HomeMy WebLinkAbout201706201205I.
IEA
An Aquarion Company
ANNUAL POLLUTANT ANALYSIS MONITORING REQUIREMENT
Report• Form A
(Revised June 1990)
Facility Information:
Page 1 of 9
NPDES Permit No: Coo S 3 Discharge (Pipe) No:O yt4 a Z Year: ajz
Facility•
Name • /�aT=/ �'i�td.���lass: County: /3L ���,/
Persons) Collecting Samples:
S
Status of facility10
wastewater treatment operation on day of sampling:
typical: _ C Yes No
If no, explain briefly:
Analytical Laboratory: Industrial and Environmental Analysts, Inc.
II. Sampling:
24 hr composite for main sample/grab sample for purgeable fraction
Date Sampled: (composite sample) Correspondin sample taken for toxicity testing:
Sampling begun (date, time): Yes
Sampling finished (date, time): Q 01 q/ y No
Date and time sampled (grab sample):
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uc
IEA
An Aquarion Company
Sample ID: 951-032-1 (001 E1f#081992)
A. Purgeable (Volatile Organic) Fraction, EPA Method 8240
Number of chemicals detected in Fraction H
Fraction STORET Number 84085
STOREY Compound
Number
Quantitation
Limit Targedd,
Pollutants to be analyzed for:
(ug/L)
Quantitation
Limit*
Page 2 of 9
Concentration
Detected
GC/MS
Confirmation?
34210 Acrolein 100 <100 X
34215 Acrylonitrile 100 <100 X
34030 Benzene 5 <5 X
32101 Bromodichloromethane 5 <5 X
32104 Bromoform . 5 <5 X
34413 Bromomethane 10 <10 X
32102 Carbon tetrachloride 5 <5 X
34301 Chlorobenzene 6 <6 X
34311 Chloroethane 10 <10 X
34576 2-Chloroethyl vinyl ether 10 <10 X
32106 Chloroform 5 <5 X
34418 Chloromethane 10 <10 X
32105 Dibromochloromethane 5 <5 X
34496 1,1-Dichloroethane 5 <5 X
34531 1,2-Dichloroethane 5 <5 X
34501 1,1-Dichloroethylene 5 <5 X
34546 trans-1,2-Dichloroethylene 5 <5 X
34541 1,2-Dichloropropane 6 <6 X
34704 cis-1,3-Dichloropropane 5 <5 X
34699 trans-1,3-Dichloropropene 5 <5 X
34371 Ethylbenzene 8 <8 X
34423 Methylene chloride 5 <5 X
34516 1,1,2,2 -Tetrachloroethane 7 <7 X
34475 Tetrachloroethylene 5 <5 X
34010 Toluene 6 <6 X
34506 1,1,1 -Trichloroethane 5 <5 X
34511 1,112 -Trichloroethane 5 <5 X
39180 Trichloroethylene 5 <5 X
34488 Trichlorofluoromethane 10 <10 X
39175 Vinyl chloride 10 <10 X
*If different from quantitation limit target
CENTRAL FILE COPY
IEA
An Aquarion Company
2. Other purgeables (up to 10 highest peaks)
Sample I.D.: 951-032-1 (001 Eff#081992)
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Page 3 of 9
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IEA
An Aquarion Company
Sample I.D.:951-032-1 (001 Eff#081992)
B. Acid Extractable Fraction, EPA Method 625
Number of chemicals detected in Fraction 0
Fraction STORET Number 45582
STOREY Compound Quantitation Quantitation
Number Limit Target Limit*
iJ
Pollutants to be analyzed for: (ug/ L (ug/L)
ti
34452 4-Chloro-3-methylphenol 10
34586 2 -Chlorophenol 10
34601 2,4-Dichlorophenol ' 10
34606 2,4 -Dimethylphenol 10
34616 2,4-Dinitrophenol 50
34657 2-Methyl-416-dinitrophenol 50
34591 2-Nitrophenol 10
34646 4-Nitrophenol 50
39032 Pentachlorophenol 50
34694 Phenol 10
34621 2,4,6 -Trichlorophenol 10
*If different from quantitation limit target
Page 4 of 9
Concentration
Detected
GC/MS
Confirmation?
