21010_Webster Poultry_Phase II ESA_20170203

WithersRavenel
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PHASE II
ENVIRONMENTAL SITE ASSESSMENT

Reman Properties LLC Property
±20.375-Acre Site
270 Moncure Pittsboro Road
Pittsboro, Chatham County, North Carolina
WR Project No. 02160652.00

Prepared for:
Capital Ready Mix Concrete
512 Three Sisters Road
Knightdale, NC 27545

Prepared by:
WithersRavenel
115 Mackenan Drive
Cary, North Carolina 27511
North Carolina Firm License No. C-0832
February 3, 2017

WithersRavenel
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115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington

February 3, 2017

Capital Ready Mix Concrete
512 Three Sisters Road
Knightdale, NC 27545

Attn: Ms. Sara Lochren

RE: Phase II Environmental Site Assessment
Reman Properties LLC Property
±20.375-Acre Site
270 Moncure Pittsboro Road
Pittsboro, Chatham County, North Carolina
WR Project No. 02160652.0

Ms. Lochren:

WithersRavenel (WR) is pleased to submit this report documenting Phase II Environmental Site Assessment
(ESA) activities for the above referenced property. Assessment activities were completed to evaluate soil and
groundwater conditions relative to historic onsite property uses and findings of the Phase I ESA completed
by WR on February 4, 2016. This report summarizes the results of WR's field activities and presents the
findings of the assessment relative to existing environmental or potential conditions at the site.

Sincerely,
WithersRavenel
Michael D. Fekete
Environmental Scientist – Environmental Professional

Patrick Farfour
Project Manager – Environmental Professional
R.S. (Butch) Lawter, Jr., PE
Director of Environmental Services

WithersRavenel
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Table of Contents
1. Purpose............................................................................................................................... 1
2. Background ........................................................................................................................ 2
3. Field Activities ................................................................................................................... 3
4. Conclusions ........................................................................................................................ 8

FIGURES
Figure 1 General Location Map
Figure 2 Site Map
Figure 3 Soil Assessment Results Map – Suspected Landfill
Figure 4 Soil Assessment Results Map – Processing Plant
Figure 5 Soil Assessment Results Map – Truck Shop
Figure 6 Groundwater Assessment Results Map
TABLES
Table 1A Summary of Soil Analytical Results – TPH/GRO & TPH/DRO
Table 1B Summary of Soil Analytical Results – VOCs
Table 1C Summary of Soil Analytical Results – SVOCs
Table 2A Summary of Groundwater Analytical Results – VOCs
Table 2B Summary of Groundwater Analytical Results – SVOCs, 8 RCRA Metals, MADEP
VPH/EPH, Ammonia
Table 3 Monitoring Well Construction Information
APPENDICES
Appendix A Boring Logs
Appendix B Well Construction Records
Appendix C Laboratory Report and Chain of Custody
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±20.375-Acre Reman Properties LLC Property WithersRavenel Project #02160652.0
Phase II Environmental Site Assessment February 2017
1

1. PURPOSE
WR has performed this Phase II ESA for a ±20.375-acre site located approximately 785 feet southeast of the
intersection of Moncure Pittsboro Road and Sanford Road in Pittsboro, Chatham County, North Carolina
(Figure 1). According to Chatham County GIS records, the subject consists of the following parcel:
Tract # Parcel # Current Owner Address Acreage
Tract 1 60773 Reman Properties LLC 270 Moncure Pittsboro Road ±20.375

The Phase II ESA was completed to investigate areas of concern identified in the Phase I ESA completed for
the property on January 6, 2017. Based on the areas identified in the Phase I ESA, subsurface investigation
activities were performed in the vicinity of the truck maintenance shop and truck scales located north of
Moncure Pittsboro Road, around various portions of the plant in the central portion of the site, and in a grassy
area in the southern portion of the site that was previously used for debris disposal.
The intent of the Phase II ESA was to provide a baseline soil and groundwater assessment to document the
current condition of the site and the presence of potential contaminants arising from the former uses of the
site. The Phase II ESA was performed to identify potential impacts to soil and groundwater in specified areas
and does not represent a comprehensive investigation to define the degree and extent of contaminant
migration from a known contaminant source, unless otherwise described. If conditions at the site change or
additional information become available that would materially affect the nature of the report, we request that
we be contacted so that any change in conditions can be properly reviewed and our report amended
accordingly.

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±20.375-Acre Reman Properties LLC Property WithersRavenel Project #02160652.0
Phase II Environmental Site Assessment February 2017
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2. BACKGROUND
WithersRavenel identified the following areas of environmental concern on the ±20.375-acre site during
completion of the Phase I ESA in December 2016. Locations of these areas are identified on Figure 2. The
following paragraphs describe the areas identified:
 A 10,000-gallon diesel fuel underground storage tank (UST) located southeast of the Truck
Maintenance Building north of Moncure Pittsboro Road along with approximately 70 feet of
underground product line and a fuel dispenser which were removed within the last year. Petroleum
contamination has been identified in soil and the release incident is currently under the guidance of
the NCDEQ-UST Section in an assessment phase.

 An approximately 550-gallon abandoned gasoline UST with approximately 50 feet of underground
product line connected to the former dispenser was identified off the northeast corner of Truck
Maintenance Building.

 A former 10,000-gallon gasoline UST was reported in historical reports and past interviews located
near the truck scales on the north side of Moncure Pittsboro Road.

 An approximately 6,000-gallon UST was used to store heating fuel oil to fuel a boiler and was located
somewhere between the south end of the processing facility and the facility maintenance building.
Historical reports mentioned that soil adjacent to this tank was sampled in 2001 with “minor
concentrations of petroleum near the tank and were submitted to the State of North Carolina for
review”. However, the NCDENR-UST Section has no record of this incident.

 A maintenance building is located on the south side of the plant that was formerly used for
maintenance activities and repairing of compressors and other equipment utilized in the main plant
building.

 A 275-gallon used refrigeration oil AST was located on the south side of the plant near a 22,000-
gallon aboveground anhydrous ammonia receiver during past plant operations and other anhydrous
ammonia equipment on the southwestern portion of the site with obvious signs of oil staining.

 The southern end of the plant contains the engine room which contained fuel powered equipment
with heavy petroleum staining noted throughout. In addition, this area of the plant was originally dirt
floors beneath the fuel powered equipment.

 A drum storage area and a chemical storage room are located on the north side of the plant
maintenance building. Currently, all materials have been removed from the site; however, petroleum
staining was noted in the drum area during WR’s previous assessment at the property. In addition, a
floor drain and staining was noted during the current assessment within the chemical storage room.

 A former air compressor area on the western portion of the site was observed to have significant
amounts of oil located in the containment wall. Signs of leakage outside the walls were observed
during WR’s assessment in 2013.

 A grass area south of the plant was utilized for disposal of plant infrastructure during upgrades and
expansions. Concrete, steel, and 55-gallon drum parts were observed protruding from the berm
along the southern extent of this area and interviews indicated that materials may have been buried
in this location in the past.
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3. FIELD ACTIVITIES
WR conducted Phase II ESA assessment activities from December 19 through 22, 2016. The following
paragraphs describe the results of the investigation.
3.1. SUBSURFACE UTILITY LOCATION
Prior to drilling, WR mobilized to the subject property to locate and mark subsurface utilities in the
investigation areas. WR also notified the North Carolina One Call Center (NC811) for the location and
marking of subsurface utilities along the right-of-way on the subject property.
3.2. SUSPECTED LANDFILL ASSESSMENT
WR monitored Eastern Environmental Management’s excavation of 10 test pits through the area of
suspected landfilling in the southern portion of the site to determine the type and approximate extents of the
buried materials. Soil was collected from the bottom of each test pit and screened for volatile organic vapors
utilizing a Foxboro® Toxic Vapor Analyzer (TVA) 1000B Photoionization Detector (PID) / Flame Ionization
Detector (FID). The PID/FID is an industry accepted screening device used to detect the presence of volatile
vapors, but is not relied upon to determine specific levels of contamination. The TVA-1000B was calibrated
in accordance with manufacturer guidelines prior to use. In addition to screening of soil samples with the
TVA, soils were characterized by moisture content, composition and other discernable characteristics,
including staining and/or odors, if present. Locations of the test pits are depicted on Figure 3.
The largest area of buried debris was identified in test pit TP-1. Debris observed in this test pit included scrap
metal, plastics, wood, several car parts, and concrete masonry blocks. Debris was encountered in TP-1 to a
depth of approximately 11 feet below land surface. Debris observed in several additional test pits to the north
and west of TP-1 included concrete, wiring, rebar, and insulated piping.
A soil sample from two of the test pits (TP-1 and TP-10) were submitted for laboratory analysis based on field
screening and the types of buried debris observed in the test pits. These samples were placed on ice in a cooler
or coolers, and ultimately transported under chain of custody to an NC certified laboratory for analysis of
volatile organic compounds (VOCs) by EPA Method 8260, total petroleum hydrocarbons (TPH) gasoline
range organics (GRO) and diesel range organics (DRO) by EPA Method 8015. Select samples were also
submitted for analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270.
The following table summarizes the field observations of the buried waste:
Test Pit ID Waste
Interval Waste Description
TP-1 2-11' Metals, plastic, car parts, Styrofoam, wood, concrete masonry blocks
TP-2 2-7' Concrete, wiring, wire cables
TP-3 2-6' Concrete masonry blocks, wiring, cloth, rebar
TP-4 2-3' Minimal debris – 2 pieces of plastic
TP-5 2-5' Insulated piping, concrete, concrete masonry blocks, plastic
TP-6 2-4' Concrete, metal, plastic
TP-7 2-4' Concrete, metal, Styrofoam, plastic, wood, glass
TP-8 No Debris Observed (Native Soils)
TP-9 No Debris Observed (Native Soils); Metal at surface
TP-10 2-4' Styrofoam, plastic, metal, wood

3.3. PROCESSING PLANT SOIL ASSESSMENT
WR along with drilling subcontractor, Quantex, Inc., conducted the subsurface investigation in the vicinity of
the former poultry processing facility utilizing a 7822DT GeoProbe® drill rig. A continuous sleeve Macro-
Core sampler was employed to collect a representative cross-section of geologic material. WR personnel
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removed the sample material from the liner and logged the lithology encountered in each of the borings. WR
completed 23 soil borings in the vicinity of the processing plant (SB-2 through SB-24). WR attempted to
complete one additional soil boring (SB-1) near the northeastern corner of the processing plant, but this
boring could not be completed due to the thickness of the concrete lab throughout this area. Representative
soil samples were collected from each of the 23 completed soil borings in 2.5-foot increments and were placed
in individual zip-lock bags. The retained soil samples were then submitted to an NC certified laboratory for
analysis of volatile organic compounds (VOCs) by EPA Method 8260, total petroleum hydrocarbons (TPH)
gasoline range organics (GRO) and diesel range organics (DRO) by EPA Method 8015. Select samples were
also submitted for analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270. Figure 4
illustrates the locations of each soil boring around the processing plant. Boring logs are included in Appendix
A.
3.4. TRUCK MAINTENANCE SHOP SOIL ASSESSMENT
WR completed five soil borings in the vicinity of the truck maintenance shop located in the northern portion
of the subject property. Three additional borings were completed in the vicinity of the truck scale located
approximately 360 feet southeast of the truck maintenance shop. Three soil samples (SB-25, SB-28, and SB-
29) were collected from around the truck shop and submitted for laboratory analysis of volatile organic
compounds (VOCs) by EPA Method 8260, total petroleum hydrocarbons (TPH) gasoline range organics
(GRO) and diesel range organics (DRO) by EPA Method 8015. Two of the three samples (SB-25 and SB-29)
were also submitted for analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270. One soil
sample was collected from the truck scale area (SB-31) and submitted for laboratory analysis of VOCs,
SVOCs, TPH-GRO, and TPH-DRO. Figure 5 illustrates the locations of each soil boring. Boring logs are
included in Appendix A.
3.5. GROUNDWATER ASSESSMENT
Six groundwater monitoring wells were installed around the processing plant, and one monitoring well was
installed in the suspected landfill area. The monitoring wells were installed to depths ranging from 20 to 39
feet below land surface. Each monitoring well was constructed with a 10 or 15-foot section of two-inch
diameter 0.010-inch slotted Schedule 40 PVC well screen placed at the base of the borehole, followed by
Schedule 40 PVC riser to land surface. A sand pack was established around the screen and two feet above
the screen. A bentonite seal was then placed over the sand pack and hydrated. The remaining annular space
was then filled with neat cement grout to grade. Boring logs are included in Appendix A, and well construction
records are included in Appendix B.
In addition to the seven monitoring wells installed by WR, two existing monitoring wells were located near
the truck maintenance shop. The nine monitoring wells were purged of water and fine sediment prior to
sampling. The groundwater samples were submitted for laboratory analysis by the following methods:
 Volatile Organic Compounds by EPA Method 8260B
 Semi-Volatile Organic Compounds by EPA Method 8270D
 Volatile Petroleum Hydrocarbons by MADEP Method for VPH
 Extractable Petroleum Hydrocarbons by MADEP Method for EPH
 8 RCRA Metals by EPA 6010C and 7470A
 Ammonia Nitrogen by EPA Method 350.1

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4. LABORATORY ANALYTICAL RESULTS
4.1. TEST PIT ANALYTICAL RESULTS
Total Petroleum Hydrocarbons
All three soil samples submitted for laboratory analysis of TPH were below laboratory detection limits for
both TPH-GRO and TPH-DRO.
A summary of the soil laboratory analytical TPH results are presented in Table 1A. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 3 illustrates the locations of each
soil boring and TPH concentrations identified in each location.
Volatile Organic Compounds
Data for analysis of soil samples by EPA Method 8260 indicated the presence of chlorobenzene,
isopropylbenzene, and trichlorofluoromethane in sample TP-1A at concentrations below their respective
Residential and Industrial Preliminary Soil Remediation (PSRGs).
A summary of the soil laboratory analytical VOCs results are presented in Table 1B. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 3 illustrates the locations of each
soil boring and concentrations of VOCs identified in each location.
Semi-Volatile Organic Compounds
Data for analysis of the one soil sample (TP-1A) by EPA Method 8270 indicated that all target analytes were
below laboratory detection limits.
A summary of the soil laboratory analytical SVOCs results are presented in Table 1C. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 3 illustrates the locations of each
soil boring and concentrations of VOCs identified in each location.
4.2. PROCESSING PLANT SOIL ANALYTICAL RESULTS
Total Petroleum Hydrocarbons
Two of the soil samples submitted for laboratory analysis of TPH-GRO had concentrations above laboratory
detection limits. The concentrations of TPH-GRO from SB-13 and SB-16 were both below the NCDEQ Action
Level of 50 mg/kg.
TPH-DRO concentrations above laboratory detection limits were reported in samples from SB-5, SB-11, SB-
13, SB-15, SB-16, and SB-20. The TPH-DRO concentrations in SB-5, SB-11, and SB-13 were reported above
the NCDEQ Action Level of 100 mg/kg.
A summary of the soil laboratory analytical TPH results are presented in Table 1A. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 4 illustrates the locations of each
soil boring and TPH concentrations identified in each location.
Volatile Organic Compounds
Data for soil samples analyzed by EPA Method 8260 indicated the presence of one or more target compounds
in samples obtained from borings SB-5, SB-7, SB-8, SB-10, SB-13, and SB-20. Concentrations of compounds
detected in these samples were all below their respective Residential and Commercial PSRGs.
A summary of the soil laboratory analytical VOCs results are presented in Table 1B. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 4 illustrates the locations of each
soil boring and concentrations of VOCs identified in each location.

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Semi-Volatile Organic Compounds
Data for soil samples analyzed by EPA Method 8270 indicated the presence of one or more target compounds
in samples obtained from borings SB-11 and SB-13. Concentrations of compounds detected in these samples
were all below their respective Residential and Commercial PSRGs.
A summary of the soil laboratory analytical SVOCs results are presented in Table 1C. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 4 illustrates the locations of each
soil boring and concentrations of VOCs identified in each location.
4.3. TRUCK MAINTENANCE SHOP SOIL ANALYTICAL RESULTS
Total Petroleum Hydrocarbons
One of the soil samples submitted for laboratory analysis of TPH-GRO and TPH-DRO (SB-29) had a reported
concentration above laboratory detection limits. The sample from SB-29 was above the NCDEQ Action Level
for both TPH-GRO and TPH-DRO. The other samples from the truck shop and truck scale were below
laboratory detection limits for TPH-GRO and TPH-DRO.
A summary of the soil laboratory analytical TPH results are presented in Table 1A. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 5 illustrates the locations of each
soil boring and TPH concentrations identified in each location.
Volatile Organic Compounds
Data for soil samples analyzed by EPA Method 8260 indicated the presence of one or more target compounds
in samples obtained from borings SB-29 and SB-31. Concentrations of compounds detected in SB-31 were
all below their respective Residential and Commercial PSRGs. The ethylbenzene concentration in SB-29
exceeds the Residential PSRG and the naphthalene concentration exceeds the Industrial PSRG.
A summary of the soil laboratory analytical VOCs results are presented in Table 1B. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 5 illustrates the locations of each
soil boring and concentrations of VOCs identified in each location.
Semi-Volatile Organic Compounds
Data for soil samples analyzed by EPA Method 8270 indicated the presence of naphthalene in the sample
from boring SB-29. The naphthalene concentration of 3.36 mg/kg is below the Residential and Industrial
PSRGs.
A summary of the soil laboratory analytical SVOCs results are presented in Table 1C. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix C. Figure 5 illustrates the locations of each
soil boring and concentrations of VOCs identified in each location
4.4. GROUNDWATER ANALYTICAL RESULTS
Suspected Landfill Area
Laboratory analysis of the groundwater sample, MW-3, collected from the monitoring well in the landfill area
reported no volatile organic compounds, semi-volatile organic compounds, ammonia nitrogen, VPH, EPH, or
8 RCRA metals concentrations above laboratory detection limits.
The laboratory analytical report is included in Appendix C. Figure 6 illustrates the locations of each
monitoring well and a summary of the groundwater analytical results.
Processing Plant
The sample collected from MW-5 showed a chloroform concentration of 204 µg/L, which exceeds the 2L
Standard of 70 µg/L. No other volatile organics or semi-volatile organics were detected in the sample from
MW-5.
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The sample collected from MW-4 had several VOCs and SVOCs at reported concentrations below their
respective 2L Standards. However, MW-4 had a reported C9-C22 Aromatics concentration of 153 µg/L,
which exceeds its 2L Standard of 10 µg/L. MW-1 had a reported sec-butylbenzene concentration of 1.3 µg/L,
which is below the 2L Standard of 70 µg/L. All VOCs, SVOCs, VPH, and EPH analytes were reported below
laboratory detection limits in MW-2, MW-6, and MW-7.
Barium was detected in five of the six monitoring wells in the vicinity of the plant at concentrations below the
2L Standard of 700 µg/L. Ammonia concentrations of 109 µg/L and 259 µg/L were detected in the samples
from MW-1 and MW-7, respectively. The 2L Standard for ammonia is 1,500 µg/L.
The laboratory analytical report is included in Appendix C. Figure 6 illustrates the locations of each
monitoring well and a summary of the groundwater analytical results.
Truck Maintenance Shop
Two existing monitoring wells were sampled near the Truck Maintenance Shop. For WR identification
purposes, the two wells were labeled as MW-A and MW-B. Multiple petroleum constituents were detected
in the samples from both of these monitoring wells. Benzene, MTBE, naphthalene, and C9-C22 aromatics
were detected in MW-A at concentrations above their respective 2L Standards. Petroleum constituents
detected in MW-B above 2L Standards include benzene, MTBE, naphthalene, n-propylbenzene, and C9-C22
aromatics. Additional compounds were detected in both wells at concentrations below 2L Standards.
The laboratory analytical report is included in Appendix C. Figure 6 illustrates the locations of each
monitoring well and a summary of the groundwater analytical results.

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5. CONCLUSIONS
WithersRavenel has completed a limited Phase II Site Assessment at the ±20.375-acre Reman Properties LLC
site located approximately 785 feet southeast of the intersection of Moncure Pittsboro Road and Sanford
Road in Pittsboro, Chatham County, North Carolina. The findings of assessment activities at the site
conducted by WR included the following:
 An area of buried debris is located in the southern portion of the property.
 Three soil samples in the vicinity of the processing plant, SB-5, SB-11, and SB-13, had TPH-DRO
concentrations above the NCDEQ Action Level of 100 mg/kg.
 Soils in the vicinity of the processing plant and in the buried debris area had reported concentrations
either below State action levels or below laboratory detection limits for EPA Method 8260B and EPA
Method 8270.
 One soil sample, SB-29, near the northeast corner of the truck maintenance shop had both TPH-GRO
and TPH-GRO concentrations above their respective NCDEQ Action Levels.
 The soil sample from SB-29 also indicated the presence of naphthalene in excess of the Industrial
PSRG and ethylbenzene above the Residential PSRG.
 The groundwater sample collected from MW-5 had a reported chloroform concentration of 204
µg/L, which exceeds the 2L Standard of 70 µg/L.
 The sample collected from MW-4 had a reported a C9-C22 aromatics concentration of 153 µg/L,
which exceeds its 2L Standard of 10 µg/L.
 Two existing monitoring wells near the truck maintenance shop both contained multiple petroleum
constituents at concentrations exceeding their respective 2L Standards.
The findings of this investigation suggest that industrial operations on the property have created areas of
impacted soil and groundwater with petroleum hydrocarbons and other constituents of concern with
concentrations above regulatory levels prescribed by the NCDEQ. Given the historical industrial use of the
property as a poultry processing facility, the identification of these impacts in proximity to the chemical and
fuel storage and distribution equipment locations is not considered unusual. It is possible that localized areas
of soil and groundwater with potentially higher concentrations of similar compounds will be identified if
additional portions of the plant building and exterior equipment are removed from the property.
It has been our pleasure to work with you in this capacity. Please do not hesitate to contact us at (919) 469-
3340 with any questions or comments regarding this work.
Sincerely,
WithersRavenel
Michael D. Fekete
Environmental Scientist – Environmental Professional

Patrick Farfour
Project Manager – Environmental Professional
R.S. Butch Lawter, Jr, P.E.
Director of Environmental Services

Figures

Tables

SOIL
SAMPLE
ID
DATE SAMPLE DEPTH
(feet bls)
TPH/GRO
(mg/kg)
TPH/DRO
(mg/kg)
SB-2 12/19/2016 2.5-5 <2.42 <5.09
SB-3 12/19/2016 5-6 <2.49 <4.93
SB-4 12/19/2016 7.5-10 <2.42 <4.67
SB-5 12/19/2016 2.5-5 <2.37 1,200
SB-6 12/19/2016 2.5-5 <2.44 <5.06
SB-7 12/19/2016 2.5-5 <2.54 <5.41
SB-8 12/19/2016 2.5-5 <2.55 <5.36
SB-9 12/19/2016 2.5-5 <2.7 <5.54
SB-10 12/19/2016 7.5-10 <2.71 <5.49
SB-11 12/19/2016 2.5-5 <2.83 419
SB-12 12/19/2016 7.5-10 <2.3 <4.9
SB-13 12/19/2016 0-2.5 4.1 497
SB-14 12/19/2016 2.5-5 <2.56 <5.39
SB-15 12/19/2016 2.5-5 <2.64 55.3
SB-16 12/19/2016 5-7.5 3.07 72.4
Notes: 1 - N/A = Not Applicable or Sampled.
2 - Results in bold and shaded exceed NCDEQ Action Level.
3 - bls = Below Land Surface.
4 - Results are in mg/kg (milligrams per kilogram).
5 - Soil samples were collected 12/19/16.
6 - TPH = Total Petroleum Hydrocarbons.
7 - BDL = Below Detection Limits

TABLE 1A
SUMMARY OF SOIL ANALYTICAL RESULTS
Reman Properties LLC
270 MONCURE PITTSBORO ROAD
PITTSBORO, CHATHAM COUNTY, NORTH CAROLINA
WR Project # 02160652.0
NCDEQ ACTION LEVEL 50 100
8 - TPH/GRO = Results generated by EPA Method 8015D.
9 - TPH/DRO = Results generated by EPA Method 8015.
SOIL
SAMPLE
ID
DATE SAMPLE DEPTH
(feet bls)
TPH/GRO
(mg/kg)
TPH/DRO
(mg/kg)
SB-17 12/19/2016 5-7.5 <2.55 <5.45
SB-18 12/19/2016 7.5-10 <2.63 <5.26
SB-19 12/19/2016 2.5-5 <2.71 <5.42
SB-20 12/19/2016 2.5-5 <2.28 5.09
SB-21 12/19/2016 5-7.5 <2.6 <5.4
SB-22 12/19/2016 7.5-10 <3.23 <6.23
SB-24 12/19/2016 2.5-5 <2.29 <5.64
SB-25 12/19/2016 5-7.5 <2.65 <4.99
SB-28 12/19/2016 5-7.5 <2.92 <5.71
SB-29 12/19/2016 7.5-10 742 146
SB-31 12/19/2016 5-7.5 <2.34 <5.26
TP-1A 12/19/2016 10 <2.07 <48.6
TP-1B 12/19/2016 13 <1.96 <4.98
TP-10B 12/19/2016 7 <2 <4.78
Notes: 1 - N/A = Not Applicable or Sampled.
2 - Results in bold and shaded exceed NCDEQ Action Level.
3 - bls = Below Land Surface.
4 - Results are in mg/kg (milligrams per kilogram).
5 - Soil samples were collected 12/19/16.
6 - TPH = Total Petroleum Hydrocarbons.
7 - BDL = Below Detection Limits

TABLE 1A
SUMMARY OF SOIL ANALYTICAL RESULTS
Reman Properties LLC
270 MONCURE PITTSBORO ROAD
PITTSBORO, CHATHAM COUNTY, NORTH CAROLINA
WR Project # 02160652.0
NCDEQ ACTION LEVEL 50 100
8 - TPH/GRO = Results generated by EPA Method 8015D.
9 - TPH/DRO = Results generated by EPA Method 8015.
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67-64-1 71-43-2 104-51-8 135-98-8 108-90-7 67-66-3 95-50-1 100-41-4 98-82-8 99-87-6 1634-04-4 91-20-3 103-65-1 127-18-4 108-88-3 79-01-6 75-69-4 95-63-6 108-67-8 75-01-4 1330-20-7
PLANT SB-2 2.5-5 12/19/2016 <0.0636 <0.00127 <0.00127 <0.00127 <0.00127 <0.00636 <0.00127 <0.00127 <0.00127 <0.00127 <0.00127 <0.00636 <0.00127 <0.00127 <0.00636 <0.00127 <0.00636 <0.00127 <0.00127 <0.00127 <0.00382
PLANT SB-3 5-6 12/19/2016 <0.0616 <0.00123 <0.00123 <0.00123 <0.00123 <0.00616 <0.00123 <0.00123 <0.00123 <0.00123 <0.00123 <0.00616 <0.00123 <0.00123 <0.00616 <0.00123 <0.00616 <0.00123 <0.00123 <0.00123 <0.0037
PLANT SB-4 7.5-10 12/19/2016 <0.0583 <0.00117 <0.00117 <0.00117 <0.00117 <0.00583 <0.00117 <0.00117 <0.00117 <0.00117 <0.00117 <0.00583 <0.00117 <0.00117 <0.00583 <0.00117 <0.00583 <0.00117 <0.00117 <0.00117 <0.0035
PLANT SB-5 2.5-5 12/19/2016 <0.0623 <0.00125 <0.00125 <0.00125 <0.00125 <0.00623 0.00247 <0.00125 <0.00125 <0.00125 <0.00125 <0.00623 <0.00125 <0.00125 <0.00623 <0.00125 <0.00623 <0.00125 <0.00125 <0.00125 <0.00374
PLANT SB-6 2.5-5 12/19/2016 <0.0633 <0.00127 <0.00127 <0.00127 <0.00127 <0.00633 <0.00127 <0.00127 <0.00127 <0.00127 <0.00127 <0.00633 <0.00127 <0.00127 <0.00633 <0.00127 <0.00633 <0.00127 <0.00127 <0.00127 <0.0038
PLANT SB-7 2.5-5 12/19/2016 0.295 <0.00135 <0.00135 <0.00135 <0.00135 <0.00676 <0.00135 <0.00135 <0.00135 <0.00135 <0.00135 <0.00676 <0.00135 <0.00135 <0.00676 <0.00135 <0.00676 <0.00135 <0.00135 <0.00135 <0.00406
PLANT SB-8 2.5-5 12/19/2016 0.0676 <0.00134 <0.00134 <0.00134 <0.00134 <0.00671 <0.00134 <0.00134 <0.00134 <0.00134 <0.00134 <0.00671 <0.00134 <0.00134 <0.00671 <0.00134 <0.00671 <0.00134 <0.00134 <0.00134 <0.00402
PLANT SB-9 2.5-5 12/19/2016 <0.0692 <0.00138 <0.00138 <0.00138 <0.00138 <0.00692 <0.00138 <0.00138 <0.00138 <0.00138 <0.00138 <0.00692 <0.00138 <0.00138 <0.00692 <0.00138 <0.00692 <0.00138 <0.00138 <0.00138 <0.00415
PLANT SB-10 7.5-10 12/19/2016 <0.0687 <0.00137 <0.00137 <0.00137 <0.00137 0.0564 <0.00137 <0.00137 <0.00137 <0.00137 <0.00137 <0.00687 <0.00137 <0.00137 <0.00687 <0.00137 <0.00687 <0.00137 <0.00137 <0.00137 <0.00412
PLANT SB-11 2.5-5 12/19/2016 <0.0683 <0.00137 <0.00137 <0.00137 <0.00137 <0.00683 <0.00137 <0.00137 <0.00137 <0.00137 <0.00137 <0.00683 <0.00137 <0.00137 <0.00683 <0.00137 <0.00683 <0.00137 <0.00137 <0.00137 <0.0041
PLANT SB-12 7.5-10 12/19/2016 <0.0613 <0.00123 <0.00123 <0.00123 <0.00123 <0.00613 <0.00123 <0.00123 <0.00123 <0.00123 <0.00123 <0.00613 <0.00123 <0.00123 <0.00613 <0.00123 <0.00613 <0.00123 <0.00123 <0.00123 <0.00368
PLANT SB-13 0-2.5 12/19/2016 <1.33 <0.0267 0.0459 0.0373 <0.0267 <0.133 <0.0267 <0.0267 <0.0267 0.0304 <0.0267 0.33 <0.0267 <0.0267 <0.133 <0.0267 <0.133 0.199 0.0544 <0.0267 <0.08
PLANT SB-14 2.5-5 12/19/2016 <0.0674 <0.00135 <0.00135 <0.00135 <0.00135 <0.00674 <0.00135 <0.00135 <0.00135 <0.00135 <0.00135 <0.00674 <0.00135 <0.00135 <0.00674 <0.00135 <0.00674 <0.00135 <0.00135 <0.00135 <0.00404
PLANT SB-15 2.5-5 12/19/2016 <0.0652 <0.0013 <0.0013 <0.0013 <0.0013 <0.00652 <0.0013 <0.0013 <0.0013 <0.0013 <0.0013 <0.00652 <0.0013 <0.0013 <0.00652 <0.0013 <0.00652 <0.0013 <0.0013 <0.0013 <0.00391
PLANT SB-16 5-7.5 12/19/2016 <0.0678 <0.00136 <0.00136 <0.00136 <0.00136 <0.00678 <0.00136 <0.00136 <0.00136 <0.00136 <0.00136 <0.00678 <0.00136 <0.00136 <0.00678 <0.00136 <0.00678 <0.00136 <0.00136 <0.00136 <0.00407
PLANT SB-17 5-7.5 12/19/2016 <0.0681 <0.00136 <0.00136 <0.00136 <0.00136 <0.00681 <0.00136 <0.00136 <0.00136 <0.00136 <0.00136 <0.00681 <0.00136 <0.00136 <0.00681 <0.00136 <0.00681 <0.00136 <0.00136 <0.00136 <0.00409
PLANT SB-18 7.5-10 12/19/2016 <0.0657 <0.00131 <0.00131 <0.00131 <0.00131 <0.00657 <0.00131 <0.00131 <0.00131 <0.00131 <0.00131 <0.00657 <0.00131 <0.00131 <0.00657 <0.00131 <0.00657 <0.00131 <0.00131 <0.00131 <0.00394
PLANT SB-19 2.5-5 12/19/2016 <0.0678 <0.00136 <0.00136 <0.00136 <0.00136 <0.00678 <0.00136 <0.00136 <0.00136 <0.00136 <0.00136 <0.00678 <0.00136 <0.00136 <0.00678 <0.00136 <0.00678 <0.00136 <0.00136 <0.00136 <0.00407
PLANT SB-20 2.5-5 12/19/2016 0.126 <0.00123 <0.00123 <0.00123 <0.00123 <0.00616 <0.00123 <0.00123 <0.00123 <0.00123 <0.00123 <0.00616 <0.00123 <0.00123 <0.00616 <0.00123 <0.00616 <0.00123 <0.00123 <0.00123 <0.0037
PLANT SB-21 5-7.5 12/19/2016 <0.0675 <0.00135 <0.00135 <0.00135 <0.00135 <0.00675 <0.00135 <0.00135 <0.00135 <0.00135 <0.00135 <0.00675 <0.00135 <0.00135 <0.00675 <0.00135 <0.00675 <0.00135 <0.00135 <0.00135 <0.00405
PLANT SB-22 7.5-10 12/19/2016 <0.0779 <0.00156 <0.00156 <0.00156 <0.00156 <0.00779 <0.00156 <0.00156 <0.00156 <0.00156 <0.00156 <0.00779 <0.00156 <0.00156 <0.00779 <0.00156 <0.00779 <0.00156 <0.00156 <0.00156 <0.00468
PLANT SB-24 2.5-5 12/19/2016 <0.0705 <0.00141 <0.00141 <0.00141 <0.00141 <0.00705 <0.00141 <0.00141 <0.00141 <0.00141 <0.00141 <0.00705 <0.00141 <0.00141 <0.00705 <0.00141 <0.00705 <0.00141 <0.00141 <0.00141 <0.00423
TRUCK SHOP SB-25 5-7.5 12/19/2016 <0.0624 <0.00125 <0.00125 <0.00125 <0.00125 <0.00624 <0.00125 <0.00125 <0.00125 <0.00125 <0.00125 <0.00624 <0.00125 <0.00125 <0.00624 <0.00125 <0.00624 <0.00125 <0.00125 <0.00125 <0.00374
TRUCK SHOP SB-28 5-7.5 12/19/2016 <0.0713 <0.00143 <0.00143 <0.00143 <0.00143 <0.00713 <0.00143 <0.00143 <0.00143 <0.00143 <0.00143 <0.00713 <0.00143 <0.00143 <0.00713 <0.00143 <0.00713 <0.00143 <0.00143 <0.00143 <0.00428
TRUCK SHOP SB-29 7.5-10 12/19/2016 <22.5 <0.45 5.16 1.85 <0.45 <2.25 <0.45 6.79 3.07 1.02 <0.45 24.7 14.5 <0.45 <2.25 <0.45 <2.25 2.89 26.5 <0.45 <1.35
TRUCK SCALE SB-31 5-7.5 12/19/2016 0.197 <0.00132 <0.00132 <0.00132 <0.00132 <0.00658 <0.00132 0.00161 <0.00132 <0.00132 <0.00132 <0.00658 <0.00132 <0.00132 <0.00658 <0.00132 <0.00658 <0.00132 <0.00132 <0.00132 0.0123
BURIED DEBRIS TP-1A 10 12/20/2016 <0.0608 <0.00122 <0.00122 <0.00122 0.00548 <0.00608 <0.00122 <0.00122 0.00214 <0.00122 <0.00122 <0.00608 <0.00122 <0.00122 <0.00608 <0.00122 3.9 <0.00122 <0.00122 <0.00122 <0.00365
BURIED DEBRIS TP-1B 13 12/20/2016 <0.0623 <0.00125 <0.00125 <0.00125 <0.00125 <0.00623 <0.00125 <0.00125 <0.00125 <0.00125 <0.00125 <0.00623 <0.00125 <0.00125 <0.00623 <0.00125 <0.00623 <0.00125 <0.00125 <0.00125 <0.00374
BURIED DEBRIS TP-10B 7 12/20/2016 <0.0597 <0.00119 <0.00119 <0.00119 <0.00119 <0.00597 <0.00119 <0.00119 <0.00119 <0.00119 <0.00119 <0.00597 <0.00119 <0.00119 <0.00597 <0.00119 <0.00597 <0.00119 <0.00119 <0.00119 <0.00358
12,200 1.2 108 145 56 0.32 360 5.8 268 NA 47 3.8 264 16.2 818 0.82 1,230 11.6 156 0.059 116
100,000 5.1 108 145 260 1.4 376 25 268 NA 210 17 264 78 818 3.8 1,230 48 182 1.7 260
24 0.0073 2.4 2.2 0.44 0.34 0.24 8.1 1.3 0.68 0.085 0.21 1.5 0.005 5.5 0.018 24 6.7 6.7 0.00019 6.1
Notes:
1)
2)
3)
4)
Result
Result
Result
Reman Properties LLC
SUMMARY OF SOIL ANALYTICAL RESULTS
Area
= Result Exceeds IHSB PSRG Industrial Concentration
Sample
ID
IHSB PSRGs = Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (March 2015)
WR Project # 02160652.0
= Result Exceeds Laboratory Detection Limits
= Result Exceeds IHSB PSRG Residential Concentration
IHSB PSRGs - Residential
IHSB PSRGs - Industrial
IHSB PSRGs - Soil-to-Groundwater
TABLE 1B
270 MONCURE PITTSBORO ROAD
8260B - Volatile Organic CompoundsAnalytical Method
Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
Sample
Depth
(Feet BLS)
Date
Collected
All results provided in mg/kg (milligrams per kilogram) or parts per million.
PITTSBORO, CHATHAM COUNTY, NORTH CAROLINA
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PLANT SB-2 2.5-5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-3 5-6 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-4 7.5-10 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-5 2.5-5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-6 2.5-5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-7 2.5-5 12/19/2016 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446
PLANT SB-8 2.5-5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-9 2.5-5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-10 7.5-10 12/19/2016 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453 <0.0453
PLANT SB-11 2.5-5 12/19/2016 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 <0.0451 0.0845 <0.0451
PLANT SB-12 7.5-10 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-13 0-2.5 12/19/2016 0.103 <0.0445 <0.0445 <0.0445 <0.0445 <0.0445 <0.0445 <0.0445 <0.0445 <0.0445 0.136 <0.0445 0.0738 0.293 <0.0445
PLANT SB-14 2.5-5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-15 2.5-5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-16 5-7.5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-17 5-7.5 12/19/2016 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449
PLANT SB-18 7.5-10 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-19 2.5-5 12/19/2016 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447
PLANT SB-20 2.5-5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-21 5-7.5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
PLANT SB-22 7.5-10 12/19/2016 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514 <0.0514
PLANT SB-24 2.5-5 12/19/2016 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465 <0.0465
TRUCK SHOP SB-25 5-7.5 12/19/2016 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412 <0.0412
TRUCK SHOP SB-28 5-7.5 12/19/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
TRUCK SHOP SB-29 7.5-10 12/19/2016 <0.0424 <0.0424 <0.0424 <0.0424 <0.0424 <0.0424 <0.0424 <0.0424 <0.0424 <0.0424 <0.0424 <0.0424 3.36 <0.0424 <0.0424
TRUCK SCALE SB-31 5-7.5 12/19/2016 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434
BURIED DEBRIS TP-1A 10 12/20/2016 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01 <2.01
BURIED DEBRIS TP-1B 13 12/20/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
BURIED DEBRIS TP-10B 7 12/20/2016 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
720 3,600 0.16 0.16 1.6 NL 0.016 16 0.016 480 460 0.16 3.8 NL 360
9,000 46,000 2.9 2.9 29 NL 0.29 290 0.29 6,000 6,000 2.9 17 68 4,600
8.4 660 0.18 0.6 5.9 NL 0.059 18 0.19 330 56 2 0.21 NL 220
Notes:
1)
2)
3)
4)
NA
Result
Result
Result
= Not Analyzed by Method Shown
= Result Exceeds Laboratory Detection Limits
= Result Exceeds IHSB PSRG Residential Concentration
All results provided in mg/kg (milligrams per kilogram) or parts per million.
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
IHSB PSRGs = Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (March 2015)
Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
= Result Exceeds IHSB PSRG Industrial Concentration
Area Sample
ID
Sample
Depth
(Feet BLS)
Date
Collected
IHSB PSRGs - Residential
IHSB PSRGs - Industrial
IHSB PSRGs - Soil-to-Groundwater
TABLE 1C
SUMMARY OF SOIL ANALYTICAL RESULTS
Reman Properties LLC
270 MONCURE PITTSBORO ROAD
PITTSBORO, CHATHAM COUNTY, NORTH CAROLINA
Analytical Method EPA-8270D
WR Project # 02160652.0
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71-43-2 108-86-1 104-51-8 135-98-8 67-66-3 107-06-2 156-59-2 108-20-3 100-41-4 98-82-8 99-87-6 1634-04-4 91-20-3 103-65-1 100-42-5 127-18-4 108-88-3 79-01-6 95-63-6 526-73-8 108-67-8 75-01-4 1330-20-7
MW-1 12/21/2016 <1 <1 <1 1.3 <5 <1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3
MW-2 12/20/2016 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3
MW-3 12/22/2016 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3
MW-4 12/20/2016 <1 <1 <1 1.99 <5 <1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3
MW-5 12/20/2016 <1 <1 <1 <1 204 <1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3
MW-6 12/22/2016 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3
MW-7 12/22/2016 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3
MW-A1 12/21/2016 92.6 2.7 4.75 4.69 <5 <1 <1 11.7 52 17.4 <1 102 81.5 26.5 <1 <1 6.98 <1 24 9.99 1.71 <1 26.2
MW-B2 12/21/2016 332 <1 14.9 8.9 <5 <1 <1 2.7 334 53.6 4.17 211 328 144 1.49 <1 28.6 <1 211 56.8 109 <1 147
1 NL 70 70 70 0.4 70 70 600 70 25 20 6 70 70 0.7 600 3 400 NL 400 0.03 500
5,000 NL 6,900 8,500 70,000 400 70,000 70,000 84,500 25,000 11,700 20,000 6,000 30,000 70,000 700 260,000 3,000 28,500 NL 25,000 30 85,500
Notes:
1)
2)
3)
4)
5)
NA
Result = Result Exceeds Laboratory Detection Limits
Result = Result Exceeds 2L Standard
Result = Result Exceeds GCL Value
= Not Analyzed by Method Shown
Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
Reman Properties LLC
Analytical Method
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
TABLE 2A
EPA-8260B - Volatile Organic Compounds
NC 2L Standard - North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L
GCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for Groundwater
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
All results provided in µg/L (micrograms per liter) or parts per billion
PITTSBORO, CHATHAM COUNTY, NORTH CAROLINA
270 MONCURE PITTSBORO ROAD
Sample
ID
Date
Collected
NC 2L Standard
GCLs for Groundwater
WR Project # 02160652.0
Page 1 of 1
EPA-7470A EPA-350.1
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83-32-9 86-73-7 91-20-3 85-01-8 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7782-49-2 7440-22-4 7439-97-6 ----7439-97-6
MW-1 12/21/2016 <1 <1 <1 <1 <10 36.6 <2 <10 <5 <10 <5 <0.2 <100 <100 <100 <100 109
MW-2 12/20/2016 <1 <1 <1 <1 <10 10.5 <2 <10 <5 <10 <5 <0.2 <100 <100 <100 <100 <100
MW-3 12/22/2016 <1 <1 <1 <1 <10 <5 <1 <10 <5 <10 <5 <0.2 <100 <100 <100 <100 <100
MW-4 12/20/2016 1.04 1.34 <1 1.8 <10 <5 <2 <10 <5 <10 <5 <0.2 <100 <100 <100 153 <100
MW-5 12/20/2016 <1 <1 <1 <1 <10 22.8 <2 <10 <5 <10 <5 <0.2 <100 <100 <100 <100 <100
MW-6 12/22/2016 <1 <1 <1 <1 <10 21.1 <1 <10 <5 <10 <5 <0.2 <100 <100 <100 <100 <100
MW-7 12/22/2016 <1 <1 <1 <1 <10 19.6 <1 <10 <5 <10 <5 <0.2 <100 <100 <100 <100 259
MW-A1 12/21/2016 2.4 2.51 46.3 4.71 <10 10.8 <2 <10 6.38 <10 <5 <0.2 1,390 <100 <100 635 NA
MW-B2 12/21/2016 <1 <1 199 <1 <10 24.8 <2 <10 5.18 <10 <5 <0.2 4,000 <100 <100 1,239 NA
80 280 6 210 NL 700 NL 10 15 NL 20 NL NL 700 NL 10 1,500
2120 950 15,500 410 NL 700,000 NL 10,000 15,000 NL 20,000 NL NL 700,000 NL 10,000 NL
Notes:
1)
2)
3)
4)
5)
NA
Result = Result Exceeds Laboratory Detection Limits
Result = Result Exceeds 2L Standard
Result = Result Exceeds GCL Value
= Not Analyzed by Method Shown
EPA-8270D SM6010C
Sample
ID
Date
Collected
Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
NC 2L Standard
GCLs for Groundwater
All results provided in µg/L (micrograms per liter) or parts per billion
NC 2L Standard - North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L
TABLE 2B
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Reman Properties LLC
270 MONCURE PITTSBORO ROAD
PITTSBORO, CHATHAM COUNTY, NORTH CAROLINA
WR Project # 02160652.0
GCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for Groundwater
Analytical Method
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
MADEP VPH / MADEP EPHMADEP VPH / MADEP EPH
Page 1 of 1
Easting Northing
MW-1 12/20/2016 2 25 10 10 - 25 NM NM NM ---1,948,202.74 710,886.08
MW-2 12/20/2016 2 20 10 10 - 20 NM 12/20/2016 10.41 ---1,948,209.11 710,781.89
MW-3 12/21/2016 2 25 10 10 - 25 NM 12/22/2016 8.35 ---1,948,136.79 710,368.59
MW-4 12/19/2016 2 39 24 24 - 39 NM 12/20/2016 16.95 ---1,948,200.17 710,706.84
MW-5 12/19/2016 2 30 15 15 - 30 NM 12/19/2016 20.64 ---1,948,110.44 710,781.00
MW-6 12/21/2016 2 30 15 15 - 30 NM 12/21/2016 22.92 ---1,948,020.22 710,761.32
MW-7 12/20/2016 2 30 10 10 - 30 NM 12/21/2016 26.34 ---1,947,965.96 710,813.37
1)
2)
All measurements shown in feet, unless otherwise indicated.
Depth-to-Water
from
Top-of-Casing
Total
Depth
Well
Casing
Depth
Date Installed
NM Denotes "Not Measured"
Notes:
Top-of-Casing
Elevation
TABLE 3
270 MONCURE PITTSBORO ROAD
MONITORING WELL CONSTRUCTION INFORMATION
Well
Casing
Diameter
(inches)
Free Product
Thickness
Reman Properties LLC
PITTSBORO, CHATHAM COUNTY, NORTH CAROLINA
WR Project # 02160652.0
Well Coordinates
(NC State Plane NAD 83 Feet)Date Water
Level
Measured
Screened
IntervalWell ID
Page 1 of 1

Appendix A
Boring Logs

Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 1.0
Boring Refusal @ 1' BLS
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Concrete
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-1 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'1.14 1.40
2.5' - 5.0'1.21 1.72
5.0 7.5
5.0' - 7.5'1.81 1.30
Boring Refusal @ 7.5' BLS
Sampled 2.5'-5.0' for TPH GRO/DRO and VOCs
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
NR=No reading ppm=parts per million
Orange, tan, red clayey SILT, 10-20% clays,
decreasing with depth to silt, dry to slightly moist, no odor
(Field USCS Classification)
Orange, tan, red clayey SILT, 20-30% clays,
trace sands, dry to slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-2 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'1.03 2.12
2.5' - 5.0'2.39 1.00
2.5 5.5
5.0' - 6.0'1.07 1.59
5.5 6.0
Boring Refusal @ 7.5' BLS
Sampled 5'-6' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
PWR
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, silty CLAY, 20-30% silt,
dry to slightly moist, no odor
Tan, red, orange clayey SILT, 30-40% clays, trace fine sand,
slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-3 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'0.00 0.15
2.5' - 5.0'0.00 0.02
5.0 7.5
5.0' - 7.5'0.00 0.12
7.5' - 10.0'0.01 0.37
Boring Terminated @ 10.0' BLS
Sampled 7.5'-10.0' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Tan, orange, red silty CLAY, 30-40% silt,
dry to slightly moist, no odor
Tan, red clayey SILT, 20-30% clays, trace very fine sand,
slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-4 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 7.0 0' - 2.5'0.98 1.85
2.5' - 5.0'1.15 1.65
7.0 7.5
5.0' - 6.0'2.00 1.95
Boring Refusal @ 7.5' BLS
Sampled 2.5'-5.0' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Tan, gray, clayey SILT, 20-30% clays,
dry to slightly moist, no odor
PWR
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-5 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'0.00 0.00
2.5' - 5.0'0.32 0.92
2.5 7.5
5.0' - 7.5'0.00 0.68
7.5 10.0 7.5' - 10.0'0.23 0.00
Boring Terminated @ 10.0' BLS
Sampled 2.5'-5.0' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Gray, tan, orange clayey SILT, decreasing clay with depth
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, orange, tan silty CLAY transitions to clayey SILT,
30-40% clays,dry to slightly moist, no odor
Tan, gray SILT, 20-30% clays, trace very fine sand, slightly
moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-6 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'0.00 1.06
2.5' - 5.0'1.01 0.92
2.5 5.0
5.0' - 7.5'0.00 0.46
5.0 10.0 7.5' - 10.0'0.01 0.59
Boring Terminated @ 10.0' BLS
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Sampled 2.5'-5.0' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
Tan, red, gray SILT, 20-30% clays, trace very fine sand,
slightly moist, no odor
(Field USCS Classification)
Red, tan, orange CLAY, 10-20% silt,dry to slightly moist, no
odor
Red, orange, tan clayey SILT, 30-40% clays,
slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-7 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'0.82 1.01
2.5' - 5.0'0.32 0.68
5.0 7.5
5.0' - 7.5'0.00 0.43
7.5 10.0 7.5' - 10.0'0.01 0.36
Boring Terminated @ 10.0' BLS
Sampled 2.5'-5.0' for TPH GRO/DRO and VOCs
SOIL BORING LOG
SB-8 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, tan, orange CLAY, trace very fine sand,
10-20% silt,dry to slightly moist, no odor
Red, orange, tan silty CLAY transitions to clayey SILT,
decreasing fines with depth
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Tan, red, clayey SILT, 20-30% clays, slightly moist, no odor
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'1.05 1.11
2.5' - 5.0'1.46 1.06
5.0 7.5
5.0' - 7.5'1.66 0.93
7.5 10.0 7.5' - 10.0'1.43 1.05
Boring Terminated @ 10.0' BLS
Sampled 2.5'-5.0' for TPH GRO/DRO and VOCs
SOIL BORING LOG
SB-9 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, tan, orange CLAY, trace very fine sand,
10-20% silt,dry to slightly moist, no odor
Red, orange, tan silty CLAY transitions to clayey SILT,
decreasing fines with depth
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Tan, red, clayey SILT, 20-30% clays, slightly moist, no odor
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'0.82 2.99
2.5' - 5.0'0.76 1.00
2.5 10.0
5.0' - 7.5'0.62 2.84
10.0 16.0 7.5' - 10.0'1.08 4.40
10' - 12.5'0.81 2.04
12.5' - 15.0'1.11 3.03
Boring Refusal @ 16.0' BLS
SOIL BORING LOG
SB-10 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
(Field USCS Classification)
Red, orange, brown silty CLAY, trace very fine sand,
20-30% silt,dry to slightly moist, no odor
Red, orange, brown clayey SILT, slightly moist - moist,
30-40% clay, no odor,
Tan, red, clayey SILT, 30-40% clays,moist, no odor
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Sampled 7.5'-10.0' for TPH GRO/DRO, VOCs, & SVOCs
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'0.72 1.92
2.5' - 5.0'1.67 3.09
2.5 17.5
5.0' - 7.5'0.34 1.75
17.5 19.0 7.5' - 10.0'0.06 1.58
10' - 12.5'0.82 0.47
12.5' - 15.0'0.81 0.45
15' - 17.5'0.35 0.55
17.5' - 19'1.15 0.57
Boring Refusal @ 19.0' BLS
SOIL BORING LOG
SB-11 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
(Field USCS Classification)
Red, orange, brown silty CLAY, trace very fine sand,
20-30% silt,dry to slightly moist, no odor
Tan, orange, red clayey SILT, slightly moist - moist,
30-40% clay, decreasing clay with depth, no odor,
Tan SILT, slightly moist, no odor, trace very fine sand.
Sampled 2.5'-5.0' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'0.00 16.13
2.5' - 5.0'0.28 12.64
2.5 10.0
5.0' - 7.5'0.00 23.68
7.5' - 10.0'0.33 24.08
Boring Terminated @ 10.0' BLS
Sampled 7.5'-10.0' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, orange, brown silty CLAY,
dry to slightly moist, no odor
Tan, orange, red clayey SILT, slightly moist,
20-30% clay, decreasing clay with depth, no odor,
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-12 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'15.05 46.48
2.5' - 5.0'6.67 35.49
2.5 7.5
5.0' - 7.5'1.23 56.53
7.5 10.0 7.5' - 10.0'0.71 57.00
Boring Terminated @ 10.0' BLS
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Sampled 0'-2.5' for TPH GRO/DRO, VOCs, & SVOCs
Orange, red, tan, silty CLAY, moist, no odor
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, orange, brown silty CLAY,
dry to slightly moist, petroleum odor
Tan, orange, red clayey SILT, slightly moist,
petroleum odor,
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-13 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'1.73 0.95
2.5' - 5.0'0.93 2.05
2.5 10.0
5.0' - 7.5'0.17 0.35
7.5' - 10.0'0.05 0.67
Boring Terminated @ 10.0' BLS
Sampled 2.5'-5.0' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, tan, silty CLAY, slightly moist, no odor
Tan, orange clayey SILT, slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-14 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'0.11 1.02
2.5' - 5.0'1.11 1.36
2.5 10.0
5.0' - 7.5'1.04 0.78
7.5' - 10.0'0.93 1.05
Boring Terminated @ 10.0' BLS
Sampled 2.5'-5.0' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Orange, red, tan, silty CLAY, dry to slightly moist, no odor
Tan clayey SILT, slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-15 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'0.00 1.03
2.5' - 5.0'1.07 1.55
2.5 10.0
5.0' - 7.5'1.28 3.57
7.5' - 10.0'1.18 0.83
Boring Terminated @ 10.0' BLS
Sampled 5.0'-7.5' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Orange, red, tan, silty CLAY, dry to slightly moist, no odor
Tan clayey SILT, slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-16 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5 0' - 2.5'1.82 1.38
2.5' - 5.0'1.72 0.83
2.5 10.0
5.0' - 7.5'1.39 1.37
7.5' - 10.0'1.28 0.78
Boring Terminated @ 10.0' BLS
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Sampled 5.0'-7.5' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Orange, red, tan, silty CLAY, dry to slightly moist, no odor
Tan clayey SILT, slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-17 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.5
0' - 5.0'1.22 0.79
2.5 7.5
5.0' - 7.5'0.86 1.76
7.5 10.0 7.5' - 10.0'1.62 1.39
Boring Terminated @ 10.0' BLS
Sampled 7.5'-10.0' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Tan, red SILT, slightly moist, no odor
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, tan, silty CLAY, slightly moist, no odor, low plasticity
Red, tan, clayey SILT, slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-18 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'1.41 1.03
2.5' - 5.0'1.98 0.99
5.0 10.0
5.0' - 7.5'1.47 1.28
7.5' - 10.0'1.43 1.66
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Sampled 2.5'-5.0' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, silty CLAY, dry to slightly moist, no odor,
low plasticity
Tan, red, orange, clayey SILT, slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-19 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'1.33 0.29
2.5' - 5.0'0.98 0.84
5.0 10.0
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Sampled 2.5'-5.0' for TPH GRO/DRO and VOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, orange, brown, silty CLAY, slightly moist - moist
no odor
Orange, red, tan, silty CLAY, saturated
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-20 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 7.5 0' - 2.5'1.57 0.33
2.5' - 5.0'1.61 1.98
7.5 10.0
5.0' - 7.5'1.19 1.94
7.5' - 10.0'1.02 1.72
Boring Terminated @ 10.0' BLS
Sampled 5.0'-7.5' for TPH GRO/DRO and VOCs
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Red, tan, silty CLAY, slightly moist, no odor
Red, tan, clayey SILT, slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-21 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0
0' - 5.0'1.02 0.23
5.0 7.5
5.0' - 7.5'0.32 1.84
7.5 10.0 7.5' - 10.0'0.96 1.86
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Red, orange, tan, clayey SILT, moist, no odor
Sampled 7.5'-10.0' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, tan silty CLAY, dry to slightly moist,
no odor, low plasticity
Tan, orange, clayey SILT, saturated
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-22 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'0.13 2.01
2.5' - 5.0'0.24 1.08
5.0 9.0
5.0' - 7.5'1.99 1.81
7.5' - 10.0'2.27 1.83
Boring Terminated @ 9.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Not Sampled
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, tan, brown silty CLAY, dry to slightly moist,
no odor
Red, tan SILT, slightly moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-23 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 10.0 0' - 2.5'1.98 8.10
2.5' - 5.0'1.68 10.62
5.0' - 7.5'1.65 1.11
7.5' - 10.0'1.66 0.08
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Sampled 2.5'-5.0' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, brown silty CLAY, dry to slightly moist,
no odor, low plasticity
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-24 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'0.91 1.98
2.5' - 5.0'0.35 0.89
5.0 10.0
5.0' - 7.5'0.73 1.14
7.5' - 10.0'1.55 0.38
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Sampled 5.0'-7.5' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, orange, tan silty CLAY, dry to slightly moist,
no odor
Orange, red, tan clayey SILT, moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-25 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'1.22 0.98
2.5' - 5.0'4.01 1.07
5.0 10.0
5.0' - 7.5'0.45 0.19
7.5' - 10.0'1.25 0.64
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Not Sampled
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, orange, tan silty CLAY, dry to slightly moist,
no odor
Orange, red, tan clayey SILT, moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-26 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'1.32 3.58
2.5' - 5.0'0.24 1.83
5.0 10.0
5.0' - 7.5'0.00 2.15
7.5' - 10.0'0.23 1.84
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Not Sampled
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, orange, tan silty CLAY, dry to slightly moist,
no odor
Orange, red, tan clayey SILT, moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-27 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'1.00 0.98
2.5' - 5.0'1.58 1.06
5.0 10.0
5.0' - 7.5'1.03 2.58
7.5' - 10.0'1.86 2.12
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Sampled 5.0'-7.5' for TPH GRO/DRO and VOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, orange, tan silty CLAY, dry to slightly moist,
no odor
Orange, red, tan clayey SILT, moist, no odor
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-28 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0 0' - 2.5'4.26 3.33
2.5' - 5.0'35.11 48.22
5.0 10.0
5.0' - 7.5'37.22 96.66
7.5' - 10.0'752.00 3,602
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Sampled 7.5'-10.0' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Red, brown, clayey SILT, dry to slightly moist,
petroleum odor
Red, tan clayey SILT, moist, strong petroleum odor,
green/gray staining
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-29 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 10.0 0' - 2.5'0.12 4.10
2.5' - 5.0'0.39 6.85
5.0' - 7.5'0.18 4.76
7.5' - 10.0'1.12 5.34
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Not Sampled
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Orange, tan, red silty CLAY, dry to slightly moist
no odor, low plasticity
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-30 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 10.0 0' - 2.5'1.39 6.81
2.5' - 5.0'0.61 4.98
5.0' - 7.5'2.93 8.69
7.5' - 10.0'1.35 5.91
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Sampled 5.0'-7.5' for TPH GRO/DRO, VOCs, & SVOCs
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Orange, tan, red silty CLAY, dry to slightly moist
no odor, low plasticity
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-31 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 10.0 0' - 2.5'0.93 0.36
2.5' - 5.0'0.95 1.02
5.0' - 7.5'0.87 0.16
7.5' - 10.0'1.11 0.36
Boring Terminated @ 10.0' BLS
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
BGS=Below ground surface USCS=Unified Soil Classification System
TOC=Top of Casing GW=Ground Water
El=Elevation
Page 1 of 1
Not Sampled
NR=No reading ppm=parts per million
NA=Not Applicable GW=Ground Water
(Field USCS Classification)
Orange, tan, red silty CLAY, dry to slightly moist
no odor, low plasticity
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
SOIL BORING LOG
SB-32 Reman Properties LLC 02160652.0
12/19/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Job Name
Site Loc.
Driller
From PID FID
Notes Notes
0.0
0.0-6.0 ft Grout
5.0 6.0-8.0 ft Bentonite
7.0
8.0-25.0 ft Sand
Notes:
1)
Page 1 of 1
Well Construction(Field USCS Classification)
Mike Fekete Quantex, Inc.GW EL Not Surveyed
NC NAD83 Northing:
WELL CONSTRUCTION LOG
MW-1 Reman Properties LLC Job #02160652.0
270 Moncure Pittsboro Rd.; Pittsboro,NC
Depth in Feet Soil Description
December 20, 2016 TOC EL Not Surveyed
25.0
Clayey SILT, orange, dry
Light brown, orange clayey
SILT
Gray granitic ROCK
10.0-25.0 ft
2" 10-Slot Well Screen
7.0
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Well ID
Date
W&R Rep
NC NAD83 Easting:
VOC's (ppm)
Boring Terminated @ 25' BLS
Ground Surface
BLS = Below land surface
0-10.0 ft
2" PVC Casing
To
5.0
WithersRavenel
Engineers | Planners | Surveyors
Job Name
Site Loc.
Driller
From PID FID
Notes Notes
0.0
0.0-6.0 ft Grout
5.0 6.0-8.0 ft Bentonite
7.5
8.0-20.0 ft Sand
Notes:
1)
Page 1 of 1
WELL CONSTRUCTION LOG
Well ID MW-2 Reman Properties LLC Job #02160652.0
W&R Rep Mike Fekete Quantex, Inc.GW EL Not Surveyed
Date December 20, 2016 270 Moncure Pittsboro Rd.; Pittsboro,NC TOC EL Not Surveyed
NC NAD83 Easting:NC NAD83 Northing:
Depth in Feet VOC's (ppm)Soil Description Well ConstructionTo(Field USCS Classification)
Orange, tan, red clayey SILT,
20-30% clays
dry to slightly moist,
no odor
Ground Surface
0-10.0 ft
2" PVC Casing5.0
Orange, tan, red clayey SILT,
10-20% clays,
dry to slightly moist,
no odor
7.5
Gray granitic ROCK
10.0-20.0 ft
2" 10-Slot Well Screen
20.0
Boring Terminated @ 30' BLS
BLS = Below land surface
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
WithersRavenel
Engineers | Planners | Surveyors
Job Name
Site Loc.
Driller
From PID FID
Notes Notes
0.0-6.0 ft Grout
0.0
6.0-8.0 ft Bentonite
11.0
13.0
8.0-25.0 ft Sand
Notes:
1)
Page 1 of 1
WELL CONSTRUCTION LOG
Well ID MW-3 Reman Properties LLC Job #02160652.0
W&R Rep Mike Fekete Quantex, Inc.GW EL Not Surveyed
Date December 21, 2016 270 Moncure Pittsboro Rd.; Pittsboro,NC TOC EL Not Surveyed
NC NAD83 Easting:NC NAD83 Northing:
Depth in Feet VOC's (ppm)Soil Description Well ConstructionTo(Field USCS Classification)
Ground Surface
0-10.0 ft
2" PVC Casing
10.0-25.0 ft
2" 10-Slot Well Screen
25.0
11.0
Brown, clayey SILT
Brown silty SAND, PWR13.0
Gray granitic ROCK
Boring Terminated @ 25' BLS
BLS = Below land surface
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
WithersRavenel
Engineers | Planners | Surveyors
Job Name
Site Loc.
Driller
From PID FID
Notes Notes
0.0
7.5 0.0-20 ft Grout
20.0-22.0 ft Bentonite
10.0
22.0-39.0 ft Sand
Notes:
1)
Page 1 of 1
WELL CONSTRUCTION LOG
Well ID MW-4 Reman Properties LLC Job #02160652.0
W&R Rep Mike Fekete Quantex, Inc.GW EL Not Surveyed
Date December 19, 2016 270 Moncure Pittsboro Rd.; Pittsboro,NC TOC EL Not Surveyed
NC NAD83 Easting:NC NAD83 Northing:
Depth in Feet VOC's (ppm)Soil Description Well ConstructionTo(Field USCS Classification)
Red, orange, tan, clayey SILT
Gray, orange SILT, PWR
Gray granitic ROCK
24.0-39.0 ft
2" 10-Slot Well Screen
39.0
Ground Surface
0-24.0 ft
2" PVC Casing7.5
10.0
Boring Terminated @ 39' BLS
BLS = Below land surface
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
WithersRavenel
Engineers | Planners | Surveyors
Job Name
Site Loc.
Driller
From PID FID
Notes Notes
0.0
0.0-11.0 ft Grout
5.0
11.0-13.0 ft Bentonite
17.5
13.0-30.0 ft Sand
Notes:
1)
Page 1 of 1
WELL CONSTRUCTION LOG
Well ID MW-5 Reman Properties LLC Job #02160652.0
W&R Rep Mike Fekete Quantex, Inc.GW EL Not Surveyed
Date December 19, 2016 270 Moncure Pittsboro Rd.; Pittsboro,NC TOC EL Not Surveyed
NC NAD83 Easting:NC NAD83 Northing:
Depth in Feet VOC's (ppm)Soil Description Well ConstructionTo(Field USCS Classification)
Red, orange silty CLAY
17.5 Red, orange, tan clayey SILT
Gray granitic ROCK
15.0-30.0 ft
2" 10-Slot Well Screen
30.0
Ground Surface
0-15.0 ft
2" PVC Casing5.0
Boring Terminated @ 30' BLS
BLS = Below land surface
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
WithersRavenel
Engineers | Planners | Surveyors
Job Name
Site Loc.
Driller
From PID FID
Notes Notes
0.0
0.0-11.0 ft Grout
5.0
11.0-13.0 ft Bentonite
17.5
13.0-30.0 ft Sand
Notes:
1)
Page 1 of 1
WELL CONSTRUCTION LOG
Well ID MW-6 Reman Properties LLC Job #02160652.0
W&R Rep Mike Fekete Quantex, Inc.GW EL Not Surveyed
Date December 21, 2016 270 Moncure Pittsboro Rd.; Pittsboro,NC TOC EL Not Surveyed
NC NAD83 Easting:NC NAD83 Northing:
Depth in Feet VOC's (ppm)Soil Description Well ConstructionTo(Field USCS Classification)
Red, orange silty CLAY
Ground Surface
0-15.0 ft
2" PVC Casing5.0
Red, orange, tan clayey SILT17.5
15.0-30.0 ft
2" 10-Slot Well Screen
Gray granitic ROCK
30.0
Boring Terminated @ 30' BLS
BLS = Below land surface
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
WithersRavenel
Engineers | Planners | Surveyors
Job Name
Site Loc.
Driller
From PID FID
Notes Notes
0.0
0.0-6.0 ft Grout
6.0-8.0 ft Bentonite
5.0
10.0
8.0-30.0 ft Sand
Notes:
1)
Page 1 of 1
WELL CONSTRUCTION LOG
Well ID MW-7 Reman Properties LLC Job #02160652.0
W&R Rep Mike Fekete Quantex, Inc.GW EL Not Surveyed
Date December 20, 2016 270 Moncure Pittsboro Rd.; Pittsboro,NC TOC EL Not Surveyed
NC NAD83 Easting:NC NAD83 Northing:
Depth in Feet VOC's (ppm)Soil Description Well ConstructionTo(Field USCS Classification)
Ground Surface
0-10.0 ft
2" PVC Casing5.0
10.0
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
10.0-30.0 ft
2" 10-Slot Well Screen
30.0
Red, orange silty CLAY
Orange red, clayey SILT
Brown silty SAND, PWR
Boring Terminated @ 30' BLS
BLS = Below land surface
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.0
2.0 11.0 10'2.33 194
11.0 13.0 13'1.94 23.75
Excavation Terminated @ 13' BLS
TP-1A collected @ 10' for TPH GRO/DRO, VOCs, and SVOCs
TP-1B collected @ 13' for TPH GRO/DRO and VOCs
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Buried Debris: Metal, plastic, car parts, Styrofoam,
wood, cinder blocks
Brown, silty SAND
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-1 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.0
2.0 7.0 10'0.33 1.26
7.0 10.0
Excavation Terminated @ 10' BLS
Not Sampled
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Brown, clayey SILT
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Buried Debris: Cement, wiring, wire cables
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-2 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.0
2.0 6.0 10'1.11 2.51
6.0 10.0
Excavation Terminated @ 10' BLS
Not Sampled
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Brown, clayey SILT
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Buried Debris: Cinder blocks, wiring, cloth, rebar
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-3 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.0
2.0 3.0 6'0.66 1.01
3.0 12.0
Excavation Terminated @ 12' BLS
Not Sampled
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Brown, clayey SILT
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Buried Debris: Minimal debris, 2 pieces of plastic
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-4 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.0
2.0 5.0 9'0.23 2.22
6.0 9.0
Excavation Terminated @ 9' BLS
Not Sampled
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Brown, clayey SILT
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Buried Debris: Insulated piping, cement, cinder blocks, plastic
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-5 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.0
2.0 4.0 7'1.15 2.26
4.0 7.0
Excavation Terminated @ 7' BLS
Not Sampled
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Brown, clayey SILT
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Buried Debris: Cement, metal, plastic
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-6 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.0
2.0 4.0 9'0.55 1.31
4.0 9.0
Excavation Terminated @ 9' BLS
Not Sampled
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Brown, clayey SILT
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Buried Debris: Cement, metal, Styrofoam, plastic, wood,
glass
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-7 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0
Excavation Terminated @ 5' BLS
Not Sampled
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-8 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 5.0
Excavation Terminated @ 5' BLS
Not Sampled
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-9 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors
Boring #Job Name Job #
Date Site Loc.Gnd EL
WR Rep Driller GW EL
Easting
From To Sample Interval PID FID
0.0 2.0
2.0 4.0 7'2.31 0.56
4.0 7.0
Excavation Terminated @ 7' BLS
TP-10B collected @ 10' for TPH GRO/DRO and VOCs
El=Elevation
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
Brown, silty SAND
NR=No reading ppm=parts per million
NA=Not Applicable
BGS=Below ground surface USCS=Unified Soil Classification System
(Field USCS Classification)
Brown, clayey SILT
Buried Debris: Styrofoam, plastic, metal, wood
Mike Fekete Quantex, Inc.NA
Northing
Depth in Feet Soil Description Total VOCs (in ppm)
TEST PIT EXCAVATION LOG
TP-10 Reman Properties LLC 02160652.0
12/20/2016 270 Moncure Pittsboro Rd.; Pittsboro,NC NA
WithersRavenel
Engineers | Planners | Surveyors

Appendix B
Well Construction Records

      
                           
 
               
 
               

           
 
  
 

  













     



    
  





      
                           
 
               
 
               

           
 
  
 

  













     



    
  





      
                           
 
               
 
               

           
 
  
 

  













     



    
  





      
                           
 
               
 
               

           
 
  
 

  













     



    
  





      
                           
 
               
 
               

           
 
  

 

  
 












     



    
  





      
                           
 
               
 
               

           
 
  
 

  













     



    
  





      
                           
 
               
 
               

           
 
  
 

  













     
 


    
  





