated vinyl ethers, Nafion' membranes and dispersion, and fluoropolymer processing aids. Chemours operates two natural gas / fuel oil -fired boilers, which provides steam for the entire facility. Also located at this facility are two tenant companies: Kuraray America Inc. and the DuPont Company. Kuraray operates the Butacite° polyvinyl butyral (PVB) thermoplastic sheet and resin manufacturing unit and the SentryGlaaO ionoplast interlayer manufacturing unit. DuPont operates two polyvinyl fluoride (PVF) resin manufacturing units.- Chemours receives and treats all of the Kuraray and DuPont process wastewater, sanitary wastewater, and contact stormwater in the Chemours' owned and operated wastewater treatment plant, and discharges that treated wastewater through Outfall 001 under the Chemours' NPDES Wastewater Discharge Permit (Permit No. NC0003573). The Kuraray and DuPont non -contact cooling waters and stormwaters are discharged through Outfall 002 under the Chemours' NPDES Wastewater Discharge Permit, XIII CERTIFICATION (see instructions) I cerbfy under penalty of law that t have personally examined and am familiar with the informafion submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in the applicatio I believe that the information is true, accurate, and complete t am aware that there are significant penalties for submitting false information, including the possibility of f and imprisonment A. NAME 8 OFFICIAL TITLE (type orprint) BSI ATURE C DATE SIGNED Ellis H. McGaughy - Plant Manager 7 Zaj COMMENTS FOR OFFICIAL USE ONLY c C 15 1e s UNITED STATES 7UART QUADRANGLE STATE OF NORTH CAROLINA �z NORTH CAROLINA DEPARTMENT OF NATURAL E T AND COMMUNITY DEVELOPMENT CI DEPARTMENT OF THE INTERIOR 7.5 MINUTE SERIES (TOPOGRAPHIC) S� GEOLOGICAL SURVEY SFA SAM PAus 15' QUADRAWGE RALEIGH, N. C. 7805 '30 _05 L I $97 5n0 ' 52' 30' 88 !CEbDnARtNNE CREEK) BM -: f ,)! •l49 •, tx it / O"ItookN b or W* 4 S , 1 fit do" X59 eCgm ,� `,_� O . .Mill a •i _ i — POW T J I\ j ..k — u- --- s — I falls AP c 96 _ B t69 Tanks 0 ` O 0 3657 -'i- ---.( _ _ — - I .�-- -- mu! , ; I'o _ - (to a�347_ a� � - \ s. FACILITY LEGAL ' � - _ - - BOUNDARY ,tYI Hush 59 Dam No 3 Q a SM 1490 00 G Da'aw'a!' r - its t IM It no 3055 we j Za _� \ Hal, - - to Loa an M 145 Radio ' - - �� - _ ,i -_ • •� • It BitRAI. SCALE 1:24 000 5 f 1000 B 1000 2000 '.___ • MMES a _-�._`_ _ a - = Y.-�- � V•� ,b _ 9000 40M - 6000 WTO 7000 9 9000 10000 FELT• Q \ N t \ 1 • .6 0 _ KI— (pMvETFBi1 2 _1000 2a00 _ — •= , � , _ 1000 0 METERS _ - � CONTOUR INTERVAL 5 FEET ! NADON D GEODETIC VERTICAL DATUM OF 1929 • \ �' • Dus22 X52 Cam a Roadside _7 THIS MAP COMPLIES WITH NATIONAL MAP ACCURACY STANDARDS , BM t� -- 47' 30" L' i FOR SAIF BY U. 5. GEOLOGICAL SURVEY• DENVER• COLORADO 80225. OR RESTON• VIRGINIA 22092 ` . A FOLDtN DESCRIBING TOPOGRAPHIC MAPS AND SVM80LS IS AVAILABLE ON REQUEST CHEMOURS COMPANY - FAYETTEVILLE WORKS LOCATIONS OF INTAKE AND DISCHARGE STRUCTURES CHEMOURS COMPANY - FAYETTEVILLE WORKS LOCATIONS OF HALARDOUS WASTE MANAGEMENT FACILITIES ` t - m� . f ki 1 14 N Or + rI too #or /*. 0 s: 11g,. FIT` - # �, ` _ 1 _I PI F I L •-C `.- . - ' _.rte_'- - _ \\ i - ' r I IC. . 1 ( IL..�` ` _ 'cam- t •� MN I t.., y14 F 4r /-• y. fog I ,T If Igo go go WI Properly Owndary fj or ,� ¢ " ?sirs +�Syer ` _ 16 _ f 9 MMMT . . Please print or type in the unshaded areas only. EPA I.D. NUMBER (r.q?r,(ram Item I ql k;irr„ 1) NCD 047 368 642 I. OUTFALL LOCATION form Approved. OMB No. 2040-0086. Approval expires 3-31-98. FORM U.S. ENVIRONMENTAL PROTECTION AGENCY 2C Vol'EPA EXISTING MANUFACTURING,"COMMERCIAL, MINING AND SILVICULTURE OPERATIONS NPDES Consolidated Permits Program I. OUTFALL LOCATION For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. A OUTFALL NUMBER B. LATITUDE C. LONGITUDE (Inr) D. RECEIVING WATER 1 DEG 2. MIN. 3 SEC 1. DEG 2. MIN. 3 SEC. 001 34,00 50,00 22,93 -78.00 50.00 11.47 Cape Fear River 002 34600 50900 21,58 -78.00 49.00 25.70 Cape Fear River II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A Attach a line drawing showing the water flow through the facility- Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations, treatment units, and outfalls. If a water balance cannot be determined (e.g., lorcertain mining activities), provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of., (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if necessary. 1 OUT- 2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT FALL b AVERAGE FLOW b LIST CODES FROM NO. (I"r) a. OPERATION (list) (u,.lrrdr u,rra) a. DESCRIPTION TABLE 2C-1 C:+etrnurs Manufacturing ProcessesBIOLOGICAL WASTEWATER TRi!ATMENT ANT P 001 .''-51 gal/day e:uraray Butacite Mfg Process y, ,S'; gal/day (1) influent Scirc _ l:1:!'aray Sentry&_las Ffq 2roces£ G t2) Equalization with mixino and aera_17+ gal/day ) nc11.-:+c PVF D[far Processes 211,f54 gal/day t31 Emergency Retention 'tank: Vemin Ware:* Neutralized aegenetate 75, OGO gal/day '41 Pre-Ciaester Tank. _ Sanitary Sewer 10,000 cat/day Activated Sludge Aeration 'Tank. A Prccess Areas Stormwater 9J, 21< 051 Clarif I -jn i3 clarifiers in ca -all"'- gal/day 1 TOTAL INFLUENT TO WWTP 1,205,0?P qal/day Evaporation from WW1'P Oczrations .50,00.0 gal/day =10LOGIrAL SLUDGE ISu_IPS) MANAGTE$12:71' Evaporation from Sludoe Drying 11) Dissolved Air Flotation 19.943 gal/day Aare: ^oetent of Landfilled Sludge (2) Rotary Filter :,493 gal/day OUi':.. _. 0nl 'i'O'fi.:- EFP JEJrT 10133,451 gal/day (3) Sludoe Filter Press (41 SLui?e Steam. -Heated Dsyerr; (5) Dlsrosal a' Off-r;,t« Lanrif+ll , `. .::tfall 001 Treated Effluen' G02 1,113,45^ gal/day Non -contact fiver water [),05/,845 gall ua� Non contact filtered water 1,923,320 gal/day c,rmaater 219,50? gal/day pediment. Removal SO, UOD oat/day Poi ler Cm•iensate =. .. ��...� 32.10000 gal/day OJTFALL 002 TOIA�j EFf:.:!_7:'i' f11),133 gal/day Discharge to sulfate water feape Fear Riv.-I) . OFFICIAL USE ONLY (:!llurnr,¢ru+l.•/uA::..nb-Ern;xruv+• ) EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE CONTINUED FROM THE FRONT C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items 11-A or B intermittent or seasonal? ❑ YES (coelydRe d,r ledlolrrr{¢ ruble) 91 NO (gip n) Set tion 111) 3 FREOUENCY 4. FLOW a DAYS PER B TOTAL VOLUME 2 OPERATION(s) WEEK b MONTHS a FLOW RATE (tn uku/) (.Ik. i/r uiriY numj 1 OUTFALL CONTRIBUTING FLOW (sift iif) PER YEAR 1 LONGTERM 2 MAXIMUM 1 LONG TERM 2 MAXIMUM C DURATION NUMBER (h)#) (tor) arrr+teJ (.)arrliar:n,,l.) AVERAGE DAILY AVERAGE DAILY (Orth!") Ill. PRODUCTION A. Does an effluent guideline limitation promulgated by EPA, under Section 304 of the Clean Water Act apply to your facility? W] YES (c,mrplrle hent 111-1t) p NO (Co r„.1'rcuou lI ) B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)? ❑ YES (caug1lrrr hem 111-r) V1 NO (to toSection 11) C. If you answered "yes" to Item III -B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the applicable effluent guideline, and indicate the affected ouffalls. 1. AVERAGE DAILY PRODUCTION a OPERATIONPRODUCT, MATERIAL, ETC2 AFFECTED OUTFALLS . . a. QUANTITY PER DAY b UNITS OF MEASURE (Ir.rou{hrll uumherr) (�prr,li) IV. IMPROVEMENTS A Are you now required by any Federal. State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions ❑ YES (rouq,l.vr rhr lnBuvrge r(ihlr) © NO (co ro lnvu /I'-11) 1. IDENTIFICATION OF CONDITION, 2. AFFECTED OUTFALLS 3 BRIEF DESCRIPTION OF PROJECT 4. FINAL COMPLIANCE DATE AGREEMENT, ETC. a NO b SOURCE OF DISCHARGE a REQUIRED b. PROJECTED B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for construction ❑ MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3 EPA Form 3510-2C (8-90) PAGE 3 or a CONTINUE ON REVERSE CONTINUED FROM THE FRONT VII, BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? ©YES (ul.•urtlrthe n..rf.y<unld. r+h.