201706201219_redacted

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO, 001 MONTH August YEAR 2014
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY
DENR
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
Jamie R. Lewis / Arnold Ray Beard
r
R IS SIC
L
3NAT IE OF OPERATOR IN RESPONSIBLE
H SIGNATURE, I CERTIFY THAT THE •••T IS
• • • •
00 0 00010 00 00 003 0
0530 00556 39700 39700
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J
Q
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EFF X
p
W
HRS
HRS
Y/N
MGD
`C
UNITS
Lb/Day
Lb/Day
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
L fkiflq
t6
Fy�
g
1
0800
24
Y
0.912
2
0800
24
1.126
9 i
Law
3
0800
24
1.102
�Pq
4
0800
24
Y
1.068
28
7.6
24.0
94.4
5
6
0800
0800
24
24
1 Y
Y
1.024
1.122
28
29
7.6
7.6
1 29.0
33.7
100.8
95.4
1
<5.0
<1
<0.01
0.07
1DAR
0.05
0.09
qPd%TnN;
0.39
7
0800
24
Y
1.044 "
8
0800
24
Y
1.066
9
0800
24
1.021
10
0800
24
1.047
11
0800
24
Y
0.889
28
7.8
17.8
100.8
12
0800
24
Y
1.049
28
7.8
21.0
91.0
13
0800
24
Y
1.048 `
28
7.7
<17.6
' 97.9
14
0800
24
Y
1.127
15
0800
24
Y =
1.049
16
0800
24
1.140
17
0800
24
1:124
18
0800
24
Y
1.202
28
7.7
<20.0
176.4
19
0800
:24
Y
1.342
28
7.6
29.1
210.4
20
0800
24
Y
1.222
27
7.5
30.6
277.2
21
0800
24
Y
1.104
22
0800
24
Y
1.062
23
0800
24
0.989
24
0800
24
1.429
25
osoo
24
Y
1.337
28
7.5
30:1
<111.5
26
osoo
24
Y
1.119
28
7.7
21.5
126.9
27
0800
24
Y
1.327
28
7.6
33:2
154.9
28
0800
24
Y
1.228
2910800
24
Y
1.231
3010800
24
1.302
31 0800 24
AVERAGE
1.285
1.133
28
22.5
127.2
0
0
0
0.07
0.05
0.09
0.39
MAXIMUM
1.429
29 7.8
33.7
277.2
<5.0
<1
<0.01
0.07
0.05
0.09
0:39
MINIMUM
0.889
27 7.5
<17.5
91.0
<5.0
<1
<0.01
0.07
0.05
0.09
0.39
Comp. (C) Grab (G)
GG
C
C
G
G
G
G
G;
G
G
Monthly Limit
2.0
182.6
303A
0.113
8.36
10.91
12.72
7.90
Daily Limit 6-9 484.7
981.5
0.5
20.85
25.44
29.96
19.65
DEM Form MR -I (12/93)

Facility Status; (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
Itthe facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance; etc., and a time table for, improvements to be made..
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Ian
Permittee (Please pri° or
�, � r
a
Signature of Permit ee
Date
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic
00080 Color (Pt -Co) 00610 Ammonia Nitrogen
00082 Color (ADMI) 00625 Totai Kjeldhal 01027 Cadmium
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Hexavalent Chromium
00300 Dissolved Oxygen 01034 Chromium
00310 BOD5 00665 Total Phosphorous
00340 COD 00720 Cyanide 01037 Total Cobalt
00400 pH 00745 Total Sulfide 01042 Copper
00530 Total Suspended 00927 Total Magnesium
Residue 00929 Total Sodium 01045 Iron
00545 Settleable Matter 00940 Total Chloride 01051 Lead
01067 Nickel 50060 Total
01077 Silver Residual
01092 Zinc Chlorine
01105 Aluminum
01147
Total Selenium
31616
Fecal Coliform
32730
Total Phenolics
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCB's
50050
Flow
71880 Formaldehyde
71900 Mercu,"ry
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation.of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)

