201706201314

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO, 001
FACILITY NAME DuPont - Fayetteville Works CLASS
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
MONTH May
3 COUNTY
YEAR 2013
Bladen
GRADE 4 PHONE [phone]
CHECK BOX IF ORC HAS CHANGED
PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV, OF WATER QUALITY �� �a I;� 013
X (9e ♦' 9� �
/
(SIGNA RE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
DENR
1617 MAIL SERVICE CENTER
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050 00010 1 00400
00310 1 00530 00556 1 39700 39700 1 01034 01042 01067 01092
E
FLOW
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=O
=Wo
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HRS
HRS
Y/N
MGD
'C
UNITS
Lb/Day
Lb/Day
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
Lb/Day
Lb/Day
1
08060
24
Y
0.853
23.
7.79;
44:1
<35.6
I
2
0800
24
Y
0.823
3
0800
24
Y
0.798
4
0800
24
0.800
5
0800
24
0.816
6
0800
24
Y
0.833
21
7.70
13.9
54.2
7
0800
24
Y
1 0.763.
21
7.73
18.5._
'<21.0
8
08001
24
Y
0.739
20
7.80
33.3
<30.8
<5.0
9
08001
24 _
Y
0.859
10
08001
24
Y
0.869
11
0800
24
0.881
12
0800
24
0.823
13
0800
24
Y
0.812.
21'
7.86._
13.5.;
<33.9
14
0800
24
Y
0.746
23
7.88
20.5
32.4
15
0800
24
Y
; 0.807
22
7.90.
20.2
<33.7
16
0800
24
Y
0.914
17
0800
24
Y
0.791
18
08001
24
0.856
19
08001
24
0.924
20
08001
24
Y
0.996
27
7.92
29.9
101.3
21
0800
24
Y
0.976
26
7.90
33.4
41.5
22
0800
24
Y
0.894
27
7.93
34.3
54.4
23
0800
24
Y
0.743
24
0800
24
Y
0.766
25
0800
24
0.788
26
08001
24
0.731
27
0800
' 24.
*
0:797
23.3
73:8
_.
28
0800
24
Y
0.805
25
7.84
25.5
63.8
29
o800
24
Y
0.884:
25
7.86
31.0
42.0
30
0800
24
Y
0.898
25
7.85
31 0800 24 Y
0.942
AVERAGE
0.836
24
26.3
35.6
0
MAXIMUM
0.996
27 7.93
44.1
101:3
<5:0
MINIMUM
0.731
20 7.70
13.5
<21
<5.0
Comp. (C) Grab (G)
G G
C
C
G
G
G
G
G
G
G
Monthly Limit
2.0
182.6
303.1
0.113
8.36
10.91
12.72
7.90
Daily Limit 6-9 484.7
981.5 0.5
20:85
25.44
29.96
19.65
DEM Form MR -I (12/93) *Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01092 Zinc
01105 Aluminum
01032 Hexavalent Chromium 01147 Total Selenium
01034 Chromium 31616 Fecal Coliform
32730 Total Phenolics
01037 Total Cobalt 34235 Benzene
01042 Copper 34481 Toluene
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water Qus
The monthly average for fecal coliform is to be reported as a C
facility's permit for reporting data
38260
MBAS
39516
PCB's
50050
Flow
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
00665 Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
01027 Cadmium
01092 Zinc
01105 Aluminum
01032 Hexavalent Chromium 01147 Total Selenium
01034 Chromium 31616 Fecal Coliform
32730 Total Phenolics
01037 Total Cobalt 34235 Benzene
01042 Copper 34481 Toluene
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water Qus
The monthly average for fecal coliform is to be reported as a C
facility's permit for reporting data
38260
MBAS
39516
PCB's
50050
Flow
01027 Cadmium
01092 Zinc
01105 Aluminum
01032 Hexavalent Chromium 01147 Total Selenium
01034 Chromium 31616 Fecal Coliform
32730 Total Phenolics
01037 Total Cobalt 34235 Benzene
01042 Copper 34481 Toluene
01045 Iron
01051 Lead
Parameter Code assitance may be obtained by calling the Water Qus
The monthly average for fecal coliform is to be reported as a C
facility's permit for reporting data
38260
MBAS
39516
PCB's
50050
Flow
[phone] extension
lance Group at
tIC mean. Use only units de
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 121 (D
)
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
581 or 534
reporting

NPDES PERMIT NO, NC0003573
EFFLUENT
DISCHARGE NO, 002 MONTH MAV YPAP
FACILITY NAME DuPont = Fayetteville Works
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton)
CLASS 3 COUNTY Bladen
(2)
2013
GRADE 4 PHONE [phone]
CHECK BOX IF ORC HAS CHANGED
PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY
X
!�
DENR
