Caroline Courtyard 2015 Annual GW Monitoring Rpt

APPENDICES

ANALYTICAL REPORT
December 23, 2015
Griffith Enterprise
Sample Delivery Group: L806319
Samples Received:12/11/2015
Project Number:
Description:Caroline Courtyard
Report To:Mr. Alan Griffith
353 Jonestown Road, PMB 312
Winston-Salem, NC 27104
Entire Report Reviewed By:
December 23, 2015
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
December 23, 2015
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 4
⁵Sr: Sample Results 5
MW-11 L806319-01 5
MW-16 L806319-02 7
MW-19 L806319-03 9
MW-23 L806319-04 11
MW-18 L806319-05 13
MW-22D L806319-06 15
MW-25 L806319-07 17
⁶Qc: Quality Control Summary 19
Volatile Organic Compounds (GC/MS) by Method 8260B 19
⁷Gl: Glossary of Terms 31
⁸Al: Accreditations & Locations 32
⁹Sc: Chain of Custody 33
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-11 L806319-01 GW M. Alan Griffith 12/10/15 09:30 12/11/15 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG837923 1 12/23/15 02:59 12/23/15 02:59 DAH
Collected by Collected date/time Received date/time
MW-16 L806319-02 GW M. Alan Griffith 12/10/15 10:00 12/11/15 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG837923 1 12/23/15 07:36 12/23/15 07:36 DAH
Collected by Collected date/time Received date/time
MW-19 L806319-03 GW M. Alan Griffith 12/10/15 10:30 12/11/15 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG837923 1 12/23/15 07:57 12/23/15 07:57 DAH
Collected by Collected date/time Received date/time
MW-23 L806319-04 GW M. Alan Griffith 12/10/15 11:00 12/11/15 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG835361 1 12/20/15 14:19 12/20/15 14:19 JAH
Collected by Collected date/time Received date/time
MW-18 L806319-05 GW M. Alan Griffith 12/10/15 11:25 12/11/15 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG835361 1 12/20/15 14:39 12/20/15 14:39 JAH
Collected by Collected date/time Received date/time
MW-22D L806319-06 GW M. Alan Griffith 12/10/15 11:55 12/11/15 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG835361 1 12/20/15 13:40 12/20/15 13:40 JAH
Collected by Collected date/time Received date/time
MW-25 L806319-07 GW M. Alan Griffith 12/10/15 12:35 12/11/15 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG835361 1 12/20/15 14:59 12/20/15 14:59 JAH
Volatile Organic Compounds (GC/MS) by Method 8260B WG837923 20 12/23/15 08:16 12/23/15 08:16 DAH
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Jimmy Hunt
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L806319
MW-11
Collected date/time: 12/10/15 09:30
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
Acetone ND 0.0500 1 12/23/2015 02:59 WG837923
Acrolein ND 0.0500 1 12/23/2015 02:59 WG837923
Acrylonitrile ND 0.0100 1 12/23/2015 02:59 WG837923
Benzene ND 0.00100 1 12/23/2015 02:59 WG837923
Bromobenzene ND 0.00100 1 12/23/2015 02:59 WG837923
Bromodichloromethane ND 0.00100 1 12/23/2015 02:59 WG837923
Bromoform ND 0.00100 1 12/23/2015 02:59 WG837923
Bromomethane ND 0.00500 1 12/23/2015 02:59 WG837923
n-Butylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
sec-Butylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
tert-Butylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
Carbon tetrachloride ND 0.00100 1 12/23/2015 02:59 WG837923
Chlorobenzene ND 0.00100 1 12/23/2015 02:59 WG837923
Chlorodibromomethane ND 0.00100 1 12/23/2015 02:59 WG837923
Chloroethane ND 0.00500 1 12/23/2015 02:59 WG837923
2-Chloroethyl vinyl ether ND J6 0.0500 1 12/23/2015 02:59 WG837923
Chloroform ND 0.00500 1 12/23/2015 02:59 WG837923
Chloromethane ND 0.00250 1 12/23/2015 02:59 WG837923
2-Chlorotoluene ND 0.00100 1 12/23/2015 02:59 WG837923
4-Chlorotoluene ND 0.00100 1 12/23/2015 02:59 WG837923
1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/23/2015 02:59 WG837923
1,2-Dibromoethane ND 0.00100 1 12/23/2015 02:59 WG837923
Dibromomethane ND 0.00100 1 12/23/2015 02:59 WG837923
1,2-Dichlorobenzene ND 0.00100 1 12/23/2015 02:59 WG837923
1,3-Dichlorobenzene ND 0.00100 1 12/23/2015 02:59 WG837923
1,4-Dichlorobenzene ND 0.00100 1 12/23/2015 02:59 WG837923
Dichlorodifluoromethane ND 0.00500 1 12/23/2015 02:59 WG837923
1,1-Dichloroethane ND 0.00100 1 12/23/2015 02:59 WG837923
1,2-Dichloroethane ND 0.00100 1 12/23/2015 02:59 WG837923
1,1-Dichloroethene ND 0.00100 1 12/23/2015 02:59 WG837923
cis-1,2-Dichloroethene ND 0.00100 1 12/23/2015 02:59 WG837923
trans-1,2-Dichloroethene ND 0.00100 1 12/23/2015 02:59 WG837923
1,2-Dichloropropane ND 0.00100 1 12/23/2015 02:59 WG837923
1,1-Dichloropropene ND 0.00100 1 12/23/2015 02:59 WG837923
1,3-Dichloropropane ND 0.00100 1 12/23/2015 02:59 WG837923
cis-1,3-Dichloropropene ND 0.00100 1 12/23/2015 02:59 WG837923
trans-1,3-Dichloropropene ND 0.00100 1 12/23/2015 02:59 WG837923
2,2-Dichloropropane ND 0.00100 1 12/23/2015 02:59 WG837923
Di-isopropyl ether ND 0.00100 1 12/23/2015 02:59 WG837923
Ethylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
Hexachloro-1,3-butadiene ND 0.00100 1 12/23/2015 02:59 WG837923
Isopropylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
p-Isopropyltoluene ND 0.00100 1 12/23/2015 02:59 WG837923
2-Butanone (MEK)ND 0.0100 1 12/23/2015 02:59 WG837923
Methylene Chloride ND 0.00500 1 12/23/2015 02:59 WG837923
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/23/2015 02:59 WG837923
Methyl tert-butyl ether ND 0.00100 1 12/23/2015 02:59 WG837923
Naphthalene ND 0.00500 1 12/23/2015 02:59 WG837923
n-Propylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
Styrene ND 0.00100 1 12/23/2015 02:59 WG837923
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/23/2015 02:59 WG837923
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/23/2015 02:59 WG837923
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/23/2015 02:59 WG837923
Tetrachloroethene ND 0.00100 1 12/23/2015 02:59 WG837923
Toluene ND 0.00500 1 12/23/2015 02:59 WG837923
1,2,3-Trichlorobenzene ND 0.00100 1 12/23/2015 02:59 WG837923
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L806319
MW-11
Collected date/time: 12/10/15 09:30
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
1,2,4-Trichlorobenzene ND 0.00100 1 12/23/2015 02:59 WG837923
1,1,1-Trichloroethane ND 0.00100 1 12/23/2015 02:59 WG837923
1,1,2-Trichloroethane ND 0.00100 1 12/23/2015 02:59 WG837923
Trichloroethene ND 0.00100 1 12/23/2015 02:59 WG837923
Trichlorofluoromethane ND 0.00500 1 12/23/2015 02:59 WG837923
1,2,3-Trichloropropane ND 0.00250 1 12/23/2015 02:59 WG837923
1,2,4-Trimethylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
1,2,3-Trimethylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
1,3,5-Trimethylbenzene ND 0.00100 1 12/23/2015 02:59 WG837923
Vinyl chloride ND 0.00100 1 12/23/2015 02:59 WG837923
Xylenes, Total ND 0.00300 1 12/23/2015 02:59 WG837923
(S) Toluene-d8 105 90.0-115 12/23/2015 02:59 WG837923
(S) Dibromofluoromethane 104 79.0-121 12/23/2015 02:59 WG837923
(S) 4-Bromofluorobenzene 102 80.1-120 12/23/2015 02:59 WG837923
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L806319
MW-16
Collected date/time: 12/10/15 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
Acetone ND J3 0.0500 1 12/23/2015 07:36 WG837923
Acrolein ND 0.0500 1 12/23/2015 07:36 WG837923
Acrylonitrile ND 0.0100 1 12/23/2015 07:36 WG837923
Benzene ND 0.00100 1 12/23/2015 07:36 WG837923
Bromobenzene ND 0.00100 1 12/23/2015 07:36 WG837923
Bromodichloromethane ND 0.00100 1 12/23/2015 07:36 WG837923
Bromoform ND 0.00100 1 12/23/2015 07:36 WG837923
Bromomethane ND 0.00500 1 12/23/2015 07:36 WG837923
n-Butylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
sec-Butylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
tert-Butylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
Carbon tetrachloride ND 0.00100 1 12/23/2015 07:36 WG837923
