201706201217-1

EFFLUENT
NPDES PERMIT NO, NC0003673 DISCHARGE NO, 001 MONTH
FACILITY NAME DuPont - Fayetteville Works CLASS 3
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE
CERTIFIED LABORATORIES (1) 1131. Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV, OF WATER QUALITY
DENR
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
November YEAR 2014
0
couNTY Bladen
PHONE [phone]
Jamie R. Lewis /Arnold Ray eard
X
GNAT[IRE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
Q
p
DEM Form MR -I (12/93) * Holiday
Y
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300
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00 0
00010
00 00
003 0
0530
00556
39700
39700
01034
01042
01067
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} Lu
od
HRS
HRS
Y/N
MGD
*C
UNITS
Lb/Day
Lb/Day
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
Lb/Day
Lb/Day
1
0800
24
1.203
2
3
osoo
0800
24
24 ;
Y
1.232
1.115 i
23
7.3
381.3
<387.8
4'M s
4
0800
24
Y
0.996
22
7.4
127.1
108.0
FiPr
9,
2n14
5
0800
24
Y
0.497
21
7.3
39.8
157.5
6
7
8
0800
osoo
0800
24
24
24
Y
Y
0.912
0.730(
1.037
fl
i 6'e.F 4
<
i
9
0800
24
0.820 ;
10
o800
24
B
0.769
20
8.0
<12.8
35.9
11
0800
24
B
0.966
19
8.1
<16.1
35.4
12
13
0800
osoo
24
24
Y
Y
1.113
1.021
20
8.0
<18.6
<46.4
14
0800
24
Y
1.012
15
0800
24
0.778
16
0800
24
0.898
17
0800
24
Y
0.999
19
7.6
<16.7
<20.8
18
osoo
24
Y
0.962
19
7.6
<16.0
28.9
19
0800
24
Y
0.857
17
7.5 -
20.7 "
25.7
<4.5
20
0800
24
Y
0.879
21
0800
24
Y
0.993
22
0800
24
0.999
23
0800
24
1.007
344.3
60.5
24
0800
24
Y
1.069
21
7.5
222.9
51.7
25
0800
24
Y
1.110 '+
21
7.5
249.9
72.2
26
0800
24'
Y
1.397
21
7.5
27
0800
24
*
1.194
28
osoo
2a
0.782
29
0800
24
0.828
30
0800
24
1.232
31 0800 24
AVERAGE
MAXIMUM
0.980
1.397
20
23 8.1
115.5
3813
48.0
<387.8
0
.<4.5
MINIMUM
0.497
17 7.3
<12.8
<20.8
<4.5
Comp. (C) Grab (G)
G G
C
C
G«
G
G
G
G
G
G
Monthly Limit
2.0
182.6
303.1
0.113
8.36
10.91
12.72
7.90
Daily Limit 6-9 `
484.7' 981.5 0,5 '
20.85
25.44
29.96
19.65

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements LIJ
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance; etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - PlantJ�Vlanager
Permittee (Please print or ape)
Zc
SP nature of Permittee�*1, a /) ! n1to
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp, Date
01067
Total Selenium
Nickel
01077
PARAMETER CODES
00010
Temperature
00556
Oil &Grease
00951
Total Fluoride
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
00300
Dissolved Oxygen
01034
Chromium
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
01037
Total Cobalt
00400
pH
00745
Total Sulfide
01042
Copper
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
01045
Iron
00545
Settleable Matter
00940
Total Chloride
01051
Lead
01067
Total Selenium
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
01147
81551
Formaldehyde
31616
Fecal Coliform
32730
Total Phenolics
34235
34481
Toluene
38260
MBAS
39516
PCB's
500 50
Flow
50060 Total
Residual
Chlorine
71880
Formaldehyde
71900
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 26.0506
(b) (2) (D)

