Burnsvile Hosiery_Site Assessment Report

Prepared for
Winter Star Corporation
Post Office Box 244
Burnsville, North Carolina
Project Number 2546

Prepared by
Altamont Environmental, Inc.
231 Haywood Street
Asheville, NC 28801
828.281.3350

Site Assessment Report
Former Burnsville Hosiery Mill
August 19, 2015

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Former Burnsville Hosiery Mill Page iii

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Table of Contents

1.0 Introduction .................................................................................................................................................. 1 
1.1 Site Background ............................................................................................................................. 1 
2.0 Scope of Work and Methods ...................................................................................................................... 2 
2.1 Health and Safety Information ...................................................................................................... 2 
2.2 Ground-Penetrating Radar (GPR) Survey ...................................................................................... 2 
2.3 UST Soil Sampling .......................................................................................................................... 2 
2.4 UST Closure ..................................................................................................................................... 3 
2.4.1 UST-1 and UST-2 ............................................................................................................................... 3 
2.4.2 UST-3 and UST-4 ............................................................................................................................... 3 
2.4.3 UST-5 ................................................................................................................................................. 4 
2.5 Additional Excavation ..................................................................................................................... 4 
2.6 Excavated Soils ............................................................................................................................... 4 
3.0 Findings ........................................................................................................................................................ 5 
4.0 Conclusions .................................................................................................................................................. 7 
5.0 References ................................................................................................................................................... 8 

Figures
1. Site Location Map
2. Site Layout Map
3. Soil Boring Location Map
4. Tank Pit 1 Sample Location Map
5. Tank Pit 2 Sample Location Map
Tables
1. Initial UST Assessment Soil Analytical Results
2. UST Closure Soil Sample Analytical Results Summary
Appendices
A. October 2014 Laboratory Analytical Report and Chain-of-Custody Form
B. UST-61 Form
C. March 2015 Laboratory Analytical Report and Chain-of-Custody Form
D. April 2015 Laboratory Analytical Report and Chain-of-Custody Form
E. Waste Disposal Manifests
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1.0 Introduction
Winter Star Corporation (Winter Star) contracted Altamont Environmental, Inc. (Altamont) to perform a Site
Assessment for the former Burnsville Hosiery Mill property (the Site) located at 54 Ferguson Hill Road in
Burnsville, Yancey County, North Carolina (Figure 1).
The Site is a 2.896-acre parcel located in Burnsville, North Carolina. The Site contains a former
manufacturing facility that is approximately 28,900 square-feet in area (Figure 2).
Boot socks for the United States Army were manufactured at the Burnsville Hosiery Mill. The mill was in
operation from the 1950s until 2010, when the Site occupants vacated the property.
1.1 Site Background
In 2014, Altamont completed a Phase I Environmental Site Assessment (ESA) of the Site. The Phase I ESA is
dated September 22, 2014. During the completion of the Phase I ESA, Altamont identified several
underground storage tanks (USTs) on-Site. The capacities and contents (if known) of the identified USTs are
described as follows:
• UST-1—500-gallon, heating oil
• UST-2—500-gallon, heating oil
• UST-3—10,000-gallon, heating oil
• UST-4—10,000-gallon, heating oil
• UST-5—1,000-gallon, unknown
At the time of the Phase I ESA visit, the top of UST-5 was exposed at the ground surface and damaged. No
obvious petroleum odors were observed at that time. The UST locations are shown on Figure 3.

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2.0 Scope of Work and Methods
At the request of Winter Star in response to the findings of the Phase I ESA, Altamont completed or observed
the following activities to address the USTs:
• UST Soil Sampling (October 2014)
• UST Closure (March 2015)
• Additional Excavation (April 2015)
The following sections detail the assessment and remedial actions completed at the Site.
2.1 Health and Safety Information
Prior to completing any intrusive work, Altamont notified the North Carolina One-Call Center to mark the
utilities in the area. A ground-penetrating radar (GPR) survey was also completed to locate potential USTs
near the former hosiery mill as well as potential utilities near proposed excavations and borings. Altamont
and sub-contractor staff participated in an initial thorough discussion of Altamont’s health and safety plan
for the Site prior to beginning work. In addition, health and safety “tailgate” meetings were held at the
beginning of each fieldwork day. All personnel wore the following safety gear, at a minimum:
• Long pants and steel-toed boots (at all times)
• Hardhats, safety glasses, cut-resistant gloves, and nitrile gloves (as appropriate for specific activities)
2.2 Ground-Penetrating Radar (GPR) Survey
An Altamont representative observed a GPR survey to locate potential USTs near the Site building. Vaughn
and Melton from Asheville, North Carolina, performed the GPR survey. The area surveyed consisted of areas
surrounding the Site building. Five USTs were identified and flagged for further assessment activities (Figure
3).
2.3 UST Soil Sampling
On October 21, 2014, Altamont oversaw installation of soil borings completed by Mounting Environmental,
Services (Mountain), a licensed North Carolina driller, using a direct-push sampling rig in the vicinity of the
USTs located on the Site.
Soil borings were installed adjacent to the identified USTs. The borings were terminated at depths presumed
to be at a lower elevation than the bottom of the adjacent UST (Figure 3). In general, soil samples were
collected at a depth between 6 and 14 feet below ground surface (ft-bgs). During boring installation, soils
were screened using a Photo Ionization Detector (PID). Samples were either collected from the boring
increment exhibiting the highest PID reading, or from a depth considered to be representative of the base of
the UST. Once collected, samples were transferred to laboratory supplied containers, placed into a cooler
with ice and transported to Pace Analytical Services (Pace) in Asheville, North Carolina under chain-of-
custody protocol.
Pace analyzed the soil samples for total petroleum hydrocarbons (TPH) diesel range organics (DRO) and
gasoline range organics (GRO). The analytical results indicated that three soil samples (SB-2, SB-4, and SB-
5) contained TPH concentrations in excess of the North Carolina Department of Environment and Natural
Resources (DENR) Division of Waste Management, UST Section Action Levels. The analytical results are
summarized on Table 1 and laboratory analytical data is included as Appendix A.
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2.4 UST Closure
Based upon the initial soil sampling completed in October 2014, soil analytical results indicated that
concentrations of petroleum constituents exceeded the UST Section Action Levels for TPH DRO and/or TPH
GRO at the location of UST-2 and UST-4 and the removal of these USTs would be required under applicable
DENR guidance. A UST-61, 24-Hour Release and UST Leak Reporting Form is included as Appendix B.
On March 11, 2015, Altamont returned to the Site to observe the removal of the USTs.
2.4.1 UST-1 and UST-2
UST-1 and UST-2 were removed on March 11, 2015 and placed adjacent to the excavation.
UST-1 showed no obvious signs of deterioration or leaking. Altamont observed the area below the UST and
no obvious signs of contamination were observed. No further excavation was performed in association with
this UST.
UST-2 was deteriorated and pitting and holes were observed. The area around this UST was over-excavated
and is referenced as Tank Pit 1. The extents of the excavation to the east and west were limited due to utility
piping located parallel to the area. The excavation extended to 13 feet below-grade-surface (ft-bgs) and was
measured to be 5 feet wide by 15 feet in length. Confirmation soil samples were collected from the base and
sidewalls (north, east, south, and west) of the excavation. Confirmation samples were identified as TP-1-N,
TP-1-S, TP-1-E, TP-1-W, and TP-1-B (Figure 4).
Each sample was split, one part from each sample was placed into its own plastic Ziploc® bag and allowed to
volatilize in a warm environment for at least 10 minutes. After each sample had been allowed to volatilize,
the samples were screened with a photoionization detector (PID). The five soil samples did not contain PID
readings over 3 parts per million (ppm).
The other portions of the split confirmation soil samples were placed into laboratory-supplied containers. The
containers were placed on ice in a cooler. The samples were then delivered via currier to Prism Laboratories
(Prism) a North Carolina certified laboratory. The soil samples were analyzed for volatile organic compounds
(VOCs) using EPA Method 8260, semivolatile organic compounds (SVOCs) using EPA Method 8270, and
extractable petroleum hydrocarbons (EPHs) and volatile petroleum hydrocarbons (VPHs) using the
Massachusetts Department of Environmental Protection (MADEP) methods. Laboratory analytical results are
summarized on Table 2 and in the attached laboratory analytical report included as Appendix C.
2.4.2 UST-3 and UST-4
Sample SB-2, collected in October 2014 adjacent to UST-4 contained a TPH DRO concentration in excess of
the UST Section Action Levels. On March 11, 2015, UST-4 was removed from the ground and soils were
over-excavated in the area of SB-2. This area is referenced as Tank Pit 2. UST-4 appeared to be in good
condition and no obvious signs of a release were observed. Confirmation soil samples were collected from
the base and sidewalls (north, east, south, and west) of the excavation. The samples were designated as TP-
2-N, TP-2-S, TP-2-E, TP-2-W, TP-2-B1, and TP-2-B2 (Figure 5). PID recordings were not collected/documented
due to heavy rain at the time of sample collection.
Samples TP-2-N, TP-2-S, TP-2-E, TP-2-W, TP-2-B1, and TP-2-B2 were collected into laboratory supplied
containers, placed in a cooler with ice. The samples were then delivered via currier to Prism. The soil
samples were analyzed for VOCs using EPA Method 8260, SVOCs using EPA Method 8270, EPH and VPH
using the MADEP methods. Laboratory analytical results are summarized on Table 2 and in the attached
laboratory analytical report included as Appendix C
Altamont contacted Ms. Jan Andersen, Supervisor of the UST Section Asheville Regional Office on March 10,
2015 to discuss UST-3, located partially underneath the facility. Based on that conversation it was
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determined that UST-3 was an unregulated tank with no documented, visual, or olfactory evidence of a
reported release. As such it was determined that it would be permissible to close UST-3 in-place.
Representatives of Winter Star have indicated that UST-3 was cleaned and filled with sand, and the UST
basin backfilled.
2.4.3 UST-5
At the time of the September 22, 2014 Phase I ESA visit, the top of UST-5 was exposed at the ground
surface and damaged. No obvious petroleum odors were observed at that time, and analysis of samples
collected from within the vicinity of UST-5 (SB-6, SB-7, and SB-8) did not identify the presence of
constituents of concern above laboratory reporting limits. The UST was excavated on March 11, 2015 and
no obvious signs indicating a release were documented. Based on the tank shape, size and location, it is
possible the tank was used as an air or water pressure vessel and was not associated with petroleum or
hazardous material storage.
2.5 Additional Excavation
One of the confirmation soil samples collected in March 2015 from Tank Pit 2 and from within the vicinity of
UST-4 had an exceedance of a Soil-to-Groundwater maximum soil contaminant concentration (MSCC). The
sample identified as TP-2-B1 contained a concentration of C11-C22 aromatics in excess of the Soil-to-
Groundwater MSCC. In response to the exceedance, on April 7, 2015, and following additional soil
excavation (approximately 12 tons of soil) from Tank Pit 2, a follow-up confirmation sample designated TP-2-
B1A was collected.
Prior to collection, the sample was split. One portion of the sample was placed into its own plastic Ziploc®
bag and allowed to volatilize in a warm environment for at least 10 minutes. After the sample had been
allowed to volatilize, the sample was screened with a PID using proper headspace screening techniques (US
Environmental Protection Agency [EPA] 2001). A headspace reading of approximately 4ppm was recorded
for TP-2-B1A. The second portion of the sample was transferred into laboratory-supplied containers. The
containers were then placed on ice in a cooler for delivery to Pace for analysis of MADEP EPH and VPH. The
second portion
2.6 Excavated Soils
Approximately 249 tons of soil associated with the Tank Pit 1 and 2 excavations were staged on-Site.
Although segregated initially, the soils associated with Tank Pit 1 and Tank Pit 2 were subsequently
stockpiled into the same area; therefore, all excavated soil was considered to be impacted. These soils were
placed into dump trucks and transported to Republic’s Foothills Regional Landfill in Lenoir, North Carolina.
Soil disposal manifests are included as Appendix E.
Prior to disposal, three stockpile characterization samples (SPC-1 through SPC-3) were collected and
analyzed for TPH DRO and TPH GRO in accordance with disposal facility requirements. Results are
summarized on Table 2 and laboratory reports are included as Appendix C.

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3.0 Findings
Altamont completed a preliminary UST assessment at the Site on October 21, 2014. Based upon the
findings of the UST assessment, concentrations of petroleum constituents exceeded the UST Action Levels
for TPH DRO or GRO at Tank Pit 2, sampling locations SB-2; and at Tank Pit 1, sampling locations SB-4 and
SB-5.
• SB-2 contained a detection of TPH DRO of 40.8 milligrams per kilogram (mg/kg). SB-2 was collected
from the eastern portion of a 10,000-gallon heating oil UST (UST-4) at a depth of 12 to 14 ft-bgs.
• The samples collected from soil borings SB-4 and SB-5 both contained TPH DRO at concentrations of
847 and 1,180 mg/kg respectively, and TPH GRO at concentrations of 44.6 and 45.4 respectively,
all exceeding the DENR UST Section Action Levels. SB-4 and SB-5 were collected from the northern
and southern ends respectively of a 500-gallon UST (UST-2) located adjacent to the eastern portion
of the facility structure at a depth of 6 to 8 ft-bgs.
In March 2015, UST removal activities were completed by a contractor to Winter Star and Yancey County.
Two 500-gallon USTs, one 1,000-gallon, and one 10,000-gallon UST were removed. Altamont collected
confirmation samples from the base and sidewalls of two of the UST excavations referenced as Tank Pit 1
and Tank Pit 2.
Tank Pit 1
Tank Pit 1 contained two 550-gallon USTs. The northernmost 550-gallon UST (UST-1) was observed to be in
good condition and no impacts or evidence of a release were observed from within the immediate vicinity of
the UST. A second 550-gallon UST (UST-2), also located within Tank Pit 1, was observed to be pitted and in
poor condition. Evidence of a release was observed and the area was over-excavated.
Confirmation samples collected from the base and four sidewalls of Tank Pit 1 identified multiple
constituents of concern above laboratory reporting limits but below applicable regulatory standards.
Laboratory results are included in Appendix C and summarized in Table 2.
Tank Pit 2
The area located south of the facility building contained two 10,000-gallon USTs (UST-3 and UST-4). One of
three initial soil borings (SB-2) installed during the preliminary UST assessment, adjacent to UST-4,
contained a TPH DRO concentration in excess of the DENR Action Levels. On March 11, 2015, the UST
closest to SB-2 (UST-4) was removed from the area and soils were over-excavated. A second 10,000-gallon
UST (UST-3), also located within Tank Pit 2, appeared to be in good condition and no obvious signs of a
release were observed. As such, and due to the positioning of UST-3, located partially beneath the Site
structure, UST-3 was left in-place.
Confirmation soil samples were collected from the base and sidewalls of the excavation. The samples were
designated as TP-2-N, TP-2-S, TP-2-E, TP-2-W, TP-2-B1, and TP-2-B2.
Confirmation samples identified multiple constituents of concern above laboratory reporting limits and an
exceedance of the standard for C11-C22 aromatics was detected at one location (TP-2-B1).
On April 7, 2015 Altamont returned to the Site to observe additional over-excavation within the vicinity of
sample location TP-2-B1. Approximately 12 tons of additional material was excavated from this area.
Altamont then collected an additional confirmation sample (TP-2-B1A) from within the vicinity of the over-
excavated area. TP-2-B1A was then submitted for analysis of MADEP EPH and VPH. Concentrations of C09-
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C18 aliphatics were reported above laboratory detection limits, but below applicable standards. No other
constituents were reported above laboratory detection limits.
The laboratory analytical reports are provided in Appendix C and D and summarized in Table 2.
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4.0 Conclusions
Based on the results previously described in this report, Altamont recommends that the previously identified
incidents associated with two tank pits at the Subject Site receive unrestricted regulatory closure and that a
Notice of No Further Action (NFA) be provided by the DENR, DWM, UST Section.

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5.0 References
Altamont. Phase I Environmental Site Assessment. Dated September 22, 2014.
DENR. Tank Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases. Dated December 1, 2013.
DENR. Table 1 MSCCs Rev. April 16, 2012

FIGURES

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DS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and
the GIS User Community
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
FIGURE3



¦

!>
!>








!A
!A
!A!A
!A
UST-2
UST-1
TP-1-N
TP-1-ETP-1-B
TP-1-W
TP-1-S
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus
DS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and
the GIS User Community





FIGURE4




¦

!A 









!A
!A
!A
!A
!A !A
UST-4
UST-3
TP-2-N
TP-2-E
TP-2-W
TP-2-5
TP-2-B2 TP-2-B1 /
TP-2-B1A
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus
DS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and
the GIS User Community





FIGURE5




¦

!A 









TABLES

TA
B
L
E

1
In
i
t
i
a
l

U
S
T

A
s
s
e
s
s
m
e
n
t

S
o
i
l

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Fo
r
m
e
r

B
u
r
n
s
v
i
l
l
e

H
o
s
i
e
r
y

M
i
l
l
Bu
r
n
s
v
i
l
l
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
Sa
m
p
l
e

I
d
e
n
t
i
f
i
c
a
t
i
o
n
:

S
B
-
1

S
B
-
2

S
B
-
3

S
B
-
4

S
B
-
5

S
B
-
6

S
B
-
7

S
B
-
8

S
B
-
9
Da
t
e

C
o
l
l
e
c
t
e
d
:
10
/
2
1
/
1
4

1
0
/
2
1
/
1
4

1
0
/
2
1
/
1
4

1
0
/
2
1
/
1
4

1
0
/
2
1
/
1
4

1
0
/
2
1
/
1
4

1
0
/
2
1
/
1
4

1
0
/
2
1
/
1
4

1
0
/
2
1
/
1
4
De
p
t
h
:
10
-
1
2

f
t

1
2
-
1
4

f
t

8
-
1
0

f
t

6
-
8

f
t

6
-
8

f
t

6
-
8

f
t

6
-
8

f
t

6
-
8

f
t

1
0
-
1
2

f
t
DE
N
R
Ac
t
i
o
n

L
e
v
e
l
DR
O

(
E
P
A

8
0
1
5
-
3
5
5
0
)
10
ND
40
.
8
ND
84
7

1
,
1
8
0
ND

N
D

N
D

N
D
GR
O

(
E
P
A

8
0
1
5
-
5
0
3
0
)
10
ND

N
D

N
D
44
.
6

4
5
.
4
ND

N
D

N
D

N
D
No
t
e
s
:

1.

B
o
l
d
e
d

v
a
l
u
e
s

i
n
d
i
c
a
t
e

c
o
n
c
e
n
t
r
a
t
i
o
n
s

t
h
a
t

h
a
v
e

e
x
c
e
e
d
e
d

s
c
r
e
e
n
i
n
g

s
t
a
n
d
a
r
d
s
.

2.

A
l
l

c
o
n
c
e
n
t
r
a
t
i
o
n
s

a
r
e

i
n

m
i
l
l
i
g
r
a
m
s

p
e
r

k
i
l
g
r
a
m

(
m
g
/
k
g
)
.
3.

N
D

d
e
n
o
t
e
s

N
o
t

D
e
t
e
c
t
e
d
.
4.

D
E
N
R

A
c
t
i
o
n

L
e
v
e
l

S
o
u
r
c
e
:

D
E
N
R
.

T
a
n
k

G
u
i
d
e
l
i
n
e
s

f
o
r

S
i
t
e

C
h
e
c
k
s
,

T
a
n
k

C
l
o
s
u
r
e
,

a
n
d

I
n
i
t
i
a
l

R
e
s
p
o
n
s
e

a
n
d

A
b
a
t
e
m
e
n
t

f
o
r

U
S
T

R
e
l
e
a
s
e
s
.

D
a
t
e
d

D
e
c
e
m
b
e
r

1
,

2
0
1
3
.
Pa
r
a
m
e
t
e
r
s
P:
\
W
i
n
t
e
r

S
t
a
r

C
o
r
p
o
r
a
t
i
o
n
\
S
i
t
e

A
s
s
e
s
s
m
e
n
t

R
e
p
o
r
t
\
T
a
b
l
e
s
\
T
a
b
l
e
s

1

-

3
Ta
b
l
e

2
US
T

C
l
o
s
u
r
e

S
o
i
l

S
a
m
p
l
e

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s

S
u
m
m
a
r
y
Fo
r
m
e
r

B
u
r
n
s
v
i
l
l
e

H
o
s
i
e
r
y

M
i
l
l
Bu
r
n
s
v
i
l
l
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
A
c
e
t
o
n
e
N
a
p
h
t
h
a
l
e
n
e
1
,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1
,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
o
-
X
y
l
e
n
e
C
9
-
C
1
8

A
l
i
p
h
a
t
i
c
s
C
1
9
-
C
3
6

A
l
i
p
h
a
t
i
c
s
C
1
1
-
C
2
2

A
r
o
m
a
t
i
c
s
C
5
-
C
8

A
l
i
p
h
a
t
i
c
s
D
R
O
GRO
TP
-
1
-
N
3/
1
1
/
2
0
1
5

<
0
.
0
5
7
<0
.
0
1
1

<
0
.
0
0
5
7

<
0
.
0
0
5
7

<
0
.
0
0
5
7

<
1
3

<
1
3

<
1
3

<
1
7
NA

N
A
TP
-
1
-
S
3/
1
1
/
2
0
1
5

<
0
.
0
0
1
6
<0
.
0
1
3

<
0
.
0
0
6
5

<
0
.
0
0
6
5

<
0
.
0
0
6
5
39
13

J
<1
5

<
1
9
NA

N
A
TP
-
1
-
E
3/
1
1
/
2
0
1
5

<
0
.
0
7
0
0.0
0
8
1

J

0
.
0
0
3
1

J
<0
.
0
0
7
0

<
0
.
0
0
7
0
16
9.
5

J

3
.
9

J
<2
0
NA

N
A
TP
-
1
-
W
3/
1
1
/
2
0
1
5

<
0
.
0
6
9
0.0
1
1

J

0
.
0
0
4
7

J
<0
.
0
0
6
9
0.0
0
3
8

J
<1
5

<
1
5

<
1
5

<
1
7
NA

N
A
TP
-
1
-
B
3/
1
1
/
2
0
1
5

<
0
.
0
5
6
<0
.
0
1
1

<
0
.
0
0
5
6

<
0
.
0
0
5
6

<
0
.
0
0
6
5

<
1
4

<
1
4

<
1
4

<
1
6
NA

N
A
TP
-
2
-
N
3/
1
1
/
2
0
1
5

<
0
.
0
0
6
8
<0
.
0
1
4

<
0
.
0
0
5
1

<
0
.
0
0
6
8

<
0
.
0
0
6
8
3.5

J
<1
6

<
1
6

<
2
3
NA

N
A
TP
-
2
-
S
3/
1
1
/
2
0
1
5

<
0
.
0
5
9
<0
.
0
1
2
<0
.
0
0
5
9
<0
.
0
0
5
9

<
0
.
0
0
5
9
1.0

J
<1
4

<
1
4

<
2
0
NA

N
A
TP
-
2
-
E
3/
1
1
/
2
0
1
5

<
0
.
0
6
7
<0
.
0
1
3

<
0
.
0
0
6
7

<
0
.
0
0
6
7

<
0
.
0
0
6
7

<
1
4

<
1
4

<
1
4

<
1
9
NA

N
A
TP
-
2
-
W
3/
1
1
/
2
0
1
5
0.
1
4
<0
.
0
1
1

<
0
.
0
0
5
7

<
0
.
0
0
5
7

<
0
.
0
0
5
7
6.2

J
14
<1
3

<
1
8
NA

N
A
TP
-
2
-
B
1
3/
1
1
/
2
0
1
5
0.0
9
0
<0
.
0
1
1

<
0
.
0
0
5
5
0.0
1
4
<0
.
0
0
5
5
54
0

3
2
0
43
9
.
3
<1
8
NA

N
A
TP
-
2
-
B
1
A
4/
7
/
2
0
1
5

N
A

N
A

N
A

N
A

N
A
16
9
<5
7
.
4

<
1
4
.
4

<
3
.
6
NA

N
A
TP
-
2
-
B
2
3/
1
1
/
2
0
1
5
0.0
7
6
<0
.
0
1
1

<
0
.
0
0
5
4

<
0
.
0
0
5
4

<
0
.
0
0
5
4
7.1

J

5
.
4

J
<1
4

<
1
7
NA

N
A
SP
C
-
1
3/
1
1
/
2
0
1
5

N
A
NA

N
A

N
A

N
A

N
A
NA
NA

N
A
36
<6.5
SP
C
-
2
3/
1
1
/
2
0
1
5

N
A
NA

N
A

N
A

N
A

N
A
NA
NA

N
A
33
<4.8
SP
C
-
3
3/
1
1
/
2
0
1
5

N
A
NA

N
A

N
A

N
A

N
A
NA
NA

N
A
70
<5.8
10

1
0
24

0
.
1
6

8
.
5

8
.
3

4
.
6

5
4
0
Co
n
s
i
d
e
r
e
d

Im
m
o
b
i
l
e
31

6
8
NS

N
S
14
,
0
0
0

3
1
3

7
8
2

7
8
2

3
,
1
2
9

1
,
5
0
0

3
1
,
0
0
0

4
6
9

9
3
9

N
S

N
S
36
0
,
0
0
0

8
,
1
7
6

2
0
,
4
4
0

2
0
,
4
4
0

8
1
,
7
6
0

4
0
,
0
0
0

8
1
0
,
0
0
0

1
2
,
2
6
4

2
4
,
5
2
8
NS

N
S
No
t
e
s
:

1.
T
h
i
s

t
a
b
l
e

o
n
l
y

i
n
c
l
u
d
e
s

c
o
n
s
t
i
t
u
e
n
t
s

d
e
t
e
c
t
e
d

i
n

o
n
e

o
r

m
o
r
e

s
a
m
p
l
e
s
.