-Iherrpugruw�h,lint) ❑NO(Cwar.leruwn17/!) The "North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure" is performed each quarter in accordance with the requirement of condition A(4) of the facility's NPDES Permit, The NCDEQ Division of Water Resources has copies of the Form AT -1 test results that were submitted with the Discharge Monitoring Reports during the period from February 2012 through February 2016. The quarterly chronic test performed during February 2012, failed for the ceriodaphnia dubia reproduction. The required monthly chronic tests performed in March and April 2012 both passed. No other toxicity test failures occurred during the five-year term of the current permit. VIII. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? ® YES (hstthe n,iux.urlln4.% and rilephtrnenuruberr)/.,rndprlhrr,rnruualr_rJhr. �NO(gataSrorom/A) tach. tthluburat,wrwr/rruthrluu') A NAME B. ADDRESS C. TELEPHONE O. POLLUTANTS ANALYZED (urea twit• it not (list) TBL 2401 West 5th Street 910-736-6190 Chemical Oxygen Demand Lumberton, NC 28256 (COD); Total Organic Carbon (TOC); Total Suspended Solids (TSS); Ammonia (as N); Color; Fecal Coliform; Fluoride; Nitrate -Nitrite las N); Nitrogen; Total Organic (as N); Oil and Grease; Total Phosphorus (as P); Sulfate (as SO4); Surfactants; Total Aluminum; Total Iron; Total Magnesium; Total Manganese; Part C Metals, Cyanide, and Total Phenols; Part C CC/Ms - volatile Compounds; Part C GC/MS - Acid Compounds; Part C GC/t9S - Base/Neutral Compounds; Part C GCIMS Fraction - Pesticides IX. CERTIFICATION I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. t am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A NAME ti OFFICIAL TITLE (npr ur prurt) B PHONE NO. (arra wilt, (v pit)) Ellis H. McGaughy - Plant Man er (910) 678-1224 C SIGN URE ,/ ri D DATE SIGNED EPA Form 3510-2C (8-90) PAGE 4 of 4 FDRM 2C ITEM IIA: LINE DRAWING WATER BALANCE (Revised 0411.2016( Flow Units: Gallons per Day Basis, (1) All Nanu(aCludngUnits operaling (2( Maximum 304ayaverage of measured flows (2013.2016( Sedime�l POTAEIE NaOCI Fitered Water FILTERED .� � OELgNFRALQED Wafer WATERSYSTEM 916000 ��ed �w . r�:TanLN�� hnpocess Smara'e Erplm NPDES PERMIT RENEWAL APPLICATION Chemours Company • Fayefleville Works NPDES PermR No. NCOOD973 Cape Fear River / CHEMWRS KURARAYAMEPoCAS KUAARAYAMERICAS DUPONT DUPONT FLUOROPRODVCT BVTACITE� SENTRYGIdVS� POLYNNYL POLYVINYL MANUFACTURING POLYVIKBUTYRAL LAatINATE FLUORIDE FLUORIDE PROCESSES MANUFACTURING MANUFACTURING i REMN RESIN PROCESS PROCESS PROCESS 11 PROCESS12 ACTIVATED CLAPoF4 SIUDGE 100 � CATKIN Enpaa 19,943 BIOSOLIDS DEWATERJ DofddSLwje 2493 DRYING 0 22i o 3 5 ; @ @ S u u u u U 8 a g m c e 0 0 0 U U U z z i 26,81J,13J OUTFALL 001 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY, You may report some or all of this mnformabon EPA LD NUMBER (cony from Ilem i of corm 1) on separate sheets (use the same formal) instead of completing these pages SEE INSTRUCTIONS, NCD 047 368 642 V, INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 24) PART A —You must provide the results of al least one analysis for every pollutant in this table, Complete one table for each oudall, See inshclions for additional details41111111. 3, UNITS 4INTAKE 2, EFFLUENT b. MAXIMUM 30 DAY VALUE a MAXIMUM DAILYVALUE (rfmnilable) 1. POLLUTANT (1) CONCENTRATK)N (2) MASS CONCENTRATION (2) MASS a. Biochemical Oxygen 71.0 675, 9 26, 8 207.1 Demand (BOD) b, Chemical Oxygen Demand (CDD) 32 ,1 313 , 2 C. Total Organic Carbon (�1 84,9 828,4 d, Total Suspended Solids (R 44,0 387,8 22,0 177,0 e.Ammonia (Qq h9 0,414 4.0 VALUE VALUE N0, (specrfi r%blank) (nprmno c. LONG TERM AVRG, VALUE a. LONG TERM (f marl°61e) AVERAGE VALUE d. NO, OF a. CONCEN b. NO.OF CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES 5.8 37,8 465 mg/L The n/a n/a n/a 1 I mg/L lb. n/a n/a I n/a 1 mg/L lb. n/a n/a n/a 9,8 54,6 465 mg/L lb, n/a n/aFnja 1 mg/L lb, n/a n/a n/a f, Flow VAI�� VALUE 1.627 1.133 0,907 1095 MGD MGD n/a n/a g Temperature VALUE VALUE VALUE VALUE (winter) 26.0 22.2 18.4 118 'C n/a n/a h, Temperature VALUE VALUE VALUE VALUE (.manner) 32,0 30,6 29,0 118Sjn/a n/a MINIMUM JMAXIMUM MINIMUM MAXIMUMi. pH 6,37 8,47 n/a n/a 374 PART B - Mark'X' in column 2•a for each pollutant you know or have reason to believe is present, Mark'X' in column 2-b for each pollutant you believe to be absent, If you mark column 2a for any pollutant which is limited either directly, or rndirecdp but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant For other pollutants for which you mark column 2s, you must provide quantblive data or an explanation of their presence in your discharge. Complete one IaNe for each outfall. See the instructions for additional details and requirements, 2, MARK'X' 3, EFFLUENT 4, UNITS S. INTAKE (nphona() 1, POLLUTANT b. MAXIMUM 30 DAY VALUE c LONG TERM AVRG. VALUE AND a, LONG TERM AVERAGE CAS N0, a, b a. MAXIMUM DAILY VALUE (/amdable) (m%mndn6le) VALUE BELIEVED BELIEVED (t) (1) (�) d. NO.OF a. CONCEN• b N0, OF r(fa�nda6le) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION 12) MASS CONCENTRATION (2)MASS ANALYSES TRATION b, MASS CONCENTRATION (2)MASS ANALYSES a,Br,o.mide �/1.9) b CNome, Total �/ 0.03 0 , 3 Residual /� 1 mg/L lb. GCO X 10 n/a 1 PCU n/a n/a n/a n/a d. Fecal Coliform est, 2 n/a 1 col/dL n/a n/a n/a n/a e, Fluonde (16984.48.6) 170 1659 1 mg/L lb, n/a n/a n/a t Nilrale•Nihrte (asM 0365 0.6 1 mg/L lb, n/a n/a n/a EPA Form 3510.2C (8.99) PAGE Val CONTINUE ON REVERSE OUTFALL 001 ITEM V -B CONTINUED FROM FRONT EPA Form 35102C (8-90 2. MARK'X' 3. EFFLUENT 4, UNITS 5. INTAKE (opnonoO 1, POLLUTANT b. MAXIMUM 30 DAY VALUE c, LONGTERM AVRG, VALUE a, LONG TERM AND a, b a, MAXIMUM DAILY VALUE (riandable) (cJmadable) AVERAGE VALUE CAS NO, BELIEVED BELIEVED d, NO, OF a. CONCEN- b, N0, OF (1) (1) (1) (Javmlable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS (1) CONCENTRATION (2) MASS ANALYSES g. Nitrogen, Total Organie(a; x 1.016 9.9 1 mg/L The n/a n/a n/a M I I I I h.Oil andX Grease <5,6 <50.0 5,2 42,5 0,26 137 36 mg/L lb, n/a n/a n/a i Phosphorus (as P), Toler X 12,4 121,0 1 mg/L The n/a n/a n/a p123.14-0) 1. Radroac6wty (1) Alpha, Told X (2) Bela, Total (3) Radium, Total (4) Radium 226, Total k, Sulfate (0$804)X (14808.1943) 1083 10568 1 mg/L lb, n/a n/a n/a I, Sulfde m. Sulfite (ru801) X (14265.45-3) / n.Sudaclanls X 3.07 30,0 1 mg/L lb, n/a n/a n/a o. Aluminum, Total (1428.905) 0.19 1.9 1 mg/L lb, n/a n/a n/a p. Banum, Told (1440393) q, Boron, Told Q44NH) r, Cobalt, Told (7440484) so lion, Told 04394396) x 0,28 2,7 1 mg/L lb, n/a n/a n/a t. Magnesium, Total 2,26 22.1 1 mg/L lbt n/a n/a n/a (1439954) u. Molybdenum, Total p43998.7) v, Manganese, Total�( <0,005 <0.049 1 mg/L lbs n/a n/a n/a Q439.96.5) / ` w, Tin, Total (144031.5) x, Tdanium, Total (744032) ) PAGE V•2 CONTINUE ON PAGE V-3 OUTFALL 001 EPA LD, NUMBER (cony fram Item 1 offonn 1)=OUTFALLNUMBERCONTINUED FROM PAGE 3 OF FORM 2•C NCD 047 368 642 PART C • If you are a primary industry and this outfall contains process wastewater, refer to Table 2o-2 in the instructions to determine which of the GCIMS fractions you must test for, Mark 'X' in column 2a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark 'X' in column 2•b for each pollutant you know or have reason to believe is present Mark 'X' in column 2-c for each pollutant you believe is absent If you mark column 2a for any pollutant, you must provide the results of at least one one srs for that pollulant II you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant If you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolem, acrylondrde, 2,4 dinrhophend, or 2•melhylA, 6 dindrophenol, you must provide the results of at least one anatysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 1D0 ppb or greater. Otherwise, for