20094_Soil Assessment Report_20170216

Via Email
February 16, 2017

NC Department of Environmental Quality Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646
Attention: Mr. Bill Schmithorst, PG
Re: Brownfields Limited Soil Assessment Report
Former Belmont Dyers
18 Linestowe Drive Belmont, North Carolina Brownfields Project No. 20094-16-036
H&H Job No. RPH-001

Dear Bill: Please find the attached Brownfields Limited Soil Assessment Report in PDF format for the
above-referenced site.

If you have any questions or comments, please feel free to contact me.
Very truly yours,
Hart & Hickman, PC

Steven C. Hart, PG Brett Lawrence
Principal Hydrogeologist Project Geologist
Attachment

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Limited Soil Assessment
Former Belmont Dyers Facility
18 Linestowe Dr
Belmont, North Carolina H&H Job No. RPH-001

Table of Contents

1.0 Introduction .............................................................................................................................1
2.0 Background Information .......................................................................................................1
3.0 Soil Assessment ........................................................................................................................3
3.1 Soil Sampling Methodology ..................................................................................................3
3.2 Soil Sampling Results ............................................................................................................5
3.3 Risk Calculation ....................................................................................................................6
4.0 Summary ...................................................................................................................................6

List of Tables

Table 1 Summary of Soil Assessment Analytical Results

List of Figures

Figure 1 Site Location Map
Figure 2 Soil Boring Sample Location Map

List of Appendices
Appendix A Boring Logs
Appendix B Laboratory Analytical Report
Appendix C Cumulative Risk Calculation Output for SB-2

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Limited Soil Assessment
Former Belmont Dyers Facility
18 Linestowe Dr
Belmont, North Carolina H&H Job No. RPH-001

1.0 Introduction

Hart & Hickman, PC (H&H) has prepared this report to document limited soil assessment
activities conducted at the former Belmont Dyers facility located at 18 Linestowe Drive in
Belmont, Gaston County, North Carolina (site). A site location map is provided as Figure 1, and
a sample location map is provided as Figure 2.

The site is planned to be redeveloped with single-family attached and multi-family residential
units. Based upon the preliminary redevelopment grading plans, there will be approximately 3 ft
of cut soil in the northern, western, and central portions of the site, approximately 6 ft of fill soil
in the southeastern portion of the site, and 5 ft of cut soil and 5 ft of fill soil in the eastern portion
of the site. The assessment activities were conducted to provide a preliminary evaluation of soil
which may be cut and used for fill on-site and to evaluate soil which may be exposed at the
surface as a result of overlying soil removal.

A summary of background information is provided in Section 2.0, and the methods and results of
the soil assessment activities are provided in Section 3.0.

2.0 Background Information

On October 26, 2016, H&H completed a Phase I Environmental Site Assessment (ESA) for the
former Belmont Dyers facility property. The results of the Phase I ESA indicated that the site
was developed with a textile mill prior to the earliest historical resource reviewed, a 1929
Sanborn Map. At that time, the site contained a main production building, a boiler building, an
attached warehouse, caustic and sulfuric acid tanks, gasoline underground storage tanks, a
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detached warehouse, and an office building. Two railroad spurs serviced the site until the mid-
1960s. An attached dye house addition was completed by 1965.

Former textile operations at the site consisted of yarn mercerizing, bleaching, and dyeing. The
site was occupied by the Belmont Processing Company until the mid-1940s, when Aberfoyle
Manufacturing Company took over operations at the site. The site was operated by Belmont
Dyers Company from the mid-1970s until 2003. During this time period, Michelle Textiles also
operated in a portion of the building. The former mill buildings were razed beginning in mid-
2007 and the site has remained vacant since that time. The former office building is the only
structure that remains at the site.

Soil and groundwater assessment have been conducted at the site from 1991 to the present.
Assessment and remediation are currently being conducted by the Remediating Party Meridian
Specialty Yarn Group, Inc. (Meridian) pursuant to a voluntary Administrative Agreement (AA)
with the North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites
Branch (IHSB) Registered Environmental Consultant (REC) program. Currently, a Remedial
Investigation (RI) is being performed to define the extent of compounds in environmental media.

Results of groundwater assessment indicate that groundwater impacts (primarily
tetrachloroethene or PCE) are present in the central, southern, and eastern portions of the site at
concentrations exceeding North Carolina groundwater standards. Analytical results of the most
recent groundwater sampling event conducted in March 2016 indicated concentrations of PCE,
1,2,4-trichlorobenzene, and 1,4-dichlorobenzene exceeding North Carolina residential and non-
residential vapor intrusion screening levels in the southern and eastern portions of the site.

On February 6, 2007, during demolition activities at the site, a fuel line associated with a 5,000-
gallon oil aboveground storage tank (AST) was ruptured resulting in a release incident. The oil
entered a stormwater drain and discharged into the Catawba River east of the site. Because the
discharge of oil to the Catawba River violated the Clean Water Act, the United States
Environmental Protection Agency (US EPA) oversaw the assessment and remediation of the
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incident. Impacted soil was subsequently excavated and transported to an off-site facility for
disposal. H&H made a request to the US EPA Freedom of Information Act (FOIA) for
documents concerning the release and remediation, but no documents were provided at the
issuance of this report. According to Mr. Ken Rhame with US EPA, soil impacts were removed
and the incident is considered closed by US EPA.

The methods and results of the limited soil assessment performed by H&H are provided below.

3.0 Soil Assessment

Prior to conducting soil assessment activities, H&H contacted North Carolina One-Call, the
public utility locator, to mark subsurface utilities located on the site. Additionally, all of the
borings were advanced utilizing hand auger methods.

3.1 Soil Sampling Methodology

On November 21, 2016, H&H advanced five soil borings at the site to evaluate the potential for
impacts associated with historical site operations. As noted previously, preliminary grading
plans indicate that there will be approximately 3 ft of cut soil in the northern, western, and central
portions of the site, approximately 6 ft of fill soil in the southeastern portion of the site, and 5 ft
of cut soil and 5 ft of fill soil in the eastern portion of the site. Therefore, soil borings were
advanced in the following locations:
• SB-1 was advanced in the western portion of the site in an area of expected cut soil of
approximately 1 ft.
• SB-2 was advanced in the northern portion of the site in an area of expected cut soil of
approximately 3 to 4 ft.
• SB-3 was advanced in the central portion of the site in an area of expected cut soil of
approximately 3 to 4 ft.
• SB-4 was advanced in the central portion of the site in an area of expected cut soil of
approximately 4 to 5 ft.
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• SB-5 was advanced in the eastern portion of the site in an area of expected cut soil of
approximately 5 ft.

Please note that no samples were collected from areas where fill soil is expected to be placed
such as in the far northern, southeastern, and some eastern portions of the site because soil in
those areas will be covered with soil cut from other areas.

At each soil boring location, a decontaminated stainless steel hand auger was used to advance the
borings to a depth of up to 6 ft below ground surface (bgs). The boring depth of 6 ft was
determined based upon the expected cut depths of approximately 3 to 5 ft bgs. During boring
advancement, soil was logged for lithological description and field screened for indications of
potential impacts by visual observation of staining and the presence of organic vapors using a
calibrated photoionization detector (PID). Based upon field screening results, one soil sample
was collected from each soil boring at the interval most likely to be impacted based on the field
screening results. Boring locations are presented on Figure 2 and boring logs are provided in
Appendix A.

Additionally, H&H advanced one background soil boring from an area on the site that does not
appear to have been impacted by historical operations to evaluate site-specific background
concentrations of naturally occurring metals in soil for comparison to those detected in the soil
boring samples. The background sample was collected from the western portion of the site west
of Linestowe Drive in an area that has historically been undeveloped. The background sample
location is depicted on Figure 2.

Following collection, the soil samples were placed into dedicated laboratory-supplied sample
containers and then packed in an iced cooler. The samples were delivered under chain-of-
custody protocol to SGS-Accutest Laboratory (SGS), a North Carolina-certified laboratory. The
soil samples were analyzed for volatile organic compounds (VOCs) by EPA Method 8260, semi-
VOCs (SVOCs) by EPA Method 8270, and hazardous substance list (HSL) metals plus
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hexavalent chromium by EPA Methods 6010/7471/7196. The background soil sample was
analyzed for HSL metals plus hexavalent chromium by EPA Methods 6010/7471/7196 only.

Upon completion, the boreholes were abandoned by backfilling the holes with soil and bentonite.

3.2 Soil Sampling Results

The soil analytical results are summarized in Table 1. The laboratory analytical report along with
chain-of-custody record is provided in Appendix B. Because future use of the site will be
residential, the soil analytical data were compared to the DEQ IHSB Residential Preliminary Soil
Remediation Goals (PSRGs). In addition, metals concentrations were compared to the site
background sample and regional background concentrations.

The results of the laboratory analysis indicate that soil sample SB-2, located in the northern
portion of the site, contained the SVOCs benzo(a)anthracene, benzo(a)pyrene,
benzo(b)fluoranthene, dibenzo(a,h)anthracene, and indeno(1,2,3-cd)pyrene at concentrations
above their respective DEQ IHSB Residential PSRGs. According to the Agency for Toxic
Substances and Disease Registry (ATSDR) PAH Toxicological Profile, PAHs occur ubiquitously
in soil and are associated with both synthetic and natural sources such as fossil fuels, cigarette
smoke, industrial processes, and exhaust emissions from gasoline engines, oil-fired heating, and
burnt coals. No other SVOCs were detected at concentrations exceeding PSRGs.

Low levels of the VOC acetone were detected in each soil sample except SB-2 at concentrations
above laboratory reporting limits, but below PSRGs. The low level acetone detections are most
likely attributable to a laboratory artifact, as acetone is a commonly used laboratory cleaning
solvent. No other VOCs were detected at concentrations exceeding laboratory reporting limits.

The results of the metals analysis indicate metals concentrations in the soil samples are consistent
with site-specific and/or regional background levels. Manganese was detected slightly above the
site-specific background concentration and the Residential PSRG in several soil samples;
however, the detected manganese concentrations are within the range of regional background
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levels. Manganese oxides are prevalent in soil and rock in the Piedmont, and their concentration
varies widely because they are often present in thin veins. Because only one background sample
was collected from the site, the concentrations are within typical background levels reported in
the literature, and based upon our extensive experience in the region, we conclude that the
manganese concentrations are naturally occurring.

3.3 Risk Calculation

As noted above, several PAHs were detected above Residential PSRGs. However, the PSRGs
are very conservative and are based upon a lifetime incremental cancer risk of 1 x 10-6 and a non-
carcinogenic hazard index of 0.2. Mitigation is usually not considered unless the LICR exceeds
the acceptable risk range of 1 x 10-4 to 1 x 10-6 and the HI exceeds 1. Therefore, to further
evaluate the detections in SB-2, H&H used the EPA Regional Screening Level calculator to
estimate cumulative risks for a residential land use scenario for compounds detected in SB-2
(including metals which appear to be naturally occurring).

The results of the cumulative risk calculation are provided in Appendix C and indicate that the
calculated LICR for compounds detected in SB-1 is 8 x 10-6 which is within the acceptable risk
range of 1 x 10-4 to 1 x 10-6. In addition, the calculated child HI is 0.06 and the adult HI is 0.007,
which are well below the acceptable level of 1. Based upon the cumulative risk calculations, the
compounds identified in soil in SB-2 do not pose a significant risk for future residential use.

4.0 Summary

On November 21, 2016, Hart & Hickman, PC (H&H) conducted limited soil assessment
activities at the former Belmont Dyers facility. The purpose of the soil sampling activities was to
evaluate if significant soil impacts may be encountered as part of future redevelopment activities
focusing in areas where soil is expected to be cut as part of future grading activities. The results
of our assessment are summarized below:

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• Analytical results indicate VOCs were not detected in soil at concentrations exceeding
PSRGs.

• Analytical results indicate several PAHs were detected above Residential PSRGs in soil
boring SB-2 located in the northern portion of the site. The source of the PAHs is not
known but may be associated with historical activities or “background” levels in urban
environments. Results of cumulative risk calculations indicate that the soil represented by
sample SB-2 does not pose a significant risk for future residential use.

• The results of the metals analysis indicate that metals concentrations in the soil samples
are consistent with site-specific and/or published regional background levels for North
Carolina soil.

• There is no indication that soil at the site is a hazardous waste that would preclude
movement of soil at the site during site redevelopment.

Table 1 (Page 1 of 1)
Summary of Soil Analytical Results
Former Belmont Dyers Facility
18 Linestowe Drive
Belmont, North Carolina
H&H Job No. RPH-001
S:\AAA-Master Projects\Ralph Falls (RPH)\Task 2 - Brownfields\Report\Soil Data Table
2/6/2017
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Sample ID Background-1 SB-1 SB-2 SB-3 SB-4 SB-5
Date 11/21/2016 11/21/2016 11/21/2016 11/21/2016 11/21/2016 11/21/2016
Depth (ft)Range Mean 2-4 0-2 1-3 1-3 3-5 2-4
VOCs (8260B) mg/kgAcetone 12,200 ----NA 0.0234 J <0.058 0.0152 J 0.0258 J 0.0162 J
SVOCs (8270D) mg/kg
Acenaphthylene NS ----NA <0.200 0.175 J <0.210 <0.200 <0.210
Anthracene 3,600 ----NA <0.200 0.209 <0.210 <0.200 <0.210
Benzo(a) anthracene 0.16 ----NA <0.200 0.61 <0.210 <0.200 <0.210
Benzo (a) pyrene 0.016 ----NA <0.200 0.622 <0.210 <0.200 <0.210
Benzo (b) fluoranthene 0.16 ----NA <0.200 0.567 <0.210 <0.200 <0.210
Benzo (g,h,i) perylene NS ----NA <0.200 0.493 <0.210 <0.200 <0.210
Benzo (k) fluoranthene 1.6 ----NA <0.200 0.587 <0.210 <0.200 <0.210
Chrysene 16 ----NA <0.200 0.629 <0.210 <0.200 <0.210
Dibenzo(a,h)anthracene 0.016 ----NA <0.200 0.111 J <0.210 <0.200 <0.210
Fluoranthene 480 ----NA <0.200 0.779 <0.210 <0.200 <0.210
Indeno(1,2,3-cd)pyrene 0.16 ----NA <0.200 0.534 <0.210 <0.200 <0.210
Phenanthrene NS ----NA <0.200 0.244 <0.210 <0.200 <0.210
Pyrene 360 ----NA <0.200 1.02 <0.210 <0.200 <0.210
Metals (6010C/7471B/7196A) mg/kg
Antimony 6.2 <1.0 - 8.8*0.76 <6.2 <5.8 <6.1 <5.8 <5.2 <6.1
Beryllium 32 ND - 2.0 0.11 <1.5 <1.5 <1.5 <1.5 <1.3 <1.5
Cadmium 14.2 1.0 - 10*4.3 <1.2 <1.2 <1.2 <1.2 <1.0 <1.2
Copper 620 3 - 100 34 65.0 82.4 80.0 83.0 53.7 59.0
Lead 400 ND - 50 16 <6.2 <5.8 <6.1 <5.8 <5.2 <6.1
Manganese 360 <2.0 - 7,000*640 111 624 265 241 527 171
Nickel 300 ND - 150 23 44.0 <12 <12 <12 26.9 <12
Selenium 78 <0.1 - 0.8 0.42 <6.2 <5.8 <6.1 <5.8 <5.2 <6.1
Silver 78 ND - 5.0 NS <3.1 <2.9 <3.1 <2.9 <2.6 <3.0
Zinc 4,600 25 - 124 56 30.2 69.7 35.0 42.7 87.5 50.5
Chromium (Total)NS 7.0 - 300 65 116 3.3 8.5 17.4 38.2 39.0
Hexavalent Chromium 0.3 NS NS <2.5 <2.3 <2.4 <2.5 <2.4 <2.5
Trivalent Chromium**24,000 NS NS 116 3.3 8.5 17.4 38.2 39.0
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB)
Preliminary Soil Remediation Goals (PSRGs) (April 2016)
2) Range and mean values of background metals for North Carolina soils taken from Elements in
North American Soils by Dragun and Chekiri, 2005
* = Range and mean values of background metals for Southeastern USA soils
** = Total Chromium - Hexavalent Chromium = Trivalent Chromium
Bold values exceed background levels for metals and Residential PSRGs
Soil concentrations are reported in milligrams per kilogram (mg/kg)
Laboratory analytical methods are shown in parentheses
NA = Not Analyzed; NS = Not Specified; -- = Not Applicable
VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds
J = estimated value between the laboratory detection limit and the laboratory reporting limit
Background Soil Borings
Residential
PSRGs (1)
(mg/kg)
Regional Background
Metals in Soil (2)
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CITY, STATE YEAR
TITLE
PROJECT
SITE LOCATION MAP
FORMER BELMONT DYERS
18 LINESTOWE DRIVEBELMONT, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
10-18-16 0
1RPH-001

Appendix A

Boring Logs
Organic TOPSOIL
Dry, very stiff, dull red, clayey SILT
Slightly moist, very stiff, dull red, clayey SILT with trace sand(slightly micaecous)
Bottom of borehole at 4.0 feet.
0.0
0.0
0.3
0.5
DRAWN BY:KJW
BORING COMPLETED:11/21/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / HA
SAMPLING METHOD:Auger Bucket Soil sampled collected from 2'-4' intervalfor laboratory analysis.
BORING STARTED:11/21/16
LOGGED BY:KJW
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
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MATERIAL DESCRIPTION
RE
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(
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SA
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NU
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(
p
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BORING DIAGRAM
BK
G
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SA
M
P
.
Sheet 1 of 1
BORING NUMBER Background
PROJECT:Former Belmont Dyers
JOB NUMBER:RPH-001
LOCATION:Belmont, NC
BO
R
I
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L
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-