Chlorobenzene ND 0.00100 1 12/23/2015 07:36 WG837923
Chlorodibromomethane ND 0.00100 1 12/23/2015 07:36 WG837923
Chloroethane ND 0.00500 1 12/23/2015 07:36 WG837923
2-Chloroethyl vinyl ether ND 0.0500 1 12/23/2015 07:36 WG837923
Chloroform ND 0.00500 1 12/23/2015 07:36 WG837923
Chloromethane ND 0.00250 1 12/23/2015 07:36 WG837923
2-Chlorotoluene ND 0.00100 1 12/23/2015 07:36 WG837923
4-Chlorotoluene ND 0.00100 1 12/23/2015 07:36 WG837923
1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/23/2015 07:36 WG837923
1,2-Dibromoethane ND 0.00100 1 12/23/2015 07:36 WG837923
Dibromomethane ND 0.00100 1 12/23/2015 07:36 WG837923
1,2-Dichlorobenzene ND 0.00100 1 12/23/2015 07:36 WG837923
1,3-Dichlorobenzene ND 0.00100 1 12/23/2015 07:36 WG837923
1,4-Dichlorobenzene ND 0.00100 1 12/23/2015 07:36 WG837923
Dichlorodifluoromethane ND 0.00500 1 12/23/2015 07:36 WG837923
1,1-Dichloroethane ND 0.00100 1 12/23/2015 07:36 WG837923
1,2-Dichloroethane ND 0.00100 1 12/23/2015 07:36 WG837923
1,1-Dichloroethene ND 0.00100 1 12/23/2015 07:36 WG837923
cis-1,2-Dichloroethene ND 0.00100 1 12/23/2015 07:36 WG837923
trans-1,2-Dichloroethene ND 0.00100 1 12/23/2015 07:36 WG837923
1,2-Dichloropropane ND 0.00100 1 12/23/2015 07:36 WG837923
1,1-Dichloropropene ND 0.00100 1 12/23/2015 07:36 WG837923
1,3-Dichloropropane ND 0.00100 1 12/23/2015 07:36 WG837923
cis-1,3-Dichloropropene ND 0.00100 1 12/23/2015 07:36 WG837923
trans-1,3-Dichloropropene ND 0.00100 1 12/23/2015 07:36 WG837923
2,2-Dichloropropane ND 0.00100 1 12/23/2015 07:36 WG837923
Di-isopropyl ether ND 0.00100 1 12/23/2015 07:36 WG837923
Ethylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
Hexachloro-1,3-butadiene ND 0.00100 1 12/23/2015 07:36 WG837923
Isopropylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
p-Isopropyltoluene ND 0.00100 1 12/23/2015 07:36 WG837923
2-Butanone (MEK)ND J3 0.0100 1 12/23/2015 07:36 WG837923
Methylene Chloride ND 0.00500 1 12/23/2015 07:36 WG837923
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/23/2015 07:36 WG837923
Methyl tert-butyl ether ND 0.00100 1 12/23/2015 07:36 WG837923
Naphthalene ND 0.00500 1 12/23/2015 07:36 WG837923
n-Propylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
Styrene ND 0.00100 1 12/23/2015 07:36 WG837923
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/23/2015 07:36 WG837923
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/23/2015 07:36 WG837923
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/23/2015 07:36 WG837923
Tetrachloroethene 0.00869 0.00100 1 12/23/2015 07:36 WG837923
Toluene ND 0.00500 1 12/23/2015 07:36 WG837923
1,2,3-Trichlorobenzene ND 0.00100 1 12/23/2015 07:36 WG837923
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L806319
MW-16
Collected date/time: 12/10/15 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
1,2,4-Trichlorobenzene ND 0.00100 1 12/23/2015 07:36 WG837923
1,1,1-Trichloroethane ND 0.00100 1 12/23/2015 07:36 WG837923
1,1,2-Trichloroethane ND 0.00100 1 12/23/2015 07:36 WG837923
Trichloroethene ND 0.00100 1 12/23/2015 07:36 WG837923
Trichlorofluoromethane ND 0.00500 1 12/23/2015 07:36 WG837923
1,2,3-Trichloropropane ND 0.00250 1 12/23/2015 07:36 WG837923
1,2,4-Trimethylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
1,2,3-Trimethylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
1,3,5-Trimethylbenzene ND 0.00100 1 12/23/2015 07:36 WG837923
Vinyl chloride ND 0.00100 1 12/23/2015 07:36 WG837923
Xylenes, Total ND 0.00300 1 12/23/2015 07:36 WG837923
(S) Toluene-d8 106 90.0-115 12/23/2015 07:36 WG837923
(S) Dibromofluoromethane 103 79.0-121 12/23/2015 07:36 WG837923
(S) 4-Bromofluorobenzene 104 80.1-120 12/23/2015 07:36 WG837923
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L806319
MW-19
Collected date/time: 12/10/15 10:30
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
Acetone ND J3 0.0500 1 12/23/2015 07:57 WG837923
Acrolein ND 0.0500 1 12/23/2015 07:57 WG837923
Acrylonitrile ND 0.0100 1 12/23/2015 07:57 WG837923
Benzene ND 0.00100 1 12/23/2015 07:57 WG837923
Bromobenzene ND 0.00100 1 12/23/2015 07:57 WG837923
Bromodichloromethane ND 0.00100 1 12/23/2015 07:57 WG837923
Bromoform ND 0.00100 1 12/23/2015 07:57 WG837923
Bromomethane ND 0.00500 1 12/23/2015 07:57 WG837923
n-Butylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
sec-Butylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
tert-Butylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
Carbon tetrachloride ND 0.00100 1 12/23/2015 07:57 WG837923
Chlorobenzene ND 0.00100 1 12/23/2015 07:57 WG837923
Chlorodibromomethane ND 0.00100 1 12/23/2015 07:57 WG837923
Chloroethane ND 0.00500 1 12/23/2015 07:57 WG837923
2-Chloroethyl vinyl ether ND 0.0500 1 12/23/2015 07:57 WG837923
Chloroform ND 0.00500 1 12/23/2015 07:57 WG837923
Chloromethane ND 0.00250 1 12/23/2015 07:57 WG837923
2-Chlorotoluene ND 0.00100 1 12/23/2015 07:57 WG837923
4-Chlorotoluene ND 0.00100 1 12/23/2015 07:57 WG837923
1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/23/2015 07:57 WG837923
1,2-Dibromoethane ND 0.00100 1 12/23/2015 07:57 WG837923
Dibromomethane ND 0.00100 1 12/23/2015 07:57 WG837923
1,2-Dichlorobenzene ND 0.00100 1 12/23/2015 07:57 WG837923
1,3-Dichlorobenzene ND 0.00100 1 12/23/2015 07:57 WG837923
1,4-Dichlorobenzene ND 0.00100 1 12/23/2015 07:57 WG837923
Dichlorodifluoromethane ND 0.00500 1 12/23/2015 07:57 WG837923
1,1-Dichloroethane ND 0.00100 1 12/23/2015 07:57 WG837923
1,2-Dichloroethane ND 0.00100 1 12/23/2015 07:57 WG837923
1,1-Dichloroethene ND 0.00100 1 12/23/2015 07:57 WG837923
cis-1,2-Dichloroethene ND 0.00100 1 12/23/2015 07:57 WG837923
trans-1,2-Dichloroethene ND 0.00100 1 12/23/2015 07:57 WG837923
1,2-Dichloropropane ND 0.00100 1 12/23/2015 07:57 WG837923
1,1-Dichloropropene ND 0.00100 1 12/23/2015 07:57 WG837923
1,3-Dichloropropane ND 0.00100 1 12/23/2015 07:57 WG837923
cis-1,3-Dichloropropene ND 0.00100 1 12/23/2015 07:57 WG837923
trans-1,3-Dichloropropene ND 0.00100 1 12/23/2015 07:57 WG837923
2,2-Dichloropropane ND 0.00100 1 12/23/2015 07:57 WG837923
Di-isopropyl ether ND 0.00100 1 12/23/2015 07:57 WG837923
Ethylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
Hexachloro-1,3-butadiene ND 0.00100 1 12/23/2015 07:57 WG837923
Isopropylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
p-Isopropyltoluene ND 0.00100 1 12/23/2015 07:57 WG837923
2-Butanone (MEK)ND J3 0.0100 1 12/23/2015 07:57 WG837923
Methylene Chloride ND 0.00500 1 12/23/2015 07:57 WG837923
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/23/2015 07:57 WG837923
Methyl tert-butyl ether ND 0.00100 1 12/23/2015 07:57 WG837923
Naphthalene ND 0.00500 1 12/23/2015 07:57 WG837923
n-Propylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
Styrene ND 0.00100 1 12/23/2015 07:57 WG837923
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/23/2015 07:57 WG837923
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/23/2015 07:57 WG837923
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/23/2015 07:57 WG837923
Tetrachloroethene 0.00211 0.00100 1 12/23/2015 07:57 WG837923
Toluene ND 0.00500 1 12/23/2015 07:57 WG837923
1,2,3-Trichlorobenzene ND 0.00100 1 12/23/2015 07:57 WG837923
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L806319
MW-19
Collected date/time: 12/10/15 10:30
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
1,2,4-Trichlorobenzene ND 0.00100 1 12/23/2015 07:57 WG837923
1,1,1-Trichloroethane ND 0.00100 1 12/23/2015 07:57 WG837923
1,1,2-Trichloroethane ND 0.00100 1 12/23/2015 07:57 WG837923
Trichloroethene ND 0.00100 1 12/23/2015 07:57 WG837923
Trichlorofluoromethane ND 0.00500 1 12/23/2015 07:57 WG837923
1,2,3-Trichloropropane ND 0.00250 1 12/23/2015 07:57 WG837923
1,2,4-Trimethylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
1,2,3-Trimethylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
