201706201322

DuPont Fluoroproducts
22828 NC Highway 87 W
Fayetteville, NC 28306-7332
August 16, 2012
N.C. Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
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DISCHARGE MONITORING REPORT —July 2012
Attached is E. I. DuPont de Nemours &Company, Inc., Fayetteville Works Discharge
Monitoring Report for the month of July 2012.
If you have any questions, please contact Jamie R. Lewis at [phone].
JRL: bao
Attachment
cc: Ken Cook - ENGR, Old Hickory
J. R. Lewis - FW
M. E. Johnson - FW
File: F-1-3-4
E.I. du Pont de Nemours and Company

NPDES PERMIT NO. NC0003573
EFFLUENT
DISCHARGE NO
001
FACILITY NAME DuPont -Fayetteville Works
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis
CERTIFIED LABORATORIES (1) TBL Laboratory(Lumberton)
MONTH July YEAR 2012
CLASS 3 COUNTY OwnflIF
GRADE
(2)
4 PHONE [phone]
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
CENTRAL FILES
DIV,
DIV. OF WATER QUALITY
DENR
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
)(
l
(SIGNATU E OF OPERATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
00310 00530 00556 39700 39700 01034 01042 01067 01092
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EFF X
p
❑
1
HRS
0800
HRS
24
Y/N
MGD
0.979
*C
UNITS
Lb/Day
18.8
Lb/Day
65.3
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
Lb/Day
Lb/Day
2
0800
24
Y
0.838
29
7.99
36.3
76.9
3
40800
24
Y
0.912
29
8.01
4
0800
24
1 0.897
*
*
26.9
145.9
5
0800
24 ;
B
0:921
29 "
7.80
6
0800
24
B
0.981
7
0800
24
1 0.859
8
0800
24
1
1 0.890
9
0800
24
B
1.011
30
7.60
22.8
113.8
10
0800
24
B
0.929
29
7.76
18.6
108.5
11
0800
24
Y
0.923
29
7.79
20.8
49.3
<500
12
0800
24
Y
0.863
13
0800
24
Y
0.960
14
0800
24
0.909
15
0800
24
0.910
16
0800
24
Y
0.994
29
7.92
23.2
60.5
17
0800
24
Y
0.916
29
7.95
36.7
64.9
18
0800
24
Y
0.904
30
8.00
16.6
111.6
19
0800
24
Y
0.899
20
o8o0
24
Y
0.924
21
0800
24
0.837
22
0800
24
0.903
23
0800
24
B
0.971
30
7:72
17.8
97.2
24
0800
24
B
0.900
29
7.74
21.0
86.3
25
0800
24
B
0.941 '
30
7:75
17:3
51:0
26
0800
24
B
0.896
27
0800
24
B
0.930
_. .
28
0800
24
0.872
29
0800
24. -
0.931
30 0800 24 Y
31 6800 24 Y
AVERAGE
MAXIMUM
MINIMUM
0.917
1.016
0.920
1.016
0.837
30 7.80
30 7:82
29
30 8.01
29 7.60
19.9
22.9
22.8
36.7
16.6
76.5
50.8
82.8
145.9
49.3
0
<5.0
<5.0
Comp.
(C)
Grab (G)
G G
C
C
G
G
G
G
G
G
G
Monthly Limit
2.0182.6
303.1
1
0.113
8.36
10.91
12.72
7.90
Daily Limit 16-9 1 484.7 981.5 L I0.05
20.85
25.44
29.96
19.65
DEM Form MR -I (12/93) *Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements IJ
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
Ellis H. McGa
28306-7332
it
678-1315
Phone Number
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00545 Settleable Matter 00940 Total Chloride
Parameter Code assitance may be obtained by Galli
The monthly average for fecal coliform is to be
facility's permit for reporting data
01027 Cadmium
01092 Zinc
01105 Alu
minum
01032 Hexavalent Chromium 01147
01034 Chromium 31616
32730
01037 Total Cobalt 34235
01042 Copper 34481
38260
01045 Iron 39516
01051 Lead 50050
the Water Quality Compliance Group at (919
ported as a GEOMETRIC mean. Use on
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Flow
Toluene
MB
PCB's
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
33-5083, extension 581 or 534
units designated in the reporting
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory
authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
the Water Quality Compliance Group at (919
ported as a GEOMETRIC mean. Use on
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Flow
Toluene
MB
PCB's
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
33-5083, extension 581 or 534
units designated in the reporting
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory
authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)

