10047_Atherton Mill_ SSVR 2012_11_13

REPORT OF SUB-SLAB VAPOR ASSESSMENT

ATHERTON MILL PROPERTY
2000, 2100, 2130 & 2140 SOUTH BOULEVARD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA

Prepared for:

ATHERTON MILL (E&A), LLC
1221 MAIN STREET, SUITE 1000
COLUMBIA, SOUTH CAROLINA 29201

Prepared By:

AMEC ENVIRONMENT & INFRASTRUCTURE, INC.
2801 YORKMONT ROAD, SUITE 100
CHARLOTTE, NORTH CAROLINA 28208

NOVEMBER 13, 2012

AMEC PROJECT: 6228-12-0051
Atherton Mill Property – Report of Sub-Slab Vapor Assessment November 13, 2012
2000, 2100, 2130 & 2140 South Boulevard, Charlotte, North Carolina
AMEC Project 6228-12-0051

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TABLE OF CONTENTS

1. SITE HISTORY AND CHARACTERIZATION ............................................................................ 1 
2. SUB-SLAB VAPOR SAMPLING ACTIVITIES ........................................................................... 3 
3. SUB-SLAB VAPOR SAMPLING RESULTS .............................................................................. 6 
4. CONCLUSIONS ........................................................................................................................... 7 

LIST OF ATTACHMENTS

FIGURE 1 – SITE LAYOUT AND SUB-SLAB VAPOR SAMPLING LOCATIONS

TABLE 1 – HOURLY WEATHER OBSERVATIONS FOR OCTOBER 10, 2012
TABLE 2 – SUMMARY OF SUB-SLAB VAPOR ANALYTICAL RESULTS

LABORATORY ANALYTICAL REPORT AND CHAIN-OF-CUSTODY FORM

Atherton Mill Property – Report of Sub-Slab Vapor Assessment November 13, 2012
2000, 2100, 2130 & 2140 South Boulevard, Charlotte, North Carolina
AMEC Project 6228-12-0051

1

1. SITE HISTORY AND CHARACTERIZATION

The 9.78-acre subject property (subject property) is located at 2000 (Building 1), 2100
(Building 2), 2130 (Building 3) & 2140 (Building 4) South Boulevard in Charlotte, North
Carolina and consists of Mecklenburg County Tax Parcel 121-031-09. A site layout is
depicted on Figure 1. The subject property contains four buildings. According to the
Mecklenburg County Property Ownership and Land Records Information System
(POLARIS), an approximately 58,959-square foot commercial building (Building 1)
constructed in 1908 at 2000 South Boulevard, an approximately 41,166-square foot
commercial building (Building 2) constructed in 1940 at 2100 South Boulevard, an
approximately 12,422-square foot commercial building (Building 3) constructed in 1962
at 2130 South Boulevard and an approximately 6,255-square foot commercial building
(Building 4) constructed in 1932 at 2140 South Boulevard occupy the site (Figure 1).
Remaining portions of the site consist of asphalt-paved driveway and parking areas and
grass covered areas. The site is currently occupied by office retail and restaurant space.

According to the Brownfields Agreement, in the early 1900’s, the Parks-Cramer
Company initially developed 4.5-acres of the subject property at the corner of South
Boulevard and West Tremont Avenue (2000 South Boulevard). The Parks-Cramer
Company manufactured products that included humidity control equipment for textile
mills. Later, the Parks-Cramer Company manufactured and restored air handling
equipment and hoisting systems for the textile industry.

The Parks-Cramer Company expanded its holdings to the southern portion of the subject
property in the 1960’s and 1970’s. In 1962, it commenced operation of a vapor
degreasing unit for cleaning and preparation of metal parts prior to paint application at
the northern portion of the subject property. Initially, trichloroethene was used as the
solvent in the degreasing process, with 1,1,1-trichlorethane replacing it in 1976.

In 1988, the Parks-Cramer Company sold its manufacturing operation to Flakt, Inc. The
property operated under a lease until December 1992, when South Boulevard
Properties, Inc. became the owner of the subject property. In 1993, Building 1 was
renovated for use of office, restaurant and retail space. Atherton Mills (E&A), LLC
purchased the subject property on September 7, 2006.

Atherton Mill Property – Report of Sub-Slab Vapor Assessment November 13, 2012
2000, 2100, 2130 & 2140 South Boulevard, Charlotte, North Carolina
AMEC Project 6228-12-0051

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The most recent environmental sampling at the subject property reportedly occurred in
June 2004. The highest concentrations of the Volatile Organic Compounds (VOCs)
reported in June 2004 were: 1,1-dichloroethene - 26,000 µg/L, 1,1-dichloroethane – 840
µg/L, cis-1,2-dichloroethene – 1,200 µg/L, 1,1,1-trichloroethane – 16,000 µg/L,
trichloroethene (TCE) – 250,000 µg/L and tetrachloroethene (PCE) – 10,000 µg/L.
The subject property is located within the Charlotte Belt of the Piedmont Physiographic
Province. Based on a review of the Geologic Map of North Carolina (1985), the site is
underlain by granitic rock.
The Soil Survey of Mecklenburg County indicates that soils at the subject property are
classified as Urban land (Ur). This map unit consists of areas where 90 percent of the
surface is covered with buildings, streets, parking lots, and other impervious material.
The natural soils are paved over, covered, or greatly altered by cutting, filling, or grading
during the process of urban development. The original landscape and topography and
commonly the drainage pattern(s) have been changed.
Based on the USGS topographic map, the elevation of the subject property is
approximately 750 feet above mean sea level. Surface drainage patterns within the
Piedmont typically indicate the direction contaminants would be transported by surface
water or groundwater. Based on our interpretation of the topographic map and on-site
observations, surface water on the property would primarily be expected to flow
southeast toward an unnamed tributary of Little Sugar Creek.
The direction and movement of groundwater through soil is dependent on soil type and
the presence of relict structures and textures of the underlying rock. Fractures, faults,
folds and foliation planes affect the migration of groundwater in rock. Since no
significant geologic features were identified on the site, it is reasonable to assume that
the direction of groundwater flow under static conditions (no pumping interference)
approximates the surface topography of the site. Groundwater at the property would
primarily be expected to flow southeast toward an unnamed tributary of Little Sugar
Creek.
Atherton Mill Property – Report of Sub-Slab Vapor Assessment November 13, 2012
2000, 2100, 2130 & 2140 South Boulevard, Charlotte, North Carolina
AMEC Project 6228-12-0051

3

2. SUB-SLAB VAPOR SAMPLING ACTIVITIES

AMEC collected the sub-slab vapor samples in general accordance with the “DRAFT
Vapor Intrusion Guidance, NCDENR Brownfields Program”, dated March 2012,
“Supplemental Guidelines for the Evaluation of Structural Vapor Intrusion Potential for
Site Assessments and Remedial Actions Under the Inactive Hazardous Sites Branch”,
dated June 21, 2011 and “Section 3.0 of the “Assessment of Vapor Intrusion in Homes
near the Raymark Superfund Site Using Basement and Sub-Slab Air Samples”.”

AMEC originally selected 15 locations at the subject property to collect sub-slab vapor
samples. However, due to site conditions, AMEC was unable to collect vapor samples
at three of the 15 proposed locations. Firstly, a sample was proposed in the break-room
of American Community Bank (Unit 010) near the northern corner of the building. Two
concrete slabs were encountered at this location and AMEC’s subcontractor was not
able to advance the borehole past the second slab into the native soil. Secondly, a
sample was proposed in the elevator equipment room adjacent to Ferguson Enterprises,
Inc. (Unit 160). AMEC’s subcontractor was unable to penetrate the entirety of the
concrete slab in this location and native soil was not encountered. Thirdly, a sample
was proposed in the lobby adjacent to EDENS (Unit 140). Upon drilling the borehole for
this location, it was discovered a portion of the basement was located beneath this
location. Additionally, a proposed sample location in the basement was planned
beneath this sampling point. The remaining 12 sampling locations where sub-slab vapor
samples were collected are identified as follows:
 SG-1 – American Community Bank (Unit 10), in the file storage closet
adjacent to the conference room near the building’s eastern corner;
 SG-2 – ByDesign Furniture (Unit 20), in the women’s restroom, near the
building’s western corner;
 SG-3 – ByDesign Furniture (Unit 20), in the showroom, near the
building’s southern corner;
 SG-4 – IceHouse South End (Unit 40), in the kitchen storage area, along
the building’s southwestern wall;
 SG-5 – Unit 45 (vacant at time of sampling), located near the center of
the unit;
Atherton Mill Property – Report of Sub-Slab Vapor Assessment November 13, 2012
2000, 2100, 2130 & 2140 South Boulevard, Charlotte, North Carolina
AMEC Project 6228-12-0051

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 SG-6 – Atherton Mill Market (Unit 60), located near the building’s
western corner;
 SG-7 – Atherton Mill Market (Unit 60), located near the building’s
eastern corner;
 SG-8 – Unit 80 (vacant at the time of sampling), located near the
eastern corner of the unit;
 SG-9 – Electrical closet (adjacent to Unit 85);
 SG-10 – Janitorial storage room (adjacent to Unit 160);
 SG-11 – Basement located beneath the lobby adjacent to Unit 140 and
 SG-12 – Basement located beneath Unit 140;
The locations of the 12 sub-slab vapor samples that were collected and the three
proposed locations where no samples were collected are depicted on Figure 1.
On October 9, 2012, AMEC personnel mobilized to the subject property to install the
sub-slab vapor sampling kits. Prior to advancement of the borings, AMEC retained a
private utility locator, Priority Underground Locating Service (Priority), to check the
sampling locations for buried utilities. Following utility clearance, under the direction of
AMEC personnel, Priority advanced a one-inch diameter borehole through the concrete
slab at each location to the native soil using a hammer drill. After Priority advanced the
borehole, AMEC personnel advanced a dedicated soil-gas sampling tip approximately
12 inches beneath the concrete slab using an AMS Manual Soil Vapor Probe kit. The kit
consists of a dedicated soil-gas sampling tip, a 5/8” x 3’ soil-gas vapor probe rod and a
slide hammer. Teflon® tubing was attached to the dedicated sampling tip and threaded
through the probe rod prior to advancement of the probe rod. The probe rod was
advanced to a depth of approximately 12 inches below the base of the concrete slab and
then retracted, leaving the dedicated sampling tip and tubing in the borehole. The
annular space of the borehole was then filled with cement to the surface. The seal was
left to cure for 24 hours prior to sampling.
On October 10, 2012, AMEC personnel returned to the subject property to sample the
sub-slab vapor sampling locations. Prior to connecting a six-liter Summa canister to the
sample tubing, stagnant air inside the tubing was purged using a hand pump. After
purging was complete, a sample was collected into the Summa canister at a flow rate of
Atherton Mill Property – Report of Sub-Slab Vapor Assessment November 13, 2012
2000, 2100, 2130 & 2140 South Boulevard, Charlotte, North Carolina
AMEC Project 6228-12-0051

5

approximately 12.5 mL/min (8-hour sample time). A helium shroud was installed around
the sample tubing and Summa canister to assist with collection of soil-gas samples with
no breakthrough of outside air. The helium shroud consisted of plastic sheeting
surrounding the sample tubing and canister. Helium was added to the shroud and a
Dielectric MGD-2002 helium detector was used to measure the concentration of helium
within the shroud. The samples were submitted to Pace for laboratory analysis of VOCs
by EPA Method TO-15 and helium by EPA Method 3C. The samples were maintained
under a chain-of-custody protocol.
Hourly weather observations for the weather station at the Charlotte Douglas
International Airport (KCLT) (approximately 4.1 miles west from the subject property)
were obtained from Weather Underground. During the eight hour sample collection
period, the average temperature was 64.1 °F, the average barometric pressure was
30.07 in. of Hg, the average wind speed was 5.68 mph, the average wind direction was
west-southwest and no precipitation was recorded on this date. A summary of the
hourly weather data obtained from Weather Underground is provided in Table 1.

Atherton Mill Property – Report of Sub-Slab Vapor Assessment November 13, 2012
2000, 2100, 2130 & 2140 South Boulevard, Charlotte, North Carolina
AMEC Project 6228-12-0051

6

3. SUB-SLAB VAPOR SAMPLING RESULTS

The results of the sub-slab soil-gas analysis are summarized on Table 2. A copy of the
laboratory report is attached. The analysis identified several VOCs in each of the 12
sub-slab vapor samples collected. Most notably:

 PCE was identified in each of the 12 samples collected and the concentrations in
samples SG-6 (11,100 µg/m3), SG-7 (17,100 µg/m3) and SG-12 (30,200 µg/m3)
exceeded the NCDENR Inactive Hazardous Sites Branch (IHSB) Residential
Acceptable Soil-Gas concentration for PCE of 83.4 µg/m3;

 TCE was identified in 10 of the 12 samples collected and the concentrations in
samples SG-5 (95.1 µg/m3), SG-6 (26,200 µg/m3), SG-7 (37,400 µg/m3), SG-8
(39.3 µg/m3), SG-9 (87.9 µg/m3), SG-10 (3,330 µg/m3), SG-11 (8.9 µg/m3) and
SG-12 (94,600 µg/m3) exceeded the NCDENR IHSB Residential Acceptable Soil-
Gas concentration for TCE of 4.2 µg/m3;

 The concentration of chloroform identified in SG-12 (26.1 µg/m3) exceeded the
NCDENR IHSB Residential Acceptable Soil-Gas concentration of 11 µg/m3 for
chloroform,

 The concentration of 1,1-dichloroethene identified in SG-12 (10,500 µg/m3)
exceeded the NCDENR IHSB Residential Acceptable Soil-Gas concentration of
420 µg/m3 for 1,1-dichloroethene,

 The concentration of naphthalene identified in SG-1 (6.5 µg/m3), SG-5 (11.4
µg/m3), SG-8 (89.2 µg/m3), SG-9 (197 µg/m3) and SG-10 (7.3 µg/m3) NCDENR
IHSB Residential Acceptable Soil-Gas concentration of 6.2 µg/m3,

 The concentration of 1,2,4-trimethylbenzene identified in SG-3 (28.9 µg/m3), SG-
5 (43.2 µg/m3) and SG-9 (21.2 µg/m3) exceeded the NCDENR IHSB Residential
Acceptable Soil-Gas concentration of 14.6 µg/m3.

 Other VOC constituent concentrations were identified above their respective
laboratory reporting limits. However, these concentrations did not exceed their
respective NCDENR IHSB Residential Acceptable Soil-Gas concentrations.

Atherton Mill Property – Report of Sub-Slab Vapor Assessment November 13, 2012
2000, 2100, 2130 & 2140 South Boulevard, Charlotte, North Carolina
AMEC Project 6228-12-0051

7

4. CONCLUSIONS

Based on the results of the sub-slab vapor assessment AMEC offers the following
conclusions:
 Portions of the property are currently frequented by children and have the
potential in the future to be frequented by children. Therefore, the
applicable IHSB acceptable soil-gas concentrations are the IHSB
Residential Soil-Gas Concentrations;

 Chloromethane, 1,1-dichloroethene, naphthalene, PCE, TCE and 1,2,4-
trimethylbenzene were identified in one or more samples at
concentrations which exceeded their respective NCDENR IHSB
Residential Acceptable Soil-Gas concentrations; and

 Helium was not detected in the sub-slab vapor samples above the
laboratory detection limits with the exception f sample sG-3, indicating a
breakthrough of outside air occurred in sample SG-3. Breakthrough of
outside air would have diluted the sample where constituents of concern
may have not been detected above laboratory reporting limits or may
have been reported at lower concentrations. Based on the relatively low
helium concentration identified (11.5 Ng/m3), it is AMEC’s opinion that the
breakthrough of outside air did not significantly affect the integrity of
sample SG-3.