U
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Wednesday August 13, 2014
Report Number: L714757
Samples Received: 08/08/14
Client Project: TBL-25801
Description: DuPont
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Est. 1970
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed B t
Darren Reeder ESC Representative
La bora tory Certifca tion Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH -0197,
FL - E87487, GA - 923, IN - C -TN -01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures; 060302, 060303, and 060304.
Page 1 of 5

REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received August 08, 2014
Description DuPont
Sample ID E40806
Collected By Jamie Lewis
Collection Date 08/06/14 07:55
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Est. 1970
August 13, 2014
ESC Sample # : L714757-01
Site ID .
Project # : TBL-25801
Parameter Result Det. Limit Units Method Date Dil.
Base/Neutral Extractables
Acenaphthene
BDL
0.0010
mg/l
625
08/12/14 1
Acenaphthylene
BDL
0.0010
mg/l
625
08/12/14 1
Anthracene
Benzidine
BDL
0.0010
mg/l
625
08/12/14 1
Benzo(a)anthracene
BDL
BDL
0.010
0.0010
mg/l
mg/l
625
625
08/12/14 1
08/12/14 1
Benzo(b)fluoranthene
BDL
0.0010
mg/l
625
08/12/14 1
Benzo(k)fluoranthene
BDL
0.0010
mg/l
625
08/12/14 1
Benzo(g,h,i)perylene
BDL
0.0010
mg/l
625
08/12/14 1
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
BDL
BDL
0.0010
0.010
mg/l
mg/l
625
625
08/12/14 1
Bis(2-chloroethyl)ether
BDL
0.010
mg/l
625
08/12/14 1
08/12/14 1
Bis(2-chloroisopropyl)ether
BDL
0.010
mg/l
625
08/12/14 1
4-Bromophenyl-phenylether
BDL
0.010
mg/l
625
08/12/14 1
2-Chloronaphthalene
BDL
0.0010
mg/l
625
08/12/14 1
4-Chlorophenyl-phenylether
BDL
0.010
mg/l
625
08/12/14 1
Chrysene
Dibenz(a,h)anthracene
BDL
BDL
0.0010
0.0010
mg/l
mg/l
625
625
08/12/14 1
08/12/14 1
3,3-Dichlorobenzidine
BDL
0.010
mg/l
625
08/12/14 1
2,4-Dinitrotoluene
BDL
0.010
mg/l
625
08/12/14 1
2,6-Dinitrotoluene
BDL
0.010
mg/l
625
08/12/14 1
1,2-Diphenylhydrazine
BDL
0.010
mg/l
625
08/12/14 1
Fluoranthene
BDL
0.0010
mg/l
625
08/12/14 1
Fluorene
BDL
0.0010
mg/l
625
08/12/14 1
Hexachlorobenzene
BDL
0.0010
mg/l
625
08/12/14 1
Hexachloro-1,3-butadiene
BDL
0.010
mg/l
625
08/12/14 1
Hexachlorocyclopentadiene
BDL
0.010
mg/l
625
08/12/14 1
Hexachloroethane
BDL
0.010
mg/l
625
08/12/14 1
Indeno(1,2,3-cd)pyrene
BDL
0.0010
mg/l
625
08/12/14 1
Isophorone
BDL
0.010
mg/l
625
08/12/14 1
Naphthalene
Nitrobenzene
BDL
0.0010
mg/l
625
08/12/14 1
n-Nitrosodimethylamine
BDL
BDL
0.010
0.010
mg/l
mg/l
625
625
08/12/14 1
08/12/14 1
n-Nitrosodiphenylamine
BDL
0.010
mg/l
625
08/12/14 1
n-Nitrosodi-n-propylamine
BDL
0.010
mg/l
625
08/12/14 1
Phenanthrene
BDL
0.0010
mg/l
625
08/12/14 1
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
BDL
BDL
0.0030
mg/l
625
08/12/14 1
Di -n -butyl phthalate
BDL
0.0030
0.0030
mg/l
mg/l
625
625
08/12/14 1
08/12/14 1
Diethyl phthalate
Dimethyl phthalate
BDL
0.0030
mg/l
625
08/12/14 1
Di-n-octyl phthalate
BDL
BDL
0.0030
0.0030
mg/l
mg/l
625
625
08/12/14 1
08/12/14 1
Pyrene
1,2,4-Trichlorobenzene
BDL
BDL
0.0010
0.010
mg/l
625
625
08/12/14 1
mg/l
08/12/14 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 2 of 5

