Carter Woodson_2015-01-23 FINAL soil report-OCR

SUMMARY REPORT OF SOIL SAMPLING FOR
EXPOSURE ASSESSMENT
CARTER G. WOODSON MIDDLE SCHOOL
420 GOLDFLOSS STREET
WINSTON SALEM, NORTH CAROLINA

Prepared For:

Ms. Ruth Hopkins
School Administrator
Carter G. Woodson School
420 Goldfloss Street
Winston-Salem, North Carolina 27127

Ms. Hazel M. Mack
President
Challeges of the Twenty-First Century, Inc.
420 Goldfloss Street
Winston-Salem, North Carolina 27127

Prepared By:

Mid-Atlantic Associates, Inc.
409 Rogers View Court
Raleigh, North Carolina 27610

January 29, 2015

SUMMARY REPORT OF SOIL SAMPLING FOR
EXPOSURE ASSESSMENT
CARTER G. WOODSON MIDDLE SCHOOL
420 GOLDFLOSS STREET
WINSTON SALEM, NORTH CAROLINA

January 29, 2015

Mid-Atlantic Project No. 000R2592.01

Prepared for: Prepared by:

Ms. Ruth Hopkins MID-ATLANTIC ASSOCIATES, INC.
School Administrator
Carter G. Woodson School
420 Goldfloss Street
Winston-Salem, North Carolina 27127
William Service
Ms. Hazel M. Mack Senior Environmental Toxicologist
President
Challenges of the Twenty-First Century, Inc.
420 Goldfloss Street
Winston-Salem, North Carolina 27127
Daniel H. Nielsen, P.E.
Principal Engineer

TABLE OF CONTENTS

1.0 SUMMARY ............................................................................................................ 1

2.0 PROJECT INFORMATION ................................................................................... 1

3.0 METHODS ............................................................................................................ 2
3.1 Soil Sampling ..................................................................................................... 2

4.0 RESULTS .............................................................................................................. 3

5.0 DISCUSSION/CONCLUSIONS ............................................................................. 4

DRAWINGS

Drawing 1 – Topographic Site Map
Drawing 2 – Soil Sample Location Map

TABLES

Table 1 – Summary of Soil Sampling Results
Table 2 – Soil Sampling Test Results for Background Samples

APPENDIX

Laboratory Results and Chain-of-Custody Form

1.0 SUMMARY

On July 24, 2014, Mid-Atlantic Associates, Inc. (Mid-Atlantic) conducted soil sampling on the
grounds of the Carter G. Woodson Middle School located at 420 Goldfloss Street in Winston
Salem, North Carolina. The objective of sampling was to determine whether surface soil
contaminants that may have resulted from historical operation of a textile mill and a circuit
board manufacturing facility on the property could create exposure risk for students and other
occupants of the property.

A second sampling event was conducted on December 30, 2014 to provide additional data
regarding background (naturally occurring) arsenic concentrations in undisturbed soil.

There was no soil contamination identified in the soil samples collected.

There were no volatile organic compounds identified in the samples at concentrations above
the laboratory reporting limit, with the exception of two acetone detections that are assumed to
be laboratory artifacts. Detected acetone concentrations were less than 0.001 percent of the
NC Department of Environment and Natural Resources residential “Soil Remedial Goals”
(SRG’s).

Inorganic compounds (metals) were detected in surface soil samples at concentrations that are
typical for naturally occurring trace metals in Piedmont NC soils. Arsenic concentrations in four
of six samples exceeded the corresponding SRG, however, none of the samples exceeded the
site mean background concentration for arsenic in soil. None of the remaining inorganic
analytes exceeded the corresponding SRG.

2.0 PROJECT INFORMATION

Elevated levels of chemicals were recently discovered in groundwater on the grounds of the
Carter G. Woodson Middle School, located at 420 Goldfloss Street in Winston Salem, North
Carolina (Parcel 4). Phase I assessments conducted for the property determined that Arista
Cotton Mill operated on the site from 1895 to 1969. From 1970 until approximately 1988,
Western Electric (AT&T) operated a circuit board manufacturing facility on the site. A motor
freight facility is reported to have operated at the site of the Woodson Elementary School and
High School located at 427 Goldfloss Street (Parcel 3). A topographic site map is provided in
Drawing 1, attached.

In two environmental assessments that were completed for the Woodson Middle School
property; a “Phase II Environmental Site Assessment” conducted by Hart & Hickman, dated
May 16, 2014, and a “Limited Phase II Environmental Site Assessment” conducted by the EI
Group, Inc., dated June 13, 2014, chlorinated solvents were discovered in groundwater at
concentrations that exceed NC Department of Environment and Natural Resources (NCDENR)
2L Groundwater Quality Standards (NC 2L Standards). In addition, groundwater
concentrations of tetrachloroethylene (PCE), and trichloroethylene (TCE) also exceeded
Summary Report of Soil Sampling for January 29, 2015
Exposure Assessment Page 2
Carter G. Woodson Middle School
Winston-Salem, North Carolina

residential vapor intrusion screening levels established by the NCDENR, Division of Waste
Management (NCDWM). Shallow soil sampling for volatile organic compounds (VOCs) was
conducted on the property in the Phase II Environmental Site Assessment conducted by Hart
& Hickman. VOCs were not detected in the soil during that sampling event.

Indoor air sampling was conducted in the Middle School building by Mid-Atlantic on July 11,
2014, and December 30, 2014. PCE, TCE and trichlorofluoromethane were analyzed as
constituents of concern (COCs). There were no exceedances of residential indoor air
screening levels for the COCs in the collected air samples.

In the Hart & Hickman Phase II Assessment, groundwater and soil sampling was conducted on
Parcel 3 for volatile and semi-volatile organic compounds in the vicinity of the former motor
freight facility. No groundwater contaminants were detected in concentrations that exceeded
NC 2L standards and no contaminants were detected above the laboratory reporting limit in
the soil samples.

Surface water sampling was conducted in the EI, Inc. Phase II Assessment along Parkway
Branch that runs along the east and south border of Parcel 4. The results of that sampling
indicated tetrachloroethylene was detected at concentrations that exceed North Carolina 2B
Surface Water Standards for Human Health.

Soil sampling locations for EI, Inc. Phase II and the Hart & Hickman Phase II are depicted on
Drawing 2.

3.0 METHODS

3.1 Soil Sampling

Soil samples were collected on the Woodson Middle School grounds (Parcel 4) on July 24,
2014 for analysis of volatile organic compounds and select inorganic compounds (metals).
Samples were collected from surface soil at a depths from zero to one foot using a hand
auger. Sample locations are depicted in Drawing 2.

Sample locations were selected after consultation with school administrators regarding high
traffic areas on school grounds where children were most likely to have contact with soil.

Summary Report of Soil Sampling for January 29, 2015
Exposure Assessment Page 3
Carter G. Woodson Middle School
Winston-Salem, North Carolina

Six VOC samples were collected and analyzed by EPA Method 8260. Six composite soil
samples were collected and analyzed for five RCRA1 metals and hexavalent chromium using
EPA Method 2540G. The selected inorganic analytes are compounds that may have been
used in former industrial operations at the site, including arsenic, hexavalent and total
chromium, copper, and cadmium (textile dyeing); and lead (circuit board manufacturing and
textile dyeing). One soil sample was collected in the wooded area to the west of the current
athletic field for background comparison purposes. Four aliquots obtained within 50 feet of the
sample point were collected for each composite sample.

An attempt was made to collect surface water samples from Parkway Branch. However,
because the creek bed was dry on the date of sampling, no surface water samples were
obtained.

Soil sampling was planned for the Elementary School playground on Parcel 3. The playground
surface is a non-native mulch/cushioning material that covers a paved surface. Consequently,
soil samples were not collected from the playground.

A second sampling event was conducted on December 30, 2014 to provide data with regard to
naturally occurring (background) concentrations of arsenic in soil. Six composite samples were
collected from the southwest wooded portion of the property where soil appears to be
undisturbed. Sample locations are depicted in Drawing 2.

4.0 RESULTS

Of the six VOC soil samples collected, two had no detections of VOCs above laboratory
reporting limits. Acetone was detected in four of the six samples at concentrations ranging
from 0.04 to 0.08 mg/kg. The IHSB SRG for acetone is 12,000 mg/kg.

All six soil samples had concentrations of metals that are within the expected range for trace
metals in North Carolina Piedmont soils2,3,4. Arsenic concentrations ranged from 0.31 to 3.5
mg/kg in the six sample collected in July, 2014. Four of the six arsenic samples exceeded the
IHSB SRG for residential environments (0.61mg/kg).

