IDX_COMP_SITE_ASSMT_RESULTS_SUMMARY-OCR

*3SIHSSF2021 *
11111111111111111111111111
DocumentlD NONCD0001814
Site Name HAMILTON BEACH/PROCTOR SILEX
DocumentType Site Assessment Rpt (SAR)
RptSegment 9
DocDate
DocRcvd
Box
Access level
Division
Section
Program
DocCat
1/1/1999
2/20/2007
SF2021
PUBLIC
WASTE MANAGEMENT
SUPERFUND
IHS (IHS)
FACILITY
12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
Pyridine
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
o-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
sym-Trinitrobenzene
•
1198HBWW211
9811550-04A
Z9373
11/17 /98
11/19/98 11:25:00
12/03/98 18:41
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.274
0.818
0. 496
0.378
0.681
1. 38
0.334
0.917
0.357
1.25
R B S ULT S S UM MARY (Cont'd)
1198HBWW217
9811550-05A
Z9374
11/17 /98
11/19/98 11:25:00
12/03/98 19:21
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
0.269
0.803
0 .487
0.370
0.668
1.35
0.328
0.900
0.350
1.23
1198HBWW219
9811550-llA
Z9380
11/17/98
11/19/98 11:25:00
12/03/98 23:19
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.269
0.803
0 .487
0. 370
0.668
1.35
0.328
0.900
0.350
1. 23
Work Order ff 9811550
Page l§_
1198HBWW222
9811550-09A
Z9378
11/17 /98
11/19/98 11:25:00
12/03/98 22:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.269
0.803
0.487
0.370
0.668
1. 35
0.328
0.900
0.350
l.23
•
• 12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-dl4
2,4,6-Tribromophenol
1198HBWW211
9811550-04A
Z9373
11/17/98
11/19/98 11:25:00
12/03/98 18:41
1
Water
ug/L
received
Cone. DL
Recovery
%
98
97
104
100
100
96
• RESULTS S UM MAR Y (Cont'd)
1198HBWW217
9811550-05A
Z9374
11/17/98
11/19/98 11:25:00
12/03/98 19:21
1
Water
ug/L
received
Cone. DL
Recovery
%
97
94
108
95
91
91
1198HBWW219
9811550-llA
Z9380
11/17/98
11/19/98 11:25:00
12/03/98 23:19
1
Water
ug/L
received
Cone.
Recovery
%
87
88
100
92
89
87
DL
Work Order # 9811550
Page 1.2_
1198HBWW222
9811550-09A
Z9378
11/17 /98
11/19/98 11:25:00
12/03/98 22:00
1
Water
ug/L
received
Cone. DL
Recovery
%
101
98
108
101
105
103
•
12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Aniline
Anthracene
Benz(a)anthracene
Benz(a)pyrene
Benzidine
Benzo(b)fluoranthene
Ben~o(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
Carbazole
4-Chloro-3-methylphenol
p-Chloroaniline
•
1198HBWW223
9811550-08A
Z9377
11/17/98
11/19/98 11:25:00
12/03/98 21:20
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.473
0.380
0.170
0.513
8.60
0.687
0.394
0.199
0.298
29.0
0.295
0.315
0.599
31. l
0.702
0.435
0.109
0.0588
0.465
0.874
RESULTS SUMMARY ·(Cont'd)
1198HBWW225
9811550-12A
Z9381
11/17/98
11/19/98 11:25:00
12/03/98 23:59
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
0.468
0.377
0.168
0.508
8.51
0.681
0.390
0.197
0.295
28.7
0.292
0.312
0.593
30.8
0.695
0.431
0.108
0.0583
0.460
0.865
1198HBWW229
9811550-06A
Z9375
11/17/98
11/19/98 11:25:00
12/03/98 20:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.473
0.380
0.170
0.513
8.60
0.687
0.394
0.199
0.298
29.0
0.295
0.315
0.599
31. l
0.702
0.435
0.109
0.0588
0.465
0.874
Work Order # 9811550
Page 1Q_
1198HBWW230
9811550-07A
Z9376
11/17/98
11/19/98 11:25:00
12/03/98 20:40
l
Water
ug/L
received
Cone.
ND
ND
1. 02
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0 .450
0.363
0.162
0 .489
8.20
0.655
0.376
0.190
0.284
27.7
0.281
0.300
0.571
29.6
0.669
0.415
0.104
0.0561
0.443
0.833
•
• 12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Diallate
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
Diethylphthalate
1198HBWW223
9811550-0SA
Z9377
11/17/98
11/19/98 11:25:00
12/03/98 21:20
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0 .202
0.246
0.155
0.199
0.581
0.120
0.348
0.284
0.175
0.175
0.231
0.249
0.144
0.353
0.503
0.459
1.14
0.392
0.265
0.215
• RESULTS SUMMARY (Cont'd)
1198HBWW225
9811550-12A
Z9381
11/17/98
11/19/98 11:25:00
12/03/98 23:59
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.200
0.244
0.153
0.197
0.576
0.118
0.345
0.282
0.174
0.174
0.229
0.247
0 .143
0.350
0.498
0.454
1.13
0.388
0.262
0.213
1198HBWW229
9811550-06A
Z9375
11/17/98
11/19/98 11:25:00
12/03/98 20:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.202
0.246
0.155
0.199
0.581
0.120
0.348
0.284
0.175
0.175
0.231
0.249
0.144
0.353
0.503
0.459
1.14
0.392
0.265
0.215
Work Order # 9811550
Page ~
1198HBWW230
9811550-07A
Z9376
•
11/17 /98
11/19/98 11:25:00
12/03/98 20:40
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
O.J.93
0.235
0.148
0.190
0.554
0.114
0.332
0.271
0.167
0.167
0.221
0.237
0.137
0.336
0.479
0 .437
1. 08
0.374
0.252
0.205
12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
p-Dimethylaminoazobenzene
7,12-Dimethylbenz(a)anthracene
3,3'-Dimethylbenzidine
Dimethylphenethylamine
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
1,3-Dinitrobenzene
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine/N-NitrosoDPA
Ethyl methanesulfonate
bis(2-Ethylhexyllphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
•
1198HBWW223
9811550-08A
Z9377
11/17/98
11/19/98 11:25:00
12/03/98 21 :20
1
Water
ug/L
received
Cone. DL
ND 0.782
ND 0.379
ND 3.61
ND 12.7
ND 0.394
ND 0.266
ND 9.80
ND 0.517
ND 5.82
ND 0.438
ND 0.440
ND 0.630
ND 0.346
ND 5.02
ND 0.237
ND 0.316
ND . 0.405
ND 0.642
ND 5.16
ND 0.315
RBSULTS SUMMARY (Cont'd)
1198HBWW225 1198HBWW229
9811550-12A 9811550-06A
Z9381 Z9375
11/17/98 11/17 /98
11/19/98 11:25:00 11/19/98 11:25:00
12/03/98 23:59 12/03/98 20:00
l 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0. 775 ND 0.782
ND 0.376 ND 0.379
ND 3.57 ND 3.61
ND 12.6 ND 12.7
ND 0.390 ND 0.394
ND 0.263 ND 0.266
ND 9. 71 ND 9.80
ND 0.512 ND 0.517
ND 5.77 ND 5.82
ND 0.434 ND 0.438
ND 0.436 ND 0.440
ND 0.624 ND 0.630
ND 0.343 ND 0.346
1.53 J 4.97 1. 30 J 5.02
ND 0.235 ND 0.237
ND 0.313 ND 0.316
ND 0 .401 ND 0 .405
ND 0.636 ND 0.642
ND 5.11 ND 5.16
ND 0.312 ND 0.315
•
Work Order # 9811550
Page~
1198HBWW230
9811550-07A
Z9376
11/17/98
11/19/98 11:25:00
12/03/98 20:40
l
Water
ug/L
received
Cone. DL
ND o. 746
ND 0.362
ND 3.44
ND 12.l
ND 0.376
ND 0.253
ND 9.35
ND 0.493
ND 5.55
ND 0.418
ND 0.420
ND 0.601
ND 0.330
2. 00 J 4.79
ND 0.226
ND 0.301
ND 0.386
ND 0.612
ND 4. 92
ND 0.300
•
• 12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilu~ion Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Hexachloropropene
Indeno(l,2,3-cd)pyrene
r.sophorone
Isosaf role
Ke pone
Methapyrilene
Methyl methanesulfonate
3-Methylcholanthrene
2-Methylnaphthalene
4-Methylphenol/3-Methylphenol
2-Methylphenol
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
Naphthalene
1198HBWW223
9811550-08A
Z9377
11/17/98
11/19/98 11:25:00
12/03/98 21:20
1
Water
ug/L
received
Cone. DL
ND 0.804
ND 0.208
ND 0.0971
ND 1.25
ND 18.6
ND 9.26
ND 0 .413
ND 7.21
ND 0.301
ND 0.224
ND 0.210
ND 0.557
ND 0.353
ND 0.529
ND 0.604
ND 0.788
ND 0.951
ND 0.188
ND 0.788
ND 0.393
• R B S ULT S S UM M AR Y (Cont'd)
1198HBWW225 1198HBWW229
9811550-12A 9811550-06A
Z9381 Z9375
11/17/98 11/17/98
11/19/98 11:25:00 11/19/98 11:25:00
12/03/98 23:59 12/03/98 20:00
1 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.796 ND 0.804
ND 0.206 ND 0.208
ND 0.0961 ND 0.0971
ND 1.23 ND 1.25
ND 18.4 ND 18.6
ND 9.17 ND 9.26
ND 0.409 ND 0.413
ND 7.14 ND 7.21
ND 0.298 ND . 0.301
ND 0.221 ND 0.224
ND 0.208 ND 0.210
ND 0.551 ND 0.557
ND 0.350 . ND 0.353
ND 0.524 ND 0.529
ND 0.598 ND 0.604
ND 0.781 ND 0.788
ND 0. 942 ND 0.951
ND 0.186 ND 0.188
ND 0.781 ND 0.788
ND 0.389 ND 0.393
Work Order # 9811550
Page £1_
1198HBWW.230
9811550-07A
Z9376
11/17/98
•
11/19/98 11:25:00
12/03/98 20 :40
1
Water
ug/L
received
Cone. DL
ND 0.766
ND 0.198
ND 0. 0925
ND 1.19
ND 17.8
ND 8.83
ND 0.393
ND 6. 87.
ND 0.287
6.23 F 0.213
ND 0.200
ND 0.531
ND 0.336
ND 0.505
ND 0.576
ND 0.751
ND 0.907
ND 0.179
ND 0.751
ND 0.375
12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,4-Naphthoquinone
1-Naphthylamine
2-Naphthylamine
5-Nitro-o-toluidine
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-1-oxide
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
2-Picoline
Pronamide
•
1198HBWW223
9811550-08A
Z9377
11/17 /98
11/19/98 11:25:00
12/03/98 21:20
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.527
9.02
10.5
0.517
0. 641
0.589
0.578
0.587
0.566
8.45
4.99
0. 341
0.533
1.17
6.57
0.185
0.306
0.237
1.17
0 .404
R B S UL T S S UM MA R Y (Cont'd)
1198HBWW225
9811550-12A
Z9381
11/17 /98
11/19/98 11:25:00
12/03/98 23:59
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND '
ND
ND
ND
ND
•
DL
0.522
8.93
10.4
0.512
0.635
0.583
0.573
0.582
0.560
8.37
4. 94
0.338
0.528
1.16
6.50
0.183
0 .303
0.235
1.16
0 .400
1198HBWW229
9811550-06A
Z9375
11/17/98
11/19/98 11:25:00
12/03/98 20:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.51
ND
ND
DL
0.527
9.02
10.5
0.517
0. 641
0.589
0.578
0.587
0.566
8.45
4.99
0.341
0.533
1.17
6.57
0.185
0.306
0.237
1.17
0 .404
Work Order # 9811550
Page 11._
1198HBWW230
9811550-07A
Z9376
11/17/98
11/19/98 11:25:00
12/03/98 20:40
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.503
8.60
10.00
0 .493
0.611
0.562
0.551
0. 560
0.539
8.06
4.76
0. 325
0.508
1.11
6.26
0.177
0. 292
0 .226
1.11
0.385
•
• 12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
Pyridine
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
o-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Triehlorophenol
sym-Trinitrobenzene
1198HBWW223
9811550-08A
Z9377
11/17/98
11/19/98 11:25:00
12/03/98 21:20
1
Water
ug/L
received
Cone. DL
ND 0.276
ND 0.826
ND 0.501
ND 0.381
ND 0.687
ND 1. 39
ND 0.337
ND 0.926
ND 0.361
ND 1.26
• RESULTS S UM MARY (Cont'd)
1198HBWW225
9811550-12A
Z9381
11/17/98
11/19/98 11:25:00
12/03/98 23:59
1
Water
ug/L
received
Cone. DL
ND 0.274
ND 0.818
ND 0.496
ND 0,378
ND 0.681
ND 1.38
ND 0.334
ND 0. 917
ND 0.357
ND 1.25
1198HBWW229
9811550-06A
Z9375
11/17/98
11/19/98 11:25:00
12/03/98 20:00
1
Water
ug/L
received
Cone. DL
ND 0.276
ND 0.826
ND 0.501
ND 0.381
ND 0.687
ND 1. 39
ND 0.337
ND 0.926
ND 0.361
ND 1. 26
• Work Order # 9811550
Page ~
1198HBWW230
9811550-07A
Z9376
11/17 /98
11/19/98 11:25:00
12/03/98 20:40
1
Water
ug/L
received
Cone. DL
ND 0.264
ND 0.788
ND 0.478
ND 0.364
ND 0.655
ND 1.33
ND 0.321
ND 0.883.
ND 0.344
ND 1.21
12/07/98 10:24:36
Method Sernivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-dl4
2,4,6-Tribrornophenol
•
1198HBWW223
9811550-08A
Z9377
11/17 /98
11/19/98 11:25:00
12/03/98 21:20
1
Water
ug/L
received
Cone.
Recovery
%
101
101
111
103
99
100
DL
RESULTS SUM MARY (Cont'd)
1198HBWW225
9811550-12A
Z9381
11/17/98
11/19/98 11:25:00
12/03/98 23:59
'J
1
Water
ug/L
received
Cone.
Recovery
%
103
104
108
108
98
103
•
DL
1198HBWW229
9811550-0GA
Z9375
11/17/98
11/19/98 11:25:00
12/03/98 20:00
1
Water
ug/L
received
Cone.
Recovery
%
74
102
104
106
78
78
DL
Work Order # 9811550
Page l§_
1198HBWW230
9811550-07A
Z9376
11/17/98
11/19/98 11:25:00
12/03/98 20:40
1
Water
ug/L
received
Cone.
Recovery
%
92
98
107
98
94
94
DL
•
• 12/07/98 10:24:36
Method Semivolatiles by SW8270C
Test Code 827SWBOO
Initial Calibration # MSD2981121061300
Calibration Date ~l_l~/=2=1/~9~8~~~~-
Sequence/Analysis Time
1 12/03/98 12:23
2 12/03/98 12:44
3 12/03/98 14:43
4 12/03/98 16:03
5 12/03/98 16:42
6 12/03/98 17:22
7 12/03/98 18:01
8 12/03/98 18 :41
9 12/03/98 19:21
10 12/03/98 20:00
11 12/03/98 20:40
12 12/03/98 21:20
13 12/03/98 22:00
14 12/03/98 22:40
15 12/03/98 23:19
16 12/03/98 23:59
17 12/04/98 00:39
18 12/03/98 15:23
• ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSD281203122301
Analysis Start Date/Time 12/03/98 12:23:00
Analysis Stop Date/Time 12/03/98 15:23:00
Project Sample ID Lab Sample ID Sample Type
TUNE GC/MS tune files
Work Order # 9811550
Page n_
Instrument ~
Analyst MCL
Reviewer =SD~K"'-~~~~~~~
Analysis File 11
Z9363
SSTD050 Continuing Calibration Verification Z9364
LCSD986266 Lab Control Sample Z9367
9811511-0lA Sample Z9369
1198HBWW208 9811550-0lA Sample Z9370
1198HBWW209 9811550-02A Sample Z9371
1198HBWW210 9811550-03A Sample Z9372
1198HBWW211 9811550-04A Sample Z9373
1198HBWW217 9811550-05A Sample Z9374
1198HBWW229 9811550-06A sample Z9375
1198HBWW230 9811550-07A Sample Z9376
1198HBWW223 9811550-08A Sample Z9377
1198HBWW222 9811550-09A Sample Z9378
1198HBWE01 9811550-lOA Sample Z9379
1198HBWW219 9811550-llA Sample Z9380
1198HBWW225 9811550-l2A Sample Z938l
DCS986267 Detectability Check Sample Z9382
BLK984096 Blank, Method Z9368
•
12/07/98 10:24:36
Method Semivolatiles by SW8270C
Lab Sample ID
File ID
9811550-0?A
Z9376
•
Project Sample
ID/Description
' 1198HBWW230
Specification# _8_2_7~S~~
Analyte
ARALYTXCAL PROTOCOL SUMMARY
COMMBRTS/NARRATXVB
Flag Comment/Narrative
4-Methylphenol/3-Methylphenol F The F flag indicates that 3-methylphenol
coelutes with 4-methylphenol. The calibration
response factor is based on 4-methylphenol
only. Any identification for 4-methylphenol
should be regarded as a possible sum of the
two indistinguishable isomers .