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
OESC 1-800-767-5859
Fax [phone]
l,•A^
Est. 1970
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory August 13, 2014
P.O. Box 589
Lumberton, NC 28359
Date Received August 08, 2014 ESC Sample # L714757-01
Description DuPont
Sample ID E40806 Site ID'
Collected By Jamie Lewis
Project # TBL-25801
Collection Date 08/06/14 07:55
Parameter Result Det. Limit Units Method Date Dil.
Acid Extractables
4-Chloro-3-methylphenol
2 -Chlorophenol
BDL
0.010
mg/l
625
08/12/14
1
2,9-Dichlorophenol
BDL
BDL
0.010
0.010
mg/l
mg/l
625
625
08/12/14
1
2,4 -Dimethylphenol
BDL
0.010
mg/l
625
08/12/14
08/12/14
1
1
4,6-Dinitro-2-methylphenol
BDL
0.010
mg/l
625
08/12/14
1
2,4-Dinitrophenol
2-Nitrophenol
BDL
0.010
mg/l
625
08/12/14
1
4-Nitrophenol
BDL
BDL
0.010
0.010
mg/l
mg/l
625
625
08/12/14
1
Pentachlorophenol
Phenol
BDL
0.010
mg/l
625
08/12/14
08/12/14
1
1
2,4,6 -Trichlorophenol
BDL
BDL
0.010
0.010
mg/l
mg/l
625
625
08/12/14
1
Surrogate Recovery
08/12/14
1
Nitrobenzene -d5
2-Fluorobiphenyl
49.7
% Rec.
625
08/12/14
1
p-Terphenyl-dl4
54.4
52.5
% Rec.
625
08/12/14
1
Phenol -d5
33.8
% Rec.
625
08/12/14
1
2-Fluorophenol
41.8
% Rec.
625
08/12/14
1
2,4,6-Tribromophenol
45.9
% Rec.
625
08/12/14
1
% Rec.
625
06/12/19
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 08/13/14 15:55 Printed: 08/13/14 15:55
Page 3 of 5

Sample Work
Number Group
L714757-01 WG736418
Attachment A
List of Analytes with QC Qualifiers
Sample
Type Analyte
SAMP 4-Nitrophenol
Run
ID Qualifier
R2975489 J4
Page 9 of 5

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J9 The associated batch QC was outside the established quality control range
for accuracy.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 5 of 5