1 Resource Conservation and Recovery Act (RCRA)
2 United Sates Geological Survey. “Element Concentrations in Soils and Other Surficial Materials of the Conterminous
United States.” Professional Paper 1270. 1984.
3 North Carolina Department of Agriculture and Consumer Services. “Heavy Metals in North Carolina Soils;
Occurrence & Significance.” Revised September, 2008.
4 United Sates Environmental Protection Agency. “Hazardous Waste Land Treatment.” SW-874. April, 1983.
Summary Report of Soil Sampling for January 29, 2015
Exposure Assessment Page 4
Carter G. Woodson Middle School
Winston-Salem, North Carolina

Six background arsenic composite soil samples were collected on December 30, 2014. Those
six samples had concentrations of arsenic that ranged from 4.9 to 20 mg/kg, with a mean
concentration of 11.5 mg/kg.

5.0 DISCUSSION/CONCLUSIONS

Metals concentrations detected in soils samples were within the expected range for trace
metals in Piedmont soils. Arsenic, for example, is reported by the United States Geological
Survey with a mean concentration of 7.4 ppm (mg/kg) in native soils in the eastern United
States2. On page 19 of the same document, a graphic displays Piedmont North Carolina with
discreet native arsenic concentrations in the range of 0.65 to 41 ppm. The North Carolina
Department of Agriculture reports a state-wide average of 4.5 ppm3. The USEPA reports that
“In soils, the total arsenic concentration normally ranges from 1-50 ppm, though it does not
generally exceed 10 ppm.”4 The same report cites an average concentration of 5 ppm in soils.
Arsenic concentrations in soil samples collected at Woodson Middle School ranged from 0.31
to 3.5 ppm.

The mean concentration of arsenic in six background soil samples (11.5 mg/kg) collected in
December, 2014 is considerably higher than the concentrations detected in soil samples from
disturbed soils on the middle school grounds (range 0.31 to 3.5 mg/kg). This indicates that
reported arsenic concentrations in soils from the July sampling event are the result of naturally
occurring arsenic in soil.

DRAWINGS
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´
SOIL SAMPLE LOCATION MAPCARTER G. WOODSON SCHOOL420 & 437 GOLDFLOSS STREETWINSTON-SALEM, NORTH CAROLINA
DRAWN BY:
DRAFT CHECK BY:
ENGINEER CHECK BY:
APPROVED BY:
DATE: DECEMBER 30, 2014
JOB NO.: 000R2592.01
GIS NO.: 03G-2592.01-1 AS
DRAWING NO.: 2
REFERENCE: PARCEL BOUNDARY AND ROAD DATA FROM CITY OF WINSTON-SALEM AND FORSYTH COUNTY GIS. 2010 AERIAL IMAGERY FROM NC CGIA. MID-ATLANTIC FIELD NOTES.
150 0 15075 Feet
PARKWAY BRANCH
!.BACKGROUND INORGANIC SAMPLE DEC 2014
!.BACKGROUND INORGANIC SAMPLE JULY 2014
!>SOIL BORING / TEMPORARY MONITORING WELL FROM THE EI GROUP
!>SOIL BORING / TEMPORARY MONITORING WELL FROM HART & HICKMAN
!R INORGANIC COMPOSITE SAMPLE
!?VOLATILE ORGANIC COMPOUND SAMPLE
HYDROLOGIC FEATURE
PLAYGROUND AREA
SURROUNDING PROPERTY BOUNDARY
SUBJECT SITE PROPERTY BOUNDARY