Appendix C
Laboratory Report and Chain of Custody

ANALYTICAL REPORT
December 30, 2016
Withers & Ravenel Eng. - Standard
Sample Delivery Group: L880142
Samples Received:12/21/2016
Project Number:02160652.0
Description:Former Townsends Plant
Site:TOWNSEND
Report To:Patrick Farfour
115 MacKenan Drive
Cary, NC 27511
Entire Report Reviewed By:
December 30, 2016
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
December 31, 2016
Mark W. Beasley
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 4
⁴Cn: Case Narrative 10
⁵Sr: Sample Results 11
SB-2 L880142-01 11
SB-3 L880142-02 13
SB-4 L880142-03 15
SB-5 L880142-04 17
SB-6 L880142-05 19
SB-7 L880142-06 21
SB-8 L880142-07 24
SB-9 L880142-08 26
SB-10 L880142-09 28
SB-11 L880142-10 31
SB-12 L880142-11 34
SB-13 L880142-12 36
SB-14 L880142-13 39
SB-15 L880142-14 41
SB-16 L880142-15 43
SB-17 L880142-16 45
SB-18 L880142-17 48
SB-19 L880142-18 50
SB-20 L880142-19 53
SB-21 L880142-20 55
SB-22 L880142-21 57
SB-24 L880142-22 60
SB-25 L880142-23 63
SB-28 L880142-24 66
SB-29 L880142-25 68
SB-31 L880142-26 71
TP-1A L880142-27 74
TP-1B L880142-28 77
TP-10B L880142-29 79
MW-4 L880142-30 81
MW-2 L880142-31 85
MW-5 L880142-32 89
⁶Qc: Quality Control Summary 93
Total Solids by Method 2540 G-2011 93
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 2 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 2 of 142
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Wet Chemistry by Method 350.1 97
Mercury by Method 7470A 99
Metals (ICP) by Method 6010C 100
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH 101
Volatile Organic Compounds (GC) by Method 8015D/GRO 102
Volatile Organic Compounds (GC/MS) by Method 8260B 104
Semi-Volatile Organic Compounds (GC) by Method 8015 124
Semi-Volatile Organic Compounds (GC) by Method MADEPE 126
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 127
⁷Gl: Glossary of Terms 136
⁸Al: Accreditations & Locations 137
⁹Sc: Chain of Custody 138
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 3 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 3 of 142
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-2 L880142-01 Solid Mike Fekete 12/19/16 10:35 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/28/16 23:23 TH
Total Solids by Method 2540 G-2011 WG937880 1 12/22/16 11:16 12/22/16 11:27 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 19 12/19/16 10:35 12/24/16 02:47 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938076 1 12/19/16 10:35 12/26/16 19:00 JAH
Collected by Collected date/time Received date/time
SB-3 L880142-02 Solid Mike Fekete 12/19/16 10:30 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/28/16 23:35 TH
Total Solids by Method 2540 G-2011 WG937880 1 12/22/16 11:16 12/22/16 11:27 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 20.25 12/19/16 10:30 12/24/16 03:09 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938076 1 12/19/16 10:30 12/26/16 19:22 JAH
Collected by Collected date/time Received date/time
SB-4 L880142-03 Solid Mike Fekete 12/19/16 10:25 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/28/16 23:47 TH
Total Solids by Method 2540 G-2011 WG937880 1 12/22/16 11:16 12/22/16 11:27 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 20.75 12/19/16 10:25 12/24/16 03:31 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938076 1 12/19/16 10:25 12/26/16 19:43 JAH
Collected by Collected date/time Received date/time
SB-5 L880142-04 Solid Mike Fekete 12/19/16 10:20 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 5 12/28/16 14:13 12/29/16 14:50 TH
Total Solids by Method 2540 G-2011 WG937880 1 12/22/16 11:16 12/22/16 11:27 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 19 12/19/16 10:20 12/24/16 03:53 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938076 1 12/19/16 10:20 12/26/16 20:05 JAH
Collected by Collected date/time Received date/time
SB-6 L880142-05 Solid Mike Fekete 12/19/16 10:15 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 00:35 TH
Total Solids by Method 2540 G-2011 WG937880 1 12/22/16 11:16 12/22/16 11:27 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 19.25 12/19/16 10:15 12/24/16 04:15 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938076 1 12/19/16 10:15 12/26/16 20:27 JAH
Collected by Collected date/time Received date/time
SB-7 L880142-06 Solid Mike Fekete 12/19/16 10:10 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 14:20 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 00:48 TH
Total Solids by Method 2540 G-2011 WG937880 1 12/22/16 11:16 12/22/16 11:27 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 18.75 12/19/16 10:10 12/24/16 04:38 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938076 1 12/19/16 10:10 12/27/16 01:51 JAH
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 4 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 4 of 142
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-8 L880142-07 Solid Mike Fekete 12/19/16 10:00 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 01:00 TH
Total Solids by Method 2540 G-2011 WG937880 1 12/22/16 11:16 12/22/16 11:27 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 19 12/19/16 10:00 12/24/16 05:00 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 10:00 12/26/16 03:46 JAH
Collected by Collected date/time Received date/time
SB-9 L880142-08 Solid Mike Fekete 12/19/16 09:50 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 01:12 TH
Total Solids by Method 2540 G-2011 WG937880 1 12/22/16 11:16 12/22/16 11:27 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 19.5 12/19/16 09:50 12/24/16 05:22 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 09:50 12/26/16 04:08 JAH
Collected by Collected date/time Received date/time
SB-10 L880142-09 Solid Mike Fekete 12/19/16 09:10 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 14:46 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 01:24 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 19.75 12/19/16 09:10 12/24/16 05:44 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 09:10 12/26/16 04:31 JAH
Collected by Collected date/time Received date/time
SB-11 L880142-10 Solid Mike Fekete 12/19/16 09:40 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 15:12 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 01:36 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 20.75 12/19/16 09:40 12/24/16 06:06 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 09:40 12/26/16 04:54 JAH
Collected by Collected date/time Received date/time
SB-12 L880142-11 Solid Mike Fekete 12/19/16 09:30 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 02:25 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 18.75 12/19/16 09:30 12/24/16 06:28 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 09:30 12/26/16 05:16 JAH
Collected by Collected date/time Received date/time
SB-13 L880142-12 Solid Mike Fekete 12/19/16 09:20 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 15:38 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 02:37 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 19.75 12/19/16 09:20 12/28/16 08:10 DAH
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 5 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 5 of 142
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-13 L880142-12 Solid Mike Fekete 12/19/16 09:20 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 19.75 12/19/16 09:20 12/29/16 03:55 JAH
Collected by Collected date/time Received date/time
SB-14 L880142-13 Solid Mike Fekete 12/19/16 10:45 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 02:49 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 19 12/19/16 10:45 12/24/16 07:13 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 10:45 12/26/16 05:39 JAH
Collected by Collected date/time Received date/time
SB-15 L880142-14 Solid Mike Fekete 12/19/16 10:55 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 2 12/28/16 14:13 12/29/16 03:01 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 20.25 12/19/16 10:55 12/24/16 07:35 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 10:55 12/26/16 06:02 JAH
Collected by Collected date/time Received date/time
SB-16 L880142-15 Solid Mike Fekete 12/19/16 11:00 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 14:38 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 20.75 12/19/16 11:00 12/24/16 07:57 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 11:00 12/26/16 06:24 JAH
Collected by Collected date/time Received date/time
SB-17 L880142-16 Solid Mike Fekete 12/19/16 11:05 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 16:04 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 03:25 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 18.75 12/19/16 11:05 12/24/16 08:19 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 11:05 12/26/16 06:47 JAH
Collected by Collected date/time Received date/time
SB-18 L880142-17 Solid Mike Fekete 12/19/16 11:10 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 03:37 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 20 12/19/16 11:10 12/24/16 08:41 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 11:10 12/26/16 07:09 JAH
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 6 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 6 of 142
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-19 L880142-18 Solid Mike Fekete 12/19/16 11:15 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 17:48 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 03:49 TH
Total Solids by Method 2540 G-2011 WG937881 1 12/22/16 11:01 12/22/16 11:14 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938086 20 12/19/16 11:15 12/24/16 09:03 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 11:15 12/26/16 07:32 JAH
Collected by Collected date/time Received date/time
SB-20 L880142-19 Solid Mike Fekete 12/19/16 11:20 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 04:01 TH
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 18.5 12/19/16 11:20 12/28/16 14:36 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 11:20 12/26/16 07:55 JAH
Collected by Collected date/time Received date/time
SB-21 L880142-20 Solid Mike Fekete 12/19/16 11:25 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG938642 1 12/28/16 14:13 12/29/16 04:14 TH
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 19.25 12/19/16 11:25 12/28/16 15:05 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 11:25 12/26/16 08:17 JAH
Collected by Collected date/time Received date/time
SB-22 L880142-21 Solid Mike Fekete 12/19/16 11:30 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 18:14 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 1 12/22/16 23:17 12/23/16 16:16 DMG
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 20.75 12/19/16 11:30 12/28/16 15:34 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 11:30 12/26/16 08:40 JAH
Collected by Collected date/time Received date/time
SB-24 L880142-22 Solid Mike Fekete 12/19/16 11:45 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 19:57 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 1 12/22/16 23:17 12/23/16 17:41 DMG
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 16.25 12/19/16 11:45 12/28/16 16:26 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 11:45 12/26/16 09:02 JAH
Collected by Collected date/time Received date/time
SB-25 L880142-23 Solid Mike Fekete 12/19/16 15:00 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 18:39 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 1 12/22/16 23:17 12/23/16 16:28 DMG
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 7 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 7 of 142
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-25 L880142-23 Solid Mike Fekete 12/19/16 15:00 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 21.25 12/19/16 15:00 12/28/16 16:55 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 15:00 12/26/16 09:24 JAH
Collected by Collected date/time Received date/time
SB-28 L880142-24 Solid Mike Fekete 12/19/16 15:10 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 1 12/22/16 23:17 12/23/16 16:40 DMG
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 20.5 12/19/16 15:10 12/28/16 17:24 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 15:10 12/26/16 09:47 JAH
Collected by Collected date/time Received date/time
SB-29 L880142-25 Solid Mike Fekete 12/19/16 15:20 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 19:05 JF
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 5 12/29/16 01:30 12/30/16 13:10 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 1 12/22/16 23:17 12/23/16 16:52 DMG
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 350 12/19/16 15:20 12/28/16 17:53 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 350 12/19/16 15:20 12/26/16 10:09 JAH
Collected by Collected date/time Received date/time
SB-31 L880142-26 Solid Mike Fekete 12/19/16 15:45 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 1 12/29/16 01:30 12/29/16 19:31 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 1 12/22/16 23:17 12/23/16 17:05 DMG
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 17.75 12/19/16 15:45 12/28/16 18:22 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938078 1 12/19/16 15:45 12/29/16 04:16 JAH
Collected by Collected date/time Received date/time
TP-1A L880142-27 Solid Mike Fekete 12/20/16 10:00 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938702 50 12/29/16 01:30 12/30/16 13:35 JF
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 10 12/22/16 23:17 12/23/16 20:08 DMG
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 17 12/20/16 10:00 12/28/16 19:26 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938079 1 12/20/16 10:00 12/27/16 01:49 JHH
Volatile Organic Compounds (GC/MS) by Method 8260B WG938079 17 12/20/16 10:00 12/27/16 21:02 DAH
Collected by Collected date/time Received date/time
TP-1B L880142-28 Solid Mike Fekete 12/20/16 10:10 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 1 12/22/16 23:17 12/23/16 17:17 DMG
Total Solids by Method 2540 G-2011 WG937882 1 12/22/16 10:48 12/22/16 11:00 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 15.75 12/20/16 10:10 12/28/16 19:55 DWR
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 8 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 8 of 142
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TP-1B L880142-28 Solid Mike Fekete 12/20/16 10:10 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG938079 1 12/26/16 18:26 12/27/16 06:17 JHH
Collected by Collected date/time Received date/time
TP-10B L880142-29 Solid Mike Fekete 12/20/16 12:30 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi-Volatile Organic Compounds (GC) by Method 8015 WG937731 1 12/22/16 23:17 12/23/16 17:29 DMG
Total Solids by Method 2540 G-2011 WG937884 1 12/23/16 13:16 12/23/16 13:23 KDW
Volatile Organic Compounds (GC) by Method 8015D/GRO WG938087 16.75 12/20/16 12:30 12/28/16 20:23 DWR
Volatile Organic Compounds (GC/MS) by Method 8260B WG938079 1 12/26/16 18:26 12/27/16 06:37 JHH
Collected by Collected date/time Received date/time
MW-4 L880142-30 GW Mike Fekete 12/20/16 14:20 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG937807 1 12/22/16 10:27 12/23/16 10:54 NJB
Metals (ICP) by Method 6010C WG937757 1 12/23/16 11:49 12/23/16 17:45 LTB
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938069 1 12/23/16 07:08 12/27/16 13:14 JF
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG938055 1 12/22/16 15:30 12/22/16 19:10 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG938055 1 12/22/16 15:30 12/22/16 20:59 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938587 1 12/25/16 21:03 12/25/16 21:03 JAH
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 14:15 12/28/16 14:15 JAH
Wet Chemistry by Method 350.1 WG938851 1 12/27/16 16:24 12/27/16 16:24 DR
Collected by Collected date/time Received date/time
MW-2 L880142-31 GW Mike Fekete 12/20/16 14:15 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG937807 1 12/22/16 10:27 12/23/16 10:57 NJB
Metals (ICP) by Method 6010C WG937757 1 12/23/16 11:49 12/23/16 17:48 LTB
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938069 1 12/23/16 07:08 12/27/16 13:38 JF
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG938055 1 12/22/16 15:30 12/22/16 19:32 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG938055 1 12/22/16 15:30 12/22/16 20:37 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938587 1 12/25/16 21:26 12/25/16 21:26 JAH
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 14:47 12/28/16 14:47 JAH
Wet Chemistry by Method 350.1 WG938851 1 12/27/16 16:26 12/27/16 16:26 DR
Collected by Collected date/time Received date/time
MW-5 L880142-32 GW Mike Fekete 12/20/16 15:50 12/21/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG937807 1 12/22/16 10:27 12/23/16 10:59 NJB
Metals (ICP) by Method 6010C WG937757 1 12/23/16 11:49 12/23/16 17:51 LTB
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG938069 1 12/23/16 07:08 12/27/16 14:02 JF
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG938055 1 12/22/16 15:30 12/22/16 19:54 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG938055 1 12/22/16 15:30 12/22/16 20:16 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938587 1 12/25/16 21:50 12/25/16 21:50 JAH
Volatile Organic Compounds (GC/MS) by Method 8260B WG938587 5 12/28/16 21:49 12/28/16 21:49 JHH
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 15:20 12/28/16 15:20 JAH
Wet Chemistry by Method 350.1 WG938852 1 12/28/16 11:08 12/28/16 11:08 DR
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 9 of 142
ONE LAB. NATIONWIDE.CASE NARRATIVE
All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the
sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Sample Handling and Receiving
The analysis for 2-Chloroethyl Vinyl Ether was conducted from a chemically preserved container.
ESC Sample ID Project Sample ID Method
L880142-30 MW-4 8260B
L880142-31 MW-2 8260B
L880142-32 MW-5 8260B
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 10 of 142
Mark W. Beasley
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 10 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880142
SB-2
Collected date/time: 12/19/16 10:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.6 1 12/22/2016 11:27 WG937880
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.42 19 12/24/2016 02:47 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.4 59.0-128 12/24/2016 02:47 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0636 1 12/26/2016 19:00 WG938076
Acrylonitrile ND 0.0127 1 12/26/2016 19:00 WG938076
Benzene ND 0.00127 1 12/26/2016 19:00 WG938076
Bromobenzene ND 0.00127 1 12/26/2016 19:00 WG938076
Bromodichloromethane ND 0.00127 1 12/26/2016 19:00 WG938076
Bromoform ND 0.00127 1 12/26/2016 19:00 WG938076
Bromomethane ND 0.00636 1 12/26/2016 19:00 WG938076
n-Butylbenzene ND 0.00127 1 12/26/2016 19:00 WG938076
sec-Butylbenzene ND 0.00127 1 12/26/2016 19:00 WG938076
tert-Butylbenzene ND 0.00127 1 12/26/2016 19:00 WG938076
Carbon tetrachloride ND 0.00127 1 12/26/2016 19:00 WG938076
Chlorobenzene ND 0.00127 1 12/26/2016 19:00 WG938076
Chlorodibromomethane ND 0.00127 1 12/26/2016 19:00 WG938076
Chloroethane ND 0.00636 1 12/26/2016 19:00 WG938076
2-Chloroethyl vinyl ether ND 0.0636 1 12/26/2016 19:00 WG938076
Chloroform ND 0.00636 1 12/26/2016 19:00 WG938076
Chloromethane ND 0.00318 1 12/26/2016 19:00 WG938076
2-Chlorotoluene ND 0.00127 1 12/26/2016 19:00 WG938076
4-Chlorotoluene ND 0.00127 1 12/26/2016 19:00 WG938076
1,2-Dibromo-3-Chloropropane ND 0.00636 1 12/26/2016 19:00 WG938076
1,2-Dibromoethane ND 0.00127 1 12/26/2016 19:00 WG938076
Dibromomethane ND 0.00127 1 12/26/2016 19:00 WG938076
1,2-Dichlorobenzene ND 0.00127 1 12/26/2016 19:00 WG938076
1,3-Dichlorobenzene ND 0.00127 1 12/26/2016 19:00 WG938076
1,4-Dichlorobenzene ND 0.00127 1 12/26/2016 19:00 WG938076
Dichlorodifluoromethane ND 0.00636 1 12/26/2016 19:00 WG938076
1,1-Dichloroethane ND 0.00127 1 12/26/2016 19:00 WG938076
1,2-Dichloroethane ND 0.00127 1 12/26/2016 19:00 WG938076
1,1-Dichloroethene ND 0.00127 1 12/26/2016 19:00 WG938076
cis-1,2-Dichloroethene ND 0.00127 1 12/26/2016 19:00 WG938076
trans-1,2-Dichloroethene ND 0.00127 1 12/26/2016 19:00 WG938076
1,2-Dichloropropane ND 0.00127 1 12/26/2016 19:00 WG938076
1,1-Dichloropropene ND 0.00127 1 12/26/2016 19:00 WG938076
1,3-Dichloropropane ND 0.00127 1 12/26/2016 19:00 WG938076
cis-1,3-Dichloropropene ND 0.00127 1 12/26/2016 19:00 WG938076
trans-1,3-Dichloropropene ND 0.00127 1 12/26/2016 19:00 WG938076
2,2-Dichloropropane ND 0.00127 1 12/26/2016 19:00 WG938076
Di-isopropyl ether ND 0.00127 1 12/26/2016 19:00 WG938076
Ethylbenzene ND 0.00127 1 12/26/2016 19:00 WG938076
Hexachloro-1,3-butadiene ND 0.00127 1 12/26/2016 19:00 WG938076
Isopropylbenzene ND 0.00127 1 12/26/2016 19:00 WG938076
p-Isopropyltoluene ND 0.00127 1 12/26/2016 19:00 WG938076
2-Butanone (MEK)0.0240 0.0127 1 12/26/2016 19:00 WG938076
Methylene Chloride ND 0.00636 1 12/26/2016 19:00 WG938076
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 11 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 11 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880142
SB-2
Collected date/time: 12/19/16 10:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0127 1 12/26/2016 19:00 WG938076
Methyl tert-butyl ether ND 0.00127 1 12/26/2016 19:00 WG938076
Naphthalene ND 0.00636 1 12/26/2016 19:00 WG938076
n-Propylbenzene ND 0.00127 1 12/26/2016 19:00 WG938076
Styrene ND 0.00127 1 12/26/2016 19:00 WG938076
1,1,1,2-Tetrachloroethane ND 0.00127 1 12/26/2016 19:00 WG938076
1,1,2,2-Tetrachloroethane ND 0.00127 1 12/26/2016 19:00 WG938076
Tetrachloroethene ND 0.00127 1 12/26/2016 19:00 WG938076
Toluene ND 0.00636 1 12/26/2016 19:00 WG938076
1,2,3-Trichlorobenzene ND 0.00127 1 12/26/2016 19:00 WG938076
1,2,4-Trichlorobenzene ND 0.00127 1 12/26/2016 19:00 WG938076
1,1,1-Trichloroethane ND 0.00127 1 12/26/2016 19:00 WG938076
1,1,2-Trichloroethane ND 0.00127 1 12/26/2016 19:00 WG938076
1,1,2-Trichlorotrifluoroethane ND 0.00127 1 12/26/2016 19:00 WG938076
Trichloroethene ND 0.00127 1 12/26/2016 19:00 WG938076
Trichlorofluoromethane ND 0.00636 1 12/26/2016 19:00 WG938076
1,2,3-Trichloropropane ND 0.00318 1 12/26/2016 19:00 WG938076
1,2,4-Trimethylbenzene ND 0.00127 1 12/26/2016 19:00 WG938076
1,3,5-Trimethylbenzene ND 0.00127 1 12/26/2016 19:00 WG938076
Vinyl chloride ND 0.00127 1 12/26/2016 19:00 WG938076
Xylenes, Total ND 0.00382 1 12/26/2016 19:00 WG938076
(S) Toluene-d8 99.9 88.7-115 12/26/2016 19:00 WG938076
(S) Dibromofluoromethane 101 76.3-123 12/26/2016 19:00 WG938076
(S) 4-Bromofluorobenzene 95.5 69.7-129 12/26/2016 19:00 WG938076
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.09 1 12/28/2016 23:23 WG938642
(S) o-Terphenyl 73.7 50.0-150 12/28/2016 23:23 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 12 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 12 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880142
SB-3
Collected date/time: 12/19/16 10:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.2 1 12/22/2016 11:27 WG937880
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.49 20.25 12/24/2016 03:09 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.1 59.0-128 12/24/2016 03:09 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0616 1 12/26/2016 19:22 WG938076
Acrylonitrile ND 0.0123 1 12/26/2016 19:22 WG938076
Benzene ND 0.00123 1 12/26/2016 19:22 WG938076
Bromobenzene ND 0.00123 1 12/26/2016 19:22 WG938076
Bromodichloromethane ND 0.00123 1 12/26/2016 19:22 WG938076
Bromoform ND 0.00123 1 12/26/2016 19:22 WG938076
Bromomethane ND 0.00616 1 12/26/2016 19:22 WG938076
n-Butylbenzene ND 0.00123 1 12/26/2016 19:22 WG938076
sec-Butylbenzene ND 0.00123 1 12/26/2016 19:22 WG938076
tert-Butylbenzene ND 0.00123 1 12/26/2016 19:22 WG938076
Carbon tetrachloride ND 0.00123 1 12/26/2016 19:22 WG938076
Chlorobenzene ND 0.00123 1 12/26/2016 19:22 WG938076
Chlorodibromomethane ND 0.00123 1 12/26/2016 19:22 WG938076
Chloroethane ND 0.00616 1 12/26/2016 19:22 WG938076
2-Chloroethyl vinyl ether ND 0.0616 1 12/26/2016 19:22 WG938076
Chloroform ND 0.00616 1 12/26/2016 19:22 WG938076
Chloromethane ND 0.00308 1 12/26/2016 19:22 WG938076
2-Chlorotoluene ND 0.00123 1 12/26/2016 19:22 WG938076
4-Chlorotoluene ND 0.00123 1 12/26/2016 19:22 WG938076
1,2-Dibromo-3-Chloropropane ND 0.00616 1 12/26/2016 19:22 WG938076
1,2-Dibromoethane ND 0.00123 1 12/26/2016 19:22 WG938076
Dibromomethane ND 0.00123 1 12/26/2016 19:22 WG938076
1,2-Dichlorobenzene ND 0.00123 1 12/26/2016 19:22 WG938076
1,3-Dichlorobenzene ND 0.00123 1 12/26/2016 19:22 WG938076
1,4-Dichlorobenzene ND 0.00123 1 12/26/2016 19:22 WG938076
Dichlorodifluoromethane ND 0.00616 1 12/26/2016 19:22 WG938076
1,1-Dichloroethane ND 0.00123 1 12/26/2016 19:22 WG938076
1,2-Dichloroethane ND 0.00123 1 12/26/2016 19:22 WG938076
1,1-Dichloroethene ND 0.00123 1 12/26/2016 19:22 WG938076
cis-1,2-Dichloroethene ND 0.00123 1 12/26/2016 19:22 WG938076
trans-1,2-Dichloroethene ND 0.00123 1 12/26/2016 19:22 WG938076
1,2-Dichloropropane ND 0.00123 1 12/26/2016 19:22 WG938076
1,1-Dichloropropene ND 0.00123 1 12/26/2016 19:22 WG938076
1,3-Dichloropropane ND 0.00123 1 12/26/2016 19:22 WG938076
cis-1,3-Dichloropropene ND 0.00123 1 12/26/2016 19:22 WG938076
trans-1,3-Dichloropropene ND 0.00123 1 12/26/2016 19:22 WG938076
2,2-Dichloropropane ND 0.00123 1 12/26/2016 19:22 WG938076
Di-isopropyl ether ND 0.00123 1 12/26/2016 19:22 WG938076
Ethylbenzene ND 0.00123 1 12/26/2016 19:22 WG938076
Hexachloro-1,3-butadiene ND 0.00123 1 12/26/2016 19:22 WG938076
Isopropylbenzene ND 0.00123 1 12/26/2016 19:22 WG938076
p-Isopropyltoluene ND 0.00123 1 12/26/2016 19:22 WG938076
2-Butanone (MEK)0.0258 0.0123 1 12/26/2016 19:22 WG938076
Methylene Chloride ND 0.00616 1 12/26/2016 19:22 WG938076
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 13 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 13 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880142
SB-3
Collected date/time: 12/19/16 10:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0123 1 12/26/2016 19:22 WG938076
Methyl tert-butyl ether ND 0.00123 1 12/26/2016 19:22 WG938076
Naphthalene ND 0.00616 1 12/26/2016 19:22 WG938076
n-Propylbenzene ND 0.00123 1 12/26/2016 19:22 WG938076
Styrene ND 0.00123 1 12/26/2016 19:22 WG938076
1,1,1,2-Tetrachloroethane ND 0.00123 1 12/26/2016 19:22 WG938076
1,1,2,2-Tetrachloroethane ND 0.00123 1 12/26/2016 19:22 WG938076
Tetrachloroethene ND 0.00123 1 12/26/2016 19:22 WG938076
Toluene ND 0.00616 1 12/26/2016 19:22 WG938076
1,2,3-Trichlorobenzene ND 0.00123 1 12/26/2016 19:22 WG938076
1,2,4-Trichlorobenzene ND 0.00123 1 12/26/2016 19:22 WG938076
1,1,1-Trichloroethane ND 0.00123 1 12/26/2016 19:22 WG938076
1,1,2-Trichloroethane ND 0.00123 1 12/26/2016 19:22 WG938076
1,1,2-Trichlorotrifluoroethane ND 0.00123 1 12/26/2016 19:22 WG938076
Trichloroethene ND 0.00123 1 12/26/2016 19:22 WG938076
Trichlorofluoromethane ND 0.00616 1 12/26/2016 19:22 WG938076
1,2,3-Trichloropropane ND 0.00308 1 12/26/2016 19:22 WG938076
1,2,4-Trimethylbenzene ND 0.00123 1 12/26/2016 19:22 WG938076
1,3,5-Trimethylbenzene ND 0.00123 1 12/26/2016 19:22 WG938076
Vinyl chloride ND 0.00123 1 12/26/2016 19:22 WG938076
Xylenes, Total ND 0.00370 1 12/26/2016 19:22 WG938076
(S) Toluene-d8 101 88.7-115 12/26/2016 19:22 WG938076
(S) Dibromofluoromethane 103 76.3-123 12/26/2016 19:22 WG938076
(S) 4-Bromofluorobenzene 95.8 69.7-129 12/26/2016 19:22 WG938076
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 4.93 1 12/28/2016 23:35 WG938642
(S) o-Terphenyl 74.2 50.0-150 12/28/2016 23:35 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 14 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 14 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880142
SB-4
Collected date/time: 12/19/16 10:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.7 1 12/22/2016 11:27 WG937880
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.42 20.75 12/24/2016 03:31 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.2 59.0-128 12/24/2016 03:31 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0583 1 12/26/2016 19:43 WG938076
Acrylonitrile ND 0.0117 1 12/26/2016 19:43 WG938076
Benzene ND 0.00117 1 12/26/2016 19:43 WG938076
Bromobenzene ND 0.00117 1 12/26/2016 19:43 WG938076
Bromodichloromethane ND 0.00117 1 12/26/2016 19:43 WG938076
Bromoform ND 0.00117 1 12/26/2016 19:43 WG938076
Bromomethane ND 0.00583 1 12/26/2016 19:43 WG938076
n-Butylbenzene ND 0.00117 1 12/26/2016 19:43 WG938076
sec-Butylbenzene ND 0.00117 1 12/26/2016 19:43 WG938076
tert-Butylbenzene ND 0.00117 1 12/26/2016 19:43 WG938076
Carbon tetrachloride ND 0.00117 1 12/26/2016 19:43 WG938076
Chlorobenzene ND 0.00117 1 12/26/2016 19:43 WG938076
Chlorodibromomethane ND 0.00117 1 12/26/2016 19:43 WG938076
Chloroethane ND 0.00583 1 12/26/2016 19:43 WG938076
2-Chloroethyl vinyl ether ND 0.0583 1 12/26/2016 19:43 WG938076
Chloroform ND 0.00583 1 12/26/2016 19:43 WG938076
Chloromethane ND 0.00292 1 12/26/2016 19:43 WG938076
2-Chlorotoluene ND 0.00117 1 12/26/2016 19:43 WG938076
4-Chlorotoluene ND 0.00117 1 12/26/2016 19:43 WG938076
1,2-Dibromo-3-Chloropropane ND 0.00583 1 12/26/2016 19:43 WG938076
1,2-Dibromoethane ND 0.00117 1 12/26/2016 19:43 WG938076
Dibromomethane ND 0.00117 1 12/26/2016 19:43 WG938076
1,2-Dichlorobenzene ND 0.00117 1 12/26/2016 19:43 WG938076
1,3-Dichlorobenzene ND 0.00117 1 12/26/2016 19:43 WG938076
1,4-Dichlorobenzene ND 0.00117 1 12/26/2016 19:43 WG938076
Dichlorodifluoromethane ND 0.00583 1 12/26/2016 19:43 WG938076
1,1-Dichloroethane ND 0.00117 1 12/26/2016 19:43 WG938076
1,2-Dichloroethane ND 0.00117 1 12/26/2016 19:43 WG938076
1,1-Dichloroethene ND 0.00117 1 12/26/2016 19:43 WG938076
cis-1,2-Dichloroethene ND 0.00117 1 12/26/2016 19:43 WG938076
trans-1,2-Dichloroethene ND 0.00117 1 12/26/2016 19:43 WG938076
1,2-Dichloropropane ND 0.00117 1 12/26/2016 19:43 WG938076
1,1-Dichloropropene ND 0.00117 1 12/26/2016 19:43 WG938076
1,3-Dichloropropane ND 0.00117 1 12/26/2016 19:43 WG938076
cis-1,3-Dichloropropene ND 0.00117 1 12/26/2016 19:43 WG938076
trans-1,3-Dichloropropene ND 0.00117 1 12/26/2016 19:43 WG938076
2,2-Dichloropropane ND 0.00117 1 12/26/2016 19:43 WG938076
Di-isopropyl ether ND 0.00117 1 12/26/2016 19:43 WG938076
Ethylbenzene ND 0.00117 1 12/26/2016 19:43 WG938076
Hexachloro-1,3-butadiene ND 0.00117 1 12/26/2016 19:43 WG938076
Isopropylbenzene ND 0.00117 1 12/26/2016 19:43 WG938076
p-Isopropyltoluene ND 0.00117 1 12/26/2016 19:43 WG938076
2-Butanone (MEK)0.0236 0.0117 1 12/26/2016 19:43 WG938076
Methylene Chloride ND 0.00583 1 12/26/2016 19:43 WG938076
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 15 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 15 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880142
SB-4
Collected date/time: 12/19/16 10:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0117 1 12/26/2016 19:43 WG938076
Methyl tert-butyl ether ND 0.00117 1 12/26/2016 19:43 WG938076
Naphthalene ND 0.00583 1 12/26/2016 19:43 WG938076
n-Propylbenzene ND 0.00117 1 12/26/2016 19:43 WG938076
Styrene ND 0.00117 1 12/26/2016 19:43 WG938076
1,1,1,2-Tetrachloroethane ND 0.00117 1 12/26/2016 19:43 WG938076
1,1,2,2-Tetrachloroethane ND 0.00117 1 12/26/2016 19:43 WG938076
Tetrachloroethene ND 0.00117 1 12/26/2016 19:43 WG938076
Toluene ND 0.00583 1 12/26/2016 19:43 WG938076
1,2,3-Trichlorobenzene ND 0.00117 1 12/26/2016 19:43 WG938076
1,2,4-Trichlorobenzene ND 0.00117 1 12/26/2016 19:43 WG938076
1,1,1-Trichloroethane ND 0.00117 1 12/26/2016 19:43 WG938076
1,1,2-Trichloroethane ND 0.00117 1 12/26/2016 19:43 WG938076
1,1,2-Trichlorotrifluoroethane ND 0.00117 1 12/26/2016 19:43 WG938076
Trichloroethene ND 0.00117 1 12/26/2016 19:43 WG938076
Trichlorofluoromethane ND 0.00583 1 12/26/2016 19:43 WG938076
1,2,3-Trichloropropane ND 0.00292 1 12/26/2016 19:43 WG938076
1,2,4-Trimethylbenzene ND 0.00117 1 12/26/2016 19:43 WG938076
1,3,5-Trimethylbenzene ND 0.00117 1 12/26/2016 19:43 WG938076
Vinyl chloride ND 0.00117 1 12/26/2016 19:43 WG938076
Xylenes, Total ND 0.00350 1 12/26/2016 19:43 WG938076
(S) Toluene-d8 101 88.7-115 12/26/2016 19:43 WG938076
(S) Dibromofluoromethane 103 76.3-123 12/26/2016 19:43 WG938076
(S) 4-Bromofluorobenzene 97.3 69.7-129 12/26/2016 19:43 WG938076
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 4.67 1 12/28/2016 23:47 WG938642
(S) o-Terphenyl 81.2 50.0-150 12/28/2016 23:47 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 16 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 16 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L880142
SB-5
Collected date/time: 12/19/16 10:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.3 1 12/22/2016 11:27 WG937880
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.37 19 12/24/2016 03:53 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.5 59.0-128 12/24/2016 03:53 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0623 1 12/26/2016 20:05 WG938076
Acrylonitrile ND 0.0125 1 12/26/2016 20:05 WG938076
Benzene ND 0.00125 1 12/26/2016 20:05 WG938076
Bromobenzene ND 0.00125 1 12/26/2016 20:05 WG938076
Bromodichloromethane ND 0.00125 1 12/26/2016 20:05 WG938076
Bromoform ND 0.00125 1 12/26/2016 20:05 WG938076
Bromomethane ND 0.00623 1 12/26/2016 20:05 WG938076
n-Butylbenzene ND 0.00125 1 12/26/2016 20:05 WG938076
sec-Butylbenzene ND 0.00125 1 12/26/2016 20:05 WG938076
tert-Butylbenzene ND 0.00125 1 12/26/2016 20:05 WG938076
Carbon tetrachloride ND 0.00125 1 12/26/2016 20:05 WG938076
Chlorobenzene ND 0.00125 1 12/26/2016 20:05 WG938076
Chlorodibromomethane ND 0.00125 1 12/26/2016 20:05 WG938076
Chloroethane ND 0.00623 1 12/26/2016 20:05 WG938076
2-Chloroethyl vinyl ether ND 0.0623 1 12/26/2016 20:05 WG938076
Chloroform ND 0.00623 1 12/26/2016 20:05 WG938076
Chloromethane ND 0.00311 1 12/26/2016 20:05 WG938076
2-Chlorotoluene ND 0.00125 1 12/26/2016 20:05 WG938076
4-Chlorotoluene ND 0.00125 1 12/26/2016 20:05 WG938076
1,2-Dibromo-3-Chloropropane ND 0.00623 1 12/26/2016 20:05 WG938076
1,2-Dibromoethane ND 0.00125 1 12/26/2016 20:05 WG938076
Dibromomethane ND 0.00125 1 12/26/2016 20:05 WG938076
1,2-Dichlorobenzene 0.00247 0.00125 1 12/26/2016 20:05 WG938076
1,3-Dichlorobenzene ND 0.00125 1 12/26/2016 20:05 WG938076
1,4-Dichlorobenzene ND 0.00125 1 12/26/2016 20:05 WG938076
Dichlorodifluoromethane ND 0.00623 1 12/26/2016 20:05 WG938076
1,1-Dichloroethane ND 0.00125 1 12/26/2016 20:05 WG938076
1,2-Dichloroethane ND 0.00125 1 12/26/2016 20:05 WG938076
1,1-Dichloroethene ND 0.00125 1 12/26/2016 20:05 WG938076
cis-1,2-Dichloroethene ND 0.00125 1 12/26/2016 20:05 WG938076
trans-1,2-Dichloroethene ND 0.00125 1 12/26/2016 20:05 WG938076
1,2-Dichloropropane ND 0.00125 1 12/26/2016 20:05 WG938076
1,1-Dichloropropene ND 0.00125 1 12/26/2016 20:05 WG938076
1,3-Dichloropropane ND 0.00125 1 12/26/2016 20:05 WG938076
cis-1,3-Dichloropropene ND 0.00125 1 12/26/2016 20:05 WG938076
trans-1,3-Dichloropropene ND 0.00125 1 12/26/2016 20:05 WG938076
2,2-Dichloropropane ND 0.00125 1 12/26/2016 20:05 WG938076
Di-isopropyl ether ND 0.00125 1 12/26/2016 20:05 WG938076
Ethylbenzene ND 0.00125 1 12/26/2016 20:05 WG938076
Hexachloro-1,3-butadiene ND 0.00125 1 12/26/2016 20:05 WG938076
Isopropylbenzene ND 0.00125 1 12/26/2016 20:05 WG938076
p-Isopropyltoluene ND 0.00125 1 12/26/2016 20:05 WG938076
2-Butanone (MEK)0.0259 0.0125 1 12/26/2016 20:05 WG938076
Methylene Chloride ND 0.00623 1 12/26/2016 20:05 WG938076
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 17 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 17 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L880142
SB-5
Collected date/time: 12/19/16 10:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0125 1 12/26/2016 20:05 WG938076
Methyl tert-butyl ether ND 0.00125 1 12/26/2016 20:05 WG938076
Naphthalene ND 0.00623 1 12/26/2016 20:05 WG938076
n-Propylbenzene ND 0.00125 1 12/26/2016 20:05 WG938076
Styrene ND 0.00125 1 12/26/2016 20:05 WG938076
1,1,1,2-Tetrachloroethane ND 0.00125 1 12/26/2016 20:05 WG938076
1,1,2,2-Tetrachloroethane ND 0.00125 1 12/26/2016 20:05 WG938076
Tetrachloroethene ND 0.00125 1 12/26/2016 20:05 WG938076
Toluene ND 0.00623 1 12/26/2016 20:05 WG938076
1,2,3-Trichlorobenzene ND 0.00125 1 12/26/2016 20:05 WG938076
1,2,4-Trichlorobenzene ND 0.00125 1 12/26/2016 20:05 WG938076
1,1,1-Trichloroethane ND 0.00125 1 12/26/2016 20:05 WG938076
1,1,2-Trichloroethane ND 0.00125 1 12/26/2016 20:05 WG938076
1,1,2-Trichlorotrifluoroethane ND 0.00125 1 12/26/2016 20:05 WG938076
Trichloroethene ND 0.00125 1 12/26/2016 20:05 WG938076
Trichlorofluoromethane ND 0.00623 1 12/26/2016 20:05 WG938076
1,2,3-Trichloropropane ND 0.00311 1 12/26/2016 20:05 WG938076
1,2,4-Trimethylbenzene ND 0.00125 1 12/26/2016 20:05 WG938076
1,3,5-Trimethylbenzene ND 0.00125 1 12/26/2016 20:05 WG938076
Vinyl chloride ND 0.00125 1 12/26/2016 20:05 WG938076
Xylenes, Total ND 0.00374 1 12/26/2016 20:05 WG938076
(S) Toluene-d8 93.7 88.7-115 12/26/2016 20:05 WG938076
(S) Dibromofluoromethane 110 76.3-123 12/26/2016 20:05 WG938076
(S) 4-Bromofluorobenzene 78.7 69.7-129 12/26/2016 20:05 WG938076
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1200 24.9 5 12/29/2016 14:50 WG938642
(S) o-Terphenyl 101 50.0-150 12/29/2016 14:50 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 18 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 18 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L880142
SB-6
Collected date/time: 12/19/16 10:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.0 1 12/22/2016 11:27 WG937880
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.44 19.25 12/24/2016 04:15 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.5 59.0-128 12/24/2016 04:15 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0633 1 12/26/2016 20:27 WG938076
Acrylonitrile ND 0.0127 1 12/26/2016 20:27 WG938076
Benzene ND 0.00127 1 12/26/2016 20:27 WG938076
Bromobenzene ND 0.00127 1 12/26/2016 20:27 WG938076
Bromodichloromethane ND 0.00127 1 12/26/2016 20:27 WG938076
Bromoform ND 0.00127 1 12/26/2016 20:27 WG938076
Bromomethane ND 0.00633 1 12/26/2016 20:27 WG938076
n-Butylbenzene ND 0.00127 1 12/26/2016 20:27 WG938076
sec-Butylbenzene ND 0.00127 1 12/26/2016 20:27 WG938076
tert-Butylbenzene ND 0.00127 1 12/26/2016 20:27 WG938076
Carbon tetrachloride ND 0.00127 1 12/26/2016 20:27 WG938076
Chlorobenzene ND 0.00127 1 12/26/2016 20:27 WG938076
Chlorodibromomethane ND 0.00127 1 12/26/2016 20:27 WG938076
Chloroethane ND 0.00633 1 12/26/2016 20:27 WG938076
2-Chloroethyl vinyl ether ND 0.0633 1 12/26/2016 20:27 WG938076
Chloroform ND 0.00633 1 12/26/2016 20:27 WG938076
Chloromethane ND 0.00316 1 12/26/2016 20:27 WG938076
2-Chlorotoluene ND 0.00127 1 12/26/2016 20:27 WG938076
4-Chlorotoluene ND 0.00127 1 12/26/2016 20:27 WG938076
1,2-Dibromo-3-Chloropropane ND 0.00633 1 12/26/2016 20:27 WG938076
1,2-Dibromoethane ND 0.00127 1 12/26/2016 20:27 WG938076
Dibromomethane ND 0.00127 1 12/26/2016 20:27 WG938076
1,2-Dichlorobenzene ND 0.00127 1 12/26/2016 20:27 WG938076
1,3-Dichlorobenzene ND 0.00127 1 12/26/2016 20:27 WG938076
1,4-Dichlorobenzene ND 0.00127 1 12/26/2016 20:27 WG938076
Dichlorodifluoromethane ND 0.00633 1 12/26/2016 20:27 WG938076
1,1-Dichloroethane ND 0.00127 1 12/26/2016 20:27 WG938076
1,2-Dichloroethane ND 0.00127 1 12/26/2016 20:27 WG938076
1,1-Dichloroethene ND 0.00127 1 12/26/2016 20:27 WG938076
cis-1,2-Dichloroethene ND 0.00127 1 12/26/2016 20:27 WG938076
trans-1,2-Dichloroethene ND 0.00127 1 12/26/2016 20:27 WG938076
1,2-Dichloropropane ND 0.00127 1 12/26/2016 20:27 WG938076
1,1-Dichloropropene ND 0.00127 1 12/26/2016 20:27 WG938076
1,3-Dichloropropane ND 0.00127 1 12/26/2016 20:27 WG938076
cis-1,3-Dichloropropene ND 0.00127 1 12/26/2016 20:27 WG938076
trans-1,3-Dichloropropene ND 0.00127 1 12/26/2016 20:27 WG938076
2,2-Dichloropropane ND 0.00127 1 12/26/2016 20:27 WG938076
Di-isopropyl ether ND 0.00127 1 12/26/2016 20:27 WG938076
Ethylbenzene ND 0.00127 1 12/26/2016 20:27 WG938076
Hexachloro-1,3-butadiene ND 0.00127 1 12/26/2016 20:27 WG938076
Isopropylbenzene ND 0.00127 1 12/26/2016 20:27 WG938076
p-Isopropyltoluene ND 0.00127 1 12/26/2016 20:27 WG938076
2-Butanone (MEK)0.0248 0.0127 1 12/26/2016 20:27 WG938076
Methylene Chloride ND 0.00633 1 12/26/2016 20:27 WG938076
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 19 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 19 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L880142
SB-6
Collected date/time: 12/19/16 10:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0127 1 12/26/2016 20:27 WG938076
Methyl tert-butyl ether ND 0.00127 1 12/26/2016 20:27 WG938076
Naphthalene ND 0.00633 1 12/26/2016 20:27 WG938076
n-Propylbenzene ND 0.00127 1 12/26/2016 20:27 WG938076
Styrene ND 0.00127 1 12/26/2016 20:27 WG938076
1,1,1,2-Tetrachloroethane ND 0.00127 1 12/26/2016 20:27 WG938076
1,1,2,2-Tetrachloroethane ND 0.00127 1 12/26/2016 20:27 WG938076
Tetrachloroethene ND 0.00127 1 12/26/2016 20:27 WG938076
Toluene ND 0.00633 1 12/26/2016 20:27 WG938076
1,2,3-Trichlorobenzene ND 0.00127 1 12/26/2016 20:27 WG938076
1,2,4-Trichlorobenzene ND 0.00127 1 12/26/2016 20:27 WG938076
1,1,1-Trichloroethane ND 0.00127 1 12/26/2016 20:27 WG938076
1,1,2-Trichloroethane ND 0.00127 1 12/26/2016 20:27 WG938076
1,1,2-Trichlorotrifluoroethane ND 0.00127 1 12/26/2016 20:27 WG938076
Trichloroethene ND 0.00127 1 12/26/2016 20:27 WG938076
Trichlorofluoromethane ND 0.00633 1 12/26/2016 20:27 WG938076
1,2,3-Trichloropropane ND 0.00316 1 12/26/2016 20:27 WG938076
1,2,4-Trimethylbenzene ND 0.00127 1 12/26/2016 20:27 WG938076
1,3,5-Trimethylbenzene ND 0.00127 1 12/26/2016 20:27 WG938076
Vinyl chloride ND 0.00127 1 12/26/2016 20:27 WG938076
Xylenes, Total ND 0.00380 1 12/26/2016 20:27 WG938076
(S) Toluene-d8 100 88.7-115 12/26/2016 20:27 WG938076
(S) Dibromofluoromethane 104 76.3-123 12/26/2016 20:27 WG938076
(S) 4-Bromofluorobenzene 95.4 69.7-129 12/26/2016 20:27 WG938076
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.06 1 12/29/2016 00:35 WG938642
(S) o-Terphenyl 82.1 50.0-150 12/29/2016 00:35 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 20 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 20 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L880142
SB-7
Collected date/time: 12/19/16 10:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.9 1 12/22/2016 11:27 WG937880
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.54 18.75 12/24/2016 04:38 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.7 59.0-128 12/24/2016 04:38 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.295 0.0676 1 12/27/2016 01:51 WG938076
Acrylonitrile ND 0.0135 1 12/27/2016 01:51 WG938076
Benzene ND 0.00135 1 12/27/2016 01:51 WG938076
Bromobenzene ND 0.00135 1 12/27/2016 01:51 WG938076
Bromodichloromethane ND 0.00135 1 12/27/2016 01:51 WG938076
Bromoform ND 0.00135 1 12/27/2016 01:51 WG938076
Bromomethane ND 0.00676 1 12/27/2016 01:51 WG938076
n-Butylbenzene ND 0.00135 1 12/27/2016 01:51 WG938076
sec-Butylbenzene ND 0.00135 1 12/27/2016 01:51 WG938076
tert-Butylbenzene ND 0.00135 1 12/27/2016 01:51 WG938076
Carbon tetrachloride ND 0.00135 1 12/27/2016 01:51 WG938076
Chlorobenzene ND 0.00135 1 12/27/2016 01:51 WG938076
Chlorodibromomethane ND 0.00135 1 12/27/2016 01:51 WG938076
Chloroethane ND 0.00676 1 12/27/2016 01:51 WG938076
2-Chloroethyl vinyl ether ND 0.0676 1 12/27/2016 01:51 WG938076
Chloroform ND 0.00676 1 12/27/2016 01:51 WG938076
Chloromethane ND 0.00338 1 12/27/2016 01:51 WG938076
2-Chlorotoluene ND 0.00135 1 12/27/2016 01:51 WG938076
4-Chlorotoluene ND 0.00135 1 12/27/2016 01:51 WG938076
1,2-Dibromo-3-Chloropropane ND 0.00676 1 12/27/2016 01:51 WG938076
1,2-Dibromoethane ND 0.00135 1 12/27/2016 01:51 WG938076
Dibromomethane ND 0.00135 1 12/27/2016 01:51 WG938076
1,2-Dichlorobenzene ND 0.00135 1 12/27/2016 01:51 WG938076
1,3-Dichlorobenzene ND 0.00135 1 12/27/2016 01:51 WG938076
1,4-Dichlorobenzene ND 0.00135 1 12/27/2016 01:51 WG938076
Dichlorodifluoromethane ND 0.00676 1 12/27/2016 01:51 WG938076
1,1-Dichloroethane ND 0.00135 1 12/27/2016 01:51 WG938076
1,2-Dichloroethane ND 0.00135 1 12/27/2016 01:51 WG938076
1,1-Dichloroethene ND 0.00135 1 12/27/2016 01:51 WG938076
cis-1,2-Dichloroethene ND 0.00135 1 12/27/2016 01:51 WG938076
trans-1,2-Dichloroethene ND 0.00135 1 12/27/2016 01:51 WG938076
1,2-Dichloropropane ND 0.00135 1 12/27/2016 01:51 WG938076
1,1-Dichloropropene ND 0.00135 1 12/27/2016 01:51 WG938076
1,3-Dichloropropane ND 0.00135 1 12/27/2016 01:51 WG938076
cis-1,3-Dichloropropene ND 0.00135 1 12/27/2016 01:51 WG938076
trans-1,3-Dichloropropene ND 0.00135 1 12/27/2016 01:51 WG938076
2,2-Dichloropropane ND 0.00135 1 12/27/2016 01:51 WG938076
Di-isopropyl ether ND 0.00135 1 12/27/2016 01:51 WG938076
Ethylbenzene ND 0.00135 1 12/27/2016 01:51 WG938076
Hexachloro-1,3-butadiene ND 0.00135 1 12/27/2016 01:51 WG938076
Isopropylbenzene ND 0.00135 1 12/27/2016 01:51 WG938076
p-Isopropyltoluene ND 0.00135 1 12/27/2016 01:51 WG938076
2-Butanone (MEK)0.0243 0.0135 1 12/27/2016 01:51 WG938076
Methylene Chloride ND 0.00676 1 12/27/2016 01:51 WG938076
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 21 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 21 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L880142
SB-7
Collected date/time: 12/19/16 10:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0135 1 12/27/2016 01:51 WG938076
Methyl tert-butyl ether ND 0.00135 1 12/27/2016 01:51 WG938076
Naphthalene ND 0.00676 1 12/27/2016 01:51 WG938076
n-Propylbenzene ND 0.00135 1 12/27/2016 01:51 WG938076
Styrene ND 0.00135 1 12/27/2016 01:51 WG938076
1,1,1,2-Tetrachloroethane ND 0.00135 1 12/27/2016 01:51 WG938076
1,1,2,2-Tetrachloroethane ND 0.00135 1 12/27/2016 01:51 WG938076
Tetrachloroethene ND 0.00135 1 12/27/2016 01:51 WG938076
Toluene ND 0.00676 1 12/27/2016 01:51 WG938076
1,2,3-Trichlorobenzene ND 0.00135 1 12/27/2016 01:51 WG938076
1,2,4-Trichlorobenzene ND 0.00135 1 12/27/2016 01:51 WG938076
1,1,1-Trichloroethane ND 0.00135 1 12/27/2016 01:51 WG938076
1,1,2-Trichloroethane ND 0.00135 1 12/27/2016 01:51 WG938076
1,1,2-Trichlorotrifluoroethane ND 0.00135 1 12/27/2016 01:51 WG938076
Trichloroethene ND 0.00135 1 12/27/2016 01:51 WG938076
Trichlorofluoromethane ND 0.00676 1 12/27/2016 01:51 WG938076
1,2,3-Trichloropropane ND 0.00338 1 12/27/2016 01:51 WG938076
1,2,4-Trimethylbenzene ND 0.00135 1 12/27/2016 01:51 WG938076
1,3,5-Trimethylbenzene ND 0.00135 1 12/27/2016 01:51 WG938076
Vinyl chloride ND 0.00135 1 12/27/2016 01:51 WG938076
Xylenes, Total ND 0.00406 1 12/27/2016 01:51 WG938076
(S) Toluene-d8 100 88.7-115 12/27/2016 01:51 WG938076
(S) Dibromofluoromethane 101 76.3-123 12/27/2016 01:51 WG938076
(S) 4-Bromofluorobenzene 95.3 69.7-129 12/27/2016 01:51 WG938076
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.41 1 12/29/2016 00:48 WG938642
(S) o-Terphenyl 66.4 50.0-150 12/29/2016 00:48 WG938642
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0446 1 12/29/2016 14:20 WG938702
Acenaphthylene ND 0.0446 1 12/29/2016 14:20 WG938702
Anthracene ND 0.0446 1 12/29/2016 14:20 WG938702
Benzidine ND 0.451 1 12/29/2016 14:20 WG938702
Benzo(a)anthracene ND 0.0446 1 12/29/2016 14:20 WG938702
Benzo(b)fluoranthene ND 0.0446 1 12/29/2016 14:20 WG938702
Benzo(k)fluoranthene ND 0.0446 1 12/29/2016 14:20 WG938702
Benzo(g,h,i)perylene ND 0.0446 1 12/29/2016 14:20 WG938702
Benzo(a)pyrene ND 0.0446 1 12/29/2016 14:20 WG938702
Bis(2-chlorethoxy)methane ND 0.451 1 12/29/2016 14:20 WG938702
Bis(2-chloroethyl)ether ND 0.451 1 12/29/2016 14:20 WG938702
Bis(2-chloroisopropyl)ether ND 0.451 1 12/29/2016 14:20 WG938702
4-Bromophenyl-phenylether ND 0.451 1 12/29/2016 14:20 WG938702
2-Chloronaphthalene ND 0.0446 1 12/29/2016 14:20 WG938702
4-Chlorophenyl-phenylether ND 0.451 1 12/29/2016 14:20 WG938702
Chrysene ND 0.0446 1 12/29/2016 14:20 WG938702
Dibenz(a,h)anthracene ND 0.0446 1 12/29/2016 14:20 WG938702
3,3-Dichlorobenzidine ND 0.451 1 12/29/2016 14:20 WG938702
2,4-Dinitrotoluene ND 0.451 1 12/29/2016 14:20 WG938702
2,6-Dinitrotoluene ND 0.451 1 12/29/2016 14:20 WG938702
Fluoranthene ND 0.0446 1 12/29/2016 14:20 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 22 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 22 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L880142
SB-7
Collected date/time: 12/19/16 10:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0446 1 12/29/2016 14:20 WG938702
Hexachlorobenzene ND 0.451 1 12/29/2016 14:20 WG938702
Hexachloro-1,3-butadiene ND 0.451 1 12/29/2016 14:20 WG938702
Hexachlorocyclopentadiene ND 0.451 1 12/29/2016 14:20 WG938702
Hexachloroethane ND 0.451 1 12/29/2016 14:20 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0446 1 12/29/2016 14:20 WG938702
Isophorone ND 0.451 1 12/29/2016 14:20 WG938702
Naphthalene ND 0.0446 1 12/29/2016 14:20 WG938702
Nitrobenzene ND 0.451 1 12/29/2016 14:20 WG938702
n-Nitrosodimethylamine ND 0.451 1 12/29/2016 14:20 WG938702
n-Nitrosodiphenylamine ND 0.451 1 12/29/2016 14:20 WG938702
n-Nitrosodi-n-propylamine ND 0.451 1 12/29/2016 14:20 WG938702
Phenanthrene ND 0.0446 1 12/29/2016 14:20 WG938702
Benzylbutyl phthalate ND 0.451 1 12/29/2016 14:20 WG938702
Bis(2-ethylhexyl)phthalate ND 0.451 1 12/29/2016 14:20 WG938702
Di-n-butyl phthalate ND 0.451 1 12/29/2016 14:20 WG938702
Diethyl phthalate ND 0.451 1 12/29/2016 14:20 WG938702
Dimethyl phthalate ND 0.451 1 12/29/2016 14:20 WG938702
Di-n-octyl phthalate ND 0.451 1 12/29/2016 14:20 WG938702
Pyrene ND 0.0446 1 12/29/2016 14:20 WG938702
1,2,4-Trichlorobenzene ND 0.451 1 12/29/2016 14:20 WG938702
4-Chloro-3-methylphenol ND 0.451 1 12/29/2016 14:20 WG938702
2-Chlorophenol ND 0.451 1 12/29/2016 14:20 WG938702
2,4-Dichlorophenol ND 0.451 1 12/29/2016 14:20 WG938702
2,4-Dimethylphenol ND 0.451 1 12/29/2016 14:20 WG938702
4,6-Dinitro-2-methylphenol ND 0.451 1 12/29/2016 14:20 WG938702
2,4-Dinitrophenol ND J3 0.451 1 12/29/2016 14:20 WG938702
2-Nitrophenol ND 0.451 1 12/29/2016 14:20 WG938702
4-Nitrophenol ND 0.451 1 12/29/2016 14:20 WG938702
Pentachlorophenol ND 0.451 1 12/29/2016 14:20 WG938702
Phenol ND 0.451 1 12/29/2016 14:20 WG938702
2,4,6-Trichlorophenol ND 0.451 1 12/29/2016 14:20 WG938702
(S) 2-Fluorophenol 55.5 21.1-116 12/29/2016 14:20 WG938702
(S) Phenol-d5 55.2 26.3-121 12/29/2016 14:20 WG938702
(S) Nitrobenzene-d5 54.7 21.9-129 12/29/2016 14:20 WG938702
(S) 2-Fluorobiphenyl 57.8 34.9-129 12/29/2016 14:20 WG938702
(S) 2,4,6-Tribromophenol 52.8 21.6-142 12/29/2016 14:20 WG938702
(S) p-Terphenyl-d14 63.5 21.5-128 12/29/2016 14:20 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 23 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 23 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L880142
SB-8
Collected date/time: 12/19/16 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.6 1 12/22/2016 11:27 WG937880
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.55 19 12/24/2016 05:00 WG938086
(S) a,a,a-Trifluorotoluene(FID) 97.1 59.0-128 12/24/2016 05:00 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.0676 0.0671 1 12/26/2016 03:46 WG938078
Acrylonitrile ND 0.0134 1 12/26/2016 03:46 WG938078
Benzene ND 0.00134 1 12/26/2016 03:46 WG938078
Bromobenzene ND 0.00134 1 12/26/2016 03:46 WG938078
Bromodichloromethane ND 0.00134 1 12/26/2016 03:46 WG938078
Bromoform ND 0.00134 1 12/26/2016 03:46 WG938078
Bromomethane ND 0.00671 1 12/26/2016 03:46 WG938078
n-Butylbenzene ND 0.00134 1 12/26/2016 03:46 WG938078
sec-Butylbenzene ND 0.00134 1 12/26/2016 03:46 WG938078
tert-Butylbenzene ND 0.00134 1 12/26/2016 03:46 WG938078
Carbon tetrachloride ND 0.00134 1 12/26/2016 03:46 WG938078
Chlorobenzene ND 0.00134 1 12/26/2016 03:46 WG938078
Chlorodibromomethane ND 0.00134 1 12/26/2016 03:46 WG938078
Chloroethane ND 0.00671 1 12/26/2016 03:46 WG938078
2-Chloroethyl vinyl ether ND 0.0671 1 12/26/2016 03:46 WG938078
Chloroform ND 0.00671 1 12/26/2016 03:46 WG938078
Chloromethane ND 0.00335 1 12/26/2016 03:46 WG938078
2-Chlorotoluene ND 0.00134 1 12/26/2016 03:46 WG938078
4-Chlorotoluene ND 0.00134 1 12/26/2016 03:46 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00671 1 12/26/2016 03:46 WG938078
1,2-Dibromoethane ND 0.00134 1 12/26/2016 03:46 WG938078
Dibromomethane ND 0.00134 1 12/26/2016 03:46 WG938078
1,2-Dichlorobenzene ND 0.00134 1 12/26/2016 03:46 WG938078
1,3-Dichlorobenzene ND 0.00134 1 12/26/2016 03:46 WG938078
1,4-Dichlorobenzene ND 0.00134 1 12/26/2016 03:46 WG938078
Dichlorodifluoromethane ND 0.00671 1 12/26/2016 03:46 WG938078
1,1-Dichloroethane ND 0.00134 1 12/26/2016 03:46 WG938078
1,2-Dichloroethane ND 0.00134 1 12/26/2016 03:46 WG938078
1,1-Dichloroethene ND 0.00134 1 12/26/2016 03:46 WG938078
cis-1,2-Dichloroethene ND 0.00134 1 12/26/2016 03:46 WG938078
trans-1,2-Dichloroethene ND 0.00134 1 12/26/2016 03:46 WG938078
1,2-Dichloropropane ND 0.00134 1 12/26/2016 03:46 WG938078
1,1-Dichloropropene ND 0.00134 1 12/26/2016 03:46 WG938078
1,3-Dichloropropane ND 0.00134 1 12/26/2016 03:46 WG938078
cis-1,3-Dichloropropene ND 0.00134 1 12/26/2016 03:46 WG938078
trans-1,3-Dichloropropene ND 0.00134 1 12/26/2016 03:46 WG938078
2,2-Dichloropropane ND 0.00134 1 12/26/2016 03:46 WG938078
Di-isopropyl ether ND 0.00134 1 12/26/2016 03:46 WG938078
Ethylbenzene ND 0.00134 1 12/26/2016 03:46 WG938078
Hexachloro-1,3-butadiene ND 0.00134 1 12/26/2016 03:46 WG938078
Isopropylbenzene ND 0.00134 1 12/26/2016 03:46 WG938078
p-Isopropyltoluene ND 0.00134 1 12/26/2016 03:46 WG938078
2-Butanone (MEK)ND 0.0134 1 12/26/2016 03:46 WG938078
Methylene Chloride ND 0.00671 1 12/26/2016 03:46 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 24 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 24 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L880142
SB-8
Collected date/time: 12/19/16 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0134 1 12/26/2016 03:46 WG938078
Methyl tert-butyl ether ND J4 0.00134 1 12/26/2016 03:46 WG938078
Naphthalene ND 0.00671 1 12/26/2016 03:46 WG938078
n-Propylbenzene ND 0.00134 1 12/26/2016 03:46 WG938078
Styrene ND 0.00134 1 12/26/2016 03:46 WG938078
1,1,1,2-Tetrachloroethane ND 0.00134 1 12/26/2016 03:46 WG938078
1,1,2,2-Tetrachloroethane ND 0.00134 1 12/26/2016 03:46 WG938078
Tetrachloroethene ND 0.00134 1 12/26/2016 03:46 WG938078
Toluene ND 0.00671 1 12/26/2016 03:46 WG938078
1,2,3-Trichlorobenzene ND 0.00134 1 12/26/2016 03:46 WG938078
1,2,4-Trichlorobenzene ND 0.00134 1 12/26/2016 03:46 WG938078
1,1,1-Trichloroethane ND 0.00134 1 12/26/2016 03:46 WG938078
1,1,2-Trichloroethane ND 0.00134 1 12/26/2016 03:46 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00134 1 12/26/2016 03:46 WG938078
Trichloroethene ND 0.00134 1 12/26/2016 03:46 WG938078
Trichlorofluoromethane ND 0.00671 1 12/26/2016 03:46 WG938078
1,2,3-Trichloropropane ND 0.00335 1 12/26/2016 03:46 WG938078
1,2,4-Trimethylbenzene ND 0.00134 1 12/26/2016 03:46 WG938078
1,3,5-Trimethylbenzene ND 0.00134 1 12/26/2016 03:46 WG938078
Vinyl chloride ND 0.00134 1 12/26/2016 03:46 WG938078
Xylenes, Total ND 0.00402 1 12/26/2016 03:46 WG938078
(S) Toluene-d8 99.0 88.7-115 12/26/2016 03:46 WG938078
(S) Dibromofluoromethane 121 76.3-123 12/26/2016 03:46 WG938078
(S) 4-Bromofluorobenzene 98.5 69.7-129 12/26/2016 03:46 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.36 1 12/29/2016 01:00 WG938642
(S) o-Terphenyl 75.4 50.0-150 12/29/2016 01:00 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 25 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 25 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L880142
SB-9
Collected date/time: 12/19/16 09:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 72.2 1 12/22/2016 11:27 WG937880
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.70 19.5 12/24/2016 05:22 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.4 59.0-128 12/24/2016 05:22 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0692 1 12/26/2016 04:08 WG938078
Acrylonitrile ND 0.0138 1 12/26/2016 04:08 WG938078
Benzene ND 0.00138 1 12/26/2016 04:08 WG938078
Bromobenzene ND 0.00138 1 12/26/2016 04:08 WG938078
Bromodichloromethane ND 0.00138 1 12/26/2016 04:08 WG938078
Bromoform ND 0.00138 1 12/26/2016 04:08 WG938078
Bromomethane ND 0.00692 1 12/26/2016 04:08 WG938078
n-Butylbenzene ND 0.00138 1 12/26/2016 04:08 WG938078
sec-Butylbenzene ND 0.00138 1 12/26/2016 04:08 WG938078
tert-Butylbenzene ND 0.00138 1 12/26/2016 04:08 WG938078
Carbon tetrachloride ND 0.00138 1 12/26/2016 04:08 WG938078
Chlorobenzene ND 0.00138 1 12/26/2016 04:08 WG938078
Chlorodibromomethane ND 0.00138 1 12/26/2016 04:08 WG938078
Chloroethane ND 0.00692 1 12/26/2016 04:08 WG938078
2-Chloroethyl vinyl ether ND 0.0692 1 12/26/2016 04:08 WG938078
Chloroform ND 0.00692 1 12/26/2016 04:08 WG938078