No
<10
X
<10
X
<10
X
<10
X
<50
X
<50
X
<10
X
<50
X
<50
X
<10
X
<10
X
L
IEA
An Aquarion Company
2. Other acid extractables (up to 10 highest peaks)
Sample I.D.: 951-032-1 (001 Eff081992)
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IEA
An Aquarion Company
Sample I.D.: 951-032-1 (001 Eff#081992)
Co Base/Neutral Fraction, EPA Method 625 Page 6 of 9
Number of chemicals detected in Fraction 0
Fraction STORET Number 45583
STORET Commpound Quantitation Quantitation Concentration GC/MS
Number Limit Target Limit* Detected Confirmation?
Pollutants to be analyzed for: (ug/L) (ug/L) (ug/L) Yes No
34205 Acenaphthene 10 <10 X
34200 Acenaphthylene 10!% <10 X
34220 Anthracene 10� <10 X
39120 Benzidine 58 <50 X
34526 Benzo (a) anthracene 10 <10 X
34247 Benzo (a) pyrene 10 <10 X
34230 Benzo (b) fluoranthene 10 <10 X
34521 Benzo (ghi) perylene 10 <10 X
34242 Benzo (k) fluoranthene 10 <10 X
34278 Bis (2-chloroethoxy)methane 10 <10 X
34273 Bis(2-chloroethyl)ether 10 <10 x
34283 Bis(2-chloroisopropyl)ether 10 <10 X
39100 Bis(2-ethylhexyl)phthalate 10 <10 X
34636 4-Bromophenyl phenyl ether 10 <10 X
34292 Butyl benzyl phthalate 10 <10 X
34581 2-Chloronaphthalene 10 <10 X
34641 4-Chlorophenyl phenyl ether 10 <10 X
34320 Chrysene 10 <10 X
34556 Dibenzo(a,h) anthracene 10 <10 X
34536 1,2 -Dichlorobenzene 10 <10 x
34566 113 -Dichlorobenzene 10 <10 X
34571 1,4 -Dichlorobenzene 10 <10 X
34631 3,3-Dichlorobenzidine 20 <20 x
34336 Diethyl phthalate 10 <10 x
34341 Dimethyl phthalate 10 <10 x
39110 Di -n -butyl phthalate 10 <10 x
34611 2,4-Dinitrotoluene 10 <10 x
34626 216-Dinotrotoluene 10 <10 x
34596 Di-n-octyl phthalate 10 <10 x
34346 1,2-Diphenylhydrazine 10 <10 x
34376 Fluoranthene 10 <10 x
34381 Fluorene 10 <10 x
39700 Hexachlorobenzene 10 <10 x
34391 Hexachlorobutadiene 10 <10 x
34386 Hexachlorocyclopentadiene 10 �} % <10 x
34396 Hexachloroethane 10 <10 x
34403 Indeno(112,3-cd)pyrene 10 <10 x
34408 Isophorone 10 <10 x
34696 Naphthalene 10 <10 x
34447 Nitrobenzene 10 -NMAL FILE COPY <10 x
34438 N-nitrosodimethylamine 10 <10 x
34428 N-nitroso-di-n-propylamine 10 <10 x
34433 N-nitrosodiphenylamine 10 <10 x
34461 Phenanthrene 10 <10 x
34469 Pyrene 10 <10 x
34551 112,4-Trichlorobenzene 10 <10 x
*If different from quantitation target
■ An Aquarion Company
2. Other base/neutrals (up to 10 highest peaks)
Sample I.D.: 951-032-1 (001 Eff#081992)
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Page 7 of 9
CFN rRAI FILE Copy
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Page 7 of 9
CFN rRAI FILE Copy
IEA
An Aquarion Company
Sample ID: 951-032-1 (001 Eff#081992)
D. Organochlorine/Organophosphorus Pesticides and PCB's
Number of chemicals detected in Fraction N/R = Not Requested
Fraction STORET Number 00188
STOREY Compound Quantitation Quantitation Concentration Confirmation?