lakilwill
NPDES PERMIT NO. 114C0003573 DISCHARGE NO, 002 MONTH November YEAR 2014
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV, OF WATER QUALITY X I,
DENR (SIGNAT RE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
w FLOW
E rn w to
w QO Qdo 0No Fd J DEFF X w Ixo N i.i p
INE aZzwo OU
t: EJ O O O = O
(OUiVO C. N JLLZ OO a. w
W
LL = aO a0 o Q0 r
HRS HRS YIN MGD *C UNITS mg/L mg/L mg/L ug/L mg/L mg/L PIF
1 0800 24 2.112
2 0800 24 1.124
3 0800 24 Y 1.385' 20 6.6
4 0800 24 Y 1.156 20 6.6
5 0800 24 Y 1.261 20 6.7
6 0800 24 Y 1.279 20 6.8
J 0800 24 Y 1.012 , 20 6.8
8 0800 24 1.112
9 0800 24 1 1.567
10 0800 24 1 B 1 2.088 1 18 7.6
12
0800
24
Y
3.015
19
7.8
13
0800
24 '
Y
2.978
19
Z1
14
0800
24
Y
3.414
18
6.9
15
0800
24
4.100
16
0800
24
4.049
17
0800
24
Y
4.228
16
4 6.7
p
18
0800
24 1
Y
3.876
16
6.5 1
<2.0
18.7 1
22.2
1.14
1.65
19
0800
24 <
Y
3.880
14
6.5
0.031,
20
o800
24
Y
4.698
14
6.5
21
0800
24 '
Y e
4.461
13
6.6
22
0800
24
4.296
23
0800
24
19.966
24
0800
24
Y
10.435
17
6.9
25
o800
24
Y
8.596 e
17
6.8
26
0800
24
Y
2.971
17
6.7
2710800
24
*
2.501 i
*
*"
2810800
24
*
3.350
2910800
e24 +
3.387
3010800
24
2.856
31
0800
24
MAXIMUM 10.435 20 7.8 <2 18.7 = 22.2 0.031 1.14 1.65 P
MINIMUM 1.012 13 6.5 <2 18.7 22.2 0.031 1.14 1.65 P
Comp. (C) Grab (G) G 'i G C C G G C C C
Monthly Limit
Daily.Limit 6-9
DEM Form MR -I (12/93) *Holiday

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If th4F .e facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, orthose
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy -Plant Ma�'ager
Per ittee (Please print or typk
Signature of ermittee** x / / Date
22828 NC Hvvy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp, Date
01147
31616
Nickel
01077
PARAMETER CODES
00010
Temperature
00556
Oil &Grease
00951
Total Fluoride
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADM])
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
00300
Dissolved Oxygen
01034
Chromium
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
01037
Total Cobalt
00400
pH
00745
Total Sulfide
01042
Copper
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
01045
Iron
00545
Settleable Matter
00940
Total Chloride
01051
Lead
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
81551
Total Selenium
Fecal Coliform
32730
Total Phenolics
34235
34481
Toluene
38260
MBAS
39516
PCB's
5005 0
Flow
50060
71880
71900
Total
Residual
Chlorine
Formaldehyde
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on He
with the state per 15A NCAC 26.0506
(b) (2) (D)

