201706201321

NPDES PERMIT NO. NC0003573
EFFLUENT
DISCHARGE NO. 001
FACILITY NAME DuPont - Fayetteville Works
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis
CERTIFIED LABORATORIES (1) TBL Laboratory(Lumberton)
_..__._ r--� _na
MONTH September YEAR
CLASS 3 COUNTY
GRADE 4
(2)
Bladen
2012
PHONE [phone]
�.nc�n cvA n urtV reqs crlgrvG
PERSONS) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COP to.
ATTN: CENTRAL FILES OCT
iZ
DIV. OF WATER QUALITY
X
DENRCENTRAL1
(SIGNATURETF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050
00010
00400
39700 39700 01034 01042 01067 01092
00310T=)LU
FLOW
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❑
0
0
HRS
HRS
YIN
MGD
C
UNITS
Lb/Day
Lb/Day
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
Lb/Day
Lb/Day
1
0800
24
1.017
2
0800
24
0.914
3
0800
24
0.906:
4
0800
24
Y
0.812
29
7.71
16.3
1960
5
0800
24
Y
0.939
29
7.75
21.1
75.2
<5.0
6
0800
24
Y
0.736
29
7.70
**
119.7
7
0800
24
Y
0.879
8
0800
24
0.651
9
0800
24
0.565
10
0800
24
Y
0.543
27
7.45
11.8
16.8
11
0800
24
Y
0.380
26
7.68
7.6 '
13.0
12
0800
24
Y
0.240
26
7.70
7.8
26.8
13
0800
24
Y
0.428
14
0800
24
Y
0.305
15
0800
24
0.095
16
0800
24
0.000
17
0800
24
Y
0.000
SD
SD
18
0800
24
B
0.000
SD
SD
19
0800
24
Y
0.000
SD
SD
20
0800
24
Y
0.000
SD
SD
21
0800
24
Y
0.000
SID
SD
22
0800
24
0.000
23
0800
24
0.000 '
24
0800
24
Y
0.000
25
0800
24
Y
0.328
23
7.21
7.4
102.0
26
0800
24
Y
0.212
23
7.35
8.3
11.0
27
0800
24
Y
0.376
22
7.45
9.7
31.4
28
0800
24
Y
0.285
29
080o
24
0.369
30
0800
24
0.371
31 0800 24
AVERAGE
0.378
26
11.3
46.1
0
MAXIMUM
1.017
29 7.75
21.1
119.7
<5.0
TGG
-
MINIMUM
0.000
22 7.21
7.4
11.0
<5.0
Comp.
(C) Grab
(G)
G G
C
C
G
G
G
G
G
Monthly Limit
2.0
182.6
303.1
0.113
8.36
10.91
12.72
7.90
Daily Limit
6-9
484.7
981.5
0.5
20.85
25.44
29.96
19.65
DEM Form MR -I (12/93) SD -Shut Down *Holiday ** Lab Accident

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements L
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
On 9/6/12 our contract lab had a lab accident with sample ID E20906 and they were not able to provide a BOD
result for this sample. A report of analyses from the lab is included with this DMR.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy -Plant
ermitteeIrleaseprint or q
dJ
A. .1I! f n. a e vet
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332
Permittee Address
315
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co) 00610 Ammonia Nitrogen 01092 Zinc Chlorine
00082 Color (ADM]) 00625 Total Kjeldhal 01027 Cadmium 01105 Aluminum
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Hexavalent Chromium 01147 Total Selenium 71880 Formaldehyde
00300 Dissolved Oxygen 01034 Chromium 31616 Fecal Coliform 71900 Mercury
00310 BOD5 00665 Total Phosphorous 32730 Total Phenolics 81551 Xylene
00340 COD 00720 Cyanide 01037 Total Cobalt 34235 Benzene
00400 pH 00745 Total Sulfide 01042 Copper 34481 Toluene
00530 Total Suspended 00927 Total Magnesium 38260 MBAS
Residue 00929 Total Sodium 01045 Iron 39516 PCB's
00545 Settleable Matter 00940 Total Chloride 01051 Lead 50050 Flow
Parameter Code assitance may be obtained
i the Water Qualit
The monthly average for fecal coliform is to be reported as a GEO
facy's permit for reporting data
.e Group at (919) 733-5(
mean. Use only units
extension 581 or 534
gnated in the reporting
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory
authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)

Shipping:
2401 W. 5th St.
Lumberton NC 28358
E.I. DU PONT DE NEMOURS
CONTRACT SERVICES
22828 NC 87 HWY W
FAYETTEVILLE, NC 28306-
Attn: MR. JAMIE LEWIS
Mailing:
P ) Box 589
Lumberton, NC 28359
Phone: 910=738-6190
Fax: [phone]
Email:pam.hester.
tbl(c�hotmail.com
FINAL REPORT OF ANALYSES
& CO. i PROJECT NAME:
REPORT DATE: 09/12/12
SAMPLE NUMBER- 66955 SAMPLE ID- E20906
DATE SAMPLED- 09/07/12 LOCATION- NOT SPECIFIED
DATE RECEIVED- 09/07/12 SAMPLER- JAMIE LEWIS
TIME RECEIVED- 1045 DELIVERED BY- JOHNNY HESTER
Page 1 of 1
ANALYSIS
BIOCHEMICAL OXYGEN DEMAND
TOTAL SUSPENDED SOLIDS
* LAB ACCIDENT
ANALYSIS
METHOD DATE BY
SM5210B 09/07/12 THK
SM2540D 09/11/12 THK
SAMPLE MATRIX- WW
TIME SAMPLED- 0800
RECEIVED BY- THK
RESULT UNITS
L/A MG/L
19.5 MG/L
LABORATORY DIRECTOR ^]
AC46�
NCDENR DWQ # 37, NCDENR DW #37781
QUAL DET.
CODE LIMIT
2.0
0.1