Chloromethane ND 0.00346 1 12/26/2016 04:08 WG938078
2-Chlorotoluene ND 0.00138 1 12/26/2016 04:08 WG938078
4-Chlorotoluene ND 0.00138 1 12/26/2016 04:08 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00692 1 12/26/2016 04:08 WG938078
1,2-Dibromoethane ND 0.00138 1 12/26/2016 04:08 WG938078
Dibromomethane ND 0.00138 1 12/26/2016 04:08 WG938078
1,2-Dichlorobenzene ND 0.00138 1 12/26/2016 04:08 WG938078
1,3-Dichlorobenzene ND 0.00138 1 12/26/2016 04:08 WG938078
1,4-Dichlorobenzene ND 0.00138 1 12/26/2016 04:08 WG938078
Dichlorodifluoromethane ND 0.00692 1 12/26/2016 04:08 WG938078
1,1-Dichloroethane ND 0.00138 1 12/26/2016 04:08 WG938078
1,2-Dichloroethane ND 0.00138 1 12/26/2016 04:08 WG938078
1,1-Dichloroethene ND 0.00138 1 12/26/2016 04:08 WG938078
cis-1,2-Dichloroethene ND 0.00138 1 12/26/2016 04:08 WG938078
trans-1,2-Dichloroethene ND 0.00138 1 12/26/2016 04:08 WG938078
1,2-Dichloropropane ND 0.00138 1 12/26/2016 04:08 WG938078
1,1-Dichloropropene ND 0.00138 1 12/26/2016 04:08 WG938078
1,3-Dichloropropane ND 0.00138 1 12/26/2016 04:08 WG938078
cis-1,3-Dichloropropene ND 0.00138 1 12/26/2016 04:08 WG938078
trans-1,3-Dichloropropene ND 0.00138 1 12/26/2016 04:08 WG938078
2,2-Dichloropropane ND 0.00138 1 12/26/2016 04:08 WG938078
Di-isopropyl ether ND 0.00138 1 12/26/2016 04:08 WG938078
Ethylbenzene ND 0.00138 1 12/26/2016 04:08 WG938078
Hexachloro-1,3-butadiene ND 0.00138 1 12/26/2016 04:08 WG938078
Isopropylbenzene ND 0.00138 1 12/26/2016 04:08 WG938078
p-Isopropyltoluene ND 0.00138 1 12/26/2016 04:08 WG938078
2-Butanone (MEK)ND 0.0138 1 12/26/2016 04:08 WG938078
Methylene Chloride ND 0.00692 1 12/26/2016 04:08 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 26 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 26 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L880142
SB-9
Collected date/time: 12/19/16 09:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0138 1 12/26/2016 04:08 WG938078
Methyl tert-butyl ether ND J4 0.00138 1 12/26/2016 04:08 WG938078
Naphthalene ND 0.00692 1 12/26/2016 04:08 WG938078
n-Propylbenzene ND 0.00138 1 12/26/2016 04:08 WG938078
Styrene ND 0.00138 1 12/26/2016 04:08 WG938078
1,1,1,2-Tetrachloroethane ND 0.00138 1 12/26/2016 04:08 WG938078
1,1,2,2-Tetrachloroethane ND 0.00138 1 12/26/2016 04:08 WG938078
Tetrachloroethene ND 0.00138 1 12/26/2016 04:08 WG938078
Toluene ND 0.00692 1 12/26/2016 04:08 WG938078
1,2,3-Trichlorobenzene ND 0.00138 1 12/26/2016 04:08 WG938078
1,2,4-Trichlorobenzene ND 0.00138 1 12/26/2016 04:08 WG938078
1,1,1-Trichloroethane ND 0.00138 1 12/26/2016 04:08 WG938078
1,1,2-Trichloroethane ND 0.00138 1 12/26/2016 04:08 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00138 1 12/26/2016 04:08 WG938078
Trichloroethene ND 0.00138 1 12/26/2016 04:08 WG938078
Trichlorofluoromethane ND 0.00692 1 12/26/2016 04:08 WG938078
1,2,3-Trichloropropane ND 0.00346 1 12/26/2016 04:08 WG938078
1,2,4-Trimethylbenzene ND 0.00138 1 12/26/2016 04:08 WG938078
1,3,5-Trimethylbenzene ND 0.00138 1 12/26/2016 04:08 WG938078
Vinyl chloride ND 0.00138 1 12/26/2016 04:08 WG938078
Xylenes, Total ND 0.00415 1 12/26/2016 04:08 WG938078
(S) Toluene-d8 106 88.7-115 12/26/2016 04:08 WG938078
(S) Dibromofluoromethane 111 76.3-123 12/26/2016 04:08 WG938078
(S) 4-Bromofluorobenzene 99.6 69.7-129 12/26/2016 04:08 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.54 1 12/29/2016 01:12 WG938642
(S) o-Terphenyl 59.1 50.0-150 12/29/2016 01:12 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 27 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 27 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L880142
SB-10
Collected date/time: 12/19/16 09:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 72.8 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.71 19.75 12/24/2016 05:44 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.4 59.0-128 12/24/2016 05:44 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0687 1 12/26/2016 04:31 WG938078
Acrylonitrile ND 0.0137 1 12/26/2016 04:31 WG938078
Benzene ND 0.00137 1 12/26/2016 04:31 WG938078
Bromobenzene ND 0.00137 1 12/26/2016 04:31 WG938078
Bromodichloromethane ND 0.00137 1 12/26/2016 04:31 WG938078
Bromoform ND 0.00137 1 12/26/2016 04:31 WG938078
Bromomethane ND 0.00687 1 12/26/2016 04:31 WG938078
n-Butylbenzene ND 0.00137 1 12/26/2016 04:31 WG938078
sec-Butylbenzene ND 0.00137 1 12/26/2016 04:31 WG938078
tert-Butylbenzene ND 0.00137 1 12/26/2016 04:31 WG938078
Carbon tetrachloride ND 0.00137 1 12/26/2016 04:31 WG938078
Chlorobenzene ND 0.00137 1 12/26/2016 04:31 WG938078
Chlorodibromomethane ND 0.00137 1 12/26/2016 04:31 WG938078
Chloroethane ND 0.00687 1 12/26/2016 04:31 WG938078
2-Chloroethyl vinyl ether ND 0.0687 1 12/26/2016 04:31 WG938078
Chloroform 0.0564 0.00687 1 12/26/2016 04:31 WG938078
Chloromethane ND 0.00343 1 12/26/2016 04:31 WG938078
2-Chlorotoluene ND 0.00137 1 12/26/2016 04:31 WG938078
4-Chlorotoluene ND 0.00137 1 12/26/2016 04:31 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00687 1 12/26/2016 04:31 WG938078
1,2-Dibromoethane ND 0.00137 1 12/26/2016 04:31 WG938078
Dibromomethane ND 0.00137 1 12/26/2016 04:31 WG938078
1,2-Dichlorobenzene ND 0.00137 1 12/26/2016 04:31 WG938078
1,3-Dichlorobenzene ND 0.00137 1 12/26/2016 04:31 WG938078
1,4-Dichlorobenzene ND 0.00137 1 12/26/2016 04:31 WG938078
Dichlorodifluoromethane ND 0.00687 1 12/26/2016 04:31 WG938078
1,1-Dichloroethane ND 0.00137 1 12/26/2016 04:31 WG938078
1,2-Dichloroethane ND 0.00137 1 12/26/2016 04:31 WG938078
1,1-Dichloroethene ND 0.00137 1 12/26/2016 04:31 WG938078
cis-1,2-Dichloroethene ND 0.00137 1 12/26/2016 04:31 WG938078
trans-1,2-Dichloroethene ND 0.00137 1 12/26/2016 04:31 WG938078
1,2-Dichloropropane ND 0.00137 1 12/26/2016 04:31 WG938078
1,1-Dichloropropene ND 0.00137 1 12/26/2016 04:31 WG938078
1,3-Dichloropropane ND 0.00137 1 12/26/2016 04:31 WG938078
cis-1,3-Dichloropropene ND 0.00137 1 12/26/2016 04:31 WG938078
trans-1,3-Dichloropropene ND 0.00137 1 12/26/2016 04:31 WG938078
2,2-Dichloropropane ND 0.00137 1 12/26/2016 04:31 WG938078
Di-isopropyl ether ND 0.00137 1 12/26/2016 04:31 WG938078
Ethylbenzene ND 0.00137 1 12/26/2016 04:31 WG938078
Hexachloro-1,3-butadiene ND 0.00137 1 12/26/2016 04:31 WG938078
Isopropylbenzene ND 0.00137 1 12/26/2016 04:31 WG938078
p-Isopropyltoluene ND 0.00137 1 12/26/2016 04:31 WG938078
2-Butanone (MEK)ND 0.0137 1 12/26/2016 04:31 WG938078
Methylene Chloride ND 0.00687 1 12/26/2016 04:31 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 28 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 28 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L880142
SB-10
Collected date/time: 12/19/16 09:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0137 1 12/26/2016 04:31 WG938078
Methyl tert-butyl ether ND J4 0.00137 1 12/26/2016 04:31 WG938078
Naphthalene ND 0.00687 1 12/26/2016 04:31 WG938078
n-Propylbenzene ND 0.00137 1 12/26/2016 04:31 WG938078
Styrene ND 0.00137 1 12/26/2016 04:31 WG938078
1,1,1,2-Tetrachloroethane ND 0.00137 1 12/26/2016 04:31 WG938078
1,1,2,2-Tetrachloroethane ND 0.00137 1 12/26/2016 04:31 WG938078
Tetrachloroethene ND 0.00137 1 12/26/2016 04:31 WG938078
Toluene ND 0.00687 1 12/26/2016 04:31 WG938078
1,2,3-Trichlorobenzene ND 0.00137 1 12/26/2016 04:31 WG938078
1,2,4-Trichlorobenzene ND 0.00137 1 12/26/2016 04:31 WG938078
1,1,1-Trichloroethane ND 0.00137 1 12/26/2016 04:31 WG938078
1,1,2-Trichloroethane ND 0.00137 1 12/26/2016 04:31 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00137 1 12/26/2016 04:31 WG938078
Trichloroethene ND 0.00137 1 12/26/2016 04:31 WG938078
Trichlorofluoromethane ND 0.00687 1 12/26/2016 04:31 WG938078
1,2,3-Trichloropropane ND 0.00343 1 12/26/2016 04:31 WG938078
1,2,4-Trimethylbenzene ND 0.00137 1 12/26/2016 04:31 WG938078
1,3,5-Trimethylbenzene ND 0.00137 1 12/26/2016 04:31 WG938078
Vinyl chloride ND 0.00137 1 12/26/2016 04:31 WG938078
Xylenes, Total ND 0.00412 1 12/26/2016 04:31 WG938078
(S) Toluene-d8 104 88.7-115 12/26/2016 04:31 WG938078
(S) Dibromofluoromethane 111 76.3-123 12/26/2016 04:31 WG938078
(S) 4-Bromofluorobenzene 98.7 69.7-129 12/26/2016 04:31 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.49 1 12/29/2016 01:24 WG938642
(S) o-Terphenyl 71.5 50.0-150 12/29/2016 01:24 WG938642
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0453 1 12/29/2016 14:46 WG938702
Acenaphthylene ND 0.0453 1 12/29/2016 14:46 WG938702
Anthracene ND 0.0453 1 12/29/2016 14:46 WG938702
Benzidine ND 0.457 1 12/29/2016 14:46 WG938702
Benzo(a)anthracene ND 0.0453 1 12/29/2016 14:46 WG938702
Benzo(b)fluoranthene ND 0.0453 1 12/29/2016 14:46 WG938702
Benzo(k)fluoranthene ND 0.0453 1 12/29/2016 14:46 WG938702
Benzo(g,h,i)perylene ND 0.0453 1 12/29/2016 14:46 WG938702
Benzo(a)pyrene ND 0.0453 1 12/29/2016 14:46 WG938702
Bis(2-chlorethoxy)methane ND 0.457 1 12/29/2016 14:46 WG938702
Bis(2-chloroethyl)ether ND 0.457 1 12/29/2016 14:46 WG938702
Bis(2-chloroisopropyl)ether ND 0.457 1 12/29/2016 14:46 WG938702
4-Bromophenyl-phenylether ND 0.457 1 12/29/2016 14:46 WG938702
2-Chloronaphthalene ND 0.0453 1 12/29/2016 14:46 WG938702
4-Chlorophenyl-phenylether ND 0.457 1 12/29/2016 14:46 WG938702
Chrysene ND 0.0453 1 12/29/2016 14:46 WG938702
Dibenz(a,h)anthracene ND 0.0453 1 12/29/2016 14:46 WG938702
3,3-Dichlorobenzidine ND 0.457 1 12/29/2016 14:46 WG938702
2,4-Dinitrotoluene ND 0.457 1 12/29/2016 14:46 WG938702
2,6-Dinitrotoluene ND 0.457 1 12/29/2016 14:46 WG938702
Fluoranthene ND 0.0453 1 12/29/2016 14:46 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 29 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L880142
SB-10
Collected date/time: 12/19/16 09:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0453 1 12/29/2016 14:46 WG938702
Hexachlorobenzene ND 0.457 1 12/29/2016 14:46 WG938702
Hexachloro-1,3-butadiene ND 0.457 1 12/29/2016 14:46 WG938702
Hexachlorocyclopentadiene ND 0.457 1 12/29/2016 14:46 WG938702
Hexachloroethane ND 0.457 1 12/29/2016 14:46 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0453 1 12/29/2016 14:46 WG938702
Isophorone ND 0.457 1 12/29/2016 14:46 WG938702
Naphthalene ND 0.0453 1 12/29/2016 14:46 WG938702
Nitrobenzene ND 0.457 1 12/29/2016 14:46 WG938702
n-Nitrosodimethylamine ND 0.457 1 12/29/2016 14:46 WG938702
n-Nitrosodiphenylamine ND 0.457 1 12/29/2016 14:46 WG938702
n-Nitrosodi-n-propylamine ND 0.457 1 12/29/2016 14:46 WG938702
Phenanthrene ND 0.0453 1 12/29/2016 14:46 WG938702
Benzylbutyl phthalate ND 0.457 1 12/29/2016 14:46 WG938702
Bis(2-ethylhexyl)phthalate ND 0.457 1 12/29/2016 14:46 WG938702
Di-n-butyl phthalate ND 0.457 1 12/29/2016 14:46 WG938702
Diethyl phthalate ND 0.457 1 12/29/2016 14:46 WG938702
Dimethyl phthalate ND 0.457 1 12/29/2016 14:46 WG938702
Di-n-octyl phthalate ND 0.457 1 12/29/2016 14:46 WG938702
Pyrene ND 0.0453 1 12/29/2016 14:46 WG938702
1,2,4-Trichlorobenzene ND 0.457 1 12/29/2016 14:46 WG938702
4-Chloro-3-methylphenol ND 0.457 1 12/29/2016 14:46 WG938702
2-Chlorophenol ND 0.457 1 12/29/2016 14:46 WG938702
2,4-Dichlorophenol ND 0.457 1 12/29/2016 14:46 WG938702
2,4-Dimethylphenol ND 0.457 1 12/29/2016 14:46 WG938702
4,6-Dinitro-2-methylphenol ND 0.457 1 12/29/2016 14:46 WG938702
2,4-Dinitrophenol ND J3 0.457 1 12/29/2016 14:46 WG938702
2-Nitrophenol ND 0.457 1 12/29/2016 14:46 WG938702
4-Nitrophenol ND 0.457 1 12/29/2016 14:46 WG938702
Pentachlorophenol ND 0.457 1 12/29/2016 14:46 WG938702
Phenol ND 0.457 1 12/29/2016 14:46 WG938702
2,4,6-Trichlorophenol ND 0.457 1 12/29/2016 14:46 WG938702
(S) 2-Fluorophenol 57.5 21.1-116 12/29/2016 14:46 WG938702
(S) Phenol-d5 58.8 26.3-121 12/29/2016 14:46 WG938702
(S) Nitrobenzene-d5 55.9 21.9-129 12/29/2016 14:46 WG938702
(S) 2-Fluorobiphenyl 62.5 34.9-129 12/29/2016 14:46 WG938702
(S) 2,4,6-Tribromophenol 59.9 21.6-142 12/29/2016 14:46 WG938702
(S) p-Terphenyl-d14 68.0 21.5-128 12/29/2016 14:46 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 30 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L880142
SB-11
Collected date/time: 12/19/16 09:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.2 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.83 20.75 12/24/2016 06:06 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.6 59.0-128 12/24/2016 06:06 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0683 1 12/26/2016 04:54 WG938078
Acrylonitrile ND 0.0137 1 12/26/2016 04:54 WG938078
Benzene ND 0.00137 1 12/26/2016 04:54 WG938078
Bromobenzene ND 0.00137 1 12/26/2016 04:54 WG938078
Bromodichloromethane ND 0.00137 1 12/26/2016 04:54 WG938078
Bromoform ND 0.00137 1 12/26/2016 04:54 WG938078
Bromomethane ND 0.00683 1 12/26/2016 04:54 WG938078
n-Butylbenzene ND 0.00137 1 12/26/2016 04:54 WG938078
sec-Butylbenzene ND 0.00137 1 12/26/2016 04:54 WG938078
tert-Butylbenzene ND 0.00137 1 12/26/2016 04:54 WG938078
Carbon tetrachloride ND 0.00137 1 12/26/2016 04:54 WG938078
Chlorobenzene ND 0.00137 1 12/26/2016 04:54 WG938078
Chlorodibromomethane ND 0.00137 1 12/26/2016 04:54 WG938078
Chloroethane ND 0.00683 1 12/26/2016 04:54 WG938078
2-Chloroethyl vinyl ether ND 0.0683 1 12/26/2016 04:54 WG938078
Chloroform ND 0.00683 1 12/26/2016 04:54 WG938078
Chloromethane ND 0.00341 1 12/26/2016 04:54 WG938078
2-Chlorotoluene ND 0.00137 1 12/26/2016 04:54 WG938078
4-Chlorotoluene ND 0.00137 1 12/26/2016 04:54 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00683 1 12/26/2016 04:54 WG938078
1,2-Dibromoethane ND 0.00137 1 12/26/2016 04:54 WG938078
Dibromomethane ND 0.00137 1 12/26/2016 04:54 WG938078
1,2-Dichlorobenzene ND 0.00137 1 12/26/2016 04:54 WG938078
1,3-Dichlorobenzene ND 0.00137 1 12/26/2016 04:54 WG938078
1,4-Dichlorobenzene ND 0.00137 1 12/26/2016 04:54 WG938078
Dichlorodifluoromethane ND 0.00683 1 12/26/2016 04:54 WG938078
1,1-Dichloroethane ND 0.00137 1 12/26/2016 04:54 WG938078
1,2-Dichloroethane ND 0.00137 1 12/26/2016 04:54 WG938078
1,1-Dichloroethene ND 0.00137 1 12/26/2016 04:54 WG938078
cis-1,2-Dichloroethene ND 0.00137 1 12/26/2016 04:54 WG938078
trans-1,2-Dichloroethene ND 0.00137 1 12/26/2016 04:54 WG938078
1,2-Dichloropropane ND 0.00137 1 12/26/2016 04:54 WG938078
1,1-Dichloropropene ND 0.00137 1 12/26/2016 04:54 WG938078
1,3-Dichloropropane ND 0.00137 1 12/26/2016 04:54 WG938078
cis-1,3-Dichloropropene ND 0.00137 1 12/26/2016 04:54 WG938078
trans-1,3-Dichloropropene ND 0.00137 1 12/26/2016 04:54 WG938078
2,2-Dichloropropane ND 0.00137 1 12/26/2016 04:54 WG938078
Di-isopropyl ether ND 0.00137 1 12/26/2016 04:54 WG938078
Ethylbenzene ND 0.00137 1 12/26/2016 04:54 WG938078
Hexachloro-1,3-butadiene ND 0.00137 1 12/26/2016 04:54 WG938078
Isopropylbenzene ND 0.00137 1 12/26/2016 04:54 WG938078
p-Isopropyltoluene ND 0.00137 1 12/26/2016 04:54 WG938078
2-Butanone (MEK)ND 0.0137 1 12/26/2016 04:54 WG938078
Methylene Chloride ND 0.00683 1 12/26/2016 04:54 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L880142
SB-11
Collected date/time: 12/19/16 09:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0137 1 12/26/2016 04:54 WG938078
Methyl tert-butyl ether ND J4 0.00137 1 12/26/2016 04:54 WG938078
Naphthalene ND 0.00683 1 12/26/2016 04:54 WG938078
n-Propylbenzene ND 0.00137 1 12/26/2016 04:54 WG938078
Styrene ND 0.00137 1 12/26/2016 04:54 WG938078
1,1,1,2-Tetrachloroethane ND 0.00137 1 12/26/2016 04:54 WG938078
1,1,2,2-Tetrachloroethane ND 0.00137 1 12/26/2016 04:54 WG938078
Tetrachloroethene ND 0.00137 1 12/26/2016 04:54 WG938078
Toluene ND 0.00683 1 12/26/2016 04:54 WG938078
1,2,3-Trichlorobenzene ND 0.00137 1 12/26/2016 04:54 WG938078
1,2,4-Trichlorobenzene ND 0.00137 1 12/26/2016 04:54 WG938078
1,1,1-Trichloroethane ND 0.00137 1 12/26/2016 04:54 WG938078
1,1,2-Trichloroethane ND 0.00137 1 12/26/2016 04:54 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00137 1 12/26/2016 04:54 WG938078
Trichloroethene ND 0.00137 1 12/26/2016 04:54 WG938078
Trichlorofluoromethane ND 0.00683 1 12/26/2016 04:54 WG938078
1,2,3-Trichloropropane ND 0.00341 1 12/26/2016 04:54 WG938078
1,2,4-Trimethylbenzene ND 0.00137 1 12/26/2016 04:54 WG938078
1,3,5-Trimethylbenzene ND 0.00137 1 12/26/2016 04:54 WG938078
Vinyl chloride ND 0.00137 1 12/26/2016 04:54 WG938078
Xylenes, Total ND 0.00410 1 12/26/2016 04:54 WG938078
(S) Toluene-d8 105 88.7-115 12/26/2016 04:54 WG938078
(S) Dibromofluoromethane 120 76.3-123 12/26/2016 04:54 WG938078
(S) 4-Bromofluorobenzene 101 69.7-129 12/26/2016 04:54 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 419 5.46 1 12/29/2016 01:36 WG938642
(S) o-Terphenyl 99.1 50.0-150 12/29/2016 01:36 WG938642
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0451 1 12/29/2016 15:12 WG938702
Acenaphthylene ND 0.0451 1 12/29/2016 15:12 WG938702
Anthracene ND 0.0451 1 12/29/2016 15:12 WG938702
Benzidine ND 0.455 1 12/29/2016 15:12 WG938702
Benzo(a)anthracene ND 0.0451 1 12/29/2016 15:12 WG938702
Benzo(b)fluoranthene ND 0.0451 1 12/29/2016 15:12 WG938702
Benzo(k)fluoranthene ND 0.0451 1 12/29/2016 15:12 WG938702
Benzo(g,h,i)perylene ND 0.0451 1 12/29/2016 15:12 WG938702
Benzo(a)pyrene ND 0.0451 1 12/29/2016 15:12 WG938702
Bis(2-chlorethoxy)methane ND 0.455 1 12/29/2016 15:12 WG938702
Bis(2-chloroethyl)ether ND 0.455 1 12/29/2016 15:12 WG938702
Bis(2-chloroisopropyl)ether ND 0.455 1 12/29/2016 15:12 WG938702
4-Bromophenyl-phenylether ND 0.455 1 12/29/2016 15:12 WG938702
2-Chloronaphthalene ND 0.0451 1 12/29/2016 15:12 WG938702
4-Chlorophenyl-phenylether ND 0.455 1 12/29/2016 15:12 WG938702
Chrysene ND 0.0451 1 12/29/2016 15:12 WG938702
Dibenz(a,h)anthracene ND 0.0451 1 12/29/2016 15:12 WG938702
3,3-Dichlorobenzidine ND 0.455 1 12/29/2016 15:12 WG938702
2,4-Dinitrotoluene ND 0.455 1 12/29/2016 15:12 WG938702
2,6-Dinitrotoluene ND 0.455 1 12/29/2016 15:12 WG938702
Fluoranthene ND 0.0451 1 12/29/2016 15:12 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L880142
SB-11
Collected date/time: 12/19/16 09:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0451 1 12/29/2016 15:12 WG938702
Hexachlorobenzene ND 0.455 1 12/29/2016 15:12 WG938702
Hexachloro-1,3-butadiene ND 0.455 1 12/29/2016 15:12 WG938702
Hexachlorocyclopentadiene ND 0.455 1 12/29/2016 15:12 WG938702
Hexachloroethane ND 0.455 1 12/29/2016 15:12 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0451 1 12/29/2016 15:12 WG938702
Isophorone ND 0.455 1 12/29/2016 15:12 WG938702
Naphthalene ND 0.0451 1 12/29/2016 15:12 WG938702
Nitrobenzene ND 0.455 1 12/29/2016 15:12 WG938702
n-Nitrosodimethylamine ND 0.455 1 12/29/2016 15:12 WG938702
n-Nitrosodiphenylamine ND 0.455 1 12/29/2016 15:12 WG938702
n-Nitrosodi-n-propylamine ND 0.455 1 12/29/2016 15:12 WG938702
Phenanthrene 0.0845 0.0451 1 12/29/2016 15:12 WG938702
Benzylbutyl phthalate ND 0.455 1 12/29/2016 15:12 WG938702
Bis(2-ethylhexyl)phthalate ND 0.455 1 12/29/2016 15:12 WG938702
Di-n-butyl phthalate ND 0.455 1 12/29/2016 15:12 WG938702
Diethyl phthalate ND 0.455 1 12/29/2016 15:12 WG938702
Dimethyl phthalate ND 0.455 1 12/29/2016 15:12 WG938702
Di-n-octyl phthalate ND 0.455 1 12/29/2016 15:12 WG938702
Pyrene ND 0.0451 1 12/29/2016 15:12 WG938702
1,2,4-Trichlorobenzene ND 0.455 1 12/29/2016 15:12 WG938702
4-Chloro-3-methylphenol ND 0.455 1 12/29/2016 15:12 WG938702
2-Chlorophenol ND 0.455 1 12/29/2016 15:12 WG938702
2,4-Dichlorophenol ND 0.455 1 12/29/2016 15:12 WG938702
2,4-Dimethylphenol ND 0.455 1 12/29/2016 15:12 WG938702
4,6-Dinitro-2-methylphenol ND 0.455 1 12/29/2016 15:12 WG938702
2,4-Dinitrophenol ND J3 0.455 1 12/29/2016 15:12 WG938702
2-Nitrophenol ND 0.455 1 12/29/2016 15:12 WG938702
4-Nitrophenol ND 0.455 1 12/29/2016 15:12 WG938702
Pentachlorophenol ND 0.455 1 12/29/2016 15:12 WG938702
Phenol ND 0.455 1 12/29/2016 15:12 WG938702
2,4,6-Trichlorophenol ND 0.455 1 12/29/2016 15:12 WG938702
(S) 2-Fluorophenol 59.8 21.1-116 12/29/2016 15:12 WG938702
(S) Phenol-d5 61.9 26.3-121 12/29/2016 15:12 WG938702
(S) Nitrobenzene-d5 60.2 21.9-129 12/29/2016 15:12 WG938702
(S) 2-Fluorobiphenyl 61.2 34.9-129 12/29/2016 15:12 WG938702
(S) 2,4,6-Tribromophenol 68.2 21.6-142 12/29/2016 15:12 WG938702
(S) p-Terphenyl-d14 66.9 21.5-128 12/29/2016 15:12 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L880142
SB-12
Collected date/time: 12/19/16 09:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.6 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.30 18.75 12/24/2016 06:28 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.3 59.0-128 12/24/2016 06:28 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0613 1 12/26/2016 05:16 WG938078
Acrylonitrile ND 0.0123 1 12/26/2016 05:16 WG938078
Benzene ND 0.00123 1 12/26/2016 05:16 WG938078
Bromobenzene ND 0.00123 1 12/26/2016 05:16 WG938078
Bromodichloromethane ND 0.00123 1 12/26/2016 05:16 WG938078
Bromoform ND 0.00123 1 12/26/2016 05:16 WG938078
Bromomethane ND 0.00613 1 12/26/2016 05:16 WG938078
n-Butylbenzene ND 0.00123 1 12/26/2016 05:16 WG938078
sec-Butylbenzene ND 0.00123 1 12/26/2016 05:16 WG938078
tert-Butylbenzene ND 0.00123 1 12/26/2016 05:16 WG938078
Carbon tetrachloride ND 0.00123 1 12/26/2016 05:16 WG938078
Chlorobenzene ND 0.00123 1 12/26/2016 05:16 WG938078
Chlorodibromomethane ND 0.00123 1 12/26/2016 05:16 WG938078
Chloroethane ND 0.00613 1 12/26/2016 05:16 WG938078
2-Chloroethyl vinyl ether ND 0.0613 1 12/26/2016 05:16 WG938078
Chloroform ND 0.00613 1 12/26/2016 05:16 WG938078
Chloromethane ND 0.00306 1 12/26/2016 05:16 WG938078
2-Chlorotoluene ND 0.00123 1 12/26/2016 05:16 WG938078
4-Chlorotoluene ND 0.00123 1 12/26/2016 05:16 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00613 1 12/26/2016 05:16 WG938078
1,2-Dibromoethane ND 0.00123 1 12/26/2016 05:16 WG938078
Dibromomethane ND 0.00123 1 12/26/2016 05:16 WG938078
1,2-Dichlorobenzene ND 0.00123 1 12/26/2016 05:16 WG938078
1,3-Dichlorobenzene ND 0.00123 1 12/26/2016 05:16 WG938078
1,4-Dichlorobenzene ND 0.00123 1 12/26/2016 05:16 WG938078
Dichlorodifluoromethane ND 0.00613 1 12/26/2016 05:16 WG938078
1,1-Dichloroethane ND 0.00123 1 12/26/2016 05:16 WG938078
1,2-Dichloroethane ND 0.00123 1 12/26/2016 05:16 WG938078
1,1-Dichloroethene ND 0.00123 1 12/26/2016 05:16 WG938078
cis-1,2-Dichloroethene ND 0.00123 1 12/26/2016 05:16 WG938078
trans-1,2-Dichloroethene ND 0.00123 1 12/26/2016 05:16 WG938078
1,2-Dichloropropane ND 0.00123 1 12/26/2016 05:16 WG938078
1,1-Dichloropropene ND 0.00123 1 12/26/2016 05:16 WG938078
1,3-Dichloropropane ND 0.00123 1 12/26/2016 05:16 WG938078
cis-1,3-Dichloropropene ND 0.00123 1 12/26/2016 05:16 WG938078
trans-1,3-Dichloropropene ND 0.00123 1 12/26/2016 05:16 WG938078
2,2-Dichloropropane ND 0.00123 1 12/26/2016 05:16 WG938078
Di-isopropyl ether ND 0.00123 1 12/26/2016 05:16 WG938078
Ethylbenzene ND 0.00123 1 12/26/2016 05:16 WG938078
Hexachloro-1,3-butadiene ND 0.00123 1 12/26/2016 05:16 WG938078
Isopropylbenzene ND 0.00123 1 12/26/2016 05:16 WG938078
p-Isopropyltoluene ND 0.00123 1 12/26/2016 05:16 WG938078
2-Butanone (MEK)ND 0.0123 1 12/26/2016 05:16 WG938078
Methylene Chloride ND 0.00613 1 12/26/2016 05:16 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L880142
SB-12
Collected date/time: 12/19/16 09:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0123 1 12/26/2016 05:16 WG938078
Methyl tert-butyl ether ND J4 0.00123 1 12/26/2016 05:16 WG938078
Naphthalene ND 0.00613 1 12/26/2016 05:16 WG938078
n-Propylbenzene ND 0.00123 1 12/26/2016 05:16 WG938078
Styrene ND 0.00123 1 12/26/2016 05:16 WG938078
1,1,1,2-Tetrachloroethane ND 0.00123 1 12/26/2016 05:16 WG938078
1,1,2,2-Tetrachloroethane ND 0.00123 1 12/26/2016 05:16 WG938078
Tetrachloroethene ND 0.00123 1 12/26/2016 05:16 WG938078
Toluene ND 0.00613 1 12/26/2016 05:16 WG938078
1,2,3-Trichlorobenzene ND 0.00123 1 12/26/2016 05:16 WG938078
1,2,4-Trichlorobenzene ND 0.00123 1 12/26/2016 05:16 WG938078
1,1,1-Trichloroethane ND 0.00123 1 12/26/2016 05:16 WG938078
1,1,2-Trichloroethane ND 0.00123 1 12/26/2016 05:16 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00123 1 12/26/2016 05:16 WG938078
Trichloroethene ND 0.00123 1 12/26/2016 05:16 WG938078
Trichlorofluoromethane ND 0.00613 1 12/26/2016 05:16 WG938078
1,2,3-Trichloropropane ND 0.00306 1 12/26/2016 05:16 WG938078
1,2,4-Trimethylbenzene ND 0.00123 1 12/26/2016 05:16 WG938078
1,3,5-Trimethylbenzene ND 0.00123 1 12/26/2016 05:16 WG938078
Vinyl chloride ND 0.00123 1 12/26/2016 05:16 WG938078
Xylenes, Total ND 0.00368 1 12/26/2016 05:16 WG938078
(S) Toluene-d8 105 88.7-115 12/26/2016 05:16 WG938078
(S) Dibromofluoromethane 111 76.3-123 12/26/2016 05:16 WG938078
(S) 4-Bromofluorobenzene 101 69.7-129 12/26/2016 05:16 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 4.90 1 12/29/2016 02:25 WG938642
(S) o-Terphenyl 81.2 50.0-150 12/29/2016 02:25 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L880142
SB-13
Collected date/time: 12/19/16 09:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.1 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 4.10 B 2.67 19.75 12/28/2016 08:10 WG938086
(S) a,a,a-Trifluorotoluene(FID) 93.2 59.0-128 12/28/2016 08:10 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 1.33 19.75 12/29/2016 03:55 WG938078
Acrylonitrile ND 0.267 19.75 12/29/2016 03:55 WG938078
Benzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Bromobenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Bromodichloromethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
Bromoform ND 0.0267 19.75 12/29/2016 03:55 WG938078
Bromomethane ND 0.133 19.75 12/29/2016 03:55 WG938078
n-Butylbenzene 0.0459 0.0267 19.75 12/29/2016 03:55 WG938078
sec-Butylbenzene 0.0373 0.0267 19.75 12/29/2016 03:55 WG938078
tert-Butylbenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Carbon tetrachloride ND 0.0267 19.75 12/29/2016 03:55 WG938078
Chlorobenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Chlorodibromomethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
Chloroethane ND 0.133 19.75 12/29/2016 03:55 WG938078
2-Chloroethyl vinyl ether ND 1.33 19.75 12/29/2016 03:55 WG938078
Chloroform ND 0.133 19.75 12/29/2016 03:55 WG938078
Chloromethane ND 0.0667 19.75 12/29/2016 03:55 WG938078
2-Chlorotoluene ND 0.0267 19.75 12/29/2016 03:55 WG938078
4-Chlorotoluene ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,2-Dibromo-3-Chloropropane ND 0.133 19.75 12/29/2016 03:55 WG938078
1,2-Dibromoethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
Dibromomethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,2-Dichlorobenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,3-Dichlorobenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,4-Dichlorobenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Dichlorodifluoromethane ND 0.133 19.75 12/29/2016 03:55 WG938078
1,1-Dichloroethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,2-Dichloroethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,1-Dichloroethene ND 0.0267 19.75 12/29/2016 03:55 WG938078
cis-1,2-Dichloroethene ND 0.0267 19.75 12/29/2016 03:55 WG938078
trans-1,2-Dichloroethene ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,2-Dichloropropane ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,1-Dichloropropene ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,3-Dichloropropane ND 0.0267 19.75 12/29/2016 03:55 WG938078
cis-1,3-Dichloropropene ND 0.0267 19.75 12/29/2016 03:55 WG938078
trans-1,3-Dichloropropene ND 0.0267 19.75 12/29/2016 03:55 WG938078
2,2-Dichloropropane ND 0.0267 19.75 12/29/2016 03:55 WG938078
Di-isopropyl ether ND 0.0267 19.75 12/29/2016 03:55 WG938078
Ethylbenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Hexachloro-1,3-butadiene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Isopropylbenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
p-Isopropyltoluene 0.0304 0.0267 19.75 12/29/2016 03:55 WG938078
2-Butanone (MEK)ND 0.267 19.75 12/29/2016 03:55 WG938078
Methylene Chloride ND 0.133 19.75 12/29/2016 03:55 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L880142
SB-13
Collected date/time: 12/19/16 09:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.267 19.75 12/29/2016 03:55 WG938078
Methyl tert-butyl ether ND J4 0.0267 19.75 12/29/2016 03:55 WG938078
Naphthalene 0.330 0.133 19.75 12/29/2016 03:55 WG938078
n-Propylbenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Styrene ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,1,1,2-Tetrachloroethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,1,2,2-Tetrachloroethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
Tetrachloroethene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Toluene ND 0.133 19.75 12/29/2016 03:55 WG938078
1,2,3-Trichlorobenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,2,4-Trichlorobenzene ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,1,1-Trichloroethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,1,2-Trichloroethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.0267 19.75 12/29/2016 03:55 WG938078
Trichloroethene ND 0.0267 19.75 12/29/2016 03:55 WG938078
Trichlorofluoromethane ND 0.133 19.75 12/29/2016 03:55 WG938078
1,2,3-Trichloropropane ND 0.0667 19.75 12/29/2016 03:55 WG938078
1,2,4-Trimethylbenzene 0.199 0.0267 19.75 12/29/2016 03:55 WG938078
1,3,5-Trimethylbenzene 0.0544 0.0267 19.75 12/29/2016 03:55 WG938078
Vinyl chloride ND 0.0267 19.75 12/29/2016 03:55 WG938078
Xylenes, Total ND 0.0800 19.75 12/29/2016 03:55 WG938078
(S) Toluene-d8 102 88.7-115 12/29/2016 03:55 WG938078
(S) Dibromofluoromethane 95.7 76.3-123 12/29/2016 03:55 WG938078
(S) 4-Bromofluorobenzene 94.8 69.7-129 12/29/2016 03:55 WG938078
Sample Narrative:
8260B L880142-12 WG938078: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 497 5.40 1 12/29/2016 02:37 WG938642
(S) o-Terphenyl 109 50.0-150 12/29/2016 02:37 WG938642
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene 0.103 0.0445 1 12/29/2016 15:38 WG938702
Acenaphthylene ND 0.0445 1 12/29/2016 15:38 WG938702
Anthracene ND 0.0445 1 12/29/2016 15:38 WG938702
Benzidine ND 0.450 1 12/29/2016 15:38 WG938702
Benzo(a)anthracene ND 0.0445 1 12/29/2016 15:38 WG938702
Benzo(b)fluoranthene ND 0.0445 1 12/29/2016 15:38 WG938702
Benzo(k)fluoranthene ND 0.0445 1 12/29/2016 15:38 WG938702
Benzo(g,h,i)perylene ND 0.0445 1 12/29/2016 15:38 WG938702
Benzo(a)pyrene ND 0.0445 1 12/29/2016 15:38 WG938702
Bis(2-chlorethoxy)methane ND 0.450 1 12/29/2016 15:38 WG938702
Bis(2-chloroethyl)ether ND 0.450 1 12/29/2016 15:38 WG938702
Bis(2-chloroisopropyl)ether ND 0.450 1 12/29/2016 15:38 WG938702
4-Bromophenyl-phenylether ND 0.450 1 12/29/2016 15:38 WG938702
2-Chloronaphthalene ND 0.0445 1 12/29/2016 15:38 WG938702
4-Chlorophenyl-phenylether ND 0.450 1 12/29/2016 15:38 WG938702
Chrysene ND 0.0445 1 12/29/2016 15:38 WG938702
Dibenz(a,h)anthracene ND 0.0445 1 12/29/2016 15:38 WG938702
3,3-Dichlorobenzidine ND 0.450 1 12/29/2016 15:38 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L880142
SB-13
Collected date/time: 12/19/16 09:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2,4-Dinitrotoluene ND 0.450 1 12/29/2016 15:38 WG938702
2,6-Dinitrotoluene ND 0.450 1 12/29/2016 15:38 WG938702
Fluoranthene ND 0.0445 1 12/29/2016 15:38 WG938702
Fluorene 0.136 0.0445 1 12/29/2016 15:38 WG938702
Hexachlorobenzene ND 0.450 1 12/29/2016 15:38 WG938702
Hexachloro-1,3-butadiene ND 0.450 1 12/29/2016 15:38 WG938702
Hexachlorocyclopentadiene ND 0.450 1 12/29/2016 15:38 WG938702
Hexachloroethane ND 0.450 1 12/29/2016 15:38 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0445 1 12/29/2016 15:38 WG938702
Isophorone ND 0.450 1 12/29/2016 15:38 WG938702
Naphthalene 0.0738 0.0445 1 12/29/2016 15:38 WG938702
Nitrobenzene ND 0.450 1 12/29/2016 15:38 WG938702
n-Nitrosodimethylamine ND 0.450 1 12/29/2016 15:38 WG938702
n-Nitrosodiphenylamine ND 0.450 1 12/29/2016 15:38 WG938702
n-Nitrosodi-n-propylamine ND 0.450 1 12/29/2016 15:38 WG938702
Phenanthrene 0.293 0.0445 1 12/29/2016 15:38 WG938702
Benzylbutyl phthalate ND 0.450 1 12/29/2016 15:38 WG938702
Bis(2-ethylhexyl)phthalate ND 0.450 1 12/29/2016 15:38 WG938702
Di-n-butyl phthalate ND 0.450 1 12/29/2016 15:38 WG938702
Diethyl phthalate ND 0.450 1 12/29/2016 15:38 WG938702
Dimethyl phthalate ND 0.450 1 12/29/2016 15:38 WG938702
Di-n-octyl phthalate ND 0.450 1 12/29/2016 15:38 WG938702
Pyrene ND 0.0445 1 12/29/2016 15:38 WG938702
1,2,4-Trichlorobenzene ND 0.450 1 12/29/2016 15:38 WG938702
4-Chloro-3-methylphenol ND 0.450 1 12/29/2016 15:38 WG938702
2-Chlorophenol ND 0.450 1 12/29/2016 15:38 WG938702
2,4-Dichlorophenol ND 0.450 1 12/29/2016 15:38 WG938702
2,4-Dimethylphenol ND 0.450 1 12/29/2016 15:38 WG938702
4,6-Dinitro-2-methylphenol ND 0.450 1 12/29/2016 15:38 WG938702
2,4-Dinitrophenol ND J3 0.450 1 12/29/2016 15:38 WG938702
2-Nitrophenol ND 0.450 1 12/29/2016 15:38 WG938702
4-Nitrophenol ND 0.450 1 12/29/2016 15:38 WG938702
Pentachlorophenol ND 0.450 1 12/29/2016 15:38 WG938702
Phenol ND 0.450 1 12/29/2016 15:38 WG938702
2,4,6-Trichlorophenol ND 0.450 1 12/29/2016 15:38 WG938702
(S) 2-Fluorophenol 61.9 21.1-116 12/29/2016 15:38 WG938702
(S) Phenol-d5 61.0 26.3-121 12/29/2016 15:38 WG938702
(S) Nitrobenzene-d5 61.5 21.9-129 12/29/2016 15:38 WG938702
(S) 2-Fluorobiphenyl 59.9 34.9-129 12/29/2016 15:38 WG938702
(S) 2,4,6-Tribromophenol 70.3 21.6-142 12/29/2016 15:38 WG938702
(S) p-Terphenyl-d14 67.2 21.5-128 12/29/2016 15:38 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L880142
SB-14
Collected date/time: 12/19/16 10:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.2 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.56 19 12/24/2016 07:13 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.5 59.0-128 12/24/2016 07:13 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0674 1 12/26/2016 05:39 WG938078
Acrylonitrile ND 0.0135 1 12/26/2016 05:39 WG938078
Benzene ND 0.00135 1 12/26/2016 05:39 WG938078
Bromobenzene ND 0.00135 1 12/26/2016 05:39 WG938078
Bromodichloromethane ND 0.00135 1 12/26/2016 05:39 WG938078
Bromoform ND 0.00135 1 12/26/2016 05:39 WG938078
Bromomethane ND 0.00674 1 12/26/2016 05:39 WG938078
n-Butylbenzene ND 0.00135 1 12/26/2016 05:39 WG938078
sec-Butylbenzene ND 0.00135 1 12/26/2016 05:39 WG938078
tert-Butylbenzene ND 0.00135 1 12/26/2016 05:39 WG938078
Carbon tetrachloride ND 0.00135 1 12/26/2016 05:39 WG938078
Chlorobenzene ND 0.00135 1 12/26/2016 05:39 WG938078
Chlorodibromomethane ND 0.00135 1 12/26/2016 05:39 WG938078
Chloroethane ND 0.00674 1 12/26/2016 05:39 WG938078
2-Chloroethyl vinyl ether ND 0.0674 1 12/26/2016 05:39 WG938078
Chloroform ND 0.00674 1 12/26/2016 05:39 WG938078
Chloromethane ND 0.00337 1 12/26/2016 05:39 WG938078
2-Chlorotoluene ND 0.00135 1 12/26/2016 05:39 WG938078
4-Chlorotoluene ND 0.00135 1 12/26/2016 05:39 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00674 1 12/26/2016 05:39 WG938078
1,2-Dibromoethane ND 0.00135 1 12/26/2016 05:39 WG938078
Dibromomethane ND 0.00135 1 12/26/2016 05:39 WG938078
1,2-Dichlorobenzene ND 0.00135 1 12/26/2016 05:39 WG938078
1,3-Dichlorobenzene ND 0.00135 1 12/26/2016 05:39 WG938078
1,4-Dichlorobenzene ND 0.00135 1 12/26/2016 05:39 WG938078
Dichlorodifluoromethane ND 0.00674 1 12/26/2016 05:39 WG938078
1,1-Dichloroethane ND 0.00135 1 12/26/2016 05:39 WG938078
1,2-Dichloroethane ND 0.00135 1 12/26/2016 05:39 WG938078
1,1-Dichloroethene ND 0.00135 1 12/26/2016 05:39 WG938078
cis-1,2-Dichloroethene ND 0.00135 1 12/26/2016 05:39 WG938078
trans-1,2-Dichloroethene ND 0.00135 1 12/26/2016 05:39 WG938078
1,2-Dichloropropane ND 0.00135 1 12/26/2016 05:39 WG938078
1,1-Dichloropropene ND 0.00135 1 12/26/2016 05:39 WG938078
1,3-Dichloropropane ND 0.00135 1 12/26/2016 05:39 WG938078
cis-1,3-Dichloropropene ND 0.00135 1 12/26/2016 05:39 WG938078
trans-1,3-Dichloropropene ND 0.00135 1 12/26/2016 05:39 WG938078
2,2-Dichloropropane ND 0.00135 1 12/26/2016 05:39 WG938078
Di-isopropyl ether ND 0.00135 1 12/26/2016 05:39 WG938078
Ethylbenzene ND 0.00135 1 12/26/2016 05:39 WG938078
Hexachloro-1,3-butadiene ND 0.00135 1 12/26/2016 05:39 WG938078
Isopropylbenzene ND 0.00135 1 12/26/2016 05:39 WG938078
p-Isopropyltoluene ND 0.00135 1 12/26/2016 05:39 WG938078
2-Butanone (MEK)ND 0.0135 1 12/26/2016 05:39 WG938078
Methylene Chloride ND 0.00674 1 12/26/2016 05:39 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L880142
SB-14
Collected date/time: 12/19/16 10:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0135 1 12/26/2016 05:39 WG938078
Methyl tert-butyl ether ND J4 0.00135 1 12/26/2016 05:39 WG938078
Naphthalene ND 0.00674 1 12/26/2016 05:39 WG938078
n-Propylbenzene ND 0.00135 1 12/26/2016 05:39 WG938078
Styrene ND 0.00135 1 12/26/2016 05:39 WG938078
1,1,1,2-Tetrachloroethane ND 0.00135 1 12/26/2016 05:39 WG938078
1,1,2,2-Tetrachloroethane ND 0.00135 1 12/26/2016 05:39 WG938078
Tetrachloroethene ND 0.00135 1 12/26/2016 05:39 WG938078
Toluene ND 0.00674 1 12/26/2016 05:39 WG938078
1,2,3-Trichlorobenzene ND 0.00135 1 12/26/2016 05:39 WG938078
1,2,4-Trichlorobenzene ND 0.00135 1 12/26/2016 05:39 WG938078
1,1,1-Trichloroethane ND 0.00135 1 12/26/2016 05:39 WG938078
1,1,2-Trichloroethane ND 0.00135 1 12/26/2016 05:39 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00135 1 12/26/2016 05:39 WG938078
Trichloroethene ND 0.00135 1 12/26/2016 05:39 WG938078
Trichlorofluoromethane ND 0.00674 1 12/26/2016 05:39 WG938078
1,2,3-Trichloropropane ND 0.00337 1 12/26/2016 05:39 WG938078
1,2,4-Trimethylbenzene ND 0.00135 1 12/26/2016 05:39 WG938078
1,3,5-Trimethylbenzene ND 0.00135 1 12/26/2016 05:39 WG938078
Vinyl chloride ND 0.00135 1 12/26/2016 05:39 WG938078
Xylenes, Total ND 0.00404 1 12/26/2016 05:39 WG938078
(S) Toluene-d8 106 88.7-115 12/26/2016 05:39 WG938078
(S) Dibromofluoromethane 110 76.3-123 12/26/2016 05:39 WG938078
(S) 4-Bromofluorobenzene 98.8 69.7-129 12/26/2016 05:39 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.39 1 12/29/2016 02:49 WG938642
(S) o-Terphenyl 52.3 50.0-150 12/29/2016 02:49 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L880142
SB-15
Collected date/time: 12/19/16 10:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.6 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.64 20.25 12/24/2016 07:35 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.8 59.0-128 12/24/2016 07:35 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0652 1 12/26/2016 06:02 WG938078
Acrylonitrile ND 0.0130 1 12/26/2016 06:02 WG938078
Benzene ND 0.00130 1 12/26/2016 06:02 WG938078
Bromobenzene ND 0.00130 1 12/26/2016 06:02 WG938078
Bromodichloromethane ND 0.00130 1 12/26/2016 06:02 WG938078
Bromoform ND 0.00130 1 12/26/2016 06:02 WG938078
Bromomethane ND 0.00652 1 12/26/2016 06:02 WG938078
n-Butylbenzene ND 0.00130 1 12/26/2016 06:02 WG938078
sec-Butylbenzene ND 0.00130 1 12/26/2016 06:02 WG938078
tert-Butylbenzene ND 0.00130 1 12/26/2016 06:02 WG938078
Carbon tetrachloride ND 0.00130 1 12/26/2016 06:02 WG938078
Chlorobenzene ND 0.00130 1 12/26/2016 06:02 WG938078
Chlorodibromomethane ND 0.00130 1 12/26/2016 06:02 WG938078
Chloroethane ND 0.00652 1 12/26/2016 06:02 WG938078
2-Chloroethyl vinyl ether ND 0.0652 1 12/26/2016 06:02 WG938078
Chloroform ND 0.00652 1 12/26/2016 06:02 WG938078
Chloromethane ND 0.00326 1 12/26/2016 06:02 WG938078
2-Chlorotoluene ND 0.00130 1 12/26/2016 06:02 WG938078
4-Chlorotoluene ND 0.00130 1 12/26/2016 06:02 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00652 1 12/26/2016 06:02 WG938078
1,2-Dibromoethane ND 0.00130 1 12/26/2016 06:02 WG938078
Dibromomethane ND 0.00130 1 12/26/2016 06:02 WG938078
1,2-Dichlorobenzene ND 0.00130 1 12/26/2016 06:02 WG938078
1,3-Dichlorobenzene ND 0.00130 1 12/26/2016 06:02 WG938078
1,4-Dichlorobenzene ND 0.00130 1 12/26/2016 06:02 WG938078
Dichlorodifluoromethane ND 0.00652 1 12/26/2016 06:02 WG938078
1,1-Dichloroethane ND 0.00130 1 12/26/2016 06:02 WG938078
1,2-Dichloroethane ND 0.00130 1 12/26/2016 06:02 WG938078
1,1-Dichloroethene ND 0.00130 1 12/26/2016 06:02 WG938078
cis-1,2-Dichloroethene ND 0.00130 1 12/26/2016 06:02 WG938078
trans-1,2-Dichloroethene ND 0.00130 1 12/26/2016 06:02 WG938078
1,2-Dichloropropane ND 0.00130 1 12/26/2016 06:02 WG938078
1,1-Dichloropropene ND 0.00130 1 12/26/2016 06:02 WG938078
1,3-Dichloropropane ND 0.00130 1 12/26/2016 06:02 WG938078
cis-1,3-Dichloropropene ND 0.00130 1 12/26/2016 06:02 WG938078
trans-1,3-Dichloropropene ND 0.00130 1 12/26/2016 06:02 WG938078
2,2-Dichloropropane ND 0.00130 1 12/26/2016 06:02 WG938078
Di-isopropyl ether ND 0.00130 1 12/26/2016 06:02 WG938078
Ethylbenzene ND 0.00130 1 12/26/2016 06:02 WG938078
Hexachloro-1,3-butadiene ND 0.00130 1 12/26/2016 06:02 WG938078
Isopropylbenzene ND 0.00130 1 12/26/2016 06:02 WG938078
p-Isopropyltoluene ND 0.00130 1 12/26/2016 06:02 WG938078
2-Butanone (MEK)ND 0.0130 1 12/26/2016 06:02 WG938078
Methylene Chloride ND 0.00652 1 12/26/2016 06:02 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L880142
SB-15
Collected date/time: 12/19/16 10:55
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0130 1 12/26/2016 06:02 WG938078
Methyl tert-butyl ether ND J4 0.00130 1 12/26/2016 06:02 WG938078
Naphthalene ND 0.00652 1 12/26/2016 06:02 WG938078
n-Propylbenzene ND 0.00130 1 12/26/2016 06:02 WG938078
Styrene ND 0.00130 1 12/26/2016 06:02 WG938078
1,1,1,2-Tetrachloroethane ND 0.00130 1 12/26/2016 06:02 WG938078
1,1,2,2-Tetrachloroethane ND 0.00130 1 12/26/2016 06:02 WG938078
Tetrachloroethene ND 0.00130 1 12/26/2016 06:02 WG938078
Toluene ND 0.00652 1 12/26/2016 06:02 WG938078
1,2,3-Trichlorobenzene ND 0.00130 1 12/26/2016 06:02 WG938078
1,2,4-Trichlorobenzene ND 0.00130 1 12/26/2016 06:02 WG938078
1,1,1-Trichloroethane ND 0.00130 1 12/26/2016 06:02 WG938078
1,1,2-Trichloroethane ND 0.00130 1 12/26/2016 06:02 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00130 1 12/26/2016 06:02 WG938078
Trichloroethene ND 0.00130 1 12/26/2016 06:02 WG938078
Trichlorofluoromethane ND 0.00652 1 12/26/2016 06:02 WG938078
1,2,3-Trichloropropane ND 0.00326 1 12/26/2016 06:02 WG938078
1,2,4-Trimethylbenzene ND 0.00130 1 12/26/2016 06:02 WG938078
1,3,5-Trimethylbenzene ND 0.00130 1 12/26/2016 06:02 WG938078
Vinyl chloride ND 0.00130 1 12/26/2016 06:02 WG938078
Xylenes, Total ND 0.00391 1 12/26/2016 06:02 WG938078
(S) Toluene-d8 106 88.7-115 12/26/2016 06:02 WG938078
(S) Dibromofluoromethane 110 76.3-123 12/26/2016 06:02 WG938078
(S) 4-Bromofluorobenzene 96.9 69.7-129 12/26/2016 06:02 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 55.3 10.4 2 12/29/2016 03:01 WG938642
(S) o-Terphenyl 68.2 50.0-150 12/29/2016 03:01 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L880142
SB-16
Collected date/time: 12/19/16 11:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.8 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 3.07 B 2.81 20.75 12/24/2016 07:57 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.7 59.0-128 12/24/2016 07:57 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0678 1 12/26/2016 06:24 WG938078
Acrylonitrile ND 0.0136 1 12/26/2016 06:24 WG938078
Benzene ND 0.00136 1 12/26/2016 06:24 WG938078
Bromobenzene ND 0.00136 1 12/26/2016 06:24 WG938078
Bromodichloromethane ND 0.00136 1 12/26/2016 06:24 WG938078
Bromoform ND 0.00136 1 12/26/2016 06:24 WG938078
Bromomethane ND 0.00678 1 12/26/2016 06:24 WG938078
n-Butylbenzene ND 0.00136 1 12/26/2016 06:24 WG938078
sec-Butylbenzene ND 0.00136 1 12/26/2016 06:24 WG938078
tert-Butylbenzene ND 0.00136 1 12/26/2016 06:24 WG938078
Carbon tetrachloride ND 0.00136 1 12/26/2016 06:24 WG938078
Chlorobenzene ND 0.00136 1 12/26/2016 06:24 WG938078
Chlorodibromomethane ND 0.00136 1 12/26/2016 06:24 WG938078
Chloroethane ND 0.00678 1 12/26/2016 06:24 WG938078
2-Chloroethyl vinyl ether ND 0.0678 1 12/26/2016 06:24 WG938078
Chloroform ND 0.00678 1 12/26/2016 06:24 WG938078
Chloromethane ND 0.00339 1 12/26/2016 06:24 WG938078
2-Chlorotoluene ND 0.00136 1 12/26/2016 06:24 WG938078
4-Chlorotoluene ND 0.00136 1 12/26/2016 06:24 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00678 1 12/26/2016 06:24 WG938078
1,2-Dibromoethane ND 0.00136 1 12/26/2016 06:24 WG938078
Dibromomethane ND 0.00136 1 12/26/2016 06:24 WG938078
1,2-Dichlorobenzene ND 0.00136 1 12/26/2016 06:24 WG938078
1,3-Dichlorobenzene ND 0.00136 1 12/26/2016 06:24 WG938078
1,4-Dichlorobenzene ND 0.00136 1 12/26/2016 06:24 WG938078
Dichlorodifluoromethane ND 0.00678 1 12/26/2016 06:24 WG938078
1,1-Dichloroethane ND 0.00136 1 12/26/2016 06:24 WG938078
1,2-Dichloroethane ND 0.00136 1 12/26/2016 06:24 WG938078
1,1-Dichloroethene ND 0.00136 1 12/26/2016 06:24 WG938078
cis-1,2-Dichloroethene ND 0.00136 1 12/26/2016 06:24 WG938078
trans-1,2-Dichloroethene ND 0.00136 1 12/26/2016 06:24 WG938078
1,2-Dichloropropane ND 0.00136 1 12/26/2016 06:24 WG938078
1,1-Dichloropropene ND 0.00136 1 12/26/2016 06:24 WG938078
1,3-Dichloropropane ND 0.00136 1 12/26/2016 06:24 WG938078
cis-1,3-Dichloropropene ND 0.00136 1 12/26/2016 06:24 WG938078
trans-1,3-Dichloropropene ND 0.00136 1 12/26/2016 06:24 WG938078
2,2-Dichloropropane ND 0.00136 1 12/26/2016 06:24 WG938078
Di-isopropyl ether ND 0.00136 1 12/26/2016 06:24 WG938078
Ethylbenzene ND 0.00136 1 12/26/2016 06:24 WG938078
Hexachloro-1,3-butadiene ND 0.00136 1 12/26/2016 06:24 WG938078
Isopropylbenzene ND 0.00136 1 12/26/2016 06:24 WG938078
p-Isopropyltoluene ND 0.00136 1 12/26/2016 06:24 WG938078
2-Butanone (MEK)ND 0.0136 1 12/26/2016 06:24 WG938078
Methylene Chloride ND 0.00678 1 12/26/2016 06:24 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L880142
SB-16
Collected date/time: 12/19/16 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0136 1 12/26/2016 06:24 WG938078
Methyl tert-butyl ether ND J4 0.00136 1 12/26/2016 06:24 WG938078
Naphthalene ND 0.00678 1 12/26/2016 06:24 WG938078
n-Propylbenzene ND 0.00136 1 12/26/2016 06:24 WG938078
Styrene ND 0.00136 1 12/26/2016 06:24 WG938078
1,1,1,2-Tetrachloroethane ND 0.00136 1 12/26/2016 06:24 WG938078
1,1,2,2-Tetrachloroethane ND 0.00136 1 12/26/2016 06:24 WG938078
Tetrachloroethene ND 0.00136 1 12/26/2016 06:24 WG938078
Toluene ND 0.00678 1 12/26/2016 06:24 WG938078
1,2,3-Trichlorobenzene ND 0.00136 1 12/26/2016 06:24 WG938078
1,2,4-Trichlorobenzene ND 0.00136 1 12/26/2016 06:24 WG938078
1,1,1-Trichloroethane ND 0.00136 1 12/26/2016 06:24 WG938078
1,1,2-Trichloroethane ND 0.00136 1 12/26/2016 06:24 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00136 1 12/26/2016 06:24 WG938078
Trichloroethene ND 0.00136 1 12/26/2016 06:24 WG938078
Trichlorofluoromethane ND 0.00678 1 12/26/2016 06:24 WG938078
1,2,3-Trichloropropane ND 0.00339 1 12/26/2016 06:24 WG938078
1,2,4-Trimethylbenzene ND 0.00136 1 12/26/2016 06:24 WG938078
1,3,5-Trimethylbenzene ND 0.00136 1 12/26/2016 06:24 WG938078
Vinyl chloride ND 0.00136 1 12/26/2016 06:24 WG938078
Xylenes, Total ND 0.00407 1 12/26/2016 06:24 WG938078
(S) Toluene-d8 106 88.7-115 12/26/2016 06:24 WG938078
(S) Dibromofluoromethane 111 76.3-123 12/26/2016 06:24 WG938078
(S) 4-Bromofluorobenzene 95.8 69.7-129 12/26/2016 06:24 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 72.4 5.42 1 12/29/2016 14:38 WG938642
(S) o-Terphenyl 73.4 50.0-150 12/29/2016 14:38 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 44 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L880142
SB-17
Collected date/time: 12/19/16 11:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.4 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.55 18.75 12/24/2016 08:19 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.9 59.0-128 12/24/2016 08:19 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0681 1 12/26/2016 06:47 WG938078
Acrylonitrile ND 0.0136 1 12/26/2016 06:47 WG938078
Benzene ND 0.00136 1 12/26/2016 06:47 WG938078
Bromobenzene ND 0.00136 1 12/26/2016 06:47 WG938078
Bromodichloromethane ND 0.00136 1 12/26/2016 06:47 WG938078
Bromoform ND 0.00136 1 12/26/2016 06:47 WG938078
Bromomethane ND 0.00681 1 12/26/2016 06:47 WG938078
n-Butylbenzene ND 0.00136 1 12/26/2016 06:47 WG938078
sec-Butylbenzene ND 0.00136 1 12/26/2016 06:47 WG938078
tert-Butylbenzene ND 0.00136 1 12/26/2016 06:47 WG938078
Carbon tetrachloride ND 0.00136 1 12/26/2016 06:47 WG938078
Chlorobenzene ND 0.00136 1 12/26/2016 06:47 WG938078
Chlorodibromomethane ND 0.00136 1 12/26/2016 06:47 WG938078
Chloroethane ND 0.00681 1 12/26/2016 06:47 WG938078
2-Chloroethyl vinyl ether ND 0.0681 1 12/26/2016 06:47 WG938078
Chloroform ND 0.00681 1 12/26/2016 06:47 WG938078
Chloromethane ND 0.00340 1 12/26/2016 06:47 WG938078
2-Chlorotoluene ND 0.00136 1 12/26/2016 06:47 WG938078
4-Chlorotoluene ND 0.00136 1 12/26/2016 06:47 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00681 1 12/26/2016 06:47 WG938078
1,2-Dibromoethane ND 0.00136 1 12/26/2016 06:47 WG938078
Dibromomethane ND 0.00136 1 12/26/2016 06:47 WG938078
1,2-Dichlorobenzene ND 0.00136 1 12/26/2016 06:47 WG938078
1,3-Dichlorobenzene ND 0.00136 1 12/26/2016 06:47 WG938078
1,4-Dichlorobenzene ND 0.00136 1 12/26/2016 06:47 WG938078
Dichlorodifluoromethane ND 0.00681 1 12/26/2016 06:47 WG938078
1,1-Dichloroethane ND 0.00136 1 12/26/2016 06:47 WG938078
1,2-Dichloroethane ND 0.00136 1 12/26/2016 06:47 WG938078
1,1-Dichloroethene ND 0.00136 1 12/26/2016 06:47 WG938078
cis-1,2-Dichloroethene ND 0.00136 1 12/26/2016 06:47 WG938078
trans-1,2-Dichloroethene ND 0.00136 1 12/26/2016 06:47 WG938078
1,2-Dichloropropane ND 0.00136 1 12/26/2016 06:47 WG938078
1,1-Dichloropropene ND 0.00136 1 12/26/2016 06:47 WG938078
1,3-Dichloropropane ND 0.00136 1 12/26/2016 06:47 WG938078
cis-1,3-Dichloropropene ND 0.00136 1 12/26/2016 06:47 WG938078
trans-1,3-Dichloropropene ND 0.00136 1 12/26/2016 06:47 WG938078
2,2-Dichloropropane ND 0.00136 1 12/26/2016 06:47 WG938078
Di-isopropyl ether ND 0.00136 1 12/26/2016 06:47 WG938078
Ethylbenzene ND 0.00136 1 12/26/2016 06:47 WG938078
Hexachloro-1,3-butadiene ND 0.00136 1 12/26/2016 06:47 WG938078
Isopropylbenzene ND 0.00136 1 12/26/2016 06:47 WG938078
p-Isopropyltoluene ND 0.00136 1 12/26/2016 06:47 WG938078
2-Butanone (MEK)ND 0.0136 1 12/26/2016 06:47 WG938078
Methylene Chloride ND 0.00681 1 12/26/2016 06:47 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L880142
SB-17
Collected date/time: 12/19/16 11:05
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0136 1 12/26/2016 06:47 WG938078
Methyl tert-butyl ether ND J4 0.00136 1 12/26/2016 06:47 WG938078
Naphthalene ND 0.00681 1 12/26/2016 06:47 WG938078
n-Propylbenzene ND 0.00136 1 12/26/2016 06:47 WG938078
Styrene ND 0.00136 1 12/26/2016 06:47 WG938078
1,1,1,2-Tetrachloroethane ND 0.00136 1 12/26/2016 06:47 WG938078
1,1,2,2-Tetrachloroethane ND 0.00136 1 12/26/2016 06:47 WG938078
Tetrachloroethene ND 0.00136 1 12/26/2016 06:47 WG938078
Toluene ND 0.00681 1 12/26/2016 06:47 WG938078
1,2,3-Trichlorobenzene ND 0.00136 1 12/26/2016 06:47 WG938078
1,2,4-Trichlorobenzene ND 0.00136 1 12/26/2016 06:47 WG938078
1,1,1-Trichloroethane ND 0.00136 1 12/26/2016 06:47 WG938078
1,1,2-Trichloroethane ND 0.00136 1 12/26/2016 06:47 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00136 1 12/26/2016 06:47 WG938078
Trichloroethene ND 0.00136 1 12/26/2016 06:47 WG938078
Trichlorofluoromethane ND 0.00681 1 12/26/2016 06:47 WG938078
1,2,3-Trichloropropane ND 0.00340 1 12/26/2016 06:47 WG938078
1,2,4-Trimethylbenzene ND 0.00136 1 12/26/2016 06:47 WG938078
1,3,5-Trimethylbenzene ND 0.00136 1 12/26/2016 06:47 WG938078
Vinyl chloride ND 0.00136 1 12/26/2016 06:47 WG938078
Xylenes, Total ND 0.00409 1 12/26/2016 06:47 WG938078
(S) Toluene-d8 106 88.7-115 12/26/2016 06:47 WG938078
(S) Dibromofluoromethane 111 76.3-123 12/26/2016 06:47 WG938078
(S) 4-Bromofluorobenzene 98.1 69.7-129 12/26/2016 06:47 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.45 1 12/29/2016 03:25 WG938642
(S) o-Terphenyl 73.4 50.0-150 12/29/2016 03:25 WG938642
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0449 1 12/29/2016 16:04 WG938702
Acenaphthylene ND 0.0449 1 12/29/2016 16:04 WG938702
Anthracene ND 0.0449 1 12/29/2016 16:04 WG938702
Benzidine ND 0.453 1 12/29/2016 16:04 WG938702
Benzo(a)anthracene ND 0.0449 1 12/29/2016 16:04 WG938702
Benzo(b)fluoranthene ND 0.0449 1 12/29/2016 16:04 WG938702
Benzo(k)fluoranthene ND 0.0449 1 12/29/2016 16:04 WG938702
Benzo(g,h,i)perylene ND 0.0449 1 12/29/2016 16:04 WG938702
Benzo(a)pyrene ND 0.0449 1 12/29/2016 16:04 WG938702
Bis(2-chlorethoxy)methane ND 0.453 1 12/29/2016 16:04 WG938702
Bis(2-chloroethyl)ether ND 0.453 1 12/29/2016 16:04 WG938702
Bis(2-chloroisopropyl)ether ND 0.453 1 12/29/2016 16:04 WG938702
4-Bromophenyl-phenylether ND 0.453 1 12/29/2016 16:04 WG938702
2-Chloronaphthalene ND 0.0449 1 12/29/2016 16:04 WG938702
4-Chlorophenyl-phenylether ND 0.453 1 12/29/2016 16:04 WG938702
Chrysene ND 0.0449 1 12/29/2016 16:04 WG938702
Dibenz(a,h)anthracene ND 0.0449 1 12/29/2016 16:04 WG938702
3,3-Dichlorobenzidine ND 0.453 1 12/29/2016 16:04 WG938702
2,4-Dinitrotoluene ND 0.453 1 12/29/2016 16:04 WG938702
2,6-Dinitrotoluene ND 0.453 1 12/29/2016 16:04 WG938702
Fluoranthene ND 0.0449 1 12/29/2016 16:04 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L880142
SB-17
Collected date/time: 12/19/16 11:05
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0449 1 12/29/2016 16:04 WG938702
Hexachlorobenzene ND 0.453 1 12/29/2016 16:04 WG938702
Hexachloro-1,3-butadiene ND 0.453 1 12/29/2016 16:04 WG938702
Hexachlorocyclopentadiene ND 0.453 1 12/29/2016 16:04 WG938702
Hexachloroethane ND 0.453 1 12/29/2016 16:04 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0449 1 12/29/2016 16:04 WG938702
Isophorone ND 0.453 1 12/29/2016 16:04 WG938702
Naphthalene ND 0.0449 1 12/29/2016 16:04 WG938702
Nitrobenzene ND 0.453 1 12/29/2016 16:04 WG938702
n-Nitrosodimethylamine ND 0.453 1 12/29/2016 16:04 WG938702
n-Nitrosodiphenylamine ND 0.453 1 12/29/2016 16:04 WG938702
n-Nitrosodi-n-propylamine ND 0.453 1 12/29/2016 16:04 WG938702
Phenanthrene ND 0.0449 1 12/29/2016 16:04 WG938702
Benzylbutyl phthalate ND 0.453 1 12/29/2016 16:04 WG938702
Bis(2-ethylhexyl)phthalate ND 0.453 1 12/29/2016 16:04 WG938702
Di-n-butyl phthalate ND 0.453 1 12/29/2016 16:04 WG938702
Diethyl phthalate ND 0.453 1 12/29/2016 16:04 WG938702
Dimethyl phthalate ND 0.453 1 12/29/2016 16:04 WG938702
Di-n-octyl phthalate ND 0.453 1 12/29/2016 16:04 WG938702
Pyrene ND 0.0449 1 12/29/2016 16:04 WG938702
1,2,4-Trichlorobenzene ND 0.453 1 12/29/2016 16:04 WG938702
4-Chloro-3-methylphenol ND 0.453 1 12/29/2016 16:04 WG938702
2-Chlorophenol ND 0.453 1 12/29/2016 16:04 WG938702
2,4-Dichlorophenol ND 0.453 1 12/29/2016 16:04 WG938702
2,4-Dimethylphenol ND 0.453 1 12/29/2016 16:04 WG938702
4,6-Dinitro-2-methylphenol ND 0.453 1 12/29/2016 16:04 WG938702
2,4-Dinitrophenol ND J3 0.453 1 12/29/2016 16:04 WG938702
2-Nitrophenol ND 0.453 1 12/29/2016 16:04 WG938702
4-Nitrophenol ND 0.453 1 12/29/2016 16:04 WG938702
Pentachlorophenol ND 0.453 1 12/29/2016 16:04 WG938702
Phenol ND 0.453 1 12/29/2016 16:04 WG938702
2,4,6-Trichlorophenol ND 0.453 1 12/29/2016 16:04 WG938702
(S) 2-Fluorophenol 56.2 21.1-116 12/29/2016 16:04 WG938702
(S) Phenol-d5 54.6 26.3-121 12/29/2016 16:04 WG938702
(S) Nitrobenzene-d5 51.1 21.9-129 12/29/2016 16:04 WG938702
(S) 2-Fluorobiphenyl 55.7 34.9-129 12/29/2016 16:04 WG938702
(S) 2,4,6-Tribromophenol 58.1 21.6-142 12/29/2016 16:04 WG938702
(S) p-Terphenyl-d14 67.3 21.5-128 12/29/2016 16:04 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L880142
SB-18
Collected date/time: 12/19/16 11:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.1 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.63 20 12/24/2016 08:41 WG938086
(S) a,a,a-Trifluorotoluene(FID) 97.1 59.0-128 12/24/2016 08:41 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0657 1 12/26/2016 07:09 WG938078
Acrylonitrile ND 0.0131 1 12/26/2016 07:09 WG938078
Benzene ND 0.00131 1 12/26/2016 07:09 WG938078
Bromobenzene ND 0.00131 1 12/26/2016 07:09 WG938078
Bromodichloromethane ND 0.00131 1 12/26/2016 07:09 WG938078
Bromoform ND 0.00131 1 12/26/2016 07:09 WG938078
Bromomethane ND 0.00657 1 12/26/2016 07:09 WG938078
n-Butylbenzene ND 0.00131 1 12/26/2016 07:09 WG938078
sec-Butylbenzene ND 0.00131 1 12/26/2016 07:09 WG938078
tert-Butylbenzene ND 0.00131 1 12/26/2016 07:09 WG938078
Carbon tetrachloride ND 0.00131 1 12/26/2016 07:09 WG938078
Chlorobenzene ND 0.00131 1 12/26/2016 07:09 WG938078
Chlorodibromomethane ND 0.00131 1 12/26/2016 07:09 WG938078
Chloroethane ND 0.00657 1 12/26/2016 07:09 WG938078
2-Chloroethyl vinyl ether ND 0.0657 1 12/26/2016 07:09 WG938078
Chloroform ND 0.00657 1 12/26/2016 07:09 WG938078
Chloromethane ND 0.00329 1 12/26/2016 07:09 WG938078
2-Chlorotoluene ND 0.00131 1 12/26/2016 07:09 WG938078
4-Chlorotoluene ND 0.00131 1 12/26/2016 07:09 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00657 1 12/26/2016 07:09 WG938078
1,2-Dibromoethane ND 0.00131 1 12/26/2016 07:09 WG938078
Dibromomethane ND 0.00131 1 12/26/2016 07:09 WG938078
1,2-Dichlorobenzene ND 0.00131 1 12/26/2016 07:09 WG938078
1,3-Dichlorobenzene ND 0.00131 1 12/26/2016 07:09 WG938078
1,4-Dichlorobenzene ND 0.00131 1 12/26/2016 07:09 WG938078
Dichlorodifluoromethane ND 0.00657 1 12/26/2016 07:09 WG938078
