201706201207

9amgle I�1: 951-011-1 EFF -001
a. F+urgeable {VQ�.�.t�-le organic) �'ractf.on, EFA Meth¢d $240 Page 2 of 9
Number of chemicals detected in Fraction 1
P`ractic�n STOREY Number 84085
.� .� ..
��.-
�uantitatian
%aanit Target,,
Pollutants to be analy2ed fc+rs �
{ug/L) ,
ti
Quantitatioa
Y�imit+�
{ug/�)
C❑ucentrati:on
Det�Qd
{ u9/r� )
O��M�
Conf irmation?
3A�2i0 Acrt+lein 100 <loo X
34215 Acrylonitrile 100. <100 X
3403p Benzene 5 e5 X
32101 �romodichl©rrsmethane 5 �5 X
32104 Srcmcfcrm 5 �5 x
34413 Bromomethane 7.0 X10 X
32102 Carbon tet$achloride 5 �5 X
34301 Chlorabenzene 6 +C6 7C
34317. Chloroethane 10 �rti0 %
34575 2-Ch7-arosti2yl vinyl ether 10 �ci0 %
32106 Chiorotorm 5 +C5 X
$4413 Chloromethane 10 X10 X
32105 DilSromochioromethaae 5 �5 X
34456 1,1 -trichloroethane 5 �5 X
34531 1,2-D3.chloroethane 5 +�5 x
34507. 1,1-DichlordethyleriB 5 �5 x
34546 trans-1,2-Dichloroethyleae 5 <5 X
34541 1,2.-]?ichl❑r❑pr❑pane 6 <6 X
34704 cis-1,3-Dichlcr�c�+rcpaae 5 a5 X
34599 trans-l,3-Diahlaropropene 5 �5 x
34371 Sthylbenzeae 8 t8 %
34423 Methylene chle�ride 5 18 x
34516 1 � �. r 2 r�-Tatra❑hle�rc�ethane 7 C7 %
34475 '1'at.xaahiaroethylene 5 C5 X
34014 Toluene � 6 C6 SC
34506 1,7.,1 -Trichloroethane 5 CS X
34511 1,1,2-Trich�.aroethane 5 �S S
39180 TrichlQr❑ethylane 5 �5 %
34488 Trichlorofluvrc�caethaue l0 c10 %
39175 Vinyl chloride 10 X10 X
*Yf differaat fro}n quantitation limit target

09/26/91 12::9
Sample I.D.s9S1-011(0)-1 FFF-ddb
I EA XARY
B. Acid Fxtractalil.e �practxon, NPA Method 8270
Number of chemicals detected in Fraction 1
Fraction 6TORNT Number 45582
S1'ORNT �mpaund Quantitation Quantitation
Number Limit Tar at LiMt*
I
cc�x�c$r�tra� ion
Detected
�7J 006
G�/Ms
Confirmation?
Pollutants to be analyzed tors (ug/L) (ug/L) Yea No
y
34452 4-Chloro-3-mathylphanol 10 <10 S
34586 2 -Chlorophenol 10, <10 g
34601 214-Dichloraphanol; 10 C10 S
34606 2,4-Dimathylphenol: 10 C10 x
34616 2,4-Diuitrophenol 50 C50 X
34657 2-Methyl-4,6dinitrophenol 50 C50 x
34591 2-Nitropphenol 10 <10 X
3464E 4-Nitrophenol 50 a50 X
39032 Pentachlorophenol. 50 <50 X
34694 Phenol 10 et10 X
34621 2,4,6 -Trichlorophenol 10 <10 x
*If different from quantitation limit target

