201706201221

EFFLUENT
NPDES PERMIT NO, NC0003673 DISCHARGE NO, 001 MONTH January YEAR 2014
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV, OF WATER QUALITY
DENR
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
Jamie R. Lewis / Arnold Ray Beard
GNATUfE OF OPERATOR IN RESPONSIBLE
REPORTTHIS SIGNATURE, I CERTIFY THAT THE CURATE ■ COMPLETE TO THE BEST OF • ■
DATE
DEM Form MR -I (12/93) *Holiday
0 0
00 0
3 0
0 30
00
9 00
00
0 0
0 0
06
092
FLOW
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W m
0
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=
=
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O
O
F
o Q
t-
F
HRS
HRS
Y/N
MGD
C UNITS Lb/Day
Lb/Day
mg/L
ug/L Lb/Day
Lb/Day
Lb/Day
Lb/Day
Lb/Day
1
0800
24
1.005
* 20.1
<41 #9
2
0800
24
Y
1.050
21 7.7
3
0800
24
Y
0.946;
ME
4
0800
24
0.935
5
0800
24
1.045
6
0800
24
Y
1.031
19 7.8 22.4
41.3
7
0800
24
Y
0.985 ':
18 7.9 <16.4
<271
rF
8
0800
24
Y
1.001
17 7.7 32.6
<41.7
9
0800
24
Y
0.905
10
0800
24
Y
0.917
11
0800
24
0.933
12
0800
24
1.151
13
0800
24
Y
1.118
19 M ` 44.8
<46.6
14
0800
24
Y
1.069
19 7.7 20.5
46.4
iifi
15
0800
24
Y
1.028
18 : 7.7: 27.4.
<42.9
16
0800
24
Y
1.042
17
0800
24
Y
1.063
18
o800
24
1.094
19
0800
24
1.072
20
0800
24
Y
0.976
18 7.6 89.5
21
0800
24
Y
1.076
18 7.7 ' 52.9
J719<550
22
0800
24
Y
1.198
17 7.7 59.9
23
0800
24
Y
1.146
24
0800
24
Y
1.046
25
8800
24
d 1.095
26 0800 24
1.192
27 0800 24 ' Y
1.176
18 7.7
47.1
84.3
28 o800 24 Y
1.098
17 7.7
29 0800 24 Y
1.029
17 7.7
31.8 ,
46.3 <'
3010800 24 Y
1.071
82.2
39.3
3110800 24 Y
1.068
AVERAGE
1.050
18
40.9
34.4
0
MAXIMUM
1.198
21 7.9
89.5
MINIMUM
0.905
17 7.6
<16.4
<27.1
<5.0
Comp. (C) Grab (G)
G G
c
C
G .,
G
G
G
G
G
G
Monthly Limit
2.0
182.6
303.1
0.113
8.36
10.91
12.72
7.90
Daily Limit 6-9 ' 484.7 981.5 0.5 "
20.85
25.44
'29.96
19.65
DEM Form MR -I (12/93) *Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on,corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy -Plant Man,
Perm'ttee tPlease pri t ortype)
Signature of Permittee**
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] �, October 31, 2016
Permittee Address Phone Number Permit Exp, Date
31616
Total Selenium
71880 Formaldehyde
PARAMETER CODES
00010
Temperature
00556
Oil &Grease
00951
Total Fluoride
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
50050
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
00300
Dissolved Oxygen
01034
Chromium
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
01037
Total Cobalt
00400
pH
00745
Total Sulfide
01042
Copper
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
01045
Iron
00545
Settleable Matter
00940
Total Chloride
01051
Lead
01067 Nickel 50060 Total
01077 Silver Residual
01092 Zinc Chlorine
01105 Aluminum
01147
Total Selenium
71880 Formaldehyde
Fecal Coliform
71900 Mercury
32730
Total Phenolics
81551 Xylene
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCB's
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)