•
Corrective Action
Work Order # 9811550
Page £L
•
• 12/07/98 10:24:36 • QUALITY CONTROL EXCEPTION REPORT
SUMMARY
QCER # Analysis Batch Number
981203-07 MSD2981203122300
Work Order # 9811550
Page ~ •
QUALITY CONTROL EXCEPTION REPORT
LEVEL 2 -ANALYTICAL
REPORT COPY 9811550
Revised: 12/04/98 QCER # 981203-07
Analyst: CAROL LOVETT
Batch #: MSD2981203122300
Prat Spec: 827S 05.00
Instrument:m ~=s~d_#~2~~­
Matrix: liquid
Analysis File #:
Date Analyzed: 12 03
Status: ~
Client ID: CSC: Lab Sample ID:
9811550 HAM BEACH NC JAL
SAMPLE PREPARATION:
PROBLEM IDENTIFICATION
Sample Went Dry
Loss of %
of Sample
Emulsion Formed
Blank Contamination
Instrument
Hold Time
MS/MSD Not Available
Instrument
Other (Describe)
Comments:
SAMPLE ANALYSIS:
PROBLEM IDENTIFICATION
Surrogate Recovery X
MS/MSD Recovery -
LCS/LCSD Recovery x
MS/MSD Precision _
LCS/LCSD Precision x
Standard
Blank Contamination
Instrument
Hold Time
No MS/MSD Available
for Batch
Sample pH
Dil. Due to Hi-Level
Non-Target Analytes
Serial Dilution
Analytical Spike
Internal Standard
Other (Describe)
PROBABLE CAUSE
Matrix Effect
Instrument
Spiking Error
Contamination
Coelution
Unknown X
Other(Describe)
Project Sample ID:
CORRECTIVE ACTION TAKEN
Reprepare Sample
Sample Sent for Analysis
Re sample
Other (Describe)
•
CORREC'l'IVE ACTION TAltEN
Reprepare Sample
Reanalyze Sample
Reanalyze LCS/LCSD
Recalibrate Instrument
Analyze Out of Hold Time
Prepare New Standard
Flag Data
Resample
Analyze by MSA
Perform Analytical Spike
No Action Required
Level 3 QCER to Follow
Other (Describe) X
SEE BELOW
Comments: lcs986266: All analytes and surrogtes were recovered around 6% •
causing the rpds also to be out. There is ·no assignable cause.
Per CSC, only the lcsd will be reported.
Distribution: CSC, Lab, Report
12/07/98 15:35:19
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared -~R~a~d~i~a~n-=I~n~t~e~r~n~a~t~i~o~n~a~l~,-=L~L~C'­
By --=1~4~0~4~6_.:::S~u~m~m~i~t_.:::D~r~·~,_,,B~l~d~q~·-=B:.­
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW208
ll98HBWW209
1198HBWW210
1198HBWW211
1198HBWW217
ll98HBWW221
1198HBWW223
ll98HBWW222
1198HBWW225
•
ID/
WORX ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID WASHINGTON, NC
Case # ~N~A'--------~­
SDG # ~NA=-~------­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA N23EWAOO
02A N23EWAOO
03A N23EWAOO
04A N23EWAOO
05A N23EWAOO
06A N23EWAOO
07A N23EWAOO
OBA N23EWAOO
09A N23EWAOO
•
Work Order # 9811551
Page _1_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
••
• 12/07/98 15:35:19
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB CBRTIFICATIOHS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9811551
Page L
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
12/07/98 15:35:19 ANALYTICAL PROTOCOL SUMMARY
FLAG DEFINITIONS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis. NA
NC
ND
NR
NS
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No.instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon.mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation .
• •
Work Order # 9811551
Page _3_
•
• 12/07/98 15:35:19
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Method Nitrate-nitrite, EPA 353.1
Project Sample ID/Description
119BHBWW208
1198HBWW209
1198HBWW210
1198HBWW211
1198HBWW217
1198HBWW221
1198HBWW222
1198HBWW223
1198HBWW225
• AHALYTICAL PROTOCOL" SUMMARY
Extraction/Digestion
Lab Sample ID Test Code (s) Batch #
9811551-0lA N23EWAOO NA
9811551-02A N23EWAOO NA
9811551-0JA N23EWAOO NA
9811551-04A N23EWAOO NA
9811551-05A N23EWAOO NA
9811551-0GA N23EWAOO NA
9811551-08A N23EWAOO NA
9811551-0?A N23EWAOO NA
9811551-09A N23EWAOO NA
Work Order # 9811551
Page .i._
Analysis Batch jj
WLTRAC81206151601
WLTRAC81206151601
WLTRAC81206151601
WLTRAC81206151601
WLTRAC81206151601
WLTRAC81206151601
WLTRAC81206151601
WLTRAC81206151601
WLTRAC81206151601
-
•
12/07/98 15:35:19
Method Nitrate-nitrite, EPA 353.l
Test Code N23EWAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Nitrate-Nitrite as N
•
ll98HBWW208
9811551-0lA
TRAC1206-35
11/17/98
12/06/98 15:16:00
l
Water
mg/L
received
Cone.
0.949 B
DL
0.00563
RESULTS SUMMARY
ll98HBWW209
9811551-02A
TRAC1206-36
11/17/98
12/06/98 15:16:00
l
Water
mg/L
received
Cone.
0.0452 B
DL
0.00563
•
ll98HBWW210
9811551-03A
TRAC1206-37
11/17/98
12/06/98 15:16:00
l
Water
mg/L
received
Cone.
0.0418 B
DL
0.00563
Work Order U 9811551
Page _5_
ll98HBWW2ll
9811551-04A
TRAC1206-38
11/17/98
12/06/98 15:16:00
l
Water
mg/L
received
Cone. DL
0.0445 B 0.00563
•
• 12/07/98 15:35:19
Method Nitrate-nitrite, EPA 353.l
Test Code N23EWAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Nitrate-Nitrite as N
ll98HBWW2l 7
98ll55l-05A
TRAC1206-39
ll/17/98
12/06/98 15:16:00
1
Water
mg/L
received
Cone. DL
0.563 B 0.00563
• RESULTS S UM MA RY (Cont•d)
ll98HBWW221
98ll55l-06A
TRAC1206-40
11/17/98
12/06/98 15:16:00
1
Water
mg/L
received
Cone.
0.0574 B
DL
0.00563
ll98HBWW222
981155l-08A
TRAC1206-42
11/l 7 /98
12/06/98 15:16:00
1
Water
mg/L
received
Cone. DL
0.0166 B 0.00563
Work Order ff 9811551
Page _6_
ll98HBWW223
981155l-07A
TRAC1206-4l
11/l 7 /98
12/06/98 15:16:00
l
Water
mg/L
received
Cone. DL
0.0350 B 0.00563
•
12/07/98 15:35:19
Method Nitrate-nitrite, EPA 353.1
Test Code N23EWAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Nitrate-Nitrite as N
•
1198HBWW225
9811551-09A
TRAC1206-43
11/17/98
12/06/98 15:16:00
10
Water
mg/L
received
Cone. DL
8.61 B 0.0563
R B S UL T S S UM MAR Y (Cont'd)
Cone. DL Cone.
"r
•
DL
Work Order # 9811551
Page _7_
Cone. DL
•
• 12/07/98 15:35:19
Method Nitrate-nitrite, EPA 353.1
Test Code N23EWAOO
Initial Calibration ff ~N~A"-------~
Calibration Date ~--------
Sequence/Analysis Time
1 12/06/98 15:16:00
2 12/06/98 15:16:00
3 12/06/98 15:16:00
4 12/06/98 15:16:00
5 12/06/98 15:16:00
6 12/06/98 15:16:00
7 12/06/98 15:16:00
8 12/06/98 15:16:00
9 12/06/98 15:16:00
10 12/06/98 15:16:00
11 12/06/98 15:16:00
12 12/06/98 15:16:00
13 12/06/98 15:16:00
14 12/06/98 15:16:00
15 12/06/98 15:16:00
16 12/06/98 15:16:00
17 12/06/98 15:16:00
18 12/06/98 15:16:00
19 12/06/98 15:16:00
20 12/06/98 15:16:00
21 12/06/98 15:16:00
22 12/06/98 15:16:00
23 12/06/98 15:16:00
24 12/06/98 15:16:00
25 12/06/98 15:16:00
26 12/06/98 15:16:00
27 12/06/98 15:16:00
28 12/06/98 15:16:00
29 12/06/98 15:16:00
30 12/06/98 15:16:00
Project Sampl~
ANALYSIS BAT.SUMMARY
Analysis Batch ff WLTRAC81206151601
Analysis Start Date/Time 12/06/98 15:16:00
Analysis Stop Date/Time 12/06/98 15:16:00
ID Lab Sample ID Sample Type
PRIMER
SYSBLK Blank, System
CALSTDl Initial Calibration
CALSTD2 Initial Calibration
CALSTD3 Initial Calibration
CALSTD4 Initial Calibration
CALSTD5 Initial Calibration
CALSTD6 Initial Calibration
Standard
Standard
Standard
Standard
Standard
Standard
!CB Blank, Initial Calibration
Work Order ff 9811551
Page _8_
Instrument TRAC
Analyst ~
Reviewer =L~K~H ________ _
Analysis File ff
TRAC1206-l
TRAC1206-2
1 TRAC1206-3
2 TRAC1206-4
3 TRAC1206-5
4 TRAC1206-6
5 TRAC1206-7
6 TRAC1206-8
TRAC1206-9
!CV Initial Calibration Verification TRAC1206-10
N02REDCHECK Distilled Calibration Standard TRAC1206-ll
SYSBLK Blank, System TRAC1206-12
DCS986520 Detectability Check Sample TRAC1206-13
BLK984271 Blank, Method TRAC1206-14
LCS986519 Lab Control Sample TRAC1206-15
LCSD986519 Lab Control Sample Duplicate TRAC1206-16
SYSBLK Blank, System TRAC1206-17
9811515-04A Sample TRAC1206-18
9811515-05A Matrix _Spike TRAC1206-19
9811515-06A Matrix Spike Duplicate TRAC1206-20
SYSBLK Blank, System TRAC1206-21
9811515-0lA Sample TRAC1206-22
9811515-02A Sample TRAC1206-23
9811515-03A Sample TRAC1206-24
9811515-07A Sample TRAC1206-25
9811515-08A sample TRAC1206-26
9811515-09A Sample TRAC1206-27
9811515-lOA Sample TRAC1206-28
9811466-0lA Sample TRAC1206-29
9811466-02A Sample TRAC1206-30
•
12/07/98 15:35:19
Method Nitrate-nitrite, EPA 353.1
Test Code N23EWAOO
Initial Calibration fl _N~A~~~~~~~­
Calibration Date ~~~~~~~~
Sequence/Analysis Time
31 12/06/98 15:16:00
32 12/06/98 15:16:00
33 12/06/98 15:16:00
34 12/06/98 15:16:00
35 12/06/98 15:16:00
36 12/06/98 15:16:00
37 12/06/98 15:16:00
38 12/06/98 15:16:00
39 12/06/98 15:16:00
40 12/06/98 15:16:00
41 12/06/98 15:16:00
42 12/06/98 15:16:00
43 12/06/98 15:16:00
44 12/06/98 15:16:00
45 12/06/98 15:16:00
46 12/06/98 15:16:00
47 12/06/98 15:16:00
48 12/06/98 15:16:00
49 12/06/98 15:16:00
50 12/06/98 15:16:00
51 12/06/98 15:16:00
•
AH ALY S I S B AT C H S UHM AR Y (cont'd)
Analysis Batch # WLTRAC81206151601
Analysis Start Date/Time 12/06/98 15:16:00
Analysis Stop Date/Time 12/06/98 15:16:00
Work Order II 9811551
Page _9 _
Instrument TRAC
Analyst 8fB
Reviewer ~L~K~H~~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis Pile II
SYSBLK Blank, System TRAC1206-31
CCB Blank, Continuing Calibration TRAC1206-32
CCV Continuing Calibration Verification TRAC1206-33
9811466-03A Sample TRAC1206-34
1198HBWW208 9811551-0lA Sample TRAC1206-35
1198HBWW209 9811551-02A Sample TRAC1206-36
1198HBWW210 9811551-03A Sample TRAC1206-37
1198HBWW211 9811551-04A Sample TRAC1206-38
1198HBWW217 9811551-05A Sample TRAC1206-39
1198HBWW221 9811551-06A Sample TRAC1206-40
1198HBWW223 9811551-07A Sample TRAC1206-41
1198HBWW222 9811551-08A Samp~e TRAC1206-42
1198HBWW225 9811551-09A Sample TRAC1206-43
SYSBLK Blank, system TRAC1206-44
CCB Blank, Continuing Calibration TRAC1206-45
CCV Continuing Calibration Verification TRAC1206-46
HIGHSTD Sample TRAC1206-47
LOW STD Sample TRAC1206-48
LOWSTD Sample TRAC1206-49
SYSBLK Blank, System TRAC1206-50
PRIMER Sample TRAC1206-51
• •
• 12/07/98 15:35:19
Method Nitrate-nitrite, EPA 353.1 Specification#
Lab Sample ID
File ID
Project Sample
ID/Description Analyte
• ANALYTICAL PROTOCOL SUMMARY
COMMBHTS/HARRATIVB
Flag Comment/Narrative Corrective Action
• Work Order # 9811551
Page lQ__
•• 12/01/98 09:52:04
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared -----"R"'a"'d:.:i"'a~n--=I~n"'t"'e"'r~n"'a"'t"'i"'o~n;.:a:.:1 ..... --=L:.:L:.:C:....
By ---=1~4~0~4~6--=S;.:u~m~m:.:i .. t--=D;.:r~._.,--=B:.:l .. d~q~·--=B'­
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW208
1198HBWW209
1198HBWW210
1198HBWW211
1198HBWW217
1198HBWW221
1198HBWW223
1198HBWW222
ID/
• WORX ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Fa9ility WASHINGTON,NC
Work ID WASHINGTON, NC
Case # ~N~A'"--------­
SDG # _NA--~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA ALKEWACP
02A ALKEWACP
03A ALKEWACP
04A ALKEWACP
OSA ALKEWACP
06A ALKEWACP
07A ALKEWACP
OBA ALKEWACP
Work Order # 9811552
Page!.__
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
•
12/0l/98 09:52:04
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STATE CBRTIPICATIOlfS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
•
Work Order # 9811552
Page _2_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
• • 12/01/98 09:52:04 ANALYTICAL PROTOCOL SUMMARY
FLAG DBFIBITIOBS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis. NA
NC
ND
NR
NS
A
B
c
RPD and/or \ Recovery not calculated. See Narrative for explanation,
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification ~riteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA).
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation.
Work Order # 9811552
Page _3_ •
12/01/98 09:52:04
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Method Alkalinity by E310.l
Project Sample ID/Description
1198HBWW208
1198HBWW209
1198HBWW210
1198HBWW211
1198HBWW217
1198HBWW221
1198HBWW222
1198HBWW223
•
AHALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9811552-0lA ALKEWACP NA
9811552-02A ALKEWACP NA
9811552-0JA ALKEWACP NA
9811552-04A ALKEWACP NA
9811552-05A ALKEWACP NA
9811552-0GA ALKEWACP NA
9811552-08A ALKEWACP NA
9811552-0?A ALKEWACP NA
•
Work Order # 9811552
Page .$.._.
Analysis Batch #
WLOTT081120110201
WLOTT081120110201
WLOTT081120110201
WLOTT081120110201
WLOTT081120110201
WLOTT081120110201
WLOTT081120110201
WLOTT081120110201
•
• 12/01/98 09:52:04
Method Alkalinity by E310.l
Test Code ALKEWACP
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Colunm:
Analyte
Bicarbonate
Carbonate
Hydroxide
Total Alkalinity
1198HBWW208
9811552-0lA
OTT01120-10
11/17/98
11/20/98 11:02:00
1
Water
mg/L
received
Cone.
18.5 B
0
0
18.5 B
DL
0.358
• RESULTS SUMMARY
1198HBWW209
9811552-02A
OTT01120-11
11/17/98
11/20/98 11:02:00
1
Water
mg/L
received
Cone.
111 B
0
0
111 B
DL
0.358
1198HBWW210
9811552-03A
OTT01120-12
11/17/98
11/20/98 11:02:00
1
Water
mg/L
received
Cone.
64.0 B
0
0
64. 0 B
DL
0.358
Work Order # 9811552
Page _5_
1198HBWW211
9811552-04A
OTT01120-13
11/17 /98
11/20/98 11:02:00
l
Water
mg/L
received
Cone.
12.6 B
0
0
12.6 B
DL
0.358
•
12/01/98 09:52:04
Method Alkalinity by E310.l
Test Code ALKEWACP
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Bicarbonate
Carbonate
Hydroxide
Total Alkalinity
ll98HBWW217
98ll552-05A
OTT0ll20-14
11/17/98
11/20/98 11:02:00
1
Water
rng/L
received
Cone.
0.754 B
0
0
0.754 B
DL
0.358
RB S ULT S S UM MARY (Cont'd)
ll98HBWW221
9811552-0GA
OTTOll20-15
11/17/98
11/20/98 11:02:00
1
Water
rng/L
received
Cone.
3.95 B
0
0
3.95 B
DL
0.358
1198HBWW222
98ll552-08A
OTT01120-17
11/17/98
11/20/98 11:02:00
1
Water
rng/L
received
Cone.
174 B
0
0
174 B"
DL
0.358
Work Order # 9811552
Page _6_
ll98HBWW223
98ll552-07A
OTT01120-16
11/17/98
11/20/98 11:02:00
1
Water
rng/L
received
Cone.