polutants for which you mark column 2b, you must either submit at least one analysis or bnefly describe the reasons the pollutant Is expected to be discharged, Note that there are 7 pages to this pad, please review each carefully Complete one table (all 7 pages) for each outiall See instructions for additional details and requirements, 2, MARK AX3, EFFLUENT 4, UNITS 5, INTAKE (opnom 1. POLLUTANT b MAXIMUM 3D DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND :REQUIRIEDPRESENT b c a. MAXIMUM DAILY VALUE (fmndable) VALUE (rf madable) AVERAGE VALUE CAS NUMBER EVED BELIEVED (�) (�) (1) d. NO* OF a. CONCEN- (1) b NO.OF kj (ifmadable) ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATm (2)MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS ��at�)y,Tdd X <0,002 <0,020 1 mg/L 1b. n/a n/a n/a 2M,Arseno,Told /\ <0.005 <0.049 1 m L lb, ria ria ri a p440*2) g/ / / / U44MIR7) ,Totd V <0.001 <0,010 1 mg/L lb, n/a n/a n/a 4M,Ca mi m, Total X <0,002 <0,020 1 mg/L lb, n/a n/a n/a X 070 010 0 070 0 010 0 otalaomum, T .,., 0,004 0,034 4 Total (1440-07.3) 0mg/L lb. n/a n/a n/a Copper, V 0.007 0,050 0,007 0,050 0,0055 0,047 4 mg/L lbo n/a n/a n/a X 1M. Lead, Total <0,003 <0,029 1 m L lb, n/a n/a n/a p439.92.1) g/ BM Mercury, Total <0,0002 <0, 002 1 p439.97.6) rig/L lb, n/a n/a n/a 9M. Nickel, Total 0,012 0,090 0.012 0,090 0,0083 0,065 4 m L lb, n/a n a n a (7441}02.0) 9/ / / 10M.Selenium, <0.005 <0,049 1 m L lb, n/a n/a ri a Total (776249.2) g/ / IM0 42 iiv4jTotal V <0,002 <0.020 1 mg/L lb, n/a n/a n/a 12M Thallium, /� <0,005 <0.049 1 Total(7440.2H) mg/L lba n/a n/a n/a (74 4MR)otal 0.042 0390 0.042 00390 0.0343 0.286 4 mg/L lb, n/a n/a n/a 14M. Cyanide, l <0, 005 <0, 1 m 049 Total (67=124) %\ g/L lb, n/a n/a n/a 15M6 Phenols, <0.0400 <0,390 1 Total X mg/L lb. n/a n/a n/a DIOXIN 2,3,1,&Tetra•\ / BESCRIBE RESULTS Not applicable chlorodiemo•P• /X\ Doxin (1764-01.6) EPA Form 35104C (8.90) PAGE V•3 CONTINUE ON REVERSE OUTFALL 001 CONTINUED FROM THE FRONT 2. MARK 'X 3 EFFLUENT 4, UNITS 5. INTAKE (optional 1, POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND am b c a, MAXIMUM DAILY VALUE (fmntlable) VALUE (f mbrlable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (t) (1) (1) d, NO.OF a, CONCEN- (1) b, NO OF (f Varlable) REQUIRED PRESENT ABSENT I CONCENTRATION (2) NAS8 CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b, MASS CONCENTRATIDN (2) MASS ANALYSES GCIMS FRACTION VOLATILE COMPOUNDS IV, Accrolem <0,0500 <0.488 1 mg/L lb. n/a n/a n/a 2V. Acrylondrde (10713.1) (0.0100 (0.096 1 mg/L lb, n/a n/a n/a 3V. Benzene�/ 81.43.2) ^ <0,00100 (0.10 1 mg/L lb, n/a n/a n/a 4V, &s (Chloro• x methiY EUter Not Req ired per NCDWR NPDES Permitt'g Unit (5428&1) 5 , Btomof Drm X c0 , 00100 <0.10 1 mg/L lb. n/a n/a n/a sv Carbon ` , Tetrachloride X c0.00100 <0.10 1 mg/L lb, n/a n/a n/a (%n� 7V. C�� enzene V <0,00100 <0.10 1 mg/L lb. n/a n/a n/a 8V. ChbW" x /�bromomethane <0.00100 c0,10 1 mg/L lb. n/a n/a n/a (12448.1) 9V. Chloroelhane j7) <0.00500 (0.049 1 mg/L The n/a n/a n/a 10V, 2 -Chloro• ethftnyl Ether (0.0500 (0,488 1 mg/L lb. n/a n/a n/a (110w7&8) 11V. Chloroform (67.663)<0.00500 (0,049 1 mg/L lb, n/a n/a n/a 12V. Dichloro• bromomethane <0.00100 <0.10 1 mg/L lb, n/a n/a n/a Q&274) 13V, Uchloro- di0uoromethane <0.00500 <0.049 1 mg/L lb, n/a n/a n/a (1541.8) 14V.1610chloro- 10 1 0 00100 <0. <. m L lb, ri a ri a ri elhene(75�43) 9/ a / / / 15V.1,2wDichloro- <0.00100 <0,10 1 m L lb. ria n/a n/a elhane (107462) g/ / 1W IJ&Dichloro• <0.00100 <0.10 1 L lb. ria ria ri a ethylene p5.35-0)/ / / / 17V.1,2-Dkldoro- propane q8,87&5) (0,00100 (0,10 1 mq/L lbt n/a n/a n/a 118V,1,3•Dichlao- x propylene <0,00100 <0.10 1 mg/L lb, n/a n/a n/a (542.75.6) 19VV E' ylbenzene V (0.00100 <0.10 1 mg/L lb, n/a n/a n/a x 20VMe1hylX c0000500 <0.049 BronadeU483.9) 1 mg/L lbs n/a n/a n/a 2IV, Melhyl <0.00250 <0.024 1 mg/L lb,, n/a n/a n/a Chloride (7487.3) EPA Form 3510.2C (8-90) PAGE V4 CONTINUE ON PAGE Vm5 OUTFALL 001 CONTINUED FROM PAGE V4 2, MARK OX3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1 POLLUTANT b. MAXIMUM 30 DAYVALUEJ C, LONG TERM AVRG. a. LONG TERM AND :TESTING . b c a MAXIMUM DAILY VALUE (�ifmadable) VALUE(Jrnaulable) AVERAGE VALUE CAS NUMBER BELIEVED BELIEVED 1► 1 d. NO.OF a CONCEN b. NO.OF (i/mntlable) IRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (1)MASS CONCENTRATION (2►MASS ANALYSES TRATION b MASS CONCENTRATION 12l MASS ANALYSES GC/MS FRACTION VOLATILE COMPOUNDS (eonmee4 22V,Mefhylene v <0,00500 <0,049 Chlodde(/5,W) 1 mg/L lb, n/a n/a n/a 23V,1,1,2,2- ` , TeVachloroelhane X <0,00100 (0,010 1 mg/L lb, n/a n/a n/a 834• 24V.Telrachloro- v(0,00100 (0.010 elhylene(121.184) 1 mg/L lb, n/a n/a n/a (1 Toluene <0,00500 <0,049 / (108.88.3) 1 mg/L lb, n/a n/a n a 26V,1,2•Trans• DdloroelhyleneX <0,00100 (0.010 1 mg/L lb, n/a n/a n/a 156.60.5 27V, 1,1,1-Trkhbro4 <0.00100 <0,010 efhane(11556) 1 mg/L lb. n/a n/a n/a 28V 1,1,2-Tnchloro X <0.00100 <0,010 1 mg/L The n/a n/a n/a 29VT6chloro- <00 q 00100 <0,010 1 m /L The n/a n/a n/a done (19.01.6) 30V, Tnchloro• \ / flooromethane /j(\ <0,00500 <0,049 1 mg/L The n/a n/a n/a 54 95-oi4ylChlodde V <0,00100 <0,010 1 mg/L lb, n/a n/a n/a GC/MS FRACTION =ACID COMPOUNDS 1A.2•Chlorophenol <0.0100 <0.098 (95.51.8) 1 mg/L lb, n/a n/a n/a 2A.214•achbro- X <0.0100 (0.098 / / phenol (120.83.2) /\ 1 mg/L lb. n a n a n/a 3A.2,4hpl• phenol(166(10567.9) 1 mq/ <0.0100 <0.098 L lbo n/a n/a n/a 4A416•Dhivo•0• <0.0100 <0,098 Cresol(M52.1) 1 mg/L lb. n/a n/a n/a 5A ol(51 8w <0,0100 <0,098 1 m L lb, n a n/a n/a phenol (51•z6.5) q/ / 6A 2•Ndrophenol <0.0100 0100 <0 , 098 / (88.155) 1 mg/L lb, n a n/a n/ a (�2�phend X (0,0100 (0.098 1 mg/L lbs n/a En/an/a n/a Cr ol(%ro•M• v <0.0100 <0,098 / Cresol (59.50.7) ^ 1 mg/L lb, n a 9A Penfaehloro- <0,0100 <0.098 1 phenol(81.86.5) mg/L lb. n/a n/a n/a 10A.Phenol <0,0100 <0,098 1 m L lb, n a n/a n (108.952) 9/ a / / IIA2,4,6•Trdboo (0,0100 <0,098 1 . m L 71bn a n/a n/a phend (88-052) q// EPA Form 3510.2C (8.90) PAGE V-5 CONTINUE ON REVERSE OUTFALL 001 CONTINUED FROM THE FRONT EPA Form 3510o 2. MARK •X' 3. EFFLUENT 4, UNITS 5. INTAKE (oprmmwl) 1 POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG, poem a, LONG TERM AND a. b c. a MAXIMUM DAILY VALUE (f mamlahleJ VALUE (Jmnmlahle) AVERAGE VALUE CAS NUMBER TESTING BEl1EVED BELIEVED d, NO.OF a, CONCEN- NO, OF (i)1 (1) eeeeeeeeb (rfmndahle) REQUIRED PRESENT ABSENT CONCENTRATION (2)KASS CONCENTRATION (2)MASS I CONCENTRATION 1 (2)MASS ANALYSES TRATION b. MASS (1) I CONCENTRATION (2)MASS ANALYSES lommom GCIMS FRACTION - BASEINEUTRAL COMPOUNDS 1B.Acenmphthene (e?•32•e) <0.00100 <0.01 1 m L gl lb, n a I n a l n l a 28.Acenaphlylene (299")38. V (0.00100 <0.01 1 mg/L lbs n/a n/a n/a (12x127) X <0.00100 (0.01 1 mg/L The n/a n/a n/a (�B..BBendine V /� <0,0100 (0.098 1 mg/L lb. n/a n/a n/a 5B, Benzo (a) Anthracene X <0.00100 <0.01 1 mg/L lb. n/a n/a n/a (%55.3) 6BBenzo (a) Pyrene (5x32.8) <0.00100 (0,01 1 m L g/ lb. n a / n a / n a / 7B, 3,4-Benzo- Ouoranihene <0.00100 <0.01 1 mg/L lbo n/a n/a n/a (205.99.2) 89. Benzollli) Pe*e (191.24.2) x <0.00100 <0.01 1 ONE m L 9/ lb, n a / n a / ri a / 9B Bew (k) %rentheneX (0.00100 <0.01 1 mg/L lb, n/a n/a n/a (tot oB s) 10B, Bis erhoq) McNne�( x <0.0100 <0.098 1 mg/L The n/a n/a n/a (111.91.1) I I& &s (1-Chlomw eAg1 (111 .44.4)444) <0.0100 <0.098 1 mg/ L lb, n/a n/a n/ a 1213. Bis (1• Chlaomproprlj <0.0100 <0,098 1 m g/L lb, n/a n / a n/a Elher(102*11) 13B, Bis (14ihrl• henlj Phlhalale x <0.00300 <0.029 1 mg/L The n/a n/a n/a (11181.7) 14B 4•Bromopheryl Phenyl Ether (101.55.3) /\ <0.0100 <0.098 1 mg/L lb, n/a n/a n/a 15BOBuy Benzyl Phlhalale(85.68.7) /\ X <0.00300 <0.029 1 mg/L lb. n/a n/a n/a 165.2•Chloro- naphthalene�( <0,00100 <0.01 1 mg/L lb, n/a n/a n/a (91.58.7) 118, 4•Chloro• phenyl Phenyl Ether (1005.12.3) <0.0100 <0.098 1 mg/L lba n/a n/a n/a 18B Chrysene (218.01.9) <0.00100 <0.01 1 m L g/ lb, n a / n a / n a / 19B Dbenzo(o,h) Anthracene (53.7x3) <0,00100 <0,01 1 m L 9/ lb, n/a n a / n/a 20B.1,2•Drchloro• benzene (95.5x1)/ <0.00100 <0,01 1 L lb, n/a n a / n/a 21 Be1,3•Drchtoro• benzene(541.73.1) <0.00100 <0.01 1 mg/ L lb. n a / n a n a 2C (6.90) PAGE V-6 CONTINUE ON PAGE V•7 OUTFALL 001 CONTINUED FROM PAGE V•6 2. MARK "X' 3 EFFLUENT 4. UNITS 5 INTAKE (opnowo 1. POLLUTANT b, MAXIMUM 30 DAYVALUE c, LONG TERM AVRG. a. LONG TERM AND a. b, c a. MAXIMUM DAILY VALUE (f mailai VALUE (f mailable) AVERAGE VALUE CAS NUMBER TESTING[BELIEVED BELIEVED t�d. NO.OF a. CONCEN• b. NO.OF (farodable) REQUIREDSENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)h1AS5 CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES GCIMS FRACTION-BASEINEUTRAL COMPOUNDS (cononuA 228. 