EFFLUENT
NPDES PERMIT NO, NC0003573 DISCHARGE NO, 002 MONTH September YEAR 2012
FACILITY NAME DuPont -Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED L� PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES-�
DIV, OF WATER QUALITY )(
DENR (SIGNATOR OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
I
v r FLOW
E In W
W A o EFF X M o U W
~ E U E 4 N
Q Q ap O W J G. N 0
`o a `o U a. W Q U D
dN O J W W U m LL
0 0 Q ~
Q
HRS HRS YIN MGD 'C UNITS mg/L mg/L mg/L
1 0800 24 21.121
2 0800 24 21.262
3 0800 24 21.148
4 0800 24 Y 20.325 29 7.26
5 0800 24 Y 19.868 29 7.34
6 0800 24 Y 18.307 29 7.29
7 0800 24 Y 15.891 ' 29 7.34
8 0800 24 14.934
9 0800 24 11.647
10 0800 24 Y 10.356 27 7.61
11 0800 24 Y 8.941 27 8.30
12 0800 24 Y 9.842 25 7.74
13 0800 24 Y 8.490 25 7.84
14 0800 24 Y 7.259 25 7.80
15 0800 24 3.582
16 0800 24 0.000
17 0800 24 Y 0.000 SID SID
18 0800 24 B 0.000 SD SD
19
Q �
O 2 U }
o U Q O Q O Z~
F- U
Q u 2 0 It O
a U 0 Z U H
O a
ug/L mg/L mg/L P/F
0.075
0.49 12.76
osao 24 Y 0.000 SD SD
20 osao 24 Y 0.000 SD SD
21 0800 24 Y 0.000 SID SD
22 0800 24 0.000
23 0800 24 2.184
24 0800 24 Y 4.561 21 7.15
25 0800 '24 Y 9.781 21 7.21
26 0800 24 Y 8.972 21 7.20
27 0800 24 Y 10.840 21 7.36
28 0800 24 Y 8.169 22 7.43
29 0800 24 11.757
30 0800 24 12.092
31 0800 24
AVERAGE 9.378 25 0.075 0.49 2.76
MAXIMUM 21.262 29 8.30Ic
0.075 0.49 2.76
MINIMUM 0.000 21 7.150.075 0.49 2.76
Comp. (C) Grab (G) G G G G C C C
Monthly Limit
Daily Limit 6.9
DEM Form MR -I (12/93) *Holiday SD -Shut Down

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
Ellis H. McGaugh
Permittee (Please
of
28306-7332
nt
i
315
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co) 00610 Ammonia Nitrogen
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc Chlorine
01105 Aluminum
327
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc Chlorine
01105 Aluminum
327
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc Chlorine
01105 Aluminum
01147 Total Selenium 71880 Formaldehyde
31616 Fecal Coliform 71900 Mercury
30 Total Phenolics 81551 Xylene
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the repo
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A,0202
(b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
327
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the repo
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A,0202
(b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)

NPDES NO: NC0003573 DISCHARGE NO:
FACILITY: DuPont - Fayetteville Works
STREAM: Cape Fear River
LOCATION: DuPont River Pump Station
UPSTREAM
002
MONTH: September YEAR: _
2012
COUNTY: Bladen
STREAM: Cape Fear River
LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
DOWNSTREAM
DWQ Form MR -3 (Revised 7/2000)
O V
00010 00400 00310 00610 00530 00094
Y
V C
_O 0)
U N N w
o a o O E >
a�
a o L v
=3U a V
E 4) LO o u E o
~ E U) m o U
LL
rn
H m 6
HRS °C units mal ma/I rn„
wini „mti m
5
3
2
4
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Average
Maximum
Minimum

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements L
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
Ellis H. McGaughy -Plant
Permittee (Please print or t)
28306-7332
one Number
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co) 00610 Ammonia Nitrogen
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00625 Total Kjeldha)
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water C
The monthly average for fecal coliform is to be reported as a
facility's permit for reporting data
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics
34235 Benzene
34481 Toluene
38260 WAS
39516 PCB's
50050 Flow
liance Group at
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
extension 581 or 534
SIC mean. Use only units designated in the
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
00625 Total Kjeldha)
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water C
The monthly average for fecal coliform is to be reported as a
facility's permit for reporting data
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics
34235 Benzene
34481 Toluene
38260 WAS
39516 PCB's
50050 Flow
liance Group at
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
extension 581 or 534
SIC mean. Use only units designated in the
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water C
The monthly average for fecal coliform is to be reported as a
facility's permit for reporting data
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics
34235 Benzene
34481 Toluene
38260 WAS
39516 PCB's
50050 Flow
liance Group at
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
extension 581 or 534
SIC mean. Use only units designated in the
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
liance Group at
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
extension 581 or 534
SIC mean. Use only units designated in the
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)