EFFLUENT
NPDES PERMIT NO, NC0003573 DISCHARGE NO, 002 MONTH January YEAR 2014
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY
DENR
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
(SIGNATURF�OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
DATE
DEM Form MR -I (12/93) *Holiday
0
0 0
0
3 0
0 0
009
2
6
0 0
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FLOW
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HRS HRS YIN
MGD
`C
UNITS
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
P/F
1 0800 24
102591
2 0800 24 Y
10.549
15
7.5
3 0800 24 Y
9.843
14
7.4
4 0800 24
9.865
5 0800 24
9.968
6 0800 24 Y
10.743
15
7.5
7 0800 24 i Y
10.745
14
7.4
8 0800 24 Y
10.817
14
7.5
9 0800 24 ` Y
10385
14
7.6
10 0800 24 Y
12.000
15
7.6
11 080o 24
14.245
12 0800 24
10.780
13 0800 24 Y
11.605
16 `
7.5
14 0800 24 Y
11.717
16
7.6
15 0800 24 Y
11.282
15
7.5
0.012
16 0800 24 Y
10.751
15
7.6
17 0800 24 Y
10.984
15
7.6
18 0800 24
10.211
19 0800 24 =
10.973:
20 0800 24 Y
11.127
14
7.4
21 0800 24 ' Y
11.294'
14
7.5
0.94 1
4.01
22 0800 24 Y
10.342
13
7.5
23 0800 24 Y
10.617
13
7.6
24 0800 24 Y
10.557
13
7.5
25 0800 24
11.285
26 0800 24
11.467
27 0800 24 Y
8.834
14
7.7
28 0800 24 Y
8.517
13
7.7
29 0800 24 Y
7.906
13
7.7
30 0800 24 Y
8.867
12
7.7.
3110800 24 Y
10.503
13
7.8
AVERAGE
10.625
14
0.012T0s944v01
MAXIMUM
14.245
16
7.8
0.012
MINIMUM
7.906
12
7.4
0.012
0.94TffE
Comp, (C) Grab (G)
G
G `i
C
C
G
G
C
Monthly Limit
Daily Limit
6-9
DEM Form MR -I (12/93) *Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements LIJ
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Plant�Vlanager
Per ittee (Please print or ype)
Signature of Permitt ** Date
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp, Date
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic
00080 Color (Pt -Co) 00610 Ammonia Nitrogen
00082 Color (ADMI) 00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Hexavalent Chromium 01147
00300 Dissolved Oxygen 01034 Chromium31616
00310 BOD5 00665 Total Phosphorous 32730
00340 COD 00720 Cyanide 01037 Total Cobalt
00400 pH 00745 Total Sulfide 01042 Copper
00530 Total Suspended 00927 Total Magnesium
Residue 00929 Total Sodium 01045 Iron
00545 Settleable Matter 00940 Total Chloride 01051 Lead
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
81551
Total Selenium
Fecal Coliform
Total Phenolics
34235
34481
Toluene
38260
MBAS
39516
PCB's
50050
Flow
50060
71880
71900
Total
Residual
Chlorine
Formaldehyde
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506
(b) (2) (D)

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: January YEAR: 2014
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM
n1
�c
U
N
~
00010
00400
00310
00610
00530
00094
51521
a (n
N _3
N
U
CL
a)
I
2
a
U
MCI
o
N
>
a
0
O
00
c
o�
O
'0
?

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements L
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy -Plant
PerMlittee (Pleassje print or�+t
/f Aav(
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 (910) 678-115 October 31, 2016
Permittee Address Phone Number Permit Exp, Date
00010 Temperature
00076 Turbidity
PARAMETER CODES
00080 Color (Pt -Co)
00082 Color (ADMI)
00095
Conductivity
00300
Dissolved Oxygen
00310
BOD5
00340
COD
00400
pH
00530
Total Suspended
Residue
00545
Settleable Matter
00556
00600
00610
00625
00630
00665
00720
00745
00927
00929
00940
Oil &Grease 00951 Total Fluoride
Total Nitrogen 01002 Total Arsenic
Ammonia Nitrogen
Total I<jeldhal 1027
Nitrogen
Nitrates/Nitrites
Total
Phosphorous
Cyanide
Total
Sulfide
Total
Magnesium
Total
Sodium
Total
Chloride
0Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
3273
01147 Total Selenium
31616 Fecal Coliform
0 Total Phenolics 81551
34235 Benzene
34481 Toluene
38260 WAS
39516 PCB's
50050 Flow
50060
71880
71900
Total
Residual
Chlorine
Formaldehyde
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed yo el than the pre
mttee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506
(b) (2) (D)
3273
50060
71880
71900
Total
Residual
Chlorine
Formaldehyde
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed yo el than the pre
mttee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506
(b) (2) (D)

Field Parameter Bench Sheet
Revised Date: 07/27/12
r i ecnnician
I Comments
.101eN 11M y.00 % •u? Ice
I.79.H 122S u .ob to . c'1 2-0 a *3 e
W 04 .oD lb .04 -03 'lam
il,'yo. 1" a 14.00 to . a4 .03 Sv
0149 y .00 ko .off •� 3 SL
*The pH check buffer must be within +/- 0.1 1 H units of the buffers true value,