1,400ro- <0, 00100 <0, 001 1 m L lb. n a n a n benzene (106-06.7) 9/ a / / / 23B.3,3•DKIdoro- V <0.0100 <0.098 1 m benzidine(91.941) g/L Be n/a n/a n/a 248, aelhyl Phlhalale(84662) (0,00300 (0.029 1 mg/L The n/a n/a n/a 158. Dimethyl ( 19iax a113) <0.00300 (0.029 1 mg/L lb, n/a n/a n/a 26B. DFN*Bble(84.7 <0.00300 <0.029 1 m L lb, n/a n/a n/a memo MENOMINEE Phlhalale (84742) g/ 278.2,4Dindro- <0,0100 <0.098 1 m L lb, n/a n/a n/a Wene (121142) g/ 6aniUo- 16me(60620.2) 1 m9/ <0.0100 <0,098 L lb, n/a n/a n/a oh,ene 29BODi•N•Ocy g/ <0.00300 <0,029 1 m L lb. n/a n/a n/a Phlh�ale (11784 0) 30B.1,24phenyl• hydrazme(as Azo- L lb, n/a n/a n <0.0100 <0.098 1 m a benzene) (12266.7) g/ / 31B Flww mene x <0,00100 <0.001 1 mg/L lbs n/a n/a n/a ( `73,T�rene V <0.00100 <0.001 1 mg/L lba n/a n/a n/a woo 3313.Hexacftr <0.00100 (0.001 1 m L lb. n/a n a n/a benzene (116741) g/ / 34B,Hexachloro- <0.0100 <0,098 1 m L lb, n/a n/a n/a butadiene (87.663) g/ dome 358. Hexachloro- cyclopenladiene <0,0100 <0.098 1 mg/L lb, n/a n/a n/a (77.474) libellee 36BHexachbro- (0.0100 <0,098 1 m L lb, n a n a n ethane (61.72.1) 9/ a / / / 37B.Indeno (1,2,30 Pyrene <0.00100 <0.001 1 mg/L lb, n/a n/a n/a (193.39.5) 38BIs1oorone X <0,0100 <0,098 1 mg/L lb, n/a n/a n/a x 39thNene <0,00100 <0,001 1 m L lb, n a n a n (91.20.3)40*3) g/ a / / / 408,NVobenzene�/ <0,0100 <0.098 1 mg/L lb, n/a n/a n/a 41B.N•NR* /� 'odl5,9ylam�ne (0,0100 (0.098 1 mg/L lb, n/a n/a n/a 42B. N•Ndrosodi• N•Prop famine X <0.0100 (0.098 1 mg/L The n/a (621,64.7) /\ EPA form 3510.2C (690) PAGE V•7 CONTINUE ON REVERSE OUTFALL 001 CONTINUED FROM THE FRONT 2 MARK'X' 3 EFFLUENT 4. UNITS 5 INTAKE (opaono� 1. POLLUTANT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG, a. LONG TERM AND a b c pMUMDAItYVAIUE (Jmnrlo6le) VALUE(fnvarinM1le) AVERAGEVALUE CAS NUMBER TESTING BEl1EVED BELIEVED1) (1) (1)d,N0,OF a,CONCEN (1) b. NO.OF (f mniloble) REQUIRED PRESENT ABSENT TRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSESI TRATION b. MASS CONCENTRATION (2) LASS ANALYSES GCIMS FRACTION— BASEINEUTRAL COMPOUNDS (connnue4 43B, Wro, sodiphenylamineX (0.0100 (0.098 1 mg/L lb. n/a n/a n/a (86. H) 44B Phenamhrene <0,00100 <0.001 1 mg/L lb, n/a n/a n/a (Ole X <0,00100 <0.001 1 mg/L lb, n/a n/a n/a 46B.1,2,4•TrF chlorobenzene <0.0100 (0,098 1 L lb. n a n/a n a (%82.1) X m9/ / / GC/MS FRACTION= PESTICIDES � 2) X <0.000050 <5e-4 1 mg/L lb, n/a n/a n/a 9 19a•BB4•H6) X <0,000050 <5e-4 1 mg/L The n/a n/a n/a 3P,pBHc V <0,000050 <5e-4 1 / / mg/L lb, n/a n a n a 4P pBHCV <0.000050 <5e-4 1 mg/L lb, n/a n/a n/a ( X ) (3i &B x <0.000050 <5e-4 1 mg/L lb, n/a n/a n/a 6P,ChWdane <0,000050 <0.005 1 L lb. n/a n a n a (57.74.9) mg/ / / (%�3) X <0,000050 <5e-4 1 mg/L lb, n/a n/a n/a BP,4,49)DDE X <0,000050 <5e-4 1 mg/L lbo n/a n/a n/a 24�41WI) V <0.000050 <5e-4 1 mg/L lb, n/a n/a n/a IOP,Dieldnn /� <0.000050 <5e-4 1 (64 M) X mg/L lba n/a n/a n/a (11.aEn sultan �/ <0.000050 <5e-4 1 mg/L lb. n/a n/a n/a 12P, �E*sulfan<0 , 000050 <5e-4 1 (115297) X mg/L lb, n/a n/a n/a 13P Endosulfan Sulfate <0.000050 <5e-4 1 mg/L lb, n/a n/a n/a (1031-07.8) (72.20•B)nn x(0.000050 <5e-4 1 mg/L lb, n/a n/a n/a 15P, Endnn Aldehyde �( <0,000050 <5e-4 1 mg/L lbs n/a n/a n/a (7421.934) 16P, Heptachlor �/ n (0.000050 <5e-4 1 mg/L lb, n/a n/a n/a EPA Form 3510.2C (8.90) PAGE V•8 CONTINUE ON PAGE V•9 OUTFALL 001 EPA I D. NUMBER (cwpvfmmltem I of form I) OUTFALL NUMBER CONTINUED FROM PAGE V•8 NCD 047 368 642 001 2. MARK "X' 3, EFFLUENT 4 UNITS 5. INTAKE (optional) 1, POLLUTANT b MAXIMUM 30 DAY VALUE c. LONG TERM AVRG, a, LONG TERM AND e, D, c a. MAXIMUM DAILY VALUE (f available) VALUE (f mridable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (1) (t)(1) d, N0, OF a. CONCEN (1) b, NO, OF (f mudoNe) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION I b, MASS CONCENTRATION (2) MASS NALYSE: GCIMS FRACTION - PESTICIDES (canonneA) ttP, Heptachlor x Epude <0.000050 <5e-4 1 mg/L The n/a n/a n/a (1024.57.3) 18P.PCIM242 <0.000500 <0.005 1 (5346921.9) mg/L lb, n/a n/a n/a 1C l) g/ (110971097.69.1) <0.000500 <0.005 1 m L lb, n/a n/a n/a (11146,2) <0.000500 <0.005 1 m L The n/a n/a n/a (ttto4-2x•21 g/ 21P41416s 232 <0. 000500 <0. 005 1 / / / (tt141.16.5) /� mg/L lb. n a n a n a 22P. PCB•l248 (12672.296) X <0,000500 <0.005 1 mg/L The n/a n/a n/a 23P, PC&1260 (11096.82-5) X <0.000500 <0.005 1 mg/L lb. n/a n/a n/a 24P, PCB -1016 (12674.1t•2) X <0.000500 <04005 1 mg/L lbo n/a n/a n/a 25P, Toxaphene \ / (80015.2)<0.000500 <0.000500 <0.005 1 mg/L The n/a n/a n/a EPA Form 3510.2C (8.90) PAGE V-9 OUTFALL 002 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I,D, NUMBER (copvfrom Item 1 oJform I) on separate sheets (use the same forma() instead of completing these pages. NCD 047 368 642 SEE INSTRUCTIONS, OUTFALL N0. V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2•C) oos PART A —You must provide the results of at least one anatysis for every pollutant in this table. Complete one table for each outfall, See instructions for additional details, 3. UNITS 4. INTAKE 2, EFFLUENT (sped if blank) (ophonoo b. MAXIMUM 30 DAY VALUE c LONGTERM AVRG. VALUE a, LONG TERM a, MAXIMUM DAILY VALUE (fmndable) (1faradable) AVERAGEVALUE d, NO OF a. CONCEN• (t) b. NO, OF 1. POLLUTANT CONCENTRATION (2) MASS CONCENTRATION (2) MASS (t) CONCENTRATION (2) MASS ANALYSES TRATION b, MASS CONCENTRATION (2) MASS ANALYSES a, Biochemical Oxygen 33 9 762 ,1 3 e9 762,1 1, 4 185 s7 12 mg/L The n/a n/a n/a Demand (80D) b. Chemical Oxygen 33,7 4898 33,7 4898 4,37 458,6 12 mg/L lb, n/a n/a n/a Demand (COD) (To;lOrganic Carbon 1248 1135 1 mg/L lb. n/a n/a n/a d, Total Suspended Solids (M 10.6 939.7 1 mg/L lb. n/a n/a n/a e. Ammonia (asM 0.410 36.3 1 mg/L lb, n/a n/a n/a VALUE VALUE VALUE VALUE f, Flow 34,791 26,813 14.556 1095 MGD MGD n/a n/a g. Temperature VALUE VALUE VALUE VALUE (winner) 22.0 18,6 14.1 188 °C n/a n/a h Temperature VALUE VALUE VALUE VALUE (summer) 33.0 3101 30,0 190 'C n/a n/a MINIMUM MAXIMUM MINIMUM MAXIMUM i, PH 6 ,11 8o16 n/a n/a 647 STANDARD UNITS PART B - Mark'X' in column 2-a for each polutant you know or have reason to believe is present Mark'X' m column 2wb for each pollutant you believe to be absent If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressty, in an effluent limdalions guideline, you must provide the results of at least one analysis for That pollutant For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one lade for each outfall. See the instructions for additional detalls and requirements. 