T
h
e

c
o
m
p
l
e
t
e

s
u
i
t
e

o
f

c
o
m
p
o
u
n
d
s

c
a
n

b
e

f
o
u
n
d

i
n

t
h
e

a
n
a
l
y
t
i
c
a
l

r
e
p
o
r
t
.
2.
A
l
l

c
o
n
c
e
n
t
r
a
t
i
o
n
s

a
r
e

i
n

m
i
l
l
i
g
r
a
m
s

p
e
r

k
i
l
o
g
r
a
m

(
m
g
/
k
g
)
.
3.
N
A

=

N
o
t

A
n
a
l
y
z
e
d
4.
N
S

=

N
o

S
t
a
n
d
a
r
d
5.
M
A
D
E
P

E
P
H

a
n
d

V
P
H

=

M
a
s
s
a
c
h
u
s
e
t
t
s

D
e
p
a
r
t
m
e
n
t

o
f

E
n
v
i
r
o
n
m
e
n
t
a
l

P
r
o
t
e
c
t
i
o
n

E
x
t
r
a
c
t
a
b
l
e

P
e
t
r
o
l
e
u
m

H
y
d
r
o
c
a
r
b
o
n
s

a
n
d

V
o
l
a
t
i
l
e

P
e
t
r
o
l
e
u
m

H
y
d
r
o
c
a
r
b
o
n
s
6.
M
S
C
C
s

=

M
a
x
i
m
u
m

S
o
i
l

C
o
n
t
a
m
i
n
a
n
t

C
o
n
c
e
n
t
r
a
t
i
o
n

L
e
v
e
l
s

(
M
S
C
C
s
)

S
o
i
l
-
t
o
-
W
a
t
e
r

M
a
x
i
m
u
m

C
o
n
t
a
m
i
n
a
n
t

C
o
n
e
c
n
t
r
a
t
i
o
n
s

a
n
d

I
n
d
u
s
t
r
i
a
l
/
C
o
m
m
e
r
c
i
a
l
S
o
i
l

C
l
e
a
n
u
p

L
e
v
e
l
s

a
r
e

f
r
o
m

t
h
e

N
o
r
t
h

C
a
r
o
l
i
n
a

D
e
p
a
r
t
m
e
n
t

o
f

E
n
v
i
r
o
n
m
e
n
t

a
n
d

N
a
t
u
r
a
l

R
e
s
o
u
r
c
e
s

(
D
E
N
R
)

U
n
d
e
r
g
r
o
u
n
d

S
t
o
r
a
g
e

T
a
n
k

G
u
i
d
e
l
i
n
e
s

f
o
r

S
i
t
e

C
h
e
c
k
s
,

T
a
n
k

C
l
o
s
u
r
e
,

a
n
d

I
n
i
t
i
a
l

R
e
s
p
o
n
s
e

a
n
d

A
b
a
t
e
m
e
n
t

f
o
r

U
S
T

R
e
l
e
a
s
e
s
,

e
f
f
e
c
t
i
v
e

D
e
c
e
m
b
e
r

1
,

2
0
1
3
.

7.
<
0
.
3
9

i
n
d
i
c
a
t
e
s

t
h
a
t

t
h
e

c
o
n
s
t
i
t
u
e
n
t

w
a
s

n
o
t

d
e
t
e
c
t
e
d

a
t

a

c
o
n
c
e
n
t
r
a
t
i
o
n

a
b
o
v
e

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
.
8.
B
o
l
d
e
d

n
u
m
b
e
r
s

i
n
d
i
c
a
t
e

t
h
a
t

t
h
e

c
o
n
s
i
t
u
e
n
t

w
a
s

d
e
t
e
c
t
e
d

a
t

a

c
o
n
c
e
n
t
r
a
t
i
o
n

a
b
o
v
e

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
.
9.
S
h
a
d
e
d

c
e
l
l
s

i
n
d
i
c
a
t
e

t
h
a
t

t
h
e

c
o
n
s
t
i
t
u
e
n
t

c
o
n
c
e
n
t
r
a
t
i
o
n

e
x
c
e
e
d
e
d

t
h
e

a
p
p
l
i
c
a
b
l
e

s
t
a
n
d
a
r
d
.

10
.

T
P
H
,

D
R
O
,

G
R
O

=

T
o
t
a
l

P
e
t
r
o
l
e
u
m

H
y
d
r
o
c
a
r
b
o
n
s
,

D
i
e
s
e
l

R
a
n
g
e

O
r
g
a
n
i
c
s
,

G
a
s
o
l
i
n
e

R
a
n
g
e

O
r
g
a
n
i
c
s
TP
H
Co
m
m
e
r
c
i
a
l

S
o
i
l

M
S
C
C
S
Vo
l
i
t
a
l
e

O
r
g
a
n
i
c

C
o
m
p
o
u
n
d
s

M
A
D
E
P

E
P
H

a
n
d

V
P
H
Sa
m
p
l
e

ID

Da
t
e

Co
l
l
e
c
t
e
d
So
i
l
-
t
o
-
W
a
t
e
r

M
S
C
C
s
Re
s
i
d
e
n
t
i
a
l

S
o
i
l

M
S
C
C
s
DE
N
R

S
c
r
e
e
n
i
n
g

L
e
v
e
l
s
No
t

A
p
p
l
i
c
a
b
l
e
P:\
W
i
n
t
e
r

S
t
a
r

C
o
r
p
o
r
a
t
i
o
n
\
S
i
t
e

A
s
s
e
s
s
m
e
n
t

R
e
p
o
r
t
\
T
a
b
l
e
s
\
T
a
b
l
e
s

1

-

3
Page 1 of 1
Ta
b
l
e

3
Gr
o
u
n
d
w
a
t
e
r

A
n
a
l
y
t
i
c
a
l

R
e
s
u
l
t
s
Fo
r
m
e
r

B
u
r
n
s
v
i
l
l
e

H
o
s
i
e
r
y

M
i
l
l
Bu
r
n
s
v
i
l
l
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
VO
C
s
T
e
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e
TM
W
-
1
3/
1
8
/
2
0
1
5

<
0
.
0
9
8
TM
W
-
2
3/
1
8
/
2
0
1
5

<
0
.
0
9
8
TM
W
-
3
3/
1
8
/
2
0
1
5
1.
6
0.
7
No
t
e
s
:

1.

T
h
i
s

t
a
b
l
e

o
n
l
y

i
n
c
l
u
d
e
s

c
o
n
s
t
i
t
u
e
n
t
s

d
e
t
e
c
t
e
d

i
n

o
n
e

o
r

m
o
r
e

s
a
m
p
l
e
s
.

T
h
e

c
o
m
p
l
e
t
e

s
u
i
t
e

o
f

c
o
m
p
o
u
n
d
s

c
a
n

b
e

f
o
u
n
d

i
n

t
h
e

a
t
t
a
c
h
e
d

a
n
a
l
y
t
i
c
a
l

r
e
p
o
r
t
.

2.

A
l
l

c
o
n
c
e
n
t
r
a
t
i
o
n
s

a
r
e

i
n

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r

(
u
g
/
L
)
.
3.

V
O
C
s

=

V
o
l
i
t
i
l
e

O
r
g
a
i
n
i
c

C
o
m
p
o
u
n
d
s
4.

<
0
.
0
9
8

i
n
d
i
c
a
t
e
s

t
h
a
t

t
h
e

c
o
n
s
t
i
t
u
e
n
t

w
a
s

n
o
t

d
e
t
e
c
t
e
d

a
t

a

c
o
n
c
e
n
t
r
a
t
i
o
n

a
b
o
v
e

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
m
i
t
.
5.

B
o
l
d
e
d

n
u
m
b
e
r
s

i
n
d
i
c
a
t
e

t
h
a
t

t
h
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Page 1 of 1

APPENDIX A

October 2014 Laboratory Analytical Report and Chain-of-
Custody Form

#=CL#
October 29, 2014
LIMS USE: FR - MIKE FALKNOR
LIMS OBJECT ID: 92222341
92222341
Project:
Pace Project No.:
RE:
Mr. Mike Falknor
Altamont Environmental
231 Haywood Street
Asheville, NC 28806
Burnsville Hosiery 2546.02
Dear Mr. Falknor:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92222341001 SB-1 (10-12')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
92222341002 SB-2 (12-14')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
92222341003 SB-3 (8-10')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
92222341004 SB-4 (6-8')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
92222341005 SB-5 (6-8')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
92222341006 SB-6 (6-8')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
92222341007 SB-7 (6-8')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
92222341008 SB-8 (6-8')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
92222341009 SB-9 (10-12')EPA 8015 Modified 2 PASI-CRES
EPA 8015 Modified 2 PASI-CBFW
ASTM D2974-87 1 PASI-CACS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-1 (10-12')Lab ID: 92222341001 Collected: 10/21/14 11:00 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 10/28/14 17:3710/24/14 09:057.0 1
Surrogates
n-Pentacosane (S)61 %10/28/14 17:37 629-99-210/24/14 09:0541-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/23/14 14:4310/23/14 09:258.5 1
Surrogates
4-Bromofluorobenzene (S)93 %10/23/14 14:43 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 28.6 %10/24/14 13:030.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-2 (12-14')Lab ID: 92222341002 Collected: 10/21/14 11:30 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)40.8 mg/kg 10/28/14 01:2110/24/14 09:056.1 1
Surrogates
n-Pentacosane (S)78 %10/28/14 01:21 629-99-210/24/14 09:0541-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/23/14 15:0610/23/14 09:257.5 1
Surrogates
4-Bromofluorobenzene (S)92 %10/23/14 15:06 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.7 %10/24/14 13:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-3 (8-10')Lab ID: 92222341003 Collected: 10/21/14 11:45 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 10/28/14 18:0110/24/14 09:056.8 1
Surrogates
n-Pentacosane (S)66 %10/28/14 18:01 629-99-210/24/14 09:0541-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/23/14 15:2910/23/14 09:258.0 1
Surrogates
4-Bromofluorobenzene (S)95 %10/23/14 15:29 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 26.3 %10/24/14 13:030.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-4 (6-8')Lab ID: 92222341004 Collected: 10/21/14 12:00 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)847 mg/kg 10/28/14 18:0110/24/14 09:0525.6 4
Surrogates
n-Pentacosane (S)86 %10/28/14 18:01 629-99-210/24/14 09:0541-119 4
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)44.6 mg/kg 10/23/14 15:5110/23/14 09:257.5 1
Surrogates
4-Bromofluorobenzene (S)110 %10/23/14 15:51 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.9 %10/24/14 13:030.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-5 (6-8')Lab ID: 92222341005 Collected: 10/21/14 12:15 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)1180 mg/kg 10/28/14 18:2410/24/14 09:0527.0 4
Surrogates
n-Pentacosane (S)70 %10/28/14 18:24 629-99-210/24/14 09:0541-119 4
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)45.4 mg/kg 10/23/14 16:3710/23/14 09:257.6 1
Surrogates
4-Bromofluorobenzene (S)105 %10/23/14 16:37 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 26.0 %10/24/14 13:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-6 (6-8')Lab ID: 92222341006 Collected: 10/21/14 12:45 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 10/28/14 02:0810/24/14 09:056.1 1
Surrogates
n-Pentacosane (S)71 %10/28/14 02:08 629-99-210/24/14 09:0541-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/23/14 17:2310/23/14 09:257.2 1
Surrogates
4-Bromofluorobenzene (S)88 %10/23/14 17:23 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.7 %10/24/14 13:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-7 (6-8')Lab ID: 92222341007 Collected: 10/21/14 13:00 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 10/28/14 18:2410/24/14 09:055.6 1
Surrogates
n-Pentacosane (S)69 %10/28/14 18:24 629-99-210/24/14 09:0541-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/23/14 17:4610/23/14 09:256.1 1
Surrogates
4-Bromofluorobenzene (S)94 %10/23/14 17:46 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.7 %10/24/14 13:040.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-8 (6-8')Lab ID: 92222341008 Collected: 10/21/14 13:15 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 10/28/14 02:3210/24/14 09:056.4 1
Surrogates
n-Pentacosane (S)77 %10/28/14 02:32 629-99-210/24/14 09:0541-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/23/14 18:0910/23/14 09:257.7 1
Surrogates
4-Bromofluorobenzene (S)94 %10/23/14 18:09 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.4 %10/24/14 13:040.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Sample: SB-9 (10-12')Lab ID: 92222341009 Collected: 10/21/14 13:45 Received: 10/21/14 17:03 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 10/28/14 18:4810/24/14 09:056.3 1
Surrogates
n-Pentacosane (S)66 %10/28/14 18:48 629-99-210/24/14 09:0541-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/23/14 18:3210/23/14 09:257.7 1
Surrogates
4-Bromofluorobenzene (S)90 %10/23/14 18:32 460-00-410/23/14 09:2570-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.1 %10/24/14 13:040.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8694
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples:92222341001, 92222341002, 92222341003, 92222341004, 92222341005, 92222341006, 92222341007,
92222341008, 92222341009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1313230
Associated Lab Samples: 92222341001, 92222341002, 92222341003, 92222341004, 92222341005, 92222341006, 92222341007,
92222341008, 92222341009
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 10/23/14 10:32
4-Bromofluorobenzene (S)%91 70-167 10/23/14 10:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1313231LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 54.650 109 70-165
4-Bromofluorobenzene (S)%94 70-167
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1313232MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92222545008
1313233
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Gas Range Organics (C6-C10) mg/kg 46.3 130 47-187151 1546.3ND 60.8 70.4
4-Bromofluorobenzene (S) %96 70-167100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/30674
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples:92222341001, 92222341002, 92222341003, 92222341004, 92222341005, 92222341006, 92222341007,
92222341008, 92222341009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1314328
Associated Lab Samples: 92222341001, 92222341002, 92222341003, 92222341004, 92222341005, 92222341006, 92222341007,
92222341008, 92222341009
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 10/28/14 15:28
n-Pentacosane (S)%79 41-119 10/28/14 15:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1314329LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28) mg/kg 51.266.7 77 49-113
n-Pentacosane (S)%80 41-119
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1314330MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92222341001
1314331
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Range Organics(C10-
C28)mg/kg 93.5 66 10-14673 993.5ND 63.2 69.3
n-Pentacosane (S)%68 41-11972
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7159
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92222341002, 92222341005, 92222341006
Parameter Units
Dup
Result QualifiersRPDResult
92222323001
1313256SAMPLE DUPLICATE:
Percent Moisture %32.5 132.3
Parameter Units
Dup
Result QualifiersRPDResult
92222392004
1313257SAMPLE DUPLICATE:
Percent Moisture %57.4 359.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7161
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92222341001, 92222341003, 92222341004, 92222341007, 92222341008, 92222341009
Parameter Units
Dup
Result QualifiersRPDResult
92222341001
1313713SAMPLE DUPLICATE:
Percent Moisture %27.9 328.6
Parameter Units
Dup
Result QualifiersRPDResult
92222502001
1313714SAMPLE DUPLICATE:
Percent Moisture %22.9 022.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
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Asheville, NC 28804
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Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 21
#=MEXR
METHOD CROSS REFERENCE TABLE
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Parameter Matrix Preparation MethodAnalytical Method
8015 GCS THC-Diesel Solid SW 846 3546 SW 846 8015C
Gasoline Range Organics Solid SW 846 8015C SW 846 5030B
Percent Moisture Solid ASTM D2974-87 N/A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92222341
Burnsville Hosiery 2546.02
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92222341001 OEXT/30674 GCSV/19306SB-1 (10-12')EPA 3546 EPA 8015 Modified
92222341002 OEXT/30674 GCSV/19306SB-2 (12-14')EPA 3546 EPA 8015 Modified
92222341003 OEXT/30674 GCSV/19306SB-3 (8-10')EPA 3546 EPA 8015 Modified
92222341004 OEXT/30674 GCSV/19306SB-4 (6-8')EPA 3546 EPA 8015 Modified
92222341005 OEXT/30674 GCSV/19306SB-5 (6-8')EPA 3546 EPA 8015 Modified
92222341006 OEXT/30674 GCSV/19306SB-6 (6-8')EPA 3546 EPA 8015 Modified
92222341007 OEXT/30674 GCSV/19306SB-7 (6-8')EPA 3546 EPA 8015 Modified
92222341008 OEXT/30674 GCSV/19306SB-8 (6-8')EPA 3546 EPA 8015 Modified
92222341009 OEXT/30674 GCSV/19306SB-9 (10-12')EPA 3546 EPA 8015 Modified
92222341001 GCV/8694 GCV/8698SB-1 (10-12')EPA 5035A/5030B EPA 8015 Modified
92222341002 GCV/8694 GCV/8698SB-2 (12-14')EPA 5035A/5030B EPA 8015 Modified
92222341003 GCV/8694 GCV/8698SB-3 (8-10')EPA 5035A/5030B EPA 8015 Modified
92222341004 GCV/8694 GCV/8698SB-4 (6-8')EPA 5035A/5030B EPA 8015 Modified
92222341005 GCV/8694 GCV/8698SB-5 (6-8')EPA 5035A/5030B EPA 8015 Modified
92222341006 GCV/8694 GCV/8698SB-6 (6-8')EPA 5035A/5030B EPA 8015 Modified
92222341007 GCV/8694 GCV/8698SB-7 (6-8')EPA 5035A/5030B EPA 8015 Modified
92222341008 GCV/8694 GCV/8698SB-8 (6-8')EPA 5035A/5030B EPA 8015 Modified
92222341009 GCV/8694 GCV/8698SB-9 (10-12')EPA 5035A/5030B EPA 8015 Modified
92222341001 PMST/7161SB-1 (10-12')ASTM D2974-87
92222341002 PMST/7159SB-2 (12-14')ASTM D2974-87
92222341003 PMST/7161SB-3 (8-10')ASTM D2974-87
92222341004 PMST/7161SB-4 (6-8')ASTM D2974-87
92222341005 PMST/7159SB-5 (6-8')ASTM D2974-87
92222341006 PMST/7159SB-6 (6-8')ASTM D2974-87
92222341007 PMST/7161SB-7 (6-8')ASTM D2974-87
92222341008 PMST/7161SB-8 (6-8')ASTM D2974-87
92222341009 PMST/7161SB-9 (10-12')ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 10/29/2014 05:09 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 21
Page 20 of 21
Page 21 of 21

APPENDIX B

UST-61 Form

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY)
Incident # ________ Risk (H,I,L,U)_______
Received On ________ Received By ________
Reported by (circle one): Phone, Fax or Report
Region _______
Suspected Contamination? (Y/N) ________
Confirmed GW Contamination? (Y/N) ______
Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______
Free Product? (Y/N) _____ If Yes, State Greatest
Thickness ______________
Facility ID Number ______________
Date Leak Discovered ___________
Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address:County:
City/Town:Zip Code:Regional Office (circle one): Asheville, Mooresville, Fayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) :Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)T GPS
T Topographic map
T GIS Address matching
T Other
T Unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
T Release Detection Equipment or Methods
T During UST Closure/Removal
T Property Transfer
T Visual/Odor
T Water in Tank
T Water Supply Well Contamination
T Groundwater Contamination
T Surface Water Contamination
T Other (specify) _______________
SOURCE OF CONTAMINATION
Source of Release
(Check one to indicate primary
source)
Cause of Release
(Check one to indicate primary
cause)
Type of Release
(Check one)
Product Type Released
(Check one to indicate primary product type
released)
T Tank
T Piping
T Dispenser
T Submersible Turbine Pump
T Delivery Problem
T Other
T Unknown
Definitions presented on reverse
T Spill
T Overfill
T Corrosion
T Physical or Mechanical
Damage
T Install Problem
T Other
T Unknown
Definitions presented on reverse
T Petroleum
T Non-Petroleum
T Both
Location
(Check one)
T Facility
T Residence
T Other
T Gasoline/ Diesel/
Kerosene
T Heating Oil
T Other Petroleum
Products
T Metals
T Other Inorganics
T Other Organics
T Diesel/Veg. Oil
Blend
T Vegetable Oil 100%
T E10 – E20
T E21 – E84
T E85 – E99
T Ethanol 100%
T E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/08)Page 1 of 2
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/08)Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser:includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage:use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion:use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

