HomeMy WebLinkAbout201706201205-1ANNUAL POLLUTANT ANALYSIS MONITORING REQUIREMENT
Report Form A
(Revised June 1990)
I. Facility Information:
NPDES Permit No: /���pAp3 Discharge (Pipe) No: 6p( �f-ooZ Year:/M MiML
Facility Name: �r1Fk f-Ft1VEi'T la s: �L County: :ZLAp5U
5
Person(s) Collecting Samples: 7j�g
Status of facility wastewater treatment operation on day of sampling:
typical: _� Yea No
If no, explain briefly:
Analytical Laboratory: Industrial and Environmental Analysts, Inc.
II. Sampling:
24 hr composite for main sample/grab sample for purgeable fraction
Date Sampled: (composite sample) Corresponding sample taken
or
Sampling begun (date, time):
Sampling finished .(date, time), Z, stz
Date and time sampled (grab sample):
Sample I.D.: 951-022-1 (Pipe 001)
Field Parameters: pH 7.05
Temperature,18.6 Degrees C
ftoxicity testing:
Yes
No
A14 19C
1492
CENTRAL FILE C®py
Sample ID: 951-022-1 (Pipe 001)
A. Purgeable (Volatile Organic) Fraction, EPA Method 8240
Number of chemicals detected in Fraction 1
Fraction STORET Number 84085
STOREY Compound Quantitation Quantitation
Number Limit Target s� Limit*
Pollutants to be analyzed for: (ug/L) (ug/L)
y
Page 2 of 9
Concentration
Detected
GC/MS
Conf ir[hat ion?
34210 Acrolein 100 <100 X
34215 Acrylonitrile 100 <100 X
34030 Benzene 5 <5 X
32101 Bromodichloromethane 5 <5 X
32104 Bromof6rm 5 <5 X
34413 Bromomethane 10 <10 X
32102 Carbon tetrachloride 5 <5 X
34301 Chlorobenzene 6 <6 X
34311 Chloroethane 10 <10 X
34576 2-Chloroethyl vinyl ether 10 <10 X
32106 Chloroform 5 <5 X
34418 Chloromethane 10 <10 X
32105 Dibromochloromethane 5 <5 X
34496 1,1-Dlchloroethane .5 <5 X
34531 1,2-Dlchloroethane 5 <5 X
34501 l,l-Dichloroethylene 5 <5 X
34546 trans-1,2-Dichloroethylene 5 <5 X
34541 1,2-Dichloropropane 6 <6 X
34704 cis-1,3-Dichloropropane 5 <5 X
34699 trans-l,3-Dlchloropropene 5 <5 X
34371 Ethylbenzene 8 <8 X.
34423 Methylene chloride 5 <5 X
34516 111,212 -Tetrachloroethane 7 <7 X
34475 Tetrachloroethylene 5 <5 X
34010 Toluene 6 <6 X
34506 1,1,1 -Trichloroethane 5 <5 X
34511 1,1,2 -Trichloroethane 5 <5 X
39180 Trichloroethylene 5 <5 X
34488 Trichlorofluoromethane 10 <10 X
39175 Vinyl chloride 10 <10 X
*If different from quantitation limit target
2. Other purgeables (up to 10 highest peaks)
Sample I.D.: 951-022-1 (Pipe 001)
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Page 3 of 9
"I 1 A
199
CENTRAL FILE Colplf
Sample I.D.: 951-022-1 (Pipe 0011
B. Acid Extractable Fraction, EPA Method 8270'
Number of chemicals detected in Fraction 0
Fraction STORET Number 45582
STOREY Compound Quantitation Quantitation
Number Limit Targe Limit*
Pollutants to be analyzed for: (ug/L), (ug/L)
y
Page 4 of 9
Concentration
Dgtected
GC/MS
Confirmation?
