20017 Asheville Tannery PRII 2015.10.22

October 22, 2015

Mr. Chris Eller
Foundation Studios, LLC
9 Pack Square SW, Suite 210
Asheville, North Carolina 28801

Subject: Limited Phase II Environmental Site Assessment
Former Asheville Tannery/Day’s Tobacco Warehouse Property
339 Old Lyman Street, Asheville, North Carolina
Amec Foster Wheeler Project 6252-15-0214

Dear Mr. Eller:

Amec Foster Wheeler Environment & Infrastructure, Inc. (Amec Foster Wheeler) is
pleased to submit our Limited Phase II Environmental Site Assessment “update” report to
Foundation Studios, LLC for the approximate 13-acre former Asheville Tannery/Day’s
Tobacco Warehouse property (site), comprised of three Buncombe County tax parcels
9638-93-9759, 9638-94-6281 and 9638-93-6763, located at 339 Old Lyman Street in
Asheville, North Carolina (Figure 1 and Figure 2). This report summarizes background
information, field activities, laboratory analytical results, and conclusions from
environmental sampling performed at the subject property.

BACKGROUND INFORMATION
The Hans Rees’ Sons Tannery began operations at the site in approximately 1898. The
tannery was reportedly sold to C.T. Day in 1955, and C.T. Day and Day’s Warehouses
and/or Big Burley Tobacco primarily utilized the site for cattle, tobacco, auctions and
warehousing. The buildings at the site have had various commercial/industrial tenants
since the 1960s and several of the buildings were used for chemical storage during the
1960s and 1970s. The site currently contains nine buildings, which were observed to be
primarily vacant during a site visit on September 2, 2015.

Amec Foster Wheeler (formerly MACTEC) completed a Phase I Environmental Site
Assessment (ESA), dated April 4, 2007, and a Phase II Limited Site Assessment (LSA),
dated March 21, 2008, for an approximate ten-acre portion of the site comprised of the
two Buncombe County tax parcels with PINs 9638-93-9759 and 9638-94-6281. These
reports were prepared for a former owner of the site. The Phase I ESA identified several
recognized environmental conditions (RECs) at the site relating to the historical use and
operations at the site. The RECs identified included the presence of a heating oil storage
tank at Building #1, reported gasoline storage tanks and a former oil house northwest of
Building #1, the past use of the property for chemical storage, a machine shop, and as a
fitness equipment manufacturer utilizing solvents; upgradient, off-site, potential
contamination from the railroad and/or potential leaching of contaminants used in the
wood preserving process of the railroad ties; and the presence of a car crushing operation
Former Asheville Tannery/Day’s Tobacco Warehouse – Limited Phase II ESA Report October 22, 2015
339 Old Lyman Street, Asheville, North Carolina
Amec Foster Wheeler Project 6252-15-0214
2

in Building #3. The Phase II LSA identified chlorinated VOCs in soil and groundwater
above applicable standards near or below Buildings #s 1/1B/1C, 4, and 8. Petroleum-
related compounds were detected in soil and groundwater near or below Building #3
where a car crushing operation was located. It is our understanding that a consultant, on
behalf of the car crushing business, performed additional environmental services including
excavation of contaminated soil in Building #3; however, Amec Foster Wheeler has not
been provided environmental reports regarding these activities and the report was not
available from the North Carolina Department of Environmental Quality (NCDEQ)
Brownfield Program. The concentrations of some chlorinated volatile organic compounds
(VOCs) detected in groundwater samples collected in March 2008 exceed the current
NCDEQ Division of Waste Management’s (DWM) Non-Residential Vapor Intrusion
Concentrations (dated September 2015) Groundwater Screening Levels (GWSLs).

A Phase I ESA, dated April 14, 2010 (revised May 18, 2010), and a Phase II ESA, dated
July 19, 2011, for an approximate three-acre portion of the site comprised of the
Buncombe County tax parcel with PIN 9638-93-6763, were performed by Amec Foster
Wheeler as part of potential redevelopment of the site under a Brownfields Agreement for
a former owner of the site. The Phase I ESA identified RECs at the approximate three-
acre parcel including operation of a metal recycling business; the reported presence of
black sludge in subsurface tanning vats; and the known presence of soil and groundwater
contamination at the upgradient property. The Phase II ESA of the approximate three-acre
parcel identified the location of subsurface tanning vats via a geophysical survey.
Reported sludge material sampled from the vats was determined to not be a hazardous
waste. Additionally, semivolatile organic compounds and metals were detected in soil and
groundwater at concentrations that exceed applicable maximum allowable concentrations
or standards at the approximate three-acre parcel.

Foundation Studios, LLC has recently purchased the site and has requested this limited
Phase II Environmental Site Assessment “update” to assess the current condition of
groundwater in the general vicinity of areas where previous detections of chlorinated
VOCs in groundwater were identified (i.e., around Buildings #1C and #1/1B) and to
assess potential sub-slab soil gas/vapor intrusion associated with the identified
groundwater contamination beneath Building #1C and previously-identified petroleum-
impacted soil beneath Building #3.

FIELD ACTIVITIES
The following sections describe Amec Foster Wheeler’s field activities to evaluate the
current groundwater conditions in the vicinity of Buildings #1C and #1/1B, and sub-slab
soil gas conditions in Buildings #1C and #3.

Pre-Mobilization Activities
Amec Foster Wheeler updated the site Health and Safety Plan (HASP) in accordance with
OSHA 1910.120 requirements. The HASP identified general and known/suspected site-
specific health and safety hazards, and described procedures for addressing health and
safety hazards potentially associated with the site. Prior to intrusive activities, Amec
Foster Wheeler contacted North Carolina One Call to have the location of underground
public utilities marked at the site.
Former Asheville Tannery/Day’s Tobacco Warehouse – Limited Phase II ESA Report October 22, 2015
339 Old Lyman Street, Asheville, North Carolina
Amec Foster Wheeler Project 6252-15-0214
3

Groundwater Sampling
On October 7, 2015, Geologic Exploration, Inc. under subcontract to Amec Foster
Wheeler, mobilized a track-mounted GeoProbe direct-push technology sampling
equipment to the site to advanced five borings, DP-101 through DP-105. Prior to
advancement of the borings, the sampling equipment was decontaminated with an
industrial detergent and water solution. Individual, new, non-latex gloves were worn by
personnel handling in-hole equipment and sampling materials. Investigative derived
waste, including decontamination fluids and purge water were containerized in a 55-gallon
drum, which was properly sealed, labeled, and stored on the property.

A hand auger was utilized to advance the borings to five feet to clear utilities and for soil
description purposes. Soil samples were collected from each of the hand auger borings in
one foot intervals from ground surface to approximately five feet below ground surface (bgs)
and the soil lithology was described in general accordance with the Unified Soil
Classification System. The borings were advanced to approximately nine feet bgs with a
stainless steel screen point sampler for the collection of groundwater samples. The target
depth was below the depth of the apparent surficial water table, which was encountered at
approximately four feet below ground surface.

Groundwater in the screen point sampler was purged with a peristaltic pump and new
polyethylene tubing. Groundwater samples, TW-101 through TW-105, were collected from
the screen point sampler after the turbidity was reduced. A field duplicate sample, FD-101,
was also collected from boring DP-103. The groundwater samples were labeled with
sample information, packed in an ice-chilled cooler and delivered with chain-of-custody
records to Environmental Science Corporation in Mt. Juliet, Tennessee (an accredited
North Carolina laboratory) for analysis of VOCs according to EPA Method 8260B. The
samples were submitted for a standard laboratory turnaround time. After the groundwater
samples were collected, the screen point sampler was removed from the borings and the
boreholes were backfilled with hand auger soil cuttings and hydrated bentonite, as
needed.

Borings DP-101 and DP-102 were advanced to the west of Building #1C (TW-101
groundwater sample in general vicinity of former TW-13 groundwater sample), boring DP-
103 was advanced to the north of Building #1C (TW-103 groundwater sample in general
vicinity of former TW-14 groundwater sample), and borings DP-104 and DP-105 were
advanced between Buildings #1C and #1/1B (TW-105 groundwater sample in general
vicinity of former TW-12 groundwater sample). Figure 3 shows the locations of the soil
borings and associated groundwater samples. The soil retrieved/collected in hand auger soil
cuttings were screened for the presence of volatile organics with a photoionization detector
(PID). Relatively minor PID detections were observed in the TW-101 and TW-102 borings
with maximum detections of 0.5 parts per million (ppm) and 1.5 ppm, respectively, observed
in the four to five foot intervals which are near the groundwater table. Fill soil was generally
encountered from the ground surface to approximately two feet bgs at each of the
sampling locations. Coal fragments were observed in the surficial fill at the TW-102 and
TW-103 locations. Alluvial sediments were generally encountered at approximately two
feet bgs at each of the sampling locations, and consisted of brown, silty fine sand with
some mica.
Former Asheville Tannery/Day’s Tobacco Warehouse – Limited Phase II ESA Report October 22, 2015
339 Old Lyman Street, Asheville, North Carolina
Amec Foster Wheeler Project 6252-15-0214
4

Sub-Slab Soil Gas Sampling
On October 1, 2015, Amec Foster Wheeler collected four sub-slab soil gas samples, SG-1
through SG-4, and one field duplicate, FD-1, beneath the concrete floors in Buildings #1C
and #3. Sub-slab soil gas samples SG-1 and SG-2/FD-1 were collected in Building #1C,
and SG-3 and SG-4 were collected in Building #3. Figure 3 shows the locations of the sub-
slab soil gas samples. The sample locations were determined based on the construction of
the buildings’ floors, and were generally evenly distributed within the footprint of the
building. The soil gas samples were collected in general accordance with NCDEQ–DWM’s
Vapor Intrusion (VI) Guidelines, dated April 2014, with the exception that only two sub-
slab soil gas samples were collected in Building #3. The VI Guidelines recommend
collection of one sub-slab soil gas sample per 1,000-square feet of first-floor building area.
Building #3 is approximately 48,000 square feet; therefore additional samples would be
required to comply with the recommendation in the VI Guidelines.

The soil gas samples were collected using one-liter, batch-certified, Summa canisters
fitted with a critical orifice to allow for collection of samples over an approximate 30-minute
period (approximately 30 milliliters per minute). An approximate one-half-inch diameter
hole was advanced into soil (e.g. fill) below the concrete slab using a hammer drill. The
Summa canisters were attached to a flow controller (e.g. critical orifice), gauge and tubing
(sample train), and a shut-in test was performed with a syringe to determine if there were
leaks in the sample train. Tubing was advanced beneath the concrete slab, and hydrated
bentonite was installed around the tubing at the top of the concrete slab to create an air
tight seal.

A helium leak test was performed to validate the bentonite seal at each location. A helium
shroud (e.g. stainless steel bowl with two barbed fittings and an open hole) was installed
over the sealed sample port and the sample port tubing was sealed with hydrated
bentonite where it protruded from the open hole in the helium shroud. A helium bottle was
fitted with tubing and opened so that helium entered the shroud. The helium concentration
within the shroud was increased to greater than 50% and measured with a helium
detector. A lung sampler was connected to the sample port tubing to generate vacuum
pressure to inflate a Tedlar bag. Once filled, the Tedlar bag was detached from the lung
sampler and the helium detector was utilized to measure the concentration of helium.
Helium concentrations were not detected in the Tedlar bag at each sample location.

Subsurface conditions were allowed to equilibrate for thirty minutes prior to collecting air
samples. At least three tubing purge volumes were purged using a syringe. Following
purging, a Summa canister was attached to the tubing for sample collection.

Vacuum gauge readings were recorded before and after sample collection. A field
duplicate sample and a trip blank sample were also collected/submitted with the sub-slab
soil gas samples. The soil gas samples were submitted to ALS Environmental in Simi
Valley, California for analysis of VOCs according to USEPA Method TO-15.
Former Asheville Tannery/Day’s Tobacco Warehouse – Limited Phase II ESA Report October 22, 2015
339 Old Lyman Street, Asheville, North Carolina
Amec Foster Wheeler Project 6252-15-0214
5

ANALYTICAL RESULTS
The groundwater laboratory analytical results are summarized in Table 1. Concentrations
of eight VOCs were detected above the laboratory reporting limits in the submitted
groundwater samples.

The sub-slab soil gas laboratory analytical results are summarized in Table 2.
Concentrations of 29 VOCs were detected above the laboratory reporting limits in the
submitted sub-slab soil gas samples.

Copies of the laboratory reports and chain-of-custody records are attached.

DISCUSSION AND CONCLUSIONS
Groundwater Samples
The laboratory analytical results of the groundwater samples were evaluated with respect
to the current North Carolina Groundwater Classification and Standards, 15A NCAC 2L
.0202, effective April 1, 2013 (Groundwater Standards), which includes applicable interim
standards, and the current GWSLs from NCDEQ-DWM’s Non-Residential Vapor Intrusion
Concentrations table, dated September 2015. Concentrations of 1,1-dichloroethane were
detected above the groundwater standard, but below the Non-Residential GWSL, in the
TW-101, TW-103/FD-101 and TW-104 groundwater samples. Concentrations of
tetrachlorethene (PCE) were detected above the groundwater standard, but below the
Non-Residential GWSL, in the TW-101, TW-102 and TW-103/FD-101 groundwater
samples. A concentration of trichloroethene (TCE) was detected above the groundwater
standard, but below the Non-Residential GWSL, in the TW-105 groundwater sample. A
concentration of TCE was detected above the groundwater standard and above the Non-
Residential GWSL in the TW-101 groundwater sample. A concentration of vinyl chloride
was detected above the groundwater standard, but below the Non-Residential GWSL, in
the TW-101 groundwater sample.

In general, the concentrations of VOCs detected in groundwater in the area of Building
#1C and #1/1B are less than those concentrations detected in 2008.

One VOC, TCE, was detected above the Non-Residential GWSL in one groundwater
sample at location TW-101, which is within 100 feet of Building #1C. This detection would
prompt a vapor intrusion evaluation, which is addressed with the sub-slab soil gas
samples as discussed below.

Sub-Slab Soil Gas Samples
The laboratory analytical results of the sub-slab soil gas samples were evaluated with
respect to Sub-Slab and Exterior Soil Gas Screening Levels (SGSLs) from NCDEQ-
DWM’s Non-Residential Vapor Intrusion Concentrations table, dated September 2015.
The reported concentrations of 16 VOCs that have established SGSLs were below their
respective SGSLs. Five of the VOCs that were detected above the laboratory reporting
limits do not have SGSLs established for vapor intrusion evaluation purposes.

In general, the concentrations of VOCs detected in sub-slab soil gas are more than an
order of magnitude less than their respective SGSLs.