TABLES
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APPENDIX

LABORATORY RESULTS AND
CHAIN-OF-CUSTODY FORM

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
August 5, 2014
William Service
Mid-Atlantic Associates, Inc. - Raleigh, NC
409 Rogers View Court
Raleigh, NC 27610
Project Location: Hillsborough, NC
Client Job Number:
Project Number: 2259200
Laboratory Work Order Number: 14G1210
Enclosed are results of analyses for samples received by the laboratory on July 25, 2014. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
Page 1 of 52
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 5
Sample Results 8
14G1210-01 8
14G1210-02 10
14G1210-03 13
14G1210-04 15
14G1210-05 18
14G1210-06 20
14G1210-07 23
14G1210-08 26
14G1210-09 28
14G1210-10 31
14G1210-11 33
Sample Preparation Information 35
QC Data 37
Volatile Organic Compounds by GC/MS 37
B101254 37
Metals Analyses (Total) 42
B101186 42
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 43
B101121 43
B101124 43
B101342 43
Flag/Qualifier Summary 44
Certifications 45
Page 2 of 52
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Table of Contents (continued)
Chain of Custody/Sample Receipt 48
Page 3 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
8/5/2014
Mid-Atlantic Associates, Inc. - Raleigh, NC
409 Rogers View Court
Raleigh, NC 27610
ATTN: William Service
2259200
14G1210
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Hillsborough, NC
IC-6 14G1210-01 Soil SM 2540G
SM2580 A
SW-846 6020A
SW-846 7196A
SW-846 9045C
VOC-5 14G1210-02 Soil SM 2540G
SW-846 8260B
IC-3 14G1210-03 Soil SM 2540G
SM2580 A
SW-846 6020A
SW-846 7196A
SW-846 9045C
VOC-2 14G1210-04 Soil SM 2540G
SW-846 8260B
IC-4 14G1210-05 Soil SM 2540G
SM2580 A
SW-846 6020A
SW-846 7196A
SW-846 9045C
VOC-4 14G1210-06 Soil SM 2540G
SW-846 8260B
VOC-1 14G1210-07 Soil SM 2540G
SW-846 8260B
IC-2 14G1210-08 Soil SM 2540G
SM2580 A
SW-846 6020A
SW-846 7196A
SW-846 9045C
VOC-3 14G1210-09 Soil SM 2540G
SW-846 8260B
IC-5 14G1210-10 Soil SM 2540G
SM2580 A
SW-846 6020A
SW-846 7196A
SW-846 9045C
BIC-1 14G1210-11 Soil SM 2540G
SM2580 A
SW-846 6020A
SW-846 7196A
SW-846 9045C
[TOC_1]Sample Summary[TOC]
Page 4 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
Page 5 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SW-846 6020A
Qualifications:
Matrix spike recovery outside of control limits. Possibility of sample matrix effects that lead to a high bias for reported result or
non-homogeneous sample aliquots cannot be eliminated.
Analyte & Samples(s) Qualified:
MS-11
Chromium
14G1210-01[IC-6], B101186-MS1
Duplicate relative percent difference (RPD) is a less useful indicator of sample precision for sample results that are <5 times the reporting
limit (RL).
Analyte & Samples(s) Qualified:
R-04
Cadmium
14G1210-01[IC-6], B101186-DUP1
SW-846 7196A
Qualifications:
Elevated method reporting limit due to intense color of sample
Analyte & Samples(s) Qualified:
W-06
Hexavalent Chromium
14G1210-01[IC-6], 14G1210-03[IC-3], 14G1210-05[IC-4], 14G1210-08[IC-2], 14G1210-10[IC-5], 14G1210-11[BIC-1]
SW-846 8260B
Qualifications:
Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is
associated with the reported value which is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
V-05
Naphthalene
14G1210-02[VOC-5], 14G1210-04[VOC-2], 14G1210-06[VOC-4], 14G1210-07[VOC-1], 14G1210-09[VOC-3], B101254-BLK1, B101254-BS1, B101254-BSD1
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported
result.
Analyte & Samples(s) Qualified:
V-16
1,4-Dioxane
14G1210-02[VOC-5], 14G1210-04[VOC-2], 14G1210-06[VOC-4], 14G1210-07[VOC-1], 14G1210-09[VOC-3], B101254-BLK1, B101254-BS1, B101254-BSD1
tert-Butyl Alcohol (TBA)
14G1210-02[VOC-5], 14G1210-04[VOC-2], 14G1210-06[VOC-4], 14G1210-07[VOC-1], 14G1210-09[VOC-3], B101254-BLK1, B101254-BS1, B101254-BSD1
Tetrahydrofuran
14G1210-02[VOC-5], 14G1210-04[VOC-2], 14G1210-06[VOC-4], 14G1210-07[VOC-1], 14G1210-09[VOC-3], B101254-BLK1, B101254-BS1, B101254-BSD1
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Acetone
B101254-BS1, B101254-BSD1
SW-846 9045C
Qualifications:
Sample received after recommended holding time was exceeded.
Analyte & Samples(s) Qualified:
H-03
pH
14G1210-01[IC-6], 14G1210-03[IC-3], 14G1210-05[IC-4], 14G1210-08[IC-2], 14G1210-10[IC-5], 14G1210-11[BIC-1], B101121-DUP1
Page 6 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Laboratory Manager
Page 7 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-01
Field Sample #: IC-6
Sample Matrix: Soil
Sampled: 7/24/2014 14:15
[TOC_2]14G1210-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
2.3 0.28 7/31/14 15:52 KSHmg/Kg dry0.068 7/28/14SW-846 6020A5Arsenic
27 6.9 7/31/14 15:52 KSHmg/Kg dry0.034 7/28/14SW-846 6020A5MS-11Chromium
21 6.9 7/31/14 15:52 KSHmg/Kg dry 7/28/14SW-846 6020A5Copper
18 2.8 7/31/14 15:52 KSHmg/Kg dry0.0049 7/28/14SW-846 6020A5Lead
0.014 0.53 7/31/14 15:52 KSHmg/Kg dry0.0032 7/28/14SW-846 6020A5R-04, JCadmium
[TOC_1]Sample Results[TOC]
Page 8 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-01
Field Sample #: IC-6
Sample Matrix: Soil
Sampled: 7/24/2014 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 0.86 7/31/14 14:20 LLmg/Kg dry0.47 7/30/14SW-846 7196A5W-06Hexavalent Chromium
110 7/26/14 17:15 ABHmV7/26/14SM2580 A1Oxidation/Reduction Potential
6.4 7/26/14 16:47 ABHpH Units 7/26/14SW-846 9045C1H-03pH @22°C
90.0 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 9 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-02
Field Sample #: VOC-5
Sample Matrix: Soil
Sampled: 7/24/2014 14:00
[TOC_2]14G1210-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.080 7/29/14 11:52 MFFmg/Kg dry0.019 7/29/14SW-846 8260B1Acetone
ND 0.0048 7/29/14 11:52 MFFmg/Kg dry0.0020 7/29/14SW-846 8260B1Acrylonitrile
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1Benzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1Bromobenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Bromochloromethane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00048 7/29/14SW-846 8260B1Bromodichloromethane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Bromoform
ND 0.0080 7/29/14 11:52 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1Bromomethane
ND 0.032 7/29/14 11:52 MFFmg/Kg dry0.014 7/29/14SW-846 8260B12-Butanone (MEK)
ND 0.032 7/29/14 11:52 MFFmg/Kg dry0.017 7/29/14SW-846 8260B1V-16tert-Butyl Alcohol (TBA)
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1n-Butylbenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1sec-Butylbenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1tert-Butylbenzene
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00048 7/29/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0048 7/29/14 11:52 MFFmg/Kg dry0.0027 7/29/14SW-846 8260B1Carbon Disulfide
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1Carbon Tetrachloride
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1Chlorobenzene
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1Chlorodibromomethane
ND 0.016 7/29/14 11:52 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B1Chloroethane
ND 0.0032 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1Chloroform
ND 0.0080 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1Chloromethane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B12-Chlorotoluene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B14-Chlorotoluene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00089 7/29/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00048 7/29/14SW-846 8260B1Dibromomethane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0032 7/29/14 11:52 MFFmg/Kg dry0.00097 7/29/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.016 7/29/14 11:52 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B11,1-Dichloroethane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B11,2-Dichloroethane
ND 0.0032 7/29/14 11:52 MFFmg/Kg dry0.00089 7/29/14SW-846 8260B11,1-Dichloroethylene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B11,2-Dichloropropane
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B11,3-Dichloropropane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B12,2-Dichloropropane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B11,1-Dichloropropene
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.016 7/29/14 11:52 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1Diethyl Ether
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-02
Field Sample #: VOC-5
Sample Matrix: Soil
Sampled: 7/24/2014 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00048 7/29/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.080 7/29/14 11:52 MFFmg/Kg dry0.046 7/29/14SW-846 8260B1V-161,4-Dioxane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1Ethylbenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1Hexachlorobutadiene
ND 0.016 7/29/14 11:52 MFFmg/Kg dry0.0088 7/29/14SW-846 8260B12-Hexanone (MBK)
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0032 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.016 7/29/14 11:52 MFFmg/Kg dry0.0057 7/29/14SW-846 8260B1Methylene Chloride
ND 0.016 7/29/14 11:52 MFFmg/Kg dry0.0061 7/29/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0032 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1V-05Naphthalene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1n-Propylbenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00048 7/29/14SW-846 8260B1Styrene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.00080 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1Tetrachloroethylene
ND 0.0080 7/29/14 11:52 MFFmg/Kg dry0.0018 7/29/14SW-846 8260B1V-16Tetrahydrofuran