(SIGNATU E OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050 00010 00400
00310 00340 00951 51521 00665 00600 TGP3B
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a
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HRS
HRS
Y/N
MGD
*C
UNITS
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
P/F
1
0800
24
Y
20.615
-24
7.35
2
0800
24
Y
20.697
24
7.31
3
00
24
Y
14.529
24
7.48
4
00
j0800
24
9.772
5
` 24
10.333
6
oo
24
Y
10.927
23
7.39
7
o8o0
24
Y
9.721
24 "'
' 7.42
3:9
<30.0
060:
3:12
8
0800
24
Y
9.318
24
7.45
0.030
9
0800
24
Y
96286
24
7.51
10
0800
24
Y
10.289
25
7.36
11
0800
24
10.388
12
0800
24
10.366
13
0800
24
Y
: 12:649 _
25
7.30
P
14
osoo
24
Y
10.750
25
7.34
15
0800
24
Y
11.475
24
7.35
13.6
16
osoo
24
Y
17.655
24
7.37
17
osoo
24
Y
20.747
24
7.41
v
18
0800
24
20.058
19
0800
24
200407
20
0800
24
Y
24.110
25
7.35
21
0800
24
Y
24.309
24
7:39
22
0800
24
Y
22.946
25
7.43
23
0800
24
Y
19.990
26
7.37
24
0800
24
Y
25.084
25
7.22
25
0800
24
7.741
9F
26
0800
24
9.239
27
osoo
24
9.754
28
0800
24
Y
9.883
26
7.20
29
'0800
24
Y
11.674
26
7.24
30
0800
24
Y
19.619
26
7.22
31 0800 24 Y
22.511 ;
26 7.29
AVERAGE
15.059
25
3,9
0.0
13.6
0.030
0.60
3.12
P
MAXIMUM
25.084
26 7.51
3.9
<30
13.6
0.030
0.60
3.12
P
MINIMUM
7.741
23 7.20
3.9
<30
13.6
0.030
0.60
3.12
P
Comp.
(C)
Grab
(G)
G G
C
C
G
G
C
C
C
Monthly Limit
Daily Limit g-9
DEM Form MR -I (12/93) *Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BOD5
00340
COD
00400
pH
00530
Total Suspended
00929
Residue
00545
Settleable Matter
Parameter Code assitance
Ellis H.
NC, 28306-7332
-Plan# Manager
5
Phone
PARAMETER CODES
00556 Oil &Grease 00951 Total Fluoride
00600 Total Nitrogen 01002 Total Arsenic
00610 Ammonia Nitrogen
00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00630 Nitrates/Nitrites
00665
Total
Phosphorous
00720
Cyanide
Zinc
00745
Total
Sulfide
00927
Total
Magnesium
00929
Total
Sodium
00940
Total
Chloride
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
01032 Hexavalent Chromium 01147
be obtained by calling the Water
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean.
facility's permit for reporting data
Fecal Coliform
Total Phenolics 81551
Benzene
Toluene
MB
PCB's
Total Selenium
01034 Chromium 31616
32730
01037 Total Cobalt 34235
01042 Copper 34481
38260
01045 Iron 39516
01051 Lead 50050 Flow
Date
October 31, 2016
Permit Exp. Date
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
at [phone], extension 581 or 534
Use only units designated in the repo
* ORC must visit facility and document visitation of facility as required per 15A NCAC
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 05/23/13
Facility: DUPONT FAYETTEVILLE WORKS NPDES#: NC0003573 Pipe#: 002 County: BLADEN
Labora,tQry Perform ng Test: MERITECH LABS, INC.
Comments*
X
ure
• of
ponsible
upervisor
* PASSED: -11.740 Reduction
Work • der* ---
Environmental Sciences
MAIL •' TO: of - Quality
Raleigh,1621 Mail Service Center
North C •Carolina
Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced II24I22I26I25I24I23I26I24I16�20I22I12
Adult (L)ive (D)ead IIL IL IL IL �L IL �L �L �L �L �L �L
effluent a: 3.30
CREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced II24I24I26I26I26I27I22I28I22I20�25I25
Adult (L)ive (D)ead IIL IL IL IL IL IL IL IL IL IL IL IL
pH
Control
Treatment 2
1st sample 1st sample 2nd sample
8.05
o Mortality
t
8.12
a
8.09
r
d
8.09
0
s s
o Mortality
t
e
a
n
r
d
t
1st sample
8.12
o Mortality
8.07
e
a
8.07
r
8.05
0
0
t
1st sample
8.13
o Mortality
t
e
a
n
r
d.
t
1st sample
8.13
o Mortality
8.05
7.51
a
8.09
r
8.02
0
0
t
2nd sample
.;78 7.55
n n
vvControl
Treatment 2
7.94
o Mortality
7.55
7.51
a
n
r
d
t
2nd sample
.;78 7.55
n n
vvControl
Treatment 2
7.94
o Mortality
7.55
7.51
7.74
7.83
7.54
7.53
0
0
7.91
o Mortality
7.58
7.51
7.74
0.00
Treatment 2
7.54
0
7
o Mortality
7_.77
7.51
22.00
Control
0.00
Treatment 2
Chronic Test
pr
Results
Calculated t =
Tabular t =
Reduction = -11.74
Control CV
19089a
.