PREPAREDBY DATE CHECKEDBY DATE JOB NUMBER FIGURE012024036048060Feet 16228-12-0051
Source: Mecklenburg County Aerial Photography, dated 2009.!(!(!(!(!(!(!(!(!(!(!(!(!(!(!(BUILDING 1
BUILDING 2
BUILDING 3
BUILDING 4
SG-11
SG-5
SG-6
SG-4
SG-2
SG-1
SG-8
SG-9
SG-12
SG-10
SG-3
SG-7
SUB-SLAB VAPOR SAMPLING LOCATIONSATHERTON MILL PROPERTY2000, 2100, 2130 & 2140 SOUTH BOULEVARDCHARLOTTE, NORTH CAROLINA!(Sub-Slab Vapor Samples Collected on October 10, 2012 !(Proposed Sub-Slab Vapor Samples Not Collected
AJF RCF11/12/12 11/12/12
Time (EST) Temperature (°F) Pressure (in. of Hg) Wind Speed (mph) Wind Direction Precipitation (in.)8:52 52.0 30.12 5.8 W 0.09:52 55.0 30.11 5.8 SW 0.010:52 59.0 30.09 8.1 SW 0.011:52 62.6 30.09 3.5 Variable 0.012:52 66.0 30.06 4.6 SW 0.013:52 68.0 30.05 5.8 W 0.014:52 70.0 30.04 5.8 WSW 0.015:52 70.0 30.04 4.6 W 0.016:52 71.1 30.02 5.8 Variable 0.017:52 71.1 30.03 9.2 WNW 0.018:52 64.9 30.06 4.6 NNW 0.019:52 59.0 30.08 4.6 N 0.0Average 64.1 30.07 5.68 WSW 0.0Notes:1. Data collected at Charlotte Douglas International Airport (KCLT) Prepared By/Date: AJF 11-2-122. Data obtained from Weather Underground (www.wunderground.com)3. EST = Eastern Standard TimeChecked By/Date: RCF 11-12-124. °F = Degrees Fahrenheit5. in. of Hg = Inches of Mercury6. mph = Miles per hour7. in. = InchesTable 1: Hourly Weather Observations for October 10, 2012Atherton Mill PropertyCharlotte, North CarolinaAMEC Project: 6228-12-0051
Constituent SG-1 SG-2 SG-3 SG-4 SG-5 SG-6 SG-7 SG-8 SG-9 SG-10 SG-11 SG-12IHSB Residential Acceptable Soil-Gas ConcentrationsAcetone88.9 84.3 119 21.2 227 56.4 124 56.2 499 39.3 37.3 17.264,000Benzene1.1 0.48 0.92 0.76 3.7<0.441.9 0.74 1.6 0.54 0.58 2.631Bromomethane <1.11.2<1.1 <1.2 <1.1 <1.1 <1.1 <1.1 <2.3 <1.1 <1.1 <1.2 NSL2-Butanone (MEK)17.2 10.3 15.9 4.9 95.2 3.8 11.2 6.9 25.4 6.8 3.3 1.310,400Carbon disulfide2.2 99.8 98.7<0.9425.9 7.6 24.9 2.6 38.1<0.91 <0.91 <0.98 1,460Carbon tetrachloride <0.92 <0.92 <0.86 <0.95 <0.92 <0.86 <0.86 <0.92 <1.8 <0.92 <0.921.041Chloroethane <0.78151<0.72 <0.80 <0.78 <0.72 <0.72 <0.78 <1.6 <0.78 <0.78 <0.84 NSLChloroform <1.4 <1.4 <1.32.5 4.3 2.9 9.2 2.7<2.93.3<1.426.111Chloromethane <0.60 <0.60 <0.56 <0.63 <0.60 <0.56 <0.56 <0.60 <1.2 <0.600.96<0.65 188Cyclohexane1.2 1.5 2.2 2.3<1.0 <0.94 <0.94 <1.05.0<1.0 <1.01.1NSL1,4-Dichlorobenzene <1.8 <1.8 <1.62.3 9.7<1.6 <1.6 <1.8 <3.5 <1.8 <1.8 <1.9 22Dichlorodifluoromethane2.5 2.8 2.8 2.5 3.5 2.9 3.1 2.6<2.93.2 3.3 2.82001,1-Dichloroethane <1.2 <1.2 <1.1 <1.2 <1.2 <1.1 <1.1 <1.2 <2.4 <1.2 <1.23.71501,2-Dichloroethane <059 <0.590.64<0.61 <0.59 <0.55 <0.55 <0.59 <1.2 <0.59 <0.59 <0.64 9.41,1-Dichloroethene <1.2 <1.2 <1.1 <1.2 <1.2 <1.1 <1.12.6<2.3 <1.2 <1.210,500420cis-1,2-Dichloroethene <1.2 <1.2 <1.1 <1.2 <1.210.2<1.1 <1.2 <2.3 <1.2 <1.296.7NSLtrans-1,2-Dichloroethene <1.2 <1.2 <1.1 <1.2 <1.2 <1.1 <1.1 <1.2 <2.3 <1.2 <1.214.4126Ethylbenzene1.4<1.32.6<1.37.1<1.2 <1.2 <1.33.8<1.3 <1.3 <1.4 974-Ethyltoluene <1.4 <1.44.8<1.58.2<1.3 <1.3 <1.46.6<1.4 <1.4 <1.6 NSLn-Heptane2.4<1.2 <1.11.3<1.2 <1.1 <1.11.4 2.5<1.21.5<1.3 NSLn-Hexane <1.0 <1.0 <0.962.6<1.015.9 37.0 12.9<2.1 <1.0 <1.0 <1.3 1,4602-Hexanone <1.22.2 3.9<1.221.9<1.11.9 1.5 7.8 2.1<1.2 <1.3 NSLMethylene Chloride <1.0 <1.0 <0.955.6<1.058.4 71.5 26.4<2.0 <1.01.5<1.1 1,3004-Methyl-2-pentanone (MIBK) <1.21.6 1.9<1.210.1<1.12.4<1.23.3<1.2 <1.2 <1.3 6,200Naphthalene6.5 2.8 5.7 2.3 11.4<1.4 <1.489.2 197 7.3 3.4<1.7 6.2Styrene2.6<1.33.6<1.3 <1.3 <1.2 <1.2 <1.32.8<1.3 <1.3 <1.3 2,000Tetrachloroethene (PCE)1.5 2.2 1.9 3.0 14.4 11,100 17,100 27.2 24.2 8.5 1.8 30,20083.4Tetrahydrofuran <0.86 <0.864.0<0.89 <0.86 <0.80 <0.80 <0.86 <1.7 <0.86 <0.86 <0.93 NSLTHC as Gas2,900 1,170 1,780 1,510 2,080 4,730 5,690 955 3,450 1,610 246 9,890NSLToluene5.4 8.0 23.0 5.5 170 5.6 5.7 3.1 16.7<1.11.9 1.710,4001,2,4-Trichlorobenzene <2.2 <2.22.8<2.2 <2.2 <2.0 <2.0 <2.2 <4.3 <2.2 <2.2 <2.3 4.21,1,1-Trichloroethane <1.6 <1.6 <1.5 <1.75.9 71.4 184 1.6 5.8 2.2<1.61,49010,400Trichloroethene (TCE) <0.791.1 3.8<0.8295.1 26,200 37,400 39.3 87.9 3,330 8.9 94,6004.2Trichlorofluoromethane17.6<1.6 <1.5 <1.7 <1.61.6 1.8 1.7<3.31.7 1.8 1.91,4601,2,4-Trimethylbenzene3.7 7.3 28.9 5.5 43.2 2.1 2.1 5.0 21.2 2.1 1.9<1.5 14.61,3,5-Trimethylbenzene2.0 2.6 8.7 3.1 14.1<1.3 <1.32.2 7.5 1.5<1.4 <1.5 NSLm&p-Xylene5.2 2.7 6.3<2.632.5<2.42.6<2.514.0<2.53.4<2.7 200o-Xylene2.7 1.4 3.8 1.6 15.4<1.2 <1.2 <1.36.1<1.31.4<1.4 200Helium <5.8 <3.811.5<3.8 <3.2 <4.2 <3.3 <4.4 <9.6 <4.4 <5.9 <5.0 NSLNotes:1. Concentrations shown in µg/m3Prepared By/Date: AJF 11-2-122. IHSB = Inactive Hazardous Sites Branch3. NSL = No standard listsChecked By/Date: RCF 11-12-124. Bold values indicate a concentration exceeding the laboratory reporting limit5. Shaded values indicate a concentration exceeding the IHSB Residential Acceptable Soil-Gas Concentration6. THC = Total Hydrocarbons7. Helium was used as a leak check8. Samples collected on October 10, 2012Table 2: Summary of Sub-Slab Vapor Analytical ResultsAtherton Mill PropertyCharlotte, North CarolinaAMEC Project: 6228-12-0051
October 25, 2012
LIMS USE: FR - ANDREW FRANTZ
LIMS OBJECT ID: 92134797
92134797
Project:
Pace Project No.:
RE:
Mr. Andrew Frantz
AMEC-Charlotte
2801 Yorkmont Road
Suite 100
Charlotte, NC 28208
ATHERTON MILLS 6228-12-0051
Dear Mr. Frantz:
Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Minnesota Certification IDs1700 Elm Street SE Suite 200, Minneapolis, MN 55414A2LA Certification #: 2926.01
Alaska Certification #: UST-078Alaska Certification #MN00064Arizona Certification #: AZ-0014Arkansas Certification #: 88-0680California Certification #: 01155CA
Colorado Certification #PaceConnecticut Certification #: PH-0256EPA Region 8 Certification #: PaceFlorida/NELAP Certification #: E87605Georgia Certification #: 959
Hawaii Certification #PaceIdaho Certification #: MN00064Illinois Certification #: 200011Kansas Certification #: E-10167Louisiana Certification #: 03086
Louisiana Certification #: LA080009Maine Certification #: 2007029Maryland Certification #: 322Michigan DEQ Certification #: 9909Minnesota Certification #: 027-053-137
Mississippi Certification #: Pace
Montana Certification #: MT CERT0092Nevada Certification #: MN_00064
Nebraska Certification #: PaceNew Jersey Certification #: MN-002New York Certification #: 11647North Carolina Certification #: 530North Dakota Certification #: R-036
North Dakota Certification #: R-036AOhio VAP Certification #: CL101Oklahoma Certification #: 9507Oregon Certification #: MN200001Oregon Certification #: MN300001
Pennsylvania Certification #: 68-00563Puerto Rico CertificationTennessee Certification #: 02818Texas Certification #: T104704192Utah Certification #: MN00064
Virginia/DCLS Certification #: 002521Virginia/VELAP Certification #: 460163Washington Certification #: C754West Virginia Certification #: 382Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92134797001 SG-1 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797002 SG-2 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797003 SG-3 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797004 SG-4 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797005 SG-5 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797006 SG-6 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797007 SG-7 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797008 SG-8 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797009 SG-9 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797010 SG-10 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797011 SG-11 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
92134797012 SG-12 Method 3C Gases 1 PASI-MRTP
TO-15 59 PASI-MCJR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-1 Lab ID:92134797001 Collected:10/10/12 10:35 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %1.61 10/18/12 12:34 7440-59-75.8
TO15 MSV AIR Analytical Method: TO-15
Acetone 88.9 ug/m3 1.44 10/20/12 18:18 67-64-10.69
Benzene 1.1 ug/m3 1.44 10/20/12 18:18 71-43-20.47
Bromodichloromethane ND ug/m3 1.44 10/20/12 18:18 75-27-42.0
Bromoform ND ug/m3 1.44 10/20/12 18:18 75-25-23.0
Bromomethane ND ug/m3 1.44 10/20/12 18:18 74-83-91.1
1,3-Butadiene ND ug/m3 1.44 10/20/12 18:18 106-99-00.65
2-Butanone (MEK)17.2 ug/m3 1.44 10/20/12 18:18 78-93-30.86
Carbon disulfide 2.2 ug/m3 1.44 10/20/12 18:18 75-15-0 SS0.91
Carbon tetrachloride ND ug/m3 1.44 10/20/12 18:18 56-23-50.92
Chlorobenzene ND ug/m3 1.44 10/20/12 18:18 108-90-71.4
Chloroethane ND ug/m3 1.44 10/20/12 18:18 75-00-30.78
Chloroform ND ug/m3 1.44 10/20/12 18:18 67-66-31.4
Chloromethane ND ug/m3 1.44 10/20/12 18:18 74-87-30.60
Cyclohexane 1.2 ug/m3 1.44 10/20/12 18:18 110-82-71.0
Dibromochloromethane ND ug/m3 1.44 10/20/12 18:18 124-48-12.5
1,2-Dibromoethane (EDB)ND ug/m3 1.44 10/20/12 18:18 106-93-42.2
1,2-Dichlorobenzene ND ug/m3 1.44 10/20/12 18:18 95-50-11.8
1,3-Dichlorobenzene ND ug/m3 1.44 10/20/12 18:18 541-73-11.8
1,4-Dichlorobenzene ND ug/m3 1.44 10/20/12 18:18 106-46-71.8
Dichlorodifluoromethane 2.5 ug/m3 1.44 10/20/12 18:18 75-71-81.5
1,1-Dichloroethane ND ug/m3 1.44 10/20/12 18:18 75-34-31.2
1,2-Dichloroethane ND ug/m3 1.44 10/20/12 18:18 107-06-20.59
1,1-Dichloroethene ND ug/m3 1.44 10/20/12 18:18 75-35-41.2
cis-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 18:18 156-59-21.2
trans-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 18:18 156-60-51.2
1,2-Dichloropropane ND ug/m3 1.44 10/20/12 18:18 78-87-51.4
cis-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 18:18 10061-01-51.3
trans-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 18:18 10061-02-61.3
Dichlorotetrafluoroethane ND ug/m3 1.44 10/20/12 18:18 76-14-22.0
Ethyl acetate ND ug/m3 1.44 10/20/12 18:18 141-78-61.1
Ethylbenzene 1.4 ug/m3 1.44 10/20/12 18:18 100-41-41.3
4-Ethyltoluene ND ug/m3 1.44 10/20/12 18:18 622-96-81.4
n-Heptane 2.4 ug/m3 1.44 10/20/12 18:18 142-82-51.2
Hexachloro-1,3-butadiene ND ug/m3 1.44 10/20/12 18:18 87-68-33.2
n-Hexane ND ug/m3 1.44 10/20/12 18:18 110-54-31.0
2-Hexanone ND ug/m3 1.44 10/20/12 18:18 591-78-61.2
Methylene Chloride ND ug/m3 1.44 10/20/12 18:18 75-09-21.0
4-Methyl-2-pentanone (MIBK)ND ug/m3 1.44 10/20/12 18:18 108-10-11.2
Methyl-tert-butyl ether ND ug/m3 1.44 10/20/12 18:18 1634-04-41.1
Naphthalene 6.5 ug/m3 1.44 10/20/12 18:18 91-20-31.5
Propylene ND ug/m3 1.44 10/20/12 18:18 115-07-10.50
Styrene 2.6 ug/m3 1.44 10/20/12 18:18 100-42-51.3
1,1,2,2-Tetrachloroethane ND ug/m3 1.44 10/20/12 18:18 79-34-51.0
