201706201311

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO, 001 MONTH November YEAR 2013
FACILITY NAME DuPont - Fayetteville Works CLASS 3
COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY X 071440Z
DENR (SIGNAT RE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050 00010 00400 00310 00530 00556 39700 39700 01034 01042 01067 01092
FLOW
o
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=N
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F
FQ-
OF
c
O
a
O
=� f-
Q q
F
FQ-
O
O
=
=
O
F
O
HRS
HRS
Y/N
MGD
*C
UNITS
Lb/Day
Lb/Day
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
Lb/Day
Lb/Day
1
68001
24
Y
02980
2
08001
24
0.958
3
08001
24
1 0.835
4
08001
24
B
1.000
27
1 7,58
21.7
108.4
5
08001
24
B
0.919
26
7.55
19.9
90.4
6
08001
24
B
0.972
24
7.66
25.1
110.2
<5.0
7
;0900
24
B
1.003�"`
:.,
8
o800l
24
B
0.914
.
9
108001
24
1
06900
10
08001
24
0.892
11
08001
24
Y
0.884
22
7.85
37.6
57.5
12
08001
24
Y
0.832
22
7.81
28.4
45.8
13
08001
24
Y
0.626
21
7.92
35.5,
<512
14
08001
24
Y
0.775
15
08001
24
Y
0:813
16
08001
24
0.899
17
08001
24
0.887
18
08001
24
Y
0.790
24
7.82
29.0
36.9
19
06001
24 1
Y
09870
24
7.80
20.3
<36.3
-
w
�-
20
08001
24
Y
0.782
22
7.89
15.7
<32,6
21
08001
24
Y
0.922
22
08001
24
Y
0.888
23
08001
24
0:901
a
24
08001
24
0.851
39.0
68.1
25
08001
24
Y
0.912
16
7.91
20.5
<76.1
26
08001
24
Y
1.007
16
7.85
23.5
55.4
27
0.800
'24
Y
0,968
1 17
7.82
28
0800
24
0.820
29
o800
24
0.853
30
0800
24
0.925
g22
31 0800 24
AVERAGE
0.886
26.4
47.7
0
MAXIMUM
1.007
27 7.92
39.0
110:2
<5.0
MINIMUM
0.626
16 7.55
15.7
<32.6
<5.0
Comp. (C) Grab (G)
G G
C
C
G
G
G
G
G
`' G
G
Monthly Limit
2.0
182.6
303.1
0.113
8.36
10.91
12.72
7.90
Daily Limit
6-9
484.7
981.5
0.5
20.85
25.44
29.96
19.65
DEM Form MR -I (12/93) *Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
Ellis H.
NC
678-1315
Phone
October 31, 2016
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
0066$; Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
Parameter Code assitance maybe obtained i
The monthly average for fecal coliform is
facility's permit for reporting data
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics 81551
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
g the
Water Quality Compliance Group at
reported as a GEOMETRIC mean. Us
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
X19) 733-5083, extension 581 or 534
only units designated in the repo
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
ng
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506
00610 Ammonia Nitrogen
00625 Total Kjeldhal
Nitrogen
00630 Nitrates/Nitrites
0066$; Total Phosphorous
00720 Cyanide
00745 Total Sulfide
00927 Total Magnesium
00929 Total Sodium
00940 Total Chloride
Parameter Code assitance maybe obtained i
The monthly average for fecal coliform is
facility's permit for reporting data
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics 81551
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
g the
Water Quality Compliance Group at
reported as a GEOMETRIC mean. Us
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
X19) 733-5083, extension 581 or 534
only units designated in the repo
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
ng
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506
The monthly average for fecal coliform is
facility's permit for reporting data
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092 Zinc
01105 Aluminum
327
01147 Total Selenium
31616 Fecal Coliform
30 Total Phenolics 81551
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
g the
Water Quality Compliance Group at
reported as a GEOMETRIC mean. Us
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
X19) 733-5083, extension 581 or 534
only units designated in the repo
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
ng
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506
g the
Water Quality Compliance Group at
reported as a GEOMETRIC mean. Us
Chlorine
71880 Formaldehyde
71900 Mercury
Xylene
X19) 733-5083, extension 581 or 534
only units designated in the repo
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
ng
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO,
FACILITY NAME DuPont - Fayetteville Works
002
CLASS
MONTH November YEAR 2013
3
COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV, OF WATER QUALITY X
DENR (SIGNAT RE OF OPERATOR IN RESPONSIBLE CHARGE) DATE J
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699A617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050 00010 1 00400 00310 00340 00951 1 51521 00665 00600 TGP3B
d d FLOW
E U5 W O !n
m o ,� EFF X �cn v
Lu w 0¢ o w
2 v NINF EJ �..'= 0 ❑ OU J W J
E O Z
Qo 1= LuN N O O =j0 F2 FO 0 V
°
00 `o v a. LU v M LL 0an Ow Ix
N w 0 O J Q.' Q �'.. U) �-- 1-' = O
N A i-
a a - Lu m u aa* U S Z V F-
0 0 o a
HRS
HRS
Y/N
MGD
'C
UNITS
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
P/F
1
08001
24
Y
11.012
20
7.18
2
08001
24
11.624
3
40800
24
10.775
4
08001
24
B
11.560
21
7.32
P
5
08001
24
B
11.669
19
7.27
2.8
<300
ell
Ose9l,j
elm54,l,
ell
6
08001
24
B
11.890
20
7.36
34.9
1 L
7-
080o
24
'B
"11°:179%
21
.;7x35
8
08001
24
B
11.792
18
7.38
9
08001
24
11:674
10
08001
24
11.334
11
0800
Ieii124
Y
10.068
19
7.30
12
08001
24
1 Y
10.268
18
7.42
13
.'08001
24
1 Y
8.166
16
7.64
14
08001
24
1 Y
8.938
14
7.67
15
08001
24 1
Y
9.532
14
7.60
16
08001
24
9.126
17
08001
24
9.115
18
08001
24
Y
9.500
20
7.95
19
08001
24
Y
8116
19
7.96
20
08001
24
Y
10.177
17
8.16
0.027
21
08001
24
Y
9:250
16
8.10
22
08001
24
Y
9.468
16
8.13
23
08001
24
9.424
24
0800
24
9.214
25
08001
°24
Y
9:376
15
8.05
26
08001
24
Y
14.995
16
7.96
27
o800l
24 1
Y
10.997
17
7.90
28
0800
24
8.932
29
0800
24
*
9.768
30
0800
24
10.470
31 0800 24
AVERAGE
10.314
18
2.8
0.0
34.9
0.027
0.93
1.54
P
MAXIMUM
140995
21 8616 1
2.8
<30
34.9
0.027
0.93'
1.54
P
MINIMUM
8.166
14 7.18
2.8
<30
34.9
0.027
0.93
1.54
P
Comp.
(C) Grab
(G)
G G
C
C
G
G
C
C
C
Monthly Limit
Daily Limit 6-9
DEM Form MR -I (12/93) *Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penal ' ting false information,
including the possibility of fines and imprisonment for ay io ation.5sj
22828 NC Hwy 87
Permittee Address
678-1315
Phone Number
1r3IQC97 fZ_/S-zo�3
October 31, 2016
Permit
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
01027 Cadmium
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
01037
Total Cobalt
34235
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
00300
Dissolved Oxygen
38260
MBAS
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545 Settleable Matter 00940 Total Chloride
01092 Zinc Chlorine
01105 Aluminum
01032 Hexavalent Chromium 01147 Total Selenium
01034
Chromium
31616
Fecal Coliform
32730
Total Phenolics
01037
Total Cobalt
34235
Benzene
01042
Copper
34481
Toluene
38260
MBAS
01045
Iron
39516
PCB's
01051
Lead
50050
Flow
Parameter Code assitance maybe obtained by calling the Water Quality Compliance Group at (919) 733
The monthly average for fecal coliform is to be repo
facty's permit for reporting data
as a GEOMETRIC mean. Use only un
71880 Formaldehyde
71900 Mercury
81551 Xylene
extension 581 or 534
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
signed by other than the premittee, delegation of signatory authority must eon file with the state per 15A NCAC 26 .0506
(b) (2) (M
in the reporting