2 MARK'X' 3. EFFLUENT 4. UNITS S, INTAKE (opuowl 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG VALUE a, LONG TERM AVERAGE AND a b a. MAXIMUM DALY VALUE (f ovmloble) (fmmloble) VALUE CAS NO. BELIEVED BELIEVED (t) (1) (t) d. NO. OF a, CONCEN• (r) b, NO.OF (favailoble) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATION (2) MASS ANALYSES a, Brordde (24959.67.9) b, Chlorine, Total 0614 12 , 4 1 m L lb, n a n a n a Residual 9/ / / / c. Cola X 27 n/a 1 PCU n/a n/a n/a n/a d Fecal Coliform X est, 2 n/a 1 col/dL n/a n/a n/a n/a ��gg 84u�46e.B) X 35.1 4110 35.1 4110 173 1783 12 mg/L lb, n/a n/a n/a ELI,NitraleWrite V 2.4 442.9 2.4 442,9 1.04 127,5 36 mg/L 1b. n/a n/a n/a (as M X EPA Form 3510.2C (8.90) PAGE Vol CONTINUE ON REVERSE OUTFALL 002 ITEM V -B CONTINUED FROM FRONT EPA Form 35142C (8-90) PAGE V•2 CONTINUE ON PAGE V•3 2, MARK 'X' 3, EFFLUENT 4, UNITS 5, INTAKE (optional) 1, POLLUTANT b, MAXIMUM 30 DAY VALUE c, LONGTERM AVRG, VALUE a, LONG TERM AND a b a, MAXIMUM DAILY VALUE (favailable) (fmadoble) AVERAGEVALUE CAS NO, BELIEVED BELIEVED(1) NO, OF a, CONCEN- b, NO, OF 0) (1)111111NN11111111d (f avylilable) PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b, MASS (�) CONCENTRATION (2) MASS ANALYSES g, Nitrogen, Total Organic (m x 0.362 32,1 1 mg/L The n/a n/a n/a M 1111poh I h. Oiland X <4,76 <422 1 mg/L lb, n/a n/a n/a i, Phosphorus \ / (as P), Told X 152 154 1,2 154 088 853 36 mg/L lb. n/a n/a n/a (1723.14-0) 1, Radioactivity (1)Alpha,Total X MENNEN (2) Bela, Total (3) Radium, Total (4) Radium 226, Total k, Sulfate (mSO')X (14886-79$) 105 9309 1 mg/L The n/a n/a n/a I. SuMde (4 m, Sulfile (as 514) (14265453) noSuraclanls X 0,552 48.9 1 mg/L lb4 n/a n/a n/a D, Aluminum, moommon Total (1429.90.5) X 1.27 112,6 1 mg/L lb, n/a n/a n/a p. Barium, Total \ (7440.39.3) x q Boron, Total (7440-02.8) XNE r, Cobalt, Total �/ (744048.4) x MENEM g43MM�l X 1.15 102,0 1 mg/L The n/a n/a n/a L Magnesium, Totalx2,26 200.4 1 mg/L The n/a n/a n/a (7439.954) u, Molybdenum, Total X Q439.98.7) V, Manganese, Total (743x96.5) 0.069 6 ,12 1 mg/L lb, n/a n a / n/a w, Tin, Total (7440.31.5) x, Titanium, Total (144432.6) MAN EPA Form 35142C (8-90) PAGE V•2 CONTINUE ON PAGE V•3 OUTFALL 002 CONTINUED FROM PAGE 3 OF FORM 2•C EPA I,D. NUMBER (coppfmm hem l of ponn l) OUTFALL NUMBER NCD 047 368 642 002 PART C - 9 you are a primary industry and this outfall contains process wastewater, refer to Table 2x2 in the rnstruchons to determine which of the GCIMS fractions you must test for, Mat 7' in column 2•a for all such GCIMS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols, If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nWequrred GC/MS fracdons), mat W in column 2•b for each pollutant you know or have reason to believe is present, Mark 'X' in column 2•c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant d you know or have reason to beleve d mlI be discharged in concentrations of 10 ppb or greater If you mark column 2b for acrolem, acrylondde, 2,4 dinrlrophend, or 2-methyk, 6 dindrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe That you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly descnbe the reasons the pollutant is expected to be discharged Note that there are 7 pages to this part, please review each carefully Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 2, MARK'X' 3, EFFLUENT 4, UNITS 5. INTAKE (opuoita 1, POLLUTANT b, MAXIMUM 30 DAY VALUE c. LONG TERM AVRG.. a, LONG TERM AND a b c a, MAXIMUM DAILY VALUE (f mlarlable) VALUE (f aradable) AVERAGE VALUE CAS NUMBER TESTING[BELIEVED BELIEVED OF a. CONCEN• NO OF (1) (1) (1)d,NO, (1)b (ifawdoble) REQUIREDESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)NASS ANALYSES TRATION b MASS CONCENTRATIDN (2)MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1M, Antimony, TotalV x <0,002 <0.177 1 mg/L lbo n/a n/a n/a (744x36-0) 2M Arsenic, Total X x <0.005 <0.443 1 mg/L lb. n/a (144x38.2) 3M.Beryllium, Total <0.001 <O.OB9 1 mg/L lb, Ean/a n/a n/a (7440At•7) /� 4M Cadmiu043*9)m,Tolal V <0.002 <0.177 1 mg/L lb. n/a n/a n/a (744x43.9) /� 5M,Chromum, V <0.005 <0.433 1 mg/L lbo n/a n/a n/a Total (7440-07-3) /� 6M. Copper, Told 00005 0.443 1 mg/L The n/a n/a n/a (744x50 e) Lead, X <0,003 <0,266 mg/L lb, n/aU4399.1 n/a n/a BMM•97fi'TotN X <010002 <0,018 1 mg/L lbs n/a n/a n/a 9M.Nxkel,Told<0.005 X x <0.433 1 mg/L lb. n/a n/a n/a (744x02.0) 10M.Selenium,X <0.005 <0,433 1 mg/L lb, n/a n/a n/a Total(7782494)x 11 M. Silver, TotalX x <0.002 <0.177 1 mg/L lb, n/a n/a n/a (7440.224) 12M.Thaumm,�/ x <0,005 <0,433 1 mg/L lb, n/a n/a n/a Tolal (744x28-0) (13M0=6, Zincc, Total �/ /� 06008 00709 1 mg/L lb, n/a n/a n/a 14M. Cyanide, Total (57424) X <0.005 <0.433 1 mg/L lb, n/a n/a n/a Phenols, �/ 0.0433 3.84 1 mg/L The n/a n/a n/a Total l /� DIOXIN 2,3,7,xTetra•\ / ESCRIBE RESULTS Not applicable chlorodibentomP• Diovan (116401.6) /X\ EPA Form 3510.2C (8.9D) PAGE V-3 CONTINUE ON REVERSE OUTFALL 002 CONTINUED FROM THE FRONT 2 MARK'X' 3, EFFLUENT 4 UNITS 5, INTAKE (optional) 1 POLLUTANT b, MAXIMUM 30 DAY VALUE c, LONG TERM AVRG, a, LONG TERM AND a b c a MAXIMUMDAILYVALUE (rjmnrinhle) VALUE(rfmnrlable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d, N0. OF a, CONCEN• (1) b NO, OF (f mbilable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b, MASS CONCENTRATION (2) MASS ANALYSES GCIMS FRACTION VOLATILE COMPOUNDS %Accrolein <0,0500 <4,433 (1 07.02.8) 1 mg/L lb. n/a n/a n/a 2V,Aaytondnle <0,0100 <0.881 1 (107•t3 t) mg/L The n/a n/a n/a g143*2) V <0000100 <0.089 1 mg/L lb, n/a n/a n/a ,�3. 4V, Bis (Chla* \ / merinOEther x Not Req ired per NCDWR NPDES Permitt'g Unit (542.88.1) 5V Brandon X <0.00100 <0.089 1 / / mg/L lb. n 0, n 0, n/a 6V, Carbon TehachWe <0,00100 <0.089 1 mg/L lb, n/a n/a n/a (58.23.5) (shglorobenzene V <0,00100 <0,089 1 mg/L lb, n/a n/a n/a 8V. ChlDrD& \/�/ bromomethane X <0,00100 <0.089 1 mg/L lb. n/a n/a n/a (124-08.1) / \ 9w thane V <0.00500 <0.443 1 mg/L lb, n/a n/a n/a 1OV, 2•Chloro- ethylmny Efher <0.0500 <4,433 1 mg/L lb. n/a n/a n/a (110,75.8) 11V, Chloroform (67.66,3) X 0,0248 2,199 1 mg/L lb, n/a n/a n/a 12V, D chloro- bromomelhane 0.00422 0,374 1 1/ L (75.271) / / lb, n/0, n d n 0, chlorom 13V, lhmelha dmaoromelhane (15.71.8) <0.00500 <0.443 1 mg/L lb. n/a n/a n/a 14V,1,1•Dkhloro- <0,00100 <0,089 1 m L lb, n a n a n a ethane p5*3) g/ / / / ekne'D�clOor) V <0.00100 <0.089 1 mg/L lb. n/a n/a n/a ethane 101.Ofr2 /� el V. ne05,354) <0,00100 <0.089 1 / / / elhylene(15.35d) mg/L lb. n 0, n 0, n 0, plpane�8hlori V <0.00100 <0,089 1 mg/L lb, n/a n/a n/a propene 8.87.5 /� 16V,1,3•DichlaaEE\ propylene X <0,00100 <0,089 1 mg/L lb• n/a n/a n/a (542.758) 19V.EMAenzene <0000100 <0,089 1 m L lb, n a n a n a (10041.4) 9/ / / / 20V Methyl BromideUO3.9) <0.00500 <0.443 1 mg/L lb, n/0, n/0, n/0, ChUdefU <0,00250 <0,222 1 L lb, n a n/a n/a Chbride p4-67.3) mg/ / , EPA Form 3510.2C (8.90) PAGE VA CONTINUE ON PAGE V•5 OUTFALL 002 CONTINUED FROM PAGE V4 2. MARK'X' 3, EFFLUENT 4, UNITS 5 INTAKE (opnona() 1. POLLUTANT b. MAXIMUM 30 DAY VALUE c, LONG TERM AVRG, a. LONGTERM AND :REQUIIREDPRESENT be c a. MAXIMUM DAILY VALUE (fmnilahle) VALUE(faindahle) AVERAGEVALUE CAS NUMBER IEVED BELIEVED (1) (1) (1) d. NO, OF a. CONCEN• (1) b, NO OF (jmailahle) ABSENT CONCENTRATKA4 (2)MASS CONCENTRATION (2)IIASS CONCENTRATION (2►MASS ANALYSES TRATION b. MASS CONCENTRATION (2)MASS ANALYSES GCIMS FRACTION -VOLATILE COMPOUNDS (eonrnnrerl) 2 bnd60ne2 v <0.00500 <0.443 1 mg/L lb, n/a n/a n/a P ) We 111,2,2- TeVachbroelhane X <0.00100 <0.089 1 mg/L lb, n/a n/a n/a 9• 24V.Terachbro•X <0.00100 <0.089 1 mg/L lb. n/a n/a n/a elhplene (127.184) x 25V, Toluene <0.00500 <0,443 1 mg/L lbn/a n/a n/a (IW8.3) 26V,112•Tr8ns• Dichloroelhylene X <0.00100 <0.089 1 mg/L lb. n/a n/a n/a 156.60.5 27V,I1111•Trichloro• V (0.00100 (0,089 1 mg/L lb, n/a n/a n/a ethane (71.556) A 28V,1,1,2•TncNoro•X <0.00100 <0.089 1 mg/L lb. n/a n/a n/a &ffie (79-00.5) x 29VTnchbro• X <0.00100 <0,089 1 mg/L lb, n/a n/a n/a el Irlene(T9.Ot•6) /\ 3OV, Tnchbro- x toromelhane <0.00500 <0.443 1 mg/L lb. n/a n/a n/a 5.694 31V, Viny Chlcdde X <0.00100 <0,089 1 mg/L lb, n/a n/a n/a GCIMS FRACTION -ACID COMPOUNDS IA.2•Chbrophenol X E<0.0100 <0,887 1 mg/L lb• n/a' n/a n/a (951.8) /\ 2A2,4Dchloro• V <0,0100 <0.8B7 1 mg/L lb. n/a n/a n/a phenol (120.83.2) 3A.2,4•Dm&67v,9 X <0.0100 <0.887 1 mg/L lb. n/a n/a n/a phenol (105.61.9) /\ 4a4416•DhiroO• X <0.0100 <0.887 1 mg/L lb. En/an/a n/a Cresol(534.62.1)5A.2,4•Dindro• <0.0100 <0.887 1 mg/L lb. n/a n/a phenol (51.28.5) 6A2441rophend X (88.750 <0.0100 <0.887 1 mg/L lb, n/a n/a n/a /\ 1A4-NdrophendX <0.0100 <0.887 1 mg/L lb. n/a n/a n/a (100-02.7) x BA.P•Chloro•M• X <0.0100 <0.887 1 mg/L The n/a n/a n/a Crew (59.50.7) /\ 9A Penlachlo* <0.0100 <0.887 1 mg/L lb. n/a n/a n/a phenol (87.86.5) 10A Phenol Y <0.0100 <0.887 1 mg/L The n/a n/a n/a 11A2,4,6Tdchbro <0.0100 <0.887 1 m a phenol (86.05.2) g/L lb, n/a n/a n/ EPA Form 3510.2C (8.90) PAGE V•5 CONTINUE ON REVERSE OUTFALL 002 CONTINUED FROM THE FRONT un• tits lt• Chloroanpro 2. MARK OX' 3. EFFLUENT 4. UNITS 5 INTAKE (opnona 1. POLLUTANT b, MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM AND TRTESaTING8EUbEVED C. a• MAXIMUM DAILY VALUE (fmiodable) VALUE (f available) AVERAGEVALUE CAS NUMBER BEUMD d. NO.OF a. CONCEN• b NO.OF (1) (1) 1 (f available) ABSENT CONCENMTION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b MASS CONCENTRATION (2)MASS ANALYSES GCIMS FRACTION - BASE/NEUTRAL COMPOUNDS (83429aphlhene X <0,00100 <0,089 1 mg/L lb, n/a n/a n/a 6�A•�ephrylene x (0.00100 <0.089 1 mg/L 1b, n/a n/a n/a 3B,Anlhracene (12412.7) �/ /� <0.00100 <0.089 1 mg/L lb. n a / n a / n/a 4B.Benzidme (927.5) %\ <0.0100 <0.887 1 m9/ L lb. n a / n or / n a / 56, Benzo (a) Anthracene (56.553) �( <0.00100 <0.089 1 mg/L lbo n/a n/a n/a 6B Benzo (a) Pyrene (5032.8) <0.00100 <0.089 089 1 m L g/ 1b, n a / n a / n a / 7B.3,4•Benzo• Ouoranlhene X <0.00100 <0,089 1 mg/L lb, n/a n/a n/a (205.99.2) 88. Benzo 01) Perylene(191.242) X (0.00100 <0,089 1 mg/L lb, n/a n/a n/a 9B. Benzo (k) Fluoranthene �( <0,00100 <0.089 1 mg/L lbo n/a n/a n/a (201-08.9) 10B. Bis (Wilonr ediny)Melhane <0.0100 <0.887 1 L lb. n a / n a / n a / (111.91.1)1/ 11B Bis(1•C7dora Bi(2 11B Ell X <0.0100 (0.887F 1 mg/L lb, n/a n/a n/a pv� (0.0100 (0.887 1 L lb, n or n or n or Elher(IO2.841) 13B. Bis (24%00• hc.}7Phlhowe �( (0.00300 <0,266 1 mg/L lb. n/a n/a n/a (11781.7) /\ 148.4•Bromopher yl PhenylEmer �( <0.0100 <0.887 1 mg/L lb, n/a n/a n/a (101.55.3) /\ 15B Butyl Benzyl <0.00300 <0.266 1 m L 1b. n/a n/a n/a Phlhalate (85667) 9/ 16B• 2 -Chloro• naphthalene �( <0.00100 <0,089 1 / / (91.58.7) / \ mg/L lb. n/a n a n a 17B.4•Chloro• phenyl PhenylElhe( X <0.0100 <0.887 1 mg/L 1b. n/a n/a n/a (7005.72-3) x (21HIr1) <0.00100 <0.089 1 m L lb. n a n a n a tim (218-01.9} g/ / / / 19B• abenzo (a,b) Anhracene <0.00100 <0.089 1 L lb. n a n a n a (53.743)/ / / / 20B• 1,2•Dichloro• <0.00100 <0 , 089 1 m L lb. n a n or n a benzene (95.541) /\ 9/ / / / 21B•1,3DFchlora (0.00100 (0,089 1 m L lb, n or n or n or benzene (541.73.1) 9/ / / / EPA Form 35142C (8.90) PAGE Vs6 CONTINUE ON PAGE V•7 t r OUTFALL 002 CONTINUED FROM PAGE V•6 2. MARK 4X' 3 EFFLUENT 4, UNITS 5 INTAKE (aprronal) 1, POLLUTANT b. MAXIMUM 30 DAY VALUE c, LONGTERM AVRG,a, LONG TERM AND a b c, a, MAXIMUM DAILY VALUE (if available) VALUE (Jmmlable) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BELIEVED 0) (1) (i) d NO OF a, CONCEN• (1) b N0, OF f available) REpUIRED PRESENT ABSENT CONCENTRATION(2) MAASS CONCENTRATION (2) LIASS CONCEMRATION (2) MA55 ANALYSES TRATION b. MASS Gp�NgpON (2) MASS CALYSES GCIMS FRACTION- BASE/NEUTRAL COMPOUNDS (ronunued) 22B.1,4DkNoro•V <0,00100 <0.089 1 mg/L lb. n/a n/a n/a benzene (10646.7) x 238.3,$Drchloro• <0,0100 <0.887 1 m L lb, n/a n/a n/a benzidine (81.94.1) g/ 246 Diethyl <0,00300 <0.226 1 L lb, n a n/a n/a Phlhalale (84.662) �/ / 21 amelhyl X Phthalate <0,00300 <0.226 1 mg/L lb, n/a n/a n/a (131 .11.3) 26B.NN•BuyV <0.00300 <0,226 1 mg/L lb, n/a n/a n/a Phlhalale (84.74.2) x 27B,2,4Dindro•V <0.0100 <0.887 1 mg/L lb, n/a n/a n/a Iduene (121.14.2) x 28B.2,6Dinilro• <0.0100 <0,887 1 mg/L lbt n/a n/a n/a toluene (60620.2) 29B. D404 g/ <0.00300 <0,226 1 m L lb, n/a n/a n/a Phlhalale (117.840) 30B 1,20pheny1• hydrune(as Azo• <0,0100 <0.887 1 mg/L lb, n/a n/a n/a benzene) (122.66.7) (18,FFluojanlhene x <0.00100 <0,089 1 mg/L The n/a n/a n/a 32B,FIuorene�/ <0.00100 <0,089 1 mg/L lb, n/a n/a n/a (6673.7) x 33B.Hexachlora• <0.00100 <0.089 1 m L lb. n a n a n a benzene (11674.1) g/ / / / 34B,Hexachloro• g/ <0.0100 <0.887 1 m L lb, n/a n/a n/a butadiene (81.663] 35B. Hexachloro- cydopenladiene <0,0100 <0,887 1 mg/L lb, n/a n/a n/a (77474) 36BHexa%oro• V <0,0100 <0,887 1 mg/L lb, n/a n/a n/a elhane(67.72.1) A 31B.Indeno (1,2,3•tdlPyrene <0.00100 <0,089 1 mg/L lb, n/a n/a n/a (193.39.5) 38B.Isophoronex <0.0100 <0,887 1 mg/L lb, n/a n/a n/a (1659.1) 9B3 hthalene V <0.00100 <0.089 1 mg/L lb, n/a n/a n/a x 40B,Nitr enzenex <0.0100 <0,887 1 mg/L lb, n/a n/a n/a 41 B N•Ndro- sodunethplamme <0.0100 <0,887 1 mg/L The n/a n/a n/a (62.1x9) 428, "itrosodF N•Propylafn e X <0.0100 <0,887 1 mg/L lb. n/a n/a n/a (621647) EPA Form 351WC (8.90) PAGE V•7 CONTINUE ON REVERSE OUTFALL 002 CONTINUED FROM THE FRONT 2, MARK 71 3 EFFLUENT 4, UNITS 5. INTAKE (opnonal 1, POLLUTANT b, MAXIMUM 30 DAY VALUE C. LONG TERM AVRG. a. LONG TERM AND a be c a MAXIMUM DAILY VALUE (ifmmin6le) VALUE(ifamilable) AVERAGEVALUE CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) 11) d. NO OF a CONCEN• (1) b. NO OF (f avndable) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CDNCENTRATIDN (2) MASS CANCENTRATION (2) MASS ANALYSES TRATION b, MASS CDNCENTRATION (2) MASS ANALYSES GCIMS FRACTION,, BASE/NEUTRAL COMPOUNDS (conunu4 43B, N-Ndro- sodlphenylamine �( <0,0100 <0.887 1 mg/L The n/a n/a n/a 44BPhenanlhrene <0.00100 <0,089 1 m L lb, n a n a n (85-01.8) 9/ a / / / 45B,Pyrene 40,00100 c0.089 (12m)1 mg/L The n/a n/a n/a /� 46B.1,1,4TrF chloftizene X <0.0100 <0.887 1 / / / (120&82.1) /\ mg/L lb, n 0& n 0& n 0& GC/MS FRACTION — PESTICIDES � 2) X 40,000050 c0,005 1 mg/L lb, n/0& n/0& n/0& 2P.aBIC <0,000050 <0,005 (319.846) 1 mg/L lb, n/'a n/a n/a (3i� 7) X <0,000050 40,005 1 mg/L The n/a n/a n/a �5Pg.gg."y� X 40.000050 <06005 1 mg/L lb, n/0& n/0& n/0& (3199m) %( <08000050 <0.005 1 mg/L lb, n/a n/a n/a 9rdane (574 40,000050 40,044 1 m L lb, n a n a n (51.749) g/ a / / / 7P,4,4�DDT <D,000050 <0,005 1 L lb, n a n a n a (50.29.3) mg/ / / / BP.4,4 DoE (0,000050 <0.005 1 m L lb, n a n a n p2.55.9) 9/ amen / / / (.4�4'B-)DD V <0,000050 (0,005 1 mg/L lb, n/a n/a n/a UMO) (OP,IAjddn <0,000050 <0,005 1 mg/L lb, n/a n/a n/a ` 1P,a,nsu0an �/ <0,000050 <0,005 1 mg/L The n/a n/a n/a 115.2& 111P,. EEndosulfan <0,000050 <0,005 1 mg/L The n/a n/a n/a 13P. Endosolfan Sulfale <0,000050 40,005 1 , n/a n/a n L lba (1031pOM) / / / / 14P Endnn X <0,000050 <0,005 1 mg/L lb. n/a n/a n/a 15P. Endrin Aldehyde�( <0.000050 <0,005 1 mg/L lb, n/a n/a n/a (1421.93.4) 16P,B,lachlw V <0,000050 <0,005 1 mg/L lb, n/a n/a n/a EPA Form 3510,,2C (8.90) PAGE V•a CONTINUE ON PAGE V•9 OUTFALL 002 CONTINUED FROM PAGE V-8 EPA I.D. NUMBER (cnpy fmin lien I of conn 1) 1OUTFALL NUMBER NCD 047 368 642 1 002 EPA Form 3510-2C (8-90) PAGE V•9 2. MARK W 3 EFFLUENT 4, UNITS 5, INTAKE (optinwo 1. POLLUTANT b, MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a, LONG TERM AND a, b c a, MAXIMUM DAILY VALUE (i/mnilnble) VALUE (�mndahle) AVERAGE VALUE CAS NUMBER TESTING BELIEVED BEUEVEO d. NO, OF a, CONCEN- b NO OF (1) (1) (1) (1) i mbdable U ) REQUIRED PRESENT ABSENT CONCENTRATION (2) MASS CONCENTRATKNJ (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSE GC/MS FRACTION — PESTICIDES (conmme4 17P HeplacNa Epoade x <0.000050 <0.005 1 mg/L The n/a n/a n/a (1020703) 18P.PC&1242X (53469.21.9) /\ <0,000500 <0.044 1 mg/L lb. n/a n/a n/a 19P PC&1254 (11097.89.1) X /\ <0,000500 <0,044 1 mg/L lb, n/a n/a n/a 20P PC&1221 (11104.2&2) <0.000500 <0.044 1/ L The n/a n/a n/a 21P,PM1232<0.000500 (11141.1&5) X <0,044 1 m /L Mg/L lb, n/a n/a