09/26/91 13&06 172 IEA,CARY
OL
i
Sample I.D.: 951�011(0)�1 EFF -001
C. Base/Neutral Fraction, EPA Method 8270 page 6 of 9
Number of chemicals detected in Fraction 5
Fraction STORET Number 45583
6T0R1RT commpaund QuantitaticSn guantitatian Cc Lxcgm trn G+0/M8
Number Limit Target Limit* Det.eoted confirpat.iOA7
Pollutants to be analyzed For: (ug/L) (ug/L) (ug/L) Yea No
34305 Acenaphthene 50(7
34200 Acenaphthylene 1C
34220 Anthracene 10
39120 Benzidine 56
34526 Benzo (a) anthracene 10
34247 Benzo (a) pyrene 10
34230 Benzo (b) fluoranthene 10
34521 Benzo (ghi) perylene 10
34242 Benzo (k) fluoranthene 10
34278 Bis (2-chloroethoxy)methane 10
34273 Eis (2-chloroethyl) ether 10
34283 Bis(22 chloroisopropyl)ether 10
39100 Bis(2-ethylhexyl)phthalate 10
34636 4-Bromophanyl phenyl ether 10
34292 Butyl benzyl phthalate 10
34581 2-chlrronaphthalene 10
34641 4-Chlorophenyl phenyl ether 10
34320 Chryaene 10
34556 Diben.zo(a.h) anthracene 10
34536 1,2 -Dichlorobenzene, 10
34566 1,3 -Dichlorobenzene 10
34571 114 --Dichlorobenzene 10
34631 3,3�Dichlorobenzidine 20
34336 Diethyl phthalate 10
343.41 Dimethyl phthalate 10
39110 Di -n -butyl. phthalate 10
34611 214�Dinitrotoluene 10
34626 216-Dinotrotoluene 10
34596 Di-n-octyl phthalate 10
34346 1,2�Diphenylhydrazine** 10
34376 Pluoranthene 10
34381 Fluorene 10
39700 Hexachlorabenzene 10
34391 Hexachlorobutadi.ene 1.0
34386 Hexachlorocyclopentadiene 10
34396 Ilexachloroethane 10
34403 zndeno(1,2,3-c4)pyrone 10
34408 Isophorone 10
34696 Naphthalene 10
34447 Nitrobenzene 10
34438 Ni nitrosadimethylamine 10
34428 N-nitresc-di-n-propylamine 10
34433 X-nitrosodiphenylamine 10
34461 Phenanthrene 10
34469 Pyrene 10
34551 11214�Trichlorobenzene 10
*If different from quantitation target
**As Azabenzene
<10 X
<10 x
<10 x
<50 x
<10 x
<10 x
<10 x
<10 x
<10 x
<10 x
<10 x `
<10 x
<10 x
<10 x
<10 x
<10 x
«0 x
<10 X
<10 .x
<10 x
<10 x
<20 x
<10 x
<10 x
<10 x
<10 x
<16 x
<10 x
<10 x
<10 x
<20 x
<10 x
<10 x
<10 x
<10 x
<10 x
<10 x
<10 x
<10 x
<10 x
<10 x
<10
<1
<1
<1 QC$ 1
UU8