Tetrachloroethene 1.5 ug/m3 1.44 10/20/12 18:18 127-18-40.99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 4 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-1 Lab ID:92134797001 Collected:10/10/12 10:35 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.44 10/20/12 18:18 109-99-90.86
THC as Gas 2900 ug/m3 1.44 10/20/12 18:1887.6
Toluene 5.4 ug/m3 1.44 10/20/12 18:18 108-88-31.1
1,2,4-Trichlorobenzene ND ug/m3 1.44 10/20/12 18:18 120-82-12.2
1,1,1-Trichloroethane ND ug/m3 1.44 10/20/12 18:18 71-55-61.6
1,1,2-Trichloroethane ND ug/m3 1.44 10/20/12 18:18 79-00-50.79
Trichloroethene ND ug/m3 1.44 10/20/12 18:18 79-01-60.79
Trichlorofluoromethane 17.6 ug/m3 1.44 10/20/12 18:18 75-69-41.6
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.44 10/20/12 18:18 76-13-12.3
1,2,4-Trimethylbenzene 3.7 ug/m3 1.44 10/20/12 18:18 95-63-61.4
1,3,5-Trimethylbenzene 2.0 ug/m3 1.44 10/20/12 18:18 108-67-81.4
Vinyl acetate ND ug/m3 1.44 10/20/12 18:18 108-05-41.0
Vinyl chloride ND ug/m3 1.44 10/20/12 18:18 75-01-40.37
m&p-Xylene 5.2 ug/m3 1.44 10/20/12 18:18 179601-23-12.5
o-Xylene 2.7 ug/m3 1.44 10/20/12 18:18 95-47-61.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 5 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-2 Lab ID:92134797002 Collected:10/10/12 18:07 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %1.06 10/18/12 12:52 7440-59-73.8
TO15 MSV AIR Analytical Method: TO-15
Acetone 84.3 ug/m3 1.44 10/20/12 18:47 67-64-10.69
Benzene 0.48 ug/m3 1.44 10/20/12 18:47 71-43-20.47
Bromodichloromethane ND ug/m3 1.44 10/20/12 18:47 75-27-42.0
Bromoform ND ug/m3 1.44 10/20/12 18:47 75-25-23.0
Bromomethane 1.2 ug/m3 1.44 10/20/12 18:47 74-83-91.1
1,3-Butadiene ND ug/m3 1.44 10/20/12 18:47 106-99-00.65
2-Butanone (MEK)10.3 ug/m3 1.44 10/20/12 18:47 78-93-30.86
Carbon disulfide 99.8 ug/m3 1.44 10/20/12 18:47 75-15-0 SS0.91
Carbon tetrachloride ND ug/m3 1.44 10/20/12 18:47 56-23-50.92
Chlorobenzene ND ug/m3 1.44 10/20/12 18:47 108-90-71.4
Chloroethane 151 ug/m3 7.75 10/22/12 13:57 75-00-3 2g4.2
Chloroform ND ug/m3 1.44 10/20/12 18:47 67-66-31.4
Chloromethane ND ug/m3 1.44 10/20/12 18:47 74-87-30.60
Cyclohexane 1.5 ug/m3 1.44 10/20/12 18:47 110-82-71.0
Dibromochloromethane ND ug/m3 1.44 10/20/12 18:47 124-48-12.5
1,2-Dibromoethane (EDB)ND ug/m3 1.44 10/20/12 18:47 106-93-42.2
1,2-Dichlorobenzene ND ug/m3 1.44 10/20/12 18:47 95-50-11.8
1,3-Dichlorobenzene ND ug/m3 1.44 10/20/12 18:47 541-73-11.8
1,4-Dichlorobenzene ND ug/m3 1.44 10/20/12 18:47 106-46-71.8
Dichlorodifluoromethane 2.8 ug/m3 1.44 10/20/12 18:47 75-71-81.5
1,1-Dichloroethane ND ug/m3 1.44 10/20/12 18:47 75-34-31.2
1,2-Dichloroethane ND ug/m3 1.44 10/20/12 18:47 107-06-20.59
1,1-Dichloroethene ND ug/m3 1.44 10/20/12 18:47 75-35-41.2
cis-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 18:47 156-59-21.2
trans-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 18:47 156-60-51.2
1,2-Dichloropropane ND ug/m3 1.44 10/20/12 18:47 78-87-51.4
cis-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 18:47 10061-01-51.3
trans-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 18:47 10061-02-61.3
Dichlorotetrafluoroethane ND ug/m3 1.44 10/20/12 18:47 76-14-22.0
Ethyl acetate ND ug/m3 1.44 10/20/12 18:47 141-78-61.1
Ethylbenzene ND ug/m3 1.44 10/20/12 18:47 100-41-41.3
4-Ethyltoluene ND ug/m3 1.44 10/20/12 18:47 622-96-81.4
n-Heptane ND ug/m3 1.44 10/20/12 18:47 142-82-51.2
Hexachloro-1,3-butadiene ND ug/m3 1.44 10/20/12 18:47 87-68-33.2
n-Hexane ND ug/m3 1.44 10/20/12 18:47 110-54-31.0
2-Hexanone 2.2 ug/m3 1.44 10/20/12 18:47 591-78-61.2
Methylene Chloride ND ug/m3 1.44 10/20/12 18:47 75-09-21.0
4-Methyl-2-pentanone (MIBK)1.6 ug/m3 1.44 10/20/12 18:47 108-10-11.2
Methyl-tert-butyl ether ND ug/m3 1.44 10/20/12 18:47 1634-04-41.1
Naphthalene 2.8 ug/m3 1.44 10/20/12 18:47 91-20-31.5
Propylene ND ug/m3 1.44 10/20/12 18:47 115-07-10.50
Styrene ND ug/m3 1.44 10/20/12 18:47 100-42-51.3
1,1,2,2-Tetrachloroethane ND ug/m3 1.44 10/20/12 18:47 79-34-51.0
Tetrachloroethene 2.2 ug/m3 1.44 10/20/12 18:47 127-18-40.99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 6 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-2 Lab ID:92134797002 Collected:10/10/12 18:07 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.44 10/20/12 18:47 109-99-90.86
THC as Gas 1170 ug/m3 1.44 10/20/12 18:4787.6
Toluene 8.0 ug/m3 1.44 10/20/12 18:47 108-88-31.1
1,2,4-Trichlorobenzene ND ug/m3 1.44 10/20/12 18:47 120-82-12.2
1,1,1-Trichloroethane ND ug/m3 1.44 10/20/12 18:47 71-55-61.6
1,1,2-Trichloroethane ND ug/m3 1.44 10/20/12 18:47 79-00-50.79
Trichloroethene 1.1 ug/m3 1.44 10/20/12 18:47 79-01-60.79
Trichlorofluoromethane ND ug/m3 1.44 10/20/12 18:47 75-69-41.6
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.44 10/20/12 18:47 76-13-12.3
1,2,4-Trimethylbenzene 7.3 ug/m3 1.44 10/20/12 18:47 95-63-61.4
1,3,5-Trimethylbenzene 2.6 ug/m3 1.44 10/20/12 18:47 108-67-81.4
Vinyl acetate ND ug/m3 1.44 10/20/12 18:47 108-05-41.0
Vinyl chloride ND ug/m3 1.44 10/20/12 18:47 75-01-40.37
m&p-Xylene 2.7 ug/m3 1.44 10/20/12 18:47 179601-23-12.5
o-Xylene 1.4 ug/m3 1.44 10/20/12 18:47 95-47-61.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 7 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-3 Lab ID:92134797003 Collected:10/10/12 18:15 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium 11.5 %1.12 10/18/12 13:00 7440-59-74.0
TO15 MSV AIR Analytical Method: TO-15
Acetone 119 ug/m3 1.34 10/20/12 19:16 67-64-1 E0.64
Benzene 0.92 ug/m3 1.34 10/20/12 19:16 71-43-20.44
Bromodichloromethane ND ug/m3 1.34 10/20/12 19:16 75-27-41.8
Bromoform ND ug/m3 1.34 10/20/12 19:16 75-25-22.8
Bromomethane ND ug/m3 1.34 10/20/12 19:16 74-83-91.1
1,3-Butadiene ND ug/m3 1.34 10/20/12 19:16 106-99-00.60
2-Butanone (MEK)15.9 ug/m3 1.34 10/20/12 19:16 78-93-30.80
Carbon disulfide 98.7 ug/m3 1.34 10/20/12 19:16 75-15-0 SS0.84
Carbon tetrachloride ND ug/m3 1.34 10/20/12 19:16 56-23-50.86
Chlorobenzene ND ug/m3 1.34 10/20/12 19:16 108-90-71.3
Chloroethane ND ug/m3 1.34 10/20/12 19:16 75-00-30.72
Chloroform ND ug/m3 1.34 10/20/12 19:16 67-66-31.3
Chloromethane ND ug/m3 1.34 10/20/12 19:16 74-87-30.56
Cyclohexane 2.2 ug/m3 1.34 10/20/12 19:16 110-82-70.94
Dibromochloromethane ND ug/m3 1.34 10/20/12 19:16 124-48-12.3
1,2-Dibromoethane (EDB)ND ug/m3 1.34 10/20/12 19:16 106-93-42.1
1,2-Dichlorobenzene ND ug/m3 1.34 10/20/12 19:16 95-50-11.6
1,3-Dichlorobenzene ND ug/m3 1.34 10/20/12 19:16 541-73-11.6
1,4-Dichlorobenzene ND ug/m3 1.34 10/20/12 19:16 106-46-71.6
Dichlorodifluoromethane 2.8 ug/m3 1.34 10/20/12 19:16 75-71-81.4
1,1-Dichloroethane ND ug/m3 1.34 10/20/12 19:16 75-34-31.1
1,2-Dichloroethane 0.64 ug/m3 1.34 10/20/12 19:16 107-06-20.55
1,1-Dichloroethene ND ug/m3 1.34 10/20/12 19:16 75-35-41.1
cis-1,2-Dichloroethene ND ug/m3 1.34 10/20/12 19:16 156-59-21.1
trans-1,2-Dichloroethene ND ug/m3 1.34 10/20/12 19:16 156-60-51.1
1,2-Dichloropropane ND ug/m3 1.34 10/20/12 19:16 78-87-51.3
cis-1,3-Dichloropropene ND ug/m3 1.34 10/20/12 19:16 10061-01-51.2
trans-1,3-Dichloropropene ND ug/m3 1.34 10/20/12 19:16 10061-02-61.2
Dichlorotetrafluoroethane ND ug/m3 1.34 10/20/12 19:16 76-14-21.9
Ethyl acetate ND ug/m3 1.34 10/20/12 19:16 141-78-60.98
Ethylbenzene 2.6 ug/m3 1.34 10/20/12 19:16 100-41-41.2
4-Ethyltoluene 4.8 ug/m3 1.34 10/20/12 19:16 622-96-81.3
n-Heptane ND ug/m3 1.34 10/20/12 19:16 142-82-51.1
Hexachloro-1,3-butadiene ND ug/m3 1.34 10/20/12 19:16 87-68-32.9
n-Hexane ND ug/m3 1.34 10/20/12 19:16 110-54-30.96
2-Hexanone 3.9 ug/m3 1.34 10/20/12 19:16 591-78-61.1
Methylene Chloride ND ug/m3 1.34 10/20/12 19:16 75-09-20.95
4-Methyl-2-pentanone (MIBK)1.9 ug/m3 1.34 10/20/12 19:16 108-10-11.1
Methyl-tert-butyl ether ND ug/m3 1.34 10/20/12 19:16 1634-04-40.98
Naphthalene 5.7 ug/m3 1.34 10/20/12 19:16 91-20-31.4
Propylene ND ug/m3 1.34 10/20/12 19:16 115-07-10.47
Styrene 3.6 ug/m3 1.34 10/20/12 19:16 100-42-51.2
1,1,2,2-Tetrachloroethane ND ug/m3 1.34 10/20/12 19:16 79-34-50.94
Tetrachloroethene 1.9 ug/m3 1.34 10/20/12 19:16 127-18-40.92
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 8 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-3 Lab ID:92134797003 Collected:10/10/12 18:15 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran 4.0 ug/m3 1.34 10/20/12 19:16 109-99-90.80
THC as Gas 1780 ug/m3 1.34 10/20/12 19:1681.5
Toluene 23.0 ug/m3 1.34 10/20/12 19:16 108-88-31.0
1,2,4-Trichlorobenzene 2.8 ug/m3 1.34 10/20/12 19:16 120-82-12.0
1,1,1-Trichloroethane ND ug/m3 1.34 10/20/12 19:16 71-55-61.5
1,1,2-Trichloroethane ND ug/m3 1.34 10/20/12 19:16 79-00-50.74
Trichloroethene 3.8 ug/m3 1.34 10/20/12 19:16 79-01-60.74
Trichlorofluoromethane ND ug/m3 1.34 10/20/12 19:16 75-69-41.5
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.34 10/20/12 19:16 76-13-12.1
1,2,4-Trimethylbenzene 28.9 ug/m3 1.34 10/20/12 19:16 95-63-61.3
1,3,5-Trimethylbenzene 8.7 ug/m3 1.34 10/20/12 19:16 108-67-81.3
Vinyl acetate ND ug/m3 1.34 10/20/12 19:16 108-05-40.96
Vinyl chloride ND ug/m3 1.34 10/20/12 19:16 75-01-40.35
m&p-Xylene 6.3 ug/m3 1.34 10/20/12 19:16 179601-23-12.4
o-Xylene 3.8 ug/m3 1.34 10/20/12 19:16 95-47-61.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 9 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-4 Lab ID:92134797004 Collected:10/10/12 17:23 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %1.05 10/18/12 13:09 7440-59-73.8
TO15 MSV AIR Analytical Method: TO-15
Acetone 21.2 ug/m3 1.49 10/20/12 19:45 67-64-10.72
Benzene 0.76 ug/m3 1.49 10/20/12 19:45 71-43-20.48
Bromodichloromethane ND ug/m3 1.49 10/20/12 19:45 75-27-42.0
Bromoform ND ug/m3 1.49 10/20/12 19:45 75-25-23.1
Bromomethane ND ug/m3 1.49 10/20/12 19:45 74-83-91.2
1,3-Butadiene ND ug/m3 1.49 10/20/12 19:45 106-99-00.67
2-Butanone (MEK)4.9 ug/m3 1.49 10/20/12 19:45 78-93-30.89
Carbon disulfide ND ug/m3 1.49 10/20/12 19:45 75-15-00.94
Carbon tetrachloride ND ug/m3 1.49 10/20/12 19:45 56-23-50.95
Chlorobenzene ND ug/m3 1.49 10/20/12 19:45 108-90-71.4
Chloroethane ND ug/m3 1.49 10/20/12 19:45 75-00-30.80
Chloroform 2.5 ug/m3 1.49 10/20/12 19:45 67-66-31.5
Chloromethane ND ug/m3 1.49 10/20/12 19:45 74-87-30.63
Cyclohexane 2.3 ug/m3 1.49 10/20/12 19:45 110-82-71.0
Dibromochloromethane ND ug/m3 1.49 10/20/12 19:45 124-48-12.6
1,2-Dibromoethane (EDB)ND ug/m3 1.49 10/20/12 19:45 106-93-42.3
1,2-Dichlorobenzene ND ug/m3 1.49 10/20/12 19:45 95-50-11.8
1,3-Dichlorobenzene ND ug/m3 1.49 10/20/12 19:45 541-73-11.8
1,4-Dichlorobenzene 2.3 ug/m3 1.49 10/20/12 19:45 106-46-71.8
Dichlorodifluoromethane 2.5 ug/m3 1.49 10/20/12 19:45 75-71-81.5
1,1-Dichloroethane ND ug/m3 1.49 10/20/12 19:45 75-34-31.2
1,2-Dichloroethane ND ug/m3 1.49 10/20/12 19:45 107-06-20.61
1,1-Dichloroethene ND ug/m3 1.49 10/20/12 19:45 75-35-41.2
