Loading...
HomeMy WebLinkAboutBoxmeer_Amended Comp Site Assessment 10-27-94Coopnn Exvtnoxrunxrtt ENGINEERS . GEOLOGISTS o SCIENTISTS AIVITNDED COMPRTHTNSI1IE SITE ASSESSMENT RIPORT sToRK SCREENS AMERTCA, INC. CEI PROJECT No.94147 ocToBER 1994 C oop n n E r,tw noN MELITAT ENGINEERS . GEOLOGISTS . SCIENTISTS October 27, 1994 Mr. Allen Schiff Norttr Carolina Department of Environment, Health, and Natural Resources 919 North Main Street Mooresville, North Carolina 28115 RE: Amended Comprehensive Site Assessment Stork Screens Arrrerica, Inc. 32Ol North I-85 Charlotte, North Carolina 28213 Dear Mr. Sctriff: Please find attached an Amended Comprehensive Site Assessment Report for Stork Screens America, [nc. Should you have any questions please contact me at l704l845-2OOO. Sincerely, G(XIPER. ETVTRONIIEIITAr,, ItrC. /a /a Michael S. Crouch Hydrogcologrst MSC\kab\mcI 23OO SARDIS ROAD NORT.H O SWTE Q CHARLOTTE, NORTH CAROUNA ' 28227 QAq 8$-2000. FAX (7oq e4t-8901 AMENDED COMPREHENSTIIE SITE ASSESSMENT REPORT Stork Screens America Lrc. 320L N-I-85 Charlotte, North Carolina 282L3 CEI Project No. 94147 Ground Water Incident # 11398 Prepared for: Stork Screens America Inc. 320t N-r85 Charlotte, North Carolina 282L3 Prepared by: cooPER ENITTRoNMENTAL, II[C. 2300 Sardis Road North, Suite Q Charlotte, North Carolina 28227 AMENDED COMPREHENSTVE SITE ASSESSMENT Stork Screens America Inc. 3201 N-r85 Charlotte, North Carolina CEI Project No. 94147 This report was prepared by COOPTR EIWIRONMTNTAL' INC. /o- *-r , John T. Burkart Project Manager Ttris work was prepared under the responsible charge of: President Norttr Carolina Licensed Engineer No. 16562 rU- st-cr - Date AJh. z-f rtf/ AL Y{a NC TABLE OF CONTENTS 1.O E'(ECUTNIESI'MMARY 2.O INTRODUSrION 2.1 Rrrpose 2.2 Scope of Work BACKGROI'ND II{FORMATION 3.1 Site Description and Location 3.2 Site Topography and Surface Water Features 3.3 Previous Investigation 3.4 Utility Sunzey 3.5 Water Supply Well Sunrey 3.6 Potential Contamination Source Inventory 3.7 Property Ownership and Land Use 3.8 Potential Receptors and Migration Pathways PROJECT FIITDINGS 4.L Regional Geolory 4.2 Site Geolory 4.3 Soil Sample Analytical Results 4.4 RegionalHydrogeolory 4.5 Site Hydrogeolory 4.5.1 Occurrence of Ground Water 4.5.2 Ground Water Flow Direction 4.6 Ground Water Analytical Results 2 2 3 3.O 4.O 3 3 4 4 5 5 6 6 6 7 7 7 8 9 10 10 l0 11 L2 13 13 5.O CONCLUSTONS 6.0 RECOMMEITDATIOITS 7.O RTFERTNCES TABLES TABLE I. SPATCO Soil and Ground Water Analyticat Results TABLE II. Soil Analytical Results TABLE III. Ground Water Elevation Data TABLE IV. Summary of Ground Water Analytical Results FIGIIRTS FIGURE 1. General Site Location Map FIGURE 2. Site Location Map FIGURE 3. GeoProbe Location Map FIGURE 4. Utility Location Map FIGURE 5. Cross Section Transect A-A'(Unsaturated Zonel FIGURE 6. Cross Section A-A' FIGURE 7. Soil Boring Map FIGURE 8 Monitoring Well Location Map FIGURE 9 Ground Water Equipotential Map FIGURE 10. Total Volatiles Isoconcentration Map APPEI{DICES APPENDIX I. SPATCO Environmental Preliminary Site Assessment APPENDIX II. Initial Site Characterization Map APPENDIX III. Water Supply Well Survey APPENDX IV. Well Construction Records APPENDIX V. Soil Boring Logs APPENDX VI. Soil Analytical Results APPENDIX VII. CEI's Anatytical Data - Ground Water 1.O E'(ECUTTIfE SI'IIMARY The following summary provides background information concerning Stork Screens America, Inc. SPATCO Environmental completed a Tank Closure Report dated October 25, lggs and a Preliminary Site Assessment dated April 78, 1994 for Stork Screens America, Inc. The reports provided information on the removal of one I,OOO gallon oil/water separator and one 550 gallon waste oil underground storage tank (UST). SPATCO collected soil samples from beneath the UST and from beneath the oil/water separator. SPATCO, in conjunction with the UST soil sa:rrpling, collected six GeoProbe@ samples and installed one Ilpe II monitoring well, labeled MVV-I. The amount of arry release from the USf or from the oilf water separator is unlmown Laboratory analysis of the soil samples collected by tJ:e geoprobes and the installation of the monitoring well identi{ied concentrations of oil & grease, l,L dichloroetJrene, ethylbenzene, methylene chloride, tetrachloroethene, 1,1,1 trichloroethane, 1,1,2 trichloroethene and total:rylenes. SPATCO collected one ground water quality sample from monitoring well MW-l. The aaalytical report indicated several volatile organic compounds and chrornium were present. Stork along with SPATCO submitted the report on or about April 18, 1994. On June 22, 1994 the North Carolina Department of Environment, Health and Natural Resources (NCDEHNR) issued a Notice of Violation (NOV) to Stork Screens America, Lrc. (Stork). The NOV requested Stork submit a water well sunrey and complete an Initiaf Site Characterization Report. Cooper Environmental, Inc. (CEI) submitted the water well survey report on July L4, L994 and the Initial Site Characterization Report (ISCR) on August L2, 1994. CEI began the Comprehensive Site Assessment (CSA) on August 12, 1994, and a report was submitted to DEHNR on September 7, L994. CEI proposed a schedule to further delineate the extent of impacted ground water that was observed in previous reports. CEI followed that schedule and will present the additional freld information obtained from the installation of three shallow monitoring wells and one vertical extent monitoring well. 2.O Based on the investigation, the hydrocarbon impact appears to be losalized around the former UST location. Hydrocarbons were detected in only MW-l. The area impacted by chromium is larger than that of the hydrocarbon plume, but also appears to be localtzed to the UST area. The presence of chlorinated volatile organics in soil and or ground water samples collected from MW-2, MW-6 and VE-l indicate the chlorinated volatiles migrated from the potential source area but are generally delineated. On this basis, CEI recourmends preparation of a corrective action plan. IT{TRODUCTION The following sections summarize the purpose and scope of work conducted by Cooper Environmental, Inc. (CEI) at Stork Screens American (Stork) located at 3201. I-85 Charlotte, North Carolina. 2.1 Purpose On September 14, 1994, Stork retained CEI to conduct an Amended Comprehensive Site Assessment (CSA) for their Charlotte facility. Ttre purpose of the Amended CSA is to determine the extent and magnitude of volatile orgarric compounds and inorganic chemicals in the subsurface soil and ground water, possibly resulting from Stork's operation and use of an underground storage tank (UST); to identiff potential receptors and migration pathways; to propose preliminary corrective actions to mitigate the effects of the compounds in the subsurface; and to reduce risks to potential receptors. This report has been prepared for submission to the North Carolina Department of Environment, Health, and Nahrral Resources (DEHNR) in accordance urit.l- guidelines issued by that agency in March 1993; (updated June 1993) Norttt Carolina Administrative Code Tifle 15A, Subchapter 2L, which was arnended November 1, 1993; and a DEHNR policy guidance dated September 2, 1993. O 2.2 Scope of Work To date, the scope of work for this project included: o Collection of background information from existing reports and other sources; o Evaluation of existing data; . Advancement and logging of ten soil borings; o Collection of soil samples from soil borings for the purpose of freld screening and development of analytical results; o Installation of five shallow monitor wells; o Installation of one vertical extent (deep) monitoring well; o Collection of water level data from five shallow monitoring wells, one water supply well, and one vertical extent (deep) monitoring well; r Closure of one water supply well; o Reconnaissance for water supply wells, and other potential contarninant sources located within 1500 feet of the site; and a . Preparation of the Comprehensive Site Assessment Report 3.O BACKGROI'NDINTORMATIO$ The following sub-sections provid.e background. information for the project and project site. 3.1 Site Description and Location Stork Screens America Inc. is a manufacturing facility located at 32Ol l- 85 in Charlotte, North Carolina, at latitude 35o 16' 18" north and longitude 80o 49' 26" west. Charlotte is located in Mecklenburg Count5r, which is situated in the south-central area of the state. Figure 1 depicts tJle general site location. Figure 2 includes an exce{pt of the Derita 7.5 minute USGS topographic map illustrating the site in greater detail. Land use around the site is a mix of both residential and commercial. Commercial ventures in the vicinity of the site were addressed in the Initial Site Characterization Report. 3.2 Site Topogaphy and Surface Water Features As shown in the topographic location map (Figure 2), the site is at an altitude of approximately 73O feet above mean sea level. Local topographic relief is approximately 50 feet between ridge tops and stream valleys. CEI reviewed the topographic map for the area and noted that a water impounclment is located approximately 1,000 feet to tJ:e north of the Stork Screens property. This water impoundment is used for possible storm water nrnoff. Ground water of North Carolina are classified as Class C or higher by 15A NCAC 28 .O2LL. The best usage for Class C waters is reported by this regulation to be fishing, secondar5r recreation, agriculture, and any other usage except primary recreation or as a source of water supply for drinking, culinar5r, or food processing purposes. CEI observed that an intermittent branch of Irwin Creek originates at tJ:e impoundment and flows southeast from the impoundment towards hwin Creek. Irwin Creek flows southwest from the area and enters Sugar Creek. Sugar Creek flows southward, artd evenhrally empties into the Catawba River north of Fort Mill, South Carolina. Other than the Catawba River, CEI is unaware of these surface waters being used for a supply of potable water. 3.3 Previous Investieations CEI is aware of previous environmental investigations performed by SPATCO Environmental (SPATCO). SPATCO apparently completed five GeoProbe@ soil samples, around a former UST. These samples were designated GO-2 through GO-6. SPATCO obtained two deeper samples from the GO-4 location at depths ranging from 24 feet to 35 feet below grade level (BGL). Ttre locations of the borings are indicated in Figure 3. SPATCO apparently analped the soil sarrrples for oil and grease (EPA Method 9071) and volatile orgarrics (EPA Method 8021). Appendix I provides a copy of the April 18, 199+ SPATCO PSA Report. SPATCO installed one monitoring well labeled MW-l to a depth of 5O feet below land surface (BLS). The monitoring well was placed in the former UST 3.4 basin. Section 3.5.1 describes the installation and Figure 8 illustrates the monitoring well location. SPATCO submitted the samples to EnviroTech Mid-Atlantic Inc. Table 1 summarizes soil and ground water analytical results from the sampling events performed by SPATCO. CEI completed an Initial Site Characterization Report and submitted the required information to NCDEHNR on August L2, L994. Appendix II provides a copy of the Initial Site Characteizatron Report. CEI submitted an initial Comprehensive Site Assessment Report dated September 7, L994. This report represents an arnended version of the original CSA. utiliw Survev Underground utilities were identified by Stork and CEI prior to site drilling activities. Ttre locations of identified utilities are noted in Figure 4. The area is served by a municipal water supply system. Most businesses and residences appear to be connected to this system. Ground water occurs at depths greater than tl:e Brpical depth of underground utilities. As discussed in sub-section 3.5.1, ground water occurs at depths ranging from approximately 28 to 3O feet below grade level (BGL). Underground utilities are typically located less than 5 feet below grade. Tfterefore, it is unlikely that underground utilities act as preferential ground water migration pathways. 3.5 Water Supplv Well Surrev Areas along streets within 1,500 feet of the site were reconnoitered for the presence of water supply wells. CEI did identi$ water supply wells during the reconnaissance. We reported their locations in a water supply well survey that CEI submitted to NCDEHNR. Appendix III provides a copy of the water supply well sunrey in addition to the lnitial Site Characterization Report. 5 3.6 Potential Contamination Source Inventory CEI conducted a reconnaissance to identify potential contamination sources within 1,500 feet of the site. CEI identifred one potential conta:mination source within 1,500 feet of the site. A Shell Service Station located to the east of Stork Screen America, Inc. was identified along the I-85 service road. CEI did not observe monitoring wells at the retail gasoline site, which tlryically indicate a reported release. 3.7 Propertv Ownership and Use lhe current property owner is Stork Screens America, Inc. The property is surrounded by commercial business to the west and northwest of the site. To the South Leterstate I-85 adjoins the property. IGrights Inn is located to the north of the property. A Shell retail gasoline outlet and Bradleys' Diesel Truck Service are located to the west. a 3.8 Potential Receptors and Mieration Pathwavg CEI completed an area reconnaissance and noted the surrounding properties. CEI noted the primary use is commercial and industrial, howe\rer, nrithin the limits of the 1,500 foot radius CEI noted several water supply wells. CEI reported the location of these water supply wells in a report submitted July t4, L994. CEI identified a water supply well on the Stork property. CEI directed Air DriUing Co. to abandon the water supply well on October 7, 1994 in accordance with DEM guidelines. Air Dri[ing Co. sealed the well with 33 bags of cement mixed with 198 gallons of water. Air Driling Company submitted to DEHNR a well abandonment record detailing these activities. Appendix IV provides a copy of tl:e well constmction records and a copy of the well abandonment form. A1l other supply wells identified in the supply well reconnaissance are near the perimeter of the 1500 foot radius area and do not appear to be in the direction of ground water flow. Additionally, it is possible that an intermittent branch of Irwin Creek may be a ground water discharge zo,Ie. 6 Ground water measurements collected at the site indicate that the depttr of ground water is 30 feet below land surface (BLS). CEI does not believe that artificial migratory pathways are present since most utility lines are five to seven feet BLS. 4.O PROJECT FINDINGS The sections that follow summarize project findings. Generally accepted methods and procedures were used during the investigation. 4.1 Resional Geoloqv The geologlc map of North Carolina (North Carolina Geologic Sunrey, 19SS) indicates that the site lies within the Charlotte geologic belt. The bedrock in the Charlotte area is described as biotite gneiss and schists. T?re gneiss and schist are massive to strongly foliated and can contain abundant amounts of potassic feldspar and garnet. The gneiss and schist of th,e Charlotte Belt are often interlayered with, and can also exhibit, a grading into calc-silicate rocks, sillimanite rocks, sillimanite-mica schist, mica schist, and amphibolite. Small masses of quartzite can also be found within the biotite, gneiss and schist of the Charlotte Belt. Intrusive rocks associated with the gneiss and schists are granite and diorite (North Carolina Geologic Sunrey, 1e8s). 4.2 Site Geoloerv CEI characterized the subsurface soil based on the information obtained during the field loggrng of ten soil borings. CEI has included tl:e soil boring logs as Appendix V. The SPATCO monitoring well log is attached to their report. CEI utilized the available boring logs to prepare a cross section describing soil characteristics in the unsahrrated zone. Figure 5 illustrates the location of cross section A-A', while Figures 6 shows the cross section. , CEI used the Unified Soil Classification System (USCS) to classiff the subsurface soils and prepare the cross section. As illustrated in the cross section, the subsurface material typicaliy consists of reddish orange to reddish yellow silts and clays. 4.3 Soil Sample Collection and Analvtical Results Soil samples were collected with a split spoon sampler continuously for the two monitoring wells and every five feet for the soil borings to their terminus. CEI split the soil core, placing approximately one-half of the sanple in a resealable plastic bag to be field screened, while the replicate sample was placed in a laboratory prepared soil jar in preparation for laboratory shipment. CEI allowed the screening soil samples to remain undisturbed and out of direct sunlight for approximately 1O minutes. CEI used the field screening results to select a soil sample from each boring for laboratory analysis. Soil samples prepared for laboratory analysis vrere placed in a cooler pre-chilled te approximately 4 C. CEI submitted soil samples from directly above tl:e apparent water table for laboratory analysis of total petroleum hydrocarbons (TPH) by EPA Method 3550/503O, hexavalent chromium by Method 7L96 and for oil and grease by Method 9071. TPH and chromium levels were below detectable concentrations for all borings. Soil samples from soil borings SB-2, SB-3 SB-4, SB-5, 5B-6, SB-7, and SB-8 were reported to be below quantification limits for oil and grease. Soil samples collected for soil borings SB-9, SB-10 and SB-11 indicated concentrations of oil and grease at 190 ppm (30J,27O ppm (10') and 260 ppm (30), 150 ppm (15) and 180 ppm (30), respectively. The action level for oil and grease is 250 ppm however, CEI believes the concentrations detected are false positives from organics naturally found in the soil. Table II summarizes the results. Appendix VI provides a copy of the soil analytical results from SB-9, SB-10 and SB-11. CEI installed SB-2/MW-2 in a upgradient location of tl,-e UST area, between soil borings SB-3 and the northern property boundary. Sam.ples collected from soil boring SB-2 exhibited the highest PID readings of the soil sqmples collected and analyzed. Figure 7 illustrates the soil boring locations. Ttre soil borings were converted to monitoring wells completed as follows: SB- 8 2/MW-2, SB-7/MW-3, SB-9/MW-4, SB-10/MW-5, and SB-11/MW-6. The vertical extent well was drilled next to the soil boring labeled SB-3. 4.4 Reeional Hvdroeeolos/ Ttre site lies within the Piedmont water region (Heath, 1983). The water bearing system consists of fractured crystalline and metamorphic rocks overlain by a veneer of regolith typically ranging in thickness from l0 to 20 meters. Water is present in pore space in the regolith and in fractures in the bedrock. The regolith is typically low yielding and water supply wells within the regolith are generally restricted to large diameter bored wells with high reservoir capacities. The regolith is typically saprolitic in origin, but in many valleys, especially those of larger streams, alluvial deposits may be found. The regolith contains water in pore space between soil grains. The underlying bedrock does not have signi{icant intergranular porosity. Water in bedrock is contained within openings along fractures. Because of the significant dilference in porosity between the regolith and the bedrock, the regolith is often viewed as a ground water resenroir and fractures in bedrock as ground water pipelines. The yields of wells completed into bedrock depends on tJre size, frequency, and interconnectiveness of bedrock fractures, as well as ground water replenishment from the overlying regolith. The elevation of the top of the ground water surface in the region is typically at its lowest seasonal level during the fall. Ground water levels tJrpically rise in response to recharge from winter precipitation and decreased wapotranspiration, until its maximum level is reached in the eady spring. Ground water levels then decline until the fall due to an increase in evapotranspiration. Although monthly mean precipitation is t;pically at a maximum during the surtmer, ground water levels still decline because anapotranspiration exceeds the recharge available to ground water from precipitation. I 4.5 Site Hvdrogeoloqv This section describes site hydrogeolory including the occurrence of ground water and ground water flow direction. 4.5.1 Occurrence of Ground Water There are currently six shallow monitor wells (MW-1 through MW-6) and one vertical extent monitoring well VE-l completed in the unconsolidated materials at the site. Figure 8 illustrates the well locations. Copies of the well completion records are included as Appendix IV. Ground water elevation data has been tabulated and is presented in Table III. Ground water occurs in the unconsolidated materials at depths ranging from approximately 28 to 3O feet below land surface. Bedrock is encountered at 65 feet below land surface. Therefore, CEI has installed monitoring wells throughout the upper ground water system. 4.5.2 Ground Water Flow Direction CEI suneyed the elevation of the top of casing for each monitoring well relative to the sewer manhole at the facility. The location of this manhole is shown on Figure 4. The finished {loor elevation was assumed to be LOO feet as a temporary benchmark. The water table elevations range from 71.88 feet to 61.90 feet. CEI collected readings of depth to water from each monitoring well on July 26, L994, August 12, L994 and September 22, 1994. CEI has prepared a potentiometric map (Figure 9) from the September 22, 1994 data, which illustrates a southeastwardly ground water trend. The southeastwardly trend is toward I-85Interstate Highway. CEI prepared the ground water potentiometric map, presented as Figure 9, using data from September L994. As shown in Figure 9, the inferred ground water flow direction is to the southeast. Since the individual hydrograph lines for each monitor well approximately parallels one another, the ground water flow direction remains constant. 10 Using data collected from soil borings, ground water level gauging, and publication, CEI calculated the average linear ground water flow velocities. Fetter (1993) defines average linear ground water flow velocity as the rate at which water moves through pore spaces. Average linear ground water velocity (V) can be calculated by the following formula: =[** E"^tn, 1983)ndt where, K is hydraulic conductivity; n is porosity; and dh/dl is hydraulic gradient. Ttre following input values were utilized to solve the equation: K=5.4 x 10'g ftlday (research data) n=0.45 (reasonable value for silts and clays,Freeze and Cherry, L9791 dh/dl=0.O11 ftlft Calculated average linear ground water flow velocities using tllis input data are as follows: _5.4x10-' fr ldsy 0.45 These calculated values for ground water flow velocity should be viewed as approximations that are limited to site specific hydraulic and physical parameters that may be influenced by numerolls factors. Actual waste constituent migration rates may vary due to each individual chemical's solubility, attenuation, dispersion, retardation, diftrsion and other characteristics. Ground Water Analvtical Results Monitoring well MW-l was sampled in March 1994 by SPATCO. The sample was analyzed for acid/base neutral-extractables (EPA Method 625l., volatile organics (EPA Method 624l. and RCRA Metals. The results are summarized in Table l. A total benzene, toluene, :iqrlene, and ethylbetvrune *.011fr1fi=.005frlyear 4.6 11 (BTEX) concentration of 282 ppb was indicated, however all BTEX compounds were below the NCAC 2L standards except ethylbenzene (32 pg/l) which was slighfly above tJ:e standard of 29 pg/|. Additionally, the SPATCO analysis indicated tJre presence of several chlorinated compounds and RCRA metals (principafly chromium) above t}:e 2L standards in MW-l. CEI resampled MW-l on July 26, 1994 to confirm the presence of chromium. The presence of trivalent and hexavalent chromium was confirmed. CEI sampled monitoring wells MW-2 and MW-3 and supply well PW- 1 on August L2, Lgg4. Wells MW-4, MW-s, MW-6 and VE-l were sampled on September 26, 1994. AIl samples were xralyzed by EPA Method 6Al /602, EPA Method 625 and for trivalent and hexavalent chromium. Table IV surnrnarizes the analytical results and Appendix VII contains the laboratory reports. Ttre results show volatile organic compounds in MW-2, MW-6 and VE-l above the NCAC 2L standards. Only tetrachlorethene (PCE or Perc) (38 ttg/ll and chloroform (7.5 pg/l) were detected above tl:e standard of .7 1tgll. and .L9 1tgll, respectively in M\M-6. In the deep well (VE-I), only tetrachlorethene 0.a pg/l1 and chloroform (4.3 pg/l) were detected above the standard. Figure 10 illustrates the total volatile plume configuration. Chromium was detected above the NCAC 2L standard of 50 pg/l in MW- 2 (188 pg/l), MW4 (125 pglI), and MW-s 152 yrg/ll. Hexavalent chromiufi. was not detected in MW-4, MW-s, or MW-6. It was detected at 30 pg/lin VE-l and was not anal5'zed in MW-2 and MW-3. 5.O CONCLUSIONS CEI has reviewed SPATCO Environmental's April 18, 1994 report and has conducted its own site assessment at Stork Screens America, lnc.'s Charlotte, North Carolina facility. CEI has concluded that several organic compounds are above NCDEHNR 2L limits. A sample from MW-l contained constihrents above the 2L standards for chloroforrn, 1,1-dichloretfrene, ethylbenzene, methyelene chloride, tetrachlorethene, trichloroethene, calcium, chromium, lead and mercury. The MW-2 sarnple contained 1,1-dichloroethene, 1,l-dichlorethane, 1,1,l-trichloroethane, tetrachloroethene and chromium above the 2L standard. t2 The horizontal and vertical extent of impact by chlorinated compounds has been generally determined. MW-6 is the downgradient well and contains only PCE and chloroform slightly above the 2L standard. The deep well (VE-l) also contains only PCE and chloroform at levels slightly above the standards. The chromium plume is delineated downgradient of the waste oil tank. S[ghtly elevated concentrations exist upgradient in MW-2, MW-4 and crossgradient in MW-5. 6.0 RTCOMMENDATIONS CEI proposes that Stork proceed to prepare a Corrective Action Plan. 7.O RTFERENCES Cooper Environmental, Inc., August 1994, Initial Site Characterization, Stork Sc-reens America, Inc., Charlotte, North CaroLina, unpub[shed professional report. Fetter, G.W.; 1994 Applied Hydrogeolory, Third Edition; Bell & Howell, Columbus, Ohio. Freeze, R.A. and J.A. Cherry, L979, Groundwater; Prentice-Hall, Ittc., Englewood Cliffs, New Jersey. Ground Water Chemicals Desk Reference, 1990, Lewis hrblisher. Heath, R.L., 1983, Basic Ground-water Hydrolory; U.S. Geological Sunrey Water Supply Paper 2220. Nortlr Carolina Geolory and Mineral Resources, 1976, A Foundation for Progress. North Carolina Geologic M"p, 1985, Department of Nafirral Resources and Community Development. 13 SPATCO Environmental, April 1994, Preliminary Site Assessment, Stork Screen America, Inc., Charlotte, North Carolina, unpublished professional report. JB\clh\jb155 L4 TABLES a otsoH ,!4 ESx-3 oo co o00t- Iom -]o -]om -]om Ioa Jola ii{ ! ot\o o\o(f) Jom Joo Jom -lAo .Iotr Jotr ii;l .loE Jon Ja m Jo m ot e.t$ Joo Joo t i#$F ooct o CO Joo Jno Jotr e{+ Joo Jotr !, $gs Joo t,- Joo JA c0 or o@ Jo ca *loo t He EEa,H o(rr co @ Jotr .1am .1otr Jotrl JAo Joo *€g tE rg Jo m \o Jotr Jotr t:od) Joo Joo Jao u oG E r{ etE ootOIc-l olr0f.- oo otCo ot.ocf) o00 C\I o(o tO !+ gs 1l)ci LOrf)tf,cl tN tC.l o(f)sf C.l tO(\ st ;i I ts c-{ *CIIor! Cf) Iort tIo(l tIo(t roIoa \oIori o+,d t)SB8trEE 1+ S FH iitr Etr =E{ o.g EsgTHb2'5a tOrO -o Jo 0) dJ1 oF TABLE l coatinued SPATCO Environmental Ground Water Sample Results for MW-1 March l, \994 Compound Concentratioa (ug/tl NCAC 2L Ltmtts (ug/tl Benzene BDL I Chloroform 7.8 0.19 1,1-Dichloroethane 33 700 1,1-Dichloroethene 61 7 Ethylbenzene 32 29 Methylene chloride 100 5 Tetrachloroethene t3 o.7 Toluene BDL 1000 I , 1 , l-Trichloroethane 145 200 Trichloroethene 13 2.8 Xylenes 250 530 Cadmium 7 5 Chromium 1,880 50 kad 100 15 Mercury 18 1.1 BDL =BDL = Below detection NE - Not established JTB\kate\CLHjb155 !0I Nb0oqot 11 az az az az az az az aZ az az az o(rr oD-ot o\o(\I oro oo ET FE}oZ o2 oz oz oZ oz oz oz oz oz az az az az az az o8o ;Bu)-G, oz oz oz az oz oz oz oz oz oz oz az az oz o2 oz € €+,Ee,o rOo I o b C-,1 I oo -o CI I Ao F. I tf) t- I ro bcl I oo bc-t I oo bc,l I oo N I b NN I oN Nol I bN b(f)o bc') rO b(f) Eo +,rt(,oq)a Nttra ottma (f) Ima (Y) Ioa tItra +Itra LO Ima \oItra t-Ima NIoa 6Ioa oIoa o Ima Ioa kooP+,H =cl;J (J d-T J€ * fi gg€F E€ T.<k o-=F a O lJ.,E oF +? E, E€.gE u)vd u)8?i*o ':? A iJ.1l r tlAa Yzz g d.t/ot-t rt'oo ;N To c,>.9FH= k(,*,GI F o\o oi\o roOld\o (adF. N \c,\o +,c(, Ee,lrao-rtlEar- Ek(,+,cl B oq Otol to(f, L,-dN roo\ c,(e co .Jd !,-Eg, h0c o(,o @q chor at oio 6t-o \o Cot-o oo coqoo\ eIq oro tcldo No cjo rot F,-o r..o6Ot rfi e{ rri ot(f) 'fi oq \o ri-sf, t- oqt c0q sf o\c! ln to('i (f) r.*rj ocl,)d 6N6 +,co+,d5- E }PEL Cr-Jltor{tFI oqto (t?+o n\(ao $c!\fo +iI o6+ (o + CoF.+ F- OTt- Eo{il.oo(,o o.u€EQA =a;d EB t-kaDA AHa6 EHaol{bI) I tsE bI) odo I B aokbo (v) I ts = bo Hada (o IBE b0Ep ko o C) 9uio.y,r!.LeC)otr boHiU'Er ti (.),dE-P lctraoLh0 e-ltF = b0trod() e-lI F c-{q otor =laF c.lI B ttrao,{u0+I B b0 E al,do+I BtslA t aotrM roI B u0 o(Uo roI tsE f-q \ool lnI B = Itr E- og d>ootr EEE T9d sEfi HE(,)0{ uH Ia EoIcl D0r-H= L(,+,dF Nq \o {c 0, E0,Lao-dci0)- =L(,{JdF oq ro CO !o +,alD(r-Eg t0H odo lotocn oo? @Ol Nt.t-o F.q F-o r{ort.+ toq tr) (f)q \o oq \o a,E!, +, ESeL O-+, ]rao*tEH rOq (f,o F,.o c"io +€ol/) + ro(f) r/i co ar* li(,oq)o o dO. () o o oO o.E dA. oob0Eri ealI caF Eg o!b0 \0I B b0g odo \o I B = Nf.-t-o \oIB (f) ImF P"o (U B (d 0)& _g€I dxd,e .9 99E 6 h'-I .E6Fs iExE fig€e b 9gE (DS B4+(atE6 rO LO 3'i? () o d @Fa r{-A}>3 oz az lo 0,. +(o +u! E c.tto c; (aqo QrEiiE= (f)Az oz @(a ro D..h0 E oz az Uit <E}E :r- oz a2 oz az oz b0 E e.Iroqo oz t-iiiEr. oz Az oz oz (r) cj h0 H l/)e{ ct CI2 rdd EE oz Az Az oz oz h0 oz aZ (Dr*EE=. oz az az Az nz b0 E lost'o az N-B}E3 ooor.- o!r)!i oooOl oN az b0 E 66..:az 6L(,*,t, E(tk nfr o o I0)olio ooI tu (d o o () oIN lu d G)o o () F 0)k C) +)oo o 6L oF L.o oLro O Ea o! o Eot< a I Ho cl dx(.) g Asilo\,iE dtr:Ij F{ffI F{ EE or-{ <t €H 2> Efl gE s8H etP oi.9E drh; frE$ aa Eo *cE!Bf;g H:o o.ozzz[[ll u]frlc/)O dzzz F- o FIGURTS a I e;{ffiOC - Fffi,\ G9.:i l:"Urli ,t,=3 /i ??/lrllo o,m:gru 2 !-r'Ert; oo iaalru i 6,, L$\)t i i rqitliE; E?s.. I ii = \l i{lP3.EX'::€1As t_t^ _: -__NF E:F9dE ij#l 3==S: aF U'I FzlrJo@ aF U1(,oJo1r,(9 oEtrJlr,z6 lrj o. 2o F (JoE: gFu J EfrlztrlU C)2 <.U:E Oa'dr^ez pE rHr,le,roooDNetL&oFo z Jo (J F&oz dFFoJpa j (J oF F z r-: a rOO .