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 11/26/14
Facility: DUPONT FAYETTEVILLE WORKS NPDES#: NC0003573 Pipe#: 002 County: BLADEN
Laboratory Perf ming Test: MERITECH LABS, INC.
Comments*
XAsekwA
ure
GJ
or Labora
r in xespons
* PASSED: -10.62% Reduction
Chronic Pass/Fail Reproduction Toxicity Test
�ONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced ��22�29�25�25�26�29I21I15I23I10I27I21
effluent o: 3.30
CREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced ��26�27�29�25�26I27I27I26I11I27I26I25
Adult (L)ive (D)ead IIL IL IL IL IL IL IL IL IL IL IL IL
Chronic Test Results
Calculated t =
Tabular t =
Reduction = -10.62
Control CV
24.661%
control orgs
producing 3rd
brood
1000
PASS FAIL
X
Check One
.,u
1st sample 1st sample 2nd sample IT Complete This For Either Test
r-
Control
Treatment 2
8.14
o Mortality
Avg.Reprod.
0.00
Control
22.75
Control
0.00
Treatment 2
25.17
Treatment 2
High
0n"
Control CV
24.661%
control orgs
producing 3rd
brood
1000
PASS FAIL
X
Check One
.,u
1st sample 1st sample 2nd sample IT Complete This For Either Test
r-
Control
Treatment 2
8.14
8.03
7.55
8.19
7.97
High
0n"
8.09
8.05
7.55
8.08
8.07
High
0n"
1 C.5.'L 7 LarL Late: 11/ly/14
8.16 Collection (Start) Date
Sample 1: 11/17/14 Sample 2: 11/19/14
S
S
8.15
7.55
8.16
6.35
High
0n"
ample Type/Duration 2nd
s s Grab Comp. Duration D
1st PIF
t e t e t e I S S
a n a n a n Sample 1 X 24.0 hrs L A A
r d r d r d U M M
t t t Sample 2 X 24.0 hrs T P P
n
1st sample 1st sample 2nd sample
✓ v Control
Treatment 2
7.59
7.55
7.55
High
0n"
7.74
7.55
High
0n"
7.26
7.55
High
0n"
ample temp. at receipt(OC)
expressed .replicates)
ConcentrationNote* Please
0 E
start/end
LC50 = o Method of Determination
Control
95o Confi�ce LLimits Moving Average Probit
Spearman Karber
- Other
pH
Organism Tested: Ceriodaphnia dubia Duration (hrs):
Copied from DWQ form Al (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.
High
0n"
pH
Organism Tested: Ceriodaphnia dubia Duration (hrs):
Copied from DWQ form Al (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

NPDES NO: NC0003573
FACILITY:
STREAM:
LOCATION
DISCHARGE NO: 002 MONTH: November YEAR: 2014
DuPont - Fayetteville Works COUNTY: Bladen
Cape Fear River STREAM: Cape Fear River
DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM
O
U
o
N
E
P
00010
00400
00310
00610
00530
00094
51521
�
a
O N
o
12
flU
Ep
=
0
U
m
N
�•'
`n
m
C
't
a
a)
o
N
cm
p
E
0
0
(D
u
'V
=3
U
U
@
0
`0
'E
a)
IL
units
HRS
°C
units
I mg/L
mg/L
#/100m1
pmho/cm
ug/L
+1
2
2
3
3
4
4
5
5
7
6
8
7
9`•
8
10
9
11
10
12
11
13
12
14
13"
16
14
17
15,
18
16
19
17,
20
18
21
19
11:00
22
0.030
20
23
21
25
22
26
23
27
24
28
25'
29
26
30
27'
31'
Average
28
Maximum
29'
30
31`
Average
0.030
Maximum `
"30
Minimum
OA30
DWQ Form MR -3 (Revised 7/2000)
..0.
L)
O
U
O
Nt
N
00010
00400
00310
00610
00530
00094
O
N ?
w a)
CL C)
E
N
Q
U
0)
a
N
co
`n
m
C
O
U)
rn
af6i
O E
V
aa)i 0
LL a)
>
U
HRS
°C
units
mg/L
mg/L
#/100m1
Wnho/am
'1
2
3
4
5
6
7
8
9`•
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31'
Average
Maximum
Minimum

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughv -Plant
print or e)
of Permittee
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp. Date
01147
31616
34235
34481
39516
Nickel
01077
PARAMETER CODES
00010
Temperature
00556
Oil &Grease
00951
Total Fluoride
00076
Turbidity
00600
Total Nitrogen
01002
Total Arsenic
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
00300
Dissolved Oxygen
01034
Chromium
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
01037
Total Cobalt
00400
pH
00745
Total Sulfide
01042
Copper
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
01045
Iron
00545
Settleable Matter
00940
Total Chloride
01051
Lead
01067
Nickel
01077
Silver
01092
Zinc
01105
Aluminum
50060
71880
71900
81551
Total
Residual
Chlorine
Formaldehyde
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must eon
file with the state per 15A NCAC 2B .0506
(b) (Z) (D)
Total Selenium
Fecal Coliform
32730
Total Phenolics
Benzene
Toluene
38260
MBAS
PCB's
50050
Flow
50060
71880
71900
81551
Total
Residual
Chlorine
Formaldehyde
Mercury
Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must eon
file with the state per 15A NCAC 2B .0506
(b) (Z) (D)