0.489 B
0
DL
0
0.489 B 0.358
•
• 12/01/98 09:52:04
Method Alkalinity by E310.1
Test Code ALKEWACP
Initial Calibration # ~N~A'--~~~~~~­
Calibration Date ~~~~~~~~
Sequence/Analysis Time
1 11/20/98 11:02:00
2 11/20/98 11:02:00
3 11/20/98 11:02:00
4 11/20/98 11:02:00
5 11/20/98 11:02:00
6 11/20/98 11:02:00
7 11/20/98 11:02:00
8 11/20/98 11:02:00
9 11/20/98 11:02:00
10 11/20/98 11:02:00
11 11/20/98 11:02:00
12 11/20/98 11:02:00
13 11/20/98 11:02:00
14 11/20/98 11:02:00
15 11/20/98 11:02:00
16 11/20/98 11:02:00
17 11/20/98 11:02:00
18 11/20/98 11:02:00
19 11/20/98 11:02:00
20 11/20/98 11:02:00
21 11/20/98 11:02:00
22 11/20/98 11:02:00
23 11/.20/98 11:02:00
24 11/20/98 11:02:00
25 11/20/98 11: 02: 00
• ANALYSIS BATCH SUMMARY
Analysis Batch # WLOTT081120110201
Analysis Start Date/Time 11/20/98 11:02:00
Analysis Stop Date/Time 11/20/98 15:27:00
Project Sample ID Lab Sample ID Sample Type
csv Second Source Standard
BLK984209 Blank, Method
LCS986425 Lab Control Sample
LCSD986425 Lab Control Sample Duplicate
9811468-0lA Sample
9811468-0lA Matrix Spike
9811468-0lA Matrix Spike Duplicate
9811468-02A Sample
9811468-03A Sample
1198HBWW208 9811552-0lA Sample
1198HBWW209 9811552-02A Sample
1198HBWW210 9811552-03A Sample
1198HBWW211 9811552-04A Sample
1198HBWW217 9811552-05A Sample
1198HBWW221 9811552-06A Sample
1198HBWW223 9811552-07A Sample
1198HBWW222 9811552-08A Sample
9811370-0lA Sample
9811370-02A Sample
9811370-03A Sample
98ll370-04A Sample
9811370-05A Sample
9811370-06A Sample
9811370-07A Sample
csv Second Source Standard
Work Order # 9811552
Page _7 _
Instrument ~
Analyst N&
Reviewer ~A~C~R~~~~~~~~
Analysis File #
OTT01120-l
OTT01120-2
OTT01120-3
OTT01120-4
OTT01120-5
OTT01120-6
OTT01120-7
OTT01120-8
OTT01120-9
OTT01120-10
OTT01120-ll
OTT01120-12
OTT01120-13
OTT01120-14
OTT01120-15
OTT01120-16
OTT01120-17
OTT01120-18
OTT01120-19
OTT01120-20
OTT01120-21
OTT01120-22
OTT01120-23
OTT01120-24
OTT01120-25
•
12/01/98 09:52:04
Method Alkalinity by E310.l Specification# ~AL--.-K __ _
Lab Sample ID
File ID
•
Project Sample
ID/Description Analyte
ABALYTICAL PROTOCOL SUMMARY
COMMEBTS/BARRATIVB
Flag Comment/Narrative
•
Corrective Action
Work Order # 9811552
Page _s_
•
11/30/98 12:49:38
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared -~R~a_d_i~a_n_I_n~t_e_r_n~a~t_i_o_n~a~l~·-L~L~C­
By --=1~4~0~4~6-=S~u~m~m~i~t-=D~r~·~·-=B~l~d~g~·-=B:....
P. o. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
ll98HBWW208
ll98HBWW209
ll98HBWW210
ll98HBWW2ll
ll98HBWW217
ll98HBWW221
ll98HBWW223
ll98HBWW222
•
ID/
NORK ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID WASHINGTON, NC
Case # .N~A~-------­
SDG # ~N~A'---------­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA XXIEWASF
02A XXIEWASF
03A XXIEWASF
04A XXIEWASF
OSA XXIEWASF
06A XXIEWASF
07A XXIEWASF
OBA XXIEWASF
•
Anions
Anions
Anions
Anions
Anions
Anions
Anions
Anions
Work Order # 9811553
Page 1.._
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
by IC
by IC
by IC
by IC
by IC
by IC
by IC
by IC
•
• 11/30/98 12:49:38
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB CBRTIPICATIOHS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9811553
Page L
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
11/30/98 12:49:38 ANALYTICAL PROTOCOL SUMMARY
FLAG DEFINITIONS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis. NA
NC
ND
NR
NS
A
B
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hy.drocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
c Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
p Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
s· Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
x See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation .
• •
Work Order # 9811553
Page _3_
•
• 11/30/98 12:49:38
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Method IC EPA 300.0
Project Sample ID/Description
1198HBWW208
1198HBWW209
1198HBWW210
1198HBWW211
1198HBWW217
1198HBWW221
1198HBWW222
1198HBWW223
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9811553-0lA XXIEWASF NA
9811553-02A XXIEWASF NA
9811553-03A XXIEWASF NA
9811553-04A XXIEWASF NA
9811553-05A XXIEWASF NA
9811553-0GA XXIEWASF NA
9811553-08A XXIEWASF NA
9811553-0?A XXIEWASF NA
Work Order # 9811553
Page _4 _
Analysis Batch #
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
•
11/30/98 12:49:38
Method IC EPA 300.0
Test Code XXIEWASF
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Sulfate
•
1198HBWW208
9811553-0lA
Xl001123-18
11/17/98
11/23/98 13:45:38
1
Water
mg/L
received
Cone.
11.2
DL
0.0421
RESULTS SUMMARY
1198HBWW209
9811553-02A
Xl001123-19
11/17/98
11/23/98 14:01:16
1
Water
mg/L
received
Cone.
2.96
DL
0.0421
•
1198HBWW210
9811553-03A
Xl001123-20
11/17/98
11/23/98 14:16:56
1
Water
mg/L
received
Cone.
0 J
DL
0.0421
Work Order # 9811553
Page _5_
1198HBWW211
9811553-04A
Xl001123-21
11/17/98
11/23/98 14:32:36
1
Water
mg/L
received
Cone.
10.5
DL
0. 0421
•
• 11/30/98 12:49:38
Method IC EPA 300.0
Test Code XXIEWASF
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Sulfate
1198HBWW217
9811553-05A
Xl001123-22
11/17/98
11/23/98 14:48:17
1
Water
mg/L
received
Cone.
37.3
DL
0.0421
• R B S ULT S S UH HAR Y (Corit'd)
1198HBWW221
9811553-06A
Xl001123-23
11/17/98
11/23/98 15:03:55
l
Water
mg/L
received
Cone. DL
5.13 0.0421
,j
1198HBWW222
9 811553 -OBA
Xl00ll23-25
11/17/98
11/23/98 15:35:08
1
Water
mg/L
received
Cone. DL
21. 7 0. 0421
Work Order ~ 9811553
Page _6_
1198HBWW223
9811553-07A
Xl001123-24
11/17/98
11/23/98 15:19:29
1
Water
mg/L
received
Cone. DL
19.4 0. 0421
•
11/30/98 12:49:38
Method IC EPA 300.0
Test Code XXIEWASF
Initial Calibration # N~A~~~~~~~~
Calibration Date
Sequence/Analysis Time
1 11/23/98 09:17:38
2 11/23/98 09:33:08
3 11/23/98 09:49:25
4 11/23/98 10:05:05
5 11/23/98 10:20:27
6 11/23/98 10:37:50
7 11/23/98 10:53:28
8 11/23/98 11:09:06
9 11/23/98 11:24:45
10 11/23/98 11:40:24
11 11/23/98 11:56:03
12 11/23/98 12:11:42
13 11/23/98 12:27:22
14 11/23/98 12:43:00
15 11/23/98 12:58:22
16 11/23/98 13:13:48
17 11/23/98 13:29:17
18 11/23/98 13:45:38
19 11/23/98 14:01:16
20 11/23/98 14:16:56
21 11/23/98 14:32:36
22 11/23/98 14:48:17
23 11/23/98 15:03:55
24 11/23/98 15:19:29
25 11/23/98 15:35:08
26 11/23/98 15 :50:46
27 11/23/98 16:06:25
28 11/23/98 16:22:05
29 11/23/98 16:37:42
30 11/23/98 16:53:35
•
ANALYSIS BATCH SUMMARY
Analysis Batch # WLX10081123091701
Analysis Start Date/Time 11/23/98 09:17:00
Analysis Stop Date/Time 11/23/98 18:58:39
Work Order # 9811553
Page _7 _
Instrument ~
Analyst .QI&
Reviewer =A~CR'"'-~~~~~~~-
Project Sample ID Lab Sample ID Sample Type Analysis File #
sysblk Blank, System X1001123-1
rev Initial Calibration Verification X1001123-2
BLK984146 Blank, Method X1001123-3
LCS986339 Lab Control Sample X1001123-4
LCSD986339 Lab Control Sample Duplicate Xl001123-5
9811249-0lA Sample Xl001123-6
9811249-02A Sample X1001123-7
9811249-0lA Sample X1001123-8
9811249-0lA Matrix Spike X1001123-9
9811249-0lA Matrix Spike Duplicate X1001123-10
9811249-02A Sample Xl001123-11
9811497-0lA Sample Xl001123-12
9811497-02A Sample X1001123-13
9811497-03A Sample X1001123-l4
9811497-0lA Matrix Spike X1001123-15
9811497-0lA Matrix Spike Duplicate X1001123-16
CCV Continuing Calibration Verification Xl001123-17
1198HBWW208 9811553-0lA Sample Xl001123-l8
1198HBWW209 9811553-02A Sample X1001123-l9
1198HBWW210 9811553-03A Sample Xl001123-20
1198HBWW211 9811553-04A Sample X1001123-21
1198HBWW217 9811553-05A Sample Xl001123-22
1198HBWW22l 9811553-06A Sample Xl001123-23
1198HBWW223 9811553-07A Sample Xl001123-24
1198HBWW222 9811553-08A Sample Xl001123-25
CCV Continuing Calibration Verification Xl001123-26
9811569-0lA Sampl.e Xl001123-27
9811569-02A Sample Xl001123-28
9811569-03A Matrix Spike Xl001123-29
9811569-04A Matrix Spike Duplicate Xl001123-30
• •
• 11/30/98 12:49:38
Method IC EPA 300.0
Test Code XXIEWASF
Initial Calibration # ~N~A'--------~
Calibration Date
Sequence/Analysis Time
31 11/23/98 17:09:15
32 11/23/98 17:24:53
33 11/23/98 17:40:20
34 11/23/98 17:56:03
35 11/23/98 18:11:42
36 11/23/98 18:27:22
37 11/23/98 18:43:00
38 11/23/98 18:58:39
Project Sample
• AR AL Y S I S B AT C H S UM MA R Y (cont'd)
Analysis Batch# WLX10081123091701
Analysis Start Date/Time 11/23/98 09:17:00
Analysis Stop Date/Time 11/23/98 18:58:39
ID Lab Sample .ID Sample Type
9811569-05A Sample
9811569-06A Matrix Spike
9811569-07A Matrix Spike
9811569-08A Sample
9811569-09A Sample
9811569-lOA Sample
9811569-llA Sample
Duplicate
Work Order # 9811553
Page _8_
Instrument 29:..QQ__.
Analyst DLC
Reviewer _A~C~R ________ _
Analysis File #
Xl001123-31
Xl001123-32
Xl001123-33
X1001123-34
Xl001123-35
X1001123-36
Xl001123-37
CCV Continuing Calibration Verification Xl001123-38
•
ll/30/98 12:49:38
Method IC EPA 300.0
Lab Sample ID
File ID
Project Sample
ID/Description
•
Specification# _x_x_I_E_~
Analyte
ARALYTICAL PROTOCOL SUMMARY
COMMBRTS/RARRATIVB
Flag Comment/Narrative
•
Corrective Action
Work Order # 9811553
Page _9_
•
• ll/30/98 12:49:38 • QUALITY CONTROL BXCBPTIOH RB PORT
SUMMARY
QCER # Analysis Batch Number
98ll23-l2 Xl0098ll2309l700
...
Work Order # 9811553
Page 1Q_ •
QUALITY CONTROL EXCEPTION REPORT
LEVEL 2 -ANALYTICAL
REPORT COPY 981.1569
1CER # 981123-1.2 Revised: 11./25/98
Analyst: DAVID CARRUTHERS
Batch#: Xl00981123091700
~rot Spec: AL/SPC034
Instrument: =D=X~l~O~O~~­
Matrix: ~W=a=t=e=r~~­
Analysis File #:
Date Analyzed: 11 23
Status: ~
Analyte: 804
Client ID: CSC: Lab Sample ID:
9811.569
9811553
9811497
HAM BEACH NC
HAM BEACH NC
HAM BEACH NC
JAL
JAL
JAL
9811249
SAMPLE PREPARATION:
PROBLEM IDENTIFICATION
Sample Went Dry
Loss of %
of Sample
Emulsion Formed
Blank Contamination
Instrument
Hold Time
MS/MSD Not Available
Instrument
Other (Describe)
Comments:
SAMPLE ANALYSIS:
PROBLEM IDENTIFICATION
Surrogate Recovery _
MS/MSD Recovery X
LCS/LCSD Recovery
MS/MSD Precision
LCS/LCSD Precision
Standard
Blank Contamination
Instrument
Hold Time
No MS/MSD Available
for Batch
Sample pH
Dil. Due to Hi-Level
Non-Target Analytes
Serial Dilution
Analytical Spike
Internal Standard
Other (Desc:i;:-ibe)
PROBABLE CAUSE
Matrix Effect
Instrument
Spiking Error
Contamination
Coelution
Unknown X
Other(Describe)
Project Sample ID:
CORRECTIVE ACTION TAKEN
Reprepare Sample
Sample Sent for Analysis
Re sample
Other (Describe)
;
CORRECTIVE ACTION TAKEN
Reprepare Sample
Reanalyze Sample
Reanalyze LCS/LCSD
Recalibrate Instrument
Analyze Out of Hold Time
Prepare New Standard
Flag Data X
Re sample
Analyze by MSA _
Perform Analytical Spike _
No Action Required X
Level 3 QCER to Follow
Other (Describe)
•
Comments: The MS and MSD (9811497-0lAS and 9811497-0lASD) recoveries of
109% each are outside of tolerance. The LCS/LCSD recoveries •
of 101% and 99% are acceptable. No action taken per protocol
specification.
Distribution: CSC, Lab, Report
12/08/98 16:33:09
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared --"'R"'a"'d"'i""a_n'-"I'"n"'t"'e"'r'"n"'a"'t"'i"'o"'n"'a"'l"',-"L"'L""C'-
By --=1-4~0_4~6-=S~u~m~m~i_t-=D~r~·~·-=B-l_d_g~·-=B~
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW210
1198HBWW211
1198HBWW223
1198HBWW222
•
ID/
MORK ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON.NC
Work ID WASHINGTON, NC
Case # _N_A __ ~~~~~~~~
SDG # _NA~~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA TDSEWAOO
02A TDSEWAOO
03A TDSEWAOO
04A TDSEWAOO
•
Total
Total
Total
Total
Work Order # 9811554
Page .!..__
RCN 650138. 0602
New York ELAP ID #: 10915
Method Desciption
Dissolved Solids
Dissolved Solids
Dissolved Solids
Dissolved Solids
•
• 12/08/98 16:33:09
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB CBRTIFICATIOHS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order ff 9811554
Page L
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
12/08/98 16:33:09 A H A L Y T I C A L P R 0 T 0 C 0 L" S U M M A R Y
FLAG DBPIHITIOHS
Flag Definition
< DL
NA
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
NC RPD and/or \ Recovery not calculated. See Narrative for explanation.
ND Not detected. No instrument response for analyte or result less than zero.
NR Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
NS Analyte not spiked.
A Presence o{ hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit {and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions {MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation .
• •
Work Order # 9811554
Page _3_
•
• 12/08/98 16:33:09
Client: HAMILTON BEACH
Facility WASHINGTON NC
Client: Code HAM BEACH NC
Method TDS E160.1
Project: Sample ID/Description
1198HBWW210
1198HBWW2l0
1198HBWW211
1198HBWW211
1198HBWW211
1198HBWW222
1198HBWW222
1198HBWW223
1198HBWW223
• ANALYTICAL PROTOCOL SUMMARY
Ext:ract:ion/Digest:ion
Lab Sample ID Test: Cdde(s) Batch ff
9811554-0lA TDSEWAOO NA
9811554-0lA TDSEWAOO NA
9811554-02A TDSEWAOO NA
9811554-02A TDSEWAOO NA
98ll554-02A TDSEWAOO NA
9811554-04A TDSEWAOO NA
9811554-04A TDSEWAOO NA
9811554-03A TDSEWAOO NA
9811554-03A TDSEWAOO NA
Work Order ff 9811554
Page _4 _
Analysis Batch u
WLTDS_81120120001
WLTDS_8ll3012000l
WLTDS_8ll20l20001
WLTDS_8ll30l20001
WLTDS_81130120001
WLTDS_8ll20l2000l
WLTDS_81l30120001
WLTDS_8ll20120001
WLTDS_81130120001
•
12/08/98 16:33:09
Method TDS El60.l
Test Code TDSEWAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Total dissolved solids
•
ll98HBWW210
9811554-0lA
TDS1120-14
11/17 /98
11/20/98 12:00:00
l
Water
mg/L
received
Cone.
420 B
DL
5.26
RESULTS SUMMARY
ll98HBWW210
9811554-0lA
TDS1130-5
11/17/98
11/30/98 12:00:00
l
Water
mg/L
received
Cone.
228 BX
•
DL
5.26
ll98HBWW2ll
9811554-02A
TDSll20-15
11/17/98
11/20/98 12:00:00
1
Water
mg/L
received
Cone.
296 B
DL
5.26
Work Order # 9811554
Page _5_
ll98HBWW211
9811554-02A
TDS1130-6
11/17/98
11/30/98 12:00:00
1
Water
mg/L
received
Cone. DL
92.0 BX 5.26
•
• 12/08/98 16:33:09
Method TDS El60.l
Test Code TDSEWAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Total dissolved solids
1198HBWW211
9811554-02A
TDS1130-9
11/17/98
11/30/98 12:00:00
l
Water
mg/L
received
Cone. DL
84.0 BX 5.26
• RB S ULT S S UM MAR Y (Cont'd)
1198HBWW222
9811554-04A
TDS1120-17
11/17/98
11/20/98 12:00:00
1
Water
mg/L
received
Cone. DL
472 B 5.26
1198HBWW222
9811554-04A
TDS1130-8
11/17 /98
11/30/98 12:00:00
1
Water
mg/L
received
Cone. DL
298 BX 5.26
Work Order # 9811554
Page _6_
1198HBWW223
9811554-03A
TDS1120-16
11/17 /98
11/20/98 12:00:00
1
Water
mg/L
received
Cone. DL
·•
348 B 5.26
12/08/98 16:33:09
Method TDS El60.l
Test Code TDSEWAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Total dissolved solids
•
1198HBWW223
9811554-03A
TDS1130-7
11/17 /98
11/30/98 12:00:00
l
Water
mg/L
received
Cone. DL
134 BX 5.26
RESULTS SUMMARY (Cont'd)
Cone. DL Cone.