APPENDIX C

March 2015 Laboratory Analytical Report and Chain-of-
Custody Form

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
03/20/2015
Altamont Environmental Inc
Mike Falknor
231 Haywood Street
Asheville, NC 28801
Project: Burnsville Hosiery
Lab Submittal Date: 03/13/2015
Prism Work Order: 5030255
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 82
Sample Receipt Summary
03/20/2015
Prism Work Order: 5030255
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
5030255-01 03/11/15TP-1-N 03/13/15Solid
5030255-02 03/11/15TP-1-S 03/13/15Solid
5030255-03 03/11/15TP-1-E 03/13/15Solid
5030255-04 03/11/15TP-1-W 03/13/15Solid
5030255-05 03/11/15TP-1-B 03/13/15Solid
5030255-06 03/11/15TP-2-N 03/13/15Solid
5030255-07 03/11/15TP-2-S 03/13/15Solid
5030255-08 03/11/15TP-2-E 03/13/15Solid
5030255-09 03/11/15TP-2-W 03/13/15Solid
5030255-10 03/11/15TP-2-B1 03/13/15Solid
5030255-11 03/11/15TP-2-B2 03/13/15Solid
5030255-12 03/11/15SPC-1 03/13/15Solid
5030255-13 03/11/15SPC-2 03/13/15Solid
5030255-14 03/11/15SPC-3 03/13/15Solid
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 82
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 5030255
03/20/2015
Summary of Detections
39 mg/kg dry5030255-02 TP-1-S C9-C18 Aliphatics MADEP EPH
13 J mg/kg dry5030255-02 TP-1-S C19-C36 Aliphatics MADEP EPH
16 mg/kg dry5030255-03 TP-1-E C9-C18 Aliphatics MADEP EPH
9.5 J mg/kg dry5030255-03 TP-1-E C19-C36 Aliphatics MADEP EPH
3.9 J mg/kg dry5030255-03 TP-1-E C11-C22 Aromatics MADEP EPH
0.0031 J mg/kg dry5030255-03 TP-1-E 1,2,4-Trimethylbenzene 8260B
0.0081 J mg/kg dry5030255-03 TP-1-E Naphthalene 8260B
0.0047 J mg/kg dry5030255-04 TP-1-W 1,2,4-Trimethylbenzene 8260B
0.011 J mg/kg dry5030255-04 TP-1-W Naphthalene 8260B
0.0038 J mg/kg dry5030255-04 TP-1-W o-Xylene 8260B
0.0038 J mg/kg dry5030255-04 TP-1-W Xylenes, total 8260B
3.5 J mg/kg dry5030255-06 TP-2-N C9-C18 Aliphatics MADEP EPH
1.0 J mg/kg dry5030255-07 TP-2-S C9-C18 Aliphatics MADEP EPH
6.2 J mg/kg dry5030255-09 TP-2-W C9-C18 Aliphatics MADEP EPH
14 mg/kg dry5030255-09 TP-2-W C19-C36 Aliphatics MADEP EPH
0.14 mg/kg dry5030255-09 TP-2-W Acetone 8260B
540 mg/kg dry5030255-10 TP-2-B1 C9-C18 Aliphatics MADEP EPH
320 mg/kg dry5030255-10 TP-2-B1 C19-C36 Aliphatics MADEP EPH
430 mg/kg dry5030255-10 TP-2-B1 C11-C22 Aromatics MADEP EPH
0.014 mg/kg dry5030255-10 TP-2-B1 1,3,5-Trimethylbenzene 8260B
0.090 mg/kg dry5030255-10 TP-2-B1 Acetone 8260B
9.3 J mg/kg dry5030255-10 TP-2-B1 C9-C10 Aromatics MADEP VPH
7.1 J mg/kg dry5030255-11 TP-2-B2 C9-C18 Aliphatics MADEP EPH
5.4 J mg/kg dry5030255-11 TP-2-B2 C19-C36 Aliphatics MADEP EPH
0.076 mg/kg dry5030255-11 TP-2-B2 Acetone 8260B
36 mg/kg dry5030255-12 SPC-1 Diesel Range Organics *8015C
33 mg/kg dry5030255-13 SPC-2 Diesel Range Organics *8015C
70 mg/kg dry5030255-14 SPC-3 Diesel Range Organics *8015C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-N
Prism Sample ID: 5030255-01
Prism Work Order: 5030255
Time Collected: 03/11/15 11:30
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P5C02581133/17/15 19:33 KCmg/kg dry 0.73C9-C18 Aliphatics
BRL MADEP EPH P5C02581133/17/15 19:33 KCmg/kg dry 3.0C19-C36 Aliphatics
BRL MADEP EPH P5C02581133/17/15 19:33 KCmg/kg dry 2.3C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14064 %1-Chlorooctadecane
40-14076 %o-Terphenyl
40-14089 %2-Fluorobiphenyl
40-14077 %2-Bromonaphthalene
General Chemistry Parameters
78.3 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0661,2,4-Trichlorobenzene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0641,2-Dichlorobenzene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0591,3-Dichlorobenzene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0621,4-Dichlorobenzene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0811-Methylnaphthalene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0792,4,6-Trichlorophenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0812,4-Dichlorophenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0652,4-Dimethylphenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0592,4-Dinitrophenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0512,4-Dinitrotoluene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0602-Chlorophenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0672-Methylnaphthalene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0542-Methylphenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0772-Nitrophenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0833,3'-Dichlorobenzidine
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0634,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0724-Bromophenyl phenyl ether
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0514-Chloroaniline
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0554-Chlorophenyl phenyl ether
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.0654-Nitrophenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.057Acenaphthene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.061Acenaphthylene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.068Anthracene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.056Azobenzene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.046Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-N
Prism Sample ID: 5030255-01
Prism Work Order: 5030255
Time Collected: 03/11/15 11:30
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.055Benzo(k)fluoranthene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.035Benzoic Acid
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.056Benzyl alcohol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.073bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.059Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.072Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.053Chrysene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.051Dibenzo(a,h)anthracene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.064Dibenzofuran
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.058Diethyl phthalate
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.060Di-n-butyl phthalate
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.052Di-n-octyl phthalate
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.054Fluoranthene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.060Fluorene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.067Hexachlorobenzene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.076Hexachlorobutadiene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.075Hexachlorocyclopentadiene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.071Hexachloroethane
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.048Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.057Isophorone
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.068Naphthalene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.060Nitrobenzene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.066N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.050Pentachlorophenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.055Phenanthrene
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.062Phenol
BRL 8270D P5C026410.42 3/17/15 15:49 KCmg/kg dry 0.056Pyrene
Surrogate Recovery Control Limits
39-13283 %2,4,6-Tribromophenol
44-11577 %2-Fluorobiphenyl
35-11576 %2-Fluorophenol
37-12281 %Nitrobenzene-d5
34-12177 %Phenol-d5
54-12795 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000471,1,1,2-Tetrachloroethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000281,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-N
Prism Sample ID: 5030255-01
Prism Work Order: 5030255
Time Collected: 03/11/15 11:30
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000391,1,2,2-Tetrachloroethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000511,1,2-Trichloroethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000731,2,3-Trichloropropane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000421,2,4-Trichlorobenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000441,2,4-Trimethylbenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000341,2-Dichloroethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000431,3,5-Trimethylbenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000381,3-Dichlorobenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000291,3-Dichloropropane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000344-Chlorotoluene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.000274-Isopropyltoluene
BRL 8260B P5C026210.057 3/16/15 21:21 MSCmg/kg dry 0.0014Acetone
BRL 8260B P5C026210.0034 3/16/15 21:21 MSCmg/kg dry 0.00033Benzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00048Bromobenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00031Bromochloromethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00032Bromodichloromethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00065Bromoform
BRL 8260B P5C026210.011 3/16/15 21:21 MSCmg/kg dry 0.00070Bromomethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00030Chlorobenzene
BRL 8260B P5C026210.011 3/16/15 21:21 MSCmg/kg dry 0.00048Chloroethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00041Chloroform
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00038Chloromethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00026Dichlorodifluoromethane
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00022Ethylbenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00034Isopropylbenzene (Cumene)
BRL 8260B P5C026210.011 3/16/15 21:21 MSCmg/kg dry 0.00053m,p-Xylenes
BRL 8260B P5C026210.057 3/16/15 21:21 MSCmg/kg dry 0.00052Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C026210.11 3/16/15 21:21 MSCmg/kg dry 0.00052Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-N
Prism Sample ID: 5030255-01
Prism Work Order: 5030255
Time Collected: 03/11/15 11:30
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.057 3/16/15 21:21 MSCmg/kg dry 0.00049Methyl Isobutyl Ketone
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00032Methylene Chloride
BRL 8260B P5C026210.011 3/16/15 21:21 MSCmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P5C026210.011 3/16/15 21:21 MSCmg/kg dry 0.00018Naphthalene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00029n-Butylbenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00034n-Propylbenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00023o-Xylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00028sec-Butylbenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00034Styrene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00033Toluene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00037Trichloroethylene
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00037Trichlorofluoromethane
BRL 8260B P5C026210.029 3/16/15 21:21 MSCmg/kg dry 0.00078Vinyl acetate
BRL 8260B P5C026210.0057 3/16/15 21:21 MSCmg/kg dry 0.00028Vinyl chloride
BRL 8260B P5C026210.017 3/16/15 21:21 MSCmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130112 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12999 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100173/18/15 19:18 ANGmg/kg dry 0.67C5-C8 Aliphatics
BRL MADEP VPH P5C0303100173/18/15 19:18 ANGmg/kg dry 1.6C9-C12 Aliphatics
BRL MADEP VPH P5C0303100173/18/15 19:18 ANGmg/kg dry 0.15C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130109 %2,5-Dibromotoluene (PID)
70-130102 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-S
Prism Sample ID: 5030255-02
Prism Work Order: 5030255
Time Collected: 03/11/15 11:23
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
39 MADEP EPH P5C02581153/17/15 20:09 KCmg/kg dry 0.86C9-C18 Aliphatics
13 MADEP EPH P5C02581153/17/15 20:09 KCJmg/kg dry 3.5C19-C36 Aliphatics
BRL MADEP EPH P5C02581153/17/15 20:09 KCmg/kg dry 2.7C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14083 %1-Chlorooctadecane
40-14082 %o-Terphenyl
40-14080 %2-Fluorobiphenyl
40-14068 %2-Bromonaphthalene
General Chemistry Parameters
66.1 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0781,2,4-Trichlorobenzene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0761,2-Dichlorobenzene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0701,3-Dichlorobenzene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0731,4-Dichlorobenzene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0961-Methylnaphthalene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0932,4,6-Trichlorophenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0962,4-Dichlorophenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0762,4-Dimethylphenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0702,4-Dinitrophenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0612,4-Dinitrotoluene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0662,6-Dinitrotoluene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0722-Chloronaphthalene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0712-Chlorophenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0802-Methylnaphthalene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0642-Methylphenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0912-Nitrophenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0983,3'-Dichlorobenzidine
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0613/4-Methylphenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0754,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0864-Bromophenyl phenyl ether
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0704-Chloro-3-methylphenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0604-Chloroaniline
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0654-Chlorophenyl phenyl ether
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.0774-Nitrophenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.068Acenaphthene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.072Acenaphthylene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.080Anthracene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.066Azobenzene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.065Benzo(a)anthracene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.054Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-S
Prism Sample ID: 5030255-02
Prism Work Order: 5030255
Time Collected: 03/11/15 11:23
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.058Benzo(b)fluoranthene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.055Benzo(g,h,i)perylene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.065Benzo(k)fluoranthene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.042Benzoic Acid
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.066Benzyl alcohol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.087bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.070Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.085Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.074Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.071Butyl benzyl phthalate
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.063Chrysene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.061Dibenzo(a,h)anthracene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.076Dibenzofuran
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.069Diethyl phthalate
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.066Dimethyl phthalate
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.071Di-n-butyl phthalate
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.061Di-n-octyl phthalate
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.064Fluoranthene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.072Fluorene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.079Hexachlorobenzene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.090Hexachlorobutadiene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.089Hexachlorocyclopentadiene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.083Hexachloroethane
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.057Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.067Isophorone
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.080Naphthalene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.071Nitrobenzene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.079N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.076N-Nitrosodiphenylamine
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.059Pentachlorophenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.065Phenanthrene
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.074Phenol
BRL 8270D P5C026410.50 3/17/15 16:10 KCmg/kg dry 0.066Pyrene
Surrogate Recovery Control Limits
39-13285 %2,4,6-Tribromophenol
44-11582 %2-Fluorobiphenyl
35-11584 %2-Fluorophenol
37-12287 %Nitrobenzene-d5
34-12181 %Phenol-d5
54-12797 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000531,1,1,2-Tetrachloroethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000311,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-S
Prism Sample ID: 5030255-02
Prism Work Order: 5030255
Time Collected: 03/11/15 11:23
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000441,1,2,2-Tetrachloroethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000571,1,2-Trichloroethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000291,1-Dichloroethylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000361,1-Dichloropropylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000371,2,3-Trichlorobenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000831,2,3-Trichloropropane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000481,2,4-Trichlorobenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000501,2,4-Trimethylbenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000261,2-Dibromoethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000301,2-Dichlorobenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000391,2-Dichloroethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000401,2-Dichloropropane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000491,3,5-Trimethylbenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000431,3-Dichlorobenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000331,3-Dichloropropane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000312,2-Dichloropropane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000332-Chlorotoluene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000394-Chlorotoluene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.000314-Isopropyltoluene
BRL 8260B P5C026210.065 3/16/15 21:52 MSCmg/kg dry 0.0016Acetone
BRL 8260B P5C026210.0039 3/16/15 21:52 MSCmg/kg dry 0.00038Benzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00054Bromobenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00036Bromochloromethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00036Bromodichloromethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00074Bromoform
BRL 8260B P5C026210.013 3/16/15 21:52 MSCmg/kg dry 0.00080Bromomethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00032Carbon Tetrachloride
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00034Chlorobenzene
BRL 8260B P5C026210.013 3/16/15 21:52 MSCmg/kg dry 0.00054Chloroethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00047Chloroform
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00044Chloromethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00028cis-1,2-Dichloroethylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00027Dibromochloromethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00029Dichlorodifluoromethane
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00025Ethylbenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00038Isopropylbenzene (Cumene)
BRL 8260B P5C026210.013 3/16/15 21:52 MSCmg/kg dry 0.00060m,p-Xylenes
BRL 8260B P5C026210.065 3/16/15 21:52 MSCmg/kg dry 0.00059Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C026210.13 3/16/15 21:52 MSCmg/kg dry 0.00059Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-S
Prism Sample ID: 5030255-02
Prism Work Order: 5030255
Time Collected: 03/11/15 11:23
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.065 3/16/15 21:52 MSCmg/kg dry 0.00055Methyl Isobutyl Ketone
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00036Methylene Chloride
BRL 8260B P5C026210.013 3/16/15 21:52 MSCmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P5C026210.013 3/16/15 21:52 MSCmg/kg dry 0.00021Naphthalene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00033n-Butylbenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00039n-Propylbenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00027o-Xylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00031sec-Butylbenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00039Styrene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00022tert-Butylbenzene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00031Tetrachloroethylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00037Toluene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00039trans-1,2-Dichloroethylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00034trans-1,3-Dichloropropylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00042Trichloroethylene
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00042Trichlorofluoromethane
BRL 8260B P5C026210.032 3/16/15 21:52 MSCmg/kg dry 0.00089Vinyl acetate
BRL 8260B P5C026210.0065 3/16/15 21:52 MSCmg/kg dry 0.00031Vinyl chloride
BRL 8260B P5C026210.019 3/16/15 21:52 MSCmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130111 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-129100 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100193/18/15 19:51 ANGmg/kg dry 0.71C5-C8 Aliphatics
BRL MADEP VPH P5C0303100193/18/15 19:51 ANGmg/kg dry 1.7C9-C12 Aliphatics
BRL MADEP VPH P5C0303100193/18/15 19:51 ANGmg/kg dry 0.16C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130126 %2,5-Dibromotoluene (PID)
70-130118 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-E
Prism Sample ID: 5030255-03
Prism Work Order: 5030255
Time Collected: 03/11/15 11:15
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
16 MADEP EPH P5C02581163/17/15 20:46 KCmg/kg dry 0.94C9-C18 Aliphatics
9.5 MADEP EPH P5C02581163/17/15 20:46 KCJmg/kg dry 3.8C19-C36 Aliphatics
3.9 MADEP EPH P5C02581163/17/15 20:46 KCJmg/kg dry 3.0C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14095 %1-Chlorooctadecane
40-14080 %o-Terphenyl
40-14083 %2-Fluorobiphenyl
40-14080 %2-Bromonaphthalene
General Chemistry Parameters
60.8 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0851,2,4-Trichlorobenzene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0821,2-Dichlorobenzene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0761,3-Dichlorobenzene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0791,4-Dichlorobenzene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.101-Methylnaphthalene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.102,4,6-Trichlorophenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.102,4-Dichlorophenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0832,4-Dimethylphenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0762,4-Dinitrophenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0662,4-Dinitrotoluene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0722,6-Dinitrotoluene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0792-Chloronaphthalene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0772-Chlorophenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0872-Methylnaphthalene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0702-Methylphenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0992-Nitrophenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.113,3'-Dichlorobenzidine
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0673/4-Methylphenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0814,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0934-Bromophenyl phenyl ether
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0764-Chloro-3-methylphenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0654-Chloroaniline
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0704-Chlorophenyl phenyl ether
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.0844-Nitrophenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.074Acenaphthene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.079Acenaphthylene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.087Anthracene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.072Azobenzene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.071Benzo(a)anthracene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.059Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-E
Prism Sample ID: 5030255-03
Prism Work Order: 5030255
Time Collected: 03/11/15 11:15
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.063Benzo(b)fluoranthene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.059Benzo(g,h,i)perylene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.071Benzo(k)fluoranthene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.046Benzoic Acid
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.071Benzyl alcohol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.094bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.077Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.093Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.081Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.077Butyl benzyl phthalate
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.068Chrysene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.066Dibenzo(a,h)anthracene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.082Dibenzofuran
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.075Diethyl phthalate
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.072Dimethyl phthalate
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.077Di-n-butyl phthalate
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.067Di-n-octyl phthalate
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.069Fluoranthene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.078Fluorene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.086Hexachlorobenzene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.097Hexachlorobutadiene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.097Hexachlorocyclopentadiene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.091Hexachloroethane
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.062Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.073Isophorone
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.087Naphthalene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.077Nitrobenzene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.085N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.082N-Nitrosodiphenylamine
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.064Pentachlorophenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.070Phenanthrene
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.080Phenol
BRL 8270D P5C026410.54 3/17/15 16:32 KCmg/kg dry 0.072Pyrene
Surrogate Recovery Control Limits
39-13283 %2,4,6-Tribromophenol
44-11579 %2-Fluorobiphenyl
35-11583 %2-Fluorophenol
37-12285 %Nitrobenzene-d5
34-12180 %Phenol-d5
54-12791 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000571,1,1,2-Tetrachloroethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000341,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-E
Prism Sample ID: 5030255-03
Prism Work Order: 5030255
Time Collected: 03/11/15 11:15
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000621,1,2-Trichloroethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000311,1-Dichloroethylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000401,2,3-Trichlorobenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000891,2,3-Trichloropropane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000521,2,4-Trichlorobenzene
0.0031 8260B P5C026210.0070 3/17/15 0:00 MSCJmg/kg dry 0.000531,2,4-Trimethylbenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000331,2-Dichlorobenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000531,3,5-Trimethylbenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000461,3-Dichlorobenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000351,3-Dichloropropane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000362-Chlorotoluene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.000344-Isopropyltoluene
BRL 8260B P5C026210.070 3/17/15 0:00 MSCmg/kg dry 0.0017Acetone
BRL 8260B P5C026210.0042 3/17/15 0:00 MSCmg/kg dry 0.00040Benzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00058Bromobenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00038Bromochloromethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00039Bromodichloromethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00079Bromoform
BRL 8260B P5C026210.014 3/17/15 0:00 MSCmg/kg dry 0.00086Bromomethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00035Carbon Tetrachloride
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00037Chlorobenzene
BRL 8260B P5C026210.014 3/17/15 0:00 MSCmg/kg dry 0.00058Chloroethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00050Chloroform
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00047Chloromethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00030cis-1,2-Dichloroethylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00032Dichlorodifluoromethane
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00027Ethylbenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P5C026210.014 3/17/15 0:00 MSCmg/kg dry 0.00064m,p-Xylenes
BRL 8260B P5C026210.070 3/17/15 0:00 MSCmg/kg dry 0.00063Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C026210.14 3/17/15 0:00 MSCmg/kg dry 0.00063Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-E
Prism Sample ID: 5030255-03
Prism Work Order: 5030255
Time Collected: 03/11/15 11:15
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.070 3/17/15 0:00 MSCmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00039Methylene Chloride
BRL 8260B P5C026210.014 3/17/15 0:00 MSCmg/kg dry 0.00022Methyl-tert-Butyl Ether
0.0081 8260B P5C026210.014 3/17/15 0:00 MSCJmg/kg dry 0.00022Naphthalene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00029o-Xylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00034sec-Butylbenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00042Styrene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00024tert-Butylbenzene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00040Toluene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00042trans-1,2-Dichloroethylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00037trans-1,3-Dichloropropylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00045Trichloroethylene
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00045Trichlorofluoromethane
BRL 8260B P5C026210.035 3/17/15 0:00 MSCmg/kg dry 0.00095Vinyl acetate
BRL 8260B P5C026210.0070 3/17/15 0:00 MSCmg/kg dry 0.00034Vinyl chloride
BRL 8260B P5C026210.021 3/17/15 0:00 MSCmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130111 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-129100 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100203/18/15 20:23 ANGmg/kg dry 0.78C5-C8 Aliphatics
BRL MADEP VPH P5C0303100203/18/15 20:23 ANGmg/kg dry 1.8C9-C12 Aliphatics
BRL MADEP VPH P5C0303100203/18/15 20:23 ANGmg/kg dry 0.17C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130119 %2,5-Dibromotoluene (PID)
70-130112 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-W
Prism Sample ID: 5030255-04
Prism Work Order: 5030255
Time Collected: 03/11/15 11:05
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P5C02581153/17/15 21:22 KCmg/kg dry 0.84C9-C18 Aliphatics
BRL MADEP EPH P5C02581153/17/15 21:22 KCmg/kg dry 3.4C19-C36 Aliphatics
BRL MADEP EPH P5C02581153/17/15 21:22 KCmg/kg dry 2.7C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14080 %1-Chlorooctadecane
40-14071 %o-Terphenyl
40-14075 %2-Fluorobiphenyl
40-14060 %2-Bromonaphthalene
General Chemistry Parameters
67.9 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0761,2,4-Trichlorobenzene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0741,2-Dichlorobenzene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0681,3-Dichlorobenzene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0711,4-Dichlorobenzene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0941-Methylnaphthalene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0912,4,6-Trichlorophenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0942,4-Dichlorophenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0742,4-Dimethylphenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0682,4-Dinitrophenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0592,4-Dinitrotoluene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0652,6-Dinitrotoluene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0702-Chloronaphthalene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0692-Chlorophenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0782-Methylnaphthalene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0622-Methylphenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0882-Nitrophenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0963,3'-Dichlorobenzidine