1,3,5-Trimethylbenzene ND 0.00100 1 12/23/2015 07:57 WG837923
Vinyl chloride ND 0.00100 1 12/23/2015 07:57 WG837923
Xylenes, Total ND 0.00300 1 12/23/2015 07:57 WG837923
(S) Toluene-d8 106 90.0-115 12/23/2015 07:57 WG837923
(S) Dibromofluoromethane 103 79.0-121 12/23/2015 07:57 WG837923
(S) 4-Bromofluorobenzene 103 80.1-120 12/23/2015 07:57 WG837923
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:52 10 of 33
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L806319
MW-23
Collected date/time: 12/10/15 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
Acetone ND 0.0500 1 12/20/2015 14:19 WG835361
Acrolein ND 0.0500 1 12/20/2015 14:19 WG835361
Acrylonitrile ND 0.0100 1 12/20/2015 14:19 WG835361
Benzene ND 0.00100 1 12/20/2015 14:19 WG835361
Bromobenzene ND 0.00100 1 12/20/2015 14:19 WG835361
Bromodichloromethane ND J4 0.00100 1 12/20/2015 14:19 WG835361
Bromoform ND 0.00100 1 12/20/2015 14:19 WG835361
Bromomethane ND 0.00500 1 12/20/2015 14:19 WG835361
n-Butylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
sec-Butylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
tert-Butylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
Carbon tetrachloride ND 0.00100 1 12/20/2015 14:19 WG835361
Chlorobenzene ND 0.00100 1 12/20/2015 14:19 WG835361
Chlorodibromomethane ND 0.00100 1 12/20/2015 14:19 WG835361
Chloroethane ND 0.00500 1 12/20/2015 14:19 WG835361
2-Chloroethyl vinyl ether ND J4 0.0500 1 12/20/2015 14:19 WG835361
Chloroform ND 0.00500 1 12/20/2015 14:19 WG835361
Chloromethane ND 0.00250 1 12/20/2015 14:19 WG835361
2-Chlorotoluene ND 0.00100 1 12/20/2015 14:19 WG835361
4-Chlorotoluene ND 0.00100 1 12/20/2015 14:19 WG835361
1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/20/2015 14:19 WG835361
1,2-Dibromoethane ND 0.00100 1 12/20/2015 14:19 WG835361
Dibromomethane ND 0.00100 1 12/20/2015 14:19 WG835361
1,2-Dichlorobenzene ND 0.00100 1 12/20/2015 14:19 WG835361
1,3-Dichlorobenzene ND 0.00100 1 12/20/2015 14:19 WG835361
1,4-Dichlorobenzene ND 0.00100 1 12/20/2015 14:19 WG835361
Dichlorodifluoromethane ND 0.00500 1 12/20/2015 14:19 WG835361
1,1-Dichloroethane ND 0.00100 1 12/20/2015 14:19 WG835361
1,2-Dichloroethane ND J4 0.00100 1 12/20/2015 14:19 WG835361
1,1-Dichloroethene ND 0.00100 1 12/20/2015 14:19 WG835361
cis-1,2-Dichloroethene ND 0.00100 1 12/20/2015 14:19 WG835361
trans-1,2-Dichloroethene ND 0.00100 1 12/20/2015 14:19 WG835361
1,2-Dichloropropane ND 0.00100 1 12/20/2015 14:19 WG835361
1,1-Dichloropropene ND 0.00100 1 12/20/2015 14:19 WG835361
1,3-Dichloropropane ND 0.00100 1 12/20/2015 14:19 WG835361
cis-1,3-Dichloropropene ND 0.00100 1 12/20/2015 14:19 WG835361
trans-1,3-Dichloropropene ND 0.00100 1 12/20/2015 14:19 WG835361
2,2-Dichloropropane ND J4 0.00100 1 12/20/2015 14:19 WG835361
Di-isopropyl ether ND 0.00100 1 12/20/2015 14:19 WG835361
Ethylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
Hexachloro-1,3-butadiene ND 0.00100 1 12/20/2015 14:19 WG835361
Isopropylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
p-Isopropyltoluene ND 0.00100 1 12/20/2015 14:19 WG835361
2-Butanone (MEK)ND 0.0100 1 12/20/2015 14:19 WG835361
Methylene Chloride ND 0.00500 1 12/20/2015 14:19 WG835361
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/20/2015 14:19 WG835361
Methyl tert-butyl ether ND 0.00100 1 12/20/2015 14:19 WG835361
Naphthalene ND 0.00500 1 12/20/2015 14:19 WG835361
n-Propylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
Styrene ND 0.00100 1 12/20/2015 14:19 WG835361
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/20/2015 14:19 WG835361
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/20/2015 14:19 WG835361
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/20/2015 14:19 WG835361
Tetrachloroethene 0.0253 0.00100 1 12/20/2015 14:19 WG835361
Toluene ND 0.00500 1 12/20/2015 14:19 WG835361
1,2,3-Trichlorobenzene ND 0.00100 1 12/20/2015 14:19 WG835361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:18 11 of 33
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:52 11 of 33
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L806319
MW-23
Collected date/time: 12/10/15 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
1,2,4-Trichlorobenzene ND 0.00100 1 12/20/2015 14:19 WG835361
1,1,1-Trichloroethane ND 0.00100 1 12/20/2015 14:19 WG835361
1,1,2-Trichloroethane ND 0.00100 1 12/20/2015 14:19 WG835361
Trichloroethene ND 0.00100 1 12/20/2015 14:19 WG835361
Trichlorofluoromethane ND 0.00500 1 12/20/2015 14:19 WG835361
1,2,3-Trichloropropane ND 0.00250 1 12/20/2015 14:19 WG835361
1,2,4-Trimethylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
1,2,3-Trimethylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
1,3,5-Trimethylbenzene ND 0.00100 1 12/20/2015 14:19 WG835361
Vinyl chloride ND 0.00100 1 12/20/2015 14:19 WG835361
Xylenes, Total ND 0.00300 1 12/20/2015 14:19 WG835361
(S) Toluene-d8 106 90.0-115 12/20/2015 14:19 WG835361
(S) Dibromofluoromethane 115 79.0-121 12/20/2015 14:19 WG835361
(S) 4-Bromofluorobenzene 96.9 80.1-120 12/20/2015 14:19 WG835361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:18 12 of 33
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:52 12 of 33
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L806319
MW-18
Collected date/time: 12/10/15 11:25
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
Acetone ND 0.0500 1 12/20/2015 14:39 WG835361
Acrolein ND 0.0500 1 12/20/2015 14:39 WG835361
Acrylonitrile ND 0.0100 1 12/20/2015 14:39 WG835361
Benzene ND 0.00100 1 12/20/2015 14:39 WG835361
Bromobenzene ND 0.00100 1 12/20/2015 14:39 WG835361
Bromodichloromethane ND J4 0.00100 1 12/20/2015 14:39 WG835361
Bromoform ND 0.00100 1 12/20/2015 14:39 WG835361
Bromomethane ND 0.00500 1 12/20/2015 14:39 WG835361
n-Butylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
sec-Butylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
tert-Butylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
Carbon tetrachloride ND 0.00100 1 12/20/2015 14:39 WG835361
Chlorobenzene ND 0.00100 1 12/20/2015 14:39 WG835361
Chlorodibromomethane ND 0.00100 1 12/20/2015 14:39 WG835361
Chloroethane ND 0.00500 1 12/20/2015 14:39 WG835361
2-Chloroethyl vinyl ether ND J4 0.0500 1 12/20/2015 14:39 WG835361
Chloroform ND 0.00500 1 12/20/2015 14:39 WG835361
Chloromethane ND 0.00250 1 12/20/2015 14:39 WG835361
2-Chlorotoluene ND 0.00100 1 12/20/2015 14:39 WG835361
4-Chlorotoluene ND 0.00100 1 12/20/2015 14:39 WG835361
1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/20/2015 14:39 WG835361
1,2-Dibromoethane ND 0.00100 1 12/20/2015 14:39 WG835361
Dibromomethane ND 0.00100 1 12/20/2015 14:39 WG835361
1,2-Dichlorobenzene ND 0.00100 1 12/20/2015 14:39 WG835361
1,3-Dichlorobenzene ND 0.00100 1 12/20/2015 14:39 WG835361
1,4-Dichlorobenzene ND 0.00100 1 12/20/2015 14:39 WG835361
Dichlorodifluoromethane ND 0.00500 1 12/20/2015 14:39 WG835361
1,1-Dichloroethane ND 0.00100 1 12/20/2015 14:39 WG835361
1,2-Dichloroethane ND J4 0.00100 1 12/20/2015 14:39 WG835361
1,1-Dichloroethene ND 0.00100 1 12/20/2015 14:39 WG835361
cis-1,2-Dichloroethene ND 0.00100 1 12/20/2015 14:39 WG835361
trans-1,2-Dichloroethene ND 0.00100 1 12/20/2015 14:39 WG835361
1,2-Dichloropropane ND 0.00100 1 12/20/2015 14:39 WG835361
1,1-Dichloropropene ND 0.00100 1 12/20/2015 14:39 WG835361
1,3-Dichloropropane ND 0.00100 1 12/20/2015 14:39 WG835361
cis-1,3-Dichloropropene ND 0.00100 1 12/20/2015 14:39 WG835361
trans-1,3-Dichloropropene ND 0.00100 1 12/20/2015 14:39 WG835361
2,2-Dichloropropane ND J4 0.00100 1 12/20/2015 14:39 WG835361
Di-isopropyl ether ND 0.00100 1 12/20/2015 14:39 WG835361
Ethylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
Hexachloro-1,3-butadiene ND 0.00100 1 12/20/2015 14:39 WG835361
Isopropylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
p-Isopropyltoluene ND 0.00100 1 12/20/2015 14:39 WG835361
2-Butanone (MEK)ND 0.0100 1 12/20/2015 14:39 WG835361
Methylene Chloride ND 0.00500 1 12/20/2015 14:39 WG835361
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/20/2015 14:39 WG835361
Methyl tert-butyl ether ND 0.00100 1 12/20/2015 14:39 WG835361
Naphthalene ND 0.00500 1 12/20/2015 14:39 WG835361
n-Propylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
Styrene ND 0.00100 1 12/20/2015 14:39 WG835361
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/20/2015 14:39 WG835361
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/20/2015 14:39 WG835361
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/20/2015 14:39 WG835361
Tetrachloroethene 0.127 0.00100 1 12/20/2015 14:39 WG835361
Toluene ND 0.00500 1 12/20/2015 14:39 WG835361
1,2,3-Trichlorobenzene ND 0.00100 1 12/20/2015 14:39 WG835361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:18 13 of 33
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:52 13 of 33
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L806319
MW-18
Collected date/time: 12/10/15 11:25
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
1,2,4-Trichlorobenzene ND 0.00100 1 12/20/2015 14:39 WG835361
1,1,1-Trichloroethane ND 0.00100 1 12/20/2015 14:39 WG835361
1,1,2-Trichloroethane ND 0.00100 1 12/20/2015 14:39 WG835361
Trichloroethene ND 0.00100 1 12/20/2015 14:39 WG835361
Trichlorofluoromethane ND 0.00500 1 12/20/2015 14:39 WG835361
1,2,3-Trichloropropane ND 0.00250 1 12/20/2015 14:39 WG835361
1,2,4-Trimethylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
1,2,3-Trimethylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
1,3,5-Trimethylbenzene ND 0.00100 1 12/20/2015 14:39 WG835361
Vinyl chloride ND 0.00100 1 12/20/2015 14:39 WG835361
Xylenes, Total ND 0.00300 1 12/20/2015 14:39 WG835361
(S) Toluene-d8 107 90.0-115 12/20/2015 14:39 WG835361
(S) Dibromofluoromethane 115 79.0-121 12/20/2015 14:39 WG835361
(S) 4-Bromofluorobenzene 97.0 80.1-120 12/20/2015 14:39 WG835361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:18 14 of 33
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:52 14 of 33
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L806319
MW-22D
Collected date/time: 12/10/15 11:55
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
Acetone ND 0.0500 1 12/20/2015 13:40 WG835361
Acrolein ND 0.0500 1 12/20/2015 13:40 WG835361
Acrylonitrile ND 0.0100 1 12/20/2015 13:40 WG835361
Benzene ND 0.00100 1 12/20/2015 13:40 WG835361
Bromobenzene ND 0.00100 1 12/20/2015 13:40 WG835361
Bromodichloromethane ND J4 J5 0.00100 1 12/20/2015 13:40 WG835361
Bromoform ND 0.00100 1 12/20/2015 13:40 WG835361
Bromomethane ND 0.00500 1 12/20/2015 13:40 WG835361
n-Butylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
sec-Butylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
tert-Butylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
Carbon tetrachloride ND 0.00100 1 12/20/2015 13:40 WG835361
Chlorobenzene ND 0.00100 1 12/20/2015 13:40 WG835361
Chlorodibromomethane ND 0.00100 1 12/20/2015 13:40 WG835361
Chloroethane ND 0.00500 1 12/20/2015 13:40 WG835361
2-Chloroethyl vinyl ether ND J4 J6 0.0500 1 12/20/2015 13:40 WG835361
Chloroform ND 0.00500 1 12/20/2015 13:40 WG835361
Chloromethane ND 0.00250 1 12/20/2015 13:40 WG835361
2-Chlorotoluene ND 0.00100 1 12/20/2015 13:40 WG835361
4-Chlorotoluene ND 0.00100 1 12/20/2015 13:40 WG835361
1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/20/2015 13:40 WG835361
1,2-Dibromoethane ND 0.00100 1 12/20/2015 13:40 WG835361
Dibromomethane ND 0.00100 1 12/20/2015 13:40 WG835361
1,2-Dichlorobenzene ND 0.00100 1 12/20/2015 13:40 WG835361
1,3-Dichlorobenzene ND 0.00100 1 12/20/2015 13:40 WG835361
1,4-Dichlorobenzene ND 0.00100 1 12/20/2015 13:40 WG835361
Dichlorodifluoromethane ND J5 0.00500 1 12/20/2015 13:40 WG835361
1,1-Dichloroethane ND 0.00100 1 12/20/2015 13:40 WG835361
1,2-Dichloroethane ND J4 J5 0.00100 1 12/20/2015 13:40 WG835361
1,1-Dichloroethene ND 0.00100 1 12/20/2015 13:40 WG835361
cis-1,2-Dichloroethene ND 0.00100 1 12/20/2015 13:40 WG835361
trans-1,2-Dichloroethene ND 0.00100 1 12/20/2015 13:40 WG835361
1,2-Dichloropropane ND 0.00100 1 12/20/2015 13:40 WG835361
1,1-Dichloropropene ND 0.00100 1 12/20/2015 13:40 WG835361
1,3-Dichloropropane ND 0.00100 1 12/20/2015 13:40 WG835361
cis-1,3-Dichloropropene ND 0.00100 1 12/20/2015 13:40 WG835361
trans-1,3-Dichloropropene ND 0.00100 1 12/20/2015 13:40 WG835361
2,2-Dichloropropane ND J4 J5 0.00100 1 12/20/2015 13:40 WG835361
Di-isopropyl ether ND 0.00100 1 12/20/2015 13:40 WG835361
Ethylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
Hexachloro-1,3-butadiene ND 0.00100 1 12/20/2015 13:40 WG835361
Isopropylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
p-Isopropyltoluene ND 0.00100 1 12/20/2015 13:40 WG835361
2-Butanone (MEK)ND 0.0100 1 12/20/2015 13:40 WG835361
Methylene Chloride ND 0.00500 1 12/20/2015 13:40 WG835361
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/20/2015 13:40 WG835361
Methyl tert-butyl ether ND 0.00100 1 12/20/2015 13:40 WG835361
Naphthalene ND 0.00500 1 12/20/2015 13:40 WG835361
n-Propylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
Styrene ND 0.00100 1 12/20/2015 13:40 WG835361
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/20/2015 13:40 WG835361
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/20/2015 13:40 WG835361
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/20/2015 13:40 WG835361
Tetrachloroethene 0.161 V 0.00100 1 12/20/2015 13:40 WG835361
Toluene ND 0.00500 1 12/20/2015 13:40 WG835361
1,2,3-Trichlorobenzene ND 0.00100 1 12/20/2015 13:40 WG835361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:18 15 of 33
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Griffith Enterprise L806319 12/23/15 12:52 15 of 33
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L806319
MW-22D
Collected date/time: 12/10/15 11:55
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
1,2,4-Trichlorobenzene ND 0.00100 1 12/20/2015 13:40 WG835361
1,1,1-Trichloroethane ND J5 0.00100 1 12/20/2015 13:40 WG835361
1,1,2-Trichloroethane ND 0.00100 1 12/20/2015 13:40 WG835361
Trichloroethene ND 0.00100 1 12/20/2015 13:40 WG835361
Trichlorofluoromethane ND 0.00500 1 12/20/2015 13:40 WG835361
1,2,3-Trichloropropane ND 0.00250 1 12/20/2015 13:40 WG835361
1,2,4-Trimethylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
1,2,3-Trimethylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
1,3,5-Trimethylbenzene ND 0.00100 1 12/20/2015 13:40 WG835361
Vinyl chloride ND 0.00100 1 12/20/2015 13:40 WG835361
Xylenes, Total ND 0.00300 1 12/20/2015 13:40 WG835361
(S) Toluene-d8 105 90.0-115 12/20/2015 13:40 WG835361
(S) Dibromofluoromethane 115 79.0-121 12/20/2015 13:40 WG835361
(S) 4-Bromofluorobenzene 96.2 80.1-120 12/20/2015 13:40 WG835361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L806319
MW-25
Collected date/time: 12/10/15 12:35
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
Acetone ND 0.0500 1 12/20/2015 14:59 WG835361
Acrolein ND 0.0500 1 12/20/2015 14:59 WG835361
Acrylonitrile ND 0.0100 1 12/20/2015 14:59 WG835361
Benzene ND 0.00100 1 12/20/2015 14:59 WG835361
Bromobenzene ND 0.00100 1 12/20/2015 14:59 WG835361
Bromodichloromethane ND J4 0.00100 1 12/20/2015 14:59 WG835361
Bromoform ND 0.00100 1 12/20/2015 14:59 WG835361
Bromomethane ND 0.00500 1 12/20/2015 14:59 WG835361
n-Butylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
sec-Butylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
tert-Butylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
Carbon tetrachloride ND 0.00100 1 12/20/2015 14:59 WG835361
Chlorobenzene ND 0.00100 1 12/20/2015 14:59 WG835361