cis-1,2-Dichloroethene ND ug/m3 1.49 10/20/12 19:45 156-59-21.2
trans-1,2-Dichloroethene ND ug/m3 1.49 10/20/12 19:45 156-60-51.2
1,2-Dichloropropane ND ug/m3 1.49 10/20/12 19:45 78-87-51.4
cis-1,3-Dichloropropene ND ug/m3 1.49 10/20/12 19:45 10061-01-51.4
trans-1,3-Dichloropropene ND ug/m3 1.49 10/20/12 19:45 10061-02-61.4
Dichlorotetrafluoroethane ND ug/m3 1.49 10/20/12 19:45 76-14-22.1
Ethyl acetate ND ug/m3 1.49 10/20/12 19:45 141-78-61.1
Ethylbenzene ND ug/m3 1.49 10/20/12 19:45 100-41-41.3
4-Ethyltoluene ND ug/m3 1.49 10/20/12 19:45 622-96-81.5
n-Heptane 1.3 ug/m3 1.49 10/20/12 19:45 142-82-51.2
Hexachloro-1,3-butadiene ND ug/m3 1.49 10/20/12 19:45 87-68-33.3
n-Hexane 2.6 ug/m3 1.49 10/20/12 19:45 110-54-31.1
2-Hexanone ND ug/m3 1.49 10/20/12 19:45 591-78-61.2
Methylene Chloride 5.6 ug/m3 1.49 10/20/12 19:45 75-09-21.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 1.49 10/20/12 19:45 108-10-11.2
Methyl-tert-butyl ether ND ug/m3 1.49 10/20/12 19:45 1634-04-41.1
Naphthalene 2.3 ug/m3 1.49 10/20/12 19:45 91-20-31.6
Propylene ND ug/m3 1.49 10/20/12 19:45 115-07-10.52
Styrene ND ug/m3 1.49 10/20/12 19:45 100-42-51.3
1,1,2,2-Tetrachloroethane ND ug/m3 1.49 10/20/12 19:45 79-34-51.0
Tetrachloroethene 3.0 ug/m3 1.49 10/20/12 19:45 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 10 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-4 Lab ID:92134797004 Collected:10/10/12 17:23 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.49 10/20/12 19:45 109-99-90.89
THC as Gas 1510 ug/m3 1.49 10/20/12 19:4590.6
Toluene 5.5 ug/m3 1.49 10/20/12 19:45 108-88-31.1
1,2,4-Trichlorobenzene ND ug/m3 1.49 10/20/12 19:45 120-82-12.2
1,1,1-Trichloroethane ND ug/m3 1.49 10/20/12 19:45 71-55-61.7
1,1,2-Trichloroethane ND ug/m3 1.49 10/20/12 19:45 79-00-50.82
Trichloroethene ND ug/m3 1.49 10/20/12 19:45 79-01-60.82
Trichlorofluoromethane ND ug/m3 1.49 10/20/12 19:45 75-69-41.7
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.49 10/20/12 19:45 76-13-12.4
1,2,4-Trimethylbenzene 5.5 ug/m3 1.49 10/20/12 19:45 95-63-61.5
1,3,5-Trimethylbenzene 3.1 ug/m3 1.49 10/20/12 19:45 108-67-81.5
Vinyl acetate ND ug/m3 1.49 10/20/12 19:45 108-05-41.1
Vinyl chloride ND ug/m3 1.49 10/20/12 19:45 75-01-40.39
m&p-Xylene ND ug/m3 1.49 10/20/12 19:45 179601-23-12.6
o-Xylene 1.6 ug/m3 1.49 10/20/12 19:45 95-47-61.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 11 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-5 Lab ID:92134797005 Collected:10/10/12 18:30 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %0.9 10/18/12 13:18 7440-59-73.2
TO15 MSV AIR Analytical Method: TO-15
Acetone 227 ug/m3 14.4 10/22/12 12:01 67-64-1 2g6.9
Benzene 3.7 ug/m3 1.44 10/20/12 20:14 71-43-20.47
Bromodichloromethane ND ug/m3 1.44 10/20/12 20:14 75-27-42.0
Bromoform ND ug/m3 1.44 10/20/12 20:14 75-25-23.0
Bromomethane ND ug/m3 1.44 10/20/12 20:14 74-83-91.1
1,3-Butadiene ND ug/m3 1.44 10/20/12 20:14 106-99-00.65
2-Butanone (MEK)95.2 ug/m3 1.44 10/20/12 20:14 78-93-30.86
Carbon disulfide 25.9 ug/m3 1.44 10/20/12 20:14 75-15-0 SS0.91
Carbon tetrachloride ND ug/m3 1.44 10/20/12 20:14 56-23-50.92
Chlorobenzene ND ug/m3 1.44 10/20/12 20:14 108-90-71.4
Chloroethane ND ug/m3 1.44 10/20/12 20:14 75-00-30.78
Chloroform 4.3 ug/m3 1.44 10/20/12 20:14 67-66-31.4
Chloromethane ND ug/m3 1.44 10/20/12 20:14 74-87-30.60
Cyclohexane ND ug/m3 1.44 10/20/12 20:14 110-82-71.0
Dibromochloromethane ND ug/m3 1.44 10/20/12 20:14 124-48-12.5
1,2-Dibromoethane (EDB)ND ug/m3 1.44 10/20/12 20:14 106-93-42.2
1,2-Dichlorobenzene ND ug/m3 1.44 10/20/12 20:14 95-50-11.8
1,3-Dichlorobenzene ND ug/m3 1.44 10/20/12 20:14 541-73-11.8
1,4-Dichlorobenzene 9.7 ug/m3 1.44 10/20/12 20:14 106-46-71.8
Dichlorodifluoromethane 3.5 ug/m3 1.44 10/20/12 20:14 75-71-81.5
1,1-Dichloroethane ND ug/m3 1.44 10/20/12 20:14 75-34-31.2
1,2-Dichloroethane ND ug/m3 1.44 10/20/12 20:14 107-06-20.59
1,1-Dichloroethene ND ug/m3 1.44 10/20/12 20:14 75-35-41.2
cis-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 20:14 156-59-21.2
trans-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 20:14 156-60-51.2
1,2-Dichloropropane ND ug/m3 1.44 10/20/12 20:14 78-87-51.4
cis-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 20:14 10061-01-51.3
trans-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 20:14 10061-02-61.3
Dichlorotetrafluoroethane ND ug/m3 1.44 10/20/12 20:14 76-14-22.0
Ethyl acetate ND ug/m3 1.44 10/20/12 20:14 141-78-61.1
Ethylbenzene 7.1 ug/m3 1.44 10/20/12 20:14 100-41-41.3
4-Ethyltoluene 8.2 ug/m3 1.44 10/20/12 20:14 622-96-81.4
n-Heptane ND ug/m3 1.44 10/20/12 20:14 142-82-51.2
Hexachloro-1,3-butadiene ND ug/m3 1.44 10/20/12 20:14 87-68-33.2
n-Hexane ND ug/m3 1.44 10/20/12 20:14 110-54-31.0
2-Hexanone 21.9 ug/m3 1.44 10/20/12 20:14 591-78-61.2
Methylene Chloride ND ug/m3 1.44 10/20/12 20:14 75-09-21.0
4-Methyl-2-pentanone (MIBK)10.1 ug/m3 1.44 10/20/12 20:14 108-10-11.2
Methyl-tert-butyl ether ND ug/m3 1.44 10/20/12 20:14 1634-04-41.1
Naphthalene 11.4 ug/m3 1.44 10/20/12 20:14 91-20-31.5
Propylene ND ug/m3 1.44 10/20/12 20:14 115-07-10.50
Styrene ND ug/m3 1.44 10/20/12 20:14 100-42-51.3
1,1,2,2-Tetrachloroethane ND ug/m3 1.44 10/20/12 20:14 79-34-51.0
Tetrachloroethene 14.4 ug/m3 1.44 10/20/12 20:14 127-18-40.99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 12 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-5 Lab ID:92134797005 Collected:10/10/12 18:30 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.44 10/20/12 20:14 109-99-90.86
THC as Gas 2080 ug/m3 1.44 10/20/12 20:1487.6
Toluene 170 ug/m3 14.4 10/22/12 12:01 108-88-3 2g11.1
1,2,4-Trichlorobenzene ND ug/m3 1.44 10/20/12 20:14 120-82-12.2
1,1,1-Trichloroethane 5.9 ug/m3 1.44 10/20/12 20:14 71-55-61.6
1,1,2-Trichloroethane ND ug/m3 1.44 10/20/12 20:14 79-00-50.79
Trichloroethene 95.1 ug/m3 1.44 10/20/12 20:14 79-01-60.79
Trichlorofluoromethane ND ug/m3 1.44 10/20/12 20:14 75-69-41.6
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.44 10/20/12 20:14 76-13-12.3
1,2,4-Trimethylbenzene 43.2 ug/m3 1.44 10/20/12 20:14 95-63-61.4
1,3,5-Trimethylbenzene 14.1 ug/m3 1.44 10/20/12 20:14 108-67-81.4
Vinyl acetate ND ug/m3 1.44 10/20/12 20:14 108-05-41.0
Vinyl chloride ND ug/m3 1.44 10/20/12 20:14 75-01-40.37
m&p-Xylene 32.5 ug/m3 1.44 10/20/12 20:14 179601-23-12.5
o-Xylene 15.4 ug/m3 1.44 10/20/12 20:14 95-47-61.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 13 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-6 Lab ID:92134797006 Collected:10/10/12 16:57 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %1.18 10/18/12 13:27 7440-59-74.2
TO15 MSV AIR Analytical Method: TO-15
Acetone 56.4 ug/m3 1.34 10/20/12 20:43 67-64-10.64
Benzene ND ug/m3 1.34 10/20/12 20:43 71-43-20.44
Bromodichloromethane ND ug/m3 1.34 10/20/12 20:43 75-27-41.8
Bromoform ND ug/m3 1.34 10/20/12 20:43 75-25-22.8
Bromomethane ND ug/m3 1.34 10/20/12 20:43 74-83-91.1
1,3-Butadiene ND ug/m3 1.34 10/20/12 20:43 106-99-00.60
2-Butanone (MEK)3.8 ug/m3 1.34 10/20/12 20:43 78-93-30.80
Carbon disulfide 7.6 ug/m3 1.34 10/20/12 20:43 75-15-00.84
Carbon tetrachloride ND ug/m3 1.34 10/20/12 20:43 56-23-50.86
Chlorobenzene ND ug/m3 1.34 10/20/12 20:43 108-90-71.3
Chloroethane ND ug/m3 1.34 10/20/12 20:43 75-00-30.72
Chloroform 2.9 ug/m3 1.34 10/20/12 20:43 67-66-31.3
Chloromethane ND ug/m3 1.34 10/20/12 20:43 74-87-30.56
Cyclohexane ND ug/m3 1.34 10/20/12 20:43 110-82-70.94
Dibromochloromethane ND ug/m3 1.34 10/20/12 20:43 124-48-12.3
1,2-Dibromoethane (EDB)ND ug/m3 1.34 10/20/12 20:43 106-93-42.1
1,2-Dichlorobenzene ND ug/m3 1.34 10/20/12 20:43 95-50-11.6
1,3-Dichlorobenzene ND ug/m3 1.34 10/20/12 20:43 541-73-11.6
1,4-Dichlorobenzene ND ug/m3 1.34 10/20/12 20:43 106-46-71.6
Dichlorodifluoromethane 2.9 ug/m3 1.34 10/20/12 20:43 75-71-81.4
1,1-Dichloroethane ND ug/m3 1.34 10/20/12 20:43 75-34-31.1
1,2-Dichloroethane ND ug/m3 1.34 10/20/12 20:43 107-06-20.55
1,1-Dichloroethene ND ug/m3 1.34 10/20/12 20:43 75-35-41.1
cis-1,2-Dichloroethene 10.2 ug/m3 1.34 10/20/12 20:43 156-59-21.1
trans-1,2-Dichloroethene ND ug/m3 1.34 10/20/12 20:43 156-60-51.1
1,2-Dichloropropane ND ug/m3 1.34 10/20/12 20:43 78-87-51.3
cis-1,3-Dichloropropene ND ug/m3 1.34 10/20/12 20:43 10061-01-51.2
trans-1,3-Dichloropropene ND ug/m3 1.34 10/20/12 20:43 10061-02-61.2
Dichlorotetrafluoroethane ND ug/m3 1.34 10/20/12 20:43 76-14-21.9
Ethyl acetate ND ug/m3 1.34 10/20/12 20:43 141-78-60.98
Ethylbenzene ND ug/m3 1.34 10/20/12 20:43 100-41-41.2
4-Ethyltoluene ND ug/m3 1.34 10/20/12 20:43 622-96-81.3
n-Heptane ND ug/m3 1.34 10/20/12 20:43 142-82-51.1
Hexachloro-1,3-butadiene ND ug/m3 1.34 10/20/12 20:43 87-68-32.9
n-Hexane 15.9 ug/m3 1.34 10/20/12 20:43 110-54-30.96
2-Hexanone ND ug/m3 1.34 10/20/12 20:43 591-78-61.1
Methylene Chloride 58.4 ug/m3 1.34 10/20/12 20:43 75-09-20.95
4-Methyl-2-pentanone (MIBK)ND ug/m3 1.34 10/20/12 20:43 108-10-11.1
Methyl-tert-butyl ether ND ug/m3 1.34 10/20/12 20:43 1634-04-40.98
Naphthalene ND ug/m3 1.34 10/20/12 20:43 91-20-31.4
Propylene ND ug/m3 1.34 10/20/12 20:43 115-07-10.47
Styrene ND ug/m3 1.34 10/20/12 20:43 100-42-51.2
1,1,2,2-Tetrachloroethane ND ug/m3 1.34 10/20/12 20:43 79-34-50.94
Tetrachloroethene 11100 ug/m3 1715.2 10/22/12 18:25 127-18-4 A31180
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 14 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-6 Lab ID:92134797006 Collected:10/10/12 16:57 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.34 10/20/12 20:43 109-99-90.80
THC as Gas 4730 ug/m3 1.34 10/20/12 20:4381.5
Toluene 5.6 ug/m3 1.34 10/20/12 20:43 108-88-31.0
1,2,4-Trichlorobenzene ND ug/m3 1.34 10/20/12 20:43 120-82-12.0
1,1,1-Trichloroethane 71.4 ug/m3 1.34 10/20/12 20:43 71-55-61.5
1,1,2-Trichloroethane ND ug/m3 1.34 10/20/12 20:43 79-00-50.74
Trichloroethene 26200 ug/m3 1715.2 10/22/12 18:25 79-01-6 A3943
Trichlorofluoromethane 1.6 ug/m3 1.34 10/20/12 20:43 75-69-41.5
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.34 10/20/12 20:43 76-13-12.1
1,2,4-Trimethylbenzene 2.1 ug/m3 1.34 10/20/12 20:43 95-63-61.3
1,3,5-Trimethylbenzene ND ug/m3 1.34 10/20/12 20:43 108-67-81.3
Vinyl acetate ND ug/m3 1.34 10/20/12 20:43 108-05-40.96
Vinyl chloride ND ug/m3 1.34 10/20/12 20:43 75-01-40.35
m&p-Xylene ND ug/m3 1.34 10/20/12 20:43 179601-23-12.4
o-Xylene ND ug/m3 1.34 10/20/12 20:43 95-47-61.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 15 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-7 Lab ID:92134797007 Collected:10/10/12 17:05 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %0.91 10/18/12 13:35 7440-59-73.3
TO15 MSV AIR Analytical Method: TO-15