n/a PCB•1248 (12672.29.6) x <0,000500 <0,044 1 mg/L lb. n/a n/a n/a 23P,PCB-1260\/ (llD9&825) n <0.000500 c0.044 1 mg/L lb, n/a n/a n/a 24P, PC&1016 (12674.11.2) X <0,000500 <0,044 1 mg/L lb n/a n/a n/a 25P. Toxaphene (8001.35,2) X <0,000500 <0,044 1 mg/L lbo n/a 7n/an/a EPA Form 3510-2C (8-90) PAGE V•9 4 th Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Sludge Management Plan The Chemours Company — Fayetteville Works operates a Class 3 Wastewater Treatment Plant which is comprised of a single -stage activated sludge biological system. Excess sludge is removed from the system by diverting part of the Recycled Activated Sludge (at approximately 0.6% solids) from the clarifiers to a Dissolved Air Floatation ("DAF") unit for initial thickening. The sludge from the DAF (at approximately 3%solids) is transferred to a Mix Tank where polymer agents are added to enhance the dewatering process. The semi -thickened sludge is transferred from the Mix Tank to a Rotary Filter for final thickening, whereby the sludge is thickened to 6% solids. The thickened sludge is then transferred to a Screw Press where it is dewatered to a concentration of 9-20% solids. Following the Screw Press, the sludge is typically dried in steam heated dryers to a concentration of 40-55% solids. The dried sludge, or on occasion the dewatered sludge, is transported off-site to a commercial Subtitle D landfill. This sludge is currently being disposed of at the Waste Industries "Sampson County" Landfill near Roseboro, NC, In 2015, the average weekly quantity of generated wasted sludge was approximately 35,000 lb. s y Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Current Facility Wastewater Management Process wastewater and stormwater from the various manufacturing areas are collected in the respective area sumps and ultimately conveyed via a gravity flow underground process sewer pipe to the facility's central wastewater treatment plant ("WWTP"). Sanitary sewage is conveyed via a separate underground sewer system to the WWTP. The permitted flowrate of the WWTP is 2.0 MGD, with an actual average flowrate of approximately 1.2 MGD. This untreated process wastewater is commingled in the WWTP Influent Sump where it is pumped to an 850,000 -gallon Equalization Basin. The Equalization Basin is mixed with two fl oating submerged mixers. Three floating surface aerators in the basin cool and aerate the incoming wastewater. A 175,000 -gallon Emergency Retention Tank is available for temporary storage of untreated wastewater which may need additional treatment or acclimation in the WWTP activated sludge process at a controlled rate that allows for proper biological treatment. Untreated wastewater from the Equalization Basin is normally pumped to a 250,000 -gallon Predigester Tank in which initial biological activity with the WWTP activated sludge begins. The Predigester Tank is aerated. The partially treated wastewater from the Predigester Tank is pumped to a 1,700,000 -gallon Aeration Tank. The Aeration Tank is the unit where the majority of the biological activity occurs. The Aeration Tank is aerated primarily by a diffused air system located in the bottom of the tank. The tank can have supplemental aeration via one or two floating Biomixers® that injects air through submerged rotors. The biologically treated wastewater is then sent to one of two in -ground clarifiers (119,000 gallons and 168,000 gallons respectively) or an above -ground 679,000 -gallon clarifier; with all clarifiers being operated in parallel. The clarified treated effluent is discharged to and through Outfall 001. The wasted activated sludge is sent to a Dissolved Air Floatation (DAF) unit, then to a 47,000 gallon Sludge Storage Tank, and finally to a Rotary Filter for thickening. The thickened sludge is dewatered in a Sludge Press, and can be dried in a steam -heated dryer for additional moisture removal. The dewatered sludge or dewatered/dried sludge is transported off-site to a commercial Subtitle D landfill. Non -contact process cooling water an d non -process stormwater are conveyed via surface ditches. In addition, excess riverwater flow and Outfall 001 effluent are discharged directly to a surface ditch. The combined, total flow of water from the site is discharged through and monitored at Outfall 002. The discharged treated wastewater is conveyed via an underground pipe to the Cape Fear River, where it enters the river at a point approximately 1,500 feet upstream of the William O. Huske Lock & Dam (a.k.a Lock & Dam No. 3). r W Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application - April 27, 2016 Current Facility Operating Conditions Chemours Fluoromonomers/Nafion® Membrane Manufacturing Area: The Chemours Company —Fayetteville Works' Fluoromonomers /Nafion® Membrane manufacturing area produces several final products. ChemoursTM Nafion® Membrane is a plastic film used in the chloroalkali industry and in electrochemical fuel cells. ChemoursTM Nafion® Polymer Dispersions are used in the fabrication of thin films and coating formulations for fuel cells membranes, catalyst coatings, sensors, and a variety of electrochemical applications. The HFPO monomer and the Vinyl Ether monomers are used to manufacture various fluorochemical products such as ChemoursTM Teflon®. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. Chemours Polymer Processing Aid ("P_?�) Manufacturing Area: NL The Chemours Company — Fayetteville Works' PPA manufacturing area produces a polymer processing aid. � The processing aid produced in this unit is used in the manufacturing of �fluoropolymers and fluorinated telomers, •but none of the produced processing aid is used at the Fayetteville Works site. All process wastewater generated from this manufacturing facility is ``X ' collected and shipped off-site for disposal. No process wastewater from this manufacturing facility is discharged to the Chemours' wastewater treatment plant or to the Cape Fear River, Kuraray Butacite® Manufacturing Area: The Kuraray America Inc. — Fayetteville Plant's Butacite® manufacturing area produces two final �;1 products. KurarayTM Butacite® Interlayer plastic sheeting is the final product used in safety glass such as automobile windshields. Polyvinyl butyral resin is shipped off-site as a transfer to other Kuraray locations for final processing. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. Kuraray SentryGlas® Manufacturing Area: The Kuraray America Inc. —Fayetteville Plant's SentryGlas® manufacturing area produces �C9,1`'' KurarayTM SentryGlas® ionoplast interlayer laminate. SentryGlas® interlayer is used for laminated safety glass in side, rear, and overhead automobile windows. It is also used in architectural applications desiring safety glass. There is no contact process wastewater generated from this manufacturing facility, therefore only sanitary waste from this area is treated in the Chemours' wastewater treatment plant. This manufacturing facility does discharge non -contact cooling water to a surface ditch and ultimately to Outfall 002. DuPont Polyvinyl Fluoride ("PVF") Manufacturing Area: 2 L� 1 OS J ` -, .