{.ol F()lno&o. L f k-- ffi)7/-/-G. ia6;--i_ 'Rt- DERTTA OUADR.A,NGLE NORTH CAROLINA-MECKLENBURG CO. 7.5 MINUTE SERTES GOPOGRAPHTC)fl QUADRANGLE LOCATION ENGINEERS GEOLOGISTS SCIENTISTS STORK SCREENS AI{EBICA 3201 I-85 NORTIT CHARLOTTE. NORTH CAROUNA ECT: 94147 DATE: 10 aFo Fzlr,6a aFo(,o olrJI anEt!Llz fJzll, A. zoF UoFI ETEoEA.o!{I zJoE,QL<iEuo_z* 35tZ *9torNEgJ3 G () Qe ET tnzB] EAEt)o x&o-tn (! r:ie, o f- E ag E3JA6t.=vJA6 ql ;u Efi O. oz6J =o (,z6 5co oL<o ELJ =oo. o oC' € !o(9 a=rE5 t $ r; Dolr U)FU)FzlrJ6a ]nFUI IoJolfJ(, tne.lrju,z(,z UJ 0- 2 zoF oJ FI E-:) z o () F0toz =< !l'e ez e3trI,lEl B8 xEot-a t-. il ::rJ Qa h- o Z>qo:)F@aIYi()oJ@ z d,au Pz_o<r o-o= aaAzrao<f,E0l=-0. o o. rll rlIlt ztY5rl H/ tiq \ \ ts i,Ill _t\H[tltlt & Ez0--I 0. f4 &r =o0. E E v oFm oz F Eo k* .Aa zo E- (JI (,z ololn .toa l,, Itrlv) ozEI(, B u2>qir=o5FCoatN4H(JorJ rEl o .A ln zsx8 384 o io.o= trlooa Jo LtazF<u)*- E s Itrlv) \ frlE- u Itro (D I caU) J T N Itrtt) a o =o't;o -lErIEi =ax<o rtl0tE o-E<oz (D Iaa Io.A a EElE-- (., fLo xl (, Frl FHA aFI(,oJol!o oELJLIz,6zLl t)z 3'=Eii =zp3 Itl *flltll d B8c,x0aoE-v) o o o o6it o oln(, 3(J 5 v) th tsoj frt J() 5 U) v) =oJFIf.l E<*Io EII(J &o zEI ErltrU U aF]JFFo 5 U) >.F] 3L) zr'ltrIEu F u3 HIa frl s tr]uz o azz F{ az tal)-a5a FIF - E-dtn EI sL) trl rnotZmila)o ofrlE pt EI o()trlR oz su 5a trtoz &o otrIE ag E-trE]A. E:oF! Etr p-v) &: --fli FrE<tt6 EF.f,It) .A u) zo E< L)oJ uz&orE -Iotn cc IEac AztrlU E uz>Ec=ODFIDatl.3(,oJa -u- o .Aa z EBFELF384 o io"o=r,lOO ul -lo }4ta2F<v) 1- = Ec] I@v) \ frlLk(J Iaa .+ Itrl.u CD IrEa Ftrl ln IE J T a AI Itrlv) ao =o o Ftn &r E-Eoz bTJ: -IE]F a Xo0iAo" ;lF.o.Dv) tr E-- aFaizg c,a aF9(,oJoIJ(, oEtJLi-(92t, 0. zo E< UorI u2 0loa }loa L)Z j LJ iE 0d'e =z2qrHETC:F BRa:,vcot-t) a\ EiE o h o o o ts- to tE: + zo Fr L)oJ -1JA lrl2=tdrl (JEzJE,oFzo = 2>q ODF TEIar14iL,o*Itrl TT IC, I. + z3HtlilF 6e"4 o i0"o= trloou) -1o vtazE-<aE1 F 6EHiE-s-fi> Ifsl + trIE- (, .'J *+ = A T 1 a o =o f62 I- = Fa rIl F o b JrdE< =xo 0.p" j Jtr: 0.E.Da Et'l?- oF o UIFu'lFzlr.l6ah tnFa6oJoIJ(9 aELJLl =(9zUJ p. zo F. ()oJ hl-lE{ =(,2 0aot-2ox oZ 3te,n =z2qldEElEid BRc,x0toFu) o o a e,trtriDFo<F= OAuz fr= EEkF oi.)>Z rr:- f:] Ooa95 EE EB Fxoi o =:5Ut1 =tr )+ zoz-o J f,l$-r E<!e gEe H.,loE z -ar F aH k =)L JI')z o<o o,tr: n6la, q-' =9 \ o. c. coala-qE'E F -..-A^ffzEOf,,oor20 tr. 5.;rtrlF xofr0"0. o. ;10"A a pi trlr<- c. G. aFatrzlrJ5UI ant-tn (9oJoUJ(9 tr1ELJlrl =ozur 0. J3t-ztrlt-og !)aE] GE]ti 'o2potrTJ () =j (JTE oa i, =z2qEI-E:cii BB vE0 fr k- \ \ 9ar6-i :E 19 + \ \ \ \ \ \ \ \ I N(o crj(o lo,ri*, =r+trIE* () \ o o a &5 H8 =zFO<U lir 9z\ -o$EEd E-.F<Fo>ZEoE524a pY EtE \ II \\ --- z=oe =kk=ooaJZ -orr: E =(J<r=z EHF-2kOJ l+a=v zE]ufrl-] l; ,/!- .,T*/ F ,/ A F o ,0 Fa EI F&oz a,/ oo ItrtF XoEp"A J0"p* IN 0lF]Er- I I \ aFatrzIJoa aFtn(,oJolrJ(, oE,lrJLJz(9zL, 0. zo Er trFzl'1U2o()ou) &IJ E{Io .tsoF oz S=&ig6ez 2q EIcld BB )4EoF.ln bF I r;i-luv) o t;i Dn fi -k- / ::/', Ft/ ?\t\x+l I / - - - u2>Etr=a3F IEIattiiC,oJ@ E-V.= =V ]="H ]l8?fi t r/O./.-E ./ '/ I cr6E ,/./e*- -' -...---\ ./\ Yt- -<u 5.Eu 11-F llt} lr *=/ APPENDf,K I SPATCO Envlronmental Preliminary Site Assessment PREUMINARY SITE ASSESSMENT Stork Screens of America 3201 North I-85 Charlotte, North Carolina 28213 SPATCO Work Order 190004908 PREPARED FOR: Fred Monroe Stork Screens of America 3201 North I-85 Charlotte, NC 28213 PREPARED BY: SPATCO Environmental 5100 North I-85, Suite 7 Charlotte, North Carolina 28206 April 18, 1994 TABLE OF CONTENTS CERTIFICATION ....iii 1.0 INTRODUCTION 1 2.0 SITEDESCRIPfiON .....1 3.0 FIELDMETHODS... 1 4.0 LABORATORY RESIJLTS 2 LIST OF FIGURES Figrre 1 USGS Quadrangle Map Figure 2 Site fvlap Figure 3 Soil oil and Grease Concentrations APPENDICES Appendix I Boring log and well constnrction details Appendix tr Iaboratory Results u$lu* ku ofLr.io., PttA, V0r9-a90t, llt g CER,TIFICATION This report has been prepared under the guidance of a North Carolina Licensed Geologist to meet the requirements for the North Carolina Department of Environment, Health and Natural Resources. The information and conclusions expressed in this report are based upon normal standards of the profession and limited to information available at this time. Chemical analysis of samples associated with this report were performed by a subconffi.cted independent certified laboratory. Iaboratory results have been accepted on the basis of subcontractor's internal laboratory procedures and should be considered qualitative unless verified with appropriate QA/QC samples analysis. .?o l?tal NC Licensed Geologist #1160 9or* fua otfxb, PtlA, V(N*490r, 3lt-r1 iii 1.0 IN]RODUCTION On September 16, 1993, SPATCO removed one underground stofirge tank and one oiUwater sepaxator from the Stork Screens of America site located at 3201North I-85 in Charloue. Soil samples were collected from below the tank excavation. I-a,boratory analysis of the samples indicated concentrations of petroleum hydrocarbons and halocarbons in excess of regulatory guidelines in the samples collected from beneath the UST and oiUwater separator. In Febnrary 1994, SPATCO conducted a preliminary soil and ground water assessment to determine if ground water had been impacted by the petroleum hydrocarbons and to delineate the extent of petroleum hydrocarbons and halocarbons in the soil at the site. As part of the assessment, SPATCO collected soil samples from around the former UST excavation with a GEOPROBE6 direct push sampler, and insalled a monitoring well in the formerUST excavation and collected soil and ground-water samples from the well. This report details the soil assessment, well insallation and soil and ground-water sampling results. 2.0 STTE DESCRTPTION The site is a textile machinery manufacturing facility located at 3201 North I-85 in Charlotte, North Carolina. The site is located in an indusnial area. Figure 1 is a copy of the USGS 7% minute quadrangle showing the location of the site. Water is provided to the site and surrounding properties by the City of Charlotte. 3.0 FIELD MEfiIODS On February 28,1994, SPATCO Environmenal installed one T)pe tr monitoring wd, Ivflil-l. Figure 2 is a site plan showing the location of the well. A soil boring was advancd through the former UST excavation using hollow stem auger methods. Soil samples wene collected from the boring every five feet utilizing a qplit-spoon sampler. The boring was compleEd as a two- inch diameter monitor well. The well was constructed at a depth of 50 feet using Schedule 40 PVC casing and 20 feet of 10 slot screen. The well annulus was filled with #l typ filter pack and a mo foot bentonite seal was placed two feet above the top of the screen. The well was st l Sorr, r/zlurrlA, PSll, 'VOrt-49U, *lE-91 completed flush to grade with a locking cap, water-tight seal, and a bolt-down manhoie. A boring log and well constnrction detaiis are attached in Appendix I. The soil sample collected from the boring exhibiting the highest organic vapor concentrations and the sample collected from above the water table were analyzel for oil and grease (EPA method 907L) and Volatile organics (EPA method 8021). On March l, 1994, SPATCO collected a ground-water sample from I{W-l. Prior to sampling, the well was gauged for depth to water and presence of liquid phase hydrocarbons (LPH) using a decontaminated interface probe. The well was purged of at least three well volumes using a disposable Teflon bailer. The sample was collected using a Teflon bailer and analyzed for acid/base neutral-extractables (EPA Method 625), volatile organics (EPA Method 624) nd RCRA metals by EPA Method 3030c. To delineate the extent of petroleum hydrocarbons and halocarbons in the soil at the site, SPATCO Environmental used a GEOPROBEP sampler to collect soil samples from the area. The GEOPROBEo sampler hydraulically pushes a 3|4lrrrch sampler to the desird sampling . depth. Once the sampler is at the sample depth, a stop plug is removed from the sampler, and the sampler is pusher past the sample depth and the sample is collected in a new acetate liner. On March 30 and 31, 1994, SPATCO Environmental collected soil samples &om around the former UST excavation with a GEOPROBE0 direct push sampler. Soil sample locations are shown on Figure 2. Soil samples were collected from the borings every ten feet and screened with a porhble gas chromatograph with a photoinoziation detector @ID). The sample exhibiting the highest PID reading were shined to a laboratory and analyzed for oil urd grease (EPA method 9071) urd Volatile organics (EPA method 8021). 4.0 I"ABORATORY RESIJLTS Soil sample ualytical results are summzuized in Table I, and the laboratory reports a.re attached as Appendix B. 2fu* *an olAn-b, PSA, W0rr-lr0t, &rr-N Referring to Table I, the extent of the hydrocarbon and halocarbon impacted soil appears to be delineated. Figure 3 shows the areal extent of the impacted soil. I-aboratory results of the water sample collected from well [d\M-l are summarized in Table tr. Referring b Table II, the ground water at the site appears to be impacted by a release of petroleum hydrocarbons and halocarbons. Soe* 9* ct,Uub, 84 f,O#lr*,,t rt-l, ta*i-'(tqII d g tn:. I T{ta HE899xe ooo od o€f- -]o c0 Jo ca Jopa Jola Jo ca Jo Ea c,.EAc\ogg0 1E.,EE -l---J-F o$\o o\om Joca JnE JA EO Jnpa Jn ca Ja ca :-E EB -1€.8 E-:trEgF Joca Jola J CIca JA ca o\c.l+Joo JnE I € Hecrs OAEaeF oor o(q Joca Jola Jn ca ol$ Jara "lo 4a Bss Jop0 F- Joc0 rloE o\oco Jnm Jne ESa s6F-' rll oo\oo @ JoE ,.]o c0 Jorq Joo .Io 00 Jno . i ea =€#B Jo EA \o Joca rloca -loca Jn FA Joca Jnm E 88: gEoeE oo(\lN ov1C. oo\otca oC-oo\(a o€c\l o COln €ate u.)sl rn(a $c\l -iol tol o(7)r+(\l ta(\l TEtrclss a>$oo Too YoQ *Ioo rnIoo \oIoo v, u,o& (BoH.aEr -bJ 'cd 3€Fg E Ec,v) =ov) : a :,*'---.---- itU.S.G.S. Topogrophic Mop ;D€RITA QUADRANGLE SCALE 1:2,T0OO o XILOMETER SPATCO Tenvironmentot NGURE T: sJonx_EFEffi2201 NORTH t-ss C}IARLOTTE. NORIH CAROUNA -" lvgt L:-d*+q:t =* = trJ oo trJ iod,o-0- (,zo 5(D 4- LrJ UJEoq E,o a tr,,t7'=o ldu = () =td () a 3o L, 6. a oUI do TABLE tr Ground Water Sample Results for N{\il-1 3lLl94 Compound Concentration (ug/l)NCAC 2L Limits (ug/l) Benzene BDL I Chloroform 7.8 0.19 1,l-Dichloroethane 33 700 1,l-Dichloroethene 51 NE Ethylbenzene 32 29 Methylene chloride 100 5 Tetrachloroethene 13 0.7 Toluene BDL 1000 1, 1, l-Trichloroethane t45 2W Trichloroethene 13 2.8 Xylenes 2s0 530 Cadmium 7 5 Chromium 1,990 50 Leg,d 100 15 Mercury 18 1.1 W tuw olk bt PSA. wOl9.49N, +IE-N a 369 E3JG6l .= fil sliil o. 9lJlo= ZH=o(D. E :m, (, z-6Jfcl I 'Ie € Io<,aI =6EG o-{* otr vt Elrl =oo. o oo (,z6 5d) :co ECo!-.; Cq) \oO 0_a Iu.lrJr=>ur va? = lrl ;HE U.r 9EEE. dPfL(NC) ;(D z =E tct, oN + ui c\l €oq,tU'aIt (J = e 6E EZJAat.: fil Eltll zPJlo= EEc. ffi; (, z-dJfo !E!o.8g za,tE* ioe =$Bo \EA.aalcrOo,(:, roa EA€a3s(,rta Efo. 11, EanaJsoltt E{ Eaioa 3a(,N, 0L3o E,lrl =oo. o oa, (9z6J =(D E+)C 0) Eco.; C 0) \o C) o-a az<)uzhlfrLt(/,t-oYJe.G,o<ao APPENDIX I North Carolina - Department of Environment, Health, and Natural Resources Division of Environmental Management - Groundwater Section P.O. Box 29535 - Raleigh, N.C. 27626-0535 Phone (919) 733-3221 WELL CONSTRUCTION RECOHD DRILLING CONTRACTOFI: Geoloqic Exploration, Inc. ORILLEH REGISTEATION NUMBEB: 117s STATE WELL CONSTHUCTION PEFMIT NUMBER: 1. WELL LOCATION: (Show sketch of the location below) Nearest Town:Charlotte County: 3201 I-85 Service Road (Boad, Community, or Subdivision and Lot No.) 2. OWNER Stork Screens of America ADDRESS 3201 North I-85, P.o. Box 26458 Char].otte, (Slroet or Boute No.) NC 2A22t City orTown Stale Zip Code DATE DBtLLgg 2-28-ea USE OF WELL lglrtot __._TOTALDEPTH 5O.O' curflNGS ooLLECTED YES El NOE DOESWELL REPLACE EXTSTTNG WELL? YES f:] NOIE STATIC WATEH LEVEL BelowTop of Casing: 36.0 FT. (Use '+' il Above Top of Casing)8. TOP OF CASING lS 0.0 FT. Above Land Surface' 'Cerlng Tormlnetrd eUor bolow land eudaca lrltlcgal unlesl a varlanco ls lssued ln rccordrncr xlth 15A NCAC 2C .01189. YIELD(gpm): u/4, METHODOFTEST N/A 16"Asphalt 16"15'Oranqe fine sandy silty clay Tan orange silty clay Mecklenburg DEPTH From To DRILLING LOG Formation Oescriplion 3. 4. 5. 6. 7. 52'15' ato. wArER zoNES (dePth): 11. CHLOFINATTON: Type r/e Amount N/A 12. CASING: Wall Thickness or WeighUFtSch. 4O ll additional space is needed use back of lorm Deoth DiameterFrom O To 3O.O pr. 2 inch From- To- Ft- From -To- Ft.- 13. GROUT: LOCATTON SKETgH (Show direction and distance lrom gt least tulo State Roads, or other map reference points) /'l.J f,-1rf) Se.vi, r-r-c-,.1 -w N v Material PVC Depth Material Method From 1.0 1o 26.5 Ft.Por$and/Bentoryy From To -Ft. - 14. SCREEN: Deoth Diameter Slot Size pronl 30.0 1o 50.0 Ft 2 in. .010 From -To - FL- in. D€othrromT:S 'io so'o tt From - To- Ft Material PVCin. in. From - To - FL- in. in. - 15. SAND/GHAVEL PACK: 20/60Size MaterialFine silica sand tvwl. 5t ,a. 1a 6. BEMABKS: !lw-l, Bentonite pellets from 26.5 to 27.5 feet I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDAROS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.q.i 1'y-'i SIGNATURE OF CONTBAUTOR OR AGENT DATEGW..1.iEY:.9P-1:i::::=:==.=.=:..-.-a:!.}.+-SUbmitongina!t-oDivi5i.rn-u.En4'i'gEJlBl'lFi-€-o*r'f'Erc oo lrJ2 0-(loouro =E,trjk = J- vc.)f; o aI IJ' v,o nJC) T u1 =od,dt. Ffg Fa o-2 3 C) 5vl - =oE,@ F !IJ F( 6 Jo TJ6 =ouo E!o J , lr! eco U t! cV. E =F a =ou,o E+(,) Eo 7 o6lrl OE-zlll>= Ea.o, o t\a CD oN G'o c c o ,2o=dg Ot I I ro I6 Io t!r) IN c{ Iql I(o Io Io Iti I(:t I c.,l Iolc{o lrl C a. al::<=vtz tn o ro oN tt,(\on oro c{ort oln LJNo od eH i.l Y=?(9O.zJ trJ *a <ltnl-l l I o-o E o =4E,a riio F(9zI ria3E 5 Effi3E sObolrj < oulo.Eo-(,l ,lolorlrl * E UJouo Eo = rh =EllJG td 1n -l JI TI"l du, Jtr6 H a _tll =l zo oLtr ldo j lrJ = a tr-Jo Zotr() =0a azoO LLI.= bJ o_ oz. CI C) CIZ a.om E3 APPENDIX II April 12,1994 Client: Attention: Report #: Project: .P.O. #: EnviroTech Mid-Atlantic Virginia Tech Corporate Research Center 1861 Pratt Drive Blaclcsburg, Virginia 24060 (703) 231-3983 FAX (703) 231-3984 SPATCO Environmental 5100 North I-85, Suite 7 Charlotte, NC 28206 Mke Shaw 6954 Stork Screens, Charlotte, NC Fax 704-596-8605 Date Received: 4105194 Project #: 4908 Page 1 of 3 Sample Matrix a Sample Identificatlon Samples zubmitted and ideutified by client as: Field Identification Date Time Collected 69s4A 69548 6954C 6954D 6954F 6954F GOz.24 GO3.24 GO4.24 GO4.30 GOs.24 GO6.25 3130t94 3R0t94 3R0194 3R0t94 3fiot94 3l3L194 10:40 12:15 15:15 16:00 l7:20 10:35 Soil Soil Soil Soil Soil Soil .{Il analyscs wcr= pcrfonncd in accordaace with EPA methods refcrenccd iu "IVlethods for Chcnicd Aaal;trls of \ilatcr and Wasteso, EPA 600/4.79 reniscd March 19ff1 and/or "Test Mcthods for Evaluatiug Solid Wattc, PhysicaUChcmical Methods", SW-E46, 3rd Edition. Projecfi Stork Screens - Charlotte, NC Analvsis DtL HALOGENATED VOIATILES (p/kg) F.NVIROTE CE MID.ATI.ANTIC April 12, 1994 Page 2 of3 69544 69s4B 69s4C 69s4D 6954E 69s4F GO2.24 GO3.24 GO4.24 GO4.30 GO5.24 GO6.25 Benzene Bromobenzeue Bromodichloromethane Bromoform Bronomethane u-Burylbenzeue sec-Butylbenzeue tert-Butylbenzene Carbon tetrachloride Chlorobenzene Clhlorodibromomethane Chlorocthane Chloroform Chloromethane 2-Chlorotolueue 4-Chlorotoluene cb-12-Dichloroethene 1 3-Dibromo-3-chloropropaue 13-Dibromoethane Dibromomethane 1"2-Dichlorobenzeae 1,3-Dichlorobenzeae 1,4 Dichlorobeazene Dichlorodifluorome thane 1,l-Dichloroethane 1J-Dichloroethane 1,l-Dichloroethone trans-1 l-Dichloroethene 13-Dichloropropane 1,3-Dichloropropane 2J-Dichloropropane 1,l-Dichloropropetre cb-l!-Dichlon propene trans- 1 3- Dichloropropeue Ethylbonzeae Hexa&lorobutadiene Isopropylbeuzene plropropyltoluooo Methylcne chloride Naphthaleuc n-Propylbeazeue Styreno 1, 1,1 r2-Tctrachloroe thaue t,L H-T etnchloroethane 10 10 10 10 20 10 10 10 10 10 10 20 10 za 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 t0 10 10 10 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 10 10 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 91 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL .BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 180 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL D& - Detection Limit BDL - Bclow Dctcc'tion Umit Soil results are r=ported on a dry weight basis unless otherrrise noted. \ Project- Stork Screens - Charlotte, NC Tetrachloroetheae Tolueue 1 "2,lTrichlorobenzeue 1 3,4-Tric,hlorobenzene 1, 1,l-Trichloroethane 1, 1,2-Trichloroethane Trichloroethene Tric,hlorofluorome thane 123-Trichloropropane 134-Trinethylbeuzene 135-Trimethylbeniaetre Vinyl c.hloride Totd Xyleues Oil & Grease (ng/kg) Analysis ET.IVIROTECE MID.Afl.A}Ifl C April 12, 1994 Page 3 of3 Analvsirs DIL HALOGENATED VOI-ATILES ( Wfirg) (coatinued) 6954A 69548 GO2.24 GO3.24 6954E 6954FGO5.24 co6.2s BDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDL 69s4C GO4.24 BDL BDL BDL BDL 79 BDL BDL BDL BDL BDL BDL BDL BDL 170 6954D GO4.30 42 BDL BDL BDL 42 BDL BDL BDL BDL BDL BDL BDL BDL 390 10 10 10 10 t0 10 10 10 10 10 10 20 10 10 BDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDLBDL BDL 340190 ?30 530 Quatity Coutrol Data VoffD VoSpke VoRD EPA#Aaalyst Date Aaalyzcd Ilalogenated Volatiles 1,1 DCE TCE C Beuzeae Bcnzene Tolueae Oil & Grease 2.7 2.0)) 3.3 4.3 L4 75 98 91 91 93 9189 8021 A. Campbell 4tw94 907L S. Peters 4fi?D4 D&. Detection Umit BDL . Below Dctection Limit Soil rcsults arc r.eported on a dry wcight basis unless othenvise noted.a J :'j-:.-::.:.==::::::..-__.-.*--.-,.-:-:.-.:.._:-.---!..-1.i?.-+€::?..!-==:- [.aboratory Direaor J o uJ\- <J;e,ulg< 0o asN '4 lr1 \0r\l +JJ CDE, c,\r r r t$ r lddqEJ 4 -1 I,qf; fr $El 'B =cE\l \l - E E H-A E E ? T E #3 =,N E = d{il gI$g ololfl ;urcl!Eo }< TE 3 JJStJ $$ $gU'GgEE9='{, ]U =EOU' ]C ooo(r E'o ct, o oc'6 o t (6 co ECoL- C tUo C) ila olgF(aIJ:loUG.ttultt, z 6t ts AC o 9urt= G:)F df.l BI ,n-l atIJJG{ &:U s$- Gr6 =52 x.Eh = c ctl!C> =CEg, \,E F{ u.t o s] ,$l so fi 6\ l{,Y ut =F oYo $ N 9 rJ oa.t ol\l rl o =I t utq =6 ! Efu q u,Jo- =U' INc{ FT... '\T ii \,.1+ a(. oA? !- \t'l t{et \t,\l ..d t Enviro Tech Mid-Atlantic Virginia Tech Corporate Research Center 1861 Pratt Drive Blaclsburg, Virginia 24060 (703) 23r-3983 FN( (703) 231-3984 March 17,1994 CIient: Attention: Report #: Project P.O. #: SPATCO Enviroumental 5100 North I-85, Suite 7 Charlotte, NC 28206 Mike Shaw 6779 Stork Screen - Ctarlotte, NC Fa:c 704-596-8605 Date Received: 3lMl94 Project #: 4908 Page 1 of 6 Sample Matrix Sample Identification Samples submitted aud identified by client as: Field Identification Date Time ColleEted 6779A 6779F_ 67:79C Soil Soil HrO MW-1-25 MW-1-3s MW-1 2l28te4 2n8D4 3101,194 4:05 4:2L 9:45 All analyscs werc pcrforned in accotdance with EPA methods rcfercnced in'lVlcthods for Chcmicat Analyck of Watcr and Wrstcs', gPA 6Nl4-?9 revised March 1983 and/or "Test Methods for Evaluatiug Solid Wastc, PhycicaUChcmical Mcthodsn, SW-846, 3rd Edition. Project Stork Screen - Charlotte, NC Analvsis Oil & Grease (mg&g) Benzene Bromobenzene Bromodichloromethaue Bromoform Bromomethane u-Butylbenzeae sec-Butylbenzene tert-Butylbenzeae Carbon tetrachloride Chlorobenzene CLlorodibromomethane Chloroethaae Ctloroforrr Chloromotheae 2-Chlorotoluene &Ctlorotolueae cis- l3-Dichtoroethene I l-D ibromo-3-chloropropane l2-Dibromoethaue Dibromomethane 13-Dichlorobenzeno 13-Dichlorobenzeae 1,4 Dichlorobeuzene Dichlorodifl uoromethaue 1,1,-Dichloroethatre 13-Dichloroethane 1,1-Dichlorocthene trans- 1,2-D ichloroetheoe 12-Dichloropropano 1j-Dichloropr,psne 23-Dichloropropare 1,l-Dichloropropcne cis,, 1 J-Dichloropn,peoe traos- 1 "3-DichlorcpropetreEthylbenzene Hexachlorobutadiene Isopropylbenzeue plsopropyltolueae EI{VTROTECH MID.ATII,IYTIC March L7, L994 Page 2 of6 A"nalvsis !)& HALOGENATED VOIATILES (p/kg) 6779A 67798 MW-1-25 MW-l-35 2290 1750 6779A 67798 MW-1-25 DtL MW-1-35 BDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 20 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL ZO BDLBDL 10 BDLBDL 20 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL IO BDLBDL 10 61BDL 10 BDLBDL 10 BDLBDL TO BDLBDL 10 BDLBDL 10 BDLBDL 10 BDLBDL 10 BDL890 10 81BDL 10 BDLBDL 10 BDLBDL 10 BDL DIL 10 100 100 100 100 240 100 100 100 100 100 100 200 100 ?00 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 D& - Dctedion Limit BDL. Below Detcction Limit SoiI results arc reported on a dry wcight basis unless othcnrise notcd. ProjecE Stork Screen - Charlotte, NC Analvsis }IALOGENATED VOI-ATILES Methylene chloride Naphtbaleue n-Propylbonzene Styrene 1,1,1 3-Tetrachloroethane 1,1 A2-T etruchloroethan e Tetrachloroethene Toluene 133-Trichlorobenzene 1 3,4-Trichlorobeazene 1,1,1-Trichloroethane 1,13-Trichloroethane Trichloroetheae Trichlorofl uoromethaue 133-Trichloropropaae 1 l,4.Trimethylboozeae 1Jj-Trimethylbenzene Vinyt e.hloride Total Xyleues Amlv:sis vorATrLE oRcAr{rcs (ygl) Beuzone Bromodichloromethane Bronofora Bromomethane Carbon tetrachloride Chlorobeozcoe Chloroctherc 2-Chloroethyl vinyl ether Cbloroform Chloromcthane Dibnomochlorometiane l3-Dichlorobeuzcaa 1,&Di&lorobeEiacae 1,&Di*lorobcuzeue 1,I-Dichlorocthaae 1,}Di&loroethanc l,l-Dichlorocthenc trans- I l-Di&lorcethene 12-Dichloropropanc EI.IVIROTECE MID.ATIAIYTIC March 17,1994 Page 3 of6 DIL D& - Detection Limit Soil rcsults are reported on 6779AuL Mw-1-2s DIL jgtkil (continued)100 BDL 10100 BDL 10100 BDL 10100 BDL 10100 BDL 10100 BDL 10100 1,200 10100 BDL 10100 BDL 10100 BDL 10100 BDL 10100 640 10100 BDL 10100 BDL 10100 BDL 10100 BDL 10100 BDL 1020a BDL Z0100 18,000 10 6779C MW-1 BDL BDL BDL BDL BDL BDL BDL BDL 7.8 BDL BDL BDL BDL BDL 33 BDL 61 BDL BDL 67798 MW-1-35 71 BDL BDL BDL BDL BDL 130 BDL BDL BDL BDL 360 BDL BDL BDL BDL BDL BDL 780 5.0 5.0 5.0 10.0 5.0 5.0 10.0 10.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 BDL - Below Detcction Limit a dry weight basis unless othcnrise noted. Project Stork Screen - Charlotte, NC 6779CAnalvsis UL l,fi/-l VOIATILE ORGAIIICS ( HelL) (continued)cis'lJ-Dichloropropene 5.0 BDL traas-lJ-Dichloropropene 5.0 BDLEthylbeuzeue 5.0 32 Methylene chloride 5.0 100 L,L!,,2-Tetrtchloroethane 5.0 BDLTetrachloroethene 5.0 L3Toluene 5.0 BDL1,1,1-Trichloroethane 5.0 145l,l2-Trichloroethane 5.0 BDLTrichloroethene 5.0 13Trichlorofluoromethane 5.0 BDL Vinyl chloride 10.0 BDLXyleaes 5.0 250 ACID/BASE NEUTRAL HffRACTABLES (dL) EiYVIROTECH MID.ATI"A}{TIC March 17,1994 Page 4 of6 Aceaaphthene Accnaphthyleae Aathracene Benzidine Benzo(a)aathracene Beuzo(a)pyrcae Benzo(b)fluorautheae Beuzo(g"h,r)peryleue Benzo(k)fluorasthetre Bcnzyl butyl phthalate B is(2-chloroetho:ry)methane B is(2-chloroethyl)e ther B is(2-chloroisopropyl)e ther B is (2-ethylhexyl)phthalate &Bromophenyl phenyl ether 4-Chloro-3-methylphenol 2-Chloronaphthaleue 2-Chlorophenol ,4-Chlorophenyl phenyl ether Chryseue Dibenzo(a,h)anthrancen€ 1l-Dichlorobenzene 13-Dichlorobenzeue 1,,1-Didlorobenzene 33-Dichlorobeazidine 2"4-Dichloropheaol Diethyl phthalatc 2,4-Dimethylphenol Dimethyl phthalate Di-n-butylphthalate 10 BDL10 BDL10 BDL10 BDL10 BDL10 BDL 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 BDL BDL BDL BDL BDL BDL BDL 14 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL D/L - Dctcction Limit BDL - Below Dctcction Lirnit SoiI rcsults arc rcpofted on a dry weight basis unless othenvise noted. Projecf Stork Scrcen - Charlotte, NC Analvsis DIL 6779C MW-t ACIDEASE NEIJTRAL EXTRACTABLES ( dL) (continued) EI\IVIROTECE MID.ATI."{IYTIC*'"*#;'3il 2,4-Dinitrophenol 2,4-Dinitrotoluene 46.Dioitrotolueae Di-o-octylphthalate Diphenylhydrazine Fluoranthene Fluorene Hexachlorobetrzene Hexachlorobutadiene flexachloroethaae Indeuo( 1,2,3-cd)pyrene Isophorone 2-Methyl-4,6-diaitrophenol Naphthaleue Nitroberzene 2-Nitrophenol 4-Nitropheaol N-Nitrosodimcthylamine N-Nitrosodi-a-propylamine N-Nitrosodipheoylaoine Pentachlorophenol Phsnaathrene Phenol Ppene lS4Trichlorobenzene 2"4,6'Trichlorophenol 1,,1-Dimethylbenzene 2-Ethoxy Acetate Ethanol 4-Hydroxy-3-mcthyl Bcazaldehyde 4-Methyl Peatanoic Acid Dphenyl Etheae 3030C Metals (ne/L) Arsenic (As) Barium @a) Cadmiun (Cd) Chromium (Cr) Lcad (Pb) Mercury (Hg) Silvcr (fu) Sclenium (Se) 10 10 10 l0 10 10 10 10 10 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL Hexacfrlorocyclopentadiene 10 10 10 10 10 10 10 10 10 10 10 10 TENTATTVELY IDENTIFIED COMPOUNDS 10 BDL10 BDL10 BDL10 BDL10 BDL10 BDL =A:rrount 35 3s0 16 24 t2 0.002 BDL0.1 020.005 0.0070.05 1.E80.1 0.1 0.0001 0.0180O.O5 BDL0.002 0.00s pElL 1) 2) 3) 4) 5) D/L - Dctcction Limit BDL - Below Dctcctioa Limit SoiI results are reported on a dry weight basis unless othcnrise noted. Project Stork Screen - Charloffe, NC Analysis Quality Control Data VoSTD ToSpike VoRD EPA# ET\-VIROTE CE MID.ATI"ANTIC March 17, L994 . Page 6 of6 Analyst Date Aaalped Oil & Grease Ilalogenated Volatiles 1,1 DCE TCE C Benzene Benzene Toluoae Volatile Organics 1,1 DCE TCE C Bcnzcue Benzene Toluene AIBN F.xtractables 45Vo Aciil95Vo Base 3030C Metals Arsenic (As) Bariua @a) Caduium (Cd) Chromium (Cr) Irad (Pb) Mercury (Hg) Sitvcr (fu) Selcnium (Se) 9393 9071 8021 S. Peters A. Campbell M. Buchanan S. Croy 3t08t94 3/t0t94 iftap* 3tL7t94 95 8.,t98 3.i94 2.t103 2.991 2.2 95 8.498 3.194 LL103 2.991 L2 624 A. Campbell 3n9p4 62s 95 96 108 108 11E 115 110 110 110 t02 105 110 110 100 108 93 <1 <1<l <1 <1 <1 <1 <1 7j/62 6010 6010 6010 6010 245.1 6010 n0.2 DIL - Dctection Limit BDL - Below Dctection Umit SoiI results ane reported on a dr7 weight basis unlcss othenuise notcd. Elizabeth Smiley u,lFat,u5ou,E at UJU' Jz ( )! Feo ; $ '- .\I\- uo tt Inl 3: f,:l6[s' ozD9ur<= )FlE fI atu,Er oc 3.c tc $l :trL a' =ul n EBo =-\n x.E =T -s c-.I orA> =Ea ] ul ct s.sk !a ti $ N Ja * u, = l/l oJ il { s G =o g u,Jo- =3r, \\ \ \} T F V) ci u,r =@ ,T E MI 3 *z u.I B-\sv! -o {G-FrrUr3 \JdJl{- {.,1 J{ : ol(rl -l--l 1 U':<.E =UJG, ct)2o () Eu,z (JulGa, o Et-'o c)otr E'o . ct, =o oc (U g Co Ec .g 't- UJool- H U) Eo Ef;n= -aoY|aarlElgsuJt-o 8I ET E gEF o? t G,lrJctc,o-Eo = zo z,lrJ t- cD3t,ut CEcro g 1 o--o-! o o-OI- o5/L3/94 15:58 e703 231 3s64 tday 13, 1gg4 Clieof Atrcution: Rcport *t: Project P.O. Ch Enviro Tech Mid-Atlantic Virginia Tcch Corpontc Rcseacch Ccrttcr 186l PratiDrive Blaclsburg, Ifirghie 2a060 o0o 23t-3983 FAX O03) 23t-3984 SPATCO Eurrirorunental 51fi! NortL I{5, Suitc 7 Char{otte, NC 28205 lvfikeShaw : t69s4 Stort Screens, Charlotts, NC EI}L{ Fax ft4-595-9605 Darc Rcceive*, 4M194 Project # 4908, Page t of,Z i-- SPATCo CllC @ oor -) o Simple fdcafi$catou Saspl* subuired and identificd by dieat as: .Fietd Idcutification .SeEFIc Mardx Date TIne Cotlcmd 6954A 69548 6954C 6954D 6954E 6954F SoiI Soil Soil Soit Soil Soil @L24 @324 @424 GO430 CrOs24 @6.25 3ROE4 380t94 3F}0t94 3fioD4 3mtg4 3BW4 t0:tO tL75 15:15 16:00 fi-2fr 10:35 A[ 0r$lr8 mr pcrforrcd h accodfucc t ilt EPA uc&o& reftrcncld h "ldrttods for Chr.aicrl AqrSnb ol Wtr U lf,1gtld, ff,6{lflT?lt l! ild !f,rlcL 1983 ead/or Tc.t M.ttodr for Erelnedag So[d WrcC ' ltftrcdrcUuisl!fi!6odtl' Sf-t{63rdElttoa. : os/L3/94 15:59 6ZOe 231 3S8.r Project Stork Screens, Charlotte il-C Aratesis ToaI RCRA Mcals (Eg/kg) AEcric (As) Barinm (Ba) CatutoB (Cd) ChroDrisa (C0 kad (lb) Merery (IIg) Sclonium (Se) Silvcr (Ig) ETtr,I,+,+ SPATCo CNC ENVIROIECE MIII.IIITIAI{UC Mrry 1i,U)9t{ PagG 2 of? 6954A 69548 6954C 6%4D 69s4E 6954F@U4 @324 @424 @430 ffis.A erO625 @ ooz UL qE E, CoEEoIData %SiSTD ' %Sp&o %98 EPAit 1:: -_t0308 o.rtz 03331.E Tt 3.9oJu a.M6 0,;g34u o09 aJ001 01 0-3 0.0010 0.0010 0.0010 0.015 0.05 a.uzBDL BDL BDL ArdF Datc Aaelyaod . offI3 0Jr60.1 7J0.0w 0.s2s0.u7 91101 0J 0.0001 0.00100.003 oGEO.T7 BDL 0265u 0-qfi 0.0E 03 0.0010 0 013 BDL 0-169 1.6 0.92L 0.76 0.1 0.0010 0.015 BDL AralFto TotdRCRA lfictels AEsr+ (As) B.dnrrr (88)fa;'r.in'rr (Cd) Chrouiun (Cr) Lsd (Pt) lfi!8rnr, (Eg) Sdaiuu $o) Sihcr (fu) S. Croy stlw41U lXtt@, 10099 104106 109101 100&5 tfi E594 95 <1 <1'a <1 <1 <1 <1 ?fi62 nt.L n3.L 21EJ 89.t ZlS.L 7ii02flLt t bombrtDircctor DtL - Detccdon Ltnrit BDL. Bclow Dctccioa Limit ,HF{Y l3 '.=4 t6:t3 FRUI1 z EnvlroTech Mid.Attantic P Cl fYaw* 72 !08 S. ra.h srr€ctGrdrutt wgini1 !r$t1 (EOa) rn'1gg't :' rtn,,<a<iFA5--tce Pgti= -6a7tZQZI I !_-JUUUer I'ATEIIAL CHAFAGTENTZA?IOI{ FOFII Err NO. Eavtrofccltffia-------*Mid-ldandc o GEXEiATOB IOETTIflCTTTON: EuslN€ss ,lure STO{<ScBEep s AfiCtrcA tilc ,^ruNc^uo.ess /.o._ dax 76tlf9 afi-gl9E!-.stara Pc JogLocArortr j)ol N'L-/.{, anvChiuuifg - . Er^18-&- 4ct.1- ^u"heitzsE ^Gzxr FQAI fioilb€ 7v1s-Fpvtoortnepatv-i;pr{t7oY'53@- "r/p| OfCONTatlllIrNT N SOIL fiGrrah noi6.ur2 O0 trOno tud Oil t'Orrr On ly'E{,-t2&- TY?E OF ptt6E3i' OgHeBA?tNo nrl3 MA?EBI^L trl.er,riag undrrld.rrc 3u.'q3a Terrx G3ul.rr Spill" UATEllll.Cr{^!IC?FBZATI0N: Aarlyrir tn**'-t l€'5 Anrnrc. 00t- *rr Solelirrr rr' frOt- na Earcrrq " ttOt' tW 6arftm, | -a1,' g11rq' AOu *l'rr ?t usnc .99oo - 'rlb "r*rrrr^' -g,L--t* ,gg 6Ot eo'n EhyuDetru!'t 'Jo*' * ;;;.7-; Mo,.iu'. ll' ? x rota' rv.n s |u* * IL..d' ll----rpm rlr 'l' wx 3 r|"rq.$Y'-9!y* 'prq af@ rya .gv TCIJ, nt rnoc "Ey fq.p fitlmo it $la€. sgill PITYStrAL SifE: 85ars ClicuicrSlgav OSur . 9r6OuG: pdrr GOruaC Nir,na.t- lrfr- ouu( voLutre Eron It ccoc€ Yrr6- t HEFII{HIL rrl}ol{il tlulc artorcr xlulle -l?. Et:- - -E!.'.(Y':?!a 1. ^n'ess a* €tlgcoa st^tE/' rarpHoN! 7a y - fl c- 3e a r {!rbs*u{t. nlhfi4tz Stfr,--sx}sl'tH:ruN '|'t tvmt- e't^v luTl{ofllzrflol{:. ., t'rc cg€* cEoc'oca *,I *ol, g€!rt'a!s6 ,a6 c ,t.iso€ 39i!, I ccrlity that UrG f,Icg fiargbt "lc cadrc'y ltoa lq:arr'oqt ,cal Ft.(,laen. Strgrure r, AguptiuBrJ aggrl Pri,,rdgrnr. Tlua-Oatr- ?lrr ea:tverc eSovr ,.ra 9rd6nnd s . rrr...6csir szmgo eocrpcdo C Etia sci €c0G..d-b12 ec9rccd-@f P :,ror, Co riroOC ounirr.C h ,iOnVet 51r Cr{3. CrrOFcr f. ihb b 6 66atrgfc On{ aEarrlta CarctiPtrtt olgr? aC. !A: :13y cartif, [rir r.dri.l L .rra ftafaloira G rbGnJ t t U-.t n1ssr.:rr&rr (DoD U.3. Alrio.!.oral FVolG. .oo i6eac7 IEPIL Stla'c, l€l ,lgul.d€at. Slgnerrrrc C ArgrorisGt terllr' r r€s rrlt a ar', cucai..ta. cca* E! qn d o., cL4g,,. Cnrrrt lrL vA Ol€.1 .,q!'r!or tsc'3tirrgL YA lrlr$ rtrct$:!acocncrrug. ve GrEll lflrle9o t b{ rrn al tw, & fui o to, f,lurrl| r|' |, n .al *ls q b autot (W {,er{0|n Dh, }qr !.!t Ji Ji TOTEL FHGE.Eg? T.