Acetone 124 ug/m3 1.34 10/20/12 21:12 67-64-1 E0.64
Benzene 1.9 ug/m3 1.34 10/20/12 21:12 71-43-20.44
Bromodichloromethane ND ug/m3 1.34 10/20/12 21:12 75-27-41.8
Bromoform ND ug/m3 1.34 10/20/12 21:12 75-25-22.8
Bromomethane ND ug/m3 1.34 10/20/12 21:12 74-83-91.1
1,3-Butadiene ND ug/m3 1.34 10/20/12 21:12 106-99-00.60
2-Butanone (MEK)11.2 ug/m3 1.34 10/20/12 21:12 78-93-30.80
Carbon disulfide 24.9 ug/m3 1.34 10/20/12 21:12 75-15-0 SS0.84
Carbon tetrachloride ND ug/m3 1.34 10/20/12 21:12 56-23-50.86
Chlorobenzene ND ug/m3 1.34 10/20/12 21:12 108-90-71.3
Chloroethane ND ug/m3 1.34 10/20/12 21:12 75-00-30.72
Chloroform 9.2 ug/m3 1.34 10/20/12 21:12 67-66-31.3
Chloromethane ND ug/m3 1.34 10/20/12 21:12 74-87-30.56
Cyclohexane ND ug/m3 1.34 10/20/12 21:12 110-82-70.94
Dibromochloromethane ND ug/m3 1.34 10/20/12 21:12 124-48-12.3
1,2-Dibromoethane (EDB)ND ug/m3 1.34 10/20/12 21:12 106-93-42.1
1,2-Dichlorobenzene ND ug/m3 1.34 10/20/12 21:12 95-50-11.6
1,3-Dichlorobenzene ND ug/m3 1.34 10/20/12 21:12 541-73-11.6
1,4-Dichlorobenzene ND ug/m3 1.34 10/20/12 21:12 106-46-71.6
Dichlorodifluoromethane 3.1 ug/m3 1.34 10/20/12 21:12 75-71-81.4
1,1-Dichloroethane ND ug/m3 1.34 10/20/12 21:12 75-34-31.1
1,2-Dichloroethane ND ug/m3 1.34 10/20/12 21:12 107-06-20.55
1,1-Dichloroethene ND ug/m3 1.34 10/20/12 21:12 75-35-41.1
cis-1,2-Dichloroethene ND ug/m3 1.34 10/20/12 21:12 156-59-21.1
trans-1,2-Dichloroethene ND ug/m3 1.34 10/20/12 21:12 156-60-51.1
1,2-Dichloropropane ND ug/m3 1.34 10/20/12 21:12 78-87-51.3
cis-1,3-Dichloropropene ND ug/m3 1.34 10/20/12 21:12 10061-01-51.2
trans-1,3-Dichloropropene ND ug/m3 1.34 10/20/12 21:12 10061-02-61.2
Dichlorotetrafluoroethane ND ug/m3 1.34 10/20/12 21:12 76-14-21.9
Ethyl acetate ND ug/m3 1.34 10/20/12 21:12 141-78-60.98
Ethylbenzene ND ug/m3 1.34 10/20/12 21:12 100-41-41.2
4-Ethyltoluene ND ug/m3 1.34 10/20/12 21:12 622-96-81.3
n-Heptane ND ug/m3 1.34 10/20/12 21:12 142-82-51.1
Hexachloro-1,3-butadiene ND ug/m3 1.34 10/20/12 21:12 87-68-32.9
n-Hexane 37.0 ug/m3 1.34 10/20/12 21:12 110-54-30.96
2-Hexanone 1.9 ug/m3 1.34 10/20/12 21:12 591-78-61.1
Methylene Chloride 71.5 ug/m3 1.34 10/20/12 21:12 75-09-20.95
4-Methyl-2-pentanone (MIBK)2.4 ug/m3 1.34 10/20/12 21:12 108-10-11.1
Methyl-tert-butyl ether ND ug/m3 1.34 10/20/12 21:12 1634-04-40.98
Naphthalene ND ug/m3 1.34 10/20/12 21:12 91-20-31.4
Propylene ND ug/m3 1.34 10/20/12 21:12 115-07-10.47
Styrene ND ug/m3 1.34 10/20/12 21:12 100-42-51.2
1,1,2,2-Tetrachloroethane ND ug/m3 1.34 10/20/12 21:12 79-34-50.94
Tetrachloroethene 17100 ug/m3 3430.4 10/22/12 17:57 127-18-4 2g,A32360
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 16 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-7 Lab ID:92134797007 Collected:10/10/12 17:05 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.34 10/20/12 21:12 109-99-90.80
THC as Gas 5690 ug/m3 1.34 10/20/12 21:1281.5
Toluene 5.7 ug/m3 1.34 10/20/12 21:12 108-88-31.0
1,2,4-Trichlorobenzene ND ug/m3 1.34 10/20/12 21:12 120-82-12.0
1,1,1-Trichloroethane 184 ug/m3 1.34 10/20/12 21:12 71-55-61.5
1,1,2-Trichloroethane ND ug/m3 1.34 10/20/12 21:12 79-00-50.74
Trichloroethene 37400 ug/m3 3430.4 10/22/12 17:57 79-01-6 2g,A31890
Trichlorofluoromethane 1.8 ug/m3 1.34 10/20/12 21:12 75-69-41.5
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.34 10/20/12 21:12 76-13-12.1
1,2,4-Trimethylbenzene 2.1 ug/m3 1.34 10/20/12 21:12 95-63-61.3
1,3,5-Trimethylbenzene ND ug/m3 1.34 10/20/12 21:12 108-67-81.3
Vinyl acetate ND ug/m3 1.34 10/20/12 21:12 108-05-40.96
Vinyl chloride ND ug/m3 1.34 10/20/12 21:12 75-01-40.35
m&p-Xylene 2.6 ug/m3 1.34 10/20/12 21:12 179601-23-12.4
o-Xylene ND ug/m3 1.34 10/20/12 21:12 95-47-61.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 17 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-8 Lab ID:92134797008 Collected:10/10/12 17:37 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %1.21 10/18/12 13:43 7440-59-74.4
TO15 MSV AIR Analytical Method: TO-15
Acetone 56.2 ug/m3 1.44 10/20/12 22:10 67-64-10.69
Benzene 0.74 ug/m3 1.44 10/20/12 22:10 71-43-20.47
Bromodichloromethane ND ug/m3 1.44 10/20/12 22:10 75-27-42.0
Bromoform ND ug/m3 1.44 10/20/12 22:10 75-25-23.0
Bromomethane ND ug/m3 1.44 10/20/12 22:10 74-83-91.1
1,3-Butadiene ND ug/m3 1.44 10/20/12 22:10 106-99-00.65
2-Butanone (MEK)6.9 ug/m3 1.44 10/20/12 22:10 78-93-30.86
Carbon disulfide 2.6 ug/m3 1.44 10/20/12 22:10 75-15-0 SS0.91
Carbon tetrachloride ND ug/m3 1.44 10/20/12 22:10 56-23-50.92
Chlorobenzene ND ug/m3 1.44 10/20/12 22:10 108-90-71.4
Chloroethane ND ug/m3 1.44 10/20/12 22:10 75-00-30.78
Chloroform 2.7 ug/m3 1.44 10/20/12 22:10 67-66-31.4
Chloromethane ND ug/m3 1.44 10/20/12 22:10 74-87-30.60
Cyclohexane ND ug/m3 1.44 10/20/12 22:10 110-82-71.0
Dibromochloromethane ND ug/m3 1.44 10/20/12 22:10 124-48-12.5
1,2-Dibromoethane (EDB)ND ug/m3 1.44 10/20/12 22:10 106-93-42.2
1,2-Dichlorobenzene ND ug/m3 1.44 10/20/12 22:10 95-50-11.8
1,3-Dichlorobenzene ND ug/m3 1.44 10/20/12 22:10 541-73-11.8
1,4-Dichlorobenzene ND ug/m3 1.44 10/20/12 22:10 106-46-71.8
Dichlorodifluoromethane 2.6 ug/m3 1.44 10/20/12 22:10 75-71-81.5
1,1-Dichloroethane ND ug/m3 1.44 10/20/12 22:10 75-34-31.2
1,2-Dichloroethane ND ug/m3 1.44 10/20/12 22:10 107-06-20.59
1,1-Dichloroethene 2.6 ug/m3 1.44 10/20/12 22:10 75-35-41.2
cis-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 22:10 156-59-21.2
trans-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 22:10 156-60-51.2
1,2-Dichloropropane ND ug/m3 1.44 10/20/12 22:10 78-87-51.4
cis-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 22:10 10061-01-51.3
trans-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 22:10 10061-02-61.3
Dichlorotetrafluoroethane ND ug/m3 1.44 10/20/12 22:10 76-14-22.0
Ethyl acetate ND ug/m3 1.44 10/20/12 22:10 141-78-61.1
Ethylbenzene ND ug/m3 1.44 10/20/12 22:10 100-41-41.3
4-Ethyltoluene ND ug/m3 1.44 10/20/12 22:10 622-96-81.4
n-Heptane 1.4 ug/m3 1.44 10/20/12 22:10 142-82-51.2
Hexachloro-1,3-butadiene ND ug/m3 1.44 10/20/12 22:10 87-68-33.2
n-Hexane 12.9 ug/m3 1.44 10/20/12 22:10 110-54-31.0
2-Hexanone 1.5 ug/m3 1.44 10/20/12 22:10 591-78-61.2
Methylene Chloride 26.4 ug/m3 1.44 10/20/12 22:10 75-09-21.0
4-Methyl-2-pentanone (MIBK)ND ug/m3 1.44 10/20/12 22:10 108-10-11.2
Methyl-tert-butyl ether ND ug/m3 1.44 10/20/12 22:10 1634-04-41.1
Naphthalene 89.2 ug/m3 1.44 10/20/12 22:10 91-20-31.5
Propylene ND ug/m3 1.44 10/20/12 22:10 115-07-10.50
Styrene ND ug/m3 1.44 10/20/12 22:10 100-42-51.3
1,1,2,2-Tetrachloroethane ND ug/m3 1.44 10/20/12 22:10 79-34-51.0
Tetrachloroethene 27.2 ug/m3 1.44 10/20/12 22:10 127-18-40.99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 18 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-8 Lab ID:92134797008 Collected:10/10/12 17:37 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.44 10/20/12 22:10 109-99-90.86
THC as Gas 955 ug/m3 1.44 10/20/12 22:1087.6
Toluene 3.1 ug/m3 1.44 10/20/12 22:10 108-88-31.1
1,2,4-Trichlorobenzene ND ug/m3 1.44 10/20/12 22:10 120-82-12.2
1,1,1-Trichloroethane 1.6 ug/m3 1.44 10/20/12 22:10 71-55-61.6
1,1,2-Trichloroethane ND ug/m3 1.44 10/20/12 22:10 79-00-50.79
Trichloroethene 39.3 ug/m3 1.44 10/20/12 22:10 79-01-60.79
Trichlorofluoromethane 1.7 ug/m3 1.44 10/20/12 22:10 75-69-41.6
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.44 10/20/12 22:10 76-13-12.3
1,2,4-Trimethylbenzene 5.0 ug/m3 1.44 10/20/12 22:10 95-63-61.4
1,3,5-Trimethylbenzene 2.2 ug/m3 1.44 10/20/12 22:10 108-67-81.4
Vinyl acetate ND ug/m3 1.44 10/20/12 22:10 108-05-41.0
Vinyl chloride ND ug/m3 1.44 10/20/12 22:10 75-01-40.37
m&p-Xylene ND ug/m3 1.44 10/20/12 22:10 179601-23-12.5
o-Xylene ND ug/m3 1.44 10/20/12 22:10 95-47-61.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 19 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-9 Lab ID:92134797009 Collected:10/10/12 17:41 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %2.68 10/18/12 14:17 7440-59-79.6
TO15 MSV AIR Analytical Method: TO-15
Acetone 499 ug/m3 2.88 10/22/12 12:30 67-64-1 E1.4
Benzene 1.6 ug/m3 2.88 10/22/12 12:30 71-43-20.94
Bromodichloromethane ND ug/m3 2.88 10/22/12 12:30 75-27-43.9
Bromoform ND ug/m3 2.88 10/22/12 12:30 75-25-26.0
Bromomethane ND ug/m3 2.88 10/22/12 12:30 74-83-92.3
1,3-Butadiene ND ug/m3 2.88 10/22/12 12:30 106-99-01.3
2-Butanone (MEK)25.4 ug/m3 2.88 10/22/12 12:30 78-93-31.7
Carbon disulfide 38.1 ug/m3 2.88 10/22/12 12:30 75-15-0 SS1.8
Carbon tetrachloride ND ug/m3 2.88 10/22/12 12:30 56-23-51.8
Chlorobenzene ND ug/m3 2.88 10/22/12 12:30 108-90-72.7
Chloroethane ND ug/m3 2.88 10/22/12 12:30 75-00-31.6
Chloroform ND ug/m3 2.88 10/22/12 12:30 67-66-32.9
Chloromethane ND ug/m3 2.88 10/22/12 12:30 74-87-31.2
Cyclohexane 5.0 ug/m3 2.88 10/22/12 12:30 110-82-72.0
Dibromochloromethane ND ug/m3 2.88 10/22/12 12:30 124-48-15.0
1,2-Dibromoethane (EDB)ND ug/m3 2.88 10/22/12 12:30 106-93-44.5
1,2-Dichlorobenzene ND ug/m3 2.88 10/22/12 12:30 95-50-13.5
1,3-Dichlorobenzene ND ug/m3 2.88 10/22/12 12:30 541-73-13.5
1,4-Dichlorobenzene ND ug/m3 2.88 10/22/12 12:30 106-46-73.5
Dichlorodifluoromethane ND ug/m3 2.88 10/22/12 12:30 75-71-82.9
1,1-Dichloroethane ND ug/m3 2.88 10/22/12 12:30 75-34-32.4
1,2-Dichloroethane ND ug/m3 2.88 10/22/12 12:30 107-06-21.2
1,1-Dichloroethene ND ug/m3 2.88 10/22/12 12:30 75-35-42.3
cis-1,2-Dichloroethene ND ug/m3 2.88 10/22/12 12:30 156-59-22.3
trans-1,2-Dichloroethene ND ug/m3 2.88 10/22/12 12:30 156-60-52.3
1,2-Dichloropropane ND ug/m3 2.88 10/22/12 12:30 78-87-52.7
cis-1,3-Dichloropropene ND ug/m3 2.88 10/22/12 12:30 10061-01-52.6
trans-1,3-Dichloropropene ND ug/m3 2.88 10/22/12 12:30 10061-02-62.6
Dichlorotetrafluoroethane ND ug/m3 2.88 10/22/12 12:30 76-14-24.1
Ethyl acetate ND ug/m3 2.88 10/22/12 12:30 141-78-62.1
Ethylbenzene 3.8 ug/m3 2.88 10/22/12 12:30 100-41-42.5
4-Ethyltoluene 6.6 ug/m3 2.88 10/22/12 12:30 622-96-82.9
n-Heptane 2.5 ug/m3 2.88 10/22/12 12:30 142-82-52.4
Hexachloro-1,3-butadiene ND ug/m3 2.88 10/22/12 12:30 87-68-36.3
n-Hexane ND ug/m3 2.88 10/22/12 12:30 110-54-32.1
2-Hexanone 7.8 ug/m3 2.88 10/22/12 12:30 591-78-62.4
Methylene Chloride ND ug/m3 2.88 10/22/12 12:30 75-09-22.0
4-Methyl-2-pentanone (MIBK)3.3 ug/m3 2.88 10/22/12 12:30 108-10-12.4
Methyl-tert-butyl ether ND ug/m3 2.88 10/22/12 12:30 1634-04-42.1
Naphthalene 197 ug/m3 2.88 10/22/12 12:30 91-20-33.1
Propylene ND ug/m3 2.88 10/22/12 12:30 115-07-11.0
Styrene 2.8 ug/m3 2.88 10/22/12 12:30 100-42-52.5
1,1,2,2-Tetrachloroethane ND ug/m3 2.88 10/22/12 12:30 79-34-52.0