PASS FAIL
control orgs X
oducing 3rd
bro1001000 Check Check One
Complete This For Either Test
Test Start Date: 05/15/13
Collection (Start) Date
Sample 1: 05/13/13 Sample 2: 05/15/13
S
s
t •e
ample Type/Duration 2nd
1st P/F
Grab Comp, Duration D
I S S
Sample 1 •X 24 hrs L A A
U M M
Sample 2 X 24 hrs T P P
Hardness(mg/1) 44
Spec. Cond.(umhos) 169 588 647
Chlorine (mg/1) 0. 1 0. 1
LC50/Acute Toxicity Test Sample temp, at receipt(°C)wom9awasym1.0 1.2
(Mortality expressed as o, combining replicates)
0 Note: Please
o Mortality
Avg .Reprod.
0.00
Control
22.00
Control
0.00
Treatment 2
24.58
Treatment 2
0
0
Control CV
19089a
.
PASS FAIL
control orgs X
oducing 3rd
bro1001000 Check Check One
Complete This For Either Test
Test Start Date: 05/15/13
Collection (Start) Date
Sample 1: 05/13/13 Sample 2: 05/15/13
S
s
t •e
ample Type/Duration 2nd
1st P/F
Grab Comp, Duration D
I S S
Sample 1 •X 24 hrs L A A
U M M
Sample 2 X 24 hrs T P P
Hardness(mg/1) 44
Spec. Cond.(umhos) 169 588 647
Chlorine (mg/1) 0. 1 0. 1
LC50/Acute Toxicity Test Sample temp, at receipt(°C)wom9awasym1.0 1.2
(Mortality expressed as o, combining replicates)
0 Note: Please
0
0
0
o
a
o
0
0
0
0
0
%
0
%
0
%
0
0
0
0 %
% 0
0
Concentration
Mortality
start/end
LC50 = o Method of Determination
950 Confi ence Limits Moving Average Probit
Spearman Kar`ber - Other
Organism Tested: Ceriodaphnia dubia Duration(hrs):
.:opiea rrom DWQ form AT -1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
Complete This
Section Also
start/end
1D
Control
High
f nn n
H
D.O.

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: May YEAR: 2013
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM DOWNSTREAM
00010 00400 00310 00610 00530 00094 51521
x U v
U C U
CaU a > 0
(D a (n o x 2 E
.C)� N .=3 = AO ` 'V N
CU N N O_ O O U D O
E m U
1- a `n U) a) O U O
E
° m a) =3a
� m , ° a
HRS °C units mg/L mg/L #/100m1 µmho/cm ug/L
1 .
f►:
DWQ Form MR -3 (Revised 7/2000)
3
Y
U
_O
U
o
"
F-
00010
00400
00310
00610
00530
00094
aa)
N
aur
O
mU a)
a
a)
U
v
O
O
m
C
m
x
co
°
E cu
O
O
U
ro 0
ua)
_
w
a
U
HRS
°C
units
mg/L
mg/L
#/100ml
µmho/cm
1
F64
2
3
7
4
8
11:00
0.016
9'
6
10
7,
11'
8
12
9
13
10
14
11`
15
12
16
13
17
14
18
15
19
16
20
17
21
18
22
19
23
20
24
21
25
22
26
23
27
24
28
25
29
26
30
27
31
Average
28
0.016
Maximum
10.016
Minimum
0.016
DWQ Form MR -3 (Revised 7/2000)
m
°
Y
U
_O
U
o
"
F-
00010
00400
00310
00610
00530
00094
aa)
N
aur
O
mU a)
a
a)
U
v
O
O
m
C
m
x
co
°
E cu
O
O
U
ro 0
ua)
_
w
a
U
HRS
°C
units
mg/L
mg/L
#/100ml
µmho/cm
1
2
3
4
5,
6
7,
8
9
10
11`
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Average
Maximum
Minimum

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BOD5
00340
COD
00400
pH
00530
Total Suspended
Residue
00545
Settleable Matter
00556
00600
00610
00625
00630
00665
00720
00745
00927
00929
00940
Ellis H. McGaughy -Plant
Permittee (Please print or v
Ile, NC, 28306-7332
PARAMETER CODES
Oil &Grease 00951 Total Fluoride
Total Nitrogen 01002 Total Arsenic
Ammonia Nitrogen
Total Kjeldhal 01027
Nitrogen
Nitrates/Nitrites
ber
Total Phosphorous
Cyanide
Total Sulfide
Total Magnesium
Total Sodium �
Total Chloride
Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Date
October 31, 2016
Permit Exp. Date
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the repo
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A.0202
(b) (5) (B).
ng
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
327
Date
October 31, 2016
Permit Exp. Date
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the repo
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A.0202
(b) (5) (B).
ng
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)