^ Envir o T ech Mid'Atlantic Virghia Tcch Corpontc Research Ccntcr 1861 Pran Drivc Btacksbr:rg, Virginia 24960 oo3) 231-3983 FA)( (703) 23r'3984 DAIE October 4, 1993 CLIENT : SPATCO ADDRESS: 5100 N-I 85 SUIIE G clIARLorTE, NC 2 8206 ATTENEION: MIKE SITAW PROJECT: STORK SCREENS PROJECI NO3 PITRCH4SE ORDER z 4484 1:. --t REpORT # : 5048 DATE RECETVED: 9/22/93 FAJ(: 704-59 6-8605 / PAGE 1 OT 3 DATE,/TIME COLLECSED 9-L6-93/2240 9-L6-9312t 41 9-2L-93/ L1:15 9-2L-93/12t30 6048A DlL 60488 SA}TPLE IDENTITICATION A!.ID A}IALYSIS RESUI.TS Samples submitted and identified by'clieat as: FTELD ID ow1 owz DB1 DB2 DlL 1ug/k9)s00 500 500 500 500 500 SAUPLE 6048A 60488 6048C 6048D ANALYSIS TIAI.OGENATED VOI,AIILES BroroodLchloromethaae Bromof,om Bromometbane Carbou tetrachloride Chlorobe[zeue Chloroethaae2-ChloroetbylChlorofom Chloronetbane Dibronochloromethane 1 r 2-Dichlorobenzeae 1,3-DLchlorobenzeo,e 1, {-Dl.chlorobenzeneDichlorodif luorometbaae 1, l-DLchloroethane 1r 2-Dlchloroethane viayl ether500 500 500 500 500 500 500 500 500 500 BDt BDL BDL BDL BDL BDt BDL BDt BDt BDL BDt BDL BDt BDI, BDL BDL 100 100 100 100 100 100 100 100 100 100'"*= 1oo 100 100 100 100 100 BDt BDL BDL . BDL BDt BDt BDI, BDL BDI, BDL BDL BDt BDI., BDt , BDfJ BDL vor.ATrLE AROMATTCS ( uglkg) 1rl-Dichloroetheue 500 tiaos-l, 2-Dicbloroetbeue 500 L,2-DLcLloroProPatre 500 cis 1r3-DichloroProPetre 500 trans 1, 3-DichloroProPeae500 Metbylene chloride 500 1, 1, 2, 2-rexrachloroethaneS 00gitiaiirloroethene 5oo LrLrl-Trichloroethane 500 L'rL'r2-Trichloroethaue 500riiiUforoethene 5oo lrichlorofluoromethane 500 Vinyl chloride 500 Beniene 5ooo October 4, 1993 A}.TALYSIS Ethylberzene ToluenetotaL XYlenes A}IA&YSTS OIL e GREASE (nglkg) 5000 5000 5000 DlL 10 ANAI,TSIS EATOGENATED VOLATILES (ug/kg) Bromodichloromethane Bromoform Bromomethane Carboa tetrachloride CblorobetrzeaeChloroethaae2-Chloroethyl vinY1 ether Chloroform Chlororaethane Dibromochloromethane 1, 2-Dicblorobetrzeoe 1, 3-Dichlorobenzetre 1, 4-DicblorobeozeneDicblorodif luoronethane 1r l-Dichloroethane f , Z-Oichloroethaire1,1-DichLoroethene E}WIROTECH MID.ATI,ANT IC REPORT: 6048 PAGE 2 OF 3 ac/ t6048A D lL BDL 1OOBDt 100BDL 1OO.BDr 100BDI, 1OOBDL 1OOBDL lOOBDL 1OOBDL 1OOBDL 1OOBDL lOOBDL 1OOBDL 1OOBDL 100 110r 000 100 44r 000 100 580r 000 100 6048A 49 r 800 DlL 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 :,00 100 60488 t 13., 950 ,w:/ 50488 BDt BDL BDI., BDI, BDL 800 BDL 280 BDt BDt BDt BDL BDIJ BDt 2r3oo 5s0 12, 0oo seP BDIJ BDL BDI, BDI, BDI, BDI, BDL BDL BDI., BDL BDI, BDt BDL BDI, BDI, BDI, BDL .::. . -i 6048C BDt BDL BDL BDL BDL BDI, BDL BDL BDI, BDL BDI, BDL BDL BDL BDI, BDL BDL October 4, 1993 AIIAtrYSIS IIOI"OCENATED VOLATILES ( ug/kg) traas - 1 r 2 =Dichloroetheae1, 2-DichloroProPanecis 1r3-DichloroProPeaetraas 1, 3-DichloroProPeneMethylene chloride L, l, 2, Z-leEtachloroethaue Tetrachloroethene L, L, 1-Trichloroethanel, l, 2-TrichloroethaneErichloroetbeneTricblorof luo romethaaeVinyl chloride. Benzeae Ethylbeazene Tolueuetotal Xylenes A}IALYSIS oIIJ & GREASE (nglkg) E}TVIROTECH MID-ATI.,ANTIC REPORT: 6048 PAGE 3 OF 3 D/L 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 DlL 6p48c BDL BDL. BDE.. BDL. BDI, BDL BDL 2A0 BDL BDL BDL BDL BDL BDL BDI, 240 6048C 760 6048p BDI, BDT, BDI, BDt BDt BDL BDL 430 BDL BDI, BDL BDIJ BDL BDI, BDL 630 6048p 460 -! 10 T,}IALYSIS ISTD VOI,AEILES1r1 DCE TCE C BENZENE BENZENE TOLT'ENE OIIr & GREASE 95 QUAIJITY CONTROLTSPIKE tRD AITALYSI CAI'{PBELt DASA EPA *DATE tolt/9393 9s L02t02 94 98 90 16 4.2- 2.0 2.0 2.L 2.4 2 8021 DlL - DETECBTON Llllrl 907.t s PETERS 9/24/93 BDt - BELOW DETECTION LIUIT ElLzabeth B. Smiley I l JJ rl T { { a EG, ?t 6 E G B2 B \t$oo N] ei r$l - !J@G, ciI E =(,2a.c. o s E $ cro lll .S!o!IG LJ ooottr Ifo*.o ora-oc G $lEo Ecol- c I,Uo()l- H @ Eo. Eo EEE! -tDuroCraEEgslltt-ro 85rg a)EsEE ul = a! = lr, EI u, ct ag D5,z ,lE EEtul ullJu, BIr lllr g E lr, 5 6ot{ 6:lo JE'c 6c!rgulr|(,EG U H af'HSN HFJEnr nc*E* i-r 5= Elt {Z=El'll rl EnviroTech Mid-Atlantic Yngiria Tech Corpontc Rcscarch Ccnter 186l Pratt Drivc Blaclsburg, Virginia 24O6o (703) 231-3983 FA)( (703) Z3r-3984 October t4, L993 CIient: AttentiQn: Rcpofi #: Projec* P.O. #: SPATCO Environrnental 51@ Nonh I-85, Suite 6 Charlotte, NC 28206 .. Mike Shaw 613r Stork Scrcens 4484- <t a Fax: 8O+596-96d5 Date Received: N/A7193 Project #: . .P"g" L of,Z SamPIe Identification Sanples submitted and identified by client as: Sample Matrix Field Ideatification Date Time Collected 6A1A 6Ui18 Soil Soil DBA DBlA 0e/2t/93 oe/21/93 130 11:15 AII 1gulyscs vcrc pcrformcd in reordancc with EPA mcttnds rcfaarced t1!1p*!ot Chankel-Atulysts ol Vai ota W*i'ii anl 600 l1-7g rcviscd March 1983 aad I or 'Tcst Mctlods for Evatutlng Solld Vastc, Phystcal t Cxtctnical Mcthods', Sl{'814 ird Edition- c APPENDf,K TI Initial Site Characterizatiou Report C oo p r n E r,,tw no r,t ru n trul ENGINEERS . GEOLOGISTS . SCIENTISTS INITIAL SITE CIIARACTERIZATION REPORT sToRK SCREENS OF AMERICA, rNC. AUGUST 1994 cooPER ENITIRONMEIITAL, INC. 23OO SARDIS ROAD NORTII, SIIITE QCEARLOTTE, NORTH CAROLTNA 28227 l7o+l84s-2ooo C oop n n E xw noirt ME r,{TAL ENGINEERS o GEOLOGISTS . SCIENTISTS August L2, L994 Mr. Allan Sctrifi NCDEHNR 919 North Main Street Mooresville, NC 281f5 Initiat Site Characterization Report Stork Screens of Am.erica, Inc. 32Ol I-85 North Charlotte, North Carolina CEI Project No. 94105 Groundwater Incident No. 11398 Dear Mr. Schitr: Cooper Environmental, Inc. (CEI) has prepared this report on behalf of Stork Screens of America, Inc. to provide an Initial Site Characterization [SC] for the referenced site. SPATCO Environmental previously submitted a Preliminary Site Assessment dated April 18, 1994 to the North Carolina Department of Environment, Health, and Nahrral Resources (NCDEHNR). This report indicated that petroleum-impacted soils and ground water as well as chromium were noted in and around the former underground storage tank (UST) basin. SPATCO closed the UST by excavation on September 16, 1993. The date and quantity of release are unknown. NCDEHNR issued a Notice of Regulatory Requirements (NORR) dated June 22, 1994 to Stork Screens which indicated that a Initial Site Characterization is required. The NORR indicated that the report describing the characterization should, in particular, include information on surounding populations, water gualiff, and the use and approximate location of water supply wells potentially affected by a release of petroleum from the Stork Screens facility. CEI has prepared this report to satisff this particular requirement of the NORR. 23OO SARDIS ROAD NORTIT. SUITE Q CHARLOTTE, NORT.H CAROUNA. 28227 (704) 845-2000. FAX (704t 841-8901 Mr. Allen Schiff August L2, L994 Page 2 On JuIy 6, 1994, CEI personnel reconnoitered the area within 1,500 feet of the Stork Screens site. CEI developed information to prepare this report on the basis of this reconnaiss€urce. CEI prepared Figure I which is an excerpt from the 7.5 minute U.S.G.S. topographic map for the area (Derita). CEI has drawn a circle with a 1,500-foot radius surrounding the site indicating tJre area of interest. Land Use and Surroundine Populations CEI obsenred land within 1,500 feet of Stork Screens to be used for industrial, corlmercial, and residential purposes. CEI observed numerous industrial and co'nmercial businesses to the west and northwest of the site along Statesville Road, Burch Drive, and to the south along Interstate I-85. CEI also observed a residential area approximately 1,100 feet to 1,50O feet norttrwest of the site along Auten Avenue and portiorrs of Riley Avenue and to the north along portions of Highland Avenue. The Stork Sc-reen property abuts beterstate I-85 to the south, a Knights Inn located on Burctr Drive to t.Le north, o.d a wooded area to the norttr and northeast of the site. CEI observed a Shell retail gasoline outlet located approximately 750 feet east of the Stork Screen site on Statesville Road. CEI also observed a tnrcking company located approximately 750 feet north-northeast of the Stork Screen site on Burch Drive. It is not lorown if USTs are present at the tntcking company facility. Ttre human population which may be present at any given time within the area of interest includes, but is not limited to, employees of Stork Screens and the other commerciat/industrial ventures, persons staying at the l&rights Inn, and residents living along Auten Avenue and portions of Riley Avenue and Highland Avenue. Water Oualitv The ground water underlying the site is classified as Class GA waters by 15A NCAC 2L .O3O2. The best usage of Class GA waters, as reported b,y 15A Mr. Allen Schiff August 12,7994 Page 3 NCAC 2L .2O1, is as an existing or potential source of drinking water supply for humans. CEI reviewed the topographic map for the area and noted. that a water impounrlrnent is located approximately I,OOO feet to the north of the Stork Screens ProPerty. Fresh waters of North Carolina are classified as Class C or higher by 15A NCAC 2B .O2tl. The best usage for Class C waters is reported by tJlis regulation to be fishing, secondary recreation, agriculture, and any other usage except primary recreation or as a source of water supply for drinking, culinar5r, or food processing purposes. cEI observed that an intermitteat branch of Inpin Creek originates at the impoundment and flows souttreast from the impounrtment towards h:rnrin Creek. The branch of Irwin Creek enters Irwin Creek approximately 2,OOO feet southeast of the site. Inrin Creek flows southwest from the area and enters Sugar Creek. Sugar Creelc flows soutbward, and eventually empties into the Catawba River north of Fort Mill, South Carolina. Other ttran the Catawba River, CEI is unaware of these surface waters being used for a supply of potable water. Use and Location of Water Supplv Wells CEI conducted a vehicular survey on July 6, 199t4 and observed several water supply wells within 1,500 feet of the site. Water supply wells are located on Auten Avenue, Statesville Road, Highland Avenue, and on the Stork Scteen property. See Figure 2 for water supply well locations. CEI reviewed Mooresville Regional files for water supply well locations on July 7, 1994 and noted water supply wells existing at 1388 Auten Avenue and 4255 Statewille Road. CEI believes ttrat these two wells are duplicates of wells obsen ed during the vehicular sunrey. The water supply well located at the Stork Screen facitity is not in use. Additional information concerning water supply wells was submitted to NCDEHNRin a report dated July 14, L994. Municipal potable water and sewerage appears available throughout the area of interest as evidenced by the presence of water meters, water valve boxes, and sewer manholes. CEI contacted the Charlotte-Mecklenburg Utility District (CMUD) and learned that the area of interest is served by the CMUD. Mr. Allen Schiff August L2, 1994 Page 4 Monitorine Well Installation On JuIy 2L, 1994 CEI supervised the advancement of 7 soil borings (SB- 2 through SB-8) at the Stork Screens facility. Five soil borings, SB-3, SB-4, SB-5, S8-6, and SB-8, were advanced to 20 feet below land surfrace (bls) and 2 soil borings, SB-2 and SB-7, were advanced to 50 feet bls and convsted to monitoring wells. Monitoring wells MW-2 and MW-3 were respectively completed within soil borings SB-2 and SB-7. The borings and monitoring wells were installed by McCall Brothers Drilling Comparry. See Figure 3 for the soil boring locations and Figure 4 for the monitoring well locations. Eadr of the newly installed monitoring wells were completed at a depth of 50 feet bls. Ttre monitoring wells were constnrcted with 20-foot long sections of 2-inch di4rneter, 0.010-inch slotted, polydnyl chloride (PVC) well screea. TLre well screen was set from 30 feet bls to 50 feet bls in each monitoring well. A 30 foot long section of 2-inch diameter PVC well casing was connected to the well screen in each well and extended to the land surface. An artificiat filter pacL consisting of sand was placed around and above the scteen in each well from total depth of the well to 2 feet above the top of the well screen. A t$/o-foot thick bentonite seal was placed in each well above the artificiat filter padr and the remaining annulus was grouted to land surface with a portland/beatonite slur4r. Ttre well head for each monitoring well was completed with a 2-foot by 2- foot by 4-inch thick concrete pad, 8-inch bolt-dorrm manhole, and tocking watertight cap. Silts and clays gpical of the Piedmont Geologic Province werc encountered during borehole advancement. Red-orange clayey silt was encountered from the surface to approximately 16 feet bls and tan-green-gay clayey silt (saprolite) with red-orange clayey silt was encountered from approximately 16 feet bls to 50 feet bls. Relic bedding feahrres were observed in a split-spoon 5amples collected from soil boring SB-2 at approximately t6 feet bls. The analytical results of soil sarnpling were reported by Pace, Inc. and is attached to this report. The soil samples were analyzed for total petroleum Mr. Allen Schiff August L2,1994 Page 5 hydrocarbons by EPA Method 3550 analyzed for hexavalent chromium. and 3550/8015. CEI also had the soil The analytical results were reported by Pace, Lrc. to be non-detect or "ND" for requested parameters. On July 22, L994, CEI measured depth to ground water and conducted a well survey level run in order to evaluate a direction of ground water flow. Table 1 provides the measurement collected from the survey run. Accordi'rg to the information obtained during the water lwel measurement ev61t, the apparent direction of ground water flow is to the southeast. See Figure 5 for the Apparent Ground Water Flow Direction Map. CEI collected one ground water sample to determine the validity of SPATCO chromium srmpling event, from the previously installed monitoring well, MW-l. CEI collected a field filtered and an unfiltered grouud water earnple. Ttre analytical results for the unfrltered sample were reported by Pace, Inc. to be 43 mgll (milligrams per liter) for hexavalent chromium and 35 mg/l for trivalent chromium. Milligrams per liter can also be extrrressed as parts per rnillisl. Hexavalent chromium and trivalent ctrromium concentrations in the filtered ground water sample was reported to be 46 rrg/l and 34 orgll, respectively. The state action level for chromium in ground water is 0.05 mg/l. Attached to this ISC is a copy of the analytical results. Summanr . CEI observed sweral water supply wells within 1,500 feet of the Stork Screens site during the vehicular survey. CEI noted two water supply wells within 1,500 feet of the site during the water well records search condusted in NCDEHNR Regional Office in Mooresville. A water supply well which is not in use is located on-site. . CEI observed two possible off-site contaminant sources within 1,500 feet of the site, a Shell gasoline retail outlet and a tmcking comPany. Mr. Allen Schiff August L2, 1994 Page 6 . CEI supervised the advancement of seven soil borings at the Stork Sc-reens site. The soil borings encountered silts and clays tSpical of tJle Piedmont Geologic Province. T\nro of the seven soil borings were advanced below the water table for completion as monitoring wells. . La.boratory analysis of soil did not detect total petroleum hydrocarbons or hexavalent chromium. Laboratory analysis of the ground water sample indicated trivalent chromium and he>ravalent chromium aborre state action levels. . Ttre apparent direction of ground water flow at the Stork Screens site is to the southeast. If you have question or cornrnents regardiag this report or project, please contact us at (7041845-2000. 'AL, r![C. t28L J,AT John T. Burkart Project Manager Vice President of Operatioas Dl\win\storkl.doc Sincerely, o d C) r{ko d B $rod\o oq N\o roqor.- 0) H!)L odc) =ka) rd B \fqo(Y) ro\o C,l !. cjN € o C6 0) hI ul ado oqoo \oc? F.o oo olq or Or € I N lri clq TD oq !o tqf- oqt @q\r oc! lf) ot o oH o oqto a?to + oqt o? \f o CII{oo0)o !oIKE(l)-lge.ra bE E !B E 38|y')HFF{ E aoLbl IF ht o CUo IF 7o b/ (v) IF = hl o(!o (Y) IF birop lio koo .jbiia.lc rq uo I OdXrr.l t ,ita +J .lF: EFoo E okhl c-f!F h/ 6do clIFE i HPs: € q i =! o H!o E E g }EH4t'Ioa \ \_/ vrrrl€Root(uAY . I.EGE}ID' -: I park fi tntcrstate, Turapike\r' Population Ccoter Sbect, Road f, - HuryRaup tvtajor SrectrRoad -InterstarcHighumy - River ENGINEERS GEOLOGISIS SCIENIISTS STORK SCREENS WELL SURVEY STORK SCREENS 3e01 I-85 NoRTH CHARLOTTE. NORTH CAROLINA ALE: I : 15,6?5 FIGURE: 2 zoF uo-t(,z &60zElE{r{oda c, Itrlth o t@.l tEta 5}E.a 2 I @ An L_l FIzlEl I =ltI>l4to.l l-o Eoaf'f =frl>FJ<-F>fiqx<6EH ea.Fii o- otE<O<-z = -I-=loo F.lt:,F.-< Yz J 2 () Uz>q o5FEaIYdC) J@ z,Oe&{89 d;kila<o >o.o=rlt 9092 J5 tnzF<(n? = \ \ rI]F o UIFgFzlrJoV' V,,-vl (9oJour(9 oGL,L, =(,zL, o. =zo F L)oJ (,zEoIE Iou, d = LJE E,-H =zU'B1tt;f.lGd BB Y0.o ln vEoLh 2 = ts- u.'1 E* 5 0.m FIzlfrf I>lf:l I>l<l0-l Eeo oarrl A T l':Iz.rdb |4z J z (J 2ae.4-i E:l I 3=Ea<o \o-o=r,J20a Jo cazF<a, = tnFtn FzLlJ6tn aFl/t(,oJol.JI ooaIJLJz(9zl.J { l-r Rkl Ra z o o F&oz F 3tr () () =d ez 2q EI o()ra(\le,EEoFo F i U: c a;z! ts- zoz.tr9 g- JgE JE_El =tL !i -:- 'tr- ==(, == :i- Z, =^ 2 .-,2E^-E.=r,9>*z.iE ==F 3=;OEE=g =e=u5 et 'c11 c,-i=b \E \i'6 =(D-@ 5 4Eh o J\r-T1 il' z,lf.I I =lE:I>l<lo. bo ET(,a91 e,l+- = jor rOlq=c=F 'oqo &r(,zE:lL Y J OO1>"Et E=o= o=r3z A@ZILO MEril -E E-Fd fElEL<=<-a oFtn g Qan o 9(,o oLJo tl,etr,lLJz6ztr, E,frlF =oz z o (J Fgoz ()z o=c,ir'I=ez 2qtd:lil&- BBvEI llt ffi BEPOBT OF TABORATOBY ANATYSIS lr{t lssuilict 0t 0ulurt August 08, 1994 ilr. John Burkart Cooper Environmental, Inc. 2300 Sardis Road North, Suite QCharlotte, NC 28227 RE: PACE Project No. 64A7?5.502CIient Reference: 94105-Stork Dear Mr. Burkart: Enclosed ls the report of laboratory analyses for samples recelved July 25, 1994. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel freeto contact us. Sincerely, L/* L /*.--.b*.--(rls H. Kommalan ProJect Manager Encl osures 8E00 lhoy Imr* $irr 100hnnrnr rc il078 tlL: ?0&trE.90t! FAI: 70tt875.9091 rnEqd0mnnfir&dryu ffi REPOBT OF LABOHATOBY ANATYSIS a rt€ rssuirflct 0f oulr,rTY Oroor., Environmental, Inc. 2300 Sardls Road North, Suite Q Charlotte, NC 28227 Attn: ilr. John Burkart Cl ient Reference: 94105-Stork PACE Sample ilumber: Date Collected: Date Recelved:Cllent Sample ID: Parameter August 08, 1994 PACE Project Numberz 640725502 92 0237960 07120194 071251s4 sB-2 I'll,l-2Units ilDL 9'-10.5' fiffH00 DATE ANATYZED ORGANIC A}IALYSIS INDIVIDUAL PARAT.IETERSrxtiaiiion - Hyaiocarbons as Diesel 072694' 35s0 9I-1.?9.1.91Fercint Solids' % 0.01 70 071271e4 Petroieum Hydrocarbons as Dlesel mg/kg 5.0 ND 3550/8015 07126194 t& lhcry lilrr &rt! 100lhcrlr lG 28078l& r0+olr0r2 FrI; 70+87t.90il An€CrdomfinfyArybIr ffi REPORT OF LABOBATORY ANALYSISrxf rssuirict 0r 0uarlrr Orr. John BurkartPage 2 Cl ient Reference: 94105-Stork PACE Sample Number: Date Collected: Date Recelved: Cllent Sample ID: Parameter August 08, 1994 PACE Project Number: 540725502 92 0237978 071201s4 07l25le4 sB-2 l.ltl-2Units MDL 18'-20' l,lETll0D DATE AI{ALYZED ORGANIC ANALYSIS INOIVIDUAL PARAI{FTERS Extractlon - Hydrocarbons as Diesel 072694 3550 07126194 Percent Sollds % 0.01 62 07127194 Petroleun Hydrocarbons as Diesel mg/kg 5.0 llD 3550/8015 07126194 3Em IhEry &,rr, &ir 100krcrdr. XC 2t0r8I& ro+ottou tA* 70+t75.mgr &EqOSpo'tnryEneh|r nss3,BEPOHT OF TABORATOBY ANATYSIStxt rssuirxct 0r 0uluIr l.lr. John BurkartPage 3 Ctient Reference: 94105-Stork PACE Sample Number: Date Collected: Oate Received: Cllent Sample ID: Parameter ORGANIC ANALYSIS August 08, 1994 PACE Project Numberz 64A725502 92 0237986 07lztle4 a7lzsle4 sB-3 18'-20'Units UtO ns/k9 I'lDL I.IET}IOD DATE AIIALYZED INDIYIDUAL PARAI,IETERS Extractlon - Hydrocarbons Percent Sollds Petroleum Hydrocarbons as as Diesel Di eseJ 0.01 5.0 072794 74 lrD 3sso 071271e4 071271e43s50/801s 07128/94 g8S ltcr &m. Srdr 100hrrra. IC 28018I& rotlolsn FAt 70+t7t.t00t &EqtcS'onntyAnpbylf R(!33,REPOBT OF LABORATORY ANATYSE lxE rssurrrct 0t 0u^rttr [1r. John Burkart August 08' 1994 Page 4 PACE Proiect Numberz 640725502 CI ient Reference: g*tOs-Stork PACE Sample Number: Date Collected: Date Recelved: Client Sample ID: Parameter 92 0237994 07lztle4 07123/e4 sB-3Units UDL 5'-7' MffH0D DATE AMLYZED ORGA}IIC ANIILYSIS INDIVIDUAL PARAI{ETERS Extractlon - Hydrocarbons as Diese'l 072794 3550 07127194 Percent Sollds % 0.01 8l 07127194 Petroleum Hydrocarbons as Dlesel mg/kg 5.0 ND 3550/8015 07128194 e800 rhur lm. S{tu 100lluocrlr. tlg 2t0raI& ror{r}t0ir FA* '0+€?5.8091 An hrd 09e0]t!dty &pbytt f,,(!s3,REPOBT OF LABORATORY ANAIYSElxt Assuilict 0t 0ulutY I'lr. John Burkart August 08, 1994Page 5 PACE Project Numberz 640725502 CIient Reference: 94105-Stork PACE Sample Number: Date Collected: Date Recelved: Cllent Sample ID: Paraneter 92 0238001 07lztlel 07lzsle4 sB-{Units ilDL 5'-7' tlETllOD 0ATE AIIALYZED oRcA{rc AMLYSIS INDIVIDUAL PARAIIIETERS Extractlon_- Hydrocarbons as Diesel 072794 3550 07127194 Percent Sollds % 0.01 74 07127194 Petroleum Hydrocarbons as Diesel mg/kg 5.0 ND 3550/8015 07128194 88@ fhry A,rur, Sub 100llurmlr llC 28078r& ?0logmnrl* 70&87l.t8r ln hOomoadtySndotfir nss3,BEPORT OF LABORATOHY ANALYSIS tx€ rssuirtcE 0f 0uAUIr Hr. John BurkartPage 6 Client Reference: 94105-Stork August 08, 1994 PACE Project Numberz 64072550? PACE Sample Number: Date Collected: Date Recelved: Client Sample ID: Pararneter ORGAIIIC ANALYSIS 92 0238010 0712t/e4 071251e4 sB-4Units !,lDL 18'-20' ilEffiOD DATE AI{ALYZED INDIVIDUAL PARAI,IETEN Extraction - Hydrocarbons as Diesel 072794 3550 07127194 Percent Sollds % 0.01 77 07127194 Petroleum Hydrocarbons as Diesel mg/kg 5.0 ND 3550/8015 07128194 08S lh..t |rrl* Sdh 100hnm*, tt0 28078 lBs r0a{7Gt0g2 rA* 704{75.e0sr A,t Eqlc Soofint, BnCoyu ffi BEPORT OF LABORATORY ANATYSIS lxt rsSuilr{ct 0t 0urIrIr Hr. John BurkartPage 7 Cl ient Reference: 94105-Stork August 08, 1994 PACE Project llumber: 64072550? PACE Sample Number: Date Collected: Oate Recelved:CIlent Sanple ID: Parameter ORGANIC NALYSIS 92 0238028 07latle4 a7lzsle4 sB-5Units I'IDL 18'-20' }|EIHOD DATE ANALYZED I I{DIVIDUAL PARA!,IETERSfitractlon - Hydrocarbons as Diesel 072794 3550 9U.?7-1.9^lPercent Sollds- % 0.01 80 07127194 Petroleum Hydrocarbons as Diesel mg/kg 5.0 ND 3550/8015 07128194 $00 fE kn,Srtu 100kildr, tG 2t078I& r0+tru.10t2 FA* 70&t?5.gmr ftr EqCo0gortdvEmelo,.t nssg,BEPOBT OF IABOBATORY ANAIYSE rll rssuilicE 0f 0uruIr lnr. John BurkartPage 8 Client Reference: 94105-Stork PACE Sample I'lumber: Date Collected: Date Recelved: Cllent Sample ID: Parameter August 08, 1994 PACE Project Number: 540725502 92 0238036 07lztls4 071251e4 units l,tDL i3;!ro' ilEmoD DATE ANALyZED ORGA}IIC ANALYSIS INDIVIDUAL PAMilTTERS Extractlon - Hydrocarbons as Diesel 072794 3550 07127194 Percent Solids % - '' 0.01 8t 07127194 Petroleum Hydrocarbons as Diesel mg/kg 5.0 ND 3550/8015 07128194 3800 fnr InL &dr 100ltluttr. [c2t0rt tEu 70+t?$t092fl* ,0+875.909r An EsCog0rtrttyBa0by!. assS REPOHT OF LABOHATOHY AIUAIYSElxl lSsurrict 0t 0uruIr Orr. John BurkartPage 9 Client Reference: 94105-Stork PACE Sanple Jlumber: Date Collected: Date Recelved: Cllent Sample ID: Parameter ORGAIIIC AIIALYSIS INDIVIDUAL PARA!{FTERSExtractlon - Hydrocarbons Percent SoIlds Petroleum Hydrocarbons as Units I'lDL August 08, 1994 PACE Project Numberr 64A725502 92 0?38044 07lztleL 07lzsle4 sB-7 Mtrl-3IO'-12' UTruOD DATE AI{ALYZED as Diesel Dlesel Ulo mg/k9 072794 78 ND 0.01 5.0 35s0 071271e4 o7l27le43550/801s a7l28le4 geo rbc? fte.. tdh t00hmrrfl E l80rlIAi r0+Ol.a0tl fAk ?0tt{75.909t rnEscoggort dtyffirr ffi BEPORT OF LABORATORY ANALYSIS lrf rssuirrcE 0t 0urilrr r. John Burkart Page t0 CI ient Reference: 94105-Stork PACE Sample Number: Date Collected: Date Recelved:Cllent Sample ID: Parameter ORGA}IIC ANALYSIS INDIVIOUAL PARAfiFTERS Extractlon - Hydrocarbons Percent Soltds Petroleum Hydrocarbons as August 08, 1994 PACE ProJect Number: 640723502 Uni ts l,lDL 92 0238052 07l2rle4 071251e4 sB-7 ill,l-3 20'-22',UETHOD DATE A}UILYZED as Dlesel Diesel atlo mg/kg 080294 65 ND 0.01 5.0 3sso o8lo2l94 071271e43ss0/8ors 081021e4 $0 hr hal &tr 100lrmlrra. ilC 2t07ErE r!+fr3.$n Fr* 70rt7t900r AnEcCQfamtyffipr ffi REPOHT OF LABORATORY ANALYSIS rrt tssuilxcE 0f 0urutl Ot. John Burkart Page ll CIient Reference: 94105-Stork PACE Sauple Number: Date Collected: Date Received: Cllent Sample ID: Parameter August 08, 1994 PACE Project Numbert 6407?5502 92 0238060 a7lzrle4 07lzsle4 sB-8Units I'IDL 5'-7' l,lEll{00 DATE AMTYZED ORGAI{IC AilALYSIS IND IVIDUAL PARII.IETERS Extractlon - Hydrocarbons as Diesel 080294 3550 W.9U.2lPercent Soltds' % 0.01 78 07127194 Petroleum Hydrocarbons as Diesel mg/kg 5.0 N0 3550/8015 08102194 $m fEr tu. Sdr 100llutrrar tlC 2!078fE: ?83fr}@fi& r0+879.80il An €snlhcteilt€nFloylr ass"3,BEPORT OF LABORATOBY ANALYSE IxE lssuilIct 0t 0urltIY ;l4r. John Burkart Page 12 CIient Reference: 94105-Stork August 08, 1994 PACE Project Number: 640725502 92 0238079 07lztls4 0712s/e4 sB-8Units l.lDL 20'-22' ilfiH0l, DATE AI{IILYZED PACE Sample Number: Date Collected: [)ate Recelved:Client Sarrple ID: Parameter ORGANIC A}UILYSIS INDIVIDUAL PARAI-IETERS Extractlon - Hydrocarbons as Diesel 080294 3550 08lAZl94 Percent Sollds % 0.01 80 07127194 Petroleum Hydrocarbons as Diesel mg/kg 5.0 ND 3550/8015 Wl02l94 $O ecr, &rn, Srtu t00hmir, [C 2!078I& ?ta{r}t0lln& r0+t75.909t An ECrd ofortdy Euoylt ffi BEPOBT OF LABOHATOBY ANATYSIS or,. Page Ir: rssuilrcE 0, 0urUlr John Burkart l3 Client Reference: 94105-Stork PACE Sanple l{umber: Date Collected: Date Received:Cllent Sanple ID: Parameter INORGANIC ANALYSIS II{D IVIDUAL PAMIiIETERS Chromium, Hexavalent Units ns/L 0.02 ND August 08, 1994 PACE Project llumber: 6407255A2 92 0238338 071201e4 071261e4 sB-2 litt{-29'.10.5' I{ETHOD DATE AI{ALYZEDrry- 7196 07l27le4 MDL 38S frt h, Srf! t00hmtrt ll0 2!0rttE; r0a{r+t0t2 FrB 70+87$E0gr &@WyBumrs ffi HEPOBT OF LABOHAT(]BY ANATYSF Hr. John Burkart Page 14 Cllent Reference: 94105-Stork PACE Sample Number: Date Collected: Date Recelved: Cllent Sample ID: Parameter INORGANIC ANALYSIS INOIVIDUAL PARAI.IETERS Chromium, Hexavalent Units mg/L 0.02 ND August 08, 1994 PACE Project Number: 640725502 92 0238346 07l20le4 07126194 sB-2 Mtl-218'-20' I{ET}IOO DATE AiIALYZEDTTI- 7te6 071271e4 I'IDL t8ll0 lhcr, hr. Stfit 100Itaratar tlG 28078I& 70+O&St2 f0(: 704.875.9091 An &udofpoftsdt, Emehylt PSl33,BEPORT OF TABOBATOBY ANATYSIS lr,lt lssuirrcE 0f 0ulUIr o I'lr. John Burkart Page 15 Client Reference: 94105-Stork PACE Sample l{umber: Date Collected: Date Recelved: CIlent Sample ID: Parameter INORGANIC ANALYSIS INDIVIDUAL PARAT,IETERS Chromium, Hexavalent August 08, 1994 PACE Project Number: 640725502 Uni ts MDL nglL 92 0238354 07lztle4 07126/e4 sB-3 18'-20,Gl--MET}IOD DATE AN'ILYZED 0.02 ND 7196 07 /27le4 f@ fhcl lrar l}rlr 100Itrrrll*. ilc 2E078T& r0+rru.$!2tr& 70&875.9091 fn Equ.l oggofrnty @ot/rt ass3,HEPOHT OF TABOHAT(]RY ANALYSE - llt rssu8lrrct 0f oulr,ltY August 08, 1994 PACE Project Numberz 640725502 92 0238362 07l2ue4 07126ls4 sB-3Units l4DL 5'-7' UEIE9O DAlE_AlLl.YZEqTTT- INORGANIC ANALYSIS INDIVIDUAL PAMT'IfiERS Chromium, Hexavalent ng/L 0.02 ND 7196 07127194 Hr. John Burkart Page 16 Cllent Reference: 94105-Stork PACE Sample Nunrber: Date Collected: Date Recelved:CIlent Sanple ID: Paraneter 9tm frr &rrr Srrb 100 tfinandla rc 2E0r8T& roadr$ror2 Fl& ,0+Er5.90gt An Ecld oDFtlrly Bttdoytr ffi BEPOHT OF LABORATOBY ANATYSE IXt ASSUiI'rCt 0f 0uruIt O *r. John Burkart Page 17 Client Reference: 94105-Stork PACE Sanple Number: Date Collected: Date Recelved:CIlent Sample ID: Parameter August 08, 1994 PACE Project Numberr 6407255A? 92 023837007lztle| 071261e4 sB-4Units lllDL 5'-7'GI-I{FTI{OD DATE A}IALYZED INORGANIC ANALYSIS INDIVIDUAL PARAfiTTERS Chromium, Hexavalent mg/L A.AZ ilD 7196 All27l94 0m fhc.? lilc& $i! 100fimtrflr tlG 280rtl& ro+t $t0t2 Fr* ,0&8r5.909t Xr ESC 09g6td, &tglotrt PSl33,BEPOBT OF LABORATORY ANALYSE IXI lssurrxcl 0t 0ulr,ltY Mr. John Burkart August 08' 1994 Page 18 PACE Proiect Numberz 640725502 Cllent Reference: 94105-Stork PACE Sample Number: Date Collected: Date Recefved: Cllent Sample ID: Parameter 92 0238389 07lLtle4 071261e4 sB-4Units MDL lg'_:?A' ilETH0D DATE AI{ALYZEDrI)- INORGANIC AMLYSIS IND IVIDUAL PARAI,IETERS Chromium, Hexavalent ng/L 0.AZ ND 7796 07127194 9800 E:rt frrr Stto 100ttilrd.. tC 2t0r8t& ,I}rsror2 rAr 70&t7l.s0$ rnEqaomltl*yS@yl ffi HEPOBT OF LABOBATI)BY ANALYSIS IXt rssuiAilct 0t 0uAUIt Mr. John Burkart Page 19 Client Reference: 94105-Stork August 08, 1994 PACE Project Numberz 640725502 92 0238397 0712t194 071261s4 sB-5Units MDL l3,-2A' fiEfiO0 DATE AllltLYIEDTI}- ms/L 0.02 ND 7195 07127194 PACE Sample l{umber: Date Collected: Date Recelved: Cllent Sanple ID: Parameter INORGAI,IIC AT{ALYS IS INOIVIDUAL PARA!{ETERS Chromlum, Hexavalent 8lm hr A,ui S 100lhflr, rlC 21078l*,0+l76t0ttilx m+t7!.gogr ra&dSptnnyhtCrytt ffi BEPOHT OF LABORATOBY ANALYSIS IXE ASSUTTtCE 0' 0UruIt I'lr. John Burkart Page 20 Client Reference: 94105-Stork PACE Sample Number: Date Collected: Date Recelved:Client Sample ID: Parameter August 08, 1994 PACE Project Numberz 640725502 92 0238400 07lztl94 071261e4 sB-6Units l.|DL 181-?q' ilETHOD DATE AIIALYZEDrry- : I},|ORGAI{IC AI'IALYSIS II.ID IVIDUAL PARAI{ETERS Chromium, Hexavalent nglL 0.02 ND 7196 07127194 1800 h, filrnr trtu 100 lluaonrf. m Z$71 tEE r0+fr$r0r2 Fl& 70+875.909r An Eqd oeDcuuy Endo,lt n,$ce BEPORT OF TABOHATORY ANATYSE or,. Page Ixt lssulllrcl 0t 0ulutr John Burkart 2l Client Reference: 94105-Stork PACE Sample l{umber: Date Collected: Date Recelved: Cllent Sample ID: Parameter INORGANIC AMLYSIS I}IDIVIDUAL PARAfiETEN Chromlum, Hexavalent August 08, 1994 PACE Project l{umber: 640725502 92 0238419 07l2ue4 07l?61e4 sB-7 Mtf-3Units l'lDL 10'-12' _ UEIHQD 0AIE-MLIZEDru.- mg/L 0.02 ND 7196 07127194 9E08 err }e1 S.ir 100llmnr-, tG 2t0r8IIL r!+Or.r0r2 tAk 70&t7l.gmt fn Eqd opcorldt Er4bylr ffi BEPOBT OF LABOBATORY ANALYSE IHf rssunrtct 0r gurUrt August 08, 1994 PACE Project Number: 640725502 92 0238427 07l2rls4 07126le4 sB-7 !{l,l-3Units }lDL 20'-22' l{EfH0D DATE A}IALYZEDrry- ms/L 0.0? ND 7196 07127194 O.. John Burkart Page 22 CIlent Reference: 94105-Stork PACE Sanple ilumber: Date Collected: Date Recelved:Cllent Sample ID: Parameter II.IORGANIC AMLYSIS INDIVIDUAL PARAI{ETERS Chromlum, Hexavalent 988 lho,4,.8, Srnn 100ItmndL IrC 28078IE r0+olt0t2 Fr* ,0&t7t.909t /Lt&rrdomodrrryEnptolr ffi HEPOHT OF LABORATOBY ANALYSE Orr. John Burkart Page 23 Cl ient Reference: 94105-Stork PACE Sanple ilumber: Date Collected: Date Recelved: CIlent Sanple ID: Paraneter INORGAT{IC AMLYSIS INDIVIDUAL PARAI,IEIERS Chroalun, Hexavalent August 08, 1994 PACE Project Numberz 640725502 92 0238435 07lztle4 071261e4 sB-85'-7' }IETHOD DATE AMLYZEDrry-Units I,IDL nglL 0.02 ND 7196 071271e4 380lhcr &ul, Srdr 100hmrlN} ilc ttor!IA: r0tst $$nrm r0+t75.3@t raEcdorostlryEmby.r R,ns3,HEPORT OF TABOBATOBY ANATYSIS,Nt rs ulrilct 0t 0ul!L I'lr. John Burkart Page 24 C'lient Reference: 94105-Stork PACE Sample ilumber: Date CoIIected: Date Received: CIient Sample ID: Parameter ,"'*-" ANALYSIS IND IVIDUAL PARAI'IETERS Chromium, Hexavalent Sample results are reported on These data have been reviewed1A o filillli, ni,lillll l'rn.,i strv argaret S. Harding anager, 0rganic Chemistry Units I'IDL ns/L 0.02 ND a dry weight basis. and are approved for release. August 08, 1994 PACE Project Numberz 640725502 92 0238443 07|?tls4 07126/e4 sB-820'-22' I,IET}IOD DATE ANALYZEO(I).- 7196 07 l?7 le4 9800 lhctr Arurn $rlrr t00&nrrrnr. ilC 28078 IEl,: 70+t7t.l0ll FAX: 70'0.875.909 I All&ulogpoturitrBtnlo/r o ffi HEPORT OF TABORATORY ANALYSF l.lr. John Burkart FOOTNOTES August 08, 1994 Page 25 for pages I through 24 PACE Proiect l{umberz 64072550? Client Reference: 94105-Stork llDL Hethod Detection LimitND l{ot detected at or above the HDL.(l) AII analysis performed on Toxic Characteristic Leachate. 