Tetrachloroethene 24.2 ug/m3 2.88 10/22/12 12:30 127-18-42.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 20 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-9 Lab ID:92134797009 Collected:10/10/12 17:41 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 2.88 10/22/12 12:30 109-99-91.7
THC as Gas 3450 ug/m3 2.88 10/22/12 12:30175
Toluene 16.7 ug/m3 2.88 10/22/12 12:30 108-88-32.2
1,2,4-Trichlorobenzene ND ug/m3 2.88 10/22/12 12:30 120-82-14.3
1,1,1-Trichloroethane 5.8 ug/m3 2.88 10/22/12 12:30 71-55-63.2
1,1,2-Trichloroethane ND ug/m3 2.88 10/22/12 12:30 79-00-51.6
Trichloroethene 87.9 ug/m3 2.88 10/22/12 12:30 79-01-61.6
Trichlorofluoromethane ND ug/m3 2.88 10/22/12 12:30 75-69-43.3
1,1,2-Trichlorotrifluoroethane ND ug/m3 2.88 10/22/12 12:30 76-13-14.6
1,2,4-Trimethylbenzene 21.2 ug/m3 2.88 10/22/12 12:30 95-63-62.9
1,3,5-Trimethylbenzene 7.5 ug/m3 2.88 10/22/12 12:30 108-67-82.9
Vinyl acetate ND ug/m3 2.88 10/22/12 12:30 108-05-42.1
Vinyl chloride ND ug/m3 2.88 10/22/12 12:30 75-01-40.75
m&p-Xylene 14.0 ug/m3 2.88 10/22/12 12:30 179601-23-15.1
o-Xylene 6.1 ug/m3 2.88 10/22/12 12:30 95-47-62.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 21 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-10 Lab ID:92134797010 Collected:10/10/12 17:56 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %1.23 10/18/12 14:37 7440-59-74.4
TO15 MSV AIR Analytical Method: TO-15
Acetone 39.3 ug/m3 1.44 10/20/12 22:39 67-64-10.69
Benzene 0.54 ug/m3 1.44 10/20/12 22:39 71-43-20.47
Bromodichloromethane ND ug/m3 1.44 10/20/12 22:39 75-27-42.0
Bromoform ND ug/m3 1.44 10/20/12 22:39 75-25-23.0
Bromomethane ND ug/m3 1.44 10/20/12 22:39 74-83-91.1
1,3-Butadiene ND ug/m3 1.44 10/20/12 22:39 106-99-00.65
2-Butanone (MEK)6.8 ug/m3 1.44 10/20/12 22:39 78-93-30.86
Carbon disulfide ND ug/m3 1.44 10/20/12 22:39 75-15-00.91
Carbon tetrachloride ND ug/m3 1.44 10/20/12 22:39 56-23-50.92
Chlorobenzene ND ug/m3 1.44 10/20/12 22:39 108-90-71.4
Chloroethane ND ug/m3 1.44 10/20/12 22:39 75-00-30.78
Chloroform 3.3 ug/m3 1.44 10/20/12 22:39 67-66-31.4
Chloromethane ND ug/m3 1.44 10/20/12 22:39 74-87-30.60
Cyclohexane ND ug/m3 1.44 10/20/12 22:39 110-82-71.0
Dibromochloromethane ND ug/m3 1.44 10/20/12 22:39 124-48-12.5
1,2-Dibromoethane (EDB)ND ug/m3 1.44 10/20/12 22:39 106-93-42.2
1,2-Dichlorobenzene ND ug/m3 1.44 10/20/12 22:39 95-50-11.8
1,3-Dichlorobenzene ND ug/m3 1.44 10/20/12 22:39 541-73-11.8
1,4-Dichlorobenzene ND ug/m3 1.44 10/20/12 22:39 106-46-71.8
Dichlorodifluoromethane 3.2 ug/m3 1.44 10/20/12 22:39 75-71-81.5
1,1-Dichloroethane ND ug/m3 1.44 10/20/12 22:39 75-34-31.2
1,2-Dichloroethane ND ug/m3 1.44 10/20/12 22:39 107-06-20.59
1,1-Dichloroethene ND ug/m3 1.44 10/20/12 22:39 75-35-41.2
cis-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 22:39 156-59-21.2
trans-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 22:39 156-60-51.2
1,2-Dichloropropane ND ug/m3 1.44 10/20/12 22:39 78-87-51.4
cis-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 22:39 10061-01-51.3
trans-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 22:39 10061-02-61.3
Dichlorotetrafluoroethane ND ug/m3 1.44 10/20/12 22:39 76-14-22.0
Ethyl acetate ND ug/m3 1.44 10/20/12 22:39 141-78-61.1
Ethylbenzene ND ug/m3 1.44 10/20/12 22:39 100-41-41.3
4-Ethyltoluene ND ug/m3 1.44 10/20/12 22:39 622-96-81.4
n-Heptane ND ug/m3 1.44 10/20/12 22:39 142-82-51.2
Hexachloro-1,3-butadiene ND ug/m3 1.44 10/20/12 22:39 87-68-33.2
n-Hexane ND ug/m3 1.44 10/20/12 22:39 110-54-31.0
2-Hexanone 2.1 ug/m3 1.44 10/20/12 22:39 591-78-61.2
Methylene Chloride ND ug/m3 1.44 10/20/12 22:39 75-09-21.0
4-Methyl-2-pentanone (MIBK)ND ug/m3 1.44 10/20/12 22:39 108-10-11.2
Methyl-tert-butyl ether ND ug/m3 1.44 10/20/12 22:39 1634-04-41.1
Naphthalene 7.3 ug/m3 1.44 10/20/12 22:39 91-20-31.5
Propylene ND ug/m3 1.44 10/20/12 22:39 115-07-10.50
Styrene ND ug/m3 1.44 10/20/12 22:39 100-42-51.3
1,1,2,2-Tetrachloroethane ND ug/m3 1.44 10/20/12 22:39 79-34-51.0
Tetrachloroethene 8.5 ug/m3 1.44 10/20/12 22:39 127-18-40.99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 22 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-10 Lab ID:92134797010 Collected:10/10/12 17:56 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.44 10/20/12 22:39 109-99-90.86
THC as Gas 1610 ug/m3 1.44 10/20/12 22:3987.6
Toluene ND ug/m3 1.44 10/20/12 22:39 108-88-31.1
1,2,4-Trichlorobenzene ND ug/m3 1.44 10/20/12 22:39 120-82-12.2
1,1,1-Trichloroethane 2.2 ug/m3 1.44 10/20/12 22:39 71-55-61.6
1,1,2-Trichloroethane ND ug/m3 1.44 10/20/12 22:39 79-00-50.79
Trichloroethene 3330 ug/m3 460.8 10/22/12 15:24 79-01-6 2g,A3253
Trichlorofluoromethane 1.7 ug/m3 1.44 10/20/12 22:39 75-69-41.6
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.44 10/20/12 22:39 76-13-12.3
1,2,4-Trimethylbenzene 2.1 ug/m3 1.44 10/20/12 22:39 95-63-61.4
1,3,5-Trimethylbenzene 1.5 ug/m3 1.44 10/20/12 22:39 108-67-81.4
Vinyl acetate ND ug/m3 1.44 10/20/12 22:39 108-05-41.0
Vinyl chloride ND ug/m3 1.44 10/20/12 22:39 75-01-40.37
m&p-Xylene ND ug/m3 1.44 10/20/12 22:39 179601-23-12.5
o-Xylene ND ug/m3 1.44 10/20/12 22:39 95-47-61.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 23 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-11 Lab ID:92134797011 Collected:10/10/12 19:15 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %1.63 10/18/12 14:46 7440-59-75.9
TO15 MSV AIR Analytical Method: TO-15
Acetone 37.3 ug/m3 1.44 10/20/12 23:08 67-64-10.69
Benzene 0.58 ug/m3 1.44 10/20/12 23:08 71-43-20.47
Bromodichloromethane ND ug/m3 1.44 10/20/12 23:08 75-27-42.0
Bromoform ND ug/m3 1.44 10/20/12 23:08 75-25-23.0
Bromomethane ND ug/m3 1.44 10/20/12 23:08 74-83-91.1
1,3-Butadiene ND ug/m3 1.44 10/20/12 23:08 106-99-00.65
2-Butanone (MEK)3.3 ug/m3 1.44 10/20/12 23:08 78-93-30.86
Carbon disulfide ND ug/m3 1.44 10/20/12 23:08 75-15-00.91
Carbon tetrachloride ND ug/m3 1.44 10/20/12 23:08 56-23-50.92
Chlorobenzene ND ug/m3 1.44 10/20/12 23:08 108-90-71.4
Chloroethane ND ug/m3 1.44 10/20/12 23:08 75-00-30.78
Chloroform ND ug/m3 1.44 10/20/12 23:08 67-66-31.4
Chloromethane 0.96 ug/m3 1.44 10/20/12 23:08 74-87-30.60
Cyclohexane ND ug/m3 1.44 10/20/12 23:08 110-82-71.0
Dibromochloromethane ND ug/m3 1.44 10/20/12 23:08 124-48-12.5
1,2-Dibromoethane (EDB)ND ug/m3 1.44 10/20/12 23:08 106-93-42.2
1,2-Dichlorobenzene ND ug/m3 1.44 10/20/12 23:08 95-50-11.8
1,3-Dichlorobenzene ND ug/m3 1.44 10/20/12 23:08 541-73-11.8
1,4-Dichlorobenzene ND ug/m3 1.44 10/20/12 23:08 106-46-71.8
Dichlorodifluoromethane 3.3 ug/m3 1.44 10/20/12 23:08 75-71-81.5
1,1-Dichloroethane ND ug/m3 1.44 10/20/12 23:08 75-34-31.2
1,2-Dichloroethane ND ug/m3 1.44 10/20/12 23:08 107-06-20.59
1,1-Dichloroethene ND ug/m3 1.44 10/20/12 23:08 75-35-41.2
cis-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 23:08 156-59-21.2
trans-1,2-Dichloroethene ND ug/m3 1.44 10/20/12 23:08 156-60-51.2
1,2-Dichloropropane ND ug/m3 1.44 10/20/12 23:08 78-87-51.4
cis-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 23:08 10061-01-51.3
trans-1,3-Dichloropropene ND ug/m3 1.44 10/20/12 23:08 10061-02-61.3
Dichlorotetrafluoroethane ND ug/m3 1.44 10/20/12 23:08 76-14-22.0
Ethyl acetate ND ug/m3 1.44 10/20/12 23:08 141-78-61.1
Ethylbenzene ND ug/m3 1.44 10/20/12 23:08 100-41-41.3
4-Ethyltoluene ND ug/m3 1.44 10/20/12 23:08 622-96-81.4
n-Heptane 1.5 ug/m3 1.44 10/20/12 23:08 142-82-51.2
Hexachloro-1,3-butadiene ND ug/m3 1.44 10/20/12 23:08 87-68-33.2
n-Hexane ND ug/m3 1.44 10/20/12 23:08 110-54-31.0
2-Hexanone ND ug/m3 1.44 10/20/12 23:08 591-78-61.2
Methylene Chloride 1.5 ug/m3 1.44 10/20/12 23:08 75-09-21.0
4-Methyl-2-pentanone (MIBK)ND ug/m3 1.44 10/20/12 23:08 108-10-11.2
Methyl-tert-butyl ether ND ug/m3 1.44 10/20/12 23:08 1634-04-41.1
Naphthalene 3.4 ug/m3 1.44 10/20/12 23:08 91-20-31.5
Propylene ND ug/m3 1.44 10/20/12 23:08 115-07-10.50
Styrene ND ug/m3 1.44 10/20/12 23:08 100-42-51.3
1,1,2,2-Tetrachloroethane ND ug/m3 1.44 10/20/12 23:08 79-34-51.0
Tetrachloroethene 1.8 ug/m3 1.44 10/20/12 23:08 127-18-40.99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 24 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-11 Lab ID:92134797011 Collected:10/10/12 19:15 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.44 10/20/12 23:08 109-99-90.86
THC as Gas 246 ug/m3 1.44 10/20/12 23:0887.6
Toluene 1.9 ug/m3 1.44 10/20/12 23:08 108-88-31.1
1,2,4-Trichlorobenzene ND ug/m3 1.44 10/20/12 23:08 120-82-12.2
1,1,1-Trichloroethane ND ug/m3 1.44 10/20/12 23:08 71-55-61.6
1,1,2-Trichloroethane ND ug/m3 1.44 10/20/12 23:08 79-00-50.79
Trichloroethene 8.9 ug/m3 1.44 10/20/12 23:08 79-01-60.79
Trichlorofluoromethane 1.8 ug/m3 1.44 10/20/12 23:08 75-69-41.6
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.44 10/20/12 23:08 76-13-12.3
1,2,4-Trimethylbenzene 1.9 ug/m3 1.44 10/20/12 23:08 95-63-61.4
1,3,5-Trimethylbenzene ND ug/m3 1.44 10/20/12 23:08 108-67-81.4
Vinyl acetate ND ug/m3 1.44 10/20/12 23:08 108-05-41.0
Vinyl chloride ND ug/m3 1.44 10/20/12 23:08 75-01-40.37
m&p-Xylene 3.4 ug/m3 1.44 10/20/12 23:08 179601-23-12.5
o-Xylene 1.4 ug/m3 1.44 10/20/12 23:08 95-47-61.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 25 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-12 Lab ID:92134797012 Collected:10/10/12 19:17 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Method 3C AIR - Fixed Gases Analytical Method: Method 3C Gases
Helium ND %1.38 10/18/12 14:56 7440-59-75.0
TO15 MSV AIR Analytical Method: TO-15
Acetone 17.2 ug/m3 1.55 10/20/12 23:37 67-64-10.74
Benzene 2.6 ug/m3 1.55 10/20/12 23:37 71-43-20.50
Bromodichloromethane ND ug/m3 1.55 10/20/12 23:37 75-27-42.1
Bromoform ND ug/m3 1.55 10/20/12 23:37 75-25-23.3
Bromomethane ND ug/m3 1.55 10/20/12 23:37 74-83-91.2
1,3-Butadiene ND ug/m3 1.55 10/20/12 23:37 106-99-00.70
2-Butanone (MEK)1.3 ug/m3 1.55 10/20/12 23:37 78-93-30.93
Carbon disulfide ND ug/m3 1.55 10/20/12 23:37 75-15-00.98
Carbon tetrachloride 1.0 ug/m3 1.55 10/20/12 23:37 56-23-50.99
Chlorobenzene ND ug/m3 1.55 10/20/12 23:37 108-90-71.5
Chloroethane ND ug/m3 1.55 10/20/12 23:37 75-00-30.84
Chloroform 26.1 ug/m3 1.55 10/20/12 23:37 67-66-31.5
Chloromethane ND ug/m3 1.55 10/20/12 23:37 74-87-30.65
Cyclohexane 1.1 ug/m3 1.55 10/20/12 23:37 110-82-71.1
Dibromochloromethane ND ug/m3 1.55 10/20/12 23:37 124-48-12.7
1,2-Dibromoethane (EDB)ND ug/m3 1.55 10/20/12 23:37 106-93-42.4
1,2-Dichlorobenzene ND ug/m3 1.55 10/20/12 23:37 95-50-11.9
1,3-Dichlorobenzene ND ug/m3 1.55 10/20/12 23:37 541-73-11.9
1,4-Dichlorobenzene ND ug/m3 1.55 10/20/12 23:37 106-46-71.9
Dichlorodifluoromethane 2.8 ug/m3 1.55 10/20/12 23:37 75-71-81.6
1,1-Dichloroethane 3.7 ug/m3 1.55 10/20/12 23:37 75-34-31.3
1,2-Dichloroethane ND ug/m3 1.55 10/20/12 23:37 107-06-20.64