H
A
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H
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D
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G
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J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
0
1
2
3
4
Slightly moist, medium, brown, sandy SILT
Slightly moist, medium, brown, sandy SILT (slightly micaecous)
Bottom of borehole at 6.0 feet.
0.0
0.0
0.0
0.1
0.1
0.1
DRAWN BY:KJW
BORING COMPLETED:11/21/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / HA
SAMPLING METHOD:Auger Bucket Soil sampled collected from 0'-2' intervalfor laboratory analysis.
BORING STARTED:11/21/16
LOGGED BY:KJW
TOTAL DEPTH: 6 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
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H
(f
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)
LI
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H
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MATERIAL DESCRIPTION
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(
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SA
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(
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BORING DIAGRAM
BK
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SA
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Sheet 1 of 1
BORING NUMBER SB-1
PROJECT:Former Belmont Dyers
JOB NUMBER:RPH-001
LOCATION:Belmont, NC
BO
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L
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
0.0
2.5
5.0
GRAVEL
Slightly moist, stiff, dull red orange, SILT
Moist, medium, tan red, SILT
Bottom of borehole at 6.0 feet.
0.0
0.0
0.0
0.1
0.1
0.1
DRAWN BY:KJW
BORING COMPLETED:11/21/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / HA
SAMPLING METHOD:Auger Bucket Soil sampled collected from 1'-3' intervalfor laboratory analysis.
BORING STARTED:11/21/16
LOGGED BY:KJW
TOTAL DEPTH: 6 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
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H
O
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MATERIAL DESCRIPTION
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(
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BORING DIAGRAM
BK
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Sheet 1 of 1
BORING NUMBER SB-2
PROJECT:Former Belmont Dyers
JOB NUMBER:RPH-001
LOCATION:Belmont, NC
BO
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H
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
0.0
2.5
5.0
GRAVEL
Slightly moist, stiff, dull red orange, clayey SILT
Moist, medium, red orange with black mottling, clayey SILT
Bottom of borehole at 6.0 feet.
0.0
0.0
0.0
0.2
0.1
0.1
DRAWN BY:KJW
BORING COMPLETED:11/21/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / HA
SAMPLING METHOD:Auger Bucket Soil sampled collected from 1'-3' intervalfor laboratory analysis.
BORING STARTED:11/21/16
LOGGED BY:KJW
TOTAL DEPTH: 6 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
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MATERIAL DESCRIPTION
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(
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SA
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(
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BORING DIAGRAM
BK
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SA
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Sheet 1 of 1
BORING NUMBER SB-3
PROJECT:Former Belmont Dyers
JOB NUMBER:RPH-001
LOCATION:Belmont, NC
BO
R
I
N
G

L
O
G

-

H
A
R
T

H
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C
K
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A
N
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G
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T

-

1
/
1
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1
7

0
8
:
2
3

-

S
:
\
B
B
B

M
A
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E
R

G
I
N
T

P
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E
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0
0
1

B
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O
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D
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E
R
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.
G
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
0.0
2.5
5.0
GRAVEL mixed with red orange, clayey silt
Slightly moist, very stiff, dull red orange, clayey SILT
Moist, medium, tan red with black mottling, sandy SILT
Bottom of borehole at 6.0 feet.
0.0
0.0
0.0
0.2
0.2
0.1
DRAWN BY:KJW
BORING COMPLETED:11/21/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / HA
SAMPLING METHOD:Auger Bucket Soil sampled collected from 3'-5' intervalfor laboratory analysis.
BORING STARTED:11/21/16
LOGGED BY:KJW
TOTAL DEPTH: 6 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
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E
NU
M
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A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-4
PROJECT:Former Belmont Dyers
JOB NUMBER:RPH-001
LOCATION:Belmont, NC
BO
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-

H
A
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-

1
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1
3
/
1
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0
8
:
2
3

-

S
:
\
B
B
B

M
A
S
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E
R

G
I
N
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P
R
O
J
E
C
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\
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H
-
0
0
1

B
E
L
O
M
N
T

D
Y
E
R
S
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
0.0
2.5
5.0
Organic TOPSOIL
Slightly moist, very stiff, dull red, clayey SILT (slightly micaecous)
Dry, very stiff, dull red, clayey SILT (slightly micaecous)
Slightly moist, stiff, dull red orange, SILT (slightly micaecous)
Bottom of borehole at 6.0 feet.
0.0
0.0
0.0
3.0
2.2
0.8
DRAWN BY:KJW
BORING COMPLETED:11/21/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / HA
SAMPLING METHOD:Auger Bucket Soil sampled collected from 2'-4' intervalfor laboratory analysis.
BORING STARTED:11/21/16
LOGGED BY:KJW
TOTAL DEPTH: 6 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-5
PROJECT:Former Belmont Dyers
JOB NUMBER:RPH-001
LOCATION:Belmont, NC
BO
R
I
N
G