•
DL
Work Order tt 9811554
Page 2_
Cone. DL
•
• 12/08/98 16:33:09
Method TDS E160.1
Test Code TDSEWAOO
Initial Calibration # ~N~A~~~~~~~­
Calibration Date
Sequence/Analysis Time
1 11/20/98 12:00:00
2 11/20/98 12:00:00
3 11/20/98 12:00:00
4 11/20/98 12:00:00
5 11/20/98 12:00:00
6 11/20/98 12:00:00
7 11/20/98 12:00:00
8 11/20/98 12:00:00
9 11/20/98 12:00:00
10 11/20/98 12:00:00
11 11/20/98 12:00:00
12 11/20/98 12:00:00
13 11/20/98 12:00:00
14 11/20/98 12:00:00
15 11/20/98 12:00:00
16 11/20/98 12:00:00
17 11/20/98 12:00:00
Project Sample
1198HBWW210
1198HBWW211
1198HBWW223
1198HBWW222
• A !if A L Y S I S B A T C H S U M M A R Y
Analysis Batch # WLTDS 81120120001
Analysis Start Date/Time 11/20/98 12:00:00
Analysis Stop Date/Time 11/23/98 12:00:00
ID Lab Sample ID Sample Type
BLK984129 Blank, Method
LCS986323 Lab Control Sample
LCSD986323 Lab Control Sample
9811469-0lA Sample
A9811514-01 Sample
A9811514-02 Sample
A9811514-03 Sample
A9811514-04 Sample
A9811514-05 Sample Duplicate
A9811514-06 Sample
A9811514-07 Sample
A9811514-08 Sample
A9811514-09 Sample
9811554-0lA Sample
9811554-02A Sample
9811554-03A Sample
9811554-04A Sample
Duplicate
Work Order # 9811554
Page _8 _
Instrument 112§__
Analyst !':!!!!
Reviewer ~AC~R"-~~~~~~~
Analysis File #
TDS1120-1
TDS1120-2
TDS1120-3
TDS1120-4
TDS1120-5
TDS1120-6
TDS1120-7
TDS1120-8
TDS1120-9
TDS1120-10
TDS1120-11
TDS1120-12
TDS1120-13
TDS1120-14
TDS1120-15
TDS1120-16
TDS1120-17
•
12/08/98 16:33:09
Method TDS E160.1
Test Code TDSEWAOO
Initial Calibration # ~N~A'--~~~~~~­
Calibration Date
Sequence/Analysis Time
1 11/30/98 12:00:00
2 11/30/98 12:00:00
3 11/30/98 12:00:00
4 11/30/98 12:00:00
5 11/30/98 12:00:00
6 11/30/98 12:00:00
7 11/30/98 12:00:00
8 11/30/98 12:00:00
9 11/30/98 12:00:00
••
AHALYSIS BATCH SUMMARY
Analysis Batch # WLTDS 81130120001
Analysis Start Date/Time 11/30/98 12:00:00
Analysi~ Stop Date/Time 11/30/98 12:00:00
Project Sample ID Lab Sample ID Sample Type
BLK984199 Blank, Method
LCS986415 Lab Control Sample
LCSD986415 Lab Control Sample
9811469-0lA Sample
1198HBWW210 9811554-0lA Sample
1198HBWW211 9811554-02A Sample
1198HBWW223 9811554-03A Sample
1198HBWW222 9811554-04A Sample
1198HBWW211 9811554-02A Sample Duplicate
•
Duplicate
Work Order # 9811554
Page _9 _
Instrument I!2§___
Analyst .!:1!:!!
Reviewer ~A~C~R~~~~~~~~
Analysis·File II
TDS1130-1
TDS1130-2
TDS1130-3
TDS1130-4
TDS1130-5
TDS1130-6
TDS1130-7
TDS1130-8
TDS1130-9
•
• 12/08/98 16:33:09
Method TDS El60.l
Lab Sample ID
File ID
9811554-0lA
TDS1130-5
Project Sample
ID/Description
1198HBWW210
Specification# TDSE
Analyte
TDS
• ANALYTICAL PROTOCOL SUMMARY Work • Order # 9811554
COMMBHTS/HARRATIVB Page 1Q_
Flag Comment/Narrative Corrective Action
x Samples were analyzed outside of hold time.
: }
12/08/98 16:33:09
•
QUALITY CONTROL BICBPTIOll RB PORT
SUMMARY
QCER II Analysis Batch Number
981120-15 TDS98ll20120000
•
Work Order # 9811554
Page .!.L
•
QUALITY CONTROL EXCEPTION REPORT
LEVEL 2 -ANALYTICAL
REPORT COPY 9811~54
.. # 981120-15 Revised:
~alyst: M A THEISEN
Batch #: TDS981120120000
Prot Spec: ALSPC022
Instrument: ~T=D=·s'--~~~
Matrix: ~W~a~t~e=r---~~
Analysis File #:
Date Analyzed: 11/20/98
Status: Q
Analyte: TDS
Client ID: CSC: Lab Sample ID:
9b11469
9811554
HAM BEACH NC
HAM BEACH NC
JAL
JAL
SAMPLE PREPARATION:
PROB~EM IDENTIFICATION
Sample Went Dry
Loss of %
of Sample
Emulsion Formed
Blank Contamination
Instrument
Hold Time
MS/MSD Not Available
Instrument
Other (Describe)
Aents:
SAMPLE ANALYSIS:
PROBLEM IDENTIFICATION
Surrogate Recovery
MS/MSD Recovery
LCS/LCSD Recovery X
MS/MSD Precision
LCS/LCSD Precision
Standard
Blank Contamination X
Instrument
Hold Time
No MS/MSD Available
for Batch
Sample.pH
Dil. Due to Hi-Level
Non-Target Analytes
Serial Dilution
Analytical Spike
Internal Standard
Other (Describe) ·---
PROBABLE CAUSE
Matrix Effect
Instrument
Spiking Error
Contamination X
Coelution
Unknown
Other(Describe)
Project SamFle ID:
CORRECTIVE ACTION TAKEN
Reprepare Sample
Sample Sent for Analysis
Res ample
Other (Describe)
CORRECTIVE ACTION TAKEN
Reprepare Sample X
Reanalyze Sample X
Reanalyze LCS/LCSD
Recalibrate Instrument
Analyze Out of Hold Time X
Prepare New Standard
Flag Data X
Resample
Analyze by MSA _
Perform Analytical Spike
No Action Required
Level 3 QCER to Follow
Other (Describe)
Comments: The LCS/LCSD recoveries of 130% and 126% are outside of
tolerance. In addtion, the method blank (BLK984129)
concentration of 208mg/L is above the PRDL of 15mg/L. Likely
cause is contaminated water in wash bottle used for rinsining.
Distribution: CSC, Lab, Report
QCER # 981120-15
QUALITY CONTROL EXCEPTION REPORT (Cont'd)
LEVEL 2 -ANALYTICAL
Revised:
Samples were re-prepared and re-analyzed outside of hold time. Results
for re-analysis are reported in batch:TDS981130120000. The results
are "x" flagged; the 11 x 11 comment explains that the samples were
analyzed outside of hold time.
•
•
12/01/98 13:42:59
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared -~R~a~d""i~a~n'--=I~n:!:t:!:e""r~n~a:!:t~i;.::o~n~a~l~,_;L::L~C._
By --=l..:4.::0..:4.::6_:::S,,u:::;m:::;m"°i"'t'-"D::r-'.-''--"B:i!l:.::d:::iqL.:. . .....:B:....
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW208
1198HBWW209
1198HBWW210
119BHBWW211
TRIP BLANK #1
119BHBWW229
119BHBWW230
1198HBWW231
1198HBWW223
•
ID/
WORK ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID WASHINGTON, NC
Case # .N_A..__ _______ _
SDG # ~N~A~~~~~~~~
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA 826SWACM
OlB SPAREBOO
OlC SPAREBOO
02A 826SWACM
02B SPAREBOO
02C SPAREBOO
03A 826SWACM
03B SPAREBOO
03C SPAREBOO
04A B26SWACM
04B SPAREBOO
04C SPAREBOO
05A 826SWACM
06A 826SWACM
06B SPAREBOO
06C SPAREBOO
07A 826SWACM
07B SPAREBOO
07C SPAREBOO
OBA 826SWACM
OBB SPAREBOO
OBC SPAREBOO
09A 826SWACM
•
Work Order # 9811555
Page _1_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile.Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
•
• 12/01/98 13:42:59
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
. Prepared _.....:;R"'a"'d"'i"'a~n:......;:Io:;n:.::t;.::e::r'"'n"'a"'t"'i"'o"'n"'a"'l"',_,L,.L!:.C:...
By --=1:..:4:..:0...:4:..:6-=S:..:u"'m"'m:.:i:..:t'-=D"'r"'.-''-=B:.:l:..:d:.;;qi..::·.......:;B:...
P. O. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW223
ll98HBWW222
ll98HBWE01
TRIP BLANK #2
1198HBWW208
ID/
• llORI: ORDBR SUMMARY {Cont'd)
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID WASHINGTON, NC
Case # ~N~A'--~~~~~~~~
SDG # .,N...,A'----------
RAS # 80903AJAL
Lab Sample ID Test Code(s)
09B SPAREBOO
09C SPAREBOO
lOA 826SWACM
lOB SPAREBOO
lOC SPAREBOO
llA 826SWACM
llB SPAREBOO
11C .SPAREBOO
12A 826SWACM
12B SPAREBOO
13A MS 826SWAMS
14A MSD 826SWAMS
Work Order # 9811555
Page L
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Spare Sample
Volatile Organics by GC/MS
Spare Sample
Volatile Organics by GC/MS
Volatile Organics by GC/MS
•
12/01/98 13:42:59
•
MORI ORDBR COMMBRTS
The standard Method 8260A surrogate tolerances are laboratory derived from
historical data. Project specific tolerances may differ .
•
Work Order # 9811555
Page _3_
•
• 12/01/98 13:42:59
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Ol:lahoma
South Carolina
Utah
Wisconsin
• STATB CERTIFICATIONS
Agency
Depar,tment of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey ~epartmen~ of Environmental Prot.ecti~n
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9811555
Page _4_
Certification JD
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
12/01/98 13:42:59 AliALYTICAL PROTOCOL SUMMARY
P L A G D B P I Ii I T I 0 Ii S
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis. NA
NC
ND
NR
NS
RPD and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero).
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation .
• •
Work Order tt 9811555
Page _5_
•
• 12/01/98 13:42:59
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Volatile Organics SW8260B
Project: Sample ID/Description
1198HBWE01
1198HBWW208
1198HBWW209
1198HBWW209
1198HBWW210
119BHBWW210
1198HBWW210
1198HBWW211
1198HBWW211
1198HBWW222
1198HBWW223
1198HBWW229
1198HBWW229
1198HBWW229
1198HBWW230
1198HBWW230
1198HBWW231
1198HBWW231
1198HBWW231
TRIP BLANK #1
TRIP BLANK #1
TRIP BLANK #2
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9811555-llA 826SWACM NA
9811555-0lA 826SWACM NA
9811555-02A 826SWACM NA
9811555-02B 826SWACM NA
9811555-03A 826SWACM NA
9811555-03B 826SWACM NA
9811555-Q3C 826SWACM NA
9811555-04A 826SWACM NA
9811555-04B 826SWACM NA
9811555-lOA 826SWACM NA
9811555-09A 826SWACM NA
9811555-0GA 826SWACM NA
9811555-0GC 826SWACM NA
9811555-0GC 826SWACM NA
9811555-0?A 826SWACM NA
9811555-0?B 826SWACM NA
9811555-08A 826SWACM NA
9811555-08B 826SWACM NA
9811555-08C 826SWACM NA
9811555-05A 826SWACM NA
9811555-05A 826SWACM NA
9811555-12A 826SWACM NA
" I
Work Order # 9811555
Page _6 _
Analysis Batch #
MSMSDB81120015201
MSMSDB81120015201
MSMSDB81120015201
MSMSDB81121035401
MSMSDB81120015201
MSMSDB81121035401
MSMSDC81123170401
MSMSDB81120015201
MSMSDB81121035401
MSMSDB81120015201
MSMSDB81120015201
MSMSDB81120015201
MSMSDC81123170401
MSMSDC81123170401
MSMSDB81120015201
MSMSDB81121035401
MSMSDB81120015201
MSMSDB81121035401
MSMSDC81123170401
MSMSDB81120015201
MSMSDB81121035401
MSMSDB81120015201
•
12/0l/9B 13:42:59
Method Volatile Organics SWB260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone(MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2~Chloro-l,3-butadiene
Chlorobenzene
Chloroethane
•
1198HBWE01
9811555-llA
81120820
11/17 /9B 13: 00
00:00:00
11/20/98 10:18:00
1
Water
ug/L
received
Cone. DL
ND 0.413
ND 5.72
ND 7.17
ND 0.333
ND 0.0375
ND 0.0928
ND 0.0624
ND 0.0828
ND 0.0634
ND 0.0547
ND 0.0467
ND 0.222
ND 0.116
ND 0.07B2
ND O.OB23
ND 0.0547
ND 0.0576
ND 0.0719
ND 0.0453
ND 0.0441
R. B S U L T S S U M M A R. Y
119BHBWW20B
9811555-0lA
Bll20BOB
11/17/98 13:25
00:00:00
11/20/98 04:40:00
1
Water
ug/L
received
Cone. DL
ND 0.413
ND 5.72
ND 7.17
ND 0.333
ND 0.0375
ND 0.0928
ND 0.0624
ND O.OB2B
ND 0.0634
ND 0.0547
ND 0.0467
ND 0.222
ND 0.116
ND 0.07B2
ND 0.0823
ND 0.0547
ND 0.0576
ND 0.0719
ND 0.0453
ND 0.0441
•
ll9BHBWW209
9811555-02A
81120811
11/17/9B 14:00
00:00:00
ll/20/9B 06:05:00
l
Water
ug/L
received
Cone. DL
11.0 0.413
ND 5.72
ND 7.17
ND 0.333
ND 0.0375
ND 0.0928
ND 0.0624
ND O.OB28
ND 0.0634
ND 0.0547
ND 0.0467
3.82 0.222
ND 0.116
ND 0.07B2
ND 0.0823
ND 0.0547
ND 0.0576
ND 0.0719
ND 0.0453
1.16 0.0441
Work Order # 9811555
Page _7_
119BHBWW209
9811555-028
81121811
11/17/98 14:00
00:00:00
ll/21/9B OB:08:00
50
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
20.6
2B6
35B
16.6
l. BB
4.64
3.12
4.14
3.17
2.74
2.34
11.l
5.80
3.91
4.12
2.74
2.88
3.60
2.26
2.20
•
• 12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane 1
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodif luoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1198H8WE01
9811555-llA
81120820
11/17/98 13:00
00:00:00
11/20/98 10:18:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.188 z
ND
DL
0.0480
0.0605
0.0521
0.0605
0.0881
0.0538
0.194
0.0769
0.0435
0.118
0 .412
0.0733
0.0469
0.0466
0.176
0.0576
0.0348
0.0715
0.0383
0.0618
• R. B S UL TS S UM MAR Y (Cont'd)
1198H8WW208
9811555-0lA
81120808
11/17/98 13:25
00:00:00
11/20/98 04:40:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0480
0.0605
0.0521
0.0605
0.0881
0.0538
0.194
0.0769
0.0435
0.118
0 .412
0.0733
0. 0469
0.0466
0.176
0.0576
0.0348
0 .0715
0.0383
0.0618
1198H8WW209
9811555-02A
81120811
11/17 /98 14: 00
00:00:00
11/20/98 06:05:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
499 ER
14. l
50.5
47.7
l.46
DL
0. 0480
0.0605
0.0521
0.0605
0.0881
0.0538
0.194
0.0769
0.0435
0.118
0.412
0.0733
0.0469
0.0466
0.176
0.0576
0.0348
0. 0715
0.0383
0.0618
Work Order # 9811555
Page _8_
1198H8WW209
•
9811555-028
81121811
11/17/98 14:00
00:00:00
11/21/98 08:08:00
50
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1040
14.0
63 .·9
59.0
ND
DL
2.40
3.02
2.60
3.02
4.40
2.69
9.70
3.84
2.i0
5.90
20.6
3.66
2.34
2.33
8.80
2.88
l. 74
3.58
l. 92
3.09
• 12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units,
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
1198HBWE01
9811555-llA
81120820
11/17/98 13:00
00:00:00
11/20/98 10:18:00
1
Water
ug/L
received
Cone. DL
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.699
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0578
0.0848
0.102
0.0515
0.489
0.0522
0.0896
0 .113
0.0658
0.0602
0. 0892
0.0473
0.0514
0.0986
0.0952
0.0800
0. 0929
0.0639
0.115
0. 0414
• R KS ULT S S UM MAR y· (Cont'd)
1198HBWW208
9811555-0lA
81120808
11/17/98 13:25
00:00:00
11/20/98 04:40:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0578
0.0848
0.102
0.0515
0.489
0.0522
0.0896
0.113
0.0658
0.0602
0.0892
0. 0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0. 0414
1198H8WW209
9811555-02A
81120811
11/17/98 14 :00
00:00:00
11/20/98 06:05:00
1
W~ter
ug/L
received
Cone.
ND
ND
ND
ND
ND
3.24
ND
ND
ND
1.58
3.27
ND
ND
ND
ND
ND
ND
1. 69
ND
ND
DL
0.0578
0.0848
0.102
0.0515
0 .489
0.0522
0.0896
0.113
0.0658
0.0602
0.0892
0.0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0. 0414
Work Order U 9811555
Page 1.Q_
1198H8WW209
9811555-028
81121811
•
11/17 /98 14: 00
00:00:00
11/21/98 08:08:00
50
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.36 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
2.89
4.24
5.10
2.58
24.4
2.61
4.48
5.65
3.29
3.01
4.46
2.36
2.57
4.93
4.76
4.00
4.64
3.20
5.75
2.07
12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
•
1198H8WE01
9811555-llA
81120820
11/17 /98 13: 00
00:00:00
11/20/98 10:16:00
1
Water
ug/L
received
Cone.