1,1-Dichloroethene 10500 ug/m3 396.8 10/24/12 06:12 75-35-4 A3321
cis-1,2-Dichloroethene 96.7 ug/m3 1.55 10/20/12 23:37 156-59-21.3
trans-1,2-Dichloroethene 14.4 ug/m3 1.55 10/20/12 23:37 156-60-51.3
1,2-Dichloropropane ND ug/m3 1.55 10/20/12 23:37 78-87-51.5
cis-1,3-Dichloropropene ND ug/m3 1.55 10/20/12 23:37 10061-01-51.4
trans-1,3-Dichloropropene ND ug/m3 1.55 10/20/12 23:37 10061-02-61.4
Dichlorotetrafluoroethane ND ug/m3 1.55 10/20/12 23:37 76-14-22.2
Ethyl acetate ND ug/m3 1.55 10/20/12 23:37 141-78-61.1
Ethylbenzene ND ug/m3 1.55 10/20/12 23:37 100-41-41.4
4-Ethyltoluene ND ug/m3 1.55 10/20/12 23:37 622-96-81.6
n-Heptane ND ug/m3 1.55 10/20/12 23:37 142-82-51.3
Hexachloro-1,3-butadiene ND ug/m3 1.55 10/20/12 23:37 87-68-33.4
n-Hexane ND ug/m3 1.55 10/20/12 23:37 110-54-31.1
2-Hexanone ND ug/m3 1.55 10/20/12 23:37 591-78-61.3
Methylene Chloride ND ug/m3 1.55 10/20/12 23:37 75-09-21.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 1.55 10/20/12 23:37 108-10-11.3
Methyl-tert-butyl ether ND ug/m3 1.55 10/20/12 23:37 1634-04-41.1
Naphthalene ND ug/m3 1.55 10/20/12 23:37 91-20-31.7
Propylene ND ug/m3 1.55 10/20/12 23:37 115-07-10.54
Styrene ND ug/m3 1.55 10/20/12 23:37 100-42-51.3
1,1,2,2-Tetrachloroethane ND ug/m3 1.55 10/20/12 23:37 79-34-51.1
Tetrachloroethene 30200 ug/m3 396.8 10/24/12 06:12 127-18-4 1g,A3273
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 26 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Sample:SG-12 Lab ID:92134797012 Collected:10/10/12 19:17 Received:10/11/12 08:30 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
TO15 MSV AIR Analytical Method: TO-15
Tetrahydrofuran ND ug/m3 1.55 10/20/12 23:37 109-99-90.93
THC as Gas 9890 ug/m3 1.55 10/20/12 23:3794.2
Toluene 1.7 ug/m3 1.55 10/20/12 23:37 108-88-31.2
1,2,4-Trichlorobenzene ND ug/m3 1.55 10/20/12 23:37 120-82-12.3
1,1,1-Trichloroethane 1490 ug/m3 396.8 10/24/12 06:12 71-55-6 A3440
1,1,2-Trichloroethane ND ug/m3 1.55 10/20/12 23:37 79-00-50.85
Trichloroethene 94600 ug/m3 7936 10/23/12 16:39 79-01-6 A34360
Trichlorofluoromethane 1.9 ug/m3 1.55 10/20/12 23:37 75-69-41.8
1,1,2-Trichlorotrifluoroethane ND ug/m3 1.55 10/20/12 23:37 76-13-12.5
1,2,4-Trimethylbenzene ND ug/m3 1.55 10/20/12 23:37 95-63-61.5
1,3,5-Trimethylbenzene ND ug/m3 1.55 10/20/12 23:37 108-67-81.5
Vinyl acetate ND ug/m3 1.55 10/20/12 23:37 108-05-41.1
Vinyl chloride ND ug/m3 1.55 10/20/12 23:37 75-01-40.40
m&p-Xylene ND ug/m3 1.55 10/20/12 23:37 179601-23-12.7
o-Xylene ND ug/m3 1.55 10/20/12 23:37 95-47-61.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 27 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
AIR/15970
Method 3C Gases
Method 3C Gases
METHOD 3C AIR - FIXED GASES
Associated Lab Samples:92134797001, 92134797002, 92134797003, 92134797004, 92134797005, 92134797006, 92134797007,
92134797008, 92134797009, 92134797010, 92134797011, 92134797012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1312336
Associated Lab Samples:92134797001, 92134797002, 92134797003, 92134797004, 92134797005, 92134797006, 92134797007,
92134797008, 92134797009, 92134797010, 92134797011, 92134797012
Matrix:Air
Analyzed
Helium %ND 3.6 10/18/12 12:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1312337LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1312338
Helium %18.618 103 70-1309116.5 12 30
Parameter Units
Dup
Result QualifiersRPDResult
92134797001
1312418SAMPLE DUPLICATE:
Helium %NDND
Parameter Units
Dup
Result QualifiersRPDResult
92134797009
1312542SAMPLE DUPLICATE:
Helium %6.8ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 28 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
AIR/15992
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92134797001, 92134797002, 92134797003, 92134797004, 92134797005, 92134797006, 92134797007,
92134797008, 92134797010, 92134797011, 92134797012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1314621
Associated Lab Samples:92134797001, 92134797002, 92134797003, 92134797004, 92134797005, 92134797006, 92134797007,
92134797008, 92134797010, 92134797011, 92134797012
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 10/20/12 15:25
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 10/20/12 15:25
1,1,2-Trichloroethane ug/m3 ND 0.55 10/20/12 15:25
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 10/20/12 15:25
1,1-Dichloroethane ug/m3 ND 0.82 10/20/12 15:25
1,1-Dichloroethene ug/m3 ND 0.81 10/20/12 15:25
1,2,4-Trichlorobenzene ug/m3 ND 1.5 10/20/12 15:25
1,2,4-Trimethylbenzene ug/m3 ND 1.0 10/20/12 15:25
1,2-Dibromoethane (EDB)ug/m3 ND 1.6 10/20/12 15:25
1,2-Dichlorobenzene ug/m3 ND 1.2 10/20/12 15:25
1,2-Dichloroethane ug/m3 ND 0.41 10/20/12 15:25
1,2-Dichloropropane ug/m3 ND 0.94 10/20/12 15:25
1,3,5-Trimethylbenzene ug/m3 ND 1.0 10/20/12 15:25
1,3-Butadiene ug/m3 ND 0.45 10/20/12 15:25
1,3-Dichlorobenzene ug/m3 ND 1.2 10/20/12 15:25
1,4-Dichlorobenzene ug/m3 ND 1.2 10/20/12 15:25
2-Butanone (MEK)ug/m3 ND 0.60 10/20/12 15:25
2-Hexanone ug/m3 ND 0.83 10/20/12 15:25
4-Ethyltoluene ug/m3 ND 1.0 10/20/12 15:25
4-Methyl-2-pentanone (MIBK)ug/m3 ND 0.83 10/20/12 15:25
Acetone ug/m3 ND 0.48 10/20/12 15:25
Benzene ug/m3 ND 0.32 10/20/12 15:25
Bromodichloromethane ug/m3 ND 1.4 10/20/12 15:25
Bromoform ug/m3 ND 2.1 10/20/12 15:25
Bromomethane ug/m3 ND 0.79 10/20/12 15:25
Carbon disulfide ug/m3 ND 0.63 10/20/12 15:25
Carbon tetrachloride ug/m3 ND 0.64 10/20/12 15:25
Chlorobenzene ug/m3 ND 0.94 10/20/12 15:25
Chloroethane ug/m3 ND 0.54 10/20/12 15:25
Chloroform ug/m3 ND 0.99 10/20/12 15:25
Chloromethane ug/m3 ND 0.42 10/20/12 15:25
cis-1,2-Dichloroethene ug/m3 ND 0.81 10/20/12 15:25
cis-1,3-Dichloropropene ug/m3 ND 0.92 10/20/12 15:25
Cyclohexane ug/m3 ND 0.70 10/20/12 15:25
Dibromochloromethane ug/m3 ND 1.7 10/20/12 15:25
Dichlorodifluoromethane ug/m3 ND 1.0 10/20/12 15:25
Dichlorotetrafluoroethane ug/m3 ND 1.4 10/20/12 15:25
Ethyl acetate ug/m3 ND 0.73 10/20/12 15:25
Ethylbenzene ug/m3 ND 0.88 10/20/12 15:25
Hexachloro-1,3-butadiene ug/m3 ND 2.2 10/20/12 15:25
m&p-Xylene ug/m3 ND 1.8 10/20/12 15:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 29 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1314621
Associated Lab Samples:92134797001, 92134797002, 92134797003, 92134797004, 92134797005, 92134797006, 92134797007,
92134797008, 92134797010, 92134797011, 92134797012
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 0.73 10/20/12 15:25
Methylene Chloride ug/m3 ND 0.71 10/20/12 15:25
n-Heptane ug/m3 ND 0.83 10/20/12 15:25
n-Hexane ug/m3 ND 0.72 10/20/12 15:25
Naphthalene ug/m3 ND 1.1 10/20/12 15:25
o-Xylene ug/m3 ND 0.88 10/20/12 15:25
Propylene ug/m3 ND 0.35 10/20/12 15:25
Styrene ug/m3 ND 0.87 10/20/12 15:25
Tetrachloroethene ug/m3 ND 0.69 10/20/12 15:25
Tetrahydrofuran ug/m3 ND 0.60 10/20/12 15:25
THC as Gas ug/m3 ND 60.8 10/20/12 15:25
Toluene ug/m3 ND 0.77 10/20/12 15:25
trans-1,2-Dichloroethene ug/m3 ND 0.81 10/20/12 15:25
trans-1,3-Dichloropropene ug/m3 ND 0.92 10/20/12 15:25
Trichloroethene ug/m3 ND 0.55 10/20/12 15:25
Trichlorofluoromethane ug/m3 ND 1.1 10/20/12 15:25
Vinyl acetate ug/m3 ND 0.72 10/20/12 15:25
Vinyl chloride ug/m3 ND 0.26 10/20/12 15:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1314622LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 53.955.5 97 72-129
1,1,2,2-Tetrachloroethane ug/m3 71.869.8 103 73-131
1,1,2-Trichloroethane ug/m3 59.155.5 107 71-128
1,1,2-Trichlorotrifluoroethane ug/m3 72.877.9 93 65-132
1,1-Dichloroethane ug/m3 39.241.2 95 67-132
1,1-Dichloroethene ug/m3 39.340.3 98 68-134
1,2,4-Trichlorobenzene ug/m3 72.275.5 96 48-150
1,2,4-Trimethylbenzene ug/m3 49.750 99 72-127
1,2-Dibromoethane (EDB)ug/m3 85.278.1 109 75-130
1,2-Dichlorobenzene ug/m3 59.461.2 97 71-132
1,2-Dichloroethane ug/m3 41.041.2 100 70-131
1,2-Dichloropropane ug/m3 47.847 102 73-130
1,3,5-Trimethylbenzene ug/m3 48.850 98 70-133
1,3-Butadiene ug/m3 21.122.5 94 69-132
1,3-Dichlorobenzene ug/m3 60.261.2 98 71-128
1,4-Dichlorobenzene ug/m3 61.561.2 101 72-131
2-Butanone (MEK)ug/m3 28.730 96 69-131
2-Hexanone ug/m3 45.641.7 110 71-134
4-Ethyltoluene ug/m3 49.450 99 71-129
4-Methyl-2-pentanone (MIBK)ug/m3 44.741.7 107 69-135
Acetone ug/m3 24.024.2 99 61-139
Benzene ug/m3 32.432.5 100 69-134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 30 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1314622LABORATORY CONTROL SAMPLE:
LCSSpike
Bromodichloromethane ug/m3 71.568.2 105 71-130
Bromoform ug/m3 104105 99 70-130
Bromomethane ug/m3 37.639.5 95 69-125
Carbon disulfide ug/m3 28.7 SS31.7 91 66-131
Carbon tetrachloride ug/m3 60.964 95 68-128
Chlorobenzene ug/m3 47.746.8 102 75-128
Chloroethane ug/m3 26.126.8 97 66-131
Chloroform ug/m3 48.249.7 97 68-132
Chloromethane ug/m3 19.521 93 60-139
cis-1,2-Dichloroethene ug/m3 43.340.3 107 73-130
cis-1,3-Dichloropropene ug/m3 50.946.2 110 74-134
Cyclohexane ug/m3 35.735 102 67-136
Dibromochloromethane ug/m3 95.086.6 110 69-131
Dichlorodifluoromethane ug/m3 47.450.3 94 67-131
Dichlorotetrafluoroethane ug/m3 66.371.1 93 66-130
Ethyl acetate ug/m3 40.436.6 110 71-131
Ethylbenzene ug/m3 44.844.2 101 69-139
Hexachloro-1,3-butadiene ug/m3 151108 140 41-150
m&p-Xylene ug/m3 90.788.3 103 66-137
Methyl-tert-butyl ether ug/m3 35.136.7 96 70-132
Methylene Chloride ug/m3 31.935.3 90 73-134
n-Heptane ug/m3 42.441.7 102 70-134
n-Hexane ug/m3 32.835.8 92 65-133
Naphthalene ug/m3 50.553.3 95 57-150
o-Xylene ug/m3 43.944.2 99 69-138
Propylene ug/m3 15.417.5 88 70-134
Styrene ug/m3 50.043.3 116 72-132
Tetrachloroethene ug/m3 67.469 98 70-130
Tetrahydrofuran ug/m3 31.830 106 74-128
THC as Gas ug/m3 29303030 97 66-131
Toluene ug/m3 37.638.3 98 71-132
trans-1,2-Dichloroethene ug/m3 37.840.3 94 72-128
trans-1,3-Dichloropropene ug/m3 47.946.2 104 73-130
Trichloroethene ug/m3 50.354.6 92 72-131
Trichlorofluoromethane ug/m3 51.957.1 91 66-129
Vinyl acetate ug/m3 40.935.8 114 71-131
Vinyl chloride ug/m3 24.526 94 70-131
Parameter Units
Dup
Result QualifiersRPDResult
10208592001
1315099SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 31 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Parameter Units
Dup
Result QualifiersRPDResult
10208592001
1315099SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 46.9 649.6
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 12.8 713.7
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 31.5 231.9
2-Butanone (MEK)ug/m3 11.0 511.6
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 22.8 624.2
4-Methyl-2-pentanone (MIBK)ug/m3 4.6 44.4
Acetone ug/m3 82.6 688.1
Benzene ug/m3 1.8 .71.8
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 .6JND