8tO fE kirr Snir 100 lbnotrrL tlG 28078IB: r0+8r$t0i2frx ,00875.90st Atr ftulonprytnitywllt ffi REPORT OF TABOBATORY ANATYSIS Mr. John Burkart QUALITY C0NTR0L DATA August 08, 1994 Page 26 PACE Proiect Numberz 640725502 Client Reference: 94105-Stork Chromium, Hexavalent Batch: 92 ?9499 Samples: 92 0238338, 92 0238346, 9? 0238354, 92 0238362, 92 0238370 92 0238389, 92 0238397, 92 0238400, 92 0238419, 92 0238427 92 0238435, 92 0238443 I'IETHOD BLAIIK: MethodParameter Units MDL Blank ChTomi'jfr; Hexavalent mszf tr.0,2 ND- SPIKE: Spike RecvlTtfrParametertIiFofiffi; Hexavalent I.ABORATORY CONTROL SA}IPLE: Parameter Chromiimr, Hexavalent 920238338 sB-z MU-2 Uni ts ilDL 9'-10.5' Spl kem?r u.Tz NroTr Units ilDLms/f tr32 ReferenceValue Recvlmr wfr 9800 fhot e,rni, Scir. 100 !&nmodb. rG 2m78I& r0+trE.t0!2 FIr* 70t1.875.90il An&rd@rlnrdf Etphyt' ffi REPORT t)F TABORATOBY ANALYSE txt rssunrtcE 0t 0ulutr arr. John Burkart Page 27 Client Reference: 94105-Stork Petroleum Hydrocarbons as Diesel Batch: 92 29587 Samplest 92 0237960, 92 0237978 I,IET}IOO BLAI{K: l,lethodParameter Units MDL BlankEiE]ffi Hydrocarbons as Dlese] mgng 5.T RD- LABORATORY C0I{TROL SAI,IPLE: ReferenceParameter Units l'lDL Val ue Recv P6[r6"iEfr'Hydrocarbons as Diesel nglF?, 53 -T6f -Iffi gtlt0 [hat A,rn, $fir 100 hmautr, ttC 28018IlL: ?0llr+rOsz FA& 70a{75.S09t qUALITY CONTR0L DATA August 08, 1994 PACE Project l{umberz 640725502 Atr&rC0monnilyBlutqtf a$s3,REPOHT OF LABOBATORY ANALYSIS rHt rssuilxct 0t 0urUtr r. John Burkart Page 28 CI ient Reference: 94105-Stork Petroleum Hydrocarbons as Diesel Batch: 92 29718 Samples: 92 0237986, 92 0237994, 92 0238036, 92 0238044 I,IETHOD BI.ANK: ParameterEti6lffi Hydrocarbons as Diesel SPIKE A}ID SPIKE DUPLICATE: ParameterEtio=Iffi Hydrocarbons as Diesel LAB0RATORY C0t'lTR0L SAI.IPLE: Q.r*.t."EtF61ffi llydrocarbons as Diesel QUALITY CONTROL DATA 92 0238001, 92 0238010,92 0238028 August 08, 1994 PACE Project Numbert 640725502 9?02368?3 SolkeTr- r,i,- Splke DupI Recv RPD Uni ts ms/Ts Method BI ankNTMDL !i.3 Units MDLms7Es Il.0 T.,IDL Ei:o Spike Recv3g ix 4ffi ReferenceValue Recv-rrr -Bg S800 thct, 4,01&dr t00Itma;lr fC 2m78 IEl,: 70tllr&i012 fAk 70't875.900t An qrdopgodrmfiy&r9F'tI n$s3,REPORT OF TABORATORY ANALYSE _ ,xt tssuirtct 0t 0urilIt Cr. John Burkart qUALITY CONTROL DATA August 08, 1994 Page 29 PACE Project Numberz 640725502 Client Reference: 94105-Stork Petroleum Hydrocarbons as Diesel Batch: 92 29745 Samples: 92 0238052, 92 0238060, 92 0238079 UETHOO BI.ANK: l.lethodParameter Units I'IDL Bl ankEiidlffi Hydrocarbons as Diese'l mgZEE 53 flf SPIKE AND SPIKE DUPLICATE: 920238052SB-7 Splkelltr-3 Splke DuplParameter Units UDL 20'-22' Spike Recv Recv RPD -LAB0RAT0RY C0i{TR0L SAI,IPLE: ReferenceIP.r*"t.r Units MDL Yalue RecvIEffi]ffi Hydrocarbons as Diesel mTzkg 53 -5U- -6If 9800 fur Alrtrl. Suir 100 Itnoratlr. ffi 2t078T& m+ol.totz Fl* 70&t75.90il An E$C Sportrtrdty Endolis ms3"BEPOBT OF TABOBATI]BY ANALYSElxt ltsutrtcE or 0urUrr l.lr. John Burkart FOOTNOTES August 08, 1994Page 30 for pages 25 through 29 PACE Project Number: 640725502 Client Reference: 94105-Stork l,tDL ilethod Detection LimitND l{ot detected at or above the l.lDL.RPD Relative Percent Difference $00 fh6? &n . &lh 100ltnrrrf, iC 2E0rtI& r0+t?s!0r2n& 70+8r5.c0gt &EqlcopeatilyErEtqlf C.\. \. \Y a_ :/Jsq, o c0s?.- tccQ $fiHfi fifi fi a CE tuE,azoFo EFa =Eolrt!o cn UJoE UJ Eltr IJIluo :(_) (*bv -J, )-S q-t+-{/\Js- s5' itiooooDo 3r,0,:c,oE S S$ ctz o oz \6 N \a{a:\ A-J P do?) o g d-i- n Yx+i rt,fir f{ :l z CEg tD !o E ( Y ooa6 o, =l(JioiEI o-lolotdtel .ri ,C,I $+ sNl B--/.1 =€l6=lC' EIE6lEBIEfl o IEoolrlE ool-o =o ri.oIz .Lo e lt'- C\Jrlf-s-l ffi REPOBT OF TABOBATORY ANALYSE TI: lSSUtrnCl 0r 0UlrlIY August 09, 1994 tlr. John Burkart Cooper Envlronmental, Inc. 2300 Sardis Road North, Suite QCharlotte, NC 28227 RE: PACE ProJect No. 640726.507 CIient Peferenre: 94105 Dear ilr. Burkart: Enclosed ls the report of laboratory analyses for samples received July 25, 1994. Footnotes are glven at the end of the report. If you have any questions concerning this report, please feel free to contact us. Slncerely, A;-LL,*t^^.-- Krls H. Konrnalan ProJect lilanager hnc I osures 8e fEf, rrm. $ritr 100 llmm,*. rG ZmrSlll,: ,0*t &t!12tl* 70'!t75.9091 AoE$.1&rtdrffi l?sls3,BEP(]BT OF IABI]HAT(]HY ANATYSE fxt rssuilic! 0f 0uailIt Oroor." Environmental, Inc. 2300 Sardis Road North, Suite QCharlotte, NC 28227 Attn: Mr. John Burkart CIient Reference: 94105 PACE Sample l{umber: Oate CoIIected: Date Received: CIient Sample ID:Parameter Units August 09, 1994 PACE Project Numberz 640726507 9? 0?38737 071261e4 071261s4 lrt{- tMDL Filtered I'IETHOD DATE ANALYZED INORGANIC ANALYSIS INDIVIDUAL PARAI,IETERS Chromium Chromlum, Hexavalent mg/L ms/L 0.010 0.02 200.7 7196 08loels4 07127194 34 46 e800 ec., &rnr. Suir 100lhnraflr nC 28078 rtL r0+fr&r0t2 rAr ,0&875.t0st tu €$nl 0rporunrty EmConr n,ns9,BEPORT OF LABOBATI]BY ANATYSIS fr.. John BurkartPage 2 C'lient Reference: 94105 PACE SampJe Number: Date Collected: Date Recelved:Cllent Sample ID: Parameter IHE rSSUirICt 0t 0uruII August 09, 1994 PACE ProJect Number: 640726507 92 0238745 07126/e4 07126ls4 Ml,l-tUnits MDL Unfiltered I'|ETHOD DATE AI{TILYZED INORGANIC ANALYSIS INDMDUAL PARAI'IETERSChromium mg/L 0.010 35 200.7 08109194 Chromium, Hexavalent mg/L 0.02 43 7196 07127194 These data have been reviewed and are approved for release.4a Charles il. Cabaniss l4anager, Inorganlc Chemistry 9800 Xhcrr &m. &rftr 100l*nomil ilC 2t0ra IEl,: ?otStr5.t0tz FA* 7llr0-871.9091 tu Eqtd ogpmmiuEmdqlt ffi REPORT OF LABOHATORY ANALYSE Mr. John Burkart FQQTNOTES August 09, 1994page 3 for pages I through 2 PACE Proiect Numberz 640726507 Client Reference: 94105 I'IDL l,lethod Detection Llmit 8800 ficry kur. Sont 100Itnnr} tC 28078l& r0+t7t tott rA& 70e875.S08r fn EqO omortstty Ernploylr nslsS REPOBT OF LABORATORY ANALYSIS rflt rssuirNct 0f 0urUt, I'lr. John BurkartPage 4 Client Reference: 94105 Chromium, Hexavalent Batch: 92 29499 Samples: 92 0238737, 92 0238745 MF'H,D BLANK: HethodParameter Uni ts MDL B'lank C[ro'ni6 Hexava'lent mgTf- m2 NII- SPIKE: Spi keParameter Units MDL 920238338 Spike Recv crr-o',illum; Hexavatent ms/r- 6.3;2 ND- CIr TZT* QUALITY C0NTR0L DATA August 09, 1994 PACE Project Number: 640726507 ReferenceVaIue RecvTIT I2OT I.ABORATORY CONTROL SAI'IPLE: df;i#ittr Hexavarent Unitsmsrr MDL 0'32 g8m [hcr1 &]rr. &in 100lfimrrtlr. tlC 28078lEL:,0+t t.90gt FAx: 704.875.909t A0 Ecurl opporn try &rCoylr ffi BEPOHT OF LABORATORY ANALYSE IIt rssurrict 0f 0ururt Mr. John BurkartPage 5 Client Reference: 94105 ICP QUALITY CoNTR0L Batch: 92 29672 Samples: 92 0238737, 92 0238745 METHOD BI.ANK: Parameter QUALITY CoNTR0L DATA August 09, 1994 PACE Project Numberz 640726507 Units tlethod Bl ank , INDIVIDUAL PAMT'IETERS Cal ci um ilagnesi um I'lolybdenum Potassium Sodl um ICP QUALITY C0NTRoL t{ickel Cadnium o[:ffi.'*Barlum Copper Chroml um Beryl I i um Zinc Coba'lt Iron Si I ver Manganese A]uminum ns/L ms/L mg/L mg/L mg/L tnglL mg/L mg/L mg/L ng/L mg/L mg/L mg/L mg/L ms/L mg/L ms/L mg/L m9/L Uni ts mg/L ms/L rng/L mg/L mg/L 0.10 ND0.10 ND0.020 ND0.10 ND0.10 ND 0.010 0.010 0.010 0.10 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.005 0.010 0.010 ND ND ND ND ND ND ND NO ND ND ND ND ND ND LABORATORY CONTROL SAI'IPLE: Parameter INOIVIDUAL PAMIIETERS CaI cium I'lagnesi um l.lolyMenum Potasslum Sodi um 0. t0 0.10 0.020 0.10 0. l0 Reference Val ue 5.0 5.0 0.500 5.0 5.0 Recv 98r 96r l05r 86r 100,5 1800 lhor |rru. $in 100X{rrrfl} tlG 280rEr& r0+t?l.t0l2 FA* 70t1.875.9091 Xt&rdop9ofiu{f tfi0t|y',t R$33,REPOHT OF IABORAT()BY ANALYSIS ., trt rssuirrcE 0r 0uluTt Orr. John BurkartPage 6 Client Reference: 94105 ICP QUALITY Cor{rRoL Batch: 92 29672 Samp'les: 92 0238737, 92 0238745 LABORATORY CO}ITROL SA}IPLE: Parameter rcP QUA!-ITY CoNTBCL Nicke] Cadmlum Vanadium Lead Bari um Copper Chromium Beryll ium eil:,.Silver I'langanese Aluminum QUALITY CONTROL DATA August 09, 1994 PACE Project Number: 640726507 Units Reference Val ue Recv mg/L mg/L n9/L mg/L ms/L n9/L ns/L mg/L mg/L ms/L ms/L ms/L mg/L mg/L MDL 0.010 0.010 0.010 0.10 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.005 0.010 0.010 0.500 0.500 0.500 98r0.500 97,.0.500 l03r0.50 t05r0.500 t08g0.500 t01r 0.500 Nafr0.500 100*0.500 tou0.500 97r0.500 lolx0.050 96r 98r 99X 88@ Iirrr &rrr &ir 100 linundlr fC 28078I& roffin$m FAX '0+87t.g0gt An Equrl 0pprtttriU En bylr ffi BEPORT OF LABOBATOBY ANALYSE Mr. John Burkart FOQTNOTES August 09' 1994 Rage i - for pages 4 through 6 PACE Proiect Numberz 640725507 Client Reference: 94105 MDL l,lethod Detection LimitNI) Not detected at or above the MDL. 8e kq 4,.u. S&. 100llwrrl.llG 28078I& ro+oltsrz Fl& 70+875.909r Ar@@ftntyBmloyrr rc) -l H \ f: rot- CO$ a cc uJ cc s \\> r'/\ o(!oo oEooo(toG, oz o (Ez o S azoFo Et-az E,oIL UJo6 lrJa cE IJJ uJE UJ UJo !oo. .l,oor!o o o oo .9*aFNg)$lO(of\@ olcEl8 ^lli_pl E3=l{e sl HE €Iz* 6l,itE ero< o-l O-,f-.@<f ccrl APPEIIDXK III Water Supply Well Sunrey Report Coopnn Er,mnoNMEt{TAL ENGINEERS . GEOLOGISTS . SCIENTISTS JuIy 14, 1994 Mr. Allan Schiff Mooresville Regional Office NCDEHNR 919 North Main Street Moorewille, North Carolina 28115 RE:Stork Screen America, Inc. Groundwater Incident # 1 1398 Mecklenburg Counff, North Carolina CEI Project No. 94105 Dear Mr. Schiff: Cooper Environmental, Inc. (CEI) is pleased to provide you thls letter concerning our investigation into water supply wells \rithin 1500 feet of tl,e above referenced site. ' Pertaining to your June 22, 1994 letter, CEI reviewed Moorewille Regioaal files for water supply wells, completed a site walkthrough, and performed a vehicle reconnaissance to identify water supply wells. In our file revieur conducted on JuIy 7, 1994, CEI identified at least tlrree wells tlrat are within the boundary of 1500-foot radius. CEI completed a vehicle reconnaissance on JuIy 6, 1994. During the vehicle reconnaissance, CEI identified nine water supply wells. At this time, CEI can not determine if tl:e wells are abandoned or active. Ttrese wells are located on Riley Road, Auten Road, Highland Road, and Statesville Avenue. Please refer to Figure I for the location of the water supply wells. T\nro water supply wells identified during tJre vehicle reconnaissance have frles at the Mooresville Regional Office. Table 1 provides a summary of the water supply well sunrey. 23OO SARDIS ROAD NOR771 . SUITE Q CHARLOTTE, NARTH CAROUNA. 28227 (704) 545-2ooo . FAX 004) 841-890t Mr. Allan Schiff July 14, L994 Page 2 TABLE 1 Water Suppiy Well Survey Stork Screens July 1L, L994 Dcscriptlon File # Address Comrnents Iocatioa * Indicates identilied well with 1500-foot radius + Indicates possible duplicate Attached to this letter is a copy of the water supply wells constnrction logs retrieved in our file review. CEI identified up to six water supply wells within 1500 feet of the referenced site (two which may be duplicates of frle review and vehicle reconnaissance). CEI did not sample the water supply wells because the wells are at the limits of the 1500-foot radius and ground water direction has not Charlotte*ME2481 Statesville Rd WeIldepth 130' Charlotte ME2120 Kendrick Ave Outside 1 500-foot rad.ius Charlotte ME2119 Kendrick Ave Outside 1 500-foot radius Charlotte ME1080 Summit Ave Outside 1500-foot radius Charlotte ME1445 Summit Ave Outside 1 500-foot radius Charlotte*ME1920 Auten Ave Well dept]l 150' Charlotte*unknown 3201N r-85 On Site Chadotte unknown 3140 Riley Ave Not obser,red in file review Outside 1500-foot radius Charlotte unknown 32OL Riley Ave Not observed in {ile review Outside 1 500-foot radius Charlotte unknown Redvnans HaIl Not observed in file rerriew Outside 1500-foot radius Charlotte*+unlcnown 4255 Statesville Well possibly identical to ME2481 Charlotte*+unknown 1388 Auten Well possible identical to ME1920 Charlotte*unknown Hiehland Ave Not observed in file review Charlotti unlarown Riley Ave Vacant lot outside the 1500-foot radius Charlotte unknown Auten Ave Vacant lot outside 1500- foot radius Mr. Allan Schiff JuIy 14, 1994 Page 3 been determined. The only exception is the on site well, which will be sa'npled as set forth below. CEI is currenfly working on completing an initial site characterization (ISC) which wiU include soil borings and possible monitoring well installation. CEI is currently scheduled to drill at Stork Screen America, Inc. on July 20, 1994. Upon review of the s6sfarnin4lt levels, CEI wiil be able to determine if the water supply wells are potential receptors. On July 12, L994, CEI completed a site walkthrough and identified one on site water supply well. Stork Screens America currently is not using thewell. CEI observed that the well is topographically downgradient of the reported release area. T?re well appears to be six inches in diarneter and constmcted with a steel outer casing with galvarized piping installed to a submersible pump. In order to measure and collect a sainple from the well, CEI believes the well piping a:rd pump must be pulled. If CEI does not obsenre constituents detected upgradient, CEI will assist Stork in closing tlre water supply well. It is CEI's understanding that the ISC is due August 8, 1994. CEI \ri[ provide laboratory data of Stork's water supply well, soil samples, and potential monitoring well sarnples. CEI will provide recorn"nendations on sarnple collections for the other water supply wells upon review of groundwater flow . Should you have any questions concerning this survey please contact me at (7041845-2000. w EITVIRONMENTAL, INC. T6rJa^k SincerelR John T. Burkart Project Manager JTB\katcUbl26 i\cEt'rd Project Geologist l-r.rrcllMloN tircc)oMlDV Pa* Intcrstatg Turnpikc Population Center Strcct, Road Hury Ramp - lvlajor SrcetrRoad -IntcrsAte HighwaY - River Scale I : 15,625 (at center) F-rmur6d l--soulffi-{ W/NERMKV1AY ASAJR' STRORK SCREENS WELL SI'RVEY I\,Iag 15.00 Trrc Jul05 10:55:00 1994 aF C i,i iJ i i :1 ,.r,:i i,\, I,r,tr nrZo.cj 9. CAS: l',i: 0tcttr,o* O i- 9Q. iri\ l-lr-i-iil lLlLl'l I ui iits i uilaL AIYU Et/ullui'il lu i,LJUl Oii:ICI CF IYATIR AilD AIR RESOURCES GROUND ITATER DIVISION P. 00. BCX 27687 - RALEIGH, N. C. 2T6IT .n.,1 i: /ii o i.lj )- , / e-v 93L!..t s s9IE91'"- Cge.Uigig:j[9, t. !i:LL LOCATiCfi: (Sl-r:r o s:-rci oi rhe locolioh on bcck ol forn) li€'rtest To.a: Ch: r] Of,il e Z. Cllli;-l: aes,;g33: 423 5 States.]d]]-L T.?rrCGtlAPHY: drgs, vollrr, riap.t hilltsp, tl€l use oF |VELL:Seni-public onra IZ/L) /Z) co€s THrs ",ELL REPLACE A\ EXlSilliG \iELL2 dditiona rorJL oEpTH: 'l 5O - F.iG ryPE oe r,rEaroc{;tglBt8al FO:...ATlOlt SAMH-:S COt.LEaTEo: f-]fes llo. ci Eoss - 3. 4. 5. 6. 7. 8. N PtrPMIT /{, ar 30 -5*- .t ;) ruo}.-802 nite Y/oll lhid(.crreirhr / lt.rEiq-Gffi tO. Gftlr.:f. ori:i @lertol Frun----..,1Q- ri--; .2O, Saf,kfj-t-e-- I l. S.': jit: or3tlt Oicrt.TY6. and Cce;,na Fr...: lo I'l atho i t tz.G.i:vgl: o.r:h Sire lJ3l.ricl Fr{.r._ lo 11. wATEt ZttiESl.:.r!ni: !4 srA:i. '#arEdLlvEu:*]-J-r; -- rcp of :r:inq. b *!oq Ccrin: ic---g-lt. on-"'e :gnd !'rrtoq:' ELEV.Lrr. u":',oi" *.-iiltellilll Y:Elii3pmt: 5 - t,i€r:-.';J OF TESTIi\iil: - Aif Pu$?i.rc ryr7=F L E! €L :.1Q0-- i. ot' e, -..----hotrsot 5 --.tpn'Chi!fiiliaTrOli: T;lr-EIE----Arncun'* cup t rq: E,i, OU.l|.t TY!_._-_ -.-_._T g'\,t i: g :t ArU AE(. F )-- ! ilr r! i€. t7. t8. r9.P€Fli$IENT PUItP:(shob o rl'i:h ol rcll heoit cn boch ol lorrn) oaro rnrron.d 1 ) / 1 lt. -rra.Deep.lte1,L Hct. l&.€rs_ csiocly--I0---(geml *" * lnlst{ o.pih Airlinr oaPlh 20.tliYd Y.]l INFOiUE0 Trli r':t.L OWIIER 0F TlrE oai:; rr/slr?S FeijiJrEd j,ri.n I : ary0 E€COM}iE|.IAT!OI.S 2-LEg- 21.F:r.t!t{s: I do hrrrb; cttlit, rh3l lhis rzil racord is lrue 6!rd erocr' I cr SubCi'ri;iar cnd Lci |'o.i For ni G lr.i itihiie Ccpy.Sff;ce tf iYater and Air Rescurces;gi'.:e'[)tillets Copy; Green'o'r,nefs Copy IT|ELL IEAD COlfPi,ETfON :Brar,r a skeich of the seals, vents, access well head shor,ring casing, pump piping,port, gz'out, and enciosure. J.l f '"1 , f'4n K ,rl w aOi^al ')l , L'rP,ihrl- Ifldll t0CAtI0l[: Draw a location sketch sho'*i4g the di-rectlon and distance of the weIL to at least t,ro (Z) ,aearbJr referenc€ poi!^,,s stlch es road,s, iaterseetions aad. s!36.amq. fd,eatify roads with State Hlgbray road identification uu.abers. Sf" mF--. /t$i ,HEEA.rh: ig/it g:at r : II, itl I -#;i=-'-_- /71r" -t .i.:-l?: WELL RECORD NtjRIH CAROL INA ,/r' t]EPARThIENT t]IVISION t]F g Bax 27M8 - OF }IATER ANI] AIR RESOURCES GROUNI] HATER RALEIG}I, N. C.o D rill ing contractor ,?f:€y'21f -l l.rc- i Ree. llo. 7 -{- Helt Pen:rit }to. 7 O rcrn -t Quadrangl e Ho. County ,.ffP DRILLING t. 2. 3. Locat i on --of fo rnrShow a sketch of I ocat i on on back Addrrrc t','.tl 2c f XA'Yrzln'1-r rr- Topogreshy3 .drarL, slosei [il ltop, v,ul{y('tfit'4' ffa^ ;:;' r",,.iil{'*tl*!,lorr, c*ct"t"'i ? ' lfr '7 ' Rig typr or ncthod fiLi+, Total Deptn I %fr'' ::::"2-Hte-,,.ffi.t,^. d )ff 0es th l}. E 6. 7. I a 8. €rout: -9:*h }latcri al,,",'-GJrLrr.ffit Scrsaa: Oepth Fron - to -' ft. D ian. -in. Typa and openinq I ,1 Llrlrr Tarar vhlch is lr.ft. above land surface. E'lev. i_..- 0ate tz. Yield (ep6) j0 Hsthod of testins - A; 13. Punping trtar Level: af ft' after 'l- htt' at -J4- gon. Iti. Hater Qual itY rcll cterll izrtlon nathod Pernanant Pung: -Typc Hake lnstal tcd- - Date-8 Capac i ty -(gpil) HP. lntakc dapth Airl inc depth Renarks: t5. t6. t7. I do hcroby certify that racord is truc cnd cract. th wcl IIs I CO}ITRACTOR Hhitc copy - Dcpartmant of Yater & Air Resources; Elue-Drillcrs copy; Green-0wncrts cogy' Forn GY- I W rLL U R,I LLI N C:-P U MP I N STALLATT6FT-BOCAT I O N S & D I RECTI O N S ti ,' li i!t:"Address Location : r., 'lif'*/'*"na-lur'ftltY ' tt :*) -'t 4$ {($ie rt Tttttilfr: fi,tIJ **; ,\ I .., .t ';'. i's{,rtltd T LL RE NORTH CAROLINA DEPARTMENT OF NATURAL AND ECONOMIC RESOURCES OFFICE OF IYATER AND AIR RESOURCES GROUND WATER DIVISION P. O. BOX 21687 _ RALEIGH, N. C. 27611 II!9 , * z. 3. 4. ORILLING CONTRACTOR Ntorcsl Torn: sblch ol tfia .1.-! ra r- l,on on boch of form)LOCATIOI.I: ? /ntr 2/zo 2v 6 -5-'Oa Fri ...r-,- "'.. Oil'NER: A00RESSi TOPOGRAPTry: l!'+7F.t{tr.+o.ci+ffiri f lol b. 7. 8. 3. 5. usE oFweur-: J*r fl^ F oarc: 1' 3, L- 73 DOES THIS WELL REPLACE AN EXISTING Y'ELLz TorAL 'EPTH, L D / RIG TYPE oR LtETHoo: FoRMATIoN sAMpLEs coLLEcTED: f-lvEs No.of 8oe CAS]NG: Deolhr,*, D T/2 r. GROUT: Oeolh From--.rii-n-ZA- tt SCREEil: ggg1[ From-lo- tL Tvoe ond Ooenino 12, GRAVEL: 'D.plh Si rc Moleriol From-lo- tl. _--; r3. WATER ZONESUcrlhl: olnside 0iom..-l ro. 14. srATlc vt$,earJlveu.1*ft. m lop ol cosins. r5. 16. CoslnE lsJl-,i:-'1[. obovr lond sutfoce. ELEV DATE IIE YIELO(Epmt puMprNG wATER LEvELz 2 / * otr", -3{l-laour!ot *S--.qe^. WATEROUALITY:- Gr n TETPERATUREfF) - 20. HAVE YOU I}IFORMEO THE WELL OWNER OF THE OEPARTilET.'TS REOUREUENTS AT{D RECOMM€NOATIOT.IS 7 cHLoRrNArtoN | tu" fl T- ,H o^o*r*2-Z-s n.r?. t8. 19.PERilANENT PutrlPdShoio 3h.lch ol rrlt heod on boch of forml oorc tnrrottrdl '" ('? 2 tw, G f nora /: J Ltt cococlryLlqeml aP '/z- latolc Oceirr &- Airllna Dcalh O.,. RErrARrs: I do lrrr.ly crrlily llrct liir tdl /?,cotd is ltuc oad rroct, / -23a Fo/m GwJ SIGNATURS OF Ylhite cocv'0ffice of \Yater and Air Resources;Blue'Orillers copyl Green'0wnels copy I{E.AD CO}@LETTON:Draw a sketch of the weIL head showing casing, purop piping, seaIs, vents, access port, grout, and enclosure' I | !::=: F I.lELt f,ocAfl0l[: Drav a locatioa sketch shou'ing the directlon and distaace of the veLL to at Least tno (2) aearty refereace poLnts such aE roads, Lntersections and. strea.ms. IdLntify road's tr|th State Hlghuay road' ldentification nrmberg . ?\ - t\=, ,./ ../ ,..'"./t',ai/," ."/,;//..ff/,r /-it/ {b.,'tl/U/ .? Ittc locotion on bock of lorm) SIGNATU.qE '. Molrricl '14. 'Sf:'i'tC iaren leveUr * ,r. 3?tr .. , .cc':i-, is 5 Ln. &;;;il. i,o,?l::. '' lop of gLEV cosing. '''..-i.;:-... ..O;T!: i:.t5.....,. ti:iir(.rprn} .J7 r Merxo'ti'or rgsrtNc: 16.'.lJl,illrc 'rrATER LEVEL:- .29.-.tt ottcr: 5 1 nours:.. ot '7 17. .. CFLOR!.tATlOlt:. .Type.:-Effi ;_._4rlouarlIhlgL' .- t8: Y,'ATEF. trALlTy!- . . ,B9Od EMPERATdRE(.F) : _'leRfiANEtiT pUHp{Shor o :lacir oI rrlt bcod oi,ibo"t of torm) 'csrc i.rctor.ho l-3r?3 rypr 'Je+ u.r. ni.w . ' WELL OWIIER OF THE , I{E:i :i:.tJ COygtE?fON: I'I'l I t,itt/ IIt; ti.' ilI'. !tlt !ii- rtU., ,d/ RTCO Rtl li0RT'ri CARCI- IIA DEPARTME)lT 0i //ATER RESCU?CES DIVISIC}I CF GROU}iD "{ATERtsox 9392 - RALE I Cil, i{ . c. /7/ - t44s Ct I LLES: ocritoi{: tolvtt t-) .,.' -REG. lr0. A. r+. c. o. 7.slot size tyPe B: AZ /4 -ft o 3. i5 S ,l 8. ITATER Z0XES (dePth): g.qUALlTY: - TEUP:- .L I l- I I) 10. STATIC WATER LEYEL!,'1 ','''' ft. below toP of casing nhich is s ) ,. ytElb: Geal * r? Fror, purip, Bair, Est. i:'*:8'-:ii"l"::;i3lll"ot "'::: ' . l& puHplltc IIATER LEVEL: ft. after hrs' pumping at-gPm' sPec' caP' : gpm/ft' of dd' lffi:t:rt"''" , lntake decth ' Gap' '1 spn' Hp' # , IIi,,REHARKS: I5. DRILL LOG:0eP th From To Soil and Rock Fornation Dep th Fronr To Soi I and Rock Fo rr,rat i on t- .^ .: i/ ,.1-ltr: :.- ;'.-; ,,.:. id.t ,, !'. -: 1';r- I .'l L/ HORTH CARCLIiIA DEPARTUEI{T OF DlYlsl0li 0r GR0UND 30x 9392 - RALEIGH', WATER RESCURCT'J 'dATER ll. c. /r/ Ll [: ,JU "..iELL RECORD iit.-,- ,i .4 ':--:: neo. ro' I COUHTY //!/l) . L' a:- QUAoRAI{GLE }t0 ' OCATIOT: FOA f. i.i ;l A,DRESS: ^t t"'' "ff"i)-'iae"3. To?oGRApHy: dra!,, slope, nl-l''.'jll -,.,V ij .,r :: ;^';.:';.;"Ett'"ll'', ? in; rr'" -.- .!. n-^+h -f-TMethod ,'Grout: De9th -; : n'ilrres -r-! -i,- tYPg 7. SCREEII: from (ft') to (ft') slot size t/ ==js. IIATER zonas (decth): TEMP:s 'lllli[;^mwtopofcasin9whichisd..-::'::i*i:"i:':'".i! rt.,(above, rrx.l r*o .,lill'"."r* iiJg-" * o tli.;it:lirr:l"i:*ii , .,-. ^t ,Lti.REl,lARXS: ' , . :T Depth. gePth.^ soil and 15' DRILL LoG: soil andl!sc!-!g!!91 From To *n (.t{= * t.J 3: i-*'€ t ,4ti7r tlc AtnectS Cn?1. APPENDf,K tV trIell Construction Records NORTH CAROUT{A OEPAfiTI€HT OF HATURAL RESOURCSS ATII) COMT'U${TY O€Vg,OPl'CilT DNlsrot{ oF E}MROr$i:ilrAL UAIIAGEL€NT - OfCt N)WATER 6ECnOC{' P.O. 80x 276{t7 - R^r-Etoftttc. 276!1. F}(tiG (e rs) 7st-5083 WELL CONSTRUCTION RECORD ORILLING CONTRACTOR ItCall Bnottrers Inc. DRILLER REGISTRATION NUMBER STATE WEIJ. CONSTRUCTION PERMIT NUMBER t. WELL LOCATION: (Show sketch ol the locatioo below) N.arest torrn, Chrlotte Comttr Oepth ORILLING LOG(Road. Commrrrlty. or Subdivision and Lot ilo., Stork Screens Amica lra.From 0 To 5 __lbtrled ffiation o"Fffig:t *,2. OWNER 10 L2T=-Ibmled clay PID 0.0 pp I-bttled clay PID 2.0tf 18 n bttled clay relicCity or Town 3. ,ATE 'RILLED 7-214t+ Slate USE OF TI'ELL Zio Code beddjig fesent PID 31.5 4. ToTAL DEPTH 9 CUTTINGS COLTECTED SV"" fINO 5. DOES WELL REPLACE EXTSTING WELL? E Vo G N,o. 6- STATTC WATER LEVEL: 2E.17? FT. g above TOp OF CASING.E bebw TOP OF CASING IS .I- FT. ABOIG LANO SURFACE tlal Thickness' Depth Diameter or Weight/Ft. Material From -10--to 0 pt. lt S.h 4n PVn lhter table 45 I'bttled dst grsuy clay l+5 *fi Yellori$ stiff ret S.ltv clav ll addhional space is needed uso back ol tonrt LociTIoN SKETCH (Show direction and distance ,rom at least two State Roads. or brrdr map relerence points) 39r s 7. YIELD (gPm): - N/A METH.D oF TEsr UTER zol.lEs (deothJ:N/A Type N/A Amgq;1l9. CHLORINATION: IO. CASING: Frora -To -Ft.- From - To -Fi:- I I. GROUT: Oepth Method traieFrom 26 to 0 FL Eoirt From - To- FL- I2. SCREEN: Material Hrc Oepn Size Material d$ca sandr'o'--IQ-u-E-n. LZlfi Frorn-To- Ft.- Deprr Diameter Slot Size From 50 ro S ,r. /' it - .010 in. Frrrn - To- Ft. - h- in. From - To- Ft. - h- h. I3. GRAVEL PACK: o 4. FIE I.IARKS:Mtz S2 I OC HER€BY CERTIFY THAT THIS WELL WAS CONSTRUCTEO,IN ACCORDANCE WITH I5 NCAC 2C. WELL CONSTRUCTIO{ STANDAROS. ANO THAT A COPY OF TIIS NECORD HAS EEEN PROVIOED TO THE.WELL OWNER. SIGNATURE OF CONTRACTOR OR AGENT oArE ttORTH CAROLIT{A O€PAf,TIIEHT OF HATT RALFESCT.TRCFa Al{) COMiAJ${TY OEVEITPMEI\rr Dvrstot{ oF EI.MRONd={TAL r/iAflAOEnA{T - GRqff WATER 6ACTtOi{' p-o. 8ox 276s7 - RAr€tOt(r(C.27AtL Pilot\E (919, 733-60S3 WELL CONSTRUCTION RECORD 9RILLING CONTRACT6g ItCaI[s Brothens Inc. DRILLER REGTSTRATION NUMBER STATE WELL CONSTRUCflON PERMIT NUMBER: t. WELL LOCATION: (Show sketch of the location belowl Nearesr Town: QeElgEEe County D€pth DRILLING LOG(Boad. Community. or Subdivision and Lot No.) Stork Screens .{mica Irc.From0 To 5 lt)trIed [lry"t'on D""ffi813.2 ppnOWNER G,arlotte, tbmh G$6flri{ Rout" No'l lbttled clay PIF 2.4 psn lbttled day PID= 2.2 pgn 10 L2t4- L6 18- n lbttled day PID - 3.5 ppm 3. DATE ORILLED City or Town .'7'n4t+ 7. YIELD (spmt N/A METHoo oF.TEST bil€r 25r to 50r State USE OF WELL Zip Code 2hb-5'-I"bttled day 4. TOTAL OEPTH CUTTINGS COLLECTED EV"" EruO 5. OOES WELL BEPLACE EXISTING WELL? fI VO E HO. 6. STATIC WATER TEVEU Q'G FT. -O AbOVC TOP OF CASING. SVE'',1*, suRFAceTOP OF CASNG IS...g- FT. AT lbter table 35? 50'feUohri.dr sriff uet silty clay ]ren zol'lEs (dePrn): 9. CHLORINATION: IO. CASING: Tvpe N/A Amount ' DePth FromIto0rt. Wall Thicknessor WeighUFt. Material &h 40 Hrc Diameter !t lf additional space b necded use back ot lorm. ILOCATION SKETCH (Show direction and distance lrom el least lwo Slaie Roads. or bdreir map reference points)From - To -Ft.- Frorn - To -Fi-- I I. GROUT: From % to 0 r,. grrcut From - To- Ft.- I2. SCREEN: Oepth Diameler Slot Size From 50 ro--3Q_ rr. /' irr.-:QlQ- in. FrJm - To- Ft. - in- in- From- To- Ft. - in.- in. 13. GRAVEL PACK: Deplh Size o t(. RE Oepth trilaterial From 50 To 8 rt L2/5 From-To_ Ft. Method trenie Material H'C Malerial sillca srd I'rtB SB7I'ARKS: I OC HEBEBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCOROANCE WITH t5 NCAC 2C. WELL CONSTRUCTION STANOAROS. ANO THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO lHE WELL OWNER. SIGNATUNE OF CONTRACIOR OR AGENT OAIE -; Crolnr - orpertmrnl ol Envltonmrnl, llcalth, r.d Neturel flcrourcea Dhddon ol Envlronmrnld Menrgtrnrnl - Groulrdwrlrr Erollorr P.O. Eox 2e6t6 - Flrlolgh, N.C. 27020.oct6 Phorrr (9191 7C3-:1221 WELL CONSTRUCTION HECOBD =olho CONTRACTOR: Gss t ogic-.Exploral-LorI r .11lc, gilLLtF IIIOIITFATION NUMEEFT ll75 gTATE WELL CONSTRUCTION PERMIT NUMBETIT t, WELL LOCATION: (Show nkelelt ol llre krr:nllorr lrolow) Nrllrt Town:-Charlotte I85 e St3te_gv_i_Ils Boed . -.(Ford. Corrntlrlly. or Stlhdlvlelorr anrl l.ol f.to I OWNEF Stork-- ADDHE9S_32OI I-8J .N.qr!h _(8lrr.l o, noulc No.lCharlotte N,-C_-_- (lornly: MeCklenbUfg 2. l.rl:l'l ll I rrrtrt I rr trntlt_tN-G Loo l'ornrnllnrr I lcrrrlpllotr itp t1",in wt:t I monitor _--0_____rc-____-__eEe!ss_e!Iq - grtr --__- ___1Q____40 reddish -__40____50_____tan tiebr cley-GtrcTorn Stato OATE OR;L1ED -_9--28-94 lrsF ()t. TOTALDEPTH --5O. . 3. a,t. C. 7. CUTTII{(IS COLLEo I El, YEB k.l r,to| ..fOOEBY\,ELLREPLACE Exts'ttNG Wrt r z Vi':l I I i{(,tw IATATIC WATEB LEVEI- Betow to;r ot ()nnhrg: ,'t '^ ' r. rop oF c^srNs rs - e,o . $?:;i;;#'il,il'X;:i,l*:'t Gr-l TerrrladrJ rlbr bobrv trnd aurr.o lr ltteger rrntr.r r varlrncr 6 r...r..,h r.Jrbrr rl0t rt^ rOAO rO .ot rae. YEI..D (gpn[ tlA .-. ME'rl IOD oF 't t! s I NA t0. WATEF ZONEB (deplhl:. Nn tt. CIILOBINATON: I'ype . ra.lHtruo: OepttrFronr 30 To --9--From- To-- From -To-.---. 13. 0F0JT: t.lA Arrrrxlrrl NA Wnll llilr:hrmrrUlerlrolor nr W6lghUll Matorlnl Ft. -_-? Sclr 40 . .qvc Ft.---.-..-. Ft.--.. .. . Melerlnl MeltrorJ -qomgnt grout t,remle .. .-... Errvlrorurrerrtal or Errqissgs6irru rirm'Cooper Envlronnental 23OO Sardie Rd. N. Suite eCharolt,ter NC 28277 ll nrftlllhrnnl rgrnr:e lr nerrlcrl rrrc hnck ol lornr LOCA ! tON St(E tCt ! (Slrow rlhecllorr nlrrl rllslnrrce lrorrr ol lenrl lwo Slalc llonrlq. nr olhnr rrrnp lelctcrrcn polrrh) N(:A(:2r), WFl.[ t(f iltF wFt I ()wNFn. t cpth Fwn 26 ro i----.ruFm To _..._-....Ft.II. SCREEN:tleplh Dlarneler Slol Stre MaterlntFrom 5() To --*?0_ Fl _L_.. hr. ,010 hr. pyC From - To ---- Fl. - .- . lrr. lrr, From - To -- Ft. ._- -. ftr, trr.I'. SATICI,ORAVEI PACK: t,rpth She Mntertnt From 50 To --L8-. Ft. .Ja:35 alllea aarrl From - To-._.... Ft....- . tC. REMARI€:_Erntglftg_Jrsx!.. Zg Lo 26 rrtr{-4 I OO ]EffiBY CEFRFY IHAT 't l.ll8 wEl.L w^s coNs I nUC r Et.t tN A(:o(rnt )AN(:G wt I I I I 5AG$CItt CIKXI ST NOA]IDB, AND lt'lA'r A C()FY (,r lllls nEcont) ilAs nEFN pllrrvltrFD l0-7-94firu,-,e,.* sl(rN^ I trnE ordrxr nnbton ()r{ A(IEN Icw.t my,*Dt srhrrlt orlgrtrel ro trMdorr or Erw&ornr"'rral Mnrngnrrrnr{ nrrrl enpy ro wel owrnr. t AtE 'iL.gF-* '' t{orlft Crolnr . Orprrlmonl ol Envlronmrnl, I helllr. rrrd Nrlurrl fleroutcet OMdon ol Erwkonmrnlrl Mrnrgom.nl - Oroutdwtllt Srcllort P.O. Eox 20!36 . Rrblgh' N.O. 2782e'o68t Phonr lglgl7Cg-3221 WELL CONSTHUCTION BECOHD olxo corrRACTOR: Geologic__ExploraLlorr, l1c. DilLLtR nlOltTRATtON NUMBIFT ll75 gTATE WELL CONSTRUCTION PERMIT NUMEENT l. WELL IOCATION: (Show nkalelt ol llte ktcnllrttt lrnlow) Nrmrl Town:- charlotte I85 & State_gvj_f].e .Bsed ...lFord. Ccrmunlly. or Euhrllvlelon rltl l.ol No I2. OWNEH Stork-- A9DRE gs-3201 EsJ . N.qrlh _ lElrcat or lloulc No ) (:ourrtyt MeCklenbUrg l.rtil'1 il I rotr I rr r)lltLr-tN-G Log l'or trrnllmt I lerr.llpllott 9ATE oBtLrED .9-28-94 TOTAL DE"T}I -.45 7lp (iorlo wt:t I monitortrsF ( )l'3. a, 6. c. 7. CUTTINOBCOLLECIEl, vrsll.l t,to| ..1ooEEWELL REPLACE EX|SilNG Wrt I ? vi.s I I r.t(,lx I8TAT|C WATER LEVEI- Eelow tolr ot Onrtns: t'I !. rop oF cABrNo !s - e,o [?:;i;,1#il,fU::i,;#1't O*ll &mlrrli alrat balott l.nd .rrll.o l. lll.git urtt..r r vmlrrrco lr trrrrorttr.-tGrrDrlh ttA ltcao 2c .otrtt YEL[, (gpmr: llA .-. ME'rltOD oF 'r tis I Nn tO. W TEF ZOIIEB (dep[rl: . NA. tt. CI{LORF{ATON: Typerlfuro: snvlrtlrutrarr[al or Errc|[rrccrlrrg FlrmCooper Envirorurentai 23OO Sardis Rd. N. SuiteCharoltte, NC 28277 ll nrhlllhrrrnl rpnr:e ls rrnerlprl rtm beck ol lornr a .l{A.Atttourrl NA DeotltFom s ro -9---- l=tpJg;n- TO- Ft Wnll ll*:hranrUlatrrolor or WcldrUft Matorlnlz Sclr 40 pYC LOCA I tON St(E tct I lShnw rlhacllrxr nrrl rlhlnrrcc horrr al lrnrl lvro Sldr llonrl,r, or olhcr lnap rclcrernn polnlr) From -To---_-. Ft.._ . . tg. GffiUT: Deplh Materlat MethorJFrqn 26 . ro --9--.--Ft. -c.emqtt grout Eremle..Frun To _. ___..Ft. .- TI. SCFEEN: Deplh Dlarneter Slol Stre MatertntFrom 45 To 3O _ Ft ---?._.. hr. ,Ol0 trr, pyC From - To --*-- F1... . _ . hr. ln. Flom - To --- Ft. --.--... hr. ln. TI. SATIIO'OBAI'EI PACK: t eplh $lre MnlerlnlFlq,n 45 fo -.29---. f[ .J2:35 ell lea aarrl From - To---... Ft. ... . fC. REMARfiSI_ grniglrfls_.frsn Zg Lo 26 MW_5 I OO ]EreBY CEnTIFY THAT rlll8 WEI.L WA8 (;()its r nlrc rEt) tN A(:C(,lll]AN(:F Wt I I I t 5A N(:Ar: 21;. yypl-1goiltrmroTbNSTANOAnOE,ANDlll^'rAcoFY(rr illrsnEconr)tnsnEFNrn(lvtt)FD t(r tf tF*rtr.owurn. lqi:g{- uitEil.lffilr.$t Olvhlon ol Errviorrnnlrl Mnrmgnlrnnl nrrrl en;ry lrr wol orumr. ; crolnr . Drprrlmrnl ol Enyhonmrnl, I helrh. erd Nrrurrl llcrouroor DMdon ol Erwlronmonld Menrgrmrrrl , Gloundwrll Erotlon P.O, Eor 2e63t. Rdolgh, N.C, 27620.os3lt Phonr (919,733.322t WELL CONSTRUCTION RECOHD ol,no CONTFACTOB: 6sstoglc .ExploraLlorr, .lrrs.. DiLLtR iIOIITITATION NUMEER: LL75 STATE WEIL CONSTRUCTION PEFI]TIIT NUMI'ENT -' -_"......... l. WELL LOCATION: (Show nkelelt ol lhe locnlkrn lrnlow) NolrotTown: CharloLte I85 & State_qvifle .Rpad...(Fbld. Corrnunlty. or Suhdlvieion mr.t i oi ii. 12. OWNER Stork-_ apessgs 32Ol.