Recovery
\
94
94
100
DL
RESULTS S UM MAR Y (Cont'd)
1198H8WW208
9811555-0lA
81120808
11/17/98 13:25
00:00:00
ll/20/98 04:40:00
1.
Water
ug/L
received
Cone.
Recovery
'
98
93
94
•
DL
1198H8WW209
9811555-02A
81120811
11/17/98 14:00
00:00:00
11/20/9e oG:os:oo
1
Water
ug/L
received
Cone.
Recovery
\
94
96
96
DL
Work Order # 9811555
Page ll_
1198HBWW209
9811555-028
Bll21811
11/17/98 14:00
00:00:00
11/21/98 08:08:00
50
Water
ug/L
received
Cone.
Recovery
\
94
93
100
DL
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof orm
8romomethane
2-8utanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
1198HBWW210
9811555-03A
81120812
11/17/98 15:05
00:00:00
11/20/98 06:33:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.413
5. 72
7.17
0.333
0.0375
0.0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0.0719
0.0453
0.0441
• RBS ULT S SUMMARY (Cont'd)
!'.
1198HBWW210
9811555-038
81121813
11/17/98 15:05
00:00:00
11/21/98 09:07:00
100
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
41.3
572
717
33.3
3.75
9.28
6.24
8.28
6.34
5.47
4.67
22.2
11.6
7.82
8.23
5.47
5.76
7.19
4.53
4.41
1198H8WW210
9811555-03C
Cll23817
11/17/98 15:05
00:00:00
11/23/98 23:55:00
5000
Water
ug/L
received
Cone.
ND
ND
ND
.ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
4040
22800
20700
3900
324
520
1910
468
520
890
620
1160
565
780
820
660
715
210
945
488
• Work Order ff 9811555
Page 1L
1198HBWW211
9811555-04A
81120813
11/17/98 14:45
00:00:00
11/20/98 07:01:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.78
DL
0.413
5. 72
7.17
0.333
0.0375
0.0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0.0719
0.0453
0.0441
12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
•
1198H8WW210
9811555-03A
81120812
11/17/98 15:05
00:00:00
11/20/98 06:33:00
1
Water
ug/L
received
Cone. DL
0.226 0.0480
ND 0.0605
ND 0.0521
ND 0.0605
ND 0.0881
ND 0.0538
ND 0.194
ND 0.0769
ND 0.0435
ND 0.118
ND 0.412
ND 0.0733
ND 0.0469
ND 0.0466
ND 0.176
18.8 z 0.0576
ND 0.0348
48.5 0. 0715
2580 ER 0.0383
188 ER 0.0618
R. B S ULT S S UH HAR. Y (Cont'd)
1198HBWW210 1198H8WW210
9811555-038 9811555-03C
81121813 C1123817
11/17/98 15:05 11/17/98 15:05
00:00:00 00:00:00
11/21/98 09:07:00 11/23/98 23:55:00
100 5000
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 4.80 ND 466
ND 6.05 ND 785
ND 5.21 ND 438
ND 6.05 ND 452
ND 8.81 ND 1480
ND 5.38 ND 1560
ND 19.4 ND 7150
ND 7.69 ND 381
ND 4.35 ND 438
ND 11.8 ND 1020
ND 41.2 ND 1430
ND 7.33 ND 1670
ND 4.69 ND 1640
ND 4.66 ND 1760
ND 17.6 ND 338
ND 5.76 ND 182
ND 3.48 ND 494
75.6 7.15 ND 635
17000 ER 3.83 11600 232
96.1 6.18 ND 418
•
Work Order U 9811555
Page 1l_
1198H8WW211
9811555-04A
81120813
11/17 /98 14:45
00:00:00
11/20/98 07:01:00
1
Water
ug/L
received
Cone. DL
ND 0.0480
ND 0.0605
ND 0.0521
ND 0.0605
ND 0.0881
ND 0.0538
ND 0.194
ND 0.0769
ND 0.0435
ND 0.118
ND 0.412
ND 0.0733
ND 0.0469
ND 0. 0466
ND 0.176
4.50 z 0.0576
ND 0.0348
20.1 0. 0715
471 ER 0.0383
16.5 z 0.0618
•
• 12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
1198H8WW210
9811555-03A
81120812
11/17/98 15:05
00:00:00
11/20/98 06:33:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
6.26
ND
ND
ND
ND
0.688
ND
ND
ND
0.404 B
ND
ND
ND
DL
0.0631
0.0397
0.0769
0.0444
0. 0421
0.0643
0.0361
0.0928
0.115
0.232
0.0291
0.0661
0.106
0.130
0.0365
0.160
0.137
0.578
0.390
0.0577
• R B S U LT S S UM MAR Y (Cont'd)
1198HBWW210
9811555-038
81121813
11/17/98 15:05
00:00:00
11/21/98 09:07:00
100
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
5.52 J
ND
ND
ND
ND
ND
ND
ND
ND
23.5 B
ND
ND
ND
DL
6.31
3.97
7.69
4.44
4.21
6.43
3.61
9.28
11.5
23.2
2. 91
6.61
10.6
13.0
3.65
16.0
13.7
57.8
39.0
5. 77
1198H8WW210
9811555-03C
Cl123817
11/17/98 15:05
00:00:00
11/23/98 23:55:00
5000
Water
ug/L
received
Cone.
ND
ND
ND
ND.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1600 B
ND
ND
ND
DL
730
309
350
795
580
200
306
1170
2770
3680
595
1280
680
620
323
685
1090
1170
2900
1200
• Work Order # 9811555
Page 11....
1198HBWW211
9811555-04A
81120813
11/17 /98 14: 45
00:00:00
11/20/98 07:01:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.332
ND
ND
ND
0.156 B
ND
ND
ND
DL
0.0631
0.0397
0.0769
0.0444
0. 0421
0.0643
0.0361
0.0928
0.115
0.232
0. 0291
0.0661
0.106
0.130
0.0365
0.160
0.137
0.578
0.390
0.0577
12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
•
1198HBWW210
9811555-03A
81120812
11/17/98 15:05
00:00:00
11/20/98 06:33:00
1
Water
ug/L
received
Cone. DL
ND 0.0578
ND 0. 0848
0.645 0.102
250 ER 0.0515
ND 0.489
14.l 0.0522
ND 0.0896
ND 0.113
ND 0.0658
ND 0.0602
5530 ER 0.0892
ND 0.0473
ND 0.0514
ND 0.0986
ND 0.0952
ND 0.0800
ND 0.0929
8.02 0. 0639
0.860 0.115
0.292 0. 0414
R B S ULT S S UM MAR Y (Cont'd)
1198HBWW210 1198H8WW210
9811555-038 9811555-03C
81121813 Cll23817
11/17/98 15:05 11/17/98 15:05
00:00:00 00:00:00
11/21/98 09:07:00 11/23/98 23:55:00
100 5000
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 5.78 ND 970
ND 8.48 ND 790
ND 10.2 ND 485
502 5.15 ND 1700
ND 48.9 ND 4600
33.8 5.22 ND 705
ND 8.96 ND 1750
ND 11.3 ND 1660
ND 6.58 ND 482
ND 6.02 ND 440
54700 ER 8.92 45800 1100
ND 4.73 ND 910
ND 5.14 ND 1260
ND 9.86 ND 565
ND 9.52 ND 1020
ND 8.00 ND 1020
ND 9.29 ND 374
ND 6.39 ND 810
ND 11.5 ND 2500
ND 4.14 ND 1300
•
Work Order # 9811555
Page 12_
1198H8WW211
9811555-04A
81120813
11/17/98 14:45
00:00:00
11/20/98 07:01:00
1
Water
ug/L
received
Cone. DL
ND 0.0578
ND 0.0848
ND 0.102
0.454 z 0.0515
8.11 0.489
15.6 0.0522
ND 0.0896
ND 0.113
0.187 0.0658
ND 0.0602
83.0 z 0.0892
ND 0.0473
ND 0.05i4
ND 0.0986
ND 0.0952
ND 0.0800
ND 0.0929
o. 771 0.0639
ND 0.115
ND 0. 0414
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Mat'rix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
1198HBWW210
9811555-03A
Bll20812
11/17/98 15:05
00:00:00
11/20/98 06:33:00
1
Water
ug/L
received
Cone.
Recovery
\
101
110
90
DL
• ll B SULT S S UM MA ll Y (Cont'd)
1198HBWW210 1198HBWW210
9811555-03B 9811555-03C
Bll21813 C1123817
11/17/98 15:05 11/17/98 15:05
00:00:00 00:00:00
11/21/98 09:07:00 11/23/98 23:55:00
100 5000
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
Recovery Recovery
\ \
96 95
93 105
99 103
Work Order tt 9811555
Page lL
1198HBWW211
9811555-04A
B1120813
11/17/98 14:45
00:00:00
11/20/98 07:01:00
1
Water
ug/L
received
Cone. DL
Recovery
\
94
76
88
•
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 626SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone(MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
•
1196HBWW211
9 811555-048
81121812
11/17/98 14:45
00:00:00
11/21/96 08:36:00
so
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
20.6
286
358
16.6
1. 88
4.64
3.12
4.14
3.17
2.74
2.34
11.1
5.80
3.91
4.12
2.74
2.88
3.60
2.26
2.20
R B S UL TS S UH HA R Y (Cont'd)
1196HBWW222
9811555-lOA
Bll20619
11/17/96 10:45
00:00:00
11/20/96 09:50:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
0.413
5. 72
7.17
0.333
0.0375
0. 0928
0.0624
0.0826
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0.0719
0.0453
0.0441
1198HBWW223
9811555-09A
Bll20618
11/17/96 10:50
00:00:00
11/20/98 09:22:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.413
5.72
7.17
0.333
0.0375
o. 0920
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0762
o. 082-3
0.0547
0.0576
0.0719
0.0453
o. 0441
Work Order # 9811555
Page .!]_
1198HBWW229
9811555-06A
81120815
11/17/98 08:25
00:00:00
11/20/98 07:57:00
1
Water
ug/L
received
Cone.
31. 0
ND
ND
ND
0.539
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.68
DL
0 .413
5. 72
7.17
0.333
0.0375
0.0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0. 0547
0.0576
0.0719
0. 0453
0. 0441
•
• 12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodif luoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1198HBWW211
9811555-048
81121812
11/17/98 14:45
00:00:00
11/21/98 08:38:00
50
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
37.2
1520
11.8
DL
2.40
3.02
2.60
3.02
4.40
2.69
9.70
3.84
2.18
5.90
20.6
3.66
2.34
2.33
8.80
2.88
1.74
3.58
1. 92
3.09
• R B S U L T S S U M M A R Y (Cont• d)
. ,\'
1198H8WW222
9811555-lOA
81120819
ll/17/98 10:45
00:00:00
11/20/98 09:50:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.223 z
ND
DL
0.0480
0.0605
0.0521
0.0605
0.0881
0.0538
0,194
0.0769
0.0435
0.118
0.4p
0.0733
0.0469
0.0466
0.176
0.0576
0.0348
0.0715
0.0383
0.0618
1198H8WW223
9811555-09A
81120818
11/17/98 10:50
00:00:00
11/20/98 09:22:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.369 z
ND
DL
0.0480
0.0605
0.0521
0.0605
0.0881
0.0538
0 .194
0.0769
0.0435
0.118
0.412
0.0733
0.0469
0.0466
0.176
0.0576
0.0348
0.0715
0.0383
0.0618
• Work Order # 9811555
Page 1!L
1198H8WW229
9811555-06A
81120815
11/17/98 08:25
00:00:00
11/20/98 07:57:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
927 ER
49. 7
535 ER
2290 ER
72.4
DL
0.0480
0.0605
0.0521
0.0605
0.0881
0.0538
0.194
0.0769
0.0435
0.118
0 .412
0.0733
0. 0469
0.0466
0.176
0.0576
0.0348
0.0715
0.0383
0.0618
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethyl benzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone{MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
•
1198HBWW211
9811555-04B
Bll21812
11/17/98 14:45
00:00:00
11/21/98 08:38:00
so
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12.0 B
ND
ND
ND
DL
3.16
1. 98
3.84
2.22
2.10
3.22
1.80
4.64
5.75
11.6
1.46
3.30
5.30
6.50
1. 82
8.00
6.85
28.9
19.5
2.88
R. B S ULT S S UM MAR. Y (Cont'd)
1198HBWW222
9811555-lOA
Bll20819
11/17/98 10:45
00:00:00
11/20/98 09:50:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.237 B
ND
ND
ND
•
DL
0.0631
0.0397
0.0769
0.0444
0.0421
0.0643
0.0361
0.0928
0.115
0.232
0.0291
0.0661
0.106
0.130
0.0365
0.160
0.137
0.578
0.390
0.0577
1198HBWW223
9811555-09A
Bll20818
11/17/98 10:50
00:00:00
11/20/98 09:22:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.228 B
ND
ND
ND
DL
0.0631
0.0397
0.0769
0.0444
0. 0421
0.0643
0.0361
0. 0928
0.115
0.232
0.0291
0.0661
0.106
0.130
0.0365
0.160
0.137
0.578
0.390
0.0577
Work Order ff 9811555
Page lL
1198HBWW229
9811555-06A
Bll20815
11/17/98 08:25
00:00:00
11/20/98 07:57:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.89 B
ND
ND
ND
DL
0.0631
0.0397
0.0769
0.0444
0.0421
0.0643
0.0361
0. 0928
0.115
0.232
0.0291
0.0661
0.106
0.130
0.0365
0.160
0.137
0.578
0.390
0.0577
•
• 12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri~hlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
1198H8WW211
9811555-048
81121812
11/17/98 14:45
00:00:00
11/21/98 08:38:00
50
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
24.9
ND
ND
. ND
ND
81. 6
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
2.89
4.24
5.10
2.58
24.4
2.61
4.48
5.65
3.29
3.01
4.46
2.36
2.57
4.93
4.76
4.00
4.64
3.20
5.75
2.07
• R B S U LT S S UM MA R Y '(Cont'd)
1198H8WW222
9811555-lOA
81120819
11/17/98 10:45
00:00:00
11/20/98 09:50:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.832
ND
ND
ND
ND
ND'
ND
ND
ND
ND
DL
0.0578
0.0848
0.102
0.0515
0.489
0.0522
0.0896
0.113
0.0658
0.0602
0.0892
0.0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0.0414
1198H8WW223
9811555-09A
81120818
11/17/98 10:50
00:00:00
11/20/98 09:22:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.10
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0578
0.0848
0.102
0.0515
0.489
0.0522
0.0896
0.113
0.0658
0.0602
0.0892
0.0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0.0414
• Work Order # 9811555
Page £Q_
ll98H8WW229
9811555-06A
81120815
11/17/98 08:25
00:00:00
11/20/98 07:57:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
0.323
ND
ND
ND
3.41
20.3
ND
ND
ND
ND
ND
ND
41.2
ND
ND
DL
0.0578
0.0848
0.102
0.0515
0.489
0.0522
0. 0896
0.113
0.0658
0.0602
0.0892
0.0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0. 0414
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-8romofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
•
1198HBWW211
9811555-04B
B1121812
11/17/98 14:45
00:00:00
11/21/98 08:38:00
50
Water
ug/L
received
Cone.
Recovery
%
97
92
98
DL
R B S 0 L T S S 0 M M A R Y (Cont'd)
1198HBWW222
9811555-lOA
Bll20819
11/17/98 10:45
00:00:00
11/20/98 09:50:00
1
Water
ug/L
received
Cone.
Recovery
%
95
95
93
•
DL
1198HBWW223
9811555-09A
81120818
11/17/98 10:50
00:00:00
11/20/98 09:22:00
1
Water
ug/L
received
Cone.
Recovery
%
94
96
90
DL
Work Order tt 9811555
Page~
1198H8WW229
9811555-0GA
81120815
11/17/98 08:25
00:00:00
11/20/98 07:57:00
1
Water
ug/L
received
Cone.