Chlorodibromomethane ND 0.00100 1 12/20/2015 14:59 WG835361
Chloroethane ND 0.00500 1 12/20/2015 14:59 WG835361
2-Chloroethyl vinyl ether ND J4 0.0500 1 12/20/2015 14:59 WG835361
Chloroform ND 0.00500 1 12/20/2015 14:59 WG835361
Chloromethane ND 0.00250 1 12/20/2015 14:59 WG835361
2-Chlorotoluene ND 0.00100 1 12/20/2015 14:59 WG835361
4-Chlorotoluene ND 0.00100 1 12/20/2015 14:59 WG835361
1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/20/2015 14:59 WG835361
1,2-Dibromoethane ND 0.00100 1 12/20/2015 14:59 WG835361
Dibromomethane ND 0.00100 1 12/20/2015 14:59 WG835361
1,2-Dichlorobenzene ND 0.00100 1 12/20/2015 14:59 WG835361
1,3-Dichlorobenzene ND 0.00100 1 12/20/2015 14:59 WG835361
1,4-Dichlorobenzene ND 0.00100 1 12/20/2015 14:59 WG835361
Dichlorodifluoromethane ND 0.00500 1 12/20/2015 14:59 WG835361
1,1-Dichloroethane ND 0.00100 1 12/20/2015 14:59 WG835361
1,2-Dichloroethane ND J4 0.00100 1 12/20/2015 14:59 WG835361
1,1-Dichloroethene ND 0.00100 1 12/20/2015 14:59 WG835361
cis-1,2-Dichloroethene 0.446 0.0200 20 12/23/2015 08:16 WG837923
trans-1,2-Dichloroethene 0.00800 0.00100 1 12/20/2015 14:59 WG835361
1,2-Dichloropropane ND 0.00100 1 12/20/2015 14:59 WG835361
1,1-Dichloropropene ND 0.00100 1 12/20/2015 14:59 WG835361
1,3-Dichloropropane ND 0.00100 1 12/20/2015 14:59 WG835361
cis-1,3-Dichloropropene ND 0.00100 1 12/20/2015 14:59 WG835361
trans-1,3-Dichloropropene ND 0.00100 1 12/20/2015 14:59 WG835361
2,2-Dichloropropane ND J4 0.00100 1 12/20/2015 14:59 WG835361
Di-isopropyl ether ND 0.00100 1 12/20/2015 14:59 WG835361
Ethylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
Hexachloro-1,3-butadiene ND 0.00100 1 12/20/2015 14:59 WG835361
Isopropylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
p-Isopropyltoluene ND 0.00100 1 12/20/2015 14:59 WG835361
2-Butanone (MEK)ND 0.0100 1 12/20/2015 14:59 WG835361
Methylene Chloride ND 0.00500 1 12/20/2015 14:59 WG835361
4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/20/2015 14:59 WG835361
Methyl tert-butyl ether ND 0.00100 1 12/20/2015 14:59 WG835361
Naphthalene ND 0.00500 1 12/20/2015 14:59 WG835361
n-Propylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
Styrene ND 0.00100 1 12/20/2015 14:59 WG835361
1,1,1,2-Tetrachloroethane ND 0.00100 1 12/20/2015 14:59 WG835361
1,1,2,2-Tetrachloroethane ND 0.00100 1 12/20/2015 14:59 WG835361
1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/20/2015 14:59 WG835361
Tetrachloroethene 0.738 0.0200 20 12/23/2015 08:16 WG837923
Toluene ND 0.00500 1 12/20/2015 14:59 WG835361
1,2,3-Trichlorobenzene ND 0.00100 1 12/20/2015 14:59 WG835361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L806319
MW-25
Collected date/time: 12/10/15 12:35
Volatile Organic Compounds (GC/MS) by Method 8260B
5eVXlt 4XaliIieU 5'L 'ilXtioQ $Qal\ViV %atcK
$Qal\te mg/l mg/l date / time
1,2,4-Trichlorobenzene ND 0.00100 1 12/20/2015 14:59 WG835361
1,1,1-Trichloroethane ND 0.00100 1 12/20/2015 14:59 WG835361
1,1,2-Trichloroethane ND 0.00100 1 12/20/2015 14:59 WG835361
Trichloroethene 0.163 0.00100 1 12/20/2015 14:59 WG835361
Trichlorofluoromethane ND 0.00500 1 12/20/2015 14:59 WG835361
1,2,3-Trichloropropane ND 0.00250 1 12/20/2015 14:59 WG835361
1,2,4-Trimethylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
1,2,3-Trimethylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
1,3,5-Trimethylbenzene ND 0.00100 1 12/20/2015 14:59 WG835361
Vinyl chloride ND 0.00100 1 12/20/2015 14:59 WG835361
Xylenes, Total ND 0.00300 1 12/20/2015 14:59 WG835361
(S) Toluene-d8 102 90.0-115 12/20/2015 14:59 WG835361
(S) Dibromofluoromethane 114 79.0-121 12/20/2015 14:59 WG835361
(S) 4-Bromofluorobenzene 93.2 80.1-120 12/20/2015 14:59 WG835361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG835361
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-04,05,06,07
Method Blank (MB)
(MB) 12/20/15 10:18
0% 5eVXlt 0% 4XaliIieU 0% 5'L
$Qal\te mg/l mg/l
Acetone ND 0.0500
Acrolein ND 0.0500
Acrylonitrile ND 0.0100
Benzene ND 0.00100
Bromobenzene ND 0.00100
Bromodichloromethane ND 0.00100
Bromoform ND 0.00100
Bromomethane ND 0.00500
n-Butylbenzene ND 0.00100
sec-Butylbenzene ND 0.00100
tert-Butylbenzene ND 0.00100
Carbon tetrachloride ND 0.00100
Chlorobenzene ND 0.00100
Chlorodibromomethane ND 0.00100
Chloroethane ND 0.00500
2-Chloroethyl vinyl ether ND 0.0500
Chloroform ND 0.00500
Chloromethane ND 0.00250
2-Chlorotoluene ND 0.00100
4-Chlorotoluene ND 0.00100
1,2-Dibromo-3-Chloropropane ND 0.00500
1,2-Dibromoethane ND 0.00100
Dibromomethane ND 0.00100
1,2-Dichlorobenzene ND 0.00100
1,3-Dichlorobenzene ND 0.00100
1,4-Dichlorobenzene ND 0.00100
Dichlorodifluoromethane ND 0.00500
1,1-Dichloroethane ND 0.00100
1,2-Dichloroethane ND 0.00100
1,1-Dichloroethene ND 0.00100
cis-1,2-Dichloroethene ND 0.00100
trans-1,2-Dichloroethene ND 0.00100
1,2-Dichloropropane ND 0.00100
1,1-Dichloropropene ND 0.00100
1,3-Dichloropropane ND 0.00100
cis-1,3-Dichloropropene ND 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG835361
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-04,05,06,07
Method Blank (MB)
(MB) 12/20/15 10:18
0% 5eVXlt 0% 4XaliIieU 0% 5'L
$Qal\te mg/l mg/l
trans-1,3-Dichloropropene ND 0.00100
2,2-Dichloropropane ND 0.00100
Di-isopropyl ether ND 0.00100
Ethylbenzene ND 0.00100
Hexachloro-1,3-butadiene ND 0.00100
Isopropylbenzene ND 0.00100
p-Isopropyltoluene ND 0.00100
2-Butanone (MEK)ND 0.0100
Methylene Chloride ND 0.00500
4-Methyl-2-pentanone (MIBK)ND 0.0100
Methyl tert-butyl ether ND 0.00100
Naphthalene ND 0.00500
Tetrachloroethene ND 0.00100
n-Propylbenzene ND 0.00100
Styrene ND 0.00100
1,1,1,2-Tetrachloroethane ND 0.00100
1,1,2,2-Tetrachloroethane ND 0.00100
Toluene ND 0.00500
1,1,2-Trichlorotrifluoroethane ND 0.00100
1,2,3-Trichlorobenzene ND 0.00100
1,2,4-Trichlorobenzene ND 0.00100
1,1,1-Trichloroethane ND 0.00100
1,1,2-Trichloroethane ND 0.00100
Trichloroethene ND 0.00100
Trichlorofluoromethane ND 0.00500
1,2,3-Trichloropropane ND 0.00250
1,2,3-Trimethylbenzene ND 0.00100
1,2,4-Trimethylbenzene ND 0.00100
1,3,5-Trimethylbenzene ND 0.00100
Vinyl chloride ND 0.00100
Xylenes, Total ND 0.00300
(S) Toluene-d8 104 90.0-115
(S) Dibromofluoromethane 113 79.0-121
(S) 4-Bromofluorobenzene 95.3 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG835361
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 12/20/15 03:22 • (LCSD) 12/20/15 07:37
6SiNe $moXQt LC6 5eVXlt LC6' 5eVXlt LC6 5ec LC6' 5ec 5ec LimitV LC6 4XaliIieU LC6' 4XaliIieU 53' 53' LimitV
$Qal\te mg/l mg/l mg/l % % %% %
Acetone 0.125 0.144 0.155 115 124 28.7-175 7.45 20.9
Acrolein 0.125 0.0990 0.106 79.2 85.1 40.4-172 7.10 20
Acrylonitrile 0.125 0.128 0.137 103 109 58.2-145 6.30 20
Benzene 0.0250 0.0254 0.0252 102 101 73.0-122 0.940 20
Bromobenzene 0.0250 0.0264 0.0250 106 100 81.5-115 5.18 20
Bromodichloromethane 0.0250 0.0319 0.0306 127 122 75.5-121 J4 J4 4.17 20
Bromoform 0.0250 0.0235 0.0235 94.0 94.0 71.5-131 0.0500 20
Bromomethane 0.0250 0.0231 0.0213 92.4 85.3 22.4-187 8.00 20
n-Butylbenzene 0.0250 0.0314 0.0302 126 121 75.9-134 3.92 20
sec-Butylbenzene 0.0250 0.0274 0.0257 110 103 80.6-126 6.32 20
tert-Butylbenzene 0.0250 0.0266 0.0248 106 99.3 79.3-127 7.00 20
Carbon tetrachloride 0.0250 0.0307 0.0300 123 120 70.9-129 2.25 20
Chlorobenzene 0.0250 0.0237 0.0225 94.9 90.1 79.7-122 5.19 20
Chlorodibromomethane 0.0250 0.0266 0.0259 106 103 78.2-124 2.82 20
Chloroethane 0.0250 0.0252 0.0238 101 95.4 41.2-153 5.44 20
2-Chloroethyl vinyl ether 0.125 0.222 0.226 177 181 23.4-162 J4 J4 1.95 23.5
Chloroform 0.0250 0.0300 0.0297 120 119 73.2-125 1.05 20
Chloromethane 0.0250 0.0272 0.0253 109 101 55.8-134 7.24 20
2-Chlorotoluene 0.0250 0.0254 0.0242 102 97.0 76.4-125 4.73 20
4-Chlorotoluene 0.0250 0.0266 0.0254 106 102 81.5-121 4.58 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0214 0.0237 85.5 94.6 64.8-131 10.1 20