93>�11'r<ii
NPDES PERMIT NO. NC0003573 DISCHARGE NO, 002 MONTH August YEAR 2014
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE (910) 678=1219
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV, OF WATER QUALITY X m
DENR (SIGNAT kE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
60050 00010 00400 00310 00340 00951 51521 00665
DEM Form MR -I (12/93)
00600
3
LU
FM
E
"o
'2
mpe`N
oo
d
y
o
0
o
FLOW
W
�
g 55
~W
V
m
o
U
w
MLL
LL
D
o
�
�
Z
a0
fn
0
°aooE
a
O
a0
W
OKZz
U�
�XC
0•
EFF
~X
Uj
HRS
HRS
Y/N
MGD
`C
UNITS
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
P/F
1
0800
24
Y
18.877
31
7.4'
2
0800
24
22.343
3
0800
:24
22.272
4
0800
24
Y
21.194
31
7.3
5
0800
24
Y
22.306
31
7.4
2.6
<30.0
0.78
5.53
P
6
0800
24
Y
23.030
31
7.4
21.4
7
0800
24
Y
23.154
32
7.5 '<
8
0800
24
Y
25.016
32
7.5
9
0800
24
24.181
10
0800
24
22.193
11
0800
24 `
Y
20.575
31 '
7.4
12
0800
24
1 Y
24.035
31
7.4
13
0800
24
Y
23.579
31
7.4
0.019
14
0800
24
Y
22.358
31
7.5
15
0800
24
Y `
21.938
32
7:5 '
16
0800
24
23.777
17
0800
24 `
24.997
18
0800
24
Y
24.889
32
7.4
19
0800
24
Y
28.529
32
7.4
20
0800
24
Y
17.703
31
7.1
21
0800
24
Y -
14.865
32
7.5
22
0800
24
Y
14.094
31
7.4
23
0800
24
16.698
24
0800
24
14.595
25
0800
24
Y
13.977
31
26
0800
24
Y
14.349
31
27
0800
24
Y
14:393
30
E7s
28
0800
24
Y
14.318
30
0800
24"
Y
14:203
30
L31
0800
24
14.837
08001 24 1
AVERAGE
14.128
19.916
31
2.6
0.0
21.4
0.019
0.78
5.53
P
MAXIMUM
28.529
32 7.5
2.6
<30
21.4
0.019
0.78
5.53
P
MINIMUM
13.977
30 7.1
2.6
<30
21.4
0.019
0.78
5.53
P
Comp. (C) Grab (G)
GG
C
C
G
G
C
C
C
Monthly Limit
Daily Limit
6-9
DEM Form MR -I (12/93)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements LX
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintehance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,'
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H.
(Please pr�r�t or
►irrrec��lll�uu
r
Date
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp, Date
PARAMETER CODES
00010 Temperature 00556 Oil &Grease 00951 Total Fluoride
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic
00080 Color (Pt -Co) 00610 Ammonia Nitrogen
00082 Color (ADMI) 00625 Total Kjeldhal 01027 Cadmium
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Hexavalent Chromium 01147
00300 Dissolved Oxygen 01034 Chromium 31616
00310 BOD5 00665 Total Phosphorous
00340 COD 00720 Cyanide 01037 Total Cobalt
00400 pH 00745 Total Sulfide 01042 Copper
00530 Total Suspended 00927 Total Magnesium
Residue 00929 Total Sodium 01045 Iron
00545 Settleable Matter 00940 Total Chloride 01051 Lead
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
50060
71880
71900
81551
Total
Residual
Chlorine
Formaldehyde
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 121
(D)
Total Selenium
Fecal Coliform
32730
Total Phenolics
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCB's
5005 0
Flow
50060
71880
71900
81551
Total
Residual
Chlorine
Formaldehyde
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) 121
(D)