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0603/4-Methylphenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0734,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0834-Bromophenyl phenyl ether
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0684-Chloro-3-methylphenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0584-Chloroaniline
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0634-Chlorophenyl phenyl ether
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.0754-Nitrophenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.066Acenaphthene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.070Acenaphthylene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.078Anthracene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.064Azobenzene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.064Benzo(a)anthracene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.053Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-W
Prism Sample ID: 5030255-04
Prism Work Order: 5030255
Time Collected: 03/11/15 11:05
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.056Benzo(b)fluoranthene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.053Benzo(g,h,i)perylene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.064Benzo(k)fluoranthene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.041Benzoic Acid
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.064Benzyl alcohol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.084bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.069Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.083Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.072Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.069Butyl benzyl phthalate
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.061Chrysene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.059Dibenzo(a,h)anthracene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.074Dibenzofuran
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.067Diethyl phthalate
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.064Dimethyl phthalate
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.069Di-n-butyl phthalate
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.060Di-n-octyl phthalate
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.062Fluoranthene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.070Fluorene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.077Hexachlorobenzene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.087Hexachlorobutadiene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.087Hexachlorocyclopentadiene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.081Hexachloroethane
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.056Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.066Isophorone
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.078Naphthalene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.069Nitrobenzene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.076N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.074N-Nitrosodiphenylamine
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.057Pentachlorophenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.063Phenanthrene
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.072Phenol
BRL 8270D P5C026410.49 3/17/15 16:53 KCmg/kg dry 0.064Pyrene
Surrogate Recovery Control Limits
39-13283 %2,4,6-Tribromophenol
44-11579 %2-Fluorobiphenyl
35-11578 %2-Fluorophenol
37-12282 %Nitrobenzene-d5
34-12176 %Phenol-d5
54-12796 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000571,1,1,2-Tetrachloroethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000341,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-W
Prism Sample ID: 5030255-04
Prism Work Order: 5030255
Time Collected: 03/11/15 11:05
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000611,1,2-Trichloroethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000311,1-Dichloroethylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000881,2,3-Trichloropropane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000521,2,4-Trichlorobenzene
0.0047 8260B P5C026210.0069 3/17/15 0:31 MSCJmg/kg dry 0.000531,2,4-Trimethylbenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000331,2-Dichlorobenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000521,3,5-Trimethylbenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000461,3-Dichlorobenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000351,3-Dichloropropane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000362-Chlorotoluene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.000334-Isopropyltoluene
BRL 8260B P5C026210.069 3/17/15 0:31 MSCmg/kg dry 0.0017Acetone
BRL 8260B P5C026210.0042 3/17/15 0:31 MSCmg/kg dry 0.00040Benzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00058Bromobenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00038Bromochloromethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00039Bromodichloromethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00079Bromoform
BRL 8260B P5C026210.014 3/17/15 0:31 MSCmg/kg dry 0.00086Bromomethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00035Carbon Tetrachloride
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00037Chlorobenzene
BRL 8260B P5C026210.014 3/17/15 0:31 MSCmg/kg dry 0.00058Chloroethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00050Chloroform
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00047Chloromethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00030cis-1,2-Dichloroethylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00027Ethylbenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P5C026210.014 3/17/15 0:31 MSCmg/kg dry 0.00064m,p-Xylenes
BRL 8260B P5C026210.069 3/17/15 0:31 MSCmg/kg dry 0.00063Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C026210.14 3/17/15 0:31 MSCmg/kg dry 0.00063Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-W
Prism Sample ID: 5030255-04
Prism Work Order: 5030255
Time Collected: 03/11/15 11:05
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.069 3/17/15 0:31 MSCmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00039Methylene Chloride
BRL 8260B P5C026210.014 3/17/15 0:31 MSCmg/kg dry 0.00022Methyl-tert-Butyl Ether
0.011 8260B P5C026210.014 3/17/15 0:31 MSCJmg/kg dry 0.00022Naphthalene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00041n-Propylbenzene
0.0038 8260B P5C026210.0069 3/17/15 0:31 MSCJmg/kg dry 0.00028o-Xylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00034sec-Butylbenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00042Styrene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00040Toluene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00045Trichloroethylene
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00045Trichlorofluoromethane
BRL 8260B P5C026210.035 3/17/15 0:31 MSCmg/kg dry 0.00095Vinyl acetate
BRL 8260B P5C026210.0069 3/17/15 0:31 MSCmg/kg dry 0.00034Vinyl chloride
0.0038 8260B P5C026210.021 3/17/15 0:31 MSCJmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130115 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100173/18/15 20:56 ANGmg/kg dry 0.65C5-C8 Aliphatics
BRL MADEP VPH P5C0303100173/18/15 20:56 ANGmg/kg dry 1.5C9-C12 Aliphatics
BRL MADEP VPH P5C0303100173/18/15 20:56 ANGmg/kg dry 0.15C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130112 %2,5-Dibromotoluene (PID)
70-130106 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-B
Prism Sample ID: 5030255-05
Prism Work Order: 5030255
Time Collected: 03/11/15 11:37
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P5C02581143/17/15 21:59 KCmg/kg dry 0.78C9-C18 Aliphatics
BRL MADEP EPH P5C02581143/17/15 21:59 KCmg/kg dry 3.2C19-C36 Aliphatics
BRL MADEP EPH P5C02581143/17/15 21:59 KCmg/kg dry 2.4C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14082 %1-Chlorooctadecane
40-14077 %o-Terphenyl
40-14079 %2-Fluorobiphenyl
40-14066 %2-Bromonaphthalene
General Chemistry Parameters
73.2 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0701,2,4-Trichlorobenzene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0681,2-Dichlorobenzene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0631,3-Dichlorobenzene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0661,4-Dichlorobenzene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0871-Methylnaphthalene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0852,4,6-Trichlorophenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0872,4-Dichlorophenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0692,4-Dimethylphenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0632,4-Dinitrophenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0552,4-Dinitrotoluene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0602,6-Dinitrotoluene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0652-Chloronaphthalene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0642-Chlorophenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0722-Methylnaphthalene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0582-Methylphenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0822-Nitrophenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0893,3'-Dichlorobenzidine
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0563/4-Methylphenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0684,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0774-Bromophenyl phenyl ether
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0634-Chloro-3-methylphenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0544-Chloroaniline
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0594-Chlorophenyl phenyl ether
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.0694-Nitrophenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.061Acenaphthene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.065Acenaphthylene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.073Anthracene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.060Azobenzene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.059Benzo(a)anthracene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.049Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-B
Prism Sample ID: 5030255-05
Prism Work Order: 5030255
Time Collected: 03/11/15 11:37
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.052Benzo(b)fluoranthene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.049Benzo(g,h,i)perylene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.059Benzo(k)fluoranthene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.038Benzoic Acid
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.059Benzyl alcohol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.078bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.064Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.077Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.067Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.064Butyl benzyl phthalate
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.057Chrysene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.055Dibenzo(a,h)anthracene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.069Dibenzofuran
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.062Diethyl phthalate
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.060Dimethyl phthalate
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.064Di-n-butyl phthalate
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.055Di-n-octyl phthalate
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.057Fluoranthene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.065Fluorene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.072Hexachlorobenzene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.081Hexachlorobutadiene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.080Hexachlorocyclopentadiene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.075Hexachloroethane
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.052Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.061Isophorone
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.072Naphthalene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.064Nitrobenzene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.071N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.069N-Nitrosodiphenylamine
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.053Pentachlorophenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.059Phenanthrene
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.066Phenol
BRL 8270D P5C026410.45 3/17/15 17:14 KCmg/kg dry 0.060Pyrene
Surrogate Recovery Control Limits
39-13296 %2,4,6-Tribromophenol
44-11595 %2-Fluorobiphenyl
35-11593 %2-Fluorophenol
37-12299 %Nitrobenzene-d5
34-12190 %Phenol-d5
54-127108 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000461,1,1,2-Tetrachloroethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000271,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-B
Prism Sample ID: 5030255-05
Prism Work Order: 5030255
Time Collected: 03/11/15 11:37
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000381,1,2,2-Tetrachloroethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000501,1,2-Trichloroethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000721,2,3-Trichloropropane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000421,2,4-Trichlorobenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000431,2,4-Trimethylbenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000261,2-Dichlorobenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000331,2-Dichloroethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000421,3,5-Trimethylbenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000371,3-Dichlorobenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000281,3-Dichloropropane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000334-Chlorotoluene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.000274-Isopropyltoluene
BRL 8260B P5C026210.056 3/16/15 22:24 MSCmg/kg dry 0.0014Acetone
BRL 8260B P5C026210.0034 3/16/15 22:24 MSCmg/kg dry 0.00033Benzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00047Bromobenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00031Bromochloromethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00031Bromodichloromethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00064Bromoform
BRL 8260B P5C026210.011 3/16/15 22:24 MSCmg/kg dry 0.00069Bromomethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00030Chlorobenzene
BRL 8260B P5C026210.011 3/16/15 22:24 MSCmg/kg dry 0.00047Chloroethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00041Chloroform
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00038Chloromethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00026Dichlorodifluoromethane
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00022Ethylbenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00033Isopropylbenzene (Cumene)
BRL 8260B P5C026210.011 3/16/15 22:24 MSCmg/kg dry 0.00052m,p-Xylenes
BRL 8260B P5C026210.056 3/16/15 22:24 MSCmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C026210.11 3/16/15 22:24 MSCmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-1-B
Prism Sample ID: 5030255-05
Prism Work Order: 5030255
Time Collected: 03/11/15 11:37
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.056 3/16/15 22:24 MSCmg/kg dry 0.00048Methyl Isobutyl Ketone
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00032Methylene Chloride
BRL 8260B P5C026210.011 3/16/15 22:24 MSCmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P5C026210.011 3/16/15 22:24 MSCmg/kg dry 0.00018Naphthalene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00029n-Butylbenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00033n-Propylbenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00023o-Xylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00027sec-Butylbenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00034Styrene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00032Toluene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00036Trichloroethylene
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00036Trichlorofluoromethane
BRL 8260B P5C026210.028 3/16/15 22:24 MSCmg/kg dry 0.00077Vinyl acetate
BRL 8260B P5C026210.0056 3/16/15 22:24 MSCmg/kg dry 0.00027Vinyl chloride
BRL 8260B P5C026210.017 3/16/15 22:24 MSCmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130108 %4-Bromofluorobenzene
84-123100 %Dibromofluoromethane
76-12993 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100163/18/15 21:29 ANGmg/kg dry 0.63C5-C8 Aliphatics
BRL MADEP VPH P5C0303100163/18/15 21:29 ANGmg/kg dry 1.5C9-C12 Aliphatics
BRL MADEP VPH P5C0303100163/18/15 21:29 ANGmg/kg dry 0.14C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130110 %2,5-Dibromotoluene (PID)
70-130104 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-N
Prism Sample ID: 5030255-06
Prism Work Order: 5030255
Time Collected: 03/11/15 12:50
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
3.5 MADEP EPH P5C02581163/17/15 23:12 KCJmg/kg dry 0.91C9-C18 Aliphatics
BRL MADEP EPH P5C02581163/17/15 23:12 KCmg/kg dry 3.7C19-C36 Aliphatics
BRL MADEP EPH P5C02581163/17/15 23:12 KCmg/kg dry 2.9C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14077 %1-Chlorooctadecane
40-14080 %o-Terphenyl
40-14084 %2-Fluorobiphenyl
40-14075 %2-Bromonaphthalene
General Chemistry Parameters
62.8 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0821,2,4-Trichlorobenzene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0801,2-Dichlorobenzene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0741,3-Dichlorobenzene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0771,4-Dichlorobenzene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.101-Methylnaphthalene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0982,4,6-Trichlorophenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.102,4-Dichlorophenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0802,4-Dimethylphenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0732,4-Dinitrophenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0642,4-Dinitrotoluene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0702,6-Dinitrotoluene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0762-Chloronaphthalene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0742-Chlorophenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0842-Methylnaphthalene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0672-Methylphenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0962-Nitrophenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.103,3'-Dichlorobenzidine
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0653/4-Methylphenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0794,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0904-Bromophenyl phenyl ether
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0744-Chloro-3-methylphenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0634-Chloroaniline
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0684-Chlorophenyl phenyl ether
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.0814-Nitrophenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.071Acenaphthene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.076Acenaphthylene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.085Anthracene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.069Azobenzene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.069Benzo(a)anthracene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.057Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-N
Prism Sample ID: 5030255-06
Prism Work Order: 5030255
Time Collected: 03/11/15 12:50
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.061Benzo(b)fluoranthene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.058Benzo(g,h,i)perylene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.069Benzo(k)fluoranthene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.044Benzoic Acid
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.069Benzyl alcohol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.091bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.074Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.090Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.078Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.075Butyl benzyl phthalate
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.066Chrysene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.064Dibenzo(a,h)anthracene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.080Dibenzofuran
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.072Diethyl phthalate
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.069Dimethyl phthalate
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.075Di-n-butyl phthalate
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.065Di-n-octyl phthalate
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.067Fluoranthene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.075Fluorene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.083Hexachlorobenzene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.094Hexachlorobutadiene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.094Hexachlorocyclopentadiene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.088Hexachloroethane
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.060Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.071Isophorone
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.084Naphthalene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.075Nitrobenzene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.083N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.080N-Nitrosodiphenylamine
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.062Pentachlorophenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.068Phenanthrene
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.077Phenol
BRL 8270D P5C026410.52 3/17/15 17:35 KCmg/kg dry 0.069Pyrene
Surrogate Recovery Control Limits
39-13287 %2,4,6-Tribromophenol
44-11587 %2-Fluorobiphenyl
35-11585 %2-Fluorophenol
37-12287 %Nitrobenzene-d5
34-12185 %Phenol-d5
54-12797 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000561,1,1,2-Tetrachloroethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000331,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-N
Prism Sample ID: 5030255-06
Prism Work Order: 5030255
Time Collected: 03/11/15 12:50
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000461,1,2,2-Tetrachloroethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000601,1,2-Trichloroethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000871,2,3-Trichloropropane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000511,2,4-Trichlorobenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000521,2,4-Trimethylbenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000421,2-Dichloropropane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000521,3,5-Trimethylbenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000451,3-Dichlorobenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.000334-Isopropyltoluene
BRL 8260B P5C026210.068 3/16/15 22:56 MSCmg/kg dry 0.0017Acetone
BRL 8260B P5C026210.0041 3/16/15 22:56 MSCmg/kg dry 0.00040Benzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00057Bromobenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00037Bromochloromethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00038Bromodichloromethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00077Bromoform
BRL 8260B P5C026210.014 3/16/15 22:56 MSCmg/kg dry 0.00084Bromomethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00034Carbon Tetrachloride
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00036Chlorobenzene
BRL 8260B P5C026210.014 3/16/15 22:56 MSCmg/kg dry 0.00057Chloroethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00049Chloroform
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00046Chloromethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00026Ethylbenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00040Isopropylbenzene (Cumene)
BRL 8260B P5C026210.014 3/16/15 22:56 MSCmg/kg dry 0.00063m,p-Xylenes
BRL 8260B P5C026210.068 3/16/15 22:56 MSCmg/kg dry 0.00062Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C026210.14 3/16/15 22:56 MSCmg/kg dry 0.00062Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-N
Prism Sample ID: 5030255-06
Prism Work Order: 5030255
Time Collected: 03/11/15 12:50
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.068 3/16/15 22:56 MSCmg/kg dry 0.00058Methyl Isobutyl Ketone
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00038Methylene Chloride
BRL 8260B P5C026210.014 3/16/15 22:56 MSCmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P5C026210.014 3/16/15 22:56 MSCmg/kg dry 0.00022Naphthalene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00040n-Propylbenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00028o-Xylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00041Styrene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00039Toluene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00044Trichloroethylene
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00044Trichlorofluoromethane
BRL 8260B P5C026210.034 3/16/15 22:56 MSCmg/kg dry 0.00093Vinyl acetate
BRL 8260B P5C026210.0068 3/16/15 22:56 MSCmg/kg dry 0.00033Vinyl chloride
BRL 8260B P5C026210.020 3/16/15 22:56 MSCmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130108 %4-Bromofluorobenzene
84-12398 %Dibromofluoromethane
76-12999 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100233/18/15 22:01 ANGmg/kg dry 0.89C5-C8 Aliphatics
BRL MADEP VPH P5C0303100233/18/15 22:01 ANGmg/kg dry 2.1C9-C12 Aliphatics
BRL MADEP VPH P5C0303100233/18/15 22:01 ANGmg/kg dry 0.20C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130120 %2,5-Dibromotoluene (PID)
70-130113 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-S
Prism Sample ID: 5030255-07
Prism Work Order: 5030255
Time Collected: 03/11/15 12:58
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
1.0 MADEP EPH P5C02581143/17/15 23:49 KCJmg/kg dry 0.79C9-C18 Aliphatics
BRL MADEP EPH P5C02581143/17/15 23:49 KCmg/kg dry 3.2C19-C36 Aliphatics
BRL MADEP EPH P5C02581143/17/15 23:49 KCmg/kg dry 2.5C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14084 %1-Chlorooctadecane
40-14082 %o-Terphenyl
40-14084 %2-Fluorobiphenyl
40-14064 %2-Bromonaphthalene
General Chemistry Parameters
72.4 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0711,2,4-Trichlorobenzene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0691,2-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0641,3-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0671,4-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0881-Methylnaphthalene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0852,4,6-Trichlorophenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0882,4-Dichlorophenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0702,4-Dimethylphenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0642,4-Dinitrophenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0552,4-Dinitrotoluene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0612,6-Dinitrotoluene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0662-Chloronaphthalene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0652-Chlorophenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0732-Methylnaphthalene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0582-Methylphenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0832-Nitrophenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0903,3'-Dichlorobenzidine
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0563/4-Methylphenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0694,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0784-Bromophenyl phenyl ether
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0644-Chloro-3-methylphenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0554-Chloroaniline
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0594-Chlorophenyl phenyl ether
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.0704-Nitrophenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.062Acenaphthene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.066Acenaphthylene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.073Anthracene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.060Azobenzene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.060Benzo(a)anthracene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.049Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-S
Prism Sample ID: 5030255-07
Prism Work Order: 5030255
Time Collected: 03/11/15 12:58
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.053Benzo(b)fluoranthene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.050Benzo(g,h,i)perylene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.060Benzo(k)fluoranthene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.038Benzoic Acid
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.060Benzyl alcohol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.079bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.064Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.078Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.068Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.065Butyl benzyl phthalate
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.057Chrysene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.056Dibenzo(a,h)anthracene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.069Dibenzofuran
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.063Diethyl phthalate
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.060Dimethyl phthalate
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.065Di-n-butyl phthalate
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.056Di-n-octyl phthalate
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.058Fluoranthene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.065Fluorene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.072Hexachlorobenzene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.082Hexachlorobutadiene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.081Hexachlorocyclopentadiene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.076Hexachloroethane
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.052Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.062Isophorone
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.073Naphthalene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.065Nitrobenzene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.072N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.069N-Nitrosodiphenylamine
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.054Pentachlorophenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.059Phenanthrene
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.067Phenol
BRL 8270D P5C026410.46 3/17/15 17:56 KCmg/kg dry 0.060Pyrene
Surrogate Recovery Control Limits
39-13287 %2,4,6-Tribromophenol
44-11584 %2-Fluorobiphenyl
35-11587 %2-Fluorophenol
37-12289 %Nitrobenzene-d5
34-12185 %Phenol-d5
54-12797 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000491,1,1,2-Tetrachloroethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000291,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-S
Prism Sample ID: 5030255-07
Prism Work Order: 5030255
Time Collected: 03/11/15 12:58
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000401,1,2,2-Tetrachloroethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000521,1,2-Trichloroethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000261,1-Dichloroethylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000321,1-Dichloropropylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000341,2,3-Trichlorobenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000761,2,3-Trichloropropane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000441,2,4-Trichlorobenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000451,2,4-Trimethylbenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000281,2-Dichlorobenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000351,2-Dichloroethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000371,2-Dichloropropane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000451,3,5-Trimethylbenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000391,3-Dichlorobenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000301,3-Dichloropropane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000282,2-Dichloropropane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000312-Chlorotoluene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000354-Chlorotoluene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.000294-Isopropyltoluene