L
O
G

-

H
A
R
T

H
I
C
K
M
A
N
.
G
D
T

-

1
/
1
3
/
1
7

0
8
:
2
3

-

S
:
\
B
B
B

M
A
S
T
E
R

G
I
N
T

P
R
O
J
E
C
T
S
\
R
P
H
-
0
0
1

B
E
L
O
M
N
T

D
Y
E
R
S
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
0.0
2.5
5.0

Appendix B

Laboratory Analytical Report
12/02/16
Technical Report for
Hart & Hickman
Belmont Dyers Site; Belmont, NC
RPH-001.2
SGS Accutest Job Number: FA38946
Sampling Date: 11/21/16
Report to:
Hart & Hickman
2923 S Tryon St Suite 100
Charlotte, NC 28203
[e-mail]; [e-mail]
ATTN: Brett Lawrence
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(L-A-B L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast 12/02/16
e-Hardcopy 2.0
Automated Report
79
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
1 of 79
FA38946
Table of Contents
-1-
Sections:
Section 1: Sample Summary ................................................................................................... 3
Section 2: Summary of Hits .................................................................................................... 4
Section 3: Sample Results ........................................................................................................6
3.1: FA38946-1: BACKGROUND (2-4') ............................................................................ 7
3.2: FA38946-2: SB-1 (0-2') ................................................................................................ 9
3.3: FA38946-3: SB-2 (1-3') ................................................................................................ 15
3.4: FA38946-4: SB-3 (1-3') ................................................................................................ 21
3.5: FA38946-5: SB-4 (3-5') ................................................................................................ 27
3.6: FA38946-6: SB-5 (2-4') ................................................................................................ 33
Section 4: Misc. Forms ............................................................................................................39
4.1: Chain of Custody ........................................................................................................... 40
Section 5: GC/MS Volatiles - QC Data Summaries .............................................................. 43
5.1: Method Blank Summary ................................................................................................ 44
5.2: Blank Spike Summary ................................................................................................... 50
5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 56
Section 6: GC/MS Semi-volatiles - QC Data Summaries ..................................................... 62
6.1: Method Blank Summary ................................................................................................ 63
6.2: Blank Spike Summary ................................................................................................... 65
6.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 67
Section 7: Metals Analysis - QC Data Summaries ................................................................ 69
7.1: Prep QC MP31219: Sb,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Zn ............................................ 70
Section 8: General Chemistry - QC Data Summaries .......................................................... 76
8.1: Method Blank and Spike Results Summary .................................................................. 77
8.2: Duplicate Results Summary .......................................................................................... 78
8.3: Matrix Spike Results Summary ..................................................................................... 79
1
2
3
4
5
6
7
8
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SGS Accutest
Sample Summary
Hart & Hickman
Job No:FA38946
Belmont Dyers Site; Belmont, NC
Project No: RPH-001.2
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA38946-1 11/21/16 10:00 KW 11/22/16 SO Soil BACKGROUND (2-4')
FA38946-2 11/21/16 12:15 KW 11/22/16 SO Soil SB-1 (0-2')
FA38946-3 11/21/16 12:25 KW 11/22/16 SO Soil SB-2 (1-3')
FA38946-4 11/21/16 12:35 KW 11/22/16 SO Soil SB-3 (1-3')
FA38946-5 11/21/16 13:35 KW 11/22/16 SO Soil SB-4 (3-5')
FA38946-6 11/21/16 14:35 KW 11/22/16 SO Soil SB-5 (2-4')
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 79
FA38946
1
Summary of Hits Page 1 of 2
Job Number:FA38946
Account:Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Collected:11/21/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA38946-1 BACKGROUND (2-4')
Chromium a 116 3.1 mg/kg SW846 6010C
Copper a 65.0 7.7 mg/kg SW846 6010C
Manganese a 111 4.6 mg/kg SW846 6010C
Nickel a 44.0 12 mg/kg SW846 6010C
Zinc a 30.2 6.2 mg/kg SW846 6010C
FA38946-2 SB-1 (0-2')
Acetone 23.4 J 55 11 ug/kg SW846 8260B
Chromium a 3.3 2.9 mg/kg SW846 6010C
Copper a 82.4 7.3 mg/kg SW846 6010C
Manganese a 624 4.4 mg/kg SW846 6010C
Zinc a 69.7 5.8 mg/kg SW846 6010C
FA38946-3 SB-2 (1-3')
Acenaphthylene 175 J 200 26 ug/kg SW846 8270D
Anthracene 209 200 30 ug/kg SW846 8270D
Benzo(a)anthracene 610 200 24 ug/kg SW846 8270D
Benzo(a)pyrene 622 200 22 ug/kg SW846 8270D
Benzo(b)fluoranthene 567 200 26 ug/kg SW846 8270D
Benzo(g,h,i)perylene 493 200 20 ug/kg SW846 8270D
Benzo(k)fluoranthene 587 200 29 ug/kg SW846 8270D
Chrysene 629 200 28 ug/kg SW846 8270D
Dibenzo(a,h)anthracene 111 J 200 22 ug/kg SW846 8270D
Fluoranthene 779 200 25 ug/kg SW846 8270D
Indeno(1,2,3-cd)pyrene 534 200 31 ug/kg SW846 8270D
Phenanthrene 244 200 25 ug/kg SW846 8270D
Pyrene 1020 200 38 ug/kg SW846 8270D
Chromium a 8.5 3.1 mg/kg SW846 6010C
Copper a 80.0 7.7 mg/kg SW846 6010C
Manganese a 265 4.6 mg/kg SW846 6010C
Zinc a 35.0 6.1 mg/kg SW846 6010C
FA38946-4 SB-3 (1-3')
Acetone 15.2 J 54 11 ug/kg SW846 8260B
Chromium a 17.4 2.9 mg/kg SW846 6010C
Copper a 83.0 7.3 mg/kg SW846 6010C
Manganese a 241 4.4 mg/kg SW846 6010C
Zinc a 42.7 5.8 mg/kg SW846 6010C
4 of 79
FA38946
2
Summary of Hits Page 2 of 2
Job Number:FA38946
Account:Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Collected:11/21/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA38946-5 SB-4 (3-5')
Acetone 25.8 J 54 11 ug/kg SW846 8260B
Chromium a 38.2 2.6 mg/kg SW846 6010C
Copper a 53.7 6.6 mg/kg SW846 6010C
Manganese a 527 3.9 mg/kg SW846 6010C
Nickel a 26.9 10 mg/kg SW846 6010C
Zinc a 87.5 5.2 mg/kg SW846 6010C
FA38946-6 SB-5 (2-4')
Acetone 16.2 J 64 13 ug/kg SW846 8260B
Chromium a 39.0 3.0 mg/kg SW846 6010C
Copper a 59.0 7.6 mg/kg SW846 6010C
Manganese a 171 4.6 mg/kg SW846 6010C
Zinc a 50.5 6.1 mg/kg SW846 6010C
(a) Sample dilution required due to difficult matrix.
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2
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
6 of 79
FA38946
3
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:BACKGROUND (2-4')
Lab Sample ID:FA38946-1 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:77.7
Project:Belmont Dyers Site; Belmont, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <6.2 6.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Beryllium a <1.5 1.5 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Cadmium a <1.2 1.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Chromium a 116 3.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Copper a 65.0 7.7 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Lead a <6.2 6.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Manganese a 111 4.6 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Nickel a 44.0 12 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Selenium a <6.2 6.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Silver a <3.1 3.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Zinc a 30.2 6.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA13602
(2) Prep QC Batch: MP31219
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
7 of 79
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3
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1
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:BACKGROUND (2-4')
Lab Sample ID:FA38946-1 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:77.7
Project:Belmont Dyers Site; Belmont, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.5 2.5 mg/kg 1 12/01/16 12:47 FN SW846 3060A/7196A
Solids, Percent 77.7 % 1 11/23/16 11:28 VK SM19 2540G
RL = Reporting Limit
8 of 79
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3
3
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1
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:SB-1 (0-2')
Lab Sample ID:FA38946-2 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:85.5
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0080954.D 1 11/22/16 EP n/a n/a VF2783
Run #2
Initial Weight Final Volume
Run #1 5.36 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone 23.4 55 11 ug/kg J
71-43-2 Benzene ND 5.5 1.4 ug/kg
108-86-1 Bromobenzene ND 5.5 1.3 ug/kg
74-97-5 Bromochloromethane ND 5.5 1.2 ug/kg
75-27-4 Bromodichloromethane ND 5.5 1.1 ug/kg
75-25-2 Bromoform ND 5.5 1.1 ug/kg
78-93-3 2-Butanone (MEK)ND 27 9.9 ug/kg
104-51-8 n-Butylbenzene ND 5.5 1.1 ug/kg
135-98-8 sec-Butylbenzene ND 5.5 1.1 ug/kg
98-06-6 tert-Butylbenzene ND 5.5 1.1 ug/kg
56-23-5 Carbon Tetrachloride ND 5.5 1.9 ug/kg
108-90-7 Chlorobenzene ND 5.5 1.1 ug/kg
75-00-3 Chloroethane ND 5.5 2.2 ug/kg
67-66-3 Chloroform ND 5.5 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.5 1.1 ug/kg
106-43-4 p-Chlorotoluene ND 5.5 1.1 ug/kg
124-48-1 Dibromochloromethane ND 5.5 1.1 ug/kg
106-93-4 1,2-Dibromoethane ND 5.5 1.1 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.5 2.7 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.5 1.1 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.5 1.1 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.5 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.5 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.5 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.5 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.5 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.5 1.7 ug/kg
78-87-5 1,2-Dichloropropane ND 5.5 1.7 ug/kg
142-28-9 1,3-Dichloropropane ND 5.5 1.1 ug/kg
594-20-7 2,2-Dichloropropane ND 5.5 1.1 ug/kg
563-58-6 1,1-Dichloropropene ND 5.5 1.4 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.5 2.1 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 79
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SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:SB-1 (0-2')
Lab Sample ID:FA38946-2 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:85.5
Project:Belmont Dyers Site; Belmont, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.5 1.1 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.5 1.3 ug/kg
64-17-5 Ethyl Alcohol ND 440 91 ug/kg
100-41-4 Ethylbenzene ND 5.5 1.2 ug/kg
591-78-6 2-Hexanone ND 27 9.5 ug/kg
98-82-8 Isopropylbenzene ND 5.5 1.5 ug/kg
99-87-6 p-Isopropyltoluene ND 5.5 1.1 ug/kg
74-83-9 Methyl Bromide ND 5.5 2.8 ug/kg
74-87-3 Methyl Chloride ND 5.5 2.6 ug/kg
75-09-2 Methylene Chloride ND 11 4.4 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 27 12 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.5 1.2 ug/kg
91-20-3 Naphthalene ND 5.5 2.2 ug/kg
103-65-1 n-Propylbenzene ND 5.5 1.4 ug/kg
100-42-5 Styrene ND 5.5 1.1 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.5 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.5 2.4 ug/kg
127-18-4 Tetrachloroethylene ND 5.5 1.4 ug/kg
108-88-3 Toluene ND 5.5 1.2 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.5 2.2 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.5 1.6 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.5 1.1 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.5 2.0 ug/kg
79-01-6 Trichloroethylene ND 5.5 1.3 ug/kg
75-69-4 Trichlorofluoromethane ND 5.5 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.5 1.8 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.5 1.1 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.5 1.1 ug/kg
108-05-4 Vinyl Acetate ND 27 10 ug/kg
75-01-4 Vinyl Chloride ND 5.5 1.8 ug/kg
m,p-Xylene ND 11 1.9 ug/kg
95-47-6 o-Xylene ND 5.5 1.2 ug/kg
1330-20-7 Xylene (total)ND 16 3.1 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 121%75-124%
17060-07-0 1,2-Dichloroethane-D4 125%72-135%
2037-26-5 Toluene-D8 92%75-126%
460-00-4 4-Bromofluorobenzene 94%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 79
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SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:SB-1 (0-2')
Lab Sample ID:FA38946-2 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:85.5
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 4D73.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
Run #2
Initial Weight Final Volume
Run #1 29.6 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 990 200 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 200 30 ug/kg
95-57-8 2-Chlorophenol ND 200 25 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 28 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 24 ug/kg
51-28-5 2,4-Dinitrophenol ND 990 200 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 400 79 ug/kg
95-48-7 2-Methylphenol ND 200 21 ug/kg
3&4-Methylphenol ND 200 47 ug/kg
88-75-5 2-Nitrophenol ND 200 24 ug/kg
100-02-7 4-Nitrophenol ND 990 160 ug/kg
87-86-5 Pentachlorophenol ND 990 160 ug/kg
108-95-2 Phenol ND 200 23 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 24 ug/kg
83-32-9 Acenaphthene ND 200 25 ug/kg
208-96-8 Acenaphthylene ND 200 25 ug/kg
120-12-7 Anthracene ND 200 29 ug/kg
56-55-3 Benzo(a)anthracene ND 200 23 ug/kg
50-32-8 Benzo(a)pyrene ND 200 21 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 25 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 28 ug/kg
100-51-6 Benzyl Alcohol ND 200 26 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 23 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 40 ug/kg
106-47-8 4-Chloroaniline ND 200 28 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 200 30 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 35 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 200 29 ug/kg
91-58-7 2-Chloronaphthalene ND 200 27 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 25 ug/kg
218-01-9 Chrysene ND 200 27 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-1 (0-2')
Lab Sample ID:FA38946-2 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:85.5
Project:Belmont Dyers Site; Belmont, NC
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 200 21 ug/kg
132-64-9 Dibenzofuran ND 200 25 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 20 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 22 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 24 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 200 22 ug/kg
84-66-2 Diethyl Phthalate ND 400 40 ug/kg
131-11-3 Dimethyl Phthalate ND 200 40 ug/kg
117-84-0 Di-n-octyl Phthalate ND 200 40 ug/kg
84-74-2 Di-n-butyl Phthalate ND 400 79 ug/kg
122-66-7 1,2-Diphenylhydrazine ND 200 33 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 400 40 ug/kg
206-44-0 Fluoranthene ND 200 24 ug/kg
86-73-7 Fluorene ND 200 25 ug/kg
118-74-1 Hexachlorobenzene ND 200 24 ug/kg
87-68-3 Hexachlorobutadiene ND 200 22 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 40 ug/kg
67-72-1 Hexachloroethane ND 200 23 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 30 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
90-12-0 1-Methylnaphthalene ND 200 31 ug/kg
91-57-6 2-Methylnaphthalene ND 200 22 ug/kg
91-20-3 Naphthalene ND 200 30 ug/kg
98-95-3 Nitrobenzene ND 200 26 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 200 21 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 38 ug/kg
85-01-8 Phenanthrene ND 200 24 ug/kg
129-00-0 Pyrene ND 200 37 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 24 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 65%40-102%
4165-62-2 Phenol-d5 71%41-100%
118-79-6 2,4,6-Tribromophenol 72%42-108%
4165-60-0 Nitrobenzene-d5 63%40-105%
321-60-8 2-Fluorobiphenyl 66%43-107%
1718-51-0 Terphenyl-d14 80%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-1 (0-2')
Lab Sample ID:FA38946-2 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:85.5
Project:Belmont Dyers Site; Belmont, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.8 5.8 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Beryllium a <1.5 1.5 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Cadmium a <1.2 1.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Chromium a 3.3 2.9 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Copper a 82.4 7.3 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Lead a <5.8 5.8 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Manganese a 624 4.4 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Nickel a <12 12 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Selenium a <5.8 5.8 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Silver a <2.9 2.9 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Zinc a 69.7 5.8 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA13602
(2) Prep QC Batch: MP31219
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
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Client Sample ID:SB-1 (0-2')
Lab Sample ID:FA38946-2 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:85.5
Project:Belmont Dyers Site; Belmont, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.3 2.3 mg/kg 1 12/01/16 12:47 FN SW846 3060A/7196A
Solids, Percent 85.5 % 1 11/23/16 11:28 VK SM19 2540G
RL = Reporting Limit
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Client Sample ID:SB-2 (1-3')
Lab Sample ID:FA38946-3 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:81.5
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0080955.D 1 11/22/16 EP n/a n/a VF2783
Run #2
Initial Weight Final Volume
Run #1 5.26 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 58 12 ug/kg
71-43-2 Benzene ND 5.8 1.5 ug/kg
108-86-1 Bromobenzene ND 5.8 1.4 ug/kg
74-97-5 Bromochloromethane ND 5.8 1.3 ug/kg
75-27-4 Bromodichloromethane ND 5.8 1.2 ug/kg
75-25-2 Bromoform ND 5.8 1.2 ug/kg
78-93-3 2-Butanone (MEK)ND 29 11 ug/kg
104-51-8 n-Butylbenzene ND 5.8 1.2 ug/kg
135-98-8 sec-Butylbenzene ND 5.8 1.2 ug/kg
98-06-6 tert-Butylbenzene ND 5.8 1.2 ug/kg
56-23-5 Carbon Tetrachloride ND 5.8 2.1 ug/kg
108-90-7 Chlorobenzene ND 5.8 1.2 ug/kg
75-00-3 Chloroethane ND 5.8 2.3 ug/kg
67-66-3 Chloroform ND 5.8 1.4 ug/kg
95-49-8 o-Chlorotoluene ND 5.8 1.2 ug/kg
106-43-4 p-Chlorotoluene ND 5.8 1.2 ug/kg
124-48-1 Dibromochloromethane ND 5.8 1.2 ug/kg
106-93-4 1,2-Dibromoethane ND 5.8 1.2 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.8 2.9 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.8 1.2 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.8 1.2 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.8 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.8 2.0 ug/kg
107-06-2 1,2-Dichloroethane ND 5.8 1.2 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.8 1.2 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.8 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.8 1.8 ug/kg
78-87-5 1,2-Dichloropropane ND 5.8 1.9 ug/kg
142-28-9 1,3-Dichloropropane ND 5.8 1.2 ug/kg
594-20-7 2,2-Dichloropropane ND 5.8 1.2 ug/kg
563-58-6 1,1-Dichloropropene ND 5.8 1.5 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.8 2.2 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-2 (1-3')
Lab Sample ID:FA38946-3 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:81.5
Project:Belmont Dyers Site; Belmont, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.8 1.2 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.8 1.4 ug/kg