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TABLE 2
Summary of Sub-slab Soil Gas Analytical Results
Former Asheville Tannery / Day's Tobacco Warehouse
339 Old Lyman Street, Asheville, North Carolina
Amec Foster Wheeler Project 6252-15-0214
Constituent SGSL SG-1 SG-2
FD-1
(SG-2) SG-3 SG-4
Acenotrile 175 6.1 2.3 2.8
Acetone 2,720,000 140 34 43 77 370
Benzene 1,570 150 6.3 19 2.5 7.2
1,3-Butadiene 175 4.0
Building #1C Building #3
2-Butanone 1,880,000 26
Carbon Disulfide 61,300 21 54
Cyclohexane 526,000 83 81 160 4.4
Dichlorodifluoromethane 8,760 2.3 2.3 2.2 2.3 25
1,4-Dioxane 2,450 1.8
Ethanol*NE 26.0 72 28 31 180
Ethyl Acetate 6,130 5.0 4.3 50 5.0y
Ethylbenzene 4,910 9.3
n-Heptane NE 34 8.1 20 3.4
n-Hexane 61,300 31 18 38 3.1
2-Hexanone 2,630
d-Limonene NE 3.9 2.5 3.8
Methyl Methacrylate 61,300 20
n-Nonane 1,750 9.5 6.2n Nonane 1,750 9.5 6.2
n-Octane NE 20 3.7 6.9 4.7
alpha-Pinene NE 7.5 7.9 5.9 7.0
Propene 33 4.8 4 4.9 35 27
Tetrachloroethene 3,500 44 15 84
Tetrahydrofuran 175,000 1.9 2.8 4.1
Toluene*438,000 81 8.3 25 11
Trichloroethene 175 17 49 38Trichloroethene17517493.8
1,1,1-Trichloroethene 438,000 16 14 28
1,2,4-Trimethylbenzene 613
m,p-Xylenes 8,760 56.0
o-Xylenes 8,760 9.1
Notes:
1. SGSL-Sub-Slab/Exterior Soil Gas Screening Levels from North Carolina Department of Environmental Quality1. SGSL Sub Slab/Exterior Soil Gas Screening Levels from North Carolina Department of Environmental Quality
Division of Waste Management's Non-Residential Vapor Intrusion Concentrations, dated September 2015.
2. Concentrations are in micrograms per cubic meter (ug/m3).
3. NE - SGSL has not been established for associated compound.
4. Blank cells indicate constituent not detected above the labratory reporting limit.
5. * - Compound detected in trip blank above the labratory reporting limit.
Prepared By: RMC 10/19/15
Checked By: MRG 10/22/15
ANALYTICAL REPORT
October 16, 2015
AMEC - Asheville, NC
Sample 'elivery *roup: L793474
Samples ReceiveG:10/08/2015
3roMect Number:6252-15-0214
'escription:Asheville Tannery/'ay
s Tobacco :arehouse
Report To:RoGney ClarN
1308-C 3atton Avenue
Asheville, NC 28806
Entire Report RevieZeG %y:
October 16, 2015
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
October 16, 2015
Jimmy Hunt
Technical Service Representative
ONE LA% NAT,ON:,'ETA%LE O) CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 4
⁵Sr: Sample Results 5
T:-101 L793474-01 5
T:-102 L793474-02 7
T:-103 L793474-03 9
T:-104 L793474-04 11
)'-101 L793474-05 13
T%-101 L793474-06 15
T:-105 L793474-07 17
⁶Qc: Quality Control Summary 19
9olatile OrJanic CompounGs *C/MS by MethoG 8260% 19
⁷Gl: Glossary of Terms 31
⁸Al: Accreditations & Locations 32
⁹Sc: Chain of Custody 33
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 2 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 2 of 35
ONE LA% NAT,ON:,'ESAM3LE S8MMAR<
Collected by Collected date/time Received date/time
T:-101 L793474-01 *:Rodney M. Clark 10/07/15 09:47 10/08/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG820841 1 10/12/15 16:53 10/12/15 16:53 KLO
Collected by Collected date/time Received date/time
T:-102 L793474-02 *:Rodney M. Clark 10/07/15 11:03 10/08/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG820841 1 10/12/15 17:10 10/12/15 17:10 KLO
Collected by Collected date/time Received date/time
T:-103 L793474-03 *:Rodney M. Clark 10/07/15 12:25 10/08/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG820841 1 10/12/15 17:28 10/12/15 17:28 KLO
Collected by Collected date/time Received date/time
T:-104 L793474-04 *:Rodney M. Clark 10/07/15 13:15 10/08/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG820841 1 10/12/15 17:45 10/12/15 17:45 KLO
Collected by Collected date/time Received date/time
)'-101 L793474-05 *:Rodney M. Clark 10/07/15 00:00 10/08/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG820841 1 10/12/15 18:03 10/12/15 18:03 KLO
Collected by Collected date/time Received date/time
T%-101 L793474-06 *:Rodney M. Clark 10/07/15 00:00 10/08/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG821485 1 10/15/15 14:36 10/15/15 14:36 KLO
Collected by Collected date/time Received date/time
T:-105 L793474-07 *:Rodney M. Clark 10/07/15 14:45 10/08/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG821485 1 10/15/15 19:36 10/15/15 19:36 KLO
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 3 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 3 of 35
ONE LA% NAT,ON:,'ECASE NARRAT,9E
All sample aliTuots Zere receiveG at the correct temperature, in the proper containers, Zith the
appropriate preservatives, anG Zithin methoG specifieG holGinJ times All M'L LO' anG R'L LO4
values reporteG for environmental samples have been correcteG for the Gilution factor useG in the
analysis All MethoG anG %atch 4uality Control are Zithin establisheG criteria e[cept Zhere aGGresseG
in this case narrative, a non-conformance form or properly TualifieG Zithin the sample results %y my
GiJital siJnature beloZ, , affirm to the best of my NnoZleGJe, all problems/anomalies observeG by the
laboratory as havinJ the potential to affect the Tuality of the Gata have been iGentifieG by the
laboratory, anG no information or Gata have been NnoZinJly ZithhelG that ZoulG affect the Tuality of the
Gata
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 4 of 35
Jimmy Hunt
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 4 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 01
L793474
TW-101
Collected date/time: 10/07/15 09:47
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 10/12/2015 16:53 WG820841
Acrolein ND 50.0 1 10/12/2015 16:53 WG820841
Acrylonitrile ND 10.0 1 10/12/2015 16:53 WG820841
Benzene ND 1.00 1 10/12/2015 16:53 WG820841
Bromobenzene ND 1.00 1 10/12/2015 16:53 WG820841
Bromodichloromethane ND 1.00 1 10/12/2015 16:53 WG820841
Bromoform ND 1.00 1 10/12/2015 16:53 WG820841
Bromomethane ND 5.00 1 10/12/2015 16:53 WG820841
n-Butylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
sec-Butylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
tert-Butylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
Carbon tetrachloride ND 1.00 1 10/12/2015 16:53 WG820841
Chlorobenzene ND 1.00 1 10/12/2015 16:53 WG820841
Chlorodibromomethane ND 1.00 1 10/12/2015 16:53 WG820841
Chloroethane ND 5.00 1 10/12/2015 16:53 WG820841
2-Chloroethyl vinyl ether ND J4 50.0 1 10/12/2015 16:53 WG820841
Chloroform ND 5.00 1 10/12/2015 16:53 WG820841
Chloromethane ND 2.50 1 10/12/2015 16:53 WG820841
2-Chlorotoluene ND 1.00 1 10/12/2015 16:53 WG820841
4-Chlorotoluene ND 1.00 1 10/12/2015 16:53 WG820841
1,2-Dibromo-3-Chloropropane ND 5.00 1 10/12/2015 16:53 WG820841
1,2-Dibromoethane ND 1.00 1 10/12/2015 16:53 WG820841
Dibromomethane ND 1.00 1 10/12/2015 16:53 WG820841
1,2-Dichlorobenzene ND 1.00 1 10/12/2015 16:53 WG820841
1,3-Dichlorobenzene ND 1.00 1 10/12/2015 16:53 WG820841
1,4-Dichlorobenzene ND 1.00 1 10/12/2015 16:53 WG820841
Dichlorodifluoromethane ND 5.00 1 10/12/2015 16:53 WG820841
1,1-Dichloroethane 6.29 1.00 1 10/12/2015 16:53 WG820841
1,2-Dichloroethane ND 1.00 1 10/12/2015 16:53 WG820841
1,1-Dichloroethene ND 1.00 1 10/12/2015 16:53 WG820841
cis-1,2-Dichloroethene 31.3 1.00 1 10/12/2015 16:53 WG820841
trans-1,2-Dichloroethene ND 1.00 1 10/12/2015 16:53 WG820841
1,2-Dichloropropane ND 1.00 1 10/12/2015 16:53 WG820841
1,1-Dichloropropene ND 1.00 1 10/12/2015 16:53 WG820841
1,3-Dichloropropane ND 1.00 1 10/12/2015 16:53 WG820841
cis-1,3-Dichloropropene ND 1.00 1 10/12/2015 16:53 WG820841
trans-1,3-Dichloropropene ND 1.00 1 10/12/2015 16:53 WG820841
2,2-Dichloropropane ND 1.00 1 10/12/2015 16:53 WG820841
Di-isopropyl ether ND 1.00 1 10/12/2015 16:53 WG820841
Ethylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
Hexachloro-1,3-butadiene ND 1.00 1 10/12/2015 16:53 WG820841
Isopropylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
p-Isopropyltoluene ND 1.00 1 10/12/2015 16:53 WG820841
2-Butanone (MEK)ND 10.0 1 10/12/2015 16:53 WG820841
Methylene Chloride ND 5.00 1 10/12/2015 16:53 WG820841
4-Methyl-2-pentanone (MIBK) ND 10.0 1 10/12/2015 16:53 WG820841
Methyl tert-butyl ether ND 1.00 1 10/12/2015 16:53 WG820841
Naphthalene ND 5.00 1 10/12/2015 16:53 WG820841
n-Propylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
Styrene ND 1.00 1 10/12/2015 16:53 WG820841
1,1,1,2-Tetrachloroethane ND 1.00 1 10/12/2015 16:53 WG820841
1,1,2,2-Tetrachloroethane ND 1.00 1 10/12/2015 16:53 WG820841
1,1,2-Trichlorotrifluoroethane ND 1.00 1 10/12/2015 16:53 WG820841
Tetrachloroethene 42.2 1.00 1 10/12/2015 16:53 WG820841
Toluene ND 5.00 1 10/12/2015 16:53 WG820841
1,2,3-Trichlorobenzene ND 1.00 1 10/12/2015 16:53 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 5 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 5 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 01
L793474
TW-101
Collected date/time: 10/07/15 09:47
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2,4-Trichlorobenzene ND 1.00 1 10/12/2015 16:53 WG820841
1,1,1-Trichloroethane 1.55 1.00 1 10/12/2015 16:53 WG820841
1,1,2-Trichloroethane ND 1.00 1 10/12/2015 16:53 WG820841
Trichloroethene 5.99 1.00 1 10/12/2015 16:53 WG820841
Trichlorofluoromethane ND 5.00 1 10/12/2015 16:53 WG820841
1,2,3-Trichloropropane ND 2.50 1 10/12/2015 16:53 WG820841
1,2,4-Trimethylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
1,2,3-Trimethylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
1,3,5-Trimethylbenzene ND 1.00 1 10/12/2015 16:53 WG820841
Vinyl chloride 2.01 1.00 1 10/12/2015 16:53 WG820841
Xylenes, Total ND 3.00 1 10/12/2015 16:53 WG820841
(S) Toluene-d8 97.7 90.0-115 10/12/2015 16:53 WG820841
(S) Dibromofluoromethane 94.9 79.0-121 10/12/2015 16:53 WG820841
(S) 4-Bromofluorobenzene 99.6 80.1-120 10/12/2015 16:53 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 6 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 6 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 02
L793474
TW-102
Collected date/time: 10/07/15 11:03
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 10/12/2015 17:10 WG820841
Acrolein ND 50.0 1 10/12/2015 17:10 WG820841
Acrylonitrile ND 10.0 1 10/12/2015 17:10 WG820841
Benzene ND 1.00 1 10/12/2015 17:10 WG820841
Bromobenzene ND 1.00 1 10/12/2015 17:10 WG820841
Bromodichloromethane ND 1.00 1 10/12/2015 17:10 WG820841
Bromoform ND 1.00 1 10/12/2015 17:10 WG820841
Bromomethane ND 5.00 1 10/12/2015 17:10 WG820841
n-Butylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
sec-Butylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
tert-Butylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
Carbon tetrachloride ND 1.00 1 10/12/2015 17:10 WG820841
Chlorobenzene ND 1.00 1 10/12/2015 17:10 WG820841
Chlorodibromomethane ND 1.00 1 10/12/2015 17:10 WG820841
Chloroethane ND 5.00 1 10/12/2015 17:10 WG820841
2-Chloroethyl vinyl ether ND J4 50.0 1 10/12/2015 17:10 WG820841
Chloroform ND 5.00 1 10/12/2015 17:10 WG820841
Chloromethane ND 2.50 1 10/12/2015 17:10 WG820841
2-Chlorotoluene ND 1.00 1 10/12/2015 17:10 WG820841
4-Chlorotoluene ND 1.00 1 10/12/2015 17:10 WG820841
1,2-Dibromo-3-Chloropropane ND 5.00 1 10/12/2015 17:10 WG820841
1,2-Dibromoethane ND 1.00 1 10/12/2015 17:10 WG820841
Dibromomethane ND 1.00 1 10/12/2015 17:10 WG820841
1,2-Dichlorobenzene ND 1.00 1 10/12/2015 17:10 WG820841
1,3-Dichlorobenzene ND 1.00 1 10/12/2015 17:10 WG820841
1,4-Dichlorobenzene ND 1.00 1 10/12/2015 17:10 WG820841
Dichlorodifluoromethane ND 5.00 1 10/12/2015 17:10 WG820841
1,1-Dichloroethane ND 1.00 1 10/12/2015 17:10 WG820841
1,2-Dichloroethane ND 1.00 1 10/12/2015 17:10 WG820841
1,1-Dichloroethene ND 1.00 1 10/12/2015 17:10 WG820841
cis-1,2-Dichloroethene 13.9 1.00 1 10/12/2015 17:10 WG820841
trans-1,2-Dichloroethene ND 1.00 1 10/12/2015 17:10 WG820841
1,2-Dichloropropane ND 1.00 1 10/12/2015 17:10 WG820841
1,1-Dichloropropene ND 1.00 1 10/12/2015 17:10 WG820841
1,3-Dichloropropane ND 1.00 1 10/12/2015 17:10 WG820841
cis-1,3-Dichloropropene ND 1.00 1 10/12/2015 17:10 WG820841
trans-1,3-Dichloropropene ND 1.00 1 10/12/2015 17:10 WG820841
2,2-Dichloropropane ND 1.00 1 10/12/2015 17:10 WG820841
Di-isopropyl ether ND 1.00 1 10/12/2015 17:10 WG820841
Ethylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
Hexachloro-1,3-butadiene ND 1.00 1 10/12/2015 17:10 WG820841
Isopropylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
p-Isopropyltoluene ND 1.00 1 10/12/2015 17:10 WG820841
2-Butanone (MEK)ND 10.0 1 10/12/2015 17:10 WG820841
Methylene Chloride ND 5.00 1 10/12/2015 17:10 WG820841
4-Methyl-2-pentanone (MIBK) ND 10.0 1 10/12/2015 17:10 WG820841
Methyl tert-butyl ether ND 1.00 1 10/12/2015 17:10 WG820841
Naphthalene ND 5.00 1 10/12/2015 17:10 WG820841
n-Propylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
Styrene ND 1.00 1 10/12/2015 17:10 WG820841
1,1,1,2-Tetrachloroethane ND 1.00 1 10/12/2015 17:10 WG820841
1,1,2,2-Tetrachloroethane ND 1.00 1 10/12/2015 17:10 WG820841
1,1,2-Trichlorotrifluoroethane ND 1.00 1 10/12/2015 17:10 WG820841
Tetrachloroethene 29.0 1.00 1 10/12/2015 17:10 WG820841
Toluene ND 5.00 1 10/12/2015 17:10 WG820841
1,2,3-Trichlorobenzene ND 1.00 1 10/12/2015 17:10 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 7 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 7 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 02
L793474
TW-102
Collected date/time: 10/07/15 11:03
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2,4-Trichlorobenzene ND 1.00 1 10/12/2015 17:10 WG820841
1,1,1-Trichloroethane ND 1.00 1 10/12/2015 17:10 WG820841
1,1,2-Trichloroethane ND 1.00 1 10/12/2015 17:10 WG820841
Trichloroethene 2.15 1.00 1 10/12/2015 17:10 WG820841
Trichlorofluoromethane ND 5.00 1 10/12/2015 17:10 WG820841
1,2,3-Trichloropropane ND 2.50 1 10/12/2015 17:10 WG820841
1,2,4-Trimethylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
1,2,3-Trimethylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
1,3,5-Trimethylbenzene ND 1.00 1 10/12/2015 17:10 WG820841
Vinyl chloride ND 1.00 1 10/12/2015 17:10 WG820841
Xylenes, Total ND 3.00 1 10/12/2015 17:10 WG820841
(S) Toluene-d8 99.1 90.0-115 10/12/2015 17:10 WG820841
(S) Dibromofluoromethane 95.4 79.0-121 10/12/2015 17:10 WG820841
(S) 4-Bromofluorobenzene 98.8 80.1-120 10/12/2015 17:10 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 8 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 8 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 03
L793474
TW-103
Collected date/time: 10/07/15 12:25
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 10/12/2015 17:28 WG820841
Acrolein ND 50.0 1 10/12/2015 17:28 WG820841
Acrylonitrile ND 10.0 1 10/12/2015 17:28 WG820841
Benzene ND 1.00 1 10/12/2015 17:28 WG820841
Bromobenzene ND 1.00 1 10/12/2015 17:28 WG820841
Bromodichloromethane ND 1.00 1 10/12/2015 17:28 WG820841
Bromoform ND 1.00 1 10/12/2015 17:28 WG820841
Bromomethane ND 5.00 1 10/12/2015 17:28 WG820841
n-Butylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
sec-Butylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
tert-Butylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
Carbon tetrachloride ND 1.00 1 10/12/2015 17:28 WG820841
Chlorobenzene ND 1.00 1 10/12/2015 17:28 WG820841
Chlorodibromomethane ND 1.00 1 10/12/2015 17:28 WG820841
Chloroethane ND 5.00 1 10/12/2015 17:28 WG820841
2-Chloroethyl vinyl ether ND J4 50.0 1 10/12/2015 17:28 WG820841
Chloroform ND 5.00 1 10/12/2015 17:28 WG820841
Chloromethane ND 2.50 1 10/12/2015 17:28 WG820841
2-Chlorotoluene ND 1.00 1 10/12/2015 17:28 WG820841
4-Chlorotoluene ND 1.00 1 10/12/2015 17:28 WG820841
1,2-Dibromo-3-Chloropropane ND 5.00 1 10/12/2015 17:28 WG820841
1,2-Dibromoethane ND 1.00 1 10/12/2015 17:28 WG820841
Dibromomethane ND 1.00 1 10/12/2015 17:28 WG820841
1,2-Dichlorobenzene ND 1.00 1 10/12/2015 17:28 WG820841
1,3-Dichlorobenzene ND 1.00 1 10/12/2015 17:28 WG820841
1,4-Dichlorobenzene ND 1.00 1 10/12/2015 17:28 WG820841
Dichlorodifluoromethane ND 5.00 1 10/12/2015 17:28 WG820841
1,1-Dichloroethane 8.62 1.00 1 10/12/2015 17:28 WG820841
1,2-Dichloroethane ND 1.00 1 10/12/2015 17:28 WG820841
1,1-Dichloroethene ND 1.00 1 10/12/2015 17:28 WG820841
cis-1,2-Dichloroethene 9.52 1.00 1 10/12/2015 17:28 WG820841
trans-1,2-Dichloroethene ND 1.00 1 10/12/2015 17:28 WG820841
1,2-Dichloropropane ND 1.00 1 10/12/2015 17:28 WG820841
1,1-Dichloropropene ND 1.00 1 10/12/2015 17:28 WG820841
1,3-Dichloropropane ND 1.00 1 10/12/2015 17:28 WG820841
cis-1,3-Dichloropropene ND 1.00 1 10/12/2015 17:28 WG820841
trans-1,3-Dichloropropene ND 1.00 1 10/12/2015 17:28 WG820841
2,2-Dichloropropane ND 1.00 1 10/12/2015 17:28 WG820841
Di-isopropyl ether ND 1.00 1 10/12/2015 17:28 WG820841
Ethylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
Hexachloro-1,3-butadiene ND 1.00 1 10/12/2015 17:28 WG820841
Isopropylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
p-Isopropyltoluene ND 1.00 1 10/12/2015 17:28 WG820841
2-Butanone (MEK)ND 10.0 1 10/12/2015 17:28 WG820841
Methylene Chloride ND 5.00 1 10/12/2015 17:28 WG820841
4-Methyl-2-pentanone (MIBK) ND 10.0 1 10/12/2015 17:28 WG820841
Methyl tert-butyl ether ND 1.00 1 10/12/2015 17:28 WG820841
Naphthalene ND 5.00 1 10/12/2015 17:28 WG820841
n-Propylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
Styrene ND 1.00 1 10/12/2015 17:28 WG820841
1,1,1,2-Tetrachloroethane ND 1.00 1 10/12/2015 17:28 WG820841
1,1,2,2-Tetrachloroethane ND 1.00 1 10/12/2015 17:28 WG820841
1,1,2-Trichlorotrifluoroethane ND 1.00 1 10/12/2015 17:28 WG820841
Tetrachloroethene 7.01 1.00 1 10/12/2015 17:28 WG820841
Toluene ND 5.00 1 10/12/2015 17:28 WG820841
1,2,3-Trichlorobenzene ND 1.00 1 10/12/2015 17:28 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 9 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 9 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 03
L793474
TW-103
Collected date/time: 10/07/15 12:25
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2,4-Trichlorobenzene ND 1.00 1 10/12/2015 17:28 WG820841
1,1,1-Trichloroethane ND 1.00 1 10/12/2015 17:28 WG820841
1,1,2-Trichloroethane ND 1.00 1 10/12/2015 17:28 WG820841
Trichloroethene 1.57 1.00 1 10/12/2015 17:28 WG820841
Trichlorofluoromethane ND 5.00 1 10/12/2015 17:28 WG820841
1,2,3-Trichloropropane ND 2.50 1 10/12/2015 17:28 WG820841
1,2,4-Trimethylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
1,2,3-Trimethylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
1,3,5-Trimethylbenzene ND 1.00 1 10/12/2015 17:28 WG820841
Vinyl chloride ND 1.00 1 10/12/2015 17:28 WG820841
Xylenes, Total ND 3.00 1 10/12/2015 17:28 WG820841
(S) Toluene-d8 99.1 90.0-115 10/12/2015 17:28 WG820841
(S) Dibromofluoromethane 97.2 79.0-121 10/12/2015 17:28 WG820841
(S) 4-Bromofluorobenzene 100 80.1-120 10/12/2015 17:28 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 10 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 10 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 04
L793474
TW-104
Collected date/time: 10/07/15 13:15
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 10/12/2015 17:45 WG820841
Acrolein ND 50.0 1 10/12/2015 17:45 WG820841
Acrylonitrile ND 10.0 1 10/12/2015 17:45 WG820841
Benzene ND 1.00 1 10/12/2015 17:45 WG820841
Bromobenzene ND 1.00 1 10/12/2015 17:45 WG820841
Bromodichloromethane ND 1.00 1 10/12/2015 17:45 WG820841
Bromoform ND 1.00 1 10/12/2015 17:45 WG820841
Bromomethane ND 5.00 1 10/12/2015 17:45 WG820841
n-Butylbenzene ND 1.00 1 10/12/2015 17:45 WG820841
sec-Butylbenzene 2.47 1.00 1 10/12/2015 17:45 WG820841
tert-Butylbenzene ND 1.00 1 10/12/2015 17:45 WG820841
Carbon tetrachloride ND 1.00 1 10/12/2015 17:45 WG820841
Chlorobenzene ND 1.00 1 10/12/2015 17:45 WG820841
Chlorodibromomethane ND 1.00 1 10/12/2015 17:45 WG820841
Chloroethane ND 5.00 1 10/12/2015 17:45 WG820841
2-Chloroethyl vinyl ether ND J4 50.0 1 10/12/2015 17:45 WG820841
Chloroform ND 5.00 1 10/12/2015 17:45 WG820841
Chloromethane ND 2.50 1 10/12/2015 17:45 WG820841
2-Chlorotoluene ND 1.00 1 10/12/2015 17:45 WG820841
4-Chlorotoluene ND 1.00 1 10/12/2015 17:45 WG820841
1,2-Dibromo-3-Chloropropane ND 5.00 1 10/12/2015 17:45 WG820841
1,2-Dibromoethane ND 1.00 1 10/12/2015 17:45 WG820841
Dibromomethane ND 1.00 1 10/12/2015 17:45 WG820841
1,2-Dichlorobenzene ND 1.00 1 10/12/2015 17:45 WG820841
1,3-Dichlorobenzene ND 1.00 1 10/12/2015 17:45 WG820841
1,4-Dichlorobenzene ND 1.00 1 10/12/2015 17:45 WG820841
Dichlorodifluoromethane ND 5.00 1 10/12/2015 17:45 WG820841
1,1-Dichloroethane 20.0 1.00 1 10/12/2015 17:45 WG820841
1,2-Dichloroethane ND 1.00 1 10/12/2015 17:45 WG820841
1,1-Dichloroethene ND 1.00 1 10/12/2015 17:45 WG820841
cis-1,2-Dichloroethene 3.02 1.00 1 10/12/2015 17:45 WG820841
trans-1,2-Dichloroethene ND 1.00 1 10/12/2015 17:45 WG820841
1,2-Dichloropropane ND 1.00 1 10/12/2015 17:45 WG820841
1,1-Dichloropropene ND 1.00 1 10/12/2015 17:45 WG820841
1,3-Dichloropropane ND 1.00 1 10/12/2015 17:45 WG820841
cis-1,3-Dichloropropene ND 1.00 1 10/12/2015 17:45 WG820841
trans-1,3-Dichloropropene ND 1.00 1 10/12/2015 17:45 WG820841
2,2-Dichloropropane ND 1.00 1 10/12/2015 17:45 WG820841
Di-isopropyl ether ND 1.00 1 10/12/2015 17:45 WG820841