34452 4-Chloro-3-methylphenol 10 <10 x
34586 2 -Chlorophenol 10 <10 X
34601 2,4-Dichlorophenol 10 <10 X
34606 2,4 -Dimethylphenol 10 <10 x
34616 2,4-Dinitrophenol 50 <50 X
34657 2-Methyl-4,6-dini_trophenol 50 <50 X
34591 2-Nitrophenol 10 <10 x
34646 4-Nitrophenol 50 <50 x
39032 Pentachlorophenol 50 <50 x
34694 Phenol 10 <10 x
34621 214,6 -Trichlorophenol 10 <10 x
*If different from quantitation limit target
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CENTF? U FILE Copy
Mier acid extractables (up to IOs.highest peaks)
Sample I.D.: 951-022-1 (Pipe 001)
6
Page 5 of 9
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Sample I.D.: 951-022-1 (Pipe 0011
C. Base/Neutral Fraction, EPA Method 8270 Page 6 of 9
Number of chemicals detected in Fraction 10
Fraction STORET Number 45583 Fe
STOREY Commpound Quantitation Quantitation Concentration GC/MS
Number Limit Target Limit* Detected Confirmation?
Pollutants to be analyzed for: (ug/L) (ug/L) (ug/L) Yes No
34205 Acenaphthene 10
34200 Acenaphthylene 10 1
34220 Anthracene 10
39120 Benzidine 50
34526 Benzo (a) anthracene 10
34247 Benzo (a) pyrene 10
34230 Benzo (b) fluoranthene 10
34521 Benzo (ghi) perylene 10
34242 Benzo (k) fluoranthene 10
34278 Bis (2-chloroethoxy)methane 10
34273 Bis(2-chloroethyl)ether 10
34283 Bis(2-chloroisopropyl)ether 10
39100 Bi-s-(2=ethyihexyl)phthalate 10
34636 4-Bromophenyl phenyl ether 10
34292 Butyl benzyl phthalate 10
34581 2-Chloronaphthalene 10
34641 4-Chlorophenyl phenyl ether 10
34320 Chrysene. 10
34556 Dibenzo(a,h) anthracene 10
34536 1,2 -Dichlorobenzene 10
34566 1,3 -Dichlorobenzene 10
34571 1,4 -Dichlorobenzene 10
34631 3,3-Dichlorobenzidine 20
34336 Diethyl phthalate 10
34341 Dimethyl phthalate 10
39110 Di_ -n -butyl phthalate 10
34611 2,4-Dlnitrotoluene 10
34626 2,6-Dlnotrotoluene 10
34596 Di-n-octyl phthalate 10
34346 1,2-Dlphenylhydrazlne 10
34376 Fluoranthene 10
34381 Fluorehe 10
39700 Hexachlorobenzene f10
34391 Hexachlorobutadiene 10
34386 Hexachlorocyclopentadi.ene 10
34396 Hexachloroethane 10
34403 Indeno(1,2,3-cd)pyrene 10
34408 Isophorone 10
34696 Naphthalene 10
34447 Nitrobenzene 10
34438 N-nitrosodimethylamine 10
34428 N-nitroso-di-n-propylamine 10
34433 N-ni.trosodiphenylamine 10
34461 Phenanthrene 10
34469 Pyrene 10
34551 1,2,4-Trlchlorobenzene 10
*If different from quantitation target
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NTR4. FILE Copy
2. Other base/neutrals (up to 10 highest peaks)
Sample I.D.: 95 1 —022-1 (Pipe 00 1)
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Page 7 of 9
"IR 1 P
1997
CENr/?AL FILE Cop,
Sample ID: 951-022-1
(Pipe 001)
D. Organochlorine/Organophosphorus Pesticides and PCB's
Number of chemicals detected in Fraction 0
Fraction STORET Number 00188
Page 8 of 9
STOREY Compound Quantitation Quantitation Concentration Confirmation?