1,1-Dichloroethane ND 0.00131 1 12/26/2016 07:09 WG938078
1,2-Dichloroethane ND 0.00131 1 12/26/2016 07:09 WG938078
1,1-Dichloroethene ND 0.00131 1 12/26/2016 07:09 WG938078
cis-1,2-Dichloroethene ND 0.00131 1 12/26/2016 07:09 WG938078
trans-1,2-Dichloroethene ND 0.00131 1 12/26/2016 07:09 WG938078
1,2-Dichloropropane ND 0.00131 1 12/26/2016 07:09 WG938078
1,1-Dichloropropene ND 0.00131 1 12/26/2016 07:09 WG938078
1,3-Dichloropropane ND 0.00131 1 12/26/2016 07:09 WG938078
cis-1,3-Dichloropropene ND 0.00131 1 12/26/2016 07:09 WG938078
trans-1,3-Dichloropropene ND 0.00131 1 12/26/2016 07:09 WG938078
2,2-Dichloropropane ND 0.00131 1 12/26/2016 07:09 WG938078
Di-isopropyl ether ND 0.00131 1 12/26/2016 07:09 WG938078
Ethylbenzene ND 0.00131 1 12/26/2016 07:09 WG938078
Hexachloro-1,3-butadiene ND 0.00131 1 12/26/2016 07:09 WG938078
Isopropylbenzene ND 0.00131 1 12/26/2016 07:09 WG938078
p-Isopropyltoluene ND 0.00131 1 12/26/2016 07:09 WG938078
2-Butanone (MEK)ND 0.0131 1 12/26/2016 07:09 WG938078
Methylene Chloride ND 0.00657 1 12/26/2016 07:09 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L880142
SB-18
Collected date/time: 12/19/16 11:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0131 1 12/26/2016 07:09 WG938078
Methyl tert-butyl ether ND J4 0.00131 1 12/26/2016 07:09 WG938078
Naphthalene ND 0.00657 1 12/26/2016 07:09 WG938078
n-Propylbenzene ND 0.00131 1 12/26/2016 07:09 WG938078
Styrene ND 0.00131 1 12/26/2016 07:09 WG938078
1,1,1,2-Tetrachloroethane ND 0.00131 1 12/26/2016 07:09 WG938078
1,1,2,2-Tetrachloroethane ND 0.00131 1 12/26/2016 07:09 WG938078
Tetrachloroethene ND 0.00131 1 12/26/2016 07:09 WG938078
Toluene ND 0.00657 1 12/26/2016 07:09 WG938078
1,2,3-Trichlorobenzene ND 0.00131 1 12/26/2016 07:09 WG938078
1,2,4-Trichlorobenzene ND 0.00131 1 12/26/2016 07:09 WG938078
1,1,1-Trichloroethane ND 0.00131 1 12/26/2016 07:09 WG938078
1,1,2-Trichloroethane ND 0.00131 1 12/26/2016 07:09 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00131 1 12/26/2016 07:09 WG938078
Trichloroethene ND 0.00131 1 12/26/2016 07:09 WG938078
Trichlorofluoromethane ND 0.00657 1 12/26/2016 07:09 WG938078
1,2,3-Trichloropropane ND 0.00329 1 12/26/2016 07:09 WG938078
1,2,4-Trimethylbenzene ND 0.00131 1 12/26/2016 07:09 WG938078
1,3,5-Trimethylbenzene ND 0.00131 1 12/26/2016 07:09 WG938078
Vinyl chloride ND 0.00131 1 12/26/2016 07:09 WG938078
Xylenes, Total ND 0.00394 1 12/26/2016 07:09 WG938078
(S) Toluene-d8 102 88.7-115 12/26/2016 07:09 WG938078
(S) Dibromofluoromethane 121 76.3-123 12/26/2016 07:09 WG938078
(S) 4-Bromofluorobenzene 98.1 69.7-129 12/26/2016 07:09 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.26 1 12/29/2016 03:37 WG938642
(S) o-Terphenyl 75.7 50.0-150 12/29/2016 03:37 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L880142
SB-19
Collected date/time: 12/19/16 11:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.8 1 12/22/2016 11:14 WG937881
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.71 20 12/24/2016 09:03 WG938086
(S) a,a,a-Trifluorotoluene(FID) 96.5 59.0-128 12/24/2016 09:03 WG938086
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0678 1 12/26/2016 07:32 WG938078
Acrylonitrile ND 0.0136 1 12/26/2016 07:32 WG938078
Benzene ND 0.00136 1 12/26/2016 07:32 WG938078
Bromobenzene ND 0.00136 1 12/26/2016 07:32 WG938078
Bromodichloromethane ND 0.00136 1 12/26/2016 07:32 WG938078
Bromoform ND 0.00136 1 12/26/2016 07:32 WG938078
Bromomethane ND 0.00678 1 12/26/2016 07:32 WG938078
n-Butylbenzene ND 0.00136 1 12/26/2016 07:32 WG938078
sec-Butylbenzene ND 0.00136 1 12/26/2016 07:32 WG938078
tert-Butylbenzene ND 0.00136 1 12/26/2016 07:32 WG938078
Carbon tetrachloride ND 0.00136 1 12/26/2016 07:32 WG938078
Chlorobenzene ND 0.00136 1 12/26/2016 07:32 WG938078
Chlorodibromomethane ND 0.00136 1 12/26/2016 07:32 WG938078
Chloroethane ND 0.00678 1 12/26/2016 07:32 WG938078
2-Chloroethyl vinyl ether ND 0.0678 1 12/26/2016 07:32 WG938078
Chloroform ND 0.00678 1 12/26/2016 07:32 WG938078
Chloromethane ND 0.00339 1 12/26/2016 07:32 WG938078
2-Chlorotoluene ND 0.00136 1 12/26/2016 07:32 WG938078
4-Chlorotoluene ND 0.00136 1 12/26/2016 07:32 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00678 1 12/26/2016 07:32 WG938078
1,2-Dibromoethane ND 0.00136 1 12/26/2016 07:32 WG938078
Dibromomethane ND 0.00136 1 12/26/2016 07:32 WG938078
1,2-Dichlorobenzene ND 0.00136 1 12/26/2016 07:32 WG938078
1,3-Dichlorobenzene ND 0.00136 1 12/26/2016 07:32 WG938078
1,4-Dichlorobenzene ND 0.00136 1 12/26/2016 07:32 WG938078
Dichlorodifluoromethane ND 0.00678 1 12/26/2016 07:32 WG938078
1,1-Dichloroethane ND 0.00136 1 12/26/2016 07:32 WG938078
1,2-Dichloroethane ND 0.00136 1 12/26/2016 07:32 WG938078
1,1-Dichloroethene ND 0.00136 1 12/26/2016 07:32 WG938078
cis-1,2-Dichloroethene ND 0.00136 1 12/26/2016 07:32 WG938078
trans-1,2-Dichloroethene ND 0.00136 1 12/26/2016 07:32 WG938078
1,2-Dichloropropane ND 0.00136 1 12/26/2016 07:32 WG938078
1,1-Dichloropropene ND 0.00136 1 12/26/2016 07:32 WG938078
1,3-Dichloropropane ND 0.00136 1 12/26/2016 07:32 WG938078
cis-1,3-Dichloropropene ND 0.00136 1 12/26/2016 07:32 WG938078
trans-1,3-Dichloropropene ND 0.00136 1 12/26/2016 07:32 WG938078
2,2-Dichloropropane ND 0.00136 1 12/26/2016 07:32 WG938078
Di-isopropyl ether ND 0.00136 1 12/26/2016 07:32 WG938078
Ethylbenzene ND 0.00136 1 12/26/2016 07:32 WG938078
Hexachloro-1,3-butadiene ND 0.00136 1 12/26/2016 07:32 WG938078
Isopropylbenzene ND 0.00136 1 12/26/2016 07:32 WG938078
p-Isopropyltoluene ND 0.00136 1 12/26/2016 07:32 WG938078
2-Butanone (MEK)ND 0.0136 1 12/26/2016 07:32 WG938078
Methylene Chloride ND 0.00678 1 12/26/2016 07:32 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L880142
SB-19
Collected date/time: 12/19/16 11:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0136 1 12/26/2016 07:32 WG938078
Methyl tert-butyl ether ND J4 0.00136 1 12/26/2016 07:32 WG938078
Naphthalene ND 0.00678 1 12/26/2016 07:32 WG938078
n-Propylbenzene ND 0.00136 1 12/26/2016 07:32 WG938078
Styrene ND 0.00136 1 12/26/2016 07:32 WG938078
1,1,1,2-Tetrachloroethane ND 0.00136 1 12/26/2016 07:32 WG938078
1,1,2,2-Tetrachloroethane ND 0.00136 1 12/26/2016 07:32 WG938078
Tetrachloroethene ND 0.00136 1 12/26/2016 07:32 WG938078
Toluene ND 0.00678 1 12/26/2016 07:32 WG938078
1,2,3-Trichlorobenzene ND 0.00136 1 12/26/2016 07:32 WG938078
1,2,4-Trichlorobenzene ND 0.00136 1 12/26/2016 07:32 WG938078
1,1,1-Trichloroethane ND 0.00136 1 12/26/2016 07:32 WG938078
1,1,2-Trichloroethane ND 0.00136 1 12/26/2016 07:32 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00136 1 12/26/2016 07:32 WG938078
Trichloroethene ND 0.00136 1 12/26/2016 07:32 WG938078
Trichlorofluoromethane ND 0.00678 1 12/26/2016 07:32 WG938078
1,2,3-Trichloropropane ND 0.00339 1 12/26/2016 07:32 WG938078
1,2,4-Trimethylbenzene ND 0.00136 1 12/26/2016 07:32 WG938078
1,3,5-Trimethylbenzene ND 0.00136 1 12/26/2016 07:32 WG938078
Vinyl chloride ND 0.00136 1 12/26/2016 07:32 WG938078
Xylenes, Total ND 0.00407 1 12/26/2016 07:32 WG938078
(S) Toluene-d8 104 88.7-115 12/26/2016 07:32 WG938078
(S) Dibromofluoromethane 111 76.3-123 12/26/2016 07:32 WG938078
(S) 4-Bromofluorobenzene 97.9 69.7-129 12/26/2016 07:32 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.42 1 12/29/2016 03:49 WG938642
(S) o-Terphenyl 66.2 50.0-150 12/29/2016 03:49 WG938642
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0447 1 12/29/2016 17:48 WG938702
Acenaphthylene ND 0.0447 1 12/29/2016 17:48 WG938702
Anthracene ND 0.0447 1 12/29/2016 17:48 WG938702
Benzidine ND 0.451 1 12/29/2016 17:48 WG938702
Benzo(a)anthracene ND 0.0447 1 12/29/2016 17:48 WG938702
Benzo(b)fluoranthene ND 0.0447 1 12/29/2016 17:48 WG938702
Benzo(k)fluoranthene ND 0.0447 1 12/29/2016 17:48 WG938702
Benzo(g,h,i)perylene ND 0.0447 1 12/29/2016 17:48 WG938702
Benzo(a)pyrene ND 0.0447 1 12/29/2016 17:48 WG938702
Bis(2-chlorethoxy)methane ND 0.451 1 12/29/2016 17:48 WG938702
Bis(2-chloroethyl)ether ND 0.451 1 12/29/2016 17:48 WG938702
Bis(2-chloroisopropyl)ether ND 0.451 1 12/29/2016 17:48 WG938702
4-Bromophenyl-phenylether ND 0.451 1 12/29/2016 17:48 WG938702
2-Chloronaphthalene ND 0.0447 1 12/29/2016 17:48 WG938702
4-Chlorophenyl-phenylether ND 0.451 1 12/29/2016 17:48 WG938702
Chrysene ND 0.0447 1 12/29/2016 17:48 WG938702
Dibenz(a,h)anthracene ND 0.0447 1 12/29/2016 17:48 WG938702
3,3-Dichlorobenzidine ND 0.451 1 12/29/2016 17:48 WG938702
2,4-Dinitrotoluene ND 0.451 1 12/29/2016 17:48 WG938702
2,6-Dinitrotoluene ND 0.451 1 12/29/2016 17:48 WG938702
Fluoranthene ND 0.0447 1 12/29/2016 17:48 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L880142
SB-19
Collected date/time: 12/19/16 11:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0447 1 12/29/2016 17:48 WG938702
Hexachlorobenzene ND 0.451 1 12/29/2016 17:48 WG938702
Hexachloro-1,3-butadiene ND 0.451 1 12/29/2016 17:48 WG938702
Hexachlorocyclopentadiene ND 0.451 1 12/29/2016 17:48 WG938702
Hexachloroethane ND 0.451 1 12/29/2016 17:48 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0447 1 12/29/2016 17:48 WG938702
Isophorone ND 0.451 1 12/29/2016 17:48 WG938702
Naphthalene ND 0.0447 1 12/29/2016 17:48 WG938702
Nitrobenzene ND 0.451 1 12/29/2016 17:48 WG938702
n-Nitrosodimethylamine ND 0.451 1 12/29/2016 17:48 WG938702
n-Nitrosodiphenylamine ND 0.451 1 12/29/2016 17:48 WG938702
n-Nitrosodi-n-propylamine ND 0.451 1 12/29/2016 17:48 WG938702
Phenanthrene ND 0.0447 1 12/29/2016 17:48 WG938702
Benzylbutyl phthalate ND 0.451 1 12/29/2016 17:48 WG938702
Bis(2-ethylhexyl)phthalate ND 0.451 1 12/29/2016 17:48 WG938702
Di-n-butyl phthalate ND 0.451 1 12/29/2016 17:48 WG938702
Diethyl phthalate ND 0.451 1 12/29/2016 17:48 WG938702
Dimethyl phthalate ND 0.451 1 12/29/2016 17:48 WG938702
Di-n-octyl phthalate ND 0.451 1 12/29/2016 17:48 WG938702
Pyrene ND 0.0447 1 12/29/2016 17:48 WG938702
1,2,4-Trichlorobenzene ND 0.451 1 12/29/2016 17:48 WG938702
4-Chloro-3-methylphenol ND 0.451 1 12/29/2016 17:48 WG938702
2-Chlorophenol ND 0.451 1 12/29/2016 17:48 WG938702
2,4-Dichlorophenol ND 0.451 1 12/29/2016 17:48 WG938702
2,4-Dimethylphenol ND 0.451 1 12/29/2016 17:48 WG938702
4,6-Dinitro-2-methylphenol ND 0.451 1 12/29/2016 17:48 WG938702
2,4-Dinitrophenol ND J3 0.451 1 12/29/2016 17:48 WG938702
2-Nitrophenol ND 0.451 1 12/29/2016 17:48 WG938702
4-Nitrophenol ND 0.451 1 12/29/2016 17:48 WG938702
Pentachlorophenol ND 0.451 1 12/29/2016 17:48 WG938702
Phenol ND 0.451 1 12/29/2016 17:48 WG938702
2,4,6-Trichlorophenol ND 0.451 1 12/29/2016 17:48 WG938702
(S) 2-Fluorophenol 56.0 21.1-116 12/29/2016 17:48 WG938702
(S) Phenol-d5 54.2 26.3-121 12/29/2016 17:48 WG938702
(S) Nitrobenzene-d5 53.9 21.9-129 12/29/2016 17:48 WG938702
(S) 2-Fluorobiphenyl 57.8 34.9-129 12/29/2016 17:48 WG938702
(S) 2,4,6-Tribromophenol 57.0 21.6-142 12/29/2016 17:48 WG938702
(S) p-Terphenyl-d14 61.9 21.5-128 12/29/2016 17:48 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L880142
SB-20
Collected date/time: 12/19/16 11:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.2 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.28 18.5 12/28/2016 14:36 WG938087
(S) a,a,a-Trifluorotoluene(FID) 99.1 59.0-128 12/28/2016 14:36 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.126 0.0616 1 12/26/2016 07:55 WG938078
Acrylonitrile ND 0.0123 1 12/26/2016 07:55 WG938078
Benzene ND 0.00123 1 12/26/2016 07:55 WG938078
Bromobenzene ND 0.00123 1 12/26/2016 07:55 WG938078
Bromodichloromethane ND 0.00123 1 12/26/2016 07:55 WG938078
Bromoform ND 0.00123 1 12/26/2016 07:55 WG938078
Bromomethane ND 0.00616 1 12/26/2016 07:55 WG938078
n-Butylbenzene ND 0.00123 1 12/26/2016 07:55 WG938078
sec-Butylbenzene ND 0.00123 1 12/26/2016 07:55 WG938078
tert-Butylbenzene ND 0.00123 1 12/26/2016 07:55 WG938078
Carbon tetrachloride ND 0.00123 1 12/26/2016 07:55 WG938078
Chlorobenzene ND 0.00123 1 12/26/2016 07:55 WG938078
Chlorodibromomethane ND 0.00123 1 12/26/2016 07:55 WG938078
Chloroethane ND 0.00616 1 12/26/2016 07:55 WG938078
2-Chloroethyl vinyl ether ND 0.0616 1 12/26/2016 07:55 WG938078
Chloroform ND 0.00616 1 12/26/2016 07:55 WG938078
Chloromethane ND 0.00308 1 12/26/2016 07:55 WG938078
2-Chlorotoluene ND 0.00123 1 12/26/2016 07:55 WG938078
4-Chlorotoluene ND 0.00123 1 12/26/2016 07:55 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00616 1 12/26/2016 07:55 WG938078
1,2-Dibromoethane ND 0.00123 1 12/26/2016 07:55 WG938078
Dibromomethane ND 0.00123 1 12/26/2016 07:55 WG938078
1,2-Dichlorobenzene ND 0.00123 1 12/26/2016 07:55 WG938078
1,3-Dichlorobenzene ND 0.00123 1 12/26/2016 07:55 WG938078
1,4-Dichlorobenzene ND 0.00123 1 12/26/2016 07:55 WG938078
Dichlorodifluoromethane ND 0.00616 1 12/26/2016 07:55 WG938078
1,1-Dichloroethane ND 0.00123 1 12/26/2016 07:55 WG938078
1,2-Dichloroethane ND 0.00123 1 12/26/2016 07:55 WG938078
1,1-Dichloroethene ND 0.00123 1 12/26/2016 07:55 WG938078
cis-1,2-Dichloroethene ND 0.00123 1 12/26/2016 07:55 WG938078
trans-1,2-Dichloroethene ND 0.00123 1 12/26/2016 07:55 WG938078
1,2-Dichloropropane ND 0.00123 1 12/26/2016 07:55 WG938078
1,1-Dichloropropene ND 0.00123 1 12/26/2016 07:55 WG938078
1,3-Dichloropropane ND 0.00123 1 12/26/2016 07:55 WG938078
cis-1,3-Dichloropropene ND 0.00123 1 12/26/2016 07:55 WG938078
trans-1,3-Dichloropropene ND 0.00123 1 12/26/2016 07:55 WG938078
2,2-Dichloropropane ND 0.00123 1 12/26/2016 07:55 WG938078
Di-isopropyl ether ND 0.00123 1 12/26/2016 07:55 WG938078
Ethylbenzene ND 0.00123 1 12/26/2016 07:55 WG938078
Hexachloro-1,3-butadiene ND 0.00123 1 12/26/2016 07:55 WG938078
Isopropylbenzene ND 0.00123 1 12/26/2016 07:55 WG938078
p-Isopropyltoluene ND 0.00123 1 12/26/2016 07:55 WG938078
2-Butanone (MEK)ND 0.0123 1 12/26/2016 07:55 WG938078
Methylene Chloride ND 0.00616 1 12/26/2016 07:55 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L880142
SB-20
Collected date/time: 12/19/16 11:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0123 1 12/26/2016 07:55 WG938078
Methyl tert-butyl ether ND J4 0.00123 1 12/26/2016 07:55 WG938078
Naphthalene ND 0.00616 1 12/26/2016 07:55 WG938078
n-Propylbenzene ND 0.00123 1 12/26/2016 07:55 WG938078
Styrene ND 0.00123 1 12/26/2016 07:55 WG938078
1,1,1,2-Tetrachloroethane ND 0.00123 1 12/26/2016 07:55 WG938078
1,1,2,2-Tetrachloroethane ND 0.00123 1 12/26/2016 07:55 WG938078
Tetrachloroethene ND 0.00123 1 12/26/2016 07:55 WG938078
Toluene ND 0.00616 1 12/26/2016 07:55 WG938078
1,2,3-Trichlorobenzene ND 0.00123 1 12/26/2016 07:55 WG938078
1,2,4-Trichlorobenzene ND 0.00123 1 12/26/2016 07:55 WG938078
1,1,1-Trichloroethane ND 0.00123 1 12/26/2016 07:55 WG938078
1,1,2-Trichloroethane ND 0.00123 1 12/26/2016 07:55 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00123 1 12/26/2016 07:55 WG938078
Trichloroethene ND 0.00123 1 12/26/2016 07:55 WG938078
Trichlorofluoromethane ND 0.00616 1 12/26/2016 07:55 WG938078
1,2,3-Trichloropropane ND 0.00308 1 12/26/2016 07:55 WG938078
1,2,4-Trimethylbenzene ND 0.00123 1 12/26/2016 07:55 WG938078
1,3,5-Trimethylbenzene ND 0.00123 1 12/26/2016 07:55 WG938078
Vinyl chloride ND 0.00123 1 12/26/2016 07:55 WG938078
Xylenes, Total ND 0.00370 1 12/26/2016 07:55 WG938078
(S) Toluene-d8 106 88.7-115 12/26/2016 07:55 WG938078
(S) Dibromofluoromethane 110 76.3-123 12/26/2016 07:55 WG938078
(S) 4-Bromofluorobenzene 97.0 69.7-129 12/26/2016 07:55 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 5.09 4.93 1 12/29/2016 04:01 WG938642
(S) o-Terphenyl 55.8 50.0-150 12/29/2016 04:01 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 54 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L880142
SB-21
Collected date/time: 12/19/16 11:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.1 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.60 19.25 12/28/2016 15:05 WG938087
(S) a,a,a-Trifluorotoluene(FID) 99.1 59.0-128 12/28/2016 15:05 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0675 1 12/26/2016 08:17 WG938078
Acrylonitrile ND 0.0135 1 12/26/2016 08:17 WG938078
Benzene ND 0.00135 1 12/26/2016 08:17 WG938078
Bromobenzene ND 0.00135 1 12/26/2016 08:17 WG938078
Bromodichloromethane ND 0.00135 1 12/26/2016 08:17 WG938078
Bromoform ND 0.00135 1 12/26/2016 08:17 WG938078
Bromomethane ND 0.00675 1 12/26/2016 08:17 WG938078
n-Butylbenzene ND 0.00135 1 12/26/2016 08:17 WG938078
sec-Butylbenzene ND 0.00135 1 12/26/2016 08:17 WG938078
tert-Butylbenzene ND 0.00135 1 12/26/2016 08:17 WG938078
Carbon tetrachloride ND 0.00135 1 12/26/2016 08:17 WG938078
Chlorobenzene ND 0.00135 1 12/26/2016 08:17 WG938078
Chlorodibromomethane ND 0.00135 1 12/26/2016 08:17 WG938078
Chloroethane ND 0.00675 1 12/26/2016 08:17 WG938078
2-Chloroethyl vinyl ether ND 0.0675 1 12/26/2016 08:17 WG938078
Chloroform ND 0.00675 1 12/26/2016 08:17 WG938078
Chloromethane ND 0.00337 1 12/26/2016 08:17 WG938078
2-Chlorotoluene ND 0.00135 1 12/26/2016 08:17 WG938078
4-Chlorotoluene ND 0.00135 1 12/26/2016 08:17 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00675 1 12/26/2016 08:17 WG938078
1,2-Dibromoethane ND 0.00135 1 12/26/2016 08:17 WG938078
Dibromomethane ND 0.00135 1 12/26/2016 08:17 WG938078
1,2-Dichlorobenzene ND 0.00135 1 12/26/2016 08:17 WG938078
1,3-Dichlorobenzene ND 0.00135 1 12/26/2016 08:17 WG938078
1,4-Dichlorobenzene ND 0.00135 1 12/26/2016 08:17 WG938078
Dichlorodifluoromethane ND 0.00675 1 12/26/2016 08:17 WG938078
1,1-Dichloroethane ND 0.00135 1 12/26/2016 08:17 WG938078
1,2-Dichloroethane ND 0.00135 1 12/26/2016 08:17 WG938078
1,1-Dichloroethene ND 0.00135 1 12/26/2016 08:17 WG938078
cis-1,2-Dichloroethene ND 0.00135 1 12/26/2016 08:17 WG938078
trans-1,2-Dichloroethene ND 0.00135 1 12/26/2016 08:17 WG938078
1,2-Dichloropropane ND 0.00135 1 12/26/2016 08:17 WG938078
1,1-Dichloropropene ND 0.00135 1 12/26/2016 08:17 WG938078
1,3-Dichloropropane ND 0.00135 1 12/26/2016 08:17 WG938078
cis-1,3-Dichloropropene ND 0.00135 1 12/26/2016 08:17 WG938078
trans-1,3-Dichloropropene ND 0.00135 1 12/26/2016 08:17 WG938078
2,2-Dichloropropane ND 0.00135 1 12/26/2016 08:17 WG938078
Di-isopropyl ether ND 0.00135 1 12/26/2016 08:17 WG938078
Ethylbenzene ND 0.00135 1 12/26/2016 08:17 WG938078
Hexachloro-1,3-butadiene ND 0.00135 1 12/26/2016 08:17 WG938078
Isopropylbenzene ND 0.00135 1 12/26/2016 08:17 WG938078
p-Isopropyltoluene ND 0.00135 1 12/26/2016 08:17 WG938078
2-Butanone (MEK)ND 0.0135 1 12/26/2016 08:17 WG938078
Methylene Chloride ND 0.00675 1 12/26/2016 08:17 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L880142
SB-21
Collected date/time: 12/19/16 11:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0135 1 12/26/2016 08:17 WG938078
Methyl tert-butyl ether ND J4 0.00135 1 12/26/2016 08:17 WG938078
Naphthalene ND 0.00675 1 12/26/2016 08:17 WG938078
n-Propylbenzene ND 0.00135 1 12/26/2016 08:17 WG938078
Styrene ND 0.00135 1 12/26/2016 08:17 WG938078
1,1,1,2-Tetrachloroethane ND 0.00135 1 12/26/2016 08:17 WG938078
1,1,2,2-Tetrachloroethane ND 0.00135 1 12/26/2016 08:17 WG938078
Tetrachloroethene ND 0.00135 1 12/26/2016 08:17 WG938078
Toluene ND 0.00675 1 12/26/2016 08:17 WG938078
1,2,3-Trichlorobenzene ND 0.00135 1 12/26/2016 08:17 WG938078
1,2,4-Trichlorobenzene ND 0.00135 1 12/26/2016 08:17 WG938078
1,1,1-Trichloroethane ND 0.00135 1 12/26/2016 08:17 WG938078
1,1,2-Trichloroethane ND 0.00135 1 12/26/2016 08:17 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00135 1 12/26/2016 08:17 WG938078
Trichloroethene ND 0.00135 1 12/26/2016 08:17 WG938078
Trichlorofluoromethane ND 0.00675 1 12/26/2016 08:17 WG938078
1,2,3-Trichloropropane ND 0.00337 1 12/26/2016 08:17 WG938078
1,2,4-Trimethylbenzene ND 0.00135 1 12/26/2016 08:17 WG938078
1,3,5-Trimethylbenzene ND 0.00135 1 12/26/2016 08:17 WG938078
Vinyl chloride ND 0.00135 1 12/26/2016 08:17 WG938078
Xylenes, Total ND 0.00405 1 12/26/2016 08:17 WG938078
(S) Toluene-d8 107 88.7-115 12/26/2016 08:17 WG938078
(S) Dibromofluoromethane 122 76.3-123 12/26/2016 08:17 WG938078
(S) 4-Bromofluorobenzene 98.4 69.7-129 12/26/2016 08:17 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.40 1 12/29/2016 04:14 WG938642
(S) o-Terphenyl 68.8 50.0-150 12/29/2016 04:14 WG938642
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 56 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21
L880142
SB-22
Collected date/time: 12/19/16 11:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 64.2 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 3.23 20.75 12/28/2016 15:34 WG938087
(S) a,a,a-Trifluorotoluene(FID) 99.4 59.0-128 12/28/2016 15:34 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0779 1 12/26/2016 08:40 WG938078
Acrylonitrile ND 0.0156 1 12/26/2016 08:40 WG938078
Benzene ND 0.00156 1 12/26/2016 08:40 WG938078
Bromobenzene ND 0.00156 1 12/26/2016 08:40 WG938078
Bromodichloromethane ND 0.00156 1 12/26/2016 08:40 WG938078
Bromoform ND 0.00156 1 12/26/2016 08:40 WG938078
Bromomethane ND 0.00779 1 12/26/2016 08:40 WG938078
n-Butylbenzene ND 0.00156 1 12/26/2016 08:40 WG938078
sec-Butylbenzene ND 0.00156 1 12/26/2016 08:40 WG938078
tert-Butylbenzene ND 0.00156 1 12/26/2016 08:40 WG938078
Carbon tetrachloride ND 0.00156 1 12/26/2016 08:40 WG938078
Chlorobenzene ND 0.00156 1 12/26/2016 08:40 WG938078
Chlorodibromomethane ND 0.00156 1 12/26/2016 08:40 WG938078
Chloroethane ND 0.00779 1 12/26/2016 08:40 WG938078
2-Chloroethyl vinyl ether ND 0.0779 1 12/26/2016 08:40 WG938078
Chloroform ND 0.00779 1 12/26/2016 08:40 WG938078
Chloromethane ND 0.00390 1 12/26/2016 08:40 WG938078
2-Chlorotoluene ND 0.00156 1 12/26/2016 08:40 WG938078
4-Chlorotoluene ND 0.00156 1 12/26/2016 08:40 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00779 1 12/26/2016 08:40 WG938078
1,2-Dibromoethane ND 0.00156 1 12/26/2016 08:40 WG938078
Dibromomethane ND 0.00156 1 12/26/2016 08:40 WG938078
1,2-Dichlorobenzene ND 0.00156 1 12/26/2016 08:40 WG938078
1,3-Dichlorobenzene ND 0.00156 1 12/26/2016 08:40 WG938078
1,4-Dichlorobenzene ND 0.00156 1 12/26/2016 08:40 WG938078
Dichlorodifluoromethane ND 0.00779 1 12/26/2016 08:40 WG938078
1,1-Dichloroethane ND 0.00156 1 12/26/2016 08:40 WG938078
1,2-Dichloroethane ND 0.00156 1 12/26/2016 08:40 WG938078
1,1-Dichloroethene ND 0.00156 1 12/26/2016 08:40 WG938078
cis-1,2-Dichloroethene ND 0.00156 1 12/26/2016 08:40 WG938078
trans-1,2-Dichloroethene ND 0.00156 1 12/26/2016 08:40 WG938078
1,2-Dichloropropane ND 0.00156 1 12/26/2016 08:40 WG938078
1,1-Dichloropropene ND 0.00156 1 12/26/2016 08:40 WG938078
1,3-Dichloropropane ND 0.00156 1 12/26/2016 08:40 WG938078
cis-1,3-Dichloropropene ND 0.00156 1 12/26/2016 08:40 WG938078
trans-1,3-Dichloropropene ND 0.00156 1 12/26/2016 08:40 WG938078
2,2-Dichloropropane ND 0.00156 1 12/26/2016 08:40 WG938078
Di-isopropyl ether ND 0.00156 1 12/26/2016 08:40 WG938078
Ethylbenzene ND 0.00156 1 12/26/2016 08:40 WG938078
Hexachloro-1,3-butadiene ND 0.00156 1 12/26/2016 08:40 WG938078
Isopropylbenzene ND 0.00156 1 12/26/2016 08:40 WG938078
p-Isopropyltoluene ND 0.00156 1 12/26/2016 08:40 WG938078
2-Butanone (MEK)ND 0.0156 1 12/26/2016 08:40 WG938078
Methylene Chloride ND 0.00779 1 12/26/2016 08:40 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21
L880142
SB-22
Collected date/time: 12/19/16 11:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0156 1 12/26/2016 08:40 WG938078
Methyl tert-butyl ether ND J4 0.00156 1 12/26/2016 08:40 WG938078
Naphthalene ND 0.00779 1 12/26/2016 08:40 WG938078
n-Propylbenzene ND 0.00156 1 12/26/2016 08:40 WG938078
Styrene ND 0.00156 1 12/26/2016 08:40 WG938078
1,1,1,2-Tetrachloroethane ND 0.00156 1 12/26/2016 08:40 WG938078
1,1,2,2-Tetrachloroethane ND 0.00156 1 12/26/2016 08:40 WG938078
Tetrachloroethene ND 0.00156 1 12/26/2016 08:40 WG938078
Toluene ND 0.00779 1 12/26/2016 08:40 WG938078
1,2,3-Trichlorobenzene ND 0.00156 1 12/26/2016 08:40 WG938078
1,2,4-Trichlorobenzene ND 0.00156 1 12/26/2016 08:40 WG938078
1,1,1-Trichloroethane ND 0.00156 1 12/26/2016 08:40 WG938078
1,1,2-Trichloroethane ND 0.00156 1 12/26/2016 08:40 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00156 1 12/26/2016 08:40 WG938078
Trichloroethene ND 0.00156 1 12/26/2016 08:40 WG938078
Trichlorofluoromethane ND 0.00779 1 12/26/2016 08:40 WG938078
1,2,3-Trichloropropane ND 0.00390 1 12/26/2016 08:40 WG938078
1,2,4-Trimethylbenzene ND 0.00156 1 12/26/2016 08:40 WG938078
1,3,5-Trimethylbenzene ND 0.00156 1 12/26/2016 08:40 WG938078
Vinyl chloride ND 0.00156 1 12/26/2016 08:40 WG938078
Xylenes, Total ND 0.00468 1 12/26/2016 08:40 WG938078
(S) Toluene-d8 105 88.7-115 12/26/2016 08:40 WG938078
(S) Dibromofluoromethane 111 76.3-123 12/26/2016 08:40 WG938078
(S) 4-Bromofluorobenzene 99.5 69.7-129 12/26/2016 08:40 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 6.23 1 12/23/2016 16:16 WG937731
(S) o-Terphenyl 63.4 50.0-150 12/23/2016 16:16 WG937731
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0514 1 12/29/2016 18:14 WG938702
Acenaphthylene ND 0.0514 1 12/29/2016 18:14 WG938702
Anthracene ND 0.0514 1 12/29/2016 18:14 WG938702
Benzidine ND 0.519 1 12/29/2016 18:14 WG938702
Benzo(a)anthracene ND 0.0514 1 12/29/2016 18:14 WG938702
Benzo(b)fluoranthene ND 0.0514 1 12/29/2016 18:14 WG938702
Benzo(k)fluoranthene ND 0.0514 1 12/29/2016 18:14 WG938702
Benzo(g,h,i)perylene ND 0.0514 1 12/29/2016 18:14 WG938702
Benzo(a)pyrene ND 0.0514 1 12/29/2016 18:14 WG938702
Bis(2-chlorethoxy)methane ND 0.519 1 12/29/2016 18:14 WG938702
Bis(2-chloroethyl)ether ND 0.519 1 12/29/2016 18:14 WG938702
Bis(2-chloroisopropyl)ether ND 0.519 1 12/29/2016 18:14 WG938702
4-Bromophenyl-phenylether ND 0.519 1 12/29/2016 18:14 WG938702
2-Chloronaphthalene ND 0.0514 1 12/29/2016 18:14 WG938702
4-Chlorophenyl-phenylether ND 0.519 1 12/29/2016 18:14 WG938702
Chrysene ND 0.0514 1 12/29/2016 18:14 WG938702
Dibenz(a,h)anthracene ND 0.0514 1 12/29/2016 18:14 WG938702
3,3-Dichlorobenzidine ND 0.519 1 12/29/2016 18:14 WG938702
2,4-Dinitrotoluene ND 0.519 1 12/29/2016 18:14 WG938702
2,6-Dinitrotoluene ND 0.519 1 12/29/2016 18:14 WG938702
Fluoranthene ND 0.0514 1 12/29/2016 18:14 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21
L880142
SB-22
Collected date/time: 12/19/16 11:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0514 1 12/29/2016 18:14 WG938702
Hexachlorobenzene ND 0.519 1 12/29/2016 18:14 WG938702
Hexachloro-1,3-butadiene ND 0.519 1 12/29/2016 18:14 WG938702
Hexachlorocyclopentadiene ND 0.519 1 12/29/2016 18:14 WG938702
Hexachloroethane ND 0.519 1 12/29/2016 18:14 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0514 1 12/29/2016 18:14 WG938702
Isophorone ND 0.519 1 12/29/2016 18:14 WG938702
Naphthalene ND 0.0514 1 12/29/2016 18:14 WG938702
Nitrobenzene ND 0.519 1 12/29/2016 18:14 WG938702
n-Nitrosodimethylamine ND 0.519 1 12/29/2016 18:14 WG938702
n-Nitrosodiphenylamine ND 0.519 1 12/29/2016 18:14 WG938702
n-Nitrosodi-n-propylamine ND 0.519 1 12/29/2016 18:14 WG938702
Phenanthrene ND 0.0514 1 12/29/2016 18:14 WG938702
Benzylbutyl phthalate ND 0.519 1 12/29/2016 18:14 WG938702
Bis(2-ethylhexyl)phthalate ND 0.519 1 12/29/2016 18:14 WG938702
Di-n-butyl phthalate ND 0.519 1 12/29/2016 18:14 WG938702
Diethyl phthalate ND 0.519 1 12/29/2016 18:14 WG938702
Dimethyl phthalate ND 0.519 1 12/29/2016 18:14 WG938702
Di-n-octyl phthalate ND 0.519 1 12/29/2016 18:14 WG938702
Pyrene ND 0.0514 1 12/29/2016 18:14 WG938702
1,2,4-Trichlorobenzene ND 0.519 1 12/29/2016 18:14 WG938702
4-Chloro-3-methylphenol ND 0.519 1 12/29/2016 18:14 WG938702
2-Chlorophenol ND 0.519 1 12/29/2016 18:14 WG938702
2,4-Dichlorophenol ND 0.519 1 12/29/2016 18:14 WG938702
2,4-Dimethylphenol ND 0.519 1 12/29/2016 18:14 WG938702
4,6-Dinitro-2-methylphenol ND 0.519 1 12/29/2016 18:14 WG938702
2,4-Dinitrophenol ND J3 0.519 1 12/29/2016 18:14 WG938702
2-Nitrophenol ND 0.519 1 12/29/2016 18:14 WG938702
4-Nitrophenol ND 0.519 1 12/29/2016 18:14 WG938702
Pentachlorophenol ND 0.519 1 12/29/2016 18:14 WG938702
Phenol ND 0.519 1 12/29/2016 18:14 WG938702
2,4,6-Trichlorophenol ND 0.519 1 12/29/2016 18:14 WG938702
(S) 2-Fluorophenol 58.9 21.1-116 12/29/2016 18:14 WG938702
(S) Phenol-d5 57.0 26.3-121 12/29/2016 18:14 WG938702
(S) Nitrobenzene-d5 55.3 21.9-129 12/29/2016 18:14 WG938702
(S) 2-Fluorobiphenyl 61.5 34.9-129 12/29/2016 18:14 WG938702
(S) 2,4,6-Tribromophenol 57.4 21.6-142 12/29/2016 18:14 WG938702
(S) p-Terphenyl-d14 71.2 21.5-128 12/29/2016 18:14 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22
L880142
SB-24
Collected date/time: 12/19/16 11:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 71.0 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.29 16.25 12/28/2016 16:26 WG938087
(S) a,a,a-Trifluorotoluene(FID) 99.1 59.0-128 12/28/2016 16:26 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0705 1 12/26/2016 09:02 WG938078
Acrylonitrile ND 0.0141 1 12/26/2016 09:02 WG938078
Benzene ND 0.00141 1 12/26/2016 09:02 WG938078
Bromobenzene ND 0.00141 1 12/26/2016 09:02 WG938078
Bromodichloromethane ND 0.00141 1 12/26/2016 09:02 WG938078
Bromoform ND 0.00141 1 12/26/2016 09:02 WG938078
Bromomethane ND 0.00705 1 12/26/2016 09:02 WG938078
n-Butylbenzene ND 0.00141 1 12/26/2016 09:02 WG938078
sec-Butylbenzene ND 0.00141 1 12/26/2016 09:02 WG938078
tert-Butylbenzene ND 0.00141 1 12/26/2016 09:02 WG938078
Carbon tetrachloride ND 0.00141 1 12/26/2016 09:02 WG938078
Chlorobenzene ND 0.00141 1 12/26/2016 09:02 WG938078
Chlorodibromomethane ND 0.00141 1 12/26/2016 09:02 WG938078
Chloroethane ND 0.00705 1 12/26/2016 09:02 WG938078
2-Chloroethyl vinyl ether ND 0.0705 1 12/26/2016 09:02 WG938078
Chloroform ND 0.00705 1 12/26/2016 09:02 WG938078
Chloromethane ND 0.00352 1 12/26/2016 09:02 WG938078
2-Chlorotoluene ND 0.00141 1 12/26/2016 09:02 WG938078
4-Chlorotoluene ND 0.00141 1 12/26/2016 09:02 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00705 1 12/26/2016 09:02 WG938078
1,2-Dibromoethane ND 0.00141 1 12/26/2016 09:02 WG938078
Dibromomethane ND 0.00141 1 12/26/2016 09:02 WG938078
1,2-Dichlorobenzene ND 0.00141 1 12/26/2016 09:02 WG938078
1,3-Dichlorobenzene ND 0.00141 1 12/26/2016 09:02 WG938078
1,4-Dichlorobenzene ND 0.00141 1 12/26/2016 09:02 WG938078
Dichlorodifluoromethane ND 0.00705 1 12/26/2016 09:02 WG938078
1,1-Dichloroethane ND 0.00141 1 12/26/2016 09:02 WG938078
1,2-Dichloroethane ND 0.00141 1 12/26/2016 09:02 WG938078
1,1-Dichloroethene ND 0.00141 1 12/26/2016 09:02 WG938078
cis-1,2-Dichloroethene ND 0.00141 1 12/26/2016 09:02 WG938078
trans-1,2-Dichloroethene ND 0.00141 1 12/26/2016 09:02 WG938078
1,2-Dichloropropane ND 0.00141 1 12/26/2016 09:02 WG938078
1,1-Dichloropropene ND 0.00141 1 12/26/2016 09:02 WG938078
1,3-Dichloropropane ND 0.00141 1 12/26/2016 09:02 WG938078
cis-1,3-Dichloropropene ND 0.00141 1 12/26/2016 09:02 WG938078
trans-1,3-Dichloropropene ND 0.00141 1 12/26/2016 09:02 WG938078
2,2-Dichloropropane ND 0.00141 1 12/26/2016 09:02 WG938078
Di-isopropyl ether ND 0.00141 1 12/26/2016 09:02 WG938078
Ethylbenzene ND 0.00141 1 12/26/2016 09:02 WG938078
Hexachloro-1,3-butadiene ND 0.00141 1 12/26/2016 09:02 WG938078
Isopropylbenzene ND 0.00141 1 12/26/2016 09:02 WG938078
p-Isopropyltoluene ND 0.00141 1 12/26/2016 09:02 WG938078
2-Butanone (MEK)ND 0.0141 1 12/26/2016 09:02 WG938078
Methylene Chloride ND 0.00705 1 12/26/2016 09:02 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22
L880142
SB-24
Collected date/time: 12/19/16 11:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0141 1 12/26/2016 09:02 WG938078
Methyl tert-butyl ether ND J4 0.00141 1 12/26/2016 09:02 WG938078
Naphthalene ND 0.00705 1 12/26/2016 09:02 WG938078
n-Propylbenzene ND 0.00141 1 12/26/2016 09:02 WG938078
Styrene ND 0.00141 1 12/26/2016 09:02 WG938078
1,1,1,2-Tetrachloroethane ND 0.00141 1 12/26/2016 09:02 WG938078
1,1,2,2-Tetrachloroethane ND 0.00141 1 12/26/2016 09:02 WG938078
Tetrachloroethene ND 0.00141 1 12/26/2016 09:02 WG938078
Toluene ND 0.00705 1 12/26/2016 09:02 WG938078
1,2,3-Trichlorobenzene ND 0.00141 1 12/26/2016 09:02 WG938078
1,2,4-Trichlorobenzene ND 0.00141 1 12/26/2016 09:02 WG938078
1,1,1-Trichloroethane ND 0.00141 1 12/26/2016 09:02 WG938078
1,1,2-Trichloroethane ND 0.00141 1 12/26/2016 09:02 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00141 1 12/26/2016 09:02 WG938078
Trichloroethene ND 0.00141 1 12/26/2016 09:02 WG938078
Trichlorofluoromethane ND 0.00705 1 12/26/2016 09:02 WG938078
1,2,3-Trichloropropane ND 0.00352 1 12/26/2016 09:02 WG938078
1,2,4-Trimethylbenzene ND 0.00141 1 12/26/2016 09:02 WG938078
1,3,5-Trimethylbenzene ND 0.00141 1 12/26/2016 09:02 WG938078
Vinyl chloride ND 0.00141 1 12/26/2016 09:02 WG938078
Xylenes, Total ND 0.00423 1 12/26/2016 09:02 WG938078
(S) Toluene-d8 108 88.7-115 12/26/2016 09:02 WG938078
(S) Dibromofluoromethane 123 76.3-123 12/26/2016 09:02 WG938078
(S) 4-Bromofluorobenzene 91.6 69.7-129 12/26/2016 09:02 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.64 1 12/23/2016 17:41 WG937731
(S) o-Terphenyl 61.6 50.0-150 12/23/2016 17:41 WG937731
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0465 1 12/29/2016 19:57 WG938702
Acenaphthylene ND 0.0465 1 12/29/2016 19:57 WG938702
Anthracene ND 0.0465 1 12/29/2016 19:57 WG938702
Benzidine ND 0.469 1 12/29/2016 19:57 WG938702
Benzo(a)anthracene ND 0.0465 1 12/29/2016 19:57 WG938702
Benzo(b)fluoranthene ND 0.0465 1 12/29/2016 19:57 WG938702
Benzo(k)fluoranthene ND 0.0465 1 12/29/2016 19:57 WG938702
Benzo(g,h,i)perylene ND 0.0465 1 12/29/2016 19:57 WG938702
Benzo(a)pyrene ND 0.0465 1 12/29/2016 19:57 WG938702
Bis(2-chlorethoxy)methane ND 0.469 1 12/29/2016 19:57 WG938702
Bis(2-chloroethyl)ether ND 0.469 1 12/29/2016 19:57 WG938702
Bis(2-chloroisopropyl)ether ND 0.469 1 12/29/2016 19:57 WG938702
4-Bromophenyl-phenylether ND 0.469 1 12/29/2016 19:57 WG938702
2-Chloronaphthalene ND 0.0465 1 12/29/2016 19:57 WG938702
4-Chlorophenyl-phenylether ND 0.469 1 12/29/2016 19:57 WG938702
Chrysene ND 0.0465 1 12/29/2016 19:57 WG938702
Dibenz(a,h)anthracene ND 0.0465 1 12/29/2016 19:57 WG938702
3,3-Dichlorobenzidine ND 0.469 1 12/29/2016 19:57 WG938702
2,4-Dinitrotoluene ND 0.469 1 12/29/2016 19:57 WG938702
2,6-Dinitrotoluene ND 0.469 1 12/29/2016 19:57 WG938702
Fluoranthene ND 0.0465 1 12/29/2016 19:57 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22
L880142
SB-24
Collected date/time: 12/19/16 11:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0465 1 12/29/2016 19:57 WG938702
Hexachlorobenzene ND 0.469 1 12/29/2016 19:57 WG938702
Hexachloro-1,3-butadiene ND 0.469 1 12/29/2016 19:57 WG938702
Hexachlorocyclopentadiene ND 0.469 1 12/29/2016 19:57 WG938702
Hexachloroethane ND 0.469 1 12/29/2016 19:57 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0465 1 12/29/2016 19:57 WG938702
Isophorone ND 0.469 1 12/29/2016 19:57 WG938702
Naphthalene ND 0.0465 1 12/29/2016 19:57 WG938702
Nitrobenzene ND 0.469 1 12/29/2016 19:57 WG938702
n-Nitrosodimethylamine ND 0.469 1 12/29/2016 19:57 WG938702
n-Nitrosodiphenylamine ND 0.469 1 12/29/2016 19:57 WG938702
n-Nitrosodi-n-propylamine ND 0.469 1 12/29/2016 19:57 WG938702
Phenanthrene ND 0.0465 1 12/29/2016 19:57 WG938702
Benzylbutyl phthalate ND 0.469 1 12/29/2016 19:57 WG938702
Bis(2-ethylhexyl)phthalate ND 0.469 1 12/29/2016 19:57 WG938702
Di-n-butyl phthalate ND 0.469 1 12/29/2016 19:57 WG938702
Diethyl phthalate ND 0.469 1 12/29/2016 19:57 WG938702
Dimethyl phthalate ND 0.469 1 12/29/2016 19:57 WG938702
Di-n-octyl phthalate ND 0.469 1 12/29/2016 19:57 WG938702
Pyrene ND 0.0465 1 12/29/2016 19:57 WG938702
1,2,4-Trichlorobenzene ND 0.469 1 12/29/2016 19:57 WG938702
4-Chloro-3-methylphenol ND 0.469 1 12/29/2016 19:57 WG938702
2-Chlorophenol ND 0.469 1 12/29/2016 19:57 WG938702
2,4-Dichlorophenol ND 0.469 1 12/29/2016 19:57 WG938702
2,4-Dimethylphenol ND 0.469 1 12/29/2016 19:57 WG938702
4,6-Dinitro-2-methylphenol ND 0.469 1 12/29/2016 19:57 WG938702
2,4-Dinitrophenol ND J3 0.469 1 12/29/2016 19:57 WG938702
2-Nitrophenol ND 0.469 1 12/29/2016 19:57 WG938702
4-Nitrophenol ND 0.469 1 12/29/2016 19:57 WG938702
Pentachlorophenol ND 0.469 1 12/29/2016 19:57 WG938702
Phenol ND 0.469 1 12/29/2016 19:57 WG938702
2,4,6-Trichlorophenol ND 0.469 1 12/29/2016 19:57 WG938702
(S) 2-Fluorophenol 56.2 21.1-116 12/29/2016 19:57 WG938702
(S) Phenol-d5 55.2 26.3-121 12/29/2016 19:57 WG938702
(S) Nitrobenzene-d5 53.3 21.9-129 12/29/2016 19:57 WG938702
(S) 2-Fluorobiphenyl 57.5 34.9-129 12/29/2016 19:57 WG938702
(S) 2,4,6-Tribromophenol 55.3 21.6-142 12/29/2016 19:57 WG938702
(S) p-Terphenyl-d14 60.9 21.5-128 12/29/2016 19:57 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 62 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23
L880142
SB-25
Collected date/time: 12/19/16 15:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.2 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.65 21.25 12/28/2016 16:55 WG938087
(S) a,a,a-Trifluorotoluene(FID) 99.7 59.0-128 12/28/2016 16:55 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0624 1 12/26/2016 09:24 WG938078
Acrylonitrile ND 0.0125 1 12/26/2016 09:24 WG938078
Benzene ND 0.00125 1 12/26/2016 09:24 WG938078
Bromobenzene ND 0.00125 1 12/26/2016 09:24 WG938078
Bromodichloromethane ND 0.00125 1 12/26/2016 09:24 WG938078
Bromoform ND 0.00125 1 12/26/2016 09:24 WG938078
Bromomethane ND 0.00624 1 12/26/2016 09:24 WG938078
n-Butylbenzene ND 0.00125 1 12/26/2016 09:24 WG938078
sec-Butylbenzene ND 0.00125 1 12/26/2016 09:24 WG938078
tert-Butylbenzene ND 0.00125 1 12/26/2016 09:24 WG938078
Carbon tetrachloride ND 0.00125 1 12/26/2016 09:24 WG938078
Chlorobenzene ND 0.00125 1 12/26/2016 09:24 WG938078
Chlorodibromomethane ND 0.00125 1 12/26/2016 09:24 WG938078
Chloroethane ND 0.00624 1 12/26/2016 09:24 WG938078
2-Chloroethyl vinyl ether ND 0.0624 1 12/26/2016 09:24 WG938078
Chloroform ND 0.00624 1 12/26/2016 09:24 WG938078
Chloromethane ND 0.00312 1 12/26/2016 09:24 WG938078
2-Chlorotoluene ND 0.00125 1 12/26/2016 09:24 WG938078
4-Chlorotoluene ND 0.00125 1 12/26/2016 09:24 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00624 1 12/26/2016 09:24 WG938078
1,2-Dibromoethane ND 0.00125 1 12/26/2016 09:24 WG938078
Dibromomethane ND 0.00125 1 12/26/2016 09:24 WG938078
1,2-Dichlorobenzene ND 0.00125 1 12/26/2016 09:24 WG938078
1,3-Dichlorobenzene ND 0.00125 1 12/26/2016 09:24 WG938078
1,4-Dichlorobenzene ND 0.00125 1 12/26/2016 09:24 WG938078
Dichlorodifluoromethane ND 0.00624 1 12/26/2016 09:24 WG938078
1,1-Dichloroethane ND 0.00125 1 12/26/2016 09:24 WG938078
1,2-Dichloroethane ND 0.00125 1 12/26/2016 09:24 WG938078
1,1-Dichloroethene ND 0.00125 1 12/26/2016 09:24 WG938078
cis-1,2-Dichloroethene ND 0.00125 1 12/26/2016 09:24 WG938078
trans-1,2-Dichloroethene ND 0.00125 1 12/26/2016 09:24 WG938078
1,2-Dichloropropane ND 0.00125 1 12/26/2016 09:24 WG938078
1,1-Dichloropropene ND 0.00125 1 12/26/2016 09:24 WG938078
1,3-Dichloropropane ND 0.00125 1 12/26/2016 09:24 WG938078
cis-1,3-Dichloropropene ND 0.00125 1 12/26/2016 09:24 WG938078
trans-1,3-Dichloropropene ND 0.00125 1 12/26/2016 09:24 WG938078
2,2-Dichloropropane ND 0.00125 1 12/26/2016 09:24 WG938078
Di-isopropyl ether ND 0.00125 1 12/26/2016 09:24 WG938078
Ethylbenzene ND 0.00125 1 12/26/2016 09:24 WG938078
Hexachloro-1,3-butadiene ND 0.00125 1 12/26/2016 09:24 WG938078
Isopropylbenzene ND 0.00125 1 12/26/2016 09:24 WG938078
p-Isopropyltoluene ND 0.00125 1 12/26/2016 09:24 WG938078
2-Butanone (MEK)ND 0.0125 1 12/26/2016 09:24 WG938078
Methylene Chloride ND 0.00624 1 12/26/2016 09:24 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 63 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23
L880142
SB-25
Collected date/time: 12/19/16 15:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0125 1 12/26/2016 09:24 WG938078
Methyl tert-butyl ether ND J4 0.00125 1 12/26/2016 09:24 WG938078
Naphthalene ND 0.00624 1 12/26/2016 09:24 WG938078
n-Propylbenzene ND 0.00125 1 12/26/2016 09:24 WG938078
Styrene ND 0.00125 1 12/26/2016 09:24 WG938078
1,1,1,2-Tetrachloroethane ND 0.00125 1 12/26/2016 09:24 WG938078
1,1,2,2-Tetrachloroethane ND 0.00125 1 12/26/2016 09:24 WG938078
Tetrachloroethene ND 0.00125 1 12/26/2016 09:24 WG938078
Toluene ND 0.00624 1 12/26/2016 09:24 WG938078
1,2,3-Trichlorobenzene ND 0.00125 1 12/26/2016 09:24 WG938078
1,2,4-Trichlorobenzene ND 0.00125 1 12/26/2016 09:24 WG938078
1,1,1-Trichloroethane ND 0.00125 1 12/26/2016 09:24 WG938078
1,1,2-Trichloroethane ND 0.00125 1 12/26/2016 09:24 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00125 1 12/26/2016 09:24 WG938078
Trichloroethene ND 0.00125 1 12/26/2016 09:24 WG938078
Trichlorofluoromethane ND 0.00624 1 12/26/2016 09:24 WG938078
1,2,3-Trichloropropane ND 0.00312 1 12/26/2016 09:24 WG938078
1,2,4-Trimethylbenzene ND 0.00125 1 12/26/2016 09:24 WG938078
1,3,5-Trimethylbenzene ND 0.00125 1 12/26/2016 09:24 WG938078
Vinyl chloride ND 0.00125 1 12/26/2016 09:24 WG938078
Xylenes, Total ND 0.00374 1 12/26/2016 09:24 WG938078
(S) Toluene-d8 106 88.7-115 12/26/2016 09:24 WG938078
(S) Dibromofluoromethane 112 76.3-123 12/26/2016 09:24 WG938078
(S) 4-Bromofluorobenzene 98.0 69.7-129 12/26/2016 09:24 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 4.99 1 12/23/2016 16:28 WG937731
(S) o-Terphenyl 64.6 50.0-150 12/23/2016 16:28 WG937731
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0412 1 12/29/2016 18:39 WG938702
Acenaphthylene ND 0.0412 1 12/29/2016 18:39 WG938702
Anthracene ND 0.0412 1 12/29/2016 18:39 WG938702
Benzidine ND 0.415 1 12/29/2016 18:39 WG938702
Benzo(a)anthracene ND 0.0412 1 12/29/2016 18:39 WG938702
Benzo(b)fluoranthene ND 0.0412 1 12/29/2016 18:39 WG938702
Benzo(k)fluoranthene ND 0.0412 1 12/29/2016 18:39 WG938702
Benzo(g,h,i)perylene ND 0.0412 1 12/29/2016 18:39 WG938702
Benzo(a)pyrene ND 0.0412 1 12/29/2016 18:39 WG938702
Bis(2-chlorethoxy)methane ND 0.415 1 12/29/2016 18:39 WG938702
Bis(2-chloroethyl)ether ND 0.415 1 12/29/2016 18:39 WG938702
Bis(2-chloroisopropyl)ether ND 0.415 1 12/29/2016 18:39 WG938702
4-Bromophenyl-phenylether ND 0.415 1 12/29/2016 18:39 WG938702
2-Chloronaphthalene ND 0.0412 1 12/29/2016 18:39 WG938702
4-Chlorophenyl-phenylether ND 0.415 1 12/29/2016 18:39 WG938702
Chrysene ND 0.0412 1 12/29/2016 18:39 WG938702
Dibenz(a,h)anthracene ND 0.0412 1 12/29/2016 18:39 WG938702
3,3-Dichlorobenzidine ND 0.415 1 12/29/2016 18:39 WG938702
2,4-Dinitrotoluene ND 0.415 1 12/29/2016 18:39 WG938702
2,6-Dinitrotoluene ND 0.415 1 12/29/2016 18:39 WG938702
Fluoranthene ND 0.0412 1 12/29/2016 18:39 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 64 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23
L880142
SB-25
Collected date/time: 12/19/16 15:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0412 1 12/29/2016 18:39 WG938702
Hexachlorobenzene ND 0.415 1 12/29/2016 18:39 WG938702
Hexachloro-1,3-butadiene ND 0.415 1 12/29/2016 18:39 WG938702
Hexachlorocyclopentadiene ND 0.415 1 12/29/2016 18:39 WG938702
Hexachloroethane ND 0.415 1 12/29/2016 18:39 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0412 1 12/29/2016 18:39 WG938702
Isophorone ND 0.415 1 12/29/2016 18:39 WG938702
Naphthalene ND 0.0412 1 12/29/2016 18:39 WG938702
Nitrobenzene ND 0.415 1 12/29/2016 18:39 WG938702
n-Nitrosodimethylamine ND 0.415 1 12/29/2016 18:39 WG938702
n-Nitrosodiphenylamine ND 0.415 1 12/29/2016 18:39 WG938702
n-Nitrosodi-n-propylamine ND 0.415 1 12/29/2016 18:39 WG938702
Phenanthrene ND 0.0412 1 12/29/2016 18:39 WG938702
Benzylbutyl phthalate ND 0.415 1 12/29/2016 18:39 WG938702
Bis(2-ethylhexyl)phthalate ND 0.415 1 12/29/2016 18:39 WG938702
Di-n-butyl phthalate ND 0.415 1 12/29/2016 18:39 WG938702
Diethyl phthalate ND 0.415 1 12/29/2016 18:39 WG938702
Dimethyl phthalate ND 0.415 1 12/29/2016 18:39 WG938702
Di-n-octyl phthalate ND 0.415 1 12/29/2016 18:39 WG938702
Pyrene ND 0.0412 1 12/29/2016 18:39 WG938702
1,2,4-Trichlorobenzene ND 0.415 1 12/29/2016 18:39 WG938702
4-Chloro-3-methylphenol ND 0.415 1 12/29/2016 18:39 WG938702
2-Chlorophenol ND 0.415 1 12/29/2016 18:39 WG938702
2,4-Dichlorophenol ND 0.415 1 12/29/2016 18:39 WG938702
2,4-Dimethylphenol ND 0.415 1 12/29/2016 18:39 WG938702
4,6-Dinitro-2-methylphenol ND 0.415 1 12/29/2016 18:39 WG938702
2,4-Dinitrophenol ND J3 0.415 1 12/29/2016 18:39 WG938702
2-Nitrophenol ND 0.415 1 12/29/2016 18:39 WG938702
4-Nitrophenol ND 0.415 1 12/29/2016 18:39 WG938702
Pentachlorophenol ND 0.415 1 12/29/2016 18:39 WG938702
Phenol ND 0.415 1 12/29/2016 18:39 WG938702
2,4,6-Trichlorophenol ND 0.415 1 12/29/2016 18:39 WG938702
(S) 2-Fluorophenol 62.8 21.1-116 12/29/2016 18:39 WG938702
(S) Phenol-d5 61.1 26.3-121 12/29/2016 18:39 WG938702
(S) Nitrobenzene-d5 54.6 21.9-129 12/29/2016 18:39 WG938702
(S) 2-Fluorobiphenyl 60.1 34.9-129 12/29/2016 18:39 WG938702
(S) 2,4,6-Tribromophenol 56.8 21.6-142 12/29/2016 18:39 WG938702
(S) p-Terphenyl-d14 64.3 21.5-128 12/29/2016 18:39 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 65 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 65 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24
L880142
SB-28
Collected date/time: 12/19/16 15:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 70.1 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.92 20.5 12/28/2016 17:24 WG938087
(S) a,a,a-Trifluorotoluene(FID) 98.8 59.0-128 12/28/2016 17:24 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0713 1 12/26/2016 09:47 WG938078
Acrylonitrile ND 0.0143 1 12/26/2016 09:47 WG938078
Benzene ND 0.00143 1 12/26/2016 09:47 WG938078
Bromobenzene ND 0.00143 1 12/26/2016 09:47 WG938078
Bromodichloromethane ND 0.00143 1 12/26/2016 09:47 WG938078
Bromoform ND 0.00143 1 12/26/2016 09:47 WG938078
Bromomethane ND 0.00713 1 12/26/2016 09:47 WG938078
n-Butylbenzene ND 0.00143 1 12/26/2016 09:47 WG938078
sec-Butylbenzene ND 0.00143 1 12/26/2016 09:47 WG938078
tert-Butylbenzene ND 0.00143 1 12/26/2016 09:47 WG938078
Carbon tetrachloride ND 0.00143 1 12/26/2016 09:47 WG938078
Chlorobenzene ND 0.00143 1 12/26/2016 09:47 WG938078
Chlorodibromomethane ND 0.00143 1 12/26/2016 09:47 WG938078
Chloroethane ND 0.00713 1 12/26/2016 09:47 WG938078
2-Chloroethyl vinyl ether ND 0.0713 1 12/26/2016 09:47 WG938078
Chloroform ND 0.00713 1 12/26/2016 09:47 WG938078
Chloromethane ND 0.00357 1 12/26/2016 09:47 WG938078
2-Chlorotoluene ND 0.00143 1 12/26/2016 09:47 WG938078
4-Chlorotoluene ND 0.00143 1 12/26/2016 09:47 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00713 1 12/26/2016 09:47 WG938078
1,2-Dibromoethane ND 0.00143 1 12/26/2016 09:47 WG938078
Dibromomethane ND 0.00143 1 12/26/2016 09:47 WG938078
1,2-Dichlorobenzene ND 0.00143 1 12/26/2016 09:47 WG938078
1,3-Dichlorobenzene ND 0.00143 1 12/26/2016 09:47 WG938078
1,4-Dichlorobenzene ND 0.00143 1 12/26/2016 09:47 WG938078
Dichlorodifluoromethane ND 0.00713 1 12/26/2016 09:47 WG938078
1,1-Dichloroethane ND 0.00143 1 12/26/2016 09:47 WG938078
1,2-Dichloroethane ND 0.00143 1 12/26/2016 09:47 WG938078
1,1-Dichloroethene ND 0.00143 1 12/26/2016 09:47 WG938078
cis-1,2-Dichloroethene ND 0.00143 1 12/26/2016 09:47 WG938078
trans-1,2-Dichloroethene ND 0.00143 1 12/26/2016 09:47 WG938078
1,2-Dichloropropane ND 0.00143 1 12/26/2016 09:47 WG938078
1,1-Dichloropropene ND 0.00143 1 12/26/2016 09:47 WG938078
1,3-Dichloropropane ND 0.00143 1 12/26/2016 09:47 WG938078
cis-1,3-Dichloropropene ND 0.00143 1 12/26/2016 09:47 WG938078
trans-1,3-Dichloropropene ND 0.00143 1 12/26/2016 09:47 WG938078
2,2-Dichloropropane ND 0.00143 1 12/26/2016 09:47 WG938078
Di-isopropyl ether ND 0.00143 1 12/26/2016 09:47 WG938078
Ethylbenzene ND 0.00143 1 12/26/2016 09:47 WG938078
Hexachloro-1,3-butadiene ND 0.00143 1 12/26/2016 09:47 WG938078
Isopropylbenzene ND 0.00143 1 12/26/2016 09:47 WG938078
p-Isopropyltoluene ND 0.00143 1 12/26/2016 09:47 WG938078
2-Butanone (MEK)ND 0.0143 1 12/26/2016 09:47 WG938078
Methylene Chloride ND 0.00713 1 12/26/2016 09:47 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 66 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 66 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24
L880142
SB-28
Collected date/time: 12/19/16 15:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0143 1 12/26/2016 09:47 WG938078
Methyl tert-butyl ether ND J4 0.00143 1 12/26/2016 09:47 WG938078
Naphthalene ND 0.00713 1 12/26/2016 09:47 WG938078
n-Propylbenzene ND 0.00143 1 12/26/2016 09:47 WG938078
Styrene ND 0.00143 1 12/26/2016 09:47 WG938078
1,1,1,2-Tetrachloroethane ND 0.00143 1 12/26/2016 09:47 WG938078
1,1,2,2-Tetrachloroethane ND 0.00143 1 12/26/2016 09:47 WG938078
Tetrachloroethene ND 0.00143 1 12/26/2016 09:47 WG938078
Toluene ND 0.00713 1 12/26/2016 09:47 WG938078
1,2,3-Trichlorobenzene ND 0.00143 1 12/26/2016 09:47 WG938078
1,2,4-Trichlorobenzene ND 0.00143 1 12/26/2016 09:47 WG938078
1,1,1-Trichloroethane ND 0.00143 1 12/26/2016 09:47 WG938078
1,1,2-Trichloroethane ND 0.00143 1 12/26/2016 09:47 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00143 1 12/26/2016 09:47 WG938078
Trichloroethene ND 0.00143 1 12/26/2016 09:47 WG938078
Trichlorofluoromethane ND 0.00713 1 12/26/2016 09:47 WG938078
1,2,3-Trichloropropane ND 0.00357 1 12/26/2016 09:47 WG938078
1,2,4-Trimethylbenzene ND 0.00143 1 12/26/2016 09:47 WG938078
1,3,5-Trimethylbenzene ND 0.00143 1 12/26/2016 09:47 WG938078
Vinyl chloride ND 0.00143 1 12/26/2016 09:47 WG938078
Xylenes, Total ND 0.00428 1 12/26/2016 09:47 WG938078
(S) Toluene-d8 101 88.7-115 12/26/2016 09:47 WG938078
(S) Dibromofluoromethane 124 J1 76.3-123 12/26/2016 09:47 WG938078
(S) 4-Bromofluorobenzene 98.3 69.7-129 12/26/2016 09:47 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.71 1 12/23/2016 16:40 WG937731
(S) o-Terphenyl 63.9 50.0-150 12/23/2016 16:40 WG937731
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 67 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25
L880142
SB-29
Collected date/time: 12/19/16 15:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.8 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 742 45.0 350 12/28/2016 17:53 WG938087
(S) a,a,a-Trifluorotoluene(FID) 98.7 59.0-128 12/28/2016 17:53 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 22.5 350 12/26/2016 10:09 WG938078
Acrylonitrile ND 4.50 350 12/26/2016 10:09 WG938078
Benzene ND 0.450 350 12/26/2016 10:09 WG938078
Bromobenzene ND 0.450 350 12/26/2016 10:09 WG938078
Bromodichloromethane ND 0.450 350 12/26/2016 10:09 WG938078
Bromoform ND 0.450 350 12/26/2016 10:09 WG938078
Bromomethane ND 2.25 350 12/26/2016 10:09 WG938078
n-Butylbenzene 5.16 0.450 350 12/26/2016 10:09 WG938078
sec-Butylbenzene 1.85 0.450 350 12/26/2016 10:09 WG938078
tert-Butylbenzene ND 0.450 350 12/26/2016 10:09 WG938078
Carbon tetrachloride ND 0.450 350 12/26/2016 10:09 WG938078
Chlorobenzene ND 0.450 350 12/26/2016 10:09 WG938078
Chlorodibromomethane ND 0.450 350 12/26/2016 10:09 WG938078
Chloroethane ND 2.25 350 12/26/2016 10:09 WG938078
2-Chloroethyl vinyl ether ND 22.5 350 12/26/2016 10:09 WG938078
Chloroform ND 2.25 350 12/26/2016 10:09 WG938078
Chloromethane ND 1.12 350 12/26/2016 10:09 WG938078
2-Chlorotoluene ND 0.450 350 12/26/2016 10:09 WG938078
4-Chlorotoluene ND 0.450 350 12/26/2016 10:09 WG938078
1,2-Dibromo-3-Chloropropane ND 2.25 350 12/26/2016 10:09 WG938078
1,2-Dibromoethane ND 0.450 350 12/26/2016 10:09 WG938078
Dibromomethane ND 0.450 350 12/26/2016 10:09 WG938078
1,2-Dichlorobenzene ND 0.450 350 12/26/2016 10:09 WG938078
1,3-Dichlorobenzene ND 0.450 350 12/26/2016 10:09 WG938078
1,4-Dichlorobenzene ND 0.450 350 12/26/2016 10:09 WG938078
Dichlorodifluoromethane ND 2.25 350 12/26/2016 10:09 WG938078
1,1-Dichloroethane ND 0.450 350 12/26/2016 10:09 WG938078
1,2-Dichloroethane ND 0.450 350 12/26/2016 10:09 WG938078
1,1-Dichloroethene ND 0.450 350 12/26/2016 10:09 WG938078
cis-1,2-Dichloroethene ND 0.450 350 12/26/2016 10:09 WG938078
trans-1,2-Dichloroethene ND 0.450 350 12/26/2016 10:09 WG938078
1,2-Dichloropropane ND 0.450 350 12/26/2016 10:09 WG938078
1,1-Dichloropropene ND 0.450 350 12/26/2016 10:09 WG938078
1,3-Dichloropropane ND 0.450 350 12/26/2016 10:09 WG938078
cis-1,3-Dichloropropene ND 0.450 350 12/26/2016 10:09 WG938078
trans-1,3-Dichloropropene ND 0.450 350 12/26/2016 10:09 WG938078
2,2-Dichloropropane ND 0.450 350 12/26/2016 10:09 WG938078
Di-isopropyl ether ND 0.450 350 12/26/2016 10:09 WG938078
Ethylbenzene 6.79 0.450 350 12/26/2016 10:09 WG938078
Hexachloro-1,3-butadiene ND 0.450 350 12/26/2016 10:09 WG938078
Isopropylbenzene 3.07 0.450 350 12/26/2016 10:09 WG938078
p-Isopropyltoluene 1.02 0.450 350 12/26/2016 10:09 WG938078
2-Butanone (MEK)ND 4.50 350 12/26/2016 10:09 WG938078
Methylene Chloride ND 2.25 350 12/26/2016 10:09 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 68 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25
L880142
SB-29
Collected date/time: 12/19/16 15:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 4.50 350 12/26/2016 10:09 WG938078
Methyl tert-butyl ether ND J4 0.450 350 12/26/2016 10:09 WG938078
Naphthalene 24.7 2.25 350 12/26/2016 10:09 WG938078
n-Propylbenzene 14.5 0.450 350 12/26/2016 10:09 WG938078
Styrene ND 0.450 350 12/26/2016 10:09 WG938078
1,1,1,2-Tetrachloroethane ND 0.450 350 12/26/2016 10:09 WG938078
1,1,2,2-Tetrachloroethane ND 0.450 350 12/26/2016 10:09 WG938078
Tetrachloroethene ND 0.450 350 12/26/2016 10:09 WG938078
Toluene ND 2.25 350 12/26/2016 10:09 WG938078
1,2,3-Trichlorobenzene ND 0.450 350 12/26/2016 10:09 WG938078
1,2,4-Trichlorobenzene ND 0.450 350 12/26/2016 10:09 WG938078
1,1,1-Trichloroethane ND 0.450 350 12/26/2016 10:09 WG938078
1,1,2-Trichloroethane ND 0.450 350 12/26/2016 10:09 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.450 350 12/26/2016 10:09 WG938078
Trichloroethene ND 0.450 350 12/26/2016 10:09 WG938078
Trichlorofluoromethane ND 2.25 350 12/26/2016 10:09 WG938078
1,2,3-Trichloropropane ND 1.12 350 12/26/2016 10:09 WG938078
1,2,4-Trimethylbenzene 2.89 0.450 350 12/26/2016 10:09 WG938078
1,3,5-Trimethylbenzene 26.5 0.450 350 12/26/2016 10:09 WG938078
Vinyl chloride ND 0.450 350 12/26/2016 10:09 WG938078
Xylenes, Total ND 1.35 350 12/26/2016 10:09 WG938078
(S) Toluene-d8 106 88.7-115 12/26/2016 10:09 WG938078
(S) Dibromofluoromethane 108 76.3-123 12/26/2016 10:09 WG938078
(S) 4-Bromofluorobenzene 102 69.7-129 12/26/2016 10:09 WG938078
Sample Narrative:
8260B L880142-25 WG938078: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 146 5.14 1 12/23/2016 16:52 WG937731
(S) o-Terphenyl 66.7 50.0-150 12/23/2016 16:52 WG937731
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0424 1 12/29/2016 19:05 WG938702
Acenaphthylene ND 0.0424 1 12/29/2016 19:05 WG938702
Anthracene ND 0.0424 1 12/29/2016 19:05 WG938702
Benzidine ND 0.428 1 12/29/2016 19:05 WG938702
Benzo(a)anthracene ND 0.0424 1 12/29/2016 19:05 WG938702
Benzo(b)fluoranthene ND 0.0424 1 12/29/2016 19:05 WG938702
Benzo(k)fluoranthene ND 0.0424 1 12/29/2016 19:05 WG938702
Benzo(g,h,i)perylene ND 0.0424 1 12/29/2016 19:05 WG938702
Benzo(a)pyrene ND 0.0424 1 12/29/2016 19:05 WG938702
Bis(2-chlorethoxy)methane ND 0.428 1 12/29/2016 19:05 WG938702
Bis(2-chloroethyl)ether ND 0.428 1 12/29/2016 19:05 WG938702
Bis(2-chloroisopropyl)ether ND 0.428 1 12/29/2016 19:05 WG938702
4-Bromophenyl-phenylether ND 0.428 1 12/29/2016 19:05 WG938702
2-Chloronaphthalene ND 0.0424 1 12/29/2016 19:05 WG938702
4-Chlorophenyl-phenylether ND 0.428 1 12/29/2016 19:05 WG938702
Chrysene ND 0.0424 1 12/29/2016 19:05 WG938702
Dibenz(a,h)anthracene ND 0.0424 1 12/29/2016 19:05 WG938702
3,3-Dichlorobenzidine ND 0.428 1 12/29/2016 19:05 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 69 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 69 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25
L880142
SB-29
Collected date/time: 12/19/16 15:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2,4-Dinitrotoluene ND 0.428 1 12/29/2016 19:05 WG938702
2,6-Dinitrotoluene ND 0.428 1 12/29/2016 19:05 WG938702
Fluoranthene ND 0.0424 1 12/29/2016 19:05 WG938702
Fluorene ND 0.0424 1 12/29/2016 19:05 WG938702
Hexachlorobenzene ND 0.428 1 12/29/2016 19:05 WG938702
Hexachloro-1,3-butadiene ND 0.428 1 12/29/2016 19:05 WG938702
Hexachlorocyclopentadiene ND 0.428 1 12/29/2016 19:05 WG938702
Hexachloroethane ND 0.428 1 12/29/2016 19:05 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0424 1 12/29/2016 19:05 WG938702
Isophorone ND 0.428 1 12/29/2016 19:05 WG938702
Naphthalene 3.36 0.212 5 12/30/2016 13:10 WG938702
Nitrobenzene ND 0.428 1 12/29/2016 19:05 WG938702
n-Nitrosodimethylamine ND 0.428 1 12/29/2016 19:05 WG938702
n-Nitrosodiphenylamine ND 0.428 1 12/29/2016 19:05 WG938702
n-Nitrosodi-n-propylamine ND 0.428 1 12/29/2016 19:05 WG938702
Phenanthrene ND 0.0424 1 12/29/2016 19:05 WG938702
Benzylbutyl phthalate ND 0.428 1 12/29/2016 19:05 WG938702
Bis(2-ethylhexyl)phthalate ND 0.428 1 12/29/2016 19:05 WG938702
Di-n-butyl phthalate ND 0.428 1 12/29/2016 19:05 WG938702
Diethyl phthalate ND 0.428 1 12/29/2016 19:05 WG938702
Dimethyl phthalate ND 0.428 1 12/29/2016 19:05 WG938702
Di-n-octyl phthalate ND 0.428 1 12/29/2016 19:05 WG938702
Pyrene ND 0.0424 1 12/29/2016 19:05 WG938702
1,2,4-Trichlorobenzene ND 0.428 1 12/29/2016 19:05 WG938702