64-17-5 Ethyl Alcohol ND 470 98 ug/kg
100-41-4 Ethylbenzene ND 5.8 1.3 ug/kg
591-78-6 2-Hexanone ND 29 10 ug/kg
98-82-8 Isopropylbenzene ND 5.8 1.6 ug/kg
99-87-6 p-Isopropyltoluene ND 5.8 1.2 ug/kg
74-83-9 Methyl Bromide ND 5.8 3.0 ug/kg
74-87-3 Methyl Chloride ND 5.8 2.8 ug/kg
75-09-2 Methylene Chloride ND 12 4.7 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 29 12 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.8 1.3 ug/kg
91-20-3 Naphthalene ND 5.8 2.3 ug/kg
103-65-1 n-Propylbenzene ND 5.8 1.4 ug/kg
100-42-5 Styrene ND 5.8 1.2 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.8 1.3 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.8 2.6 ug/kg
127-18-4 Tetrachloroethylene ND 5.8 1.5 ug/kg
108-88-3 Toluene ND 5.8 1.3 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.8 2.3 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.8 1.7 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.8 1.2 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.8 2.1 ug/kg
79-01-6 Trichloroethylene ND 5.8 1.4 ug/kg
75-69-4 Trichlorofluoromethane ND 5.8 2.2 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.8 1.9 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.8 1.2 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.8 1.2 ug/kg
108-05-4 Vinyl Acetate ND 29 11 ug/kg
75-01-4 Vinyl Chloride ND 5.8 1.9 ug/kg
m,p-Xylene ND 12 2.0 ug/kg
95-47-6 o-Xylene ND 5.8 1.3 ug/kg
1330-20-7 Xylene (total)ND 17 3.3 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%75-124%
17060-07-0 1,2-Dichloroethane-D4 124%72-135%
2037-26-5 Toluene-D8 92%75-126%
460-00-4 4-Bromofluorobenzene 95%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-2 (1-3')
Lab Sample ID:FA38946-3 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:81.5
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 4D74.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 200 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 200 31 ug/kg
95-57-8 2-Chlorophenol ND 200 26 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 29 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 25 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 200 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 410 82 ug/kg
95-48-7 2-Methylphenol ND 200 22 ug/kg
3&4-Methylphenol ND 200 48 ug/kg
88-75-5 2-Nitrophenol ND 200 25 ug/kg
100-02-7 4-Nitrophenol ND 1000 160 ug/kg
87-86-5 Pentachlorophenol ND 1000 160 ug/kg
108-95-2 Phenol ND 200 24 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 25 ug/kg
83-32-9 Acenaphthene ND 200 26 ug/kg
208-96-8 Acenaphthylene 175 200 26 ug/kg J
120-12-7 Anthracene 209 200 30 ug/kg
56-55-3 Benzo(a)anthracene 610 200 24 ug/kg
50-32-8 Benzo(a)pyrene 622 200 22 ug/kg
205-99-2 Benzo(b)fluoranthene 567 200 26 ug/kg
191-24-2 Benzo(g,h,i)perylene 493 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene 587 200 29 ug/kg
100-51-6 Benzyl Alcohol ND 200 27 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 24 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 41 ug/kg
106-47-8 4-Chloroaniline ND 200 29 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 200 31 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 37 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 200 30 ug/kg
91-58-7 2-Chloronaphthalene ND 200 28 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 26 ug/kg
218-01-9 Chrysene 629 200 28 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-2 (1-3')
Lab Sample ID:FA38946-3 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:81.5
Project:Belmont Dyers Site; Belmont, NC
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene 111 200 22 ug/kg J
132-64-9 Dibenzofuran ND 200 26 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 20 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 23 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 25 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 200 23 ug/kg
84-66-2 Diethyl Phthalate ND 410 41 ug/kg
131-11-3 Dimethyl Phthalate ND 200 41 ug/kg
117-84-0 Di-n-octyl Phthalate ND 200 41 ug/kg
84-74-2 Di-n-butyl Phthalate ND 410 82 ug/kg
122-66-7 1,2-Diphenylhydrazine ND 200 34 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 410 41 ug/kg
206-44-0 Fluoranthene 779 200 25 ug/kg
86-73-7 Fluorene ND 200 26 ug/kg
118-74-1 Hexachlorobenzene ND 200 25 ug/kg
87-68-3 Hexachlorobutadiene ND 200 23 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 41 ug/kg
67-72-1 Hexachloroethane ND 200 24 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene 534 200 31 ug/kg
78-59-1 Isophorone ND 200 21 ug/kg
90-12-0 1-Methylnaphthalene ND 200 32 ug/kg
91-57-6 2-Methylnaphthalene ND 200 23 ug/kg
91-20-3 Naphthalene ND 200 31 ug/kg
98-95-3 Nitrobenzene ND 200 27 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 200 22 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 39 ug/kg
85-01-8 Phenanthrene 244 200 25 ug/kg
129-00-0 Pyrene 1020 200 38 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 25 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 68%40-102%
4165-62-2 Phenol-d5 72%41-100%
118-79-6 2,4,6-Tribromophenol 76%42-108%
4165-60-0 Nitrobenzene-d5 67%40-105%
321-60-8 2-Fluorobiphenyl 72%43-107%
1718-51-0 Terphenyl-d14 76%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-2 (1-3')
Lab Sample ID:FA38946-3 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:81.5
Project:Belmont Dyers Site; Belmont, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <6.1 6.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Beryllium a <1.5 1.5 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Cadmium a <1.2 1.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Chromium a 8.5 3.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Copper a 80.0 7.7 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Lead a <6.1 6.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Manganese a 265 4.6 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Nickel a <12 12 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Selenium a <6.1 6.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Silver a <3.1 3.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Zinc a 35.0 6.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA13602
(2) Prep QC Batch: MP31219
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
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Lab Sample ID:FA38946-3 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:81.5
Project:Belmont Dyers Site; Belmont, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.4 2.4 mg/kg 1 12/01/16 12:47 FN SW846 3060A/7196A
Solids, Percent 81.5 % 1 11/23/16 11:28 VK SM19 2540G
RL = Reporting Limit
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Client Sample ID:SB-3 (1-3')
Lab Sample ID:FA38946-4 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:79.8
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0080956.D 1 11/22/16 EP n/a n/a VF2783
Run #2
Initial Weight Final Volume
Run #1 5.82 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone 15.2 54 11 ug/kg J
71-43-2 Benzene ND 5.4 1.4 ug/kg
108-86-1 Bromobenzene ND 5.4 1.3 ug/kg
74-97-5 Bromochloromethane ND 5.4 1.2 ug/kg
75-27-4 Bromodichloromethane ND 5.4 1.1 ug/kg
75-25-2 Bromoform ND 5.4 1.1 ug/kg
78-93-3 2-Butanone (MEK)ND 27 9.8 ug/kg
104-51-8 n-Butylbenzene ND 5.4 1.1 ug/kg
135-98-8 sec-Butylbenzene ND 5.4 1.1 ug/kg
98-06-6 tert-Butylbenzene ND 5.4 1.1 ug/kg
56-23-5 Carbon Tetrachloride ND 5.4 1.9 ug/kg
108-90-7 Chlorobenzene ND 5.4 1.1 ug/kg
75-00-3 Chloroethane ND 5.4 2.2 ug/kg
67-66-3 Chloroform ND 5.4 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.4 1.1 ug/kg
106-43-4 p-Chlorotoluene ND 5.4 1.1 ug/kg
124-48-1 Dibromochloromethane ND 5.4 1.1 ug/kg
106-93-4 1,2-Dibromoethane ND 5.4 1.1 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.4 2.7 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.4 1.1 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.4 1.1 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.4 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.4 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.4 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.4 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.4 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.4 1.6 ug/kg
78-87-5 1,2-Dichloropropane ND 5.4 1.7 ug/kg
142-28-9 1,3-Dichloropropane ND 5.4 1.1 ug/kg
594-20-7 2,2-Dichloropropane ND 5.4 1.1 ug/kg
563-58-6 1,1-Dichloropropene ND 5.4 1.4 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.4 2.0 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-3 (1-3')
Lab Sample ID:FA38946-4 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:79.8
Project:Belmont Dyers Site; Belmont, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.4 1.1 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.4 1.3 ug/kg
64-17-5 Ethyl Alcohol ND 430 90 ug/kg
100-41-4 Ethylbenzene ND 5.4 1.2 ug/kg
591-78-6 2-Hexanone ND 27 9.4 ug/kg
98-82-8 Isopropylbenzene ND 5.4 1.5 ug/kg
99-87-6 p-Isopropyltoluene ND 5.4 1.1 ug/kg
74-83-9 Methyl Bromide ND 5.4 2.8 ug/kg
74-87-3 Methyl Chloride ND 5.4 2.6 ug/kg
75-09-2 Methylene Chloride ND 11 4.3 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 27 12 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.4 1.2 ug/kg
91-20-3 Naphthalene ND 5.4 2.2 ug/kg
103-65-1 n-Propylbenzene ND 5.4 1.3 ug/kg
100-42-5 Styrene ND 5.4 1.1 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.4 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.4 2.4 ug/kg
127-18-4 Tetrachloroethylene ND 5.4 1.4 ug/kg
108-88-3 Toluene ND 5.4 1.2 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.4 2.1 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.4 1.6 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.4 1.1 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.4 1.9 ug/kg
79-01-6 Trichloroethylene ND 5.4 1.3 ug/kg
75-69-4 Trichlorofluoromethane ND 5.4 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.4 1.8 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.4 1.1 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.4 1.1 ug/kg
108-05-4 Vinyl Acetate ND 27 10 ug/kg
75-01-4 Vinyl Chloride ND 5.4 1.8 ug/kg
m,p-Xylene ND 11 1.9 ug/kg
95-47-6 o-Xylene ND 5.4 1.2 ug/kg
1330-20-7 Xylene (total)ND 16 3.1 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%75-124%
17060-07-0 1,2-Dichloroethane-D4 124%72-135%
2037-26-5 Toluene-D8 91%75-126%
460-00-4 4-Bromofluorobenzene 95%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-3 (1-3')
Lab Sample ID:FA38946-4 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:79.8
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 4D75.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 210 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 210 31 ug/kg
95-57-8 2-Chlorophenol ND 210 26 ug/kg
120-83-2 2,4-Dichlorophenol ND 210 29 ug/kg
105-67-9 2,4-Dimethylphenol ND 210 25 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 210 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 410 82 ug/kg
95-48-7 2-Methylphenol ND 210 22 ug/kg
3&4-Methylphenol ND 210 49 ug/kg
88-75-5 2-Nitrophenol ND 210 26 ug/kg
100-02-7 4-Nitrophenol ND 1000 160 ug/kg
87-86-5 Pentachlorophenol ND 1000 160 ug/kg
108-95-2 Phenol ND 210 24 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 210 25 ug/kg
83-32-9 Acenaphthene ND 210 27 ug/kg
208-96-8 Acenaphthylene ND 210 26 ug/kg
120-12-7 Anthracene ND 210 30 ug/kg
56-55-3 Benzo(a)anthracene ND 210 24 ug/kg
50-32-8 Benzo(a)pyrene ND 210 22 ug/kg
205-99-2 Benzo(b)fluoranthene ND 210 26 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 210 21 ug/kg
207-08-9 Benzo(k)fluoranthene ND 210 29 ug/kg
100-51-6 Benzyl Alcohol ND 210 27 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 210 24 ug/kg
85-68-7 Butyl benzyl phthalate ND 210 41 ug/kg
106-47-8 4-Chloroaniline ND 210 29 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 210 31 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 210 37 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 210 30 ug/kg
91-58-7 2-Chloronaphthalene ND 210 28 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 210 26 ug/kg
218-01-9 Chrysene ND 210 28 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-3 (1-3')
Lab Sample ID:FA38946-4 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:79.8
Project:Belmont Dyers Site; Belmont, NC
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 210 22 ug/kg
132-64-9 Dibenzofuran ND 210 26 ug/kg
95-50-1 1,2-Dichlorobenzene ND 210 21 ug/kg
541-73-1 1,3-Dichlorobenzene ND 210 23 ug/kg
106-46-7 1,4-Dichlorobenzene ND 210 25 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 210 23 ug/kg
84-66-2 Diethyl Phthalate ND 410 41 ug/kg
131-11-3 Dimethyl Phthalate ND 210 41 ug/kg
117-84-0 Di-n-octyl Phthalate ND 210 41 ug/kg
84-74-2 Di-n-butyl Phthalate ND 410 82 ug/kg
122-66-7 1,2-Diphenylhydrazine ND 210 34 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 410 41 ug/kg
206-44-0 Fluoranthene ND 210 25 ug/kg
86-73-7 Fluorene ND 210 26 ug/kg
118-74-1 Hexachlorobenzene ND 210 25 ug/kg
87-68-3 Hexachlorobutadiene ND 210 23 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 210 41 ug/kg
67-72-1 Hexachloroethane ND 210 24 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 210 32 ug/kg
78-59-1 Isophorone ND 210 21 ug/kg
90-12-0 1-Methylnaphthalene ND 210 32 ug/kg
91-57-6 2-Methylnaphthalene ND 210 23 ug/kg
91-20-3 Naphthalene ND 210 31 ug/kg
98-95-3 Nitrobenzene ND 210 27 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 210 22 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 210 39 ug/kg
85-01-8 Phenanthrene ND 210 25 ug/kg
129-00-0 Pyrene ND 210 39 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 210 25 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 67%40-102%
4165-62-2 Phenol-d5 72%41-100%
118-79-6 2,4,6-Tribromophenol 74%42-108%
4165-60-0 Nitrobenzene-d5 65%40-105%
321-60-8 2-Fluorobiphenyl 69%43-107%
1718-51-0 Terphenyl-d14 76%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-3 (1-3')
Lab Sample ID:FA38946-4 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:79.8
Project:Belmont Dyers Site; Belmont, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.8 5.8 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Beryllium a <1.5 1.5 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Cadmium a <1.2 1.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Chromium a 17.4 2.9 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Copper a 83.0 7.3 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Lead a <5.8 5.8 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Manganese a 241 4.4 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Nickel a <12 12 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Selenium a <5.8 5.8 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Silver a <2.9 2.9 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Zinc a 42.7 5.8 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA13602
(2) Prep QC Batch: MP31219
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
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Client Sample ID:SB-3 (1-3')
Lab Sample ID:FA38946-4 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:79.8
Project:Belmont Dyers Site; Belmont, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.5 2.5 mg/kg 1 12/01/16 12:47 FN SW846 3060A/7196A
Solids, Percent 79.8 % 1 11/23/16 11:28 VK SM19 2540G
RL = Reporting Limit
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Client Sample ID:SB-4 (3-5')
Lab Sample ID:FA38946-5 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:83.7
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0080957.D 1 11/22/16 EP n/a n/a VF2783
Run #2
Initial Weight Final Volume
Run #1 5.53 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone 25.8 54 11 ug/kg J
71-43-2 Benzene ND 5.4 1.4 ug/kg
108-86-1 Bromobenzene ND 5.4 1.3 ug/kg
74-97-5 Bromochloromethane ND 5.4 1.2 ug/kg
75-27-4 Bromodichloromethane ND 5.4 1.1 ug/kg
75-25-2 Bromoform ND 5.4 1.1 ug/kg
78-93-3 2-Butanone (MEK)ND 27 9.8 ug/kg
104-51-8 n-Butylbenzene ND 5.4 1.1 ug/kg
135-98-8 sec-Butylbenzene ND 5.4 1.1 ug/kg
98-06-6 tert-Butylbenzene ND 5.4 1.1 ug/kg
56-23-5 Carbon Tetrachloride ND 5.4 1.9 ug/kg
108-90-7 Chlorobenzene ND 5.4 1.1 ug/kg
75-00-3 Chloroethane ND 5.4 2.2 ug/kg
67-66-3 Chloroform ND 5.4 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.4 1.1 ug/kg
106-43-4 p-Chlorotoluene ND 5.4 1.1 ug/kg
124-48-1 Dibromochloromethane ND 5.4 1.1 ug/kg
106-93-4 1,2-Dibromoethane ND 5.4 1.1 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.4 2.7 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.4 1.1 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.4 1.1 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.4 1.1 ug/kg
75-34-3 1,1-Dichloroethane ND 5.4 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.4 1.1 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.4 1.1 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.4 1.3 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.4 1.6 ug/kg
78-87-5 1,2-Dichloropropane ND 5.4 1.7 ug/kg
142-28-9 1,3-Dichloropropane ND 5.4 1.1 ug/kg
594-20-7 2,2-Dichloropropane ND 5.4 1.1 ug/kg
563-58-6 1,1-Dichloropropene ND 5.4 1.4 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.4 2.1 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-4 (3-5')
Lab Sample ID:FA38946-5 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:83.7
Project:Belmont Dyers Site; Belmont, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.4 1.1 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.4 1.3 ug/kg
64-17-5 Ethyl Alcohol ND 430 91 ug/kg
100-41-4 Ethylbenzene ND 5.4 1.2 ug/kg
591-78-6 2-Hexanone ND 27 9.4 ug/kg
98-82-8 Isopropylbenzene ND 5.4 1.5 ug/kg
99-87-6 p-Isopropyltoluene ND 5.4 1.1 ug/kg
74-83-9 Methyl Bromide ND 5.4 2.8 ug/kg
74-87-3 Methyl Chloride ND 5.4 2.6 ug/kg
75-09-2 Methylene Chloride ND 11 4.3 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 27 12 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.4 1.2 ug/kg
91-20-3 Naphthalene ND 5.4 2.2 ug/kg
103-65-1 n-Propylbenzene ND 5.4 1.3 ug/kg
100-42-5 Styrene ND 5.4 1.1 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.4 1.2 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.4 2.4 ug/kg
127-18-4 Tetrachloroethylene ND 5.4 1.4 ug/kg
108-88-3 Toluene ND 5.4 1.2 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.4 2.1 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.4 1.6 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.4 1.1 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.4 2.0 ug/kg
79-01-6 Trichloroethylene ND 5.4 1.3 ug/kg
75-69-4 Trichlorofluoromethane ND 5.4 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.4 1.8 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.4 1.1 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.4 1.1 ug/kg
108-05-4 Vinyl Acetate ND 27 10 ug/kg
75-01-4 Vinyl Chloride ND 5.4 1.8 ug/kg
m,p-Xylene ND 11 1.9 ug/kg
95-47-6 o-Xylene ND 5.4 1.2 ug/kg
1330-20-7 Xylene (total)ND 16 3.1 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 120%75-124%
17060-07-0 1,2-Dichloroethane-D4 121%72-135%
2037-26-5 Toluene-D8 92%75-126%
460-00-4 4-Bromofluorobenzene 95%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-4 (3-5')
Lab Sample ID:FA38946-5 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:83.7
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 4D76.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 990 200 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 200 30 ug/kg
95-57-8 2-Chlorophenol ND 200 25 ug/kg
120-83-2 2,4-Dichlorophenol ND 200 28 ug/kg
105-67-9 2,4-Dimethylphenol ND 200 24 ug/kg
51-28-5 2,4-Dinitrophenol ND 990 200 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 400 79 ug/kg
95-48-7 2-Methylphenol ND 200 21 ug/kg