[;B_5 .N.ocrh _ (Slrccl or floulr No t (:orrnly: MeCk).enbUfg Charlotte N..C- _-_Cty or Torn OArE ORTLLED ._y2B-94 TOTAL DEPTH -5OCUTTINO8 COLLECtEt) yEB l-x.l r,tn| ...1 St"il' lrsF ( )t' wt:t I 7lp Onrln rnonitor l)l:l'lll l'rrrrrr lit rrnrLr_tN_G Loo t'.!iltrnllott l lorr.r lpllorr rlrE t. a, 6.C, OOEEWETI REPLACE EXISIIN6 WFI I ? Yi:II I7. ETATIC WATER LEVEI- Batow top ot ()nrtng: r. rop oF clarr.ro rs - e,o . [?:;l,J#'il,,11'""::,H#:'t(I*tt Tltilf'taba rllrr Drlor land aurl.o l. lll.tit rmt... . var6rrer Ir t..p.rlh rrtrthrr rl0t ta^ llo^o eC .ot t.e. YELD (epmr: ltl .-. Mr'rlt1lrr oF mis t NA lO. WATER Z@{Eg (depth}:. NA .l{A.Attroutrl NA wafl t|rhk''om LOCA llON Sl(E lcll 0,. .?]1"]t" "'Stilr',f[l Bi'U"' (slrow rlhnr:llon nrxl rlhln,ree horrr nt lcnst two srrro Fl,_---- -.- - .. '- : ,tonrl,r. rr olhar trrn;r rnlarcnen polnlr| Ft._- . I it(,lx If' I llrrvlrorurrcrrbal or Errq tssqg61,,UCooper EnvironmenEal 23OO Sardie Rd. N. Suite eCharoltte t \tC 28277 : It. ClltOBlilATON: Type .rzfruo: Deptlr From s To --o----FrOor- To__ From -To-----. t3. G8OiIT: Deplh Malertat MeilrorJFtqa 26 To -Q__-.Ft. _ssfitgtrt grouL Eremle.-From To _...--...F1. ... T{.SCFEEN: Depth Dlanreier Slol Stre Malerlnt From 5o To s - Ft 3-._.. ln. .010 hr. pyc F om - To ---..-- Ft... - hr. hr. Frqn - To -.-. F|....-.. .. . hr. ln. '6. EAilDreRAVEL PACK: EA D3pth AA Slze MRlerlnl From _w To_i]_--. Ft..JZ_35 al.t lea aarrtt Ftqn - To_._.. Ft..-. tC. REMAFI(8:_-B.nterrfB-s_.frsrn.. 2A L9 26 Mw_6 IooHEREEYCEFTIFYTHAT'll'll8wE[LWA$(:oNsrnrrcrEtrtNA(:(;(IilrA]t(:Fwililtfi^ N(,n(:?(:.wFt.tCOilOTRI'OT|ON8TANOAilOS.ANOlllArAconY(,r llllsllEcOnlllllsnEFin'n()VttrFn t(, ntFwFtr (,WNFn. ll nrftlillorrnl npnr:e ls trenrlerl tr:p trae.h ol lornr OW.l ffiV,9,ll \e =--o@?*-r</-- ,Zea+.r<- ro-z-94 Bt(rNAil'nE orllt)t.ltn^ctonufiAoFNt {--'r- -* srfillrlr orfutrnl tf tnhbu or Erwhorrrnrrrnr Mnrngnrrro,r arrrr rn;ry * * o*rr.t'ot E l{orfh Crofinr - Oeperlmenl ol Envlronmrnl. I le ellh. errd Nalurel flerource a DMdon ol Erwlronmrnlrl Mrnrgemenl - Groundwelor Srcllorr P.O. Box 29696 - Fhblgh, N.C. 27026.0636 Phonr (919f 7O9-'3221 WELL CONSTRUCTION FECOHD o*tno CONTBACTOB: Gsot.cglc -ExploraLiorr,,Irrc,. OnlLLlA RIO|8TIIATION NUMEIF: lrTs STATE WELL CONSTRUCTION PEFMIT NUMEENI t. WELL LOCATION: (Show skelelt ol llte krr:nllorr lrnlow) NrrrorlTorvn: Charlotte I85 & Statesvitle .Rp.Ad...(Rord. Corrourrlty. or Eubdlvhlrrr nrrd l.ol No.f2. OWNEB Stoqk-- ADDFESS 3201 't1_85 _N.qr!h _ l)orrrrly: MeCklenbUrg (Shcol or noulo No.)Charlotte N,e-__- .__---_. Glly or Tonn Steto OATE ORILLED .:f28-94 r,sF ()t- TOTAL DEPT}I 35 .grey graniteCUTTINOSCOTLECIEt) YEsl_.l r.l(ll**; OOES WELL BEPLACE ExtS'nN6 Wr:l r z 9f=r9 Pf,s#51'-,35?*?? :I,',:llllg lTlll .Jr,' r I N( ,t xt7. STATIC WATEB LEVEL Betow'Iop ot Oanhrs:l- | !. rop oF cAErNG rs- Q,o [i:;i;:i#'il,IH:J;;il:', 'Grrlng Torrnltrlii rllor brlow land aurl.o l. lll.g.{ ulrhrr I yerlrrrco lr trerrorthrcodf,tIrlor tt^roAo rc .ottt9. YIELD(mn): Ne '.-.METltOr)oF'nist NA lo. W TER ZOIIES (depthl: . N^ lJl:l'il t lJntLt_tNG Log 3. a. 6. ll. CHLOFINATION: Type -.- l{A.-rzfnc: Deprtr ohrnarnr i:'lJjfi|iiil' From ffi To o _- Ft. __6_ Sch 40 From ffi to o Ft.---.-a. .:' " From -To-_-. Ft._ . ,.. 13. GFOTIT: D€plh Malertat MeilrorJFrom 53 To -O-..-. Ft. -.cemsnL grauU Eremle .-From To -._-..Ft. ._" . 14. SCHEEN: Dopth Dlameter $lol Stre MaterlntFrom 65 To ---@_- Ft -2__.. hr. ,0I0 tn, pyC . From - To ---- Fl. -... ".-. . hr. hr. From - To -- Ft. --._.. hr. trr. T5. SA'{OfOMVEL PACK:thplh Slze Malerlnl Fronr -55--- To-5,z--.Ft..J2:35 . alrlea sattd Frqn - To*.*... Ft. ..-. .. lC. REMARK9:_ sentgrl!,c_-frgn- 5Z Lo 53 l'rrrrrr ln ,'rrrtnllonllcrerlpllolr --O-----lQ. --o-Eanqe clay Errvlrr"lruterr|:al or Orrt,[11ss61rnr FlrmCooper Environmental 23OO Sardie Rd. lt. Suite eCharoltte, NC 28277 : ll nrhlitionnl spnr:n ls rreatlerl rrre bnck ol lornr LOCA'tON St(E'C't (Slrow dhncllon nrrl rllslnrrca honr nl lenrl lwo Slelo flonrlq, or olher lrrnJr relcrenen polnh! VFI 7tp tl"in wt,t I monitor Atttounl NA Mrlorlnl .P_vg . U!-.. .. --- looHEREBYCERT|FYTHATTl.llSWEi.LWAS(;(,NsrntrctEDtNAC(}()nI)AN(':FWilllt5A N(:A(:2(;,WFLICOiltTmJCTIONBT NDAnDS,ANDIInTACopY()rllllsnEconl)ll^sBEFNt'n()Vlt)FDt()iltEwFil.()WNFn. \-? a.-<A--eaG /AtuL Lo-7-s4 sKrNAilrnE or crfltn^cr(,n ()n agtrur o^tEstftndl or[hrel lo tllvldotr ol Erwhorrmrrrnl Mn*ogonrn,r nrrr rnpy ro wol ofimr. gw.r REv.crt Departrnent of rrrrru,,,],.rit, ii*iiii a Natrrral Resources Dlvlslon of Envlronrnental Managlernent Grotrndwater Sectlon P.O. Box z<ls3f - Raletgtr, N.C. 226a6-.o.srs WELL ABAT{DONMENT RE CORT) coNrnAcToR REG NC) l. WELL LOCATION: (Show a sketch of the localton on back of fornr.l I-85 & Statesville _Bgr._(Road. Commrrnlty. Subdlvlslorr, NearestTown: Charrlotte Corrnty MPekl enhtrrg W WEt.l, DIAGRAM: Draw a detatled sketch of the well showlng tolal depth. depth and dla- rrreter o[ screens remalnlrrg ln tlre well. gravel hrlerval. hrtervals of caslng perforailons. and depllrs arrtl lypes of llll rnaterlals used. Date 10-7-94 I.ot No.) 2. OWNER Stork 32OI I-85 N. Charlotte NC3. ADDRESS: 6. TOTI\L DEPfiI: -I39-DIAMEI.EIT: 7. CA.SING REMOVED: fcct none dlarneter 6. USE OF WELL:t.;rl.ar t.ra'l'l 8. SEAUNG MATERIAL: Neat cemerrt bags of cemort 33 - gals. of water 198 DATE: o-?^-q4 6- Sarrd cernent bags of ccrrrerrt yds. of sarrd gals. of water Other T)pe matcrlal none Amount- 9. BXPI.AIN MEffiIOD EMPI,ACEME}TT OF MATERIAL. trernie grotrt frcm bottom up Slgnaturc of Contractor on WEIL I.OCATTON: I do hcreby certlfy that tlrls well abarrdorrruent record ls trrre and exact. tlon and dlstance of the well to at least two (21 nearby referinee polnts suclr as roatls. lntersecltorrs and strearns. ldortlfy roads wlth state lllgh way road ldenllllcal lon rurrnbers. Submtt orlglnal to the Dlvlslon of Errvlrorunental Managenrent. orre copy to the Drlller. and one copy to the owrrer. Gltf-3o Revlsed 3l8l9' APPENDDT V Soil Boring Logs COOPER EINTI.BOI{I4EN:IAL.Boring Log:Soil Boring SB-3 Project:STORK ENG I N E E RS G EO LOG I STS SC/E/V-]'IS7S 2300 Sardis Road North Suite Q Charlotte, North Carolina 28227 Telephone: (704) 845 -2000 Fa:r: (704) 845 - 8901 Date:07-21-94 Proiect No:94105 Drilling Conr McCALL BROTHERS Prepared By:DALE LA}IIER County:Mecklenburg Address:I.U5 NUI(IH Charlotte, N.C. Total Depth 20 feet Hole Diameter:3 l/4 inch Lgth Coring Device:Split-spoon 2fect Boring Methods GroundwaterO bsenations Driiling Method:H.S.A. Hollow StemAuger: X GW Encountered at:N\A Drilling Fluid:None HandAuger GW After Completion:N\A unller:lda*G. Other GWAfrer:Hammer Wcight:l,$0lbs GW Volumes:HammerDrop:30 inch Pcnctra- Blow Per 6" Sample Type Depth (FT)Soil Description D Remarks NS 0- l Asphalt Base Coarse DRY CRUMBLY RED ORA}IGE SILTY CLAY DRY CRTJMBLY RED ORAI{GE CLAYEY SILT DRY CRUMBLY RED ORA}IGE CLA}'EY SILT MOIST CRUMBLY TA}.INISH ORA}IGE CLAYEY SILT 6.9-n- l4 SS 5-7 9:38 PID = 4.3 ppm 5-7-7- l1 SS t0-12 9:52 PID = 2.8 opm 5-6-7- 9- SS t4-16 10:06 PID = 1.4 ppm 9-9-tZ- l8 SS l&20 l0:16 PID = 1.0 oom SS - Split Spoon ST- ShelbyTube PS - Piston Sample AS - PowerAuger Sample WS - Vlash Sample IIA - Hand Auger Sample BS - Misc. Bag or Bottle Samplc NR-No Rccovery RB - Rock Bit RC -RockCorp COOPER EI{TIRONMENTAL ENG I N E E N G E O LO C I SN SC/E/Tr/STS 2300 Sardis Road North Suite Q Charlotte, North Carolina 28227 Telephone: (704) 845 -2000 Fa,r: (704) 845 - 8901 Soil Description PID = 1.4 PID = 0.6 ppm Asphalt Base Coarse DRY CRI.'MBLY RED ORAI{GE SILTY CLAY DRY CRIJMBLY RED ORAI{GE CLA\'EY SILT DRY CRI.JMBLY RED ORA}.IGE CLAYEY SILT GRADING AT 15.5' TO GREEN GRAY CLAYEY SILT RELIC STUCTTJRE PRESENT DRY CRI'MBLY DARK GREEN GRAY CLAYEY SILT SS - Split Spoon ST- ShelbyT[be PS - Piston Sample AS - PowerAuger Sample WS - Wash Sample IIA - Hand Auger Sample BS - Misc. Bag or Bottle Sanple NR-NoRecovery RB -RockBit RC - Rock Corc COOPER ETr1,IIRONMENTAL ENGI N E E N G EO LOG ISTS SC'EMISIS 2300 Sardis RoadNorth Suite Q Charlotte, North Carolina 28227 Telephone: (704) 845-2000 Fa:r: (704) 845 - 8901 Lgth Coring Device: Penctsa. Blow Per 5"Soil Descriptiou PID = 0.0 ppm PID = 0.0 ppm SS - Split Spoon ST - Shelby Tirbc PS - Piston Sample Asphalt Base Coarse DRY CRI.JMBLY RED ORA}IGE CLAYEY SILT GRADING LIGIIT GREEN SILTY SAI.{D DRY HARD LIGHT GREEN SILTY SAI{D GRADING TO DRY ORAI{GE SA}IDY SILT DRY CRI.,MBLY ORAI.{GE CLAYEY SILT SLIGHTLY MOIST ORANIGE TO LGTIT GREEN CLAYEY SILT RELIC BEDDING FEATI.'RES AS - PowerAuger Sample \[/S - Srrash Sample IIA - Hand Auger Sample BS - Misc. Bag or Bottle Sample NR-No Recovery RB - Rock Bit RC - Rock Core COOPER ENI/IRONMENTAL Boring Log:Soil Boring 58-6 Project:STORK EN G I N E E RS G E O LOG I SN SCIEI{IISIS 2300 Sardis Road North Suite Q Charlotte, North Carolina 2421 Telephone: (704) 845 -2000 Fa,r (704) 845 - 8901 Date:07-2t-94 Project No:94105 Drilling Cont McCALL BRO'II{ERS Prepared lJy; DALE LANIER County:Mecklenburg Addrcss:I.85 NORTH Charloue N.C. Total Dep*r 20 feet Hole Diameten 3 l/4 inch Lgth Coring Device:Split-spoon 2feet Boring Methods GroundwaterObservations DrillingMethod:H.S.A Hollow Stem Auger: X GW Encountered at:}.{\A Drilling Fluid:None Hand Auger GW AfterCompletion:l.I\A Driller:tvla*G. Other UW AITCN HammerWeight:Itto lbs GWVolumcs:HammcrDrcp:30 inch Penct'zr- Blow Per 6' Sample Type Depth (FT) Soil Description D Remarks NS 0- l Asphalt Base Coarse NO RECOVERY WHITE SILTY SAND SLIGHTLY MOIST CRI.JMBLY ORA}IGE SILTY CLAY DRY MODERATELY HARD WHITE PINK BLACK SAI{DY SILT ss 5-7 l&ll- l0-9 SS t0-t2 3:53 PID - 0.4 ppm +5-5-7 ss t4-t6 4:09 PID = 0.3 ppm 5-7-t L- l7 ss l8-20 4:20 PID.{.0ppm O SS - Split Spoon AS -PowerAuger Sample BS - Misc. Bag orBottle Smrple ST - Shclby Tirbe WS - Wash Sample NR - No Recovery RB - Rock Bit PS - Piston Sample IIA - Hand Auger Sample RC - Rock Core c ooPERlENInBe N ITENIAL-Boring Log:Soil Boring SB-8 Project:STORK ENGINEEN CEOLOGISTS SCIENNST:j 2300 Sardis Road North Suite Q Charlotte, North Carolina 28227 Telephone: (704) 845 - 2000 Fa,r: (704) 845 - 8901 Date:07-21-94 Proiect No:94t05 Drilling Conr McCALL BRO HERS Prepared By:JOHNBURKART County:Mecklenburg Address:I-85NORTH Charlotte, N.C. Total Depth 2O feet Hole Diameten 3 l/4 inch Lgth Coring Device:Split-spoon 2feet Boring Methods GroundwaterObservations Drilling Method:H.SA Hollow StemAusen X GW Encountercd at:N\A Drilling Fluid:None HandAuger GW After Completion:N\A IJnllen MarrG. Othcr GWAfter HammerWeight:l40lbs GSy'Volumes:HammerDrop:30 inch Pcncta Blow Per 6" Sample Type Depth GT) Soil Description D Remarks NS 0- l Asphatt Base Coarse 3-3-34 SS 5-7 MOTTLED CLAY DRY CRI.'MBLY MOTTLED CLAY SOFT MOIST REIJC BEDDING FEATTJRES DARK BROWN TOBROWN CLAY ROOT A}ID ROCK FRAGMENTS NOTICED MOTTLED CLAY GRADING TO DENSE REDDISH YELLOW CLAY 12:00 YELLOWNH I-IN-I NOTICED PID=0.0ppm 5-5-6-7 SS L0-12 l2zl0 2I IN. RECOVERY PID = 0.0 pprn +5-5-7 ss l4-16 L2:30 17IN. RECOVERY PID= 1.7 ppm 6&ll- t7 SS l&20 12240 2I IN. REcovERYTrl={'o PPm SS - Split Spoon ST- Shclby Tube PS - Piston Sample AS - PowerAuger Sample lVS - Wash Sample HA - Hand Auger Samplc BS - Misc. Bag or Bottlc Saurple NR - No Recovery RB - Rock Bit RC - Rock Core COOPER ENTIIRONMENTAL ENGINEERS GEOLOGISTS SC/&VTTSIS 2300 Sardis Road North Suite Q Charlotte, North Carolin a 28221 Telephone: (704) 845 - 2000 Fax: (704) 845 - 8901 Soil Description PID = 2.0 ppmv 1.5 ft PID = 1.4 ppmv I ft terminated boring sampling at 30 ft set 2 in well at 50 ft SS - Split Spoon ST - Shelby Tube PS - Piston Sample A- horizon grass root organics yellowish red, dry crumbly silty clay reddish orange dry dense silty clay mottled reddish orange yellow soft claY mottled reddish orange yellow soft clay relict features C horizon mottled reddish orange soft moist clay relict features mottled reddish orange soft moist clay redish orange to yellow clay AS - Power Auger Sample WS - Wash Sample HA - Hand Auger Sample BS - Misc. Bag or Bottlc Sample NR-No Recovery RB - Rock Bit RC - Rock Core COOPER ENT/IRONMEN?AL E NG I N EE RS G EO LOG I SN .SC]E}/ZS7S 2300 Sardis Road North Suite Q Charlotte, North Carolin a 28227 Telephone: (704) 845 -2000 Fa,r: (704) 845 - 8901 Soil Description PID=3.6ppmv I ft of recovery CL no signs of = 6.6 ppmv I recovery CL facies change at 10.5 ft =2.7 ppmv I recovery CL facies changc at25.7 ft, sampling at 30 ft set 2 in well at45 ft SS - Split Spoon ST- ShelbyTUbe PS - Piston Sample mottled reddish orange yellow clay mottled reddish orange dry dense clay grading to yellow tan mottled clay mottled reddish orange yellow soft clay mottled reddish orange yellow soft clay relict features C horizon mottled reddish orange soft moist clay relict features grading to tannish yellow mottled clay mottled reddish orange soft moist clay redish oftlnge to yellow clay encountered denser material possibly bedrock AS - Power Auger Sarrple WS - Wash Sample HA - Hand Auger Sample BS - Misc. Bag or Bottle Sample NR - No Recovery RB - Rock Bit RC - Rock Core COOPER ENYIRONMENTAL E NG N E ERS G EO LO G I SN SCIEIV"IISIS 2300 Sardis Road North Suite Q Charlotte, North Carolin a 28227 Telephone: (704) 845 - 2000 Fax (704) 845 - 8901 Peiretra Blow Per 6"Soil Description PID=4.6ppmv 1.5 PID = 7.5 ppmv I recovery CL PID = insuffient amount to field screen 8in recovery CL PID = insuffient amountto fieldscreen I ftrecovery CL sampling at 30 ft set 2 in well at 50 ft o A horizon grass roots organics reddish orange yellow silty clay dry crumbly tannish yellow dry dense clay mottled white to tan to gray clay with relict features and angular fragment of possible granitic material mottled white tannish white to yellow clay relict features C horizon mottled tannish yellow soft moist clay relict features tannish white yellow clay yellow clay AS - Power Auger Sample WS - Wash Sample HA - Hand Auger Sample BS - Misc. Bag or Botle Sample NR - No Recovery RB - Rock Bit RC - Rock Core SS - Split Spoon ST- ShelbyTubc PS - Piston Sample APPENDDX VI Soil Analytical Results , %r September 30, 1994 l4r. John Burkart Cooper Environmental, Inc. 2300 Sardis Road North, Suite Q Charlotte, NC 28227 RE: PACE Proiect No. 640922.509 Client Reference: Stork 94147 Dear Mr. Burkart: Enclosed is the report of laboratory analyses for samples received September 22, 1994. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. Sincerely, I I CJar*" Ifutuu* Kris H. Kommalan Project Manager Encl osures 9800 Kincey Avenuo, Suits 100 Huntsrsvillo, NC 28078 TEL:70+8r$90m FAX: 704-875-9091 An Equal 0pportunity EmPloYer , ff REPORT OF LABORATORY ANALYSISENVIFON M ENTAL LABORATO RI ES Cooper Envjronmental, Inc. 2300 Sardis Road North, Suite QCharlotte, NC 28227 Attn: Mr. John Burkart Client Reference: Stork 94147 PACE Sample Number: Date Collected: Date Received: C'lient Sample ID: Parameter PETROLEUM HYDROCARBONS Percent Sol lds September 30, 1994 PACE Project Number: 640922509 92 0257893 0e 121/94 09 /22/e4 sB-1 1 Mt,l.6Units MDL 15 Ft. METHOD. DATE ANALYZED % 0.01 86 0e /26/e4 0elzele4 ael27le$ ae/26/94 INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Oiis e-ereas" by Soxhlet Extraction mg/kg l0 150 9071 09129194 ORGANIC ANALYSIS 5030/3s50 oEilHl;l[,'I0ilfiil::ffi.ii 3l'i?1,., ms/ks 5'0 u!,,,0 Petroleum Hydrocarbons as Gasol'ine mg/kg 6.0 ND 9&10 Kincey Avenue, Suite 100 Huntorsvills, NC 28078 TEL: r0+.8r$qEz FAX: 704-875-9091 An Equal 0pportunity Employor , ffi REPORT OF LABORATORY ANALYSISENVIRONMENTALLABOBATORIES TILI IJIII I'T LfIgI'IT'TIV! Mr. John BurkartPage 2 Client Reference: Stork 94147 PACE Sample Number: Date Col I ected: Date Received: Client Sample ID: Parameter September 30, 1994 PACE Project Number: 640922509 92 0267907 091211e4 0e /221e4sB-t I Mt,l-6Units MDL 30 Ft. METHOD DATE ANALYZED INORGANIC ANALYSIS INDIVIDUAL PARAMETERS 0i1s & Grease by Soxhlet Extraction mg/kg 10 180 9071 09129194 ORGANIC ANALYSIS PETR0LEUM HYDROCARBONS 5030/3550 Percent Sot ids % 0.01 78 09126/94 Petroleum Hydrocarbons as Diesel mg/kg 5.0 ND 991?9191Extraction i Hydrocarbons as Diesel - 092794 q9l?7/94 Petroleum Hydrbcarbons as Gasoline mg/kg 6.0 ND 09126194 Otn.r. data have been reviewed and are approved for release. Char'les l,l. Cabaniss li'lanager, Inorgani c Chemi stry Margaret S. Harding Manager, 0rganic Chem'istry 9800 Kincey Avenue, Suite 1 00 Huntersville, NC 28078 IEL:,0{-t 5-90!n FM: 704-875-$91 An Equal 0pportunrty Employor a ffi REPOBT OF LABORATORY ANALYSIS Mr. John Burkart FOOTNOTES September 30, 1994 Page 3 for pages I through 2 PACE Proiect Number: 640922509 Client Reference: Stork 94147 l,lDL Method Detection LimitND Not detected at or above the MDL. S(il (incey dvenue, Suite 100 Huntersvillo, NC 28078 IEL: r0+3rE'W FAX: 704-875-$91 An Equal 0pponunity Employer a ffi REPORT OF LABORATORY ANALYSIS Mr. John Burkart QUALITY C0NTR0L DATA September 30, 1994Page 4 PACE Project Number: 540922509 CIient Reference: Stork 94147 0ils & Grease by Soxhlet Extraction Batch: 92 30830 Samples: 92 0257893, 92 0267907 METHOD BLANK: MethodParameter Uni ts MDL BI ank0TfsT-mease by Soxhlet Extraction ms-7k0 IIf ND- LABORATORY CONTROL SAMPLE: ReferenceParameter Uni ts MDL Val ue Recv 0[I-sT'Tease by Soxhlet Extraction mg/Ts m- TTO-d- T00B 9800 Kincey Avenue, Suite 100 Huntersvillo, NC 28078 fEL: 104.875- FAX: 704-875-9091 An Equal 0pportnity Emplryer a ffi REPORT OF LABORATORY ANALYSIS Mr. John Burkart QUALITY C0NTROL DATA September 30, 1994Page 5 PACE Project Numberz 6409?2509 Client Reference: Stork 94147 Petroleum Hydrocarbons as Gasoline Batch: 92 30714 Samples: 92 0267893, 92 0267907 METH'D BLANK: MethodParameter Units MDL Bl ank Etroleum Hydrocarbons as Gasoljne mgTIg 6;0 ND-- SPIKE AND SPIKE DUPLICATE: SPi keSpike DuplUnjts MDL 920268644 Spike Recv Recv RPDParameter - LABORATORY CONTROL SAMPLE: ReferenceOP.r.r.t., Units MDL Val ue Recvpetroleum Hydrocarbons as Gasoline mgl@ 6T -T0- I06s lEfil Kincey Avenue, Suito 100 Hunterwille, NC 28078 TEL:r0eD5-W FAX: 7B-875-9091 An Equal 0pportuoity Employtr a ENVIBONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Mr. John Burkart FOOTNOTES September 30, 1994page 6 for pages 4 through 5 PACE Project Number: 640922509 Client Reference: Stork 94147 MDL Method Detection LimitND Not detected at or above the MDL.RPD Relative Percent Difference 98fi1 Kincey Avenue, SuitE 100 Huntersvillo, NC ?8{178 TEL: rll&lrS909 FAX: 704-875-9091 An Equal 0pportunity Employor a ?tsr ffi REPORT OF LABORATORY ANALYSIS September 28, 1994 Mr. John Burkart Coopei Environmental, Inc. 2300 Sard'is Road North, Su'ite QCharlotte, NC 28227 RE: PACE Project No. 640921.50i CIient Reference: Stork Screens Dear Mr. Burkart: Enclosed is the report of laboratory analyses for samples received September 21, 1994. Footnotes are given at the end of the report. If you have any questions concern'ing this report, please feel freeto contact us. Sincerelyr ' , LU^*,; Alorrr: Kris H. Kommalan Project l,lanager Encl osures 9800 Kincey Avenus, Suite 1 00 Huntersville. NC 28078 TEL:70a-t 5-qID FAX: 704-875-9091 An Equal 0pportunity Employer / ffi RrpoRr or unoRRronYRuRtYsls Cooper Environmental, Inc. 2300 Sard'is Road North, Suite QCharlotte, NC 282?7 Attn: Mr. John Burkart Client Reference: Stork Screens PACE Sample Number: Date Col I ected: Date Received: Cl i ent Samp'l e ID: Parameter INORGANIC ANALYSIS IND IVIDUAL PARAI'IETERSOils & Grease by Soxhlet ORGANIC ANALYSIS MDL September 28, 1994 PACt Project Number: 54092I501 92 0266455 0e l?o le4 0912t le4 sB-9 Mt^l-430' METHOD DATE ANALYZED Di esel as Diesel Gasol i ne Units ulo mg/kg ms/kg 59 ND 092694 ND 0e122/e4 0e l?.6/e4 09126194 0el26le4 Extraction mg/kg l0 9071 091221e4 5030/3550 190 PETROLEUM HYDROCARBONS Percent SoI ids Petroleum Hydrocarbons as Extraction - Hydrocarbons Petroleum Hydrocarbons as 0.01 5.0 5.0 9800 Kincey Avenue, Suite 100 Huntsrsville. NC 28078 TEl.:70&8ni-qM FAX: 704-875-!1091 An Equrl 0pponunity Employer / ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Mr. John BurkartPage 2 Client Reference: Stork Screens PACE Sample Number: Date Collected: Date Received: CIient Sample ID: Parameter September 28, 1994 PACE Project Number: 640921501 92 0265463 os l20le4 09 /21/e4 SB-10 MU-5Units MDL l0' METHOD DATE ANALYZED INORGANIC ANALYSIS INDIVIDUAL PARAMETERS 0'il s & Grease by Soxhlet Extraction mg/kg l0 270 9071 09/22/94 ORGANIC ANALYSIS PETRoLEUM HYDRoCARB0NS 5030/3550 Percent Sol ids % 0.0I 72 09122194 Petroleum Hydrocarbons as Diesel mg/kg 5.0 ND 09/26194 Extraction - Hydrocarbons as Diesel 092694 09126194 Petroleum Hydrocarbons as Gasoline mg/kg 6.0 ND 09/26194 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 lEL 70f-trs-9092 FAX: 704-875-9091 An Equal 0pfortunity Employer ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Mr. John BurkartPage 3 Client Reference: Stork Screens PACE Sample Number: Date Col I ected: Date Received:Client Sample ID: Parameter INORGANIC ANALYSIS INDIVIDUAL PARAMETERS 0i1s & Grease by Soxhlet Extractjon ORGANIC ANALYSIS Units l',lDL September 28, 1994 PACE Project Number: 640921501 92 0266471 49120194 09 /2r /e4 sB-10 Mt^l.530' METHOD DATE ANALYZED PETROLEUI4 HYDROCARBONS Percent Sol ids Petroleum Hydrocarbons as Extraction - Hydrocarbons Petro'leum Hydrocarbons as mg/kg 10 % ng/kg ms/ kg 9071 0e/221e4 5030/3sso 0el22le4 0e/26/e4 0s/26/e4 0s/26/e4 260 0i esel as Diesel Gasol i ne 0.01 5.0 6.0 69 ND 092694 ND Orn.r. data have been reviewed and are approved for release.4tu: Charles M. Cabaniss f'lanager, Inorganic Chemi stry .,li,i,tctto vl Poro.., !e' ns't Margaret S. Harding Manager, 0rganic Chemistry 98m Kincey Avenus, Suito 100 Huntarsville. NC 28078 TEL:70{-875-9G2 FAX: 704-875-909' An Equal 0pportunity Employer / ffi REPORT OF LABORATORY ANALYSIS Mr. John Burkart FOOTNQTES September 28, 1994 Page 4 for pages I through 3 PACE Project Number: 64092150i Cl 'ient Reference: Stork Screens MDL Method Detection LimitND Not detected at or above the MDL. 98fi) Kincay Avenue, Suite 100 Huntersville. NC 28078 IEl.: r0t-Er5-s!n FAX: 704-875-9091 An Equal 0pponunity Employer a ffi nrpoRr or LnaoRRroRY RllRlYsts Mr. John Burkart QUALITY C0NTROL DATA September 28, 1994 Page 5 PACE Project Number: 540921501 Client Reference: Stork Screens Petroleum Hydrocarbons as Diesel Batch: 92 30724 Samples: 92 0265455, 92 0266463, 92 0265471 METHOD BLANK: MethodParameter Units MDL Bl ank Pdfrdfeum Hydrocarbons as Diesel mg/R-g m ND- LABORATORY CONTROL SAMPLE: ReferenceParameter Units MDL Value RecvIEtffi]ffi Hydrocarbons as Diesel mgng 5.0. -T70- A% 9800 Kincey Avenus, Sujte 100 Huntgrsville, NC ?8078 IEt: r0{-gr5-$m FAX: 704-875-9091 An Equal 0pportunity Emgloyor / ffi REPORT OF LABORATORY ANALYSIS Mr. John Burkart QUALITY C0NTR0L DATA September 28, 1994 Page 6 Client Reference: Stork Screens Petroleum Hydrocarbons as Gasol'ine Batch: 92 30714 Samples: 92 0266455, 92 0256463, 92 0266471 PACE Project Number: 64092I501 MtrHoD BLANK: MethodParameter Units MDL Bl ank Et-roTeum Hydrocarbons as Gasoline mg7k0 6-3 ND-- SPIKE AND SPIKE DUPIICATE.. Spi ke Spi ke Dup'lParameter Units MDL 920258644 Spike Recv Recv RPqitffi Hydrocarbons as Gasoline -gA0 6T ND- TbA- i6ifr i{f, -T96 LABORATORY CONTROL SAMPLE: eb.".*.t.,Reference Uni ts MDL Val ue RecvEfidlffi Hydrocarbons as Gasol 'ine mgTkg 6.0 -m-- TO5% 98fi) Kincey Avenue, Suite 100 Hunterwille, NC 28078 TEk r0H75-$0 FAX: 704-875-9091 An Equal 0pportunity Employer , M REPORT OF LABORATORYANALYSIS Mr. John Burkart FOOTNOTES September 28, 1994 Page 7 for pages 5 through 6 PACE Proiect Number: 54092i50i Client Reference: Stork Screens MDL Method Detect'i on Li mi tND Not detected at or above the MDL.RPD Relative Percent Difference 9800 Kincey Avonue, Suite 100 Huntersville, NC 28078 TEL: r0f.t75-m FAX: 704-875-9091 An Equal 0pportunity Employer a:<E LUE,U'zoFo =EFo =Eolr UJoa uloEul tuG UJula r! \ !go- E(Eog(!o \e \-s '(t -\ \\ i '<o i\l\N\.\l,' :r\ $a\)z(:.(E'\ifro\ i E-' tr6a oc@ EEoo (Ec.9.=EE id(!oofoEooo,oq,tr oo,(uc6 (-,q)'e-' Lo()do_ I I I dl() Cf]_-))3olzl-tcl(l,lololol6lo-l oEooIIJE o-Oot-q,E*qe 6Ei'E =>fEo< e@ @(Y) oc F{ l"l I lil I ddtl61 2pl il -a =lOl9col al (L ail J I-tlil J q EIE'I<l U=tY:l O:l G;] APPENDEK VII CEI's Analytical Data - Ground Water ffi REPORT OF TABORATORY ANATYSIS THE ASSUBANCE Of OUALITY August 24, 1994 llr. John Burkart Cooper Environmental, Inc. 2300 Sardis Road North, Suite Q Charlotte, NC 28?27 RE: PACE Proiect No. 640812.509 CIient Reference: Laboratory Analysis Oear ltlr. Burkart: Enclosed is the report of laboratory analyses for samples received August 12, 1994. Footnotes are given at the end of the report. If you have any questions concerning this report, please fee'l free to contact us. Sincerely, L/;* Ll*^,*lo,- Kris H. Kommalan ProJect l,lanager EncI osures S800 (LtoI triltr, Suit 100 ltumdlr, ll0 28078 lEL: r0et76-e0tl FAt 704.875.909r An Equol opportunrty Emphyor ffi REPORT OF I.ABOBATORY ANATYSIS THE ASSURANCE Of OUATITY Oroor., Environmental, Inc. Chl oroform I ,2-Di chl oroethane l, 1, l-Trl chl oroethane Carbon tetrachloride Bromodi chl onnethane I ,2-0i chl oropropane trans- I , 3-Di chl oropropenel, l, 2-Trichl oroethene Dt bromochl oromethane I , I ,2-Tri chI oroethane ci s-1, 3-Di chl oropropenea August 24, 1994 PACE Project Number: 6408125092300 Sardis Road North, Suite QCharlotte, NC 282?7 Attn: l,lr. John Burkart Cl ient Reference: Laboratory Analysis PACE Sample l{umber: Date Collected: Date Received: CIient Sample ID: Parameter II{ORGAI{IC ANALYSIS INDIVIDUAL PARA,I,IETERS Chromlum Chromlum, Hexava'lent ORGAI{IC ANALYSIS Ii{DIYIDUAL PAM}IETERS Semivol. Tentative. Ident. Cpd. PURGEABLE HALOCARBONS AND AROIJIATICS Chloromethane Bromomethane Di chI orodl fI uoromethane Chloroethene (Vinyl chloride) Chl oroethane Di chl oromethane Tri chI orofl uoromethane I , l-Di chI oroethenel, l-0ichloroethane trans- I , 2-Di chl oroethene 92 024753t 08l12le4 08112/e4 Pt.l-1 Units nglL mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L 0.010 0.02 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 081994 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND l,lD ND ND ilD ND 6011602 081241e4 08lt2le4 08lt9le4 08ltele408lt9le4 08lt9ls4 08lt9le4 08lt9le4 08lrele4 08ltele4 08ltele4 08lt9le4 08lLel94 08/tele4 08/re/e4 081t9194 08ltele4 08l19le4 08l19ls4 a8/$le+ 08ltele4 08119194 08llele4 08lt9le4 Ir,tDL I{ETHOD DATE ANALYZED 200.7 7195 ND ND 0800 lftrrr AYmr, &ito 100 tknurrvifr, ilC 28078 rEL r0+t?t.e0u tAX: 704-875.9001 An Equal Opportunrty Employor ffi HEPORT OF TABORATORY ANATYSIS l,lr. John BurkartPage 2 C'lient Reference: Laboratory Analysis PACE Sample Number: Date CoIIected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS PURGEABLE HALOCARBONS AND AROMATICS 2-Chl oroethoxyethane Bromoform l, 1,2,Z-Tetrachl oroethane Tetrachl oroetheneilethyl-t-butyl ether Isopropyl ether Benzene Tol uene Chlorobenzene Ethyl benzene Xylenes I ,3-Dl chl orobenzene I ,4-01 chl orobenzene I ,2-Di chl orobenzene BASE/ilEUTRALS AND ACrDS Date Extracted, Base/Neutrals and N-Ni trosodimethyl ami ne bi s(2-Chl oroethyl ) ether Pheno'l z-Cht orophenol I,3-Di chl orobenzene I ,4-Di chl orobenzene 1,2-DichI orobenzene bi s (Z-ChI oroi sopropyl ) ether Hexachloroethane N-Ni trosod I -n-propyl ami ne Nitrobenzene 3, 5, S-Trimethyl -2-cycl ohexanone 2-t{ttrophenol 2, d-llimethyl phenol August 24, 1994 PACE Project Number: 640812509 92 0247531 08lt2le4 08lt2le4 P[-l }IETHOD DATE ANALYZEDUni ts ug/L ug/L uglL ug/L ug/L ug/L Acids Date ug/L ug/L us/L us/L us/L uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L 60t1602 us/L ug/L us/L ug/L ug/L ug/L ug/L ug/L 1.0 0.5 t.0 0.5 1.0 1.0 1.0 1.0 1.0t.0 1.0 1.0 1.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 625 ND ND l'lD ND ND t'lD ND t{D ND ND t{D ND t{D ND 081794 ND ND ND ND ND t{D lrD ND t{D ND ND ND ND l,lD NO 08lt9le4 08ltele4 08lt9le4 08lt9ls4 08ltelefi 08/tele4 08ltsl94 08ltele4 08lrele408lrele{au$le4 08lrele4 08lle/e4 asl,9le4 08lt7le4 08ltel94 08lrele4 08ltele4 08lL9le4 08ltele4 08ltele4 08lt9le4 08ltslel 08l19le4 08ltele4 08lrele4 08lrel94 08lrele4 08119/e4 081r9/94 abt s (Z-Chl oroethoxY)methane 98fi! l0rry tumr, Suit! 100ttmnrt, tC 18078 Itl.: ,0+8ri.e0l2 FAX: 7ll&875.9091 An Equd 0ppoltunrty Emplqyor 0ss9"BEPOBT OF LABOBATOBY ANATYSE l.lr. John BurkartPage 3 CIient Reference: Laboratory Analysis PACE Sample Nunber: Date Collected: Date Recelved: CIient Sample ID: Parameter August 24, 1994 PACE Project Number: 640812509 92 024753r 081t2/s4 08/t2le4 Pt{-l I-IETHOD DATE AI{AIYZED ORGANIC A}IALYSIS. BASE/]{EUTRALS AND ACIDS 2, {-Di chI orophenol 1,2, 4-Trlchl orobenzene Naphthal ene Hexachl orobutadi ene 4-Chl oro-3-methyl pheno'l Hexachl orocycl opentadi ene 2, 4, 6-Trl chl orophenol Z-Chl oronaphthal ene Acenaphthyl ene oB:H8lrl,tllxil:t: Acenaphthene 2,4-Dinltrophenol 2,4-Dinitrotol uene 4-Nitrophenol Fl uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-llethyl -4,6-di ni trophenol N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachlorobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate Fluoranthene Benzidine Pyrene Benzyl butyl phthalate 3, 3-0i chl orobenzi d i ne Units ug/L u9/L ug/L us/L ug/L us/L ug/L uglL ug/L ug/L uslL ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L ug/L ug/L uglL ug/L ug/L us/L ug/L us/L us/L ug/L ug/L ug/L 625 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 42 6.0 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 t7 ND ND ND ND ND lrD ND ND l{D ND l{D ND ND ND ND ND ND ND ND ND ND ilD ND t{D ND t{D ND irD ND ND ND 08lrele4 08/rele4 08ltele4 08llele4 08l19le4 a8l$le$ 08lrel94 08llele4 08ltelefi 08lt9le4 08119194 08ltel94 08l19le4 08lrele4 08lrele4 08l19le4 08lrele4 08lrele4 a8l$le4 08ltele4 08lrele4 08ltelefl 08llele4 08lrele4 08119194 08lrel94 08lrele4 a8lrcle408llele[ 08ltele4 08ltele4 S800 firry &aL. Suits 100ltrffi., ilC 28078 IEl.: 70+t76.t002 FA* 704.875.9119t An Equ.l oppodunily Emphyar llsl.s3.REPOBT OF TABORATORY ANATYSIS o ilr. Page IHE ASSURANCE OF OUAI. ITY John Burkart 4 CIient Reference: Laboratory PACE Sample ilurnber: Date Collected: Date Recelved:Client Sample ID: Parameter ORGATIIC A}IALYSIS August 24, 1994 PACE Project Number: 640812509 Analysi s 92 0247531 08l12le4 08lt2le4 Pt{-l Uni ts MDL I'IETHOD DATE ANALYZED BASE/]TEUTRALS AND ACIDS BenzIa] anthracene Chrysene bi s(2-Ethyl hexyl )phthal ate Dl-n-octyl phthal ate BenzoIb]fl uoranthene BenzoIk] fI uoranthene Benzotalpyrene IndenoI I ,2,3, -cdJpyrene - Di benzta.hlanthracene o!:ptlg;xiillil,l 8[:ros ate )Phenol-d5, (Surrogate) ilitrobenzene-dS, (Surrogate) 2-Fluorobtphenyl, (Surrogate) 2,4,i-Trlbromphenol, (Surrogate) Terphenyl-d14, (Surrogate) 625 ug/L ug/L ug/L us/L ug/L uglL ug/L ug/L u9/L ug/L % % 8.