4-Chloro-3-methylphenol ND 0.428 1 12/29/2016 19:05 WG938702
2-Chlorophenol ND 0.428 1 12/29/2016 19:05 WG938702
2,4-Dichlorophenol ND 0.428 1 12/29/2016 19:05 WG938702
2,4-Dimethylphenol ND 0.428 1 12/29/2016 19:05 WG938702
4,6-Dinitro-2-methylphenol ND 0.428 1 12/29/2016 19:05 WG938702
2,4-Dinitrophenol ND J3 0.428 1 12/29/2016 19:05 WG938702
2-Nitrophenol ND 0.428 1 12/29/2016 19:05 WG938702
4-Nitrophenol ND 0.428 1 12/29/2016 19:05 WG938702
Pentachlorophenol ND 0.428 1 12/29/2016 19:05 WG938702
Phenol ND 0.428 1 12/29/2016 19:05 WG938702
2,4,6-Trichlorophenol ND 0.428 1 12/29/2016 19:05 WG938702
(S) 2-Fluorophenol 58.5 21.1-116 12/29/2016 19:05 WG938702
(S) 2-Fluorophenol 60.6 21.1-116 12/30/2016 13:10 WG938702
(S) Phenol-d5 59.5 26.3-121 12/30/2016 13:10 WG938702
(S) Phenol-d5 59.8 26.3-121 12/29/2016 19:05 WG938702
(S) Nitrobenzene-d5 67.9 21.9-129 12/29/2016 19:05 WG938702
(S) Nitrobenzene-d5 70.5 21.9-129 12/30/2016 13:10 WG938702
(S) 2-Fluorobiphenyl 62.4 34.9-129 12/30/2016 13:10 WG938702
(S) 2-Fluorobiphenyl 61.1 34.9-129 12/29/2016 19:05 WG938702
(S) 2,4,6-Tribromophenol 57.5 21.6-142 12/29/2016 19:05 WG938702
(S) 2,4,6-Tribromophenol 48.5 21.6-142 12/30/2016 13:10 WG938702
(S) p-Terphenyl-d14 65.9 21.5-128 12/30/2016 13:10 WG938702
(S) p-Terphenyl-d14 65.1 21.5-128 12/29/2016 19:05 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 70 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26
L880142
SB-31
Collected date/time: 12/19/16 15:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.0 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.34 17.75 12/28/2016 18:22 WG938087
(S) a,a,a-Trifluorotoluene(FID) 99.6 59.0-128 12/28/2016 18:22 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone 0.197 0.0658 1 12/29/2016 04:16 WG938078
Acrylonitrile ND 0.0132 1 12/29/2016 04:16 WG938078
Benzene ND 0.00132 1 12/29/2016 04:16 WG938078
Bromobenzene ND 0.00132 1 12/29/2016 04:16 WG938078
Bromodichloromethane ND 0.00132 1 12/29/2016 04:16 WG938078
Bromoform ND 0.00132 1 12/29/2016 04:16 WG938078
Bromomethane ND 0.00658 1 12/29/2016 04:16 WG938078
n-Butylbenzene ND 0.00132 1 12/29/2016 04:16 WG938078
sec-Butylbenzene ND 0.00132 1 12/29/2016 04:16 WG938078
tert-Butylbenzene ND 0.00132 1 12/29/2016 04:16 WG938078
Carbon tetrachloride ND 0.00132 1 12/29/2016 04:16 WG938078
Chlorobenzene ND 0.00132 1 12/29/2016 04:16 WG938078
Chlorodibromomethane ND 0.00132 1 12/29/2016 04:16 WG938078
Chloroethane ND 0.00658 1 12/29/2016 04:16 WG938078
2-Chloroethyl vinyl ether ND 0.0658 1 12/29/2016 04:16 WG938078
Chloroform ND 0.00658 1 12/29/2016 04:16 WG938078
Chloromethane ND 0.00329 1 12/29/2016 04:16 WG938078
2-Chlorotoluene ND 0.00132 1 12/29/2016 04:16 WG938078
4-Chlorotoluene ND 0.00132 1 12/29/2016 04:16 WG938078
1,2-Dibromo-3-Chloropropane ND 0.00658 1 12/29/2016 04:16 WG938078
1,2-Dibromoethane ND 0.00132 1 12/29/2016 04:16 WG938078
Dibromomethane ND 0.00132 1 12/29/2016 04:16 WG938078
1,2-Dichlorobenzene ND 0.00132 1 12/29/2016 04:16 WG938078
1,3-Dichlorobenzene ND 0.00132 1 12/29/2016 04:16 WG938078
1,4-Dichlorobenzene ND 0.00132 1 12/29/2016 04:16 WG938078
Dichlorodifluoromethane ND 0.00658 1 12/29/2016 04:16 WG938078
1,1-Dichloroethane ND 0.00132 1 12/29/2016 04:16 WG938078
1,2-Dichloroethane ND 0.00132 1 12/29/2016 04:16 WG938078
1,1-Dichloroethene ND 0.00132 1 12/29/2016 04:16 WG938078
cis-1,2-Dichloroethene ND 0.00132 1 12/29/2016 04:16 WG938078
trans-1,2-Dichloroethene ND 0.00132 1 12/29/2016 04:16 WG938078
1,2-Dichloropropane ND 0.00132 1 12/29/2016 04:16 WG938078
1,1-Dichloropropene ND 0.00132 1 12/29/2016 04:16 WG938078
1,3-Dichloropropane ND 0.00132 1 12/29/2016 04:16 WG938078
cis-1,3-Dichloropropene ND 0.00132 1 12/29/2016 04:16 WG938078
trans-1,3-Dichloropropene ND 0.00132 1 12/29/2016 04:16 WG938078
2,2-Dichloropropane ND 0.00132 1 12/29/2016 04:16 WG938078
Di-isopropyl ether ND 0.00132 1 12/29/2016 04:16 WG938078
Ethylbenzene 0.00161 0.00132 1 12/29/2016 04:16 WG938078
Hexachloro-1,3-butadiene ND 0.00132 1 12/29/2016 04:16 WG938078
Isopropylbenzene ND 0.00132 1 12/29/2016 04:16 WG938078
p-Isopropyltoluene ND 0.00132 1 12/29/2016 04:16 WG938078
2-Butanone (MEK)ND 0.0132 1 12/29/2016 04:16 WG938078
Methylene Chloride ND 0.00658 1 12/29/2016 04:16 WG938078
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 71 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 71 of 142
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26
L880142
SB-31
Collected date/time: 12/19/16 15:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND 0.0132 1 12/29/2016 04:16 WG938078
Methyl tert-butyl ether ND J4 0.00132 1 12/29/2016 04:16 WG938078
Naphthalene ND 0.00658 1 12/29/2016 04:16 WG938078
n-Propylbenzene ND 0.00132 1 12/29/2016 04:16 WG938078
Styrene ND 0.00132 1 12/29/2016 04:16 WG938078
1,1,1,2-Tetrachloroethane ND 0.00132 1 12/29/2016 04:16 WG938078
1,1,2,2-Tetrachloroethane ND 0.00132 1 12/29/2016 04:16 WG938078
Tetrachloroethene ND 0.00132 1 12/29/2016 04:16 WG938078
Toluene ND 0.00658 1 12/29/2016 04:16 WG938078
1,2,3-Trichlorobenzene ND 0.00132 1 12/29/2016 04:16 WG938078
1,2,4-Trichlorobenzene ND 0.00132 1 12/29/2016 04:16 WG938078
1,1,1-Trichloroethane ND 0.00132 1 12/29/2016 04:16 WG938078
1,1,2-Trichloroethane ND 0.00132 1 12/29/2016 04:16 WG938078
1,1,2-Trichlorotrifluoroethane ND 0.00132 1 12/29/2016 04:16 WG938078
Trichloroethene ND 0.00132 1 12/29/2016 04:16 WG938078
Trichlorofluoromethane ND 0.00658 1 12/29/2016 04:16 WG938078
1,2,3-Trichloropropane ND 0.00329 1 12/29/2016 04:16 WG938078
1,2,4-Trimethylbenzene ND 0.00132 1 12/29/2016 04:16 WG938078
1,3,5-Trimethylbenzene ND 0.00132 1 12/29/2016 04:16 WG938078
Vinyl chloride ND 0.00132 1 12/29/2016 04:16 WG938078
Xylenes, Total 0.0123 0.00395 1 12/29/2016 04:16 WG938078
(S) Toluene-d8 101 88.7-115 12/29/2016 04:16 WG938078
(S) Dibromofluoromethane 96.3 76.3-123 12/29/2016 04:16 WG938078
(S) 4-Bromofluorobenzene 95.0 69.7-129 12/29/2016 04:16 WG938078
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 5.26 1 12/23/2016 17:05 WG937731
(S) o-Terphenyl 53.4 50.0-150 12/23/2016 17:05 WG937731
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0434 1 12/29/2016 19:31 WG938702
Acenaphthylene ND 0.0434 1 12/29/2016 19:31 WG938702
Anthracene ND 0.0434 1 12/29/2016 19:31 WG938702
Benzidine ND 0.438 1 12/29/2016 19:31 WG938702
Benzo(a)anthracene ND 0.0434 1 12/29/2016 19:31 WG938702
Benzo(b)fluoranthene ND 0.0434 1 12/29/2016 19:31 WG938702
Benzo(k)fluoranthene ND 0.0434 1 12/29/2016 19:31 WG938702
Benzo(g,h,i)perylene ND 0.0434 1 12/29/2016 19:31 WG938702
Benzo(a)pyrene ND 0.0434 1 12/29/2016 19:31 WG938702
Bis(2-chlorethoxy)methane ND 0.438 1 12/29/2016 19:31 WG938702
Bis(2-chloroethyl)ether ND 0.438 1 12/29/2016 19:31 WG938702
Bis(2-chloroisopropyl)ether ND 0.438 1 12/29/2016 19:31 WG938702
4-Bromophenyl-phenylether ND 0.438 1 12/29/2016 19:31 WG938702
2-Chloronaphthalene ND 0.0434 1 12/29/2016 19:31 WG938702
4-Chlorophenyl-phenylether ND 0.438 1 12/29/2016 19:31 WG938702
Chrysene ND 0.0434 1 12/29/2016 19:31 WG938702
Dibenz(a,h)anthracene ND 0.0434 1 12/29/2016 19:31 WG938702
3,3-Dichlorobenzidine ND 0.438 1 12/29/2016 19:31 WG938702
2,4-Dinitrotoluene ND 0.438 1 12/29/2016 19:31 WG938702
2,6-Dinitrotoluene ND 0.438 1 12/29/2016 19:31 WG938702
Fluoranthene ND 0.0434 1 12/29/2016 19:31 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26
L880142
SB-31
Collected date/time: 12/19/16 15:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluorene ND 0.0434 1 12/29/2016 19:31 WG938702
Hexachlorobenzene ND 0.438 1 12/29/2016 19:31 WG938702
Hexachloro-1,3-butadiene ND 0.438 1 12/29/2016 19:31 WG938702
Hexachlorocyclopentadiene ND 0.438 1 12/29/2016 19:31 WG938702
Hexachloroethane ND 0.438 1 12/29/2016 19:31 WG938702
Indeno(1,2,3-cd)pyrene ND 0.0434 1 12/29/2016 19:31 WG938702
Isophorone ND 0.438 1 12/29/2016 19:31 WG938702
Naphthalene ND 0.0434 1 12/29/2016 19:31 WG938702
Nitrobenzene ND 0.438 1 12/29/2016 19:31 WG938702
n-Nitrosodimethylamine ND 0.438 1 12/29/2016 19:31 WG938702
n-Nitrosodiphenylamine ND 0.438 1 12/29/2016 19:31 WG938702
n-Nitrosodi-n-propylamine ND 0.438 1 12/29/2016 19:31 WG938702
Phenanthrene ND 0.0434 1 12/29/2016 19:31 WG938702
Benzylbutyl phthalate ND 0.438 1 12/29/2016 19:31 WG938702
Bis(2-ethylhexyl)phthalate ND 0.438 1 12/29/2016 19:31 WG938702
Di-n-butyl phthalate ND 0.438 1 12/29/2016 19:31 WG938702
Diethyl phthalate ND 0.438 1 12/29/2016 19:31 WG938702
Dimethyl phthalate ND 0.438 1 12/29/2016 19:31 WG938702
Di-n-octyl phthalate ND 0.438 1 12/29/2016 19:31 WG938702
Pyrene ND 0.0434 1 12/29/2016 19:31 WG938702
1,2,4-Trichlorobenzene ND 0.438 1 12/29/2016 19:31 WG938702
4-Chloro-3-methylphenol ND 0.438 1 12/29/2016 19:31 WG938702
2-Chlorophenol ND 0.438 1 12/29/2016 19:31 WG938702
2,4-Dichlorophenol ND 0.438 1 12/29/2016 19:31 WG938702
2,4-Dimethylphenol ND 0.438 1 12/29/2016 19:31 WG938702
4,6-Dinitro-2-methylphenol ND 0.438 1 12/29/2016 19:31 WG938702
2,4-Dinitrophenol ND J3 0.438 1 12/29/2016 19:31 WG938702
2-Nitrophenol ND 0.438 1 12/29/2016 19:31 WG938702
4-Nitrophenol ND 0.438 1 12/29/2016 19:31 WG938702
Pentachlorophenol ND 0.438 1 12/29/2016 19:31 WG938702
Phenol ND 0.438 1 12/29/2016 19:31 WG938702
2,4,6-Trichlorophenol ND 0.438 1 12/29/2016 19:31 WG938702
(S) 2-Fluorophenol 52.3 21.1-116 12/29/2016 19:31 WG938702
(S) Phenol-d5 54.1 26.3-121 12/29/2016 19:31 WG938702
(S) Nitrobenzene-d5 50.5 21.9-129 12/29/2016 19:31 WG938702
(S) 2-Fluorobiphenyl 57.2 34.9-129 12/29/2016 19:31 WG938702
(S) 2,4,6-Tribromophenol 57.1 21.6-142 12/29/2016 19:31 WG938702
(S) p-Terphenyl-d14 61.9 21.5-128 12/29/2016 19:31 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 27
L880142
TP-1A
Collected date/time: 12/20/16 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.3 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.07 17 12/28/2016 19:26 WG938087
(S) a,a,a-Trifluorotoluene(FID) 98.9 59.0-128 12/28/2016 19:26 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0608 1 12/27/2016 01:49 WG938079
Acrylonitrile ND J3 J6 0.0122 1 12/27/2016 01:49 WG938079
Benzene ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
Bromobenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
Bromodichloromethane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
Bromoform ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
Bromomethane ND 0.00608 1 12/27/2016 01:49 WG938079
n-Butylbenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
sec-Butylbenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
tert-Butylbenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
Carbon tetrachloride ND J6 0.00122 1 12/27/2016 01:49 WG938079
Chlorobenzene 0.00548 J6 0.00122 1 12/27/2016 01:49 WG938079
Chlorodibromomethane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
Chloroethane ND 0.00608 1 12/27/2016 01:49 WG938079
2-Chloroethyl vinyl ether ND J6 0.0608 1 12/27/2016 01:49 WG938079
Chloroform ND J3 J6 0.00608 1 12/27/2016 01:49 WG938079
Chloromethane ND J6 0.00304 1 12/27/2016 01:49 WG938079
2-Chlorotoluene ND J6 0.00122 1 12/27/2016 01:49 WG938079
4-Chlorotoluene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,2-Dibromo-3-Chloropropane ND J6 0.00608 1 12/27/2016 01:49 WG938079
1,2-Dibromoethane ND J3 J4 J6 0.00122 1 12/27/2016 01:49 WG938079
Dibromomethane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
1,2-Dichlorobenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,3-Dichlorobenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,4-Dichlorobenzene ND J4 J6 0.00122 1 12/27/2016 01:49 WG938079
Dichlorodifluoromethane ND J6 0.00608 1 12/27/2016 01:49 WG938079
1,1-Dichloroethane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
1,2-Dichloroethane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
1,1-Dichloroethene ND J6 0.00122 1 12/27/2016 01:49 WG938079
cis-1,2-Dichloroethene ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
trans-1,2-Dichloroethene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,2-Dichloropropane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
1,1-Dichloropropene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,3-Dichloropropane ND J3 J4 J6 0.00122 1 12/27/2016 01:49 WG938079
cis-1,3-Dichloropropene ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
trans-1,3-Dichloropropene ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
2,2-Dichloropropane ND J6 0.00122 1 12/27/2016 01:49 WG938079
Di-isopropyl ether ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
Ethylbenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
Hexachloro-1,3-butadiene ND J6 0.00122 1 12/27/2016 01:49 WG938079
Isopropylbenzene 0.00214 J6 0.00122 1 12/27/2016 01:49 WG938079
p-Isopropyltoluene ND J6 0.00122 1 12/27/2016 01:49 WG938079
2-Butanone (MEK)ND J3 J6 0.0122 1 12/27/2016 01:49 WG938079
Methylene Chloride ND J3 J6 0.00608 1 12/27/2016 01:49 WG938079
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 27
L880142
TP-1A
Collected date/time: 12/20/16 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND J3 J6 0.0122 1 12/27/2016 01:49 WG938079
Methyl tert-butyl ether ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
Naphthalene ND J6 0.00608 1 12/27/2016 01:49 WG938079
n-Propylbenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
Styrene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,1,1,2-Tetrachloroethane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
1,1,2,2-Tetrachloroethane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
Tetrachloroethene ND J6 0.00122 1 12/27/2016 01:49 WG938079
Toluene ND J6 0.00608 1 12/27/2016 01:49 WG938079
1,2,3-Trichlorobenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,2,4-Trichlorobenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,1,1-Trichloroethane ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,1,2-Trichloroethane ND J3 J6 0.00122 1 12/27/2016 01:49 WG938079
1,1,2-Trichlorotrifluoroethane ND J6 0.00122 1 12/27/2016 01:49 WG938079
Trichloroethene ND J6 0.00122 1 12/27/2016 01:49 WG938079
Trichlorofluoromethane 3.90 0.103 17 12/27/2016 21:02 WG938079
1,2,3-Trichloropropane ND J3 J6 0.00304 1 12/27/2016 01:49 WG938079
1,2,4-Trimethylbenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
1,3,5-Trimethylbenzene ND J6 0.00122 1 12/27/2016 01:49 WG938079
Vinyl chloride ND J6 0.00122 1 12/27/2016 01:49 WG938079
Xylenes, Total ND J6 0.00365 1 12/27/2016 01:49 WG938079
(S) Toluene-d8 99.1 88.7-115 12/27/2016 01:49 WG938079
(S) Toluene-d8 102 88.7-115 12/27/2016 21:02 WG938079
(S) Dibromofluoromethane 92.8 76.3-123 12/27/2016 21:02 WG938079
(S) Dibromofluoromethane 111 76.3-123 12/27/2016 01:49 WG938079
(S) 4-Bromofluorobenzene 94.0 69.7-129 12/27/2016 01:49 WG938079
(S) 4-Bromofluorobenzene 98.9 69.7-129 12/27/2016 21:02 WG938079
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 48.6 10 12/23/2016 20:08 WG937731
(S) o-Terphenyl 69.0 50.0-150 12/23/2016 20:08 WG937731
Sample Narrative:
8015 L880142-27 WG937731: Cannot run at lower dilution due to viscosity of extract
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 2.01 50 12/30/2016 13:35 WG938702
Acenaphthylene ND 2.01 50 12/30/2016 13:35 WG938702
Anthracene ND 2.01 50 12/30/2016 13:35 WG938702
Benzidine ND 20.2 50 12/30/2016 13:35 WG938702
Benzo(a)anthracene ND 2.01 50 12/30/2016 13:35 WG938702
Benzo(b)fluoranthene ND 2.01 50 12/30/2016 13:35 WG938702
Benzo(k)fluoranthene ND 2.01 50 12/30/2016 13:35 WG938702
Benzo(g,h,i)perylene ND 2.01 50 12/30/2016 13:35 WG938702
Benzo(a)pyrene ND 2.01 50 12/30/2016 13:35 WG938702
Bis(2-chlorethoxy)methane ND 20.2 50 12/30/2016 13:35 WG938702
Bis(2-chloroethyl)ether ND 20.2 50 12/30/2016 13:35 WG938702
Bis(2-chloroisopropyl)ether ND 20.2 50 12/30/2016 13:35 WG938702
4-Bromophenyl-phenylether ND 20.2 50 12/30/2016 13:35 WG938702
2-Chloronaphthalene ND 2.01 50 12/30/2016 13:35 WG938702
4-Chlorophenyl-phenylether ND 20.2 50 12/30/2016 13:35 WG938702
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 27
L880142
TP-1A
Collected date/time: 12/20/16 10:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Chrysene ND 2.01 50 12/30/2016 13:35 WG938702
Dibenz(a,h)anthracene ND 2.01 50 12/30/2016 13:35 WG938702
3,3-Dichlorobenzidine ND 20.2 50 12/30/2016 13:35 WG938702
2,4-Dinitrotoluene ND 20.2 50 12/30/2016 13:35 WG938702
2,6-Dinitrotoluene ND 20.2 50 12/30/2016 13:35 WG938702
Fluoranthene ND 2.01 50 12/30/2016 13:35 WG938702
Fluorene ND 2.01 50 12/30/2016 13:35 WG938702
Hexachlorobenzene ND 20.2 50 12/30/2016 13:35 WG938702
Hexachloro-1,3-butadiene ND 20.2 50 12/30/2016 13:35 WG938702
Hexachlorocyclopentadiene ND 20.2 50 12/30/2016 13:35 WG938702
Hexachloroethane ND 20.2 50 12/30/2016 13:35 WG938702
Indeno(1,2,3-cd)pyrene ND 2.01 50 12/30/2016 13:35 WG938702
Isophorone ND 20.2 50 12/30/2016 13:35 WG938702
Naphthalene ND 2.01 50 12/30/2016 13:35 WG938702
Nitrobenzene ND 20.2 50 12/30/2016 13:35 WG938702
n-Nitrosodimethylamine ND 20.2 50 12/30/2016 13:35 WG938702
n-Nitrosodiphenylamine ND 20.2 50 12/30/2016 13:35 WG938702
n-Nitrosodi-n-propylamine ND 20.2 50 12/30/2016 13:35 WG938702
Phenanthrene ND 2.01 50 12/30/2016 13:35 WG938702
Benzylbutyl phthalate ND 20.2 50 12/30/2016 13:35 WG938702
Bis(2-ethylhexyl)phthalate ND 20.2 50 12/30/2016 13:35 WG938702
Di-n-butyl phthalate ND 20.2 50 12/30/2016 13:35 WG938702
Diethyl phthalate ND 20.2 50 12/30/2016 13:35 WG938702
Dimethyl phthalate ND 20.2 50 12/30/2016 13:35 WG938702
Di-n-octyl phthalate ND 20.2 50 12/30/2016 13:35 WG938702
Pyrene ND 2.01 50 12/30/2016 13:35 WG938702
1,2,4-Trichlorobenzene ND 20.2 50 12/30/2016 13:35 WG938702
4-Chloro-3-methylphenol ND 20.2 50 12/30/2016 13:35 WG938702
2-Chlorophenol ND 20.2 50 12/30/2016 13:35 WG938702
2,4-Dichlorophenol ND 20.2 50 12/30/2016 13:35 WG938702
2,4-Dimethylphenol ND 20.2 50 12/30/2016 13:35 WG938702
4,6-Dinitro-2-methylphenol ND 20.2 50 12/30/2016 13:35 WG938702
2,4-Dinitrophenol ND J3 20.2 50 12/30/2016 13:35 WG938702
2-Nitrophenol ND 20.2 50 12/30/2016 13:35 WG938702
4-Nitrophenol ND 20.2 50 12/30/2016 13:35 WG938702
Pentachlorophenol ND 20.2 50 12/30/2016 13:35 WG938702
Phenol ND 20.2 50 12/30/2016 13:35 WG938702
2,4,6-Trichlorophenol ND 20.2 50 12/30/2016 13:35 WG938702
(S) 2-Fluorophenol 62.3 J7 21.1-116 12/30/2016 13:35 WG938702
(S) Phenol-d5 65.6 J7 26.3-121 12/30/2016 13:35 WG938702
(S) Nitrobenzene-d5 61.7 J7 21.9-129 12/30/2016 13:35 WG938702
(S) 2-Fluorobiphenyl 69.7 J7 34.9-129 12/30/2016 13:35 WG938702
(S) 2,4,6-Tribromophenol 38.6 J7 21.6-142 12/30/2016 13:35 WG938702
(S) p-Terphenyl-d14 72.1 J7 21.5-128 12/30/2016 13:35 WG938702
Sample Narrative:
8270D L880142-27 WG938702: Dilution due to matrix
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28
L880142
TP-1B
Collected date/time: 12/20/16 10:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.3 1 12/22/2016 11:00 WG937882
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 1.96 15.75 12/28/2016 19:55 WG938087
(S) a,a,a-Trifluorotoluene(FID) 99.3 59.0-128 12/28/2016 19:55 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0623 1 12/27/2016 06:17 WG938079
Acrylonitrile ND 0.0125 1 12/27/2016 06:17 WG938079
Benzene ND 0.00125 1 12/27/2016 06:17 WG938079
Bromobenzene ND 0.00125 1 12/27/2016 06:17 WG938079
Bromodichloromethane ND 0.00125 1 12/27/2016 06:17 WG938079
Bromoform ND 0.00125 1 12/27/2016 06:17 WG938079
Bromomethane ND 0.00623 1 12/27/2016 06:17 WG938079
n-Butylbenzene ND 0.00125 1 12/27/2016 06:17 WG938079
sec-Butylbenzene ND 0.00125 1 12/27/2016 06:17 WG938079
tert-Butylbenzene ND 0.00125 1 12/27/2016 06:17 WG938079
Carbon tetrachloride ND 0.00125 1 12/27/2016 06:17 WG938079
Chlorobenzene ND 0.00125 1 12/27/2016 06:17 WG938079
Chlorodibromomethane ND 0.00125 1 12/27/2016 06:17 WG938079
Chloroethane ND 0.00623 1 12/27/2016 06:17 WG938079
2-Chloroethyl vinyl ether ND 0.0623 1 12/27/2016 06:17 WG938079
Chloroform ND 0.00623 1 12/27/2016 06:17 WG938079
Chloromethane ND 0.00311 1 12/27/2016 06:17 WG938079
2-Chlorotoluene ND 0.00125 1 12/27/2016 06:17 WG938079
4-Chlorotoluene ND 0.00125 1 12/27/2016 06:17 WG938079
1,2-Dibromo-3-Chloropropane ND J3 0.00623 1 12/27/2016 06:17 WG938079
1,2-Dibromoethane ND J4 0.00125 1 12/27/2016 06:17 WG938079
Dibromomethane ND 0.00125 1 12/27/2016 06:17 WG938079
1,2-Dichlorobenzene ND 0.00125 1 12/27/2016 06:17 WG938079
1,3-Dichlorobenzene ND 0.00125 1 12/27/2016 06:17 WG938079
1,4-Dichlorobenzene ND J4 0.00125 1 12/27/2016 06:17 WG938079
Dichlorodifluoromethane ND 0.00623 1 12/27/2016 06:17 WG938079
1,1-Dichloroethane ND 0.00125 1 12/27/2016 06:17 WG938079
1,2-Dichloroethane ND 0.00125 1 12/27/2016 06:17 WG938079
1,1-Dichloroethene ND 0.00125 1 12/27/2016 06:17 WG938079
cis-1,2-Dichloroethene ND 0.00125 1 12/27/2016 06:17 WG938079
trans-1,2-Dichloroethene ND 0.00125 1 12/27/2016 06:17 WG938079
1,2-Dichloropropane ND 0.00125 1 12/27/2016 06:17 WG938079
1,1-Dichloropropene ND 0.00125 1 12/27/2016 06:17 WG938079
1,3-Dichloropropane ND J4 0.00125 1 12/27/2016 06:17 WG938079
cis-1,3-Dichloropropene ND 0.00125 1 12/27/2016 06:17 WG938079
trans-1,3-Dichloropropene ND 0.00125 1 12/27/2016 06:17 WG938079
2,2-Dichloropropane ND 0.00125 1 12/27/2016 06:17 WG938079
Di-isopropyl ether ND 0.00125 1 12/27/2016 06:17 WG938079
Ethylbenzene ND 0.00125 1 12/27/2016 06:17 WG938079
Hexachloro-1,3-butadiene ND 0.00125 1 12/27/2016 06:17 WG938079
Isopropylbenzene ND 0.00125 1 12/27/2016 06:17 WG938079
p-Isopropyltoluene ND 0.00125 1 12/27/2016 06:17 WG938079
2-Butanone (MEK)ND 0.0125 1 12/27/2016 06:17 WG938079
Methylene Chloride ND 0.00623 1 12/27/2016 06:17 WG938079
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28
L880142
TP-1B
Collected date/time: 12/20/16 10:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND J3 0.0125 1 12/27/2016 06:17 WG938079
Methyl tert-butyl ether ND 0.00125 1 12/27/2016 06:17 WG938079
Naphthalene ND 0.00623 1 12/27/2016 06:17 WG938079
n-Propylbenzene ND 0.00125 1 12/27/2016 06:17 WG938079
Styrene ND 0.00125 1 12/27/2016 06:17 WG938079
1,1,1,2-Tetrachloroethane ND 0.00125 1 12/27/2016 06:17 WG938079
1,1,2,2-Tetrachloroethane ND 0.00125 1 12/27/2016 06:17 WG938079
Tetrachloroethene ND 0.00125 1 12/27/2016 06:17 WG938079
Toluene ND 0.00623 1 12/27/2016 06:17 WG938079
1,2,3-Trichlorobenzene ND 0.00125 1 12/27/2016 06:17 WG938079
1,2,4-Trichlorobenzene ND 0.00125 1 12/27/2016 06:17 WG938079
1,1,1-Trichloroethane ND 0.00125 1 12/27/2016 06:17 WG938079
1,1,2-Trichloroethane ND 0.00125 1 12/27/2016 06:17 WG938079
1,1,2-Trichlorotrifluoroethane ND 0.00125 1 12/27/2016 06:17 WG938079
Trichloroethene ND 0.00125 1 12/27/2016 06:17 WG938079
Trichlorofluoromethane ND 0.00623 1 12/27/2016 06:17 WG938079
1,2,3-Trichloropropane ND J3 0.00311 1 12/27/2016 06:17 WG938079
1,2,4-Trimethylbenzene ND 0.00125 1 12/27/2016 06:17 WG938079
1,3,5-Trimethylbenzene ND 0.00125 1 12/27/2016 06:17 WG938079
Vinyl chloride ND 0.00125 1 12/27/2016 06:17 WG938079
Xylenes, Total ND 0.00374 1 12/27/2016 06:17 WG938079
(S) Toluene-d8 103 88.7-115 12/27/2016 06:17 WG938079
(S) Dibromofluoromethane 109 76.3-123 12/27/2016 06:17 WG938079
(S) 4-Bromofluorobenzene 99.8 69.7-129 12/27/2016 06:17 WG938079
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 4.98 1 12/23/2016 17:17 WG937731
(S) o-Terphenyl 61.1 50.0-150 12/23/2016 17:17 WG937731
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 29
L880142
TP-10B
Collected date/time: 12/20/16 12:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.8 1 12/23/2016 13:23 WG937884
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction ND 2.00 16.75 12/28/2016 20:23 WG938087
(S) a,a,a-Trifluorotoluene(FID) 99.6 59.0-128 12/28/2016 20:23 WG938087
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.0597 1 12/27/2016 06:37 WG938079
Acrylonitrile ND 0.0119 1 12/27/2016 06:37 WG938079
Benzene ND 0.00119 1 12/27/2016 06:37 WG938079
Bromobenzene ND 0.00119 1 12/27/2016 06:37 WG938079
Bromodichloromethane ND 0.00119 1 12/27/2016 06:37 WG938079
Bromoform ND 0.00119 1 12/27/2016 06:37 WG938079
Bromomethane ND 0.00597 1 12/27/2016 06:37 WG938079
n-Butylbenzene ND 0.00119 1 12/27/2016 06:37 WG938079
sec-Butylbenzene ND 0.00119 1 12/27/2016 06:37 WG938079
tert-Butylbenzene ND 0.00119 1 12/27/2016 06:37 WG938079
Carbon tetrachloride ND 0.00119 1 12/27/2016 06:37 WG938079
Chlorobenzene ND 0.00119 1 12/27/2016 06:37 WG938079
Chlorodibromomethane ND 0.00119 1 12/27/2016 06:37 WG938079
Chloroethane ND 0.00597 1 12/27/2016 06:37 WG938079
2-Chloroethyl vinyl ether ND 0.0597 1 12/27/2016 06:37 WG938079
Chloroform ND 0.00597 1 12/27/2016 06:37 WG938079
Chloromethane ND 0.00298 1 12/27/2016 06:37 WG938079
2-Chlorotoluene ND 0.00119 1 12/27/2016 06:37 WG938079
4-Chlorotoluene ND 0.00119 1 12/27/2016 06:37 WG938079
1,2-Dibromo-3-Chloropropane ND J3 0.00597 1 12/27/2016 06:37 WG938079
1,2-Dibromoethane ND J4 0.00119 1 12/27/2016 06:37 WG938079
Dibromomethane ND 0.00119 1 12/27/2016 06:37 WG938079
1,2-Dichlorobenzene ND 0.00119 1 12/27/2016 06:37 WG938079
1,3-Dichlorobenzene ND 0.00119 1 12/27/2016 06:37 WG938079
1,4-Dichlorobenzene ND J4 0.00119 1 12/27/2016 06:37 WG938079
Dichlorodifluoromethane ND 0.00597 1 12/27/2016 06:37 WG938079
1,1-Dichloroethane ND 0.00119 1 12/27/2016 06:37 WG938079
1,2-Dichloroethane ND 0.00119 1 12/27/2016 06:37 WG938079
1,1-Dichloroethene ND 0.00119 1 12/27/2016 06:37 WG938079
cis-1,2-Dichloroethene ND 0.00119 1 12/27/2016 06:37 WG938079
trans-1,2-Dichloroethene ND 0.00119 1 12/27/2016 06:37 WG938079
1,2-Dichloropropane ND 0.00119 1 12/27/2016 06:37 WG938079
1,1-Dichloropropene ND 0.00119 1 12/27/2016 06:37 WG938079
1,3-Dichloropropane ND J4 0.00119 1 12/27/2016 06:37 WG938079
cis-1,3-Dichloropropene ND 0.00119 1 12/27/2016 06:37 WG938079
trans-1,3-Dichloropropene ND 0.00119 1 12/27/2016 06:37 WG938079
2,2-Dichloropropane ND 0.00119 1 12/27/2016 06:37 WG938079
Di-isopropyl ether ND 0.00119 1 12/27/2016 06:37 WG938079
Ethylbenzene ND 0.00119 1 12/27/2016 06:37 WG938079
Hexachloro-1,3-butadiene ND 0.00119 1 12/27/2016 06:37 WG938079
Isopropylbenzene ND 0.00119 1 12/27/2016 06:37 WG938079
p-Isopropyltoluene ND 0.00119 1 12/27/2016 06:37 WG938079
2-Butanone (MEK)ND 0.0119 1 12/27/2016 06:37 WG938079
Methylene Chloride ND 0.00597 1 12/27/2016 06:37 WG938079
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 29
L880142
TP-10B
Collected date/time: 12/20/16 12:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
4-Methyl-2-pentanone (MIBK) ND J3 0.0119 1 12/27/2016 06:37 WG938079
Methyl tert-butyl ether ND 0.00119 1 12/27/2016 06:37 WG938079
Naphthalene ND 0.00597 1 12/27/2016 06:37 WG938079
n-Propylbenzene ND 0.00119 1 12/27/2016 06:37 WG938079
Styrene ND 0.00119 1 12/27/2016 06:37 WG938079
1,1,1,2-Tetrachloroethane ND 0.00119 1 12/27/2016 06:37 WG938079
1,1,2,2-Tetrachloroethane ND 0.00119 1 12/27/2016 06:37 WG938079
Tetrachloroethene ND 0.00119 1 12/27/2016 06:37 WG938079
Toluene ND 0.00597 1 12/27/2016 06:37 WG938079
1,2,3-Trichlorobenzene ND 0.00119 1 12/27/2016 06:37 WG938079
1,2,4-Trichlorobenzene ND 0.00119 1 12/27/2016 06:37 WG938079
1,1,1-Trichloroethane ND 0.00119 1 12/27/2016 06:37 WG938079
1,1,2-Trichloroethane ND 0.00119 1 12/27/2016 06:37 WG938079
1,1,2-Trichlorotrifluoroethane ND 0.00119 1 12/27/2016 06:37 WG938079
Trichloroethene ND 0.00119 1 12/27/2016 06:37 WG938079
Trichlorofluoromethane ND 0.00597 1 12/27/2016 06:37 WG938079
1,2,3-Trichloropropane ND J3 0.00298 1 12/27/2016 06:37 WG938079
1,2,4-Trimethylbenzene ND 0.00119 1 12/27/2016 06:37 WG938079
1,3,5-Trimethylbenzene ND 0.00119 1 12/27/2016 06:37 WG938079
Vinyl chloride ND 0.00119 1 12/27/2016 06:37 WG938079
Xylenes, Total ND 0.00358 1 12/27/2016 06:37 WG938079
(S) Toluene-d8 102 88.7-115 12/27/2016 06:37 WG938079
(S) Dibromofluoromethane 112 76.3-123 12/27/2016 06:37 WG938079
(S) 4-Bromofluorobenzene 99.4 69.7-129 12/27/2016 06:37 WG938079
Semi-Volatile Organic Compounds (GC) by Method 8015
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
TPH (GC/FID) High Fraction ND 4.78 1 12/23/2016 17:29 WG937731
(S) o-Terphenyl 57.0 50.0-150 12/23/2016 17:29 WG937731
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 30
L880142
MW-4
Collected date/time: 12/20/16 14:20
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ammonia Nitrogen ND 100 1 12/27/2016 16:24 WG938851
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Mercury ND 0.200 1 12/23/2016 10:54 WG937807
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Arsenic ND 10.0 1 12/23/2016 17:45 WG937757
Barium ND 5.00 1 12/23/2016 17:45 WG937757
Cadmium ND 2.00 1 12/23/2016 17:45 WG937757
Chromium ND 10.0 1 12/23/2016 17:45 WG937757
Lead ND 5.00 1 12/23/2016 17:45 WG937757
Selenium ND 10.0 1 12/23/2016 17:45 WG937757
Silver ND 5.00 1 12/23/2016 17:45 WG937757
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 12/28/2016 14:15 WG938472
Unadjusted C9-C12 Aliphatics ND 100 1 12/28/2016 14:15 WG938472
Unadjusted C9-C10 Aromatics ND 100 1 12/28/2016 14:15 WG938472
Total VPH ND 100 1 12/28/2016 14:15 WG938472
(S) 2,5-Dibromotoluene(FID) 82.1 70.0-130 12/28/2016 14:15 WG938472
(S) 2,5-Dibromotoluene(PID) 73.9 70.0-130 12/28/2016 14:15 WG938472
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/25/2016 21:03 WG938587
Acrolein ND J4 50.0 1 12/25/2016 21:03 WG938587
Acrylonitrile ND 10.0 1 12/25/2016 21:03 WG938587
Benzene ND 1.00 1 12/25/2016 21:03 WG938587
Bromobenzene ND 1.00 1 12/25/2016 21:03 WG938587
Bromodichloromethane ND 1.00 1 12/25/2016 21:03 WG938587
Bromoform ND 1.00 1 12/25/2016 21:03 WG938587
Bromomethane ND 5.00 1 12/25/2016 21:03 WG938587
n-Butylbenzene ND 1.00 1 12/25/2016 21:03 WG938587
sec-Butylbenzene 1.99 1.00 1 12/25/2016 21:03 WG938587
tert-Butylbenzene ND 1.00 1 12/25/2016 21:03 WG938587
Carbon tetrachloride ND 1.00 1 12/25/2016 21:03 WG938587
Chlorobenzene ND 1.00 1 12/25/2016 21:03 WG938587
Chlorodibromomethane ND 1.00 1 12/25/2016 21:03 WG938587
Chloroethane ND 5.00 1 12/25/2016 21:03 WG938587
2-Chloroethyl vinyl ether ND 50.0 1 12/25/2016 21:03 WG938587
Chloroform ND 5.00 1 12/25/2016 21:03 WG938587
Chloromethane ND J4 2.50 1 12/25/2016 21:03 WG938587
2-Chlorotoluene ND 1.00 1 12/25/2016 21:03 WG938587
4-Chlorotoluene ND 1.00 1 12/25/2016 21:03 WG938587
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/25/2016 21:03 WG938587
1,2-Dibromoethane ND 1.00 1 12/25/2016 21:03 WG938587
Dibromomethane ND 1.00 1 12/25/2016 21:03 WG938587
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 30
L880142
MW-4
Collected date/time: 12/20/16 14:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2-Dichlorobenzene ND 1.00 1 12/25/2016 21:03 WG938587
1,3-Dichlorobenzene ND 1.00 1 12/25/2016 21:03 WG938587
1,4-Dichlorobenzene ND 1.00 1 12/25/2016 21:03 WG938587
Dichlorodifluoromethane ND 5.00 1 12/25/2016 21:03 WG938587
1,1-Dichloroethane ND 1.00 1 12/25/2016 21:03 WG938587
1,2-Dichloroethane ND 1.00 1 12/25/2016 21:03 WG938587
1,1-Dichloroethene ND 1.00 1 12/25/2016 21:03 WG938587
cis-1,2-Dichloroethene ND 1.00 1 12/25/2016 21:03 WG938587
trans-1,2-Dichloroethene ND 1.00 1 12/25/2016 21:03 WG938587
1,2-Dichloropropane ND 1.00 1 12/25/2016 21:03 WG938587
1,1-Dichloropropene ND 1.00 1 12/25/2016 21:03 WG938587
1,3-Dichloropropane ND 1.00 1 12/25/2016 21:03 WG938587
cis-1,3-Dichloropropene ND 1.00 1 12/25/2016 21:03 WG938587
trans-1,3-Dichloropropene ND 1.00 1 12/25/2016 21:03 WG938587
2,2-Dichloropropane ND 1.00 1 12/25/2016 21:03 WG938587
Di-isopropyl ether ND 1.00 1 12/25/2016 21:03 WG938587
Ethylbenzene ND 1.00 1 12/25/2016 21:03 WG938587
Hexachloro-1,3-butadiene ND 1.00 1 12/25/2016 21:03 WG938587
Isopropylbenzene ND 1.00 1 12/25/2016 21:03 WG938587
p-Isopropyltoluene ND 1.00 1 12/25/2016 21:03 WG938587
2-Butanone (MEK)ND 10.0 1 12/25/2016 21:03 WG938587
Methylene Chloride ND 5.00 1 12/25/2016 21:03 WG938587
4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/25/2016 21:03 WG938587
Methyl tert-butyl ether ND 1.00 1 12/25/2016 21:03 WG938587
Naphthalene ND 5.00 1 12/25/2016 21:03 WG938587
n-Propylbenzene ND 1.00 1 12/25/2016 21:03 WG938587
Styrene ND 1.00 1 12/25/2016 21:03 WG938587
1,1,1,2-Tetrachloroethane ND 1.00 1 12/25/2016 21:03 WG938587
1,1,2,2-Tetrachloroethane ND 1.00 1 12/25/2016 21:03 WG938587
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/25/2016 21:03 WG938587
Tetrachloroethene ND 1.00 1 12/25/2016 21:03 WG938587
Toluene ND 1.00 1 12/25/2016 21:03 WG938587
1,2,3-Trichlorobenzene ND 1.00 1 12/25/2016 21:03 WG938587
1,2,4-Trichlorobenzene ND 1.00 1 12/25/2016 21:03 WG938587
1,1,1-Trichloroethane ND 1.00 1 12/25/2016 21:03 WG938587
1,1,2-Trichloroethane ND 1.00 1 12/25/2016 21:03 WG938587
Trichloroethene ND 1.00 1 12/25/2016 21:03 WG938587
Trichlorofluoromethane ND 5.00 1 12/25/2016 21:03 WG938587
1,2,3-Trichloropropane ND 2.50 1 12/25/2016 21:03 WG938587
1,2,4-Trimethylbenzene ND 1.00 1 12/25/2016 21:03 WG938587
1,2,3-Trimethylbenzene ND 1.00 1 12/25/2016 21:03 WG938587
1,3,5-Trimethylbenzene ND 1.00 1 12/25/2016 21:03 WG938587
Vinyl chloride ND 1.00 1 12/25/2016 21:03 WG938587
Xylenes, Total ND 3.00 1 12/25/2016 21:03 WG938587
(S) Toluene-d8 105 90.0-115 12/25/2016 21:03 WG938587
(S) Dibromofluoromethane 103 79.0-121 12/25/2016 21:03 WG938587
(S) 4-Bromofluorobenzene 100 80.1-120 12/25/2016 21:03 WG938587
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/22/2016 19:10 WG938055
Unadjusted C19-C36 Aliphatics ND 100 1 12/22/2016 19:10 WG938055
Unadjusted C11-C22 Aromatics 153 B 100 1 12/22/2016 20:59 WG938055
Unadjusted Total Petroleum Hydrocarbons 153 100 1 12/22/2016 19:10 WG938055
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 30
L880142
MW-4
Collected date/time: 12/20/16 14:20
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
(S) o-Terphenyl 72.7 40.0-140 12/22/2016 20:59 WG938055
(S) 1-Chloro-octadecane 57.8 40.0-140 12/22/2016 19:10 WG938055
(S) 2-Fluorobiphenyl 83.6 40.0-140 12/22/2016 20:59 WG938055
(S) 2-Bromonaphthalene 84.2 40.0-140 12/22/2016 20:59 WG938055
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene 1.04 1.00 1 12/27/2016 13:14 WG938069
Acenaphthylene ND 1.00 1 12/27/2016 13:14 WG938069
Anthracene ND 1.00 1 12/27/2016 13:14 WG938069
Benzidine ND 10.0 1 12/27/2016 13:14 WG938069
Benzo(a)anthracene ND 1.00 1 12/27/2016 13:14 WG938069
Benzo(b)fluoranthene ND 1.00 1 12/27/2016 13:14 WG938069
Benzo(k)fluoranthene ND 1.00 1 12/27/2016 13:14 WG938069
Benzo(g,h,i)perylene ND 1.00 1 12/27/2016 13:14 WG938069
Benzo(a)pyrene ND 1.00 1 12/27/2016 13:14 WG938069
Bis(2-chlorethoxy)methane ND 10.0 1 12/27/2016 13:14 WG938069
Bis(2-chloroethyl)ether ND 10.0 1 12/27/2016 13:14 WG938069
Bis(2-chloroisopropyl)ether ND 10.0 1 12/27/2016 13:14 WG938069
4-Bromophenyl-phenylether ND 10.0 1 12/27/2016 13:14 WG938069
2-Chloronaphthalene ND 1.00 1 12/27/2016 13:14 WG938069
4-Chlorophenyl-phenylether ND 10.0 1 12/27/2016 13:14 WG938069
Chrysene ND 1.00 1 12/27/2016 13:14 WG938069
Dibenz(a,h)anthracene ND 1.00 1 12/27/2016 13:14 WG938069
3,3-Dichlorobenzidine ND 10.0 1 12/27/2016 13:14 WG938069
2,4-Dinitrotoluene ND 10.0 1 12/27/2016 13:14 WG938069
2,6-Dinitrotoluene ND 10.0 1 12/27/2016 13:14 WG938069
Fluoranthene ND 1.00 1 12/27/2016 13:14 WG938069
Fluorene 1.34 1.00 1 12/27/2016 13:14 WG938069
Hexachlorobenzene ND 1.00 1 12/27/2016 13:14 WG938069
Hexachloro-1,3-butadiene ND 10.0 1 12/27/2016 13:14 WG938069
Hexachlorocyclopentadiene ND 10.0 1 12/27/2016 13:14 WG938069
Hexachloroethane ND 10.0 1 12/27/2016 13:14 WG938069
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/27/2016 13:14 WG938069
Isophorone ND 10.0 1 12/27/2016 13:14 WG938069
Naphthalene ND 1.00 1 12/27/2016 13:14 WG938069
Nitrobenzene ND 10.0 1 12/27/2016 13:14 WG938069
n-Nitrosodimethylamine ND 10.0 1 12/27/2016 13:14 WG938069
n-Nitrosodiphenylamine ND 10.0 1 12/27/2016 13:14 WG938069
n-Nitrosodi-n-propylamine ND 10.0 1 12/27/2016 13:14 WG938069
Phenanthrene 1.80 1.00 1 12/27/2016 13:14 WG938069
Benzylbutyl phthalate ND 3.00 1 12/27/2016 13:14 WG938069
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/27/2016 13:14 WG938069
Di-n-butyl phthalate ND 3.00 1 12/27/2016 13:14 WG938069
Diethyl phthalate ND 3.00 1 12/27/2016 13:14 WG938069
Dimethyl phthalate ND 3.00 1 12/27/2016 13:14 WG938069
Di-n-octyl phthalate ND 3.00 1 12/27/2016 13:14 WG938069
Pyrene ND 1.00 1 12/27/2016 13:14 WG938069
1,2,4-Trichlorobenzene ND 10.0 1 12/27/2016 13:14 WG938069
4-Chloro-3-methylphenol ND 10.0 1 12/27/2016 13:14 WG938069
2-Chlorophenol ND 10.0 1 12/27/2016 13:14 WG938069
2,4-Dichlorophenol ND 10.0 1 12/27/2016 13:14 WG938069
2,4-Dimethylphenol ND 10.0 1 12/27/2016 13:14 WG938069
4,6-Dinitro-2-methylphenol ND 10.0 1 12/27/2016 13:14 WG938069
2,4-Dinitrophenol ND 10.0 1 12/27/2016 13:14 WG938069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 30
L880142
MW-4
Collected date/time: 12/20/16 14:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Nitrophenol ND 10.0 1 12/27/2016 13:14 WG938069
4-Nitrophenol ND 10.0 1 12/27/2016 13:14 WG938069
Pentachlorophenol ND 10.0 1 12/27/2016 13:14 WG938069
Phenol ND 10.0 1 12/27/2016 13:14 WG938069
2,4,6-Trichlorophenol ND 10.0 1 12/27/2016 13:14 WG938069
(S) 2-Fluorophenol 24.4 10.0-77.9 12/27/2016 13:14 WG938069
(S) Phenol-d5 19.1 5.00-70.1 12/27/2016 13:14 WG938069
(S) Nitrobenzene-d5 32.5 21.8-123 12/27/2016 13:14 WG938069
(S) 2-Fluorobiphenyl 46.7 29.5-131 12/27/2016 13:14 WG938069
(S) 2,4,6-Tribromophenol 91.2 11.2-130 12/27/2016 13:14 WG938069
(S) p-Terphenyl-d14 90.9 29.3-137 12/27/2016 13:14 WG938069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 31
L880142
MW-2
Collected date/time: 12/20/16 14:15
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ammonia Nitrogen ND 100 1 12/27/2016 16:26 WG938851
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Mercury ND 0.200 1 12/23/2016 10:57 WG937807
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Arsenic ND 10.0 1 12/23/2016 17:48 WG937757
Barium 10.5 5.00 1 12/23/2016 17:48 WG937757
Cadmium ND 2.00 1 12/23/2016 17:48 WG937757
Chromium ND 10.0 1 12/23/2016 17:48 WG937757
Lead ND 5.00 1 12/23/2016 17:48 WG937757
Selenium ND 10.0 1 12/23/2016 17:48 WG937757
Silver ND 5.00 1 12/23/2016 17:48 WG937757
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 12/28/2016 14:47 WG938472
Unadjusted C9-C12 Aliphatics ND 100 1 12/28/2016 14:47 WG938472
Unadjusted C9-C10 Aromatics ND 100 1 12/28/2016 14:47 WG938472
Total VPH ND 100 1 12/28/2016 14:47 WG938472
(S) 2,5-Dibromotoluene(FID) 84.1 70.0-130 12/28/2016 14:47 WG938472
(S) 2,5-Dibromotoluene(PID) 76.2 70.0-130 12/28/2016 14:47 WG938472
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/25/2016 21:26 WG938587
Acrolein ND J4 50.0 1 12/25/2016 21:26 WG938587
Acrylonitrile ND 10.0 1 12/25/2016 21:26 WG938587
Benzene ND 1.00 1 12/25/2016 21:26 WG938587
Bromobenzene ND 1.00 1 12/25/2016 21:26 WG938587
Bromodichloromethane ND 1.00 1 12/25/2016 21:26 WG938587
Bromoform ND 1.00 1 12/25/2016 21:26 WG938587
Bromomethane ND 5.00 1 12/25/2016 21:26 WG938587
n-Butylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
sec-Butylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
tert-Butylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
Carbon tetrachloride ND 1.00 1 12/25/2016 21:26 WG938587
Chlorobenzene ND 1.00 1 12/25/2016 21:26 WG938587
Chlorodibromomethane ND 1.00 1 12/25/2016 21:26 WG938587
Chloroethane ND 5.00 1 12/25/2016 21:26 WG938587
2-Chloroethyl vinyl ether ND 50.0 1 12/25/2016 21:26 WG938587
Chloroform ND 5.00 1 12/25/2016 21:26 WG938587
Chloromethane ND J4 2.50 1 12/25/2016 21:26 WG938587
2-Chlorotoluene ND 1.00 1 12/25/2016 21:26 WG938587
4-Chlorotoluene ND 1.00 1 12/25/2016 21:26 WG938587
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/25/2016 21:26 WG938587
1,2-Dibromoethane ND 1.00 1 12/25/2016 21:26 WG938587
Dibromomethane ND 1.00 1 12/25/2016 21:26 WG938587
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 31
L880142
MW-2
Collected date/time: 12/20/16 14:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2-Dichlorobenzene ND 1.00 1 12/25/2016 21:26 WG938587
1,3-Dichlorobenzene ND 1.00 1 12/25/2016 21:26 WG938587
1,4-Dichlorobenzene ND 1.00 1 12/25/2016 21:26 WG938587
Dichlorodifluoromethane ND 5.00 1 12/25/2016 21:26 WG938587
1,1-Dichloroethane ND 1.00 1 12/25/2016 21:26 WG938587
1,2-Dichloroethane ND 1.00 1 12/25/2016 21:26 WG938587
1,1-Dichloroethene ND 1.00 1 12/25/2016 21:26 WG938587
cis-1,2-Dichloroethene ND 1.00 1 12/25/2016 21:26 WG938587
trans-1,2-Dichloroethene ND 1.00 1 12/25/2016 21:26 WG938587
1,2-Dichloropropane ND 1.00 1 12/25/2016 21:26 WG938587
1,1-Dichloropropene ND 1.00 1 12/25/2016 21:26 WG938587
1,3-Dichloropropane ND 1.00 1 12/25/2016 21:26 WG938587
cis-1,3-Dichloropropene ND 1.00 1 12/25/2016 21:26 WG938587
trans-1,3-Dichloropropene ND 1.00 1 12/25/2016 21:26 WG938587
2,2-Dichloropropane ND 1.00 1 12/25/2016 21:26 WG938587
Di-isopropyl ether ND 1.00 1 12/25/2016 21:26 WG938587
Ethylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
Hexachloro-1,3-butadiene ND 1.00 1 12/25/2016 21:26 WG938587
Isopropylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
p-Isopropyltoluene ND 1.00 1 12/25/2016 21:26 WG938587
2-Butanone (MEK)ND 10.0 1 12/25/2016 21:26 WG938587
Methylene Chloride ND 5.00 1 12/25/2016 21:26 WG938587
4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/25/2016 21:26 WG938587
Methyl tert-butyl ether ND 1.00 1 12/25/2016 21:26 WG938587
Naphthalene ND 5.00 1 12/25/2016 21:26 WG938587
n-Propylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
Styrene ND 1.00 1 12/25/2016 21:26 WG938587
1,1,1,2-Tetrachloroethane ND 1.00 1 12/25/2016 21:26 WG938587
1,1,2,2-Tetrachloroethane ND 1.00 1 12/25/2016 21:26 WG938587
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/25/2016 21:26 WG938587
Tetrachloroethene ND 1.00 1 12/25/2016 21:26 WG938587
Toluene ND 1.00 1 12/25/2016 21:26 WG938587
1,2,3-Trichlorobenzene ND 1.00 1 12/25/2016 21:26 WG938587
1,2,4-Trichlorobenzene ND 1.00 1 12/25/2016 21:26 WG938587
1,1,1-Trichloroethane ND 1.00 1 12/25/2016 21:26 WG938587
1,1,2-Trichloroethane ND 1.00 1 12/25/2016 21:26 WG938587
Trichloroethene ND 1.00 1 12/25/2016 21:26 WG938587
Trichlorofluoromethane ND 5.00 1 12/25/2016 21:26 WG938587
1,2,3-Trichloropropane ND 2.50 1 12/25/2016 21:26 WG938587
1,2,4-Trimethylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
1,2,3-Trimethylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
1,3,5-Trimethylbenzene ND 1.00 1 12/25/2016 21:26 WG938587
Vinyl chloride ND 1.00 1 12/25/2016 21:26 WG938587
Xylenes, Total ND 3.00 1 12/25/2016 21:26 WG938587
(S) Toluene-d8 104 90.0-115 12/25/2016 21:26 WG938587
(S) Dibromofluoromethane 104 79.0-121 12/25/2016 21:26 WG938587
(S) 4-Bromofluorobenzene 98.8 80.1-120 12/25/2016 21:26 WG938587
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/22/2016 19:32 WG938055
Unadjusted C19-C36 Aliphatics ND 100 1 12/22/2016 19:32 WG938055
Unadjusted C11-C22 Aromatics ND 100 1 12/22/2016 20:37 WG938055
Unadjusted Total Petroleum Hydrocarbons ND 100 1 12/22/2016 19:32 WG938055
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 31
L880142
MW-2
Collected date/time: 12/20/16 14:15
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
(S) o-Terphenyl 73.1 40.0-140 12/22/2016 20:37 WG938055
(S) 1-Chloro-octadecane 54.5 40.0-140 12/22/2016 19:32 WG938055
(S) 2-Fluorobiphenyl 83.6 40.0-140 12/22/2016 20:37 WG938055
(S) 2-Bromonaphthalene 82.8 40.0-140 12/22/2016 20:37 WG938055
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 12/27/2016 13:38 WG938069
Acenaphthylene ND 1.00 1 12/27/2016 13:38 WG938069
Anthracene ND 1.00 1 12/27/2016 13:38 WG938069
Benzidine ND 10.0 1 12/27/2016 13:38 WG938069
Benzo(a)anthracene ND 1.00 1 12/27/2016 13:38 WG938069
Benzo(b)fluoranthene ND 1.00 1 12/27/2016 13:38 WG938069
Benzo(k)fluoranthene ND 1.00 1 12/27/2016 13:38 WG938069
Benzo(g,h,i)perylene ND 1.00 1 12/27/2016 13:38 WG938069
Benzo(a)pyrene ND 1.00 1 12/27/2016 13:38 WG938069
Bis(2-chlorethoxy)methane ND 10.0 1 12/27/2016 13:38 WG938069
Bis(2-chloroethyl)ether ND 10.0 1 12/27/2016 13:38 WG938069
Bis(2-chloroisopropyl)ether ND 10.0 1 12/27/2016 13:38 WG938069
4-Bromophenyl-phenylether ND 10.0 1 12/27/2016 13:38 WG938069
2-Chloronaphthalene ND 1.00 1 12/27/2016 13:38 WG938069
4-Chlorophenyl-phenylether ND 10.0 1 12/27/2016 13:38 WG938069
Chrysene ND 1.00 1 12/27/2016 13:38 WG938069
Dibenz(a,h)anthracene ND 1.00 1 12/27/2016 13:38 WG938069
3,3-Dichlorobenzidine ND 10.0 1 12/27/2016 13:38 WG938069
2,4-Dinitrotoluene ND 10.0 1 12/27/2016 13:38 WG938069
2,6-Dinitrotoluene ND 10.0 1 12/27/2016 13:38 WG938069
Fluoranthene ND 1.00 1 12/27/2016 13:38 WG938069
Fluorene ND 1.00 1 12/27/2016 13:38 WG938069
Hexachlorobenzene ND 1.00 1 12/27/2016 13:38 WG938069
Hexachloro-1,3-butadiene ND 10.0 1 12/27/2016 13:38 WG938069
Hexachlorocyclopentadiene ND 10.0 1 12/27/2016 13:38 WG938069
Hexachloroethane ND 10.0 1 12/27/2016 13:38 WG938069
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/27/2016 13:38 WG938069
Isophorone ND 10.0 1 12/27/2016 13:38 WG938069
Naphthalene ND 1.00 1 12/27/2016 13:38 WG938069
Nitrobenzene ND 10.0 1 12/27/2016 13:38 WG938069
n-Nitrosodimethylamine ND 10.0 1 12/27/2016 13:38 WG938069
n-Nitrosodiphenylamine ND 10.0 1 12/27/2016 13:38 WG938069
n-Nitrosodi-n-propylamine ND 10.0 1 12/27/2016 13:38 WG938069
Phenanthrene ND 1.00 1 12/27/2016 13:38 WG938069
Benzylbutyl phthalate ND 3.00 1 12/27/2016 13:38 WG938069
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/27/2016 13:38 WG938069
Di-n-butyl phthalate ND 3.00 1 12/27/2016 13:38 WG938069
Diethyl phthalate ND 3.00 1 12/27/2016 13:38 WG938069
Dimethyl phthalate ND 3.00 1 12/27/2016 13:38 WG938069
Di-n-octyl phthalate ND 3.00 1 12/27/2016 13:38 WG938069
Pyrene ND 1.00 1 12/27/2016 13:38 WG938069
1,2,4-Trichlorobenzene ND 10.0 1 12/27/2016 13:38 WG938069
4-Chloro-3-methylphenol ND 10.0 1 12/27/2016 13:38 WG938069
2-Chlorophenol ND 10.0 1 12/27/2016 13:38 WG938069
2,4-Dichlorophenol ND 10.0 1 12/27/2016 13:38 WG938069
2,4-Dimethylphenol ND 10.0 1 12/27/2016 13:38 WG938069
4,6-Dinitro-2-methylphenol ND 10.0 1 12/27/2016 13:38 WG938069
2,4-Dinitrophenol ND 10.0 1 12/27/2016 13:38 WG938069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 31
L880142
MW-2
Collected date/time: 12/20/16 14:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Nitrophenol ND 10.0 1 12/27/2016 13:38 WG938069
4-Nitrophenol ND 10.0 1 12/27/2016 13:38 WG938069
Pentachlorophenol ND 10.0 1 12/27/2016 13:38 WG938069
Phenol ND 10.0 1 12/27/2016 13:38 WG938069
2,4,6-Trichlorophenol ND 10.0 1 12/27/2016 13:38 WG938069
(S) 2-Fluorophenol 45.8 10.0-77.9 12/27/2016 13:38 WG938069
(S) Phenol-d5 30.5 5.00-70.1 12/27/2016 13:38 WG938069
(S) Nitrobenzene-d5 55.1 21.8-123 12/27/2016 13:38 WG938069
(S) 2-Fluorobiphenyl 64.1 29.5-131 12/27/2016 13:38 WG938069
(S) 2,4,6-Tribromophenol 82.4 11.2-130 12/27/2016 13:38 WG938069
(S) p-Terphenyl-d14 89.9 29.3-137 12/27/2016 13:38 WG938069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 32
L880142
MW-5
Collected date/time: 12/20/16 15:50
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ammonia Nitrogen ND 100 1 12/28/2016 11:08 WG938852
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Mercury ND 0.200 1 12/23/2016 10:59 WG937807
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Arsenic ND 10.0 1 12/23/2016 17:51 WG937757
Barium 22.8 5.00 1 12/23/2016 17:51 WG937757
Cadmium ND 2.00 1 12/23/2016 17:51 WG937757
Chromium ND 10.0 1 12/23/2016 17:51 WG937757
Lead ND 5.00 1 12/23/2016 17:51 WG937757
Selenium ND 10.0 1 12/23/2016 17:51 WG937757
Silver ND 5.00 1 12/23/2016 17:51 WG937757
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 12/28/2016 15:20 WG938472
Unadjusted C9-C12 Aliphatics ND 100 1 12/28/2016 15:20 WG938472
Unadjusted C9-C10 Aromatics ND 100 1 12/28/2016 15:20 WG938472
Total VPH ND 100 1 12/28/2016 15:20 WG938472
(S) 2,5-Dibromotoluene(FID) 84.7 70.0-130 12/28/2016 15:20 WG938472
(S) 2,5-Dibromotoluene(PID) 77.4 70.0-130 12/28/2016 15:20 WG938472
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/25/2016 21:50 WG938587
Acrolein ND J4 50.0 1 12/25/2016 21:50 WG938587
Acrylonitrile ND 10.0 1 12/25/2016 21:50 WG938587
Benzene ND 1.00 1 12/25/2016 21:50 WG938587
Bromobenzene ND 1.00 1 12/25/2016 21:50 WG938587
Bromodichloromethane ND 1.00 1 12/25/2016 21:50 WG938587
Bromoform ND 1.00 1 12/25/2016 21:50 WG938587
Bromomethane ND 5.00 1 12/25/2016 21:50 WG938587
n-Butylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
sec-Butylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
tert-Butylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
Carbon tetrachloride ND 1.00 1 12/25/2016 21:50 WG938587
Chlorobenzene ND 1.00 1 12/25/2016 21:50 WG938587
Chlorodibromomethane ND 1.00 1 12/25/2016 21:50 WG938587
Chloroethane ND 5.00 1 12/25/2016 21:50 WG938587
2-Chloroethyl vinyl ether ND 50.0 1 12/25/2016 21:50 WG938587
Chloroform 204 25.0 5 12/28/2016 21:49 WG938587
Chloromethane ND J4 2.50 1 12/25/2016 21:50 WG938587
2-Chlorotoluene ND 1.00 1 12/25/2016 21:50 WG938587
4-Chlorotoluene ND 1.00 1 12/25/2016 21:50 WG938587
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/25/2016 21:50 WG938587
1,2-Dibromoethane ND 1.00 1 12/25/2016 21:50 WG938587
Dibromomethane ND 1.00 1 12/25/2016 21:50 WG938587
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 32
L880142
MW-5
Collected date/time: 12/20/16 15:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,2-Dichlorobenzene ND 1.00 1 12/25/2016 21:50 WG938587
1,3-Dichlorobenzene ND 1.00 1 12/25/2016 21:50 WG938587
1,4-Dichlorobenzene ND 1.00 1 12/25/2016 21:50 WG938587
Dichlorodifluoromethane ND 5.00 1 12/25/2016 21:50 WG938587
1,1-Dichloroethane ND 1.00 1 12/25/2016 21:50 WG938587
1,2-Dichloroethane ND 1.00 1 12/25/2016 21:50 WG938587
1,1-Dichloroethene ND 1.00 1 12/25/2016 21:50 WG938587
cis-1,2-Dichloroethene ND 1.00 1 12/25/2016 21:50 WG938587
trans-1,2-Dichloroethene ND 1.00 1 12/25/2016 21:50 WG938587
1,2-Dichloropropane ND 1.00 1 12/25/2016 21:50 WG938587
1,1-Dichloropropene ND 1.00 1 12/25/2016 21:50 WG938587
1,3-Dichloropropane ND 1.00 1 12/25/2016 21:50 WG938587
cis-1,3-Dichloropropene ND 1.00 1 12/25/2016 21:50 WG938587
trans-1,3-Dichloropropene ND 1.00 1 12/25/2016 21:50 WG938587
2,2-Dichloropropane ND 1.00 1 12/25/2016 21:50 WG938587
Di-isopropyl ether ND 1.00 1 12/25/2016 21:50 WG938587
Ethylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
Hexachloro-1,3-butadiene ND 1.00 1 12/25/2016 21:50 WG938587
Isopropylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
p-Isopropyltoluene ND 1.00 1 12/25/2016 21:50 WG938587
2-Butanone (MEK)ND 10.0 1 12/25/2016 21:50 WG938587
Methylene Chloride ND 5.00 1 12/25/2016 21:50 WG938587
4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/25/2016 21:50 WG938587
Methyl tert-butyl ether ND 1.00 1 12/25/2016 21:50 WG938587
Naphthalene ND 5.00 1 12/25/2016 21:50 WG938587
n-Propylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
Styrene ND 1.00 1 12/25/2016 21:50 WG938587
1,1,1,2-Tetrachloroethane ND 1.00 1 12/25/2016 21:50 WG938587
1,1,2,2-Tetrachloroethane ND 1.00 1 12/25/2016 21:50 WG938587
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/25/2016 21:50 WG938587
Tetrachloroethene ND 1.00 1 12/25/2016 21:50 WG938587
Toluene ND 1.00 1 12/25/2016 21:50 WG938587
1,2,3-Trichlorobenzene ND 1.00 1 12/25/2016 21:50 WG938587
1,2,4-Trichlorobenzene ND 1.00 1 12/25/2016 21:50 WG938587
1,1,1-Trichloroethane ND 1.00 1 12/25/2016 21:50 WG938587
1,1,2-Trichloroethane ND 1.00 1 12/25/2016 21:50 WG938587
Trichloroethene ND 1.00 1 12/25/2016 21:50 WG938587
Trichlorofluoromethane ND 5.00 1 12/25/2016 21:50 WG938587
1,2,3-Trichloropropane ND 2.50 1 12/25/2016 21:50 WG938587
1,2,4-Trimethylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
1,2,3-Trimethylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
1,3,5-Trimethylbenzene ND 1.00 1 12/25/2016 21:50 WG938587
Vinyl chloride ND 1.00 1 12/25/2016 21:50 WG938587
Xylenes, Total ND 3.00 1 12/25/2016 21:50 WG938587
(S) Toluene-d8 105 90.0-115 12/25/2016 21:50 WG938587
(S) Toluene-d8 106 90.0-115 12/28/2016 21:49 WG938587
(S) Dibromofluoromethane 105 79.0-121 12/28/2016 21:49 WG938587
(S) Dibromofluoromethane 106 79.0-121 12/25/2016 21:50 WG938587
(S) 4-Bromofluorobenzene 101 80.1-120 12/25/2016 21:50 WG938587
(S) 4-Bromofluorobenzene 120 80.1-120 12/28/2016 21:49 WG938587
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 32
L880142
MW-5
Collected date/time: 12/20/16 15:50
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/22/2016 19:54 WG938055
Unadjusted C19-C36 Aliphatics ND 100 1 12/22/2016 19:54 WG938055
Unadjusted C11-C22 Aromatics ND 100 1 12/22/2016 20:16 WG938055
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 12/22/2016 19:54 WG938055
(S) o-Terphenyl 61.5 40.0-140 12/22/2016 20:16 WG938055
(S) 1-Chloro-octadecane 44.1 40.0-140 12/22/2016 19:54 WG938055
(S) 2-Fluorobiphenyl 87.7 40.0-140 12/22/2016 20:16 WG938055
(S) 2-Bromonaphthalene 87.4 40.0-140 12/22/2016 20:16 WG938055
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 12/27/2016 14:02 WG938069
Acenaphthylene ND 1.00 1 12/27/2016 14:02 WG938069
Anthracene ND 1.00 1 12/27/2016 14:02 WG938069
Benzidine ND 10.0 1 12/27/2016 14:02 WG938069
Benzo(a)anthracene ND 1.00 1 12/27/2016 14:02 WG938069
Benzo(b)fluoranthene ND 1.00 1 12/27/2016 14:02 WG938069
Benzo(k)fluoranthene ND 1.00 1 12/27/2016 14:02 WG938069
Benzo(g,h,i)perylene ND 1.00 1 12/27/2016 14:02 WG938069
Benzo(a)pyrene ND 1.00 1 12/27/2016 14:02 WG938069
Bis(2-chlorethoxy)methane ND 10.0 1 12/27/2016 14:02 WG938069
Bis(2-chloroethyl)ether ND 10.0 1 12/27/2016 14:02 WG938069
Bis(2-chloroisopropyl)ether ND 10.0 1 12/27/2016 14:02 WG938069
4-Bromophenyl-phenylether ND 10.0 1 12/27/2016 14:02 WG938069
2-Chloronaphthalene ND 1.00 1 12/27/2016 14:02 WG938069
4-Chlorophenyl-phenylether ND 10.0 1 12/27/2016 14:02 WG938069
Chrysene ND 1.00 1 12/27/2016 14:02 WG938069
Dibenz(a,h)anthracene ND 1.00 1 12/27/2016 14:02 WG938069
3,3-Dichlorobenzidine ND 10.0 1 12/27/2016 14:02 WG938069
2,4-Dinitrotoluene ND 10.0 1 12/27/2016 14:02 WG938069
2,6-Dinitrotoluene ND 10.0 1 12/27/2016 14:02 WG938069
Fluoranthene ND 1.00 1 12/27/2016 14:02 WG938069
Fluorene ND 1.00 1 12/27/2016 14:02 WG938069
Hexachlorobenzene ND 1.00 1 12/27/2016 14:02 WG938069
Hexachloro-1,3-butadiene ND 10.0 1 12/27/2016 14:02 WG938069
Hexachlorocyclopentadiene ND 10.0 1 12/27/2016 14:02 WG938069
Hexachloroethane ND 10.0 1 12/27/2016 14:02 WG938069
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/27/2016 14:02 WG938069
Isophorone ND 10.0 1 12/27/2016 14:02 WG938069
Naphthalene ND 1.00 1 12/27/2016 14:02 WG938069
Nitrobenzene ND 10.0 1 12/27/2016 14:02 WG938069
n-Nitrosodimethylamine ND 10.0 1 12/27/2016 14:02 WG938069
n-Nitrosodiphenylamine ND 10.0 1 12/27/2016 14:02 WG938069
n-Nitrosodi-n-propylamine ND 10.0 1 12/27/2016 14:02 WG938069
Phenanthrene ND 1.00 1 12/27/2016 14:02 WG938069
Benzylbutyl phthalate ND 3.00 1 12/27/2016 14:02 WG938069
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/27/2016 14:02 WG938069
Di-n-butyl phthalate ND 3.00 1 12/27/2016 14:02 WG938069
Diethyl phthalate ND 3.00 1 12/27/2016 14:02 WG938069
Dimethyl phthalate ND 3.00 1 12/27/2016 14:02 WG938069
Di-n-octyl phthalate ND 3.00 1 12/27/2016 14:02 WG938069
Pyrene ND 1.00 1 12/27/2016 14:02 WG938069
1,2,4-Trichlorobenzene ND 10.0 1 12/27/2016 14:02 WG938069
4-Chloro-3-methylphenol ND 10.0 1 12/27/2016 14:02 WG938069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 32
L880142
MW-5
Collected date/time: 12/20/16 15:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Chlorophenol ND 10.0 1 12/27/2016 14:02 WG938069
2,4-Dichlorophenol ND 10.0 1 12/27/2016 14:02 WG938069
2,4-Dimethylphenol ND 10.0 1 12/27/2016 14:02 WG938069
4,6-Dinitro-2-methylphenol ND 10.0 1 12/27/2016 14:02 WG938069
2,4-Dinitrophenol ND 10.0 1 12/27/2016 14:02 WG938069
2-Nitrophenol ND 10.0 1 12/27/2016 14:02 WG938069
4-Nitrophenol ND 10.0 1 12/27/2016 14:02 WG938069
Pentachlorophenol ND 10.0 1 12/27/2016 14:02 WG938069
Phenol ND 10.0 1 12/27/2016 14:02 WG938069
2,4,6-Trichlorophenol ND 10.0 1 12/27/2016 14:02 WG938069
(S) 2-Fluorophenol 44.0 10.0-77.9 12/27/2016 14:02 WG938069
(S) Phenol-d5 30.6 5.00-70.1 12/27/2016 14:02 WG938069
(S) Nitrobenzene-d5 51.3 21.8-123 12/27/2016 14:02 WG938069
(S) 2-Fluorobiphenyl 66.7 29.5-131 12/27/2016 14:02 WG938069
(S) 2,4,6-Tribromophenol 96.8 11.2-130 12/27/2016 14:02 WG938069
(S) p-Terphenyl-d14 91.8 29.3-137 12/27/2016 14:02 WG938069
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG937880
Total Solids by Method 2540 G-2011 L880142-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3186873-1 12/22/16 11:27
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000100
L880142-08 Original Sample (OS) • Duplicate (DUP)
(OS) L880142-08 12/22/16 11:27 • (DUP) R3186873-3 12/22/16 11:27
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 72.2 70.7 1 2.20 5
Laboratory Control Sample (LCS)
(LCS) R3186873-2 12/22/16 11:27