Recovery
%
94
101
97
DL
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
8romobenzene
8romochloromethane
8romodichloromethane
Bromoform
8romomethane
2-Butanone (MEK)
n-8utylbenzene
sec-8utylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
ll98HBWW229
9811555-06C
Cll23818
11/17/98 08:25
00:00:00
11/24/98 00:22:00
1000
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
809
4570
4140
780
64.7
104
382
93.5
104
178
124
231
113
156
164
132
143
42.0
189
97.7
• R B S U LT S S UM MAR Y (Cont'd)
ll98H8WW229
9811555-06C
Cll23829
11/17 /98 08: 25
00:00:00
11/24/98 14:56:00
500
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
404
2280
2070
390
32.4
52.0
191
46.8
52.0
89.0
62.0
116
56.5
78.0
82.0
66.0
71.5
21. 0
94.5
48.8
ll98H8WW230
9811555-07A
81120816
11/17/98 09:30
00:00:00
11/20/98 08:25:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.413
5. 72
7.17
0.333
0.0375
0.0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0.0719
0.0453
0.0441
• Work Order # 9811555
Page~
ll98H8WW230
9811555-078
Bll21809
11/17/98 09:30
00:00:00
11/21/98 07:11:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0 .413
5. 72
7.17
0.333
0.0375
0.0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0. 0719
0.0453
0.0441
12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
l,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluorometh~ne
1;1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
•
1198H8WW229
9811555-06C
Cll23818
11/17/98 08:25
00:00:00
11/24/98 00:22:00
1000
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
N!J
1770
ND
467
7940
ND
DL
93.3
157
87.6
90.5
297
312
1430
76.2
87.5
205
286
334
328
352
67.5
36.3
98.9
127
46.5
83.5
R B S ULT S S 0 MM AR Y, (Cont'd)
1198H8WW229
9811555-06C
Cll23829
11/17/98 08:25
00:00:00
11/24/98 14:56:00
500
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1750'
ND
467
7770
ND
•
DL
46.6
78.5
43.8
45.2
148
156
715
38.1
43.8
102
143
167
164
176
33.8
18.2
49 .4
63.5
23.2
41.8
1198H8WW230
9811555-07A
81120816
11/17/98 09:30
00:00:00
11/20/98 08:25:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.306 R
2 .67 R
ND
DL
0. 0480
0.0605
0.0521
0.0605
0.0881
0.0538
0.194
0.0769
0.0435
0.118
0.412
0.0733
0.0469
0,0466
0.176
0.0576
0.0348
0.0715
0.0383
0.0618
Work Order # 9811555
Page £1__
1198H8WW230
9811555-078
81121809
11/17 /98 09: 30
00:00:00
11/21/98 07:11:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0. 0480
0.0605
0.0521
0.0605
0.0881
0.0538
0.194
0.0769
0.0435
0.118
0.412
0.0733
0. 0469
0.0466
C.176
0.0576
u. 0348
0. 0715
0.0383
0. 0618
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
1198HBWW229
9811555-06C
Cl123818
11/17 /98 08: 25
00:00:00
11/24/98 00:22:00
1000
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
242 B
ND
ND
ND
DL
146
61. 8
69.9
159
116
40.0
61.2
234
554
737
119
255
136
124
64.6
137
218
234
580
239
• Iii. B S ULT S S UM MA Iii. Y ·(Cont'd)
ll98HBWW229
9811555-06C
Cl123829
11/17/98 08:25
00:00:00
11/24/98 14:56:00
500
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
134 B
ND
ND
ND
DL
73.0
30.9
35.0
79.5
58.0
20.0
30.6
117
277
368
59.5
128
68.0
62.0
32.3
68.5
109
117
290
120
ll98HBWW230
9811555-07A
Bll20816
11/17/98 09:30
00:00:00
11/20/98 08:25:00
l
Water
ug/L
receiyed
Cone. DL
ND 0.0631"
ND 0.0397
ND 0.0769
ND 0.0444
ND 0.0421
ND 0.0643
ND 0.0361
ND 0.0928
ND 0.115
ND 0.232
ND 0.0291
ND 0.0661
ND 0.106
ND 0.130
ND 0.0365
ND 0.160
0.218 B 0.137
ND 0.578
ND 0.390
ND 0.0577
Work Order # 9811555
Page ~
1198HBWW230
9811555-0?B
Bll21809
11/17 /98 09: 30
00:00:00
11/21/98 07:11:00
l
Water
ug/L
received
Cone. DL
•
ND 0.0631
ND 0.0397
ND 0.0769
ND 0.0444
ND 0.0421
ND 0.0643
ND 0.0361
ND 0.0928
ND 0.115
ND 0.232
ND 0.0291
ND 0.0661
ND 0.106
ND 0.130
ND 0.0365
ND 0.160
0.298 B 0.137
ND 0.578
ND 0.390
ND 0.0577
12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
a-Xylene
•
1198HBWW229
9811555-06C
Cll23818
11/17/98 08:25
00:00:00
11/24/98 00:22:00
1000
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
194
158
97.0
340
920
141
350
333
96.5
88.1
219
182
253
113
205
205
74.9
162
500
259
R. B S U LT S S UM MA R. Y (Cont'd)
1198H8WW229
9811555-0GC
Cl123829
11/17/98 08:25
00:00:00
11/24/98 14:56:00
500
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
97.0
79.0
48.5
170
460
70.5
175
166
48.2
44.0
110
91. 0
126
56.5
102
102
37.4
81.0
250
130
1198H8WW230
981155S-07A
81120816
11/17/98 09:30
00:00:00
11/20/98 08:25:00
1
Water
ug/L
received
Cone. DL
ND 0.0578
ND 0.0848
ND 0.102
ND 0.0515
ND 0.489
ND 0.0522
ND 0.0896
ND 0.113
ND 0.0658
ND 0.0602
2.05 0.0892
ND 0.0473
ND 0.0514
ND 0.0986
ND 0.0952
ND 0.0800
ND 0.0929
ND 0.0639
ND 0.115
ND 0.0414
Work Order ff 9811555
Page £2..._
1198H8WW230
9811555-078
81121809
11/17/98 09:30
00:00:00
11/21/98 07:11:00
1
water
ug/L
received
Cone. DL
ND 0.0578
ND 0.0848
ND 0.102
ND 0.0515
ND 0.489
ND 0.0522
ND 0.0896
ND 0.113
ND 0.0658
ND 0.0602
0.160 0.0892
ND 0.0473
ND 0.0514
ND 0.0986
ND 0.0952
ND 0.0800
ND 0.0929
ND 0.0639
ND 0.115
ND 0.0414
•
• 12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
l,4-8romofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
1198HBWW229
9811555-06C
Cll23818
11/17/98 08:25
00:00:00
11/24/98 00:22:00
1000
Water
ug/L
received
Cone.
Recovery
\
96
105
104
DL
• R B S ULT S S UM MAR Y (Cont'd)
1198H8WW229
9811555-06C
C1123829
11/17/98 08:25
00:00:00
11/24/98 14:56:00
500
Water
ug/L
received
Cone. DL
Recovery
\
96
102
104
1198H8WW230
9811555-07A
81120816
11/17/98 09:30
00:00:00
11/20/98 08:25:00
l
Water
ug/L
received
Cone.
Recovery
\
94
94
94
DL
Work Order U 9811555
Page a
1198H8WW230
9811555-078
81121809
11/17/98 09:30
00:00:00
11/21/98 07:11:00
l
Water
ug/L
received
Cone. DL
Recovery
\
94
95
97
•
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
•
1198HBWW231
9811555-08A
Bl120817
11/17/98 08:50
00:00:00
11/20/98 08:53100
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0 .413
5. 72
7.17
0.333
0.0375
0. 0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0. 0719
0.0453
0. 0441
RB S 0 LT S S 0 MM AR. Y (Cont'd)
1196HBWW231
9811555-08B
81121810
11/17/98 08:50
00:00:00
11/21/98 07:39:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
0.413
5. 72
7.17
0.333
0. 0375
0. 0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0. 0719
0.0453
0.0441
l198HBWW231
9811555-08C
Cll23816
11/17/98 08:50
00:00:00
11/23/98 23:27:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0441 BJ
ND
ND
ND
ND
DL
0.809
4.57
4 .14
0.780
0.0647
0.104
0.382
0.0935
0.104
0.178
0.124
0.231
0.113
0.156
0.164
0.132
0.143
0.0420
0.189
0.0977
Work Order # 9811555
Page ~
TRIP BLANK #1
9811555-05A
Bll20614
11/17/96
00:00:00
11/20/98 07:29:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0 .413
5. 72
7.17
0.333
0.0375
0.0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0. 0719
0.0453
0. 0441
•
• 12/01/98 13:42:59
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
l,2-Dichlorobenzene
l,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodif luoromethane
1,1-Dichloroethane
l,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1198H8WW23l
9811555-08A
81120817
11/17/98 08:50
00:00:00
11/20/98 08:53:00
1
Water
ug/L
received
Cone. DL
ND 0.0480
ND 0.0605
ND 0.0521
ND 0.0605
ND 0.0881
ND 0.0538
ND 0.194
ND 0.0769
ND 0.0435
ND 0.118
ND 0.412
ND 0.0733
ND 0. 0469
ND 0.0466
ND 0.176
2.24 0.0576
ND 0.0348
0.357 z 0.0715
0.736 R 0.0383
ND 0.0618
• RB S ULT S S UM MAR Y (Cont'd}
1198H8WW231
9811555-088
81121810
11/17/98 08:50
00:00:00
11/21/98 07:39:00
1
Water
ug/L
received
Cone. DL
ND 0.0480
ND 0.0605
ND 0.0521
ND 0.0605
ND 0.0881
.ND 0. 0538
ND 0.194
ND 0.0769
ND 0.0435
ND 0.118
ND 0.412
ND 0.0733
ND 0.0469
ND O. 0466
ND 0.176
3.9~ 0.0576
ND 0.0348
0.795 0.0715
ND 0.0383
ND 0.0618
ll98H8WW231
9811555-08C
C1123816
11/17 /98 08: 50
00:00:00
11/23/98 23:27:00
1
Water
ug/L
received
Cone. DL
ND 0.0933
ND 0.157
ND 0.0876
ND 0.0905
ND 0.297
ND 0.312
ND 1. 43
ND 0.0762
ND 0.0875
ND 0.205
ND 0.286
ND 0.334
ND 0.328
ND 0.352
ND 0.0675
5.17 0.0363
ND 0.0989
1.08 0.127
ND 0.0465
ND 0.0835
Work Order tt 9811555
Page £!!._
TRIP BLANK #1
9811555-05A
81120814
11/17/98
00:00:00
11/20/98 07:29:00
1
Water
ug/L
received
Cone. DL
•
ND 0.0480
ND 0.0605
ND 0.0521
ND 0.0605
ND 0.0881
ND 0.0538
ND 0.194
ND 0.0769
ND 0.0435
ND 0.118
ND 0.412
ND 0.0733
ND 0.0469
ND 0.0466
ND 0.176
ND 0.0576
ND 0.0348
ND 0.0715
0.895 z 0.0383
ND 0.0618
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
l,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene ch;oride
Naphthalene
Propanenitrile
n-Propylbenzene
•
1198HBWW231
98ll555-08A
81120817
11/17/98 08:50
00:00:00
11/20/98 08:53:00
1
Water
ug/L
received
Cone. DL
ND 0.0631
ND 0.0397
ND 0.0769
ND 0.0444
ND 0. 0421
ND 0.0643
ND 0.0361
ND 0. 0928
ND 0.115
ND 0.232
ND 0.0291
ND 0.0661
ND 0.106
ND 0.130
ND 0.0365
ND 0.160
0.263 B 0.137
ND 0.578
ND 0.390
ND 0.0577
R B S 0 L T S S UM MAR Y (Cont'd)
1198HBWW231 1198HBWW23l
9811555-088 98ll555-08C
81121810 Cll23816
11/17/98 08:50 11/17/98 08:50
00:00:00 00:00:00
11/21/98 07:39:00 11/23/98 23:27:00
1 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.0631 ND 0.146
ND 0.0397 ND 0.0618
ND 0.0769 ND 0.0699
ND 0.0444 ND 0.159
ND 0.0421 ND 0.116
ND 0.0643 ND 0.0400
ND 0.0361 ND 0.0612
ND 0. 0928 ND 0.234
ND 0.115 ND 0.554
ND 0.232 ND 0.737
ND 0.0291 ND 0.119
ND 0.0661 ND 0.255
ND 0.106 ND 0.136
ND 0.130 ND 0.124
ND 0.0365 ND 0.0646
ND 0.160 ND 0.137
0. 271 B 0.137 0.328 B 0.218
ND 0.578 ND 0.234
ND 0.390 ND 0.580
ND 0.0577 ND 0.239
•
Work Order # 9811555
Page .£2._
TRIP BLANK #1
9811555-05A
81120814
11/17 /98
00 :_00: 00
11/20/98 07:29:00
1
Water
ug/L
received
Cone. DL
ND 0.0631
ND 0.0397
ND 0.0769
ND 0.0444
ND 0. 0421
ND 0. 0643
ND 0.0361
ND 0. 0928
ND 0.115
ND 0.232
ND 0.0291
ND 0.0661
ND 0.106
ND 0.130
ND 0.0365
ND 0.160
0.538 B 0.137
ND 0.578
ND 0.390
ND 0.0577
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
. 1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
1198HBWW231
9811555-08A
81120817
11/17 /98 08: 50
00:00:00
11/20/98 08:53:00
1
Water
ug/L
received
Cone. DL
ND 0.0578
ND 0.0848
ND 0.102
0.192 0.0515
ND 0.489
ND 0.0522
ND 0.0896
ND 0.113
ND 0.0658
ND 0.0602
1.50 0.0892
l~J) 0.0473
ND 0.0514
ND 0.0986
ND 0.0952
ND 0.0800
ND 0.0929
ND 0.0639
ND 0.115
ND 0.0414
• R E S ULT S S UM MA R Y (Cont'd)
1198HBWW231
9811555-088
81121810
11/17/98 08:50
00:00:00
11/21/98 07:39:00
1
Water
ug/L
received
Cone. DL
ND 0.0578
ND 0.0848
ND 0.102
0.177 0.0515
ND 0.489
ND 0.0522
ND 0.0896
ND 0.113
ND 0.0658
ND 0.0602
0.0766 J 0.0892
ND 0.0473
ND 0.0514
ND 0.0986
ND 0.0952
ND 0.0800
ND 0.0929
ND 0.0639
ND 0.115
ND 0.0414
1198HBWW231
9811555-08C
Cll23816
11/17/98 08:50
00:00:00
11/23/98 23:27:00
l
Water
ug/L
received
Cone.
ND
ND
ND
0.231" J
ND
ND
ND
ND
0.0437 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.194
0.158
0.0970
0.340
0.920
0.141
0.350
0.333
0.0965
0.0881
0.219
0.182
0.253
0.113
0 .205
0.205
0.0749
0.162
0.500
0.259
• Work Order # 9811555
Page lQ_
TRIP BLANK #1
9811555-05A
81120814
11/17/98
00:00:00
11/20/98 07:29:00
]_
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
6. 03 z
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0578
0.0848
0.102
0.0515
0.489
0.0522
0.0896
0.113
0.0658
0.0602
0. 0892
0. 0473
0.0514
C.0936
0.0952
0.0800
0.0929
0.0639
0.115
0. 0414
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
•
1198HBWW231
9811555-08A
81120817
11/17/98 08:50
00:00:00
ll/20/98 08:53:00
l
Water
ug/L
received
Cone.
Recovery
'
93
94
77 Q
DL
R B S ULT S S UM MAR Y (Cont'd)
1198HBWW23l
9811555-088
81121810
ll/17/98 08:50
00:00:00
ll/21/98 07:39:00
l
Water
ug/L
received
Cone.
Recovery
'
92
95
74 Q
•
DL
ll98HBWW231
9811555-0SC
Cll23816
11/17/98 08:50
00:00:00
11/23/98 23:27:00
1
Water
ug/L
received
Cone.
Recovery
't
95
105
80 Q
DL
Work Order # 9811555
Page .1L
TRIP BLANK #1
9811555-05A
Bll20814
ll/l 7 /98
00:00:00
11/20/98 07:29:00
l
Water
ug/L
received
Cone.
Recovery
%
96
94
96
DL
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SwACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l,3-butadiene
Chlorobenzene
Chloroethane
TRIP BLANK #l
98ll555-05A
Bll2l808
ll/17/98
00:00:00
ll/21/98 06:43:00
l
Water
ug/L
received
Cone. DL
ND R 0.413
ND R 5.72
ND R 7.17
ND R 0.333
ND R 0.0375
ND R 0.0928
ND R 0.0624
ND R 0.0828
ND R 0.0634
ND R 0.0547
ND R 0.0467
ND R 0.222
ND R 0.116
ND R 0.0782
ND R 0.0823
ND R 0.0547
ND R 0.0576
ND R 0. 0719
ND R o. 0453
ND R 0.0441
• R B S 0 L T S S 0 MM AR Y (Cont'd)
TRIP BLANK #2
98ll555-12A
Bll2082l
ll/l 7 /98
00:00:00
ll/20/98 10:46:00
l
Water
ug/L
received
Cone. DL
ND 0.413
ND 5. 72
ND 7.17
ND 0.333
ND 0.0375
ND 0.0928
ND 0.0624
ND 0.0828
ND 0.0634
ND o. 0547
ND 0.0467
ND 0.222
ND 0.116
ND 0.0782
ND 0.0823
ND 0.0547
ND 0.0576
ND 0.0719
ND 0.0453
ND 0.0441
Cone. DL
Work Order # 9811555
Page E_
Cone. DL
•
--
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
l,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-l,4-Dichloro-2-butene
1;2-Dichlorobenzene
l,3-Dichlorobenzene
l,4-Dichlorobenzene
Dichlorodif luoromethane
l,l-Dichloroethane
1,2-Dichloroethane
l,l-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
•
TRIP BLANK #l
9811555-05A
Bll21808
ll/17/98
00:00:00
11/21/98 06:43:00
1
Water
ug/L
received
Cone. DL
ND R 0.0480
ND R 0.0605
ND R 0.0521
ND R 0.0605
ND R 0.0881
ND R 0.0538
ND R 0.194
ND R 0.0769
ND R 0.0435
·ND R 0.118
ND R 0.412
ND R 0.0733
ND R 0.0469
ND R 0.0466
ND R 0.176
ND R 0.0576
ND R 0.0348
ND R 0.0715
ND y 0.0383
ND R 0.0618
R B S ULT S S UM MAR Y (Cont'd)
TRIP BLANK #2
9811555-l2A
Bll2082l
11/17/98
00:00:00
11/20/98 10:46:00
1
Water
ug/L
received
Cone. DL
ND 0.0480
ND 0.0605
ND 0.0521
ND 0.0605
ND 0.0881
ND 0.0538
ND 0.194
ND 0.0769
ND 0.0435
ND 0.118
ND 0.412
ND 0.0733
ND 0.0469
ND 0.0466
ND 0.176
ND 0.0576
ND 0.0348
ND 0 .0715
0.0881 z 0.0383
ND 0.0618
•
Cone. DL
Work Order # 9811555
Page ;u_
Cone. DL
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
TRIP BLANK #1
9811555-05A
Bll21808
11/17/98
00:00:00
11/21/98 06:43:00
1
Water
ug/L
received
Cone. DL
ND R 0.0631
ND R 0.0397
ND R 0.0769
ND R 0.0444
ND R 0.0421
ND R 0.0643
ND R 0.0361
ND R 0. 0928
ND R 0.115
ND R 0.232
ND R 0.0291
ND R 0.0661
ND R 0.106
ND R 0.130
ND R 0.0365
ND R 0.160
0.472 R 0.137
ND R 0.578
ND R 0.390
ND R 0.0577
• RBS ULT S SUMMARY (Cont'd)
TRIP BLANK #2
9811555-12A
Bll20821
11/17/98
00:00:00
11/20/98 10:46:00
1
Water
ug/L
received
Cone. DL
ND 0.0631
ND 0.0397
ND 0.0769
ND 0.0444
ND 0.0421
ND 0.0643
ND 0.0361
ND 0.0928
ND 0.115
ND 0.232
ND 0.0291
ND 0.0661
ND 0.106
ND 0.130
ND 0.0365
ND 0.160
0. 502 B 0.137
ND 0.578
ND 0.390
ND 0. 0577
Cone. DL
Work Order # ~~
Page .11._
Cone.