�-_- �S� S The DuPont Company — Fayetteville Works' PVF manufacturing area produces polyvinyl fluoride resin that is used in the electronics industry as a backing for photovoltaic cells, as well as many other uses. Wastewater generated from this manufacturing facility is discharged to the Chemours' wastewater treatment plant. M 61 Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Alternate Application Schedule for §316(b) of the Clean Water Act Final regulations implementing §316(b) of the Clean Water Act, which establish requirements for cooling water intake structures at existing facilities, were published in the Federal Register on August 15, 2014 with an effective date of October 14, 2014. The Chemours Company —Fayetteville Works ("Chemours") operates a cooling water intake structure on the Cape Fear River that is subject to this new Federal Cooling Water Intake Structure Rule ("the Rule") as codified in 40 CFR Part 125. The Rule requires the owner or operator of a facility subject to Subpart J whose currently effective permit expires after July 14, 2018, to submit to the Director the information required in the applicable provisions of 40 CFR 122.21(r) when applying for a subsequent permit. Pursuant to 40 CFR 125.95(a)(2), the owner or operator of a facility subject to Part 12S Subpart J, "Requirements Applicable to Cooling Water Intake Structures for Existing Facilities Under Section 316(b) of the Clean Water Act", whose currently effective permit expires prior to July 14, 2018, may request the Director to establish an alternate schedule for the submission of the information required in 40 CFR 122.21(r) when applying for a subsequent (renewed) permit. On October 20, 2015, a letter was sent from Michael E. Johnson, Environmental Manager, Chemours Company — Fayetteville Works, to Dr. Sergei Chernikov, NCDEQ Division of Water Resources' NPDES Complex Permitting Unit, requesting an alternate schedule whereby all the materials required by the Rule will be submitted with the 2021 renewal application. On February 26, 2016, a letter was sent from S. Jay Zimmerman, Director, NC DEQ Division of Water Resources, to Michael E. Johnson, Environmental Manager, Chemours Company — Fayetteville Works, wherein the requested alternate schedule for submission of required CWIS information with the next permit renewal in 2021 was approved. A copy of Mr. Zimmerman's letter is attached to this application package. cls WaterResource•s ENVIRONMENTAL QUALITY PAT MCCRORY Gorcrnor DONALD R. VAN DER VAART Secrelnry S. JAY ZIMMERMAN February 26, 2016 Mr. Michael E. Johnson, P.E. Environmental Manager Chemours Company 22828 NC Highway 87 West Fayetteville, North Carolina 28306-7332 Subject: Alternate CWA 316(b) Application Schedule NPDES Permit NC0003573 Fayetteville Works Bladen County Dear Mr. Johnson: Direcmr The Clean Water Act Section 316(b) Cooling Water Intake Structure (CWIS) Final Rule outlines regulations and standards for the design and operation of cooling water intake structures under the NPDES program. Your current permit expires October 31, 2016, with renewal application due by May 4, 2016. Since your permit expires prior to July 14, 2018, under 40 CFR 125.95(a)(2), you have requested an alternative schedule for submission of CWIS permit application information required in 40 CFR Part 122.21( r). Based on Division review, an alternate schedule for submission of required CWIS information with the next permit renewal in 2021 is approved. This schedule date will be established in the 2016 permit renewal as well. Please note that facilities should begin to adapt their systems to comply with CWA Section 316(b) requirements. If you have any questions, please contact Tom Belnick with the NPDES Permitting Unit at 919407-6390 or via email: tom.belnick@ncdenr.jzov Sin�ely, i S. Jay Zimmerman, P.G. Director, Division of Water Resources Cc: NPDES File Central File Ec: US EPA Region 4 US FWS NC WRC NC DWR/Fayetteville Region Chemours Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Elimination of Monitoring Requirement for PFOA In December 2002, the DuPont Company —Fayetteville Works began production of, ammonium perfluorooctanoate ("APFO"), which is the ammonium salt of perfluorooctanoic acid ("PFOA"). The renewed NPDES Permit No. NC0003573 that became effective on July 1, 2007, included a requirement for monthly monitoring of PFOA at Outfall 002, In 2006 the North Carolina Division of Water Quality , in consultation with the North Carolina Division of Waste Management and the North Carolina Department of Health and Human Services, established an Interim Maximum Allowable Concentration ("IMAC") of 2 µg/L for PFOA, which was intended for the protection of groundwater as a source of drinking water. Following the issuance of this temporary health -based level, DWQ requested the assistance of the North Carolina Secretary's Science Advisory Board on Toxic Air Pollutants ("NCSAB") in reviewing the toxicological literature on PFOA and recommending to DWQ an update of the IMAC for PFOA in groundwater. On August 10, 2012, the NCSAB issued their recommendation to DWQ that the IMAC for PFOA in groundwater be reduced to 1 µg/L. During the 3 -year period from 2013 to 2015, the average monthly concentration of the final effluent discharge at Outfall 002 was 0.027 µg/L PFOA, with a maximum concentration of 0.088 µg/L PFOA. During the same period, the average monthly concentration of the incoming water from the Cape Fear River to the site, which is 99% of the effluent flow at Outfall 002, was 0.012 µg/L PFOA, with a maximum concentration of 0.031 µg/L PFOA. The production of APFO at this facility ceased in Apri12013. The Chemours Company —Fayett eville Works (formerly the DuPont Company —Fayetteville Works) is requesting that the monthly monitoring requirement for PFOA at Outfall 002 be eliminated in the renewed NPDES Permit No. NC0003573 for the following reasons: • APFO is no longer manufactured at this facility and has not been produced at the facility since Apri12013; • APFO is not and has never been used as a process aid or a raw material at this facility; • The 3 -year average concentration at Outfall 002 was 0.027 µg/L PFOA, versus the current NC-DWR IMAC of 2µg/L PFOA and the NCSAB recommended 1µg/L PFOA; and • PFOA is present at low concentrations throughout the Cape Fear River basin, and that background level of PFOA in the Cape Fear River water contributes to the concentration measured at Outfall 002. Chemours' Company —Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information — Permit Renewal Application — April 27, 2016 Form 2C Perrnit Application — Bis(chloromethyl) ether Bis(chloromethyl) ether (CAS No. 542-8 ) was not analyzed for, and consequently was not reported on Page V4 of Form 2C for both Outfall 001 and Outfall 002, On November 28, 2014, the State of Oregon's Department of Environmental Quality ("ODEQ") issued a memorandum (Note �> addressing the issue of analyzing for bis(chloromethyl) ether ("BCME"). In this memorandum, ODEQ states: "Based on the chemical's rapid hydrolysis in water, there are no analytical methods to measure BCME in water samples. Currently, the only analytical techniques available for this compound are for air samples. Region 10 EPA staff queried its Manchester Environmental Lab in Port Orchard, WA about potential, analytical methods for BCME. Staff at the lab confirmed that there is no EPA method for BCME because of its rapid degradation in water." Because of the lack of anEPA approved analytical method for bis(chloromethyl) ether in a water matrix, ODEQ concluded: "Given its rapid hydrolysis in water, there are no recommended analytical methods for BCME in water samples. Because BCME is not quantifiable in wastewater, DEQ will not require permit holders to monitor or conduct reasonable potential analyses for this toxic pollutant." In an April 13, 2106, email from Tom Belnick, Supervisor of the NCDEQ Division of Water Resources' NI -DES Complex Permitting Unit, to Michael Johnson, Environmental Manager, Chemours Company — Fayetteville Works, Mr. Belnick stated: "I checked with our DWR analytical lab, and they concur with Oregon's position and are not awaA e of any labs using even R&D methods L analyte. Therefore, you can omit this parameter from your application renewal." Note 1: http://www.deq.state.or.us/wq/standards/docs/toxics/BisChloromethylMemo.pdf