1,2-Dibromoethane 0.0250 0.0235 0.0233 93.8 93.2 79.8-122 0.610 20
Dibromomethane 0.0250 0.0286 0.0278 114 111 79.5-118 2.72 20
1,2-Dichlorobenzene 0.0250 0.0257 0.0253 103 101 84.7-118 1.57 20
1,3-Dichlorobenzene 0.0250 0.0249 0.0231 99.4 92.4 77.6-127 7.29 20
1,4-Dichlorobenzene 0.0250 0.0253 0.0249 101 99.6 82.2-114 1.78 20
Dichlorodifluoromethane 0.0250 0.0322 0.0307 129 123 56.0-134 4.76 20
1,1-Dichloroethane 0.0250 0.0284 0.0284 113 114 71.7-127 0.120 20
1,2-Dichloroethane 0.0250 0.0331 0.0331 132 133 65.3-126 J4 J4 0.140 20
1,1-Dichloroethene 0.0250 0.0292 0.0283 117 113 59.9-137 3.26 20
cis-1,2-Dichloroethene 0.0250 0.0257 0.0255 103 102 77.3-122 1.03 20
trans-1,2-Dichloroethene 0.0250 0.0252 0.0246 101 98.6 72.6-125 2.24 20
1,2-Dichloropropane 0.0250 0.0281 0.0276 112 111 77.4-125 1.60 20
1,1-Dichloropropene 0.0250 0.0286 0.0280 114 112 72.5-127 2.23 20
1,3-Dichloropropane 0.0250 0.0241 0.0242 96.3 97.0 80.6-115 0.690 20
cis-1,3-Dichloropropene 0.0250 0.0294 0.0286 118 114 77.7-124 2.98 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG835361
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 12/20/15 03:22 • (LCSD) 12/20/15 07:37
6SiNe $moXQt LC6 5eVXlt LC6' 5eVXlt LC6 5ec LC6' 5ec 5ec LimitV LC6 4XaliIieU LC6' 4XaliIieU 53' 53' LimitV
$Qal\te mg/l mg/l mg/l % % %% %
trans-1,3-Dichloropropene 0.0250 0.0279 0.0277 112 111 73.5-127 0.730 20
2,2-Dichloropropane 0.0250 0.0343 0.0339 137 135 61.3-134 J4 J4 1.31 20
Di-isopropyl ether 0.0250 0.0301 0.0302 120 121 65.1-135 0.610 20
Ethylbenzene 0.0250 0.0225 0.0218 90.0 87.1 80.9-121 3.35 20
Hexachloro-1,3-butadiene 0.0250 0.0258 0.0243 103 97.4 73.7-133 5.88 20
Isopropylbenzene 0.0250 0.0260 0.0247 104 98.6 81.6-124 5.26 20
p-Isopropyltoluene 0.0250 0.0278 0.0257 111 103 77.6-129 7.68 20
2-Butanone (MEK)0.125 0.133 0.144 106 115 46.4-155 8.26 20
Methylene Chloride 0.0250 0.0223 0.0223 89.1 89.4 69.5-120 0.280 20
4-Methyl-2-pentanone (MIBK)0.125 0.142 0.148 114 118 63.3-138 3.99 20
Methyl tert-butyl ether 0.0250 0.0262 0.0272 105 109 70.1-125 3.54 20
Naphthalene 0.0250 0.0232 0.0232 92.7 92.9 69.7-134 0.280 20
n-Propylbenzene 0.0250 0.0254 0.0242 101 96.8 81.9-122 4.72 20
Styrene 0.0250 0.0251 0.0240 100 96.2 79.9-124 4.33 20
1,1,1,2-Tetrachloroethane 0.0250 0.0261 0.0252 105 101 78.5-125 3.61 20
Tetrachloroethene 0.0250 0.0230 0.0226 92.1 90.2 73.5-130 2.00 20
1,1,2,2-Tetrachloroethane 0.0250 0.0238 0.0241 95.3 96.2 79.3-123 0.910 20
Toluene 0.0250 0.0257 0.0247 103 98.7 77.9-116 4.11 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0183 0.0165 73.2 65.9 62.0-141 10.5 20
1,2,3-Trichlorobenzene 0.0250 0.0253 0.0239 101 95.7 75.7-134 5.74 20
1,2,4-Trichlorobenzene 0.0250 0.0269 0.0255 108 102 76.1-136 5.26 20
1,1,1-Trichloroethane 0.0250 0.0321 0.0313 128 125 71.1-129 2.58 20
1,1,2-Trichloroethane 0.0250 0.0236 0.0231 94.4 92.3 81.6-120 2.21 20
Trichloroethene 0.0250 0.0255 0.0240 102 96.2 79.5-121 5.70 20
Trichlorofluoromethane 0.0250 0.0309 0.0311 123 124 49.1-157 0.790 20
1,2,3-Trichloropropane 0.0250 0.0235 0.0230 93.9 92.0 74.9-124 2.07 20
1,2,3-Trimethylbenzene 0.0250 0.0272 0.0265 109 106 79.9-118 2.89 20
1,2,4-Trimethylbenzene 0.0250 0.0241 0.0225 96.5 89.9 79.0-122 7.13 20
1,3,5-Trimethylbenzene 0.0250 0.0264 0.0247 105 98.7 81.0-123 6.57 20
Vinyl chloride 0.0250 0.0270 0.0261 108 104 61.5-134 3.56 20
Xylenes, Total 0.0750 0.0730 0.0701 97.3 93.5 79.2-122 3.99 20
(S) Toluene-d8 106 106 90.0-115
(S) Dibromofluoromethane 112 113 79.0-121
(S) 4-Bromofluorobenzene 98.7 97.3 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG835361
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-04,05,06,07
L806319-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 12/20/15 13:40 • (MS) 12/20/15 12:02 • (MSD) 12/20/15 12:22
6SiNe $moXQt 2UiJiQal 5eVXlt 06 5eVXlt 06' 5eVXlt 06 5ec 06' 5ec 'ilXtioQ 5ec LimitV 06 4XaliIieU 06' 4XaliIieU 53' 53' LimitV
$Qal\te mg/l mg/l mg/l mg/l % %%% %
Acetone 0.125 0.00453 0.0732 0.0758 54.9 57.0 1 25.0-156 3.49 21.5
Acrolein 0.125 ND 0.120 0.123 96.2 98.4 1 34.0-194 2.34 21.5
Acrylonitrile 0.125 ND 0.154 0.161 123 129 1 55.9-161 4.67 20
Benzene 0.0250 ND 0.0283 0.0286 113 114 1 58.6-133 1.25 20
Bromobenzene 0.0250 ND 0.0274 0.0283 110 113 1 70.6-125 3.23 20
Bromodichloromethane 0.0250 ND 0.0334 0.0342 134 137 1 69.2-127 J5 J5 2.47 20
Bromoform 0.0250 ND 0.0257 0.0269 103 108 1 66.3-140 4.64 20
Bromomethane 0.0250 ND 0.0262 0.0270 105 108 1 16.6-183 3.14 20.5
n-Butylbenzene 0.0250 ND 0.0318 0.0325 127 130 1 64.8-145 2.34 20
sec-Butylbenzene 0.0250 ND 0.0282 0.0285 113 114 1 66.8-139 1.29 20
tert-Butylbenzene 0.0250 ND 0.0271 0.0277 108 111 1 67.1-138 2.34 20
Carbon tetrachloride 0.0250 ND 0.0333 0.0339 133 135 1 60.6-139 1.55 20
Chlorobenzene 0.0250 ND 0.0248 0.0252 99.2 101 1 70.1-130 1.49 20
Chlorodibromomethane 0.0250 ND 0.0286 0.0293 114 117 1 71.6-132 2.46 20
Chloroethane 0.0250 ND 0.0286 0.0291 114 117 1 33.3-155 1.99 20
2-Chloroethyl vinyl ether 0.125 ND 0.000830 0.000875 0.664 0.700 1 5.00-149 J6 J6 5.21 40
Chloroform 0.0250 0.000292 0.0323 0.0331 128 131 1 66.1-133 2.44 20
Chloromethane 0.0250 ND 0.0323 0.0333 129 133 1 40.7-139 3.23 20
2-Chlorotoluene 0.0250 ND 0.0260 0.0266 104 107 1 66.9-134 2.49 20
4-Chlorotoluene 0.0250 ND 0.0271 0.0273 108 109 1 66.8-134 0.950 20
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.0245 0.0269 98.1 107 1 63.9-142 9.11 20.2
1,2-Dibromoethane 0.0250 ND 0.0262 0.0272 105 109 1 73.8-131 3.73 20
Dibromomethane 0.0250 ND 0.0313 0.0319 125 127 1 72.8-127 1.87 20
1,2-Dichlorobenzene 0.0250 ND 0.0268 0.0277 107 111 1 77.4-127 2.97 20
1,3-Dichlorobenzene 0.0250 ND 0.0249 0.0253 99.7 101 1 67.9-136 1.65 20
1,4-Dichlorobenzene 0.0250 ND 0.0262 0.0268 105 107 1 74.4-123 2.09 20
Dichlorodifluoromethane 0.0250 ND 0.0384 0.0395 154 158 1 42.2-146 J5 J5 2.87 20
1,1-Dichloroethane 0.0250 ND 0.0316 0.0319 126 127 1 64.0-134 0.830 20
1,2-Dichloroethane 0.0250 ND 0.0371 0.0377 148 151 1 60.7-132 J5 J5 1.49 20
1,1-Dichloroethene 0.0250 ND 0.0326 0.0325 131 130 1 48.8-144 0.430 20
cis-1,2-Dichloroethene 0.0250 0.000360 0.0289 0.0290 114 115 1 60.6-136 0.290 20
trans-1,2-Dichloroethene 0.0250 ND 0.0284 0.0290 113 116 1 61.0-132 2.12 20
1,2-Dichloropropane 0.0250 ND 0.0308 0.0315 123 126 1 69.7-130 2.06 20
1,1-Dichloropropene 0.0250 ND 0.0319 0.0322 128 129 1 61.5-136 0.950 20
1,3-Dichloropropane 0.0250 ND 0.0263 0.0274 105 109 1 74.3-123 3.83 20
cis-1,3-Dichloropropene 0.0250 ND 0.0304 0.0315 122 126 1 71.1-129 3.52 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG835361
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-04,05,06,07
L806319-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 12/20/15 13:40 • (MS) 12/20/15 12:02 • (MSD) 12/20/15 12:22
6SiNe $moXQt 2UiJiQal 5eVXlt 06 5eVXlt 06' 5eVXlt 06 5ec 06' 5ec 'ilXtioQ 5ec LimitV 06 4XaliIieU 06' 4XaliIieU 53' 53' LimitV
$Qal\te mg/l mg/l mg/l mg/l % %%% %
trans-1,3-Dichloropropene 0.0250 ND 0.0304 0.0313 121 125 1 66.3-136 3.15 20
2,2-Dichloropropane 0.0250 ND 0.0358 0.0363 143 145 1 54.9-142 J5 J5 1.20 20
Di-isopropyl ether 0.0250 ND 0.0332 0.0339 133 136 1 59.9-140 2.16 20
Ethylbenzene 0.0250 ND 0.0238 0.0241 95.0 96.2 1 62.7-136 1.22 20
Hexachloro-1,3-butadiene 0.0250 ND 0.0254 0.0259 102 104 1 61.1-144 1.92 20.1
Isopropylbenzene 0.0250 ND 0.0269 0.0274 108 110 1 67.4-136 2.01 20
p-Isopropyltoluene 0.0250 ND 0.0279 0.0283 112 113 1 62.8-143 1.35 20
2-Butanone (MEK)0.125 ND 0.104 0.113 83.0 90.6 1 45.0-156 8.77 20.8
Methylene Chloride 0.0250 0.000155 0.0251 0.0254 99.7 101 1 61.5-125 1.17 20
4-Methyl-2-pentanone (MIBK)0.125 ND 0.157 0.172 125 138 1 60.7-150 9.38 20
Methyl tert-butyl ether 0.0250 ND 0.0298 0.0313 119 125 1 61.4-136 4.90 20