Ethylbenzene ND 1.00 1 10/12/2015 17:45 WG820841
Hexachloro-1,3-butadiene ND 1.00 1 10/12/2015 17:45 WG820841
Isopropylbenzene 1.52 1.00 1 10/12/2015 17:45 WG820841
p-Isopropyltoluene ND 1.00 1 10/12/2015 17:45 WG820841
2-Butanone (MEK)ND 10.0 1 10/12/2015 17:45 WG820841
Methylene Chloride ND 5.00 1 10/12/2015 17:45 WG820841
4-Methyl-2-pentanone (MIBK) ND 10.0 1 10/12/2015 17:45 WG820841
Methyl tert-butyl ether ND 1.00 1 10/12/2015 17:45 WG820841
Naphthalene ND 5.00 1 10/12/2015 17:45 WG820841
n-Propylbenzene 1.08 1.00 1 10/12/2015 17:45 WG820841
Styrene ND 1.00 1 10/12/2015 17:45 WG820841
1,1,1,2-Tetrachloroethane ND 1.00 1 10/12/2015 17:45 WG820841
1,1,2,2-Tetrachloroethane ND 1.00 1 10/12/2015 17:45 WG820841
1,1,2-Trichlorotrifluoroethane ND 1.00 1 10/12/2015 17:45 WG820841
Tetrachloroethene ND 1.00 1 10/12/2015 17:45 WG820841
Toluene ND 5.00 1 10/12/2015 17:45 WG820841
1,2,3-Trichlorobenzene ND 1.00 1 10/12/2015 17:45 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 11 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 11 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 04
L793474
TW-104
Collected date/time: 10/07/15 13:15
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2,4-Trichlorobenzene ND 1.00 1 10/12/2015 17:45 WG820841
1,1,1-Trichloroethane ND 1.00 1 10/12/2015 17:45 WG820841
1,1,2-Trichloroethane ND 1.00 1 10/12/2015 17:45 WG820841
Trichloroethene ND 1.00 1 10/12/2015 17:45 WG820841
Trichlorofluoromethane ND 5.00 1 10/12/2015 17:45 WG820841
1,2,3-Trichloropropane ND 2.50 1 10/12/2015 17:45 WG820841
1,2,4-Trimethylbenzene ND 1.00 1 10/12/2015 17:45 WG820841
1,2,3-Trimethylbenzene ND 1.00 1 10/12/2015 17:45 WG820841
1,3,5-Trimethylbenzene ND 1.00 1 10/12/2015 17:45 WG820841
Vinyl chloride ND 1.00 1 10/12/2015 17:45 WG820841
Xylenes, Total ND 3.00 1 10/12/2015 17:45 WG820841
(S) Toluene-d8 102 90.0-115 10/12/2015 17:45 WG820841
(S) Dibromofluoromethane 94.6 79.0-121 10/12/2015 17:45 WG820841
(S) 4-Bromofluorobenzene 111 80.1-120 10/12/2015 17:45 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 12 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 12 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 05
L793474
FD-101
Collected date/time: 10/07/15 00:00
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 10/12/2015 18:03 WG820841
Acrolein ND 50.0 1 10/12/2015 18:03 WG820841
Acrylonitrile ND 10.0 1 10/12/2015 18:03 WG820841
Benzene ND 1.00 1 10/12/2015 18:03 WG820841
Bromobenzene ND 1.00 1 10/12/2015 18:03 WG820841
Bromodichloromethane ND 1.00 1 10/12/2015 18:03 WG820841
Bromoform ND 1.00 1 10/12/2015 18:03 WG820841
Bromomethane ND 5.00 1 10/12/2015 18:03 WG820841
n-Butylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
sec-Butylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
tert-Butylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
Carbon tetrachloride ND 1.00 1 10/12/2015 18:03 WG820841
Chlorobenzene ND 1.00 1 10/12/2015 18:03 WG820841
Chlorodibromomethane ND 1.00 1 10/12/2015 18:03 WG820841
Chloroethane ND 5.00 1 10/12/2015 18:03 WG820841
2-Chloroethyl vinyl ether ND J4 50.0 1 10/12/2015 18:03 WG820841
Chloroform ND 5.00 1 10/12/2015 18:03 WG820841
Chloromethane ND 2.50 1 10/12/2015 18:03 WG820841
2-Chlorotoluene ND 1.00 1 10/12/2015 18:03 WG820841
4-Chlorotoluene ND 1.00 1 10/12/2015 18:03 WG820841
1,2-Dibromo-3-Chloropropane ND 5.00 1 10/12/2015 18:03 WG820841
1,2-Dibromoethane ND 1.00 1 10/12/2015 18:03 WG820841
Dibromomethane ND 1.00 1 10/12/2015 18:03 WG820841
1,2-Dichlorobenzene ND 1.00 1 10/12/2015 18:03 WG820841
1,3-Dichlorobenzene ND 1.00 1 10/12/2015 18:03 WG820841
1,4-Dichlorobenzene ND 1.00 1 10/12/2015 18:03 WG820841
Dichlorodifluoromethane ND 5.00 1 10/12/2015 18:03 WG820841
1,1-Dichloroethane 9.48 1.00 1 10/12/2015 18:03 WG820841
1,2-Dichloroethane ND 1.00 1 10/12/2015 18:03 WG820841
1,1-Dichloroethene ND 1.00 1 10/12/2015 18:03 WG820841
cis-1,2-Dichloroethene 9.05 1.00 1 10/12/2015 18:03 WG820841
trans-1,2-Dichloroethene ND 1.00 1 10/12/2015 18:03 WG820841
1,2-Dichloropropane ND 1.00 1 10/12/2015 18:03 WG820841
1,1-Dichloropropene ND 1.00 1 10/12/2015 18:03 WG820841
1,3-Dichloropropane ND 1.00 1 10/12/2015 18:03 WG820841
cis-1,3-Dichloropropene ND 1.00 1 10/12/2015 18:03 WG820841
trans-1,3-Dichloropropene ND 1.00 1 10/12/2015 18:03 WG820841
2,2-Dichloropropane ND 1.00 1 10/12/2015 18:03 WG820841
Di-isopropyl ether ND 1.00 1 10/12/2015 18:03 WG820841
Ethylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
Hexachloro-1,3-butadiene ND 1.00 1 10/12/2015 18:03 WG820841
Isopropylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
p-Isopropyltoluene ND 1.00 1 10/12/2015 18:03 WG820841
2-Butanone (MEK)ND 10.0 1 10/12/2015 18:03 WG820841
Methylene Chloride ND 5.00 1 10/12/2015 18:03 WG820841
4-Methyl-2-pentanone (MIBK) ND 10.0 1 10/12/2015 18:03 WG820841
Methyl tert-butyl ether ND 1.00 1 10/12/2015 18:03 WG820841
Naphthalene ND 5.00 1 10/12/2015 18:03 WG820841
n-Propylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
Styrene ND 1.00 1 10/12/2015 18:03 WG820841
1,1,1,2-Tetrachloroethane ND 1.00 1 10/12/2015 18:03 WG820841
1,1,2,2-Tetrachloroethane ND 1.00 1 10/12/2015 18:03 WG820841
1,1,2-Trichlorotrifluoroethane ND 1.00 1 10/12/2015 18:03 WG820841
Tetrachloroethene 4.84 1.00 1 10/12/2015 18:03 WG820841
Toluene ND 5.00 1 10/12/2015 18:03 WG820841
1,2,3-Trichlorobenzene ND 1.00 1 10/12/2015 18:03 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 13 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 13 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 05
L793474
FD-101
Collected date/time: 10/07/15 00:00
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2,4-Trichlorobenzene ND 1.00 1 10/12/2015 18:03 WG820841
1,1,1-Trichloroethane ND 1.00 1 10/12/2015 18:03 WG820841
1,1,2-Trichloroethane ND 1.00 1 10/12/2015 18:03 WG820841
Trichloroethene 1.36 1.00 1 10/12/2015 18:03 WG820841
Trichlorofluoromethane ND 5.00 1 10/12/2015 18:03 WG820841
1,2,3-Trichloropropane ND 2.50 1 10/12/2015 18:03 WG820841
1,2,4-Trimethylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
1,2,3-Trimethylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
1,3,5-Trimethylbenzene ND 1.00 1 10/12/2015 18:03 WG820841
Vinyl chloride ND 1.00 1 10/12/2015 18:03 WG820841
Xylenes, Total ND 3.00 1 10/12/2015 18:03 WG820841
(S) Toluene-d8 99.5 90.0-115 10/12/2015 18:03 WG820841
(S) Dibromofluoromethane 96.5 79.0-121 10/12/2015 18:03 WG820841
(S) 4-Bromofluorobenzene 101 80.1-120 10/12/2015 18:03 WG820841
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 14 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 14 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 06
L793474
TB-101
Collected date/time: 10/07/15 00:00
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 10/15/2015 14:36 WG821485
Acrolein ND 50.0 1 10/15/2015 14:36 WG821485
Acrylonitrile ND 10.0 1 10/15/2015 14:36 WG821485
Benzene ND 1.00 1 10/15/2015 14:36 WG821485
Bromobenzene ND 1.00 1 10/15/2015 14:36 WG821485
Bromodichloromethane ND 1.00 1 10/15/2015 14:36 WG821485
Bromoform ND 1.00 1 10/15/2015 14:36 WG821485
Bromomethane ND 5.00 1 10/15/2015 14:36 WG821485
n-Butylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
sec-Butylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
tert-Butylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
Carbon tetrachloride ND 1.00 1 10/15/2015 14:36 WG821485
Chlorobenzene ND 1.00 1 10/15/2015 14:36 WG821485
Chlorodibromomethane ND 1.00 1 10/15/2015 14:36 WG821485
Chloroethane ND 5.00 1 10/15/2015 14:36 WG821485
2-Chloroethyl vinyl ether ND J4 50.0 1 10/15/2015 14:36 WG821485
Chloroform ND 5.00 1 10/15/2015 14:36 WG821485
Chloromethane ND 2.50 1 10/15/2015 14:36 WG821485
2-Chlorotoluene ND 1.00 1 10/15/2015 14:36 WG821485
4-Chlorotoluene ND 1.00 1 10/15/2015 14:36 WG821485
1,2-Dibromo-3-Chloropropane ND 5.00 1 10/15/2015 14:36 WG821485
1,2-Dibromoethane ND 1.00 1 10/15/2015 14:36 WG821485
Dibromomethane ND 1.00 1 10/15/2015 14:36 WG821485
1,2-Dichlorobenzene ND 1.00 1 10/15/2015 14:36 WG821485
1,3-Dichlorobenzene ND 1.00 1 10/15/2015 14:36 WG821485
1,4-Dichlorobenzene ND 1.00 1 10/15/2015 14:36 WG821485
Dichlorodifluoromethane ND 5.00 1 10/15/2015 14:36 WG821485
1,1-Dichloroethane ND 1.00 1 10/15/2015 14:36 WG821485
1,2-Dichloroethane ND 1.00 1 10/15/2015 14:36 WG821485
1,1-Dichloroethene ND 1.00 1 10/15/2015 14:36 WG821485
cis-1,2-Dichloroethene ND 1.00 1 10/15/2015 14:36 WG821485
trans-1,2-Dichloroethene ND 1.00 1 10/15/2015 14:36 WG821485
1,2-Dichloropropane ND 1.00 1 10/15/2015 14:36 WG821485
1,1-Dichloropropene ND 1.00 1 10/15/2015 14:36 WG821485
1,3-Dichloropropane ND 1.00 1 10/15/2015 14:36 WG821485
cis-1,3-Dichloropropene ND 1.00 1 10/15/2015 14:36 WG821485
trans-1,3-Dichloropropene ND 1.00 1 10/15/2015 14:36 WG821485
2,2-Dichloropropane ND 1.00 1 10/15/2015 14:36 WG821485
Di-isopropyl ether ND 1.00 1 10/15/2015 14:36 WG821485
Ethylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
Hexachloro-1,3-butadiene ND 1.00 1 10/15/2015 14:36 WG821485
Isopropylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
p-Isopropyltoluene ND 1.00 1 10/15/2015 14:36 WG821485
2-Butanone (MEK)ND 10.0 1 10/15/2015 14:36 WG821485
Methylene Chloride ND 5.00 1 10/15/2015 14:36 WG821485
4-Methyl-2-pentanone (MIBK) ND 10.0 1 10/15/2015 14:36 WG821485
Methyl tert-butyl ether ND 1.00 1 10/15/2015 14:36 WG821485
Naphthalene ND 5.00 1 10/15/2015 14:36 WG821485
n-Propylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
Styrene ND 1.00 1 10/15/2015 14:36 WG821485
1,1,1,2-Tetrachloroethane ND 1.00 1 10/15/2015 14:36 WG821485
1,1,2,2-Tetrachloroethane ND 1.00 1 10/15/2015 14:36 WG821485
1,1,2-Trichlorotrifluoroethane ND 1.00 1 10/15/2015 14:36 WG821485
Tetrachloroethene ND 1.00 1 10/15/2015 14:36 WG821485
Toluene ND 5.00 1 10/15/2015 14:36 WG821485
1,2,3-Trichlorobenzene ND 1.00 1 10/15/2015 14:36 WG821485
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 15 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 15 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 06
L793474
TB-101
Collected date/time: 10/07/15 00:00
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2,4-Trichlorobenzene ND 1.00 1 10/15/2015 14:36 WG821485
1,1,1-Trichloroethane ND 1.00 1 10/15/2015 14:36 WG821485
1,1,2-Trichloroethane ND 1.00 1 10/15/2015 14:36 WG821485
Trichloroethene ND 1.00 1 10/15/2015 14:36 WG821485
Trichlorofluoromethane ND 5.00 1 10/15/2015 14:36 WG821485
1,2,3-Trichloropropane ND 2.50 1 10/15/2015 14:36 WG821485
1,2,4-Trimethylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
1,2,3-Trimethylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
1,3,5-Trimethylbenzene ND 1.00 1 10/15/2015 14:36 WG821485
Vinyl chloride ND 1.00 1 10/15/2015 14:36 WG821485
Xylenes, Total ND 3.00 1 10/15/2015 14:36 WG821485
(S) Toluene-d8 101 90.0-115 10/15/2015 14:36 WG821485
(S) Dibromofluoromethane 99.5 79.0-121 10/15/2015 14:36 WG821485
(S) 4-Bromofluorobenzene 92.9 80.1-120 10/15/2015 14:36 WG821485
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 16 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 16 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 07
L793474
TW-105
Collected date/time: 10/07/15 14:45
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 10/15/2015 19:36 WG821485
Acrolein ND 50.0 1 10/15/2015 19:36 WG821485
Acrylonitrile ND 10.0 1 10/15/2015 19:36 WG821485
Benzene ND 1.00 1 10/15/2015 19:36 WG821485
Bromobenzene ND 1.00 1 10/15/2015 19:36 WG821485
Bromodichloromethane ND 1.00 1 10/15/2015 19:36 WG821485
Bromoform ND 1.00 1 10/15/2015 19:36 WG821485
Bromomethane ND 5.00 1 10/15/2015 19:36 WG821485
n-Butylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
sec-Butylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
tert-Butylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
Carbon tetrachloride ND 1.00 1 10/15/2015 19:36 WG821485
Chlorobenzene ND 1.00 1 10/15/2015 19:36 WG821485
Chlorodibromomethane ND 1.00 1 10/15/2015 19:36 WG821485
Chloroethane ND 5.00 1 10/15/2015 19:36 WG821485
2-Chloroethyl vinyl ether ND J4 50.0 1 10/15/2015 19:36 WG821485
Chloroform ND 5.00 1 10/15/2015 19:36 WG821485
Chloromethane ND 2.50 1 10/15/2015 19:36 WG821485
2-Chlorotoluene ND 1.00 1 10/15/2015 19:36 WG821485
4-Chlorotoluene ND 1.00 1 10/15/2015 19:36 WG821485
1,2-Dibromo-3-Chloropropane ND 5.00 1 10/15/2015 19:36 WG821485
1,2-Dibromoethane ND 1.00 1 10/15/2015 19:36 WG821485
Dibromomethane ND 1.00 1 10/15/2015 19:36 WG821485
1,2-Dichlorobenzene ND 1.00 1 10/15/2015 19:36 WG821485
1,3-Dichlorobenzene ND 1.00 1 10/15/2015 19:36 WG821485
1,4-Dichlorobenzene ND 1.00 1 10/15/2015 19:36 WG821485
Dichlorodifluoromethane ND 5.00 1 10/15/2015 19:36 WG821485
1,1-Dichloroethane ND 1.00 1 10/15/2015 19:36 WG821485
1,2-Dichloroethane ND 1.00 1 10/15/2015 19:36 WG821485
1,1-Dichloroethene ND 1.00 1 10/15/2015 19:36 WG821485
cis-1,2-Dichloroethene ND 1.00 1 10/15/2015 19:36 WG821485
trans-1,2-Dichloroethene ND 1.00 1 10/15/2015 19:36 WG821485
1,2-Dichloropropane ND 1.00 1 10/15/2015 19:36 WG821485
1,1-Dichloropropene ND 1.00 1 10/15/2015 19:36 WG821485
1,3-Dichloropropane ND 1.00 1 10/15/2015 19:36 WG821485
cis-1,3-Dichloropropene ND 1.00 1 10/15/2015 19:36 WG821485
trans-1,3-Dichloropropene ND 1.00 1 10/15/2015 19:36 WG821485
2,2-Dichloropropane ND 1.00 1 10/15/2015 19:36 WG821485
Di-isopropyl ether ND 1.00 1 10/15/2015 19:36 WG821485
Ethylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
Hexachloro-1,3-butadiene ND 1.00 1 10/15/2015 19:36 WG821485
Isopropylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
p-Isopropyltoluene ND 1.00 1 10/15/2015 19:36 WG821485
2-Butanone (MEK)ND 10.0 1 10/15/2015 19:36 WG821485
Methylene Chloride ND 5.00 1 10/15/2015 19:36 WG821485
4-Methyl-2-pentanone (MIBK) ND 10.0 1 10/15/2015 19:36 WG821485
Methyl tert-butyl ether ND 1.00 1 10/15/2015 19:36 WG821485
Naphthalene ND 5.00 1 10/15/2015 19:36 WG821485
n-Propylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
Styrene ND 1.00 1 10/15/2015 19:36 WG821485
1,1,1,2-Tetrachloroethane ND 1.00 1 10/15/2015 19:36 WG821485
1,1,2,2-Tetrachloroethane ND 1.00 1 10/15/2015 19:36 WG821485
1,1,2-Trichlorotrifluoroethane ND 1.00 1 10/15/2015 19:36 WG821485
Tetrachloroethene ND 1.00 1 10/15/2015 19:36 WG821485
Toluene ND 5.00 1 10/15/2015 19:36 WG821485
1,2,3-Trichlorobenzene ND 1.00 1 10/15/2015 19:36 WG821485
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 17 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 17 of 35
ONE LA% NAT,ON:,'ESAM3LE RES8LTS - 07
L793474
TW-105
Collected date/time: 10/07/15 14:45
9olatile OrJanic CompounGs *C/MS by MethoG 8260%
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2,4-Trichlorobenzene ND 1.00 1 10/15/2015 19:36 WG821485
1,1,1-Trichloroethane 14.1 1.00 1 10/15/2015 19:36 WG821485
1,1,2-Trichloroethane ND 1.00 1 10/15/2015 19:36 WG821485
Trichloroethene 3.30 1.00 1 10/15/2015 19:36 WG821485
Trichlorofluoromethane ND 5.00 1 10/15/2015 19:36 WG821485
1,2,3-Trichloropropane ND 2.50 1 10/15/2015 19:36 WG821485
1,2,4-Trimethylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
1,2,3-Trimethylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
1,3,5-Trimethylbenzene ND 1.00 1 10/15/2015 19:36 WG821485
Vinyl chloride ND 1.00 1 10/15/2015 19:36 WG821485
Xylenes, Total ND 3.00 1 10/15/2015 19:36 WG821485
(S) Toluene-d8 103 90.0-115 10/15/2015 19:36 WG821485
(S) Dibromofluoromethane 102 79.0-121 10/15/2015 19:36 WG821485
(S) 4-Bromofluorobenzene 95.3 80.1-120 10/15/2015 19:36 WG821485
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 18 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 18 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-01,02,03,04,05
MethoG %lanN M%
M% 10/12/15 10:03
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Acetone N'00500
Acrolein N'00500
Acrylonitrile N'00100
%en]ene N'000100
%romoben]ene N'000100
%romoGichloromethane N'000100
%romoform N'000100
%romomethane N'000500
n-%utylben]ene N'000100
sec-%utylben]ene N'000100
tert-%utylben]ene N'000100
Carbon tetrachloriGe N'000100
Chloroben]ene N'000100
ChloroGibromomethane N'000100
Chloroethane N'000500
2-Chloroethyl vinyl ether N'00500
Chloroform N'000500
Chloromethane N'000250
2-Chlorotoluene N'000100
4-Chlorotoluene N'000100
1,2-'ibromo-3-Chloropropane N'000500
1,2-'ibromoethane N'000100
'ibromomethane N'000100
1,2-'ichloroben]ene N'000100
1,3-'ichloroben]ene N'000100
1,4-'ichloroben]ene N'000100
'ichloroGifluoromethane N'000500
1,1-'ichloroethane N'000100
1,2-'ichloroethane N'000100
1,1-'ichloroethene N'000100
cis-1,2-'ichloroethene N'000100
trans-1,2-'ichloroethene N'000100
1,2-'ichloropropane N'000100
1,1-'ichloropropene N'000100
1,3-'ichloropropane N'000100
cis-1,3-'ichloropropene N'000100
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 19 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 19 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-01,02,03,04,05
MethoG %lanN M%
M% 10/12/15 10:03
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
trans-1,3-'ichloropropene N'000100
2,2-'ichloropropane N'000100
'i-isopropyl ether N'000100
Ethylben]ene N'000100
He[achloro-1,3-butaGiene N'000100
,sopropylben]ene N'000100
p-,sopropyltoluene N'000100
2-%utanone ME.N'00100
Methylene ChloriGe N'000500
4-Methyl-2-pentanone M,%.N'00100
Methyl tert-butyl ether N'000100
Naphthalene N'000500
n-3ropylben]ene N'000100
Styrene N'000100
1,1,1,2-Tetrachloroethane N'000100
1,1,2,2-Tetrachloroethane N'000100
Tetrachloroethene N'000100
Toluene N'000500
1,1,2-Trichlorotrifluoroethane N'000100
1,2,3-Trichloroben]ene N'000100
1,2,4-Trichloroben]ene N'000100
1,1,1-Trichloroethane N'000100
1,1,2-Trichloroethane N'000100
Trichloroethene N'000100
Trichlorofluoromethane N'000500
1,2,3-Trichloropropane N'000250
1,2,3-Trimethylben]ene N'000100
1,2,4-Trimethylben]ene N'000100
1,3,5-Trimethylben]ene N'000100
9inyl chloriGe N'000100
;ylenes, Total N'000300
(S) Toluene-d8 101 90.0-115
(S) Dibromofluoromethane 96.0 79.0-121
(S) 4-Bromofluorobenzene 100 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 20 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 20 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-01,02,03,04,05
Laboratory Control Sample LCS Ş Laboratory Control Sample 'uplicate LCS'
LCS 10/12/15 08:51 Ş LCS' 10/12/15 09:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % %% %
Acetone 0125 0126 0132 101 106 287-175 513 209
Acrolein 0125 0105 0110 839 881 404-172 491 20
Acrylonitrile 0125 0136 0140 108 112 582-145 325 20
%en]ene 00250 00259 00260 104 104 730-122 0240 20
%romoben]ene 00250 00246 00253 982 101 815-115 301 20
%romoGichloromethane 00250 00245 00247 981 987 755-121 0660 20
%romoform 00250 00266 00285 106 114 715-131 686 20
%romomethane 00250 00276 00273 110 109 224-187 104 20
n-%utylben]ene 00250 00249 00266 995 107 759-134 683 20
sec-%utylben]ene 00250 00242 00258 968 103 806-126 633 20
tert-%utylben]ene 00250 00249 00266 997 107 793-127 665 20
Carbon tetrachloriGe 00250 00273 00271 109 109 709-129 0540 20
Chloroben]ene 00250 00259 00268 104 107 797-122 335 20
ChloroGibromomethane 00250 00254 00272 102 109 782-124 672 20
Chloroethane 00250 00257 00254 103 101 412-153 151 20
2-Chloroethyl vinyl ether 0125 0485 0453 388 363 234-162 E J4 E J4 674 235
Chloroform 00250 00256 00255 102 102 732-125 0290 20
Chloromethane 00250 00253 00249 101 994 558-134 161 20
2-Chlorotoluene 00250 00254 00265 101 106 764-125 440 20
4-Chlorotoluene 00250 00255 00267 102 107 815-121 453 20
1,2-'ibromo-3-Chloropropane 00250 00223 00251 892 100 648-131 117 20
1,2-'ibromoethane 00250 00262 00271 105 108 798-122 326 20
'ibromomethane 00250 00258 00260 103 104 795-118 0650 20
1,2-'ichloroben]ene 00250 00250 00262 100 105 847-118 465 20
1,3-'ichloroben]ene 00250 00249 00266 997 106 776-127 637 20
1,4-'ichloroben]ene 00250 00234 00245 936 981 822-114 466 20
'ichloroGifluoromethane 00250 00239 00240 956 960 560-134 0380 20
1,1-'ichloroethane 00250 00259 00260 104 104 717-127 00800 20
1,2-'ichloroethane 00250 00238 00243 951 971 653-126 200 20
1,1-'ichloroethene 00250 00253 00253 101 101 599-137 0120 20
cis-1,2-'ichloroethene 00250 00265 00267 106 107 773-122 0780 20
trans-1,2-'ichloroethene 00250 00269 00265 107 106 726-125 158 20
1,2-'ichloropropane 00250 00260 00262 104 105 774-125 0630 20
1,1-'ichloropropene 00250 00266 00268 106 107 725-127 0940 20
1,3-'ichloropropane 00250 00247 00255 986 102 806-115 333 20
cis-1,3-'ichloropropene 00250 00269 00273 107 109 777-124 170 20
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 21 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 21 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-01,02,03,04,05
Laboratory Control Sample LCS Ş Laboratory Control Sample 'uplicate LCS'
LCS 10/12/15 08:51 Ş LCS' 10/12/15 09:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % %% %
trans-1,3-'ichloropropene 00250 00259 00266 103 107 735-127 287 20
2,2-'ichloropropane 00250 00263 00261 105 104 613-134 0960 20
'i-isopropyl ether 00250 00269 00262 108 105 651-135 261 20