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG937881
Total Solids by Method 2540 G-2011 L880142-09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R3186872-1 12/22/16 11:14
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000200
L880142-09 Original Sample (OS) • Duplicate (DUP)
(OS) L880142-09 12/22/16 11:14 • (DUP) R3186872-3 12/22/16 11:14
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 72.8 73.0 1 0.194 5
Laboratory Control Sample (LCS)
(LCS) R3186872-2 12/22/16 11:14
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG937882
Total Solids by Method 2540 G-2011 L880142-19,20,21,22,23,24,25,26,27,28
Method Blank (MB)
(MB) R3186871-1 12/22/16 11:00
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000300
L880142-28 Original Sample (OS) • Duplicate (DUP)
(OS) L880142-28 12/22/16 11:00 • (DUP) R3186871-3 12/22/16 11:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 80.3 81.1 1 0.986 5
Laboratory Control Sample (LCS)
(LCS) R3186871-2 12/22/16 11:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG937884
Total Solids by Method 2540 G-2011 L880142-29
Method Blank (MB)
(MB) R3187294-1 12/23/16 13:23
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000900
L880142-29 Original Sample (OS) • Duplicate (DUP)
(OS) L880142-29 12/23/16 13:23 • (DUP) R3187294-3 12/23/16 13:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 83.8 80.7 1 3.69 5
Laboratory Control Sample (LCS)
(LCS) R3187294-2 12/23/16 13:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938851
Wet Chemistry by Method 350.1 L880142-30,31
Method Blank (MB)
(MB) R3187478-1 12/27/16 15:27
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ammonia Nitrogen U 31.7 100
L880045-05 Original Sample (OS) • Duplicate (DUP)
(OS) L880045-05 12/27/16 15:35 • (DUP) R3187478-4 12/27/16 15:37
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte ug/l ug/l %%
Ammonia Nitrogen 2340 2320 1 1 20
L880045-14 Original Sample (OS) • Duplicate (DUP)
(OS) L880045-14 12/27/16 15:57 • (DUP) R3187478-6 12/27/16 16:04
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte ug/l ug/l %%
Ammonia Nitrogen ND 0.000 1 0 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187478-2 12/27/16 15:29 • (LCSD) R3187478-3 12/27/16 15:30
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ammonia Nitrogen 7500 7020 7110 94 95 90-110 1 20
L880045-06 Original Sample (OS) • Matrix Spike (MS)
(OS) L880045-06 12/27/16 15:38 • (MS) R3187478-5 12/27/16 15:40
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ammonia Nitrogen 10000 5910 15600 97 1 90-110
L880135-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880135-01 12/27/16 16:15 • (MS) R3187478-7 12/27/16 16:21 • (MSD) R3187478-8 12/27/16 16:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Ammonia Nitrogen 10000 ND 9560 9590 96 96 1 90-110 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938852
Wet Chemistry by Method 350.1 L880142-32
Method Blank (MB)
(MB) R3187733-1 12/28/16 11:01
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ammonia Nitrogen U 31.7 100
L880143-01 Original Sample (OS) • Duplicate (DUP)
(OS) L880143-01 12/28/16 11:09 • (DUP) R3187733-4 12/28/16 11:11
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte ug/l ug/l %%
Ammonia Nitrogen ND 0.000 1 0 20
L880157-01 Original Sample (OS) • Duplicate (DUP)
(OS) L880157-01 12/28/16 11:24 • (DUP) R3187733-6 12/28/16 11:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte ug/l ug/l %%
Ammonia Nitrogen ND 0.000 1 0 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187733-2 12/28/16 11:03 • (LCSD) R3187733-3 12/28/16 11:05
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ammonia Nitrogen 7500 7260 7330 97 98 90-110 1 20
L880146-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L880146-01 12/28/16 11:12 • (MS) R3187733-5 12/28/16 11:14
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ammonia Nitrogen 10000 ND 10400 104 1 90-110
L880169-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880169-01 12/28/16 11:27 • (MS) R3187733-7 12/28/16 11:28 • (MSD) R3187733-8 12/28/16 11:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Ammonia Nitrogen 10000 ND 10100 10200 101 102 1 90-110 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG937807
Mercury by Method 7470A L880142-30,31,32
Method Blank (MB)
(MB) R3186983-1 12/23/16 10:03
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.0490 0.200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3186983-2 12/23/16 10:11 • (LCSD) R3186983-3 12/23/16 10:14
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Mercury 3.00 2.69 2.93 90 98 80-120 9 20
L880135-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880135-01 12/23/16 10:16 • (MS) R3186983-4 12/23/16 10:19 • (MSD) R3186983-5 12/23/16 10:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 ND 3.03 2.98 101 99 1 75-125 2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG937757
Metals (ICP) by Method 6010C L880142-30,31,32
Method Blank (MB)
(MB) R3187254-1 12/23/16 17:04
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Arsenic U 6.50 10.0
Barium U 1.70 5.00
Cadmium U 0.700 2.00
Chromium U 1.40 10.0
Lead U 1.90 5.00
Selenium U 7.40 10.0
Silver U 2.80 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187254-2 12/23/16 17:07 • (LCSD) R3187254-3 12/23/16 17:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Arsenic 1000 982 984 98 98 80-120 0 20
Barium 1000 1010 1010 101 101 80-120 0 20
Cadmium 1000 997 1000 100 100 80-120 0 20
Chromium 1000 1000 1010 100 101 80-120 1 20
Lead 1000 1010 1010 101 101 80-120 0 20
Selenium 1000 1000 1000 100 100 80-120 0 20
Silver 200 177 179 89 89 80-120 1 20
L880080-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880080-08 12/23/16 17:12 • (MS) R3187254-5 12/23/16 17:18 • (MSD) R3187254-6 12/23/16 17:20
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 1000 ND 1060 1050 106 105 1 75-125 1 20
Barium 1000 6.23 1010 999 101 99 1 75-125 1 20
Cadmium 1000 ND 1060 1050 106 105 1 75-125 1 20
Chromium 1000 13.9 1020 1010 101 99 1 75-125 2 20
Lead 1000 6.15 1040 1030 104 103 1 75-125 1 20
Selenium 1000 ND 1090 1080 109 108 1 75-125 1 20
Silver 200 ND 195 192 97 96 1 75-125 2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 100 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938472
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH L880142-30,31,32
Method Blank (MB)
(MB) R3187959-3 12/28/16 12:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID) 83.6 70.0-130
(S) 2,5-Dibromotoluene(PID) 75.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187959-1 12/28/16 11:14 • (LCSD) R3187959-2 12/28/16 11:46
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1240 1200 104 99.6 70.0-130 4.02 25
Unadjusted C9-C12 Aliphatics 1400 1600 1560 114 112 70.0-130 2.50 25
Unadjusted C9-C10 Aromatics 200 184 179 91.9 89.6 70.0-130 2.64 25
Total VPH 2800 3030 2940 108 105 70.0-130 3.13 25
(S) 2,5-Dibromotoluene(FID)82.2 82.5 70.0-130
(S) 2,5-Dibromotoluene(PID)73.4 73.9 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938086
Volatile Organic Compounds (GC) by Method 8015D/GRO L880142-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R3187459-3 12/23/16 23:58
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.0414 J 0.0217 0.100
(S) a,a,a-Trifluorotoluene(FID) 96.1 59.0-128
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187459-1 12/23/16 22:52 • (LCSD) R3187459-2 12/23/16 23:14
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.50 5.81 5.93 106 108 63.5-137 2.13 20
(S) a,a,a-Trifluorotoluene(FID)102 103 59.0-128
L880079-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880079-01 12/24/16 02:03 • (MS) R3187459-4 12/24/16 00:56 • (MSD) R3187459-5 12/24/16 01:18
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 11.4 ND 118 118 43.3 43.2 23.5 28.5-138 0.330 23.6
(S) a,a,a-Trifluorotoluene(FID)97.3 98.1 59.0-128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938087
Volatile Organic Compounds (GC) by Method 8015D/GRO L880142-19,20,21,22,23,24,25,26,27,28,29
Method Blank (MB)
(MB) R3187958-3 12/28/16 12:07
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.0217 0.100
(S) a,a,a-Trifluorotoluene(FID) 99.8 59.0-128
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187958-1 12/28/16 10:34 • (LCSD) R3187958-2 12/28/16 11:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.50 5.15 5.44 93.7 98.9 63.5-137 5.46 20
(S) a,a,a-Trifluorotoluene(FID)99.3 99.2 59.0-128
L880252-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880252-01 12/28/16 20:52 • (MS) R3187958-4 12/28/16 13:09 • (MSD) R3187958-5 12/28/16 13:38
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 5.50 ND 3.86 3.90 70.3 70.8 1 28.5-138 0.820 23.6
(S) a,a,a-Trifluorotoluene(FID)94.6 93.6 59.0-128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938076
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-01,02,03,04,05,06
Method Blank (MB)
(MB) R3187746-3 12/26/16 12:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938076
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-01,02,03,04,05,06
Method Blank (MB)
(MB) R3187746-3 12/26/16 12:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK) U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 101 88.7-115
(S) Dibromofluoromethane 96.0 76.3-123
(S) 4-Bromofluorobenzene 93.2 69.7-129
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187746-1 12/26/16 10:27 • (LCSD) R3187746-2 12/26/16 10:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.144 0.137 115 110 25.3-178 4.42 22.9
Acrylonitrile 0.125 0.134 0.135 107 108 57.8-143 0.660 20
Benzene 0.0250 0.0227 0.0223 90.9 89.3 72.6-120 1.74 20
Bromobenzene 0.0250 0.0230 0.0222 91.9 88.8 80.3-115 3.47 20
Bromodichloromethane 0.0250 0.0228 0.0229 91.2 91.6 75.3-119 0.380 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938076
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187746-1 12/26/16 10:27 • (LCSD) R3187746-2 12/26/16 10:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.0250 0.0261 0.0260 104 104 69.1-135 0.270 20
Bromomethane 0.0250 0.0232 0.0232 92.9 92.8 23.0-191 0.0600 20
n-Butylbenzene 0.0250 0.0225 0.0223 89.9 89.2 74.2-134 0.740 20
sec-Butylbenzene 0.0250 0.0228 0.0220 91.4 88.2 77.8-129 3.57 20
tert-Butylbenzene 0.0250 0.0237 0.0227 94.7 90.9 77.2-129 4.15 20
Carbon tetrachloride 0.0250 0.0226 0.0218 90.4 87.2 69.4-129 3.62 20
Chlorobenzene 0.0250 0.0237 0.0233 95.0 93.2 78.9-122 1.91 20
Chlorodibromomethane 0.0250 0.0252 0.0254 101 102 76.4-126 0.730 20
Chloroethane 0.0250 0.0234 0.0218 93.5 87.4 47.2-147 6.83 20
2-Chloroethyl vinyl ether 0.125 0.164 0.177 131 141 16.7-162 7.70 23.7
Chloroform 0.0250 0.0224 0.0219 89.8 87.6 73.3-122 2.52 20
Chloromethane 0.0250 0.0211 0.0202 84.4 80.7 53.1-135 4.47 20
2-Chlorotoluene 0.0250 0.0229 0.0223 91.6 89.3 74.6-127 2.52 20
4-Chlorotoluene 0.0250 0.0230 0.0222 91.9 88.7 79.5-123 3.51 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0243 0.0255 97.1 102 64.9-131 4.76 20
1,2-Dibromoethane 0.0250 0.0240 0.0242 96.0 96.6 78.7-123 0.660 20
Dibromomethane 0.0250 0.0248 0.0243 99.2 97.1 78.5-117 2.15 20
1,2-Dichlorobenzene 0.0250 0.0229 0.0228 91.4 91.1 83.6-119 0.320 20
1,3-Dichlorobenzene 0.0250 0.0236 0.0228 94.6 91.3 75.9-129 3.56 20
1,4-Dichlorobenzene 0.0250 0.0227 0.0225 91.0 89.9 81.0-115 1.23 20
Dichlorodifluoromethane 0.0250 0.0176 0.0172 70.6 68.9 50.9-139 2.45 20
1,1-Dichloroethane 0.0250 0.0236 0.0230 94.6 92.1 71.7-125 2.66 20
1,2-Dichloroethane 0.0250 0.0229 0.0225 91.5 90.0 67.2-121 1.73 20
1,1-Dichloroethene 0.0250 0.0223 0.0213 89.3 85.1 60.6-133 4.84 20
cis-1,2-Dichloroethene 0.0250 0.0226 0.0222 90.3 88.8 76.1-121 1.64 20
trans-1,2-Dichloroethene 0.0250 0.0228 0.0218 91.2 87.2 70.7-124 4.54 20
1,2-Dichloropropane 0.0250 0.0237 0.0242 94.7 96.7 76.9-123 2.08 20
1,1-Dichloropropene 0.0250 0.0240 0.0237 95.9 94.6 71.2-126 1.33 20
1,3-Dichloropropane 0.0250 0.0240 0.0242 96.1 96.7 80.3-114 0.600 20
cis-1,3-Dichloropropene 0.0250 0.0252 0.0260 101 104 77.3-123 3.18 20
trans-1,3-Dichloropropene 0.0250 0.0226 0.0234 90.2 93.5 73.0-127 3.55 20
2,2-Dichloropropane 0.0250 0.0217 0.0217 86.8 86.7 61.9-132 0.110 20
Di-isopropyl ether 0.0250 0.0232 0.0228 92.7 91.4 67.2-131 1.40 20
Ethylbenzene 0.0250 0.0232 0.0227 92.6 90.6 78.6-124 2.19 20
Hexachloro-1,3-butadiene 0.0250 0.0242 0.0241 96.7 96.5 69.2-136 0.160 20
Isopropylbenzene 0.0250 0.0228 0.0223 91.2 89.2 79.4-126 2.21 20
p-Isopropyltoluene 0.0250 0.0240 0.0231 95.9 92.4 75.4-132 3.66 20
2-Butanone (MEK)0.125 0.132 0.145 105 116 44.5-154 9.23 21.3
Methylene Chloride 0.0250 0.0221 0.0216 88.4 86.5 68.2-119 2.11 20
4-Methyl-2-pentanone (MIBK) 0.125 0.135 0.141 108 112 61.1-138 4.22 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938076
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187746-1 12/26/16 10:27 • (LCSD) R3187746-2 12/26/16 10:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Methyl tert-butyl ether 0.0250 0.0222 0.0221 88.8 88.5 70.2-122 0.400 20
Naphthalene 0.0250 0.0238 0.0244 95.2 97.5 69.9-132 2.39 20
n-Propylbenzene 0.0250 0.0231 0.0223 92.4 89.3 80.2-124 3.45 20
Styrene 0.0250 0.0248 0.0242 99.1 96.7 79.4-124 2.48 20
1,1,1,2-Tetrachloroethane 0.0250 0.0248 0.0240 99.3 95.9 76.7-127 3.48 20
1,1,2,2-Tetrachloroethane 0.0250 0.0236 0.0237 94.5 94.6 78.8-124 0.120 20
Tetrachloroethene 0.0250 0.0236 0.0229 94.3 91.7 71.1-133 2.74 20
Toluene 0.0250 0.0219 0.0221 87.5 88.2 76.7-116 0.850 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0228 0.0216 91.0 86.3 62.6-138 5.34 20
1,2,3-Trichlorobenzene 0.0250 0.0245 0.0251 98.0 100 72.5-137 2.34 20
1,2,4-Trichlorobenzene 0.0250 0.0249 0.0251 99.4 100 74.0-137 0.820 20
1,1,1-Trichloroethane 0.0250 0.0227 0.0223 90.8 89.4 69.9-127 1.54 20
1,1,2-Trichloroethane 0.0250 0.0228 0.0230 91.2 91.9 81.9-119 0.780 20
Trichloroethene 0.0250 0.0233 0.0234 93.4 93.7 77.2-122 0.350 20
Trichlorofluoromethane 0.0250 0.0223 0.0213 89.1 85.2 51.5-151 4.51 20
1,2,3-Trichloropropane 0.0250 0.0244 0.0237 97.6 94.7 74.0-124 3.06 20
1,2,4-Trimethylbenzene 0.0250 0.0230 0.0222 91.8 88.7 77.1-124 3.42 20
1,3,5-Trimethylbenzene 0.0250 0.0225 0.0218 89.9 87.1 79.0-125 3.10 20
Vinyl chloride 0.0250 0.0219 0.0213 87.5 85.1 58.4-134 2.86 20
Xylenes, Total 0.0750 0.0691 0.0674 92.1 89.9 78.1-123 2.42 20
(S) Toluene-d8 98.9 99.7 88.7-115
(S) Dibromofluoromethane 99.4 97.2 76.3-123
(S) 4-Bromofluorobenzene 95.8 92.5 69.7-129
L880100-24 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880100-24 12/26/16 13:58 • (MS) R3187746-4 12/27/16 02:13 • (MSD) R3187746-5 12/27/16 02:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 ND 3.33 2.82 89.5 75.8 29.75 10.0-130 16.5 31.5
Acrylonitrile 0.125 ND 3.68 3.54 98.9 95.3 29.75 39.3-152 3.71 27.2
Benzene 0.0250 ND 0.539 0.537 72.4 72.2 29.75 47.8-131 0.320 22.8
Bromobenzene 0.0250 ND 0.591 0.581 79.4 78.1 29.75 40.0-130 1.74 27.4
Bromodichloromethane 0.0250 ND 0.609 0.603 81.9 81.1 29.75 50.6-128 1.02 22.8
Bromoform 0.0250 ND 0.671 0.634 90.2 85.3 29.75 43.3-139 5.60 25.9
Bromomethane 0.0250 ND 0.322 0.299 43.3 40.2 29.75 5.00-189 7.44 26.7
n-Butylbenzene 0.0250 ND 0.484 0.485 65.0 65.2 29.75 23.6-146 0.300 39.2
sec-Butylbenzene 0.0250 ND 0.570 0.552 76.6 74.3 29.75 31.0-142 3.15 34.7
tert-Butylbenzene 0.0250 ND 0.619 0.599 83.3 80.6 29.75 36.9-142 3.27 31.7
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 107 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 107 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938076
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-01,02,03,04,05,06
L880100-24 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880100-24 12/26/16 13:58 • (MS) R3187746-4 12/27/16 02:13 • (MSD) R3187746-5 12/27/16 02:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.0250 ND 0.519 0.521 69.8 70.1 29.75 46.0-140 0.490 27.2
Chlorobenzene 0.0250 ND 0.595 0.585 80.1 78.7 29.75 44.1-134 1.75 25.7
Chlorodibromomethane 0.0250 ND 0.662 0.670 89.0 90.0 29.75 49.7-134 1.10 24
Chloroethane 0.0250 ND 0.150 0.149 20.2 20.0 29.75 5.00-164 1.04 28.4
2-Chloroethyl vinyl ether 0.125 ND 4.61 4.67 124 126 29.75 5.00-159 1.20 40
Chloroform 0.0250 ND 0.587 0.583 78.9 78.4 29.75 51.2-133 0.600 22.8
Chloromethane 0.0250 ND 0.401 0.385 53.9 51.8 29.75 31.4-141 3.96 24.6
2-Chlorotoluene 0.0250 ND 0.575 0.560 77.4 75.3 29.75 36.1-137 2.72 28.9
4-Chlorotoluene 0.0250 ND 0.546 0.531 73.5 71.4 29.75 35.4-137 2.89 29.8
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.600 0.585 80.7 78.7 29.75 40.4-138 2.45 30.8
1,2-Dibromoethane 0.0250 ND 0.616 0.605 82.8 81.3 29.75 50.2-133 1.80 23.6
Dibromomethane 0.0250 ND 0.608 0.603 81.7 81.1 29.75 52.4-128 0.800 23
1,2-Dichlorobenzene 0.0250 ND 0.594 0.599 79.8 80.5 29.75 34.6-139 0.870 29.9
1,3-Dichlorobenzene 0.0250 ND 0.570 0.540 76.6 72.6 29.75 28.4-142 5.39 31.2
1,4-Dichlorobenzene 0.0250 ND 0.548 0.548 73.7 73.7 29.75 35.0-133 0.0500 31.1
Dichlorodifluoromethane 0.0250 ND 0.445 0.439 59.8 59.1 29.75 31.2-144 1.16 30.2
1,1-Dichloroethane 0.0250 ND 0.610 0.603 82.0 81.1 29.75 49.1-136 1.18 22.9
1,2-Dichloroethane 0.0250 ND 0.601 0.591 80.8 79.5 29.75 47.1-129 1.61 22.7
1,1-Dichloroethene 0.0250 ND 0.408 0.387 54.9 52.0 29.75 36.1-142 5.51 25.6
cis-1,2-Dichloroethene 0.0250 ND 0.565 0.570 76.0 76.7 29.75 50.6-133 0.850 23
trans-1,2-Dichloroethene 0.0250 ND 0.422 0.428 56.7 57.6 29.75 43.8-135 1.59 24.8
1,2-Dichloropropane 0.0250 ND 0.655 0.654 88.0 88.0 29.75 50.3-134 0.0400 22.7
1,1-Dichloropropene 0.0250 ND 0.493 0.495 66.3 66.5 29.75 43.0-137 0.350 26.4
1,3-Dichloropropane 0.0250 ND 0.640 0.640 86.0 86.0 29.75 51.4-127 0.0500 23.1
cis-1,3-Dichloropropene 0.0250 ND 0.652 0.660 87.6 88.8 29.75 48.4-134 1.34 23.6
trans-1,3-Dichloropropene 0.0250 ND 0.582 0.587 78.3 79.0 29.75 46.6-135 0.850 25.3
2,2-Dichloropropane 0.0250 ND 0.513 0.521 69.0 70.0 29.75 45.2-141 1.48 26.6
Di-isopropyl ether 0.0250 ND 0.654 0.659 87.9 88.6 29.75 46.7-140 0.770 23.5
Ethylbenzene 0.0250 ND 0.559 0.556 75.2 74.7 29.75 44.8-135 0.690 26.9
Hexachloro-1,3-butadiene 0.0250 ND 0.537 0.564 72.2 75.8 29.75 10.0-149 4.84 40
Isopropylbenzene 0.0250 ND 0.571 0.561 76.8 75.4 29.75 41.9-139 1.84 29.3
p-Isopropyltoluene 0.0250 ND 0.566 0.550 76.1 73.9 29.75 27.3-146 2.97 35.1
2-Butanone (MEK)0.125 0.714 3.58 2.86 77.1 57.8 29.75 23.9-170 22.3 28.3
Methylene Chloride 0.0250 ND 0.521 0.528 70.0 71.0 29.75 46.7-125 1.33 22.2
4-Methyl-2-pentanone (MIBK) 0.125 ND 3.53 3.43 94.9 92.2 29.75 42.4-146 2.88 26.7
Methyl tert-butyl ether 0.0250 ND 0.614 0.600 82.6 80.7 29.75 50.4-131 2.33 24.8
Naphthalene 0.0250 ND 0.580 0.612 78.0 82.2 29.75 18.4-145 5.29 34
n-Propylbenzene 0.0250 ND 0.545 0.530 73.2 71.2 29.75 35.2-139 2.79 31.9
Styrene 0.0250 ND 0.601 0.598 80.8 80.5 29.75 39.7-137 0.410 28.2
1,1,1,2-Tetrachloroethane 0.0250 ND 0.670 0.667 90.1 89.7 29.75 48.8-136 0.420 25.5
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938076
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-01,02,03,04,05,06
L880100-24 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880100-24 12/26/16 13:58 • (MS) R3187746-4 12/27/16 02:13 • (MSD) R3187746-5 12/27/16 02:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.0250 ND 0.635 0.619 85.3 83.2 29.75 45.7-140 2.51 26.4
Tetrachloroethene 0.0250 ND 0.467 0.469 62.8 63.0 29.75 37.7-140 0.280 29.2
Toluene 0.0250 ND 0.521 0.527 70.1 70.9 29.75 47.8-127 1.18 24.3
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.472 0.465 63.4 62.6 29.75 35.7-146 1.35 28.8
1,2,3-Trichlorobenzene 0.0250 ND 0.566 0.587 76.1 78.9 29.75 10.0-150 3.53 38.5
1,2,4-Trichlorobenzene 0.0250 ND 0.513 0.527 69.0 70.9 29.75 10.0-153 2.70 39.3
1,1,1-Trichloroethane 0.0250 ND 0.570 0.565 76.6 76.0 29.75 49.0-138 0.850 25.3
1,1,2-Trichloroethane 0.0250 ND 0.640 0.630 86.0 84.7 29.75 52.3-132 1.59 23.4
Trichloroethene 0.0250 ND 0.534 0.525 71.8 70.6 29.75 48.0-132 1.71 24.8
Trichlorofluoromethane 0.0250 ND 0.294 0.307 39.6 41.3 29.75 12.8-169 4.28 29.7
1,2,3-Trichloropropane 0.0250 ND 0.648 0.637 87.1 85.6 29.75 44.4-138 1.70 26.3
1,2,4-Trimethylbenzene 0.0250 ND 0.563 0.541 75.7 72.7 29.75 32.9-139 3.97 30.6
1,3,5-Trimethylbenzene 0.0250 ND 0.548 0.534 73.7 71.8 29.75 37.1-138 2.62 30.6
Vinyl chloride 0.0250 ND 0.432 0.422 58.0 56.7 29.75 32.0-146 2.25 26.3
Xylenes, Total 0.0750 ND 1.65 1.63 73.8 73.0 29.75 42.7-135 1.15 26.6
(S) Toluene-d8 100 100 88.7-115
(S) Dibromofluoromethane 97.4 96.7 76.3-123
(S) 4-Bromofluorobenzene 95.5 92.8 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 109 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938078
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-07,08,09,10,11,12,13,14,15,16,17,18,19,20,21,22,23,24,25,26
Method Blank (MB)
(MB) R3187691-3 12/26/16 01:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938078
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-07,08,09,10,11,12,13,14,15,16,17,18,19,20,21,22,23,24,25,26
Method Blank (MB)
(MB) R3187691-3 12/26/16 01:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK) U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 105 88.7-115
(S) Dibromofluoromethane 107 76.3-123
(S) 4-Bromofluorobenzene 100 69.7-129
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187691-1 12/25/16 23:39 • (LCSD) R3187691-2 12/26/16 00:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.154 0.188 123 151 25.3-178 20.2 22.9
Acrylonitrile 0.125 0.122 0.141 97.7 113 57.8-143 14.2 20
Benzene 0.0250 0.0251 0.0253 100 101 72.6-120 0.760 20
Bromobenzene 0.0250 0.0237 0.0233 95.0 93.3 80.3-115 1.83 20
Bromodichloromethane 0.0250 0.0232 0.0233 92.9 93.2 75.3-119 0.340 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 111 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938078
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-07,08,09,10,11,12,13,14,15,16,17,18,19,20,21,22,23,24,25,26
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187691-1 12/25/16 23:39 • (LCSD) R3187691-2 12/26/16 00:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.0250 0.0213 0.0217 85.1 86.7 69.1-135 1.91 20
Bromomethane 0.0250 0.0259 0.0269 104 108 23.0-191 3.54 20
n-Butylbenzene 0.0250 0.0252 0.0251 101 100 74.2-134 0.500 20
sec-Butylbenzene 0.0250 0.0244 0.0236 97.7 94.5 77.8-129 3.27 20
tert-Butylbenzene 0.0250 0.0246 0.0243 98.3 97.2 77.2-129 1.12 20
Carbon tetrachloride 0.0250 0.0242 0.0243 97.0 97.1 69.4-129 0.130 20
Chlorobenzene 0.0250 0.0257 0.0250 103 99.9 78.9-122 2.75 20
Chlorodibromomethane 0.0250 0.0250 0.0245 99.8 98.1 76.4-126 1.71 20
Chloroethane 0.0250 0.0273 0.0273 109 109 47.2-147 0.170 20
2-Chloroethyl vinyl ether 0.125 0.152 0.160 122 128 16.7-162 5.12 23.7
Chloroform 0.0250 0.0259 0.0267 104 107 73.3-122 2.94 20
Chloromethane 0.0250 0.0229 0.0225 91.7 89.9 53.1-135 1.98 20
2-Chlorotoluene 0.0250 0.0244 0.0237 97.8 94.9 74.6-127 2.99 20
4-Chlorotoluene 0.0250 0.0248 0.0242 99.2 96.8 79.5-123 2.39 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0206 0.0215 82.6 86.1 64.9-131 4.25 20
1,2-Dibromoethane 0.0250 0.0249 0.0249 99.5 99.8 78.7-123 0.300 20
Dibromomethane 0.0250 0.0260 0.0263 104 105 78.5-117 1.05 20
1,2-Dichlorobenzene 0.0250 0.0254 0.0258 102 103 83.6-119 1.33 20
1,3-Dichlorobenzene 0.0250 0.0249 0.0245 99.8 98.2 75.9-129 1.65 20
1,4-Dichlorobenzene 0.0250 0.0249 0.0252 99.5 101 81.0-115 1.19 20
Dichlorodifluoromethane 0.0250 0.0258 0.0257 103 103 50.9-139 0.400 20
1,1-Dichloroethane 0.0250 0.0264 0.0294 106 118 71.7-125 10.8 20
1,2-Dichloroethane 0.0250 0.0266 0.0268 106 107 67.2-121 0.580 20
1,1-Dichloroethene 0.0250 0.0273 0.0273 109 109 60.6-133 0.0100 20
cis-1,2-Dichloroethene 0.0250 0.0262 0.0265 105 106 76.1-121 1.33 20
trans-1,2-Dichloroethene 0.0250 0.0264 0.0284 106 114 70.7-124 7.14 20
1,2-Dichloropropane 0.0250 0.0253 0.0249 101 99.4 76.9-123 1.63 20
1,1-Dichloropropene 0.0250 0.0256 0.0253 102 101 71.2-126 1.10 20
1,3-Dichloropropane 0.0250 0.0256 0.0251 103 100 80.3-114 2.29 20
cis-1,3-Dichloropropene 0.0250 0.0251 0.0254 101 102 77.3-123 0.970 20
trans-1,3-Dichloropropene 0.0250 0.0249 0.0253 99.4 101 73.0-127 1.75 20
2,2-Dichloropropane 0.0250 0.0236 0.0240 94.4 96.2 61.9-132 1.94 20
Di-isopropyl ether 0.0250 0.0275 0.0311 110 125 67.2-131 12.3 20
Ethylbenzene 0.0250 0.0250 0.0243 100 97.1 78.6-124 2.90 20
Hexachloro-1,3-butadiene 0.0250 0.0221 0.0231 88.5 92.5 69.2-136 4.38 20
Isopropylbenzene 0.0250 0.0247 0.0239 98.9 95.5 79.4-126 3.53 20
p-Isopropyltoluene 0.0250 0.0247 0.0242 98.8 96.9 75.4-132 1.94 20
2-Butanone (MEK)0.125 0.123 0.138 98.3 111 44.5-154 11.9 21.3
Methylene Chloride 0.0250 0.0253 0.0272 101 109 68.2-119 7.37 20
4-Methyl-2-pentanone (MIBK) 0.125 0.116 0.123 92.8 98.4 61.1-138 5.84 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938078
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-07,08,09,10,11,12,13,14,15,16,17,18,19,20,21,22,23,24,25,26
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187691-1 12/25/16 23:39 • (LCSD) R3187691-2 12/26/16 00:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Methyl tert-butyl ether 0.0250 0.0263 0.0308 105 123 70.2-122 J4 15.5 20
Naphthalene 0.0250 0.0236 0.0255 94.4 102 69.9-132 7.81 20
n-Propylbenzene 0.0250 0.0245 0.0239 98.0 95.7 80.2-124 2.35 20
Styrene 0.0250 0.0248 0.0241 99.2 96.2 79.4-124 3.11 20
1,1,1,2-Tetrachloroethane 0.0250 0.0249 0.0242 99.4 96.9 76.7-127 2.56 20
1,1,2,2-Tetrachloroethane 0.0250 0.0232 0.0235 92.8 93.8 78.8-124 1.06 20
Tetrachloroethene 0.0250 0.0238 0.0232 95.3 92.7 71.1-133 2.83 20
Toluene 0.0250 0.0242 0.0239 96.7 95.4 76.7-116 1.36 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0284 0.0285 114 114 62.6-138 0.240 20
1,2,3-Trichlorobenzene 0.0250 0.0239 0.0253 95.5 101 72.5-137 5.65 20
1,2,4-Trichlorobenzene 0.0250 0.0249 0.0258 99.8 103 74.0-137 3.57 20
1,1,1-Trichloroethane 0.0250 0.0253 0.0257 101 103 69.9-127 1.59 20
1,1,2-Trichloroethane 0.0250 0.0245 0.0247 98.1 98.8 81.9-119 0.720 20
Trichloroethene 0.0250 0.0255 0.0254 102 102 77.2-122 0.180 20
Trichlorofluoromethane 0.0250 0.0312 0.0309 125 124 51.5-151 1.15 20
1,2,3-Trichloropropane 0.0250 0.0238 0.0241 95.4 96.3 74.0-124 0.980 20
1,2,4-Trimethylbenzene 0.0250 0.0244 0.0239 97.8 95.8 77.1-124 2.07 20
1,3,5-Trimethylbenzene 0.0250 0.0250 0.0246 99.8 98.2 79.0-125 1.62 20
Vinyl chloride 0.0250 0.0288 0.0287 115 115 58.4-134 0.0200 20
Xylenes, Total 0.0750 0.0748 0.0722 99.8 96.3 78.1-123 3.61 20
(S) Toluene-d8 105 104 88.7-115
(S) Dibromofluoromethane 109 109 76.3-123
(S) 4-Bromofluorobenzene 99.1 97.3 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 113 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 113 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938079
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-27,28,29
Method Blank (MB)
(MB) R3187313-3 12/26/16 23:36
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 114 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 114 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938079
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-27,28,29
Method Blank (MB)
(MB) R3187313-3 12/26/16 23:36
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK) U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 102 88.7-115
(S) Dibromofluoromethane 96.7 76.3-123
(S) 4-Bromofluorobenzene 101 69.7-129
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187313-1 12/26/16 22:05 • (LCSD) R3187313-2 12/26/16 22:56
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.115 0.140 91.6 112 25.3-178 20.4 22.9
Acrylonitrile 0.125 0.122 0.146 97.9 117 57.8-143 17.7 20
Benzene 0.0250 0.0247 0.0274 98.8 109 72.6-120 10.2 20
Bromobenzene 0.0250 0.0238 0.0274 95.2 109 80.3-115 13.9 20
Bromodichloromethane 0.0250 0.0259 0.0297 104 119 75.3-119 13.6 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 115 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 115 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938079
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-27,28,29
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187313-1 12/26/16 22:05 • (LCSD) R3187313-2 12/26/16 22:56
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.0250 0.0241 0.0284 96.2 114 69.1-135 16.6 20
Bromomethane 0.0250 0.0243 0.0273 97.3 109 23.0-191 11.4 20
n-Butylbenzene 0.0250 0.0263 0.0293 105 117 74.2-134 10.9 20
sec-Butylbenzene 0.0250 0.0255 0.0288 102 115 77.8-129 12.3 20
tert-Butylbenzene 0.0250 0.0258 0.0294 103 118 77.2-129 13.1 20
Carbon tetrachloride 0.0250 0.0238 0.0267 95.3 107 69.4-129 11.3 20
Chlorobenzene 0.0250 0.0263 0.0298 105 119 78.9-122 12.5 20
Chlorodibromomethane 0.0250 0.0260 0.0302 104 121 76.4-126 15.1 20
Chloroethane 0.0250 0.0232 0.0260 92.8 104 47.2-147 11.6 20
2-Chloroethyl vinyl ether 0.125 0.171 0.195 137 156 16.7-162 13.1 23.7
Chloroform 0.0250 0.0245 0.0273 97.9 109 73.3-122 10.9 20
Chloromethane 0.0250 0.0216 0.0241 86.2 96.6 53.1-135 11.3 20
2-Chlorotoluene 0.0250 0.0242 0.0274 96.8 110 74.6-127 12.4 20
4-Chlorotoluene 0.0250 0.0244 0.0276 97.7 110 79.5-123 12.3 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0239 0.0298 95.8 119 64.9-131 J3 21.7 20
1,2-Dibromoethane 0.0250 0.0267 0.0311 107 125 78.7-123 J4 15.2 20
Dibromomethane 0.0250 0.0251 0.0287 100 115 78.5-117 13.5 20
1,2-Dichlorobenzene 0.0250 0.0252 0.0288 101 115 83.6-119 13.3 20
1,3-Dichlorobenzene 0.0250 0.0243 0.0275 97.0 110 75.9-129 12.7 20
1,4-Dichlorobenzene 0.0250 0.0254 0.0289 101 116 81.0-115 J4 13.1 20
Dichlorodifluoromethane 0.0250 0.0220 0.0243 87.9 97.3 50.9-139 10.2 20
1,1-Dichloroethane 0.0250 0.0240 0.0267 95.8 107 71.7-125 11.0 20
1,2-Dichloroethane 0.0250 0.0259 0.0295 103 118 67.2-121 13.3 20
1,1-Dichloroethene 0.0250 0.0238 0.0262 95.1 105 60.6-133 9.51 20
cis-1,2-Dichloroethene 0.0250 0.0240 0.0267 96.0 107 76.1-121 10.7 20
trans-1,2-Dichloroethene 0.0250 0.0239 0.0264 95.6 106 70.7-124 9.94 20
1,2-Dichloropropane 0.0250 0.0242 0.0273 96.8 109 76.9-123 11.9 20
1,1-Dichloropropene 0.0250 0.0256 0.0282 103 113 71.2-126 9.54 20
1,3-Dichloropropane 0.0250 0.0262 0.0299 105 119 80.3-114 J4 13.3 20
cis-1,3-Dichloropropene 0.0250 0.0265 0.0299 106 120 77.3-123 11.9 20
trans-1,3-Dichloropropene 0.0250 0.0278 0.0314 111 126 73.0-127 12.2 20
2,2-Dichloropropane 0.0250 0.0237 0.0248 94.8 99.4 61.9-132 4.69 20
Di-isopropyl ether 0.0250 0.0236 0.0269 94.4 108 67.2-131 12.9 20
Ethylbenzene 0.0250 0.0255 0.0288 102 115 78.6-124 12.1 20
Hexachloro-1,3-butadiene 0.0250 0.0249 0.0278 99.6 111 69.2-136 10.9 20
Isopropylbenzene 0.0250 0.0253 0.0287 101 115 79.4-126 12.6 20
p-Isopropyltoluene 0.0250 0.0253 0.0285 101 114 75.4-132 11.8 20
2-Butanone (MEK)0.125 0.118 0.143 94.7 114 44.5-154 18.9 21.3
Methylene Chloride 0.0250 0.0216 0.0244 86.3 97.6 68.2-119 12.4 20
4-Methyl-2-pentanone (MIBK) 0.125 0.139 0.170 111 136 61.1-138 J3 20.3 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 116 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 116 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938079
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-27,28,29
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187313-1 12/26/16 22:05 • (LCSD) R3187313-2 12/26/16 22:56
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Methyl tert-butyl ether 0.0250 0.0234 0.0275 93.6 110 70.2-122 16.1 20
Naphthalene 0.0250 0.0233 0.0271 93.4 109 69.9-132 15.1 20
n-Propylbenzene 0.0250 0.0250 0.0282 99.9 113 80.2-124 12.2 20
Styrene 0.0250 0.0254 0.0291 102 117 79.4-124 13.7 20
1,1,1,2-Tetrachloroethane 0.0250 0.0248 0.0285 99.1 114 76.7-127 13.9 20
1,1,2,2-Tetrachloroethane 0.0250 0.0248 0.0299 99.1 119 78.8-124 18.6 20
Tetrachloroethene 0.0250 0.0264 0.0291 106 116 71.1-133 9.72 20
Toluene 0.0250 0.0252 0.0279 101 111 76.7-116 10.1 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0246 0.0270 98.4 108 62.6-138 9.22 20
1,2,3-Trichlorobenzene 0.0250 0.0224 0.0252 89.7 101 72.5-137 11.6 20
1,2,4-Trichlorobenzene 0.0250 0.0242 0.0267 96.8 107 74.0-137 9.80 20
1,1,1-Trichloroethane 0.0250 0.0247 0.0270 98.9 108 69.9-127 8.98 20
1,1,2-Trichloroethane 0.0250 0.0256 0.0297 102 119 81.9-119 14.9 20
Trichloroethene 0.0250 0.0254 0.0279 102 112 77.2-122 9.59 20
Trichlorofluoromethane 0.0250 0.0255 0.0275 102 110 51.5-151 7.45 20
1,2,3-Trichloropropane 0.0250 0.0244 0.0299 97.5 119 74.0-124 J3 20.2 20
1,2,4-Trimethylbenzene 0.0250 0.0242 0.0277 96.6 111 77.1-124 13.6 20
1,3,5-Trimethylbenzene 0.0250 0.0251 0.0283 100 113 79.0-125 12.2 20
Vinyl chloride 0.0250 0.0222 0.0246 89.0 98.5 58.4-134 10.2 20
Xylenes, Total 0.0750 0.0751 0.0850 100 113 78.1-123 12.4 20
(S) Toluene-d8 103 102 88.7-115
(S) Dibromofluoromethane 99.9 99.1 76.3-123
(S) 4-Bromofluorobenzene 98.6 98.1 69.7-129
L880142-27 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880142-27 12/27/16 01:49 • (MS) R3187313-4 12/27/16 00:49 • (MSD) R3187313-5 12/27/16 01:09
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.152 ND 0.0397 0.0441 14.1 17.1 1 10.0-130 10.7 31.5
Acrylonitrile 0.152 ND 0.0229 0.0322 15.1 21.2 1 39.3-152 J6 J3 J6 33.5 27.2
Benzene 0.0304 ND 0.00372 0.00495 12.2 16.3 1 47.8-131 J6 J3 J6 28.4 22.8
Bromobenzene 0.0304 ND 0.00258 0.00338 8.50 11.1 1 40.0-130 J6 J6 26.7 27.4
Bromodichloromethane 0.0304 ND 0.00369 0.00502 12.1 16.5 1 50.6-128 J6 J3 J6 30.5 22.8
Bromoform 0.0304 ND 0.00350 0.00471 11.5 15.5 1 43.3-139 J6 J3 J6 29.6 25.9
Bromomethane 0.0304 ND 0.00295 0.00350 9.72 11.5 1 5.00-189 16.9 26.7
n-Butylbenzene 0.0304 ND 0.00292 0.00332 9.61 10.9 1 23.6-146 J6 J6 12.8 39.2
sec-Butylbenzene 0.0304 ND 0.00283 0.00324 9.32 10.7 1 31.0-142 J6 J6 13.4 34.7
tert-Butylbenzene 0.0304 ND 0.00276 0.00333 9.09 11.0 1 36.9-142 J6 J6 18.6 31.7
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 117 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 117 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938079
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-27,28,29
L880142-27 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880142-27 12/27/16 01:49 • (MS) R3187313-4 12/27/16 00:49 • (MSD) R3187313-5 12/27/16 01:09
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.0304 ND 0.00414 0.00474 13.6 15.6 1 46.0-140 J6 J6 13.4 27.2
Chlorobenzene 0.0304 0.00548 0.00479 0.00537 0.000 0.000 1 44.1-134 J6 J6 11.3 25.7
Chlorodibromomethane 0.0304 ND 0.00336 0.00468 11.1 15.4 1 49.7-134 J6 J3 J6 32.8 24
Chloroethane 0.0304 ND 0.00458 0.00479 15.1 15.7 1 5.00-164 4.30 28.4
2-Chloroethyl vinyl ether 0.152 ND ND ND 0.000 0.000 1 5.00-159 J6 J6 0.000 40
Chloroform 0.0304 ND 0.00380 0.00492 12.5 16.2 1 51.2-133 J6 J3 J6 25.6 22.8
Chloromethane 0.0304 ND 0.00299 0.00316 9.83 10.4 1 31.4-141 J6 J6 5.52 24.6
2-Chlorotoluene 0.0304 ND 0.00264 0.00328 8.67 10.8 1 36.1-137 J6 J6 21.7 28.9
4-Chlorotoluene 0.0304 ND 0.00254 0.00313 8.37 10.3 1 35.4-137 J6 J6 20.7 29.8
1,2-Dibromo-3-Chloropropane 0.0304 ND 0.00403 0.00542 13.3 17.8 1 40.4-138 J6 J6 29.5 30.8
1,2-Dibromoethane 0.0304 ND 0.00384 0.00535 12.6 17.6 1 50.2-133 J6 J3 J6 33.0 23.6
Dibromomethane 0.0304 ND 0.00393 0.00538 12.9 17.7 1 52.4-128 J6 J3 J6 31.2 23
1,2-Dichlorobenzene 0.0304 ND 0.00267 0.00341 8.79 11.2 1 34.6-139 J6 J6 24.5 29.9
1,3-Dichlorobenzene 0.0304 ND 0.00249 0.00300 8.18 9.87 1 28.4-142 J6 J6 18.7 31.2
1,4-Dichlorobenzene 0.0304 ND 0.00275 0.00342 9.05 11.2 1 35.0-133 J6 J6 21.7 31.1
Dichlorodifluoromethane 0.0304 ND 0.00511 0.00429 16.8 14.1 1 31.2-144 J6 J6 17.3 30.2
1,1-Dichloroethane 0.0304 ND 0.00389 0.00492 12.8 16.2 1 49.1-136 J6 J3 J6 23.3 22.9
1,2-Dichloroethane 0.0304 ND 0.00412 0.00569 13.6 18.7 1 47.1-129 J6 J3 J6 32.1 22.7
1,1-Dichloroethene 0.0304 ND 0.00470 0.00490 15.5 16.1 1 36.1-142 J6 J6 4.32 25.6
cis-1,2-Dichloroethene 0.0304 ND 0.00354 0.00471 11.6 15.5 1 50.6-133 J6 J3 J6 28.3 23
trans-1,2-Dichloroethene 0.0304 ND 0.00390 0.00470 12.8 15.5 1 43.8-135 J6 J6 18.5 24.8
1,2-Dichloropropane 0.0304 ND 0.00350 0.00475 11.5 15.6 1 50.3-134 J6 J3 J6 30.4 22.7
1,1-Dichloropropene 0.0304 ND 0.00395 0.00489 13.0 16.1 1 43.0-137 J6 J6 21.3 26.4
1,3-Dichloropropane 0.0304 ND 0.00383 0.00534 12.6 17.6 1 51.4-127 J6 J3 J6 33.0 23.1
cis-1,3-Dichloropropene 0.0304 ND 0.00343 0.00472 11.3 15.5 1 48.4-134 J6 J3 J6 31.7 23.6
trans-1,3-Dichloropropene 0.0304 ND 0.00374 0.00497 12.3 16.4 1 46.6-135 J6 J3 J6 28.3 25.3
2,2-Dichloropropane 0.0304 ND 0.00413 0.00493 13.6 16.2 1 45.2-141 J6 J6 17.6 26.6
Di-isopropyl ether 0.0304 ND 0.00377 0.00497 12.4 16.4 1 46.7-140 J6 J3 J6 27.5 23.5
Ethylbenzene 0.0304 ND 0.00292 0.00380 9.62 12.5 1 44.8-135 J6 J6 26.0 26.9
Hexachloro-1,3-butadiene 0.0304 ND 0.00242 0.00242 7.95 7.95 1 10.0-149 J6 J6 0.0500 40
Isopropylbenzene 0.0304 0.00214 0.00424 0.00462 6.91 8.16 1 41.9-139 J6 J6 8.62 29.3
p-Isopropyltoluene 0.0304 ND 0.00281 0.00315 9.24 10.4 1 27.3-146 J6 J6 11.5 35.1
2-Butanone (MEK)0.152 ND 0.0246 0.0335 12.4 18.3 1 23.9-170 J6 J3 J6 30.7 28.3
Methylene Chloride 0.0304 ND 0.00343 0.00446 11.3 14.7 1 46.7-125 J6 J3 J6 26.0 22.2
4-Methyl-2-pentanone (MIBK) 0.152 ND 0.0319 0.0430 21.0 28.3 1 42.4-146 J6 J3 J6 29.6 26.7
Methyl tert-butyl ether 0.0304 ND 0.00428 0.00559 14.1 18.4 1 50.4-131 J6 J3 J6 26.6 24.8
Naphthalene 0.0304 ND 0.00274 0.00324 9.02 10.7 1 18.4-145 J6 J6 16.9 34
n-Propylbenzene 0.0304 ND 0.00294 0.00350 9.69 11.5 1 35.2-139 J6 J6 17.1 31.9
Styrene 0.0304 ND 0.00234 0.00285 7.68 9.39 1 39.7-137 J6 J6 20.0 28.2
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 118 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 118 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938079
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-27,28,29
L880142-27 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880142-27 12/27/16 01:49 • (MS) R3187313-4 12/27/16 00:49 • (MSD) R3187313-5 12/27/16 01:09
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,1,2-Tetrachloroethane 0.0304 ND 0.00294 0.00400 9.69 13.2 1 48.8-136 J6 J3 J6 30.4 25.5
1,1,2,2-Tetrachloroethane 0.0304 ND 0.00400 0.00538 13.2 17.7 1 45.7-140 J6 J3 J6 29.3 26.4
Tetrachloroethene 0.0304 ND 0.00331 0.00408 10.9 13.4 1 37.7-140 J6 J6 20.8 29.2
Toluene 0.0304 ND 0.00467 0.00534 0.000 0.000 1 47.8-127 J6 J6 13.5 24.3
1,1,2-Trichlorotrifluoroethane 0.0304 ND 0.00640 0.00570 21.1 18.8 1 35.7-146 J6 J6 11.6 28.8
1,2,3-Trichlorobenzene 0.0304 ND 0.00212 0.00229 6.98 7.52 1 10.0-150 J6 J6 7.39 38.5
1,2,4-Trichlorobenzene 0.0304 ND 0.00225 0.00241 7.40 7.93 1 10.0-153 J6 J6 7.03 39.3
1,1,1-Trichloroethane 0.0304 ND 0.00412 0.00491 13.6 16.2 1 49.0-138 J6 J6 17.5 25.3
1,1,2-Trichloroethane 0.0304 ND 0.00394 0.00540 13.0 17.8 1 52.3-132 J6 J3 J6 31.4 23.4
Trichloroethene 0.0304 ND 0.00360 0.00456 11.9 15.0 1 48.0-132 J6 J6 23.5 24.8
Trichlorofluoromethane 0.0304 1.03 0.0113 0.0122 0.000 0.000 1 12.8-169 V V 6.95 29.7
1,2,3-Trichloropropane 0.0304 ND 0.00421 0.00565 13.9 18.6 1 44.4-138 J6 J3 J6 29.2 26.3
1,2,4-Trimethylbenzene 0.0304 ND 0.00319 0.00366 9.00 10.5 1 32.9-139 J6 J6 13.5 30.6
1,3,5-Trimethylbenzene 0.0304 ND 0.00306 0.00360 10.1 11.8 1 37.1-138 J6 J6 16.3 30.6
Vinyl chloride 0.0304 ND 0.00450 0.00420 14.8 13.8 1 32.0-146 J6 J6 6.76 26.3
Xylenes, Total 0.0912 ND 0.00863 0.0109 9.47 12.0 1 42.7-135 J6 J6 23.5 26.6
(S) Toluene-d8 101 101 88.7-115
(S) Dibromofluoromethane 105 103 76.3-123
(S) 4-Bromofluorobenzene 96.8 94.7 69.7-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 119 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 119 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938587
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-30,31,32
Method Blank (MB)
(MB) R3187465-1 12/25/16 16:44
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 10.0 50.0
Acrolein U 8.87 50.0
Acrylonitrile U 1.87 10.0
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride U 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
2-Chloroethyl vinyl ether U 3.01 50.0
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
cis-1,3-Dichloropropene U 0.418 1.00
trans-1,3-Dichloropropene U 0.419 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 120 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 120 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938587
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-30,31,32
Method Blank (MB)
(MB) R3187465-1 12/25/16 16:44
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Hexachloro-1,3-butadiene U 0.256 1.00
Isopropylbenzene U 0.326 1.00
p-Isopropyltoluene U 0.350 1.00
2-Butanone (MEK)U 3.93 10.0
Methylene Chloride U 1.00 5.00
4-Methyl-2-pentanone (MIBK) U 2.14 10.0
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.349 1.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,1,2-Trichlorotrifluoroethane U 0.303 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
Trichloroethene U 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,3-Trimethylbenzene U 0.321 1.00
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Vinyl chloride U 0.259 1.00
Xylenes, Total U 1.06 3.00
(S) Toluene-d8 105 90.0-115
(S) Dibromofluoromethane 103 79.0-121
(S) 4-Bromofluorobenzene 101 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187465-2 12/25/16 17:25 • (LCSD) R3187465-3 12/25/16 17:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 125 156 159 125 128 28.7-175 2.35 20.9
Acrolein 125 471 491 377 392 40.4-172 J4 J4 4.13 20
Acrylonitrile 125 154 154 123 123 58.2-145 0.160 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 121 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 121 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938587
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-30,31,32
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187465-2 12/25/16 17:25 • (LCSD) R3187465-3 12/25/16 17:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 25.0 28.4 27.2 114 109 73.0-122 4.32 20
Bromobenzene 25.0 25.2 25.2 101 101 81.5-115 0.0300 20
Bromodichloromethane 25.0 26.5 26.5 106 106 75.5-121 0.120 20
Bromoform 25.0 24.0 25.1 96.1 100 71.5-131 4.15 20
Bromomethane 25.0 25.0 23.3 99.9 93.2 22.4-187 6.94 20
n-Butylbenzene 25.0 26.3 25.1 105 100 75.9-134 4.68 20
sec-Butylbenzene 25.0 23.7 23.3 94.8 93.0 80.6-126 1.91 20
tert-Butylbenzene 25.0 24.6 23.7 98.5 94.6 79.3-127 4.04 20
Carbon tetrachloride 25.0 24.5 22.3 98.0 89.4 70.9-129 9.26 20
Chlorobenzene 25.0 26.4 26.5 106 106 79.7-122 0.280 20
Chlorodibromomethane 25.0 26.0 26.6 104 106 78.2-124 2.25 20
Chloroethane 25.0 29.8 26.5 119 106 41.2-153 11.6 20
2-Chloroethyl vinyl ether 125 152 152 122 122 23.4-162 0.300 23.5
Chloroform 25.0 28.4 27.2 114 109 73.2-125 4.30 20
Chloromethane 25.0 34.0 32.4 136 130 55.8-134 J4 4.91 20
2-Chlorotoluene 25.0 25.8 25.7 103 103 76.4-125 0.390 20
4-Chlorotoluene 25.0 26.4 26.3 105 105 81.5-121 0.390 20
1,2-Dibromo-3-Chloropropane 25.0 24.7 25.5 98.6 102 64.8-131 3.41 20
1,2-Dibromoethane 25.0 25.5 26.3 102 105 79.8-122 2.99 20
Dibromomethane 25.0 25.9 26.4 104 106 79.5-118 1.99 20
1,2-Dichlorobenzene 25.0 27.3 26.7 109 107 84.7-118 2.40 20
1,3-Dichlorobenzene 25.0 24.3 24.6 97.1 98.5 77.6-127 1.36 20
1,4-Dichlorobenzene 25.0 25.2 24.8 101 99.1 82.2-114 1.76 20
Dichlorodifluoromethane 25.0 24.8 21.8 99.0 87.1 56.0-134 12.8 20
1,1-Dichloroethane 25.0 29.3 27.6 117 110 71.7-127 5.93 20
1,2-Dichloroethane 25.0 26.5 26.4 106 105 65.3-126 0.460 20
1,1-Dichloroethene 25.0 28.8 25.9 115 104 59.9-137 10.5 20
cis-1,2-Dichloroethene 25.0 30.0 29.0 120 116 77.3-122 3.40 20
trans-1,2-Dichloroethene 25.0 29.9 27.5 120 110 72.6-125 8.42 20
1,2-Dichloropropane 25.0 28.4 28.0 114 112 77.4-125 1.56 20
1,1-Dichloropropene 25.0 29.7 27.1 119 109 72.5-127 9.01 20
1,3-Dichloropropane 25.0 26.4 26.7 106 107 80.6-115 1.08 20
cis-1,3-Dichloropropene 25.0 27.5 27.1 110 109 77.7-124 1.43 20
trans-1,3-Dichloropropene 25.0 28.7 28.3 115 113 73.5-127 1.62 20
2,2-Dichloropropane 25.0 28.9 26.8 116 107 61.3-134 7.45 20
Di-isopropyl ether 25.0 26.4 25.9 105 103 65.1-135 1.94 20
Ethylbenzene 25.0 26.5 25.9 106 104 80.9-121 2.16 20
Hexachloro-1,3-butadiene 25.0 20.3 19.3 81.2 77.0 73.7-133 5.28 20
Isopropylbenzene 25.0 25.0 24.3 99.9 97.2 81.6-124 2.70 20
p-Isopropyltoluene 25.0 25.5 24.8 102 99.2 77.6-129 2.63 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 122 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 122 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938587
Volatile Organic Compounds (GC/MS) by Method 8260B L880142-30,31,32
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187465-2 12/25/16 17:25 • (LCSD) R3187465-3 12/25/16 17:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
2-Butanone (MEK)125 147 149 117 119 46.4-155 1.56 20
Methylene Chloride 25.0 27.2 26.9 109 108 69.5-120 1.06 20
4-Methyl-2-pentanone (MIBK) 125 135 139 108 111 63.3-138 2.71 20
Methyl tert-butyl ether 25.0 27.0 27.3 108 109 70.1-125 1.23 20
Naphthalene 25.0 25.3 25.5 101 102 69.7-134 0.810 20
n-Propylbenzene 25.0 25.5 25.0 102 100 81.9-122 1.96 20
Styrene 25.0 27.2 26.8 109 107 79.9-124 1.56 20
1,1,1,2-Tetrachloroethane 25.0 24.7 24.6 98.7 98.5 78.5-125 0.230 20
1,1,2,2-Tetrachloroethane 25.0 26.7 27.9 107 112 79.3-123 4.64 20
Tetrachloroethene 25.0 24.6 23.6 98.4 94.6 73.5-130 3.95 20
Toluene 25.0 27.7 26.6 111 106 77.9-116 4.16 20
1,1,2-Trichlorotrifluoroethane 25.0 28.0 25.0 112 99.9 62.0-141 11.6 20
1,2,3-Trichlorobenzene 25.0 23.3 23.3 93.1 93.2 75.7-134 0.150 20
1,2,4-Trichlorobenzene 25.0 24.6 24.4 98.3 97.7 76.1-136 0.610 20
1,1,1-Trichloroethane 25.0 27.3 24.6 109 98.3 71.1-129 10.5 20
1,1,2-Trichloroethane 25.0 25.5 26.1 102 104 81.6-120 2.07 20
Trichloroethene 25.0 26.5 25.4 106 101 79.5-121 4.51 20
Trichlorofluoromethane 25.0 26.6 23.9 107 95.7 49.1-157 10.7 20
1,2,3-Trichloropropane 25.0 26.4 27.2 106 109 74.9-124 2.85 20
1,2,3-Trimethylbenzene 25.0 27.0 26.8 108 107 79.9-118 0.960 20
1,2,4-Trimethylbenzene 25.0 25.2 25.2 101 101 79.0-122 0.180 20
1,3,5-Trimethylbenzene 25.0 24.3 23.9 97.2 95.7 81.0-123 1.56 20
Vinyl chloride 25.0 27.7 25.7 111 103 61.5-134 7.42 20
Xylenes, Total 75.0 78.0 76.9 104 103 79.2-122 1.43 20
(S) Toluene-d8 104 106 90.0-115
(S) Dibromofluoromethane 104 104 79.0-121
(S) 4-Bromofluorobenzene 97.4 101 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 123 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 123 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG937731
Semi-Volatile Organic Compounds (GC) by Method 8015 L880142-21,22,23,24,25,26,27,28,29
Method Blank (MB)
(MB) R3187036-1 12/23/16 09:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terphenyl 81.0 50.0-150
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187036-2 12/23/16 10:03 • (LCSD) R3187036-3 12/23/16 10:15
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 60.0 37.9 45.6 63.2 76.0 50.0-150 18.4 20
(S) o-Terphenyl 68.9 83.5 50.0-150
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 124 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 124 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938642
Semi-Volatile Organic Compounds (GC) by Method 8015 L880142-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3187879-1 12/28/16 22:46
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terphenyl 83.3 50.0-150
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187879-2 12/28/16 22:58 • (LCSD) R3187879-3 12/28/16 23:10
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 60.0 46.8 50.8 78.0 84.6 50.0-150 8.04 20
(S) o-Terphenyl 88.1 93.6 50.0-150
L880142-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880142-03 12/28/16 23:47 • (MS) R3187879-4 12/28/16 23:59 • (MSD) R3187879-5 12/29/16 00:11
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 70.0 ND 58.4 61.1 80.4 84.2 1 50.0-150 4.43 20
(S) o-Terphenyl 103 95.4 50.0-150
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 125 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 125 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938055
Semi-Volatile Organic Compounds (GC) by Method MADEPE L880142-30,31,32
Method Blank (MB)
(MB) R3186834-1 12/22/16 16:38
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
Unadjusted Total Petroleum
Hydrocarbons U 33.3 100
(S) 1-Chloro-octadecane 66.5 40.0-140
Method Blank (MB)
(MB) R3186834-4 12/22/16 17:43
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 33.5 J 33.3 100
Unadjusted Total Petroleum
Hydrocarbons U 33.3 100
(S) o-Terphenyl 76.9 40.0-140
(S) 2-Fluorobiphenyl 81.6 40.0-140
(S) 2-Bromonaphthalene 81.2 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3186834-2 12/22/16 17:00 • (LCSD) R3186834-3 12/22/16 17:22
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 293 303 48.9 50.6 40.0-140 3.33 25
Unadjusted C19-C36 Aliphatics 800 618 653 77.3 81.6 40.0-140 5.49 25
(S) 1-Chloro-octadecane 70.0 68.3 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3186834-5 12/22/16 18:05 • (LCSD) R3186834-6 12/22/16 18:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1090 1190 64.3 69.9 40.0-140 8.26 25
(S) o-Terphenyl 85.2 86.0 40.0-140
(S) 2-Fluorobiphenyl 83.4 89.8 40.0-140
(S) 2-Bromonaphthalene 83.0 88.8 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 126 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 126 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938069
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-30,31,32
Method Blank (MB)
(MB) R3187437-3 12/27/16 10:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroethyl)ether U 1.62 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 0.304 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate 0.327 J 0.278 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 127 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 127 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938069
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-30,31,32
Method Blank (MB)
(MB) R3187437-3 12/27/16 10:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
4-Chloro-3-methylphenol U 0.263 10.0
2-Chlorophenol U 0.283 10.0
2-Nitrophenol U 0.320 10.0
4-Nitrophenol U 2.01 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 0.334 10.0
2,4,6-Trichlorophenol U 0.297 10.0
2,4-Dichlorophenol U 0.284 10.0
2,4-Dimethylphenol U 0.264 10.0
4,6-Dinitro-2-methylphenol U 2.62 10.0
2,4-Dinitrophenol U 3.25 10.0
(S) Nitrobenzene-d5 25.1 21.8-123
(S) 2-Fluorobiphenyl 35.6 29.5-131
(S) p-Terphenyl-d14 91.4 29.3-137
(S) Phenol-d5 15.7 5.00-70.1
(S) 2-Fluorophenol 22.1 10.0-77.9
(S) 2,4,6-Tribromophenol 55.7 11.2-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187437-1 12/27/16 10:03 • (LCSD) R3187437-2 12/27/16 10:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 35.1 35.2 70.1 70.4 38.7-109 0.300 21.5
Acenaphthylene 50.0 35.7 35.8 71.5 71.5 36.0-106 0.130 21
Anthracene 50.0 38.9 39.1 77.9 78.2 43.6-113 0.400 18.8
Benzidine 50.0 25.6 28.5 51.3 57.0 10.0-165 10.5 40
Benzo(a)anthracene 50.0 39.5 39.0 79.0 78.0 51.2-112 1.26 20
Benzo(b)fluoranthene 50.0 40.0 38.9 80.0 77.7 47.6-111 2.93 20
Benzo(k)fluoranthene 50.0 42.0 41.4 83.9 82.7 49.4-114 1.40 20
Benzo(g,h,i)perylene 50.0 43.8 42.0 87.7 83.9 45.2-117 4.32 20
Benzo(a)pyrene 50.0 39.8 39.1 79.5 78.2 45.6-106 1.62 20
Bis(2-chlorethoxy)methane 50.0 26.6 29.0 53.3 58.0 37.2-111 8.43 24.1
Bis(2-chloroethyl)ether 50.0 19.3 20.7 38.6 41.4 22.6-108 7.14 27.9
Bis(2-chloroisopropyl)ether 50.0 22.5 26.3 45.1 52.5 32.9-100 15.3 25.1
4-Bromophenyl-phenylether 50.0 41.7 41.6 83.3 83.1 40.7-116 0.280 21
2-Chloronaphthalene 50.0 30.6 31.3 61.2 62.7 33.6-105 2.46 23
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938069
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-30,31,32
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187437-1 12/27/16 10:03 • (LCSD) R3187437-2 12/27/16 10:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
4-Chlorophenyl-phenylether 50.0 41.9 41.9 83.9 83.8 39.0-113 0.0400 20.9
Chrysene 50.0 43.4 42.4 86.8 84.8 54.6-120 2.30 20
Dibenz(a,h)anthracene 50.0 43.2 41.9 86.3 83.7 42.8-118 3.06 20
3,3-Dichlorobenzidine 50.0 44.5 45.0 89.0 90.0 27.2-142 1.09 22.3
2,4-Dinitrotoluene 50.0 45.0 44.8 90.1 89.7 31.2-105 0.440 22
2,6-Dinitrotoluene 50.0 39.8 40.0 79.6 80.0 30.6-106 0.480 23.1
Fluoranthene 50.0 44.2 43.6 88.3 87.2 45.9-115 1.33 20
Fluorene 50.0 39.2 38.9 78.5 77.8 41.0-112 0.780 20.2
Hexachlorobenzene 50.0 43.8 43.9 87.6 87.8 38.5-116 0.180 20.1
Hexachloro-1,3-butadiene 50.0 23.5 25.8 46.9 51.5 16.1-104 9.41 31.2
Hexachlorocyclopentadiene 50.0 22.4 25.1 44.8 50.2 10.0-121 11.2 27.9
Hexachloroethane 50.0 16.3 17.3 32.6 34.6 16.5-89.8 5.92 30.7
Indeno(1,2,3-cd)pyrene 50.0 43.8 42.1 87.5 84.2 45.0-116 3.80 20
Isophorone 50.0 31.9 32.7 63.7 65.4 35.4-112 2.52 21.5
Naphthalene 50.0 24.2 26.6 48.4 53.1 32.2-101 9.31 23.8
Nitrobenzene 50.0 24.0 26.6 48.1 53.2 31.4-106 10.1 25.7
n-Nitrosodimethylamine 50.0 9.84 11.0 19.7 21.9 10.0-80.1 10.9 37.5
n-Nitrosodiphenylamine 50.0 37.7 37.9 75.5 75.7 44.4-113 0.380 20
n-Nitrosodi-n-propylamine 50.0 23.9 27.8 47.9 55.7 33.2-106 15.0 23.7
Phenanthrene 50.0 37.7 37.7 75.4 75.4 46.4-113 0.0600 20
Benzylbutyl phthalate 50.0 40.1 39.7 80.2 79.4 31.8-123 0.970 20.7
Bis(2-ethylhexyl)phthalate 50.0 38.9 38.2 77.9 76.5 36.9-134 1.80 23.6
Di-n-butyl phthalate 50.0 41.1 41.3 82.3 82.7 41.8-120 0.450 20.2
Diethyl phthalate 50.0 43.4 43.4 86.7 86.8 36.5-129 0.130 20
Dimethyl phthalate 50.0 41.7 41.5 83.4 82.9 35.3-128 0.620 20.8
Di-n-octyl phthalate 50.0 40.0 39.4 79.9 78.8 39.7-112 1.40 21.1
Pyrene 50.0 39.0 38.1 77.9 76.2 46.3-117 2.19 20
1,2,4-Trichlorobenzene 50.0 23.0 26.0 46.0 51.9 22.9-96.1 12.1 27.5
4-Chloro-3-methylphenol 50.0 35.3 36.1 70.6 72.2 35.7-100 2.30 22.9
2-Chlorophenol 50.0 20.9 23.2 41.8 46.5 26.2-91.5 10.7 26.5
2,4-Dichlorophenol 50.0 30.7 33.7 61.4 67.4 31.4-103 9.40 24.9
2,4-Dimethylphenol 50.0 29.2 32.3 58.3 64.6 31.9-107 10.1 25.7
4,6-Dinitro-2-methylphenol 50.0 42.4 43.1 84.9 86.2 18.4-148 1.61 24.4
2,4-Dinitrophenol 50.0 36.3 34.3 72.6 68.6 24.2-128 5.68 20.5
2-Nitrophenol 50.0 29.1 31.5 58.2 63.0 25.9-106 7.89 26.9
4-Nitrophenol 50.0 19.8 19.1 39.7 38.3 10.0-52.7 3.63 40
Pentachlorophenol 50.0 40.6 40.4 81.3 80.9 10.0-97.4 0.500 35.1
Phenol 50.0 11.8 12.9 23.6 25.7 10.0-57.9 8.70 35
2,4,6-Trichlorophenol 50.0 40.8 41.0 81.6 81.9 29.8-107 0.410 24.1
(S) Nitrobenzene-d5 46.9 51.5 21.8-123
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938069
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-30,31,32
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187437-1 12/27/16 10:03 • (LCSD) R3187437-2 12/27/16 10:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
(S) 2-Fluorobiphenyl 63.6 65.3 29.5-131
(S) p-Terphenyl-d14 86.1 82.4 29.3-137
(S) Phenol-d5 22.5 26.9 5.00-70.1
(S) 2-Fluorophenol 32.1 34.4 10.0-77.9
(S) 2,4,6-Tribromophenol 93.3 91.0 11.2-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938702
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-06,09,10,12,16,18,21,22,23,25,26,27
Method Blank (MB)
(MB) R3188056-3 12/29/16 11:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0330
Acenaphthylene U 0.00671 0.0330
Anthracene U 0.00632 0.0330
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0330
Benzo(b)fluoranthene U 0.00695 0.0330
Benzo(k)fluoranthene U 0.00582 0.0330
Benzo(g,h,i)perylene U 0.00721 0.0330
Benzo(a)pyrene U 0.00548 0.0330
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0330
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0330
Dibenz(a,h)anthracene U 0.00821 0.0330
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0330
Fluorene U 0.00682 0.0330
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0330
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0330
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.00594 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0330
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938702
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-06,09,10,12,16,18,21,22,23,25,26,27
Method Blank (MB)
(MB) R3188056-3 12/29/16 11:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.0123 0.0330
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 52.0 21.9-129
(S) 2-Fluorobiphenyl 56.2 34.9-129
(S) p-Terphenyl-d14 70.7 21.5-128
(S) Phenol-d5 55.1 26.3-121
(S) 2-Fluorophenol 55.3 21.1-116
(S) 2,4,6-Tribromophenol 51.7 21.6-142
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188056-1 12/29/16 10:53 • (LCSD) R3188056-2 12/29/16 11:19
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.667 0.470 0.439 70.5 65.7 48.9-107 6.92 20
Acenaphthylene 0.667 0.469 0.441 70.4 66.2 49.2-111 6.15 20
Anthracene 0.667 0.466 0.454 69.9 68.1 52.0-112 2.71 20
Benzidine 0.667 0.149 0.138 22.3 20.7 10.0-48.0 7.36 40
Benzo(a)anthracene 0.667 0.467 0.466 70.0 69.9 52.3-106 0.0700 20
Benzo(b)fluoranthene 0.667 0.442 0.446 66.3 66.9 51.3-106 0.940 20
Benzo(k)fluoranthene 0.667 0.486 0.454 72.8 68.0 52.9-107 6.85 20
Benzo(g,h,i)perylene 0.667 0.480 0.494 72.0 74.1 45.8-108 2.95 20
Benzo(a)pyrene 0.667 0.479 0.467 71.9 70.0 51.9-106 2.65 20
Bis(2-chlorethoxy)methane 0.667 0.356 0.334 53.4 50.0 44.9-108 6.46 20
Bis(2-chloroethyl)ether 0.667 0.342 0.319 51.3 47.8 32.5-112 7.03 26
Bis(2-chloroisopropyl)ether 0.667 0.393 0.364 59.0 54.6 40.4-99.0 7.60 20.7