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1Toluene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00048 7/29/14SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00097 7/29/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1Trichloroethylene
ND 0.0080 7/29/14 11:52 MFFmg/Kg dry0.00089 7/29/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00089 7/29/14SW-846 8260B11,2,3-Trichloropropane
ND 0.0080 7/29/14 11:52 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00048 7/29/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.0080 7/29/14 11:52 MFFmg/Kg dry0.00089 7/29/14SW-846 8260B1Vinyl Chloride
ND 0.0032 7/29/14 11:52 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1m+p Xylene
ND 0.0016 7/29/14 11:52 MFFmg/Kg dry0.00056 7/29/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.8 7/29/14 11:5270-130
Toluene-d8 100 7/29/14 11:5270-130
4-Bromofluorobenzene 98.5 7/29/14 11:5270-130
Page 11 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-02
Field Sample #: VOC-5
Sample Matrix: Soil
Sampled: 7/24/2014 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
93.7 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 12 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-03
Field Sample #: IC-3
Sample Matrix: Soil
Sampled: 7/24/2014 14:30
[TOC_2]14G1210-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.8 0.28 7/31/14 15:56 KSHmg/Kg dry0.069 7/28/14SW-846 6020A5Arsenic
60 7.0 7/31/14 15:56 KSHmg/Kg dry0.034 7/28/14SW-846 6020A5Chromium
28 7.0 7/31/14 15:56 KSHmg/Kg dry 7/28/14SW-846 6020A5Copper
26 2.8 7/31/14 15:56 KSHmg/Kg dry0.0050 7/28/14SW-846 6020A5Lead
0.043 0.53 7/31/14 15:56 KSHmg/Kg dry0.0032 7/28/14SW-846 6020A5JCadmium
Page 13 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-03
Field Sample #: IC-3
Sample Matrix: Soil
Sampled: 7/24/2014 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 0.88 7/31/14 14:20 LLmg/Kg dry0.48 7/30/14SW-846 7196A5W-06Hexavalent Chromium
140 7/26/14 17:15 ABHmV7/26/14SM2580 A1Oxidation/Reduction Potential
5.9 7/26/14 16:47 ABHpH Units 7/26/14SW-846 9045C1H-03pH @22°C
89.2 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 14 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-04
Field Sample #: VOC-2
Sample Matrix: Soil
Sampled: 7/24/2014 14:45
[TOC_2]14G1210-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.067 0.10 7/29/14 12:19 MFFmg/Kg dry0.024 7/29/14SW-846 8260B1JAcetone
ND 0.0061 7/29/14 12:19 MFFmg/Kg dry0.0025 7/29/14SW-846 8260B1Acrylonitrile
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1Benzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B1Bromobenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1Bromochloromethane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00061 7/29/14SW-846 8260B1Bromodichloromethane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1Bromoform
ND 0.010 7/29/14 12:19 MFFmg/Kg dry0.0017 7/29/14SW-846 8260B1Bromomethane
ND 0.040 7/29/14 12:19 MFFmg/Kg dry0.018 7/29/14SW-846 8260B12-Butanone (MEK)
ND 0.040 7/29/14 12:19 MFFmg/Kg dry0.021 7/29/14SW-846 8260B1V-16tert-Butyl Alcohol (TBA)
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1n-Butylbenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1sec-Butylbenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B1tert-Butylbenzene
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.00061 7/29/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0061 7/29/14 12:19 MFFmg/Kg dry0.0033 7/29/14SW-846 8260B1Carbon Disulfide
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B1Carbon Tetrachloride
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1Chlorobenzene
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1Chlorodibromomethane
ND 0.020 7/29/14 12:19 MFFmg/Kg dry0.0015 7/29/14SW-846 8260B1Chloroethane
ND 0.0040 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1Chloroform
ND 0.010 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B1Chloromethane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B12-Chlorotoluene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B14-Chlorotoluene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00061 7/29/14SW-846 8260B1Dibromomethane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0040 7/29/14 12:19 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.020 7/29/14 12:19 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B11,1-Dichloroethane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,2-Dichloroethane
ND 0.0040 7/29/14 12:19 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,1-Dichloroethylene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,2-Dichloropropane
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B11,3-Dichloropropane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B12,2-Dichloropropane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B11,1-Dichloropropene
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.020 7/29/14 12:19 MFFmg/Kg dry0.0018 7/29/14SW-846 8260B1Diethyl Ether
Page 15 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-04
Field Sample #: VOC-2
Sample Matrix: Soil
Sampled: 7/24/2014 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.00061 7/29/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.10 7/29/14 12:19 MFFmg/Kg dry0.058 7/29/14SW-846 8260B1V-161,4-Dioxane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B1Ethylbenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1Hexachlorobutadiene
ND 0.020 7/29/14 12:19 MFFmg/Kg dry0.011 7/29/14SW-846 8260B12-Hexanone (MBK)
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0040 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.020 7/29/14 12:19 MFFmg/Kg dry0.0072 7/29/14SW-846 8260B1Methylene Chloride
ND 0.020 7/29/14 12:19 MFFmg/Kg dry0.0077 7/29/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0040 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1V-05Naphthalene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1n-Propylbenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00061 7/29/14SW-846 8260B1Styrene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0010 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B1Tetrachloroethylene
ND 0.010 7/29/14 12:19 MFFmg/Kg dry0.0022 7/29/14SW-846 8260B1V-16Tetrahydrofuran
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B1Toluene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00061 7/29/14SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B1Trichloroethylene
ND 0.010 7/29/14 12:19 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,2,3-Trichloropropane
ND 0.010 7/29/14 12:19 MFFmg/Kg dry0.00091 7/29/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00081 7/29/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00061 7/29/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.010 7/29/14 12:19 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Vinyl Chloride
ND 0.0040 7/29/14 12:19 MFFmg/Kg dry0.0017 7/29/14SW-846 8260B1m+p Xylene
ND 0.0020 7/29/14 12:19 MFFmg/Kg dry0.00071 7/29/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.8 7/29/14 12:1970-130
Toluene-d8 96.2 7/29/14 12:1970-130
4-Bromofluorobenzene 91.5 7/29/14 12:1970-130
Page 16 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-04
Field Sample #: VOC-2
Sample Matrix: Soil
Sampled: 7/24/2014 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
87.5 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 17 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-05
Field Sample #: IC-4
Sample Matrix: Soil
Sampled: 7/24/2014 15:00
[TOC_2]14G1210-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.5 0.25 7/31/14 16:00 KSHmg/Kg dry0.061 7/28/14SW-846 6020A5Arsenic
19 6.1 7/31/14 16:00 KSHmg/Kg dry0.030 7/28/14SW-846 6020A5Chromium
10 6.1 7/31/14 16:00 KSHmg/Kg dry 7/28/14SW-846 6020A5Copper
13 2.5 7/31/14 16:00 KSHmg/Kg dry0.0044 7/28/14SW-846 6020A5Lead
0.036 0.47 7/31/14 16:00 KSHmg/Kg dry0.0028 7/28/14SW-846 6020A5JCadmium
Page 18 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-05
Field Sample #: IC-4
Sample Matrix: Soil
Sampled: 7/24/2014 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 0.33 7/31/14 14:20 LLmg/Kg dry0.18 7/30/14SW-846 7196A2W-06Hexavalent Chromium
140 7/26/14 17:15 ABHmV7/26/14SM2580 A1Oxidation/Reduction Potential
6.2 7/26/14 16:47 ABHpH Units 7/26/14SW-846 9045C1H-03pH @21.7°C
96.0 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 19 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-06
Field Sample #: VOC-4
Sample Matrix: Soil
Sampled: 7/24/2014 15:15
[TOC_2]14G1210-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.080 0.11 7/29/14 12:47 MFFmg/Kg dry0.027 7/29/14SW-846 8260B1JAcetone
ND 0.0069 7/29/14 12:47 MFFmg/Kg dry0.0029 7/29/14SW-846 8260B1Acrylonitrile
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1Benzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B1Bromobenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0016 7/29/14SW-846 8260B1Bromochloromethane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00069 7/29/14SW-846 8260B1Bromodichloromethane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0016 7/29/14SW-846 8260B1Bromoform
ND 0.011 7/29/14 12:47 MFFmg/Kg dry0.0020 7/29/14SW-846 8260B1Bromomethane
ND 0.046 7/29/14 12:47 MFFmg/Kg dry0.020 7/29/14SW-846 8260B12-Butanone (MEK)
ND 0.046 7/29/14 12:47 MFFmg/Kg dry0.024 7/29/14SW-846 8260B1V-16tert-Butyl Alcohol (TBA)
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1n-Butylbenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1sec-Butylbenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1tert-Butylbenzene
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.00069 7/29/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0069 7/29/14 12:47 MFFmg/Kg dry0.0038 7/29/14SW-846 8260B1Carbon Disulfide