BRL 8260B P5C026210.059 3/16/15 23:28 MSCmg/kg dry 0.0014Acetone
BRL 8260B P5C026210.0036 3/16/15 23:28 MSCmg/kg dry 0.00034Benzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00049Bromobenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00033Bromochloromethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00033Bromodichloromethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00067Bromoform
BRL 8260B P5C026210.012 3/16/15 23:28 MSCmg/kg dry 0.00073Bromomethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00029Carbon Tetrachloride
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00031Chlorobenzene
BRL 8260B P5C026210.012 3/16/15 23:28 MSCmg/kg dry 0.00049Chloroethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00043Chloroform
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00040Chloromethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00025cis-1,2-Dichloroethylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00027Dichlorodifluoromethane
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00023Ethylbenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00024Isopropyl Ether
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00035Isopropylbenzene (Cumene)
BRL 8260B P5C026210.012 3/16/15 23:28 MSCmg/kg dry 0.00055m,p-Xylenes
BRL 8260B P5C026210.059 3/16/15 23:28 MSCmg/kg dry 0.00054Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C026210.12 3/16/15 23:28 MSCmg/kg dry 0.00054Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-S
Prism Sample ID: 5030255-07
Prism Work Order: 5030255
Time Collected: 03/11/15 12:58
Time Submitted: 03/13/15 13:45
BRL 8260B P5C026210.059 3/16/15 23:28 MSCmg/kg dry 0.00050Methyl Isobutyl Ketone
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00033Methylene Chloride
BRL 8260B P5C026210.012 3/16/15 23:28 MSCmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P5C026210.012 3/16/15 23:28 MSCmg/kg dry 0.00019Naphthalene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00030n-Butylbenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00035n-Propylbenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00024o-Xylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00036Styrene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00028Tetrachloroethylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00034Toluene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00035trans-1,2-Dichloroethylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00031trans-1,3-Dichloropropylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00038Trichloroethylene
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00038Trichlorofluoromethane
BRL 8260B P5C026210.030 3/16/15 23:28 MSCmg/kg dry 0.00081Vinyl acetate
BRL 8260B P5C026210.0059 3/16/15 23:28 MSCmg/kg dry 0.00029Vinyl chloride
BRL 8260B P5C026210.018 3/16/15 23:28 MSCmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130108 %4-Bromofluorobenzene
84-123101 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100203/18/15 22:34 ANGmg/kg dry 0.78C5-C8 Aliphatics
BRL MADEP VPH P5C0303100203/18/15 22:34 ANGmg/kg dry 1.9C9-C12 Aliphatics
BRL MADEP VPH P5C0303100203/18/15 22:34 ANGmg/kg dry 0.18C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130120 %2,5-Dibromotoluene (PID)
70-130114 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-E
Prism Sample ID: 5030255-08
Prism Work Order: 5030255
Time Collected: 03/11/15 13:06
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P5C02581143/18/15 8:58 KCmg/kg dry 0.79C9-C18 Aliphatics
BRL MADEP EPH P5C02581143/18/15 8:58 KCmg/kg dry 3.2C19-C36 Aliphatics
BRL MADEP EPH P5C02581143/18/15 8:58 KCmg/kg dry 2.5C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14075 %1-Chlorooctadecane
40-14080 %o-Terphenyl
40-14082 %2-Fluorobiphenyl
40-14068 %2-Bromonaphthalene
General Chemistry Parameters
72.2 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0711,2,4-Trichlorobenzene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0691,2-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0641,3-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0671,4-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0881-Methylnaphthalene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0862,4,6-Trichlorophenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0882,4-Dichlorophenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0702,4-Dimethylphenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0642,4-Dinitrophenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0552,4-Dinitrotoluene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0612,6-Dinitrotoluene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0662-Chloronaphthalene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0652-Chlorophenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0732-Methylnaphthalene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0582-Methylphenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0832-Nitrophenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0903,3'-Dichlorobenzidine
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0563/4-Methylphenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0694,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0784-Bromophenyl phenyl ether
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0644-Chloro-3-methylphenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0554-Chloroaniline
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0594-Chlorophenyl phenyl ether
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.0704-Nitrophenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.062Acenaphthene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.066Acenaphthylene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.074Anthracene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.060Azobenzene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.060Benzo(a)anthracene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.049Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-E
Prism Sample ID: 5030255-08
Prism Work Order: 5030255
Time Collected: 03/11/15 13:06
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.053Benzo(b)fluoranthene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.050Benzo(g,h,i)perylene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.060Benzo(k)fluoranthene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.038Benzoic Acid
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.060Benzyl alcohol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.079bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.064Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.078Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.068Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.065Butyl benzyl phthalate
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.057Chrysene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.056Dibenzo(a,h)anthracene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.069Dibenzofuran
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.063Diethyl phthalate
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.060Dimethyl phthalate
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.065Di-n-butyl phthalate
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.056Di-n-octyl phthalate
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.058Fluoranthene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.065Fluorene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.072Hexachlorobenzene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.082Hexachlorobutadiene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.081Hexachlorocyclopentadiene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.076Hexachloroethane
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.052Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.062Isophorone
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.073Naphthalene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.065Nitrobenzene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.072N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.069N-Nitrosodiphenylamine
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.054Pentachlorophenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.059Phenanthrene
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.067Phenol
BRL 8270D P5C026410.46 3/17/15 18:17 KCmg/kg dry 0.060Pyrene
Surrogate Recovery Control Limits
39-13278 %2,4,6-Tribromophenol
44-11575 %2-Fluorobiphenyl
35-11575 %2-Fluorophenol
37-12277 %Nitrobenzene-d5
34-12173 %Phenol-d5
54-12790 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000551,1,1,2-Tetrachloroethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000321,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-E
Prism Sample ID: 5030255-08
Prism Work Order: 5030255
Time Collected: 03/11/15 13:06
Time Submitted: 03/13/15 13:45
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000451,1,2,2-Tetrachloroethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000591,1,2-Trichloroethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000381,2,3-Trichlorobenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000851,2,3-Trichloropropane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000501,2,4-Trichlorobenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000511,2,4-Trimethylbenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000311,2-Dichlorobenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000401,2-Dichloroethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000411,2-Dichloropropane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000511,3,5-Trimethylbenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000441,3-Dichlorobenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000342-Chlorotoluene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000404-Chlorotoluene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.000324-Isopropyltoluene
BRL 8260B P5C028710.067 3/18/15 4:07 MSCmg/kg dry 0.0016Acetone
BRL 8260B P5C028710.0040 3/18/15 4:07 MSCmg/kg dry 0.00039Benzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00056Bromobenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00037Bromochloromethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00076Bromoform
BRL 8260B P5C028710.013 3/18/15 4:07 MSCmg/kg dry 0.00082Bromomethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00035Chlorobenzene
BRL 8260B P5C028710.013 3/18/15 4:07 MSCmg/kg dry 0.00056Chloroethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00048Chloroform
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00045Chloromethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00028cis-1,2-Dichloroethylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00030Dichlorodifluoromethane
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00026Ethylbenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00040Isopropylbenzene (Cumene)
BRL 8260B P5C028710.013 3/18/15 4:07 MSCmg/kg dry 0.00062m,p-Xylenes
BRL 8260B P5C028710.067 3/18/15 4:07 MSCmg/kg dry 0.00060Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C028710.13 3/18/15 4:07 MSCmg/kg dry 0.00060Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-E
Prism Sample ID: 5030255-08
Prism Work Order: 5030255
Time Collected: 03/11/15 13:06
Time Submitted: 03/13/15 13:45
BRL 8260B P5C028710.067 3/18/15 4:07 MSCmg/kg dry 0.00057Methyl Isobutyl Ketone
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00038Methylene Chloride
BRL 8260B P5C028710.013 3/18/15 4:07 MSCmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P5C028710.013 3/18/15 4:07 MSCmg/kg dry 0.00021Naphthalene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00034n-Butylbenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00040n-Propylbenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00027o-Xylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00032sec-Butylbenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00040Styrene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00038Toluene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00040trans-1,2-Dichloroethylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00035trans-1,3-Dichloropropylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00043Trichloroethylene
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P5C028710.033 3/18/15 4:07 MSCmg/kg dry 0.00092Vinyl acetate
BRL 8260B P5C028710.0067 3/18/15 4:07 MSCmg/kg dry 0.00032Vinyl chloride
BRL 8260B P5C028710.020 3/18/15 4:07 MSCmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130112 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-129100 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100193/18/15 23:06 ANGmg/kg dry 0.73C5-C8 Aliphatics
BRL MADEP VPH P5C0303100193/18/15 23:06 ANGmg/kg dry 1.7C9-C12 Aliphatics
BRL MADEP VPH P5C0303100193/18/15 23:06 ANGmg/kg dry 0.16C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130116 %2,5-Dibromotoluene (PID)
70-130110 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-W
Prism Sample ID: 5030255-09
Prism Work Order: 5030255
Time Collected: 03/11/15 13:12
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
6.2 MADEP EPH P5C02581133/18/15 9:34 KCJmg/kg dry 0.74C9-C18 Aliphatics
14 MADEP EPH P5C02581133/18/15 9:34 KCmg/kg dry 3.0C19-C36 Aliphatics
BRL MADEP EPH P5C02581133/18/15 9:34 KCmg/kg dry 2.3C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14071 %1-Chlorooctadecane
40-14079 %o-Terphenyl
40-14088 %2-Fluorobiphenyl
40-14074 %2-Bromonaphthalene
General Chemistry Parameters
77.1 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0601,3-Dichlorobenzene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0821-Methylnaphthalene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0802,4,6-Trichlorophenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0612-Chlorophenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0682-Methylnaphthalene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0552-Methylphenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0782-Nitrophenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0843,3'-Dichlorobenzidine
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0644,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0734-Bromophenyl phenyl ether
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0514-Chloroaniline
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.0664-Nitrophenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.058Acenaphthene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.062Acenaphthylene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.069Anthracene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.056Azobenzene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.046Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-W
Prism Sample ID: 5030255-09
Prism Work Order: 5030255
Time Collected: 03/11/15 13:12
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.056Benzo(k)fluoranthene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.036Benzoic Acid
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.056Benzyl alcohol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.074bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.060Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.073Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.054Chrysene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.065Dibenzofuran
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.059Diethyl phthalate
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.055Fluoranthene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.061Fluorene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.077Hexachlorobutadiene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.076Hexachlorocyclopentadiene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.072Hexachloroethane
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.058Isophorone
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.069Naphthalene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.061Nitrobenzene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.067N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.065N-Nitrosodiphenylamine
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.051Pentachlorophenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.056Phenanthrene
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.063Phenol
BRL 8270D P5C026410.43 3/17/15 18:38 KCmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13292 %2,4,6-Tribromophenol
44-11588 %2-Fluorobiphenyl
35-11583 %2-Fluorophenol
37-12289 %Nitrobenzene-d5
34-12182 %Phenol-d5
54-127101 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000471,1,1,2-Tetrachloroethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000271,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-W
Prism Sample ID: 5030255-09
Prism Work Order: 5030255
Time Collected: 03/11/15 13:12
Time Submitted: 03/13/15 13:45
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000381,1,2,2-Tetrachloroethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000501,1,2-Trichloroethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000721,2,3-Trichloropropane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000421,2,4-Trichlorobenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000431,2,4-Trimethylbenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000341,2-Dichloroethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000431,3,5-Trimethylbenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000371,3-Dichlorobenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000281,3-Dichloropropane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000344-Chlorotoluene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.000274-Isopropyltoluene
0.14 8260B P5C028710.057 3/18/15 4:38 MSCmg/kg dry 0.0014Acetone
BRL 8260B P5C028710.0034 3/18/15 4:38 MSCmg/kg dry 0.00033Benzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00047Bromobenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00031Bromochloromethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00032Bromodichloromethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00064Bromoform
BRL 8260B P5C028710.011 3/18/15 4:38 MSCmg/kg dry 0.00070Bromomethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00030Chlorobenzene
BRL 8260B P5C028710.011 3/18/15 4:38 MSCmg/kg dry 0.00047Chloroethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00041Chloroform
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00038Chloromethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00026Dichlorodifluoromethane
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00022Ethylbenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00034Isopropylbenzene (Cumene)
BRL 8260B P5C028710.011 3/18/15 4:38 MSCmg/kg dry 0.00052m,p-Xylenes
BRL 8260B P5C028710.057 3/18/15 4:38 MSCmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C028710.11 3/18/15 4:38 MSCmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-W
Prism Sample ID: 5030255-09
Prism Work Order: 5030255
Time Collected: 03/11/15 13:12
Time Submitted: 03/13/15 13:45
BRL 8260B P5C028710.057 3/18/15 4:38 MSCmg/kg dry 0.00048Methyl Isobutyl Ketone
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00032Methylene Chloride
BRL 8260B P5C028710.011 3/18/15 4:38 MSCmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P5C028710.011 3/18/15 4:38 MSCmg/kg dry 0.00018Naphthalene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00029n-Butylbenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00034n-Propylbenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00023o-Xylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00027sec-Butylbenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00034Styrene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00032Toluene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00037Trichloroethylene
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00037Trichlorofluoromethane
BRL 8260B P5C028710.028 3/18/15 4:38 MSCmg/kg dry 0.00078Vinyl acetate
BRL 8260B P5C028710.0057 3/18/15 4:38 MSCmg/kg dry 0.00027Vinyl chloride
BRL 8260B P5C028710.017 3/18/15 4:38 MSCmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130115 %4-Bromofluorobenzene
84-123101 %Dibromofluoromethane
76-12996 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100183/18/15 23:39 ANGmg/kg dry 0.69C5-C8 Aliphatics
BRL MADEP VPH P5C0303100183/18/15 23:39 ANGmg/kg dry 1.6C9-C12 Aliphatics
BRL MADEP VPH P5C0303100183/18/15 23:39 ANGmg/kg dry 0.15C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130122 %2,5-Dibromotoluene (PID)
70-130116 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-B1
Prism Sample ID: 5030255-10
Prism Work Order: 5030255
Time Collected: 03/11/15 13:19
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
540 MADEP EPH P5C02581133/18/15 10:11 KCmg/kg dry 0.73C9-C18 Aliphatics
320 MADEP EPH P5C02581133/18/15 10:11 KCmg/kg dry 3.0C19-C36 Aliphatics
430 MADEP EPH P5C02581133/18/15 10:11 KCmg/kg dry 2.3C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14062 %1-Chlorooctadecane
40-14073 %o-Terphenyl
40-140111 %2-Fluorobiphenyl
40-14078 %2-Bromonaphthalene
General Chemistry Parameters
78.5 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0661,2,4-Trichlorobenzene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0641,2-Dichlorobenzene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0591,3-Dichlorobenzene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0621,4-Dichlorobenzene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0811-Methylnaphthalene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0792,4,6-Trichlorophenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0812,4-Dichlorophenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0642,4-Dimethylphenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0592,4-Dinitrophenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0512,4-Dinitrotoluene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0602-Chlorophenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0672-Methylnaphthalene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0542-Methylphenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0772-Nitrophenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0833,3'-Dichlorobenzidine
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0634,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0724-Bromophenyl phenyl ether
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0514-Chloroaniline
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0554-Chlorophenyl phenyl ether
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.0654-Nitrophenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.057Acenaphthene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.061Acenaphthylene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.068Anthracene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.056Azobenzene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.045Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-B1
Prism Sample ID: 5030255-10
Prism Work Order: 5030255
Time Collected: 03/11/15 13:19
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.055Benzo(k)fluoranthene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.035Benzoic Acid
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.055Benzyl alcohol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.073bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.059Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.072Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.062Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.053Chrysene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.051Dibenzo(a,h)anthracene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.064Dibenzofuran
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.058Diethyl phthalate
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.060Di-n-butyl phthalate
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.052Di-n-octyl phthalate
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.054Fluoranthene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.060Fluorene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.067Hexachlorobenzene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.076Hexachlorobutadiene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.075Hexachlorocyclopentadiene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.070Hexachloroethane
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.048Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.057Isophorone
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.068Naphthalene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.060Nitrobenzene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.066N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.050Pentachlorophenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.055Phenanthrene
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.062Phenol
BRL 8270D P5C026410.42 3/17/15 18:59 KCmg/kg dry 0.056Pyrene
Surrogate Recovery Control Limits
39-13295 %2,4,6-Tribromophenol
44-11588 %2-Fluorobiphenyl
35-11586 %2-Fluorophenol
37-12289 %Nitrobenzene-d5
34-12184 %Phenol-d5
54-127106 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000451,1,1,2-Tetrachloroethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000271,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-B1
Prism Sample ID: 5030255-10
Prism Work Order: 5030255
Time Collected: 03/11/15 13:19
Time Submitted: 03/13/15 13:45
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000371,1,2,2-Tetrachloroethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000491,1,2-Trichloroethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000151,1-Dichloroethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000241,1-Dichloroethylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000301,1-Dichloropropylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000311,2,3-Trichlorobenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000701,2,3-Trichloropropane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000411,2,4-Trichlorobenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000421,2,4-Trimethylbenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000221,2-Dibromoethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000261,2-Dichlorobenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000331,2-Dichloroethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000341,2-Dichloropropane
0.014 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000421,3,5-Trimethylbenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000371,3-Dichlorobenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000281,3-Dichloropropane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000262,2-Dichloropropane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000282-Chlorotoluene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000334-Chlorotoluene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.000274-Isopropyltoluene
0.090 8260B P5C030010.055 3/18/15 15:27 MSCmg/kg dry 0.0013Acetone
BRL 8260B P5C030010.0033 3/18/15 15:27 MSCmg/kg dry 0.00032Benzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00046Bromobenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00030Bromochloromethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00031Bromodichloromethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00063Bromoform
BRL 8260B P5C030010.011 3/18/15 15:27 MSCmg/kg dry 0.00068Bromomethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00027Carbon Tetrachloride
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00029Chlorobenzene
BRL 8260B P5C030010.011 3/18/15 15:27 MSCmg/kg dry 0.00046Chloroethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00040Chloroform
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00037Chloromethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00025Dichlorodifluoromethane
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00021Ethylbenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00033Isopropylbenzene (Cumene)
BRL 8260B P5C030010.011 3/18/15 15:27 MSCmg/kg dry 0.00051m,p-Xylenes
BRL 8260B P5C030010.055 3/18/15 15:27 MSCmg/kg dry 0.00050Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C030010.11 3/18/15 15:27 MSCmg/kg dry 0.00050Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-B1
Prism Sample ID: 5030255-10
Prism Work Order: 5030255
Time Collected: 03/11/15 13:19
Time Submitted: 03/13/15 13:45
BRL 8260B P5C030010.055 3/18/15 15:27 MSCmg/kg dry 0.00047Methyl Isobutyl Ketone
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00031Methylene Chloride
BRL 8260B P5C030010.011 3/18/15 15:27 MSCmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P5C030010.011 3/18/15 15:27 MSCmg/kg dry 0.00017Naphthalene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00028n-Butylbenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00033n-Propylbenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00023o-Xylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00027sec-Butylbenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00033Styrene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00026Tetrachloroethylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00032Toluene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00033trans-1,2-Dichloroethylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00029trans-1,3-Dichloropropylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00036Trichloroethylene
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00036Trichlorofluoromethane
BRL 8260B P5C030010.028 3/18/15 15:27 MSCmg/kg dry 0.00076Vinyl acetate
BRL 8260B P5C030010.0055 3/18/15 15:27 MSCmg/kg dry 0.00027Vinyl chloride
BRL 8260B P5C030010.017 3/18/15 15:27 MSCmg/kg dry 0.0010Xylenes, total
Surrogate Recovery Control Limits
70-130120 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-129100 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100183/19/15 0:11 ANGmg/kg dry 0.71C5-C8 Aliphatics
BRL MADEP VPH P5C0303100183/19/15 0:11 ANGmg/kg dry 1.7C9-C12 Aliphatics
9.3 MADEP VPH P5C0303100183/19/15 0:11 ANGJmg/kg dry 0.16C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130129 %2,5-Dibromotoluene (PID)
70-130114 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-B2
Prism Sample ID: 5030255-11
Prism Work Order: 5030255
Time Collected: 03/11/15 13:27
Time Submitted: 03/13/15 13:45
Extractable Petroleum Hydrocarbons by GC/FID
7.1 MADEP EPH P5C02581143/18/15 10:47 KCJmg/kg dry 0.79C9-C18 Aliphatics
5.4 MADEP EPH P5C02581143/18/15 10:47 KCJmg/kg dry 3.2C19-C36 Aliphatics
BRL MADEP EPH P5C02581143/18/15 10:47 KCmg/kg dry 2.5C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14096 %1-Chlorooctadecane
40-14081 %o-Terphenyl
40-14083 %2-Fluorobiphenyl
40-14073 %2-Bromonaphthalene
General Chemistry Parameters
72.2 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0711,2,4-Trichlorobenzene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0691,2-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0641,3-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0671,4-Dichlorobenzene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0881-Methylnaphthalene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0862,4,6-Trichlorophenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0882,4-Dichlorophenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0702,4-Dimethylphenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0642,4-Dinitrophenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0552,4-Dinitrotoluene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0612,6-Dinitrotoluene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0662-Chloronaphthalene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0652-Chlorophenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0732-Methylnaphthalene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0582-Methylphenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0832-Nitrophenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0903,3'-Dichlorobenzidine
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0563/4-Methylphenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0694,6-Dinitro-2-methylphenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0784-Bromophenyl phenyl ether
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0644-Chloro-3-methylphenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0554-Chloroaniline