•
DL
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
o-Xylene
•
TRIP BLANK #1
9811555-05A
Bll21808
11/17/98
00:00:00
11/21/98 06:43:00
1
Water
ug/L
received
Cone. DL
ND R 0.0578
ND R 0.0848
ND R 0.102
ND R 0.0515
ND R 0.489
ND R 0.0522
ND R 0.0896
ND R 0.113
ND R 0.0658
ND R 0.0602
0.164 y 0.0892
ND R 0. 0473
ND R 0.0514
ND R 0.0986
ND R 0.0952
ND R 0.0800
ND R 0.0929
ND R 0.0639
ND R 0.115
ND R 0.0414
R B S ULT S S U MM ARY (Cont'd)
TRIP BLANK #2
9811555-12A
Bl120821
11/17 /98
00:00:00
11/20/98 10:46:00
1
Water
ug/L
received
Cone. DL
ND 0.0578
ND 0.0848
ND 0.102
ND 0.0515
ND 0.489
ND 0.0522
ND 0.0896
ND 0.113
ND 0.0658
ND 0.0602
0.568 0.0892
ND 0.0473
ND 0.0514
ND 0.0986
ND 0.0952
ND 0.0800
ND 0. 0929
ND 0.0639
ND 0.115
ND o. 0414
•
Cone. DL
Work Order II 9811555
Page }2__
Cone. DL
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
TRIP BLANK #1
9811555-05A
Bll21808
11/17 /98
00:00:00
11/21/98 06:43:00
l
Water
ug/L
received
Cone. DL
Recovery
\
95 y
93 y
98 y
• R B S 0 L T S S 0 MM AR Y (Cont'd)
TRIP BLANK #2
9811555-12A
Bll2082l
11/17 /98
00:00:00
11/20/98 10:46:00
l
Water
ug/L
received
Cone. DL
Recovery
\
94
94
96
Cone. DL
Recovery
't
Work Order # 9811555
Page 22__
Cone. DL
Recovery
't
•
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration tt MSDB981003000000
Calibration Date ~l~0~/~0~3~/~9~8~~~~
Sequence/Analysis Time
l 11/20/98 01:24:00
2 11/20/98 01:52:00
3 11/20/98 01:52:00
4 11/20/98 02:20:00
5 11/20/98 02:48:00
6 11/20/98 03:16:00
7 11/20/98 03:44:00
8 11/20/98 04:12:00
9 11/20/98 04:40:00
10 11/20/98 05:08:00
11 11/20/98 05:37:00
12 11/20/98 06:05:00
13 11/20/98 06:33:00
14 11/20/98 07:01:00
15 11/20/98 07:29:00
16 11/20/98 07:57:00
17 11/20/98 08:25:00
18 11/20/98 08:53:00
19 11/20/98 09:22:00
20 11/20/98 09:50:00
21 11/20/98 10:18:00
22 11/20/98 10:46:00
23 11/20/98 11:14:00
24 11/20/98 11:42:00
25 11/20/98 12:10:00
26 11/20/98 12:39:00
27 11/20/98 13:07:00
28 11/20/98 13:46:00
•
A Ill A L Y S I S B A T C H S U M M A R Y
Analysis Batch tt MSMSDB8ll2001520l
Analysis Start Date/Time 11/20/98 01:52:00
Analysis Stop Date/Time 11/20/98 13:46:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
VSTDCAL Continuing Calibration
LCS986013 Lab Control Sample
Work Order tt 9811555
Page }1_
Instrument ~
Analyst ~
Reviewer A==-PS:::.-~~~~~~~-
Analysis File tt
Bll2080l
Bll20802
Verification Bll20802
Bll20803
LCSD986014 Lab Control Sample Duplicate B1120804
BLK983941 Blank, Method Bll20805
9811344-08B Sample B1120806
9811344-llB Sample 81120807
1198HBWW208 9811555-0lA Sample 81120808
1198HBWW208 9811555-13A Matrix Spike 81120809
1198HBWW208 9811555-14A Matrix Spike Duplicate 81120810
1198HBWW209 9811555-02A Sample 81120811
1198HBWW210 9811555-03A Sample 81120812
1198HBWW211 9Sll555-04A Sample Bll20813
TRIP BLANK ttl 9811555-05A Sample 81120814
1198HBWW229 9811555-06A Sample 81120815
1198HBWW230 9811555-07A Sample 81120816
1198HBWW231 9811555-08A Sample Bl120817
1198HBWW223 9811555-09A Sample 81120818
1198HBWW222 9811555-lOA Sample Bll20819
1198HBWE01 9811555-llA Sample 81120820
TRIP BLANK tt2 9811555-12A Sample 81120821
9811414-03A Sample Bl120822
9811414-04A Sample Bl120823
9811414-05A Sample B1120824
9811414-06A Sample B1120825
9811414-07A .sample Bll20826
9811344-138 Sample Bll20827
•• •
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDB981003000000
Calibration Date =l~0~/~03""-/9~8"'-~~~~
Sequence/Analysis Time
1 11/21/98 03:26:00
2 11/21/98 03:54:00
3 11/21/98 03:54:00
4 11/21/98 04:22:00
5 11/21/98 04:50:00
6 11/21/98 05:18:00
7 11/21/98 05:46:00
8 11/21/98 06:14:00
9 11/21/98 06:43:00
10 11/21/98 07:11:00
11 11/21/98 07:39:00
12 11/21/98 08:08:00
13 11/21/98 08:38:00
14 11/21/98 09:07:00
15 11/21/98 09:37:00
16 11/21/98 10:06:00
17 11/21/98 10:34:00
18 11/21/98 11:03:00
19 11/21/98 11:31:00
20 11/21/98 11:59:00
21 11/21/98 12:27:00
22 11/21/98 12:55:00
23 11/21/98 13:24:00
24 11/21/98 13:52:00
25 11/21/98 14:21:00
26 11/21/98 14:49:00
27 11/21/98 15:18:00
28 11/21/98 15:46:00
• AHALYSIS BATCH SUMMARY
Analysis Batch # MSMSDB81121035401
Analysis Start Date/Time 11/21/98 03:54:00
Analysis Stop Date/Time 11/21/98 15:46:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
Work Order # 9811555
Page }§._
Instrument !:!fil2§_
Analyst !lli£
Reviewer '-'A~PS,,_ ______ _
Analysis File #
Bl121801
Bll21802
VS TD CAL Continuing Calibration Verification 81121802
LCS986017 Lab Control Sample 81121803
LCSD986018 Lab Control Sample Duplicate Bll21804
BLK983943 Blank, Method Bll21805
9811583-0lA Sample Bll21806
9811583-02A Sample Bll21807
TRIP BLANK #1 9811555-05A Sample Bll21808
1198HBWW230 9811555-078 Sample Bll21809
1198HBWW231 9811555-08B Sample Bll21810
1198HBWW209 9811555-02B Sample Bll21811
1198HBWW211 9811555-04B Sample Bll21812
1198HBWW210 9811555-03B Sample 81121813
1198HBWW229 9811555-06B Sample Bll21814
9811414-06B Sample Bll21815
9811619-0lA Sample Bll21816
9811619-02A Matrix Spike Bll21817
9811619-03A Matrix Spike Duplicate Bll21818
9811619-04A Sample 81121819
9811619-05A Matrix Spike 81121820
9811619-06A Matrix Spike Duplicate B1121821
9811619-07A Sample 81121822
9811619-08A Sample Bll21823
9811619-09A Sample B1121824
9811619-lOA Sample 81121825
9811619-llA Sample 81121826
9811619-12A Sample Bll21827
•
12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDC980921000000
Calibration Date _0_9_/2_1~/~9~8~~~~-
Sequence/Analysis Time
1 11/23/98 16:36:00
2 11/23/98 17: 04: 00
3 11/23/98 17:04:00
4 11/23/98 17:31:00
5 11/23/98 17:59:00
6 11/23/98 18:26:00
7 11/23/98 18:53:00
8 11/23/98 19:21:00
9 11/23/98 19:48:00
10 11/23/98 20:15:00
11 11/23/98 20:43:00
12 11/23/98 21:10:00
13 11/23/98 21:38:00
14 11/23/98 22:05:00
15 11/23/98 22:33:00
16 11/23/98 23:00:00
17 11/23/98 23:27:00
18 11/23/98 23:55:00
19 11/24/98 00:22:00
20 11/24/98 00:49:00
21 11/24/98 01:17:00
22 11/24/98 01:44:00
23 11/24/98 02:12:00
24 11/24/98 02:39:00
25 11/24/98 03:08:00
26 11/24/98 03:37:00
27 11/24/98 04:04:00
28 11/24/98 14:02:00
29 11/24/98 14:29:00
30 11/24/98 14:29:00
•
A!IAL'.rSIS t:JATCH SUMMARY
Analysis Batch# MSMSDC8ll2317040l
Analysis Start Date/Time ll/23/98 17:04:00
Analysis Stop Date/Time 11/24/98 15:24:00
Work Order # 9811555
Page 12....
Instrument ~
Analyst !:lliE
Reviewer ~A~P~S~~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysi.s File #
SB Blank, System Cll2380l
BFB GC/MS tune files Cll23802
VS TD CAL Continuing Calibration Verification Cll23802
LCS985987 Lab Control Sample Cll23803
LCSD985988 Lab Control Sample Duplicate Cll23804
8LK983928 Blank, Method Cll23805
9811342-0lA Sample Cll23806
9811342-02A Sample Cll23807
9811342-03A Matrix Spike Cll23808
9811342-04A Matrix Spike Duplicate Cll23809
9811342-05A Sample Cl123810
9811342-06A Sample Cll23811
9811342-07A Sample Cll23812
9811342-08A Sample Cll23813
9811342-09A Sample Cll23814
9811342-lOA Sample Cl123815
1198HBWW231 9811555-08C Sample Cl123816
1198HBWW210 9811555-03C Sample Cll23817
ll98HBWW229 9811555-06C Sample Cll23818
9811423-028 Sample Cl123819
9811619-078 Sample Cll23820
9811619-08B Sample Cll2382l
9811619-118 Sample Cll23822
:
9811619-128 Sample Cll23823
9811619-048 Sample Cll23824
9811619-098 Sample Cll23825
9811619-108 Sample Cll23826
SB Blank, System Cll23827
8FB GC/MS tune files Cll23828
VS TD CAL Continuing Calibration Verification Cll23828
• •
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDC980921000000
Calibration Date ~0~94/~2~1./~9~8~~~~-
Sequence/Analysis Time
31 11/24/98 14:56:00
32 11/24/98 15:24:00
• ABALYSIS BATCH SUMMARY (cont'd)
Analysis Batch # MSMSDC81123170401
Analysis Start Date/Time 11/23/98 17:04:00
Analysis Stop Date/Time 11/24/98 15:24:00
Project Sample ID Lab Sample ID Sample Type
1198HBWW229 9811555-06C Sample
9811619-lOC Sample
Work Order # 9811555
Page .iQ_
Instrument 1:1fil2£.._
Analyst ~
Reviewer ~A~P~S~~~~~~~~-
Analysis File #
C1123829
Cll23830
•
12/01/98 13:42:59
Method Volatile Organics SW8260B
Lab Sample ID
File ID
9811555-03A
81120812
9811555-04A
Bll20813
9811555-05A
81120814
9811555-07A
B1120816
9811555-08A
. 81120817
9811555-08A
81120817
9811555-09A
81120818
•
Project Sample
ID/Description
1198HBWW210
ll98HBWW211
TRIP BLANK #1
1198H8WW230
1198HBWW231
ll98HBWW23l
ll98H8WW223
Specification# ~~~~
Analyte
l,1-Dichloroethane
Several
Trichloroethene & C12DCE
ANALYTICAL PROTOCOL SUMMARY
COMMBHTS/NARRATIVB
Flag Comment/Narrative
z
z
z
The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these results but only
at a higher dilution since other targets were
outside of the calibration range.
The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these results but only
at a higher dilution since other targets were
outside of the calibration range.
The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these results but the
only vial available had headspace.
l,l-Dichloroethene & Cl2DCE R The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these results.
cis-1,2-Dichloroethene R
1,1-Dichloroethene z
cis-1,2-Dichloroethene z
The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these resu~ts.
The results indicated the possible presence
of instrument carryover. The sample was
reanalyzed and the reanalysis confirmed the
original results. No measurable carryover
was present.
The results indicate the possible presence
of instrument carryover. The sample was
not reanalyzed because the concentration
detected was below the PRDL .
•
Corrective Action
Work Order # 9811555
Page iL
•
• 12/01/98 13:42:59
Method Volatile Organics SW8260B
Lab Sample ID
File ID
9811555-lOA
B1120819
9811555-llA
B1120820
9811555-12A
B1120821
9811555-05A
B1121808
Project Sample
ID/Description
1198HBWW222
1198HBWE01
TRIP BLANK 112
TRIP BLANK Ill
Specif icationll ~~~~
Analyte
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
All analytes
• ANALYTICAL PROTOCOL SUMMARY
C 0 MM B R T S / RA R RAT I V B (Cont'd)
Flag Comment/Narrative
z
z
z
y
The results indicate the possible presence
of instrument carryover. The sample was
not reanalyzed because the concentration
detected was below the PRDL.
The results indicate the possible presence
of instrument carryover. The sample was
not reanalyzed because the concentration
detected was below the PRDL.
The results indicate the possible presence
of instrument carryover. The sample was
not reanalyzed because the concentration
detected was below the PRDL.
This sample was analyzed out of a vial with
headspace (due to a limited amount of
sample). The sample was previously analyzed
after a sample with high target analytes and
carryover was suspected. This analysis
should be used only for those analytes.
Corrective Action
Work0 0rde~811555
Page ~
12/01/98 13:42:59
•
QUALITY COBTlilOL BXCBPTIOB RBPORT
SUMMARY
QCER # Analysis Batch Number
981121-01 MSMSDB981121035400
981123-15 MSMSDC81123170401
.
•
Work Order # 9811555
Page il_
•
12/01/98 15:28:21
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared __ R~a~d~i~a_n_I~n~t_e_r_n~a~t~i_o_n_aMl_,~L_L~C~
By --=l_.4..::0..:4..::6-=S.,u"'m"'m:.:i:.:t'"-<:D:.:r...o·-1.•....::B:.:l:.:d:.:9'-'.--=B:...
P. O. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW212
1198HBWW213
1198HBWW214
1198HBWW215
•
ID/
NOR~ ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID WASHINGTON, NC
Case # ~NA=---------­
SDG # N~A~~~~~~~~­
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA 352SWAOO
----sITSWB\;M
CKlSWAOO
02A MS 352SWAOO
827SWBMS
CKlSWAOO
03A MSD 352SWAOO
827SWBMS
CKlSWAOO
04A 352SWAOO
827SWBCM
CKlSWAOO
05A MS 352SWAOO
827SWBMS
CKlSWAOO
06A MSD 352SWAOO
827SWBMS
CKlSWAOO
07A 352SWAOO
827SWBCM
CKlSWAOO
OBA 352SWAOO
827SWBCM
•
Work Order # 9811566
Page _1_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Liquid/Liq Extract SW846
.,-emivo-ra:ttl~GC-/MS
. Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
•
• 12/01/98 15:28:21
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared ---"R"'a"'d"'i"'a"'n'-"I"'n"'t"'e"'r.!'n,,,a,,,t"'i"'o'°'n"'a"'l:.L,-=L<=L,.,c~
By --=1..:4..::0..:4..::6--=S..::u:;:.m:;:.m,,,i..::t'-"D..::r..:·..1.•-::Bc:l..::d:.;ig"'.--=B~
P. O. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW215
1198HBWW231
1198HBWW227
1198HBWW228
1198HBWE02
ID/
• W 0 R I: 0 RD B R S UM MAR Y (Cont'd)
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID WASHINGTON, NC
Case # ~N~A=----------
SDG # ~NA.._ _______ _
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OSA CKlSWAOO
09A 352SWAOO
827SWBCM
CKlSWAOO
lOA 352SWAOO
827SWBCM
CKlSWAOO
llA 352SWAOO
827SWBCM
CKlSWAOO
12A 352SWAOO
827SWBCM
CKlSWAOO
Work Order # 9811566
Page _2_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
Liquid/Liq Extract SW846
Semivolatiles by GC/MS
Primary KD cone. SW846
•
12/01/98 15:28:21
•
'ii 0 R :I: 0 R. D B R. C 0 M M B H T S
LCS/LCSD986322 and BLK984128 are analytical batch QC for MSMSD281120143601.
These QC samples were not prepared with 9811566 .
•
Work Order # 9811566
Page _3 _
•
• 12/01/98 15:28:21
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB CBRTIPICATIOBS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9811566
Page L._
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
12/01/98 15:28:21 A H A L Y T I C A L P JI. 0 T 0 C 0 L S U M M A JI. Y
FLAG DBFIHITIOHS
Flag Definition
< DL
NA
NC
ND
NR
NS
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A
B
c
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F
G
Interference or coeiution suspected. See Narrative for explanation-. __
Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
s Analyte concentration obtained using Method of Standard Additions (MSA).
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation .