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 08/21/14
Facility: DUPONT FAYETTEVILLE WORKS NPDES#
Laboratory PerArming Test: MERITECH LABS, INC.
X r ®�
r
ator
sor
NC0003573 Pipe##: 002 County: BLADEN
Comments :
* PASSED: 9.890 Reduction
Work Order: Environmental Sciences Branch
MAIL ORIGINAL TO: Div. of Water Quality
N.C. DENR
1621 Mail Service Center
North Carolina Ceriodaphnia Raleigh, North Carolina 27699-1621
Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results
Calculated t = 1.479
Tabular t = 2.508
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 0 Reduction = 9.89
# Young Produced II25I19I16�26�24I20I21I19�29I22I22I20
Adult (L)ive (D)ead IIL IL IL IL IL IL IL IL IL �L �L �L
Effluent %; 3.30
TREATMENT 2 ORGANISMS J. 2 3 4 5 6 7 8 9 10 11 12
# Young Produced II20I20I23I24I14I21I20I19I12I20I24I20
Adult (L)ive (D)ead I�L IL IL IL IL IL IL �L �L �L �L �L
Control CV
16.3310
0 control orgs
producing 3rd
brood
1000
PASS FAIL
X
Check One
1st sample 1st sample 2nd sample I Complete This For Either Test
pH
Control
Treatment 2
8.01
0
0 Mortality
Avg .Reprod.
0.00
Control
21.92
Control
0.00
Treatment 2
19.75
Treatment 2
0
7.99
Control CV
16.3310
0 control orgs
producing 3rd
brood
1000
PASS FAIL
X
Check One
1st sample 1st sample 2nd sample I Complete This For Either Test
pH
Control
Treatment 2
8.01
0
8.00
7.98
8.04
7.62
7.85
7.70
0
7.99
0
o
8.02
0
8.00
0
8.04
7.62
8.12
7.70
8.48
0
8.12
0
7.99
7.62
8.12
7.70
lest Mart liate: 08/13/14
Collection (Start) Date
Sample 1: 08/11/14 Sample 2: 08/13/14
Sample Type/Duration 2nd
1st P/F
s s s Grab Comp. Duration D
t e 7.92
t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d U M M
t t t Sample 2 X 24 hrs T P P
D.O. lst sample 1st sample 2nd sample
Treatment 2
7.69 7.69
0=7
7.97 7.20
=74
ControlIm
8.04 7.72
0
0
0
7.62
0
7.70
ttaraness (mg/1) 46
Spec. Cond. (�unhos) 182 463 588
Chlorine(mg/1) <0.1 0.1
LC50/Acute Toxicity Test Sample temp. at receipt(OC) wnwasms"0.2 0.2
(Mortality expressed as 0, combining replicates)
0
0
0
0
7.62
0
7.70
0
,
ttaraness (mg/1) 46
Spec. Cond. (�unhos) 182 463 588
Chlorine(mg/1) <0.1 0.1
LC50/Acute Toxicity Test Sample temp. at receipt(OC) wnwasms"0.2 0.2
(Mortality expressed as 0, combining replicates)
0
0
0
0
0
0
0
0
0
,
0
o
a
o
o
0
o 0
0
0
0
0
Concentration
Mortality
start/end
LC50 = 0 Method of Determination
950 Confi ence Limits Moving Average Other
Probit
Spearman Karber -
Note: Please
Complete This
Section Also
start/end
Organism Tested: Ceriodaphnia dubia Duration(hrs):
:opiea from llWQ Corm AT -1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.
Control
High
rnn o
Organism Tested: Ceriodaphnia dubia Duration(hrs):
:opiea from llWQ Corm AT -1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: August YEAR: 2014
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM DOWNSTREAM
DWQ Form MR -3 (Revised 7/2000)
00010 00400 00310 00610 00530 00094
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1
2
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Fit
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1=
00010
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00310
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00094
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HRS
°C
units
mg/L
mg/L
#/loomi
pmho/cm
ug/L
>1
8
2
9'
3
10
4
11
5
13=
6
14
15
7
16
17
8
18
9
19"
20
10
21
11
22
12
23'
24
13
12:40
25
0,014
14
26
15
27
16
28
29
17;
30
18
31'
Average
19
Maximum
20
21
22
23
24
25
26
27
28
29
30
31'
Average
0.014
Maximum
0.014
Minimum
0.014
DWQ Form MR -3 (Revised 7/2000)
00010 00400 00310 00610 00530 00094
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U a) .o 0 E CU 2
a o •o j o K o
E
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HRS °C units jmg/Lmg/L #/tooml pmholcm
1
2
3
Fit
5
6
7
8
9'
10
11
12
13=
14
15
16
17
18
19"
20
21
22
23'
24
25
26
27
28
29
30
31'
Average
Maximum
Minimum

Facility Status; (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Pla Manager
Permittee (Please print e)
Signature o Permit ee Date
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 0) 678-1315 October 31, 2016
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080 Color (Pt -Co) 00610 Ammonia Nitrogen 01092 Zinc Chlorine
00082 Color (ADMI) 00625 Total Kjeldhal 01027 Cadmium 01105 Aluminum
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Hexavalent Chromium 01147 Total Selenium 71880 Formaldehyde
00300 Dissolved Oxygen 01034 Chromium 31616 Fecal Coliform 71900 Mercury
00310 BOD5 00665 Total Phosphorous 32730 Total Phenolics 81551 Xylene
00340 COD 00720 Cyanide 01037 Total Cobalt 34235 Benzene
00400 pH 00745 Total Sulfide 01042 Copper 34481 Toluene
00530 Total Suspended 00927 Total Magnesium 38260 MBAS
Residue 00929 Total Sodium 01045 Iron 39516 PCB's
00545 Settleable Matter 00940 Total Chloride 01051 Lead 50050 Flow
Parameter Code assitance may be obtained by calling the Water Quality
Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A.0202
(b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)