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0594-Chlorophenyl phenyl ether
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.0704-Nitrophenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.062Acenaphthene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.066Acenaphthylene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.074Anthracene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.060Azobenzene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.060Benzo(a)anthracene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.049Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-B2
Prism Sample ID: 5030255-11
Prism Work Order: 5030255
Time Collected: 03/11/15 13:27
Time Submitted: 03/13/15 13:45
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.053Benzo(b)fluoranthene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.050Benzo(g,h,i)perylene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.060Benzo(k)fluoranthene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.038Benzoic Acid
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.060Benzyl alcohol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.079bis(2-Chloroethoxy)methane
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.064Bis(2-Chloroethyl)ether
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.078Bis(2-chloroisopropyl)ether
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.068Bis(2-Ethylhexyl)phthalate
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.065Butyl benzyl phthalate
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.058Chrysene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.056Dibenzo(a,h)anthracene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.069Dibenzofuran
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.063Diethyl phthalate
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.060Dimethyl phthalate
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.065Di-n-butyl phthalate
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.056Di-n-octyl phthalate
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.058Fluoranthene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.066Fluorene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.072Hexachlorobenzene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.082Hexachlorobutadiene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.081Hexachlorocyclopentadiene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.076Hexachloroethane
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.052Indeno(1,2,3-cd)pyrene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.062Isophorone
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.073Naphthalene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.065Nitrobenzene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.072N-Nitroso-di-n-propylamine
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.069N-Nitrosodiphenylamine
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.054Pentachlorophenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.059Phenanthrene
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.067Phenol
BRL 8270D P5C026410.46 3/17/15 19:20 KCmg/kg dry 0.060Pyrene
Surrogate Recovery Control Limits
39-13272 %2,4,6-Tribromophenol
44-11571 %2-Fluorobiphenyl
35-11568 %2-Fluorophenol
37-12272 %Nitrobenzene-d5
34-12168 %Phenol-d5
54-12782 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000441,1,1,2-Tetrachloroethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000261,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-B2
Prism Sample ID: 5030255-11
Prism Work Order: 5030255
Time Collected: 03/11/15 13:27
Time Submitted: 03/13/15 13:45
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000361,1,2,2-Tetrachloroethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000471,1,2-Trichloroethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000151,1-Dichloroethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000241,1-Dichloroethylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000291,1-Dichloropropylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000301,2,3-Trichlorobenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000681,2,3-Trichloropropane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000401,2,4-Trichlorobenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000411,2,4-Trimethylbenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000221,2-Dibromoethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000251,2-Dichlorobenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000321,2-Dichloroethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000331,2-Dichloropropane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000401,3,5-Trimethylbenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000351,3-Dichlorobenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000271,3-Dichloropropane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000211,4-Dichlorobenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000252,2-Dichloropropane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000282-Chlorotoluene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000324-Chlorotoluene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.000264-Isopropyltoluene
0.076 8260B P5C028710.054 3/18/15 5:42 MSCmg/kg dry 0.0013Acetone
BRL 8260B P5C028710.0032 3/18/15 5:42 MSCmg/kg dry 0.00031Benzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00045Bromobenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00029Bromochloromethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00030Bromodichloromethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00061Bromoform
BRL 8260B P5C028710.011 3/18/15 5:42 MSCmg/kg dry 0.00066Bromomethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00027Carbon Tetrachloride
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00028Chlorobenzene
BRL 8260B P5C028710.011 3/18/15 5:42 MSCmg/kg dry 0.00045Chloroethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00039Chloroform
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00036Chloromethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00023cis-1,2-Dichloroethylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00018cis-1,3-Dichloropropylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00022Dibromochloromethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00024Dichlorodifluoromethane
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00021Ethylbenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00022Isopropyl Ether
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00032Isopropylbenzene (Cumene)
BRL 8260B P5C028710.011 3/18/15 5:42 MSCmg/kg dry 0.00049m,p-Xylenes
BRL 8260B P5C028710.054 3/18/15 5:42 MSCmg/kg dry 0.00048Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P5C028710.11 3/18/15 5:42 MSCmg/kg dry 0.00048Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: TP-2-B2
Prism Sample ID: 5030255-11
Prism Work Order: 5030255
Time Collected: 03/11/15 13:27
Time Submitted: 03/13/15 13:45
BRL 8260B P5C028710.054 3/18/15 5:42 MSCmg/kg dry 0.00046Methyl Isobutyl Ketone
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00030Methylene Chloride
BRL 8260B P5C028710.011 3/18/15 5:42 MSCmg/kg dry 0.00017Methyl-tert-Butyl Ether
BRL 8260B P5C028710.011 3/18/15 5:42 MSCmg/kg dry 0.00017Naphthalene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00027n-Butylbenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00032n-Propylbenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00022o-Xylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00026sec-Butylbenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00032Styrene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00018tert-Butylbenzene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00025Tetrachloroethylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00031Toluene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00032trans-1,2-Dichloroethylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00028trans-1,3-Dichloropropylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00035Trichloroethylene
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00035Trichlorofluoromethane
BRL 8260B P5C028710.027 3/18/15 5:42 MSCmg/kg dry 0.00073Vinyl acetate
BRL 8260B P5C028710.0054 3/18/15 5:42 MSCmg/kg dry 0.00026Vinyl chloride
BRL 8260B P5C028710.016 3/18/15 5:42 MSCmg/kg dry 0.0010Xylenes, total
Surrogate Recovery Control Limits
70-130119 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12999 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P5C0303100173/19/15 1:49 ANGmg/kg dry 0.67C5-C8 Aliphatics
BRL MADEP VPH P5C0303100173/19/15 1:49 ANGmg/kg dry 1.6C9-C12 Aliphatics
BRL MADEP VPH P5C0303100173/19/15 1:49 ANGmg/kg dry 0.15C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130109 %2,5-Dibromotoluene (PID)
70-130104 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: SPC-1
Prism Sample ID: 5030255-12
Prism Work Order: 5030255
Time Collected: 03/11/15 14:08
Time Submitted: 03/13/15 13:45
Diesel Range Organics by GC/FID
36 *8015C P5C02821103/19/15 2:59 JMVmg/kg dry 1.4Diesel Range Organics
Surrogate Recovery Control Limits
49-12482 %o-Terphenyl
Gasoline Range Organics by GC/FID
BRL *8015C P5C0284506.5 3/17/15 19:17 ANGmg/kg dry 1.4Gasoline Range Organics
Surrogate Recovery Control Limits
50-137110 %a,a,a-Trifluorotoluene
General Chemistry Parameters
70.2 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: SPC-2
Prism Sample ID: 5030255-13
Prism Work Order: 5030255
Time Collected: 03/11/15 14:13
Time Submitted: 03/13/15 13:45
Diesel Range Organics by GC/FID
33 *8015C P5C028219.7 3/19/15 3:36 JMVmg/kg dry 1.4Diesel Range Organics
Surrogate Recovery Control Limits
49-12474 %o-Terphenyl
Gasoline Range Organics by GC/FID
BRL *8015C P5C0284504.8 3/17/15 19:45 ANGmg/kg dry 1.0Gasoline Range Organics
Surrogate Recovery Control Limits
50-13774 %a,a,a-Trifluorotoluene
General Chemistry Parameters
72.5 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 82
Laboratory Report
03/20/2015
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Sample Matrix: Solid
Client Sample ID: SPC-3
Prism Sample ID: 5030255-14
Prism Work Order: 5030255
Time Collected: 03/11/15 14:20
Time Submitted: 03/13/15 13:45
Diesel Range Organics by GC/FID
70 *8015C P5C02821103/19/15 4:12 JMVmg/kg dry 1.4Diesel Range Organics
Surrogate Recovery Control Limits
49-12482 %o-Terphenyl
Gasoline Range Organics by GC/FID
BRL *8015C P5C0284505.8 3/17/15 20:13 ANGmg/kg dry 1.2Gasoline Range Organics
Surrogate Recovery Control Limits
50-137117 %a,a,a-Trifluorotoluene
General Chemistry Parameters
70.2 *SM2540 G P5C028910.100 3/17/15 17:10 MJO% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0262 - 5035
Blank (P5C0262-BLK1)Prepared & Analyzed: 03/16/15
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0262 - 5035
Blank (P5C0262-BLK1)Prepared & Analyzed: 03/16/15
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1080.0540
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 970.0485
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1000.0500
LCS (P5C0262-BS1)Prepared & Analyzed: 03/16/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0494 0.0050 0.05000 72-11599
1,1,1-Trichloroethane mg/kg wet0.0546 0.0050 0.05000 67-131109
1,1,2,2-Tetrachloroethane mg/kg wet0.0446 0.0050 0.05000 56-12689
1,1,2-Trichloroethane mg/kg wet0.0466 0.0050 0.05000 70-13393
1,1-Dichloroethane mg/kg wet0.0539 0.0050 0.05000 74-127108
1,1-Dichloroethylene mg/kg wet0.0593 0.0050 0.05000 67-149119
1,1-Dichloropropylene mg/kg wet0.0599 0.0050 0.05000 71-130120
1,2,3-Trichlorobenzene mg/kg wet0.0483 0.0050 0.05000 68-13097
1,2,3-Trichloropropane mg/kg wet0.0464 0.0050 0.05000 60-13793
1,2,4-Trichlorobenzene mg/kg wet0.0485 0.0050 0.05000 66-12597
1,2,4-Trimethylbenzene mg/kg wet0.0519 0.0050 0.05000 69-129104
1,2-Dibromoethane mg/kg wet0.0466 0.0050 0.05000 70-13293
1,2-Dichlorobenzene mg/kg wet0.0479 0.0050 0.05000 72-12396
1,2-Dichloroethane mg/kg wet0.0477 0.0050 0.05000 68-12895
1,2-Dichloropropane mg/kg wet0.0508 0.0050 0.05000 73-130102
1,3,5-Trimethylbenzene mg/kg wet0.0514 0.0050 0.05000 69-128103
1,3-Dichlorobenzene mg/kg wet0.0510 0.0050 0.05000 71-120102
1,3-Dichloropropane mg/kg wet0.0510 0.0050 0.05000 75-124102
1,4-Dichlorobenzene mg/kg wet0.0513 0.0050 0.05000 71-123103
2,2-Dichloropropane mg/kg wet0.0528 0.0050 0.05000 50-142106
2-Chlorotoluene mg/kg wet0.0508 0.0050 0.05000 67-124102
4-Chlorotoluene mg/kg wet0.0502 0.0050 0.05000 71-126100
4-Isopropyltoluene mg/kg wet0.0514 0.0050 0.05000 68-129103
Acetone mg/kg wet0.102 0.050 0.1000 29-198102
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0262 - 5035
LCS (P5C0262-BS1)Prepared & Analyzed: 03/16/15
Benzene mg/kg wet0.0558 0.0030 0.05000 74-127112
Bromobenzene mg/kg wet0.0490 0.0050 0.05000 73-12598
Bromochloromethane mg/kg wet0.0516 0.0050 0.05000 72-134103
Bromodichloromethane mg/kg wet0.0454 0.0050 0.05000 75-12291
Bromoform mg/kg wet0.0438 0.0050 0.05000 66-13588
Bromomethane mg/kg wet0.0521 0.010 0.05000 20-180104
Carbon Tetrachloride mg/kg wet0.0567 0.0050 0.05000 64-143113
Chlorobenzene mg/kg wet0.0519 0.0050 0.05000 74-118104
Chloroethane mg/kg wet0.0664 0.010 0.05000 33-149133
Chloroform mg/kg wet0.0477 0.0050 0.05000 73-12795
Chloromethane mg/kg wet0.0528 0.0050 0.05000 45-143106
cis-1,2-Dichloroethylene mg/kg wet0.0549 0.0050 0.05000 76-134110
cis-1,3-Dichloropropylene mg/kg wet0.0507 0.0050 0.05000 71-125101
Dibromochloromethane mg/kg wet0.0443 0.0050 0.05000 73-12289
Dichlorodifluoromethane mg/kg wet0.0514 0.0050 0.05000 26-146103
Ethylbenzene mg/kg wet0.0535 0.0050 0.05000 74-128107
Isopropyl Ether mg/kg wet0.0468 0.0050 0.05000 59-15994
Isopropylbenzene (Cumene)mg/kg wet0.0538 0.0050 0.05000 68-126108
m,p-Xylenes mg/kg wet0.107 0.010 0.1000 75-124107
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0508 0.050 0.05000 61-157102
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0501 0.10 0.05000 J63-149100
Methyl Isobutyl Ketone mg/kg wet0.0490 0.050 0.05000 J57-16298
Methylene Chloride mg/kg wet0.0490 0.0050 0.05000 74-12998
Methyl-tert-Butyl Ether mg/kg wet0.0518 0.010 0.05000 70-130104
Naphthalene mg/kg wet0.0474 0.010 0.05000 57-15795
n-Butylbenzene mg/kg wet0.0545 0.0050 0.05000 65-135109
n-Propylbenzene mg/kg wet0.0527 0.0050 0.05000 67-130105
o-Xylene mg/kg wet0.0521 0.0050 0.05000 74-126104
sec-Butylbenzene mg/kg wet0.0518 0.0050 0.05000 66-131104
Styrene mg/kg wet0.0516 0.0050 0.05000 77-121103
tert-Butylbenzene mg/kg wet0.0522 0.0050 0.05000 67-132104
Tetrachloroethylene mg/kg wet0.0570 0.0050 0.05000 68-130114
Toluene mg/kg wet0.0558 0.0050 0.05000 71-129112
trans-1,2-Dichloroethylene mg/kg wet0.0578 0.0050 0.05000 73-132116
trans-1,3-Dichloropropylene mg/kg wet0.0498 0.0050 0.05000 68-123100
Trichloroethylene mg/kg wet0.0564 0.0050 0.05000 75-133113
Trichlorofluoromethane mg/kg wet0.0585 0.0050 0.05000 44-146117
Vinyl acetate mg/kg wet0.0524 0.025 0.05000 85-161105
Vinyl chloride mg/kg wet0.0575 0.0050 0.05000 48-147115
Xylenes, total mg/kg wet0.159 0.015 0.1500 74-126106
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1000.0498
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 970.0487
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 990.0494
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0262 - 5035
LCS Dup (P5C0262-BSD1)Prepared & Analyzed: 03/16/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0502 0.0050 0.05000 2072-115100 2
1,1,1-Trichloroethane mg/kg wet0.0557 0.0050 0.05000 2067-131111 2
1,1,2,2-Tetrachloroethane mg/kg wet0.0474 0.0050 0.05000 2056-12695 6
1,1,2-Trichloroethane mg/kg wet0.0498 0.0050 0.05000 2070-133100 7
1,1-Dichloroethane mg/kg wet0.0556 0.0050 0.05000 2074-127111 3
1,1-Dichloroethylene mg/kg wet0.0600 0.0050 0.05000 2067-149120 1
1,1-Dichloropropylene mg/kg wet0.0602 0.0050 0.05000 2071-130120 0.6
1,2,3-Trichlorobenzene mg/kg wet0.0493 0.0050 0.05000 2068-13099 2
1,2,3-Trichloropropane mg/kg wet0.0466 0.0050 0.05000 2060-13793 0.3
1,2,4-Trichlorobenzene mg/kg wet0.0491 0.0050 0.05000 2066-12598 1
1,2,4-Trimethylbenzene mg/kg wet0.0535 0.0050 0.05000 2069-129107 3
1,2-Dibromoethane mg/kg wet0.0498 0.0050 0.05000 2070-132100 6
1,2-Dichlorobenzene mg/kg wet0.0491 0.0050 0.05000 2072-12398 2
1,2-Dichloroethane mg/kg wet0.0495 0.0050 0.05000 2068-12899 4
1,2-Dichloropropane mg/kg wet0.0517 0.0050 0.05000 2073-130103 2
1,3,5-Trimethylbenzene mg/kg wet0.0515 0.0050 0.05000 2069-128103 0.2
1,3-Dichlorobenzene mg/kg wet0.0530 0.0050 0.05000 2071-120106 4
1,3-Dichloropropane mg/kg wet0.0521 0.0050 0.05000 2075-124104 2
1,4-Dichlorobenzene mg/kg wet0.0500 0.0050 0.05000 2071-123100 3
2,2-Dichloropropane mg/kg wet0.0500 0.0050 0.05000 2050-142100 6
2-Chlorotoluene mg/kg wet0.0510 0.0050 0.05000 2067-124102 0.4
4-Chlorotoluene mg/kg wet0.0542 0.0050 0.05000 2071-126108 8
4-Isopropyltoluene mg/kg wet0.0543 0.0050 0.05000 2068-129109 6
Acetone mg/kg wet0.107 0.050 0.1000 2029-198107 5
Benzene mg/kg wet0.0590 0.0030 0.05000 2074-127118 6
Bromobenzene mg/kg wet0.0490 0.0050 0.05000 2073-12598 0.02
Bromochloromethane mg/kg wet0.0540 0.0050 0.05000 2072-134108 5
Bromodichloromethane mg/kg wet0.0484 0.0050 0.05000 2075-12297 6
Bromoform mg/kg wet0.0456 0.0050 0.05000 2066-13591 4
Bromomethane mg/kg wet0.0551 0.010 0.05000 2020-180110 6
Carbon Tetrachloride mg/kg wet0.0567 0.0050 0.05000 2064-143113 0.02
Chlorobenzene mg/kg wet0.0522 0.0050 0.05000 2074-118104 0.5
Chloroethane mg/kg wet0.0663 0.010 0.05000 2033-149133 0.2
Chloroform mg/kg wet0.0493 0.0050 0.05000 2073-12799 3
Chloromethane mg/kg wet0.0585 0.0050 0.05000 2045-143117 10
cis-1,2-Dichloroethylene mg/kg wet0.0564 0.0050 0.05000 2076-134113 3
cis-1,3-Dichloropropylene mg/kg wet0.0505 0.0050 0.05000 2071-125101 0.3
Dibromochloromethane mg/kg wet0.0455 0.0050 0.05000 2073-12291 3
Dichlorodifluoromethane mg/kg wet0.0513 0.0050 0.05000 2026-146103 0.1
Ethylbenzene mg/kg wet0.0530 0.0050 0.05000 2074-128106 1
Isopropyl Ether mg/kg wet0.0475 0.0050 0.05000 2059-15995 2
Isopropylbenzene (Cumene)mg/kg wet0.0550 0.0050 0.05000 2068-126110 2
m,p-Xylenes mg/kg wet0.108 0.010 0.1000 2075-124108 0.9
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0543 0.050 0.05000 2061-157109 7
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0503 0.10 0.05000 20 J63-149101 0.5
Methyl Isobutyl Ketone mg/kg wet0.0529 0.050 0.05000 2057-162106 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0262 - 5035
LCS Dup (P5C0262-BSD1)Prepared & Analyzed: 03/16/15
Methylene Chloride mg/kg wet0.0516 0.0050 0.05000 2074-129103 5
Methyl-tert-Butyl Ether mg/kg wet0.0522 0.010 0.05000 2070-130104 0.7
Naphthalene mg/kg wet0.0490 0.010 0.05000 2057-15798 3
n-Butylbenzene mg/kg wet0.0540 0.0050 0.05000 2065-135108 0.9
n-Propylbenzene mg/kg wet0.0516 0.0050 0.05000 2067-130103 2
o-Xylene mg/kg wet0.0533 0.0050 0.05000 2074-126107 2
sec-Butylbenzene mg/kg wet0.0550 0.0050 0.05000 2066-131110 6
Styrene mg/kg wet0.0532 0.0050 0.05000 2077-121106 3
tert-Butylbenzene mg/kg wet0.0537 0.0050 0.05000 2067-132107 3
Tetrachloroethylene mg/kg wet0.0575 0.0050 0.05000 2068-130115 0.9
Toluene mg/kg wet0.0581 0.0050 0.05000 2071-129116 4
trans-1,2-Dichloroethylene mg/kg wet0.0586 0.0050 0.05000 2073-132117 1
trans-1,3-Dichloropropylene mg/kg wet0.0522 0.0050 0.05000 2068-123104 5
Trichloroethylene mg/kg wet0.0566 0.0050 0.05000 2075-133113 0.3
Trichlorofluoromethane mg/kg wet0.0596 0.0050 0.05000 2044-146119 2
Vinyl acetate mg/kg wet0.0550 0.025 0.05000 2085-161110 5
Vinyl chloride mg/kg wet0.0632 0.0050 0.05000 2048-147126 9
Xylenes, total mg/kg wet0.161 0.015 0.1500 2074-126107 1
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1020.0510
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1000.0500
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1010.0504
Batch P5C0287 - 5035
Blank (P5C0287-BLK1)Prepared: 03/17/15 Analyzed: 03/18/15
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0287 - 5035
Blank (P5C0287-BLK1)Prepared: 03/17/15 Analyzed: 03/18/15
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1080.0541
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1010.0507
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1000.0498
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 56 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0287 - 5035
LCS (P5C0287-BS1)Prepared & Analyzed: 03/17/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0470 0.0050 0.05000 72-11594
1,1,1-Trichloroethane mg/kg wet0.0515 0.0050 0.05000 67-131103
1,1,2,2-Tetrachloroethane mg/kg wet0.0447 0.0050 0.05000 56-12689
1,1,2-Trichloroethane mg/kg wet0.0462 0.0050 0.05000 70-13392
1,1-Dichloroethane mg/kg wet0.0501 0.0050 0.05000 74-127100
1,1-Dichloroethylene mg/kg wet0.0569 0.0050 0.05000 67-149114
1,1-Dichloropropylene mg/kg wet0.0540 0.0050 0.05000 71-130108
1,2,3-Trichlorobenzene mg/kg wet0.0452 0.0050 0.05000 68-13090
1,2,3-Trichloropropane mg/kg wet0.0416 0.0050 0.05000 60-13783
1,2,4-Trichlorobenzene mg/kg wet0.0462 0.0050 0.05000 66-12592
1,2,4-Trimethylbenzene mg/kg wet0.0514 0.0050 0.05000 69-129103
1,2-Dibromoethane mg/kg wet0.0485 0.0050 0.05000 70-13297
1,2-Dichlorobenzene mg/kg wet0.0461 0.0050 0.05000 72-12392
1,2-Dichloroethane mg/kg wet0.0463 0.0050 0.05000 68-12893
1,2-Dichloropropane mg/kg wet0.0508 0.0050 0.05000 73-130102
1,3,5-Trimethylbenzene mg/kg wet0.0510 0.0050 0.05000 69-128102
1,3-Dichlorobenzene mg/kg wet0.0495 0.0050 0.05000 71-12099
1,3-Dichloropropane mg/kg wet0.0472 0.0050 0.05000 75-12494
1,4-Dichlorobenzene mg/kg wet0.0473 0.0050 0.05000 71-12395
2,2-Dichloropropane mg/kg wet0.0491 0.0050 0.05000 50-14298
2-Chlorotoluene mg/kg wet0.0498 0.0050 0.05000 67-124100
4-Chlorotoluene mg/kg wet0.0470 0.0050 0.05000 71-12694
4-Isopropyltoluene mg/kg wet0.0511 0.0050 0.05000 68-129102
Acetone mg/kg wet0.0893 0.050 0.1000 29-19889
Benzene mg/kg wet0.0525 0.0030 0.05000 74-127105
Bromobenzene mg/kg wet0.0470 0.0050 0.05000 73-12594
Bromochloromethane mg/kg wet0.0516 0.0050 0.05000 72-134103
Bromodichloromethane mg/kg wet0.0462 0.0050 0.05000 75-12292
Bromoform mg/kg wet0.0430 0.0050 0.05000 66-13586
Bromomethane mg/kg wet0.0568 0.010 0.05000 20-180114
Carbon Tetrachloride mg/kg wet0.0530 0.0050 0.05000 64-143106
Chlorobenzene mg/kg wet0.0505 0.0050 0.05000 74-118101
Chloroethane mg/kg wet0.0588 0.010 0.05000 33-149118
Chloroform mg/kg wet0.0474 0.0050 0.05000 73-12795
Chloromethane mg/kg wet0.0559 0.0050 0.05000 45-143112
cis-1,2-Dichloroethylene mg/kg wet0.0527 0.0050 0.05000 76-134105
cis-1,3-Dichloropropylene mg/kg wet0.0500 0.0050 0.05000 71-125100
Dibromochloromethane mg/kg wet0.0419 0.0050 0.05000 73-12284
Dichlorodifluoromethane mg/kg wet0.0560 0.0050 0.05000 26-146112
Ethylbenzene mg/kg wet0.0507 0.0050 0.05000 74-128101
Isopropyl Ether mg/kg wet0.0486 0.0050 0.05000 59-15997
Isopropylbenzene (Cumene)mg/kg wet0.0566 0.0050 0.05000 68-126113
m,p-Xylenes mg/kg wet0.101 0.010 0.1000 75-124101
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0440 0.050 0.05000 J61-15788
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0478 0.10 0.05000 J63-14996
Methyl Isobutyl Ketone mg/kg wet0.0434 0.050 0.05000 J57-16287
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 57 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0287 - 5035
LCS (P5C0287-BS1)Prepared & Analyzed: 03/17/15
Methylene Chloride mg/kg wet0.0520 0.0050 0.05000 74-129104
Methyl-tert-Butyl Ether mg/kg wet0.0500 0.010 0.05000 70-130100
Naphthalene mg/kg wet0.0404 0.010 0.05000 57-15781
n-Butylbenzene mg/kg wet0.0498 0.0050 0.05000 65-135100
n-Propylbenzene mg/kg wet0.0503 0.0050 0.05000 67-130101
o-Xylene mg/kg wet0.0490 0.0050 0.05000 74-12698
sec-Butylbenzene mg/kg wet0.0557 0.0050 0.05000 66-131111
Styrene mg/kg wet0.0494 0.0050 0.05000 77-12199
tert-Butylbenzene mg/kg wet0.0516 0.0050 0.05000 67-132103
Tetrachloroethylene mg/kg wet0.0514 0.0050 0.05000 68-130103
Toluene mg/kg wet0.0513 0.0050 0.05000 71-129103
trans-1,2-Dichloroethylene mg/kg wet0.0533 0.0050 0.05000 73-132107
trans-1,3-Dichloropropylene mg/kg wet0.0492 0.0050 0.05000 68-12398
Trichloroethylene mg/kg wet0.0522 0.0050 0.05000 75-133104
Trichlorofluoromethane mg/kg wet0.0550 0.0050 0.05000 44-146110
Vinyl acetate mg/kg wet0.0516 0.025 0.05000 85-161103
Vinyl chloride mg/kg wet0.0534 0.0050 0.05000 48-147107
Xylenes, total mg/kg wet0.150 0.015 0.1500 74-126100
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 990.0495
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1000.0502
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 980.0492
LCS Dup (P5C0287-BSD1)Prepared: 03/17/15 Analyzed: 03/18/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0479 0.0050 0.05000 2072-11596 2
1,1,1-Trichloroethane mg/kg wet0.0491 0.0050 0.05000 2067-13198 5
1,1,2,2-Tetrachloroethane mg/kg wet0.0487 0.0050 0.05000 2056-12697 9
1,1,2-Trichloroethane mg/kg wet0.0463 0.0050 0.05000 2070-13393 0.2
1,1-Dichloroethane mg/kg wet0.0500 0.0050 0.05000 2074-127100 0.1
1,1-Dichloroethylene mg/kg wet0.0523 0.0050 0.05000 2067-149105 9
1,1-Dichloropropylene mg/kg wet0.0538 0.0050 0.05000 2071-130108 0.4
1,2,3-Trichlorobenzene mg/kg wet0.0478 0.0050 0.05000 2068-13096 6
1,2,3-Trichloropropane mg/kg wet0.0443 0.0050 0.05000 2060-13789 6
1,2,4-Trichlorobenzene mg/kg wet0.0488 0.0050 0.05000 2066-12598 6
1,2,4-Trimethylbenzene mg/kg wet0.0504 0.0050 0.05000 2069-129101 2
1,2-Dibromoethane mg/kg wet0.0505 0.0050 0.05000 2070-132101 4
1,2-Dichlorobenzene mg/kg wet0.0492 0.0050 0.05000 2072-12398 7
1,2-Dichloroethane mg/kg wet0.0492 0.0050 0.05000 2068-12898 6
1,2-Dichloropropane mg/kg wet0.0525 0.0050 0.05000 2073-130105 3
1,3,5-Trimethylbenzene mg/kg wet0.0487 0.0050 0.05000 2069-12897 5
1,3-Dichlorobenzene mg/kg wet0.0494 0.0050 0.05000 2071-12099 0.2
1,3-Dichloropropane mg/kg wet0.0505 0.0050 0.05000 2075-124101 7
1,4-Dichlorobenzene mg/kg wet0.0484 0.0050 0.05000 2071-12397 2
2,2-Dichloropropane mg/kg wet0.0481 0.0050 0.05000 2050-14296 2
2-Chlorotoluene mg/kg wet0.0497 0.0050 0.05000 2067-12499 0.04
4-Chlorotoluene mg/kg wet0.0487 0.0050 0.05000 2071-12697 4
4-Isopropyltoluene mg/kg wet0.0490 0.0050 0.05000 2068-12998 4
Acetone mg/kg wet0.102 0.050 0.1000 2029-198102 14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 58 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0287 - 5035
LCS Dup (P5C0287-BSD1)Prepared: 03/17/15 Analyzed: 03/18/15
Benzene mg/kg wet0.0518 0.0030 0.05000 2074-127104 1
Bromobenzene mg/kg wet0.0478 0.0050 0.05000 2073-12596 2
Bromochloromethane mg/kg wet0.0527 0.0050 0.05000 2072-134105 2
Bromodichloromethane mg/kg wet0.0462 0.0050 0.05000 2075-12292 0.06
Bromoform mg/kg wet0.0442 0.0050 0.05000 2066-13588 3
Bromomethane mg/kg wet0.0542 0.010 0.05000 2020-180108 5
Carbon Tetrachloride mg/kg wet0.0528 0.0050 0.05000 2064-143106 0.4
Chlorobenzene mg/kg wet0.0497 0.0050 0.05000 2074-11899 1
Chloroethane mg/kg wet0.0475 0.010 0.05000 20 D33-14995 21
Chloroform mg/kg wet0.0465 0.0050 0.05000 2073-12793 2
Chloromethane mg/kg wet0.0520 0.0050 0.05000 2045-143104 7
cis-1,2-Dichloroethylene mg/kg wet0.0525 0.0050 0.05000 2076-134105 0.3
cis-1,3-Dichloropropylene mg/kg wet0.0492 0.0050 0.05000 2071-12598 2
Dibromochloromethane mg/kg wet0.0431 0.0050 0.05000 2073-12286 3
Dichlorodifluoromethane mg/kg wet0.0528 0.0050 0.05000 2026-146106 6
Ethylbenzene mg/kg wet0.0502 0.0050 0.05000 2074-128100 1
Isopropyl Ether mg/kg wet0.0471 0.0050 0.05000 2059-15994 3
Isopropylbenzene (Cumene)mg/kg wet0.0533 0.0050 0.05000 2068-126107 6
m,p-Xylenes mg/kg wet0.0964 0.010 0.1000 2075-12496 4
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0507 0.050 0.05000 2061-157101 14
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0501 0.10 0.05000 20 J63-149100 5
Methyl Isobutyl Ketone mg/kg wet0.0494 0.050 0.05000 20 J57-16299 13
Methylene Chloride mg/kg wet0.0510 0.0050 0.05000 2074-129102 2
Methyl-tert-Butyl Ether mg/kg wet0.0515 0.010 0.05000 2070-130103 3
Naphthalene mg/kg wet0.0454 0.010 0.05000 2057-15791 12
n-Butylbenzene mg/kg wet0.0505 0.0050 0.05000 2065-135101 1
n-Propylbenzene mg/kg wet0.0484 0.0050 0.05000 2067-13097 4
o-Xylene mg/kg wet0.0476 0.0050 0.05000 2074-12695 3
sec-Butylbenzene mg/kg wet0.0538 0.0050 0.05000 2066-131108 4
Styrene mg/kg wet0.0481 0.0050 0.05000 2077-12196 3
tert-Butylbenzene mg/kg wet0.0525 0.0050 0.05000 2067-132105 2
Tetrachloroethylene mg/kg wet0.0499 0.0050 0.05000 2068-130100 3
Toluene mg/kg wet0.0495 0.0050 0.05000 2071-12999 4
trans-1,2-Dichloroethylene mg/kg wet0.0516 0.0050 0.05000 2073-132103 3
trans-1,3-Dichloropropylene mg/kg wet0.0489 0.0050 0.05000 2068-12398 0.7
Trichloroethylene mg/kg wet0.0488 0.0050 0.05000 2075-13398 7
Trichlorofluoromethane mg/kg wet0.0526 0.0050 0.05000 2044-146105 4
Vinyl acetate mg/kg wet0.0535 0.025 0.05000 2085-161107 4
Vinyl chloride mg/kg wet0.0512 0.0050 0.05000 2048-147102 4
Xylenes, total mg/kg wet0.144 0.015 0.1500 2074-12696 4
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1010.0504
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1000.0502
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 980.0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 59 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0300 - 5035
Blank (P5C0300-BLK1)Prepared & Analyzed: 03/18/15
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 60 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0300 - 5035
Blank (P5C0300-BLK1)Prepared & Analyzed: 03/18/15
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1100.0551
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 1010.0505
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1050.0523
LCS (P5C0300-BS1)Prepared & Analyzed: 03/18/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0457 0.0050 0.05000 72-11591
1,1,1-Trichloroethane mg/kg wet0.0500 0.0050 0.05000 67-131100
1,1,2,2-Tetrachloroethane mg/kg wet0.0481 0.0050 0.05000 56-12696
1,1,2-Trichloroethane mg/kg wet0.0468 0.0050 0.05000 70-13394
1,1-Dichloroethane mg/kg wet0.0526 0.0050 0.05000 74-127105
1,1-Dichloroethylene mg/kg wet0.0552 0.0050 0.05000 67-149110
1,1-Dichloropropylene mg/kg wet0.0548 0.0050 0.05000 71-130110
1,2,3-Trichlorobenzene mg/kg wet0.0481 0.0050 0.05000 68-13096
1,2,3-Trichloropropane mg/kg wet0.0452 0.0050 0.05000 60-13790
1,2,4-Trichlorobenzene mg/kg wet0.0511 0.0050 0.05000 66-125102
1,2,4-Trimethylbenzene mg/kg wet0.0518 0.0050 0.05000 69-129104
1,2-Dibromoethane mg/kg wet0.0490 0.0050 0.05000 70-13298
1,2-Dichlorobenzene mg/kg wet0.0491 0.0050 0.05000 72-12398
1,2-Dichloroethane mg/kg wet0.0450 0.0050 0.05000 68-12890
1,2-Dichloropropane mg/kg wet0.0497 0.0050 0.05000 73-13099
1,3,5-Trimethylbenzene mg/kg wet0.0516 0.0050 0.05000 69-128103
1,3-Dichlorobenzene mg/kg wet0.0498 0.0050 0.05000 71-120100
1,3-Dichloropropane mg/kg wet0.0482 0.0050 0.05000 75-12496
1,4-Dichlorobenzene mg/kg wet0.0493 0.0050 0.05000 71-12399
2,2-Dichloropropane mg/kg wet0.0526 0.0050 0.05000 50-142105
2-Chlorotoluene mg/kg wet0.0512 0.0050 0.05000 67-124102
4-Chlorotoluene mg/kg wet0.0489 0.0050 0.05000 71-12698
4-Isopropyltoluene mg/kg wet0.0502 0.0050 0.05000 68-129100
Acetone mg/kg wet0.0901 0.050 0.1000 29-19890
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 61 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0300 - 5035
LCS (P5C0300-BS1)Prepared & Analyzed: 03/18/15
Benzene mg/kg wet0.0508 0.0030 0.05000 74-127102
Bromobenzene mg/kg wet0.0505 0.0050 0.05000 73-125101
Bromochloromethane mg/kg wet0.0500 0.0050 0.05000 72-134100
Bromodichloromethane mg/kg wet0.0434 0.0050 0.05000 75-12287
Bromoform mg/kg wet0.0422 0.0050 0.05000 66-13584
Bromomethane mg/kg wet0.0522 0.010 0.05000 20-180104
Carbon Tetrachloride mg/kg wet0.0519 0.0050 0.05000 64-143104
Chlorobenzene mg/kg wet0.0505 0.0050 0.05000 74-118101
Chloroethane mg/kg wet0.0509 0.010 0.05000 33-149102
Chloroform mg/kg wet0.0459 0.0050 0.05000 73-12792
Chloromethane mg/kg wet0.0530 0.0050 0.05000 45-143106
cis-1,2-Dichloroethylene mg/kg wet0.0528 0.0050 0.05000 76-134106
cis-1,3-Dichloropropylene mg/kg wet0.0506 0.0050 0.05000 71-125101
Dibromochloromethane mg/kg wet0.0413 0.0050 0.05000 73-12283
Dichlorodifluoromethane mg/kg wet0.0536 0.0050 0.05000 26-146107
Ethylbenzene mg/kg wet0.0504 0.0050 0.05000 74-128101
Isopropyl Ether mg/kg wet0.0477 0.0050 0.05000 59-15995
Isopropylbenzene (Cumene)mg/kg wet0.0555 0.0050 0.05000 68-126111
m,p-Xylenes mg/kg wet0.102 0.010 0.1000 75-124102
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0445 0.050 0.05000 J61-15789
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0453 0.10 0.05000 J63-14991
Methyl Isobutyl Ketone mg/kg wet0.0425 0.050 0.05000 J57-16285
Methylene Chloride mg/kg wet0.0496 0.0050 0.05000 74-12999
Methyl-tert-Butyl Ether mg/kg wet0.0467 0.010 0.05000 70-13093
Naphthalene mg/kg wet0.0446 0.010 0.05000 57-15789
n-Butylbenzene mg/kg wet0.0524 0.0050 0.05000 65-135105
n-Propylbenzene mg/kg wet0.0540 0.0050 0.05000 67-130108