Number Limit Target Limit* Detected Dual Column GC/MS
1.Pollutants to be analyzed for: (ug/L) (ug/L) (ug/L) Yes No Yes No
Organochlorine Pesticides/PCB's: EPA Method 8080 `
39330 Aldrin 0,05 `i N/R X X
39337 alpha -BHC 0.05 ) N/R X X
39338 Beta -BHC 0.05 N/R X X
34259 Delta -BHC 001 N/R X X
39340 Gamma -BHC (Lindane) 0.05 N/R X X
39350 Chlordane 0.2 N/R X X
39310 4,4' -DDD 001 N/R X X
39320 414' -DDE 001 N/R X X
39300 414' -DDT 091 N/R X X
39380 Dieldrin 0902 N/R X X
34361 Endosulfan I (alpha) 0.1 N/R X X
34356 Endosulfan II (beta) 001 N/R X X
34351 Endosulfan sulfate 0.7 N/R X X
39390 Endrin 0.06 N/R X X
34366 Endrin aldehyde 0.2 N/R X X
39410 Heptachlor 0.05 N/R X X
39420 Heptachlor epoxide 0.8 N/R X X
39480 Methoxychlor 095 N/R X X
39755 Mirex 0,2 N/R X X
39400 Toxaphene 2.4 N/R X X
34671 PCB'1016 0.5 N/R X X
39488 PCB 1221 0,5 N/R X X
39492 PCB 1232 005 "��
X
39496 PCB 1242 095 X
39500 PCB 1248 0.5 ��'" N/R X X
39504 PCB 1254 100� 'N Rc. X
/ X
39508 PCB 1260 1.0 N/R X X
Organophosphorus Pesticides EPA Method 8080
39560 Demeton 2.5 N/R X X
39540 Parathion (ethyl) 0.6 N/R X X
E. Herbicides, EPA Method 8150
Number of chemicals detected in Fraction N/R = Not Requested
Fraction STORET Number 00148
STORET Compound Quantitation Quantitation Concentration Confirmation?
Number Limit Target Limit* Detected Dual Column
Pollutants to be analyzed fore.(ug/L) (ug/L) (ug/L) Yes No
39730 214-D 12 N/R X
39045 Silvex 2 N/R X
39740 214,5-T 2 N/R X
*If different from quantitation limit target
/ IEA
An Aquarion Company
Organic Analytical Information: Page 9 of 9
Organic Fraction Method GC Operating Conditions Surrogates (Spikes)
Extraction Column Description Compound Recovery
Batch Continuous Length X ID, Film Thickness, %
Column Type, Carrier Gas & Flow
Rate, Temperature Program
Purgeable 8240 DB -6241 75 x .53 IDX3 u 112-DCE-d4 94
He - 10 ml/min, 35 Degrees C TOL-d8 104
(5 min) to 155 Degrees C: BFB 98
r1`
(0 min) at 6 Degrees C/mid
Acid Extractables 625 X 30m X 0.32mm, 0.54um, DB -5,625, Phenol -d5 52
} He, 30 cm/sec, 40 Degrees C 2-Fluorphenol 45
(4 min) -300 Degrees C, 2(4,6- 73
10 Degrees C/min Tribromophenol
Base/Neutral 625 X 30m X 0.32mm, 0.54um, DB -5,625, Nitrobenzene -d5 60
Extractable He, 30 cm/sec, 40 Degrees C 2-Fluorobiphenyl 59
(4 min) -300 Degrees C, Terphenyl-d14 36
10 Degrees C/min
GC/MS Library size (number of reference spectra): 55,000+
F. Metals and Other Chemicals
Number of Metals and Other Chemicals(as listed above) detected in Sample 0
Fraction STORET Number 78240 N/R = Not Requested
STORET Compound Quantitation Quantitation Concentration
Number Limit Target Limit* Detected
Pollutants to be analyzed for (ug/L) (ug/L) (ug/L)
01104 Aluminum 50 N/R
01097 Antimony 50 N/R
01002 Arsenic 10 N/R
01012 Beryllium 25 N/R
01027 Cadmium 2 N/R
01034 Chromium 5 N/R
01042 Copper 2 N/R
01051 Lead 10 N/R
71900 Mercury 0.2 N/R
01067 Nickel 10 N/R
01147 Selenium 5 N/R
01077 Silver 5 N/R
01092 Zinc 10 N/R
)they Inorganics: N/R
81007 Barium 500 N/R
80940 Chloride 1000 N/R
30720 Cyanide 20 N/R
30951 Fluoride 100 N/R
'If different from quantitation limit target
analytical Laboratory Representative:
')igned: !L U1,CDate:
?acility Operator in Responsible Charge (OCR):
[ certify that this report is accurate and complete to the best of my knowledge.
signed: Date:
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