4-Bromophenyl-phenylether 0.667 0.428 0.408 64.1 61.2 51.4-110 4.66 20
2-Chloronaphthalene 0.667 0.425 0.398 63.7 59.7 47.1-105 6.48 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 132 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 132 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938702
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-06,09,10,12,16,18,21,22,23,25,26,27
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188056-1 12/29/16 10:53 • (LCSD) R3188056-2 12/29/16 11:19
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
4-Chlorophenyl-phenylether 0.667 0.433 0.409 65.0 61.4 48.1-108 5.76 20
Chrysene 0.667 0.481 0.481 72.2 72.2 54.4-110 0.0300 20
Dibenz(a,h)anthracene 0.667 0.487 0.490 73.0 73.4 45.7-111 0.600 20
3,3-Dichlorobenzidine 0.667 0.453 0.461 67.9 69.1 21.0-101 1.76 22
2,4-Dinitrotoluene 0.667 0.515 0.498 77.2 74.6 53.0-112 3.34 20
2,6-Dinitrotoluene 0.667 0.462 0.441 69.2 66.1 51.6-110 4.70 20
Fluoranthene 0.667 0.441 0.427 66.2 64.1 53.7-110 3.19 20
Fluorene 0.667 0.459 0.435 68.8 65.2 51.1-109 5.35 20
Hexachlorobenzene 0.667 0.413 0.389 62.0 58.3 43.2-104 6.09 20.1
Hexachloro-1,3-butadiene 0.667 0.318 0.300 47.7 45.0 41.5-112 5.86 20
Hexachlorocyclopentadiene 0.667 0.463 0.427 69.5 64.0 13.5-123 8.22 20.7
Hexachloroethane 0.667 0.344 0.291 51.6 43.7 36.2-103 16.5 22.7
Indeno(1,2,3-cd)pyrene 0.667 0.487 0.488 73.0 73.2 47.5-109 0.370 20
Isophorone 0.667 0.400 0.367 60.0 55.0 28.8-104 8.60 20
Naphthalene 0.667 0.329 0.305 49.3 45.8 43.4-103 7.38 20
Nitrobenzene 0.667 0.336 0.316 50.4 47.4 40.7-109 6.17 21
n-Nitrosodimethylamine 0.667 0.309 0.253 46.3 38.0 18.1-122 19.7 23.5
n-Nitrosodiphenylamine 0.667 0.461 0.449 69.1 67.4 48.8-107 2.47 20
n-Nitrosodi-n-propylamine 0.667 0.418 0.385 62.6 57.7 43.3-109 8.21 20
Phenanthrene 0.667 0.457 0.442 68.5 66.3 51.6-107 3.24 20
Benzylbutyl phthalate 0.667 0.541 0.539 81.2 80.8 47.5-115 0.470 20
Bis(2-ethylhexyl)phthalate 0.667 0.538 0.534 80.6 80.0 48.1-116 0.800 20.5
Di-n-butyl phthalate 0.667 0.499 0.483 74.8 72.4 49.7-113 3.21 20
Diethyl phthalate 0.667 0.495 0.484 74.2 72.5 52.0-112 2.31 20
Dimethyl phthalate 0.667 0.469 0.453 70.3 67.9 51.4-108 3.53 20
Di-n-octyl phthalate 0.667 0.543 0.541 81.5 81.1 49.6-112 0.400 22
Pyrene 0.667 0.476 0.477 71.3 71.5 47.1-108 0.330 20
1,2,4-Trichlorobenzene 0.667 0.305 0.284 45.7 42.6 39.8-100 7.10 20
4-Chloro-3-methylphenol 0.667 0.394 0.368 59.0 55.2 51.1-113 6.73 20
2-Chlorophenol 0.667 0.368 0.326 55.2 48.9 40.8-103 12.0 20
2,4-Dichlorophenol 0.667 0.363 0.330 54.5 49.5 46.2-109 9.52 20
2,4-Dimethylphenol 0.667 0.369 0.345 55.3 51.7 42.2-110 6.61 20
4,6-Dinitro-2-methylphenol 0.667 0.430 0.351 64.4 52.7 23.1-119 20.1 23.7
2,4-Dinitrophenol 0.667 0.306 0.177 45.9 26.5 10.0-105 J3 53.6 36.5
2-Nitrophenol 0.667 0.349 0.318 52.3 47.7 44.2-113 9.21 20.9
4-Nitrophenol 0.667 0.460 0.452 68.9 67.8 34.8-109 1.56 20
Pentachlorophenol 0.667 0.357 0.327 53.6 49.0 16.2-102 8.91 22.9
Phenol 0.667 0.397 0.367 59.6 55.0 41.5-106 7.98 20
2,4,6-Trichlorophenol 0.667 0.444 0.407 66.5 61.0 44.4-108 8.62 20
(S) Nitrobenzene-d5 45.6 40.6 21.9-129
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 133 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 133 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938702
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-06,09,10,12,16,18,21,22,23,25,26,27
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188056-1 12/29/16 10:53 • (LCSD) R3188056-2 12/29/16 11:19
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
(S) 2-Fluorobiphenyl 60.2 54.2 34.9-129
(S) p-Terphenyl-d14 70.3 71.6 21.5-128
(S) Phenol-d5 57.2 50.8 26.3-121
(S) 2-Fluorophenol 55.6 46.4 21.1-116
(S) 2,4,6-Tribromophenol 60.7 54.7 21.6-142
L880142-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880142-16 12/29/16 16:04 • (MS) R3188056-4 12/29/16 16:30 • (MSD) R3188056-5 12/29/16 17:22
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.908 ND 0.633 0.698 69.7 76.8 1 32.2-134 9.70 27.3
Acenaphthylene 0.908 ND 0.658 0.705 72.5 77.7 1 38.7-129 6.95 25.9
Anthracene 0.908 ND 0.644 0.689 70.9 75.8 1 32.3-137 6.64 28.4
Benzidine 0.908 ND 0.0926 0.0903 0.290 0.0396 1 0.000-49.9 2.49 40
Benzo(a)anthracene 0.908 ND 0.616 0.671 67.8 73.9 1 33.3-124 8.64 29
Benzo(b)fluoranthene 0.908 ND 0.607 0.685 66.9 75.4 1 23.3-133 11.9 30.3
Benzo(k)fluoranthene 0.908 ND 0.598 0.676 65.9 74.4 1 31.0-129 12.2 26.7
Benzo(g,h,i)perylene 0.908 ND 0.573 0.584 63.1 64.3 1 10.0-127 1.95 31.9
Benzo(a)pyrene 0.908 ND 0.630 0.694 69.4 76.4 1 28.2-128 9.61 28.4
Bis(2-chlorethoxy)methane 0.908 ND 0.510 0.541 56.1 59.5 1 35.0-132 5.88 26.1
Bis(2-chloroethyl)ether 0.908 ND 0.521 0.549 57.3 60.5 1 28.8-128 5.35 33.6
Bis(2-chloroisopropyl)ether 0.908 ND 0.594 0.646 65.4 71.1 1 31.8-118 8.31 31.7
4-Bromophenyl-phenylether 0.908 ND 0.568 0.613 62.5 67.5 1 39.0-130 7.60 26
2-Chloronaphthalene 0.908 ND 0.601 0.647 66.2 71.3 1 37.5-123 7.42 26.5
4-Chlorophenyl-phenylether 0.908 ND 0.580 0.626 63.8 68.9 1 37.9-123 7.60 25.9
Chrysene 0.908 ND 0.650 0.714 71.5 78.6 1 36.3-129 9.43 28
Dibenz(a,h)anthracene 0.908 ND 0.588 0.613 64.7 67.5 1 10.5-128 4.18 29.5
3,3-Dichlorobenzidine 0.908 ND 0.596 0.517 65.7 56.9 1 10.0-129 14.2 40
2,4-Dinitrotoluene 0.908 ND 0.726 0.775 79.9 85.3 1 27.8-147 6.52 29.7
2,6-Dinitrotoluene 0.908 ND 0.647 0.691 71.3 76.1 1 36.5-137 6.47 29.7
Fluoranthene 0.908 ND 0.588 0.647 64.7 71.2 1 27.9-138 9.62 26.9
Fluorene 0.908 ND 0.621 0.674 68.4 74.2 1 34.0-133 8.24 27.1
Hexachlorobenzene 0.908 ND 0.555 0.596 61.1 65.6 1 34.4-116 7.02 25.4
Hexachloro-1,3-butadiene 0.908 ND 0.479 0.505 52.7 55.7 1 36.5-125 5.40 29.7
Hexachlorocyclopentadiene 0.908 ND 0.635 0.674 69.9 74.2 1 10.0-124 6.01 37.5
Hexachloroethane 0.908 ND 0.523 0.564 57.6 62.0 1 11.3-143 7.51 31.9
Indeno(1,2,3-cd)pyrene 0.908 ND 0.596 0.618 65.6 68.1 1 10.0-128 3.66 31.5
Isophorone 0.908 ND 0.559 0.593 61.5 65.3 1 25.7-116 5.94 27.7
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/30/16 18:56 134 of 142
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880142 12/31/16 16:11 134 of 142
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938702
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880142-06,09,10,12,16,18,21,22,23,25,26,27
L880142-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880142-16 12/29/16 16:04 • (MS) R3188056-4 12/29/16 16:30 • (MSD) R3188056-5 12/29/16 17:22
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.908 ND 0.488 0.517 53.7 56.9 1 36.4-121 5.64 27.2
Nitrobenzene 0.908 ND 0.494 0.526 54.4 57.9 1 30.9-134 6.10 27.8
n-Nitrosodimethylamine 0.908 ND 0.433 0.456 47.7 50.2 1 19.2-127 5.15 32
n-Nitrosodiphenylamine 0.908 ND 0.637 0.697 70.2 76.7 1 26.8-133 8.91 25.9
n-Nitrosodi-n-propylamine 0.908 ND 0.596 0.633 65.6 69.7 1 33.0-134 6.11 28.2
Phenanthrene 0.908 ND 0.624 0.680 68.7 74.9 1 30.8-137 8.61 26.5
Benzylbutyl phthalate 0.908 ND 0.698 0.761 76.9 83.8 1 33.4-128 8.59 28.5
Bis(2-ethylhexyl)phthalate 0.908 ND 0.678 0.734 74.6 80.8 1 21.8-141 7.96 35.2
Di-n-butyl phthalate 0.908 ND 0.635 0.699 69.9 76.9 1 32.2-133 9.50 25.9
Diethyl phthalate 0.908 ND 0.709 0.752 78.0 82.8 1 39.4-136 5.94 25.5
Dimethyl phthalate 0.908 ND 0.672 0.710 73.9 78.2 1 35.8-137 5.58 25.4
Di-n-octyl phthalate 0.908 ND 0.709 0.782 78.0 86.1 1 28.5-128 9.78 32.5
Pyrene 0.908 ND 0.630 0.670 69.3 73.8 1 24.1-130 6.27 29.9
1,2,4-Trichlorobenzene 0.908 ND 0.459 0.491 50.6 54.1 1 36.5-114 6.71 28.4
4-Chloro-3-methylphenol 0.908 ND 0.544 0.591 59.9 65.1 1 27.0-154 8.33 26.6
2-Chlorophenol 0.908 ND 0.560 0.592 61.7 65.2 1 33.2-121 5.48 29.3
2,4-Dichlorophenol 0.908 ND 0.523 0.556 57.6 61.2 1 34.8-134 6.04 27.3
2,4-Dimethylphenol 0.908 ND 0.545 0.577 60.0 63.5 1 12.3-149 5.59 32.3
4,6-Dinitro-2-methylphenol 0.908 ND 0.689 0.661 75.8 72.8 1 10.0-144 4.05 32.7
2,4-Dinitrophenol 0.908 ND 0.620 0.602 68.3 66.3 1 10.0-121 2.95 39.4
2-Nitrophenol 0.908 ND 0.521 0.550 57.3 60.6 1 29.5-144 5.47 29.9
4-Nitrophenol 0.908 ND 0.711 0.723 78.3 79.6 1 20.0-133 1.67 30.2
Pentachlorophenol 0.908 ND 0.612 0.641 67.4 70.5 1 10.0-139 4.51 28.3
Phenol 0.908 ND 0.576 0.603 63.4 66.4 1 25.1-130 4.56 29.6
2,4,6-Trichlorophenol 0.908 ND 0.647 0.679 71.3 74.8 1 33.8-133 4.85 28.1
(S) Nitrobenzene-d5 49.2 49.5 21.9-129
(S) 2-Fluorobiphenyl 62.0 63.5 34.9-129
(S) p-Terphenyl-d14 66.9 69.6 21.5-128
(S) Phenol-d5 59.7 62.5 26.3-121
(S) 2-Fluorophenol 61.4 62.1 21.1-116
(S) 2,4,6-Tribromophenol 63.6 67.3 21.6-142
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Our Locations
Alabama 40660
Alaska UST-080
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Georgia 1 923
Idaho TN00003
Illinois 200008
Indiana C-TN-01
Iowa 364
Kansas E-10277
Kentucky 1 90010
Kentucky 2 16
Louisiana AI30792
Maine TN0002
Maryland 324
Massachusetts M-TN003
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Mississippi TN00003
Missouri 340
Montana CERT0086
Nebraska NE-OS-15-05
Nevada TN-03-2002-34
New Hampshire 2975
New Jersey–NELAP TN002
New Mexico TN00003
New York 11742
North Carolina Env375
North Carolina 1 DW21704
North Carolina 2 41
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Ohio–VAP CL0069
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Oregon TN200002
Pennsylvania 68-02979
Rhode Island 221
South Carolina 84004
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A2LA – ISO 17025 1461.01
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USDA S-67674
State Accreditations
Third Party & Federal Accreditations
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our “one location” design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support oces, please
contact our main oce. ESC Lab Sciences performs all testing at our central laboratory.
1. Drinking Water 2. Underground Storage Tanks 3. Aquatic Toxicity 4. Chemical/Microbiological 5. Mold n/a Accreditation not applicable
1461.02A2LA – ISO 170255
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
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ANALYTICAL REPORT
December 30, 2016
Withers & Ravenel Eng. - Standard
Sample Delivery Group:L880528
Samples Received:12/22/2016
Project Number:02160652.0
Description:Townsends Plant
Report To:Patrick Farfour
115 MacKenan Drive
Cary, NC 27511
Entire Report Reviewed By:
December 30, 2016
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
December 30, 2016
Jason Romer
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 4
⁵Sr: Sample Results 5
MW-1 L880528-01 5
MW-A L880528-02 8
MW-B L880528-03 11
⁶Qc: Quality Control Summary 14
Wet Chemistry by Method 350.1 14
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH 15
Volatile Organic Compounds (GC/MS) by Method 8260B 16
Semi-Volatile Organic Compounds (GC) by Method MADEPE 20
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 21
⁷Gl: Glossary of Terms 25
⁸Al: Accreditations & Locations 26
⁹Sc: Chain of Custody 27
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L880528-01 GW J. Cates 12/21/16 08:50 12/22/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG939232 1 12/28/16 18:42 12/29/16 15:09 JF
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 15:37 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 19:28 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938592 1 12/28/16 05:24 12/28/16 05:24 DAH
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 20:13 12/28/16 20:13 JAH
Wet Chemistry by Method 350.1 WG938955 1 12/28/16 15:32 12/28/16 15:32 DR
Collected by Collected date/time Received date/time
MW-A L880528-02 GW J. Cates 12/21/16 11:00 12/22/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG939232 1 12/28/16 18:42 12/29/16 15:33 JF
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 15:58 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 19:07 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938592 1 12/28/16 05:47 12/28/16 05:47 DAH
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 20:46 12/28/16 20:46 JAH
Collected by Collected date/time Received date/time
MW-B L880528-03 GW J. Cates 12/21/16 10:15 12/22/16 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG939232 1 12/28/16 18:42 12/29/16 15:56 JF
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 16:19 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 18:46 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938592 1 12/28/16 06:11 12/28/16 06:11 DAH
Volatile Organic Compounds (GC/MS) by Method 8260B WG938592 5 12/29/16 18:09 12/29/16 18:09 BMB
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 21:19 12/28/16 21:19 JAH
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the
sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Sample Handling and Receiving
The analysis for 2-Chloroethyl Vinyl Ether was conducted from a chemically preserved container.
ESC Sample ID Project Sample ID Method
L880528-01 MW-1 8260B
L880528-02 MW-A 8260B
L880528-03 MW-B 8260B
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Jason Romer
Technical Service Representative
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880528
MW-1
Collected date/time: 12/21/16 08:50
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ammonia Nitrogen 109 100 1 12/28/2016 15:32 WG938955
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 12/28/2016 20:13 WG938472
Unadjusted C9-C12 Aliphatics ND 100 1 12/28/2016 20:13 WG938472
Unadjusted C9-C10 Aromatics ND 100 1 12/28/2016 20:13 WG938472
Total VPH ND 100 1 12/28/2016 20:13 WG938472
(S) 2,5-Dibromotoluene(FID)85.8 70.0-130 12/28/2016 20:13 WG938472
(S) 2,5-Dibromotoluene(PID)76.1 70.0-130 12/28/2016 20:13 WG938472
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/28/2016 05:24 WG938592
Acrolein ND J4 50.0 1 12/28/2016 05:24 WG938592
Acrylonitrile ND 10.0 1 12/28/2016 05:24 WG938592
Benzene ND 1.00 1 12/28/2016 05:24 WG938592
Bromobenzene ND 1.00 1 12/28/2016 05:24 WG938592
Bromodichloromethane ND 1.00 1 12/28/2016 05:24 WG938592
Bromoform ND 1.00 1 12/28/2016 05:24 WG938592
Bromomethane ND 5.00 1 12/28/2016 05:24 WG938592
n-Butylbenzene ND 1.00 1 12/28/2016 05:24 WG938592
sec-Butylbenzene 1.30 1.00 1 12/28/2016 05:24 WG938592
tert-Butylbenzene ND 1.00 1 12/28/2016 05:24 WG938592
Carbon tetrachloride ND 1.00 1 12/28/2016 05:24 WG938592
Chlorobenzene ND 1.00 1 12/28/2016 05:24 WG938592
Chlorodibromomethane ND 1.00 1 12/28/2016 05:24 WG938592
Chloroethane ND 5.00 1 12/28/2016 05:24 WG938592
2-Chloroethyl vinyl ether ND 50.0 1 12/28/2016 05:24 WG938592
Chloroform ND 5.00 1 12/28/2016 05:24 WG938592
Chloromethane ND 2.50 1 12/28/2016 05:24 WG938592
2-Chlorotoluene ND 1.00 1 12/28/2016 05:24 WG938592
4-Chlorotoluene ND 1.00 1 12/28/2016 05:24 WG938592
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/28/2016 05:24 WG938592
1,2-Dibromoethane ND 1.00 1 12/28/2016 05:24 WG938592
Dibromomethane ND 1.00 1 12/28/2016 05:24 WG938592
1,2-Dichlorobenzene ND 1.00 1 12/28/2016 05:24 WG938592
1,3-Dichlorobenzene ND 1.00 1 12/28/2016 05:24 WG938592
1,4-Dichlorobenzene ND 1.00 1 12/28/2016 05:24 WG938592
Dichlorodifluoromethane ND 5.00 1 12/28/2016 05:24 WG938592
1,1-Dichloroethane ND 1.00 1 12/28/2016 05:24 WG938592
1,2-Dichloroethane ND 1.00 1 12/28/2016 05:24 WG938592
1,1-Dichloroethene ND 1.00 1 12/28/2016 05:24 WG938592
cis-1,2-Dichloroethene ND 1.00 1 12/28/2016 05:24 WG938592
trans-1,2-Dichloroethene ND 1.00 1 12/28/2016 05:24 WG938592
1,2-Dichloropropane ND 1.00 1 12/28/2016 05:24 WG938592
1,1-Dichloropropene ND 1.00 1 12/28/2016 05:24 WG938592
1,3-Dichloropropane ND 1.00 1 12/28/2016 05:24 WG938592
cis-1,3-Dichloropropene ND 1.00 1 12/28/2016 05:24 WG938592
trans-1,3-Dichloropropene ND 1.00 1 12/28/2016 05:24 WG938592
2,2-Dichloropropane ND 1.00 1 12/28/2016 05:24 WG938592
Di-isopropyl ether ND 1.00 1 12/28/2016 05:24 WG938592
Ethylbenzene ND 1.00 1 12/28/2016 05:24 WG938592
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880528
MW-1
Collected date/time: 12/21/16 08:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Hexachloro-1,3-butadiene ND 1.00 1 12/28/2016 05:24 WG938592
Isopropylbenzene ND 1.00 1 12/28/2016 05:24 WG938592
p-Isopropyltoluene ND 1.00 1 12/28/2016 05:24 WG938592
2-Butanone (MEK)ND 10.0 1 12/28/2016 05:24 WG938592
Methylene Chloride ND 5.00 1 12/28/2016 05:24 WG938592
4-Methyl-2-pentanone (MIBK)ND 10.0 1 12/28/2016 05:24 WG938592
Methyl tert-butyl ether ND 1.00 1 12/28/2016 05:24 WG938592
Naphthalene ND 5.00 1 12/28/2016 05:24 WG938592
n-Propylbenzene ND 1.00 1 12/28/2016 05:24 WG938592
Styrene ND 1.00 1 12/28/2016 05:24 WG938592
1,1,1,2-Tetrachloroethane ND 1.00 1 12/28/2016 05:24 WG938592
1,1,2,2-Tetrachloroethane ND 1.00 1 12/28/2016 05:24 WG938592
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/28/2016 05:24 WG938592
Tetrachloroethene ND 1.00 1 12/28/2016 05:24 WG938592
Toluene ND 1.00 1 12/28/2016 05:24 WG938592
1,2,3-Trichlorobenzene ND 1.00 1 12/28/2016 05:24 WG938592
1,2,4-Trichlorobenzene ND 1.00 1 12/28/2016 05:24 WG938592
1,1,1-Trichloroethane ND 1.00 1 12/28/2016 05:24 WG938592
1,1,2-Trichloroethane ND 1.00 1 12/28/2016 05:24 WG938592
Trichloroethene ND 1.00 1 12/28/2016 05:24 WG938592
Trichlorofluoromethane ND 5.00 1 12/28/2016 05:24 WG938592
1,2,3-Trichloropropane ND 2.50 1 12/28/2016 05:24 WG938592
1,2,4-Trimethylbenzene ND 1.00 1 12/28/2016 05:24 WG938592
1,2,3-Trimethylbenzene ND 1.00 1 12/28/2016 05:24 WG938592
1,3,5-Trimethylbenzene ND 1.00 1 12/28/2016 05:24 WG938592
Vinyl chloride ND 1.00 1 12/28/2016 05:24 WG938592
Xylenes, Total ND 3.00 1 12/28/2016 05:24 WG938592
(S) Toluene-d8 105 90.0-115 12/28/2016 05:24 WG938592
(S) Dibromofluoromethane 102 79.0-121 12/28/2016 05:24 WG938592
(S) 4-Bromofluorobenzene 101 80.1-120 12/28/2016 05:24 WG938592
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/28/2016 15:37 WG939005
Unadjusted C19-C36 Aliphatics ND 100 1 12/28/2016 15:37 WG939005
Unadjusted C11-C22 Aromatics ND 100 1 12/28/2016 19:28 WG939005
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 12/28/2016 15:37 WG939005
(S) o-Terphenyl 68.9 40.0-140 12/28/2016 19:28 WG939005
(S) 1-Chloro-octadecane 60.1 40.0-140 12/28/2016 15:37 WG939005
(S) 2-Fluorobiphenyl 87.8 40.0-140 12/28/2016 19:28 WG939005
(S) 2-Bromonaphthalene 86.5 40.0-140 12/28/2016 19:28 WG939005
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 12/29/2016 15:09 WG939232
Acenaphthylene ND 1.00 1 12/29/2016 15:09 WG939232
Anthracene ND 1.00 1 12/29/2016 15:09 WG939232
Benzidine ND 10.0 1 12/29/2016 15:09 WG939232
Benzo(a)anthracene ND 1.00 1 12/29/2016 15:09 WG939232
Benzo(b)fluoranthene ND 1.00 1 12/29/2016 15:09 WG939232
Benzo(k)fluoranthene ND 1.00 1 12/29/2016 15:09 WG939232
Benzo(g,h,i)perylene ND 1.00 1 12/29/2016 15:09 WG939232
Benzo(a)pyrene ND 1.00 1 12/29/2016 15:09 WG939232
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880528
MW-1
Collected date/time: 12/21/16 08:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Bis(2-chlorethoxy)methane ND 10.0 1 12/29/2016 15:09 WG939232
Bis(2-chloroethyl)ether ND 10.0 1 12/29/2016 15:09 WG939232
Bis(2-chloroisopropyl)ether ND 10.0 1 12/29/2016 15:09 WG939232
4-Bromophenyl-phenylether ND 10.0 1 12/29/2016 15:09 WG939232
2-Chloronaphthalene ND 1.00 1 12/29/2016 15:09 WG939232
4-Chlorophenyl-phenylether ND 10.0 1 12/29/2016 15:09 WG939232
Chrysene ND 1.00 1 12/29/2016 15:09 WG939232
Dibenz(a,h)anthracene ND 1.00 1 12/29/2016 15:09 WG939232
3,3-Dichlorobenzidine ND 10.0 1 12/29/2016 15:09 WG939232
2,4-Dinitrotoluene ND 10.0 1 12/29/2016 15:09 WG939232
2,6-Dinitrotoluene ND 10.0 1 12/29/2016 15:09 WG939232
Fluoranthene ND 1.00 1 12/29/2016 15:09 WG939232
Fluorene ND 1.00 1 12/29/2016 15:09 WG939232
Hexachlorobenzene ND 1.00 1 12/29/2016 15:09 WG939232
Hexachloro-1,3-butadiene ND 10.0 1 12/29/2016 15:09 WG939232
Hexachlorocyclopentadiene ND 10.0 1 12/29/2016 15:09 WG939232
Hexachloroethane ND 10.0 1 12/29/2016 15:09 WG939232
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/29/2016 15:09 WG939232
Isophorone ND 10.0 1 12/29/2016 15:09 WG939232
Naphthalene ND 1.00 1 12/29/2016 15:09 WG939232
Nitrobenzene ND 10.0 1 12/29/2016 15:09 WG939232
n-Nitrosodimethylamine ND 10.0 1 12/29/2016 15:09 WG939232
n-Nitrosodiphenylamine ND 10.0 1 12/29/2016 15:09 WG939232
n-Nitrosodi-n-propylamine ND 10.0 1 12/29/2016 15:09 WG939232
Phenanthrene ND 1.00 1 12/29/2016 15:09 WG939232
Benzylbutyl phthalate ND 3.00 1 12/29/2016 15:09 WG939232
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/29/2016 15:09 WG939232
Di-n-butyl phthalate ND 3.00 1 12/29/2016 15:09 WG939232
Diethyl phthalate ND 3.00 1 12/29/2016 15:09 WG939232
Dimethyl phthalate ND 3.00 1 12/29/2016 15:09 WG939232
Di-n-octyl phthalate ND 3.00 1 12/29/2016 15:09 WG939232
Pyrene ND 1.00 1 12/29/2016 15:09 WG939232
1,2,4-Trichlorobenzene ND 10.0 1 12/29/2016 15:09 WG939232
4-Chloro-3-methylphenol ND 10.0 1 12/29/2016 15:09 WG939232
2-Chlorophenol ND 10.0 1 12/29/2016 15:09 WG939232
2,4-Dichlorophenol ND 10.0 1 12/29/2016 15:09 WG939232
2,4-Dimethylphenol ND 10.0 1 12/29/2016 15:09 WG939232
4,6-Dinitro-2-methylphenol ND 10.0 1 12/29/2016 15:09 WG939232
2,4-Dinitrophenol ND 10.0 1 12/29/2016 15:09 WG939232
2-Nitrophenol ND 10.0 1 12/29/2016 15:09 WG939232
4-Nitrophenol ND 10.0 1 12/29/2016 15:09 WG939232
Pentachlorophenol ND 10.0 1 12/29/2016 15:09 WG939232
Phenol ND 10.0 1 12/29/2016 15:09 WG939232
2,4,6-Trichlorophenol ND 10.0 1 12/29/2016 15:09 WG939232
(S) 2-Fluorophenol 16.9 10.0-77.9 12/29/2016 15:09 WG939232
(S) Phenol-d5 9.38 5.00-70.1 12/29/2016 15:09 WG939232
(S) Nitrobenzene-d5 52.5 21.8-123 12/29/2016 15:09 WG939232
(S) 2-Fluorobiphenyl 64.3 29.5-131 12/29/2016 15:09 WG939232
(S) 2,4,6-Tribromophenol 72.4 11.2-130 12/29/2016 15:09 WG939232
(S) p-Terphenyl-d14 78.8 29.3-137 12/29/2016 15:09 WG939232
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:05 7 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:12 7 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880528
MW-A
Collected date/time: 12/21/16 11:00
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 1390 100 1 12/28/2016 20:46 WG938472
Unadjusted C9-C12 Aliphatics 380 100 1 12/28/2016 20:46 WG938472
Unadjusted C9-C10 Aromatics 222 100 1 12/28/2016 20:46 WG938472
Total VPH 1990 100 1 12/28/2016 20:46 WG938472
(S) 2,5-Dibromotoluene(FID)88.0 70.0-130 12/28/2016 20:46 WG938472
(S) 2,5-Dibromotoluene(PID)73.9 70.0-130 12/28/2016 20:46 WG938472
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/28/2016 05:47 WG938592
Acrolein ND J4 50.0 1 12/28/2016 05:47 WG938592
Acrylonitrile ND 10.0 1 12/28/2016 05:47 WG938592
Benzene 92.6 1.00 1 12/28/2016 05:47 WG938592
Bromobenzene 2.70 1.00 1 12/28/2016 05:47 WG938592
Bromodichloromethane ND 1.00 1 12/28/2016 05:47 WG938592
Bromoform ND 1.00 1 12/28/2016 05:47 WG938592
Bromomethane ND 5.00 1 12/28/2016 05:47 WG938592
n-Butylbenzene 4.75 1.00 1 12/28/2016 05:47 WG938592
sec-Butylbenzene 4.69 1.00 1 12/28/2016 05:47 WG938592
tert-Butylbenzene ND 1.00 1 12/28/2016 05:47 WG938592
Carbon tetrachloride ND 1.00 1 12/28/2016 05:47 WG938592
Chlorobenzene ND 1.00 1 12/28/2016 05:47 WG938592
Chlorodibromomethane ND 1.00 1 12/28/2016 05:47 WG938592
Chloroethane ND 5.00 1 12/28/2016 05:47 WG938592
2-Chloroethyl vinyl ether ND 50.0 1 12/28/2016 05:47 WG938592
Chloroform ND 5.00 1 12/28/2016 05:47 WG938592
Chloromethane ND 2.50 1 12/28/2016 05:47 WG938592
2-Chlorotoluene ND 1.00 1 12/28/2016 05:47 WG938592
4-Chlorotoluene ND 1.00 1 12/28/2016 05:47 WG938592
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/28/2016 05:47 WG938592
1,2-Dibromoethane ND 1.00 1 12/28/2016 05:47 WG938592
Dibromomethane ND 1.00 1 12/28/2016 05:47 WG938592
1,2-Dichlorobenzene ND 1.00 1 12/28/2016 05:47 WG938592
1,3-Dichlorobenzene ND 1.00 1 12/28/2016 05:47 WG938592
1,4-Dichlorobenzene ND 1.00 1 12/28/2016 05:47 WG938592
Dichlorodifluoromethane ND 5.00 1 12/28/2016 05:47 WG938592
1,1-Dichloroethane ND 1.00 1 12/28/2016 05:47 WG938592
1,2-Dichloroethane ND 1.00 1 12/28/2016 05:47 WG938592
1,1-Dichloroethene ND 1.00 1 12/28/2016 05:47 WG938592
cis-1,2-Dichloroethene ND 1.00 1 12/28/2016 05:47 WG938592
trans-1,2-Dichloroethene ND 1.00 1 12/28/2016 05:47 WG938592
1,2-Dichloropropane ND 1.00 1 12/28/2016 05:47 WG938592
1,1-Dichloropropene ND 1.00 1 12/28/2016 05:47 WG938592
1,3-Dichloropropane ND 1.00 1 12/28/2016 05:47 WG938592
cis-1,3-Dichloropropene ND 1.00 1 12/28/2016 05:47 WG938592
trans-1,3-Dichloropropene ND 1.00 1 12/28/2016 05:47 WG938592
2,2-Dichloropropane ND 1.00 1 12/28/2016 05:47 WG938592
Di-isopropyl ether 11.7 1.00 1 12/28/2016 05:47 WG938592
Ethylbenzene 52.0 1.00 1 12/28/2016 05:47 WG938592
Hexachloro-1,3-butadiene ND 1.00 1 12/28/2016 05:47 WG938592
Isopropylbenzene 17.4 1.00 1 12/28/2016 05:47 WG938592
p-Isopropyltoluene ND 1.00 1 12/28/2016 05:47 WG938592
2-Butanone (MEK)ND 10.0 1 12/28/2016 05:47 WG938592
Methylene Chloride ND 5.00 1 12/28/2016 05:47 WG938592
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:05 8 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:12 8 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880528
MW-A
Collected date/time: 12/21/16 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
4-Methyl-2-pentanone (MIBK)ND 10.0 1 12/28/2016 05:47 WG938592
Methyl tert-butyl ether 102 1.00 1 12/28/2016 05:47 WG938592
Naphthalene 81.5 5.00 1 12/28/2016 05:47 WG938592
n-Propylbenzene 26.5 1.00 1 12/28/2016 05:47 WG938592
Styrene ND 1.00 1 12/28/2016 05:47 WG938592
1,1,1,2-Tetrachloroethane ND 1.00 1 12/28/2016 05:47 WG938592
1,1,2,2-Tetrachloroethane ND 1.00 1 12/28/2016 05:47 WG938592
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/28/2016 05:47 WG938592
Tetrachloroethene ND 1.00 1 12/28/2016 05:47 WG938592
Toluene 6.98 1.00 1 12/28/2016 05:47 WG938592
1,2,3-Trichlorobenzene ND 1.00 1 12/28/2016 05:47 WG938592
1,2,4-Trichlorobenzene ND 1.00 1 12/28/2016 05:47 WG938592
1,1,1-Trichloroethane ND 1.00 1 12/28/2016 05:47 WG938592
1,1,2-Trichloroethane ND 1.00 1 12/28/2016 05:47 WG938592
Trichloroethene ND 1.00 1 12/28/2016 05:47 WG938592
Trichlorofluoromethane ND 5.00 1 12/28/2016 05:47 WG938592
1,2,3-Trichloropropane ND 2.50 1 12/28/2016 05:47 WG938592
1,2,4-Trimethylbenzene 24.0 1.00 1 12/28/2016 05:47 WG938592
1,2,3-Trimethylbenzene 9.99 1.00 1 12/28/2016 05:47 WG938592
1,3,5-Trimethylbenzene 1.71 1.00 1 12/28/2016 05:47 WG938592
Vinyl chloride ND 1.00 1 12/28/2016 05:47 WG938592
Xylenes, Total 26.2 3.00 1 12/28/2016 05:47 WG938592
(S) Toluene-d8 105 90.0-115 12/28/2016 05:47 WG938592
(S) Dibromofluoromethane 99.0 79.0-121 12/28/2016 05:47 WG938592
(S) 4-Bromofluorobenzene 101 80.1-120 12/28/2016 05:47 WG938592
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/28/2016 15:58 WG939005
Unadjusted C19-C36 Aliphatics ND 100 1 12/28/2016 15:58 WG939005
Unadjusted C11-C22 Aromatics 413 100 1 12/28/2016 19:07 WG939005
Unadjusted Total Petroleum
Hydrocarbons 413 100 1 12/28/2016 15:58 WG939005
(S) o-Terphenyl 65.2 40.0-140 12/28/2016 19:07 WG939005
(S) 1-Chloro-octadecane 50.2 40.0-140 12/28/2016 15:58 WG939005
(S) 2-Fluorobiphenyl 80.8 40.0-140 12/28/2016 19:07 WG939005
(S) 2-Bromonaphthalene 80.5 40.0-140 12/28/2016 19:07 WG939005
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene 2.40 1.00 1 12/29/2016 15:33 WG939232
Acenaphthylene ND 1.00 1 12/29/2016 15:33 WG939232
Anthracene ND 1.00 1 12/29/2016 15:33 WG939232
Benzidine ND 10.0 1 12/29/2016 15:33 WG939232
Benzo(a)anthracene ND 1.00 1 12/29/2016 15:33 WG939232
Benzo(b)fluoranthene ND 1.00 1 12/29/2016 15:33 WG939232
Benzo(k)fluoranthene ND 1.00 1 12/29/2016 15:33 WG939232
Benzo(g,h,i)perylene ND 1.00 1 12/29/2016 15:33 WG939232
Benzo(a)pyrene ND 1.00 1 12/29/2016 15:33 WG939232
Bis(2-chlorethoxy)methane ND 10.0 1 12/29/2016 15:33 WG939232
Bis(2-chloroethyl)ether ND 10.0 1 12/29/2016 15:33 WG939232
Bis(2-chloroisopropyl)ether ND 10.0 1 12/29/2016 15:33 WG939232
4-Bromophenyl-phenylether ND 10.0 1 12/29/2016 15:33 WG939232
2-Chloronaphthalene ND 1.00 1 12/29/2016 15:33 WG939232
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:05 9 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:12 9 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880528
MW-A
Collected date/time: 12/21/16 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
4-Chlorophenyl-phenylether ND 10.0 1 12/29/2016 15:33 WG939232
Chrysene ND 1.00 1 12/29/2016 15:33 WG939232
Dibenz(a,h)anthracene ND 1.00 1 12/29/2016 15:33 WG939232
3,3-Dichlorobenzidine ND 10.0 1 12/29/2016 15:33 WG939232
2,4-Dinitrotoluene ND 10.0 1 12/29/2016 15:33 WG939232
2,6-Dinitrotoluene ND 10.0 1 12/29/2016 15:33 WG939232
Fluoranthene ND 1.00 1 12/29/2016 15:33 WG939232
Fluorene 2.51 1.00 1 12/29/2016 15:33 WG939232
Hexachlorobenzene ND 1.00 1 12/29/2016 15:33 WG939232
Hexachloro-1,3-butadiene ND 10.0 1 12/29/2016 15:33 WG939232
Hexachlorocyclopentadiene ND 10.0 1 12/29/2016 15:33 WG939232
Hexachloroethane ND 10.0 1 12/29/2016 15:33 WG939232
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/29/2016 15:33 WG939232
Isophorone ND 10.0 1 12/29/2016 15:33 WG939232
Naphthalene 46.3 1.00 1 12/29/2016 15:33 WG939232
Nitrobenzene ND 10.0 1 12/29/2016 15:33 WG939232
n-Nitrosodimethylamine ND 10.0 1 12/29/2016 15:33 WG939232
n-Nitrosodiphenylamine ND 10.0 1 12/29/2016 15:33 WG939232
n-Nitrosodi-n-propylamine ND 10.0 1 12/29/2016 15:33 WG939232
Phenanthrene 4.71 1.00 1 12/29/2016 15:33 WG939232
Benzylbutyl phthalate ND 3.00 1 12/29/2016 15:33 WG939232
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/29/2016 15:33 WG939232
Di-n-butyl phthalate ND 3.00 1 12/29/2016 15:33 WG939232
Diethyl phthalate ND 3.00 1 12/29/2016 15:33 WG939232
Dimethyl phthalate ND 3.00 1 12/29/2016 15:33 WG939232
Di-n-octyl phthalate ND 3.00 1 12/29/2016 15:33 WG939232
Pyrene ND 1.00 1 12/29/2016 15:33 WG939232
1,2,4-Trichlorobenzene ND 10.0 1 12/29/2016 15:33 WG939232
4-Chloro-3-methylphenol ND 10.0 1 12/29/2016 15:33 WG939232
2-Chlorophenol ND 10.0 1 12/29/2016 15:33 WG939232
2,4-Dichlorophenol ND 10.0 1 12/29/2016 15:33 WG939232
2,4-Dimethylphenol ND 10.0 1 12/29/2016 15:33 WG939232
4,6-Dinitro-2-methylphenol ND 10.0 1 12/29/2016 15:33 WG939232
2,4-Dinitrophenol ND 10.0 1 12/29/2016 15:33 WG939232
2-Nitrophenol ND 10.0 1 12/29/2016 15:33 WG939232
4-Nitrophenol ND 10.0 1 12/29/2016 15:33 WG939232
Pentachlorophenol ND 10.0 1 12/29/2016 15:33 WG939232
Phenol ND 10.0 1 12/29/2016 15:33 WG939232
2,4,6-Trichlorophenol ND 10.0 1 12/29/2016 15:33 WG939232
(S) 2-Fluorophenol 19.3 10.0-77.9 12/29/2016 15:33 WG939232
(S) Phenol-d5 11.0 5.00-70.1 12/29/2016 15:33 WG939232
(S) Nitrobenzene-d5 60.0 21.8-123 12/29/2016 15:33 WG939232
(S) 2-Fluorobiphenyl 63.5 29.5-131 12/29/2016 15:33 WG939232
(S) 2,4,6-Tribromophenol 72.9 11.2-130 12/29/2016 15:33 WG939232
(S) p-Terphenyl-d14 76.4 29.3-137 12/29/2016 15:33 WG939232
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:05 10 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:12 10 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880528
MW-B
Collected date/time: 12/21/16 10:15
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 4000 100 1 12/28/2016 21:19 WG938472
Unadjusted C9-C12 Aliphatics 1670 100 1 12/28/2016 21:19 WG938472
Unadjusted C9-C10 Aromatics 835 100 1 12/28/2016 21:19 WG938472
Total VPH 6500 100 1 12/28/2016 21:19 WG938472
(S) 2,5-Dibromotoluene(FID)86.7 70.0-130 12/28/2016 21:19 WG938472
(S) 2,5-Dibromotoluene(PID)69.7 J2 70.0-130 12/28/2016 21:19 WG938472
Sample Narrative:
MTDEQ VPH L880528-03 WG938472: Surrogate failure due to matrix interference.
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/28/2016 06:11 WG938592
Acrolein ND J4 50.0 1 12/28/2016 06:11 WG938592
Acrylonitrile ND 10.0 1 12/28/2016 06:11 WG938592
Benzene 332 5.00 5 12/29/2016 18:09 WG938592
Bromobenzene ND 1.00 1 12/28/2016 06:11 WG938592
Bromodichloromethane ND 1.00 1 12/28/2016 06:11 WG938592
Bromoform ND 1.00 1 12/28/2016 06:11 WG938592
Bromomethane ND 5.00 1 12/28/2016 06:11 WG938592
n-Butylbenzene 14.9 1.00 1 12/28/2016 06:11 WG938592
sec-Butylbenzene 8.90 1.00 1 12/28/2016 06:11 WG938592
tert-Butylbenzene ND 1.00 1 12/28/2016 06:11 WG938592
Carbon tetrachloride ND 1.00 1 12/28/2016 06:11 WG938592
Chlorobenzene ND 1.00 1 12/28/2016 06:11 WG938592
Chlorodibromomethane ND 1.00 1 12/28/2016 06:11 WG938592
Chloroethane ND 5.00 1 12/28/2016 06:11 WG938592
2-Chloroethyl vinyl ether ND 50.0 1 12/28/2016 06:11 WG938592
Chloroform ND 5.00 1 12/28/2016 06:11 WG938592
Chloromethane ND 2.50 1 12/28/2016 06:11 WG938592
2-Chlorotoluene ND 1.00 1 12/28/2016 06:11 WG938592
4-Chlorotoluene ND 1.00 1 12/28/2016 06:11 WG938592
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/28/2016 06:11 WG938592
1,2-Dibromoethane ND 1.00 1 12/28/2016 06:11 WG938592
Dibromomethane ND 1.00 1 12/28/2016 06:11 WG938592
1,2-Dichlorobenzene ND 1.00 1 12/28/2016 06:11 WG938592
1,3-Dichlorobenzene ND 1.00 1 12/28/2016 06:11 WG938592
1,4-Dichlorobenzene ND 1.00 1 12/28/2016 06:11 WG938592
Dichlorodifluoromethane ND 5.00 1 12/28/2016 06:11 WG938592
1,1-Dichloroethane ND 1.00 1 12/28/2016 06:11 WG938592
1,2-Dichloroethane ND 1.00 1 12/28/2016 06:11 WG938592
1,1-Dichloroethene ND 1.00 1 12/28/2016 06:11 WG938592
cis-1,2-Dichloroethene ND 1.00 1 12/28/2016 06:11 WG938592
trans-1,2-Dichloroethene ND 1.00 1 12/28/2016 06:11 WG938592
1,2-Dichloropropane ND 1.00 1 12/28/2016 06:11 WG938592
1,1-Dichloropropene ND 1.00 1 12/28/2016 06:11 WG938592
1,3-Dichloropropane ND 1.00 1 12/28/2016 06:11 WG938592
cis-1,3-Dichloropropene ND 1.00 1 12/28/2016 06:11 WG938592
trans-1,3-Dichloropropene ND 1.00 1 12/28/2016 06:11 WG938592
2,2-Dichloropropane ND 1.00 1 12/28/2016 06:11 WG938592
Di-isopropyl ether 2.70 1.00 1 12/28/2016 06:11 WG938592
Ethylbenzene 334 5.00 5 12/29/2016 18:09 WG938592
Hexachloro-1,3-butadiene ND 1.00 1 12/28/2016 06:11 WG938592
Isopropylbenzene 53.6 1.00 1 12/28/2016 06:11 WG938592
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:05 11 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:12 11 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880528
MW-B
Collected date/time: 12/21/16 10:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
p-Isopropyltoluene 4.17 1.00 1 12/28/2016 06:11 WG938592
2-Butanone (MEK)ND 10.0 1 12/28/2016 06:11 WG938592
Methylene Chloride ND 5.00 1 12/28/2016 06:11 WG938592
4-Methyl-2-pentanone (MIBK)ND 10.0 1 12/28/2016 06:11 WG938592
Methyl tert-butyl ether 211 5.00 5 12/29/2016 18:09 WG938592
Naphthalene 328 25.0 5 12/29/2016 18:09 WG938592
n-Propylbenzene 144 1.00 1 12/28/2016 06:11 WG938592
Styrene 1.49 1.00 1 12/28/2016 06:11 WG938592
1,1,1,2-Tetrachloroethane ND 1.00 1 12/28/2016 06:11 WG938592
1,1,2,2-Tetrachloroethane ND 1.00 1 12/28/2016 06:11 WG938592
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/28/2016 06:11 WG938592
Tetrachloroethene ND 1.00 1 12/28/2016 06:11 WG938592
Toluene 28.6 1.00 1 12/28/2016 06:11 WG938592
1,2,3-Trichlorobenzene ND 1.00 1 12/28/2016 06:11 WG938592
1,2,4-Trichlorobenzene ND 1.00 1 12/28/2016 06:11 WG938592
1,1,1-Trichloroethane ND 1.00 1 12/28/2016 06:11 WG938592
1,1,2-Trichloroethane ND 1.00 1 12/28/2016 06:11 WG938592
Trichloroethene ND 1.00 1 12/28/2016 06:11 WG938592
Trichlorofluoromethane ND 5.00 1 12/28/2016 06:11 WG938592
1,2,3-Trichloropropane ND 2.50 1 12/28/2016 06:11 WG938592
1,2,4-Trimethylbenzene 211 5.00 5 12/29/2016 18:09 WG938592
1,2,3-Trimethylbenzene 56.8 1.00 1 12/28/2016 06:11 WG938592
1,3,5-Trimethylbenzene 109 1.00 1 12/28/2016 06:11 WG938592
Vinyl chloride ND 1.00 1 12/28/2016 06:11 WG938592
Xylenes, Total 147 3.00 1 12/28/2016 06:11 WG938592
(S) Toluene-d8 103 90.0-115 12/28/2016 06:11 WG938592
(S) Toluene-d8 104 90.0-115 12/29/2016 18:09 WG938592
(S) Dibromofluoromethane 96.5 79.0-121 12/29/2016 18:09 WG938592
(S) Dibromofluoromethane 97.5 79.0-121 12/28/2016 06:11 WG938592
(S) 4-Bromofluorobenzene 103 80.1-120 12/28/2016 06:11 WG938592
(S) 4-Bromofluorobenzene 99.4 80.1-120 12/29/2016 18:09 WG938592
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/28/2016 16:19 WG939005
Unadjusted C19-C36 Aliphatics ND 100 1 12/28/2016 16:19 WG939005
Unadjusted C11-C22 Aromatics 404 100 1 12/28/2016 18:46 WG939005
Unadjusted Total Petroleum
Hydrocarbons 404 100 1 12/28/2016 16:19 WG939005
(S) o-Terphenyl 60.1 40.0-140 12/28/2016 18:46 WG939005
(S) 1-Chloro-octadecane 43.7 40.0-140 12/28/2016 16:19 WG939005
(S) 2-Fluorobiphenyl 79.1 40.0-140 12/28/2016 18:46 WG939005
(S) 2-Bromonaphthalene 78.2 40.0-140 12/28/2016 18:46 WG939005
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 12/29/2016 15:56 WG939232
Acenaphthylene ND 1.00 1 12/29/2016 15:56 WG939232
Anthracene ND 1.00 1 12/29/2016 15:56 WG939232
Benzidine ND 10.0 1 12/29/2016 15:56 WG939232
Benzo(a)anthracene ND 1.00 1 12/29/2016 15:56 WG939232
Benzo(b)fluoranthene ND 1.00 1 12/29/2016 15:56 WG939232
Benzo(k)fluoranthene ND 1.00 1 12/29/2016 15:56 WG939232
Benzo(g,h,i)perylene ND 1.00 1 12/29/2016 15:56 WG939232
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880528 12/30/16 15:12 12 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880528
MW-B
Collected date/time: 12/21/16 10:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Benzo(a)pyrene ND 1.00 1 12/29/2016 15:56 WG939232
Bis(2-chlorethoxy)methane ND 10.0 1 12/29/2016 15:56 WG939232
Bis(2-chloroethyl)ether ND 10.0 1 12/29/2016 15:56 WG939232
Bis(2-chloroisopropyl)ether ND 10.0 1 12/29/2016 15:56 WG939232
4-Bromophenyl-phenylether ND 10.0 1 12/29/2016 15:56 WG939232
2-Chloronaphthalene ND 1.00 1 12/29/2016 15:56 WG939232
4-Chlorophenyl-phenylether ND 10.0 1 12/29/2016 15:56 WG939232
Chrysene ND 1.00 1 12/29/2016 15:56 WG939232
Dibenz(a,h)anthracene ND 1.00 1 12/29/2016 15:56 WG939232
3,3-Dichlorobenzidine ND 10.0 1 12/29/2016 15:56 WG939232
2,4-Dinitrotoluene ND 10.0 1 12/29/2016 15:56 WG939232
2,6-Dinitrotoluene ND 10.0 1 12/29/2016 15:56 WG939232
Fluoranthene ND 1.00 1 12/29/2016 15:56 WG939232
Fluorene ND 1.00 1 12/29/2016 15:56 WG939232
Hexachlorobenzene ND 1.00 1 12/29/2016 15:56 WG939232
Hexachloro-1,3-butadiene ND 10.0 1 12/29/2016 15:56 WG939232
Hexachlorocyclopentadiene ND 10.0 1 12/29/2016 15:56 WG939232
Hexachloroethane ND 10.0 1 12/29/2016 15:56 WG939232
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/29/2016 15:56 WG939232
Isophorone ND 10.0 1 12/29/2016 15:56 WG939232
Naphthalene 199 1.00 1 12/29/2016 15:56 WG939232
Nitrobenzene ND 10.0 1 12/29/2016 15:56 WG939232
n-Nitrosodimethylamine ND 10.0 1 12/29/2016 15:56 WG939232
n-Nitrosodiphenylamine ND 10.0 1 12/29/2016 15:56 WG939232
n-Nitrosodi-n-propylamine ND 10.0 1 12/29/2016 15:56 WG939232
Phenanthrene ND 1.00 1 12/29/2016 15:56 WG939232
Benzylbutyl phthalate ND 3.00 1 12/29/2016 15:56 WG939232
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/29/2016 15:56 WG939232
Di-n-butyl phthalate ND 3.00 1 12/29/2016 15:56 WG939232
Diethyl phthalate ND 3.00 1 12/29/2016 15:56 WG939232
Dimethyl phthalate ND 3.00 1 12/29/2016 15:56 WG939232
Di-n-octyl phthalate ND 3.00 1 12/29/2016 15:56 WG939232
Pyrene ND 1.00 1 12/29/2016 15:56 WG939232
1,2,4-Trichlorobenzene ND 10.0 1 12/29/2016 15:56 WG939232
4-Chloro-3-methylphenol ND 10.0 1 12/29/2016 15:56 WG939232
2-Chlorophenol ND 10.0 1 12/29/2016 15:56 WG939232
2,4-Dichlorophenol ND 10.0 1 12/29/2016 15:56 WG939232
2,4-Dimethylphenol ND 10.0 1 12/29/2016 15:56 WG939232
4,6-Dinitro-2-methylphenol ND 10.0 1 12/29/2016 15:56 WG939232
2,4-Dinitrophenol ND 10.0 1 12/29/2016 15:56 WG939232
2-Nitrophenol ND 10.0 1 12/29/2016 15:56 WG939232
4-Nitrophenol ND 10.0 1 12/29/2016 15:56 WG939232
Pentachlorophenol ND 10.0 1 12/29/2016 15:56 WG939232
Phenol ND 10.0 1 12/29/2016 15:56 WG939232
2,4,6-Trichlorophenol ND 10.0 1 12/29/2016 15:56 WG939232
(S) 2-Fluorophenol 19.6 10.0-77.9 12/29/2016 15:56 WG939232
(S) Phenol-d5 12.7 5.00-70.1 12/29/2016 15:56 WG939232
(S) Nitrobenzene-d5 56.2 21.8-123 12/29/2016 15:56 WG939232
(S) 2-Fluorobiphenyl 65.0 29.5-131 12/29/2016 15:56 WG939232
(S) 2,4,6-Tribromophenol 68.5 11.2-130 12/29/2016 15:56 WG939232
(S) p-Terphenyl-d14 75.6 29.3-137 12/29/2016 15:56 WG939232
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938955
Wet Chemistry by Method 350.1 L880528-01
Method Blank (MB)
(MB) R3187735-1 12/28/16 14:36
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ammonia Nitrogen U 31.7 100
L880359-06 Original Sample (OS) • Duplicate (DUP)
(OS) L880359-06 12/28/16 14:46 • (DUP) R3187735-4 12/28/16 14:47
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte ug/l ug/l %%
Ammonia Nitrogen 48.0 48.0 1 0 J 20
L880368-03 Original Sample (OS) • Duplicate (DUP)
(OS) L880368-03 12/28/16 15:02 • (DUP) R3187735-6 12/28/16 15:03
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte ug/l ug/l %%
Ammonia Nitrogen ND 0.000 1 0 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187735-2 12/28/16 14:38 • (LCSD) R3187735-3 12/28/16 14:40
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ammonia Nitrogen 7500 6950 7020 93 94 90-110 1 20
L880368-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L880368-01 12/28/16 14:57 • (MS) R3187735-5 12/28/16 14:59
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ammonia Nitrogen 10000 ND 9720 97 1 90-110
L880528-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880528-01 12/28/16 15:32 • (MS) R3187735-7 12/28/16 15:33 • (MSD) R3187735-8 12/28/16 15:35
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Ammonia Nitrogen 10000 109 10100 10000 100 99 1 90-110 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938472
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH L880528-01,02,03
Method Blank (MB)
(MB) R3187959-3 12/28/16 12:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID)83.6 70.0-130
(S) 2,5-Dibromotoluene(PID)75.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187959-1 12/28/16 11:14 • (LCSD) R3187959-2 12/28/16 11:46
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1240 1200 104 99.6 70.0-130 4.02 25
Unadjusted C9-C12 Aliphatics 1400 1600 1560 114 112 70.0-130 2.50 25
Unadjusted C9-C10 Aromatics 200 184 179 91.9 89.6 70.0-130 2.64 25
Total VPH 2800 3030 2940 108 105 70.0-130 3.13 25
(S) 2,5-Dibromotoluene(FID) 82.2 82.5 70.0-130
(S) 2,5-Dibromotoluene(PID) 73.4 73.9 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938592
Volatile Organic Compounds (GC/MS) by Method 8260B L880528-01,02,03
Method Blank (MB)
(MB) R3188017-3 12/27/16 21:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 10.0 50.0
Acrolein U 8.87 50.0
Acrylonitrile U 1.87 10.0
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride U 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
2-Chloroethyl vinyl ether U 3.01 50.0
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
cis-1,3-Dichloropropene U 0.418 1.00
trans-1,3-Dichloropropene U 0.419 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938592
Volatile Organic Compounds (GC/MS) by Method 8260B L880528-01,02,03
Method Blank (MB)
(MB) R3188017-3 12/27/16 21:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Hexachloro-1,3-butadiene U 0.256 1.00
Isopropylbenzene U 0.326 1.00
p-Isopropyltoluene U 0.350 1.00
2-Butanone (MEK)U 3.93 10.0
Methylene Chloride U 1.00 5.00
4-Methyl-2-pentanone (MIBK)U 2.14 10.0
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.349 1.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,1,2-Trichlorotrifluoroethane U 0.303 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
Trichloroethene U 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,3-Trimethylbenzene U 0.321 1.00
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Vinyl chloride U 0.259 1.00
Xylenes, Total U 1.06 3.00
(S) Toluene-d8 105 90.0-115
(S) Dibromofluoromethane 102 79.0-121
(S) 4-Bromofluorobenzene 100 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188017-1 12/27/16 20:41 • (LCSD) R3188017-2 12/27/16 21:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 125 116 124 92.4 99.4 28.7-175 7.30 20.9
Acrolein 125 312 324 250 260 40.4-172 J4 J4 3.75 20
Acrylonitrile 125 119 130 95.2 104 58.2-145 8.53 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938592
Volatile Organic Compounds (GC/MS) by Method 8260B L880528-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188017-1 12/27/16 20:41 • (LCSD) R3188017-2 12/27/16 21:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 25.0 27.3 26.4 109 106 73.0-122 3.17 20
Bromobenzene 25.0 24.9 25.2 99.8 101 81.5-115 1.14 20
Bromodichloromethane 25.0 25.3 25.4 101 102 75.5-121 0.210 20
Bromoform 25.0 20.9 22.4 83.6 89.5 71.5-131 6.77 20
Bromomethane 25.0 25.5 23.6 102 94.5 22.4-187 7.84 20
n-Butylbenzene 25.0 25.9 25.0 104 99.9 75.9-134 3.56 20
sec-Butylbenzene 25.0 24.3 23.3 97.1 93.4 80.6-126 3.92 20
tert-Butylbenzene 25.0 24.9 24.0 99.5 96.0 79.3-127 3.59 20
Carbon tetrachloride 25.0 22.7 21.6 90.9 86.3 70.9-129 5.13 20
Chlorobenzene 25.0 26.3 26.3 105 105 79.7-122 0.210 20
Chlorodibromomethane 25.0 24.7 25.2 98.9 101 78.2-124 1.98 20
Chloroethane 25.0 28.8 26.6 115 106 41.2-153 7.89 20
2-Chloroethyl vinyl ether 125 133 138 106 110 23.4-162 3.75 23.5
Chloroform 25.0 26.8 26.4 107 105 73.2-125 1.71 20
Chloromethane 25.0 30.6 28.8 123 115 55.8-134 6.03 20
2-Chlorotoluene 25.0 26.1 25.7 104 103 76.4-125 1.51 20
4-Chlorotoluene 25.0 26.7 26.4 107 106 81.5-121 1.01 20
1,2-Dibromo-3-Chloropropane 25.0 19.2 20.8 76.7 83.0 64.8-131 7.91 20
1,2-Dibromoethane 25.0 23.8 24.3 95.0 97.1 79.8-122 2.19 20
Dibromomethane 25.0 24.2 24.4 96.8 97.8 79.5-118 1.01 20
1,2-Dichlorobenzene 25.0 25.6 25.9 102 103 84.7-118 1.05 20
1,3-Dichlorobenzene 25.0 25.1 24.9 100 99.5 77.6-127 0.970 20
1,4-Dichlorobenzene 25.0 24.4 24.2 97.8 96.8 82.2-114 1.02 20
Dichlorodifluoromethane 25.0 24.2 22.6 96.8 90.2 56.0-134 7.07 20
1,1-Dichloroethane 25.0 27.2 26.6 109 106 71.7-127 2.49 20
1,2-Dichloroethane 25.0 24.3 24.2 97.3 96.7 65.3-126 0.630 20
1,1-Dichloroethene 25.0 28.1 25.9 113 104 59.9-137 8.17 20
cis-1,2-Dichloroethene 25.0 27.8 27.5 111 110 77.3-122 1.36 20
trans-1,2-Dichloroethene 25.0 28.7 28.0 115 112 72.6-125 2.65 20
1,2-Dichloropropane 25.0 26.7 26.3 107 105 77.4-125 1.53 20
1,1-Dichloropropene 25.0 27.7 26.0 111 104 72.5-127 6.39 20
1,3-Dichloropropane 25.0 24.9 24.9 99.8 99.4 80.6-115 0.330 20
cis-1,3-Dichloropropene 25.0 25.7 26.0 103 104 77.7-124 1.10 20
trans-1,3-Dichloropropene 25.0 26.7 26.7 107 107 73.5-127 0.270 20
2,2-Dichloropropane 25.0 27.5 26.3 110 105 61.3-134 4.43 20
Di-isopropyl ether 25.0 23.9 24.0 95.7 96.1 65.1-135 0.380 20
Ethylbenzene 25.0 26.4 25.8 105 103 80.9-121 1.98 20
Hexachloro-1,3-butadiene 25.0 20.6 19.8 82.5 79.1 73.7-133 4.26 20
Isopropylbenzene 25.0 25.2 24.5 101 98.1 81.6-124 2.68 20
p-Isopropyltoluene 25.0 26.0 25.4 104 101 77.6-129 2.52 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938592
Volatile Organic Compounds (GC/MS) by Method 8260B L880528-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188017-1 12/27/16 20:41 • (LCSD) R3188017-2 12/27/16 21:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
2-Butanone (MEK)125 108 115 86.2 92.0 46.4-155 6.52 20
Methylene Chloride 25.0 26.1 25.4 104 102 69.5-120 2.66 20
4-Methyl-2-pentanone (MIBK)125 106 111 84.7 88.7 63.3-138 4.60 20
Methyl tert-butyl ether 25.0 24.0 24.5 96.1 98.0 70.1-125 1.95 20
Naphthalene 25.0 22.3 23.4 89.4 93.6 69.7-134 4.63 20
n-Propylbenzene 25.0 26.0 25.3 104 101 81.9-122 2.78 20
Styrene 25.0 27.5 26.5 110 106 79.9-124 3.68 20
1,1,1,2-Tetrachloroethane 25.0 24.3 24.7 97.3 98.7 78.5-125 1.39 20
1,1,2,2-Tetrachloroethane 25.0 21.5 22.8 86.0 91.3 79.3-123 5.94 20
Tetrachloroethene 25.0 24.6 23.9 98.3 95.7 73.5-130 2.67 20
Toluene 25.0 26.8 26.1 107 104 77.9-116 2.66 20
1,1,2-Trichlorotrifluoroethane 25.0 25.9 23.7 103 94.9 62.0-141 8.60 20
1,2,3-Trichlorobenzene 25.0 21.9 22.4 87.8 89.5 75.7-134 1.95 20
1,2,4-Trichlorobenzene 25.0 24.2 24.8 96.8 99.3 76.1-136 2.55 20
1,1,1-Trichloroethane 25.0 25.5 23.7 102 94.7 71.1-129 7.65 20
1,1,2-Trichloroethane 25.0 24.7 25.3 98.8 101 81.6-120 2.33 20
Trichloroethene 25.0 27.3 26.1 109 105 79.5-121 4.44 20
Trichlorofluoromethane 25.0 24.5 22.9 98.1 91.4 49.1-157 6.97 20
1,2,3-Trichloropropane 25.0 23.3 24.5 93.1 97.9 74.9-124 5.04 20
1,2,3-Trimethylbenzene 25.0 25.4 25.6 101 102 79.9-118 0.760 20
1,2,4-Trimethylbenzene 25.0 25.5 25.3 102 101 79.0-122 0.880 20
1,3,5-Trimethylbenzene 25.0 24.6 24.1 98.5 96.4 81.0-123 2.19 20
Vinyl chloride 25.0 27.7 25.7 111 103 61.5-134 7.37 20
Xylenes, Total 75.0 78.3 77.0 104 103 79.2-122 1.66 20
(S) Toluene-d8 104 104 90.0-115
(S) Dibromofluoromethane 103 102 79.0-121
(S) 4-Bromofluorobenzene 101 102 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939005
Semi-Volatile Organic Compounds (GC) by Method MADEPE L880528-01,02,03
Method Blank (MB)
(MB) R3187776-1 12/28/16 13:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
Unadjusted Total Petroleum
Hydrocarbons U 33.3 100
(S) 1-Chloro-octadecane 65.1 40.0-140
Method Blank (MB)
(MB) R3187776-4 12/28/16 14:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 66.3 40.0-140
(S) 2-Fluorobiphenyl 78.4 40.0-140
(S) 2-Bromonaphthalene 77.3 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187776-2 12/28/16 13:52 • (LCSD) R3187776-3 12/28/16 14:13
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 266 277 44.3 46.1 40.0-140 3.99 25
Unadjusted C19-C36 Aliphatics 800 483 499 60.4 62.4 40.0-140 3.13 25
(S) 1-Chloro-octadecane 47.7 53.8 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187776-5 12/28/16 14:55 • (LCSD) R3187776-6 12/28/16 15:16
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1060 1140 62.5 67.2 40.0-140 7.23 25
(S) o-Terphenyl 63.7 66.0 40.0-140
(S) 2-Fluorobiphenyl 78.8 84.8 40.0-140
(S) 2-Bromonaphthalene 78.3 83.1 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939232
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880528-01,02,03
Method Blank (MB)
(MB) R3188028-3 12/29/16 11:13
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(a)pyrene U 0.340 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Bis(2-chloroethyl)ether U 1.62 10.0
Benzo(g,h,i)perylene U 0.161 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
n-Nitrosodimethylamine U 1.26 10.0
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Phenanthrene U 0.366 1.00
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Bis(2-ethylhexyl)phthalate 0.986 J 0.709 3.00
Isophorone U 0.272 10.0
Di-n-butyl phthalate U 0.266 3.00
Naphthalene U 0.372 1.00
Pyrene U 0.330 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodiphenylamine U 0.304 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Benzylbutyl phthalate U 0.275 3.00
2-Chlorophenol U 0.283 10.0
Diethyl phthalate U 0.282 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939232
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880528-01,02,03
Method Blank (MB)
(MB) R3188028-3 12/29/16 11:13
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate 1.35 J 0.278 3.00
Phenol U 0.334 10.0
1,2,4-Trichlorobenzene U 0.355 10.0
4-Chloro-3-methylphenol U 0.263 10.0
2,4-Dichlorophenol U 0.284 10.0
2,4-Dinitrophenol U 3.25 10.0
2,4-Dimethylphenol U 0.264 10.0
4,6-Dinitro-2-methylphenol U 2.62 10.0
2-Nitrophenol U 0.320 10.0
4-Nitrophenol U 2.01 10.0
Pentachlorophenol U 0.313 10.0
2,4,6-Trichlorophenol U 0.297 10.0
(S) Nitrobenzene-d5 54.3 21.8-123
(S) 2-Fluorobiphenyl 62.0 29.5-131
(S) p-Terphenyl-d14 68.8 29.3-137
(S) Phenol-d5 21.5 5.00-70.1
(S) 2-Fluorophenol 34.4 10.0-77.9
(S) 2,4,6-Tribromophenol 55.1 11.2-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188028-1 12/29/16 10:26 • (LCSD) R3188028-2 12/29/16 10:49
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzo(a)pyrene 50.0 35.2 35.3 70.3 70.6 45.6-106 0.310 20
Bis(2-chloroethyl)ether 50.0 27.5 26.9 55.1 53.7 22.6-108 2.49 27.9
3,3-Dichlorobenzidine 50.0 41.3 42.3 82.7 84.6 27.2-142 2.36 22.3
2,4-Dinitrotoluene 50.0 38.6 37.9 77.1 75.8 31.2-105 1.73 22
Acenaphthene 50.0 36.8 36.7 73.5 73.3 38.7-109 0.310 21.5
Acenaphthylene 50.0 38.8 38.0 77.5 76.0 36.0-106 2.04 21
Anthracene 50.0 39.8 38.7 79.7 77.4 43.6-113 2.89 18.8
Benzidine 50.0 27.7 32.5 55.5 65.0 10.0-165 15.8 40
Benzo(a)anthracene 50.0 38.2 38.1 76.5 76.3 51.2-112 0.230 20
n-Nitrosodimethylamine 50.0 16.5 15.6 33.0 31.2 10.0-80.1 5.49 37.5
Benzo(b)fluoranthene 50.0 39.8 40.3 79.6 80.6 47.6-111 1.25 20
Benzo(k)fluoranthene 50.0 38.4 37.3 76.8 74.5 49.4-114 3.00 20
Benzo(g,h,i)perylene 50.0 41.7 41.5 83.4 83.0 45.2-117 0.380 20
Phenanthrene 50.0 38.3 37.5 76.6 75.0 46.4-113 2.02 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939232
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880528-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188028-1 12/29/16 10:26 • (LCSD) R3188028-2 12/29/16 10:49
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bis(2-ethylhexyl)phthalate 50.0 37.7 37.3 75.4 74.6 36.9-134 1.04 23.6
Bis(2-chlorethoxy)methane 50.0 31.0 30.1 61.9 60.2 37.2-111 2.82 24.1
Di-n-butyl phthalate 50.0 41.4 40.7 82.9 81.4 41.8-120 1.75 20.2
Bis(2-chloroisopropyl)ether 50.0 32.9 31.9 65.8 63.7 32.9-100 3.29 25.1
4-Bromophenyl-phenylether 50.0 41.1 39.3 82.2 78.5 40.7-116 4.52 21
Pyrene 50.0 40.1 39.7 80.1 79.4 46.3-117 0.970 20
2-Chloronaphthalene 50.0 33.7 33.4 67.3 66.9 33.6-105 0.740 23
4-Chlorophenyl-phenylether 50.0 39.0 37.9 78.0 75.7 39.0-113 3.01 20.9
Chrysene 50.0 42.1 41.6 84.2 83.3 54.6-120 1.13 20
Dibenz(a,h)anthracene 50.0 36.2 35.7 72.4 71.5 42.8-118 1.20 20
2-Chlorophenol 50.0 28.1 29.1 56.2 58.2 26.2-91.5 3.51 26.5
2,4-Dinitrophenol 50.0 22.4 19.3 44.8 38.6 24.2-128 15.0 20.5
2,6-Dinitrotoluene 50.0 37.2 36.9 74.4 73.8 30.6-106 0.850 23.1
Fluoranthene 50.0 43.1 41.9 86.3 83.8 45.9-115 2.86 20
Fluorene 50.0 38.5 38.0 77.0 76.1 41.0-112 1.20 20.2
Hexachlorobenzene 50.0 41.1 40.2 82.1 80.5 38.5-116 2.01 20.1
Hexachloro-1,3-butadiene 50.0 28.9 28.1 57.8 56.2 16.1-104 2.88 31.2
Hexachlorocyclopentadiene 50.0 34.4 33.4 68.8 66.9 10.0-121 2.78 27.9
Hexachloroethane 50.0 24.9 24.6 49.9 49.3 16.5-89.8 1.19 30.7
Indeno(1,2,3-cd)pyrene 50.0 36.9 36.3 73.8 72.6 45.0-116 1.74 20
Isophorone 50.0 32.8 32.1 65.7 64.2 35.4-112 2.20 21.5
Phenol 50.0 12.3 13.0 24.7 26.1 10.0-57.9 5.50 35
Naphthalene 50.0 29.7 29.9 59.3 59.7 32.2-101 0.670 23.8
Nitrobenzene 50.0 29.5 28.9 59.0 57.7 31.4-106 2.21 25.7
n-Nitrosodiphenylamine 50.0 39.3 37.8 78.6 75.7 44.4-113 3.83 20
n-Nitrosodi-n-propylamine 50.0 30.2 29.4 60.5 58.8 33.2-106 2.85 23.7
Benzylbutyl phthalate 50.0 36.6 36.1 73.2 72.2 31.8-123 1.29 20.7
Diethyl phthalate 50.0 39.3 39.3 78.5 78.5 36.5-129 0.0100 20
Dimethyl phthalate 50.0 39.1 38.6 78.3 77.1 35.3-128 1.52 20.8
Di-n-octyl phthalate 50.0 37.4 37.8 74.8 75.6 39.7-112 0.990 21.1
1,2,4-Trichlorobenzene 50.0 28.0 28.2 56.1 56.5 22.9-96.1 0.710 27.5
4-Chloro-3-methylphenol 50.0 31.4 31.9 62.8 63.8 35.7-100 1.57 22.9
2,4-Dichlorophenol 50.0 32.8 33.7 65.6 67.4 31.4-103 2.82 24.9
2,4-Dimethylphenol 50.0 30.7 30.0 61.4 59.9 31.9-107 2.43 25.7
4,6-Dinitro-2-methylphenol 50.0 38.1 37.0 76.2 74.1 18.4-148 2.85 24.4
2-Nitrophenol 50.0 31.5 32.0 63.1 64.1 25.9-106 1.56 26.9
4-Nitrophenol 50.0 10.7 10.2 21.3 20.3 10.0-52.7 4.98 40
Pentachlorophenol 50.0 34.5 31.0 69.1 62.1 10.0-97.4 10.6 35.1
2,4,6-Trichlorophenol 50.0 38.2 38.5 76.4 76.9 29.8-107 0.700 24.1
(S) Nitrobenzene-d5 52.0 52.9 21.8-123
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939232
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880528-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188028-1 12/29/16 10:26 • (LCSD) R3188028-2 12/29/16 10:49
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
(S) 2-Fluorobiphenyl 66.0 64.2 29.5-131
(S) p-Terphenyl-d14 75.7 73.5 29.3-137
(S) Phenol-d5 22.2 23.4 5.00-70.1
(S) 2-Fluorophenol 32.4 34.0 10.0-77.9
(S) 2,4,6-Tribromophenol 72.9 70.3 11.2-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Our Locations
Alabama 40660
Alaska UST-080
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Arkansas 88-0469
California 01157CA
Colorado TN00003
Conneticut PH-0197
Florida E87487
Georgia NELAP
Georgia 1 923
Idaho TN00003
Illinois 200008
Indiana C-TN-01
Iowa 364
Kansas E-10277
Kentucky 1 90010
Kentucky 2 16
Louisiana AI30792
Maine TN0002
Maryland 324
Massachusetts M-TN003
Michigan 9958
Minnesota 047-999-395
Mississippi TN00003
Missouri 340
Montana CERT0086
Nebraska NE-OS-15-05
Nevada TN-03-2002-34
New Hampshire 2975
New Jersey–NELAP TN002
New Mexico TN00003
New York 11742
North Carolina Env375
North Carolina 1 DW21704
North Carolina 2 41
North Dakota R-140
Ohio–VAP CL0069
Oklahoma 9915
Oregon TN200002
Pennsylvania 68-02979
Rhode Island 221
South Carolina 84004
South Dakota n/a
Tennessee 1 4 2006
Texas T 104704245-07-TX
Texas 5 LAB0152
Utah 6157585858
Vermont VT2006
Virginia 109
Washington C1915
West Virginia 233
Wisconsin 9980939910
Wyoming A2LA
A2LA – ISO 17025 1461.01
Canada 1461.01
EPA–Crypto TN00003
AIHA 100789
DOD 1461.01
USDA S-67674
State Accreditations
Third Party & Federal Accreditations
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our “one location” design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