o-Xylene mg/kg wet0.0491 0.0050 0.05000 74-12698
sec-Butylbenzene mg/kg wet0.0573 0.0050 0.05000 66-131115
Styrene mg/kg wet0.0486 0.0050 0.05000 77-12197
tert-Butylbenzene mg/kg wet0.0528 0.0050 0.05000 67-132106
Tetrachloroethylene mg/kg wet0.0531 0.0050 0.05000 68-130106
Toluene mg/kg wet0.0510 0.0050 0.05000 71-129102
trans-1,2-Dichloroethylene mg/kg wet0.0525 0.0050 0.05000 73-132105
trans-1,3-Dichloropropylene mg/kg wet0.0483 0.0050 0.05000 68-12397
Trichloroethylene mg/kg wet0.0493 0.0050 0.05000 75-13399
Trichlorofluoromethane mg/kg wet0.0516 0.0050 0.05000 44-146103
Vinyl acetate mg/kg wet0.0528 0.025 0.05000 85-161106
Vinyl chloride mg/kg wet0.0513 0.0050 0.05000 48-147103
Xylenes, total mg/kg wet0.151 0.015 0.1500 74-126100
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 1000.0500
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 970.0483
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 980.0491
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 62 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0300 - 5035
LCS Dup (P5C0300-BSD1)Prepared & Analyzed: 03/18/15
1,1,1,2-Tetrachloroethane mg/kg wet0.0484 0.0050 0.05000 2072-11597 6
1,1,1-Trichloroethane mg/kg wet0.0480 0.0050 0.05000 2067-13196 4
1,1,2,2-Tetrachloroethane mg/kg wet0.0478 0.0050 0.05000 2056-12696 0.6
1,1,2-Trichloroethane mg/kg wet0.0452 0.0050 0.05000 2070-13390 3
1,1-Dichloroethane mg/kg wet0.0510 0.0050 0.05000 2074-127102 3
1,1-Dichloroethylene mg/kg wet0.0528 0.0050 0.05000 2067-149106 4
1,1-Dichloropropylene mg/kg wet0.0534 0.0050 0.05000 2071-130107 2
1,2,3-Trichlorobenzene mg/kg wet0.0494 0.0050 0.05000 2068-13099 3
1,2,3-Trichloropropane mg/kg wet0.0447 0.0050 0.05000 2060-13789 1
1,2,4-Trichlorobenzene mg/kg wet0.0496 0.0050 0.05000 2066-12599 3
1,2,4-Trimethylbenzene mg/kg wet0.0494 0.0050 0.05000 2069-12999 5
1,2-Dibromoethane mg/kg wet0.0504 0.0050 0.05000 2070-132101 3
1,2-Dichlorobenzene mg/kg wet0.0469 0.0050 0.05000 2072-12394 5
1,2-Dichloroethane mg/kg wet0.0450 0.0050 0.05000 2068-12890 0.04
1,2-Dichloropropane mg/kg wet0.0493 0.0050 0.05000 2073-13099 0.9
1,3,5-Trimethylbenzene mg/kg wet0.0511 0.0050 0.05000 2069-128102 0.9
1,3-Dichlorobenzene mg/kg wet0.0469 0.0050 0.05000 2071-12094 6
1,3-Dichloropropane mg/kg wet0.0517 0.0050 0.05000 2075-124103 7
1,4-Dichlorobenzene mg/kg wet0.0492 0.0050 0.05000 2071-12398 0.06
2,2-Dichloropropane mg/kg wet0.0500 0.0050 0.05000 2050-142100 5
2-Chlorotoluene mg/kg wet0.0505 0.0050 0.05000 2067-124101 1
4-Chlorotoluene mg/kg wet0.0482 0.0050 0.05000 2071-12696 2
4-Isopropyltoluene mg/kg wet0.0488 0.0050 0.05000 2068-12998 3
Acetone mg/kg wet0.0962 0.050 0.1000 2029-19896 7
Benzene mg/kg wet0.0492 0.0030 0.05000 2074-12798 3
Bromobenzene mg/kg wet0.0476 0.0050 0.05000 2073-12595 6
Bromochloromethane mg/kg wet0.0489 0.0050 0.05000 2072-13498 2
Bromodichloromethane mg/kg wet0.0437 0.0050 0.05000 2075-12287 0.7
Bromoform mg/kg wet0.0449 0.0050 0.05000 2066-13590 6
Bromomethane mg/kg wet0.0511 0.010 0.05000 2020-180102 2
Carbon Tetrachloride mg/kg wet0.0498 0.0050 0.05000 2064-143100 4
Chlorobenzene mg/kg wet0.0493 0.0050 0.05000 2074-11899 3
Chloroethane mg/kg wet0.0461 0.010 0.05000 2033-14992 10
Chloroform mg/kg wet0.0441 0.0050 0.05000 2073-12788 4
Chloromethane mg/kg wet0.0515 0.0050 0.05000 2045-143103 3
cis-1,2-Dichloroethylene mg/kg wet0.0506 0.0050 0.05000 2076-134101 4
cis-1,3-Dichloropropylene mg/kg wet0.0496 0.0050 0.05000 2071-12599 2
Dibromochloromethane mg/kg wet0.0442 0.0050 0.05000 2073-12288 7
Dichlorodifluoromethane mg/kg wet0.0514 0.0050 0.05000 2026-146103 4
Ethylbenzene mg/kg wet0.0491 0.0050 0.05000 2074-12898 3
Isopropyl Ether mg/kg wet0.0465 0.0050 0.05000 2059-15993 3
Isopropylbenzene (Cumene)mg/kg wet0.0544 0.0050 0.05000 2068-126109 2
m,p-Xylenes mg/kg wet0.103 0.010 0.1000 2075-124103 1
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0515 0.050 0.05000 2061-157103 15
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0455 0.10 0.05000 20 J63-14991 0.4
Methyl Isobutyl Ketone mg/kg wet0.0458 0.050 0.05000 20 J57-16292 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 63 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P5C0300 - 5035
LCS Dup (P5C0300-BSD1)Prepared & Analyzed: 03/18/15
Methylene Chloride mg/kg wet0.0501 0.0050 0.05000 2074-129100 0.9
Methyl-tert-Butyl Ether mg/kg wet0.0483 0.010 0.05000 2070-13097 3
Naphthalene mg/kg wet0.0454 0.010 0.05000 2057-15791 2
n-Butylbenzene mg/kg wet0.0509 0.0050 0.05000 2065-135102 3
n-Propylbenzene mg/kg wet0.0496 0.0050 0.05000 2067-13099 9
o-Xylene mg/kg wet0.0515 0.0050 0.05000 2074-126103 5
sec-Butylbenzene mg/kg wet0.0550 0.0050 0.05000 2066-131110 4
Styrene mg/kg wet0.0513 0.0050 0.05000 2077-121103 5
tert-Butylbenzene mg/kg wet0.0503 0.0050 0.05000 2067-132101 5
Tetrachloroethylene mg/kg wet0.0537 0.0050 0.05000 2068-130107 1
Toluene mg/kg wet0.0507 0.0050 0.05000 2071-129101 0.6
trans-1,2-Dichloroethylene mg/kg wet0.0524 0.0050 0.05000 2073-132105 0.2
trans-1,3-Dichloropropylene mg/kg wet0.0480 0.0050 0.05000 2068-12396 0.7
Trichloroethylene mg/kg wet0.0482 0.0050 0.05000 2075-13396 2
Trichlorofluoromethane mg/kg wet0.0490 0.0050 0.05000 2044-14698 5
Vinyl acetate mg/kg wet0.0504 0.025 0.05000 2085-161101 5
Vinyl chloride mg/kg wet0.0492 0.0050 0.05000 2048-14798 4
Xylenes, total mg/kg wet0.154 0.015 0.1500 2074-126103 2
mg/kg wet 0.05000 70-130Surrogate: 4-Bromofluorobenzene 990.0496
mg/kg wet 0.05000 84-123Surrogate: Dibromofluoromethane 990.0496
mg/kg wet 0.05000 76-129Surrogate: Toluene-d8 1010.0506
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 64 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5C0264 - 3546
Blank (P5C0264-BLK1)Prepared & Analyzed: 03/17/15
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 65 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5C0264 - 3546
Blank (P5C0264-BLK1)Prepared & Analyzed: 03/17/15
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.329 39-132Surrogate: 2,4,6-Tribromophenol 913.03
mg/kg wet 1.664 44-115Surrogate: 2-Fluorobiphenyl 881.46
mg/kg wet 3.329 35-115Surrogate: 2-Fluorophenol 892.96
mg/kg wet 1.664 37-122Surrogate: Nitrobenzene-d5 881.47
mg/kg wet 3.329 34-121Surrogate: Phenol-d5 862.87
mg/kg wet 1.664 54-127Surrogate: Terphenyl-d14 1091.81
LCS (P5C0264-BS1)Prepared & Analyzed: 03/17/15
1,2,4-Trichlorobenzene mg/kg wet1.28 0.33 1.664 34-11877
1,2-Dichlorobenzene mg/kg wet1.15 0.33 1.664 33-11769
1,3-Dichlorobenzene mg/kg wet1.13 0.33 1.664 30-11568
1,4-Dichlorobenzene mg/kg wet1.12 0.33 1.664 31-11568
1-Methylnaphthalene mg/kg wet1.27 0.33 1.664 40-11977
2,4,6-Trichlorophenol mg/kg wet1.49 0.33 1.664 39-12689
2,4-Dichlorophenol mg/kg wet1.48 0.33 1.664 40-12289
2,4-Dimethylphenol mg/kg wet1.48 0.33 1.664 30-12789
2,4-Dinitrophenol mg/kg wet1.27 0.33 1.664 27-12976
2,4-Dinitrotoluene mg/kg wet1.55 0.33 1.664 48-12693
2,6-Dinitrotoluene mg/kg wet1.56 0.33 1.664 46-12494
2-Chloronaphthalene mg/kg wet1.62 0.33 1.664 41-11497
2-Chlorophenol mg/kg wet1.35 0.33 1.664 34-12181
2-Methylnaphthalene mg/kg wet1.33 0.33 1.664 38-12280
2-Methylphenol mg/kg wet1.38 0.33 1.664 32-12283
2-Nitrophenol mg/kg wet1.36 0.33 1.664 36-12382
3,3'-Dichlorobenzidine mg/kg wet1.29 0.33 1.664 22-12178
3/4-Methylphenol mg/kg wet1.42 0.33 1.664 34-11985
4,6-Dinitro-2-methylphenol mg/kg wet1.59 0.33 1.664 29-13296
4-Bromophenyl phenyl ether mg/kg wet1.40 0.33 1.664 46-12484
4-Chloro-3-methylphenol mg/kg wet1.55 0.33 1.664 45-12293
4-Chloroaniline mg/kg wet1.36 0.33 1.664 17-10682
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 66 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5C0264 - 3546
LCS (P5C0264-BS1)Prepared & Analyzed: 03/17/15
4-Chlorophenyl phenyl ether mg/kg wet1.40 0.33 1.664 45-12184
4-Nitrophenol mg/kg wet1.58 0.33 1.664 30-13295
Acenaphthene mg/kg wet1.39 0.33 1.664 40-12383
Acenaphthylene mg/kg wet1.38 0.33 1.664 32-13283
Anthracene mg/kg wet1.53 0.33 1.664 47-12392
Azobenzene mg/kg wet1.69 0.33 1.664 39-125101
Benzo(a)anthracene mg/kg wet1.49 0.33 1.664 49-12689
Benzo(a)pyrene mg/kg wet1.59 0.33 1.664 45-12995
Benzo(b)fluoranthene mg/kg wet1.55 0.33 1.664 45-13293
Benzo(g,h,i)perylene mg/kg wet1.58 0.33 1.664 43-13495
Benzo(k)fluoranthene mg/kg wet1.63 0.33 1.664 47-13298
Benzoic Acid mg/kg wet1.06 0.33 1.664 10-8364
Benzyl alcohol mg/kg wet1.19 0.33 1.664 29-12271
bis(2-Chloroethoxy)methane mg/kg wet1.26 0.33 1.664 36-12176
Bis(2-Chloroethyl)ether mg/kg wet0.973 0.33 1.664 31-12058
Bis(2-chloroisopropyl)ether mg/kg wet1.10 0.33 1.664 33-13166
Bis(2-Ethylhexyl)phthalate mg/kg wet1.47 0.33 1.664 51-13388
Butyl benzyl phthalate mg/kg wet1.49 0.33 1.664 48-13289
Chrysene mg/kg wet1.55 0.33 1.664 50-12493
Dibenzo(a,h)anthracene mg/kg wet1.63 0.33 1.664 45-13498
Dibenzofuran mg/kg wet1.36 0.33 1.664 44-12082
Diethyl phthalate mg/kg wet1.40 0.33 1.664 50-12484
Dimethyl phthalate mg/kg wet1.40 0.33 1.664 48-12484
Di-n-butyl phthalate mg/kg wet1.51 0.33 1.664 51-12891
Di-n-octyl phthalate mg/kg wet1.57 0.33 1.664 45-14094
Fluoranthene mg/kg wet1.53 0.33 1.664 50-12792
Fluorene mg/kg wet1.38 0.33 1.664 43-12583
Hexachlorobenzene mg/kg wet1.49 0.33 1.664 45-12290
Hexachlorobutadiene mg/kg wet1.25 0.33 1.664 32-12375
Hexachlorocyclopentadiene mg/kg wet1.22 0.33 1.664 32-11773
Hexachloroethane mg/kg wet1.10 0.33 1.664 28-11766
Indeno(1,2,3-cd)pyrene mg/kg wet1.65 0.33 1.664 45-13399
Isophorone mg/kg wet1.43 0.33 1.664 30-12286
Naphthalene mg/kg wet1.23 0.33 1.664 35-12374
Nitrobenzene mg/kg wet1.32 0.33 1.664 34-12280
N-Nitroso-di-n-propylamine mg/kg wet1.25 0.33 1.664 36-12075
N-Nitrosodiphenylamine mg/kg wet1.52 0.33 1.664 38-12791
Pentachlorophenol mg/kg wet1.62 0.33 1.664 25-13397
Phenanthrene mg/kg wet1.48 0.33 1.664 50-12189
Phenol mg/kg wet1.41 0.33 1.664 34-12184
Pyrene mg/kg wet1.50 0.33 1.664 47-12790
mg/kg wet 3.329 39-132Surrogate: 2,4,6-Tribromophenol 933.11
mg/kg wet 1.664 44-115Surrogate: 2-Fluorobiphenyl 891.48
mg/kg wet 3.329 35-115Surrogate: 2-Fluorophenol 842.79
mg/kg wet 1.664 37-122Surrogate: Nitrobenzene-d5 811.34
mg/kg wet 3.329 34-121Surrogate: Phenol-d5 842.79
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 67 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5C0264 - 3546
LCS (P5C0264-BS1)Prepared & Analyzed: 03/17/15
mg/kg wet 1.664 54-127Surrogate: Terphenyl-d14 1031.71
LCS Dup (P5C0264-BSD1)Prepared & Analyzed: 03/17/15
1,2,4-Trichlorobenzene mg/kg wet1.29 0.33 1.664 2034-11878 1
1,2-Dichlorobenzene mg/kg wet1.20 0.33 1.664 2033-11772 4
1,3-Dichlorobenzene mg/kg wet1.18 0.33 1.664 2030-11571 5
1,4-Dichlorobenzene mg/kg wet1.18 0.33 1.664 2031-11571 5
1-Methylnaphthalene mg/kg wet1.32 0.33 1.664 2040-11980 4
2,4,6-Trichlorophenol mg/kg wet1.56 0.33 1.664 2039-12694 5
2,4-Dichlorophenol mg/kg wet1.53 0.33 1.664 2040-12292 3
2,4-Dimethylphenol mg/kg wet1.52 0.33 1.664 2030-12792 3
2,4-Dinitrophenol mg/kg wet1.22 0.33 1.664 2027-12973 4
2,4-Dinitrotoluene mg/kg wet1.66 0.33 1.664 2048-126100 6
2,6-Dinitrotoluene mg/kg wet1.63 0.33 1.664 2046-12498 4
2-Chloronaphthalene mg/kg wet1.73 0.33 1.664 2041-114104 7
2-Chlorophenol mg/kg wet1.40 0.33 1.664 2034-12184 4
2-Methylnaphthalene mg/kg wet1.36 0.33 1.664 2038-12282 3
2-Methylphenol mg/kg wet1.42 0.33 1.664 2032-12285 3
2-Nitrophenol mg/kg wet1.38 0.33 1.664 2036-12383 2
3,3'-Dichlorobenzidine mg/kg wet1.37 0.33 1.664 2022-12182 6
3/4-Methylphenol mg/kg wet1.52 0.33 1.664 2034-11991 7
4,6-Dinitro-2-methylphenol mg/kg wet1.60 0.33 1.664 2029-13296 0.5
4-Bromophenyl phenyl ether mg/kg wet1.47 0.33 1.664 2046-12488 5
4-Chloro-3-methylphenol mg/kg wet1.52 0.33 1.664 2045-12291 2
4-Chloroaniline mg/kg wet1.42 0.33 1.664 2017-10686 4
4-Chlorophenyl phenyl ether mg/kg wet1.42 0.33 1.664 2045-12186 2
4-Nitrophenol mg/kg wet1.64 0.33 1.664 2030-13299 4
Acenaphthene mg/kg wet1.42 0.33 1.664 2040-12386 3
Acenaphthylene mg/kg wet1.44 0.33 1.664 2032-13287 5
Anthracene mg/kg wet1.56 0.33 1.664 2047-12394 2
Azobenzene mg/kg wet1.72 0.33 1.664 2039-125104 2
Benzo(a)anthracene mg/kg wet1.57 0.33 1.664 2049-12694 5
Benzo(a)pyrene mg/kg wet1.63 0.33 1.664 2045-12998 3
Benzo(b)fluoranthene mg/kg wet1.61 0.33 1.664 2045-13297 4
Benzo(g,h,i)perylene mg/kg wet1.65 0.33 1.664 2043-13499 5
Benzo(k)fluoranthene mg/kg wet1.70 0.33 1.664 2047-132102 4
Benzoic Acid mg/kg wet0.966 0.33 1.664 2010-8358 9
Benzyl alcohol mg/kg wet1.24 0.33 1.664 2029-12275 5
bis(2-Chloroethoxy)methane mg/kg wet1.33 0.33 1.664 2036-12180 5
Bis(2-Chloroethyl)ether mg/kg wet1.33 0.33 1.664 20 D31-12080 31
Bis(2-chloroisopropyl)ether mg/kg wet1.18 0.33 1.664 2033-13171 7
Bis(2-Ethylhexyl)phthalate mg/kg wet1.52 0.33 1.664 2051-13392 4
Butyl benzyl phthalate mg/kg wet1.55 0.33 1.664 2048-13293 4
Chrysene mg/kg wet1.63 0.33 1.664 2050-12498 5
Dibenzo(a,h)anthracene mg/kg wet1.70 0.33 1.664 2045-134102 4
Dibenzofuran mg/kg wet1.39 0.33 1.664 2044-12083 2
Diethyl phthalate mg/kg wet1.47 0.33 1.664 2050-12488 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 68 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5C0264 - 3546
LCS Dup (P5C0264-BSD1)Prepared & Analyzed: 03/17/15
Dimethyl phthalate mg/kg wet1.45 0.33 1.664 2048-12487 4
Di-n-butyl phthalate mg/kg wet1.54 0.33 1.664 2051-12893 2
Di-n-octyl phthalate mg/kg wet1.62 0.33 1.664 2045-14098 3
Fluoranthene mg/kg wet1.59 0.33 1.664 2050-12796 4
Fluorene mg/kg wet1.45 0.33 1.664 2043-12587 5
Hexachlorobenzene mg/kg wet1.57 0.33 1.664 2045-12294 5
Hexachlorobutadiene mg/kg wet1.24 0.33 1.664 2032-12375 0.7
Hexachlorocyclopentadiene mg/kg wet1.27 0.33 1.664 2032-11776 4
Hexachloroethane mg/kg wet1.19 0.33 1.664 2028-11771 8
Indeno(1,2,3-cd)pyrene mg/kg wet1.72 0.33 1.664 2045-133103 4
Isophorone mg/kg wet1.45 0.33 1.664 2030-12287 1
Naphthalene mg/kg wet1.28 0.33 1.664 2035-12377 4
Nitrobenzene mg/kg wet1.41 0.33 1.664 2034-12285 6
N-Nitroso-di-n-propylamine mg/kg wet1.32 0.33 1.664 2036-12079 6
N-Nitrosodiphenylamine mg/kg wet1.57 0.33 1.664 2038-12794 3
Pentachlorophenol mg/kg wet1.64 0.33 1.664 2025-13399 1
Phenanthrene mg/kg wet1.53 0.33 1.664 2050-12192 3
Phenol mg/kg wet1.44 0.33 1.664 2034-12186 2
Pyrene mg/kg wet1.57 0.33 1.664 2047-12794 4
mg/kg wet 3.329 39-132Surrogate: 2,4,6-Tribromophenol 973.22
mg/kg wet 1.664 44-115Surrogate: 2-Fluorobiphenyl 901.50
mg/kg wet 3.329 35-115Surrogate: 2-Fluorophenol 862.85
mg/kg wet 1.664 37-122Surrogate: Nitrobenzene-d5 831.38
mg/kg wet 3.329 34-121Surrogate: Phenol-d5 852.82
mg/kg wet 1.664 54-127Surrogate: Terphenyl-d14 1061.77
Matrix Spike (P5C0264-MS1)Prepared & Analyzed: 03/17/15 Source: 5030255-01
1,2,4-Trichlorobenzene mg/kg dry1.69 0.42 2.125 BRL 34-11880
1,2-Dichlorobenzene mg/kg dry1.54 0.42 2.125 BRL 33-11773
1,3-Dichlorobenzene mg/kg dry1.52 0.42 2.125 BRL 30-11572
1,4-Dichlorobenzene mg/kg dry1.54 0.42 2.125 BRL 31-11573
1-Methylnaphthalene mg/kg dry1.70 0.42 2.125 BRL 40-11980
2,4,6-Trichlorophenol mg/kg dry2.01 0.42 2.125 BRL 39-12694
2,4-Dichlorophenol mg/kg dry1.94 0.42 2.125 BRL 40-12292
2,4-Dimethylphenol mg/kg dry1.66 0.42 2.125 BRL 30-12778
2,4-Dinitrophenol mg/kg dry1.81 0.42 2.125 BRL 27-12985
2,4-Dinitrotoluene mg/kg dry2.03 0.42 2.125 BRL 48-12696
2,6-Dinitrotoluene mg/kg dry2.10 0.42 2.125 BRL 46-12499
2-Chloronaphthalene mg/kg dry2.18 0.42 2.125 BRL 41-114103
2-Chlorophenol mg/kg dry1.80 0.42 2.125 BRL 34-12185
2-Methylnaphthalene mg/kg dry1.77 0.42 2.125 BRL 38-12283
2-Methylphenol mg/kg dry1.78 0.42 2.125 BRL 32-12284
2-Nitrophenol mg/kg dry1.89 0.42 2.125 BRL 36-12389
3,3'-Dichlorobenzidine mg/kg dry1.56 0.42 2.125 BRL 22-12173
3/4-Methylphenol mg/kg dry1.84 0.42 2.125 BRL 34-11987
4,6-Dinitro-2-methylphenol mg/kg dry2.10 0.42 2.125 BRL 29-13299
4-Bromophenyl phenyl ether mg/kg dry1.86 0.42 2.125 BRL 46-12487
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 69 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5C0264 - 3546
Matrix Spike (P5C0264-MS1)Prepared & Analyzed: 03/17/15 Source: 5030255-01
4-Chloro-3-methylphenol mg/kg dry2.03 0.42 2.125 BRL 45-12296
4-Chloroaniline mg/kg dry1.81 0.42 2.125 BRL 17-10685
4-Chlorophenyl phenyl ether mg/kg dry1.80 0.42 2.125 BRL 45-12185
4-Nitrophenol mg/kg dry2.14 0.42 2.125 BRL 30-132101
Acenaphthene mg/kg dry1.86 0.42 2.125 BRL 40-12387
Acenaphthylene mg/kg dry1.84 0.42 2.125 BRL 32-13287
Anthracene mg/kg dry1.97 0.42 2.125 BRL 47-12393
Azobenzene mg/kg dry2.20 0.42 2.125 BRL 39-125104
Benzo(a)anthracene mg/kg dry1.99 0.42 2.125 BRL 49-12693
Benzo(a)pyrene mg/kg dry2.01 0.42 2.125 BRL 45-12995
Benzo(b)fluoranthene mg/kg dry1.97 0.42 2.125 BRL 45-13292
Benzo(g,h,i)perylene mg/kg dry2.02 0.42 2.125 BRL 43-13495
Benzo(k)fluoranthene mg/kg dry2.06 0.42 2.125 BRL 47-13297
Benzoic Acid mg/kg dry1.75 0.42 2.125 BRL 10-8382
Benzyl alcohol mg/kg dry1.61 0.42 2.125 BRL 29-12276
bis(2-Chloroethoxy)methane mg/kg dry1.71 0.42 2.125 BRL 36-12181
Bis(2-Chloroethyl)ether mg/kg dry1.72 0.42 2.125 BRL 31-12081
Bis(2-chloroisopropyl)ether mg/kg dry1.51 0.42 2.125 BRL 33-13171
Bis(2-Ethylhexyl)phthalate mg/kg dry1.95 0.42 2.125 BRL 51-13392
Butyl benzyl phthalate mg/kg dry1.99 0.42 2.125 BRL 48-13293
Chrysene mg/kg dry2.06 0.42 2.125 BRL 50-12497
Dibenzo(a,h)anthracene mg/kg dry2.03 0.42 2.125 BRL 45-13495
Dibenzofuran mg/kg dry1.79 0.42 2.125 BRL 44-12084
Diethyl phthalate mg/kg dry1.87 0.42 2.125 BRL 50-12488
Dimethyl phthalate mg/kg dry1.82 0.42 2.125 BRL 48-12486
Di-n-butyl phthalate mg/kg dry1.94 0.42 2.125 BRL 51-12891
Di-n-octyl phthalate mg/kg dry1.97 0.42 2.125 BRL 45-14093
Fluoranthene mg/kg dry1.97 0.42 2.125 BRL 50-12793
Fluorene mg/kg dry1.87 0.42 2.125 BRL 43-12588
Hexachlorobenzene mg/kg dry2.02 0.42 2.125 BRL 45-12295
Hexachlorobutadiene mg/kg dry1.67 0.42 2.125 BRL 32-12379
Hexachlorocyclopentadiene mg/kg dry1.65 0.42 2.125 BRL 32-11778
Hexachloroethane mg/kg dry1.49 0.42 2.125 BRL 28-11770
Indeno(1,2,3-cd)pyrene mg/kg dry2.09 0.42 2.125 BRL 45-13398
Isophorone mg/kg dry1.90 0.42 2.125 BRL 30-12289
Naphthalene mg/kg dry1.67 0.42 2.125 BRL 35-12378
Nitrobenzene mg/kg dry1.80 0.42 2.125 BRL 34-12285
N-Nitroso-di-n-propylamine mg/kg dry1.70 0.42 2.125 BRL 36-12080
N-Nitrosodiphenylamine mg/kg dry1.92 0.42 2.125 BRL 38-12790
Pentachlorophenol mg/kg dry2.02 0.42 2.125 BRL 25-13395
Phenanthrene mg/kg dry1.93 0.42 2.125 BRL 50-12191
Phenol mg/kg dry1.83 0.42 2.125 BRL 34-12186
Pyrene mg/kg dry2.01 0.42 2.125 BRL 47-12795
mg/kg dry 4.250 39-132Surrogate: 2,4,6-Tribromophenol 913.86
mg/kg dry 2.125 44-115Surrogate: 2-Fluorobiphenyl 911.94
mg/kg dry 4.250 35-115Surrogate: 2-Fluorophenol 853.61
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 70 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5C0264 - 3546
Matrix Spike (P5C0264-MS1)Prepared & Analyzed: 03/17/15 Source: 5030255-01
mg/kg dry 2.125 37-122Surrogate: Nitrobenzene-d5 851.81
mg/kg dry 4.250 34-121Surrogate: Phenol-d5 853.62
mg/kg dry 2.125 54-127Surrogate: Terphenyl-d14 1082.29
Matrix Spike Dup (P5C0264-MSD1)Prepared & Analyzed: 03/17/15 Source: 5030255-01
1,2,4-Trichlorobenzene mg/kg dry1.61 0.42 2.128 BRL 2034-11876 5
1,2-Dichlorobenzene mg/kg dry1.50 0.42 2.128 BRL 2033-11770 3
1,3-Dichlorobenzene mg/kg dry1.48 0.42 2.128 BRL 2030-11570 3
1,4-Dichlorobenzene mg/kg dry1.45 0.42 2.128 BRL 2031-11568 6
1-Methylnaphthalene mg/kg dry1.58 0.42 2.128 BRL 2040-11974 8
2,4,6-Trichlorophenol mg/kg dry1.87 0.42 2.128 BRL 2039-12688 7
2,4-Dichlorophenol mg/kg dry1.81 0.42 2.128 BRL 2040-12285 7
2,4-Dimethylphenol mg/kg dry1.60 0.42 2.128 BRL 2030-12775 4
2,4-Dinitrophenol mg/kg dry1.79 0.42 2.128 BRL 2027-12984 2
2,4-Dinitrotoluene mg/kg dry2.00 0.42 2.128 BRL 2048-12694 2
2,6-Dinitrotoluene mg/kg dry1.94 0.42 2.128 BRL 2046-12491 8
2-Chloronaphthalene mg/kg dry2.07 0.42 2.128 BRL 2041-11497 5
2-Chlorophenol mg/kg dry1.69 0.42 2.128 BRL 2034-12180 6
2-Methylnaphthalene mg/kg dry1.67 0.42 2.128 BRL 2038-12278 6
2-Methylphenol mg/kg dry1.70 0.42 2.128 BRL 2032-12280 4
2-Nitrophenol mg/kg dry1.76 0.42 2.128 BRL 2036-12383 7
3,3'-Dichlorobenzidine mg/kg dry1.63 0.42 2.128 BRL 2022-12177 4
3/4-Methylphenol mg/kg dry1.78 0.42 2.128 BRL 2034-11983 4
4,6-Dinitro-2-methylphenol mg/kg dry2.03 0.42 2.128 BRL 2029-13295 3
4-Bromophenyl phenyl ether mg/kg dry1.73 0.42 2.128 BRL 2046-12481 7
4-Chloro-3-methylphenol mg/kg dry1.89 0.42 2.128 BRL 2045-12289 7
4-Chloroaniline mg/kg dry1.70 0.42 2.128 BRL 2017-10680 6
4-Chlorophenyl phenyl ether mg/kg dry1.70 0.42 2.128 BRL 2045-12180 6
4-Nitrophenol mg/kg dry1.93 0.42 2.128 BRL 2030-13291 10
Acenaphthene mg/kg dry1.74 0.42 2.128 BRL 2040-12382 7
Acenaphthylene mg/kg dry1.73 0.42 2.128 BRL 2032-13281 6
Anthracene mg/kg dry1.86 0.42 2.128 BRL 2047-12387 6
Azobenzene mg/kg dry2.06 0.42 2.128 BRL 2039-12597 6
Benzo(a)anthracene mg/kg dry1.88 0.42 2.128 BRL 2049-12688 5
Benzo(a)pyrene mg/kg dry1.87 0.42 2.128 BRL 2045-12988 8
Benzo(b)fluoranthene mg/kg dry1.79 0.42 2.128 BRL 2045-13284 9
Benzo(g,h,i)perylene mg/kg dry1.88 0.42 2.128 BRL 2043-13488 7
Benzo(k)fluoranthene mg/kg dry1.89 0.42 2.128 BRL 2047-13289 9
Benzoic Acid mg/kg dry1.65 0.42 2.128 BRL 2010-8378 6
Benzyl alcohol mg/kg dry1.55 0.42 2.128 BRL 2029-12273 4
bis(2-Chloroethoxy)methane mg/kg dry1.60 0.42 2.128 BRL 2036-12175 7
Bis(2-Chloroethyl)ether mg/kg dry1.62 0.42 2.128 BRL 2031-12076 6
Bis(2-chloroisopropyl)ether mg/kg dry1.43 0.42 2.128 BRL 2033-13167 5
Bis(2-Ethylhexyl)phthalate mg/kg dry1.82 0.42 2.128 BRL 2051-13385 7
Butyl benzyl phthalate mg/kg dry1.85 0.42 2.128 BRL 2048-13287 7
Chrysene mg/kg dry1.93 0.42 2.128 BRL 2050-12491 7
Dibenzo(a,h)anthracene mg/kg dry1.84 0.42 2.128 BRL 2045-13486 10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 71 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P5C0264 - 3546
Matrix Spike Dup (P5C0264-MSD1)Prepared & Analyzed: 03/17/15 Source: 5030255-01
Dibenzofuran mg/kg dry1.69 0.42 2.128 BRL 2044-12080 6
Diethyl phthalate mg/kg dry1.74 0.42 2.128 BRL 2050-12482 7
Dimethyl phthalate mg/kg dry1.76 0.42 2.128 BRL 2048-12483 4
Di-n-butyl phthalate mg/kg dry1.85 0.42 2.128 BRL 2051-12887 5
Di-n-octyl phthalate mg/kg dry1.83 0.42 2.128 BRL 2045-14086 8
Fluoranthene mg/kg dry1.85 0.42 2.128 BRL 2050-12787 7
Fluorene mg/kg dry1.73 0.42 2.128 BRL 2043-12581 7
Hexachlorobenzene mg/kg dry1.87 0.42 2.128 BRL 2045-12288 8
Hexachlorobutadiene mg/kg dry1.56 0.42 2.128 BRL 2032-12373 7
Hexachlorocyclopentadiene mg/kg dry1.53 0.42 2.128 BRL 2032-11772 7
Hexachloroethane mg/kg dry1.43 0.42 2.128 BRL 2028-11767 4
Indeno(1,2,3-cd)pyrene mg/kg dry1.96 0.42 2.128 BRL 2045-13392 6
Isophorone mg/kg dry1.77 0.42 2.128 BRL 2030-12283 7
Naphthalene mg/kg dry1.56 0.42 2.128 BRL 2035-12373 7
Nitrobenzene mg/kg dry1.68 0.42 2.128 BRL 2034-12279 7
N-Nitroso-di-n-propylamine mg/kg dry1.60 0.42 2.128 BRL 2036-12075 6
N-Nitrosodiphenylamine mg/kg dry1.82 0.42 2.128 BRL 2038-12786 5
Pentachlorophenol mg/kg dry1.92 0.42 2.128 BRL 2025-13390 5
Phenanthrene mg/kg dry1.82 0.42 2.128 BRL 2050-12185 6
Phenol mg/kg dry1.74 0.42 2.128 BRL 2034-12182 5
Pyrene mg/kg dry1.86 0.42 2.128 BRL 2047-12787 8
mg/kg dry 4.256 39-132Surrogate: 2,4,6-Tribromophenol 873.69
mg/kg dry 2.128 44-115Surrogate: 2-Fluorobiphenyl 851.81
mg/kg dry 4.256 35-115Surrogate: 2-Fluorophenol 803.42
mg/kg dry 2.128 37-122Surrogate: Nitrobenzene-d5 771.64
mg/kg dry 4.256 34-121Surrogate: Phenol-d5 823.48
mg/kg dry 2.128 54-127Surrogate: Terphenyl-d14 992.11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 72 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P5C0303 - MADEP VPH (S)
Blank (P5C0303-BLK1)Prepared & Analyzed: 03/18/15
C5-C8 Aliphatics mg/kg wetBRL5.0
C9-C12 Aliphatics mg/kg wetBRL5.0
C9-C10 Aromatics mg/kg wetBRL5.0
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (PID)949.98
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (FID)899.48
LCS (P5C0303-BS1)Prepared & Analyzed: 03/18/15
C5-C8 Aliphatics mg/kg wet33.9 5.0 32.00 70-130106
C9-C10 Aromatics mg/kg wet11.3 5.0 10.67 70-130106
C9-C12 Aliphatic mg/kg wet36.1 5.0 32.00 70-130113
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (PID)10210.9
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (FID)9610.2
LCS Dup (P5C0303-BSD1)Prepared & Analyzed: 03/18/15
C5-C8 Aliphatics mg/kg wet32.9 5.0 32.00 5070-130103 3
C9-C10 Aromatics mg/kg wet11.2 5.0 10.67 5070-130105 1
C9-C12 Aliphatic mg/kg wet35.7 5.0 32.00 5070-130112 1
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (PID)10210.8
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (FID)9610.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 73 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Gasoline Range Organics by GC/FID - Quality Control
Batch P5C0284 - 5035
Blank (P5C0284-BLK1)Prepared & Analyzed: 03/17/15
Gasoline Range Organics mg/kg wetBRL5.0
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1075.35
LCS (P5C0284-BS1)Prepared & Analyzed: 03/17/15
Gasoline Range Organics mg/kg wet56.5 5.0 50.00 41-138113
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 804.00
LCS Dup (P5C0284-BSD1)Prepared & Analyzed: 03/17/15
Gasoline Range Organics mg/kg wet58.8 5.0 50.00 2041-138118 4
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 854.25
Matrix Spike (P5C0284-MS1)Prepared & Analyzed: 03/17/15 Source: 5030255-12
Gasoline Range Organics mg/kg dry85.9 7.4 73.58 BRL 41-138117
mg/kg dry 7.358 50-137Surrogate: a,a,a-Trifluorotoluene 936.84
Matrix Spike Dup (P5C0284-MSD1)Prepared & Analyzed: 03/17/15 Source: 5030255-12
Gasoline Range Organics mg/kg dry82.0 6.8 67.96 BRL 3441-138121 5
mg/kg dry 6.796 50-137Surrogate: a,a,a-Trifluorotoluene 976.59
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 74 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P5C0258 - 3546
Blank (P5C0258-BLK1)Prepared: 03/16/15 Analyzed: 03/17/15
C9-C18 Aliphatics mg/kg wetBRL10
C19-C36 Aliphatics mg/kg wetBRL10
C11-C22 Aromatics mg/kg wetBRL10
mg/kg wet 1.996 40-140Surrogate: 1-Chlorooctadecane 801.59
mg/kg wet 1.996 40-140Surrogate: o-Terphenyl 751.49
mg/kg wet 3.992 40-140Surrogate: 2-Fluorobiphenyl 803.20
mg/kg wet 3.992 40-140Surrogate: 2-Bromonaphthalene 632.53
LCS (P5C0258-BS1)Prepared: 03/16/15 Analyzed: 03/17/15
C9-C18 Aliphatics mg/kg wet38.8 10 59.88 40-14065
C19-C36 Aliphatics mg/kg wet76.8 10 79.84 40-14096
C11-C22 Aromatics mg/kg wet15910 169.7 40-14094
mg/kg wet 1.996 40-140Surrogate: 1-Chlorooctadecane 831.65
mg/kg wet 1.996 40-140Surrogate: o-Terphenyl 851.70
mg/kg wet 3.992 40-140Surrogate: 2-Fluorobiphenyl 903.58
mg/kg wet 3.992 40-140Surrogate: 2-Bromonaphthalene 883.50
LCS Dup (P5C0258-BSD1)Prepared: 03/16/15 Analyzed: 03/17/15
C9-C18 Aliphatics mg/kg wet35.4 10 60.00 5040-14059 9
C19-C36 Aliphatics mg/kg wet69.1 10 80.00 5040-14086 11
C11-C22 Aromatics mg/kg wet15210 170.0 5040-14090 4
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 841.68
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 821.65
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 903.59
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 843.35
Matrix Spike (P5C0258-MS1)Prepared: 03/16/15 Analyzed: 03/17/15 Source: 5030255-11
C9-C18 Aliphatics mg/kg dry56.5 14 82.94 7.11 40-14060
C19-C36 Aliphatics mg/kg dry11514 110.6 5.39 40-14099
C11-C22 Aromatics mg/kg dry20514 235.0 BRL 40-14087
mg/kg dry 2.765 40-140Surrogate: 1-Chlorooctadecane 962.64
mg/kg dry 2.765 40-140Surrogate: o-Terphenyl 802.21
mg/kg dry 5.529 40-140Surrogate: 2-Fluorobiphenyl 844.65
mg/kg dry 5.529 40-140Surrogate: 2-Bromonaphthalene 754.14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 75 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P5C0258 - 3546
Matrix Spike Dup (P5C0258-MSD1)Prepared: 03/16/15 Analyzed: 03/17/15 Source: 5030255-11
C9-C18 Aliphatics mg/kg dry53.2 14 82.85 7.11 5040-14056 6
C19-C36 Aliphatics mg/kg dry11814 110.5 5.39 5040-140102 2
C11-C22 Aromatics mg/kg dry22914 234.8 BRL 5040-14098 11
mg/kg dry 2.762 40-140Surrogate: 1-Chlorooctadecane 792.19
mg/kg dry 2.762 40-140Surrogate: o-Terphenyl 902.49
mg/kg dry 5.524 40-140Surrogate: 2-Fluorobiphenyl 1005.50
mg/kg dry 5.524 40-140Surrogate: 2-Bromonaphthalene 965.32
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 76 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Diesel Range Organics by GC/FID - Quality Control
Batch P5C0282 - 3546
Blank (P5C0282-BLK1)Prepared: 03/17/15 Analyzed: 03/18/15
Diesel Range Organics mg/kg wetBRL7.0
mg/kg wet 1.333 49-124Surrogate: o-Terphenyl 670.888
LCS (P5C0282-BS1)Prepared: 03/17/15 Analyzed: 03/18/15
Diesel Range Organics mg/kg wet56.2 7.0 66.62 55-10984
mg/kg wet 1.332 49-124Surrogate: o-Terphenyl 1031.37
LCS Dup (P5C0282-BSD1)Prepared: 03/17/15 Analyzed: 03/19/15
Diesel Range Organics mg/kg wet54.8 7.0 66.64 2055-10982 2
mg/kg wet 1.333 49-124Surrogate: o-Terphenyl 1021.37
Matrix Spike (P5C0282-MS1)Prepared: 03/17/15 Analyzed: 03/19/15 Source: 5030255-12
Diesel Range Organics mg/kg dry10910 94.97 36.5 50-11777
mg/kg dry 1.899 49-124Surrogate: o-Terphenyl 1122.12
Matrix Spike Dup (P5C0282-MSD1)Prepared: 03/17/15 Analyzed: 03/19/15 Source: 5030255-12
Diesel Range Organics mg/kg dry10610 94.90 36.5 2450-11773 3
mg/kg dry 1.898 49-124Surrogate: o-Terphenyl 1182.23
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 77 of 82
3/20/15
Level II QC Report
231 Haywood Street
Project: Burnsville HosieryAltamont Environmental Inc
Asheville, NC 28801
Attn: Mike Falknor
Prism Work Order: 5030255
Time Submitted: 3/13/2015 1:45:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P5C0289 - Solids, Dry Weight
Blank (P5C0289-BLK1)Prepared & Analyzed: 03/17/15
% Solids % by Weight1000.100
Duplicate (P5C0289-DUP2)Prepared & Analyzed: 03/17/15 Source: 5030255-04
% Solids % by Weight68.4 0.100 67.9 200.7
Duplicate (P5C0289-DUP3)Prepared & Analyzed: 03/17/15 Source: 5030255-13
% Solids % by Weight73.1 0.100 72.5 200.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 78 of 82
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5C02825030255-12 03/17/15 15:2030.02 1g mL
P5C02825030255-13 03/17/15 15:2030.01 1g mL
P5C02825030255-14 03/17/15 15:20301gmL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5C02585030255-01 03/16/15 14:00102gmL
P5C02585030255-02 03/16/15 14:0010.03 2g mL
P5C02585030255-03 03/16/15 14:0010.03 2g mL
P5C02585030255-04 03/16/15 14:00102gmL
P5C02585030255-05 03/16/15 14:0010.04 2g mL
P5C02585030255-06 03/16/15 14:0010.01 2g mL
P5C02585030255-07 03/16/15 14:0010.02 2g mL
P5C02585030255-08 03/16/15 14:00102gmL
P5C02585030255-09 03/16/15 14:00102gmL
P5C02585030255-10 03/16/15 14:00102gmL
P5C02585030255-11 03/16/15 14:00102gmL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P5C02845030255-12 03/17/15 15:105.51 5g mL
P5C02845030255-13 03/17/15 15:107.12 5g mL
P5C02845030255-14 03/17/15 15:106.14 5g mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P5C02895030255-01 03/17/15 17:103030gg
P5C02895030255-02 03/17/15 17:103030gg
P5C02895030255-03 03/17/15 17:103030gg
P5C02895030255-04 03/17/15 17:103030gg
P5C02895030255-05 03/17/15 17:103030gg
P5C02895030255-06 03/17/15 17:103030gg
P5C02895030255-07 03/17/15 17:103030gg
P5C02895030255-08 03/17/15 17:103030gg
P5C02895030255-09 03/17/15 17:103030gg
P5C02895030255-10 03/17/15 17:103030gg
P5C02895030255-11 03/17/15 17:103030gg
P5C02895030255-12 03/17/15 17:103030gg
P5C02895030255-13 03/17/15 17:103030gg
P5C02895030255-14 03/17/15 17:103030gg
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5C02645030255-01 03/17/15 9:4530.02 1g mL
P5C02645030255-02 03/17/15 9:4530.06 1g mL
P5C02645030255-03 03/17/15 9:4530.03 1g mL
P5C02645030255-04 03/17/15 9:4530.04 1g mL
P5C02645030255-05 03/17/15 9:4530.02 1g mL
P5C02645030255-06 03/17/15 9:4530.04 1g mL
P5C02645030255-07 03/17/15 9:45301gmL
P5C02645030255-08 03/17/15 9:4530.07 1g mL
P5C02645030255-09 03/17/15 9:4530.04 1g mL
P5C02645030255-10 03/17/15 9:4530.01 1g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 79 of 82
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P5C02645030255-11 03/17/15 9:4530.06 1g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P5C02625030255-01 03/16/15 13:275.6 5g mL
P5C02625030255-02 03/16/15 13:275.83 5g mL
P5C02625030255-03 03/16/15 13:275.91 5g mL
P5C02625030255-04 03/16/15 13:275.31 5g mL
P5C02625030255-05 03/16/15 13:276.08 5g mL
P5C02625030255-06 03/16/15 13:275.84 5g mL
P5C02625030255-07 03/16/15 13:275.83 5g mL
P5C02875030255-08 03/17/15 15:425.18 5g mL
P5C02875030255-09 03/17/15 15:425.73 5g mL
P5C03005030255-10 03/18/15 9:105.77 5g mL
P5C02875030255-11 03/17/15 15:426.47 5g mL
Prep Method: MADEP VPH (S)
Lab Number Batch Date/TimeInitialFinal
P5C03035030255-01 03/18/15 14:425.48 16g mL
P5C03035030255-02 03/18/15 14:426.11 16g mL
P5C03035030255-03 03/18/15 14:426.11 16g mL
P5C03035030255-04 03/18/15 14:426.54 16g mL
P5C03035030255-05 03/18/15 14:426.21 16g mL
P5C03035030255-06 03/18/15 14:425.17 16g mL
P5C03035030255-07 03/18/15 14:425.09 16g mL
P5C03035030255-08 03/18/15 14:425.44 16g mL
P5C03035030255-09 03/18/15 14:425.43 16g mL
P5C03035030255-10 03/18/15 14:425.19 16g mL
P5C03035030255-11 03/18/15 14:425.96 16g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 80 of 82
Page 81 of 82
Page 82 of 82