Number Limit Target Limit* Detected Dual Column GC/MS
1.Pollutants to be analyzed for: (ug/L) (ug/L) (ug/L) Yes No Yes No
Organochlorine Pesticides/PCB's: EPA Metha' 8080
39330 Aldrin 0.05 <0.05 X X
39337 alpha -BHC 0.05 <0.05 X X
39338 Beta -BHC 0.05 <0.05 Ix X
34259 Delta -BHC 0.1 <0.1 X X
•39340 Gamma -BHC (Lindane) 0.05 <0.05 X X
39350 Chlordane 0.2 <0.2 X X
39310 414' -DDD 0.1 <0.1 X X
39320 414' -DDE 0.1 <0.1 X X
39300 414' -DDT 0.1 <0:1 X X
39380 Dieldrin 0.02 <0.02 X X
34161 Endosulfan I (alpha) 0.1 <0.1 X X
34356 Endosulfan II (beta) 0.1 <0.1 X X
34351 Endosulfan sulfate 0.7 <0.7 X X
39390 Endrin 0.06 <0.06 X X
34366 Endrin aldehyde 0.2 <0.2 X X
39410 Heptachlor 0.05 <0.05 X X
39420 Heptachlor epoxide 0.8 <0.8 X X
39480 Methoxychlor 0.5 <0.5 X X
39755 Mirex 0.2 <0.2 X X
39400 Toxaphene 2.4 <2,4 X X
34671 PCB 1016 0.5 <005 X X
39488 PCB 1221 0.5 <0.5 X X
39492 PCB 1232 0.5 <0.5 X X
39496 PCB 1242 .0.5 <0.5 X X
39500 PCB 1248 0.5 <0.5 X X
39504 PCB 1254 1.0 <1.0 X X
39508 PCB 1260 1.0 <1.0 X X
Organophosphorus Pesticides EPA Method 8080
39560 Demeton 2.5
39540 Parathion (ethyl) 0.6
E. Herbicides, EPA Method 8150
Number of chemicals detected in Fraction 0
Fraction STORET Number 00148
STOREY Compound Quantitation Quantitation Concentration Confirmation?
Number Limit Target Limit* Detected Dual Column
Pollutants to be analyzed for: (ug/L) (ug/L) (ug/L) C 8ry
R
39730 214-D 12 <12 C:f z( e
39045
Silvex 2 <2 X 4R 19
39740 21415-T 2 <2 X '99' I1
*If different from quantitation limit target CEN PAL FILE
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rganic Analytical Information: 951-022-1 (Pipe 001) Page 9 of 9
rganic Fraction Method . GC Operating Conditions Surrogates (Spikes)
Extraction Column Description Compound Recovery
Batch Continuous Length % ID, Film Thickness, g
Column Type, Carrier Gas & Flow
Rate, Temperature Program
irgeables 8240 DB6241 75m x .53 ID x 3um Be 10ml 112-Dichloroethane-d 102
(min) 35deg C (5min) to 155 Toluene -d8 100
Deg C 0 (min)at 6Deg C (min) p-Bromofluorobenzene 101
:id Extractable 8270 K F 30 x 0.32mm, 0.5um, DB -51 625 Phenol -d5 45
y He 30cm/sec, 40Deg C (4 min) 2-Fluorophenol_ 44
300 Deg C, 10 Degree C /min 2,4,6-Tribromophenol 70
ase Neutral Extractable 8270 % 30m x 0.32mm, 0.5um, DB -51 625 Nitrobenzene -d5 55
Be 30cm/sec, 40Deg C (4 min) 2-Fluorobiphenyl 51
300 Deg C. 10 (min) Terpenyl-d14 33
/MS Library size (number of reference spectra): 55,000
Metals and Other Chemicals
ober of Metals and Other Chemicals(as listed above) detected in Sample
action STORET Number 78240
DRET Compound Quantitation Quantitation
Concentration
ober Limit Target Limit*
Llutants to be analyzed for (ug/L) (ug/L)
Aluminum
50
Antimony
50
Arsenic
10
Beryllium
25
Cadmium
2
Chromium
5
Copper
2
Lead
10
Mercury
0,2
Nickel
10
Selenium
5
Silver
5
Zinc
10
G
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Detected
(ug/L)
750
<50
<10
<25
<2.0
5.6
4.0
<10
<0.2
10\
<5.0
<5.0
er inorganics:
07 Barium 500 <500
40 Chloride 1000 46,000 -
20 Cyanide 20 <10
51 Fluoride 100 160,OOO,d
different from quantitation limit target
lytical Laboratorxr Representative/:
ned: Date: ',1 41
ility Operator in Responsible Charge (OCR):
srtify that this report is accurate and complete to the best of my knowledge.
ied: Date:
i
A44 1I
199
CEN TR4L FILO Cop