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 11/14/13
Facility: DUPONT FAYETTEVILLE WORKS NPDES#: NC0003573 Pipe#: 002 County: BLADEN
Laboratory P o ing Test: MERITECH LABS, INC.
X
Comments*
Signa ure Ot qp0rator in Responsible C ar_QP
ITignature o. La oOry Supervisor * PASSED: 2.940 Reduction
Work Order: Environmental Sciences Branch
MAIL ORIGINAL TO: Div. of Water Quality
N.C. DENR
1621 Mail Service Center
North Carolina Ceriodaphnia Raleigh, North Carolina 27699-1621
Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results
Calculated t = 0.462
Tabular t 2w
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 0 R duction = 2.948
# Young Produced II26I28I26I19I24I24I20I18I26I21I18I22
Adult (L)ive (D)ead IIL IL IL IL IL IL IL ID IL IL IL IL
Effluent 0: 3.30
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced II23I24I24I19I26I15I25I25I24I16I21I22
Adult (L)ive (D)ead IIL IL IL IL IL IL IL IL IL IL IL IL
r--
Control
Control CV
1 5
.321%
0 control orgs
Iroducing 3rd
brood
91.70
PASS FAIL
x
Check One
1st sample 1st sample 2nd sample I Complete This For Either Test
8.15
Mortality
Avg.Reprod.
8.33
Control
22.67
Control
0.00
Treatment 2
22.00
Treatment 2
8.01
High
C'nn n
Control CV
1 5
.321%
0 control orgs
Iroducing 3rd
brood
91.70
PASS FAIL
x
Check One
1st sample 1st sample 2nd sample I Complete This For Either Test
8.15
7.96
8.06
8.10
7.96
7.94
7.50
8.09
7.62
8.06
7.77
7.96
7.60
7.50
8.01
High
C'nn n
s
8.15 8.00
8.07 7.95
Test start liate: 11/06/13
Collection (Start) Date
Treatment 2
s
Sample 1: 11/04/13 Sample 2: 11/06/13
Sample Type/Duration 2nd
1st P/F
s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d U M M
t t t Sample 2 X 24 hrs T P P
1st sample 1st sample 2nd sample
n n
v Control
Treatment 2
7.83
7.62
7.77
7.73
7.60
7.50
7.93
7.88
8.00
7.73
7:81
7.50
7.65
7.47
7.73
7.50
High
C'nn n
Chlorine(mg/1)
==
(Mortality expressed as Owl combining replicates)
0 0 0 0 o 0 0 0 0 0 0
0 0 0
0 0 0 0 0 0 0
Concentration
Mortality
start/end
LC50 = 0 Method of Determination
950 Confidence Limits Moving Average Probit
0 -- 0 Spearman Karber — Other —
Organism Tested: Ceriodaphnia dubia Duration hrs):
D.O.
.'
opiea from DWQ form AT -1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
Note: Please
Complete This
Section Also
start/end
Control
High
C'nn n
Concentration
Mortality
start/end
LC50 = 0 Method of Determination
950 Confidence Limits Moving Average Probit
0 -- 0 Spearman Karber — Other —
Organism Tested: Ceriodaphnia dubia Duration hrs):
D.O.
.'
opiea from DWQ form AT -1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
Note: Please
Complete This
Section Also
start/end
Control
High
C'nn n