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 ND ND ND ND ND ND ND ND ND ND 33 22 59 59 75 80 % %ulo % 08/tele4 08ltele4 08ltel94 08ltele4 08lrsle408lrelel 08lrele408ltele408ltelel 08ltele4 08ltel94 08ltele4 081t9194 081t9194 08ltele4 08ltele4 S800 XiE y Avrnn, Suitc 100 tlmtmvill, t{C 28078 IEL: ,0+tr5.0092tilL 704.875.0081 tu Eqsal opportunlty Employtr l?s"ts€.IHE ASSUBII',CE 0F 0UAtlIY SEMIVOLATILES ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTTFIED COMPOUNDS Laboratory: PACE, Incorporated Iraboratory Code: 6409L2.509 Sample I-Dt 24753.L Matrix: WATER Sample Description: PW-l Sample wtlvol: 1 L File ID: 08199410 LeveL: LOW Date Received: 08-12-94 t Moisture: N/A Date Extracted: 08-L7'94 Extract Volume: 1.0 ML Date Analyzed: 08-19-94 Injection Volume: 2uL Dilution Factor: 1.0 pH: 7 concentratj.on Units z ug/l' Number of TICg Found: 1 CAS Number Compound Name RT Est. Conc. a 1 105-50-2 Caprolactam 2 3 4 5 6 7 I 9 10 L1 L2 13 L4 15 15 15.33 7 91 S8&l lft'cry Armlr. fuh 100 lMbrr,flh, llG 28078 IEl.: 70{.17t.t002 tAX: 704.875-0091 An Equd 0pnutudly trybrrt ffi REPORT OF TABORATORY ANALYSIS THE ASSUBANCE OF OUALITY Itlr. John BurkartPage 5 Client Reference: Laboratory Analysis PACE Sample llumber: Date Collected: Date Received:CIient Sample ID: Parameter II{ORGANIC ANALYSIS INDIVIDUAL PARAI.IETERS Chrom{um ORGANIC ANALYSIS INDIVIDUAL PAMI.IETERS Semivol. Tentatlve. Ident. Cpd. PURGEABLE HALOCARBONS AND AROMATICS Chloromethane Bromonethane ea;;*:tlfltll'?[iffiln:ili.r i de )Chloroethane Dichloromthane Tri chl orofl uoromethane 1, l-DichI oroethene l, l-Dichloroethane trans- l, 2-Di chl oroethene Chloroform I ,2-Di chl oroethane l, l, l-Trichl oroethane Carbon tetrachloride Bromodi chl ormethane I ,2-Di chl oropropane trans-l ,3-0i chl oropropene l, l, 2-Trlchl oroethene Dlbromchloromethanel, l, 2-Trichl oroethane ci s-l ,3-Di chl oropropene z-Chl oroethoxyethane Bromofonn 1,1,2,z-Tetrachl oroethane fretrachl oroethene August 24, 1994 PACE Project Number: 540812509 92 0247540 08/12/e4 08l12le4 l,lt{-3 I'IETHOD DATE ANALYZED mg/L 0.010 0.045 200.7 08124/94 Uni ts ug/L ug/L ug/L ug/L ug/L ug/L u9/L u9/L ug/L u9/L ug/L us/L ug/L ug/L ug/L us/L u9/L ug/L ug/L ug/L ug/L ug/L u9/L us/L ug/L 081994 ND ND ND ND ND ND ND ND ND ND ND ND ND t{D ND ND ND ND ND ND NO t'lD ND ND ilD 601/602 08ltelefi 081t9194 08lrel94 asl,9le408lt9lel 08119194 o8/telef 08/le/e4 oslrele4 08ltele4 08l19ls4 08lrele4 08/19/e4 08/ls/e4 081t9194 081t9194 o8lt9le4 08ltele0 08l19lel 08l19lel 08ltele4 08ltele4 08l19le4. oslrele[ 08119194 08lrele4 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 t.0 1.0 1.0 0.5 1.0 0.5 8800 nrry Ararn, Suih 100 Itmncd[r. t{c 28078 TEl.: ,0+t?$0092 tAX: 70t1.875.0091 An E0ual 0oponunfiy E nplo],or REPOBT OF LABORATORY ANALYSE l.lr. John BurkartPage 6 CIient Reference: Laboratory Analysis PACE Sample l{umber: Date Collected: Date Recelved: CIient Sample ID: Parameter ORGAI{IC AilALYSIS PURGEABLE HALOCARBOilS AND AROMATICS ilethyl-t-butyl ether Isopropyl ether Benzene ToI uene ChI orobenzene Ethyl benzene Xyl enes I ,3-Dl chl orobenzene I ,4-Di chI orobenzene ^ .2-Di chl orobenzenert' BASE/I{EUTRAIS Ar{D ACIDS Date Extracted, Base/Neutrals and Acids il-Ni trosodimethyl ami ne bl s (2-Chl oroethyl ) ether PhenoI 2-Chlorophenol I ,3-Di chl orobenzene I ,4-Dt chI orobenzene I,2-Dlchl orobenzene bi s (2-ChI oroi sopropyl )ether Hexachl oroethane il-l{ i trosod i -n-propyl ami ne l{itrobenzene 3, 5, S-Trimethyl -2-cycl ohexanone 2-Nitrophenol 2,4-0lmethyl phenol bi s (2-Chl oroethoxy)methane 2,4-Di chl orophenol I , 2,4-Tri chl orobenzene llaphthalene Jexachlorobutadlene August 24, 1994 PACE Project Number: 640812509 92 0247540 08lt2le4 08lt2le4 iltr-3 I.|ETHOD DATE Ai{ALYZEDUni ts ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Date ug/L ug/L ug/L us/L u9/L 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 ND ND ilD t{D ND ND ND l{D t{D t{D 60t1602 625 08ltel94 08119194 08lt9le4 08l19le4 08l19l9408ltelel 081t9194 08lt9le4 08ltel94 08ltele4 081t7le4. 08ltele4 08/tele4 08ltel94 osltele4 08l19le4 08l19le[ 08l19le4 a8/rc/e4 08119194 08ltel94 08lrsle4 08ltele4 08/rel94 a8l,9le4 08l19le4 08ltele4 08/19lel 081t9194 08/19/94 081794 ND t{D ND ND ND ND ND it0 ND ND r{D ND ND ND ND ND I'lD ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L ug/L S800 &c.v Amr., &dh 100ltsurrfr. ilC 28078 IEL 'o+arE 90t2 FA* 70'l-875.909t An EquC Opportunity Emplryor ffi REPOHT OF LABOBATOBY ANATYSIS IHE ASSURANCE OF OUALIIY l.lr. John BurkartPage 7 August 24, 1994 PACE Project Number: 640812509 Client Reference: Laboratory Analysis PACE Sample ilumber: Date CoIlected: Date Recelved: Client Sample ID: Parameter ORGANIC AI{ALYSIS BASE/I{EUTRALS AND ACIDS 4-Chl oro-3-methyl phenol Hexachl orocycl opentadi ene 2, 4, 6-Tri chl orophenol 2-ChI oronaphthal ene Acenaphthylene Dimethyl phthalate 2,6-Dtnltrotol uene Acenaphthene 2,4-Di ni trophenol e:il;?l3llHli""' FI uorene 4-Chlorophenyl phenYl ether Diethyl phthalate 2-l{ethyl -4,6-di nl troPhenol l{-ili trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate FI uoranthene Benzidine Pyrene Benzyl butyl phthalate 3, 3-Dt chl orobenzl di ne BenzIa]anthracene Chrysene bl s ( 2-Ethyl hexyl ) phthal ate l-n-octylphthal ate 92 0247540 081t2/94 08l12le4 l-lt{-3 METHOD DATE ANALYZEDUnits ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L uglL ug/L ug/L ug/L ug/L us/L ug/L ug/L 625 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 4? 6.0 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 t7 8.0 5.0 5.0 5.0 ND ND ND ND ND ND ND ND ND t{D ilD ND ND t{D ND ND ND ND ND ND ND ND ND ND ND ND 1{D ND t{D ilD t{D 08lrel94 oslrsls4 08/tele4 o8lt9l94 08lt9le4 08/t9le4 @ltele4 a8l$194 08119194 08ltel94 oslrele4 081t9/94 08l19le4 08lt9le4 08lt9l94 08lrel94 08ltele4 08ltgle4 oslLele4 a8/N/e4 08ltele4 08ltelefi 08ltels4 08lrele4 081t9194 08l19le4 08lrel94 08l19lefl 08lrele4 08lrele4 081t9194 uglL us/L ug/L ug/L ug/L ug/L ug/LDo S800 f!8, Ailqrr, &it I00 ltnrmtr, llc 28078 IEL: 70+l76.t0tl fAX: 7l)4.875.9081 An Equal oDpoilunily Emilryor ffi HEPOBT OF TABORATORY ANALYSIS IHE ASSURANCT ()F OUAI. ITY BASE/ilETTTRALS AND ACIDS BenzoIbJfl uoranthene BenzoIkJfl uoranthene BenzoIaJpyrene Indeno I l, 2, 3, -cd] pyrene Di benz Ia, h] anthracene Benzo[9,h, i ]perylene 2-Fluorophenol, (Surrogate) % Phenol-d5, (Surogate) % ^ilitrobenzene-d5, (Surrogate) % Q;ilpillllHuk,Ii:'isfltl3l.,.r u Terphenyl-dl{, (Sumogate) % l.tr. John Burkart August 24, 1994Page 8 PACE Proiect Number: 540812509 CIient Reference: Laboratory Analysis PACE Sample l{umber: 92 0247540 Date Collected: 08/12/94 Date Received: 08112194 Client Sample ID: lll{-3Parameter Units l'|DL I.|ETHOD DATE ANALYZED ORGANIC ANALYSIS 62sug/L 5.0 NDus/L 5.0 ilDug/L 5.0 tlDus/L 5.0 N0ug/L 5.0 NDug/L 5.0 ND 08lrel94 08lt9le4 a8l,9/e4 08ltele4 081t9194 08/t9le4 08lt9le4 a8l$194 08lrel9408lt9lel 08ltele4 08lte/e4 38 25 65 63 72 76 S800 IiE ? Avonq Suit! 100 ItnonYfr, ltc 28070 Itl,: 70+tr5.l0l2 tAX: 704.875.9091 An Equal opporfullty Emph/sl nssc,THt ASSURANCE OT OUALITY SEMIVOLATII,ES ORGA}IICS A}IA],YSIS DATA SHEET TEMTAIrIIELY TDEMTIFTED COMPOUNDS Laboratory: PACE, Incorporated Laboratory code : 540812. 509 Sample \D: 24754.0 Matrix: WATER Sample Description: MW-3 Sample wX/vol: 1 L File ID: 08L99411 Level: LOW Date Received: 08-12-94 t Moisture: N/A Date Extracted: 08-17-94 Extract, Volume: 1.0 ML Date Analyzed: 08-19-94 Injection Volume: 2uL Dilution Factor: 1.0 pll: 7 Concentration Units z ug/t' llumber of TICg Found: 1 CAS Number Compound Name RT EEt. Conc. O 1 105-50-2 Caprolactam 2 3 4 5 6 7 I 9 10 11 L2 13 L4 15 16 15.37 19 91 0800 lGorf rrmn $du 100 llmunir, tl0 28070 fE[: ,0'&8r[-t0t2 fil(: 70'$875-9001 An EqtC oppoitnity Empbyr ffi BEPORT OF TABORATOBY ANALYSIS o IIII ASSIJBANCE OT OUAI.ITY l,lr. John BurkartPage 9 Cl ient Reference: Laboratory Ana'lysis PACE Sample Number: Date Collected: Date Recelved: Client Sample ID: Parameter INORGANIC ANALYSIS INDIVIDUAL PAMI.IETERS Chromi um ORGAI{IC AI{ALYSIS August 24, 1994 PACE Project Number: 640812509 Uni ts 92 0?47558 08l12le4 08lt?le4 t{u-? I.IETHOD OATE AilALYZED I NDIVIDT'AL PARA,I.'IETERS Semivol. Tentative. Ident. CPd. PURGEABLE HALOCARBONS AND AROMATICS ChI oromethane--. Bromomethane IOictrt orodi fI uoromethane- Chloroethene (Vinyl chloride) Chl oroethane Di ch] oromethane Tri chl orofl uoromethane I , I -Di chl oroethene I , 1-Di chl oroethane trans-l , 2-Di chl oroethene Chl oroform I , 2-Di chl oroethane I, l, I-Trichl oroethane Carbon tetrachloride Bromodichl ormethane I , 2-Di chI oropropane trans- I ,3-Di ch'l oroProPene 1, I ,2-Tri chl oroethene Di bromochl oromethane I , I ,2-Tri ch] oroethane ci s-1 ,3-Di ch]oropropene 2-Chl oroethoxyethane Bromoforml, 1,2,Z-Tetrachl oroethane O rrrr.chloroethene mg/L 0.010 0.188 081994 ug/L ug/L ug/L u9/L u9/L ug/L uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L 601/602 200.7 081241e4 o8ltel94 081221e4 08122194 08l22le4 o8/221e4 08122te4 081?21e4 08l22le4 081221e4 081221e4 081221e4 08l2219!. 0812?lel 081?21e4 081221e4 081221e4 081221e4 081221e4 a8122194 081221e4 081221e4 08l22le4 081221e4 08l?21e4 08l22le[ a8l22le[ ug/L ug/L ug/L ug/L ug/L ug/L 50 ND50 ND50 ND50 ND50 ND50 150 PC 50 ND250 700050 ND50 ND25 ND50 150 250 1900050 ND?5 ND50 ND50 ND50 ND 25 ND50 ND50 ND50 ND?5 ND50 ND 25 L20 9800 Klncay Avenua Suito 100 Huntersville, NC 28078 TEk 704.875.0092 FAX: 704.875.9091 An Equal opportunity Employsr ffi REPORT OF LABORATORY ANATYSIS rHt tssuEAucl 0f 0uatlTv l,lr. John Burkart Page l0 Client Reference: Laboratory Analysis PACE Sample llumber: Date CoIIected: Date Received: CIient Sample ID: Parameter oRGA{rC ANALYSIS PURGEABLE HALOCARBONS AND AROMATICS Methyl-t-butyl ether Isopropyl ether Benzene ToI uene Chl orobenzene Ethyl benzene Xyl enes I ,3-Dl chl orobenzene Ol:IBl:Rls#:l13l: BASE/NEUTRALS AND ACIDS Date Extracted, Base/Neutrals and Acids N-Ni trosodi methyl ami ne bi s (2-Chl oroethyl )ether Phenol 2-Ch1 orophenol I ,3-Di chl orobenzene I ,4-Di chI orobenzene I , 2-Di chI orobenzene bi s(2-Ch1 oroi sopropYl )ether Hexachl oroethane N-N i trosod i -n-propyl ami ne Ni trobenzene 3, 5, 5-Tri methyl -2-cYcl ohexanone 2-Nitrophenol 2,4-Dimethyl pheno'l bi s ( 2-Chl oroethoxy ) methane 2,4-Di chI orophenol I , 2,4-Tri chl orobenzene Naphthal ene 1] Hexachl orobutadi ene August 24,1994 PACE Project Number: 640812509 92 02475s8 08lt2le4 08lt2le4 nY-2 Uni ts u9/L ug/L uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L Date ug/L ug/L uglL ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L u9/L ug/L ug/L uglL ug/L ug/L ug/L ug/L 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 l.l0L 60r/602 625 DATE ATIALYZED 08l22le{'. 08122194 081221e4 081?2194 08122194 081221e4 081221e4 08l22le4 o8l22le4 au22le4 o8lr7le4 osltele4 08/le/e4au,3le4 08ltele4 osltele4 08lrelel 08llele4 08lle/e408lt9le{ 08ltel94 08lt9le4 08llel94 08lrele4 08ltele4 08ltel94 08lrele4 081t9194 oslrelel 08/1e/e4 ND ND ND ND ND ND ND ilD ND ND 081794 ND ND t{D ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 50 50 50 50 50 50 50 50 50 50 9800 Kincey Avsnue, Suits 100 Huntersville, ltl0 28078 TEL 704.875.9092 FAX: 704.875.909I An Equal opportunity Employer ffi BEPORT OF TABORATORY AIUALYSIS IIIT ASSURANCE ()T OUATITY l,lr. John Burkart Page ll CIient Reference: Laboratory Analysis PACE Sample Number: Date Collected: Date Received: CIient Sample ID: Parameter August 24, 1994 PACE Project Number: 640812509 92 0?47558 08ltue4 oslr?le4 l.lU-2 Units ug/L u9/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L us/L ug/L ug/ L ug/L ug/L uglL u9/L us/L ug/L },IDL I,IETHOD DATE AI{ALYZED ORGAI{IC ANALYSIS BASE/i{EUTRALS At{D ACIDS 4-Chl oro-3-methyl phenol Hexachl orocycl opentadi ene 2, 4, 6-Tri chl orophenol 2-ChI oronaphthal ene Acenaphthylene Dimethyl phthalate 2,5-Dinitrotoluene Acenaphthene oitr:,-Blrltl8lliffi].- 4-Nitrophenol Fl uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-t'lethyl -4, 6-d i n i trophenol N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidine Pyrene Benzyl butyl phthalate 3, 3-Di chl orobenzi di ne Benz Ia] anthracene Chrysene bi s (2-Ethyl hexyl )phthal ate I Oi-n-octyl phthal ate 625 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 42 5.0 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 17 8.0 5.0 5.0 5.0 ND ND ND ND ND NO ND ND ilD ND ilD ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND osltelel08ltelel 08ltele408ltelel osltele4av$/e4 asl,9le* 08ltele4 08l19le4 08/rele4au$le4 08lrele4 a8l,3/e4 08lt9le4 08lrel94 osltele4 08lrel94 08ltele4 08ltele4 08lrele4 08/Le/e4 08ltele4 08lt9le4 08l19le4 08119194 08lrele4 08ltgle4 08l19lefiosltelel 081t9194 o8lt9l94 9800 l$noy Avenue, Suhe 100 HuntorsYilk, NC 28078 TEL: 704.875-9092 FAX: 704.875.9091 An Equal opportu,rity Employor ffi REPORT OF LABORATORY ANATYSIS THT ASSURANCE Of OUALITY I'lr. John Burkart Page 12 Cl ient Reference: Laboratory Analysis PACE Sample Number: Date Collected: Date Received:Client Sample ID: Parameter ORGANIC AI{ALYSIS BASE/I{EUTRALS A}lD ACIDS Benzo I b] fl uoranthene BenzoIk]fl uoranthene BenzoIa]pyrene IndenoI l, 2, 3, -cd]pyrene Di benzIa, h] anthracene Benzo [9, h, i ] peryl ene Z-Fl uorophenol, (Surrogate) Phenol-d5, (Surrogate) ^Nitrobenzene-dS, (Surrogate) I-Fluorobiphenyl, (Surrogate)vz,4,G-Tri bi'omoitr6ndt, (sirrolate ) Terphenyl -d14, (Sumogate) These data have been reviewed and are Uni ts August 24, 1994 PACE Project Number: 640812509 92 A247s58 081t2/e40elnle4 i4u-2 l.lETH0D DATE ANALYZED 6?5 ug/L ug/L us/L ug/L ug/L ug/L %uh Ulo %ulo % approved 5.0 5.0 5.0 5.0 5.0 5.0 for release. ND ND ND ND ND ND 37 26 60 60 76 64 081t9194 08ltel94 08lt9l94 081t919408ltele{ 08/rel94 08/19/e{ o8/191e4 08/re/9{ 08/19/9{ 08l19le4 08/19/e4 ,G.!ft4argaret Manager, S. Harding 0rganic Chemistry 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 TE[: 704.875.9092 FAX: 704.875.9091 An Equal 0pportunity Employsr ffi THE ASSUBAT',Ct 0f 0UALlTY SEMIVOI,ATTLES ORGA}TICS AI{ALYSIS DATA SHEET TENTATIVELY IDEMTIFIED COMPOI]NDS Laboratory: PLCE, fncorporated Laboratory Code : 5408L2 .509 Samp1e fD: 24755.8 Matrix: WATER Sample Description: MW-Z Sample wtlvol: L L File ID: 081,994L2 Level: LOW Date Received: O8-L2-94 t Moisture: N/A Date Extracted: 08-17-94 Extract VoLume: 1.0 ML Date Analyzed: 08-19-94 Injection VoLume: 2uL Dilution Factor: 1.0 pII: 7 Concentration Units: ug/L Number of TICg Found: 5 C.A,S Number Compound Name RT EEt. Conc. O 1 L23-9L-1 1,4-Dioxane 2 L27-L8-4 TetrachLoroethylene 3 L05-50-2 Caprolactam Unknown Unknown 5.18 42 7.49 37 l_5.37 22 22.0L 5 34.37 37 91 98 91 4 5 6 7 I 9 10 11 t2 r.3 t4 r_5 r_6 9800 Khcey Avenue, Suils 100 Huntotsviflo, f'l0 28078 TEk 704.875.9092 FAX: 704.875.9091 An Equal 0pportmity Empbyer NSCG REPORT OF LABOBATORY ANATYSIS oMr. Page ]HT ASSUf,AIiCE ()f OUAI,IIY John Burkart t3 Cl ient Reference: Laboratory Analysis l.lDL l{ethod Oetection LimitND Not detected at or above the MDL.PC Possible laboratory contaminant. FOOTNOTES August 24, 1994for pages I through 12 PACE Project Number: 640812509 9800 Khcay Avenue, Suite t00 Huntersville, l{C 28078 TE!: 704-875.9032 FAX: 704-875-9091 An Equal 0pportunily Employsr ffi REPORT OF LABORATORY ANALYSE THT ASSURANCE Of OUATITY Itlr. John Burkart QUALITY C0NTR0L DATA August 24, 1994 Page 14 Client Reference: Laboratory Analysis Chromium, Hexavalent Batch: 92 29914 Samples: 92 0247531 }IETHOD BLANK: l,lethodParameter Units MDL Blankefiffim] Hexavalent mEtr- 012 Nf PACE Project Number: 540812509 ReferenceVaIue RecvTTO- TET LABORATORY CONTROL SAMPLE: Parameter Cfiiomlum-, Hexaval ent Units MDLmsTf- 0Tz 9800 Kincey Avanue, Suite 100 Huntersville, NC 28078 TEk 704.875.0092 FAX: 704.875.9091 An Equal Opportunity Employer n,$99"BEPORT OF I-ABOBATOBY ANATYSIS q". Page Parameter INDIV IDUAL PARAT.IETERS Cal ci um I'lagnesi um Molybdenum Potassi um Sodi um ICP QUALITY C01{TR0L Nickel Cadmium lx:l:o'*- Barium Copper Chromi um Beryl I i um Zinc Cobal t Iron Si I ver l.langanese Al uminum LABORATORY CONTROL SAI'IPLE: Parameter IilOIVIDUAL PARA}IETERS CaI ci um Magnesi um Molybdenum Potassi um Sodi um CIient Reference: Laboratory Analysis ICP QUALITY CONTROL Batch: 92 30069 Samples: 92 0247531, 92 0247540, 92 0247558 I'IETHOD BLAI{K: THE ASSURAI'lCE 0t 0UALlTY John Burkart l5 QUALITY CONTROL DATA August 24, 1994 PACE Project l{umber: 640812509 ReferenceVaIue Recv 5.0 100r5.0 96r,5.0 tt,,5.0 84f,,5.0 gffi Uni ts ms/L mg/L mg/L mg/L mg/L nglL mg/L mg/L mg/L mg/L mg/L rE/L nglL mg/L mg/L mg/L mg/L ng/L ms/L Units mg/L mg/L mg/L mg/L mg/L l,lethod BI ankI-lDL 0. r0 ND 0. l0 ND0.020 ND 0. l0 ND 0. t0 ND 0.010 0.010 0.010 0.10 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.005 0.010 0.010 0. t0 0. l0 0.020 0. l0 0. l0 ND ND ND ND ND NO ND ND ND ND ND ND ND ND 9800 Xincoy Avenuo, Suits 100 Huntsrsvilh, t{C 28078 TEL: 70&875.9092 FAX: 704.875.9091 An Equal OpportunrU Emplofr ffi REPORT OF LABORATORY ANALVSIS THT ASSURANCT OI OUAIITY Hr. John Burkart Page 15 CI ient Reference: Laboratory Analysis ICP QUALITY CoilTRoL Batch: 92 30069 Samples: 92 0247531, 9? 0247540, 92 A247558 LABORATORY COI{TROL SAIiIPLE : Parameter Uni ts QUALITY CONTROL DATA August 24,1994 PACE Project Number: 640812509 ICP QUALITY COi{TROL Ni ckel Cadmi um Vanadi um Lead Bari um Copper Chromi um d:ril:'- Iron Si I ver l.langanese Al uminum ReferenceVa]ue Recv 0.500 l00r0.500 107f,0.500 103tr0.50 104x0.500 l05s0.500 99r 0.500 10lr0.500 l08r0.500 l05r0.500 99,0.s00 106%0.050 ltax 0.s00 104r0.500 93% mg/L mg/L mg/L mg/L mg/L ng/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.010 0.010 0.010 0. l0 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.005 0.010 0.010 9800 Kincay Avenue, Suite 100 Huntcrsvile, NC 28078 TE[: 70&875.9082 FAX: 704-875.9001 An Equal oppofiunity Employer ffiIHt ASSURAI,ICE 0t 0UAl-lTY SEMIVOLATILES ORGANICS AITALYSIS DATA SHEET TE}TTATTVELY IDENTIFIED COMPOUNDS Laboratory: PACE, IncorPorated Laboratory Codet 5408L2.509 Sample ID: METHOD BLANK Matrix: WATER Sample Description: N/A Sample wc/vol: 1 L Level: LOW B Moisture: N/A Extract Vo1ume: 1.0 ML Injection Vo1ume: 2uL PH:7 FiLe ID: 08199408 Date Received: N/A Date Ext,raet,ed: 08-17-94 Date Analyzed: o8-L9-94 Dilution Factor: 1.0 correentration Units: ug/L O Number of TICE Found: O CAS Number Compound Name RT Est. Conc. A 1 2 3 4 5 6 7 I 9 t-0 l_1 t2 13 t4 15 16 9800 Kincey Avenue, Suite 100 Hunt8rsville, I{C 28078 TEk 704.875.0002 tAX: 704.875-9091 An Equal 0pponunity Employet RNSc.REPOBT OF TABIIRATORY ANALYSIS q,. ,,,, ,--::." o'F oUA TY Page l7 QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 640812509 CIient Reference: Laboratory Analysis BASE/NEUTRALS Ar{D ACIDS Batch: 92 30011 Sanples: 92 0247531, 92 0247540, 92 0247558 I.IETHOO BLANK: Parameter Uni ts l,lethod Bl ank 081994 INDIVIDUAL PAMT"IETERS Semivol. Tentative. Ident. Cpd. BASE/ilEUTRALS AND ACIDS N-Ni trosodimethyl ami ne bi s (2-Chl oroethyl ) ether PhenoI 2-ChI oropheno'l I ,3-Di chl orobenzene I ,4-Di chl orobenzene us/L ug/L ug/L uglL ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 42 ND ND ND ND ND ND ND ND NI) ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND f, , z-Dl ch rorobenzene bi s (Z-ChI oroi sopropyl ) ether Hexachl oroethane N-l{i trosodi -n-propyl ami ne Nitrobenzene 3, 5, 5-Trl methyl -2-cycl ohexanone 2-Ni trophenol 2,4-Dimethyl phenol bi s (2-ChI oroethoxy)methane 2,4-Di chl orophenol I , 2,4-Tri chl orobenzene Naphthal ene Hexachl orobutadi ene 4-Ch1 oro-3-methyl phenol Hexach'l orocycl opentadi ene 2, 4, 6-Tri chl orophenol 2-Chl oronaphthal ene Acenaphthyl ene Dimethyl phthalate 2,6-Di ni trotol uene Acenaphthene 2,4-Di ni tropheno'l 9800 Xinc-oy AYenue, Suile lll0 Huotsrsvil0, NC 28078 TEL 70&875.8002 FAX: 704.875'9091 An Equal opportunry Employer ffi REPORT OF LABOBATORY ANATYSE o I'lr. Page IHE ASSUBANCT Of OUATITY John Burkart 18 QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 540812509 Client Reference: Laboratory Analysis BASE/NEUTRALS Ar{D ACIDS Batch: 92 30011 Samples: 92 0247531, 9? 0247540, 92 0247558 }IETHOD BLAI{K: Parameter ilffinTfrotoluene4-Nitrophenol Fl uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-ilethyl -4,6-di ni trophenol N-Ni trosod i phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol cl;nu:!ffi" Di-n-butyl phthalate Fl uoranthene Benzidine Pyrene Benzyl butyl phthalate 3, 3-Di chl orobenzi di ne Benz Ia] anthracene Chrysene bi s (2-Ethyl hexyl )phthal ate Di -n-octyl phthal ate Benzo I b] fI uoranthene Benzo I k] fI uoranthene BenzoIa]pyrene Indeno I l, 2, 3, -cd] pyrene Di benz I a, h ] anthracene Benzo[g,h,i]perylene 2-Fluorophenol, (Surrogate) PhenoI-d5, (Surrogate) Nitrobenzene-d5, (Surrogate) Or-t, uorobiPhenY'l ' (Sumogate) Uni tsusrr uglL Ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L u9/L ug/L ug/L uglL ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L uglL I'lethod BI ankilr- ND r{D ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 39 25 70 57 MDL63 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 17 8.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 ug/L ug/L ug/L ug/L %utb oll0 ollo 9800 l0ncay Avrnre, Suite 100 Huntersvilh. l{C 28078 TEk 704.875.0002 FAX:704.875-9091 An Egual 0pportunity Employer ffi REPOBT OF LABORATORY ANALYSIS THT ASSUEANCE Of OUALITY }4ETHOD BLANK: Parameter Z,-f,f-IFr'bromophenol, ( S u mog at e ) Terphenyl -d14, (Surrogate) LABORATORY CONTROL S/TMPLE: ParameterFtrftro s-od i me t hyl am i n e bi s (2-ChI oroethyl ) ether PhenoI - z-Chloroohenol et:rBl:Ris#:#:t: I ,2-Di chl orobenzene bi s (2-ChI oroi sopropyl ) ether Hexachl oroethane N-Ni trosodi -n-propyl ami ne Nitrobenzene 3 , 5, 5-Tri methyl -2-cycl ohexanone 2-Nitrophenol 2,4-Dimethyl phenol bi s (Z-ChI oroethoxy)methane 2,4-Dich1 orophenol I ,2,4-Tri chl orobenzene Naphthal ene Hexachl orobutadi ene 4-Chl oro-3-methyl phenol Hexachl orocycl opentadi ene 2, 4, 6-Tr ichl orophenol 2-Chl oronaphthal ene Acenaphthyl ene Dimethyl phtha'late J'o-oinitrotol uene I'lr. John Burkart Page 19 CIient Reference; Laboratory Analysis BASE/NEUTRALS AND ACIDS Batch: 92 30011 Samples: 92 024753f, 9? 0247540, 92 0247558 QUALITY CONTROL DATA Uni tsT_ ollo 1''lDL Uni ts usTr- ug/L uglL ug/L ug/L ug/L ug/L uglL ug/L ug/L u9/L ug/L uglL ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L u9/L ug/L us/L 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 August 24, 1994 PACE Project Number: 540812509 ReferenceValue Recv-Tr -Im 68ff 66,6 56r 66r 54r 58% 4& 68% 52% 6ffi 64% 660% 76* 8ofr l,lethod BI ank5r- 80 62A 3AX 6M 4& 50r 50r 46r 48r 68f, 64* 56% M0t53 6.0 5.0 5.0 5.0 5.0 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 5 50 50 ug/L us/L 9800 fincey Avcnue, Suite 100 Humcrsvilh, l{C 28078 TEk 704.875.0092 FAX: 704.875.9091 An Equal oppoilunity Employer l),ss^3.REPOBT OF TABORATORY ANALYSIS o Mr. Page THI ASSUEAI'ICE OF llUAI.IIY John Burkart 20 Parameter ffifr'aFh'f,hene 2,4-Di ni trophenol 2,4-Dinitrotol uene 4-Nitrophenol FI uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-ilethyl -{, 6-di n i trophenol N-Ni trosodl phenyl ami ne ^4-Bromophenyl phenyl ether q:ffi:lli#ffiilffi3i Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidine Pyrene Benzyl butyl phthalate 3,3-Di ch'lorobenzi di ne BenzIa] anthracene Chrysene bi s ( 2-Ethy'l hexyl ) phthal ate Di -n-octyl phthal ate BenzoIb] fI uoranthene BenzoIk]fl uoranthene BenzoIa]pyrene Indeno [ 1,2,3,-cd] pyrene Di benzIa, h] anthracene Benzo [g , h, i ] peryl ene QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 540812509 CIient Reference: Laboratory Analysis BASE/NEUTRALS A]{D ACIDS Batch: 92 30011 Samples: 92 0247531, 92 0247540, 92 0247558 LABORATORY CONTROL SAI.IPLE : Uni tsuszr ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L ug/L uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 t7 8.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 MDL 53, 42 5.0 5.0 5.0 5.0 ReferenceValue Recv--50- a6*50 7ffi50 7#50 3&50 74%50 72r 76, 9M 98f,t4r 76r, 7U 7ffi 78% 76r, 80r t9*, 74% 7ffi 8?% 76% 8of; 78r, 7gr, 7gx 82r, 7ffi 80% 100tr 80x 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 9800 Kincey Avenue, Suile 100 Huntersville, I{C 28078 TEk 704.875.9092 FAX: 704-875.9091 An Egual opportunity Employer ffi REPORT OF LABORATOBY ANALYSIS THT ASSUSANCE OT OUATI]Y ltlr. John Burkart Page 2l Client Reference: Laboratory Analysis QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 640812509 PURGEABLE HALOCARBONS Batch: 92 30029 Samples:92 0247531, AND AROMATICS 92 0?47540 I4ETHOD BLANK: Parameter C['T6?6fr6[hane Bromomethane Di chl orodi fl uoromethane Ch'loroethene (Vinyl chloride) Chl oroethane Di chl oromethane Tri chI orofl uoromethane I, l-Dichloroethene I , l-Di chl oroethane .-.trans-l .2-Di chl oroethenee nt orof6rm- I ,2-Dichl oroethane l, I , l-Tri chl oroethane Carbon tetrach'loride BromodichI onnethane I ,2-Di chl oropropane trans-l ,3-Di chl oropropene I , I ,2-Tri chl oroethene Di bromochl oromethane I , I ,2-Tri chI oroethane ci s-1,3-Di chl oropropene 2-ChI oroethoxyethane Bromoform 1,1,2, 2-Tetrachl oroethane Tetrachl oroethene Itlethyl -t-butyl ether Isopropyl ether Benzene Tol uene Chl orobenzene Ethyl benzene Jrtenes Uni ts,gr ug/L ug/L ug/L uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L us/L ug/L ug/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L l,lethod Bl ankND- ND ND ND ND3.0 PC MDLr3 1.0 1.0 1.0 1.0 1.0 ug/L us/L 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 0.5I.0 1.0 1.0 1.0 1.0 1.0 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9800 Xhcey Avcrue, Suite .l00 Hunts.svilh, NC 280i8 TEk ?04.875.9092 FAX: 704.875.9091 An Equal opportunity Employer ffi REPOBT OF TABORATORY ANALYSIS o l4r. Page THT ASSURAI,ICE ()I OUALI]Y John Burkart 22 Client Reference: Laboratory Analysis QUALITY CONTROL DATA August 24, 1994 PACE Project l{umber: 540812509 PURGEABLE HALOCARBONS Batch: 92 30029 Samples: 92 A247531, I.IETHOD BLAilK: Parameter fFjDlEfi,.forobenzene I ,4-Di chl orobenzene I , 2-Di chl orobenzene AND AROMATICS 92 0247540 Uni ts us/L- us/L ug/L l,lDLI.3 1.0 1.0 l,lethod BI ankNT NI) ND SPIKE AND SPIKE DUPLICATE: Parameter Cfi'T6F6frdlhane ^ BromomethaneIoi ctrt orod i fl uoromethanevChloroethene (Vinyl chloride) ChI oroethane Di chl oromethane Tri ch'l orofl uoromethane I , l-Di chl oroethene I , l-Di chl oroethane trans-l ,2-Di chI oroethene ChI oroform 1,2-Di chl oroethane 1, l, l-Trichl oroethane Carbon tetrachloride Bromodi chl ormethane I , 2-Di chl oropropane trans- 1 ,3-Di chl oropropenel, l, 2-Trichl oroethene Di bromochl oromethane l, l, 2-Tri chl oroethane ci s-1, 3-Di chl oropropene Bromoforml, l, 2, 2-Tetrachl oroethane Tetrachl oroethene Or.rnrt-t-butyl ether Uni tsusrr ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL uglL ug/L ug/L ug/L ug/L uglL u9/L ug/L u9/L ug/L 920246675ND- ND ND ND ND 1.3 PC ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 27 Soi ke2f 20 20 20 20 20 Spi ke Sptke Dupl Recv Recv RPO-16* -65r rg95r t00r sf,80r 85r 6%85% 90f, 6%85r 90X 6%6% 74'6 7% MDLIT 1.0 1.0 t.0 1.0 1.0 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 0.5 1.0 0.5 1.0 20 20 20 ?0 20 20 20 ?0 20 20 20 20 ?0 ?0 20 ?0 20 20 20 6% 5r a% 0r 5% ofr 5r 5% 0% 0% 6% 0% 0% 0% 7% 7% 7% 0% 0% 80s 85r95r 10ffi90s 90fi95r" 95*9W 95*90* 90fr gffi 95r90r 95fr95% 95%90tr 90r,85X 90r95S 95% 85% 85%85fr 85r70% 75r,70f; 75r,75ff 7M90f, 90% t25fr 125,, 9800 Xincey Avenue, Suite t00 HuntslsYille, NC 28078 TEL: 70+875.3092 FAX: 704-875-9091 An Equal 0pportunity Emphyer ffi REPORT OF LABORATORY ANALYSE o Mr. Page IHE ASSURANCE OT OUAI.ITY John Burkart 23 Cl ient Reference: Laboratory Analysis QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 540812509 PURGEABLE HALOCARBONS Batch: 92 30029 Samp'les: 92 0247531 , SPIKE AND SPIKE DUPLICATE: Parameterfs@f ether Benzene ToI uene Chl orobenzene Ethyl benzene Xyl enes I ,3-Di chl orobenzene I ,4-Dichl orobenzene d ,Z-Di chl orobenzene LABORATORY CONTROL SAIIIPLE: Parameter eh'Tffifrd[hane Bromomethane Di chl orod i fl uoromethane Chloroethene (Vinyl chloride) Ch1 oroethane Di chl oromethane Tri chl orofl uoromethane I , l-Di chl oroethene I , l-Di chl oroethane trans-l ,2-Di chl oroethene Chl oroform I ,2-Di chI oroethane l, 1, l-Tri chl oroethane Carbon tetrachloride Bromodi ch'lormethane I ,2-Di chI oropropane trans- I ,3-Di chl oropropene I , I ,2-Tri ch] oroethene !t urorochl oromethane 920246675 SoikeffD- zf3.6 20ND 20ND 20ND ?O1.3 50 AND AROMATICS 92 0247540 Uni tsusTr ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L RPD-g 5r 5% 0rlls 7% MDLr3 1.0 1.0 1.0 1.0 1.0 Spi ke Spike Dupl Recv RecvJM T5Tl02r L0lr95r 100f,90r 90*90f, l00rglx 9w Uni tsus/r ug/L u9/L ug/L ug/L uglL us/L us/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L uglL uglL ug/L 1.0 1.0 1.0 I'IDLilo 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 20 20 20 ND ND ND 85r 85r 0X90s 85f, 6%90r 80r n% ReferenceValue RecY-ar- Tm20 90%20 90%20 85%20 85r20 90% 20 20 20 20 20 2A 20 ?0 20 20 20 20 20 80% 95% 8sfr 90% 90% 8sfr 90% 90r 85r 85% 90% 90r 85% 9800 Kincey Avorue, Suite 100 Huntsrsvillo, NC 28078 TEL: 704.875.9092 FAX: 704.875.9091 An Equal opportunity Employer ffi REPORT OF TABOBATORY ANATYSIS o Mr. Page ITIE ASSURANCT ()f OUAIITY John Burkart 24 CIient Reference: Laboratory Analysis QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 640812509 PURGEABLE HALOCARBONS Batch: 92 30029 Samples: 92 0247531, AND AROMATICS 92 0247540 LABORATORY CONTROL Sff,IPLE: ParameterfftTFfchl oroethane c i s- I ,3-Di chl oropropene 2-ChI oroethoxyethane Bromoform 1,1,2,l-Tetrachl oroethane Tetrachl oroethene l,lethyl-t-butyl ether Isopropyl ether Benzene , Tol uene QH;m;ffi:' Xyl enes I ,3-Di chI orobenzene I ,4-Di ch1 orobenzene I ,2-Di chI orobenzene ReferenceValue Recv-zr T5r20 7W20 50r20 80r20 7W20 85r 20 l10r20 8(H2A 9W2A 9W?0 85r20 85r Uni tsus/r ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L ug/L us/L MDLr.0 1.0 1.0 0.5 1.0 0.5 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 87X 85r 85S 80x 60 20 20 20 9800 Khcey Averus, Suhe 100 Huntsrcvilh, NC 28079 TEL: 704.876.90t2 FAX: 704.875.9091 An Egual opportunity EmploFr ffi REPOHT OF TABOBATOBY ANATYSIS oI'lr. Page THt ASSURAI'lCt 0t 0UALlTY John Burkart 25 Cl ient Reference: Laboratory Analysis PURGEABLE HALOCARBONS AND AROMATICS Batch: 92 30046 Samples: 92 0247558 I'|ETHOD BLANK: Parameter ehT6iffifhane Bromomethane Di chI orodi fl uoromethane Chloroethene (Vinyl chloride) Chloroethane Di chl oromethane Tri chI orofl uoromethane I, 1-Di chl oroethene I , 1-Di chl oroethane trans-l ,2-Di chI oroetheneIhloroformU , Z-Dr cni oroetrnane l, l, l-Tri chl oroethane Carbon tetrachloride Bromodichl ormethane I ,2-Di chl oropropane trans-l ,3-Di chl oropropene I , I ,2-Tri chl oroethene Di bromochl oromethane I , I ,2-Tri ch'l oroethane c i s- I ,3-Di chl oropropene 2-Chl oroethoxyethane Bromoform 1,1,2, Z-Tetrachl oroethane Tetrachl oroethene l,lethyl -t-butyl ether Isopropyl ether Benzene ToI uene ChI orobenzene Ethyl benzene Xvl eneso" QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 640812509 Uni tsns,f ug/L ug/L ug/L u9/L ug/L u9/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L }|DL13 1.0 1.0 1.0 1.0 1.0 Method Bl ankilD- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L ug/L 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 0.5 1.0 1.0 1.0 1.0 1.0 1.0 1.0 9800 lftcay Avsnro. Suhe 100 Huotenville, NC 28078 TEk 70&875.9092 FAX: 704.875.9091 An Equal Opporlunity Employor ffi REPORT OF LABORATORY ANATYSIS THE ASSURANCE OT OUATITY l,lr. John Burkart Page 26 Cl ient Reference: Laboratory Analysis PURGEABLE HALOCARBONS AND AROMATICS Batch: 92 30046 Samples: 92 0247558 }IETHOD BLANK: Parameter T-fdi-c5Torobenzene I ,4-Di chI orobenzene I ,2-Di chl orobenzene SPIKE AI{D SPIKE DUPLICATE: Parameter C[T6ffid[hane Bromomethane ^Oichl orodi fI uoromethane Intoroethene (Vinyl cnioride) ChI oroethane Dichloromethane Tri chl orofl uoromethane I , l-Di chl oroethene I , l-Di chl oroethane trans-l ,2-Di chI oroethene Chl oroform I , 2-Di chI oroethane l, l, l-Trichl oroethane Carbon tetrach'loride Bromodichl ormethane I ,z-Di ch'loropropane trans-l ,3-Di chl oropropene l, l, 2-Tri chl oroethene Di bromochl oromethane I , 1,2-Tri chl oroethane c i s- I ,3-Di chl oropropene Bromoforml, 1, 2, 2-Tetrachl oroethane Tetrachl oroethene fethvl -t-butY'l ether QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 540812509 Uni tsusrr us/L ug/L I'IDLrn 1.0I.0 I.IDL r.