1. Drinking Water 2. Underground Storage Tanks 3. Aquatic Toxicity 4. Chemical/Microbiological 5. Mold n/a Accreditation not applicable
1461.02A2LA – ISO 170255
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
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ANALYTICAL REPORT
January 03, 2017
Withers & Ravenel Eng. - Standard
Sample Delivery Group: L880657
Samples Received:12/23/2016
Project Number:02160652.0
Description:Former Townsends Plant
Site:TOWNSEND
Report To:Patrick Farfour
115 MacKenan Drive
Cary, NC 27511
Entire Report Reviewed By:
January 03, 2017
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
January 03, 2017
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 4
⁵Sr: Sample Results 5
MW-3 L880657-01 5
MW-6 L880657-02 9
MW-7 L880657-03 13
⁶Qc: Quality Control Summary 17
Wet Chemistry by Method 350.1 17
Mercury by Method 7470A 18
Metals (ICP) by Method 6010C 19
Metals (ICPMS) by Method 6020 20
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH 21
Volatile Organic Compounds (GC/MS) by Method 8260B 22
Semi-Volatile Organic Compounds (GC) by Method MADEPE 28
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 29
⁷Gl: Glossary of Terms 33
⁸Al: Accreditations & Locations 34
⁹Sc: Chain of Custody 35
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-3 L880657-01 GW Mike Fekete 12/22/16 10:20 12/23/16 08:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG938411 1 12/24/16 05:59 12/27/16 14:31 NJB
Metals (ICP) by Method 6010C WG938981 1 12/28/16 09:48 12/28/16 14:19 CCE
Metals (ICPMS) by Method 6020 WG938446 1 12/28/16 14:20 12/30/16 13:14 JPD
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG939381 1 12/29/16 16:23 12/30/16 13:09 SNR
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 16:40 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 18:25 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938827 1 12/30/16 13:32 12/30/16 13:32 JHH
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 21:51 12/28/16 21:51 JAH
Wet Chemistry by Method 350.1 WG940116 1 01/03/17 11:17 01/03/17 11:17 DR
Collected by Collected date/time Received date/time
MW-6 L880657-02 GW Mike Fekete 12/22/16 09:40 12/23/16 08:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG938411 1 12/24/16 05:59 12/27/16 14:54 NJB
Metals (ICP) by Method 6010C WG938981 1 12/28/16 09:48 12/28/16 14:21 CCE
Metals (ICPMS) by Method 6020 WG938446 1 12/28/16 14:20 12/30/16 13:18 JPD
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG939381 1 12/29/16 16:23 12/30/16 13:33 SNR
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 17:01 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 18:04 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938827 1 12/30/16 13:46 12/30/16 13:46 JHH
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 22:24 12/28/16 22:24 JAH
Wet Chemistry by Method 350.1 WG940116 1 01/03/17 11:25 01/03/17 11:25 DR
Collected by Collected date/time Received date/time
MW-7 L880657-03 GW Mike Fekete 12/22/16 09:00 12/23/16 08:30
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG938411 1 12/24/16 05:59 12/27/16 14:57 NJB
Metals (ICP) by Method 6010C WG938981 1 12/28/16 09:48 12/28/16 14:24 CCE
Metals (ICPMS) by Method 6020 WG938446 1 12/28/16 14:20 12/30/16 13:21 JPD
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG939381 1 12/29/16 16:23 12/30/16 13:57 SNR
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 17:22 KLM
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG939005 1 12/28/16 07:38 12/28/16 17:43 KLM
Volatile Organic Compounds (GC/MS) by Method 8260B WG938827 1 12/30/16 15:05 12/30/16 15:05 JHH
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH WG938472 1 12/28/16 22:57 12/28/16 22:57 JAH
Wet Chemistry by Method 350.1 WG940116 1 01/03/17 11:26 01/03/17 11:26 DR
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the
sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Sample Handling and Receiving
The analysis for 2-Chloroethyl Vinyl Ether was conducted from a chemically preserved container.
ESC Sample ID Project Sample ID Method
L880657-01 MW-3 8260B
L880657-02 MW-6 8260B
L880657-03 MW-7 8260B
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Jimmy Hunt
Technical Service Representative
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880657
MW-3
Collected date/time: 12/22/16 10:20
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ammonia Nitrogen ND 100 1 01/03/2017 11:17 WG940116
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Mercury ND 0.200 1 12/27/2016 14:31 WG938411
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Arsenic ND 10.0 1 12/28/2016 14:19 WG938981
Barium ND 5.00 1 12/28/2016 14:19 WG938981
Chromium ND 10.0 1 12/28/2016 14:19 WG938981
Lead ND 5.00 1 12/28/2016 14:19 WG938981
Selenium ND 10.0 1 12/28/2016 14:19 WG938981
Silver ND 5.00 1 12/28/2016 14:19 WG938981
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Cadmium ND 1.00 1 12/30/2016 13:14 WG938446
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 12/28/2016 21:51 WG938472
Unadjusted C9-C12 Aliphatics ND 100 1 12/28/2016 21:51 WG938472
Unadjusted C9-C10 Aromatics ND 100 1 12/28/2016 21:51 WG938472
Total VPH ND 100 1 12/28/2016 21:51 WG938472
(S) 2,5-Dibromotoluene(FID) 82.1 70.0-130 12/28/2016 21:51 WG938472
(S) 2,5-Dibromotoluene(PID) 70.2 70.0-130 12/28/2016 21:51 WG938472
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/30/2016 13:32 WG938827
Acrolein ND J4 50.0 1 12/30/2016 13:32 WG938827
Acrylonitrile ND 10.0 1 12/30/2016 13:32 WG938827
Benzene ND 1.00 1 12/30/2016 13:32 WG938827
Bromobenzene ND 1.00 1 12/30/2016 13:32 WG938827
Bromodichloromethane ND 1.00 1 12/30/2016 13:32 WG938827
Bromoform ND 1.00 1 12/30/2016 13:32 WG938827
Bromomethane ND 5.00 1 12/30/2016 13:32 WG938827
n-Butylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
sec-Butylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
tert-Butylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
Carbon tetrachloride ND 1.00 1 12/30/2016 13:32 WG938827
Chlorobenzene ND 1.00 1 12/30/2016 13:32 WG938827
Chlorodibromomethane ND 1.00 1 12/30/2016 13:32 WG938827
Chloroethane ND 5.00 1 12/30/2016 13:32 WG938827
2-Chloroethyl vinyl ether ND 50.0 1 12/30/2016 13:32 WG938827
Chloroform ND 5.00 1 12/30/2016 13:32 WG938827
Chloromethane ND 2.50 1 12/30/2016 13:32 WG938827
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880657
MW-3
Collected date/time: 12/22/16 10:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Chlorotoluene ND 1.00 1 12/30/2016 13:32 WG938827
4-Chlorotoluene ND 1.00 1 12/30/2016 13:32 WG938827
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/30/2016 13:32 WG938827
1,2-Dibromoethane ND 1.00 1 12/30/2016 13:32 WG938827
Dibromomethane ND 1.00 1 12/30/2016 13:32 WG938827
1,2-Dichlorobenzene ND 1.00 1 12/30/2016 13:32 WG938827
1,3-Dichlorobenzene ND 1.00 1 12/30/2016 13:32 WG938827
1,4-Dichlorobenzene ND 1.00 1 12/30/2016 13:32 WG938827
Dichlorodifluoromethane ND 5.00 1 12/30/2016 13:32 WG938827
1,1-Dichloroethane ND 1.00 1 12/30/2016 13:32 WG938827
1,2-Dichloroethane ND 1.00 1 12/30/2016 13:32 WG938827
1,1-Dichloroethene ND 1.00 1 12/30/2016 13:32 WG938827
cis-1,2-Dichloroethene ND 1.00 1 12/30/2016 13:32 WG938827
trans-1,2-Dichloroethene ND 1.00 1 12/30/2016 13:32 WG938827
1,2-Dichloropropane ND 1.00 1 12/30/2016 13:32 WG938827
1,1-Dichloropropene ND 1.00 1 12/30/2016 13:32 WG938827
1,3-Dichloropropane ND 1.00 1 12/30/2016 13:32 WG938827
cis-1,3-Dichloropropene ND 1.00 1 12/30/2016 13:32 WG938827
trans-1,3-Dichloropropene ND 1.00 1 12/30/2016 13:32 WG938827
2,2-Dichloropropane ND 1.00 1 12/30/2016 13:32 WG938827
Di-isopropyl ether ND 1.00 1 12/30/2016 13:32 WG938827
Ethylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
Hexachloro-1,3-butadiene ND 1.00 1 12/30/2016 13:32 WG938827
Isopropylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
p-Isopropyltoluene ND 1.00 1 12/30/2016 13:32 WG938827
2-Butanone (MEK)ND 10.0 1 12/30/2016 13:32 WG938827
Methylene Chloride ND 5.00 1 12/30/2016 13:32 WG938827
4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/30/2016 13:32 WG938827
Methyl tert-butyl ether ND 1.00 1 12/30/2016 13:32 WG938827
Naphthalene ND 5.00 1 12/30/2016 13:32 WG938827
n-Propylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
Styrene ND 1.00 1 12/30/2016 13:32 WG938827
1,1,1,2-Tetrachloroethane ND 1.00 1 12/30/2016 13:32 WG938827
1,1,2,2-Tetrachloroethane ND 1.00 1 12/30/2016 13:32 WG938827
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/30/2016 13:32 WG938827
Tetrachloroethene ND 1.00 1 12/30/2016 13:32 WG938827
Toluene ND 1.00 1 12/30/2016 13:32 WG938827
1,2,3-Trichlorobenzene ND 1.00 1 12/30/2016 13:32 WG938827
1,2,4-Trichlorobenzene ND 1.00 1 12/30/2016 13:32 WG938827
1,1,1-Trichloroethane ND 1.00 1 12/30/2016 13:32 WG938827
1,1,2-Trichloroethane ND 1.00 1 12/30/2016 13:32 WG938827
Trichloroethene ND 1.00 1 12/30/2016 13:32 WG938827
Trichlorofluoromethane ND 5.00 1 12/30/2016 13:32 WG938827
1,2,3-Trichloropropane ND 2.50 1 12/30/2016 13:32 WG938827
1,2,4-Trimethylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
1,2,3-Trimethylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
1,3,5-Trimethylbenzene ND 1.00 1 12/30/2016 13:32 WG938827
Vinyl chloride ND 1.00 1 12/30/2016 13:32 WG938827
Xylenes, Total ND 3.00 1 12/30/2016 13:32 WG938827
(S) Toluene-d8 106 90.0-115 12/30/2016 13:32 WG938827
(S) Dibromofluoromethane 101 79.0-121 12/30/2016 13:32 WG938827
(S) 4-Bromofluorobenzene 117 80.1-120 12/30/2016 13:32 WG938827
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880657
MW-3
Collected date/time: 12/22/16 10:20
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/28/2016 16:40 WG939005
Unadjusted C19-C36 Aliphatics ND 100 1 12/28/2016 16:40 WG939005
Unadjusted C11-C22 Aromatics ND 100 1 12/28/2016 18:25 WG939005
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 12/28/2016 16:40 WG939005
(S) o-Terphenyl 69.0 40.0-140 12/28/2016 18:25 WG939005
(S) 1-Chloro-octadecane 50.7 40.0-140 12/28/2016 16:40 WG939005
(S) 2-Fluorobiphenyl 85.0 40.0-140 12/28/2016 18:25 WG939005
(S) 2-Bromonaphthalene 84.0 40.0-140 12/28/2016 18:25 WG939005
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 12/30/2016 13:09 WG939381
Acenaphthylene ND 1.00 1 12/30/2016 13:09 WG939381
Anthracene ND 1.00 1 12/30/2016 13:09 WG939381
Benzidine ND 10.0 1 12/30/2016 13:09 WG939381
Benzo(a)anthracene ND 1.00 1 12/30/2016 13:09 WG939381
Benzo(b)fluoranthene ND 1.00 1 12/30/2016 13:09 WG939381
Benzo(k)fluoranthene ND 1.00 1 12/30/2016 13:09 WG939381
Benzo(g,h,i)perylene ND 1.00 1 12/30/2016 13:09 WG939381
Benzo(a)pyrene ND 1.00 1 12/30/2016 13:09 WG939381
Bis(2-chlorethoxy)methane ND 10.0 1 12/30/2016 13:09 WG939381
Bis(2-chloroethyl)ether ND 10.0 1 12/30/2016 13:09 WG939381
Bis(2-chloroisopropyl)ether ND 10.0 1 12/30/2016 13:09 WG939381
4-Bromophenyl-phenylether ND 10.0 1 12/30/2016 13:09 WG939381
2-Chloronaphthalene ND 1.00 1 12/30/2016 13:09 WG939381
4-Chlorophenyl-phenylether ND 10.0 1 12/30/2016 13:09 WG939381
Chrysene ND 1.00 1 12/30/2016 13:09 WG939381
Dibenz(a,h)anthracene ND 1.00 1 12/30/2016 13:09 WG939381
3,3-Dichlorobenzidine ND 10.0 1 12/30/2016 13:09 WG939381
2,4-Dinitrotoluene ND 10.0 1 12/30/2016 13:09 WG939381
2,6-Dinitrotoluene ND 10.0 1 12/30/2016 13:09 WG939381
Fluoranthene ND 1.00 1 12/30/2016 13:09 WG939381
Fluorene ND 1.00 1 12/30/2016 13:09 WG939381
Hexachlorobenzene ND 1.00 1 12/30/2016 13:09 WG939381
Hexachloro-1,3-butadiene ND 10.0 1 12/30/2016 13:09 WG939381
Hexachlorocyclopentadiene ND 10.0 1 12/30/2016 13:09 WG939381
Hexachloroethane ND 10.0 1 12/30/2016 13:09 WG939381
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/30/2016 13:09 WG939381
Isophorone ND 10.0 1 12/30/2016 13:09 WG939381
Naphthalene ND 1.00 1 12/30/2016 13:09 WG939381
Nitrobenzene ND 10.0 1 12/30/2016 13:09 WG939381
n-Nitrosodimethylamine ND 10.0 1 12/30/2016 13:09 WG939381
n-Nitrosodiphenylamine ND 10.0 1 12/30/2016 13:09 WG939381
n-Nitrosodi-n-propylamine ND 10.0 1 12/30/2016 13:09 WG939381
Phenanthrene ND 1.00 1 12/30/2016 13:09 WG939381
Benzylbutyl phthalate ND 3.00 1 12/30/2016 13:09 WG939381
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/30/2016 13:09 WG939381
Di-n-butyl phthalate ND 3.00 1 12/30/2016 13:09 WG939381
Diethyl phthalate ND 3.00 1 12/30/2016 13:09 WG939381
Dimethyl phthalate ND 3.00 1 12/30/2016 13:09 WG939381
Di-n-octyl phthalate ND 3.00 1 12/30/2016 13:09 WG939381
Pyrene ND 1.00 1 12/30/2016 13:09 WG939381
1,2,4-Trichlorobenzene ND 10.0 1 12/30/2016 13:09 WG939381
4-Chloro-3-methylphenol ND 10.0 1 12/30/2016 13:09 WG939381
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L880657
MW-3
Collected date/time: 12/22/16 10:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Chlorophenol ND 10.0 1 12/30/2016 13:09 WG939381
2,4-Dichlorophenol ND 10.0 1 12/30/2016 13:09 WG939381
2,4-Dimethylphenol ND 10.0 1 12/30/2016 13:09 WG939381
4,6-Dinitro-2-methylphenol ND 10.0 1 12/30/2016 13:09 WG939381
2,4-Dinitrophenol ND 10.0 1 12/30/2016 13:09 WG939381
2-Nitrophenol ND 10.0 1 12/30/2016 13:09 WG939381
4-Nitrophenol ND 10.0 1 12/30/2016 13:09 WG939381
Pentachlorophenol ND 10.0 1 12/30/2016 13:09 WG939381
Phenol ND 10.0 1 12/30/2016 13:09 WG939381
2,4,6-Trichlorophenol ND 10.0 1 12/30/2016 13:09 WG939381
(S) 2-Fluorophenol 27.2 10.0-77.9 12/30/2016 13:09 WG939381
(S) Phenol-d5 16.4 5.00-70.1 12/30/2016 13:09 WG939381
(S) Nitrobenzene-d5 46.4 21.8-123 12/30/2016 13:09 WG939381
(S) 2-Fluorobiphenyl 62.7 29.5-131 12/30/2016 13:09 WG939381
(S) 2,4,6-Tribromophenol 60.6 11.2-130 12/30/2016 13:09 WG939381
(S) p-Terphenyl-d14 77.0 29.3-137 12/30/2016 13:09 WG939381
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880657
MW-6
Collected date/time: 12/22/16 09:40
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ammonia Nitrogen ND 100 1 01/03/2017 11:25 WG940116
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Mercury ND 0.200 1 12/27/2016 14:54 WG938411
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Arsenic ND 10.0 1 12/28/2016 14:21 WG938981
Barium 21.1 5.00 1 12/28/2016 14:21 WG938981
Chromium ND 10.0 1 12/28/2016 14:21 WG938981
Lead ND 5.00 1 12/28/2016 14:21 WG938981
Selenium ND 10.0 1 12/28/2016 14:21 WG938981
Silver ND 5.00 1 12/28/2016 14:21 WG938981
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Cadmium ND 1.00 1 12/30/2016 13:18 WG938446
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 12/28/2016 22:24 WG938472
Unadjusted C9-C12 Aliphatics ND 100 1 12/28/2016 22:24 WG938472
Unadjusted C9-C10 Aromatics ND 100 1 12/28/2016 22:24 WG938472
Total VPH ND 100 1 12/28/2016 22:24 WG938472
(S) 2,5-Dibromotoluene(FID) 84.4 70.0-130 12/28/2016 22:24 WG938472
(S) 2,5-Dibromotoluene(PID) 74.3 70.0-130 12/28/2016 22:24 WG938472
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/30/2016 13:46 WG938827
Acrolein ND J4 50.0 1 12/30/2016 13:46 WG938827
Acrylonitrile ND 10.0 1 12/30/2016 13:46 WG938827
Benzene ND 1.00 1 12/30/2016 13:46 WG938827
Bromobenzene ND 1.00 1 12/30/2016 13:46 WG938827
Bromodichloromethane ND 1.00 1 12/30/2016 13:46 WG938827
Bromoform ND 1.00 1 12/30/2016 13:46 WG938827
Bromomethane ND 5.00 1 12/30/2016 13:46 WG938827
n-Butylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
sec-Butylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
tert-Butylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
Carbon tetrachloride ND 1.00 1 12/30/2016 13:46 WG938827
Chlorobenzene ND 1.00 1 12/30/2016 13:46 WG938827
Chlorodibromomethane ND 1.00 1 12/30/2016 13:46 WG938827
Chloroethane ND 5.00 1 12/30/2016 13:46 WG938827
2-Chloroethyl vinyl ether ND 50.0 1 12/30/2016 13:46 WG938827
Chloroform ND 5.00 1 12/30/2016 13:46 WG938827
Chloromethane ND 2.50 1 12/30/2016 13:46 WG938827
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880657
MW-6
Collected date/time: 12/22/16 09:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Chlorotoluene ND 1.00 1 12/30/2016 13:46 WG938827
4-Chlorotoluene ND 1.00 1 12/30/2016 13:46 WG938827
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/30/2016 13:46 WG938827
1,2-Dibromoethane ND 1.00 1 12/30/2016 13:46 WG938827
Dibromomethane ND 1.00 1 12/30/2016 13:46 WG938827
1,2-Dichlorobenzene ND 1.00 1 12/30/2016 13:46 WG938827
1,3-Dichlorobenzene ND 1.00 1 12/30/2016 13:46 WG938827
1,4-Dichlorobenzene ND 1.00 1 12/30/2016 13:46 WG938827
Dichlorodifluoromethane ND 5.00 1 12/30/2016 13:46 WG938827
1,1-Dichloroethane ND 1.00 1 12/30/2016 13:46 WG938827
1,2-Dichloroethane ND 1.00 1 12/30/2016 13:46 WG938827
1,1-Dichloroethene ND 1.00 1 12/30/2016 13:46 WG938827
cis-1,2-Dichloroethene ND 1.00 1 12/30/2016 13:46 WG938827
trans-1,2-Dichloroethene ND 1.00 1 12/30/2016 13:46 WG938827
1,2-Dichloropropane ND 1.00 1 12/30/2016 13:46 WG938827
1,1-Dichloropropene ND 1.00 1 12/30/2016 13:46 WG938827
1,3-Dichloropropane ND 1.00 1 12/30/2016 13:46 WG938827
cis-1,3-Dichloropropene ND 1.00 1 12/30/2016 13:46 WG938827
trans-1,3-Dichloropropene ND 1.00 1 12/30/2016 13:46 WG938827
2,2-Dichloropropane ND 1.00 1 12/30/2016 13:46 WG938827
Di-isopropyl ether ND 1.00 1 12/30/2016 13:46 WG938827
Ethylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
Hexachloro-1,3-butadiene ND 1.00 1 12/30/2016 13:46 WG938827
Isopropylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
p-Isopropyltoluene ND 1.00 1 12/30/2016 13:46 WG938827
2-Butanone (MEK)ND 10.0 1 12/30/2016 13:46 WG938827
Methylene Chloride ND 5.00 1 12/30/2016 13:46 WG938827
4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/30/2016 13:46 WG938827
Methyl tert-butyl ether ND 1.00 1 12/30/2016 13:46 WG938827
Naphthalene ND 5.00 1 12/30/2016 13:46 WG938827
n-Propylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
Styrene ND 1.00 1 12/30/2016 13:46 WG938827
1,1,1,2-Tetrachloroethane ND 1.00 1 12/30/2016 13:46 WG938827
1,1,2,2-Tetrachloroethane ND 1.00 1 12/30/2016 13:46 WG938827
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/30/2016 13:46 WG938827
Tetrachloroethene ND 1.00 1 12/30/2016 13:46 WG938827
Toluene ND 1.00 1 12/30/2016 13:46 WG938827
1,2,3-Trichlorobenzene ND 1.00 1 12/30/2016 13:46 WG938827
1,2,4-Trichlorobenzene ND 1.00 1 12/30/2016 13:46 WG938827
1,1,1-Trichloroethane ND 1.00 1 12/30/2016 13:46 WG938827
1,1,2-Trichloroethane ND 1.00 1 12/30/2016 13:46 WG938827
Trichloroethene ND 1.00 1 12/30/2016 13:46 WG938827
Trichlorofluoromethane ND 5.00 1 12/30/2016 13:46 WG938827
1,2,3-Trichloropropane ND 2.50 1 12/30/2016 13:46 WG938827
1,2,4-Trimethylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
1,2,3-Trimethylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
1,3,5-Trimethylbenzene ND 1.00 1 12/30/2016 13:46 WG938827
Vinyl chloride ND 1.00 1 12/30/2016 13:46 WG938827
Xylenes, Total ND 3.00 1 12/30/2016 13:46 WG938827
(S) Toluene-d8 107 90.0-115 12/30/2016 13:46 WG938827
(S) Dibromofluoromethane 102 79.0-121 12/30/2016 13:46 WG938827
(S) 4-Bromofluorobenzene 119 80.1-120 12/30/2016 13:46 WG938827
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 14:59 10 of 36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 10 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880657
MW-6
Collected date/time: 12/22/16 09:40
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/28/2016 17:01 WG939005
Unadjusted C19-C36 Aliphatics ND 100 1 12/28/2016 17:01 WG939005
Unadjusted C11-C22 Aromatics ND 100 1 12/28/2016 18:04 WG939005
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 12/28/2016 17:01 WG939005
(S) o-Terphenyl 62.8 40.0-140 12/28/2016 18:04 WG939005
(S) 1-Chloro-octadecane 54.0 40.0-140 12/28/2016 17:01 WG939005
(S) 2-Fluorobiphenyl 78.4 40.0-140 12/28/2016 18:04 WG939005
(S) 2-Bromonaphthalene 78.4 40.0-140 12/28/2016 18:04 WG939005
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 12/30/2016 13:33 WG939381
Acenaphthylene ND 1.00 1 12/30/2016 13:33 WG939381
Anthracene ND 1.00 1 12/30/2016 13:33 WG939381
Benzidine ND 10.0 1 12/30/2016 13:33 WG939381
Benzo(a)anthracene ND 1.00 1 12/30/2016 13:33 WG939381
Benzo(b)fluoranthene ND 1.00 1 12/30/2016 13:33 WG939381
Benzo(k)fluoranthene ND 1.00 1 12/30/2016 13:33 WG939381
Benzo(g,h,i)perylene ND 1.00 1 12/30/2016 13:33 WG939381
Benzo(a)pyrene ND 1.00 1 12/30/2016 13:33 WG939381
Bis(2-chlorethoxy)methane ND 10.0 1 12/30/2016 13:33 WG939381
Bis(2-chloroethyl)ether ND 10.0 1 12/30/2016 13:33 WG939381
Bis(2-chloroisopropyl)ether ND 10.0 1 12/30/2016 13:33 WG939381
4-Bromophenyl-phenylether ND 10.0 1 12/30/2016 13:33 WG939381
2-Chloronaphthalene ND 1.00 1 12/30/2016 13:33 WG939381
4-Chlorophenyl-phenylether ND 10.0 1 12/30/2016 13:33 WG939381
Chrysene ND 1.00 1 12/30/2016 13:33 WG939381
Dibenz(a,h)anthracene ND 1.00 1 12/30/2016 13:33 WG939381
3,3-Dichlorobenzidine ND 10.0 1 12/30/2016 13:33 WG939381
2,4-Dinitrotoluene ND 10.0 1 12/30/2016 13:33 WG939381
2,6-Dinitrotoluene ND 10.0 1 12/30/2016 13:33 WG939381
Fluoranthene ND 1.00 1 12/30/2016 13:33 WG939381
Fluorene ND 1.00 1 12/30/2016 13:33 WG939381
Hexachlorobenzene ND 1.00 1 12/30/2016 13:33 WG939381
Hexachloro-1,3-butadiene ND 10.0 1 12/30/2016 13:33 WG939381
Hexachlorocyclopentadiene ND 10.0 1 12/30/2016 13:33 WG939381
Hexachloroethane ND 10.0 1 12/30/2016 13:33 WG939381
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/30/2016 13:33 WG939381
Isophorone ND 10.0 1 12/30/2016 13:33 WG939381
Naphthalene ND 1.00 1 12/30/2016 13:33 WG939381
Nitrobenzene ND 10.0 1 12/30/2016 13:33 WG939381
n-Nitrosodimethylamine ND 10.0 1 12/30/2016 13:33 WG939381
n-Nitrosodiphenylamine ND 10.0 1 12/30/2016 13:33 WG939381
n-Nitrosodi-n-propylamine ND 10.0 1 12/30/2016 13:33 WG939381
Phenanthrene ND 1.00 1 12/30/2016 13:33 WG939381
Benzylbutyl phthalate ND 3.00 1 12/30/2016 13:33 WG939381
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/30/2016 13:33 WG939381
Di-n-butyl phthalate ND 3.00 1 12/30/2016 13:33 WG939381
Diethyl phthalate ND 3.00 1 12/30/2016 13:33 WG939381
Dimethyl phthalate ND 3.00 1 12/30/2016 13:33 WG939381
Di-n-octyl phthalate ND 3.00 1 12/30/2016 13:33 WG939381
Pyrene ND 1.00 1 12/30/2016 13:33 WG939381
1,2,4-Trichlorobenzene ND 10.0 1 12/30/2016 13:33 WG939381
4-Chloro-3-methylphenol ND 10.0 1 12/30/2016 13:33 WG939381
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 14:59 11 of 36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 11 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L880657
MW-6
Collected date/time: 12/22/16 09:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Chlorophenol ND 10.0 1 12/30/2016 13:33 WG939381
2,4-Dichlorophenol ND 10.0 1 12/30/2016 13:33 WG939381
2,4-Dimethylphenol ND 10.0 1 12/30/2016 13:33 WG939381
4,6-Dinitro-2-methylphenol ND 10.0 1 12/30/2016 13:33 WG939381
2,4-Dinitrophenol ND 10.0 1 12/30/2016 13:33 WG939381
2-Nitrophenol ND 10.0 1 12/30/2016 13:33 WG939381
4-Nitrophenol ND 10.0 1 12/30/2016 13:33 WG939381
Pentachlorophenol ND 10.0 1 12/30/2016 13:33 WG939381
Phenol ND 10.0 1 12/30/2016 13:33 WG939381
2,4,6-Trichlorophenol ND 10.0 1 12/30/2016 13:33 WG939381
(S) 2-Fluorophenol 22.1 10.0-77.9 12/30/2016 13:33 WG939381
(S) Phenol-d5 10.8 5.00-70.1 12/30/2016 13:33 WG939381
(S) Nitrobenzene-d5 55.0 21.8-123 12/30/2016 13:33 WG939381
(S) 2-Fluorobiphenyl 65.9 29.5-131 12/30/2016 13:33 WG939381
(S) 2,4,6-Tribromophenol 60.9 11.2-130 12/30/2016 13:33 WG939381
(S) p-Terphenyl-d14 67.1 29.3-137 12/30/2016 13:33 WG939381
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 14:59 12 of 36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 12 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880657
MW-7
Collected date/time: 12/22/16 09:00
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ammonia Nitrogen 259 100 1 01/03/2017 11:26 WG940116
Mercury by Method 7470A
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Mercury ND 0.200 1 12/27/2016 14:57 WG938411
Metals (ICP) by Method 6010C
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Arsenic ND 10.0 1 12/28/2016 14:24 WG938981
Barium 19.6 5.00 1 12/28/2016 14:24 WG938981
Chromium ND 10.0 1 12/28/2016 14:24 WG938981
Lead ND 5.00 1 12/28/2016 14:24 WG938981
Selenium ND 10.0 1 12/28/2016 14:24 WG938981
Silver ND 5.00 1 12/28/2016 14:24 WG938981
Metals (ICPMS) by Method 6020
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Cadmium ND 1.00 1 12/30/2016 13:21 WG938446
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 12/28/2016 22:57 WG938472
Unadjusted C9-C12 Aliphatics ND 100 1 12/28/2016 22:57 WG938472
Unadjusted C9-C10 Aromatics ND 100 1 12/28/2016 22:57 WG938472
Total VPH ND 100 1 12/28/2016 22:57 WG938472
(S) 2,5-Dibromotoluene(FID) 82.4 70.0-130 12/28/2016 22:57 WG938472
(S) 2,5-Dibromotoluene(PID) 74.0 70.0-130 12/28/2016 22:57 WG938472
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acetone ND 50.0 1 12/30/2016 15:05 WG938827
Acrolein ND J4 50.0 1 12/30/2016 15:05 WG938827
Acrylonitrile ND 10.0 1 12/30/2016 15:05 WG938827
Benzene ND 1.00 1 12/30/2016 15:05 WG938827
Bromobenzene ND 1.00 1 12/30/2016 15:05 WG938827
Bromodichloromethane ND 1.00 1 12/30/2016 15:05 WG938827
Bromoform ND 1.00 1 12/30/2016 15:05 WG938827
Bromomethane ND 5.00 1 12/30/2016 15:05 WG938827
n-Butylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
sec-Butylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
tert-Butylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
Carbon tetrachloride ND 1.00 1 12/30/2016 15:05 WG938827
Chlorobenzene ND 1.00 1 12/30/2016 15:05 WG938827
Chlorodibromomethane ND 1.00 1 12/30/2016 15:05 WG938827
Chloroethane ND 5.00 1 12/30/2016 15:05 WG938827
2-Chloroethyl vinyl ether ND 50.0 1 12/30/2016 15:05 WG938827
Chloroform ND 5.00 1 12/30/2016 15:05 WG938827
Chloromethane ND 2.50 1 12/30/2016 15:05 WG938827
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 14:59 13 of 36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 13 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880657
MW-7
Collected date/time: 12/22/16 09:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Chlorotoluene ND 1.00 1 12/30/2016 15:05 WG938827
4-Chlorotoluene ND 1.00 1 12/30/2016 15:05 WG938827
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/30/2016 15:05 WG938827
1,2-Dibromoethane ND 1.00 1 12/30/2016 15:05 WG938827
Dibromomethane ND 1.00 1 12/30/2016 15:05 WG938827
1,2-Dichlorobenzene ND 1.00 1 12/30/2016 15:05 WG938827
1,3-Dichlorobenzene ND 1.00 1 12/30/2016 15:05 WG938827
1,4-Dichlorobenzene ND 1.00 1 12/30/2016 15:05 WG938827
Dichlorodifluoromethane ND 5.00 1 12/30/2016 15:05 WG938827
1,1-Dichloroethane ND 1.00 1 12/30/2016 15:05 WG938827
1,2-Dichloroethane ND 1.00 1 12/30/2016 15:05 WG938827
1,1-Dichloroethene ND 1.00 1 12/30/2016 15:05 WG938827
cis-1,2-Dichloroethene ND 1.00 1 12/30/2016 15:05 WG938827
trans-1,2-Dichloroethene ND 1.00 1 12/30/2016 15:05 WG938827
1,2-Dichloropropane ND 1.00 1 12/30/2016 15:05 WG938827
1,1-Dichloropropene ND 1.00 1 12/30/2016 15:05 WG938827
1,3-Dichloropropane ND 1.00 1 12/30/2016 15:05 WG938827
cis-1,3-Dichloropropene ND 1.00 1 12/30/2016 15:05 WG938827
trans-1,3-Dichloropropene ND 1.00 1 12/30/2016 15:05 WG938827
2,2-Dichloropropane ND 1.00 1 12/30/2016 15:05 WG938827
Di-isopropyl ether ND 1.00 1 12/30/2016 15:05 WG938827
Ethylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
Hexachloro-1,3-butadiene ND 1.00 1 12/30/2016 15:05 WG938827
Isopropylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
p-Isopropyltoluene ND 1.00 1 12/30/2016 15:05 WG938827
2-Butanone (MEK)ND 10.0 1 12/30/2016 15:05 WG938827
Methylene Chloride ND 5.00 1 12/30/2016 15:05 WG938827
4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/30/2016 15:05 WG938827
Methyl tert-butyl ether ND 1.00 1 12/30/2016 15:05 WG938827
Naphthalene ND 5.00 1 12/30/2016 15:05 WG938827
n-Propylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
Styrene ND 1.00 1 12/30/2016 15:05 WG938827
1,1,1,2-Tetrachloroethane ND 1.00 1 12/30/2016 15:05 WG938827
1,1,2,2-Tetrachloroethane ND 1.00 1 12/30/2016 15:05 WG938827
1,1,2-Trichlorotrifluoroethane ND 1.00 1 12/30/2016 15:05 WG938827
Tetrachloroethene ND 1.00 1 12/30/2016 15:05 WG938827
Toluene ND 1.00 1 12/30/2016 15:05 WG938827
1,2,3-Trichlorobenzene ND 1.00 1 12/30/2016 15:05 WG938827
1,2,4-Trichlorobenzene ND 1.00 1 12/30/2016 15:05 WG938827
1,1,1-Trichloroethane ND 1.00 1 12/30/2016 15:05 WG938827
1,1,2-Trichloroethane ND 1.00 1 12/30/2016 15:05 WG938827
Trichloroethene ND 1.00 1 12/30/2016 15:05 WG938827
Trichlorofluoromethane ND 5.00 1 12/30/2016 15:05 WG938827
1,2,3-Trichloropropane ND 2.50 1 12/30/2016 15:05 WG938827
1,2,4-Trimethylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
1,2,3-Trimethylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
1,3,5-Trimethylbenzene ND 1.00 1 12/30/2016 15:05 WG938827
Vinyl chloride ND 1.00 1 12/30/2016 15:05 WG938827
Xylenes, Total ND 3.00 1 12/30/2016 15:05 WG938827
(S) Toluene-d8 108 90.0-115 12/30/2016 15:05 WG938827
(S) Dibromofluoromethane 104 79.0-121 12/30/2016 15:05 WG938827
(S) 4-Bromofluorobenzene 117 80.1-120 12/30/2016 15:05 WG938827
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 14:59 14 of 36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 14 of 36
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880657
MW-7
Collected date/time: 12/22/16 09:00
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 100 1 12/28/2016 17:22 WG939005
Unadjusted C19-C36 Aliphatics ND 100 1 12/28/2016 17:22 WG939005
Unadjusted C11-C22 Aromatics ND 100 1 12/28/2016 17:43 WG939005
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 12/28/2016 17:22 WG939005
(S) o-Terphenyl 64.6 40.0-140 12/28/2016 17:43 WG939005
(S) 1-Chloro-octadecane 46.0 40.0-140 12/28/2016 17:22 WG939005
(S) 2-Fluorobiphenyl 83.5 40.0-140 12/28/2016 17:43 WG939005
(S) 2-Bromonaphthalene 82.9 40.0-140 12/28/2016 17:43 WG939005
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Acenaphthene ND 1.00 1 12/30/2016 13:57 WG939381
Acenaphthylene ND 1.00 1 12/30/2016 13:57 WG939381
Anthracene ND 1.00 1 12/30/2016 13:57 WG939381
Benzidine ND 10.0 1 12/30/2016 13:57 WG939381
Benzo(a)anthracene ND 1.00 1 12/30/2016 13:57 WG939381
Benzo(b)fluoranthene ND 1.00 1 12/30/2016 13:57 WG939381
Benzo(k)fluoranthene ND 1.00 1 12/30/2016 13:57 WG939381
Benzo(g,h,i)perylene ND 1.00 1 12/30/2016 13:57 WG939381
Benzo(a)pyrene ND 1.00 1 12/30/2016 13:57 WG939381
Bis(2-chlorethoxy)methane ND 10.0 1 12/30/2016 13:57 WG939381
Bis(2-chloroethyl)ether ND 10.0 1 12/30/2016 13:57 WG939381
Bis(2-chloroisopropyl)ether ND 10.0 1 12/30/2016 13:57 WG939381
4-Bromophenyl-phenylether ND 10.0 1 12/30/2016 13:57 WG939381
2-Chloronaphthalene ND 1.00 1 12/30/2016 13:57 WG939381
4-Chlorophenyl-phenylether ND 10.0 1 12/30/2016 13:57 WG939381
Chrysene ND 1.00 1 12/30/2016 13:57 WG939381
Dibenz(a,h)anthracene ND 1.00 1 12/30/2016 13:57 WG939381
3,3-Dichlorobenzidine ND 10.0 1 12/30/2016 13:57 WG939381
2,4-Dinitrotoluene ND 10.0 1 12/30/2016 13:57 WG939381
2,6-Dinitrotoluene ND 10.0 1 12/30/2016 13:57 WG939381
Fluoranthene ND 1.00 1 12/30/2016 13:57 WG939381
Fluorene ND 1.00 1 12/30/2016 13:57 WG939381
Hexachlorobenzene ND 1.00 1 12/30/2016 13:57 WG939381
Hexachloro-1,3-butadiene ND 10.0 1 12/30/2016 13:57 WG939381
Hexachlorocyclopentadiene ND 10.0 1 12/30/2016 13:57 WG939381
Hexachloroethane ND 10.0 1 12/30/2016 13:57 WG939381
Indeno(1,2,3-cd)pyrene ND 1.00 1 12/30/2016 13:57 WG939381
Isophorone ND 10.0 1 12/30/2016 13:57 WG939381
Naphthalene ND 1.00 1 12/30/2016 13:57 WG939381
Nitrobenzene ND 10.0 1 12/30/2016 13:57 WG939381
n-Nitrosodimethylamine ND 10.0 1 12/30/2016 13:57 WG939381
n-Nitrosodiphenylamine ND 10.0 1 12/30/2016 13:57 WG939381
n-Nitrosodi-n-propylamine ND 10.0 1 12/30/2016 13:57 WG939381
Phenanthrene ND 1.00 1 12/30/2016 13:57 WG939381
Benzylbutyl phthalate ND 3.00 1 12/30/2016 13:57 WG939381
Bis(2-ethylhexyl)phthalate ND 3.00 1 12/30/2016 13:57 WG939381
Di-n-butyl phthalate ND 3.00 1 12/30/2016 13:57 WG939381
Diethyl phthalate ND 3.00 1 12/30/2016 13:57 WG939381
Dimethyl phthalate ND 3.00 1 12/30/2016 13:57 WG939381
Di-n-octyl phthalate ND 3.00 1 12/30/2016 13:57 WG939381
Pyrene ND 1.00 1 12/30/2016 13:57 WG939381
1,2,4-Trichlorobenzene ND 10.0 1 12/30/2016 13:57 WG939381
4-Chloro-3-methylphenol ND 10.0 1 12/30/2016 13:57 WG939381
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L880657
MW-7
Collected date/time: 12/22/16 09:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
2-Chlorophenol ND 10.0 1 12/30/2016 13:57 WG939381
2,4-Dichlorophenol ND 10.0 1 12/30/2016 13:57 WG939381
2,4-Dimethylphenol ND 10.0 1 12/30/2016 13:57 WG939381
4,6-Dinitro-2-methylphenol ND 10.0 1 12/30/2016 13:57 WG939381
2,4-Dinitrophenol ND 10.0 1 12/30/2016 13:57 WG939381
2-Nitrophenol ND 10.0 1 12/30/2016 13:57 WG939381
4-Nitrophenol ND 10.0 1 12/30/2016 13:57 WG939381
Pentachlorophenol ND 10.0 1 12/30/2016 13:57 WG939381
Phenol ND 10.0 1 12/30/2016 13:57 WG939381
2,4,6-Trichlorophenol ND 10.0 1 12/30/2016 13:57 WG939381
(S) 2-Fluorophenol 30.6 10.0-77.9 12/30/2016 13:57 WG939381
(S) Phenol-d5 18.3 5.00-70.1 12/30/2016 13:57 WG939381
(S) Nitrobenzene-d5 42.3 21.8-123 12/30/2016 13:57 WG939381
(S) 2-Fluorobiphenyl 56.7 29.5-131 12/30/2016 13:57 WG939381
(S) 2,4,6-Tribromophenol 57.0 11.2-130 12/30/2016 13:57 WG939381
(S) p-Terphenyl-d14 65.0 29.3-137 12/30/2016 13:57 WG939381
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG940116
Wet Chemistry by Method 350.1 L880657-01,02,03
Method Blank (MB)
(MB) R3188584-1 01/03/17 11:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ammonia Nitrogen U 31.7 100
L880617-04 Original Sample (OS) • Duplicate (DUP)
(OS) L880617-04 01/03/17 11:13 • (DUP) R3188584-4 01/03/17 11:15
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte ug/l ug/l %%
Ammonia Nitrogen 159 158 1 1 20
L880823-04 Original Sample (OS) • Duplicate (DUP)
(OS) L880823-04 01/03/17 11:32 • (DUP) R3188584-6 01/03/17 11:34
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte ug/l ug/l %%
Ammonia Nitrogen U 0.000 1 0 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188584-2 01/03/17 11:07 • (LCSD) R3188584-3 01/03/17 11:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ammonia Nitrogen 7500 7890 7720 105 103 90-110 2 20
L880657-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L880657-01 01/03/17 11:17 • (MS) R3188584-5 01/03/17 11:18
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ammonia Nitrogen 10000 ND 10500 105 1 90-110
L880832-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880832-03 01/03/17 11:45 • (MS) R3188584-7 01/03/17 11:47 • (MSD) R3188584-8 01/03/17 11:48
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Ammonia Nitrogen 10000 U 10600 10600 106 106 1 90-110 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938411
Mercury by Method 7470A L880657-01,02,03
Method Blank (MB)
(MB) R3187411-1 12/27/16 14:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.0490 0.200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187411-2 12/27/16 14:26 • (LCSD) R3187411-3 12/27/16 14:29
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Mercury 3.00 2.90 3.02 97 101 80-120 4 20
L880657-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880657-01 12/27/16 14:31 • (MS) R3187411-4 12/27/16 14:34 • (MSD) R3187411-5 12/27/16 14:44
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 ND 2.64 2.85 88 95 1 75-125 8 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938981
Metals (ICP) by Method 6010C L880657-01,02,03
Method Blank (MB)
(MB) R3187822-1 12/28/16 13:53
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Arsenic U 6.50 10.0
Barium U 1.70 5.00
Chromium U 1.40 10.0
Lead U 1.90 5.00
Selenium U 7.40 10.0
Silver U 2.80 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187822-2 12/28/16 13:55 • (LCSD) R3187822-3 12/28/16 13:58
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Arsenic 1000 987 981 99 98 80-120 1 20
Barium 1000 1000 996 100 100 80-120 1 20
Chromium 1000 989 980 99 98 80-120 1 20
Lead 1000 1000 998 100 100 80-120 0 20
Selenium 1000 984 979 98 98 80-120 1 20
Silver 200 175 173 87 87 80-120 1 20
L880846-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880846-05 12/28/16 14:00 • (MS) R3187822-5 12/28/16 14:11 • (MSD) R3187822-6 12/28/16 14:13
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 1000 U 988 984 99 98 1 75-125 0 20
Barium 1000 39.8 1030 1030 99 99 1 75-125 0 20
Chromium 1000 U 976 972 98 97 1 75-125 0 20
Lead 1000 U 1000 1000 100 100 1 75-125 0 20
Selenium 1000 U 983 989 98 99 1 75-125 1 20
Silver 200 U 173 172 87 86 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938446
Metals (ICPMS) by Method 6020 L880657-01,02,03
Method Blank (MB)
(MB) R3188239-1 12/30/16 12:17
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Cadmium U 0.160 1.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188239-2 12/30/16 12:21 • (LCSD) R3188239-3 12/30/16 12:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Cadmium 50.0 48.8 49.6 98 99 80-120 2 20
L880602-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880602-02 12/30/16 12:28 • (MS) R3188239-5 12/30/16 12:35 • (MSD) R3188239-6 12/30/16 12:39
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Cadmium 50.0 0.471 50.5 48.9 100 97 1 75-125 3 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938472
Volatile Petroleum Hydrocarbons by Method MTDEQ VPH L880657-01,02,03
Method Blank (MB)
(MB) R3187959-3 12/28/16 12:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID) 83.6 70.0-130
(S) 2,5-Dibromotoluene(PID) 75.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187959-1 12/28/16 11:14 • (LCSD) R3187959-2 12/28/16 11:46
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1240 1200 104 99.6 70.0-130 4.02 25
Unadjusted C9-C12 Aliphatics 1400 1600 1560 114 112 70.0-130 2.50 25
Unadjusted C9-C10 Aromatics 200 184 179 91.9 89.6 70.0-130 2.64 25
Total VPH 2800 3030 2940 108 105 70.0-130 3.13 25
(S) 2,5-Dibromotoluene(FID)82.2 82.5 70.0-130
(S) 2,5-Dibromotoluene(PID)73.4 73.9 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938827
Volatile Organic Compounds (GC/MS) by Method 8260B L880657-01,02,03
Method Blank (MB)
(MB) R3188405-3 12/30/16 07:49
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 10.0 50.0
Acrolein U 8.87 50.0
Acrylonitrile U 1.87 10.0
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride U 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
2-Chloroethyl vinyl ether U 3.01 50.0
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
cis-1,3-Dichloropropene U 0.418 1.00
trans-1,3-Dichloropropene U 0.419 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938827
Volatile Organic Compounds (GC/MS) by Method 8260B L880657-01,02,03
Method Blank (MB)
(MB) R3188405-3 12/30/16 07:49
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Hexachloro-1,3-butadiene U 0.256 1.00
Isopropylbenzene U 0.326 1.00
p-Isopropyltoluene U 0.350 1.00
2-Butanone (MEK)U 3.93 10.0
Methylene Chloride U 1.00 5.00
4-Methyl-2-pentanone (MIBK) U 2.14 10.0
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.349 1.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,1,2-Trichlorotrifluoroethane U 0.303 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
Trichloroethene U 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,3-Trimethylbenzene U 0.321 1.00
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Vinyl chloride U 0.259 1.00
Xylenes, Total U 1.06 3.00
(S) Toluene-d8 103 90.0-115
(S) Dibromofluoromethane 101 79.0-121
(S) 4-Bromofluorobenzene 109 80.1-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188405-1 12/30/16 06:55 • (LCSD) R3188405-2 12/30/16 07:08
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 125 198 193 159 155 28.7-175 2.58 20.9
Acrolein 125 448 424 358 340 40.4-172 J4 J4 5.43 20
Acrylonitrile 125 120 114 96.0 91.2 58.2-145 5.05 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938827
Volatile Organic Compounds (GC/MS) by Method 8260B L880657-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188405-1 12/30/16 06:55 • (LCSD) R3188405-2 12/30/16 07:08
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 25.0 24.4 24.6 97.6 98.3 73.0-122 0.730 20
Bromobenzene 25.0 25.9 26.1 104 104 81.5-115 0.660 20
Bromodichloromethane 25.0 24.7 24.7 98.9 98.8 75.5-121 0.110 20
Bromoform 25.0 27.4 27.8 110 111 71.5-131 1.18 20
Bromomethane 25.0 20.0 19.2 79.8 76.7 22.4-187 3.98 20
n-Butylbenzene 25.0 25.7 25.6 103 102 75.9-134 0.610 20
sec-Butylbenzene 25.0 24.1 24.4 96.4 97.5 80.6-126 1.13 20
tert-Butylbenzene 25.0 24.9 25.3 99.6 101 79.3-127 1.71 20
Carbon tetrachloride 25.0 23.5 23.8 93.8 95.1 70.9-129 1.38 20
Chlorobenzene 25.0 26.8 27.3 107 109 79.7-122 1.76 20
Chlorodibromomethane 25.0 27.2 27.3 109 109 78.2-124 0.600 20
Chloroethane 25.0 22.1 22.4 88.4 89.7 41.2-153 1.45 20
2-Chloroethyl vinyl ether 125 167 168 134 135 23.4-162 0.480 23.5
Chloroform 25.0 24.8 24.6 99.1 98.2 73.2-125 0.940 20
Chloromethane 25.0 20.1 20.0 80.3 79.8 55.8-134 0.560 20
2-Chlorotoluene 25.0 26.7 26.6 107 106 76.4-125 0.370 20
4-Chlorotoluene 25.0 26.9 27.3 108 109 81.5-121 1.46 20
1,2-Dibromo-3-Chloropropane 25.0 21.8 21.7 87.3 86.9 64.8-131 0.430 20
1,2-Dibromoethane 25.0 26.4 27.3 106 109 79.8-122 3.20 20
Dibromomethane 25.0 24.8 24.8 99.4 99.1 79.5-118 0.310 20
1,2-Dichlorobenzene 25.0 24.0 23.5 96.0 93.9 84.7-118 2.24 20
1,3-Dichlorobenzene 25.0 21.9 21.3 87.6 85.2 77.6-127 2.79 20
1,4-Dichlorobenzene 25.0 25.3 25.6 101 102 82.2-114 1.26 20
Dichlorodifluoromethane 25.0 25.6 25.9 102 103 56.0-134 1.20 20
1,1-Dichloroethane 25.0 23.9 23.8 95.5 95.0 71.7-127 0.530 20
1,2-Dichloroethane 25.0 26.5 26.4 106 105 65.3-126 0.720 20
1,1-Dichloroethene 25.0 22.9 22.8 91.8 91.3 59.9-137 0.440 20
cis-1,2-Dichloroethene 25.0 24.3 24.0 97.0 96.2 77.3-122 0.860 20
trans-1,2-Dichloroethene 25.0 23.7 23.2 94.8 92.8 72.6-125 2.17 20
1,2-Dichloropropane 25.0 23.3 23.4 93.0 93.4 77.4-125 0.420 20
1,1-Dichloropropene 25.0 26.5 26.7 106 107 72.5-127 0.920 20
1,3-Dichloropropane 25.0 26.6 26.8 106 107 80.6-115 0.670 20
cis-1,3-Dichloropropene 25.0 26.0 25.7 104 103 77.7-124 1.27 20
trans-1,3-Dichloropropene 25.0 26.4 26.1 106 104 73.5-127 1.09 20
2,2-Dichloropropane 25.0 23.2 23.9 92.9 95.6 61.3-134 2.86 20
Di-isopropyl ether 25.0 20.8 20.8 83.1 83.2 65.1-135 0.180 20
Ethylbenzene 25.0 25.8 26.0 103 104 80.9-121 0.800 20
Hexachloro-1,3-butadiene 25.0 19.2 19.2 76.9 76.8 73.7-133 0.0700 20
Isopropylbenzene 25.0 25.3 25.3 101 101 81.6-124 0.190 20
p-Isopropyltoluene 25.0 23.9 23.6 95.7 94.5 77.6-129 1.22 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938827
Volatile Organic Compounds (GC/MS) by Method 8260B L880657-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188405-1 12/30/16 06:55 • (LCSD) R3188405-2 12/30/16 07:08
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
2-Butanone (MEK)125 177 170 141 136 46.4-155 4.10 20
Methylene Chloride 25.0 23.9 24.1 95.6 96.2 69.5-120 0.690 20
4-Methyl-2-pentanone (MIBK) 125 118 115 94.4 91.8 63.3-138 2.77 20
Methyl tert-butyl ether 25.0 23.7 23.3 94.9 93.2 70.1-125 1.85 20
Naphthalene 25.0 22.1 22.5 88.5 90.0 69.7-134 1.69 20
n-Propylbenzene 25.0 26.0 26.2 104 105 81.9-122 0.810 20
Styrene 25.0 26.7 27.1 107 108 79.9-124 1.36 20
1,1,1,2-Tetrachloroethane 25.0 24.9 25.2 99.5 101 78.5-125 1.29 20
1,1,2,2-Tetrachloroethane 25.0 24.2 24.3 96.8 97.4 79.3-123 0.570 20
Tetrachloroethene 25.0 25.4 25.9 102 103 73.5-130 1.88 20
Toluene 25.0 24.5 24.5 98.0 97.9 77.9-116 0.110 20
1,1,2-Trichlorotrifluoroethane 25.0 24.9 25.1 99.7 100 62.0-141 0.740 20
1,2,3-Trichlorobenzene 25.0 19.7 20.4 78.9 81.7 75.7-134 3.53 20
1,2,4-Trichlorobenzene 25.0 21.4 21.8 85.8 87.0 76.1-136 1.45 20
1,1,1-Trichloroethane 25.0 23.8 24.0 95.1 95.9 71.1-129 0.770 20
1,1,2-Trichloroethane 25.0 24.8 25.2 99.2 101 81.6-120 1.56 20
Trichloroethene 25.0 25.4 25.3 101 101 79.5-121 0.340 20
Trichlorofluoromethane 25.0 24.7 24.9 98.9 99.7 49.1-157 0.820 20
1,2,3-Trichloropropane 25.0 27.8 27.7 111 111 74.9-124 0.380 20
1,2,3-Trimethylbenzene 25.0 26.3 26.3 105 105 79.9-118 0.170 20
1,2,4-Trimethylbenzene 25.0 24.9 25.1 99.6 100 79.0-122 0.720 20
1,3,5-Trimethylbenzene 25.0 25.0 25.2 100 101 81.0-123 0.910 20
Vinyl chloride 25.0 22.6 22.5 90.4 90.1 61.5-134 0.240 20
Xylenes, Total 75.0 78.2 78.8 104 105 79.2-122 0.770 20
(S) Toluene-d8 104 104 90.0-115
(S) Dibromofluoromethane 101 102 79.0-121
(S) 4-Bromofluorobenzene 107 110 80.1-120
L880625-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880625-11 12/30/16 09:09 • (MS) R3188405-4 12/30/16 09:22 • (MSD) R3188405-5 12/30/16 09:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acetone 125 ND 2360 2270 94.5 90.7 20 25.0-156 4.12 21.5
Acrolein 125 ND 24900 24500 996 979 20 34.0-194 E J5 E J5 1.76 21.5
Acrylonitrile 125 ND 2350 2190 94.1 87.5 20 55.9-161 7.22 20
Benzene 25.0 ND 458 469 91.6 93.8 20 58.6-133 2.32 20
Bromobenzene 25.0 ND 540 563 108 113 20 70.6-125 4.25 20
Bromodichloromethane 25.0 ND 515 519 103 104 20 69.2-127 0.700 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938827
Volatile Organic Compounds (GC/MS) by Method 8260B L880657-01,02,03
L880625-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880625-11 12/30/16 09:09 • (MS) R3188405-4 12/30/16 09:22 • (MSD) R3188405-5 12/30/16 09:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Bromoform 25.0 ND 575 600 115 120 20 66.3-140 4.37 20
Bromomethane 25.0 ND 256 275 51.2 55.0 20 16.6-183 7.19 20.5
n-Butylbenzene 25.0 ND 538 577 108 115 20 64.8-145 7.00 20
sec-Butylbenzene 25.0 ND 502 534 100 107 20 66.8-139 6.21 20
tert-Butylbenzene 25.0 ND 525 559 105 112 20 67.1-138 6.32 20
Carbon tetrachloride 25.0 ND 422 462 84.3 92.4 20 60.6-139 9.10 20
Chlorobenzene 25.0 ND 550 584 110 117 20 70.1-130 6.01 20
Chlorodibromomethane 25.0 ND 570 592 114 118 20 71.6-132 3.73 20
Chloroethane 25.0 ND 298 309 59.6 61.8 20 33.3-155 3.66 20
2-Chloroethyl vinyl ether 125 ND 248 245 9.92 9.80 20 5.00-149 1.21 40
Chloroform 25.0 ND 487 505 97.4 101 20 66.1-133 3.67 20
Chloromethane 25.0 ND 176 181 35.2 36.1 20 40.7-139 J6 J6 2.61 20
2-Chlorotoluene 25.0 ND 545 579 109 116 20 66.9-134 6.01 20
4-Chlorotoluene 25.0 ND 558 585 112 117 20 66.8-134 4.77 20
1,2-Dibromo-3-Chloropropane 25.0 ND 469 484 93.8 96.8 20 63.9-142 3.18 20.2
1,2-Dibromoethane 25.0 ND 555 570 111 114 20 73.8-131 2.68 20
Dibromomethane 25.0 ND 501 501 100 100 20 72.8-127 0.0400 20
1,2-Dichlorobenzene 25.0 ND 515 539 103 108 20 77.4-127 4.71 20
1,3-Dichlorobenzene 25.0 ND 448 462 89.5 92.5 20 67.9-136 3.25 20
1,4-Dichlorobenzene 25.0 ND 538 566 108 113 20 74.4-123 5.17 20
Dichlorodifluoromethane 25.0 ND 86.8 96.5 17.4 19.3 20 42.2-146 J6 J6 10.6 20
1,1-Dichloroethane 25.0 331 804 804 94.6 94.8 20 64.0-134 0.110 20
1,2-Dichloroethane 25.0 ND 518 521 104 104 20 60.7-132 0.730 20
1,1-Dichloroethene 25.0 1800 2320 2280 103 95.4 20 48.8-144 1.68 20
cis-1,2-Dichloroethene 25.0 4100 4910 4780 161 137 20 60.6-136 E V E V 2.57 20
trans-1,2-Dichloroethene 25.0 ND 404 421 80.8 84.2 20 61.0-132 4.10 20
1,2-Dichloropropane 25.0 ND 470 479 94.0 95.8 20 69.7-130 1.91 20
1,1-Dichloropropene 25.0 ND 472 497 94.3 99.4 20 61.5-136 5.28 20
1,3-Dichloropropane 25.0 ND 553 562 111 112 20 74.3-123 1.67 20
cis-1,3-Dichloropropene 25.0 ND 521 524 104 105 20 71.1-129 0.680 20
trans-1,3-Dichloropropene 25.0 ND 547 540 109 108 20 66.3-136 1.24 20
2,2-Dichloropropane 25.0 ND 436 477 87.2 95.4 20 54.9-142 8.93 20
Di-isopropyl ether 25.0 ND 402 408 80.4 81.7 20 59.9-140 1.51 20
Ethylbenzene 25.0 ND 531 564 103 110 20 62.7-136 6.13 20
Hexachloro-1,3-butadiene 25.0 ND 385 426 76.9 85.3 20 61.1-144 10.3 20.1
Isopropylbenzene 25.0 ND 515 553 103 111 20 67.4-136 7.08 20
p-Isopropyltoluene 25.0 ND 488 516 97.7 103 20 62.8-143 5.51 20
2-Butanone (MEK)125 ND 2680 2550 107 102 20 45.0-156 4.74 20.8
Methylene Chloride 25.0 ND 424 444 84.8 88.9 20 61.5-125 4.62 20
4-Methyl-2-pentanone (MIBK) 125 ND 2490 2420 99.6 96.7 20 60.7-150 2.97 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 26 of 36
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG938827
Volatile Organic Compounds (GC/MS) by Method 8260B L880657-01,02,03
L880625-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L880625-11 12/30/16 09:09 • (MS) R3188405-4 12/30/16 09:22 • (MSD) R3188405-5 12/30/16 09:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Methyl tert-butyl ether 25.0 ND 452 453 90.4 90.7 20 61.4-136 0.230 20
Naphthalene 25.0 ND 467 495 93.3 99.0 20 61.8-143 5.87 20
n-Propylbenzene 25.0 ND 535 572 107 114 20 63.2-139 6.73 20
Styrene 25.0 ND 558 588 112 118 20 68.2-133 5.24 20
1,1,1,2-Tetrachloroethane 25.0 ND 527 557 105 111 20 70.5-132 5.61 20
1,1,2,2-Tetrachloroethane 25.0 ND 532 535 106 107 20 64.9-145 0.460 20
Tetrachloroethene 25.0 43.9 529 558 97.0 103 20 57.4-141 5.45 20
Toluene 25.0 ND 487 500 97.4 99.9 20 67.8-124 2.61 20
1,1,2-Trichlorotrifluoroethane 25.0 ND 402 431 79.1 84.9 20 53.7-150 6.98 20
1,2,3-Trichlorobenzene 25.0 ND 418 443 83.6 88.6 20 65.7-143 5.73 20
1,2,4-Trichlorobenzene 25.0 ND 449 474 89.9 94.9 20 67.0-146 5.38 20
1,1,1-Trichloroethane 25.0 27.5 479 505 90.3 95.5 20 58.7-134 5.33 20
1,1,2-Trichloroethane 25.0 ND 550 567 106 110 20 74.1-130 3.01 20
Trichloroethene 25.0 154 642 656 97.8 100 20 48.9-148 2.07 20
Trichlorofluoromethane 25.0 ND 351 382 70.2 76.4 20 39.9-165 8.44 20
1,2,3-Trichloropropane 25.0 ND 587 595 117 119 20 71.5-134 1.29 20
1,2,3-Trimethylbenzene 25.0 ND 563 598 113 120 20 62.7-133 6.06 20
1,2,4-Trimethylbenzene 25.0 ND 513 541 103 108 20 60.5-137 5.23 20
1,3,5-Trimethylbenzene 25.0 ND 512 545 102 109 20 67.9-134 6.30 20
Vinyl chloride 25.0 36.0 269 275 46.5 47.8 20 44.3-143 2.33 20
Xylenes, Total 75.0 ND 1590 1700 106 113 20 65.6-133 6.24 20
(S) Toluene-d8 103 103 90.0-115
(S) Dibromofluoromethane 102 100 79.0-121
(S) 4-Bromofluorobenzene 106 107 80.1-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 27 of 36
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939005
Semi-Volatile Organic Compounds (GC) by Method MADEPE L880657-01,02,03
Method Blank (MB)
(MB) R3187776-1 12/28/16 13:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
Unadjusted Total Petroleum
Hydrocarbons U 33.3 100
(S) 1-Chloro-octadecane 65.1 40.0-140
Method Blank (MB)
(MB) R3187776-4 12/28/16 14:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 66.3 40.0-140
(S) 2-Fluorobiphenyl 78.4 40.0-140
(S) 2-Bromonaphthalene 77.3 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187776-2 12/28/16 13:52 • (LCSD) R3187776-3 12/28/16 14:13
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 266 277 44.3 46.1 40.0-140 3.99 25
Unadjusted C19-C36 Aliphatics 800 483 499 60.4 62.4 40.0-140 3.13 25
(S) 1-Chloro-octadecane 47.7 53.8 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3187776-5 12/28/16 14:55 • (LCSD) R3187776-6 12/28/16 15:16
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1060 1140 62.5 67.2 40.0-140 7.23 25
(S) o-Terphenyl 63.7 66.0 40.0-140
(S) 2-Fluorobiphenyl 78.8 84.8 40.0-140
(S) 2-Bromonaphthalene 78.3 83.1 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 28 of 36
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939381
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880657-01,02,03
Method Blank (MB)
(MB) R3188393-3 12/30/16 12:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroethyl)ether U 1.62 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 0.304 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate 0.291 J 0.278 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 29 of 36
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939381
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880657-01,02,03
Method Blank (MB)
(MB) R3188393-3 12/30/16 12:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
4-Chloro-3-methylphenol U 0.263 10.0
2-Chlorophenol U 0.283 10.0
2-Nitrophenol U 0.320 10.0
4-Nitrophenol U 2.01 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 0.334 10.0
2,4,6-Trichlorophenol U 0.297 10.0
2,4-Dichlorophenol U 0.284 10.0
2,4-Dimethylphenol U 0.264 10.0
4,6-Dinitro-2-methylphenol U 2.62 10.0
2,4-Dinitrophenol U 3.25 10.0
(S) Nitrobenzene-d5 50.3 21.8-123
(S) 2-Fluorobiphenyl 67.0 29.5-131
(S) p-Terphenyl-d14 71.6 29.3-137
(S) Phenol-d5 20.9 5.00-70.1
(S) 2-Fluorophenol 31.8 10.0-77.9
(S) 2,4,6-Tribromophenol 62.7 11.2-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188393-1 12/30/16 11:58 • (LCSD) R3188393-2 12/30/16 12:22
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 35.9 36.3 71.7 72.5 38.7-109 1.11 21.5
Acenaphthylene 50.0 36.6 37.4 73.2 74.8 36.0-106 2.12 21
Anthracene 50.0 37.3 38.7 74.6 77.3 43.6-113 3.61 18.8
Benzidine 50.0 33.0 32.9 66.1 65.8 10.0-165 0.480 40
Benzo(a)anthracene 50.0 36.7 38.1 73.4 76.3 51.2-112 3.75 20
Benzo(b)fluoranthene 50.0 37.0 38.2 74.0 76.5 47.6-111 3.25 20
Benzo(k)fluoranthene 50.0 39.4 39.2 78.9 78.4 49.4-114 0.570 20
Benzo(g,h,i)perylene 50.0 40.3 41.4 80.7 82.9 45.2-117 2.69 20
Benzo(a)pyrene 50.0 37.8 39.0 75.7 78.0 45.6-106 3.08 20
Bis(2-chlorethoxy)methane 50.0 28.1 27.9 56.1 55.8 37.2-111 0.560 24.1
Bis(2-chloroethyl)ether 50.0 25.6 24.6 51.3 49.3 22.6-108 3.95 27.9
Bis(2-chloroisopropyl)ether 50.0 32.2 30.5 64.5 61.0 32.9-100 5.57 25.1
4-Bromophenyl-phenylether 50.0 40.0 41.5 79.9 83.1 40.7-116 3.85 21
2-Chloronaphthalene 50.0 33.3 34.2 66.6 68.3 33.6-105 2.62 23
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 14:59 30 of 36
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02160652.0 L880657 01/03/17 15:16 30 of 36
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939381
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880657-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188393-1 12/30/16 11:58 • (LCSD) R3188393-2 12/30/16 12:22
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
4-Chlorophenyl-phenylether 50.0 40.5 41.1 81.0 82.3 39.0-113 1.59 20.9
Chrysene 50.0 40.3 41.4 80.6 82.8 54.6-120 2.70 20
Dibenz(a,h)anthracene 50.0 40.5 40.8 81.0 81.7 42.8-118 0.850 20
3,3-Dichlorobenzidine 50.0 45.2 46.7 90.3 93.4 27.2-142 3.30 22.3
2,4-Dinitrotoluene 50.0 42.3 43.5 84.5 87.0 31.2-105 2.88 22
2,6-Dinitrotoluene 50.0 38.1 39.1 76.1 78.2 30.6-106 2.71 23.1
Fluoranthene 50.0 41.6 42.2 83.3 84.4 45.9-115 1.40 20
Fluorene 50.0 38.0 38.5 76.0 76.9 41.0-112 1.20 20.2
Hexachlorobenzene 50.0 43.5 44.7 87.0 89.5 38.5-116 2.78 20.1
Hexachloro-1,3-butadiene 50.0 28.3 28.0 56.6 56.0 16.1-104 1.05 31.2
Hexachlorocyclopentadiene 50.0 32.1 33.6 64.2 67.2 10.0-121 4.65 27.9
Hexachloroethane 50.0 22.2 22.3 44.5 44.7 16.5-89.8 0.530 30.7
Indeno(1,2,3-cd)pyrene 50.0 40.4 41.1 80.9 82.2 45.0-116 1.65 20
Isophorone 50.0 30.6 32.0 61.2 64.1 35.4-112 4.60 21.5
Naphthalene 50.0 27.9 27.9 55.9 55.8 32.2-101 0.0400 23.8
Nitrobenzene 50.0 27.5 28.3 55.1 56.5 31.4-106 2.61 25.7
n-Nitrosodimethylamine 50.0 14.3 15.1 28.6 30.1 10.0-80.1 5.16 37.5
n-Nitrosodiphenylamine 50.0 36.4 37.7 72.7 75.4 44.4-113 3.65 20
n-Nitrosodi-n-propylamine 50.0 29.3 30.6 58.6 61.1 33.2-106 4.22 23.7
Phenanthrene 50.0 36.4 37.7 72.8 75.5 46.4-113 3.54 20
Benzylbutyl phthalate 50.0 34.5 36.4 69.0 72.8 31.8-123 5.30 20.7
Bis(2-ethylhexyl)phthalate 50.0 35.9 37.2 71.9 74.3 36.9-134 3.41 23.6
Di-n-butyl phthalate 50.0 37.9 39.2 75.8 78.5 41.8-120 3.46 20.2
Diethyl phthalate 50.0 41.2 41.9 82.4 83.9 36.5-129 1.71 20
Dimethyl phthalate 50.0 40.5 40.9 81.0 81.7 35.3-128 0.850 20.8
Di-n-octyl phthalate 50.0 37.7 38.2 75.4 76.5 39.7-112 1.49 21.1
Pyrene 50.0 36.4 37.4 72.8 74.9 46.3-117 2.76 20
1,2,4-Trichlorobenzene 50.0 28.4 27.3 56.7 54.6 22.9-96.1 3.83 27.5
4-Chloro-3-methylphenol 50.0 30.9 31.8 61.9 63.7 35.7-100 2.90 22.9
2-Chlorophenol 50.0 26.8 26.0 53.6 51.9 26.2-91.5 3.08 26.5
2,4-Dichlorophenol 50.0 31.7 33.3 63.4 66.5 31.4-103 4.70 24.9
2,4-Dimethylphenol 50.0 29.5 30.0 59.1 60.1 31.9-107 1.64 25.7
4,6-Dinitro-2-methylphenol 50.0 38.6 39.6 77.1 79.2 18.4-148 2.69 24.4
2,4-Dinitrophenol 50.0 22.4 23.1 44.8 46.1 24.2-128 2.78 20.5
2-Nitrophenol 50.0 31.9 31.5 63.8 63.1 25.9-106 1.16 26.9
4-Nitrophenol 50.0 12.7 11.5 25.4 23.0 10.0-52.7 9.99 40
Pentachlorophenol 50.0 37.3 36.2 74.6 72.4 10.0-97.4 2.92 35.1
Phenol 50.0 11.1 10.7 22.3 21.4 10.0-57.9 3.86 35
2,4,6-Trichlorophenol 50.0 39.9 40.9 79.7 81.7 29.8-107 2.49 24.1
(S) Nitrobenzene-d5 48.1 48.7 21.8-123
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG939381
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L880657-01,02,03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3188393-1 12/30/16 11:58 • (LCSD) R3188393-2 12/30/16 12:22
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
(S) 2-Fluorobiphenyl 65.6 66.0 29.5-131
(S) p-Terphenyl-d14 76.9 81.1 29.3-137
(S) Phenol-d5 21.7 19.6 5.00-70.1
(S) 2-Fluorophenol 34.4 29.5 10.0-77.9
(S) 2,4,6-Tribromophenol 82.5 84.5 11.2-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
E The analyte concentration exceeds the upper limit of the calibration range of the instrument
established by the initial calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is
high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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