3&4-Methylphenol ND 200 47 ug/kg
88-75-5 2-Nitrophenol ND 200 25 ug/kg
100-02-7 4-Nitrophenol ND 990 160 ug/kg
87-86-5 Pentachlorophenol ND 990 160 ug/kg
108-95-2 Phenol ND 200 23 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 200 24 ug/kg
83-32-9 Acenaphthene ND 200 26 ug/kg
208-96-8 Acenaphthylene ND 200 25 ug/kg
120-12-7 Anthracene ND 200 29 ug/kg
56-55-3 Benzo(a)anthracene ND 200 23 ug/kg
50-32-8 Benzo(a)pyrene ND 200 21 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 25 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 20 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 28 ug/kg
100-51-6 Benzyl Alcohol ND 200 26 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 200 23 ug/kg
85-68-7 Butyl benzyl phthalate ND 200 40 ug/kg
106-47-8 4-Chloroaniline ND 200 28 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 200 30 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 200 36 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 200 29 ug/kg
91-58-7 2-Chloronaphthalene ND 200 27 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 200 25 ug/kg
218-01-9 Chrysene ND 200 27 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-4 (3-5')
Lab Sample ID:FA38946-5 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:83.7
Project:Belmont Dyers Site; Belmont, NC
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 200 21 ug/kg
132-64-9 Dibenzofuran ND 200 25 ug/kg
95-50-1 1,2-Dichlorobenzene ND 200 20 ug/kg
541-73-1 1,3-Dichlorobenzene ND 200 22 ug/kg
106-46-7 1,4-Dichlorobenzene ND 200 24 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 200 22 ug/kg
84-66-2 Diethyl Phthalate ND 400 40 ug/kg
131-11-3 Dimethyl Phthalate ND 200 40 ug/kg
117-84-0 Di-n-octyl Phthalate ND 200 40 ug/kg
84-74-2 Di-n-butyl Phthalate ND 400 79 ug/kg
122-66-7 1,2-Diphenylhydrazine ND 200 33 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 400 40 ug/kg
206-44-0 Fluoranthene ND 200 24 ug/kg
86-73-7 Fluorene ND 200 25 ug/kg
118-74-1 Hexachlorobenzene ND 200 24 ug/kg
87-68-3 Hexachlorobutadiene ND 200 22 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 200 40 ug/kg
67-72-1 Hexachloroethane ND 200 23 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 31 ug/kg
78-59-1 Isophorone ND 200 20 ug/kg
90-12-0 1-Methylnaphthalene ND 200 31 ug/kg
91-57-6 2-Methylnaphthalene ND 200 22 ug/kg
91-20-3 Naphthalene ND 200 30 ug/kg
98-95-3 Nitrobenzene ND 200 26 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 200 21 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 200 38 ug/kg
85-01-8 Phenanthrene ND 200 24 ug/kg
129-00-0 Pyrene ND 200 37 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 200 24 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 70%40-102%
4165-62-2 Phenol-d5 75%41-100%
118-79-6 2,4,6-Tribromophenol 78%42-108%
4165-60-0 Nitrobenzene-d5 66%40-105%
321-60-8 2-Fluorobiphenyl 70%43-107%
1718-51-0 Terphenyl-d14 79%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID:SB-4 (3-5')
Lab Sample ID:FA38946-5 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:83.7
Project:Belmont Dyers Site; Belmont, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <5.2 5.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Beryllium a <1.3 1.3 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Cadmium a <1.0 1.0 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Chromium a 38.2 2.6 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Copper a 53.7 6.6 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Lead a <5.2 5.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Manganese a 527 3.9 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Nickel a 26.9 10 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Selenium a <5.2 5.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Silver a <2.6 2.6 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Zinc a 87.5 5.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA13602
(2) Prep QC Batch: MP31219
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
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Client Sample ID:SB-4 (3-5')
Lab Sample ID:FA38946-5 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:83.7
Project:Belmont Dyers Site; Belmont, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.4 2.4 mg/kg 1 12/01/16 12:47 FN SW846 3060A/7196A
Solids, Percent 83.7 % 1 11/23/16 11:28 VK SM19 2540G
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:SB-5 (2-4')
Lab Sample ID:FA38946-6 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:80.0
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0080975.D 1 11/23/16 EP n/a n/a VF2784
Run #2
Initial Weight Final Volume
Run #1 4.90 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone 16.2 64 13 ug/kg J
71-43-2 Benzene ND 6.4 1.6 ug/kg
108-86-1 Bromobenzene ND 6.4 1.6 ug/kg
74-97-5 Bromochloromethane ND 6.4 1.4 ug/kg
75-27-4 Bromodichloromethane ND 6.4 1.3 ug/kg
75-25-2 Bromoform ND 6.4 1.3 ug/kg
78-93-3 2-Butanone (MEK)ND 32 12 ug/kg
104-51-8 n-Butylbenzene ND 6.4 1.3 ug/kg
135-98-8 sec-Butylbenzene ND 6.4 1.3 ug/kg
98-06-6 tert-Butylbenzene ND 6.4 1.3 ug/kg
56-23-5 Carbon Tetrachloride ND 6.4 2.3 ug/kg
108-90-7 Chlorobenzene ND 6.4 1.3 ug/kg
75-00-3 Chloroethane ND 6.4 2.6 ug/kg
67-66-3 Chloroform ND 6.4 1.6 ug/kg
95-49-8 o-Chlorotoluene ND 6.4 1.3 ug/kg
106-43-4 p-Chlorotoluene ND 6.4 1.3 ug/kg
124-48-1 Dibromochloromethane ND 6.4 1.3 ug/kg
106-93-4 1,2-Dibromoethane ND 6.4 1.3 ug/kg
75-71-8 Dichlorodifluoromethane ND 6.4 3.2 ug/kg
95-50-1 1,2-Dichlorobenzene ND 6.4 1.3 ug/kg
541-73-1 1,3-Dichlorobenzene ND 6.4 1.3 ug/kg
106-46-7 1,4-Dichlorobenzene ND 6.4 1.3 ug/kg
75-34-3 1,1-Dichloroethane ND 6.4 2.1 ug/kg
107-06-2 1,2-Dichloroethane ND 6.4 1.3 ug/kg
75-35-4 1,1-Dichloroethylene ND 6.4 1.3 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 6.4 1.5 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 6.4 1.9 ug/kg
78-87-5 1,2-Dichloropropane ND 6.4 2.0 ug/kg
142-28-9 1,3-Dichloropropane ND 6.4 1.3 ug/kg
594-20-7 2,2-Dichloropropane ND 6.4 1.3 ug/kg
563-58-6 1,1-Dichloropropene ND 6.4 1.6 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 6.4 2.4 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:SB-5 (2-4')
Lab Sample ID:FA38946-6 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8260B Percent Solids:80.0
Project:Belmont Dyers Site; Belmont, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 6.4 1.3 ug/kg
108-20-3 Di-Isopropyl Ether ND 6.4 1.5 ug/kg
64-17-5 Ethyl Alcohol ND 510 110 ug/kg
100-41-4 Ethylbenzene ND 6.4 1.4 ug/kg
591-78-6 2-Hexanone ND 32 11 ug/kg
98-82-8 Isopropylbenzene ND 6.4 1.8 ug/kg
99-87-6 p-Isopropyltoluene ND 6.4 1.3 ug/kg
74-83-9 Methyl Bromide ND 6.4 3.3 ug/kg
74-87-3 Methyl Chloride ND 6.4 3.1 ug/kg
75-09-2 Methylene Chloride ND 13 5.1 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 32 14 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 6.4 1.4 ug/kg
91-20-3 Naphthalene ND 6.4 2.6 ug/kg
103-65-1 n-Propylbenzene ND 6.4 1.6 ug/kg
100-42-5 Styrene ND 6.4 1.3 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 6.4 1.4 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 6.4 2.8 ug/kg
127-18-4 Tetrachloroethylene ND 6.4 1.7 ug/kg
108-88-3 Toluene ND 6.4 1.4 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 6.4 2.5 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 6.4 1.9 ug/kg
71-55-6 1,1,1-Trichloroethane ND 6.4 1.3 ug/kg
79-00-5 1,1,2-Trichloroethane ND 6.4 2.3 ug/kg
79-01-6 Trichloroethylene ND 6.4 1.5 ug/kg
75-69-4 Trichlorofluoromethane ND 6.4 2.4 ug/kg
96-18-4 1,2,3-Trichloropropane ND 6.4 2.1 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 6.4 1.3 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 6.4 1.3 ug/kg
108-05-4 Vinyl Acetate ND 32 12 ug/kg
75-01-4 Vinyl Chloride ND 6.4 2.1 ug/kg
m,p-Xylene ND 13 2.2 ug/kg
95-47-6 o-Xylene ND 6.4 1.4 ug/kg
1330-20-7 Xylene (total)ND 19 3.6 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 124%75-124%
17060-07-0 1,2-Dichloroethane-D4 126%72-135%
2037-26-5 Toluene-D8 92%75-126%
460-00-4 4-Bromofluorobenzene 93%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:SB-5 (2-4')
Lab Sample ID:FA38946-6 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:80.0
Project:Belmont Dyers Site; Belmont, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 4D77.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
Run #2
Initial Weight Final Volume
Run #1 29.8 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1000 210 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 210 32 ug/kg
95-57-8 2-Chlorophenol ND 210 27 ug/kg
120-83-2 2,4-Dichlorophenol ND 210 29 ug/kg
105-67-9 2,4-Dimethylphenol ND 210 26 ug/kg
51-28-5 2,4-Dinitrophenol ND 1000 210 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 420 84 ug/kg
95-48-7 2-Methylphenol ND 210 23 ug/kg
3&4-Methylphenol ND 210 49 ug/kg
88-75-5 2-Nitrophenol ND 210 26 ug/kg
100-02-7 4-Nitrophenol ND 1000 170 ug/kg
87-86-5 Pentachlorophenol ND 1000 170 ug/kg
108-95-2 Phenol ND 210 25 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 210 25 ug/kg
83-32-9 Acenaphthene ND 210 27 ug/kg
208-96-8 Acenaphthylene ND 210 26 ug/kg
120-12-7 Anthracene ND 210 30 ug/kg
56-55-3 Benzo(a)anthracene ND 210 24 ug/kg
50-32-8 Benzo(a)pyrene ND 210 22 ug/kg
205-99-2 Benzo(b)fluoranthene ND 210 27 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 210 21 ug/kg
207-08-9 Benzo(k)fluoranthene ND 210 29 ug/kg
100-51-6 Benzyl Alcohol ND 210 28 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 210 24 ug/kg
85-68-7 Butyl benzyl phthalate ND 210 42 ug/kg
106-47-8 4-Chloroaniline ND 210 29 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 210 32 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 210 38 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 210 30 ug/kg
91-58-7 2-Chloronaphthalene ND 210 29 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 210 26 ug/kg
218-01-9 Chrysene ND 210 28 ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:SB-5 (2-4')
Lab Sample ID:FA38946-6 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Method:SW846 8270D SW846 3550C Percent Solids:80.0
Project:Belmont Dyers Site; Belmont, NC
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 210 22 ug/kg
132-64-9 Dibenzofuran ND 210 27 ug/kg
95-50-1 1,2-Dichlorobenzene ND 210 21 ug/kg
541-73-1 1,3-Dichlorobenzene ND 210 24 ug/kg
106-46-7 1,4-Dichlorobenzene ND 210 25 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 210 23 ug/kg
84-66-2 Diethyl Phthalate ND 420 42 ug/kg
131-11-3 Dimethyl Phthalate ND 210 42 ug/kg
117-84-0 Di-n-octyl Phthalate ND 210 42 ug/kg
84-74-2 Di-n-butyl Phthalate ND 420 84 ug/kg
122-66-7 1,2-Diphenylhydrazine ND 210 35 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 420 42 ug/kg
206-44-0 Fluoranthene ND 210 26 ug/kg
86-73-7 Fluorene ND 210 27 ug/kg
118-74-1 Hexachlorobenzene ND 210 26 ug/kg
87-68-3 Hexachlorobutadiene ND 210 24 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 210 42 ug/kg
67-72-1 Hexachloroethane ND 210 24 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 210 32 ug/kg
78-59-1 Isophorone ND 210 22 ug/kg
90-12-0 1-Methylnaphthalene ND 210 33 ug/kg
91-57-6 2-Methylnaphthalene ND 210 24 ug/kg
91-20-3 Naphthalene ND 210 32 ug/kg
98-95-3 Nitrobenzene ND 210 28 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 210 22 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 210 40 ug/kg
85-01-8 Phenanthrene ND 210 25 ug/kg
129-00-0 Pyrene ND 210 39 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 210 25 ug/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 67%40-102%
4165-62-2 Phenol-d5 71%41-100%
118-79-6 2,4,6-Tribromophenol 77%42-108%
4165-60-0 Nitrobenzene-d5 67%40-105%
321-60-8 2-Fluorobiphenyl 70%43-107%
1718-51-0 Terphenyl-d14 75%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:SB-5 (2-4')
Lab Sample ID:FA38946-6 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:80.0
Project:Belmont Dyers Site; Belmont, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Antimony a <6.1 6.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Beryllium a <1.5 1.5 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Cadmium a <1.2 1.2 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Chromium a 39.0 3.0 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Copper a 59.0 7.6 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Lead a <6.1 6.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Manganese a 171 4.6 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Nickel a <12 12 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Selenium a <6.1 6.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Silver a <3.0 3.0 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
Zinc a 50.5 6.1 mg/kg 5 11/28/16 11/28/16 DM SW846 6010C
1 SW846 3050B 2
(1) Instrument QC Batch: MA13602
(2) Prep QC Batch: MP31219
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
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Client Sample ID:SB-5 (2-4')
Lab Sample ID:FA38946-6 Date Sampled:11/21/16
Matrix:SO - Soil Date Received:11/22/16
Percent Solids:80.0
Project:Belmont Dyers Site; Belmont, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Chromium, Hexavalent <2.5 2.5 mg/kg 1 12/01/16 12:47 FN SW846 3060A/7196A
Solids, Percent 80 % 1 11/23/16 11:28 VK SM19 2540G
RL = Reporting Limit
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
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GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
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Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2783-MB F0080947.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 10 ug/kg
71-43-2 Benzene ND 5.0 1.3 ug/kg
108-86-1 Bromobenzene ND 5.0 1.2 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.1 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 9.1 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.8 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.6 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.9 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 1.2 ug/kg
64-17-5 Ethyl Alcohol ND 400 84 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
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Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2783-MB F0080947.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
CAS No. Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 8.7 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.4 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.6 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.4 ug/kg
75-09-2 Methylene Chloride ND 10 4.0 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 11 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.1 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.2 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 2.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 5.0 1.1 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 2.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.8 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 1.9 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.6 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 9.4 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.7 ug/kg
m,p-Xylene ND 10 1.8 ug/kg
95-47-6 o-Xylene ND 5.0 1.1 ug/kg
1330-20-7 Xylene (total)ND 15 2.9 ug/kg
CAS No. Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 109% 75-124%
17060-07-0 1,2-Dichloroethane-D4 107% 72-135%
2037-26-5 Toluene-D8 93% 75-126%
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Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2783-MB F0080947.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 101% 71-133%
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Job Number:FA38946
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Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2784-MB F0080983.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
CAS No. Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 10 ug/kg
71-43-2 Benzene ND 5.0 1.3 ug/kg
108-86-1 Bromobenzene ND 5.0 1.2 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.1 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 9.1 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.8 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.6 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.9 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 1.2 ug/kg
64-17-5 Ethyl Alcohol ND 400 84 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
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Method Blank Summary Page 2 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2784-MB F0080983.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
CAS No. Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 8.7 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.4 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.6 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.4 ug/kg
75-09-2 Methylene Chloride ND 10 4.0 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 11 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.1 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.2 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 2.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 5.0 1.1 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 2.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.8 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 1.9 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.6 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 9.4 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.7 ug/kg
m,p-Xylene ND 10 1.8 ug/kg
95-47-6 o-Xylene ND 5.0 1.1 ug/kg
1330-20-7 Xylene (total)ND 15 2.9 ug/kg
CAS No. Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 117% 75-124%
17060-07-0 1,2-Dichloroethane-D4 113% 72-135%
2037-26-5 Toluene-D8 96% 75-126%
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Method Blank Summary Page 3 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2784-MB F0080983.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 94% 71-133%
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Blank Spike Summary Page 1 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2783-BS F0080949.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
67-64-1 Acetone 250 203 81 61-152
71-43-2 Benzene 50 47.3 95 76-126
108-86-1 Bromobenzene 50 50.7 101 76-122
74-97-5 Bromochloromethane 50 47.3 95 77-120
75-27-4 Bromodichloromethane 50 45.2 90 74-130
75-25-2 Bromoform 50 44.4 89 76-127
78-93-3 2-Butanone (MEK)250 205 82 75-137
104-51-8 n-Butylbenzene 50 54.0 108 71-128
135-98-8 sec-Butylbenzene 50 51.6 103 79-135
98-06-6 tert-Butylbenzene 50 50.7 101 77-133
56-23-5 Carbon Tetrachloride 50 42.8 86 78-133
108-90-7 Chlorobenzene 50 50.0 100 81-129
75-00-3 Chloroethane 50 46.6 93 68-133
67-66-3 Chloroform 50 47.0 94 72-123
95-49-8 o-Chlorotoluene 50 50.5 101 77-129
106-43-4 p-Chlorotoluene 50 48.0 96 80-134
124-48-1 Dibromochloromethane 50 48.6 97 76-127
106-93-4 1,2-Dibromoethane 50 48.3 97 77-126
75-71-8 Dichlorodifluoromethane 50 44.3 89 68-168
95-50-1 1,2-Dichlorobenzene 50 53.3 107 80-129
541-73-1 1,3-Dichlorobenzene 50 52.8 106 81-129
106-46-7 1,4-Dichlorobenzene 50 54.3 109 76-130
75-34-3 1,1-Dichloroethane 50 44.2 88 73-125
107-06-2 1,2-Dichloroethane 50 46.1 92 74-128
75-35-4 1,1-Dichloroethylene 50 42.0 84 81-136
156-59-2 cis-1,2-Dichloroethylene 50 47.4 95 74-126
156-60-5 trans-1,2-Dichloroethylene 50 44.6 89 70-127
78-87-5 1,2-Dichloropropane 50 47.1 94 74-125
142-28-9 1,3-Dichloropropane 50 49.1 98 76-122
594-20-7 2,2-Dichloropropane 50 43.9 88 77-133
563-58-6 1,1-Dichloropropene 50 47.6 95 75-130
10061-01-5 cis-1,3-Dichloropropene 50 45.8 92 80-123
