201706201316

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO, 001 MONTH February YEAR 2013
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED C� PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV, OF WATER QUALITY MAR 2 8 ?01 X aMk
DENR �3 B (SIGNATUf E OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DEM Form MR -i (12/93)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements I_`_._I
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements u
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a'time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H.
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead '
01092 Zinc
01105 Aluminum
Chlorine
327
01147 Total Selenium 71880 Formaldehyde
31616 Fecal Coliform 71900 Mercury
30 Total Phenolics 81551 Xylene
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Parameter Code assitance maybe obtained by calling the Water Quality Compliance Group at (91
9) 733-5083, extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
(b) (2) If sig(D) ned by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead '
01092 Zinc
01105 Aluminum
Chlorine
327
01147 Total Selenium 71880 Formaldehyde
31616 Fecal Coliform 71900 Mercury
30 Total Phenolics 81551 Xylene
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Parameter Code assitance maybe obtained by calling the Water Quality Compliance Group at (91
9) 733-5083, extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
(b) (2) If sig(D) ned by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead '
01092 Zinc
01105 Aluminum
Chlorine
327
01147 Total Selenium 71880 Formaldehyde
31616 Fecal Coliform 71900 Mercury
30 Total Phenolics 81551 Xylene
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Parameter Code assitance maybe obtained by calling the Water Quality Compliance Group at (91
9) 733-5083, extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
(b) (2) If sig(D) ned by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO, 002 MONTH February YEAR 2013
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED C� PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES �
DIV. OF WATER QUALITY X
DENR (SIGNATURE bF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050 00010 00400 00310 00340 00951 51521 00665
T00600TGP3BFLOW
WW
o EFF X D
O V o>
0 0 w
o d F p a'Q in 0 ? o O J Q
0 J Q w O CD
O JO la- 2
ov 3 aW Lu p c) p u -z Oa
N Q' U O J 0: F'U) FF 20
I<
a 0 J 11W- W m u- a. V = Z O F
o
0 0 g a
HRS
HRS
Y/N
MGD
`C
UNITS
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
P/F
1
6860
24
Y
t20m3O5
M',
7.51
2
08001
24
20.534
1-1 It
; 3'
0800
1 24
20:355
4
08001
24
Y
20.379
11
7.52
5
0860
'' 24
" ° Y
20:672
12 `.
7.04
<2.0"
_ <30:0
6
0800
24
Y
20.681
11
7.34
15.5
0.87
2.65
7:
0800
> 24
Y%23s'696.-"
11
7:60 ".
8
0800
24
Y
20.775
11
7.51
`9.
0800
,r24,
20:379"
10
08001
24
20.745
11
0806 1
1 24
Y 1
21:030
13
7.41
p
12
08001
24
Y
21.051
13
7.46
10 13
0800
124
Y
20:425.,
13
7:46
0.032
14
08001
24 1
Y
20.255
13
7.50
15
oaoo
'24
Y
20:621
13
7:61 ,
16
08001
24
20.222
=17
0800
24
19:802
18
0800
24
Y
20.294
12
7.51
19
0800
24
Y ,.
20:339 1
12
7.70 t
'
vIj
20
0800
24
Y
20.132
12
7.64
21
0800
., 24
Y
20.554
: '11
7.59
22
0800
24
Y
20.681
11
7.55
23
0800 1
24 1
21111
24
08001
24 1
20.670
25
08001
24 1
Y
20324
11 1
7.70
26
0800
24
Y
22.769
11
7.62
27
0800
'24
Y
20.298
> '11
::<7M
28
0800
24
Y
20.313
11
7.59
20
0800
24
30 0800 24
31 0800 24 ;.
AVERAGE20.715
12
0.0
0:0
15.5
0.032
0.87
2.65
P
,
-
MAXIMUM t23!695
13 7.70 `
<2
<30
15.5
0 032
0:87 ; `
2:65 '
P "'
,_.
MINIMUM
19.802
11 7.04
<2
<30
15.5
0.032
0.87
7 2.65
P
"Comp:
(C)
Grab
(G)
G G
C
C
G
G
C
C
C
Monthly Limit
Daily limit 6=9
DEM Form MR -I (12/93)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements L
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy -Plant
Permittee (Please print or fi
f7i
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332
cess
678-1315
Phone Number
Date
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the repo
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
*" If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 0
(D)
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the repo
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
*" If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 0
(D)
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the repo
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
*" If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 0
(D)
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the repo
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
*" If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 0
(D)