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 .37JND
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 1.3 41.3
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.2 22.3
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 29.6 229.0
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 106 3109
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 .58JND
n-Heptane ug/m3 7.4 27.3
n-Hexane ug/m3 5.3 .065.2
Naphthalene ug/m3 6.2 56.5
o-Xylene ug/m3 36.6 538.3
Propylene ug/m3 NDND
Styrene ug/m3 23.6 .823.8
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 3.8 23.7
THC as Gas ug/m3 1720 31670
Toluene ug/m3 38.8 139.2
trans-1,2-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 32 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Parameter Units
Dup
Result QualifiersRPDResult
10208592001
1315099SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 0.94 20.96
Trichlorofluoromethane ug/m3 1.2JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 33 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
AIR/15998
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92134797009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1315289
Associated Lab Samples:92134797009
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 10/22/12 11:32
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 10/22/12 11:32
1,1,2-Trichloroethane ug/m3 ND 0.55 10/22/12 11:32
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 10/22/12 11:32
1,1-Dichloroethane ug/m3 ND 0.82 10/22/12 11:32
1,1-Dichloroethene ug/m3 ND 0.81 10/22/12 11:32
1,2,4-Trichlorobenzene ug/m3 ND 1.5 10/22/12 11:32
1,2,4-Trimethylbenzene ug/m3 ND 1.0 10/22/12 11:32
1,2-Dibromoethane (EDB)ug/m3 ND 1.6 10/22/12 11:32
1,2-Dichlorobenzene ug/m3 ND 1.2 10/22/12 11:32
1,2-Dichloroethane ug/m3 ND 0.41 10/22/12 11:32
1,2-Dichloropropane ug/m3 ND 0.94 10/22/12 11:32
1,3,5-Trimethylbenzene ug/m3 ND 1.0 10/22/12 11:32
1,3-Butadiene ug/m3 ND 0.45 10/22/12 11:32
1,3-Dichlorobenzene ug/m3 ND 1.2 10/22/12 11:32
1,4-Dichlorobenzene ug/m3 ND 1.2 10/22/12 11:32
2-Butanone (MEK)ug/m3 ND 0.60 10/22/12 11:32
2-Hexanone ug/m3 ND 0.83 10/22/12 11:32
4-Ethyltoluene ug/m3 ND 1.0 10/22/12 11:32
4-Methyl-2-pentanone (MIBK)ug/m3 ND 0.83 10/22/12 11:32
Acetone ug/m3 ND 0.48 10/22/12 11:32
Benzene ug/m3 ND 0.32 10/22/12 11:32
Bromodichloromethane ug/m3 ND 1.4 10/22/12 11:32
Bromoform ug/m3 ND 2.1 10/22/12 11:32
Bromomethane ug/m3 ND 0.79 10/22/12 11:32
Carbon disulfide ug/m3 ND 0.63 10/22/12 11:32
Carbon tetrachloride ug/m3 ND 0.64 10/22/12 11:32
Chlorobenzene ug/m3 ND 0.94 10/22/12 11:32
Chloroethane ug/m3 ND 0.54 10/22/12 11:32
Chloroform ug/m3 ND 0.99 10/22/12 11:32
Chloromethane ug/m3 ND 0.42 10/22/12 11:32
cis-1,2-Dichloroethene ug/m3 ND 0.81 10/22/12 11:32
cis-1,3-Dichloropropene ug/m3 ND 0.92 10/22/12 11:32
Cyclohexane ug/m3 ND 0.70 10/22/12 11:32
Dibromochloromethane ug/m3 ND 1.7 10/22/12 11:32
Dichlorodifluoromethane ug/m3 ND 1.0 10/22/12 11:32
Dichlorotetrafluoroethane ug/m3 ND 1.4 10/22/12 11:32
Ethyl acetate ug/m3 ND 0.73 10/22/12 11:32
Ethylbenzene ug/m3 ND 0.88 10/22/12 11:32
Hexachloro-1,3-butadiene ug/m3 ND 2.2 10/22/12 11:32
m&p-Xylene ug/m3 ND 1.8 10/22/12 11:32
Methyl-tert-butyl ether ug/m3 ND 0.73 10/22/12 11:32
Methylene Chloride ug/m3 ND 0.71 10/22/12 11:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 34 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1315289
Associated Lab Samples:92134797009
Matrix:Air
Analyzed
n-Heptane ug/m3 ND 0.83 10/22/12 11:32
n-Hexane ug/m3 ND 0.72 10/22/12 11:32
Naphthalene ug/m3 ND 1.1 10/22/12 11:32
o-Xylene ug/m3 ND 0.88 10/22/12 11:32
Propylene ug/m3 ND 0.35 10/22/12 11:32
Styrene ug/m3 ND 0.87 10/22/12 11:32
Tetrachloroethene ug/m3 ND 0.69 10/22/12 11:32
Tetrahydrofuran ug/m3 ND 0.60 10/22/12 11:32
THC as Gas ug/m3 ND 60.8 10/22/12 11:32
Toluene ug/m3 ND 0.77 10/22/12 11:32
trans-1,2-Dichloroethene ug/m3 ND 0.81 10/22/12 11:32
trans-1,3-Dichloropropene ug/m3 ND 0.92 10/22/12 11:32
Trichloroethene ug/m3 ND 0.55 10/22/12 11:32
Trichlorofluoromethane ug/m3 ND 1.1 10/22/12 11:32
Vinyl acetate ug/m3 ND 0.72 10/22/12 11:32
Vinyl chloride ug/m3 ND 0.26 10/22/12 11:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1315290LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 62.055.5 112 72-129
1,1,2,2-Tetrachloroethane ug/m3 82.369.8 118 73-131
1,1,2-Trichloroethane ug/m3 61.055.5 110 71-128
1,1,2-Trichlorotrifluoroethane ug/m3 86.977.9 111 65-132
1,1-Dichloroethane ug/m3 44.741.2 109 67-132
1,1-Dichloroethene ug/m3 44.340.3 110 68-134
1,2,4-Trichlorobenzene ug/m3 56.975.5 75 48-150
1,2,4-Trimethylbenzene ug/m3 57.150 114 72-127
1,2-Dibromoethane (EDB)ug/m3 96.578.1 123 75-130
1,2-Dichlorobenzene ug/m3 69.661.2 114 71-132
1,2-Dichloroethane ug/m3 43.941.2 107 70-131
1,2-Dichloropropane ug/m3 50.147 107 73-130
1,3,5-Trimethylbenzene ug/m3 57.350 115 70-133
1,3-Butadiene ug/m3 24.422.5 108 69-132
1,3-Dichlorobenzene ug/m3 68.261.2 112 71-128
1,4-Dichlorobenzene ug/m3 68.361.2 112 72-131
2-Butanone (MEK)ug/m3 33.030 110 69-131
2-Hexanone ug/m3 51.841.7 124 71-134
4-Ethyltoluene ug/m3 57.550 115 71-129
4-Methyl-2-pentanone (MIBK)ug/m3 46.441.7 111 69-135
Acetone ug/m3 27.024.2 112 61-139
Benzene ug/m3 36.232.5 112 69-134
Bromodichloromethane ug/m3 76.668.2 112 71-130
Bromoform ug/m3 127105 120 70-130
Bromomethane ug/m3 47.239.5 120 69-125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 35 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1315290LABORATORY CONTROL SAMPLE:
LCSSpike
Carbon disulfide ug/m3 34.8 SS31.7 110 66-131
Carbon tetrachloride ug/m3 69.064 108 68-128
Chlorobenzene ug/m3 54.846.8 117 75-128
Chloroethane ug/m3 31.126.8 116 66-131
Chloroform ug/m3 54.849.7 110 68-132
Chloromethane ug/m3 22.521 107 60-139
cis-1,2-Dichloroethene ug/m3 47.640.3 118 73-130
cis-1,3-Dichloropropene ug/m3 52.646.2 114 74-134
Cyclohexane ug/m3 38.635 110 67-136
Dibromochloromethane ug/m3 11186.6 128 69-131
Dichlorodifluoromethane ug/m3 55.950.3 111 67-131
Dichlorotetrafluoroethane ug/m3 80.071.1 112 66-130
Ethyl acetate ug/m3 41.736.6 114 71-131
Ethylbenzene ug/m3 51.444.2 116 69-139
Hexachloro-1,3-butadiene ug/m3 202 CH,L310818641-150
m&p-Xylene ug/m3 10388.3 117 66-137
Methyl-tert-butyl ether ug/m3 41.436.7 113 70-132
Methylene Chloride ug/m3 35.435.3 100 73-134
n-Heptane ug/m3 43.241.7 104 70-134
n-Hexane ug/m3 35.935.8 100 65-133
Naphthalene ug/m3 45.153.3 85 57-150
o-Xylene ug/m3 49.944.2 113 69-138
Propylene ug/m3 17.317.5 99 70-134
Styrene ug/m3 56.043.3 129 72-132
Tetrachloroethene ug/m3 86.369 125 70-130
Tetrahydrofuran ug/m3 33.830 113 74-128
THC as Gas ug/m3 31203030 103 66-131
Toluene ug/m3 39.638.3 103 71-132
trans-1,2-Dichloroethene ug/m3 45.740.3 113 72-128
trans-1,3-Dichloropropene ug/m3 49.346.2 107 73-130
Trichloroethene ug/m3 55.454.6 101 72-131
Trichlorofluoromethane ug/m3 60.757.1 106 66-129
Vinyl acetate ug/m3 52.1 CH,L335.8 145 71-131
Vinyl chloride ug/m3 29.126 112 70-131
Parameter Units
Dup
Result QualifiersRPDResult
10209005002
1315987SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 34.6 1230.8
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 21.4 819.7
1,2-Dibromoethane (EDB)ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 36 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Parameter Units
Dup
Result QualifiersRPDResult
10209005002
1315987SAMPLE DUPLICATE:
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 2.0ND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 5.4 35.2
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 3.6 123.2
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 6.3 75.9
4-Methyl-2-pentanone (MIBK)ug/m3 1JND
Acetone ug/m3 43.9 940.3
Benzene ug/m3 NDND
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 .96JND
Carbon tetrachloride ug/m3 .6JND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 NDND
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.7 112.4
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 4.1 73.9
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 15.8 614.9
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 .95JND
n-Heptane ug/m3 3.0 42.8
n-Hexane ug/m3 3.4 73.2
Naphthalene ug/m3 5.8 35.6
o-Xylene ug/m3 7.5 57.1
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 2.4 52.3
Tetrahydrofuran ug/m3 NDND
THC as Gas ug/m3 3640 63410
Toluene ug/m3 33.3 731.2
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.2JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 37 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Parameter Units
Dup
Result QualifiersRPDResult
10209005002
1315987SAMPLE DUPLICATE:
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 38 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
The internal standard recoveries associated with this sample exceed the lower control limit (-/40% of initial calibration
standard). Results confirmed by second analysis.1g
The internal standard recoveries associated with this sample exceed the upper control limit (+/40% of initial calibration
standard). Results confirmed by second analysis.2g
The sample was analyzed by serial dilution.A3
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
cCH
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
This analyte did not meet the secondary source verification criteria for the initial calibration. The reported result should be
considered an estimated value.SS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 39 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92134797
ATHERTON MILLS 6228-12-0051
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92134797001 AIR/15970SG-1 Method 3C Gases
92134797002 AIR/15970SG-2 Method 3C Gases
92134797003 AIR/15970SG-3 Method 3C Gases
92134797004 AIR/15970SG-4 Method 3C Gases
92134797005 AIR/15970SG-5 Method 3C Gases
92134797006 AIR/15970SG-6 Method 3C Gases
92134797007 AIR/15970SG-7 Method 3C Gases
92134797008 AIR/15970SG-8 Method 3C Gases
92134797009 AIR/15970SG-9 Method 3C Gases
92134797010 AIR/15970SG-10 Method 3C Gases
92134797011 AIR/15970SG-11 Method 3C Gases
92134797012 AIR/15970SG-12 Method 3C Gases
92134797001 AIR/15992SG-1 TO-15
92134797002 AIR/15992SG-2 TO-15
92134797003 AIR/15992SG-3 TO-15
92134797004 AIR/15992SG-4 TO-15
92134797005 AIR/15992SG-5 TO-15
92134797006 AIR/15992SG-6 TO-15
92134797007 AIR/15992SG-7 TO-15
92134797008 AIR/15992SG-8 TO-15
92134797009 AIR/15998SG-9 TO-15
92134797010 AIR/15992SG-10 TO-15
92134797011 AIR/15992SG-11 TO-15
92134797012 AIR/15992SG-12 TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/25/2012 04:33 PM Page 40 of 40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]