10061-02-6 trans-1,3-Dichloropropene 50 47.6 95 75-131
108-20-3 Di-Isopropyl Ether 50 44.9 90 75-122
64-17-5 Ethyl Alcohol 1000 1360 136 53-154
100-41-4 Ethylbenzene 50 49.1 98 77-123
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2783-BS F0080949.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
591-78-6 2-Hexanone 250 218 87 72-133
98-82-8 Isopropylbenzene 50 49.8 100 80-136
99-87-6 p-Isopropyltoluene 50 52.7 105 77-131
74-83-9 Methyl Bromide 50 44.6 89 65-139
74-87-3 Methyl Chloride 50 44.5 89 71-144
75-09-2 Methylene Chloride 50 42.2 84 74-137
108-10-1 4-Methyl-2-pentanone (MIBK) 250 219 88 76-132
1634-04-4 Methyl Tert Butyl Ether 50 44.2 88 77-120
91-20-3 Naphthalene 50 52.8 106 79-129
103-65-1 n-Propylbenzene 50 46.3 93 80-135
100-42-5 Styrene 50 50.9 102 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 48.9 98 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 46.4 93 71-126
127-18-4 Tetrachloroethylene 50 48.5 97 79-130
108-88-3 Toluene 50 49.0 98 76-124
87-61-6 1,2,3-Trichlorobenzene 50 56.0 112 77-128
120-82-1 1,2,4-Trichlorobenzene 50 56.6 113 78-130
71-55-6 1,1,1-Trichloroethane 50 43.6 87 70-129
79-00-5 1,1,2-Trichloroethane 50 48.8 98 74-124
79-01-6 Trichloroethylene 50 46.5 93 75-128
75-69-4 Trichlorofluoromethane 50 45.1 90 73-145
96-18-4 1,2,3-Trichloropropane 50 47.7 95 74-127
95-63-6 1,2,4-Trimethylbenzene 50 51.5 103 74-123
108-67-8 1,3,5-Trimethylbenzene 50 51.1 102 73-122
108-05-4 Vinyl Acetate 250 235 94 48-164
75-01-4 Vinyl Chloride 50 43.2 86 76-141
m,p-Xylene 100 98.2 98 80-128
95-47-6 o-Xylene 50 51.2 102 80-132
1330-20-7 Xylene (total)150 149 99 80-129
CAS No. Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97% 75-124%
17060-07-0 1,2-Dichloroethane-D4 96% 72-135%
2037-26-5 Toluene-D8 101% 75-126%
* = Outside of Control Limits.
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Blank Spike Summary Page 3 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2783-BS F0080949.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
CAS No. Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 102% 71-133%
* = Outside of Control Limits.
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Blank Spike Summary Page 1 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2784-BS F0080973.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
67-64-1 Acetone 250 258 103 61-152
71-43-2 Benzene 50 48.2 96 76-126
108-86-1 Bromobenzene 50 49.7 99 76-122
74-97-5 Bromochloromethane 50 51.8 104 77-120
75-27-4 Bromodichloromethane 50 48.9 98 74-130
75-25-2 Bromoform 50 48.0 96 76-127
78-93-3 2-Butanone (MEK)250 229 92 75-137
104-51-8 n-Butylbenzene 50 53.8 108 71-128
135-98-8 sec-Butylbenzene 50 52.4 105 79-135
98-06-6 tert-Butylbenzene 50 52.7 105 77-133
56-23-5 Carbon Tetrachloride 50 49.6 99 78-133
108-90-7 Chlorobenzene 50 50.6 101 81-129
75-00-3 Chloroethane 50 52.7 105 68-133
67-66-3 Chloroform 50 50.5 101 72-123
95-49-8 o-Chlorotoluene 50 52.0 104 77-129
106-43-4 p-Chlorotoluene 50 47.1 94 80-134
124-48-1 Dibromochloromethane 50 49.7 99 76-127
106-93-4 1,2-Dibromoethane 50 47.2 94 77-126
75-71-8 Dichlorodifluoromethane 50 48.3 97 68-168
95-50-1 1,2-Dichlorobenzene 50 52.6 105 80-129
541-73-1 1,3-Dichlorobenzene 50 51.7 103 81-129
106-46-7 1,4-Dichlorobenzene 50 52.2 104 76-130
75-34-3 1,1-Dichloroethane 50 51.7 103 73-125
107-06-2 1,2-Dichloroethane 50 49.2 98 74-128
75-35-4 1,1-Dichloroethylene 50 48.1 96 81-136
156-59-2 cis-1,2-Dichloroethylene 50 51.4 103 74-126
156-60-5 trans-1,2-Dichloroethylene 50 49.8 100 70-127
78-87-5 1,2-Dichloropropane 50 49.8 100 74-125
142-28-9 1,3-Dichloropropane 50 49.6 99 76-122
594-20-7 2,2-Dichloropropane 50 50.6 101 77-133
563-58-6 1,1-Dichloropropene 50 48.8 98 75-130
10061-01-5 cis-1,3-Dichloropropene 50 48.1 96 80-123
10061-02-6 trans-1,3-Dichloropropene 50 46.8 94 75-131
108-20-3 Di-Isopropyl Ether 50 52.9 106 75-122
64-17-5 Ethyl Alcohol 1000 932 93 53-154
100-41-4 Ethylbenzene 50 48.8 98 77-123
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2784-BS F0080973.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
591-78-6 2-Hexanone 250 218 87 72-133
98-82-8 Isopropylbenzene 50 51.9 104 80-136
99-87-6 p-Isopropyltoluene 50 52.2 104 77-131
74-83-9 Methyl Bromide 50 50.4 101 65-139
74-87-3 Methyl Chloride 50 50.6 101 71-144
75-09-2 Methylene Chloride 50 53.3 107 74-137
108-10-1 4-Methyl-2-pentanone (MIBK) 250 238 95 76-132
1634-04-4 Methyl Tert Butyl Ether 50 52.6 105 77-120
91-20-3 Naphthalene 50 56.8 114 79-129
103-65-1 n-Propylbenzene 50 47.0 94 80-135
100-42-5 Styrene 50 50.9 102 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 52.4 105 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 50.9 102 71-126
127-18-4 Tetrachloroethylene 50 47.7 95 79-130
108-88-3 Toluene 50 49.9 100 76-124
87-61-6 1,2,3-Trichlorobenzene 50 57.4 115 77-128
120-82-1 1,2,4-Trichlorobenzene 50 54.0 108 78-130
71-55-6 1,1,1-Trichloroethane 50 48.7 97 70-129
79-00-5 1,1,2-Trichloroethane 50 48.0 96 74-124
79-01-6 Trichloroethylene 50 48.6 97 75-128
75-69-4 Trichlorofluoromethane 50 48.5 97 73-145
96-18-4 1,2,3-Trichloropropane 50 49.5 99 74-127
95-63-6 1,2,4-Trimethylbenzene 50 52.4 105 74-123
108-67-8 1,3,5-Trimethylbenzene 50 52.9 106 73-122
108-05-4 Vinyl Acetate 250 250 100 48-164
75-01-4 Vinyl Chloride 50 49.3 99 76-141
m,p-Xylene 100 101 101 80-128
95-47-6 o-Xylene 50 53.2 106 80-132
1330-20-7 Xylene (total)150 154 103 80-129
CAS No. Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99% 75-124%
17060-07-0 1,2-Dichloroethane-D4 97% 72-135%
2037-26-5 Toluene-D8 97% 75-126%
* = Outside of Control Limits.
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Blank Spike Summary Page 3 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2784-BS F0080973.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
CAS No. Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 97% 71-133%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA38945-3MS F0080952.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3MSD F0080953.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3 F0080950.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3 F0080951.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
FA38945-3 Spike MS MS Spike MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD
67-64-1 Acetone ND 298 188 63 299 203 68 8 61-152/27
71-43-2 Benzene ND 59.7 47.6 80 59.8 45.6 76 4 76-126/26
108-86-1 Bromobenzene ND 59.7 48.6 81 59.8 42.4 71*14 76-122/32
74-97-5 Bromochloromethane ND 59.7 50.8 85 59.8 48.5 81 5 77-120/24
75-27-4 Bromodichloromethane ND 59.7 45.9 77 59.8 46.5 78 1 74-130/25
75-25-2 Bromoform ND 59.7 43.8 73* 59.8 41.1 69*6 76-127/26
78-93-3 2-Butanone (MEK)ND 298 213 71* 299 216 72*1 75-137/25
104-51-8 n-Butylbenzene ND 59.7 47.7 80 59.8 43.0 72 10 71-128/35
135-98-8 sec-Butylbenzene ND 59.7 50.4 84 59.8 48.2 81 4 79-135/34
98-06-6 tert-Butylbenzene ND 59.7 53.4 89 59.8 51.1 85 4 77-133/34
56-23-5 Carbon Tetrachloride ND 59.7 41.6 70* 59.8 43.6 73*5 78-133/29
108-90-7 Chlorobenzene ND 59.7 46.2 77* 59.8 41.5 69*11 81-129/29
75-00-3 Chloroethane ND 59.7 41.6 70 59.8 51.4 86 21 68-133/29
67-66-3 Chloroform ND 59.7 50.4 84 59.8 48.9 82 3 72-123/26
95-49-8 o-Chlorotoluene ND 59.7 49.9 84 59.8 49.3 82 1 77-129/33
106-43-4 p-Chlorotoluene ND 59.7 44.1 74* 59.8 40.3 67*9 80-134/33
124-48-1 Dibromochloromethane ND 59.7 48.4 81 59.8 46.1 77 5 76-127/27
106-93-4 1,2-Dibromoethane ND 59.7 47.2 79 59.8 42.4 71*11 77-126/26
75-71-8 Dichlorodifluoromethane ND 59.7 39.7 67* 59.8 43.4 73 9 68-168/29
95-50-1 1,2-Dichlorobenzene ND 59.7 45.6 76* 59.8 41.5 69*9 80-129/32
541-73-1 1,3-Dichlorobenzene ND 59.7 46.4 78* 59.8 40.6 68*13 81-129/33
106-46-7 1,4-Dichlorobenzene ND 59.7 44.5 75* 59.8 40.3 67*10 76-130/32
75-34-3 1,1-Dichloroethane ND 59.7 44.3 74 59.8 49.9 83 12 73-125/27
107-06-2 1,2-Dichloroethane ND 59.7 50.2 84 59.8 50.3 84 0 74-128/23
75-35-4 1,1-Dichloroethylene ND 59.7 43.9 74* 59.8 44.3 74*1 81-136/28
156-59-2 cis-1,2-Dichloroethylene 2.0 J 59.7 46.9 75 59.8 44.2 71*6 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 59.7 44.9 75 59.8 41.5 69*8 70-127/27
78-87-5 1,2-Dichloropropane ND 59.7 48.4 81 59.8 48.2 81 0 74-125/25
142-28-9 1,3-Dichloropropane ND 59.7 49.6 83 59.8 47.1 79 5 76-122/26
594-20-7 2,2-Dichloropropane ND 59.7 43.9 74* 59.8 47.4 79 8 77-133/28
563-58-6 1,1-Dichloropropene ND 59.7 44.5 75 59.8 39.3 66*12 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 59.7 43.7 73* 59.8 39.7 66*10 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 59.7 44.6 75 59.8 38.4 64*15 75-131/28
108-20-3 Di-Isopropyl Ether ND 59.7 47.7 80 59.8 56.4 94 17 75-122/25
64-17-5 Ethyl Alcohol ND 1190 1460 122 1200 1350 113 8 53-154/42
100-41-4 Ethylbenzene ND 59.7 48.2 81 59.8 44.6 75*8 77-123/31
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA38945-3MS F0080952.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3MSD F0080953.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3 F0080950.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3 F0080951.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
FA38945-3 Spike MS MS Spike MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD
591-78-6 2-Hexanone ND 298 219 73 299 219 73 0 72-133/26
98-82-8 Isopropylbenzene ND 59.7 47.1 79* 59.8 47.4 79*1 80-136/32
99-87-6 p-Isopropyltoluene ND 59.7 51.6 86 59.8 50.5 84 2 77-131/34
74-83-9 Methyl Bromide ND 59.7 45.1 76 59.8 47.1 79 4 65-139/31
74-87-3 Methyl Chloride ND 59.7 43.7 73 59.8 45.9 77 5 71-144/27
75-09-2 Methylene Chloride ND 59.7 55.6 93 59.8 57.9 97 4 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK) ND 298 248 83 299 277 93 11 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 59.7 53.4 89 59.8 64.4 108 19 77-120/24
91-20-3 Naphthalene ND 59.7 31.8 53* 59.8 28.7 48*10 79-129/33
103-65-1 n-Propylbenzene ND 59.7 47.3 79* 59.8 44.5 74*6 80-135/33
100-42-5 Styrene ND 59.7 44.6 75* 59.8 40.0 67*11 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 59.7 50.1 84 59.8 53.3 89 6 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 59.7 52.9 89 59.8 55.8 93 5 71-126/30
127-18-4 Tetrachloroethylene ND 59.7 49.3 83 59.8 46.9 78*5 79-130/31
108-88-3 Toluene ND 59.7 47.4 79 59.8 46.4 78 2 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 59.7 32.4 54* 59.8 30.7 51*5 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 59.7 36.0 60* 59.8 30.5 51*17 78-130/34
71-55-6 1,1,1-Trichloroethane 101
a J 59.7 44.7 -94* 59.8 45.5 -93*2 70-129/27
79-00-5 1,1,2-Trichloroethane ND 59.7 51.4 86 59.8 51.4 86 0 74-124/28
79-01-6 Trichloroethylene 19300 c 59.7 132 -32124* b59.8 162 -32003* b20 75-128/27
75-69-4 Trichlorofluoromethane ND 59.7 42.7 72* 59.8 46.1 77 8 73-145/31
96-18-4 1,2,3-Trichloropropane ND 59.7 53.8 90 59.8 54.2 91 1 74-127/27
95-63-6 1,2,4-Trimethylbenzene ND 59.7 53.3 89 59.8 53.5 89 0 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 59.7 52.7 88 59.8 53.2 89 1 73-122/33
108-05-4 Vinyl Acetate ND 298 113 38* 299 95.8 32*16 48-164/37
75-01-4 Vinyl Chloride ND 59.7 41.3 69* 59.8 42.7 71*3 76-141/27
m,p-Xylene ND 119 96.0 80 120 93.5 78*3 80-128/30
95-47-6 o-Xylene ND 59.7 50.7 85 59.8 49.0 82 3 80-132/30
1330-20-7 Xylene (total)ND 179 147 82 179 142 79*3 80-129/30
CAS No. Surrogate Recoveries MS MSD FA38945-3 FA38945-3 Limits
1868-53-7 Dibromofluoromethane 100%102%117%109% 75-124%
17060-07-0 1,2-Dichloroethane-D4 92%97%119%105% 72-135%
2037-26-5 Toluene-D8 97%105%109%94% 75-126%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA38945-3MS F0080952.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3MSD F0080953.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3 F0080950.D 1 11/22/16 EP n/a n/a VF2783
FA38945-3 F0080951.D 1 11/22/16 EP n/a n/a VF2783
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-2, FA38946-3, FA38946-4, FA38946-5
CAS No. Surrogate Recoveries MS MSD FA38945-3 FA38945-3 Limits
460-00-4 4-Bromofluorobenzene 105%108%118%96% 71-133%
(a) Result is from Run #2.
(b) Outside control limits due to high level in sample relative to spike amount.
(c) Result is from Run #3.
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA38991-7MS F0080991.D 1 11/23/16 EP n/a n/a VF2784
FA38991-7MSD F0080992.D 1 11/23/16 EP n/a n/a VF2784
FA38991-7 F0080990.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
FA38991-7 Spike MS MS Spike MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD
67-64-1 Acetone 26 U 397 176 44* 397 182 46*3 61-152/27
71-43-2 Benzene 2.6 U 79.5 65.8 83 79.3 66.4 84 1 76-126/26
108-86-1 Bromobenzene 2.6 U 79.5 74.4 94 79.3 75.0 95 1 76-122/32
74-97-5 Bromochloromethane 2.6 U 79.5 58.6 74* 79.3 68.4 86 15 77-120/24
75-27-4 Bromodichloromethane 2.6 U 79.5 67.1 84 79.3 67.2 85 0 74-130/25
75-25-2 Bromoform 2.6 U 79.5 60.3 76 79.3 64.1 81 6 76-127/26
78-93-3 2-Butanone (MEK)13 U 397 194 49* 397 221 56*13 75-137/25
104-51-8 n-Butylbenzene 2.6 U 79.5 78.4 99 79.3 77.8 98 1 71-128/35
135-98-8 sec-Butylbenzene 2.6 U 79.5 72.7 91 79.3 71.3 90 2 79-135/34
98-06-6 tert-Butylbenzene 2.6 U 79.5 72.1 91 79.3 70.6 89 2 77-133/34
56-23-5 Carbon Tetrachloride 2.6 U 79.5 59.0 74* 79.3 58.9 74*0 78-133/29
108-90-7 Chlorobenzene 2.6 U 79.5 74.5 94 79.3 73.4 93 1 81-129/29
75-00-3 Chloroethane 2.6 U 79.5 71.6 90 79.3 67.1 85 6 68-133/29
67-66-3 Chloroform 2.6 U 79.5 65.2 82 79.3 67.4 85 3 72-123/26
95-49-8 o-Chlorotoluene 2.6 U 79.5 75.0 94 79.3 73.9 93 1 77-129/33
106-43-4 p-Chlorotoluene 2.6 U 79.5 75.5 95 79.3 71.0 90 6 80-134/33
124-48-1 Dibromochloromethane 2.6 U 79.5 66.1 83 79.3 71.3 90 8 76-127/27
106-93-4 1,2-Dibromoethane 2.6 U 79.5 66.3 83 79.3 67.2 85 1 77-126/26
75-71-8 Dichlorodifluoromethane 2.6 U 79.5 51.2 64* 79.3 48.8 62*5 68-168/29
95-50-1 1,2-Dichlorobenzene 2.6 U 79.5 80.3 101 79.3 77.5 98 4 80-129/32
541-73-1 1,3-Dichlorobenzene 2.6 U 79.5 82.2 103 79.3 82.8 104 1 81-129/33
106-46-7 1,4-Dichlorobenzene 2.6 U 79.5 85.5 108 79.3 84.6 107 1 76-130/32
75-34-3 1,1-Dichloroethane 2.6 U 79.5 64.6 81 79.3 65.5 83 1 73-125/27
107-06-2 1,2-Dichloroethane 2.6 U 79.5 69.5 87 79.3 69.7 88 0 74-128/23
75-35-4 1,1-Dichloroethylene 2.6 U 79.5 65.3 82 79.3 63.9 81 2 81-136/28
156-59-2 cis-1,2-Dichloroethylene 2.6 U 79.5 53.4 67* 79.3 66.1 83 21 74-126/26
156-60-5 trans-1,2-Dichloroethylene 2.6 U 79.5 74.8 94 79.3 71.3 90 5 70-127/27
78-87-5 1,2-Dichloropropane 2.6 U 79.5 69.8 88 79.3 67.7 85 3 74-125/25
142-28-9 1,3-Dichloropropane 2.6 U 79.5 67.0 84 79.3 69.8 88 4 76-122/26
594-20-7 2,2-Dichloropropane 2.6 U 79.5 46.1 58* 79.3 55.9 70*19 77-133/28
563-58-6 1,1-Dichloropropene 2.6 U 79.5 58.7 74* 79.3 61.9 78 5 75-130/28
10061-01-5 cis-1,3-Dichloropropene 2.6 U 79.5 65.3 82 79.3 65.6 83 0 80-123/26
10061-02-6 trans-1,3-Dichloropropene 2.6 U 79.5 69.4 87 79.3 73.5 93 6 75-131/28
108-20-3 Di-Isopropyl Ether 2.6 U 79.5 65.7 83 79.3 67.7 85 3 75-122/25
64-17-5 Ethyl Alcohol 210 U 1590 1190 75 1590 1720 108 36 53-154/42
100-41-4 Ethylbenzene 2.6 U 79.5 69.8 88 79.3 71.1 90 2 77-123/31
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA38991-7MS F0080991.D 1 11/23/16 EP n/a n/a VF2784
FA38991-7MSD F0080992.D 1 11/23/16 EP n/a n/a VF2784
FA38991-7 F0080990.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
FA38991-7 Spike MS MS Spike MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD
591-78-6 2-Hexanone 13 U 397 257 65* 397 268 68*4 72-133/26
98-82-8 Isopropylbenzene 2.6 U 79.5 71.3 90 79.3 71.7 90 1 80-136/32
99-87-6 p-Isopropyltoluene 2.6 U 79.5 76.7 96 79.3 74.2 94 3 77-131/34
74-83-9 Methyl Bromide 2.6 U 79.5 63.8 80 79.3 61.3 77 4 65-139/31
74-87-3 Methyl Chloride 2.6 U 79.5 62.1 78 79.3 59.4 75 4 71-144/27
75-09-2 Methylene Chloride 5.2 U 79.5 80.0 101 79.3 78.4 99 2 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK) 13 U 397 316 79 397 318 80 1 76-132/26
1634-04-4 Methyl Tert Butyl Ether 2.6 U 79.5 70.6 89 79.3 69.2 87 2 77-120/24
91-20-3 Naphthalene 2.6 U 79.5 76.7 96 79.3 73.9 93 4 79-129/33
103-65-1 n-Propylbenzene 2.6 U 79.5 67.3 85 79.3 68.0 86 1 80-135/33
100-42-5 Styrene 2.6 U 79.5 73.9 93 79.3 72.9 92 1 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane 2.6 U 79.5 71.4 90 79.3 71.6 90 0 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane 2.6 U 79.5 68.7 86 79.3 65.8 83 4 71-126/30
127-18-4 Tetrachloroethylene 2.6 U 79.5 73.3 92 79.3 76.8 97 5 79-130/31
108-88-3 Toluene 2.6 U 79.5 68.4 86 79.3 69.5 88 2 76-124/30
87-61-6 1,2,3-Trichlorobenzene 2.6 U 79.5 83.5 105 79.3 79.0 100 6 77-128/35
120-82-1 1,2,4-Trichlorobenzene 2.6 U 79.5 89.5 113 79.3 83.1 105 7 78-130/34
71-55-6 1,1,1-Trichloroethane 2.6 U 79.5 60.0 75 79.3 59.6 75 1 70-129/27
79-00-5 1,1,2-Trichloroethane 2.6 U 79.5 68.3 86 79.3 70.4 89 3 74-124/28
79-01-6 Trichloroethylene 2.6 U 79.5 69.3 87 79.3 70.7 89 2 75-128/27
75-69-4 Trichlorofluoromethane 2.6 U 79.5 59.6 75 79.3 56.3 71*6 73-145/31
96-18-4 1,2,3-Trichloropropane 2.6 U 79.5 69.9 88 79.3 68.2 86 2 74-127/27
95-63-6 1,2,4-Trimethylbenzene 2.6 U 79.5 79.8 100 79.3 77.1 97 3 74-123/34
108-67-8 1,3,5-Trimethylbenzene 2.6 U 79.5 75.9 95 79.3 73.2 92 4 73-122/33
108-05-4 Vinyl Acetate 13 U 397 60.3 15* 397 65.7 17*9 48-164/37
75-01-4 Vinyl Chloride 2.6 U 79.5 59.5 75* 79.3 58.6 74*2 76-141/27
m,p-Xylene 5.2 U 159 140 88 159 145 91 4 80-128/30
95-47-6 o-Xylene 2.6 U 79.5 72.8 92 79.3 72.7 92 0 80-132/30
1330-20-7 Xylene (total)7.9 U 238 213 89 238 218 92 2 80-129/30
CAS No. Surrogate Recoveries MS MSD FA38991-7 Limits
1868-53-7 Dibromofluoromethane 92%95%123% 75-124%
17060-07-0 1,2-Dichloroethane-D4 93%95%119% 72-135%
2037-26-5 Toluene-D8 96%97%94% 75-126%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA38991-7MS F0080991.D 1 11/23/16 EP n/a n/a VF2784
FA38991-7MSD F0080992.D 1 11/23/16 EP n/a n/a VF2784
FA38991-7 F0080990.D 1 11/23/16 EP n/a n/a VF2784
The QC reported here applies to the following samples:Method: SW846 8260B
FA38946-6
CAS No. Surrogate Recoveries MS MSD FA38991-7 Limits
460-00-4 4-Bromofluorobenzene 94%98%103% 71-133%
* = Outside of Control Limits.
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SGS Accutest
GC/MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 6
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Method Blank Summary Page 1 of 2
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP62837-MB 4D69.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
The QC reported here applies to the following samples:Method: SW846 8270D
FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
CAS No. Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 25 ug/kg
95-57-8 2-Chlorophenol ND 170 21 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 20 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 18 ug/kg
3&4-Methylphenol ND 170 39 ug/kg
88-75-5 2-Nitrophenol ND 170 21 ug/kg
100-02-7 4-Nitrophenol ND 830 130 ug/kg
87-86-5 Pentachlorophenol ND 830 130 ug/kg
108-95-2 Phenol ND 170 20 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 20 ug/kg
83-32-9 Acenaphthene ND 170 21 ug/kg
208-96-8 Acenaphthylene ND 170 21 ug/kg
120-12-7 Anthracene ND 170 24 ug/kg
56-55-3 Benzo(a)anthracene ND 170 19 ug/kg
50-32-8 Benzo(a)pyrene ND 170 18 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 21 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 23 ug/kg
100-51-6 Benzyl Alcohol ND 170 22 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 19 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 23 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 25 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 30 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 170 24 ug/kg
91-58-7 2-Chloronaphthalene ND 170 23 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 21 ug/kg
218-01-9 Chrysene ND 170 22 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 18 ug/kg
132-64-9 Dibenzofuran ND 170 21 ug/kg
95-50-1 1,2-Dichlorobenzene ND 170 17 ug/kg