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B1Carbon Tetrachloride
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1Chlorobenzene
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1Chlorodibromomethane
ND 0.023 7/29/14 12:47 MFFmg/Kg dry0.0017 7/29/14SW-846 8260B1Chloroethane
ND 0.0046 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1Chloroform
ND 0.011 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1Chloromethane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B12-Chlorotoluene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B14-Chlorotoluene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00069 7/29/14SW-846 8260B1Dibromomethane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0046 7/29/14 12:47 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.023 7/29/14 12:47 MFFmg/Kg dry0.0015 7/29/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B11,1-Dichloroethane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0015 7/29/14SW-846 8260B11,2-Dichloroethane
ND 0.0046 7/29/14 12:47 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,1-Dichloroethylene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0015 7/29/14SW-846 8260B11,2-Dichloropropane
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B11,3-Dichloropropane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B12,2-Dichloropropane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B11,1-Dichloropropene
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.023 7/29/14 12:47 MFFmg/Kg dry0.0021 7/29/14SW-846 8260B1Diethyl Ether
Page 20 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-06
Field Sample #: VOC-4
Sample Matrix: Soil
Sampled: 7/24/2014 15:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.00069 7/29/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.11 7/29/14 12:47 MFFmg/Kg dry0.066 7/29/14SW-846 8260B1V-161,4-Dioxane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B1Ethylbenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Hexachlorobutadiene
ND 0.023 7/29/14 12:47 MFFmg/Kg dry0.013 7/29/14SW-846 8260B12-Hexanone (MBK)
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0046 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.023 7/29/14 12:47 MFFmg/Kg dry0.0081 7/29/14SW-846 8260B1Methylene Chloride
ND 0.023 7/29/14 12:47 MFFmg/Kg dry0.0087 7/29/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0046 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1V-05Naphthalene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1n-Propylbenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00069 7/29/14SW-846 8260B1Styrene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0011 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0015 7/29/14SW-846 8260B1Tetrachloroethylene
ND 0.011 7/29/14 12:47 MFFmg/Kg dry0.0025 7/29/14SW-846 8260B1V-16Tetrahydrofuran
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B1Toluene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00069 7/29/14SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B1Trichloroethylene
ND 0.011 7/29/14 12:47 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,2,3-Trichloropropane
ND 0.011 7/29/14 12:47 MFFmg/Kg dry0.0010 7/29/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00092 7/29/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00069 7/29/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.011 7/29/14 12:47 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B1Vinyl Chloride
ND 0.0046 7/29/14 12:47 MFFmg/Kg dry0.0020 7/29/14SW-846 8260B1m+p Xylene
ND 0.0023 7/29/14 12:47 MFFmg/Kg dry0.00080 7/29/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.1 7/29/14 12:4770-130
Toluene-d8 100 7/29/14 12:4770-130
4-Bromofluorobenzene 94.8 7/29/14 12:4770-130
Page 21 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-06
Field Sample #: VOC-4
Sample Matrix: Soil
Sampled: 7/24/2014 15:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
92.1 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 22 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-07
Field Sample #: VOC-1
Sample Matrix: Soil
Sampled: 7/24/2014 15:45
[TOC_2]14G1210-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.040 0.11 7/29/14 13:15 MFFmg/Kg dry0.025 7/29/14SW-846 8260B1JAcetone
ND 0.0064 7/29/14 13:15 MFFmg/Kg dry0.0027 7/29/14SW-846 8260B1Acrylonitrile
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1Benzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B1Bromobenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0015 7/29/14SW-846 8260B1Bromochloromethane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1Bromodichloromethane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0015 7/29/14SW-846 8260B1Bromoform
ND 0.011 7/29/14 13:15 MFFmg/Kg dry0.0018 7/29/14SW-846 8260B1Bromomethane
ND 0.042 7/29/14 13:15 MFFmg/Kg dry0.019 7/29/14SW-846 8260B12-Butanone (MEK)
ND 0.042 7/29/14 13:15 MFFmg/Kg dry0.022 7/29/14SW-846 8260B1V-16tert-Butyl Alcohol (TBA)
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1n-Butylbenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1sec-Butylbenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1tert-Butylbenzene
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0064 7/29/14 13:15 MFFmg/Kg dry0.0035 7/29/14SW-846 8260B1Carbon Disulfide
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B1Carbon Tetrachloride
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1Chlorobenzene
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1Chlorodibromomethane
ND 0.021 7/29/14 13:15 MFFmg/Kg dry0.0016 7/29/14SW-846 8260B1Chloroethane
ND 0.0042 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1Chloroform
ND 0.011 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1Chloromethane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B12-Chlorotoluene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B14-Chlorotoluene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1Dibromomethane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0042 7/29/14 13:15 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.021 7/29/14 13:15 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B11,1-Dichloroethane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B11,2-Dichloroethane
ND 0.0042 7/29/14 13:15 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B11,1-Dichloroethylene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B11,2-Dichloropropane
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B11,3-Dichloropropane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B12,2-Dichloropropane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B11,1-Dichloropropene
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.021 7/29/14 13:15 MFFmg/Kg dry0.0019 7/29/14SW-846 8260B1Diethyl Ether
Page 23 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-07
Field Sample #: VOC-1
Sample Matrix: Soil
Sampled: 7/24/2014 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.11 7/29/14 13:15 MFFmg/Kg dry0.061 7/29/14SW-846 8260B1V-161,4-Dioxane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B1Ethylbenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Hexachlorobutadiene
ND 0.021 7/29/14 13:15 MFFmg/Kg dry0.012 7/29/14SW-846 8260B12-Hexanone (MBK)
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0042 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.021 7/29/14 13:15 MFFmg/Kg dry0.0075 7/29/14SW-846 8260B1Methylene Chloride
ND 0.021 7/29/14 13:15 MFFmg/Kg dry0.0081 7/29/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0042 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1V-05Naphthalene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1n-Propylbenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B1Styrene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0011 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1Tetrachloroethylene
ND 0.011 7/29/14 13:15 MFFmg/Kg dry0.0023 7/29/14SW-846 8260B1V-16Tetrahydrofuran
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B1Toluene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1Trichloroethylene
ND 0.011 7/29/14 13:15 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B11,2,3-Trichloropropane
ND 0.011 7/29/14 13:15 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00085 7/29/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00064 7/29/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.011 7/29/14 13:15 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B1Vinyl Chloride
ND 0.0042 7/29/14 13:15 MFFmg/Kg dry0.0018 7/29/14SW-846 8260B1m+p Xylene
ND 0.0021 7/29/14 13:15 MFFmg/Kg dry0.00074 7/29/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 100 7/29/14 13:1570-130
Toluene-d8 97.2 7/29/14 13:1570-130
4-Bromofluorobenzene 94.3 7/29/14 13:1570-130
Page 24 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-07
Field Sample #: VOC-1
Sample Matrix: Soil
Sampled: 7/24/2014 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
92.3 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 25 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-08
Field Sample #: IC-2
Sample Matrix: Soil
Sampled: 7/24/2014 15:30
[TOC_2]14G1210-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.31 0.26 7/31/14 16:18 KSHmg/Kg dry0.065 7/28/14SW-846 6020A5Arsenic
26 6.6 7/31/14 16:18 KSHmg/Kg dry0.032 7/28/14SW-846 6020A5Chromium
85 6.6 7/31/14 16:18 KSHmg/Kg dry 7/28/14SW-846 6020A5Copper
7.6 2.6 7/31/14 16:18 KSHmg/Kg dry0.0047 7/28/14SW-846 6020A5Lead
0.028 0.50 7/31/14 16:18 KSHmg/Kg dry0.0030 7/28/14SW-846 6020A5JCadmium
Page 26 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-08
Field Sample #: IC-2
Sample Matrix: Soil