Ethylben]ene 00250 00263 00270 105 108 809-121 276 20
He[achloro-1,3-butaGiene 00250 00208 00223 831 893 737-133 714 20
,sopropylben]ene 00250 00257 00270 103 108 816-124 492 20
p-,sopropyltoluene 00250 00251 00264 100 106 776-129 538 20
2-%utanone ME.0125 0135 0142 108 113 464-155 501 20
Methylene ChloriGe 00250 00232 00228 926 914 695-120 137 20
4-Methyl-2-pentanone M,%.0125 0110 0117 877 934 633-138 629 20
Methyl tert-butyl ether 00250 00264 00262 105 105 701-125 0760 20
Naphthalene 00250 00276 00279 110 112 697-134 117 20
n-3ropylben]ene 00250 00253 00264 101 105 819-122 399 20
Styrene 00250 00253 00258 101 103 799-124 212 20
1,1,1,2-Tetrachloroethane 00250 00253 00266 101 106 785-125 492 20
1,1,2,2-Tetrachloroethane 00250 00239 00257 956 103 793-123 744 20
Tetrachloroethene 00250 00261 00271 104 108 735-130 385 20
Toluene 00250 00249 00251 997 100 779-116 0590 20
1,1,2-Trichlorotrifluoroethane 00250 00267 00265 107 106 620-141 0800 20
1,2,3-Trichloroben]ene 00250 00225 00245 900 978 757-134 837 20
1,2,4-Trichloroben]ene 00250 00244 00265 975 106 761-136 833 20
1,1,1-Trichloroethane 00250 00260 00259 104 103 711-129 0740 20
1,1,2-Trichloroethane 00250 00246 00260 984 104 816-120 572 20
Trichloroethene 00250 00261 00264 104 106 795-121 148 20
Trichlorofluoromethane 00250 00260 00256 104 102 491-157 178 20
1,2,3-Trichloropropane 00250 00235 00249 940 996 749-124 578 20
1,2,3-Trimethylben]ene 00250 00246 00260 982 104 799-118 554 20
1,2,4-Trimethylben]ene 00250 00255 00268 102 107 790-122 488 20
1,3,5-Trimethylben]ene 00250 00253 00268 101 107 810-123 575 20
9inyl chloriGe 00250 00256 00248 103 994 615-134 320 20
;ylenes, Total 00750 00784 00817 105 109 792-122 406 20
(S) Toluene-d8 101 101 90.0-115
(S) Dibromofluoromethane 99.3 98.2 79.0-121
(S) 4-Bromofluorobenzene 99.7 100 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 22 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 22 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-01,02,03,04,05
L792608-01 OriJinal Sample OS Ş Matri[ SpiNe MS Ş Matri[ SpiNe 'uplicate MS'
OS 10/12/15 11:35 Ş MS 10/12/15 11:53 Ş MS' 10/12/15 12:11
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % %%% %
Acetone 0125 0000613 00491 00484 388 382 1 250-156 155 215
Acrolein 0125 N'00816 00820 653 656 1 340-194 0530 215
Acrylonitrile 0125 N'0121 0124 971 991 1 559-161 206 20
%en]ene 00250 N'00217 00216 866 863 1 586-133 0370 20
%romoben]ene 00250 N'00233 00229 932 915 1 706-125 180 20
%romoGichloromethane 00250 N'00222 00225 890 901 1 692-127 131 20
%romoform 00250 N'00261 00266 104 106 1 663-140 164 20
%romomethane 00250 N'00189 00187 757 749 1 166-183 102 205
n-%utylben]ene 00250 N'00251 00250 100 100 1 648-145 0350 20
sec-%utylben]ene 00250 N'00244 00240 975 962 1 668-139 139 20
tert-%utylben]ene 00250 N'00252 00247 101 986 1 671-138 203 20
Carbon tetrachloriGe 00250 N'00236 00237 944 949 1 606-139 0440 20
Chloroben]ene 00250 N'00242 00237 967 946 1 701-130 220 20
ChloroGibromomethane 00250 N'00248 00246 992 985 1 716-132 0770 20
Chloroethane 00250 N'00195 00196 780 786 1 333-155 0750 20
2-Chloroethyl vinyl ether 0125 N'00197 000666 158 533 1 500-149 J3 989 40
Chloroform 00250 N'00228 00227 912 907 1 661-133 0520 20
Chloromethane 00250 N'00156 00152 624 609 1 407-139 242 20
2-Chlorotoluene 00250 N'00251 00243 100 973 1 669-134 298 20
4-Chlorotoluene 00250 N'00244 00239 976 958 1 668-134 190 20
1,2-'ibromo-3-Chloropropane 00250 N'00228 00235 913 939 1 639-142 284 202
1,2-'ibromoethane 00250 N'00243 00239 972 954 1 738-131 189 20
'ibromomethane 00250 N'00233 00235 932 941 1 728-127 0990 20
1,2-'ichloroben]ene 00250 N'00250 00247 999 987 1 774-127 114 20
1,3-'ichloroben]ene 00250 N'00246 00242 983 969 1 679-136 141 20
1,4-'ichloroben]ene 00250 N'00234 00229 935 915 1 744-123 215 20
'ichloroGifluoromethane 00250 N'00195 00186 782 743 1 422-146 511 20
1,1-'ichloroethane 00250 N'00221 00221 886 883 1 640-134 0270 20
1,2-'ichloroethane 00250 N'00209 00208 836 832 1 607-132 0540 20
1,1-'ichloroethene 00250 N'00200 00198 800 794 1 488-144 0760 20
cis-1,2-'ichloroethene 00250 N'00230 00226 920 904 1 606-136 185 20
trans-1,2-'ichloroethene 00250 N'00210 00208 839 830 1 610-132 109 20
1,2-'ichloropropane 00250 N'00229 00230 917 920 1 697-130 0360 20
1,1-'ichloropropene 00250 N'00214 00217 855 866 1 615-136 133 20
1,3-'ichloropropane 00250 N'00235 00233 939 930 1 743-123 0880 20
cis-1,3-'ichloropropene 00250 N'00234 00235 937 940 1 711-129 0380 20
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 23 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 23 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-01,02,03,04,05
L792608-01 OriJinal Sample OS Ş Matri[ SpiNe MS Ş Matri[ SpiNe 'uplicate MS'
OS 10/12/15 11:35 Ş MS 10/12/15 11:53 Ş MS' 10/12/15 12:11
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % %%% %
trans-1,3-'ichloropropene 00250 N'00234 00234 935 934 1 663-136 00600 20
2,2-'ichloropropane 00250 N'00241 00238 964 952 1 549-142 131 20
'i-isopropyl ether 00250 N'00230 00227 919 910 1 599-140 104 20
Ethylben]ene 00250 N'00243 00240 973 960 1 627-136 135 20
He[achloro-1,3-butaGiene 00250 N'00228 00227 913 907 1 611-144 0680 201
,sopropylben]ene 00250 N'00248 00243 993 973 1 674-136 205 20
p-,sopropyltoluene 00250 N'00249 00249 995 997 1 628-143 0140 20
2-%utanone ME.0125 N'00813 00818 650 654 1 450-156 0620 208
Methylene ChloriGe 00250 N'00190 00190 760 759 1 615-125 0100 20
4-Methyl-2-pentanone M,%.0125 N'0102 0103 814 825 1 607-150 137 20
Methyl tert-butyl ether 00250 N'00236 00233 942 931 1 614-136 122 20
Naphthalene 00250 0000552 00232 00240 906 938 1 618-143 341 20
n-3ropylben]ene 00250 N'00244 00238 975 954 1 632-139 216 20
Styrene 00250 N'00233 00232 933 927 1 682-133 0630 20
1,1,1,2-Tetrachloroethane 00250 N'00250 00247 999 988 1 705-132 109 20
1,1,2,2-Tetrachloroethane 00250 N'00244 00244 976 974 1 649-145 0190 20
Tetrachloroethene 00250 N'00231 00233 923 932 1 574-141 0920 20
Toluene 00250 N'00216 00215 863 859 1 678-124 0390 20
1,1,2-Trichlorotrifluoroethane 00250 N'00234 00235 937 938 1 537-150 0160 20
1,2,3-Trichloroben]ene 00250 N'00227 00232 906 928 1 657-143 231 20
1,2,4-Trichloroben]ene 00250 N'00246 00247 983 989 1 670-146 0590 20
1,1,1-Trichloroethane 00250 N'00229 00229 917 918 1 587-134 0100 20
1,1,2-Trichloroethane 00250 N'00245 00240 980 960 1 741-130 208 20
Trichloroethene 00250 N'00226 00226 902 903 1 489-148 0140 20
Trichlorofluoromethane 00250 N'00213 00212 850 847 1 399-165 0380 20
1,2,3-Trichloropropane 00250 N'00240 00238 961 952 1 715-134 0860 20
1,2,3-Trimethylben]ene 00250 N'00239 00234 958 938 1 627-133 208 20
1,2,4-Trimethylben]ene 00250 N'00242 00239 968 955 1 605-137 139 20
1,3,5-Trimethylben]ene 00250 N'00241 00239 965 957 1 679-134 0830 20
9inyl chloriGe 00250 N'00181 00178 724 713 1 443-143 157 20
;ylenes, Total 00750 N'00726 00712 967 950 1 656-133 182 20
(S) Toluene-d8 100 101 90.0-115
(S) Dibromofluoromethane 96.3 97.6 79.0-121
(S) 4-Bromofluorobenzene 99.6 98.7 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 24 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 24 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-06,07
MethoG %lanN M%
M% 10/15/15 10:59
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
Acetone N'00500
Acrolein N'00500
Acrylonitrile N'00100
%en]ene N'000100
%romoben]ene N'000100
%romoGichloromethane N'000100
%romoform N'000100
%romomethane N'000500
n-%utylben]ene N'000100
sec-%utylben]ene N'000100
tert-%utylben]ene N'000100
Carbon tetrachloriGe N'000100
Chloroben]ene N'000100
ChloroGibromomethane N'000100
Chloroethane N'000500
2-Chloroethyl vinyl ether N'00500
Chloroform N'000500
Chloromethane N'000250
2-Chlorotoluene N'000100
4-Chlorotoluene N'000100
1,2-'ibromo-3-Chloropropane N'000500
1,2-'ibromoethane N'000100
'ibromomethane N'000100
1,2-'ichloroben]ene N'000100
1,3-'ichloroben]ene N'000100
1,4-'ichloroben]ene N'000100
'ichloroGifluoromethane N'000500
1,1-'ichloroethane N'000100
1,2-'ichloroethane N'000100
1,1-'ichloroethene N'000100
cis-1,2-'ichloroethene N'000100
trans-1,2-'ichloroethene N'000100
1,2-'ichloropropane N'000100
1,1-'ichloropropene N'000100
1,3-'ichloropropane N'000100
cis-1,3-'ichloropropene N'000100
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 25 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 25 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-06,07
MethoG %lanN M%
M% 10/15/15 10:59
MB Result MB Qualifier MB RDL
Analyte mg/l mg/l
trans-1,3-'ichloropropene N'000100
2,2-'ichloropropane N'000100
'i-isopropyl ether N'000100
Ethylben]ene N'000100
He[achloro-1,3-butaGiene N'000100
,sopropylben]ene N'000100
p-,sopropyltoluene N'000100
2-%utanone ME.N'00100
Methylene ChloriGe N'000500
4-Methyl-2-pentanone M,%.N'00100
Methyl tert-butyl ether N'000100
Naphthalene N'000500
n-3ropylben]ene N'000100
Tetrachloroethene N'000100
Styrene N'000100
1,1,1,2-Tetrachloroethane N'000100
1,1,2,2-Tetrachloroethane N'000100
Toluene N'000500
1,1,2-Trichlorotrifluoroethane N'000100
Trichloroethene N'000100
1,2,3-Trichloroben]ene N'000100
1,2,4-Trichloroben]ene N'000100
1,1,1-Trichloroethane N'000100
1,1,2-Trichloroethane N'000100
Trichlorofluoromethane N'000500
1,2,3-Trichloropropane N'000250
1,2,3-Trimethylben]ene N'000100
1,2,4-Trimethylben]ene N'000100
1,3,5-Trimethylben]ene N'000100
9inyl chloriGe N'000100
;ylenes, Total N'000300
(S) Toluene-d8 99.9 90.0-115
(S) Dibromofluoromethane 98.5 79.0-121
(S) 4-Bromofluorobenzene 93.3 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 26 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 26 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-06,07
Laboratory Control Sample LCS Ş Laboratory Control Sample 'uplicate LCS'
LCS 10/15/15 09:48 Ş LCS' 10/15/15 10:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % %% %
Acetone 0125 0149 0141 119 113 287-175 570 209
Acrolein 0125 0129 0122 103 975 404-172 533 20
Acrylonitrile 0125 0149 0143 119 114 582-145 449 20
%en]ene 00250 00275 00272 110 109 730-122 101 20
%romoben]ene 00250 00258 00262 103 105 815-115 139 20
%romoGichloromethane 00250 00265 00261 106 104 755-121 137 20
%romoform 00250 00303 00295 121 118 715-131 262 20
%romomethane 00250 00300 00301 120 120 224-187 0490 20
n-%utylben]ene 00250 00273 00275 109 110 759-134 0840 20
sec-%utylben]ene 00250 00265 00268 106 107 806-126 126 20
tert-%utylben]ene 00250 00268 00275 107 110 793-127 251 20
Carbon tetrachloriGe 00250 00288 00280 115 112 709-129 294 20
Chloroben]ene 00250 00269 00273 108 109 797-122 147 20
ChloroGibromomethane 00250 00279 00272 112 109 782-124 260 20
Chloroethane 00250 00283 00279 113 111 412-153 139 20
2-Chloroethyl vinyl ether 0125 0526 0441 421 353 234-162 E J4 E J4 175 235
Chloroform 00250 00270 00267 108 107 732-125 101 20
Chloromethane 00250 00266 00267 106 107 558-134 0340 20
2-Chlorotoluene 00250 00281 00275 112 110 764-125 208 20
4-Chlorotoluene 00250 00269 00272 108 109 815-121 113 20
1,2-'ibromo-3-Chloropropane 00250 00250 00246 999 985 648-131 140 20
1,2-'ibromoethane 00250 00276 00276 110 110 798-122 00200 20
'ibromomethane 00250 00280 00268 112 107 795-118 431 20
1,2-'ichloroben]ene 00250 00267 00273 107 109 847-118 232 20
1,3-'ichloroben]ene 00250 00271 00273 108 109 776-127 0790 20
1,4-'ichloroben]ene 00250 00252 00257 101 103 822-114 221 20
'ichloroGifluoromethane 00250 00252 00251 101 100 560-134 0720 20
1,1-'ichloroethane 00250 00268 00266 107 106 717-127 0710 20
1,2-'ichloroethane 00250 00254 00251 102 101 653-126 105 20
1,1-'ichloroethene 00250 00269 00268 107 107 599-137 00700 20
cis-1,2-'ichloroethene 00250 00278 00277 111 111 773-122 0400 20
trans-1,2-'ichloroethene 00250 00278 00283 111 113 726-125 182 20
1,2-'ichloropropane 00250 00282 00275 113 110 774-125 267 20
1,1-'ichloropropene 00250 00283 00276 113 110 725-127 233 20
1,3-'ichloropropane 00250 00262 00261 105 105 806-115 0130 20
cis-1,3-'ichloropropene 00250 00290 00284 116 114 777-124 208 20
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 27 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 27 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-06,07
Laboratory Control Sample LCS Ş Laboratory Control Sample 'uplicate LCS'
LCS 10/15/15 09:48 Ş LCS' 10/15/15 10:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l % % %% %
trans-1,3-'ichloropropene 00250 00283 00277 113 111 735-127 212 20
2,2-'ichloropropane 00250 00283 00270 113 108 613-134 463 20
'i-isopropyl ether 00250 00272 00269 109 107 651-135 118 20
Ethylben]ene 00250 00276 00275 110 110 809-121 0460 20
He[achloro-1,3-butaGiene 00250 00245 00251 982 100 737-133 206 20
,sopropylben]ene 00250 00276 00271 110 108 816-124 164 20
p-,sopropyltoluene 00250 00274 00276 109 111 776-129 0930 20
2-%utanone ME.0125 0158 0149 126 119 464-155 545 20
Methylene ChloriGe 00250 00243 00240 973 961 695-120 123 20
4-Methyl-2-pentanone M,%.0125 0128 0121 102 971 633-138 497 20
Methyl tert-butyl ether 00250 00266 00270 106 108 701-125 152 20
Naphthalene 00250 00254 00253 102 101 697-134 0390 20
n-3ropylben]ene 00250 00271 00271 108 108 819-122 0120 20
Styrene 00250 00267 00266 107 106 799-124 0230 20
1,1,1,2-Tetrachloroethane 00250 00273 00272 109 109 785-125 0220 20
Tetrachloroethene 00250 00289 00281 116 112 735-130 276 20
1,1,2,2-Tetrachloroethane 00250 00270 00263 108 105 793-123 261 20
Toluene 00250 00270 00263 108 105 779-116 243 20
1,1,2-Trichlorotrifluoroethane 00250 00285 00287 114 115 620-141 0370 20
1,2,3-Trichloroben]ene 00250 00254 00253 102 101 757-134 0450 20
1,2,4-Trichloroben]ene 00250 00268 00271 107 109 761-136 140 20
1,1,1-Trichloroethane 00250 00271 00266 108 107 711-129 182 20
Trichloroethene 00250 00283 00282 113 113 795-121 0580 20
1,1,2-Trichloroethane 00250 00269 00264 108 105 816-120 205 20
Trichlorofluoromethane 00250 00291 00275 116 110 491-157 556 20
1,2,3-Trichloropropane 00250 00273 00255 109 102 749-124 666 20
1,2,3-Trimethylben]ene 00250 00261 00264 104 106 799-118 111 20
1,2,4-Trimethylben]ene 00250 00267 00271 107 108 790-122 122 20
1,3,5-Trimethylben]ene 00250 00272 00274 109 110 810-123 104 20
9inyl chloriGe 00250 00271 00269 108 108 615-134 0770 20
;ylenes, Total 00750 00827 00831 110 111 792-122 0450 20
(S) Toluene-d8 101 99.7 90.0-115
(S) Dibromofluoromethane 97.3 98.3 79.0-121
(S) 4-Bromofluorobenzene 95.9 97.4 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 28 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 28 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-06,07
L793700-02 OriJinal Sample OS Ş Matri[ SpiNe MS Ş Matri[ SpiNe 'uplicate MS'
OS 10/15/15 16:57 Ş MS 10/15/15 13:43 Ş MS' 10/15/15 14:01
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % %%% %
Acetone 0125 000774 00639 00627 450 440 1 250-156 194 215
Acrolein 0125 N'00962 00965 770 772 1 340-194 0280 215
Acrylonitrile 0125 N'0140 0140 112 112 1 559-161 0170 20
%en]ene 00250 N'00239 00246 956 983 1 586-133 279 20
%romoben]ene 00250 N'00239 00240 955 959 1 706-125 0480 20
%romoGichloromethane 00250 N'00237 00241 947 963 1 692-127 162 20
%romoform 00250 N'00269 00277 108 111 1 663-140 288 20
%romomethane 00250 N'00243 00242 974 966 1 166-183 0780 205
n-%utylben]ene 00250 N'00253 00261 101 104 1 648-145 306 20
sec-%utylben]ene 00250 N'00252 00257 101 103 1 668-139 215 20
tert-%utylben]ene 00250 N'00259 00262 103 105 1 671-138 134 20
Carbon tetrachloriGe 00250 N'00259 00269 103 108 1 606-139 388 20
Chloroben]ene 00250 N'00247 00254 986 102 1 701-130 291 20
ChloroGibromomethane 00250 N'00249 00256 995 102 1 716-132 272 20
Chloroethane 00250 N'00236 00237 944 947 1 333-155 0370 20
2-Chloroethyl vinyl ether 0125 N'00122 00131 980 105 1 500-149 653 40
Chloroform 00250 N'00243 00246 971 985 1 661-133 144 20
Chloromethane 00250 N'00201 00207 805 829 1 407-139 292 20
2-Chlorotoluene 00250 N'00252 00259 101 104 1 669-134 272 20
4-Chlorotoluene 00250 N'00247 00251 989 100 1 668-134 153 20
1,2-'ibromo-3-Chloropropane 00250 N'00241 00250 964 100 1 639-142 378 202
1,2-'ibromoethane 00250 N'00247 00257 988 103 1 738-131 412 20
'ibromomethane 00250 N'00241 00253 966 101 1 728-127 477 20
1,2-'ichloroben]ene 00250 N'00247 00252 989 101 1 774-127 200 20
1,3-'ichloroben]ene 00250 N'00252 00253 101 101 1 679-136 0570 20
1,4-'ichloroben]ene 00250 N'00230 00239 922 957 1 744-123 377 20
'ichloroGifluoromethane 00250 N'00207 00213 829 850 1 422-146 258 20
1,1-'ichloroethane 00250 N'00243 00249 971 997 1 640-134 261 20
1,2-'ichloroethane 00250 N'00222 00229 889 917 1 607-132 300 20
1,1-'ichloroethene 00250 N'00231 00240 922 959 1 488-144 387 20
cis-1,2-'ichloroethene 00250 000120 00259 00265 988 101 1 606-136 208 20
trans-1,2-'ichloroethene 00250 N'00237 00237 949 949 1 610-132 0000 20
1,2-'ichloropropane 00250 N'00252 00257 101 103 1 697-130 213 20
1,1-'ichloropropene 00250 N'00246 00251 983 100 1 615-136 206 20
1,3-'ichloropropane 00250 N'00239 00247 957 989 1 743-123 331 20
cis-1,3-'ichloropropene 00250 N'00245 00254 978 102 1 711-129 395 20
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 29 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 29 of 35
ONE LA% NAT,ON:,'E48AL,T< CONTROL S8MMAR<:G
9RODWLOHOUJDQLFCRPSRXQGVGC/MSE\MHWKRG%L793474-06,07
L793700-02 OriJinal Sample OS Ş Matri[ SpiNe MS Ş Matri[ SpiNe 'uplicate MS'
OS 10/15/15 16:57 Ş MS 10/15/15 13:43 Ş MS' 10/15/15 14:01
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l % %%% %
trans-1,3-'ichloropropene 00250 N'00243 00253 971 101 1 663-136 406 20
2,2-'ichloropropane 00250 N'00261 00267 104 107 1 549-142 233 20
'i-isopropyl ether 00250 N'00242 00252 968 101 1 599-140 391 20
Ethylben]ene 00250 N'00250 00259 100 103 1 627-136 334 20
He[achloro-1,3-butaGiene 00250 N'00235 00241 941 963 1 611-144 227 201
,sopropylben]ene 00250 N'00254 00258 101 103 1 674-136 178 20
p-,sopropyltoluene 00250 N'00257 00260 103 104 1 628-143 128 20
2-%utanone ME.0125 N'00926 00933 741 747 1 450-156 0780 208
Methylene ChloriGe 00250 N'00209 00216 835 865 1 615-125 356 20
4-Methyl-2-pentanone M,%.0125 N'0114 0115 908 917 1 607-150 0950 20
Methyl tert-butyl ether 00250 N'00238 00245 954 982 1 614-136 287 20
Naphthalene 00250 N'00238 00244 951 975 1 618-143 246 20
n-3ropylben]ene 00250 N'00249 00254 996 101 1 632-139 185 20
Styrene 00250 N'00238 00243 951 971 1 682-133 209 20
1,1,1,2-Tetrachloroethane 00250 N'00251 00260 100 104 1 705-132 352 20
Tetrachloroethene 00250 N'00250 00257 100 103 1 574-141 249 20
1,1,2,2-Tetrachloroethane 00250 N'00256 00253 103 101 1 649-145 146 20
Toluene 00250 N'00234 00241 935 962 1 678-124 286 20
1,1,2-Trichlorotrifluoroethane 00250 N'00263 00267 105 107 1 537-150 156 20
1,2,3-Trichloroben]ene 00250 N'00233 00242 932 968 1 657-143 386 20
1,2,4-Trichloroben]ene 00250 N'00244 00250 977 100 1 670-146 228 20
1,1,1-Trichloroethane 00250 N'00244 00252 976 101 1 587-134 329 20
Trichloroethene 00250 N'00246 00257 984 103 1 489-148 428 20
1,1,2-Trichloroethane 00250 N'00243 00253 971 101 1 741-130 406 20
Trichlorofluoromethane 00250 N'00252 00250 101 100 1 399-165 0620 20
1,2,3-Trichloropropane 00250 N'00241 00246 963 984 1 715-134 215 20
1,2,3-Trimethylben]ene 00250 N'00241 00247 964 989 1 627-133 257 20
1,2,4-Trimethylben]ene 00250 N'00247 00252 990 101 1 605-137 185 20
1,3,5-Trimethylben]ene 00250 N'00250 00257 100 103 1 679-134 260 20
9inyl chloriGe 00250 N'00221 00226 883 903 1 443-143 227 20
;ylenes, Total 00750 N'00750 00772 100 103 1 656-133 283 20
(S) Toluene-d8 101 100 90.0-115
(S) Dibromofluoromethane 98.8 97.8 79.0-121
(S) 4-Bromofluorobenzene 96.0 97.4 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 30 of 35
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 30 of 35
ONE LA% NAT,ON:,'E*LOSSAR< O) TERMS
Abbreviations anG 'efinitions
S'*Sample Delivery Group.
M'L Method Detection Limit.
R'L Reported Detection Limit.
N',8 Not detected at the Reporting Limit (or MDL where applicable).
R3'Relative Percent Difference.
GryResults are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
OriJinal Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
SSurrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
RecRecovery.
S'L Sample Detection Limit.
M4L Method Quantitation Limit.
8naGM M4L Unadjusted Method Quantitation Limit.
4ualifier 'escription
E The analyte concentration exceeds the upper limit of the calibration range of the instrument
established by the initial calibration (ICAL).
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 31 of 35
ONE LA% NAT,ON:,'EACCRE',TAT,ONS LOCAT,ONS
1 Cp
2Tc
3Ss
4Cn
5Sr
64c
7*l
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:28 32 of 35
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ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support oces, please
contact our main oce. ESC Lab Sciences performs all testing at our central laboratory.
1. Drinking Water 2. Underground Storage Tanks 3. Aquatic Toxicity 4. Chemical/Microbiological 5. Mold n/a Accreditation not applicable
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AMEC - Asheville, NC 6252-15-0214 L793474 10/16/15 09:34 32 of 35