-0 1.0 1.0 1.0 1.0 1.0 ilethod Bl ankND- ND ND 920246705 SoikeN0-zt-ND ?OND 20ND 20ND 20ND ?O Unitsusr uglL ug/L ug/L uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 t.0 1.0 0.5 1.0 0.5 1.0 RPDB 1of, 6X 5f; 4% 0s 0% 4% M 0% 0% 0% OT 0% 4% 5% 0% 5% 0% 0% 0% 4% 8% 5% 55% ilD ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Spl ke Sptke Dupl Recv RecvTM T5gl00r 1l0r80r 85r95r 100fr t25% 130rllox 1Iffi t00s t00xlaw tasllt5% ll5rll5x 115rltSs 1l5rlt0% llof; 110% llox 110% ll0r 130% 125%ll0% 105% 1t0% ll0%ll0* l05r t25* 125f,ll0% ll0%95% 95% t20% l15% 130% tzffill0% 105% 60% 105% 9800 Xinccy AYanuc, Suits 100 Huntcrsville. l{C 28078 TEk 70t$875.8092 FAX: 704.875.9091 An Equal opportunity Employer N,$CG.REPOBT OF TABORATOBY ANATYSIS o-l,lr. John Burkart Page 27 CIient Reference: Laboratory Analysis PURGEABLE HALOCARBONS AND AROMATICS Batch: 92 30046 Samplesz 92 0247558 SPIKE AND SPIKE DUPLICATE: Parameter fsoproFyf ether Benzene Tol uene ChI orobenzene Ethyl benzene Xyl enes I ,3-Di chl orobenzene I ,4-Di chI orobenzene I ,2-Di chl orobenzeneo LABORATORY COTITROL SA}IPLE: Parameter CEToF6frEfhane Bromomethane Di ch'lorodi fl uoromethane Chloroethene (Vinyl chloride) Chl oroethane 0ichloromethane Tri chI orofl uoromethane I , l-Di chl oroethenel, l-Dichloroethane trans-l ,2-Di chl oroethene Chl oroform I ,2-Di chl oroethane l, 1, l-Trichl oroethane Carbon tetrachloride Bromodi chl ormethane I ,2-Di chI oropropane trans-1, 3-Di chI oropropene I , I ,2-Tri chl oroethene li bromochl oromethanert QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 540812509 Unitsusr ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDLr.0 1.0 1.0 1.0 I.0 1.0 920246705 SoikeND- zfND 20ND 20ND 20N0 20ND 50 Spike Spike Dupl Recv Recv RPDiffi nM -ffi ll0r l05r 5rltor t05r 5rllsr ltof, 4*l05r l00f, 5%l03r r00r 3r Uni ts u ug/L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L ug/L us/L ug/L ug/L ug/L UgIL ug/L ug/L us/L 1.0 1.0 1.0 MDLr.0I.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 l;0 0.5 20 20 20 ND ND ND It0r l05i 5rilor l05r 5%taffi ltofi 9s Recv-9r5ts 9W 8or 95x lt5% 100fr 90% ll0% 95% 9s% 100% 95X 95% 95r r05s 95% 100% 95r u0% Reference VaI uea- 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 9800 Ktroy Avenue, Suhe 100 Huntsrsv0h, ilC 28078 TEl.: 70'0.875.9092 FAX: 704.875.9091 An Equal 0pportunity Employer ffi REPORT OF TABOBATOBY ANATYSIS IHE ASSURAiICE ()T OUAI.ITY Mr. John Burkart Page 28 Client Reference: Laboratory Analysis PURGEABLE HALOCARBONS AND ARO}4ATICS Batch: 92 30046 Samples: 92 0247558 LABORATORY CO$TROL SA}IPLE : ParameterflFTrlchloroethane ci s- I ,3-Di chl oropropene 2-ChI oroethoxyethane Bromoforml, l, 2, 2-Tetrachl oroethane Tetrachl oroethene tlethyl -t-butyl ether Isopropyl ether Benzene Tol uene ell;#;ffit' XyI enes I ,3-Di chl orobenzene I ,4-Di chl orobenzene I ,2-Di chl orobenzene QUALITY CONTROL DATA August 24, 1994 PACE Project Number: 640812509 Uni tsuszr ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L I4DLrr 1.0 1.0 0.5 1.0 0.5 t.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 8sf, 8ofr 95% 95% l00r 90r 92,/, I00fr t0o% 95% ReferenceValue RecvTr -gffi ?0 85m20 gffi20 105%?0 105%20 100ff 20 20 20 20 ?0 20 60 20 20 20 9800 lfinmy Avsnuc, &ito t00 Huntsrsvilh, llC 28078 TE[: 70t[875.9002 FAX: 704.875.9091 An Equal opportunity Emphttr ffi BEPORT OF TABORATOBY ANAIYSE o I'lr. Page IHT ASSUf,AiICE ()T Ot]AI,ITY John Burkart 29 CIient Reference: Laboratory Analysis l'lDL ]{ethod Detection LimitND l{ot detected at or above the MDL.PC Possible Iaboratory contaminant.RPD Relative Percent Difference FOOTNOTES August 24,1994for pages 14 through 28 PACE Proiect Number: 640812509 9800 lftcey Avmuc. Suite 100 Huntanvifie, tt0 28078 TEL 70&878.9032 FAX: 704.875.9091 An Equal opportunity Employcr v s\- e{\-'>- \--:"\:, +t!hl.a IoFq !El-a3 ;oIL lrjoa UJcn !Etu UJE uJIIJU' i,(!oooE0)oo5ro CE oo(E4 o(, G& EoaEC'U)g(!o tt o E Eooq o'g!t o,.':(!g ,9"o o -o. (!o t- =tr4 dt!,oE 6q) lO@t\@ CC\I8Al Epl Ese-^ o .-/-tYtr OI6e ;l =E 6lfE€ICr< E-l (r)ecor{ ooo.,E U:tqr:t 5:lfi:lU € c a e , ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS 0ctober 10, 1994 Mr. John Burkart Coopei Environmenta'l , Inc. 2300 Sardis Road North, Suite QCharlotte, NC 28227 RE: PACE Project No. 64A926.506 Client Reference: Stork 94147 Dear Hr. Burkart: Enclosed is the report of laboratory analyses for samples received September 26, 1994. Footnotes are given at the end of the report. If you have any questions concerning this report, p'lease feel freeto contact us. Si ncerely, I /,*LLrna[4^,-\_ Kris H. Kommalan Project l.lanager Encl osures 980{l (incey Avenue, Suite 100 Huntersvilla, NC 28078 TEL: m&ir5-S92 FAX: 704-875-9091 An Equal 0pportunity Employer ffi REPORT OF LABORATORY ANALYSIS Cooper Environmental, Inc. 2300 Sardjs Road North, Suite QCharlotte, NC ?8227 Attn: Mr. John Burkart Client Reference: Stork 94147 PACE Sample Number: Date Col I ected: Date Received: Cl 'ient Sampl e ID: Parameter INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Chromi um Chromium, Hexavalent ORGANIC ANALYSIS INDIVIDUAL PARAMETERS Semivol. Tentative. Ident. Cpd. Or*nroBLE HAL,.ARB,NS AND AR'MATI.' ChI oromethane Bromomethane Dichl orodi fl uoromethane Chloroethene (Vinyl chloride) Chl oroethane Di ch'l oromethane Tri chl orofl uoromethane I , 1-Di chl oroethene l, l-Dichloroethane trans- I , 2-Di chl oroethene Chl oroform I , 2-Di chI oroethane l, l, l-Tri chl oroethane Carbon tetrachloride Bromodi chl ormethane I ,2-Dichl oropropane trans- I ,3-Di ch1 oropropene l, l, 2-Trichl oroethene Di bromochl oromethane l, l, Z-Trichl oroethane O.t s-1 ,3-Di chl oropropene 0ctober 10, 1994 PACE Project Number: 540925506 92 0?6454t 09126 /94 09126/e4 Mt,l-4 Units ng/L mg/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/ L ug/L ug/L uglL ug/L uglL ug/L uglL ug/L ug/L u9/L ug/L uglL MDL METHOD DATE ANALYZED 0.010 0.02 0.125 ND 100394 ?00.7 7195 6At/602 r0105/e4 0el26le4 rc la3le4 r0107194 t0l07le4 t0l07le4 r0lo7l94 t0107 /e4 10107194 r0l07le4 10107194 r0lo7 194t0/07le4 10107 194 10107194 l0l07le4 10/071e4 l0/07194 rcla7le[ t0107194 rc/47le4 rc107194 r0/07le4 t0/07194 2.4 4.0 2.t 0.8 1.4 5.0 0.5 0.5 0.6 0.8 1.0 1.0 0.8 0.5 0.5 0.5 0.8 0.9 1.0 1.0 0.7 ND ND ND ND ND ND ND ND ND ND 3.3 ND ND ND ND ND ND ND ND ND ND 98fi1 Kincay Avenue, Suite 100 Huntorsville, NC 28078 IEL:7lF8r5-90t2 FAX: 704-875-9091 An Equal 0pportunity Employer a REPORT OF LABORATORY ANALYSISo Mr Pa ENVIRONMENTAL . John Burkartge2 C'l i ent Reference: Stork PACE Sample Number: Date Col lected: Date Received:Client Sample ID: Parameter 94147 ORGANIC ANALYSIS PURGEABLE HALOCARBONS AND AROMATICS Bromoform 1, l, 2, 2-Tetrachl oroethane Tetrach'l oroetheneMethyl-t-butyl ether Benzene Tol uene Chl orobenzene Ethyl benzene Xyl enes e :i:Blills[B:xl:l: I ,2-0ichlorobenzene BASE/NEUTRALS AND ACIDS Date Extracted, Base/Neutrals and Acids N-Ni trosod i methyl ami ne bi s (2-Chl oroethyl ) ether Phenol 2-Chl orophenol I ,3-Di chI orobenzene I ,4-Di chl orobenzene I ,2-Di chI orobenzene bi s (2-Chl oroi sopropyl ) ether Hexachl oroethane N-Ni trosodi -n-propyl ami ne Ni trobenzene 3 , 5, 5-Tri methyl -Z-cycl ohexanone 2-Ni trophenol 2,4-0imethyl phenol bi s (2-Chl oroethoxy)methane 2 ,4-Di chl orophenol I , 2, 4-Tri chl orobenzene laohthal ene October 10, 1994 PACE Project Number: 640926506 92 026454t 091261e4 0s 126 /e4 Mt.I-4 Un'i ts ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Date ug/ L ug/L ug/ L ug/L u9/L ug/L ug/L us/L ug/L ug/L ug/L ug/L u9/ L us/L ug/L ug/L UgIL ug/L l'lDL ]{ETHOD DATE ANALYZED 601 /602 2.0 0.4 0.9 5.0 0.6 1.0 1.3 0.9 0.9l.l 1.0 1.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 ND ND ND ND ND ND ND ND ND ND ND ND r0l07le4 t0l07le4 tol07le4 t0l07ls4 r0/07 /e4 r0107 /94 r0107194 rc/071e4 10107194 t0/07194 r0107194 r0107194 09130/94 t0103194 t0 /031e4 10103194 t0103194 r0la3l94 rcl03leq lo/03/94 rc /a3le4 t0103194 lola3le| t0l03le4 r0103194 tol03le4 101031e4 t0l03le4 r0l03le4 t0103194 r0l03/94 625 093094 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9800 Kincey Avenus, Suite 100 Huntersville, NC 28078 fEL: r0{-8r!-9mA FAX: 704-875-9091 An Equal 0pporrunity E,Dployer / . John Burkartge3 Client Reference: Stork 94147 PACE Sample Number: Date Col I ected: Date Received: CIient Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS Hexachl orobutadi ene 4-Chl oro-3-methyl phenol Hexachl orocycl opentadi ene 2, 4,6-T rich 1 orophenol 2-Chl oronaphthal ene Acenaphthyl ene Dimethyl phthalate 2,6-Dinitrotoluene Acenaphthene e:[BllltrlliHl. 4-Ni trophenol Fl uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-Hethyl -4,6-di ni trophenol N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether HexachJ orobenzene Pentachl oropheno'l Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidi ne Pyrene Benzyl butyl phthalate 3 ,3-Di chl orobenzi d i ne BenzIa] anthracene Chrysene Ot, s (2-Ethyl hexyl )phthal ate ffi RrpoRr or LRsoRRronY nNRLYslso Mr Pa 0ctober 10, 1994 PACE Project Number: 640926506 92 0264541 0el?61e4 0e126/e4 Mt,J-4 Un'i ts ug/L ug/L us/L us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L U9/L ug/L ug/L ug/ L ug/L us/L ug/L ug/L us/L ug/L ug/L ug/L u9/L ug/L ug/L u9/L MDL I,IETHOD DATE ANALYZED 625 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 42 6.0 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 t7 8.0 5.0 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND r0 /03194r0l03le4 t0103194 101031e4 t0l03le4 La /$ ls4 r0l03le4 t0/031e4 10103194 t0l03le4 r0103194 t0/03/e4 t0/031e4 t0103/94 10103194 10103194 t0103194 r0103194 t0103194 t0 /03 /s4 r0 /031e4 t0103194 t0103/94 tol03/94 t0/03/e4 rc la3le4 t0103194 nl03le4 t0103194 L0l03le[ l0/03/e4 98{E Kincey Avanue, &ite 100 Huntsrwille. NC 28078 IEL ?0a-0?5.gts2 FAX: 704-875-9091 An Equal 0pportunity Employcr ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Mr. John BurkartPage 4 Client Reference: Stork 94147 PACE Sample Number: Date Col lected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS Di -n-octy1 phthal ate Benzo I b] fl uoranthene Benzo I k] fl uoranthene Benzo I a] pyrene Indeno [ 1, 2, 3, -cd] pyrene Di benzIa, h] anthracene Benzo[g,h,iJperylene 2-FI uorophenol, (Surrogate) Phenol-d5, (Surrogate) -Ni trobenzene-dS, (Surrogate)az-rtuorobi phenyi,' (Surr6gat6) 2,4,6-'fribromophenol, (Sumogate) Terphenyl -d14, (Surrogate) October 10, 1994 PACE Project Number: 640926506 92 0264541 0e /26/e40el26le4 Mt^l-4 Units ug/L ug/L ug/L ug/L us/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 5.0 MDL METHOD DATE ANALYZED 625 ND ND ND ND ND ND ND 39 26 49 48 80 51 ug/L % % % ollo % Nlo l0l03le4 r0l03le4 t0/03/e4 tal03le4 lol03le4 r0la3le4 t0/03194 10103194 rcl03/94 t0/03/e4 t0/03194 r0/031e4 r0/03/94 Sff Xincry Avenue, Suite 100 Huntersvillo. NC 28078 IEL: Tllf-8r$8192 FAX: 704-875-9091 An Equal 0pportunity Employer ffi REPORT OF LABORATORY ANALYSIS Mr. John BurkartPage 5 Cl 'ient Reference: Stork 94147 PACE Sample Number: Date Col lected: Date Received: Client Sample ID: Parameter INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Chromi um Chromium, Hexavalent ORGANIC ANALYSIS INDIV IDUAL PARA}.IETERS Sem'ivol . Tentati ve. Ident. Cpd. PURGEABLE HALOCARBONS AND AROMATICS Chl oromethaneI Bromomethane!Uoi chl orodi fl uoromethane Chloroethene (Vinyl chloride) ChI oroethane Di chl oromethane Tri chl orofl uoromethane I , l-Di chl oroethene I , l-Di chl oroethane trans-1 ,2-Di chI oroethene Chl oroform I ,2-Di chl oroethane 1, l, l-Trichl oroethane Carbon tetrachloride Bromodi chl ormethane I ,2-D'ichl oropropane trans- I ,3-Di chl oropropene I , I ,2-Tri chl oroethene Di bromochl oromethane I, I, Z-Trichl oroethane c i s- I ,3-Di chl oropropene Bromoforml, l, 2, 2-Tetrachl oroethane Tetrachl oroethene October 10, 1994 PACE Project Number: 640926506 9? 0264568 09 /?61s40s/?61e4 Mt,l-5 Uni ts MDL METHOD DATE ANALYZED mg/L mg/ L 0.010 0.02 0.052 ND 100394 200.7 7196 601 /602 tol05ls4 09/26/94 l0/03194 r0107194 t0l07le4 r0107le4 l0l07le4 t0/07 /94t0/o7le4 l0l07le4 l0/071e4 t0l07ls4 l0/071e4 l0/071e4 t0l07le4 l0l07le4 t0l07le$ rcla7le4 t0107 /e4 r0/07194 t0107194 t0l07le4 r0l07le4 r0l07le4 t0/071e4 r0l07le4 r0107194 ug/ L ug/L ug/L ug/L uglL ug/L ug/L ug/L u9/L ug/L u9/ L ug/L ug/L uglL u9/L us/L ug/L ug/L ug/L ug/L u9/L ug/L us/L uglL 2.4 4.0 2.1 0.8t.4 5.0 0.5 0.5 0.6 0.8 1.0 1.0 0.8 0.5 0.6 0.5 0.8 0.9 1.0 1.0 0.7 2.0 0.4 0.9 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.0 ND ND ND ND ND ND {18{E Kincey Avenue, Suite 100 Hunlsruville, NC 28078 IEL 70+E $S02 F/v\: 704-875-S!91 An Equal 0pportunity Employer REPORT OF LABORATORY ANALYSISENVIRONMENTALLABORATORIES llLl t rll t t Lnervllrrr vrr ! 'rrurEr v'v Mr. John BurkartPage 6 Client Reference: Stork 94147 PACE Sample Number: Date Col I ected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS PURGEABLE HALOCARBONS AND Methyl-t-butyl ether Benzene Tol uene Chl orobenzene Ethyl benzene Xyl enes I ,3-Di chl orobenzene I ,4-Di chl orobenzene I ,2-Di chI orobenzene October 10, 1994 PACE Project Number: 640926506 92 0254568 0e 126/e4 0e /261e4 Mtl-5 Units MDL METHOD OATE ANALYZED AROMATICS 601/602 625 r0107194 r0l07le4 r0l07le4 r0l07le4 t0107 /e4 101071e4 t0l07le[ l0l07le4 10107 /e4 0sl30le4 r0l03le4 l0l03le4 rc/$/e4 LOl03le4 wla3le4 t0l03le4 t0l03le4 t0/03/e4 to la3 /94 r0103 /94 t0103 /94 r0103/e4 t0l03le4 rcl03le4 rcl03le$ t0103194 rcl03le4 t0l03le4 t0103/e4 r0103/e4 ug/L ug/L ug/L ug/L ug/L uglL ug/L ugi L ug/L Acids Date ug/L ug/L ug/ L ug/L ug/L ug/L u9/ L ug/L ug/L u9/L uglL ug/L ug/L ug/L u9/L ug/L ug/L ug/ L ug/L us/L 093094 ND ND ND ND ND 5.0 0.6 1.0 1.3 0.9 0.9 l.l 1.0 1.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND I{D ND ND O 4-Chloro-3-methylphenol O ,orr/NEUTRALs AND ACIDs Date Extracted, Base/Neutrals and N-Ni trosodimethyl ami ne bi s (2-Chl oroethyl ) ether PhenoI 2-Chl orophenol I ,3-Di chl orobenzene I ,4-Di chl orobenzene 1,2-Dichl orobenzene bi s (2-Chl oroi sopropyl ) ether Hexachl oroethane N-Ni trosodi -n-propyl ami ne Ni trobenzene 3 , 5, 5-Tri methyl -2-cycl ohexanone 2-Ni trophenol 2,4-Dimethyl phenol bi s (2-Chl oroethoxy)methane 2,4-Di chl orophenol I ,2,4-Tri chl orobenzene Naphthal ene Hexachl orobutadiene 9il)0 Kincey Avenue, Suite 1 00 Huotersvills, NC 28078 lf,L: ?0&875-SS2 F/tX: 704-875-9091 An Equal opportunity Employor ffi REPoRT oF LABoRAToRY ANALYSISENVTRONMENTALLABORATORTES r rLr vr r r Mr. John BurkartPage 7 Client Reference: Stork 94147 PACE Sample Number: Date Collected: Date Received: Cl ient Samp'le ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS Hexachl orocycl opentadi ene 2, 4, 6-Tri chI orophenol 2-Ch1 oronaphthal ene Acenaphthyl ene Dimethyl phthalate 2,6-Di ni trotol uene Acenaphthene 2 ,4-0i ni trophenol 2 ,4-Di n i trotol uene 4-Ni trophenol Fl uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-ilethyl -4,6-di ni trophenol N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl oropheno'l Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidine Pyrene Benzyl butyl phthalate 3 ,3-Di chl orobenzi di ne Benz I aJ anthracene Chrysene bi s (2-Ethyl hexyl ) phtha'l ate Di -n-octyl phthal ate BenzoIb] fl uoranthene 0ctober 10, 1994 PACE Project Number: 540926506 92 0264568 0e l26le4 0e 126 /e4 Ml,l-5 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L u9/L ug/L ug/L ug/L ug/ L ug/L ug/ L u9/L ug/L uglL u9/L ug/L MDL METHOD DATE ANALYZED 625 5.0 5.0 5.0 5.0 5.0 5.0 5.0 42 6.0 5.0 5.0 5.0 5.0 ?4 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 t7 8.0 5.0 5.0 5.0 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND r0/03194 r0l03le4 r0l03le4 rclc8/e4 l0/03/e4 l0/03/e4 r0l03le4 t0103/e4 t0l03le4 l0/03/s4n la3ls4 10/03/e4 10103194 l0/03/e4 t0l03le4 r0103194 L0/a3ls4 10/03/e4 l0/03/e4 Lol03le4 l0/03/e4 r0103/e4 l0/03/e4 l0/03/e4 t0l03le4 t0l03le4 r0l03le4r0l03lel rcla3le4 10/03/e4 t0103194 9&Xl Kincey Avenus, Suite 100 Huntersville, NC 28078 IEL: r0l{t8-gG2 FAX: 704-875-S)91 An Equal 0pportunity Employer ffi RrpoRr or usonRroRYRllRl-Ysts Mr. John BurkartPage 8 Client Reference: Stork 94147 PACE Sample Number: Date Col I ected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS Benzo I k] fl uoranthene BenzoI a] pyrene Indeno[1,2,3,-cd] pyrene Di benz Ia, h] anthracene Benzo [9, h, i ] peryl ene 2-FI uorophenol , (Surrogate) Phenol-d5, (Surrogate) Ni trobenzene-dS, (Surogate) 2-Fluorobiphenyl, (Surrogate) 2,4,6-Tribromophenol, (Surrogate) T,erphenyl -d14, (Surrogate) October 10, 1994 PACE Project Number: 640926506 92 0264568 0s /26/e4 0e 126 /s4 Mtl-5 Units ug/ L ug/L vglL ug/L ug/ L % MDL METHOD DATE ANALYZED 625 5.0 5.0 5.0 5.0 5.0 ND ND ND ND ND 33 23 38 37 65 55 r0/03/94 t0103/s4ta/$/e4 t0l03le4 t0l03le4 r0103/94 n la3le4t0l03le4 l0/03/s4 r0l03le4 t0l03le4 % % ollo ollo ollo S00 Xincey Avanus, SuitB I 00 Huntcrsville, NC 280i8 TEl,: r0l{?t-S9 FAX: 7M-875-9091 An Equal 0pponunity Employcr REPORT OF LABORATORY ANALYSISENVIRONMENTALLABORATORIES llLr t Irl lrr Lnrrrrrr'rlrr.rr nrrnLrvrv Mr. John BurkartPage 9 Client Reference: Stork 94147 PACE Sample Number: Date Collected: Date Received: Cljent Sample ID: Parameter INORGANIC ANALYSIS INDIVTDUAL PARAMETERS Chromi um Chromium, Hexavalent ORGANIC ANALYSIS INDIVIDUAL PARAMETERS Semivol. Tentative. Ident. CPd. PURGEABLE HALOCARBONS AND AROMATICS ChI oromethane Bromomethane Di chl orodi fl uoromethane Chloroethene (Vinyl chloride) Chl oroethane Di chl oromethane Tri chl orofl uoromethane I , l-Di chl oroethene I , 1-Di chl oroethane trans- 1,?-Dichl oroethene Chl oroform I ,2-Di chI oroethane l, I , l-Tri chl oroethane Carbon tetrachloride Bromodi chl ormethane I , 2-Di chl oropropane trans- I ,3-Di chI oropropene I , I ,2-Tri chl oroethene Di bromochl oromethane I , 1,Z-Trichl oroethane ci s-l ,3-Di chl oropropene Bromoform |, l,2,2-Tetrachl oroethane Tetrachl oroethene October 10, 1994 PACE Project Number: 640925506 92 0264592 0e 126le4 09125/94 Mt.I-6 Units MDL METHOD DATE ANALYZED mg/L mg/L 0.010 0.02 2.4 4.0 2.1 0.8 t.4 5.0 0.5 0.5 0.6 0.8 1.0 1.0 0.8 0.5 0.5 0.5 0.8 0.9 1.0 1.0 0.7 2.4 0.4 0.9 100394 ND ND 200.7 7196 rol0sls4 0el?61e4 rc la3l94 rol07le4 t0107194 t0107194 r0l07le4 10/07 /e4 r0l07le4 r0107194 r0107le4r0l07ls[ r01CI7194 wlaT leqr0l07ls4 r0107194 t0 /07 /94l0l07ls4 t0l07le[ L0l07le4 t0l07le4 r0l07le4 t0l07le4rol07le[ t0107194 rc107le4 r0l07le4 60t1602 ug/L ug/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L ND ND ND ND NO ND ND 1.3 ND ND 7.5 ND ND ND ND ND ND ND ND ND ND ND ND 38 98{X} (incey Avsnus, Suits I 00 Hunterwille. NC 28078 TEl,: ,lll-8r5-90m FAX:704-875-$9.| An Equal Oppoilunity Employer REPORT OF LABORATORY ANALYSISENVIRONMENTALLABORATOBIES tlLl trlll lrr Ltrslr, ll^rrrrtr ^rrrrbrv.Y Mr. John Burkart Page 10 Cl'ient Reference: Stork 94147 PACE Sample Number: Date Col I ected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS PURGEABLE HALOCARBONS AND Methyl -t-buty] ether Benzene Tol uene Chl orobenzene Ethyl benzene Xyl enes I ,3-Di chl orobenzene I ,4-Di chl orobenzene I , 2-Di chI orobenzene 0ctober 10, 1994 PACE Project Number: 6409265A6 92 0254s92 09 /26 /94 09126194 Ml.l.5 Units MDL METHOD DATE ANALYZED AROI'IATICS 60t1602 ug/L u9/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L Acids Date ug/L ug/L ug/L uglL ug/L ug/L ug/L uglL ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 5.0 0.6 t.0 1.3 0.9 0.9 1.1 1.0 1.0 ND ND ND ND ND ND ND ND ND r0/071e4 r0/071e4 t0/071e4 r0l07le4 t0/07 /e4t0l07le4 tol07lefinl07lefi 10107194 aeF0le4t0lo3le4 r0l03le4 t0103/s4 r0l03le4 t0l03le4 l0/03/e4 t0103194 r0/031e4 t0l03le4 10103/e4 r0l03le4 rol03/94 r0103194 r0103/e4 r0103194 r0103194 t0103/e4 t0103/e4 10/03/e4 t0l03le4 625 5.0 6.0 5.0 5.0 5.0 5.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 093094 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND O 4-Chl oro-3-methyl phenol lrorrlNEuTRALs AND AcrDS Date Extracted, Base/Neutrals and N-Ni trosodi methyl ami ne bi s ( Z-Chl oroethy'l ) ether Phenol 2-Chl orophenol I ,3-Di chl orobenzene I ,4-Di chl orobenzene 1,2-Di chl orobenzene bi s (2-Chl oroi sopropyl ) ether Hexachl oroethane N-l{i trosodi -n-propyl ami ne Ni trobenzene 3, 5, 5-Tri methyl -2-cyc'l ohexanone 2-Ni trophenol 2,4-Dimethyl phenol bi s (2-Chl oroethoxy)methane 2,4-Di chl orophenol I ,2,4-Tri chl orobenzene l{aphthalene Hexachl orobutadi ene 9flIl Kincey Avenuo, Suite 100 Huntersville, NC 28078 IEL: r0l-8r5-W FAX: 704-875-9091 An Equrl 0pportunity Employer ffi REPORT OF LABORATORY ANALYSISo Mr. Pag October 10, 1994 PACE Project Number: 540925506 John Burkarte 11 Client Reference: Stork 94147 PACE Sample Number: Date Collected: Date Received:Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACrDS Hexachl orocycl opentadi ene 2 ,4,5-Tri chl orophenol 2-Chl oronaphtha'lene Acenaphthyl ene D'imethyl phthal ate 2,6-Dinitrotoluene Acenaphthene 2,4-Di ni trophenol 2,4-Dinitrotoluenel-nt troohenol -l uorenL 4-Chlorophenyl phenyl ether Diethyl phthalate 2-Methyl -4,6-di ni trophenol N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidi ne Pyrene Benzy'l butyl phthal ate 3, 3-Di chl orobenzi di ne BenzIaJ anthracene Chrysene bi s (2-Ethyl hexyl ) phthal ate Di-n-octy'lphthal ate Jenzotbl fl uoranthene 92 0264592 0e/26/e4 0e/26/e4 Mtl-6 Units uslL ug/L ug/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L 5.0 5.0 5.0 5.0 5.0 5.0 5.0 42 6.0 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 t7 8.0 5.0 5.0 5.0 5.0 MDL METHOO OATT ANALYZED 625 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND r0l03le4 r0/03194 t0/03/s4 r0103194 rc la3l94rol03/e4 rc /43 /e4 t0103194 t0l03le4 t0103194 t0103194 10103194 t0/03/e4 t0lo3l94 10/03194 t0l03le4r0l03lel t0103194 t0103194 t0103/94 r0l03le4 rcla3le4 r0103/e4 r0l03le4 nla3le4 10103194 lo/03/94 r0l03le4 t0l03le[ t0103194 r0103194 l$fil Kincey Avenuo, Suite 100 Huntersville, NC 28078 IEL:701-t 5-9@ FAX:7&{75-91}91 An Equal 0pportunity Employer ffi BEPORT OF LABORATORY ANALYSISo Mr Pa 0ctober 10, 1994 PACE Project Number: 640926506 . John Burkartge l? Client Reference: Stork 94147 PACE Sample Number: Date Col I ected: Oate Received:Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS Benzo I k] fl uoranthene Benzo I a] pyrene Indeno I l, 2,3, -cd] pyrene Di benz Ia, h] anthracene Benzo [9, h, i ] peryl ene 2-Fluorophenol, (Surrogate) Phenol-d5, (Surrogate) Nitrobenzene-d5, (Surrogate) _ ?-Fluorobiphenyl, (Surrogate) C;hf, ;l;i lllryit;ltl ;, l:!y'.n"" These data have been reviewed and are 1*4+ Charles M. Cabaniss Manager, Inorganic Chemistry 92 0264592 0e126/e4 0e126/e4 Mtl-5 Un'i ts ug/ L ug/L u9/L ug/L ug/Lulo % % % % % approved 5.0 5.0 5.0 5.0 5.0 for rel ease. ND ND ND ND ND ?6 t8 31 30 (1) 53 44 MDL METHOD DATE ANALYZED 625 t0 /03 /e4 r0/031e4 t0la3le4 t0l03le4 t0/031e4 t0/031e4 t0/031e4 t0/o3le[ t0l03/e4 t0l03le4 r0l03le4 ret S. Harding Organic'Chemistry 98fi) Kincay Avenue. Suite 1 00 Huntsrsville, NC 28078 IEL:70+875-Sf92 FAX: 704-875-9091 An Equal 0pportunity Employer / o Mr Pa ffi Rrpont or LRgonnroRY RruRl-Ysls October 10, 1994FOOTNOTESfor pages I through 12 PACE Proiect Number: 640926506 CIient Reference: Stork 94L47 MDL l.lethod Detect i on L i mi tND Not detected at or above the MDL.(l) Suryogate recovery is sl'ightly outside in-house QC I imits. . John Burkartge 13 98fi) Kincey Avenue, Suite 1 00 Huntersville, NC 28078 TEL: 7l!f-8r5-9092 FAX: 704-875-9091 An Equal 0pportunity Employer a ffi REPORTOF LABORATOEY4MLYSIS Mr. John Burkart QUALITY C0NTROL DATA October 10, 1994 Page 14 PACE Proiect Number: 540926506 Client Reference: Stork 94147 Chromium, Hexavalent Batch: 92 30765 Samples: 92 0264541, 92 0254558, 92 0264592 METHOD BLANK: l,lethodParameter Un'its MDL Bl ank enromium, Hexavalent mg/f- 0;02 ND-- 9&10 Kincey Avenue, Suite '100 Huntersville. NC 28078 fEL:r|,{-E 5-$m FAX: 704-875-9091 An Equal 0pportunity Employer a ffi RrPoRr or HsonRroRYRIlRlYsts Mr. John Burkart QUALITY C0NTR0L DATA Page l5 Client Reference: Stork 94147 ICP QUALITY CONTROL Batch: 92 30899 Samples: 92 0264541, 92 0264568, 92 0264592 METHOD BLANK: Parameter 0ctober 10, 1994 PACE Project Number: 540926506 Reference Val ue Recv 5.0 rcz%5.0 98%0.500 94%5.0 86%5.0 90% INDIVIDUAL PARAI,IETERS Cal ci um Magnes i um Molybdenum Potass i um Sodi um rcP QUALITY CoNTRoL Ni ckel Cadmi um Vanadi um Lead Bari um Copper Chromi um Beryl I i um Zi nc Cobal t Iron S'il ver I'langanese A'lumi num LABOMTORY CONTROL SAI'IPLE: Parameter INDIVIDUAL PARAMETERS Cal ci um I'lagnes i um Molybdenum Potass i um Sodi um Units nglL m9/L mg/L ms/L mg/L mg/L mg/L mg/L mg/L m9/L mg/L mg/L mg/L mg/L nglL mg/L mg/L m9/L mg/L MethodMDL Bl ank 0. 10 ND 0. t0 ND0.020 ND 0. l0 ND 0. l0 ND 0.010 0.010 0.010 0. 10 0. 010 0.010 0.010 0.010 0.010 0.010 0.010 0.005 0.010 0.010 0.10 0. l0 0.020 0. l0 0. 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND Units ng/L m9/L mg/L mg/L mg/L 9800 Kincey Avenue, Suits 100 Huntemville, NC 28078 TEL:70{-E75-SX[ FAX: i04-875-9091 An Equal 0pportunity Employer a ffi REPORT OF LABORATORY ANALYSIS Mr. John Burkart QUALITY C0NTR0L DATA Page 16 Client Reference: Stork 94147 ICP QUALITY CONTROL Batch: 92 30899 Samples: 92 0?6454L, 92 0264568, 92 026459? LABORATORY CONTROL SAMPLE: Parameter 0ctober 10, 1994 PACE Project Number: 640926506 Reference Val ue Recv 0.500 95%0.500 95%0.500 98%0.50 96%0.500 rc?%0.500 100% ICP QUALITY CONTROL Ni ckel Cadmi um Vanadi um Lead Bari um Copper Chromi um Beryl 1 i um Zi nc Cobal t I ron Si I ver f{anganese Al umi num Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.010 0.010 0.010 0.10 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.005 0. 010 0.010 0.500 0.500 0.500 0.500 0.500 0.050 0.500 0.500 97Y" 9ty 96% 97% 98% 90% 97% 101% 98$ Kincay Avenue, Suite 100 Hunterwille, NC 28078 fEL: ,0f.8r5-gll9 FAX: 704-875-9091 An Equal 0pponuniry Enployer ffi REPORT OF LABORATORY ANALYSIS Mr. John Burkart Page 17 Client Reference: Stork 94147 EASE/NEUTRALS AND ACIDS Batch: 92 30919 Samples: 92 0264541, 92 0264568, METHOD BLANK: Parameter INDIVIDUAL PARAMETERS Semivol. Tentative. Ident. Cpd. BASE/NEUTRALS AND ACIDS N-Ni trosodimethyl ami ne bi s ( 2-Chl oroethy'l ) ether Phenol 2-ChI orophenol I ,3-Di chl orobenzene I ,4-Di chl orobenzene I ,2-Di chl orobenzene bi s(2-Chloroi sopropyl )ether Hexachl oroethane N-Ni trosodi -n-propyl ami ne Ni trobenzene 3, 5, 5-Tri methyl -2-cycl ohexanone 2-Ni trophenol 2, 4-Di methyl phenol bi s (2-Ch1 oroethoxy)methane 2,4-Di ch'loropheno'l I ,2,4-Tri chl orobenzene Naphthal ene Hexachl orobutadi ene 4-ChI oro-3-methyl phenol Hexachl orocycl opentadi ene ?, 4,6-T richl orophenol 2-Chl oronaphthal ene Acenaphthyl ene Dimethyl phthalate ?,6-Dinitrotoluene Acenaphthene QUALITY CONTROL DATA 92 0264592 Units 0ctober 10, 1994 PACE Project Number: 640926506 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/ L ug/L u9/L u9/L ug/L ug/L us/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L Method B'lank r00394 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND l,lDL 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 42 )r,4-Di n i trophenol 98{X} Kincey Avenus, Suite 100 Huntersville, NC 28078 TEL: 7ll{-875-9lBz FAX: 704-875-909 1 An Equal 0pportunity Employ6r REPORT OF LABORATORY ANALYSISENVIRONMENTALLABORATORIES l lLr vl l r t, I l-nvtvl l^t vt r l,rrrrrEr v'v l'1r. John Burkart Page l8 Cl ient Reference: Stork 94147 BASE/NEUTRALS AND ACIDS Batch: 92 30919 Samples: 92 0254541, 92 0264568, METHOD BLANK: Parameter f,T:DTnTIrotol uene 4-Ni trophenol Fl uorene 4-Chl oropheny'l phenyl ether Di ethyl phtha'l ate 2-Methyl -4,6-di ni tropheno'l N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidine Pyrene Benzyl butyl phtha'late 3,3-Di chl orobenzi di ne Benz I a] anthracene Chrysene bi s (2-Ethyl hexyl ) phthal ate Di -n-octyl phthal ate BenzoIb]fl uoranthene Benzo I k] fl uoranthene BenzoIa] pyrene Indeno [ 1,2,3,-cd] pyrene Di benz Ia, h] anthracene Benzo [9, h, i ] peryl ene 2-F'l uorophenol , (Surrogate) Phenol-d5, (Sumogate) Nitrobenzene-d5, (Surrogate) QUALITY CONTROL DATA 92 0264592 0ctober 10, 1994 PACE Project Number: 540926506 Unitsus/t- ug/L ug/L u9/ L Ug/L ug/L ug/L ug/L ug/ L ug/L ug/L ug/L ug/L us/L u9/L uglL ug/L ug/L u9/L ug/L ug/L u9/L ug/L ug/ L ug/L u9/L ug/L ug/L ollo lo MDLm 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 17 8.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 l'lethod Bl ankND'- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 38 24 49 48 % ollo O z-Fluorobiphenyl, (Surrogate) 9800 Kincey Avenue, Suite 1 00 Huntersville. NC 28078 TEtr,04-8?5-qF2 FAX: 704-875-9091 An Equal 0pportunity Employer ffi REPORT OF LABORATORY ANALYSIS QUALITY CONTROL DATA October 10, 1994 PACE Project Number: 640926506 Mr. John Burkart Page 19 Client Reference: Stork 94147 BASE/NEUTRALS AND ACIDS Batch: 92 30919 Samples: 92 0264541, 92 0264568, METHOD BLANK: Parameter 4T;6-':Tribromophenol, (Surrogate )Terphenyl-d14, (Surrogate) LABORATORY CONTROL SAMPLE: Parameter trN-{Tffiaimethyl ami ne bi s (Z-Chl oroethyl ) ether Phenol 2-ChI orophenol I ,3-Di chl orobenzene 1 ,4-Di chl orobenzene I ,2-Di chl orobenzene bi s (2-ChI oroi sopropy'l )ether Hexachl oroethane N-Ni trosodi -n-propyl ami ne Ni trobenzene 3, 5, 5-Tri methyl -Z-cycl ohexanone 2-Ni trophenol 2 ,4-Di methyl phenol bi s ( 2-Chl oroethoxy) methane 2,[-Dichl oropheno'l I , 2, 4-Tri chI orobenzene Naphtha'lene Hexachl orobutadi ene 4-Chl oro-3-methyl phenol Hexachl orocycl opentadi ene ?, 4, 6-T r ichl oropheno'l 2-Ch1 oronaphthal ene Acenaphthyl ene Dimethyl phthalate 2,6-Di ni trotol uene 92 0264592 Un'its.%- ot Units uszt- ug/L ug/L ug/L ug/L ug/ L ug/L ug/L ug/L ug/L ug/ L ug/L ug/L ug/L ug/L uglL ug/L u9/L ug/L ug/L us/L u9/ L ug/ L ug/L us/L ug/L MDL lltDLm 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 Method Bl ankm- 57 Reference Val ue Recv-m- iw"50 54%50 30%50 50%50 58%50 587, 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 5896 46% 6A% 7?