Sampled: 7/24/2014 15:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 0.33 7/31/14 14:20 LLmg/Kg dry0.18 7/30/14SW-846 7196A2W-06Hexavalent Chromium
130 7/26/14 17:15 ABHmV7/26/14SM2580 A1Oxidation/Reduction Potential
6.3 7/26/14 16:47 ABHpH Units 7/26/14SW-846 9045C1H-03pH @21.7°C
92.6 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 27 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-09
Field Sample #: VOC-3
Sample Matrix: Soil
Sampled: 7/24/2014 16:00
[TOC_2]14G1210-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.080 0.12 7/29/14 13:42 MFFmg/Kg dry0.028 7/29/14SW-846 8260B1JAcetone
ND 0.0072 7/29/14 13:42 MFFmg/Kg dry0.0030 7/29/14SW-846 8260B1Acrylonitrile
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1Benzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1Bromobenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0017 7/29/14SW-846 8260B1Bromochloromethane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1Bromodichloromethane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0017 7/29/14SW-846 8260B1Bromoform
ND 0.012 7/29/14 13:42 MFFmg/Kg dry0.0020 7/29/14SW-846 8260B1Bromomethane
ND 0.048 7/29/14 13:42 MFFmg/Kg dry0.021 7/29/14SW-846 8260B12-Butanone (MEK)
ND 0.048 7/29/14 13:42 MFFmg/Kg dry0.025 7/29/14SW-846 8260B1V-16tert-Butyl Alcohol (TBA)
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1n-Butylbenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B1sec-Butylbenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1tert-Butylbenzene
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0072 7/29/14 13:42 MFFmg/Kg dry0.0040 7/29/14SW-846 8260B1Carbon Disulfide
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1Carbon Tetrachloride
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1Chlorobenzene
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1Chlorodibromomethane
ND 0.024 7/29/14 13:42 MFFmg/Kg dry0.0018 7/29/14SW-846 8260B1Chloroethane
ND 0.0048 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1Chloroform
ND 0.012 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Chloromethane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B12-Chlorotoluene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B14-Chlorotoluene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1Dibromomethane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0048 7/29/14 13:42 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.024 7/29/14 13:42 MFFmg/Kg dry0.0016 7/29/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B11,1-Dichloroethane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0016 7/29/14SW-846 8260B11,2-Dichloroethane
ND 0.0048 7/29/14 13:42 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,1-Dichloroethylene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0016 7/29/14SW-846 8260B11,2-Dichloropropane
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B11,3-Dichloropropane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B12,2-Dichloropropane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,1-Dichloropropene
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.024 7/29/14 13:42 MFFmg/Kg dry0.0022 7/29/14SW-846 8260B1Diethyl Ether
Page 28 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-09
Field Sample #: VOC-3
Sample Matrix: Soil
Sampled: 7/24/2014 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.12 7/29/14 13:42 MFFmg/Kg dry0.069 7/29/14SW-846 8260B1V-161,4-Dioxane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1Ethylbenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B1Hexachlorobutadiene
ND 0.024 7/29/14 13:42 MFFmg/Kg dry0.013 7/29/14SW-846 8260B12-Hexanone (MBK)
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0048 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.024 7/29/14 13:42 MFFmg/Kg dry0.0086 7/29/14SW-846 8260B1Methylene Chloride
ND 0.024 7/29/14 13:42 MFFmg/Kg dry0.0092 7/29/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0048 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1V-05Naphthalene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1n-Propylbenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B1Styrene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0012 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0016 7/29/14SW-846 8260B1Tetrachloroethylene
ND 0.012 7/29/14 13:42 MFFmg/Kg dry0.0027 7/29/14SW-846 8260B1V-16Tetrahydrofuran
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B1Toluene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0012 7/29/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0014 7/29/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B1Trichloroethylene
ND 0.012 7/29/14 13:42 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B11,2,3-Trichloropropane
ND 0.012 7/29/14 13:42 MFFmg/Kg dry0.0011 7/29/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00096 7/29/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00072 7/29/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.012 7/29/14 13:42 MFFmg/Kg dry0.0013 7/29/14SW-846 8260B1Vinyl Chloride
ND 0.0048 7/29/14 13:42 MFFmg/Kg dry0.0020 7/29/14SW-846 8260B1m+p Xylene
ND 0.0024 7/29/14 13:42 MFFmg/Kg dry0.00084 7/29/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.4 7/29/14 13:4270-130
Toluene-d8 96.4 7/29/14 13:4270-130
4-Bromofluorobenzene 91.7 7/29/14 13:4270-130
Page 29 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-09
Field Sample #: VOC-3
Sample Matrix: Soil
Sampled: 7/24/2014 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
88.3 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 30 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-10
Field Sample #: IC-5
Sample Matrix: Soil
Sampled: 7/24/2014 16:15
[TOC_2]14G1210-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
3.5 0.27 7/31/14 16:22 KSHmg/Kg dry0.067 7/28/14SW-846 6020A5Arsenic
31 6.8 7/31/14 16:22 KSHmg/Kg dry0.033 7/28/14SW-846 6020A5Chromium
17 6.8 7/31/14 16:22 KSHmg/Kg dry 7/28/14SW-846 6020A5Copper
27 2.7 7/31/14 16:22 KSHmg/Kg dry0.0048 7/28/14SW-846 6020A5Lead
0.083 0.52 7/31/14 16:22 KSHmg/Kg dry0.0031 7/28/14SW-846 6020A5JCadmium
Page 31 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-10
Field Sample #: IC-5
Sample Matrix: Soil
Sampled: 7/24/2014 16:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 0.90 7/31/14 14:20 LLmg/Kg dry0.50 7/30/14SW-846 7196A5W-06Hexavalent Chromium
150 7/26/14 17:15 ABHmV7/26/14SM2580 A1Oxidation/Reduction Potential
6.4 7/26/14 16:47 ABHpH Units 7/26/14SW-846 9045C1H-03pH @21.6°C
88.4 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 32 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-11
Field Sample #: BIC-1
Sample Matrix: Soil
Sampled: 7/24/2014 16:30
[TOC_2]14G1210-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.36 0.26 7/31/14 16:25 KSHmg/Kg dry0.065 7/28/14SW-846 6020A5Arsenic
43 6.6 7/31/14 16:25 KSHmg/Kg dry0.032 7/28/14SW-846 6020A5Chromium
23 6.6 7/31/14 16:25 KSHmg/Kg dry 7/28/14SW-846 6020A5Copper
16 2.6 7/31/14 16:25 KSHmg/Kg dry0.0047 7/28/14SW-846 6020A5Lead
0.052 0.50 7/31/14 16:25 KSHmg/Kg dry0.0030 7/28/14SW-846 6020A5JCadmium
Page 33 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/25/2014
Work Order: 14G1210Sample Description:Project Location: Hillsborough, NC
Sample ID: 14G1210-11
Field Sample #: BIC-1
Sample Matrix: Soil
Sampled: 7/24/2014 16:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 0.34 7/31/14 14:20 LLmg/Kg dry0.18 7/30/14SW-846 7196A2W-06Hexavalent Chromium
140 7/26/14 17:15 ABHmV7/26/14SM2580 A1Oxidation/Reduction Potential
5.3 7/26/14 16:47 ABHpH Units 7/26/14SW-846 9045C1H-03pH @21.9°C
92.5 7/30/14 8:06 MRL% Wt 7/29/14SM 2540G1% Solids
Page 34 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B101290 07/29/1414G1210-01 [IC-6]
B101290 07/29/1414G1210-02 [VOC-5]
B101290 07/29/1414G1210-03 [IC-3]
B101290 07/29/1414G1210-04 [VOC-2]
B101290 07/29/1414G1210-05 [IC-4]
B101290 07/29/1414G1210-06 [VOC-4]
B101290 07/29/1414G1210-07 [VOC-1]
B101290 07/29/1414G1210-08 [IC-2]
B101290 07/29/1414G1210-09 [VOC-3]
B101290 07/29/1414G1210-10 [IC-5]
B101290 07/29/1414G1210-11 [BIC-1]
SM2580 A
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B101124 07/26/1450.0 50.014G1210-01 [IC-6]
B101124 07/26/1450.0 50.014G1210-03 [IC-3]
B101124 07/26/1450.0 50.014G1210-05 [IC-4]
B101124 07/26/1450.0 50.014G1210-08 [IC-2]
B101124 07/26/1450.0 50.014G1210-10 [IC-5]
B101124 07/26/1450.0 50.014G1210-11 [BIC-1]
Prep Method: SW-846 3050B-SW-846 6020A
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B101186 07/28/141.00 50.014G1210-01 [IC-6]
B101186 07/28/141.00 50.014G1210-03 [IC-3]
B101186 07/28/141.06 50.014G1210-05 [IC-4]
B101186 07/28/141.02 50.014G1210-08 [IC-2]
B101186 07/28/141.04 50.014G1210-10 [IC-5]
B101186 07/28/141.02 50.014G1210-11 [BIC-1]
SW-846 7196A
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B101342 07/30/142.58 10014G1210-01 [IC-6]
B101342 07/30/142.55 10014G1210-03 [IC-3]
B101342 07/30/142.51 10014G1210-05 [IC-4]
B101342 07/30/142.60 10014G1210-08 [IC-2]
B101342 07/30/142.50 10014G1210-10 [IC-5]
B101342 07/30/142.57 10014G1210-11 [BIC-1]
Prep Method: SW-846 5035-SW-846 8260B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B101254 07/29/146.63 10.014G1210-02 [VOC-5]
B101254 07/29/145.66 10.014G1210-04 [VOC-2]
B101254 07/29/144.73 10.014G1210-06 [VOC-4]
B101254 07/29/145.10 10.014G1210-07 [VOC-1]
B101254 07/29/144.70 10.014G1210-09 [VOC-3]
[TOC_1]Sample Preparation Information[TOC]
Page 35 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
SW-846 9045C
Lab Number [Field ID]Batch DateInitial [g]
B101121 07/26/1420.014G1210-01 [IC-6]
B101121 07/26/1420.014G1210-03 [IC-3]
B101121 07/26/1420.014G1210-05 [IC-4]
B101121 07/26/1420.014G1210-08 [IC-2]