�',
r �, i J�

NPDES NO: NC0003573
FACILITY: DuPont - Fayetteville Works
STREAM: Cape Fear River
LOCATION: DuPont River Pump Station
DISCHARGE NO:
002 MONTH: November YEAR:
COUNTY: Bladen
STREAM: Cape Fear River
LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
DWQ Form MR -3 (Revised 7/2000)
2013

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for kno a ions."
Sig ture of Mte
22828 NC Hwy 87 W, Fayetteville, N 8306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp, Date
FgATT
Tr
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BOD5
00340
COD
00400
pH
00530
Total Suspended
00929
Residue
00545
Settleable Matter
00556
Oil &Grease
00600
Total Nitrogen
00610
Ammonia Nitrogen
00625
Total Kjeldhal
Sulfide
Nitrogen
00630
Nitrates/Nitrites
00665
Total
Phosphorous
00720
Cyanide
00745
Total
Sulfide
00927
Total
Magnesium
00929
Total
Sodium
00940
Total
Chloride
00951 Total Fluoride
01002 Total Arsenic
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel 50060 Total
01077 Silver Residual
01092 Zinc Chlorine
01105 Aluminum
01147 Total Selenium 71880 Formaldehyde
31616 Fecal Coliform 71900 Mercury
30 Total Phenolics 81551 Xylene
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility
as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
327
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility
as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)