2655 Park Center Dr., Suite A
Simi Valley, CA 93065
T: [phone]
F: [phone]
www.alsglobal.com

RIGHT SOLUTIONS | RIGHT PARTNER
LABORATORY REPORT
October 16, 2015

Rodney Clark
AMEC Foster Wheeler Environment & Infrastructure Inc.
1308-C Patton Ave
Asheville, NC 28806-2604

RE: Ashville Tannery/Day's Tobacco Warehouse Property

Dear Rodney:

Enclosed are the results of the samples submitted to our laboratory on October 8, 2015. For your
reference, these analyses have been assigned our service request number P1504255.

All analyses were performed according to our laboratory’s NELAP and DoD-ELAP-approved quality
assurance program. The test results meet requirements of the current NELAP and DoD-ELAP
standards, where applicable, and except as noted in the laboratory case narrative provided. For a
specific list of NELAP and DoD-ELAP-accredited analytes, refer to the certifications section at
www.alsglobal.com. Results are intended to be considered in their entirety and apply only to the
samples analyzed and reported herein.
If you have any questions, please call me at [phone].

Respectfully submitted,
ALS | Environmental
For Kate Aguilera
Project Manager
1 of 31

2655 Park Center Dr., Suite A
Simi Valley, CA 93065
T: [phone]
F: [phone]
www.alsglobal.com

RIGHT SOLUTIONS | RIGHT PARTNER

Client: AMEC Foster Wheeler Environment & Infrastructure Inc. Service Request No: P1504255
Project: Ashville Tannery/Day's Tobacco Warehouse Property _______________________________________________________________________________
CASE NARRATIVE

The samples were received intact under chain of custody on October 8, 2015 and were stored in
accordance with the analytical method requirements. Please refer to the sample acceptance check
form for additional information. The results reported herein are applicable only to the condition of
the samples at the time of sample receipt.

Volatile Organic Compound Analysis
The samples were analyzed for volatile organic compounds in accordance with EPA Method TO-
15 from the Compendium of Methods for the Determination of Toxic Organic Compounds in
Ambient Air, Second Edition (EPA/625/R-96/010b), January, 1999. This procedure is described
in laboratory SOP VOA-TO15. The analytical system was comprised of a gas chromatograph /
mass spectrometer (GC/MS) interfaced to a whole-air preconcentrator. This method is included
on the laboratory’s NELAP and DoD-ELAP scope of accreditation, however it is not part of the
AIHA-LAP accreditation. Any analytes flagged with an X are not included on the NELAP or DoD-
ELAP accreditation.

The spike recovery of 1,4-Dioxane for the Laboratory Control Sample (LCS) analyzed on October
14, 2015 was outside the laboratory generated control criterion. The recovery error equates to
a potential high bias. However, the spike recovery of the analytes in question was within the
method criteria; therefore, the data quality has not been significantly affected. No corrective
action was taken.

The canisters were cleaned, prior to sampling, down to the method reporting limit (MRL)
reported for this project. Please note, projects which require reporting below the MRL could
have results between the MRL and method detection limit (MDL) that are biased high. ______________________________________________________________________________________
The results of analyses are given in the attached laboratory report. All results are intended to be considered in their
entirety, and ALS Environmental (ALS) is not responsible for utilization of less than the complete report.