B101121 07/26/1420.014G1210-10 [IC-5]
B101121 07/26/1420.014G1210-11 [BIC-1]
Page 36 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B101254 - SW-846 5035
[TOC_3]B101254[TOC]
Blank (B101254-BLK1) Prepared & Analyzed: 07/29/14
Acetone mg/Kg wet0.10ND
Acrylonitrile mg/Kg wet0.0060ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010ND
2-Butanone (MEK)mg/Kg wet0.040ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 V-16ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10 V-16ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040ND
[TOC_1]QC Data[TOC]
Page 37 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B101254 - SW-846 5035
Blank (B101254-BLK1) Prepared & Analyzed: 07/29/14
Methylene Chloride mg/Kg wet0.020ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020ND
Naphthalene mg/Kg wet0.0040 V-05ND
n-Propylbenzene mg/Kg wet0.0020ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010 V-16ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 97.50.0487
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 98.70.0494
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 98.00.0490
LCS (B101254-BS1) Prepared & Analyzed: 07/29/14
Acetone mg/Kg wet0.10 0.200 V-2070-16075.4 †0.151
Acrylonitrile mg/Kg wet0.0060 0.0200 70-13087.80.0176
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-13099.70.0199
Benzene mg/Kg wet0.0020 0.0200 70-13094.30.0189
Bromobenzene mg/Kg wet0.0020 0.0200 70-13090.60.0181
Bromochloromethane mg/Kg wet0.0020 0.0200 70-1301020.0204
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-1301000.0200
Bromoform mg/Kg wet0.0020 0.0200 70-13089.20.0178
Bromomethane mg/Kg wet0.010 0.0200 40-13063.7 †0.0127
2-Butanone (MEK)mg/Kg wet0.040 0.200 70-16081.9 †0.164
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 V-1640-13084.9 †0.170
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-13088.00.0176
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-13086.30.0173
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-16085.4 †0.0171
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 70-1301040.0207
Carbon Disulfide mg/Kg wet0.0060 0.0200 70-13095.10.0190
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-13095.40.0191
Chlorobenzene mg/Kg wet0.0020 0.0200 70-13086.20.0172
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-13095.60.0191
Chloroethane mg/Kg wet0.020 0.0200 70-1301050.0211
Chloroform mg/Kg wet0.0040 0.0200 70-13098.20.0196
Chloromethane mg/Kg wet0.010 0.0200 70-13085.60.0171
2-Chlorotoluene mg/Kg wet0.0020 0.0200 70-13092.60.0185
Page 38 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B101254 - SW-846 5035
LCS (B101254-BS1) Prepared & Analyzed: 07/29/14
4-Chlorotoluene mg/Kg wet0.0020 0.0200 70-13093.10.0186
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 70-13079.40.0159
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-13098.90.0198
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301020.0203
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13086.70.0173
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13083.70.0167
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13081.80.0164
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-13088.20.0176
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 J40-16084.8 †0.0170
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-13096.00.0192
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-13099.00.0198
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 70-1301020.0204
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13095.60.0191
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13094.90.0190
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13094.60.0189
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-1301000.0201
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-1301020.0204
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-13097.40.0195
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13090.70.0181
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13096.00.0192
Diethyl Ether mg/Kg wet0.020 0.0200 70-1301020.0204
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-13097.00.0194
1,4-Dioxane mg/Kg wet0.10 0.200 V-1640-16078.1 †0.156
Ethylbenzene mg/Kg wet0.0020 0.0200 70-13093.40.0187
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 70-16090.60.0181
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-16084.7 †0.169
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-13090.30.0181
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-13086.80.0174
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 70-1301010.0202
Methylene Chloride mg/Kg wet0.020 0.0200 J40-16086.7 †0.0173
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 70-16088.0 †0.176
Naphthalene mg/Kg wet0.0040 0.0200 V-0540-13061.0 †0.0122
n-Propylbenzene mg/Kg wet0.0020 0.0200 70-13092.90.0186
Styrene mg/Kg wet0.0020 0.0200 70-13093.80.0188
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 70-13096.00.0192
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-13086.20.0172
Tetrachloroethylene mg/Kg wet0.0020 0.0200 70-13098.10.0196
Tetrahydrofuran mg/Kg wet0.010 0.0200 V-1670-13075.30.0151
Toluene mg/Kg wet0.0020 0.0200 70-13089.70.0179
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13076.70.0153
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13078.70.0157
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13086.30.0173
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-13099.10.0198
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-13096.60.0193
Trichloroethylene mg/Kg wet0.0020 0.0200 70-13097.20.0194
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 70-13094.50.0189
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-13090.10.0180
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 70-13098.40.0197
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13089.60.0179
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13095.40.0191
Vinyl Chloride mg/Kg wet0.010 0.0200 40-13094.3 †0.0189
Page 39 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B101254 - SW-846 5035
LCS (B101254-BS1) Prepared & Analyzed: 07/29/14
m+p Xylene mg/Kg wet0.0040 0.0400 70-13093.80.0375
o-Xylene mg/Kg wet0.0020 0.0200 70-13091.00.0182
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 93.70.0468
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 99.00.0495
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1010.0505
LCS Dup (B101254-BSD1) Prepared & Analyzed: 07/29/14
Acetone mg/Kg wet0.10 0.200 25 V-2070-16079.6 5.47 †0.159
Acrylonitrile mg/Kg wet0.0060 0.0200 2570-13087.5 0.3420.0175
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-130106 6.030.0212
Benzene mg/Kg wet0.0020 0.0200 2570-13098.5 4.360.0197
Bromobenzene mg/Kg wet0.0020 0.0200 2570-13094.9 4.640.0190
Bromochloromethane mg/Kg wet0.0020 0.0200 2570-130106 4.130.0213
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-130107 6.380.0213
Bromoform mg/Kg wet0.0020 0.0200 2570-13091.5 2.550.0183
Bromomethane mg/Kg wet0.010 0.0200 2540-13077.8 19.9 †0.0156
2-Butanone (MEK)mg/Kg wet0.040 0.200 2570-16089.8 9.16 †0.180
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 25 V-1640-13095.5 11.7 †0.191
n-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13090.4 2.690.0181
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13092.4 6.830.0185
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-16091.9 7.33 †0.0184
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 2570-130108 4.620.0217
Carbon Disulfide mg/Kg wet0.0060 0.0200 2570-13099.6 4.620.0199
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-130101 5.700.0202
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-13091.3 5.750.0183
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130104 8.610.0208
Chloroethane mg/Kg wet0.020 0.0200 2570-130105 0.3810.0210
Chloroform mg/Kg wet0.0040 0.0200 2570-130103 5.160.0207
Chloromethane mg/Kg wet0.010 0.0200 2570-13091.2 6.330.0182
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13094.0 1.500.0188
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13096.1 3.170.0192
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 2570-13082.6 3.950.0165
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-130105 6.360.0211
Dibromomethane mg/Kg wet0.0020 0.0200 2570-130107 5.080.0214
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13090.4 4.180.0181
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13088.5 5.570.0177
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13086.7 5.820.0173
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-13098.6 11.10.0197
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 25 J40-16068.5 21.3 †0.0137
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130104 7.620.0207
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130108 8.790.0216
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 2570-130108 5.440.0215
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13098.8 3.290.0198
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13097.1 2.290.0194
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-130100 5.650.0200
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-130112 11.30.0225
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-130105 3.290.0210
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-130103 5.390.0206
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-130100 9.850.0200
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-130102 5.770.0203
Diethyl Ether mg/Kg wet0.020 0.0200 2570-130108 6.180.0217
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-130101 3.840.0202
Page 40 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B101254 - SW-846 5035