541-73-1 1,3-Dichlorobenzene ND 170 19 ug/kg
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Method Blank Summary Page 2 of 2
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP62837-MB 4D69.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
The QC reported here applies to the following samples:Method: SW846 8270D
FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
CAS No. Compound Result RL MDL Units Q
106-46-7 1,4-Dichlorobenzene ND 170 20 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 18 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
122-66-7 1,2-Diphenylhydrazine ND 170 28 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 20 ug/kg
86-73-7 Fluorene ND 170 21 ug/kg
118-74-1 Hexachlorobenzene ND 170 21 ug/kg
87-68-3 Hexachlorobutadiene ND 170 19 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 19 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 26 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 26 ug/kg
91-57-6 2-Methylnaphthalene ND 170 19 ug/kg
91-20-3 Naphthalene ND 170 25 ug/kg
98-95-3 Nitrobenzene ND 170 22 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 18 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 32 ug/kg
85-01-8 Phenanthrene ND 170 20 ug/kg
129-00-0 Pyrene ND 170 31 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 170 20 ug/kg
CAS No. Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 64% 40-102%
4165-62-2 Phenol-d5 69% 41-100%
118-79-6 2,4,6-Tribromophenol 62% 42-108%
4165-60-0 Nitrobenzene-d5 61% 40-105%
321-60-8 2-Fluorobiphenyl 66% 43-107%
1718-51-0 Terphenyl-d14 73% 45-119%
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Blank Spike Summary Page 1 of 2
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP62837-BS 4D68.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
The QC reported here applies to the following samples:Method: SW846 8270D
FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
65-85-0 Benzoic Acid 3330 2740 82 36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1320 79 52-108
95-57-8 2-Chlorophenol 1670 1240 74 48-104
120-83-2 2,4-Dichlorophenol 1670 1330 80 51-105
105-67-9 2,4-Dimethylphenol 1670 1130 68 43-96
51-28-5 2,4-Dinitrophenol 3330 1480 44 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 2460 74 64-121
95-48-7 2-Methylphenol 1670 1230 74 46-107
3&4-Methylphenol 3330 2410 72 44-111
88-75-5 2-Nitrophenol 1670 1380 83 49-104
100-02-7 4-Nitrophenol 3330 2730 82 56-116
87-86-5 Pentachlorophenol 3330 2930 88 61-114
108-95-2 Phenol 1670 1270 76 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1400 84 56-109
83-32-9 Acenaphthene 1670 1280 77 56-109
208-96-8 Acenaphthylene 1670 1310 79 56-106
120-12-7 Anthracene 1670 1430 86 61-110
56-55-3 Benzo(a)anthracene 1670 1390 83 66-111
50-32-8 Benzo(a)pyrene 1670 1410 85 59-104
205-99-2 Benzo(b)fluoranthene 1670 1440 86 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1390 83 67-113
207-08-9 Benzo(k)fluoranthene 1670 1420 85 67-114
100-51-6 Benzyl Alcohol 1670 1410 85 53-108
101-55-3 4-Bromophenyl phenyl ether 1670 1470 88 62-110
85-68-7 Butyl benzyl phthalate 1670 1480 89 65-113
106-47-8 4-Chloroaniline 1670 1290 77 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1230 74 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 1170 70 46-103
108-60-1 bis(2-Chloroisopropyl)ether 1670 1200 72 40-110
91-58-7 2-Chloronaphthalene 1670 1290 77 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1340 80 58-106
218-01-9 Chrysene 1670 1420 85 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1450 87 68-115
132-64-9 Dibenzofuran 1670 1480 89 57-108
95-50-1 1,2-Dichlorobenzene 1670 1190 71 44-102
541-73-1 1,3-Dichlorobenzene 1670 1160 70 42-100
* = Outside of Control Limits.
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Blank Spike Summary Page 2 of 2
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP62837-BS 4D68.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
The QC reported here applies to the following samples:Method: SW846 8270D
FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
106-46-7 1,4-Dichlorobenzene 1670 1170 70 40-106
91-94-1 3,3'-Dichlorobenzidine 1670 1450 87 36-114
84-66-2 Diethyl Phthalate 1670 1340 80 61-109
131-11-3 Dimethyl Phthalate 1670 1320 79 59-108
117-84-0 Di-n-octyl Phthalate 1670 1650 99 64-119
84-74-2 Di-n-butyl Phthalate 1670 1440 86 63-108
122-66-7 1,2-Diphenylhydrazine 1670 1370 82 58-112
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1520 91 64-115
206-44-0 Fluoranthene 1670 1370 82 60-108
86-73-7 Fluorene 1670 1360 82 58-109
118-74-1 Hexachlorobenzene 1670 1420 85 59-111
87-68-3 Hexachlorobutadiene 1670 1240 74 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1360 82 49-110
67-72-1 Hexachloroethane 1670 1160 70 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1440 86 66-116
78-59-1 Isophorone 1670 1280 77 42-89
90-12-0 1-Methylnaphthalene 1670 1280 77 49-106
91-57-6 2-Methylnaphthalene 1670 1380 83 47-106
91-20-3 Naphthalene 1670 1190 71 44-104
98-95-3 Nitrobenzene 1670 1240 74 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1140 68 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1420 85 62-110
85-01-8 Phenanthrene 1670 1400 84 63-111
129-00-0 Pyrene 1670 1450 87 65-115
120-82-1 1,2,4-Trichlorobenzene 1670 1230 74 45-100
CAS No. Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 72% 40-102%
4165-62-2 Phenol-d5 74% 41-100%
118-79-6 2,4,6-Tribromophenol 84% 42-108%
4165-60-0 Nitrobenzene-d5 69% 40-105%
321-60-8 2-Fluorobiphenyl 72% 43-107%
1718-51-0 Terphenyl-d14 82% 45-119%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP62837-MS 4D71.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
OP62837-MSD 4D72.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
FA38937-1 4D70.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
The QC reported here applies to the following samples:Method: SW846 8270D
FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
FA38937-1 Spike MS MS Spike MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD
65-85-0 Benzoic Acid 850 U 3440 1680 49 3440 1270 37 28 36-118/41
59-50-7 4-Chloro-3-methyl Phenol 170 U 1720 1280 74 1720 1210 70 6 52-108/21
95-57-8 2-Chlorophenol 170 U 1720 1160 68 1720 1160 68 0 48-104/26
120-83-2 2,4-Dichlorophenol 170 U 1720 1270 74 1720 1210 70 5 51-105/27
105-67-9 2,4-Dimethylphenol 170 U 1720 1080 63 1720 1050 61 3 43-96/23
51-28-5 2,4-Dinitrophenol 850 U 3440 1030 30* 3440 1100 32*7 40-119/32
534-52-1 4,6-Dinitro-o-cresol 340 U 3440 2140 62* 3440 2130 62*0 64-121/29
95-48-7 2-Methylphenol 170 U 1720 1120 65 1720 1140 66 2 46-107/24
3&4-Methylphenol 170 U 3440 2220 65 3440 2210 64 0 44-111/24
88-75-5 2-Nitrophenol 170 U 1720 1270 74 1720 1260 73 1 49-104/27
100-02-7 4-Nitrophenol 850 U 3440 2640 77 3440 2520 73 5 56-116/23
87-86-5 Pentachlorophenol 850 U 3440 2700 79 3440 2580 75 5 61-114/23
108-95-2 Phenol 170 U 1720 1170 68 1720 1160 68 1 45-110/24
88-06-2 2,4,6-Trichlorophenol 170 U 1720 1350 79 1720 1300 76 4 56-109/25
83-32-9 Acenaphthene 170 U 1720 1220 71 1720 1200 70 2 56-109/23
208-96-8 Acenaphthylene 170 U 1720 1260 73 1720 1240 72 2 56-106/23
120-12-7 Anthracene 170 U 1720 1370 80 1720 1310 76 4 61-110/21
56-55-3 Benzo(a)anthracene 170 U 1720 1320 77 1720 1290 75 2 66-111/23
50-32-8 Benzo(a)pyrene 170 U 1720 1350 79 1720 1310 76 3 59-104/23
205-99-2 Benzo(b)fluoranthene 170 U 1720 1370 80 1720 1330 77 3 67-113/24
191-24-2 Benzo(g,h,i)perylene 170 U 1720 1340 78 1720 1310 76 2 67-113/21
207-08-9 Benzo(k)fluoranthene 170 U 1720 1380 80 1720 1320 77 4 67-114/22
100-51-6 Benzyl Alcohol 170 U 1720 1300 76 1720 1270 74 2 53-108/24
101-55-3 4-Bromophenyl phenyl ether 170 U 1720 1390 81 1720 1350 79 3 62-110/21
85-68-7 Butyl benzyl phthalate 170 U 1720 1430 83 1720 1390 81 3 65-113/20
106-47-8 4-Chloroaniline 170 U 1720 1300 76 1720 1230 72 6 30-115/30
111-91-1 bis(2-Chloroethoxy)methane 170 U 1720 1160 68 1720 1150 67 1 48-105/24
111-44-4 bis(2-Chloroethyl)ether 170 U 1720 1080 63 1720 1080 63 0 46-103/27
108-60-1 bis(2-Chloroisopropyl)ether 170 U 1720 1110 65 1720 1110 65 0 40-110/25
91-58-7 2-Chloronaphthalene 170 U 1720 1240 72 1720 1230 72 1 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether 170 U 1720 1290 75 1720 1250 73 3 58-106/21
218-01-9 Chrysene 170 U 1720 1370 80 1720 1330 77 3 65-112/25
53-70-3 Dibenzo(a,h)anthracene 170 U 1720 1360 79 1720 1330 77 2 68-115/23
132-64-9 Dibenzofuran 170 U 1720 1420 83 1720 1380 80 3 57-108/22
95-50-1 1,2-Dichlorobenzene 170 U 1720 1060 62 1720 1110 65 5 44-102/28
541-73-1 1,3-Dichlorobenzene 170 U 1720 1060 62 1720 1080 63 2 42-100/30
* = Outside of Control Limits.
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Job Number:FA38946
Account:HHNCC Hart & Hickman
Project:Belmont Dyers Site; Belmont, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP62837-MS 4D71.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
OP62837-MSD 4D72.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
FA38937-1 4D70.D 1 11/25/16 ME 11/23/16 OP62837 S4D5
The QC reported here applies to the following samples:Method: SW846 8270D
FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
FA38937-1 Spike MS MS Spike MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD
106-46-7 1,4-Dichlorobenzene 170 U 1720 1070 62 1720 1090 63 2 40-106/29
91-94-1 3,3'-Dichlorobenzidine 170 U 1720 1420 83 1720 1390 81 2 36-114/28
84-66-2 Diethyl Phthalate 340 U 1720 1310 76 1720 1260 73 4 61-109/20
131-11-3 Dimethyl Phthalate 170 U 1720 1280 74 1720 1270 74 1 59-108/20
117-84-0 Di-n-octyl Phthalate 170 U 1720 1530 89 1720 1500 87 2 64-119/21
84-74-2 Di-n-butyl Phthalate 340 U 1720 1420 83 1720 1330 77 7 63-108/19
122-66-7 1,2-Diphenylhydrazine 170 U 1720 1340 78 1720 1280 74 5 58-112/22
117-81-7 bis(2-Ethylhexyl)phthalate 340 U 1720 1440 84 1720 1400 81 3 64-115/23
206-44-0 Fluoranthene 170 U 1720 1330 77 1720 1260 73 5 60-108/25
86-73-7 Fluorene 170 U 1720 1310 76 1720 1280 74 2 58-109/21
118-74-1 Hexachlorobenzene 170 U 1720 1350 79 1720 1340 78 1 59-111/21
87-68-3 Hexachlorobutadiene 170 U 1720 1180 69 1720 1160 68 2 41-108/27
77-47-4 Hexachlorocyclopentadiene 170 U 1720 1240 72 1720 1260 73 2 49-110/31
67-72-1 Hexachloroethane 170 U 1720 1050 61 1720 1050 61 0 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene 170 U 1720 1370 80 1720 1310 76 4 66-116/22
78-59-1 Isophorone 170 U 1720 1200 70 1720 1160 68 3 42-89/22
90-12-0 1-Methylnaphthalene 170 U 1720 1230 72 1720 1190 69 3 49-106/26
91-57-6 2-Methylnaphthalene 170 U 1720 1320 77 1720 1270 74 4 47-106/27
91-20-3 Naphthalene 170 U 1720 1140 66 1720 1120 65 2 44-104/27
98-95-3 Nitrobenzene 170 U 1720 1170 68 1720 1120 65 4 43-108/25
621-64-7 N-Nitrosodi-n-propylamine 170 U 1720 1050 61 1720 1050 61 0 48-108/27
86-30-6 N-Nitrosodiphenylamine 170 U 1720 1370 80 1720 1320 77 4 62-110/21
85-01-8 Phenanthrene 170 U 1720 1330 77 1720 1290 75 3 63-111/22
129-00-0 Pyrene 170 U 1720 1380 80 1720 1370 80 1 65-115/25
120-82-1 1,2,4-Trichlorobenzene 170 U 1720 1140 66 1720 1130 66 1 45-100/26
CAS No. Surrogate Recoveries MS MSD FA38937-1 Limits
367-12-4 2-Fluorophenol 65%64%73% 40-102%
4165-62-2 Phenol-d5 67%66%78% 41-100%
118-79-6 2,4,6-Tribromophenol 77%75%72% 42-108%
4165-60-0 Nitrobenzene-d5 63%61%70% 40-105%
321-60-8 2-Fluorobiphenyl 68%66%72% 43-107%
1718-51-0 Terphenyl-d14 76%75%81% 45-119%
* = Outside of Control Limits.
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SGS Accutest
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
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BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
QC Batch ID: MP31219 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 11/28/16
MB
Metal RL IDL MDL raw final
Aluminum 10 .7 1.8
Antimony 1.0 .05 .065 0.060 <1.0
Arsenic 0.50 .065 .1
Barium 10 .05 .05
Beryllium 0.25 .01 .025 -0.0050 <0.25
Cadmium 0.20 .01 .025 -0.010 <0.20
Calcium 250 2.5 2.5
Chromium 0.50 .05 .05 0.030 <0.50
Cobalt 2.5 .01 .025
Copper 1.3 .05 .05 0.065 <1.3
Iron 15 .85 .85
Lead 1.0 .05 .05 0.025 <1.0
Magnesium 250 1.8 1.8
Manganese 0.75 .025 .025 0.010 <0.75
Molybdenum 2.5 .015 .025
Nickel 2.0 .02 .025 0.0050 <2.0
Potassium 500 10 10
Selenium 1.0 .12 .12 0.085 <1.0
Silver 0.50 .035 .041 -0.0050 <0.50
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .055 .055
Tin 2.5 .045 .045
Titanium 0.50 .025 .025
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15 0.11 <1.0
Associated samples MP31219: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
QC Batch ID: MP31219 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 11/28/16 11/28/16
FA38945-1 QC FA38945-1 Spikelot QC
Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum anr
Antimony 0.96 0.67 35.6 (a) 0-20 0.96 9.7 27.5 31.8N(c) 80-120
Arsenic anr
Barium anr
Beryllium 0.13 0.12 8.0 0-20 0.13 2.9 2.75 100.9 80-120
Cadmium 0.092 0.058 45.3 (a) 0-20 0.092 2.9 2.75 102.3 80-120
Calcium anr
Chromium 15.4 12.7 19.2 0-20 15.4 22.3 11 62.8N(c) 80-120
Cobalt anr
Copper 119 110 7.9 0-20 119 119 13.7 0.0 (d) 80-120
Iron anr
Lead 179 136 27.3*(b) 0-20 179 161 27.5 -65.6(d) 80-120
Magnesium anr
Manganese 85.6 69.4 20.9*(b) 0-20 85.6 141 27.5 201.8N(c 80-120
Molybdenum
Nickel 5.2 4.2 21.3 (a) 0-20 5.2 31.0 27.5 94.0 80-120
Potassium anr
Selenium 0.14 0.0 200.0(a) 0-20 0.14 100 110 90.9 80-120
Silver 0.28 0.048 141.5(a) 0-20 0.28 2.5 2.75 80.9 80-120
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc 139 111 22.4*(b) 0-20 139 192 27.5 193.0(d) 80-120
Associated samples MP31219: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) RPD acceptable due to low duplicate and sample concentrations.
(b) High RPD due to possible sample non-homogeneity.
(c) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
(d) Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery
information.
_________________________________________________________________________________________________________
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
QC Batch ID: MP31219 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 11/28/16
FA38945-1 Spikelot MSD QC
Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum anr
Antimony 0.96 9.7 28.3 30.9N(a) 0.0 20
Arsenic anr
Barium anr
Beryllium 0.13 3.0 2.83 101.5 3.4 20
Cadmium 0.092 2.8 2.83 95.8 3.5 20
Calcium anr
Chromium 15.4 24.7 11.3 82.2 10.2 20
Cobalt anr
Copper 119 136 14.1 120.2(b) 13.3 20
Iron anr
Lead 179 187 28.3 28.3 (b) 14.9 20
Magnesium anr
Manganese 85.6 108 28.3 79.2N(a) 26.5 (c) 20
Molybdenum
Nickel 5.2 32.1 28.3 95.1 3.5 20
Potassium anr
Selenium 0.14 102 113 90.0 2.0 20
Silver 0.28 2.6 2.83 82.0 3.9 20
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc 139 147 28.3 28.3 (b) 26.5 (c) 20
Associated samples MP31219: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
(b) Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery
information.
(c) High RPD due to possible sample non-homogeneity.
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SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
QC Batch ID: MP31219 Methods: SW846 6010C
Matrix Type: SOLID Units: mg/kg
Prep Date: 11/28/16
BSP Spikelot QC
Metal Result MPFLICP2 % Rec Limits
Aluminum anr
Antimony 26.9 25 107.6 80-120
Arsenic anr
Barium anr
Beryllium 2.8 2.5 112.0 80-120
Cadmium 2.7 2.5 108.0 80-120
Calcium anr
Chromium 11.1 10 111.0 80-120
Cobalt anr
Copper 13.8 12.5 110.4 80-120
Iron anr
Lead 26.4 25 105.6 80-120
Magnesium anr
Manganese 28.1 25 112.4 80-120
Molybdenum
Nickel 27.7 25 110.8 80-120
Potassium anr
Selenium 105 100 105.0 80-120
Silver 2.5 2.5 100.0 80-120
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc 27.6 25 110.4 80-120
Associated samples MP31219: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
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SERIAL DILUTION RESULTS SUMMARY
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
QC Batch ID: MP31219 Methods: SW846 6010C
Matrix Type: SOLID Units: ug/l
Prep Date: 11/28/16
FA38945-1 QC
Metal Original SDL 1:5 %DIF Limits
Aluminum anr
Antimony 18.8 14.5 22.9 (a) 0-10
Arsenic anr
Barium anr
Beryllium 2.60 2.00 23.1 (a) 0-10
Cadmium 1.80 0.00 100.0(a) 0-10
Calcium anr
Chromium 302 325 7.8 0-10
Cobalt anr
Copper 2340 2370 1.3 0-10
Iron anr
Lead 3520 3490 0.9 0-10
Magnesium anr
Manganese 1680 1840 9.4 0-10
Molybdenum
Nickel 102 110 7.8 0-10
Potassium anr
Selenium 2.70 0.00 100.0(a) 0-10
Silver 5.50 5.30 3.6 0-10
Sodium anr
Strontium
Thallium anr
Tin
Titanium
Vanadium anr
Zinc 2740 3120 14.1*(b) 0-10
Associated samples MP31219: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
(b) Serial dilution indicates possible matrix interference.
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POST DIGESTATE SPIKE SUMMARY
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
QC Batch ID: MP31219 Methods: SW846 6010C
Matrix Type: SOLID Units: ug/l
Prep Date: 11/28/16
Sample Final FA38945-1 PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony 9.8 10 18.8 18.424 121.2 0.2 5 100 102.8 80-120
Arsenic
Barium
Beryllium 9.8 10 2.6 2.548 52.8 0.2 2.5 50 100.5 80-120
Cadmium 9.8 10 1.8 1.764 50.8 0.2 2.5 50 98.1 80-120
Calcium
Chromium 9.8 10 301.8 295.764 344.8 0.2 2.5 50 98.1 80-120
Cobalt
Copper 9.8 10 2344 2297.12 2408 0.2 5 100 110.9 80-120
Iron
Lead 9.8 10 3517 3446.66 3500 0.2 2.5 50 106.7 80-120
Magnesium
Manganese 9.8 10 1680 1646.4 1684 0.2 2.5 50 75.2*(a) 80-120
Molybdenum
Nickel 9.8 10 102.1 100.058 197.6 0.2 5 100 97.5 80-120
Potassium
Selenium 9.8 10 2.7 2.646 96.6 0.2 5 100 94.0 80-120
Silver 9.8 10 5.5 5.39 50.3 0.2 2.5 50 89.8 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc 9.8 10 2737 2682.26 2922 0.2 12.5 250 95.9 80-120
Associated samples MP31219: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(**) Corr. sample result = Raw * (sample volume / final volume)
(anr) Analyte not requested
(a) Spike recovery indicates matrix interference and/or outside control limits due to high level in
sample relative to spike amount.
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SGS Accutest
General Chemistry
QC Data Summaries
Includes the following where applicable:
• Method Blank and Blank Spike Summaries
• Duplicate Summaries
• Matrix Spike Summaries
Southeast
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METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
MB Spike BSP BSP QC
Analyte Batch ID RL Result Units Amount Result %Recov Limits
Chromium, Hexavalent GN73241 2.0 0.0 mg/kg 20.0 17.9 89.6 75-125%
Associated Samples:
Batch GN73241: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
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DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
Chromium, Hexavalent GN73241 FA38946-1 mg/kg 1.5 1.2 22.1(a) 0-20%
Solids, Percent GN73194 FA38946-4 % 79.8 79.6 0.3 0-5%
Associated Samples:
Batch GN73194: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
Batch GN73241: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
(*) Outside of QC limits
(a) RPD acceptable due to low duplicate and sample concentrations.
__________________________________________________________________________________________________________________________
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MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA38946
Account: HHNCC - Hart & Hickman
Project: Belmont Dyers Site; Belmont, NC
QC Original Spike MS QC
Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Chromium, Hexavalent GN73241 FA38946-1 mg/kg 1.5 719.3 857 119.0 75-125%
Chromium, Hexavalent GN73241 FA38946-1 mg/kg 1.5 25.34 22.7 83.9 75-125%
Associated Samples:
Batch GN73241: FA38946-1, FA38946-2, FA38946-3, FA38946-4, FA38946-5, FA38946-6
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
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Appendix C