Effluent Toxicity Report Form weChronic Pass/Fail and Acute LC50 Date: 02/22/13
Facility: DUPONT FAYETTEVILLE WORKS NPDES#: NC0003573 Pipe#: 002 County: BLADEN
Laborat yPe jfmjlng Test: MERITECH LABS, INC.
X Comments: dilution water batch 13
Signa ure of Operator in Responsible C Rrge also used: hard -42, cond-159
E�
Work Order*
• -SciencesMAIL •• • of WaterQuality
Raleigh,N.C. DENR
1621 Mail Service Center
•Carolina
Chronic Pass/Fail Reproduction Toxicity Test
�ONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced JII27I26I26I26I24I24I19I26I26I22I20I24
Effluent %: 3.30
CREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced �I29I28I27�23�27�27�27�25�25�23�23�27
Adult (L)ive (D)ead IIL IL IL IL IL IL IL IL �L L IL IL
Chronic Test Results
Calculated t = -1.831
Tabular t = 2.508
Reduction = -7.24
Control CV
10.708%
0 control orgs
producing 3rd
brood
1000
PASS FAIL
X
Check One
.0
1st sample 1st sample 2nd sample Complete This For Either Test
r--
Control
Treatment 2
8.08 8.00
8.08 7.97
8.02 8.11
8.01 8.10
8.08 8.06
8.10 7.92
s
�Cs� Late:
Collection (Start) Date
Sample 1:02/11/13 Sample 2: 02/13/13
Sample Type/Duration 2nd
1st PIF
s s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d IU M M
t t t Sample 2 X 24 hrs T P P
n
1st sample 1st sample 2nd sample
Control
.7
Treatment 2
74
0 Mortality
Avg.Reprod.
0.00
Control
24.17
Control
0.00
Treatment 2
25.92
Treatment 2
7.75
7.47
Control CV
10.708%
0 control orgs
producing 3rd
brood
1000
PASS FAIL
X
Check One
.0
1st sample 1st sample 2nd sample Complete This For Either Test
r--
Control
Treatment 2
8.08 8.00
8.08 7.97
8.02 8.11
8.01 8.10
8.08 8.06
8.10 7.92
s
�Cs� Late:
Collection (Start) Date
Sample 1:02/11/13 Sample 2: 02/13/13
Sample Type/Duration 2nd
1st PIF
s s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d IU M M
t t t Sample 2 X 24 hrs T P P
n
1st sample 1st sample 2nd sample
Control
.7
Treatment 2
74
7.59
7.76
7.70
7.80
7.57
8.02 8.11
8.01 8.10
8.08 8.06
8.10 7.92
s
�Cs� Late:
Collection (Start) Date
Sample 1:02/11/13 Sample 2: 02/13/13
Sample Type/Duration 2nd
1st PIF
s s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d IU M M
t t t Sample 2 X 24 hrs T P P
n
1st sample 1st sample 2nd sample
Control
.7
Treatment 2
74
7.59
7.76
7.70
7.80
7.57
8.08 8.06
8.10 7.92
s
�Cs� Late:
Collection (Start) Date
Sample 1:02/11/13 Sample 2: 02/13/13
Sample Type/Duration 2nd
1st PIF
s s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d IU M M
t t t Sample 2 X 24 hrs T P P
n
1st sample 1st sample 2nd sample
Control
.7
Treatment 2
74
7.59
7.76
7.70
7.80
7.57
7.75
7.47
s
�Cs� Late:
Collection (Start) Date
Sample 1:02/11/13 Sample 2: 02/13/13
Sample Type/Duration 2nd
1st PIF
s s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d IU M M
t t t Sample 2 X 24 hrs T P P
n
1st sample 1st sample 2nd sample
Control
.7
Treatment 2
74
7.59
7.76
7.70
7.80
7.57
7.75
7.47
7.87
7.76
7.97
7.80
7.75
7.47
7.79
7.48
7.80
7.47
riarGSleS s (mg/ 1 ) 4 Z ,,,,,,,, ,,,,,,,,,
Spec. Cond.(umhos) 160 478 398
Chlorine (mg/1) ,,,,,,,, 0.44 0.12
LC50/Acute Toxicity Test Sample temp. at receipt (°C) .,,,,,,,BEDROOMS:0.9 0.2
(Mortality expressed as 0, combining replicates)
Note: Please
0�0 96 01 0° % % o % % Concentration Complete This
Section Also
ow 01 �00 w06 % % Mortality
start/end start/end
LC50 = 0 Method of Determination
Control
950 Confi ence Limits Moving Average Probit
Spearman Karber - Other
I�
Organism Tested: Ceriodaphnia dubia Duration (hrs):
Copied from DWQ form AT -1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.
High
f'nn n
I�
Organism Tested: Ceriodaphnia dubia Duration (hrs):
Copied from DWQ form AT -1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

NPDES NO: NC0003573
DISCHARGE NO: 002 MONTH: February YEAR: 2013
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM
DWQ Form MR -3 (Revised 7/2000)
DOWNSTREAM

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements LJ
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements LJ
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC HwV 87 W
Ellis H.
by -Plant
pant or r
.'W A i
28306-7332
10) 67$-1315
Phone Number
lJ�
Date
October 31, 2016
Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co) 00610 Ammonia Nitrogen
00082 Color DMI
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Js
)
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
00300
Dissolved Oxygen
01034
Chromium
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
01037
Total Cobalt
00400
pH
00745
Total Sulfide
01042
Copper
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
01045
Iron
00545
Settleable Matter
00940
Total Chloride
01051
Lead
Parameter Code assitance
may be obtained
by calling the
Water Quality
Compliance Grou
facility's permit for reporting data
01092 Zinc Chlorine
01105 Alumm
inu
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
71880 Formaldehyde
71900 Mercury
81551 Xylene
e
at [phone], extension 581 or 534
only units designated in the repot
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 0
(D)
71880 Formaldehyde
71900 Mercury
81551 Xylene
e
at [phone], extension 581 or 534
only units designated in the repot
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 0
(D)