LCS Dup (B101254-BSD1) Prepared & Analyzed: 07/29/14
1,4-Dioxane mg/Kg wet0.10 0.200 50 V-1640-16071.2 9.23 †‡0.142
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-13097.9 4.700.0196
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 2570-16099.3 9.160.0199
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-16093.6 9.98 †0.187
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-13093.9 3.910.0188
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-13091.9 5.710.0184
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 2570-130108 6.880.0216
Methylene Chloride mg/Kg wet0.020 0.0200 25 J40-16093.5 7.55 †0.0187
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 2570-16095.3 7.91 †0.191
Naphthalene mg/Kg wet0.0040 0.0200 25 V-0540-13066.5 8.63 †0.0133
n-Propylbenzene mg/Kg wet0.0020 0.0200 2570-13096.5 3.800.0193
Styrene mg/Kg wet0.0020 0.0200 2570-13098.8 5.190.0198
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 2570-130101 4.980.0202
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-13096.0 10.80.0192
Tetrachloroethylene mg/Kg wet0.0020 0.0200 2570-130103 4.970.0206
Tetrahydrofuran mg/Kg wet0.010 0.0200 25 V-1670-13091.8 19.70.0184
Toluene mg/Kg wet0.0020 0.0200 2570-13095.3 6.050.0191
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13081.5 6.070.0163
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13082.2 4.350.0164
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13091.2 5.520.0182
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130104 4.630.0208
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130104 7.760.0209
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-130100 3.340.0201
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 2570-13099.0 4.650.0198
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-13098.0 8.400.0196
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 2570-130106 7.060.0211
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13095.4 6.270.0191
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13097.1 1.770.0194
Vinyl Chloride mg/Kg wet0.010 0.0200 2540-130104 9.97 †0.0208
m+p Xylene mg/Kg wet0.0040 0.0400 2570-13099.0 5.500.0396
o-Xylene mg/Kg wet0.0020 0.0200 2570-13096.4 5.760.0193
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 95.00.0475
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 97.60.0488
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1000.0501
Page 41 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B101186 - SW-846 3050B
[TOC_3]B101186[TOC]
Blank (B101186-BLK1) Prepared: 07/28/14 Analyzed: 07/31/14
Arsenic mg/Kg wet0.25ND
Chromium mg/Kg wet6.2ND
Copper mg/Kg wet6.2ND
Lead mg/Kg wet2.5 J0.093
Cadmium mg/Kg wet0.48ND
LCS (B101186-BS1) Prepared: 07/28/14 Analyzed: 07/31/14
Arsenic mg/Kg wet2.0 122 77.8-122.1111136
Chromium mg/Kg wet50 102 78.7-120.6101103
Copper mg/Kg wet50 78.0 80.4-119.611287.3
Lead mg/Kg wet20 94.5 82.4-117.8106100
Cadmium mg/Kg wet3.8 88.0 81.9-118.2115101
LCS Dup (B101186-BSD1) Prepared: 07/28/14 Analyzed: 07/31/14
Arsenic mg/Kg wet2.0 122 3077.8-122.1108 3.21132
Chromium mg/Kg wet50 102 3078.7-120.698.3 2.91100
Copper mg/Kg wet50 78.0 3080.4-119.6105 6.5881.7
Lead mg/Kg wet20 94.5 3082.4-117.8101 5.1395.1
Cadmium mg/Kg wet3.8 88.0 3081.9-118.2110 4.2596.6
Duplicate (B101186-DUP1) Prepared: 07/28/14 Analyzed: 07/31/14 Source: 14G1210-01
Arsenic mg/Kg dry0.28 3513.52.64 2.30
Chromium mg/Kg dry7.0 3517.032.2 27.2
Copper mg/Kg dry7.0 350.52421.1 21.0
Lead mg/Kg dry2.8 354.1616.9 17.6
Cadmium mg/Kg dry0.53 35 R-04, J48.4 *0.0234 0.0143
Matrix Spike (B101186-MS1) Prepared: 07/28/14 Analyzed: 07/31/14 Source: 14G1210-01
Arsenic mg/Kg dry1.1 27.6 75-12590.427.3 2.30
Chromium mg/Kg dry28 27.6 MS-1175-125127*62.3 27.2
Copper mg/Kg dry28 27.6 75-12512555.6 21.0
Lead mg/Kg dry11 27.6 75-12510947.7 17.6
Cadmium mg/Kg dry2.1 27.6 75-12510729.6 0.0143
Page 42 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B101121 - SW-846 9045C
[TOC_3]B101121[TOC]
LCS (B101121-BS1) Prepared & Analyzed: 07/26/14
pH pH Units 6.00 98.5-1021006.02
Duplicate (B101121-DUP1) Prepared & Analyzed: 07/26/14 Source: 14G1210-03
pH pH Units 5.72 H-030.005.9 5.9
Batch B101124 - SM2580 A
[TOC_3]B101124[TOC]
Duplicate (B101124-DUP1) Prepared & Analyzed: 07/26/14 Source: 14G1210-11
Oxidation/Reduction Potential mV 20.61.41141143
Batch B101342 - SW-846 7196A
[TOC_3]B101342[TOC]
Blank (B101342-BLK1) Prepared: 07/30/14 Analyzed: 07/31/14
Hexavalent Chromium mg/Kg wet0.16ND
LCS (B101342-BS1) Prepared: 07/30/14 Analyzed: 07/31/14
Hexavalent Chromium mg/Kg wet1.9 61.1 80-12010162
LCS Dup (B101342-BSD1) Prepared: 07/30/14 Analyzed: 07/31/14
Hexavalent Chromium mg/Kg wet1.9 60.2 2080-120103 1.0162
Page 43 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Sample received after recommended holding time was exceeded.H-03
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Matrix spike recovery outside of control limits. Possibility of sample matrix effects that lead to a high bias for
reported result or non-homogeneous sample aliquots cannot be eliminated.
MS-11
Duplicate relative percent difference (RPD) is a less useful indicator of sample precision for sample results that
are <5 times the reporting limit (RL).
R-04
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Increased uncertainty is associated with the reported value which is likely to be biased on the low side.
V-05
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may
be associated with reported result.
V-16
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
V-20
Elevated method reporting limit due to intense color of sampleW-06
[TOC_1]Flag/Qualifier Summary[TOC]
Page 44 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 6020A in Soil
NC,NY,VA,NJ,NHArsenic
NY,NC,NJChromium
NY,NC,NJCopper
NY,NC,NJLead
NC,NY,NJCadmium
SW-846 7196A in Soil
NY,CT,NH,NC,ME,VA,NJHexavalent Chromium
SW-846 8260B in Soil
CT,NH,NY,NC,MEAcetone
CT,NH,NY,NC,MEAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
CT,NH,NY,NC,MEBenzene
NH,NY,NC,MEBromobenzene
NH,NY,NC,MEBromochloromethane
CT,NH,NY,NC,MEBromodichloromethane
CT,NH,NY,NC,MEBromoform
CT,NH,NY,NC,MEBromomethane
CT,NH,NY,NC,ME2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
CT,NH,NY,NC,MEn-Butylbenzene
CT,NH,NY,NC,MEsec-Butylbenzene
CT,NH,NY,NC,MEtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
CT,NH,NY,NC,MECarbon Disulfide
CT,NH,NY,NC,MECarbon Tetrachloride
CT,NH,NY,NC,MEChlorobenzene
CT,NH,NY,NC,MEChlorodibromomethane
CT,NH,NY,NC,MEChloroethane
CT,NH,NY,NC,MEChloroform
CT,NH,NY,NC,MEChloromethane
CT,NH,NY,NC,ME2-Chlorotoluene
CT,NH,NY,NC,ME4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NH,NY,NC,MEDibromomethane
CT,NH,NY,NC,ME1,2-Dichlorobenzene
CT,NH,NY,NC,ME1,3-Dichlorobenzene
CT,NH,NY,NC,ME1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NY,NC,MEDichlorodifluoromethane (Freon 12)
CT,NH,NY,NC,ME1,1-Dichloroethane
CT,NH,NY,NC,ME1,2-Dichloroethane
CT,NH,NY,NC,ME1,1-Dichloroethylene
CT,NH,NY,NC,MEcis-1,2-Dichloroethylene
CT,NH,NY,NC,MEtrans-1,2-Dichloroethylene
CT,NH,NY,NC,ME1,2-Dichloropropane
[TOC_1]Certifications[TOC]
Page 45 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260B in Soil
NH,NY,NC,ME1,3-Dichloropropane
NH,NY,NC,ME2,2-Dichloropropane
NH,NY,NC,ME1,1-Dichloropropene
CT,NH,NY,NC,MEcis-1,3-Dichloropropene
CT,NH,NY,NC,MEtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
CT,NH,NY,NC,MEEthylbenzene
NH,NY,NC,MEHexachlorobutadiene
CT,NH,NY,NC,ME2-Hexanone (MBK)
CT,NH,NY,NC,MEIsopropylbenzene (Cumene)
NH,NY,NCp-Isopropyltoluene (p-Cymene)
NY,NCMethyl tert-Butyl Ether (MTBE)
CT,NH,NY,NC,MEMethylene Chloride
CT,NH,NY,NC4-Methyl-2-pentanone (MIBK)
NH,NY,NC,MENaphthalene
NH,NY,NCn-Propylbenzene
CT,NH,NY,NC,MEStyrene
CT,NH,NY,NC,ME1,1,1,2-Tetrachloroethane
CT,NH,NY,NC,ME1,1,2,2-Tetrachloroethane
CT,NH,NY,NC,METetrachloroethylene
NCTetrahydrofuran
CT,NH,NY,NC,METoluene
NC,ME1,2,3-Trichlorobenzene
NH,NY,NC,ME1,2,4-Trichlorobenzene
NC,ME1,3,5-Trichlorobenzene
CT,NH,NY,NC,ME1,1,1-Trichloroethane
CT,NH,NY,NC,ME1,1,2-Trichloroethane
CT,NH,NY,NC,METrichloroethylene
CT,NH,NY,NC,METrichlorofluoromethane (Freon 11)
NH,NY,NC,ME1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
CT,NH,NY,NC,ME1,2,4-Trimethylbenzene
CT,NH,NY,NC,ME1,3,5-Trimethylbenzene
CT,NH,NY,NC,MEVinyl Chloride
CT,NH,NY,NC,MEm+p Xylene
CT,NH,NY,NC,MEo-Xylene
Page 46 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLCAIHA 02/1/2016
M-MA100Massachusetts DEPMA 06/30/2015
PH-0567Connecticut Department of Publilc HealthCT 09/30/2015
10899 NELAPNew York State Department of HealthNY 04/1/2015
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2015
LAO00112Rhode Island Department of HealthRI 12/30/2014
652North Carolina Div. of Water QualityNC 12/31/2014
MA007 NELAPNew Jersey DEPNJ 06/30/2015
E871027 NELAPFlorida Department of HealthFL 06/30/2015
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2015
C2065State of Washington Department of EcologyWA 02/23/2015
2011028State of MaineME 06/9/2015
460217Commonwealth of VirginiaVA 12/14/2014
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2014
Page 47 of 52
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Page 1 of 25 15A0027_1 Contest_Final 01 08 15 1529
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Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
15A0027-01 5
15A0027-02 7
15A0027-03 9
15A0027-04 11
15A0027-05 13
15A0027-06 15
Sample Preparation Information 17
QC Data 18
Metals Analyses (Total) 18
B112933 18
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 19
B112921 19
Flag/Qualifier Summary 20
Certifications 21
Chain of Custody/Sample Receipt 22
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