NPDES PERMIT NO. NC0003573
EFFLUENT
DISCHARGE NO. 002 MONTH July
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED u PERSON(S) COLLECTING SAMPLES
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV, OF WATER QUALITY
DENR
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
X
YEAR 2012
Bladen
4 PHONE [phone]
Jamie R. Lewis / Arnold Ray Beard
(SIGNATU�tE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DATE
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OF
EFF X
QH
HRS
HRS
YIN
MGD
'C
UNITS
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
P/F
1
08001
24
21461
2
08001
24
Y
22.481
29
7.49
3
08061
24
Y
24.383
29
7.54
4
o800l
24
22.498
5
08001
24
rB
23.424
32
7236
6
0800
24
B
26.183
33
7.81
7
0800
24
21.577
8
0800
24
31.836
9
0800
24
B
14.289
35
7.87
10
0800
24
B
23.382
32
7.33
0.71
2.10
11
080o
24
Y
22.812
31
7.40
12
08001
24
1 Y
23.239
30
7.52
0.090
13
08001
24
1 Y
24.291
30
6.80'
14
08001
24
23.246
15
08001
24
23304
16
08001
24
Y
23.860
31
7.17
17
08001
24
F Y
23.954
31
7.21
18
o800l
24 1
Y
23.980
31
7.15
10
08061
24
F Y
23.852.
31
7.40
20
08001
24 1
Y
25.104
31
7.48
21
08001
24
23.986
22
08001
24
22.239
23
08001
24 1
B
25.956
30
6.85
24
0800
24
B
20.190
31
7.07
25
08001
24 1
B
23.035
32
7.14
26
08001
24
B
23.751
31
7.02
27
08001
24
B
23.078
32
7.05
28
08001
24
23.620
290800
24
23.526
30
0800
24
Y
26.968
31
7.15
31 0800 24 Y
AVERAGE
24.505
23.613
31 7.21
31
0.090
0.71
2.10
MAXIMUM
31.836
35 7.87
0.090
0.71
2.10
MINIMUM
14.289
29 6.80
0.090
0.71
2.10
Comp.
(C)
Grab (G)
G G
C
C
G
G
C
C
C
Monthly Limit
Daily Limit 6-9
DEM Form MR -I (12/93) * Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements �J
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements L �
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
Ellis H. McGaughy - P
Pe{mittee (Please print
le, NC, 28306-7332
678-1
Phone Num
Date
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residu I
00080 Color (Pt -Co) 00610 Ammonia Nitrogen
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water C
The monthly average for fecal coliform is to be reported as a
facility's permit for reporting data
>mpliance Gra
ETRIC mean
01092 Zinc
01105 Aluminum
327
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water C
The monthly average for fecal coliform is to be reported as a
facility's permit for reporting data
>mpliance Gra
ETRIC mean
01092 Zinc
01105 Aluminum
327
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water C
The monthly average for fecal coliform is to be reported as a
facility's permit for reporting data
>mpliance Gra
ETRIC mean
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics
34235 Benzene
34481 Toluene
38260 WAS39516 PCB's
50050 Flow
a
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
at [phone], extension 581 or 534
Jse only units designated in the repo
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory
authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
327
a
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
at [phone], extension 581 or 534
Jse only units designated in the repo
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory
authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)

NPDES NO: NC0003573
DISCHARGE NO: 002 MONTH: July YEAR: 2012
FACILITY: DuPont = Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM
DOWNSTREAM
00010 00400 00310 00610 00530 00094 51521 00010 00400 00310 00610 00530 00094
a cu U a)
Y
0 m .a m a) U 0) O) E ca
0 o U a) a T a)
m o v(n N O E c o a U) o x o f >
cu c\1d .� _ > ca m C) a) .� N O o L U
p a) m °) a @o > U iv v 0o N � a U c
E a) U UM)o v E o ° a) c`a V a > a)
E D a) ti ao) U _= E a `O w ami o 0
H O °) ~ E `� LL 0) U
m a ) m o
HRS °C units mg/L mg/L #/1 o0mI µmho/cm ug/L HRS °C units mg/L mg/L #/100ml µmho/cm
1 1
2 2
3 3
4 4
5 5
6 6
7 7_
8 8
9 9
10 10
11 11
12 11:00 0.064 12
13 13
14 14
15 15
16 16
17 17
18 18
19 19
20 20
21 21
22 22
23 23
24 24
25 25
26 26
27 27
28 28
29 29
30 30
31 31
Average 0.064 Average
Maximum 0.064 Maximum
Minimum 0.064 Minimum
DWQ Form MR -3 (Revised 7/2000)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements LL
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements L�
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
Ellis H. McGaughy -Plant M
Perm ttee (Please nt or tyK
Signature of Permittee` I
NC, 28306-7332 (�
P
678-1315
ITii1Ta7
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
Parameter Code assitance may be obtained by call.
The monthly average for fecal coliform is to be
facility's permit for reporting data
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics 81551
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
the Water Quality Compliance Group at (919) 733-5(
ported as a GEOMETRIC mean. Use only units
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
extension 581 or 534
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
"* If
b) (2) sig(D) ned by other than the premee, delegation of signatory
m the reporting
authority must be on file with the state per 15A NCAC 2B .0506
(
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
Parameter Code assitance may be obtained by call.
The monthly average for fecal coliform is to be
facility's permit for reporting data
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics 81551
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
the Water Quality Compliance Group at (919) 733-5(
ported as a GEOMETRIC mean. Use only units
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
extension 581 or 534
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
"* If
b) (2) sig(D) ned by other than the premee, delegation of signatory
m the reporting
authority must be on file with the state per 15A NCAC 2B .0506
(
Parameter Code assitance may be obtained by call.
The monthly average for fecal coliform is to be
facility's permit for reporting data
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics 81551
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
the Water Quality Compliance Group at (919) 733-5(
ported as a GEOMETRIC mean. Use only units
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
extension 581 or 534
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
"* If
b) (2) sig(D) ned by other than the premee, delegation of signatory
m the reporting
authority must be on file with the state per 15A NCAC 2B .0506
(
the Water Quality Compliance Group at (919) 733-5(
ported as a GEOMETRIC mean. Use only units
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
extension 581 or 534
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
"* If
b) (2) sig(D) ned by other than the premee, delegation of signatory
m the reporting
authority must be on file with the state per 15A NCAC 2B .0506
(