APPENDIX D

April 2015 Laboratory Analytical Report and Chain-of-Custody
Form

#=CL#
April 14, 2015
LIMS USE: FR - MIKE FALKNOR
LIMS OBJECT ID: 92244169
92244169
Project:
Pace Project No.:
RE:
Mr. Mike Falknor
Altamont Environmental
231 Haywood Street
Asheville, NC 28806
Burnsville Hosiery Mill 4/7
Dear Mr. Falknor:
Enclosed are the analytical results for sample(s) received by the laboratory on April 07, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 12
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 12
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92244169001 TP-2-B1A MADEP EPH 7 PASI-CSWB
MADEP VPH 5 PASI-CBFW
ASTM D2974-87 1 PASI-CEJK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
Sample: TP-2-B1A Lab ID: 92244169001 Collected: 04/07/15 09:48 Received: 04/07/15 10:36 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)169 mg/kg 04/14/15 14:45 N204/09/15 11:0057.4 4
Aliphatic (C19-C36)ND mg/kg 04/14/15 14:45 N204/09/15 11:0057.4 4
Aromatic (C11-C22)ND mg/kg 04/14/15 13:07 N204/09/15 11:0014.4 1
Surrogates
Nonatriacontane (S)86 %04/14/15 14:45 7194-86-704/09/15 11:0040-140 4
o-Terphenyl (S)75 %04/14/15 13:07 84-15-104/09/15 11:0040-140 1
2-Fluorobiphenyl (S)75 %04/14/15 13:07 321-60-804/09/15 11:0040-140 1
2-Bromonaphthalene (S)60 %04/14/15 13:07 580-13-204/09/15 11:0040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/09/15 01:30 N204/08/15 13:473.6 1
Aliphatic (C09-C12)ND mg/kg 04/09/15 01:30 N204/08/15 13:473.6 1
Aromatic (C09-C10)ND mg/kg 04/09/15 01:30 N204/08/15 13:473.6 1
Surrogates
4-Bromofluorobenzene (FID) (S)99 %04/09/15 01:30 460-00-404/08/15 13:4770-130 1
4-Bromofluorobenzene (PID) (S)94 %04/09/15 01:30 460-00-404/08/15 13:4770-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 30.4 %04/09/15 18:530.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/14/2015 05:01 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/9175
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples: 92244169001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1429355
Associated Lab Samples:92244169001
Matrix: Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N204/08/15 22:25
Aliphatic (C09-C12)mg/kg ND 2.5 N204/08/15 22:25
Aromatic (C09-C10)mg/kg ND 2.5 N204/08/15 22:25
4-Bromofluorobenzene (FID) (S)%100 70-130 04/08/15 22:25
4-Bromofluorobenzene (PID) (S)%95 70-130 04/08/15 22:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1429356LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1429357
Aliphatic (C05-C08)mg/kg 12.2 N2158170-1308212.3 1 25
Aliphatic (C09-C12)mg/kg 12.0 N2158030-1308412.6 5 25
Aromatic (C09-C10)mg/kg 4.2 N258370-130844.2 1 25
4-Bromofluorobenzene (FID) (S)%101 70-130100
4-Bromofluorobenzene (PID) (S)%98 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/14/2015 05:01 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/34132
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples: 92244169001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1430402
Associated Lab Samples:92244169001
Matrix: Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N204/13/15 10:49
Aliphatic (C19-C36)mg/kg ND 10.0 N204/13/15 10:49
Aromatic (C11-C22)mg/kg ND 10.0 N204/13/15 10:49
2-Bromonaphthalene (S)%69 40-140 04/13/15 10:49
2-Fluorobiphenyl (S)%81 40-140 04/13/15 10:49
Nonatriacontane (S)%72 40-140 04/13/15 10:49
o-Terphenyl (S)%78 40-140 04/13/15 10:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1430403LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1430404
Aliphatic (C09-C18)mg/kg ND N2108840-14083ND 50
Aliphatic (C19-C36)mg/kg 10.6 N213.3 79 40-1407710.3 3 50
Aromatic (C11-C22)mg/kg 19.5 N228.3 69 40-1408323.5 19 50
2-Bromonaphthalene (S)%42 40-14044
2-Fluorobiphenyl (S)%72 40-14084
Nonatriacontane (S)%83 40-14079
o-Terphenyl (S)%79 40-14091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/14/2015 05:01 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7711
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92244169001
Parameter Units
Dup
Result QualifiersRPDResult
92244169001
1430542SAMPLE DUPLICATE:
Percent Moisture %27.2 1130.4
Parameter Units
Dup
Result QualifiersRPDResult
92244477003
1430543SAMPLE DUPLICATE:
Percent Moisture %11.5 239.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/14/2015 05:01 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 12
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The lab does not hold TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/14/2015 05:01 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 12
#=MEXR
METHOD CROSS REFERENCE TABLE
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
Parameter Matrix Preparation MethodAnalytical Method
MADEP EPH NC Soil Solid MADEP, May 2004, Rev. 1.1 MADEP, May 2004, Rev. 1.1
Percent Moisture Solid ASTM D2974-87 N/A
VPH NC Soil Solid MADEP, May 2004, Rev. 1.1 MADEP, May 2004, Rev. 1.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 12
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92244169
Burnsville Hosiery Mill 4/7
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92244169001 OEXT/34132 GCSV/20941TP-2-B1A MADEP EPH MADEP EPH
92244169001 GCV/9175 GCV/9180TP-2-B1A MADEP VPH MADEP VPH
92244169001 PMST/7711TP-2-B1A ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/14/2015 05:01 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 12
Page 11 of 12
Page 12 of 12

APPENDIX E

Waste Disposal Manifests