% 68% 66% 68% 70Y" 66% 66% 60% 62% 60% 72% 44% 70Y" 68y" 68% 74% 74* 9800 Kincey Avenu€, Suite 100 Huntersville, NC 28078 TEk ?0f.8r5-9092 FAX: 704-875-9091 An Equal 0pportunity Employer ffi REPORTOFLABORru QUALITY CONTROL DATAMr. John Burkart Page 20 Cl 'ient Reference: Stork 94147 BASE/NEUTRALS AND ACIDS Batch: 92 30919 Samples: 92 0254541, 92 0254568, LABORATORY CONTROL SAMPLE: Parameter AeffifFfi'[h'ene 2,|-Din i tropheno'l 2,[-Dinj trotol uene 4-Ni trophenol FI uorene 4-Chlorophenyl phenyl ether Di ethyl phtha'l ate 2-Methyl -4,6-di ni trophenol N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidi ne Pyrene Benzyl butyl phthal ate 3, 3-Di chl orobenzi di ne Benz I a] anthracene Chrysene bi s ( 2-Ethyl hexyl ) phthal ate Di -n-octy'l phthal ate BenzoIbJfl uoranthene Benzo I k] fl uoranthene BenzoIa]pyrene Indeno [ 1, 2, 3, -cd] pyrene D'i benz I a, h ] anthracene Benzo [9, h, i ] peryl ene 0ctober 10, 1994 PACE Project Number: 640925506 92 0264592 Units usTr- us/ L ug/L ug/L ug/L ug/L Ug/L ug/L ug/L uglL ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L u9/L ug/L ug/ L u9/L u9/L ug/L ug/L ug/L ug/ L ug/ L ug/L MDL 5:O 42 6.0 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 t7 8.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 Reference Val ue Recv--80-- -TM50 66%50 72%50 32%50 74%50 72% 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 74% 76% 95% 70% 70% 76% 74% 7296 72% 76% t46v, 70% 749/' 90% 74% 76% 74% 72% 70% 70% 70% 76r 78% 78% 9800 Kincey Avenuo, Suite '100 Huntersville, NC 28078 TEL 704-375-SlSz FAX: 704-875-909'l An Equal 0pportunity Employsr / ffi REPORT OF LABORATORYANAo Mr Pa . John Burkartge 21 Client Reference: Stork 94147 l4DL I'lethod Detection LimitND Not detected at or above the MDL. FOOTNOTES 0ctober 10, 1994 for pages 14 through 20 PACE Proiect Number: 640926506 98fi1 Kincey Avenue, Suite 100 Huntersville, NC 28078 TEL:7llr-8r5-m2 tAX: 704-875-9091 An Equal 0pportunity Employer ffi THE ASSUf,AI/CE OF OUAIIIY SEMIVOLATILES ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Laboratory: PACE, IncorPoraEed Laboratory Code: 640926-506 Sample fD: METIIoD BLANK Matrix: WATER Sample Description: N/A Sample wtlvol: 1 L File ID: 10039409 Level: LOW Date Received: N/A t Moisture: N/A Date Extracted: 09/30/94 Extract Vo1ume: 1.0 PIL Date Analyzed: Lo/03/94 Injection Volume: 2uL Dilution Factor: 1.0 pH: 7 Concentration Units z UG/L O Number of TrcE Found: o Compound Name RT Est. conc. oCAS Nulnber 1 2 3 4 5 6 7 I 9 10 11 L2 13 14 15 16 08lXl lCnoy Avann, fulr 100 llmorvilr, ]{C 2m78 IEl.: ,0+t76.g0gl FAX: 70'1"875.0091 An Equd 0pgortrmhy EmSygr ffi THT ASSUf,AiICE OT OUATITY Laboratory: PACE, IncorPorated Laboratory Code : 640926.506 Matrix: WATER Sample wt/vol : 1- L Level: I,OW t Moisture: N/A Extract Volume: 1.0 ML InJection Volume: 2uL pll:7 Number of TICs Found: 0 SEMIVOLATILES ORGANICS ANALYSIS DATA SHEET TEITflIATMLY IDENIIFfED COMPOUI{DS Sample ID: 26454.L Sample Description: MW-4 File fD: 100394L2 Date Received: 09/26/94 Date Extracted 09/30/94 Date Analyzed: lo/03/94 DiluEion Factor: 1.0 Concentration Units: UG/L Compound Name RT EEt. conc. oCAS Number 1 2 3 4 5 6 7 8 9 10 11 L2 13 L4 15 x5 9800 l0nry Avann Stjtr t00 itntlr$fl., ltC 28076Itk ,0+875.!012 FAX: 70&875-9ll9l An Equd 0wturily Enrlbyot ffiIHE ASSUNAlllCE OF OUAI-ITY Laboratory: PACE, IncorPoraEed Laboratory Code : 640926.506 Matrix: WAIER Sample wt,/voI : 1 L Leve1: IrOW t Moieture: N/A Extract Volume: L.0 ML Injection Volume: 2uL PH: 7 Number of TIcs For:nd: 0 SEMMLATILES ORGAI{ICS AIr{ALYSIS DATA SHEET TEMTATIVELY IDEIflTIFIED COMPOI'NDS Sample ID: 26456.8 Sample DescriPtion: MW-5 File ID z LA039413 Date Received: 09/26/94 DaEe Extracted: 09/30/94 Date Analyzed: L0/03/94 Dilution Factor: 1.0 Concentration Units: UG/L compound Name RT EEt. conc. aCAS Number 1 2 3 4 5 5 7 I 9 10 11 t2 13 14 15 16 0800 Krrry Aumr, Suitr 100 Hunrnrflr, tl0 28078 TEk 70{.07E.90t? FAX: 704.875.9091 An Equrl 0ppottunity E t$hylt ngg€, THE ASSURANCT I)F OUALITY SEMIVOLATILES ORGANICS A}IALYSIS DATA SHEET TEMTATIVEI,Y IDEI{ITIFIED COMPOUNDS Laboratory: PACE, Incorporated Laboratory Code: 640926.506 Sample ID: 26459.2 Matrix: WATER Sample Description: MW-6 Sample wt/vol: 1 L File ID: 100394L5 Level: LOW Date Received: 09/26/94 t Moisture: N/A Date Extracted: 09/30/94 ExEracE Volume: L.0 ML Date Analyzed: Lo/03/94 Injectlon VoLume: 2uL DiLution Factor: 1.0 pH: 7 Concentration units: OG/r" Number of TICs Found: 2 CA.S Number Compound Name RT Est. Conc. A L 1-27-L8-4 TetrachloroethYlene Unknoun 7.L2 5 43.05 16 96 2 3 4 5 5 7 8 9 10 11 L2 L3 L4 15 16 98ll{, [iEoI A,rilr, &ir, 100 ltmrmlc. ilG 28078 TEk 70+t7i.s0g2 FAX: 70'l-875.9091 An Equd 0ppnunity E@yu REPORT OF LABORATORY ANALYSISENVIRONMENTALLABORATORIES rlLl vlll vr hrrvvrrrrrYr l'|r. John Burkart Page 22 Cl 'ient Reference: Stork 94747 6U /6A2 - VoLATILE HALoCARBoNS/AR0MATICS Batch: 90 55404 Samples: 92 0264541, 92 0264568, 92 0264592 METHOD BLANK: Parameter ehT6'I6ffihane Bromomethane D'ichl orodi f'l uoromethane Vinyl Chloride ChI oroethane Methylene chloride Tri chl orofl uoromethane I , l-Di chl oroethyl ene I , l-Di chl oroethane trans- I , 2-Di ch1 oroethyl ene Chl oroform I , 2-Di chl oroethane l, l, 1-Tri chl oroethane Carbon Tetrachloride Bromodi chI oromethane I ,2-Di chl oropropane trans- l, 3-Di chl oro- l-propene I , I ,2-Tri chI oroethy'l ene Di bromochl oromethanel, l, 2-Trichl oroethane ci s- I ,3-0i chl oro- l-propene Bromoforn I ,l ,2,2-Tetrachl oroethane 1, 1,2,2-Tetrachl oroethyl ene I'lethyl Tert-Butyl Ether Benzene Tol uene Chl orobenzene Ethyl benzene Xyl enes QUALITY CONTROL DATA 0ctober 10, 1994 PACE Project Number: 6409265 O ,,3-Di chl orobenzene I ,4-Di chl orobenzene Units,s7I- ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/ L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L u9/L ug/L u9/L ug/L ug/L u9/L u9/L u9/ L PRLT3 4.0 2.1 0.8 1.4 5.0 0.5 0.5 0.6 0.8 1.0 1.0 0.8 0.5 0.5 0.5 0.8 0.9 1.0 1.0 0.7 2.0 0.4 0.9 5.0 0.6 1.0 1.3 0.9 0.9 l.l 1.0 Method Bl ankND- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11800 Kincey Avenue, Suite 100 Huntersville, NC 28078 TEL: rlH-E?5-SM FAX: 704-875-9091 An Equol 0pportunity Employer ENVIBONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Mr. John Burkart Page 23 Client Reference: Stork 94147 METHOD BLANK: Parameter Tlf-Dl c-h'Io ro b e n z e n e Total VOA SPIKE AND SPIKE DUPLICATE: Parameter eFT6'F6frEThane Bromomethane D'ichl orodi fl uoromethane Vinyl Chloride Chl oroethane lllethyl ene chl ori de Tri chl orofl uoromethane I , l-Di chl oroethyl ene I , l*Di chl oroethane trans- l , 2-Di chl oroethy] ene Chl oroform I , 2-Di chl oroethane l, 1, l-Trich'l oroethane Carbon Tetrachloride Bromodi chl oromethane I ,2-Di chl oropropane trans-l ,3-Di chl oro- l-propene I , I , 2-Tri chl oroethyl ene Di bromochl oromethanel, l, 2-Tri ch'l oroethane ci s- I ,3-Di chl oro- l-propene Bromoform l, l, 2, 2-Tetrachl oroethane I , I ,2,2-Tetrachl oroethyl ene O n.rny1 Tert-Buty1 Ether QUALITY CONTROL DATA 0ctober 10, 1994 PACE Project Number: 640926506 60t 1602 - V0LATILE HAL0CARBoNS/AR0MATICS Batch: 90 55404 Samples: 92 0264541, 92 0264568, 92 0264592 Units uezr- ug/L MethodPRL Bl ankII ND--0.6 ND Un'itswr ug/L ug/L u9/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L PRL T:4 4.0 ?.1 0.8 1.4 5.0 0.5 0.5 0.6 0.8 1.0 1.0 0.8 0.5 0.5 0.5 0.8 0.9 1.0 1.0 0.7 2.0 0.4 0.9 5.0 920264541Mt{-4 SpikeND 20ND 20ND 20ND 20ND 20ND 20 Spi keSpike Dupl Recv Recv RPDiM I00i6 wo85% 95% lL% 70% 80% 13%85% 95% lr% 90% 100% LL% 105% lts% 9% 100% 110% l0% 95% 105% 1A% 95% 100% 5%90% 95% 5%89% 89% 0%85% 90% 6% ND NO ND ND 3.3 ND ND ND ND ND ND ND ND ND ND ND ND ND 20 ?0 20 20 20 20 20 ?a 20 ?0 20 20 20 20 20 20 20 2A 20 90% 95% 85% 85% 80% 105% 85y" 85% 90% 80% 75% 100% 100% 100% 0% 95% 5% 100% 5% 90% 6% 90% 6% 80% 0% 95% l0% 90% 6%90% 6% 95% 5%85% 6% 8096 6% t00% 0% ND An Equal 0gportunity Employer9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 TEL:,lH-8?5-90U FAX: 704-875-9091 a ENVIRONMENTAL LABORATORIES REPOHT OF LABORATORY ANALYSIS Mr. John Burkart Page 24 Client Reference: Stork 94147 60t /602 - V0LATILE HALoCARBoNS/ARoMATTCS Batch: 90 55404 Samples: 92 0264541, 92 0264568, 92 0264592 SPIKE AND SPIKE DUPLICATE: QUALITY CONTROL DATA 0ctober 10, 1994 PACE Project Number: 640926506 Parameter mzene Tol uene Chl orobenzene Ethy'lbenzene Xyl enes I ,3-Di chI orobenzene I ,4-Di chl orobenzene I , 2-Di chl orobenzene LABORATORY CONTROL SAMPLE: Parameter efiTffiffihane Bromomethane Di chl orodi fl uoromethaneVinyl Chloride Chl oroethane Methylene chloride Tri chl orofl uoromethane I , l-Di chl oroethyl ene I , 1-Di chl oroethane trans- I , 2-0i ch I oroethyl ene Chl oroform I ,2-Di chl oroethane l, l, l-Trichl oroethane Carbon Tetrachloride Bromodichl oromethane I , 2-0i chl oropropane trans- I , 3-Di chl oro- I -propene I , I ,2-Tri chl oroethyl ene Di bromochl oromethane Reference Val ue Recv-T- m20 90%20 105%20 95r20 90%20 105% Un'i ts uszt- ug/ L u9/ L ug/L ug/ L ug/L ug/L ug/L SpikeT ?0 ?0 20 60 ?0 RPD -Wo 0% 0% 0% a% 6% PRL 0:6 1.0 1.3 0.9 0.9l.t 92026454t Mtd-4ND-- ND ND ND ND ND Spi ke Spi ke Dup'l Recv Recv TT5,T TTMll5% 115% 115% 115% 110% ll0%il8% ll8%85% 909/ 1.0 1.0 ND ND 20 20 90% 90% 0%90% 90% 0% Unitsus/r- ug/L ug/L uglL u9/L ug/L ug/L ug/L ug/L us/L u9/L ug/L u9/ L ug/L us/L ug/L ug/L ug/L ug/L PRLTA 4.02.t 0.8 1.4 5.0 0.5 0.5 0.6 0.8 1.0 1.0 0.8 0.5 0.6 0.5 0.8 0.9 1.0 20 105%20 95%?0 90%20 85%20 90%20 85% 90% 90% 85% 85% 75Y" 95% 85% 20 ?0 20 20 20 20 20 9800 Kincey Avenue, Suite 1 00 Hunt8rsville, NC 28078 TEL: 70f-875-90S2 FAX: 704-875-9091 An Equal 0pponunity Employer / ffi REPORT OF LABORATORY ANALYSIS C'l i ent Reference: Stork 94147 50t /602 - VoLATILE HALoCARB0NS/AR0MATTCS Batch: 90 55404 Samples: 92 0264541, 92 0254568, 92 0264592 Mr. John Burkart Page 25 LABORATORY CONTROL SAMPLE: Parameterf,TFTrTchl oroethane cj s-l ,3-Di chl oro-l-propene Bromoform 1,1,2, 2-Tetrachl oroethane 1,1,2, 2-Tetrachl oroethyl ene Methyl Tert-Butyl Ether Benzene Tol uene Chl orobenzene Ethyl benzene Xyl enes I ,3-Di chl orobenzene I ,4-Di chI orobenzene I ,2-Di chl orobenzene QUALITY CONTROL DATA 0ctober 10, 1994 PACE Project Number: 640926506 UnitsuW ug/ L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L PRLm 0.7 2.0 0.4 0.9 5.0 0.5 1.0 1.3 0.9 0.9 1.1 1.0 1.0 Reference Val ue Recv--20- -E5i"t, 20 90%20 80'ft20 75%20 95%20 100% 2A 110%?0 105%20 ll0%20 1059660 110%20 85% 85% 80% 20 20 9800 Kincey Avenue, Suit€ 100 Huntersville, NC 28078 TEL r0r-875.S0m FAX: 704-875-9091 An Equal 0pportunity Employer , ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Mr. John Burkart IOOTNOTES October I0, 1994 Page 26 for pages 22 through 25 PACE Proiect Number: 640926505 Client Reference: Stork 94L47 ND Not detected at or above the PRL.PRL PACE Reporting L'imitRPD Relative Percent Difference O An Equal 0pportunity Employer98110 Kincey Avenue, Suite 100 Huntersville, NC 28078 TEL ?0{-8r5-90S tAX: 704-875-9091 U'zloFol:)'Et-:Oi =EoIL uroa IJJU'nIIJ i IJJ ,E: UJ IJJOl 6r Ufi xazu<IE .t Jfs .Nt N. "I.t )*" #rcffi u3:;:,,$ilir." L?rr: 1,,:l:,..i:i\:t -5 k) ffii &r> kt k.,,Bi:':lrsr:,.. ffi.i $&!r.i. kil.- S::r :::$iil':''.. $';..1 &!ati - ffi,) li.riii\ ry{!'m.l*q-|t., fj Y.: t!,;: rritf,, BIl' $iiili'.! F,.f,: ili -.hki&:f,r.H:E' 6 ffi:' l&:,,, R f{'$Nl,. t:l':si:,.. H- ffi, Hi.,tld -m::ffil EIL : M wEe..ffi'X Ki *!bi -:ffilwH. tL M.tm: . &" E1"ffi&t-re.. ffi. U)IIJ =k tr TIJ U) UJE(L &ir- ffi:.!,. *t;_., ffi; m x:-S.it:'ffi::: ffiffiir.' ffi}<, 14" tr^ !lH}ffia,!:,4-&:t- filts H!iiir:ilr;* lTT&f.& ffi;ffimfni:lffiffi:.w'-xffi" ffi,&{il Mffi..K:K,. w ffii&! ffi',m; ffieM,'wi' ffi w mr, &hd.wtrr. mfrw"ffi,mf1. ffi$-H? m\ voA toNH 'ostH o3AH3SSUdNn ffi'. w"ffi& >'u3NlvLNoc lo'oN ocoEEooEc.9 !,E' .} &fi. $tr,l: iti!.;:s,.-[:tr{i(iii 9*1.:, h.p M&r,r$el &:rpbl: f:iii:i,: *?i,, ffi:. He, n $.:n :tll: I iOl::i,ll: nli:= l KPl $t':' *ilrr' :ryr trk I: .+ i;\,li:lrr:}*IIIY::r,,,,,,1)*vl lrr &'i:s,tr&ffi B{' | ---l-l-lolcLIElctl@lo-. 16.. t6 I I I I .1 , I - I--- IFIz lotr lf ..(L 16lcdr 16 :; -rl i<! rl :,:.,r*') f: --:t i,'. fri,, t; diilir' t::it: t*. ffi:l4S!'-k' &-i,:. K:,:kr.-ti !*;l $i Si'T*: t *.$lij {:' s'.K;,sMEsffitl,m.'s-.wt(Ef ffi$;lm:'II':'..K":B HMlf sr,, 8i&:, ffii: $:i'*i,,., . $:r l:. 6 t6o- lo-E IE(E lru@l@ ' t:.:. ,. i ,- l F.l.(\l r:(9 l\l i-lI) 1@ r\@ ,lH "l a, (6oo oT'o q(,(Dtr JI f, E @ B--rrlol6lo-l oo6c(U ooo o- o)o6G .l ,{l{JCII al =lclo)l:lololol(6lLl o IEooIIJE o-98'A =_ BE bs =>fEo< o,\-@€ corl ) r.; c;z oE(uz oo'0 IL o,otro o)orco =iE :lF cjI € in .j ) oco o- a ffi REPOHT OF LABORATORY ANALYSIS 0ctober 18, 1994 l*lr. John Burkart Cooper Environmental, Inc. 2300 Sardis Road North, Sujte QCharlotte, NC 28?27 RE: PACE Project No. 641004.505 Client Reference: 94147-Stork Screen Dear Mr. Burkart: Enclosed 'is the report of laboratory analyses for samples recejved 0ctober 04, 1994. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel freeto contact us. Sincerely, Ur* L/,*-1--,+f*"-- Kris H. Kommalan ProJect ilanager EncJ osures 9800 Kincey Avenue, Suits 100 HuntersvillB. NC 28078Ifk r0t-8rs-90s2 FAX: 704-875-9091 An Equal Op0ortunity Employcr ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS o Cooper Env'ironmental , Inc. 2300 Sardis Road North, Sujte QCharlotte, NC 28227 Attn: Mr. John Burkart Cl ient Reference: 94147-Stork Screen PACE Sample Number: Date Col'lected: Date Received: Client Sample ID: Parameter INORGANIC ANALYSIS INDIVIOUAL PARAMETERS Chromi um Chromium, Hexavalent ORGANIC ANALYSIS IND IV IDUAL PARAT,IETERS Semivol. Tentative. Ident. Cpd. October 18, 1994 PACE Project Number: 641004505 92 0273001 r0104/e4 10 /04194 VE-1 Uni ts mg/L mg/L ug/L ug/L ug/ L ug/L ug/L ug/L u9/L ug/L ug/L ug/ L ug/L ug/L ug/L u9/ L u9/L us/L ug/L ug/L us/L ug/L us/L 0.010 0.02 0.042 0.03 ?00.7 7196 601 1602 l0 /18le4 t0104194 MDL METHOD DATE ANALYZED Orr*nrABLE HAL'.ARB.N' AND AR,MATIC' Chl oromethane Bromomethane Di ch'lorodi fl uoromethane Chloroethene (Vinyl chloride) Chl oroethane Di chI oromethane Tri chl orofl uoromethane I , l-Di chl oroethene I , 1-Di chl oroethane trans- 1, ?-Dich'l oroethene Chl oroform 1,2-Di chl oroethane 1, l, l-Tri chl oroethane Carbon tetrachloride Bromodichl ormethane I , 2-Di chl oropropane trans- I ,3-Di chl oropropene 1 , 1 ,2-Tri chl oroethene Di bromochl oromethane I , I ,2-Tri chl oroethane ci s- I ,3-Di chl oropropene 1.0t.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 ND 19 ND ND 4.3 ND ND ND ND ND ND ND 101394 r0l13le4 t0/t2/94 t0l12l94 to /t?le410lt2le4 t0l12l94 t0ltzle4 t0ltzle4 t0/12/94 t0lt2l94 r0/12le4r0llzle4 ralt?le4 l0/t2194t0lt?le4 r0/12le4t0lt2l94t0ltzle4 r0l12le4 t0/12/94 r0lrzle4 r0lt2l94 75 ND ND ND ND ND ND ND ND 98fr1 KinceyAvenue, Suite 100 Huntorsvillo, NC 28078 IEL: ?0&875-S92 FAX: 704-875-$91 An Equal 0pportunity Employer a ENVI RON M ENTAL LABO RATO R I ES REPORT OF LABORATOHY ANALYSIS Mr. John BurkartPage 2 Client Reference: 94147-Stork Screen PACE Sample Number: Date Collected: Date Received:CIient Sample ID: Parameter ORGANIC ANALYSIS PURGEABLE HALOCARBONS AND AROMATICS 2-Chl oroethoxyethane Bromoform 1, 1, 2, 2-Tetrachl oroethane Tetrachl oroethene I'lethyl -t-butyl ether Benzene Tol uene Chl orobenzene Ethy'lbenzene Xyl enes I ,3-Di chl orobenzene I ,4-Di chI orobenzene I ,2-Di chl orobenzene BASE/NEUTRALS AND ACIDS Date Extracted, Base/Neutrals and N-Ni trosodimethyl ami ne bi s (Z-ChI oroethyl ) ether Phenol 2-Chl orophenol I ,3-Di chl orobenzene I , 4-Di chl orobenzene I , 2-Di chl orobenzene bi s (2-Chl oroi sopropyl ) ether Hexachl oroethane N-Ni trosodi -n-propyl ami ne Ni trobenzene 3, 5, 5-Trimethyl -2-cyc'l ohexanone 2-Ni trophenol 2,4-Dimethyl phenol bi s (2-Ch1 oroethoxy)methane 0ctober 18, 1994 PACE Project Number: 641004505 92 027300t r0/041e4 ral04/e4 vE- t Units MDL ]',IETHOD DATE ANALYZED ug/L ug/L ug/ L ug/ L us/ L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Acids Date ug/L ug/L ug/L us/ L us/L ug/L ug/ L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 1.0 0.5 I.0 0.5 I.0 1.0 1.0 1.0 1.0 1.0 1.0 t.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 ND ND ND 1.4 ND ND ND ND ND ND ND ND ND 101094 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 601 /602 625 t0lrz le4t0/t?/e4 tol12le4 r0lt2l94 t0l12l94 t0/12le4 r0l12l94 10/12/e4 r0 /t2/94r0l12l94 t0l12le4 rc/12/94 ro lt?194 t0ltole4 r0 /13 /e4 t0 /t3 /94r0l13le4 r0 /t3194t0lt3 le4 t0 /t3le4t0lt3le4 10113194 r0l13le4 r0l13le4 r0lt3l94 t0l13le{ l0l13l94 r0lt3le4t0lt3le4 t0/13le42.4-Di chl orooheno'lo 9800 Kincey Avenus, Suite 100 Huntersville, NC 28078 TEL:70a{r5-90S2 FAX: 704-875-9091 An Equal 0ppoftunity Employer ENVI RON M ENTAL LABO RATOR I ES REPORT OF LABORATORY ANALYSIS Mr. John BurkartPage 3 Client Reference: 94147-Stork Screen PACE Sample Number: Date Collected: Date Received:Client Sample ID: Parameter ORGANIC ANALYSIS October 18,1994 PACE Project Number: 641004505 92 0273001 t0 /04 /e4 10 /041s4 vE- I Units ug/L ug/ L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL ug/L ug/L uglL ug/L uglL ug/L u9/L ug/L ug/ L ug/ L ug/L ug/L ug/L ug/L ug/L u9/L uglL u9/L ug/L ug/L MDL METHOD DATE ANALYZED BASE/NEUTRALS AND ACIDS I ,2,4-Tri chl orobenzene Naphthal ene Hexachl orobutadiene 4-Chl oro-3-methyl phenoi Hexachl orocycl opentad i ene 2, 4, 6-Tri chl orophenol 2-Ch1 oronaphthal ene Acenaphthyl ene Dimethyl phthalate 2,6-Di ni trotol uene Acenaphthene 2,4-Dini tropheno'l 2,4-Dinitrotoluene 4-Ni trophenol Fl uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-Methyl -4,6-di ni trophenol N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidi ne Pyrene Benzyl butyl phthalate 3,3-0i chl orobenzidi ne 625 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 4? 6.0 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 l7 8.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND r0 /t3 /e4 r0 / t3 ls4r0lt3le4 t0l13le4 t0 /13 /e4r0l13le4 t0l13 /e4 10113/94 r0l13l94 r0l13l94 t0/13le4 t0l13 /94 t0l13le4t0lt3le4t0lt3/e4 t0lt3l94 r0 /13194 r0l13 /94 r0l13le4 r0l13le4 t0l13ls4 r0 I 13 /e4r0lt3 le4t0lt3le4 t0lt3le4 10l13le4 tol13le0 t0/13/94 t0l13l94 t0l13le4 10111194 f Benzltlanthracene 9800 Kincey Avanuo, Suite 1 00 Huntarsville, NC 28078 TEL: Tlll-875-90f, FAX: 704-875-9091 An Equal 0pportunity Employer / ffi REPORTOF LABORAIOEYTNALYflS Mr. John BurkartPage 4 Client Reference: 94147-Stork Screen PACE Sample Number: Date Col I ected: Date Received: Cljent Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS Chrysene bi s (Z-Ethyl hexyl )phthal ate Di -n-octyl phthal ate Benzo I b] fl uoranthene Benzo I k] fl uoranthene BenzoI a] pyrene Indeno [ 1, 2, 3, -cd] pyrene Di benz Ia, h] anthracene Benzo[9,h, i ]perylene October 18,1994 PACE Project Number: 641004505 92 0273001 t0l04le4 t0l04l94 vE- l Un'i ts MDL IIIETHOO DATE ANALYZED 625 ug/L uglL ug/L ug/L ug/L ug/L ug/ L ug/L ug/L % % % 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 ND ND ND ND ND ND ND ND ND 37 23 55 60 89 58 t0 /13 /94 t0l13 /94t0lt3le4 t0l13le4 L0l13le4 t0 / 13 /e4 t0l13/e4 101131e4 t0l13/e4t0lt3/e4 t0l13 /s4 r0 /t3194 r0l13le4 t0 /13194ro/t3194 e 3; 5lX?:[Bl'?3];,[ililin "' ) Nitrobenzene-d5, (Surrogate) 2-Fluorobiphenyl, (Surrogate) 2,4,6-Trlbromophenol, (Surrogate) Terphenyl -d14, (Sumogate) These data have been reviewed and are Yo % % Charl es l,l. Cabani ss lilanager, Inorgan'ic Chemi stry A(AL/ Itlargaret S. Harding{ Manager, 0rganic Chemistry approved for release. 9000 Kincey Avenue, Suite 1 00 Huntersville, NC 2m78 IEL:70e8r5-qE2 FM: 704-875-9091 An Equal 0pportunity Emgloyer a ffi REpSRT 0F LABSRATSRY ANALYSISENVIRONMENTALLABORATORIES T ILI I'I I I VI L' TYVT T' TT Y' 0ctober 18, 1994Mr. John BurkartPage 5 Client Reference: 94147-Stork Screen MDL I'lethod Detection LimitND Not detected at or above the l'lDL. FOOTNOTESfor pages I through 4 PACE Proiect Number: 641004505 Sl0 Kincey Avenue. Suite 100 Huntorwille, NC 28078 ItL: ?ll&8 5-1192 FAX: 704-875-9091 An Equal 0pponunity Employer a 'rr. John Burkart QUPage 6 Client Reference: 94147-Stork Screen Chromi um ffi REpSRT 0F LABSRATSRY ANALYSISENVIRONMENTAL LABORATOFIES T ILI T.,I T I QUALITY C0NTR0L DATA 0ctober 18, 1994 PACE Project Number: 64i004505 Batch: 92 31236 Samples: 92 0273001 METHOD BLANK: Parameter eEromi um LABORATORY CONTROL SAMPLE: Parameter eEromi um I'lethodUn'its HDL Bl ankm07t- 0.!-10 ND-- Reference Un'i ts MDL Val ue Recvms7t- 0l0to --T:mT- I00% 9800 Kincey Avenue, Suite I00 HuntercYills. NC 28078 TEL 'O{.C'5.WFAX:7M-875-9091 An Equal Opportunity Employer / Mr. John BurkartPage 7 C'l ient Reference: 94147-Stork Screen Chromium, Hexavalent Batch t 92 30924 Samples: 92 0273001 METHOD BLANK AND SAMPLE DUPLICATE: Parameter eFr-om]um, Hexavalent QUALITY C0NTR0L DATA October I8, 1994 PACE Project Number: 641004505 Dupl icate Method 920?73001 ofUnits MDL Blank VE-l 92 0273001 RPDmsZt- C3? NIf- 0-3T- il.O5- -W, ffi REPORT OF LABORATOBY ANALYSIS LABORATORY CONTROL SAMPLE: ReferenceParameter Uni ts MDL Val ue Recv ehrordium; Hexavalent msTI- 0T2 --T;I'd- mm 9800 KinccyAvenue, Suite 100 Hunterwille, NC 28078 TEL ro&8r$Ctg FAX: 704-875-9091 An Equal 0pportun,ty Employ.r , ffi HEPORT OF LABORATORY ANALYSIS Mr. John Burkart QUALITY C0NTROL DATAPage 8 Client Reference: 94147-Stork Screen October 18, 1994 PACE Project Number: 641004505 BASE/NEUTRALS AND ACIDS Batch: 92 31184 Samples: 92 0273001 METHOD BLANK: Parameter INDIVIDUAL PARAMETERS Semivol. Tentative. Ident. Cpd. BASE/NEUTRALS AND ACIDS N-N i trosodi methyl ami ne bi s (2-Chl oroethyl )ether Phenol 2-Chlorophenol I ,3-Di chl orobenzene I ,4-Di chl orobenzene a, , 2-Di chl orobenzene bi s (Z-ChI oroi sopropyl ) ether Hexachl oroethane N-Ni trosodi -n-propyl ami ne Ni trobenzene 3 , 5, 5-Tri methyl -2-cycl ohexanone 2-Ni trophenol 2,4-0imethyl phenol bi s (Z-Chl oroethoxy) methane 2,4-Dichl orophenol I , 2,4-Tri chl orobenzene Naphthal ene Hexachl orobutadi ene 4-Ch'l oro-3-methyl phenol Hexachl orocycl opentad i ene 2, 4, 6-Tri chI orophenol 2-Chl oronaphthal ene Acenaphthyl ene Dimethyl phthalate 2,6-Dinitrotoluene Acenaphthene - 2 .4-Di ni troohenolo Units ug/L ug/L ug/L uglL ug/L u9/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L us/L ug/ L ug/L us/L us/L ug/L ug/L ug/L u9/ L ug/L ug/L ug/L ug/L ug/L ug/L MDL 5.0 6.0 5.0 5.0 5.0 5.0 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 42 ]'{ethod BI ank 101394 ND ND ND ND ND ND ND tlD ND ND ND ND ND ND ND ND ND NO ND ND ND ND ND ND ND ND ND ND 98$ Kincey Avenue, Suits 100 Huntersaille. NC 28078 IEL: rlL{r$Sn F/D(: 704-875-9091 An Equal 0pportunity Emplopr REPORT OF LABORATORY ANALYSISENVIRONMENTALLABORATORIES r lLt lrr r ! vr Lnvvr It rr Yr I I I rru rLr Y'v Mr. John Burkart QUALITY C0NTROL DATA Page 9 Client Reference: 94147-Stork Screen 0ctober 18, 1994 PACE Project Number: 641004505 BASE/NEUTRALS AND ACIDS Batch: 92 31184 Samples: 92 0273001 METHOD BLANK: Parameter eEmnTlrotol uene 4-Ni trophenol Fl uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-Methyl -4,6-di ni trophenol N-Ni trosodi phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzidine Pyrene Benzyl butyl phthal ate 3, 3-Di chl orobenzi di ne Benz I a] anthracene Chrysene bi s (Z-Ethyl hexyl ) phthal ate Di -n-octyl phthal ate Benzo Ib] fl uoranthene BenzoIk] fl uoranthene BenzoIa]pyrene Indeno I l ,2,3, -cd] pyrene 0i benzIa, h] anthracene Benzo[g,h,i]perylene 2-Fl uorophenol , (Surrogate) Phenol-d5, (Surrogate) Ni trobenzene-dS, (Surrogate) 2-Fl uorobiphenyl, (Surrogate) Unitsus/t- ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/ L u9/ L ug/L ug/L u9/L ug/L To % MDL6T 5.0 5.0 5.0 5.0 24 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 l7 8.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 Method BI ankND- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 46 28 6l 64 % % !18fi) Kincey Avenus, Suite 100 HuntErwille, NC 28078 ItL: r0e875-909? FAX: 704-875-9091 An Equd 0pportun8 Eotployer REPORT OF LABORATORY ANALYSISENVIBONMENTALLABORATORIES rrLr vlrr vr hrrvYrrrrrvr Mr. John Burkart Page l0 QUALITY CONTROL DATA UnitsT-lo % MDL Units us/t- us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L 5.0 6.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 0ctober 18, 1994 PACE Project Number: 641004505 Client Reference: 94147-Stork Screen BASE/NEUTRALS AND ACIDS Batch: 92 31184 Samples: 92 0273001 METHOD BLANK: Parameter Z;[,6trTbromophenol, ( Surrogate ) Terphenyl -d14, (Surrogate) LABORATORY CONTROL SAMPLE: Parameteril:filTffidimethyl ami ne bi s (2-Ch1 oroethyl ) ether Phenol 2-Chl orophenol I ,3-Di chl orobenzene I ,4-Di chl orobenzene I ,2-Di chl orobenzene bi s (2-ChI oroi sopropyl ) ether Hexachl oroethane N-Ni trosodi -n-propyl ami ne Ni trobenzene 3 , 5, 5-Trimethyl -2-cycl ohexanone 2-Ni trophenol 2, 4-Dimethyl phenol bi s ( 2-Cht oroethoxy ) methane 2,4-Di chl orophenol I , 2,4-Tri chl orobenzene Naphthal ene Hexachl orobutadi ene 4-Chl oro-3-methyl phenol Hexachl orocycl opentad i ene 2, 4, 6-Tri chl orophenol 2-Chl oronaphthal ene Acenaphthyl ene Dimethyl phthalate 2,6-Di ni trotol uene Method Bl ankTT- 78 I{DL 5.3 6.0 5.0 5.0 5.0 5.0 Reference Val ue Recv-50- nTx50 65%s0 32%s0 62%s0 58%50 58% uglL ug/L 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 58% 48% 66% 80% 72% l4% 72% 66% 74% 7?% 68% 64r 623 747 50% 78r, 78#, 74% 86'6 88% 98fi1 Kincey Avenua, Suite 100 Huntsrsville, NC 28078 TEL: 10&O5-91192 F/tX: 7M-875-9091 An Equrl 0pporilnity EmPloyor REPORT OF LABORATORY ANALYSISENVIRONMENTALLABORATORIES I lLl llrl I I lrl Lnlrt a lnl tlrl I I nrrnLr vrle QUALITY CONTROL DATAMr. John Burkart Page 11 Client Reference: 94147-Stork Screen BASE/NEUTRALS AND ACIDS Batch: 92 31184 Samples: 92 0273001 LABORATORY CONTROL SAMPLE: Parameter IceiEFh-ffiene 2,4-Di n i trophenol 2,4-Di ni trotol uene 4-Ni trophenol Fl uorene 4-Chlorophenyl phenyl ether Diethyl phthalate 2-Methyl -4,6-di ni trophenol N-Ni trosod i phenyl ami ne 4-Bromophenyl phenyl ether Hexachl orobenzene Pentachl orophenol Phenanthrene Anthracene Di-n-butyl phthalate Fl uoranthene Benzi di ne Pyrene Benzyl butyl phthalate 3,3-Di chl orobenzidi ne Benz Ia]anthracene Chrysene bi s(2-Ethyl hexyl )phtha'late Di -n-octyl phthal ate BenzoIb] fl uoranthene Benzo I k] fl uoranthene BenzoIa]pyrene Indeno[ 1,2,3,-cdJ pyrene Di benzIa, h] anthracene Benzo[9, h, i ] peryl ene 0ctober 18, 1994 PACE Project Number: 641004505 Unitsusrr ug/L ug/L ug/L uglL ug/ L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uglL u9/L ug/L ug/L uglL ug/L ug/L ug/ L ug/L uglL ug/L ug/L MDLm 42 6.0 5.0 5.0 5.0 5.0 24 5.'0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 50 5.0 5.0 t7 8.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 Reference Val ue Recv-50-- -T{%50 t5%50 84%50 36%50 84%50 86% 50 86%50 64%50 94%50 88%50 84r,s0 lI4% 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 86% 84% 88% 86j6 6% 86% 92% 88% 82% 86% 94% rc4?6 86% 88% 80% 78% 7ffi 82% S00 Kincey Avenue, Suite 100 Huntersville. NC 28078 TEL: rll$15-962 FM: 704-875-$91 An Equal 0pportunity Employer AL LABORA ]'1r. John Burkart Page 12 Client Reference: 94147-Stork Screen PURGEABLE HALOCARBONS AND AROMATICS Batch: 92 31161 Samples: 92 0273001 METHOD BLANK: Parameter Cfi'TdF6fr6'[hane Bromomethane Di chl orodi fl uoromethane Chloroethene (Viny'l chloride) Chl oroethane 0i chl oromethane Tr i ch I orofl uorometh ane I , l-Di chl oroethene l, l-Dichloroethane trans- 1 , 2-Di chl oroethene Chl oroform I , 2-Dichl oroethane l, l, l-Trichl oroethane Carbon tetrachloride Bromodi chl ormethane I , 2-Di chI oropropane trans- I , 3-0i chI oropropene I , 1 ,2-Tri chl oroethene 0i bronochl oromethane I , 1,2-Tri chl oroethane ci s- I ,3-Di chl oropropene 2-Chl oroethoxyethane Bromoform 1,1,2, 2-Tetrachl oroethane Tetrachl oroethenel,lethyl-t-butyl ether Benzene Tol uene Chl orobenzene EthyI benzene Xyl enes I ,3-Di chI orobenzene QUALITY CONTROL DATA October 18, 1994 PACE Project Number: 541004505 Uni ts us/L- u9/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L ug/L ug/L MDL13 1.0 1.0 1.0 1.0 1.0 Method Bl ankND-- ND ND ND NDt.2 PC ND ND ND ND ND ND ND ilD ND ND ND ND ND ND ND ND ND ND NO ND ND ND ND f,l0 ND ND ug/L ug/L 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 0.5 1.0 1.0 1.0 1.0 1.0 1.0 1.0 SlXl Krcey Avenue, Suite 100 Huntersvills. NC 28078 TEL:r0{-O$W FAX: 7&-875-9091 An Equal 0pportunity Employer REPORT OF LABORATORY ANALYSISENVIRONMENTALLABORATORIES tlLt !L'tlr rvr L^vvt rrrrv.rr rr.!rt-.v.v Mr. John Burkart Page 13 Client Reference: 94147-Stork Screen PURGEABLE HALOCARBONS AND AROI,IATICS Batch: 92 31161 Samples: 92 0273001 }IETHOD BLANK: ParameterffTI cETorobenzene I , 2-Di chl orobenzene LABORATORY CONTROL SAI,IPLE : Parameter CET6Fffi[hane Bromomethane 0i chl orodi fl uoromethane Chloroethene (Vinyl chloride) ChI oroethane 0i chl oromethane Tri ch1 orofl uoromethane I , l-Di chl oroethene I , 1-Di chl oroethane trans- I , 2-Di chl oroethene Chl oroform I ,2-Di chl oroethane l, l, I-Trichl oroethane Carbon tetrachloride Bromodichl ormethane I , 2-Di chl oropropane trans- l, 3-Di chl oropropene I , I ,2-Tri chl oroethene Di bromochl oromethanel, l, Z-Trichl oroethane ci s-l ,3-Di chl oropropene 2-ChI oroethoxyethane Bromoform I ,l ,2,2-TetrachI oroethane Tetrachl oroethene t'lethyl-t-butyl ether QUALITY CONTROL DATA 0ctober 18, 1994 PACE Project Number: 641004505 Units usTr- ug/L Method BI ankNr- ND MDLIT 1.0 Units us/t- ug/L ug/L ug/L ug/L ug/L ug/L ug/L us/L uglL ug/L ug/L u9/L ug/L ug/L ug/L uglL ug/L ug/L u9/L ug/L u9/L ug/L ug/L ug/L ug/L MDLm 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 1.0 1.0 0.5 1.0 0.5 1.0 Reference Val ue Recv-'2r-- -95[ 20 100%20 120%20 110%20 105%20 105% 20 20 20 20 20 20 20 20 20 20 20 20 20 ?0 20 20 20 20 20 20 100% 100% 100% 90r 105% 95% 95% 100% 105% t00% 100% 95% It0% 105% 105% 100% I l5% I l5% 100% 32% 9800 Kincey Avenus, Suite 1 00 Huntarsville, NC 28078 ItL:70r.8r5-W FAX: 704-875-9091 An Equal 0pportunity Employer / ffi REPoRToFLABoRAToRYANA QUALITY CONTROL DATA 0ctober 18, 1994 PACE Project Number: 641004505 Mr. John Burkart Page 14 Cl ient Reference: 94147-Stork Screen PURGEABLE HALOCARBONS AND AROMATICS Batch: 92 3t16l Samples: 92 0273001 LABORATORY CONTROL SAMPLE: Parameter Senzene Tol uene Chl orobenzene Ethyl benzene Xyl enes I ,3-Di chl orobenzene I ,4-Di chl orobenzene I ,2-Di chl orobenzene Uni ts usTr ug/L u9/L ug/L ug/L ug/L ug/ L ug/L MDLm 1.0 1.0 1.0 1.0 1.0 1.0 1.0 ReferenceValue Recv-T- ior;20 100%20 100%20 I05%50 97r,20 105% 20 105%20 tl0% Sl@ (incey,Avanue, Suite 100 Huntsrsvills, NC 28078 TSL:rOa{r5-S2 FI$( 701-875-S91 An Equal 0eportunity Employor , ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS Mr. John Burkart Page 15 Cl ient Reference: 94147-Stork Screen MDL Method Detection LimitND Not detected at or above the MDL.PC Possible laboratory contamjnant.RPD Relative Percent Difference FOOTNOTES 0ctober 18, 1994for pages 6 through 14 PACE Project Number: 541004505 9800 Kincey Avenuo, Suite 'l 00 Huntersvillo, NC 28078 IEL: r0l{rS900e FAX: 704.875-9fi11 An Equrl 0poonunity Emplover ct)Y E. =uJ E, ai6o (D,ooooo =ooE, I ..1tol 61 al =lclolololol.(61o-l o G,o @Et-o xGHgrt BE'9-g =>r(-oEtro< azol-o =EFaz Eolr IJ,Ioa ulU'E IIJ UJE IJI UJao'z oE(!.z