Naphthalene 0.0250 ND 0.0251 0.0269 100 108 1 61.8-143 7.10 20
n-Propylbenzene 0.0250 ND 0.0261 0.0268 104 107 1 63.2-139 2.82 20
Styrene 0.0250 ND 0.0259 0.0262 103 105 1 68.2-133 1.32 20
1,1,1,2-Tetrachloroethane 0.0250 ND 0.0271 0.0280 108 112 1 70.5-132 3.10 20
Tetrachloroethene 0.0250 0.161 0.110 0.113 0.000 0.000 1 57.4-141 V V 2.93 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.0263 0.0280 105 112 1 64.9-145 6.44 20
Toluene 0.0250 ND 0.0276 0.0279 110 112 1 67.8-124 1.32 20
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.0229 0.0251 91.7 101 1 53.7-150 9.17 20
1,2,3-Trichlorobenzene 0.0250 ND 0.0250 0.0264 99.9 105 1 65.7-143 5.33 20
1,2,4-Trichlorobenzene 0.0250 ND 0.0263 0.0274 105 110 1 67.0-146 4.26 20
1,1,1-Trichloroethane 0.0250 ND 0.0348 0.0351 139 140 1 58.7-134 J5 J5 0.740 20
1,1,2-Trichloroethane 0.0250 ND 0.0250 0.0268 100 107 1 74.1-130 6.76 20
Trichloroethene 0.0250 0.000301 0.0273 0.0276 108 109 1 48.9-148 1.09 20
Trichlorofluoromethane 0.0250 ND 0.0349 0.0353 140 141 1 39.9-165 1.16 20
1,2,3-Trichloropropane 0.0250 ND 0.0263 0.0276 105 110 1 71.5-134 4.80 20
1,2,3-Trimethylbenzene 0.0250 ND 0.0284 0.0291 114 116 1 62.7-133 2.41 20
1,2,4-Trimethylbenzene 0.0250 ND 0.0243 0.0248 97.2 99.4 1 60.5-137 2.15 20
1,3,5-Trimethylbenzene 0.0250 ND 0.0269 0.0270 108 108 1 67.9-134 0.400 20
Vinyl chloride 0.0250 ND 0.0316 0.0326 126 130 1 44.3-143 3.16 20
Xylenes, Total 0.0750 ND 0.0763 0.0777 102 104 1 65.6-133 1.80 20
(S) Toluene-d8 105 106 90.0-115
(S) Dibromofluoromethane 114 115 79.0-121
(S) 4-Bromofluorobenzene 98.0 99.4 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG837923
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-01,02,03,07
Method Blank (MB)
(MB) 12/23/15 01:19
0% 5eVXlt 0% 4XaliIieU 0% 5'L
$Qal\te mg/l mg/l
Acetone ND 0.0500
Acrolein ND 0.0500
Acrylonitrile ND 0.0100
Benzene ND 0.00100
Bromobenzene ND 0.00100
Bromodichloromethane ND 0.00100
Bromoform ND 0.00100
Bromomethane ND 0.00500
n-Butylbenzene ND 0.00100
sec-Butylbenzene ND 0.00100
tert-Butylbenzene ND 0.00100
Carbon tetrachloride ND 0.00100
Chlorobenzene ND 0.00100
Chlorodibromomethane ND 0.00100
Chloroethane ND 0.00500
2-Chloroethyl vinyl ether ND 0.0500
Chloroform ND 0.00500
Chloromethane ND 0.00250
2-Chlorotoluene ND 0.00100
4-Chlorotoluene ND 0.00100
1,2-Dibromo-3-Chloropropane ND 0.00500
1,2-Dibromoethane ND 0.00100
Dibromomethane ND 0.00100
1,2-Dichlorobenzene ND 0.00100
1,3-Dichlorobenzene ND 0.00100
1,4-Dichlorobenzene ND 0.00100
Dichlorodifluoromethane ND 0.00500
1,1-Dichloroethane ND 0.00100
1,2-Dichloroethane ND 0.00100
1,1-Dichloroethene ND 0.00100
cis-1,2-Dichloroethene ND 0.00100
trans-1,2-Dichloroethene ND 0.00100
1,2-Dichloropropane ND 0.00100
1,1-Dichloropropene ND 0.00100
1,3-Dichloropropane ND 0.00100
cis-1,3-Dichloropropene ND 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG837923
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-01,02,03,07
Method Blank (MB)
(MB) 12/23/15 01:19
0% 5eVXlt 0% 4XaliIieU 0% 5'L
$Qal\te mg/l mg/l
trans-1,3-Dichloropropene ND 0.00100
2,2-Dichloropropane ND 0.00100
Di-isopropyl ether ND 0.00100
Ethylbenzene ND 0.00100
Hexachloro-1,3-butadiene ND 0.00100
Isopropylbenzene ND 0.00100
p-Isopropyltoluene ND 0.00100
2-Butanone (MEK)ND 0.0100
Methylene Chloride ND 0.00500
4-Methyl-2-pentanone (MIBK)ND 0.0100
Methyl tert-butyl ether ND 0.00100
Naphthalene ND 0.00500
n-Propylbenzene ND 0.00100
Styrene ND 0.00100
1,1,1,2-Tetrachloroethane ND 0.00100
1,1,2,2-Tetrachloroethane ND 0.00100
Tetrachloroethene ND 0.00100
Toluene ND 0.00500
1,1,2-Trichlorotrifluoroethane ND 0.00100
1,2,3-Trichlorobenzene ND 0.00100
1,2,4-Trichlorobenzene ND 0.00100
1,1,1-Trichloroethane ND 0.00100
1,1,2-Trichloroethane ND 0.00100
Trichloroethene ND 0.00100
Trichlorofluoromethane ND 0.00500
1,2,3-Trichloropropane ND 0.00250
1,2,3-Trimethylbenzene ND 0.00100
1,2,4-Trimethylbenzene ND 0.00100
1,3,5-Trimethylbenzene ND 0.00100
Vinyl chloride ND 0.00100
Xylenes, Total ND 0.00300
(S) Toluene-d8 105 90.0-115
(S) Dibromofluoromethane 103 79.0-121
(S) 4-Bromofluorobenzene 104 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG837923
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-01,02,03,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 12/22/15 23:59 • (LCSD) 12/23/15 00:19
6SiNe $moXQt LC6 5eVXlt LC6' 5eVXlt LC6 5ec LC6' 5ec 5ec LimitV LC6 4XaliIieU LC6' 4XaliIieU 53' 53' LimitV
$Qal\te mg/l mg/l mg/l % % %% %
Acetone 0.125 0.0926 0.144 74.1 115 28.7-175 J3 43.4 20.9
Acrolein 0.125 0.105 0.123 84.0 98.4 40.4-172 15.8 20
Acrylonitrile 0.125 0.114 0.132 91.0 106 58.2-145 15.1 20
Benzene 0.0250 0.0232 0.0233 92.8 93.2 73.0-122 0.490 20
Bromobenzene 0.0250 0.0238 0.0234 95.0 93.6 81.5-115 1.47 20
Bromodichloromethane 0.0250 0.0224 0.0223 89.7 89.3 75.5-121 0.360 20
Bromoform 0.0250 0.0230 0.0232 91.8 92.9 71.5-131 1.13 20
Bromomethane 0.0250 0.0291 0.0278 116 111 22.4-187 4.41 20
n-Butylbenzene 0.0250 0.0247 0.0246 98.9 98.5 75.9-134 0.420 20
sec-Butylbenzene 0.0250 0.0241 0.0233 96.2 93.2 80.6-126 3.18 20
tert-Butylbenzene 0.0250 0.0240 0.0230 96.1 92.2 79.3-127 4.15 20
Carbon tetrachloride 0.0250 0.0230 0.0232 91.9 92.9 70.9-129 1.16 20
Chlorobenzene 0.0250 0.0241 0.0235 96.5 94.2 79.7-122 2.44 20
Chlorodibromomethane 0.0250 0.0241 0.0240 96.6 96.2 78.2-124 0.430 20
Chloroethane 0.0250 0.0266 0.0261 107 105 41.2-153 1.92 20
2-Chloroethyl vinyl ether 0.125 0.128 0.138 103 110 23.4-162 6.93 23.5
Chloroform 0.0250 0.0230 0.0232 92.1 92.9 73.2-125 0.800 20
Chloromethane 0.0250 0.0212 0.0215 84.9 85.9 55.8-134 1.23 20
2-Chlorotoluene 0.0250 0.0235 0.0229 93.9 91.7 76.4-125 2.37 20
4-Chlorotoluene 0.0250 0.0234 0.0231 93.8 92.4 81.5-121 1.54 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0227 0.0254 90.8 102 64.8-131 11.3 20
1,2-Dibromoethane 0.0250 0.0246 0.0249 98.6 99.7 79.8-122 1.13 20
Dibromomethane 0.0250 0.0239 0.0243 95.6 97.2 79.5-118 1.58 20
1,2-Dichlorobenzene 0.0250 0.0236 0.0239 94.6 95.7 84.7-118 1.15 20
1,3-Dichlorobenzene 0.0250 0.0236 0.0231 94.3 92.2 77.6-127 2.26 20
1,4-Dichlorobenzene 0.0250 0.0232 0.0236 92.7 94.5 82.2-114 1.94 20
Dichlorodifluoromethane 0.0250 0.0199 0.0197 79.4 78.7 56.0-134 1.00 20
1,1-Dichloroethane 0.0250 0.0235 0.0238 94.1 95.3 71.7-127 1.24 20
1,2-Dichloroethane 0.0250 0.0238 0.0243 95.1 97.2 65.3-126 2.19 20
1,1-Dichloroethene 0.0250 0.0242 0.0246 96.8 98.3 59.9-137 1.55 20
cis-1,2-Dichloroethene 0.0250 0.0237 0.0240 94.9 95.9 77.3-122 1.08 20
trans-1,2-Dichloroethene 0.0250 0.0235 0.0238 94.1 95.4 72.6-125 1.33 20
1,2-Dichloropropane 0.0250 0.0238 0.0237 95.4 94.9 77.4-125 0.500 20
1,1-Dichloropropene 0.0250 0.0237 0.0237 94.8 94.8 72.5-127 0.0300 20
1,3-Dichloropropane 0.0250 0.0243 0.0243 97.3 97.1 80.6-115 0.230 20
cis-1,3-Dichloropropene 0.0250 0.0237 0.0236 94.7 94.5 77.7-124 0.240 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG837923
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-01,02,03,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 12/22/15 23:59 • (LCSD) 12/23/15 00:19
6SiNe $moXQt LC6 5eVXlt LC6' 5eVXlt LC6 5ec LC6' 5ec 5ec LimitV LC6 4XaliIieU LC6' 4XaliIieU 53' 53' LimitV
$Qal\te mg/l mg/l mg/l % % %% %
trans-1,3-Dichloropropene 0.0250 0.0237 0.0242 95.0 97.0 73.5-127 2.11 20
2,2-Dichloropropane 0.0250 0.0219 0.0221 87.5 88.4 61.3-134 0.970 20
Di-isopropyl ether 0.0250 0.0233 0.0234 93.3 93.4 65.1-135 0.0600 20
Ethylbenzene 0.0250 0.0239 0.0232 95.8 92.9 80.9-121 3.01 20
Hexachloro-1,3-butadiene 0.0250 0.0234 0.0233 93.4 93.1 73.7-133 0.400 20
Isopropylbenzene 0.0250 0.0238 0.0231 95.3 92.5 81.6-124 3.04 20
p-Isopropyltoluene 0.0250 0.0241 0.0233 96.4 93.1 77.6-129 3.53 20
2-Butanone (MEK)0.125 0.0968 0.133 77.5 107 46.4-155 J3 31.8 20
Methylene Chloride 0.0250 0.0230 0.0234 91.9 93.6 69.5-120 1.84 20