Use of ALS Environmental (ALS)’s Name. Client shall not use ALS’s name or trademark in any marketing or reporting
materials, press releases or in any other manner (“Materials”) whatsoever and shall not attribute to ALS any test result,
tolerance or specification derived from ALS’s data (“Attribution”) without ALS’s prior written consent, which may be withheld
by ALS for any reason in its sole discretion. To request ALS’s consent, Client shall provide copies of the proposed Materials or Attribution and describe in writing Client’s proposed use of such Materials or Attribution. If ALS has not provided written
approval of the Materials or Attribution within ten (10) days of receipt from Client, Client’s request to use ALS’s name or
trademark in any Materials or Attribution shall be deemed denied. ALS may, in its discretion, reasonably charge Client for
its time in reviewing Materials or Attribution requests. Client acknowledges and agrees that the unauthorized use of ALS’s
name or trademark may cause ALS to incur irreparable harm for which the recovery of money damages will be inadequate.
Accordingly, Client acknowledges and agrees that a violation shall justify preliminary injunctive relief. For questions contact
the laboratory.

2 of 31

2655 Park Center Dr., Suite A
Simi Valley, CA 93065
T: [phone]
F: [phone]
www.alsglobal.com

RIGHT SOLUTIONS | RIGHT PARTNER
ALS Environmental – Simi Valley
CERTIFICATIONS, ACCREDITATIONS, AND REGISTRATIONS
Agency Web Site Number
AIHA http://www.aihaaccreditedlabs.org 101661
Arizona DHS http://www.azdhs.gov/lab/license/env.htm AZ0694
DoD ELAP http://www.pjlabs.com/search-accredited-labs L14-2-R1
Florida DOH
(NELAP) http://www.doh.state.fl.us/lab/EnvLabCert/WaterCert.htm E871020
Maine DHHS http://www.maine.gov/dhhs/mecdc/environmental-health/water/dwp-
services/labcert/labcert.htm 2014025
Minnesota DOH
(NELAP) http://www.health.state.mn.us/accreditation 876241
New Jersey DEP
(NELAP) http://www.nj.gov/dep/oqa/CA009
New York DOH
(NELAP) http://www.wadsworth.org/labcert/elap/elap.html 11221
Oregon PHD
(NELAP)
http://public.health.oregon.gov/LaboratoryServices/EnvironmentalLaborat
oryAccreditation/Pages/index.aspx 4068-001
Pennsylvania DEP http://www.depweb.state.pa.us/labs 68-03307
(Registration)
Texas CEQ
(NELAP) http://www.tceq.texas.gov/field/qa/env_lab_accreditation.html T104704413-
15-6
Utah DOH
(NELAP) http://www.health.utah.gov/lab/labimp/certification/index.html CA01627201
5-5
Washington DOE http://www.ecy.wa.gov/programs/eap/labs/lab-accreditation.html C946
Analyses were performed according to our laboratory’s NELAP and DoD-ELAP approved quality assurance
program. A complete listing of specific NELAP and DoD-ELAP certified analytes can be found in the
certifications section at www.alsglobal.com, or at the accreditation body’s website.
Each of the certifications listed above have an explicit Scope of Accreditation that applies to specific
matrices/methods/analytes; therefore, please contact the laboratory for information corresponding to a
particular certification.
3 of 31
P1504255_Detail Summary_1510161638_RG.xls - DETAIL SUMMARY
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.Service Request:P1504255
Project ID:Ashville Tannery/Day's Tobacco Warehouse Property
Date Received:10/8/2015
Time Received:09:40
Client Sample ID Lab Code Matrix
Date
Collected
Time
Collected
Container
ID
Pi1
(psig)
Pf1
(psig)
SG-1 P1504255-001 Air 10/1/2015 11:45 1SC01139 -2.51 5.32 X
SG-2 P1504255-002 Air 10/1/2015 13:15 1SC00522 -1.07 5.18 X
SG-3 P1504255-003 Air 10/1/2015 16:18 1SC00726 -2.55 5.37 X
SG-4 P1504255-004 Air 10/1/2015 16:58 1SC00621 -2.58 5.12 X
FD-1 P1504255-005 Air 10/1/2015 00:00 1SC00603 -2.95 5.94 X
TB-1 P1504255-006 Air 10/1/2015 00:00 1SC00999 -13.68 5.74 X
ALS ENVIRONMENTAL
DETAIL SUMMARY REPORT
TO
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1
5

-

V
O
C

C
a
n
s
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5

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f

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1
10/16/15 4:47 PMP1504255_AMEC Foster Wheeler Environment Infrastructure Inc._Ashville Tannery_Days's Tobacco Warehouse Property.xls - Page 1 of 1
ALS Environmental
Sample Acceptance Check Form
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.Work order:P1504255
Project:Ashville Tannery/Days's Tobacco Warehouse Property
Sample(s) received on:10/8/15 Date opened:10/8/15 by:ADAVID
Note: This form is used for all samples received by ALS. The use of this form for custody seals is strictly meant to indicate presence/absence and not as an indication of
compliance or nonconformity. Thermal preservation and pH will only be evaluated either at the request of the client and/or as required by the method/SOP.Yes No N/A
1 Were sample containers properly marked with client sample ID?
2 Did sample containers arrive in good condition?
3 Were chain-of-custody papers used and filled out?
4 Did sample container labels and/or tags agree with custody papers?
5 Was sample volume received adequate for analysis?
6 Are samples within specified holding times?
7 Was proper temperature (thermal preservation) of cooler at receipt adhered to?
8 Were custody seals on outside of cooler/Box/Container?
Location of seal(s)?Top of the box.Sealing Lid?
Were signature and date included?
Were seals intact?
9 
Is there a client indication that the submitted samples are pH preserved?
Were VOA vials checked for presence/absence of air bubbles?

10 Tubes: Are the tubes capped and intact?
11 Badges: Are the badges properly capped and intact?
Are dual bed badges separated and individually capped and intact?
Lab Sample ID Container Required Received Adjusted VOA Headspace
Description pH *pH pH (Presence/Absence)Comments
1.0 L Source Can
1.0 L Source Can
1.0 L Source Can
1.0 L Source Can
1.0 L Source Can
1.0 L Source Can
RSK - MEEPP, HCL (pH<2); RSK - CO2, (pH 5-8); Sulfur (pH>4)
P1504255-005.01
P1504255-006.01
Do containers have appropriate preservation, according to method/SOP or Client specified information?
Does the client/method/SOP require that the analyst check the sample pH and if necessary alter it?
Receipt / Preservation
P1504255-001.01
P1504255-002.01
P1504255-003.01
P1504255-004.01
Explain any discrepancies: (include lab sample ID numbers):
6 of 31
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ALS ENVIRONMENTAL

RESULTS OF ANALYSIS
Page 1 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-001
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC01139
Initial Pressure (psig):-2.51 Final Pressure (psig):5.32
Canister Dilution Factor:1.64

CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
115-07-1 Propene 4.8 2.1 2.8 1.2
75-71-8 Dichlorodifluoromethane (CFC 12)2.3 2.1 0.46 0.41
74-87-3 Chloromethane ND 2.1 ND 0.99
76-14-2 1,2-Dichloro-1,1,2,2-
tetrafluoroethane (CFC 114)ND 2.1 ND 0.29
75-01-4 Vinyl Chloride ND 2.1 ND 0.80
106-99-0 1,3-Butadiene ND 2.1 ND 0.93
74-83-9 Bromomethane ND 2.1 ND 0.53
75-00-3 Chloroethane ND 2.1 ND 0.78
64-17-5 Ethanol 26 21 14 11
75-05-8 Acetonitrile 6.1 2.1 3.6 1.2
107-02-8 Acrolein ND 8.2 ND 3.6
67-64-1 Acetone 140 21 57 8.6
75-69-4 Trichlorofluoromethane ND 2.1 ND 0.36
67-63-0 2-Propanol (Isopropyl Alcohol)ND 21 ND 8.3
107-13-1 Acrylonitrile ND 2.1 ND 0.95
75-35-4 1,1-Dichloroethene ND 2.1 ND 0.52
75-09-2 Methylene Chloride ND 2.1 ND 0.59
107-05-1 3-Chloro-1-propene (Allyl Chloride)ND 2.1 ND 0.66
76-13-1 Trichlorotrifluoroethane ND 2.1 ND 0.27
75-15-0 Carbon Disulfide ND 21 ND 6.6
156-60-5 trans-1,2-Dichloroethene ND 2.1 ND 0.52
75-34-3 1,1-Dichloroethane ND 2.1 ND 0.51
1634-04-4 Methyl tert-Butyl Ether ND 2.1 ND 0.57
108-05-4 Vinyl Acetate ND 21 ND 5.8
78-93-3 2-Butanone (MEK)ND 21 ND 7.0
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result
ppbV
Result
µg/m³
7 of 31
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ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 2 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-001
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC01139
Initial Pressure (psig):-2.51 Final Pressure (psig):5.32
Canister Dilution Factor:1.64
CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
156-59-2 cis-1,2-Dichloroethene ND 2.1 ND 0.52
141-78-6 Ethyl Acetate 5.0 4.1 1.4 1.1
110-54-3 n-Hexane 31 2.1 8.8 0.58
67-66-3 Chloroform ND 2.1 ND 0.42
109-99-9 Tetrahydrofuran (THF)ND 2.1 ND 0.70
107-06-2 1,2-Dichloroethane ND 2.1 ND 0.51
71-55-6 1,1,1-Trichloroethane 16 2.1 3.0 0.38
71-43-2 Benzene 150 2.1 47 0.64
56-23-5 Carbon Tetrachloride ND 2.1 ND 0.33
110-82-7 Cyclohexane 83 4.1 24 1.2
78-87-5 1,2-Dichloropropane ND 2.1 ND 0.44
75-27-4 Bromodichloromethane ND 2.1 ND 0.31
79-01-6 Trichloroethene ND 2.1 ND 0.38
123-91-1 1,4-Dioxane ND 2.1 ND 0.57
80-62-6 Methyl Methacrylate ND 4.1 ND 1.0
142-82-5 n-Heptane 34 2.1 8.2 0.50
10061-01-5 cis-1,3-Dichloropropene ND 2.1 ND 0.45
108-10-1 4-Methyl-2-pentanone ND 2.1 ND 0.50
10061-02-6 trans-1,3-Dichloropropene ND 2.1 ND 0.45
79-00-5 1,1,2-Trichloroethane ND 2.1 ND 0.38
108-88-3 Toluene 81 2.1 21 0.54
591-78-6 2-Hexanone ND 2.1 ND 0.50
124-48-1 Dibromochloromethane ND 2.1 ND 0.24
106-93-4 1,2-Dibromoethane ND 2.1 ND 0.27
123-86-4 n-Butyl Acetate ND 2.1 ND 0.43
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
ppbV

Result
µg/m³
Result
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ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 3 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-001
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC01139
Initial Pressure (psig):-2.51 Final Pressure (psig):5.32
Canister Dilution Factor:1.64
MRL MRL Data
CAS #Compound µg/m³ ppbV Qualifier
111-65-9 n-Octane 20 2.1 4.3 0.44
127-18-4 Tetrachloroethene 44 2.1 6.5 0.30
108-90-7 Chlorobenzene ND 2.1 ND 0.45
100-41-4 Ethylbenzene 9.3 2.1 2.1 0.47
179601-23-1 m,p-Xylenes 56 4.1 13 0.94
75-25-2 Bromoform ND 2.1 ND 0.20
100-42-5 Styrene ND 2.1 ND 0.48
95-47-6 o-Xylene 9.1 2.1 2.1 0.47
111-84-2 n-Nonane 9.5 2.1 1.8 0.39
79-34-5 1,1,2,2-Tetrachloroethane ND 2.1 ND 0.30
98-82-8 Cumene ND 2.1 ND 0.42
80-56-8 alpha-Pinene 7.5 2.1 1.4 0.37
103-65-1 n-Propylbenzene ND 2.1 ND 0.42
622-96-8 4-Ethyltoluene ND 2.1 ND 0.42
108-67-8 1,3,5-Trimethylbenzene ND 2.1 ND 0.42
95-63-6 1,2,4-Trimethylbenzene ND 2.1 ND 0.42
100-44-7 Benzyl Chloride ND 2.1 ND 0.40
541-73-1 1,3-Dichlorobenzene ND 2.1 ND 0.34
106-46-7 1,4-Dichlorobenzene ND 2.1 ND 0.34
95-50-1 1,2-Dichlorobenzene ND 2.1 ND 0.34
5989-27-5 d-Limonene 3.9 2.1 0.70 0.37
96-12-8 1,2-Dibromo-3-chloropropane ND 2.1 ND 0.21
120-82-1 1,2,4-Trichlorobenzene ND 2.1 ND 0.28
91-20-3 Naphthalene ND 2.1 ND 0.39
87-68-3 Hexachlorobutadiene ND 2.1 ND 0.19
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

ResultResult
Client Sample ID:
Client Project ID:
ppbV

µg/m³
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ALS ENVIRONMENTAL

RESULTS OF ANALYSIS
Page 1 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-2 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-002
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00522
Initial Pressure (psig):-1.07 Final Pressure (psig):5.18
Canister Dilution Factor:1.46

CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
115-07-1 Propene 3.5 1.8 2.0 1.1
75-71-8 Dichlorodifluoromethane (CFC 12)2.3 1.8 0.46 0.37
74-87-3 Chloromethane ND 1.8 ND 0.88
76-14-2 1,2-Dichloro-1,1,2,2-
tetrafluoroethane (CFC 114)ND 1.8 ND 0.26
75-01-4 Vinyl Chloride ND 1.8 ND 0.71
106-99-0 1,3-Butadiene ND 1.8 ND 0.83
74-83-9 Bromomethane ND 1.8 ND 0.47
75-00-3 Chloroethane ND 1.8 ND 0.69
64-17-5 Ethanol 72 18 38 9.7
75-05-8 Acetonitrile ND 1.8 ND 1.1
107-02-8 Acrolein ND 7.3 ND 3.2
67-64-1 Acetone 34 18 14 7.7
75-69-4 Trichlorofluoromethane ND 1.8 ND 0.32
67-63-0 2-Propanol (Isopropyl Alcohol)ND 18 ND 7.4
107-13-1 Acrylonitrile ND 1.8 ND 0.84
75-35-4 1,1-Dichloroethene ND 1.8 ND 0.46
75-09-2 Methylene Chloride ND 1.8 ND 0.53
107-05-1 3-Chloro-1-propene (Allyl Chloride)ND 1.8 ND 0.58
76-13-1 Trichlorotrifluoroethane ND 1.8 ND 0.24
75-15-0 Carbon Disulfide 21 18 6.8 5.9
156-60-5 trans-1,2-Dichloroethene ND 1.8 ND 0.46
75-34-3 1,1-Dichloroethane ND 1.8 ND 0.45
1634-04-4 Methyl tert-Butyl Ether ND 1.8 ND 0.51
108-05-4 Vinyl Acetate ND 18 ND 5.2
78-93-3 2-Butanone (MEK)ND 18 ND 6.2
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
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RESULTS OF ANALYSIS
Page 2 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-2 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-002
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00522
Initial Pressure (psig):-1.07 Final Pressure (psig):5.18
Canister Dilution Factor:1.46
CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
156-59-2 cis-1,2-Dichloroethene ND 1.8 ND 0.46
141-78-6 Ethyl Acetate 4.3 3.7 1.2 1.0
110-54-3 n-Hexane 18 1.8 5.1 0.52
67-66-3 Chloroform ND 1.8 ND 0.37
109-99-9 Tetrahydrofuran (THF)1.9 1.8 0.65 0.62
107-06-2 1,2-Dichloroethane ND 1.8 ND 0.45
71-55-6 1,1,1-Trichloroethane 14 1.8 2.6 0.33
71-43-2 Benzene 6.3 1.8 2.0 0.57
56-23-5 Carbon Tetrachloride ND 1.8 ND 0.29
110-82-7 Cyclohexane 81 3.7 24 1.1
78-87-5 1,2-Dichloropropane ND 1.8 ND 0.40
75-27-4 Bromodichloromethane ND 1.8 ND 0.27
79-01-6 Trichloroethene 17 1.8 3.1 0.34
123-91-1 1,4-Dioxane 1.8 1.8 0.51 0.51
80-62-6 Methyl Methacrylate ND 3.7 ND 0.89
142-82-5 n-Heptane 8.1 1.8 2.0 0.45
10061-01-5 cis-1,3-Dichloropropene ND 1.8 ND 0.40
108-10-1 4-Methyl-2-pentanone ND 1.8 ND 0.45
10061-02-6 trans-1,3-Dichloropropene ND 1.8 ND 0.40
79-00-5 1,1,2-Trichloroethane ND 1.8 ND 0.33
108-88-3 Toluene 8.3 1.8 2.2 0.48
591-78-6 2-Hexanone ND 1.8 ND 0.45
124-48-1 Dibromochloromethane ND 1.8 ND 0.21
106-93-4 1,2-Dibromoethane ND 1.8 ND 0.24
123-86-4 n-Butyl Acetate ND 1.8 ND 0.38
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
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ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 3 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-2 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-002
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00522
Initial Pressure (psig):-1.07 Final Pressure (psig):5.18
Canister Dilution Factor:1.46
MRL MRL Data
CAS #Compound µg/m³ ppbV Qualifier
111-65-9 n-Octane 3.7 1.8 0.80 0.39
127-18-4 Tetrachloroethene 15 1.8 2.2 0.27
108-90-7 Chlorobenzene ND 1.8 ND 0.40
100-41-4 Ethylbenzene ND 1.8 ND 0.42
179601-23-1 m,p-Xylenes ND 3.7 ND 0.84
75-25-2 Bromoform ND 1.8 ND 0.18
100-42-5 Styrene ND 1.8 ND 0.43
95-47-6 o-Xylene ND 1.8 ND 0.42
111-84-2 n-Nonane ND 1.8 ND 0.35
79-34-5 1,1,2,2-Tetrachloroethane ND 1.8 ND 0.27
98-82-8 Cumene ND 1.8 ND 0.37
80-56-8 alpha-Pinene 7.9 1.8 1.4 0.33
103-65-1 n-Propylbenzene ND 1.8 ND 0.37
622-96-8 4-Ethyltoluene ND 1.8 ND 0.37
108-67-8 1,3,5-Trimethylbenzene ND 1.8 ND 0.37
95-63-6 1,2,4-Trimethylbenzene ND 1.8 ND 0.37
100-44-7 Benzyl Chloride ND 1.8 ND 0.35
541-73-1 1,3-Dichlorobenzene ND 1.8 ND 0.30
106-46-7 1,4-Dichlorobenzene ND 1.8 ND 0.30
95-50-1 1,2-Dichlorobenzene ND 1.8 ND 0.30
5989-27-5 d-Limonene 2.5 1.8 0.44 0.33
96-12-8 1,2-Dibromo-3-chloropropane ND 1.8 ND 0.19
120-82-1 1,2,4-Trichlorobenzene ND 1.8 ND 0.25
91-20-3 Naphthalene ND 1.8 ND 0.35
87-68-3 Hexachlorobutadiene ND 1.8 ND 0.17
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
12 of 31
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ALS ENVIRONMENTAL

RESULTS OF ANALYSIS
Page 1 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-3 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-003
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00726
Initial Pressure (psig):-2.55 Final Pressure (psig):5.37
Canister Dilution Factor:1.65

CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
115-07-1 Propene 35 2.1 21 1.2
75-71-8 Dichlorodifluoromethane (CFC 12)2.3 2.1 0.46 0.42
74-87-3 Chloromethane ND 2.1 ND 1.0
76-14-2 1,2-Dichloro-1,1,2,2-
tetrafluoroethane (CFC 114)ND 2.1 ND 0.30
75-01-4 Vinyl Chloride ND 2.1 ND 0.81
106-99-0 1,3-Butadiene 4.0 2.1 1.8 0.93
74-83-9 Bromomethane ND 2.1 ND 0.53
75-00-3 Chloroethane ND 2.1 ND 0.78
64-17-5 Ethanol 31 21 16 11
75-05-8 Acetonitrile 2.3 2.1 1.4 1.2
107-02-8 Acrolein ND 8.3 ND 3.6
67-64-1 Acetone 77 21 32 8.7
75-69-4 Trichlorofluoromethane ND 2.1 ND 0.37
67-63-0 2-Propanol (Isopropyl Alcohol)ND 21 ND 8.4
107-13-1 Acrylonitrile ND 2.1 ND 0.95
75-35-4 1,1-Dichloroethene ND 2.1 ND 0.52
75-09-2 Methylene Chloride ND 2.1 ND 0.59
107-05-1 3-Chloro-1-propene (Allyl Chloride)ND 2.1 ND 0.66
76-13-1 Trichlorotrifluoroethane ND 2.1 ND 0.27
75-15-0 Carbon Disulfide ND 21 ND 6.6
156-60-5 trans-1,2-Dichloroethene ND 2.1 ND 0.52
75-34-3 1,1-Dichloroethane ND 2.1 ND 0.51
1634-04-4 Methyl tert-Butyl Ether ND 2.1 ND 0.57
108-05-4 Vinyl Acetate ND 21 ND 5.9
78-93-3 2-Butanone (MEK)ND 21 ND 7.0
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
13 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - Sample (3)
ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 2 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-3 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-003
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00726
Initial Pressure (psig):-2.55 Final Pressure (psig):5.37
Canister Dilution Factor:1.65
CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
156-59-2 cis-1,2-Dichloroethene ND 2.1 ND 0.52
141-78-6 Ethyl Acetate ND 4.1 ND 1.1
110-54-3 n-Hexane ND 2.1 ND 0.59
67-66-3 Chloroform ND 2.1 ND 0.42
109-99-9 Tetrahydrofuran (THF)ND 2.1 ND 0.70
107-06-2 1,2-Dichloroethane ND 2.1 ND 0.51
71-55-6 1,1,1-Trichloroethane ND 2.1 ND 0.38
71-43-2 Benzene 2.5 2.1 0.77 0.65
56-23-5 Carbon Tetrachloride ND 2.1 ND 0.33
110-82-7 Cyclohexane ND 4.1 ND 1.2
78-87-5 1,2-Dichloropropane ND 2.1 ND 0.45
75-27-4 Bromodichloromethane ND 2.1 ND 0.31
79-01-6 Trichloroethene 3.8 2.1 0.70 0.38
123-91-1 1,4-Dioxane ND 2.1 ND 0.57
80-62-6 Methyl Methacrylate ND 4.1 ND 1.0
142-82-5 n-Heptane ND 2.1 ND 0.50
10061-01-5 cis-1,3-Dichloropropene ND 2.1 ND 0.45
108-10-1 4-Methyl-2-pentanone ND 2.1 ND 0.50
10061-02-6 trans-1,3-Dichloropropene ND 2.1 ND 0.45
79-00-5 1,1,2-Trichloroethane ND 2.1 ND 0.38
108-88-3 Toluene ND 2.1 ND 0.55
591-78-6 2-Hexanone ND 2.1 ND 0.50
124-48-1 Dibromochloromethane ND 2.1 ND 0.24
106-93-4 1,2-Dibromoethane ND 2.1 ND 0.27
123-86-4 n-Butyl Acetate ND 2.1 ND 0.43
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
14 of 31
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ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 3 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-3 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-003
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00726
Initial Pressure (psig):-2.55 Final Pressure (psig):5.37
Canister Dilution Factor:1.65
MRL MRL Data
CAS #Compound µg/m³ ppbV Qualifier
111-65-9 n-Octane ND 2.1 ND 0.44
127-18-4 Tetrachloroethene ND 2.1 ND 0.30
108-90-7 Chlorobenzene ND 2.1 ND 0.45
100-41-4 Ethylbenzene ND 2.1 ND 0.48
179601-23-1 m,p-Xylenes ND 4.1 ND 0.95
75-25-2 Bromoform ND 2.1 ND 0.20
100-42-5 Styrene ND 2.1 ND 0.48
95-47-6 o-Xylene ND 2.1 ND 0.48
111-84-2 n-Nonane ND 2.1 ND 0.39
79-34-5 1,1,2,2-Tetrachloroethane ND 2.1 ND 0.30
98-82-8 Cumene ND 2.1 ND 0.42
80-56-8 alpha-Pinene ND 2.1 ND 0.37
103-65-1 n-Propylbenzene ND 2.1 ND 0.42
622-96-8 4-Ethyltoluene ND 2.1 ND 0.42
108-67-8 1,3,5-Trimethylbenzene ND 2.1 ND 0.42
95-63-6 1,2,4-Trimethylbenzene ND 2.1 ND 0.42
100-44-7 Benzyl Chloride ND 2.1 ND 0.40
541-73-1 1,3-Dichlorobenzene ND 2.1 ND 0.34
106-46-7 1,4-Dichlorobenzene ND 2.1 ND 0.34
95-50-1 1,2-Dichlorobenzene ND 2.1 ND 0.34
5989-27-5 d-Limonene ND 2.1 ND 0.37
96-12-8 1,2-Dibromo-3-chloropropane ND 2.1 ND 0.21
120-82-1 1,2,4-Trichlorobenzene ND 2.1 ND 0.28
91-20-3 Naphthalene ND 2.1 ND 0.39
87-68-3 Hexachlorobutadiene ND 2.1 ND 0.19
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
15 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - Sample (4)
ALS ENVIRONMENTAL

RESULTS OF ANALYSIS
Page 1 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-4 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-004
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00621
Initial Pressure (psig):-2.58 Final Pressure (psig):5.12
Canister Dilution Factor:1.64

CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
115-07-1 Propene 27 2.1 16 1.2
75-71-8 Dichlorodifluoromethane (CFC 12)25 2.1 5.1 0.41
74-87-3 Chloromethane ND 2.1 ND 0.99
76-14-2 1,2-Dichloro-1,1,2,2-
tetrafluoroethane (CFC 114)ND 2.1 ND 0.29
75-01-4 Vinyl Chloride ND 2.1 ND 0.80
106-99-0 1,3-Butadiene ND 2.1 ND 0.93
74-83-9 Bromomethane ND 2.1 ND 0.53
75-00-3 Chloroethane ND 2.1 ND 0.78
64-17-5 Ethanol 180 21 93 11
75-05-8 Acetonitrile 2.8 2.1 1.7 1.2
107-02-8 Acrolein ND 8.2 ND 3.6
67-64-1 Acetone 370 21 160 8.6
75-69-4 Trichlorofluoromethane ND 2.1 ND 0.36
67-63-0 2-Propanol (Isopropyl Alcohol)ND 21 ND 8.3
107-13-1 Acrylonitrile ND 2.1 ND 0.95
75-35-4 1,1-Dichloroethene ND 2.1 ND 0.52
75-09-2 Methylene Chloride ND 2.1 ND 0.59
107-05-1 3-Chloro-1-propene (Allyl Chloride)ND 2.1 ND 0.66
76-13-1 Trichlorotrifluoroethane ND 2.1 ND 0.27
75-15-0 Carbon Disulfide ND 21 ND 6.6
156-60-5 trans-1,2-Dichloroethene ND 2.1 ND 0.52
75-34-3 1,1-Dichloroethane ND 2.1 ND 0.51
1634-04-4 Methyl tert-Butyl Ether ND 2.1 ND 0.57
108-05-4 Vinyl Acetate ND 21 ND 5.8
78-93-3 2-Butanone (MEK)26 21 8.7 7.0
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
16 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - Sample (4)
ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 2 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-4 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-004
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00621
Initial Pressure (psig):-2.58 Final Pressure (psig):5.12
Canister Dilution Factor:1.64
CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
156-59-2 cis-1,2-Dichloroethene ND 2.1 ND 0.52
141-78-6 Ethyl Acetate 5.0 4.1 1.4 1.1
110-54-3 n-Hexane 3.1 2.1 0.89 0.58
67-66-3 Chloroform 3.1 2.1 0.64 0.42
109-99-9 Tetrahydrofuran (THF)4.1 2.1 1.4 0.70
107-06-2 1,2-Dichloroethane ND 2.1 ND 0.51
71-55-6 1,1,1-Trichloroethane ND 2.1 ND 0.38
71-43-2 Benzene 7.2 2.1 2.3 0.64
56-23-5 Carbon Tetrachloride ND 2.1 ND 0.33
110-82-7 Cyclohexane 4.4 4.1 1.3 1.2
78-87-5 1,2-Dichloropropane ND 2.1 ND 0.44
75-27-4 Bromodichloromethane ND 2.1 ND 0.31
79-01-6 Trichloroethene ND 2.1 ND 0.38
123-91-1 1,4-Dioxane 2.8 2.1 0.77 0.57
80-62-6 Methyl Methacrylate ND 4.1 ND 1.0
142-82-5 n-Heptane 3.4 2.1 0.82 0.50
10061-01-5 cis-1,3-Dichloropropene ND 2.1 ND 0.45
108-10-1 4-Methyl-2-pentanone 3.3 2.1 0.81 0.50
10061-02-6 trans-1,3-Dichloropropene ND 2.1 ND 0.45
79-00-5 1,1,2-Trichloroethane ND 2.1 ND 0.38
108-88-3 Toluene 11 2.1 2.9 0.54
591-78-6 2-Hexanone ND 2.1 ND 0.50
124-48-1 Dibromochloromethane ND 2.1 ND 0.24
106-93-4 1,2-Dibromoethane ND 2.1 ND 0.27
123-86-4 n-Butyl Acetate ND 2.1 ND 0.43
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
17 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - Sample (4)
ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 3 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
SG-4 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-004
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00621
Initial Pressure (psig):-2.58 Final Pressure (psig):5.12
Canister Dilution Factor:1.64
MRL MRL Data
CAS #Compound µg/m³ ppbV Qualifier
111-65-9 n-Octane 4.7 2.1 1.0 0.44
127-18-4 Tetrachloroethene ND 2.1 ND 0.30
108-90-7 Chlorobenzene ND 2.1 ND 0.45
100-41-4 Ethylbenzene ND 2.1 ND 0.47
179601-23-1 m,p-Xylenes ND 4.1 ND 0.94
75-25-2 Bromoform ND 2.1 ND 0.20
100-42-5 Styrene ND 2.1 ND 0.48
95-47-6 o-Xylene ND 2.1 ND 0.47
111-84-2 n-Nonane 6.2 2.1 1.2 0.39
79-34-5 1,1,2,2-Tetrachloroethane ND 2.1 ND 0.30
98-82-8 Cumene ND 2.1 ND 0.42
80-56-8 alpha-Pinene 7.0 2.1 1.3 0.37
103-65-1 n-Propylbenzene ND 2.1 ND 0.42
622-96-8 4-Ethyltoluene ND 2.1 ND 0.42
108-67-8 1,3,5-Trimethylbenzene ND 2.1 ND 0.42
95-63-6 1,2,4-Trimethylbenzene 4.2 2.1 0.86 0.42
100-44-7 Benzyl Chloride ND 2.1 ND 0.40
541-73-1 1,3-Dichlorobenzene ND 2.1 ND 0.34
106-46-7 1,4-Dichlorobenzene ND 2.1 ND 0.34
95-50-1 1,2-Dichlorobenzene ND 2.1 ND 0.34
5989-27-5 d-Limonene 3.8 2.1 0.68 0.37
96-12-8 1,2-Dibromo-3-chloropropane ND 2.1 ND 0.21
120-82-1 1,2,4-Trichlorobenzene ND 2.1 ND 0.28
91-20-3 Naphthalene ND 2.1 ND 0.39
87-68-3 Hexachlorobutadiene ND 2.1 ND 0.19
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
18 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - Sample (5)
ALS ENVIRONMENTAL

RESULTS OF ANALYSIS
Page 1 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
FD-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-005
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00603
Initial Pressure (psig):-2.95 Final Pressure (psig):5.94
Canister Dilution Factor:1.76

CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
115-07-1 Propene 4.9 2.2 2.9 1.3
75-71-8 Dichlorodifluoromethane (CFC 12)2.2 2.2 0.45 0.45
74-87-3 Chloromethane ND 2.2 ND 1.1
76-14-2 1,2-Dichloro-1,1,2,2-
tetrafluoroethane (CFC 114)ND 2.2 ND 0.31
75-01-4 Vinyl Chloride ND 2.2 ND 0.86
106-99-0 1,3-Butadiene ND 2.2 ND 0.99
74-83-9 Bromomethane ND 2.2 ND 0.57
75-00-3 Chloroethane ND 2.2 ND 0.83
64-17-5 Ethanol 28 22 15 12
75-05-8 Acetonitrile ND 2.2 ND 1.3
107-02-8 Acrolein ND 8.8 ND 3.8
67-64-1 Acetone 43 22 18 9.3
75-69-4 Trichlorofluoromethane ND 2.2 ND 0.39
67-63-0 2-Propanol (Isopropyl Alcohol)ND 22 ND 9.0
107-13-1 Acrylonitrile ND 2.2 ND 1.0
75-35-4 1,1-Dichloroethene ND 2.2 ND 0.56
75-09-2 Methylene Chloride ND 2.2 ND 0.63
107-05-1 3-Chloro-1-propene (Allyl Chloride)ND 2.2 ND 0.70
76-13-1 Trichlorotrifluoroethane ND 2.2 ND 0.29
75-15-0 Carbon Disulfide 54 22 17 7.1
156-60-5 trans-1,2-Dichloroethene ND 2.2 ND 0.56
75-34-3 1,1-Dichloroethane ND 2.2 ND 0.54
1634-04-4 Methyl tert-Butyl Ether ND 2.2 ND 0.61
108-05-4 Vinyl Acetate ND 22 ND 6.3
78-93-3 2-Butanone (MEK)ND 22 ND 7.5
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
19 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - Sample (5)
ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 2 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
FD-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-005
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00603
Initial Pressure (psig):-2.95 Final Pressure (psig):5.94
Canister Dilution Factor:1.76
CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
156-59-2 cis-1,2-Dichloroethene ND 2.2 ND 0.56
141-78-6 Ethyl Acetate 50 4.4 14 1.2
110-54-3 n-Hexane 38 2.2 11 0.62
67-66-3 Chloroform ND 2.2 ND 0.45
109-99-9 Tetrahydrofuran (THF)2.8 2.2 0.94 0.75
107-06-2 1,2-Dichloroethane ND 2.2 ND 0.54
71-55-6 1,1,1-Trichloroethane 28 2.2 5.2 0.40
71-43-2 Benzene 19 2.2 6.0 0.69
56-23-5 Carbon Tetrachloride ND 2.2 ND 0.35
110-82-7 Cyclohexane 160 4.4 48 1.3
78-87-5 1,2-Dichloropropane ND 2.2 ND 0.48
75-27-4 Bromodichloromethane ND 2.2 ND 0.33
79-01-6 Trichloroethene 49 2.2 9.0 0.41
123-91-1 1,4-Dioxane 3.0 2.2 0.84 0.61
80-62-6 Methyl Methacrylate 20 4.4 4.9 1.1
142-82-5 n-Heptane 20 2.2 5.0 0.54
10061-01-5 cis-1,3-Dichloropropene ND 2.2 ND 0.48
108-10-1 4-Methyl-2-pentanone ND 2.2 ND 0.54
10061-02-6 trans-1,3-Dichloropropene ND 2.2 ND 0.48
79-00-5 1,1,2-Trichloroethane ND 2.2 ND 0.40
108-88-3 Toluene 25 2.2 6.7 0.58
591-78-6 2-Hexanone ND 2.2 ND 0.54
124-48-1 Dibromochloromethane ND 2.2 ND 0.26
106-93-4 1,2-Dibromoethane ND 2.2 ND 0.29
123-86-4 n-Butyl Acetate ND 2.2 ND 0.46
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
20 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - Sample (5)
ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 3 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
FD-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-005
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00603
Initial Pressure (psig):-2.95 Final Pressure (psig):5.94
Canister Dilution Factor:1.76
MRL MRL Data
CAS #Compound µg/m³ ppbV Qualifier
111-65-9 n-Octane 6.9 2.2 1.5 0.47
127-18-4 Tetrachloroethene 84 2.2 12 0.32
108-90-7 Chlorobenzene ND 2.2 ND 0.48
100-41-4 Ethylbenzene ND 2.2 ND 0.51
179601-23-1 m,p-Xylenes ND 4.4 ND 1.0
75-25-2 Bromoform ND 2.2 ND 0.21
100-42-5 Styrene ND 2.2 ND 0.52
95-47-6 o-Xylene ND 2.2 ND 0.51
111-84-2 n-Nonane ND 2.2 ND 0.42
79-34-5 1,1,2,2-Tetrachloroethane ND 2.2 ND 0.32
98-82-8 Cumene ND 2.2 ND 0.45
80-56-8 alpha-Pinene 5.9 2.2 1.1 0.39
103-65-1 n-Propylbenzene ND 2.2 ND 0.45
622-96-8 4-Ethyltoluene ND 2.2 ND 0.45
108-67-8 1,3,5-Trimethylbenzene ND 2.2 ND 0.45
95-63-6 1,2,4-Trimethylbenzene ND 2.2 ND 0.45
100-44-7 Benzyl Chloride ND 2.2 ND 0.43
541-73-1 1,3-Dichlorobenzene ND 2.2 ND 0.37
106-46-7 1,4-Dichlorobenzene ND 2.2 ND 0.37
95-50-1 1,2-Dichlorobenzene ND 2.2 ND 0.37
5989-27-5 d-Limonene 3.8 2.2 0.68 0.39
96-12-8 1,2-Dibromo-3-chloropropane ND 2.2 ND 0.23
120-82-1 1,2,4-Trichlorobenzene ND 2.2 ND 0.30
91-20-3 Naphthalene ND 2.2 ND 0.42
87-68-3 Hexachlorobutadiene ND 2.2 ND 0.21
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
21 of 31
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ALS ENVIRONMENTAL

RESULTS OF ANALYSIS
Page 1 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
TB-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-006
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00999
Canister Dilution Factor:1.00

CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
115-07-1 Propene ND 1.3 ND 0.73
75-71-8 Dichlorodifluoromethane (CFC 12)ND 1.3 ND 0.25
74-87-3 Chloromethane ND 1.3 ND 0.61
76-14-2 1,2-Dichloro-1,1,2,2-
tetrafluoroethane (CFC 114)ND 1.3 ND 0.18
75-01-4 Vinyl Chloride ND 1.3 ND 0.49
106-99-0 1,3-Butadiene ND 1.3 ND 0.57
74-83-9 Bromomethane ND 1.3 ND 0.32
75-00-3 Chloroethane ND 1.3 ND 0.47
64-17-5 Ethanol 25 13 13 6.6
75-05-8 Acetonitrile ND 1.3 ND 0.74
107-02-8 Acrolein ND 5.0 ND 2.2
67-64-1 Acetone ND 13 ND 5.3
75-69-4 Trichlorofluoromethane ND 1.3 ND 0.22
67-63-0 2-Propanol (Isopropyl Alcohol)ND 13 ND 5.1
107-13-1 Acrylonitrile ND 1.3 ND 0.58
75-35-4 1,1-Dichloroethene ND 1.3 ND 0.32
75-09-2 Methylene Chloride ND 1.3 ND 0.36
107-05-1 3-Chloro-1-propene (Allyl Chloride)ND 1.3 ND 0.40
76-13-1 Trichlorotrifluoroethane ND 1.3 ND 0.16
75-15-0 Carbon Disulfide ND 13 ND 4.0
156-60-5 trans-1,2-Dichloroethene ND 1.3 ND 0.32
75-34-3 1,1-Dichloroethane ND 1.3 ND 0.31
1634-04-4 Methyl tert-Butyl Ether ND 1.3 ND 0.35
108-05-4 Vinyl Acetate ND 13 ND 3.6
78-93-3 2-Butanone (MEK)ND 13 ND 4.2
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
22 of 31
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ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 2 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
TB-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-006
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00999
Canister Dilution Factor:1.00
CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
156-59-2 cis-1,2-Dichloroethene ND 1.3 ND 0.32
141-78-6 Ethyl Acetate ND 2.5 ND 0.69
110-54-3 n-Hexane ND 1.3 ND 0.35
67-66-3 Chloroform ND 1.3 ND 0.26
109-99-9 Tetrahydrofuran (THF)ND 1.3 ND 0.42
107-06-2 1,2-Dichloroethane ND 1.3 ND 0.31
71-55-6 1,1,1-Trichloroethane ND 1.3 ND 0.23
71-43-2 Benzene ND 1.3 ND 0.39
56-23-5 Carbon Tetrachloride ND 1.3 ND 0.20
110-82-7 Cyclohexane ND 2.5 ND 0.73
78-87-5 1,2-Dichloropropane ND 1.3 ND 0.27
75-27-4 Bromodichloromethane ND 1.3 ND 0.19
79-01-6 Trichloroethene ND 1.3 ND 0.23
123-91-1 1,4-Dioxane ND 1.3 ND 0.35
80-62-6 Methyl Methacrylate ND 2.5 ND 0.61
142-82-5 n-Heptane ND 1.3 ND 0.31
10061-01-5 cis-1,3-Dichloropropene ND 1.3 ND 0.28
108-10-1 4-Methyl-2-pentanone ND 1.3 ND 0.31
10061-02-6 trans-1,3-Dichloropropene ND 1.3 ND 0.28
79-00-5 1,1,2-Trichloroethane ND 1.3 ND 0.23
108-88-3 Toluene 1.7 1.3 0.46 0.33
591-78-6 2-Hexanone ND 1.3 ND 0.31
124-48-1 Dibromochloromethane ND 1.3 ND 0.15
106-93-4 1,2-Dibromoethane ND 1.3 ND 0.16
123-86-4 n-Butyl Acetate ND 1.3 ND 0.26
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
23 of 31
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ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 3 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
TB-1 ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P1504255-006
Test Code:EPA TO-15 Date Collected:10/1/15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:10/8/15
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.40 Liter(s)
Test Notes:
Container ID:1SC00999
Canister Dilution Factor:1.00
MRL MRL Data
CAS #Compound µg/m³ ppbV Qualifier
111-65-9 n-Octane ND 1.3 ND 0.27
127-18-4 Tetrachloroethene ND 1.3 ND 0.18
108-90-7 Chlorobenzene ND 1.3 ND 0.27
100-41-4 Ethylbenzene ND 1.3 ND 0.29
179601-23-1 m,p-Xylenes ND 2.5 ND 0.58
75-25-2 Bromoform ND 1.3 ND 0.12
100-42-5 Styrene ND 1.3 ND 0.29
95-47-6 o-Xylene ND 1.3 ND 0.29
111-84-2 n-Nonane ND 1.3 ND 0.24
79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 ND 0.18
98-82-8 Cumene ND 1.3 ND 0.25
80-56-8 alpha-Pinene ND 1.3 ND 0.22
103-65-1 n-Propylbenzene ND 1.3 ND 0.25
622-96-8 4-Ethyltoluene ND 1.3 ND 0.25
108-67-8 1,3,5-Trimethylbenzene ND 1.3 ND 0.25
95-63-6 1,2,4-Trimethylbenzene ND 1.3 ND 0.25
100-44-7 Benzyl Chloride ND 1.3 ND 0.24
541-73-1 1,3-Dichlorobenzene ND 1.3 ND 0.21
106-46-7 1,4-Dichlorobenzene ND 1.3 ND 0.21
95-50-1 1,2-Dichlorobenzene ND 1.3 ND 0.21
5989-27-5 d-Limonene ND 1.3 ND 0.22
96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 ND 0.13
120-82-1 1,2,4-Trichlorobenzene ND 1.3 ND 0.17
91-20-3 Naphthalene ND 1.3 ND 0.24
87-68-3 Hexachlorobutadiene ND 1.3 ND 0.12
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Client Sample ID:
Client Project ID:
Result Result
µg/m³ppbV
24 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - MBlank
ALS ENVIRONMENTAL

RESULTS OF ANALYSIS
Page 1 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
Method Blank ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P151014-MB

Test Code:EPA TO-15 Date Collected:NA
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:NA
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:1.00 Liter(s)
Test Notes:

Canister Dilution Factor:1.00

CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
115-07-1 Propene ND 0.50 ND 0.29
75-71-8 Dichlorodifluoromethane (CFC 12)ND 0.50 ND 0.10
74-87-3 Chloromethane ND 0.50 ND 0.24
76-14-2 1,2-Dichloro-1,1,2,2-
tetrafluoroethane (CFC 114)ND 0.50 ND 0.072
75-01-4 Vinyl Chloride ND 0.50 ND 0.20
106-99-0 1,3-Butadiene ND 0.50 ND 0.23
74-83-9 Bromomethane ND 0.50 ND 0.13
75-00-3 Chloroethane ND 0.50 ND 0.19
64-17-5 Ethanol ND 5.0 ND 2.7
75-05-8 Acetonitrile ND 0.50 ND 0.30
107-02-8 Acrolein ND 2.0 ND 0.87
67-64-1 Acetone ND 5.0 ND 2.1
75-69-4 Trichlorofluoromethane ND 0.50 ND 0.089
67-63-0 2-Propanol (Isopropyl Alcohol)ND 5.0 ND 2.0
107-13-1 Acrylonitrile ND 0.50 ND 0.23
75-35-4 1,1-Dichloroethene ND 0.50 ND 0.13
75-09-2 Methylene Chloride ND 0.50 ND 0.14
107-05-1 3-Chloro-1-propene (Allyl Chloride)ND 0.50 ND 0.16
76-13-1 Trichlorotrifluoroethane ND 0.50 ND 0.065
75-15-0 Carbon Disulfide ND 5.0 ND 1.6
156-60-5 trans-1,2-Dichloroethene ND 0.50 ND 0.13
75-34-3 1,1-Dichloroethane ND 0.50 ND 0.12
1634-04-4 Methyl tert-Butyl Ether ND 0.50 ND 0.14
108-05-4 Vinyl Acetate ND 5.0 ND 1.4
78-93-3 2-Butanone (MEK)ND 5.0 ND 1.7
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Result
ppbV
Result
µg/m³
Client Sample ID:
Client Project ID:
25 of 31
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ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 2 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
Method Blank ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P151014-MB
Test Code:EPA TO-15 Date Collected:NA
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:NA
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:1.00 Liter(s)
Test Notes:

Canister Dilution Factor:1.00
CAS #Compound MRL MRL Data
µg/m³ ppbV Qualifier
156-59-2 cis-1,2-Dichloroethene ND 0.50 ND 0.13
141-78-6 Ethyl Acetate ND 1.0 ND 0.28
110-54-3 n-Hexane ND 0.50 ND 0.14
67-66-3 Chloroform ND 0.50 ND 0.10
109-99-9 Tetrahydrofuran (THF)ND 0.50 ND 0.17
107-06-2 1,2-Dichloroethane ND 0.50 ND 0.12
71-55-6 1,1,1-Trichloroethane ND 0.50 ND 0.092
71-43-2 Benzene ND 0.50 ND 0.16
56-23-5 Carbon Tetrachloride ND 0.50 ND 0.080
110-82-7 Cyclohexane ND 1.0 ND 0.29
78-87-5 1,2-Dichloropropane ND 0.50 ND 0.11
75-27-4 Bromodichloromethane ND 0.50 ND 0.075
79-01-6 Trichloroethene ND 0.50 ND 0.093
123-91-1 1,4-Dioxane ND 0.50 ND 0.14
80-62-6 Methyl Methacrylate ND 1.0 ND 0.24
142-82-5 n-Heptane ND 0.50 ND 0.12
10061-01-5 cis-1,3-Dichloropropene ND 0.50 ND 0.11
108-10-1 4-Methyl-2-pentanone ND 0.50 ND 0.12
10061-02-6 trans-1,3-Dichloropropene ND 0.50 ND 0.11
79-00-5 1,1,2-Trichloroethane ND 0.50 ND 0.092
108-88-3 Toluene ND 0.50 ND 0.13
591-78-6 2-Hexanone ND 0.50 ND 0.12
124-48-1 Dibromochloromethane ND 0.50 ND 0.059
106-93-4 1,2-Dibromoethane ND 0.50 ND 0.065
123-86-4 n-Butyl Acetate ND 0.50 ND 0.11
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Result
ppbV
Client Sample ID:
Client Project ID:
Result
µg/m³
26 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - MBlank
ALS ENVIRONMENTAL
RESULTS OF ANALYSIS
Page 3 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
Method Blank ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P151014-MB
Test Code:EPA TO-15 Date Collected:NA
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:NA
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:1.00 Liter(s)
Test Notes:

Canister Dilution Factor:1.00
MRL MRL Data
CAS #Compound µg/m³ ppbV Qualifier
111-65-9 n-Octane ND 0.50 ND 0.11
127-18-4 Tetrachloroethene ND 0.50 ND 0.074
108-90-7 Chlorobenzene ND 0.50 ND 0.11
100-41-4 Ethylbenzene ND 0.50 ND 0.12
179601-23-1 m,p-Xylenes ND 1.0 ND 0.23
75-25-2 Bromoform ND 0.50 ND 0.048
100-42-5 Styrene ND 0.50 ND 0.12
95-47-6 o-Xylene ND 0.50 ND 0.12
111-84-2 n-Nonane ND 0.50 ND 0.095
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 ND 0.073
98-82-8 Cumene ND 0.50 ND 0.10
80-56-8 alpha-Pinene ND 0.50 ND 0.090
103-65-1 n-Propylbenzene ND 0.50 ND 0.10
622-96-8 4-Ethyltoluene ND 0.50 ND 0.10
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ND 0.10
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ND 0.10
100-44-7 Benzyl Chloride ND 0.50 ND 0.097
541-73-1 1,3-Dichlorobenzene ND 0.50 ND 0.083
106-46-7 1,4-Dichlorobenzene ND 0.50 ND 0.083
95-50-1 1,2-Dichlorobenzene ND 0.50 ND 0.083
5989-27-5 d-Limonene ND 0.50 ND 0.090
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ND 0.052
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ND 0.067
91-20-3 Naphthalene ND 0.50 ND 0.095
87-68-3 Hexachlorobutadiene ND 0.50 ND 0.047
ND = Compound was analyzed for, but not detected above the laboratory reporting limit.
MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Result
ppbV
Result
µg/m³
Client Sample ID:
Client Project ID:

27 of 31
TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - Surrogates
ALS ENVIRONMENTAL

SURROGATE SPIKE RECOVERY RESULTS
Page 1 of 1
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
Ashville Tannery/Day's Tobacco Warehouse Property ALS Project ID:P1504255

Test Code:EPA TO-15
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date(s) Collected:10/1/15
Analyst:Evelyn Alvarez Date(s) Received:10/8/15
Sample Type:1.0 L Summa Canister(s)Date(s) Analyzed:10/14/15
Test Notes:

Client Sample ID ALS Sample ID Acceptance Data
Limits Qualifier
P151014-MB 70-130
P151014-LCS 70-130
P1504255-001 70-130
P1504255-002 70-130
P1504255-003 70-130
P1504255-004 70-130
P1504255-005 70-130
P1504255-006 70-130
Surrogate percent recovery is verified and accepted based on the on-column result.
Reported results are shown in concentration units and as a result of the calculation, may vary slightly from the on-column percent recovery.
SG-1
RecoveredRecovered
Client Project ID:
Method Blank
Lab Control Sample
TB-1
FD-1
SG-3
SG-4
SG-2
BromofluorobenzeneToluene-d81,2-Dichloroethane-d4
PercentPercentPercent
100
105
105
105
102
Recovered
100
100
99102
96
94
95
103
104
103
99
96
94
97
97
97 97
100
96
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ALS ENVIRONMENTAL

LABORATORY CONTROL SAMPLE SUMMARY
Page 1 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
Lab Control Sample ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P151014-LCS

Test Code:EPA TO-15 Date Collected:NA
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:NA
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.125 Liter(s)
Test Notes:

CAS #Compound Data
Qualifier
115-07-1 Propene 99 49-131
75-71-8 Dichlorodifluoromethane (CFC 12)96 65-117
74-87-3 Chloromethane 94 48-132
76-14-2 1,2-Dichloro-1,1,2,2-
tetrafluoroethane (CFC 114)94 65-122
75-01-4 Vinyl Chloride 97 65-128
106-99-0 1,3-Butadiene 108 62-143
74-83-9 Bromomethane 97 65-130
75-00-3 Chloroethane 93 69-126
64-17-5 Ethanol 107 57-126
75-05-8 Acetonitrile 85 51-134
107-02-8 Acrolein 100 55-146
67-64-1 Acetone 95 57-120
75-69-4 Trichlorofluoromethane 89 59-139
67-63-0 2-Propanol (Isopropyl Alcohol)100 59-129
107-13-1 Acrylonitrile 104 64-136
75-35-4 1,1-Dichloroethene 101 72-123
75-09-2 Methylene Chloride 92 63-117
107-05-1 3-Chloro-1-propene (Allyl Chloride)99 50-141
76-13-1 Trichlorotrifluoroethane 101 68-118
75-15-0 Carbon Disulfide 76 55-143
156-60-5 trans-1,2-Dichloroethene 102 69-129
75-34-3 1,1-Dichloroethane 97 66-122
1634-04-4 Methyl tert-Butyl Ether 104 55-128
108-05-4 Vinyl Acetate 118 66-140
78-93-3 2-Butanone (MEK)103 62-127
Laboratory Control Sample percent recovery is verified and accepted based on the on-column result.
Reported results are shown in concentration units and as a result of the calculation, may vary slightly.

224
12301,040
418
205
216
210
210
218
220
222
Client Sample ID:
Client Project ID:
200
202
204
200
196
188
ALS
AcceptanceSpike Amount
206
195
181
% Recovery
Limitsµg/m³
187
212
195
200
998
186
1070
212
216
214 215
1,080
216
219
1030
417
212
Result
µg/m³
204
194
222
221
180
191
193
227220
216
223
159
214
29 of 31
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ALS ENVIRONMENTAL
LABORATORY CONTROL SAMPLE SUMMARY
Page 2 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
Lab Control Sample ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P151014-LCS
Test Code:EPA TO-15 Date Collected:NA
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:NA
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.125 Liter(s)
Test Notes:

CAS #Compound Data
Qualifier
156-59-2 cis-1,2-Dichloroethene 102 65-125
141-78-6 Ethyl Acetate 111 64-132
110-54-3 n-Hexane 99 58-126
67-66-3 Chloroform 98 68-117
109-99-9 Tetrahydrofuran (THF)103 64-123
107-06-2 1,2-Dichloroethane 103 63-124
71-55-6 1,1,1-Trichloroethane 101 68-120
71-43-2 Benzene 102 61-110
56-23-5 Carbon Tetrachloride 100 65-137
110-82-7 Cyclohexane 106 68-122
78-87-5 1,2-Dichloropropane 101 67-122
75-27-4 Bromodichloromethane 106 71-124
79-01-6 Trichloroethene 102 71-121
123-91-1 1,4-Dioxane 125 67-122 L
80-62-6 Methyl Methacrylate 110 76-130
142-82-5 n-Heptane 105 67-125
10061-01-5 cis-1,3-Dichloropropene 113 73-131
108-10-1 4-Methyl-2-pentanone 106 66-132
10061-02-6 trans-1,3-Dichloropropene 117 76-135
79-00-5 1,1,2-Trichloroethane 106 73-121
108-88-3 Toluene 103 67-117
591-78-6 2-Hexanone 122 59-128
124-48-1 Dibromochloromethane 115 73-132
106-93-4 1,2-Dibromoethane 113 73-128
123-86-4 n-Butyl Acetate 118 61-136
Laboratory Control Sample percent recovery is verified and accepted based on the on-column result.
Reported results are shown in concentration units and as a result of the calculation, may vary slightly.
L = Laboratory control sample recovery outside the specified limits, results may be biased high.

226
422 466
224
218
231
424
216
449
220
220214
212
229
218
233220
210
216
220
220
230
253
245
225

269
218
ALS
219
227
232
Acceptance
Limits
% Recovery
208
Result
428 473
230
Client Sample ID:
218
Client Project ID:
µg/m³
Spike Amount
226
212
218
216
210
246
266
216
µg/m³
222
210
210
262
226
234
221
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TO15SCAN.XLS - 75 Compounds - PageNo.:P1504255_TO15_1510161620_SC.xls - LCS
ALS ENVIRONMENTAL
LABORATORY CONTROL SAMPLE SUMMARY
Page 3 of 3
Client:AMEC Foster Wheeler Environment & Infrastructure Inc.
Lab Control Sample ALS Project ID:P1504255
Ashville Tannery/Day's Tobacco Warehouse Property ALS Sample ID:P151014-LCS
Test Code:EPA TO-15 Date Collected:NA
Instrument ID:Tekmar AUTOCAN/Agilent 5975Binert/6890N/MS13 Date Received:NA
Analyst:Evelyn Alvarez Date Analyzed:10/14/15
Sample Type:1.0 L Summa Canister Volume(s) Analyzed:0.125 Liter(s)
Test Notes:

CAS #Compound Data
Qualifier
111-65-9 n-Octane 108 67-124
127-18-4 Tetrachloroethene 107 65-126
108-90-7 Chlorobenzene 105 68-120
100-41-4 Ethylbenzene 110 69-123
179601-23-1 m,p-Xylenes 113 67-125
75-25-2 Bromoform 100 68-153
100-42-5 Styrene 112 68-132
95-47-6 o-Xylene 114 67-124
111-84-2 n-Nonane 113 60-130
79-34-5 1,1,2,2-Tetrachloroethane 116 72-128
98-82-8 Cumene 111 67-124
80-56-8 alpha-Pinene 114 67-129
103-65-1 n-Propylbenzene 115 67-125
622-96-8 4-Ethyltoluene 117 66-128
108-67-8 1,3,5-Trimethylbenzene 117 65-125
95-63-6 1,2,4-Trimethylbenzene 122 62-134
100-44-7 Benzyl Chloride 122 74-145
541-73-1 1,3-Dichlorobenzene 118 63-133
106-46-7 1,4-Dichlorobenzene 113 62-129
95-50-1 1,2-Dichlorobenzene 123 62-134
5989-27-5 d-Limonene 120 66-137
96-12-8 1,2-Dibromo-3-chloropropane 113 71-147
120-82-1 1,2,4-Trichlorobenzene 108 60-145
91-20-3 Naphthalene 117 56-158
87-68-3 Hexachlorobutadiene 102 56-139
Laboratory Control Sample percent recovery is verified and accepted based on the on-column result.
Reported results are shown in concentration units and as a result of the calculation, may vary slightly.

220
µg/m³
Spike Amount

Client Sample ID:
210
ALS
Acceptance
Limits
% RecoveryResult
µg/m³
202
Client Project ID:
228
222
227
485
210
204
240
230
243
231
239
226
232
218
218
248
212 242
210
234
218
208
204
220
210
218
214
230
230
269
266
220
228
208
214
428
250
251
248
271
216
235
256
268
236
252
246
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