Cumulative Risk Calculation Output for SB-2
Output generated 06FEB2017:12:39:21
Site-specific 1
Resident Equation Inputs for Soil
Output generated 06FEB2017:12:39:21
Site-specific 1
Resident Equation Inputs for Soil
Variable Value
THQ (target hazard quotient) unitless 1
TR (target risk) unitless 1.0E-6
LT (lifetime) year 70
ETres (exposure time) hour 24
ETres-c (child exposure time) hour 24
ETres-a (adult exposure time) hour 24
ET0-2 (mutagenic exposure time) hour 24
ET2-6 (mutagenic exposure time) hour 24
ET6-16 (mutagenic exposure time) hour 24
ET16-26 (mutagenic exposure time) hour 24
EDres (exposure duration) year 26
EDres-c (exposure duration - child) year 6
EDres-a (exposure duration - adult) year 20
ED0-2 (mutagenic exposure duration) year 2
ED2-6 (mutagenic exposure duration) year 4
ED6-16 (mutagenic exposure duration) year 10
ED16-26 (mutagenic exposure duration) year 10
BWres-c (body weight - child) kg 15
BWres-a (body weight - adult) kg 80
BW0-2 (mutagenic body weight) kg 15
BW2-6 (mutagenic body weight) kg 15
BW6-16 (mutagenic body weight) kg 80
BW16-26 (mutagenic body weight) kg 80
SAres-c (skin surface area - child) cm 2/day 2373
SAres-a (skin surface area - adult) cm 2/day 6032
SA0-2 (mutagenic skin surface area) cm 2/day 2373
SA2-6 (mutagenic skin surface area) cm 2/day 2373
SA6-16 (mutagenic skin surface area) cm 2/day 6032
SA16-26 (mutagenic skin surface area) cm 2/day 6032
EFres (exposure frequency) day/year 350
EFres-c (exposure frequency - child) day/year 350
EFres-a (exposure frequency - adult) day/year 350
EF0-2 (mutagenic exposure frequency) day/year 350
Output generated 06FEB2017:12:39:21
Site-specific 2
Resident Equation Inputs for Soil
Variable Value
EF2-6 (mutagenic exposure frequency) day/year 350
EF6-16 (mutagenic exposure frequency) day/year 350
EF16-26 (mutagenic exposure frequency) day/year 350
IFSres-adj (age-adjusted soil ingestion factor) mg/kg 36750
IFSMres-adj (mutagenic age-adjusted soil ingestion factor) mg/kg 166833.33
IRSres-c (soil intake rate - child) mg/day 200
IRSres-a (soil intake rate - adult) mg/day 100
IRS0-2 (mutagenic soil intake rate) mg/day 200
IRS2-6 (mutagenic soil intake rate) mg/day 200
IRS6-16 (mutagenic soil intake rate) mg/day 100
IRS16-26 (mutagenic soil intake rate) mg/day 100
AFres-a (skin adherence factor - adult) mg/cm 2 0.07
AFres-c (skin adherence factor - child) mg/cm 2 0.2
AF0-2 (mutagenic skin adherence factor) mg/cm 2 0.2
AF2-6 (mutagenic skin adherence factor) mg/cm 2 0.2
AF6-16 (mutagenic skin adherence factor) mg/cm 2 0.07
AF16-26 (mutagenic skin adherence factor) mg/cm 2 0.07
DFSres-adj (age-adjusted soil dermal factor) mg/kg 103390
DFSMres-adj (mutagenic age-adjusted soil dermal factor) mg/kg 428260
CityPEF (Climate Zone) Selection Default
As (acres).5
Q/Cwp (inverse of the ratio of the geometric mean air concentration to the emission flu 93.77
PEF (particulate emission factor) m 3/kg 1359344438
A (PEF Dispersion Constant)16.2302
B (PEF Dispersion Constant)18.7762
C (PEF Dispersion Constant)216.108
V (fraction of vegetative cover) unitless 0.5
Um (mean annual wind speed) m/s 4.69
Ut (equivalent threshold value)11.32
F(x) (function dependant on U m/Ut) unitless 0.194
CityVF (Climate Zone) Selection Default
As (acres).5
Q/Cvol(inverse of the ratio of the geometric mean air concentration to the emission flu 68.18
Output generated 06FEB2017:12:39:21
Site-specific 3
Resident Equation Inputs for Soil
Variable Value
foc (fraction organic carbon in soil) g/g 0.006
pb (dry soil bulk density) g/cm 3 1.5
ps (soil particle density) g/cm 3 2.65
n (total soil porosity) L pore/Lsoil 0.43396
a (air-filled soil porosity) L air/Lsoil 0.28396
w (water-filled soil porosity) L water /Lsoil 0.15
T (exposure interval) s 819936000
A (VF Dispersion Constant)11.911
B (VF Dispersion Constant)18.4385
C (VF Dispersion Constant)209.7845
CityVF mass-loading (Climate Zone) Selection Default
VFml (volitization factor - mass-limit) m 3/kg .
Q/Cvol (inverse of the ratio of the geometric mean air concentration to the emission fl 68.18365
As (acres).5
T (exposure interval) yr 26
ds (depth of source) m .
pb (dry soil bulk density) g/cm 3 1.5
A (VF Dispersion Constant - Mass Limit)11.911
B (VF Dispersion Constant - Mass Limit)18.4385
C (VF Dispersion Constant - Mass Limit)209.7845
Output generated 06FEB2017:12:39:21
Site-specific 4
Resident Screening Levels (RSL) for SoilKey: I = IRIS; P = PPRTV; D = DWSHA; O = OPP; A = ATSDR; C = Cal EPA; X = APPENDIX PPRTV SCREEN (See FAQ #27); H = HEAST; F = See FAQ; J = New Jersey; E = see user
guide Section 2.3.5; L = see user guide on lead; M = mutagen; S = see user guide Section 5; V = volatile; R = RBA applied (See User Guide for Arsenic notice) ; c = cancer;
n = noncancer; * = where: n SL < 100X c SL; ** = where n SL < 10X c SL; SSL values are based on DAF=1; m = Concentration may exceed ceiling limit (See User Guide);
s = Concentration may exceed Csat (See User Guide)
Output generated 06FEB2017:12:39:21
Site-specific 4
Resident Screening Levels (RSL) for SoilKey: I = IRIS; P = PPRTV; D = DWSHA; O = OPP; A = ATSDR; C = Cal EPA; X = APPENDIX PPRTV SCREEN (See FAQ #27); H = HEAST; F = See FAQ; J = New Jersey; E = see user
guide Section 2.3.5; L = see user guide on lead; M = mutagen; S = see user guide Section 5; V = volatile; R = RBA applied (See User Guide for Arsenic notice) ; c = cancer;
n = noncancer; * = where: n SL < 100X c SL; ** = where n SL < 10X c SL; SSL values are based on DAF=1; m = Concentration may exceed ceiling limit (See User Guide);
s = Concentration may exceed Csat (See User Guide)
Chemical
CAS
Number Mutagen?VOC?
Ingestion
SF
(mg/kg-day)-1
SFO
Ref
Inhalation
Unit
Risk
(ug/m 3)-1
IUR
Ref
Chronic
RfD
(mg/kg-day)
Chronic
RfD
Ref
Chronic
RfC
(mg/m 3)
Chronic
RfC
Ref GIABS ABS RBA
Acenaphthylene 208-96-8 No Yes ----1 0.13 1
Anthracene 120-12-7 No Yes --3.00E-01 IR -1 0.13 1
Benz[a]anthracene 56-55-3 Yes Yes 1.00E-01 W 6.00E-05 W --1 0.13 1
Benzo[a]pyrene 50-32-8 Yes No 1.00E+00 I 6.00E-04 I 3.00E-04 IR 2.00E-06 IR 1 0.13 1
Benzo[b]fluoranthene 205-99-2 Yes No 1.00E-01 W 6.00E-05 W --1 0.13 1
Benzo[g,h,i]perylene 191-24-2 No No ----1 0.13 1
Benzo[k]fluoranthene 207-08-9 Yes No 1.00E-02 W 6.00E-06 W --1 0.13 1
Chromium(III), Insoluble Salts 16065-83-1 No No --1.50E+00 IR -0.013 -1
Chrysene 218-01-9 Yes No 1.00E-03 W 6.00E-07 W --1 0.13 1
Copper 7440-50-8 No No --4.00E-02 HE -1 -1
Dibenz[a,h]anthracene 53-70-3 Yes No 1.00E+00 W 6.00E-04 W --1 0.13 1
Fluoranthene 206-44-0 No No --4.00E-02 IR -1 0.13 1
Indeno[1,2,3-cd]pyrene 193-39-5 Yes No 1.00E-01 W 6.00E-05 W --1 0.13 1
Phenanthrene 85-01-8 No Yes ----1 0.13 1
Pyrene 129-00-0 No Yes --3.00E-02 IR -1 0.13 1
Zinc and Compounds 7440-66-6 No No --3.00E-01 IR -1 -1
Output generated 06FEB2017:12:39:21
Site-specific 5
Resident Screening Levels (RSL) for SoilKey: I = IRIS; P = PPRTV; D = DWSHA; O = OPP; A = ATSDR; C = Cal EPA; X = APPENDIX PPRTV SCREEN (See FAQ #27); H = HEAST; F = See FAQ; J = New Jersey; E = see user
guide Section 2.3.5; L = see user guide on lead; M = mutagen; S = see user guide Section 5; V = volatile; R = RBA applied (See User Guide for Arsenic notice) ; c = cancer;
n = noncancer; * = where: n SL < 100X c SL; ** = where n SL < 10X c SL; SSL values are based on DAF=1; m = Concentration may exceed ceiling limit (See User Guide);
s = Concentration may exceed Csat (See User Guide)
Chemical
Volatilization
Factor
(m3/kg)
Henry's
Law
Constant
(unitless)
S
(mg/L)
Koc(cm3/g)
Soil
Saturation
Concentration
(mg/kg)
Particulate
Emission
Factor
(m3/kg)
Ingestion
SL
TR=1.0E-6
(mg/kg)
Dermal
SL
TR=1.0E-6
(mg/kg)
Inhalation
SL
TR=1.0E-6
(mg/kg)
Carcinogenic
SL
TR=1.0E-6
(mg/kg)
Ingestion
SL
Child
THQ=1
(mg/kg)
Acenaphthylene 1.89E+05 4.66E-03 1.61E+01 5.03E+03 -1.36E+09 -----
Anthracene 5.23E+05 2.27E-03 4.34E-02 1.64E+04 -1.36E+09 ----2.35E+04
Benz[a]anthracene 4.41E+06 4.91E-04 9.40E-03 1.77E+05 -1.36E+09 1.53E+00 4.59E+00 7.43E+01 1.13E+00 -
Benzo[a]pyrene -1.87E-05 1.62E-03 5.87E+05 -1.36E+09 1.53E-01 4.59E-01 2.30E+03 1.15E-01 2.35E+01
Benzo[b]fluoranthene -2.69E-05 1.50E-03 5.99E+05 -1.36E+09 1.53E+00 4.59E+00 2.30E+04 1.15E+00 -
Benzo[g,h,i]perylene -1.35E-05 2.60E-04 1.95E+06 -1.36E+09 -----
Benzo[k]fluoranthene -2.39E-05 8.00E-04 5.87E+05 -1.36E+09 1.53E+01 4.59E+01 2.30E+05 1.15E+01 -
Chromium(III), Insoluble Salts -----1.36E+09 ----1.17E+05
Chrysene -2.14E-04 2.00E-03 1.81E+05 -1.36E+09 1.53E+02 4.59E+02 2.30E+06 1.15E+02 -
Copper -----1.36E+09 ----3.13E+03
Dibenz[a,h]anthracene -5.76E-06 2.49E-03 1.91E+06 -1.36E+09 1.53E-01 4.59E-01 2.30E+03 1.15E-01 -
Fluoranthene -3.62E-04 2.60E-01 5.55E+04 -1.36E+09 ----3.13E+03
Indeno[1,2,3-cd]pyrene -1.42E-05 1.90E-04 1.95E+06 -1.36E+09 1.53E+00 4.59E+00 2.30E+04 1.15E+00 -
Phenanthrene 6.43E+05 1.73E-03 1.15E+00 1.67E+04 -1.36E+09 -----
Pyrene 2.38E+06 4.87E-04 1.35E-01 5.43E+04 -1.36E+09 ----2.35E+03
Zinc and Compounds -----1.36E+09 ----2.35E+04
Output generated 06FEB2017:12:39:21
Site-specific 6
Resident Screening Levels (RSL) for SoilKey: I = IRIS; P = PPRTV; D = DWSHA; O = OPP; A = ATSDR; C = Cal EPA; X = APPENDIX PPRTV SCREEN (See FAQ #27); H = HEAST; F = See FAQ; J = New Jersey; E = see user
guide Section 2.3.5; L = see user guide on lead; M = mutagen; S = see user guide Section 5; V = volatile; R = RBA applied (See User Guide for Arsenic notice) ; c = cancer;
n = noncancer; * = where: n SL < 100X c SL; ** = where n SL < 10X c SL; SSL values are based on DAF=1; m = Concentration may exceed ceiling limit (See User Guide);
s = Concentration may exceed Csat (See User Guide)
Chemical
Dermal
SL
Child
THQ=1
(mg/kg)
Inhalation
SL
Child
THQ=1
(mg/kg)
Noncarcinogenic
SL
Child
THI=1
(mg/kg)
Ingestion
SL
Adult
THQ=1
(mg/kg)
Dermal
SL
Adult
THQ=1
(mg/kg)
Inhalation
SL
Adult
THQ=1
(mg/kg)
Noncarcinogenic
SL
Adult
THI=1
(mg/kg)
Screening
Level
(mg/kg)
Acenaphthylene -------
Anthracene 7.61E+04 -1.79E+04 2.50E+05 4.56E+05 -1.62E+05 1.79E+04 nc
Benz[a]anthracene -------1.13E+00 ca
Benzo[a]pyrene 7.61E+01 2.84E+03 1.78E+01 2.50E+02 4.56E+02 2.84E+03 1.53E+02 1.15E-01 ca
Benzo[b]fluoranthene -------1.15E+00 ca
Benzo[g,h,i]perylene -------
Benzo[k]fluoranthene -------1.15E+01 ca
Chromium(III), Insoluble Salts --1.17E+05 1.25E+06 --1.25E+06 1.17E+05 max
Chrysene -------1.15E+02 ca
Copper --3.13E+03 3.34E+04 --3.34E+04 3.13E+03 nc
Dibenz[a,h]anthracene -------1.15E-01 ca
Fluoranthene 1.01E+04 -2.39E+03 3.34E+04 6.08E+04 -2.15E+04 2.39E+03 nc
Indeno[1,2,3-cd]pyrene -------1.15E+00 ca
Phenanthrene -------
Pyrene 7.61E+03 -1.79E+03 2.50E+04 4.56E+04 -1.62E+04 1.79E+03 nc
Zinc and Compounds --2.35E+04 2.50E+05 --2.50E+05 2.35E+04 nc
Output generated 06FEB2017:12:39:21
Site-specific 7
Resident Risk for Soil
Output generated 06FEB2017:12:39:21
Site-specific 7
Resident Risk for Soil
Chemical
Ingestion
SF
(mg/kg-day)-1
SFO
Ref
Inhalation
Unit
Risk
(ug/m3)-1
IUR
Ref
Chronic
RfD
(mg/kg-day)
Chronic
RfD
Ref
Chronic
RfC
(mg/m 3)
Chronic
RfC
Ref GIABS ABS RBA
Volatilization
Factor
(m3/kg)
Henry's
Law
Constant
(unitless)
Acenaphthylene ----1 0.13 1 1.89E+05 4.66E-03
Anthracene --3.00E-01 IR -1 0.13 1 5.23E+05 2.27E-03
Benz[a]anthracene 1.00E-01 W 6.00E-05 W --1 0.13 1 4.41E+06 4.91E-04
Benzo[a]pyrene 1.00E+00 I 6.00E-04 I 3.00E-04 IR 2.00E-06 IR 1 0.13 1 -1.87E-05
Benzo[b]fluoranthene 1.00E-01 W 6.00E-05 W --1 0.13 1 -2.69E-05
Benzo[g,h,i]perylene ----1 0.13 1 -1.35E-05
Benzo[k]fluoranthene 1.00E-02 W 6.00E-06 W --1 0.13 1 -2.39E-05
Chromium(III), Insoluble Salts --1.50E+00 IR -0.013 -1 --
Chrysene 1.00E-03 W 6.00E-07 W --1 0.13 1 -2.14E-04
Copper --4.00E-02 HE -1 -1 --
Dibenz[a,h]anthracene 1.00E+00 W 6.00E-04 W --1 0.13 1 -5.76E-06
Fluoranthene --4.00E-02 IR -1 0.13 1 -3.62E-04
Indeno[1,2,3-cd]pyrene 1.00E-01 W 6.00E-05 W --1 0.13 1 -1.42E-05
Phenanthrene ----1 0.13 1 6.43E+05 1.73E-03
Pyrene --3.00E-02 IR -1 0.13 1 2.38E+06 4.87E-04
Zinc and Compounds --3.00E-01 IR -1 -1 --
*Total Risk/HI ---------
Output generated 06FEB2017:12:39:21
Site-specific 8
Resident Risk for Soil
Chemical
S
(mg/L)
Koc(cm3/g)
Soil
Saturation
Concentration
(mg/kg)
Particulate
Emission
Factor
(m3/kg)
Concentration
(mg/kg)
Ingestion
Risk
Dermal
Risk
Inhalation
Risk
Carcinogenic
Risk
Ingestion
Child
HQ
Acenaphthylene 1.61E+01 5.03E+03 -1.36E+09 1.75E-01 -----
Anthracene 4.34E-02 1.64E+04 -1.36E+09 2.09E-01 ----8.91E-06
Benz[a]anthracene 9.40E-03 1.77E+05 -1.36E+09 6.10E-01 3.98E-07 1.33E-07 8.21E-09 5.39E-07 -
Benzo[a]pyrene 1.62E-03 5.87E+05 -1.36E+09 6.22E-01 4.06E-06 1.36E-06 2.71E-10 5.42E-06 2.65E-02
Benzo[b]fluoranthene 1.50E-03 5.99E+05 -1.36E+09 5.67E-01 3.70E-07 1.24E-07 2.47E-11 4.94E-07 -
Benzo[g,h,i]perylene 2.60E-04 1.95E+06 -1.36E+09 4.93E-01 -----
Benzo[k]fluoranthene 8.00E-04 5.87E+05 -1.36E+09 5.87E-01 3.83E-08 1.28E-08 2.56E-12 5.11E-08 -
Chromium(III), Insoluble Salts ---1.36E+09 8.50E+00 ----7.25E-05
Chrysene 2.00E-03 1.81E+05 -1.36E+09 6.29E-01 4.11E-09 1.37E-09 2.74E-13 5.48E-09 -
Copper ---1.36E+09 8.00E+01 ----2.56E-02
Dibenz[a,h]anthracene 2.49E-03 1.91E+06 -1.36E+09 1.11E-01 7.25E-07 2.42E-07 4.83E-11 9.67E-07 -
Fluoranthene 2.60E-01 5.55E+04 -1.36E+09 7.79E-01 ----2.49E-04
Indeno[1,2,3-cd]pyrene 1.90E-04 1.95E+06 -1.36E+09 5.34E-01 3.49E-07 1.16E-07 2.32E-11 4.65E-07 -
Phenanthrene 1.15E+00 1.67E+04 -1.36E+09 2.44E-01 -----
Pyrene 1.35E-01 5.43E+04 -1.36E+09 1.02E+00 ----4.35E-04
Zinc and Compounds ---1.36E+09 3.50E+01 ----1.49E-03
*Total Risk/HI -----5.95E-06 1.98E-06 8.58E-09 7.94E-06 5.43E-02
Output generated 06FEB2017:12:39:21
Site-specific 9
Resident Risk for Soil
Chemical
Dermal
Child
HQ
Inhalation
Child
HQ
Noncarcinogenic
Child
HI
Ingestion
Adult
HQ
Dermal
Adult
HQ
Inhalation
Adult
HQ
Noncarcinogenic
Adult
HI
Acenaphthylene -------
Anthracene 2.75E-06 -1.17E-05 8.35E-07 4.58E-07 -1.29E-06
Benz[a]anthracene -------
Benzo[a]pyrene 8.18E-03 2.19E-04 3.49E-02 2.49E-03 1.36E-03 2.19E-04 4.07E-03
Benzo[b]fluoranthene -------
Benzo[g,h,i]perylene -------
Benzo[k]fluoranthene -------
Chromium(III), Insoluble Salts --7.25E-05 6.79E-06 --6.79E-06
Chrysene -------
Copper --2.56E-02 2.40E-03 --2.40E-03
Dibenz[a,h]anthracene -------
Fluoranthene 7.68E-05 -3.26E-04 2.33E-05 1.28E-05 -3.62E-05
Indeno[1,2,3-cd]pyrene -------
Phenanthrene -------
Pyrene 1.34E-04 -5.69E-04 4.08E-05 2.24E-05 -6.31E-05
Zinc and Compounds --1.49E-03 1.40E-04 --1.40E-04
*Total Risk/HI 8.39E-03 2.19E-04 6.29E-02 5.09E-03 1.40E-03 2.19E-04 6.71E-03