09/26/91
13:01 <�
N/R = Nct Rec,�uested
__
IEA,CARY
D. prganoahlorine/Organophosphorus Fei3ticides and PCS�e
Number of cliemicala detected in Fraction y
iPracti�n STCRET Number 00188 �'
Page 8 of 9
X1010
STORES Coulpt�u�id QuantStatian Quantitation ConGentratiQu ConfirmatiolY?
Number Liraa.t TAr$et Limit* Detected Dual Colum GC/M3
1.Po11utants to be analysed for: (ug/L) (ug/L) (ug/L} Yea No Yes No
drganochlorine Pesticides/P+~8'e: 13PA Me#�'iod $q80 � �'
39930 Aldrin 0.05• r � is/R
39337 alpha-HHC 0.05 .y N/R
39338 Be#a-$HC 0.05 N/R
3}259 )'�e1ta-BHC � 4_1 N/R
39340 gamma -BHC (Li.ndane)., 0-05 N/R
39350 Chlordane Q«2 N/R
393].0 4,4' -DDD D.1 N/R
39320 4,4' -DDE Q,�. NfR
,3430(} 4,4' -DDT 0.7. N/R
99380 Iiieldrin 0.02 N/R
.34.361 F><3dosulfan I ('alyha) 0.1. N/fit
34356 Endosulfan �_ (.tx�ta) 0. ]. N/R
34351 Endosulfan r3ulfate 0.7 N/R
39390 Endrin O.Q6 N/R
94366 Endrin aldehyde 0.2 N/R
3410 Heptachlor 0.05 N/g
39420 He�+taohlar epG�.ide 0.8 N/R
39480 Meth4xyehlor 0_5 N/R
39755 Hirex 0.2 N/A
39400 Toxaphene 2.4 N/R
34671 PCB 1015 0.5 NfR
39488 iC�CB 1221 0.5 N/R .
39492 PC8 1232 0.5 N/R
39496 FCB 1282 0.5 N/R
39500 PCB 124$ 0,5 N/g
391544 PCB 1254 l.Q N/R
39508 PC8 1260 1.0 N/R
organc�phoefshorus Pesticides EPA Methaci 8g8q
395GQ Demetcyzl 2.5 N/R
3954q Farathicyn (ethyl) 0.6 N/R
E. Herbic.iclea, LFA Method 81.50 NfR � Not Requested
Number of ohemi�als# deteCt�c9..i..n Enaction _
Fraatior� STOREY Number 0014$
3TORET Camp4uad Quantitation quantitation Conoentr$tiCri CrSrlfirmatior►�
Number Limit Target Limit* t�etected Dual Column
pollutants t4 be analysed fQr; (ug/L) (ugfL} (ug/L) Yes No
39730 2,4-D 12 N/R
39045 3ilvex 2 N/R � ��� �(�'�;;:,
*lt different Pram u `t t '����• � 'g�
q antitatiQn �.�m� arget 1

09/26/91 13:01 $ IEA;CARI'
�U11 -
i
ganio AAalytical Iniormationi PRge 9 of 9
•genic Fraotion Method CC operating Conditions Surrogates (Spikes)
Extraction Column Description Compound Re0aver
batch Continubda Length x TA, Film Thicknaca, %
Column Type? Carrier G" y Flow
Rate, Temporatura Program
lrgcnble 8240 75M x 0.53mm, Y,2-DiahlQrQetUanA-d4 98
i1-011-1 3mm D9-624, us@ 12.mt/min Rbluena-d8 97
35 (Smn), 8 deg/min, 140 p-Bromoij.uorobeft2ane 103
;id Extretotebles 8270 Y 30m z 0.32mm, 0.5um phQnol-d5 48
i1 -011{O)-1 t DB -625, Be@ 30em/808e0 2-Pluorophenol' 49
40 (4m,in),300 (IOmIn), 2,4.6-Tribromophena1 67
10deg/min Nitrobenzene -d5 45
2 Flucrobiphenyl 39
sae/neutral 8270 30m x 0.32mm, 0.5um Terphenyl-dld 36
rtractable DB -625, He@ 30cm/80sec
40 (4min),300 (10min),
ladeg/min
d/MS Library size (number 4f referenne spectra)s 49,000 � (>�iYST)
Metals end Qther ChemiCal6
umhI= of Metals and Maher Chemioals(ss listed above) datected in Sample Na Not Requested
raction STORBT Number 78240
TORET Compound Quantitation Quantitation Concentration
gmtser TAMit Target Limit* Detected
ollutants tQ be analyzed for (ug/L) (ug/L) (ug/L)
1104 /A
Aluminum
50
1047
Antimony
50
1002
Arsenic
10
1012
Beryllium
25
1027
Cadmium
2
1034
Chromium
5
1042
Copper
2
1051
Lead
10
1900
Mercury
0.2
1067
Nickel
10
1147
Selehi.um,
5
11077
Silver
5
11092
Zino
10
ether
Inorganicsi
11007
Barium
500
10940
Chloride
1000
10720
Cyanide
20
10952
Fluoride
100
,If different from
quantitation limit target
�nalytiCal Laboratory Representative:
patr3: �1h� � 1
H
N/R
bilR
NfR
N/R
n/R
N/R
N/R
N/R
?acilltperatoY' in Reaponoible Charge (OCR)
[ certifp that this report is accurate and o4mpj-eta to the hent of my knowledge,
signed; Date
j
ITRAL FILE'