4-Methyl-2-pentanone (MIBK)0.125 0.115 0.125 92.1 99.8 63.3-138 8.06 20
Methyl tert-butyl ether 0.0250 0.0238 0.0248 95.3 99.4 70.1-125 4.16 20
Naphthalene 0.0250 0.0239 0.0257 95.5 103 69.7-134 7.25 20
n-Propylbenzene 0.0250 0.0235 0.0230 94.0 91.8 81.9-122 2.33 20
Styrene 0.0250 0.0245 0.0242 98.1 96.8 79.9-124 1.38 20
1,1,1,2-Tetrachloroethane 0.0250 0.0231 0.0226 92.3 90.5 78.5-125 1.90 20
1,1,2,2-Tetrachloroethane 0.0250 0.0227 0.0233 90.7 93.0 79.3-123 2.51 20
Tetrachloroethene 0.0250 0.0234 0.0230 93.8 92.1 73.5-130 1.76 20
Toluene 0.0250 0.0224 0.0222 89.7 88.8 77.9-116 1.02 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0245 0.0253 98.1 101 62.0-141 3.25 20
1,2,3-Trichlorobenzene 0.0250 0.0229 0.0242 91.6 96.9 75.7-134 5.68 20
1,2,4-Trichlorobenzene 0.0250 0.0231 0.0237 92.6 94.9 76.1-136 2.45 20
1,1,1-Trichloroethane 0.0250 0.0235 0.0236 94.0 94.4 71.1-129 0.400 20
1,1,2-Trichloroethane 0.0250 0.0245 0.0246 98.1 98.6 81.6-120 0.450 20
Trichloroethene 0.0250 0.0243 0.0243 97.3 97.0 79.5-121 0.310 20
Trichlorofluoromethane 0.0250 0.0244 0.0243 97.5 97.2 49.1-157 0.310 20
1,2,3-Trichloropropane 0.0250 0.0239 0.0246 95.6 98.3 74.9-124 2.73 20
1,2,3-Trimethylbenzene 0.0250 0.0233 0.0234 93.1 93.5 79.9-118 0.390 20
1,2,4-Trimethylbenzene 0.0250 0.0230 0.0222 92.0 88.8 79.0-122 3.51 20
1,3,5-Trimethylbenzene 0.0250 0.0229 0.0220 91.5 87.9 81.0-123 4.01 20
Vinyl chloride 0.0250 0.0233 0.0232 93.2 92.7 61.5-134 0.610 20
Xylenes, Total 0.0750 0.0710 0.0696 94.6 92.8 79.2-122 1.95 20
(S) Toluene-d8 107 106 90.0-115
(S) Dibromofluoromethane 103 102 79.0-121
(S) 4-Bromofluorobenzene 103 99.9 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG837923
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-01,02,03,07
L806319-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 12/23/15 02:59 • (MS) 12/23/15 01:39 • (MSD) 12/23/15 01:59
6SiNe $moXQt 2UiJiQal 5eVXlt 06 5eVXlt 06' 5eVXlt 06 5ec 06' 5ec 'ilXtioQ 5ec LimitV 06 4XaliIieU 06' 4XaliIieU 53' 53' LimitV
$Qal\te mg/l mg/l mg/l mg/l % %%% %
Acetone 0.125 ND 0.0544 0.0532 43.5 42.6 1 25.0-156 2.21 21.5
Acrolein 0.125 ND 0.0954 0.0987 76.4 78.9 1 34.0-194 3.33 21.5
Acrylonitrile 0.125 ND 0.120 0.124 96.4 99.5 1 55.9-161 3.19 20
Benzene 0.0250 ND 0.0191 0.0201 76.5 80.2 1 58.6-133 4.74 20
Bromobenzene 0.0250 ND 0.0212 0.0218 84.7 87.2 1 70.6-125 2.95 20
Bromodichloromethane 0.0250 ND 0.0202 0.0215 80.9 85.8 1 69.2-127 5.87 20
Bromoform 0.0250 ND 0.0215 0.0225 85.9 90.0 1 66.3-140 4.70 20
Bromomethane 0.0250 ND 0.0182 0.0194 72.8 77.5 1 16.6-183 6.16 20.5
n-Butylbenzene 0.0250 ND 0.0224 0.0238 89.6 95.3 1 64.8-145 6.17 20
sec-Butylbenzene 0.0250 ND 0.0215 0.0228 86.0 91.4 1 66.8-139 6.03 20
tert-Butylbenzene 0.0250 ND 0.0214 0.0228 85.7 91.1 1 67.1-138 6.13 20
Carbon tetrachloride 0.0250 ND 0.0196 0.0203 78.5 81.2 1 60.6-139 3.44 20
Chlorobenzene 0.0250 ND 0.0206 0.0217 82.4 86.7 1 70.1-130 5.04 20
Chlorodibromomethane 0.0250 ND 0.0220 0.0228 87.8 91.1 1 71.6-132 3.61 20
Chloroethane 0.0250 ND 0.0193 0.0202 77.4 80.7 1 33.3-155 4.24 20
2-Chloroethyl vinyl ether 0.125 ND 0.000340 0.000368 0.272 0.295 1 5.00-149 J6 J6 7.88 40
Chloroform 0.0250 ND 0.0211 0.0221 84.3 88.6 1 66.1-133 4.98 20
Chloromethane 0.0250 ND 0.0138 0.0144 55.0 57.4 1 40.7-139 4.26 20
2-Chlorotoluene 0.0250 ND 0.0208 0.0217 83.3 86.6 1 66.9-134 3.92 20
4-Chlorotoluene 0.0250 ND 0.0207 0.0219 82.8 87.5 1 66.8-134 5.52 20
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.0239 0.0253 95.6 101 1 63.9-142 5.51 20.2
1,2-Dibromoethane 0.0250 ND 0.0214 0.0226 85.6 90.2 1 73.8-131 5.20 20
Dibromomethane 0.0250 ND 0.0207 0.0219 82.9 87.5 1 72.8-127 5.48 20
1,2-Dichlorobenzene 0.0250 ND 0.0219 0.0231 87.7 92.2 1 77.4-127 5.03 20
1,3-Dichlorobenzene 0.0250 ND 0.0213 0.0223 85.1 89.1 1 67.9-136 4.62 20
1,4-Dichlorobenzene 0.0250 ND 0.0212 0.0222 84.7 88.8 1 74.4-123 4.81 20
Dichlorodifluoromethane 0.0250 ND 0.0148 0.0151 59.0 60.4 1 42.2-146 2.31 20
1,1-Dichloroethane 0.0250 ND 0.0205 0.0214 82.0 85.7 1 64.0-134 4.43 20
1,2-Dichloroethane 0.0250 ND 0.0206 0.0218 82.5 87.2 1 60.7-132 5.50 20
1,1-Dichloroethene 0.0250 ND 0.0189 0.0191 75.5 76.4 1 48.8-144 1.19 20
cis-1,2-Dichloroethene 0.0250 ND 0.0201 0.0211 80.4 84.3 1 60.6-136 4.79 20
trans-1,2-Dichloroethene 0.0250 ND 0.0175 0.0182 70.1 72.7 1 61.0-132 3.58 20
1,2-Dichloropropane 0.0250 ND 0.0209 0.0220 83.6 87.9 1 69.7-130 5.10 20
1,1-Dichloropropene 0.0250 ND 0.0184 0.0189 73.6 75.6 1 61.5-136 2.68 20
1,3-Dichloropropane 0.0250 ND 0.0214 0.0224 85.8 89.7 1 74.3-123 4.46 20
cis-1,3-Dichloropropene 0.0250 ND 0.0200 0.0213 80.2 85.3 1 71.1-129 6.16 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG837923
Volatile Organic Compounds (GC/MS) by Method 8260B L806319-01,02,03,07
L806319-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 12/23/15 02:59 • (MS) 12/23/15 01:39 • (MSD) 12/23/15 01:59
6SiNe $moXQt 2UiJiQal 5eVXlt 06 5eVXlt 06' 5eVXlt 06 5ec 06' 5ec 'ilXtioQ 5ec LimitV 06 4XaliIieU 06' 4XaliIieU 53' 53' LimitV
$Qal\te mg/l mg/l mg/l mg/l % %%% %
trans-1,3-Dichloropropene 0.0250 ND 0.0209 0.0224 83.5 89.4 1 66.3-136 6.81 20
2,2-Dichloropropane 0.0250 ND 0.0199 0.0206 79.6 82.3 1 54.9-142 3.39 20
Di-isopropyl ether 0.0250 ND 0.0210 0.0218 84.1 87.3 1 59.9-140 3.82 20
Ethylbenzene 0.0250 ND 0.0203 0.0211 81.2 84.5 1 62.7-136 3.98 20
Hexachloro-1,3-butadiene 0.0250 ND 0.0222 0.0235 88.7 93.9 1 61.1-144 5.70 20.1
Isopropylbenzene 0.0250 ND 0.0209 0.0220 83.4 88.0 1 67.4-136 5.28 20
p-Isopropyltoluene 0.0250 ND 0.0212 0.0227 85.0 90.7 1 62.8-143 6.49 20
2-Butanone (MEK)0.125 ND 0.0803 0.0835 64.2 66.8 1 45.0-156 3.90 20.8
Methylene Chloride 0.0250 0.000409 0.0187 0.0196 73.2 76.9 1 61.5-125 4.77 20
4-Methyl-2-pentanone (MIBK)0.125 ND 0.113 0.122 90.7 97.5 1 60.7-150 7.21 20
Methyl tert-butyl ether 0.0250 ND 0.0222 0.0237 88.7 94.7 1 61.4-136 6.53 20
Naphthalene 0.0250 ND 0.0237 0.0258 94.7 103 1 61.8-143 8.55 20
n-Propylbenzene 0.0250 ND 0.0207 0.0216 82.6 86.3 1 63.2-139 4.35 20
Styrene 0.0250 ND 0.0215 0.0223 86.0 89.0 1 68.2-133 3.44 20
1,1,1,2-Tetrachloroethane 0.0250 ND 0.0207 0.0218 83.0 87.2 1 70.5-132 5.00 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.0226 0.0238 90.5 95.2 1 64.9-145 5.12 20
Tetrachloroethene 0.0250 0.000135 0.0187 0.0187 74.4 74.4 1 57.4-141 0.000 20
Toluene 0.0250 ND 0.0185 0.0196 74.0 78.4 1 67.8-124 5.85 20
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.0218 0.0218 87.2 87.2 1 53.7-150 0.0500 20
1,2,3-Trichlorobenzene 0.0250 ND 0.0230 0.0246 91.8 98.2 1 65.7-143 6.75 20
1,2,4-Trichlorobenzene 0.0250 ND 0.0222 0.0239 89.0 95.6 1 67.0-146 7.12 20
1,1,1-Trichloroethane 0.0250 ND 0.0204 0.0215 81.6 85.9 1 58.7-134 5.15 20
1,1,2-Trichloroethane 0.0250 ND 0.0223 0.0233 89.2 93.1 1 74.1-130 4.27 20
Trichloroethene 0.0250 ND 0.0195 0.0206 78.0 82.3 1 48.9-148 5.40 20
Trichlorofluoromethane 0.0250 ND 0.0189 0.0198 75.7 79.1 1 39.9-165 4.42 20
1,2,3-Trichloropropane 0.0250 ND 0.0235 0.0246 93.9 98.3 1 71.5-134 4.63 20
1,2,3-Trimethylbenzene 0.0250 ND 0.0208 0.0223 83.4 89.1 1 62.7-133 6.68 20
1,2,4-Trimethylbenzene 0.0250 ND 0.0202 0.0214 80.7 85.4 1 60.5-137 5.65 20
1,3,5-Trimethylbenzene 0.0250 ND 0.0198 0.0211 79.3 84.4 1 67.9-134 6.21 20
Vinyl chloride 0.0250 ND 0.0157 0.0162 62.6 64.8 1 44.3-143 3.39 20
Xylenes, Total 0.0750 ND 0.0599 0.0628 79.9 83.7 1 65.6-133 4.58 20
(S) Toluene-d8 105 106 90.0-115
(S) Dibromofluoromethane 104 102 79.0-121
(S) 4-Bromofluorobenzene 101 99.9 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND,U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
SDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is
high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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