• •
Work Order # 9811566
Page 2._
•
• 12/01/98 15:28:21
Client HAMILTON BEACH
Facility WASHINGTON,NC
Client Code HAM BEACH NC
Method Semivolatiles by SW8270C
Project Sample ID/Description
1198HBWE02
1198HBWW212
1198HBWW213
1198HBWW214
1198HBWW215
1198HBWW227
1198HBWW228
1198HBWW228
1198HBWW231
Lab
9811566-12A
9811566-0lA
9811566-04A
9811566-0?A
9811566-08A
9811566-lOA
9811566-llA
9811566-llA
9811566-09A
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Sample ID Test Code{s) Batch II
827SWBCM 3520981120112500
827SWBCM 3520981120112500
827SWBCM 3520981120112500
827SWBCM 3520981120112500
827SWBCM 3520981120112500
827SWBCM 3520981120112500
827SWBCM 3520981120112500
827SWBcM 3520981120112500
827SWBCM 3520981120112500
Work Order # 9811566
Page _6 _
Analysis Batch #
MSMSD181124083501
MSMSD181124083501
MSMSD181124083501
MSMSD181124083501
MSMSD181124083501
MSMSD181124083501
MSMSD181124083501
MSMSD181125082401
MSMSD181124083501
•
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Aniline
Anthracene
Benz(a)anthracene
Benz(a)pyrene
Benzidine
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
Carbazole
4-Chloro-3-methylphenol
p-Chloroaniline
•
1198HBWE02
9811566-12A
X8339
11/18/98
11/20/98 11:25:00
11/25/98 00:41
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.386
0.356
0.833
0 .410
7.36
1.65
0.408
0.296
0.269
9.81
0.336
0.151
0.335
32.5
o. 779
0 .217
0.206
0.239
0. 710
1.14
RESULTS SUMMARY
1198HBWW212
9811566-0lA
X8328
11/18/98
11/20/98 11:25:00
11/24/98 17:23
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
0.386
0 .35"6
0.833
0.410
7.36
1.65
0.408
0.296
0.269
9.81
0.336
0.151
0.335
32.5
0. 779
0.217
0.206
0.239
0. 710
1.14
1198HBWW213
9811566-04A
X8331
11/18/98
11/20/98 11:25:00
11/24/98 19:22
1
Water
ug/L
received
Cone. DL
Work Order tt 9811566
Pagel_
ll98HBWW214
9811566-07A
X8334
11/18/98
11/20/98 11:25:00
11/24/98 21: 22
l
Water
ug/L
received
Cone. DL
ND 0.386 ND 0.386
ND 0.356 ND -0.3%·
ND 0.833 ND 0.833
ND 0.410 ND 0.410
ND 7.36 ND 7.36
-~-m:i~~~~~~1-:-6-5>~-1~~~~-NB~~~~~~1-:-65·~-1~~~~~~-
ND 0.408 ND 0 .. 408
0.313 0.296 ND 0.296
ND 0.269 ND 0.269
ND 9.81 ND 9.81
ND 0.336 ND 0.336
ND 0.151 ND 0.151
ND 0.335 ND 0.335
ND 3'2.5 ND 32.5
ND 0.779 ND 0.779
ND 0.217 ND 0.217
ND 0.206 ND 0.206
ND 0.239 ND 0.239
ND 0.710 ND 0.710
ND 1.14 ND 1.14
•
\
• 12/01/98 15:28:21
Method Semivolatiles by SWB270C
Test Code 827SW8CM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Diallate
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
Diethylphthalate
1198HBWE02
9811566-12A
X8339
11/18/98
11/20/98 11:25:00
11/25/98 00:41
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.264
0 .303
0.156
0.192
0.557
0.337
0.366
0.380
0.199
0.228
0.251
0.171
0.350
0.627
0 .495
0.513
0.972
0.571
0.527
0.277
• RBS ULT S SUMMARY (Cont'd)
1198HBWW212
9811566-0lA
X8328
11/18/98
11/20/98 11:25:00
11/24/98 17:23
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND'
ND
ND
ND
ND
DL
0.264
0.303
0.156
0.192
0.557
0.337
0.366
0.380
0.199
0.228
0.251
0.171
0.350
0.627
0.495
0.513
0.972
0.571
0.527
0.277
1198H8WW213
9811566-04A
X8331
11/18/98
11/20/98 11:25:00
11/24/98 19:22
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.264
0.303
0.156
0.192
0.557
0.337
0.366
0.380
0.199
0.228
0.251
0.171
0.350
0.627
0.495
0.513
0.972
0.571
0.527
0.277
work Order # 9811566
Page _a_
1198H8WW214
•
9811566-07A
X8334
11/18/98
11/20/98 11:25:00
11/24/98 21:22
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.264
0.303
0.156
0.192
0.557
0.337
0.366
0.380.
0.199
0.228
0.251
0.171
0.350
0.627
0.495
0.513
0.972
0 .571
0.527
0.277
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
p-Dimethylaminoazobenzene
7 ,-12--Dimethylbenz fa) anthracene - -
3,3°-Dimethylbenzidine
Dimethylphenethylamine
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
1,3-Dinitrobenzene
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine/N-NitrosoDPA
Ethyl methanesulfonate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
•
1198HBWE02
9811566-12A
X8339
11/18/98
11/20/98 11:25:00
11/25/98 00:41
1
Water
ug/L
received
Cone. DL
ND 0.644
NI> i.51
ND 1. 93
ND 27.9
ND 0.465
ND 0.247
ND 0.991
ND 0.649
ND 6.79
ND 0.365
ND 0.991
ND 0.607
ND 0.218
ND 4.20
ND 0.205
ND 0.350
ND 0.379
ND 0.589
ND 7.69
ND 0.758
RESULTS S UM MAR Y (Cont'd)
1198HBWW212 1198HBWW213
9811566-0lA 9811566-04A
X8328 X8331
11/18/98 11/18/98
11/20/98 11:25:00 11/20/98 11:25:00
11/24/98 17:23 11/24/98 19:22
1 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.644 ND 0.644
ND 1.51 ---ND----LS"l
ND 1. 93 ND 1.93
ND 27.9 ND 27.9
ND 0.465 ND 0.465
ND 0.247 ND 0.247
ND 0.991 ND 0.991
ND 0.649 ND 0. 649
ND 6.79 ND 6.79
ND 0.365 ND 0.365
ND 0.991 ND 0.991
ND 0.607 ND 0.607
ND 0.218 ND 0.218
ND 4.20 2.63 J 4.20
ND 0.205 0.817 0.205
ND 0.350 ND 0.350
ND 0.379 ND 0.379
ND 0.589 ND 0.589
ND 7.69 ND 7.69
ND 0.758 ND 0.758
•
Work Order # 9811566
Page L
1198HBWW214
9811566-07A
X8334
11/18/98
11/20/98 11:25:00
11/24/98 21:22
1
Water
ug/L
received
Cone. DL
ND 0.644
ND -i. 51
ND 1. 93
ND 27.9
ND 0.465
ND 0.247
ND 0.991
ND 0.649
ND 6.79
ND 0.365
ND 0.991
ND 0.607
ND 0.218
1.24 J 4.20
ND 0.205
ND 0.350
ND 0.379
ND 0.589
ND 7. 69
ND 0.758
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Hexachloropropene
Indeno(l,2,3-cd)pyrene
Isophorone
Isosafrole
Ke pone
Methapyrilene
Methyl me_thanesulfonate
3-Methylcholanthrene
2-Methylnaphthalene
4-Methylphenol/3-Methylphenol
2-Methylphenol
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiethylamine
N-Nitrosod~methylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
Naphthalene
1198HBWE02
9811566-12A
X8339
11/18/98
11/20/98 11:25:00
11/25/98 00:41
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.791
0.0822
0.275
0. 721
2.37
6.46
0.739
6.49
0.279
0.581
0.446
0.878
0.733
1.43
0.563
1. 83
0. 641
0.299
0.737
0.424
• R B S UL T S S UM MAR Y (Cont'd)
1198HBWW212
9811566-0lA
X8328
11/18/98
11/20/98 11:25:00
11/24/98 17:23
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.791
0.0822
0.275
0. 721
2.37
6 .46
0.739
6.49
0.279
0.581
0.446
0.878
0.733
1.43
0.563
1. 83
0.641
0.299
0.737
0.424
1198HBWW213
9811566-04A
X8331
11/18/98
11/20/98 11:25:00
11/24/98 19:22
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
9.19
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
16.4
DL
0.791
0.0822
0.275
0. 721
2.37
6 .46
0.739
6 .49
0.279
0.581
0.446
0.878
o. 733
1.43
0.563
1.83
0.641
0.299
0.737
0.424
• Work Order # 9811566
Page 1.Q_
1198HBWW214
9811566-07A
X8334
11/18/98
11/20/98 11:25:00
11/24/98 21:22
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.791
0.0822
0.275
0. 721
2.37
6.46
0.739
6 .49.
0.279
0.581
0 .446
0.878
0. 733
1.43
0.563
1. 83
0. 641
0.299
0.737
0.424
12/01/98 15:28:21
Method Sernivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,4-Napht~oquinone
1-Naphthylarnine
2-Naphthylarnine
5-Nitro-o-toluidine
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-1-oxide
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
2-Picoline
Pronarnide
•
1198HBWE02
9811566-12A
X8339
11/18/98
11/20/98 11:25:00
11/25/98 00:41
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.748
5.66
3.50
0.700
0.247
0.512
l. 36
0.796
0.899
7.68
3.88
0.448
0.813
1.50
6.21
0.368
0.480
0.209
2.33
0.209
R B S ULT S S UM MARY (Cont'd)
1198HBWW212
9811566-0lA
X8328
11/18/98
11/20/98 11:25:00
11/24/98 17:23
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND ,
ND
ND
ND
ND
•
DL
0. 748
5.66
3.50
0.700
0.247
0.512
1.36
0.796
0.899
7.68
3.88
0.448
0.813
l.50
6.21
0.368
0.480
0.209
2.33
0.209
1198HBWW213
9 8115 6 6 -04A
X8331
11/18/98
11/20/98 11:25:00
11/24/98 19: 22
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.513
ND
ND
ND
DL
0.748
-5.66
3.50
0.700
0.247
0.512
l.36
0.796
0.899
7.68
3.88
0.448
0.813
l.50
6.21
0.368
0.480
0.209
2.33
0.209
Work Order # 9811566
Page ll_
1198HBWW214
9811566-07A
X8334
11/18/98
11/20/98 11:25:00
11/24/98 21:22
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.748
5.66
3.50
0.700
0.247
0.512
l.36
0. 796
0.899
7.68
3.88
0 .448
0.813
1.50
6.21
0.368
0 .480
0.209
2.33
0 .209
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
Pyridine
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
o-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
sym-Trinitrobenzene
1198HBWE02
9811566-12A
X8339
11/18/98
11/20/98 11:25:00
11/25/98 00:41
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.302
2.45
1. 01 ·
0.362
0.751
0.707
0.372
0.338
0.405
0.833
• R B SUL T S S UM MAR Y "(Cont'd)
1198HBWW212
9811566-0lA
X8328
11/18/98
11/20/98 11:25:00
11/24/98 17: 23
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.302
2.45
1. 01
0.362
0.751
0.707
0.372
0.338
0.405
0.833
1198HBWW213
9811566-04A
X8331
11/18/98
11/20/98 11:25:00
11/24/98 19:22
1
Water
ug/L
received
Cone. DL
0.666 0.302
ND 2.45
ND 1. 01
ND 0.362
ND 0.751
ND 0.707
ND 0.372
ND 0.338
ND 0.405
ND 0.833
Work Order # 9811566
Page g_ •
1198HBWW214
9811566-07A
X8334
11/18/98
11/20/98 11:25:00
11/24/98 21:22
1
Water
ug/L
received
Cone. DL
ND 0.302
ND 2.45
ND 1. 01
ND 0.362
ND o. 751
ND 0.707
ND 0.372
ND 0.338
ND 0.405
ND 0.833
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-dl4
2,4,6-Tribromophenol
•
1198HBWE02
9811566-12A
X8339
11/18/98
11/20/98 11:25:00
11/25/98 00:41
1
Water
ug/L
received
Cone.
Recovery
%
107
101
115
106
111
113
DL
R B S ULT S S UM MAR Y (Cont'd)
1198HBWW212
9811566-0lA
X8328
11/18/98
11/20/98 11:25:00
11/24/98 17:23
1
Water
ug/L
received
Cone.
Recovery
%
105
114
124
113
108
106
•
DL
1198HBWW213
9811566-04A
X8331
11/18/98
11/20/98 11:25:00
11/24/98 19:22
1
Water
ug/L
received
Cone.
Recovery
%
103
103
111
109
104
112
DL
Work Order # 9811566
Page ll._
1198HBWW214
9811566-07A
X8334
11/18/98
11/20/98 11:25:00
11/24/98 21:22
1
Water
ug/L
received
Cone.
Recovery
%
109
116
119
118
106
116
DL
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Aniline
Anthracene
Benz(a)anthracene
Benz(a)pyrene
Benzidine
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
Carbazole
4-Chloro-3-methylphenol
p-Chloroaniline
1198HBWW215
9811566-08A
X8335
11/18/98
11/20/98 11:25:00
11/24/98 22:02
1
Water
ug/L
received
Cone. DL
ND 0.393
ND 0.363
ND 0.849
ND 0.418
ND 7.50
ND 1. 69
ND 0.416
ND 0.302
ND 0.274
ND 10.00
ND 0.343
ND 0.154
ND 0. 341
ND 33.1
ND 0.793
ND 0.221
ND 0.210
ND 0.244
ND o. 724
ND 1.16
• R B S ULT S S UH HAR Y (Cont'd)
1198HBWW227 1198HBWW228
9811566-lOA 9811566-llA
X8337 X8338
11/18/98 11/18/98
11/20/98 11:25:00 11/20/98 11:25:00
11/24/98 23:22 11/25/98 00:02
1 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.386 3.41 0.393
ND 0.356 ND 0.363
ND 0.833 22.4 0. 849
ND 0.410 ND 0.418
ND 7.36 ND 7.50
ND 1.65 ND 1. 69
ND 0.408 ND 0.416
ND 0.296 ND 0.302
ND 0.269 ND 0.274
ND 9.81 ND 10.00
ND 0.336 ND 0.343
ND 0.151 ND 0.154
ND 0.335 ND 0. 341
4.09 J 32.5 114 33.1
ND 0.779 8.05 0.793
ND 0.217 ND 0.221
ND 0.206 ND 0.210
ND 0.239 ND 0.244
ND 0. 710 ND 0. 724
ND 1.14 ND 1.16
( .
Work Order # 9811566
Page 1.1_
1198HBWW228
9811566-llA
X8356
11/18/98
•
11/20/98 11:25:00
11/25/98 17:14
20
Water
ug/L
received
Cone. DL
NA 7.87
NA 7.26
NA 17.0
NA 8.36
NA 150
NA 33.7
NA 8.32
NA 6.04
NA 5.49
NA 200
NA 6.86
NA 3.09
NA 6.82
NA 663
NA 15.9
NA 4.42
NA 4.19
NA 4.88
NA 14.5
NA 23.2
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chlorobenzilate
-b_is-( 2 -Chloroethoxy-)-methane-
bis ( 2 -Chloroethyl) ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Diallate
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
Diethylphthalate
•
1198HBWW215
9811566-08A
X8335
11/18/98
11/20/98 11:25:00
11/24/98 22:02
1
Water
ug/L
received
Cone.
ND
-ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.269
0.309
0.159
0.195
0.568
0.344
0.373
0.388
0.203
0.232
0.256
0.174
0.356
0.639
0.505
0.523
0.990
0.582
0.537
0.282
RB S UL T S S UM MAR Y (Cont'd) Work Order # 9811566
Page li..
1198HBWW227
9811566-lOA
X8337
11/18/98
11/20/98 11:25:00
11/24/98 23:22
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
•
DL
0.264
0 .30-3
0.156
0.192
0.557
0.337
0.366
0.380
0.199
0.228
0.251
0.171
0.350
0.627
0 .495
0.513
0.972
0.571
0.527
0.277
1198HBWW228
9811566-llA
X8338
11/18/98
11/20/98 11:25:00
11/25/98 00:02
1
Water
ug/L
received
Cone.
ND
--ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.39
ND
ND
ND
ND
ND
ND
ND
DL
0.269
0-.309 --
0.159
0.195
0.568
0.344
0.373
0.388
0.203
0.232
0.256
0.174
0.356
0.639
0.505
0.523
0.990
0.582
0.537
0.282
1198HBWW228
9811566-llA
X8356
11/18/98
11/20/98 11:25:00
11/25/98 17:14
20
Water
ug/L
received
Cone.
NA
NA-
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
DL
5.37
6.17
3.18
3.90
11.4
6.88
7.47
7.75
4.06
4.65
5.12
3.49
7.12
12.8
10.1
10.5
19.8
11.6
10.7
5.64
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
p-Dimethylaminoazobenzene
7,12-Dimethylbenz(a)anthracene
3,3'-Dimethylbenzidine
Dimethylphenethylamine
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
1,3-Dinitrobenzene
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine/N-NitrosoDPA
Ethyl methanesulfonate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
1198HBWW215
9811566-08A
X8335
11/18/98
11/20/98 11;25:00
11/24/98 22: 02
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.656
1.54
1.97
28.4
0.474
0.251
1. 01
0.661
6.92
0.372
1.01
0.618
0.222
4.28
0.209
0.357
0.386
0.600
7.84
0. 772
• R B S UL TS S UM MAR Y (Cont'd)
1198HBWW227 1198HBWW228
9811566-lOA 9811566-llA
X8337 X8338
11/18/98 11/18/98
11/20/98 11:25:00 11/20/98 11:25:00
11/24/98 23:22 11/25/98 00:02
1 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.644 ND 0.656
ND 1. 51 ND 1.54
ND 1. 93 ND 1. 97
ND 27.9 ND 28.4
ND 0.465 ND 0.474
ND 0.247 ND 0.251
ND 0.991 ND 1.01
ND 0. 649 ND 0.661
ND 6.79 ND 6.92
ND 0.365 ND 0.372
ND 0.991 ND 1. 01
ND 0.607 ND 0.618
ND 0.218 ND 0.222
ND 4.20 ND 4.28
ND 0.205 ND 0.209
ND: 0.350 3.90 0.357
ND 0.379 ND 0.386
ND 0.589 ND 0.600
ND 7.69 ND 7.84
ND 0.758 ND 0. 772
work Order # 9811566
Page 1£_
1198HBWW228
9811566-llA
X8356
11/18/98
•
11/20/98 11:25:00
11/25/98 17:14
20
Water
ug/L
received
Cone. DL
NA 13.1
NA 30.9
NA 39.4
NA 568
NA 9 .49
NA 5.03
NA 20.2
NA 13.2
NA 138
NA 7.45
NA 20.2
NA 12.4
NA 4.44
NA 85.5
NA 4.17
NA 7.14
NA 7.71
NA 12.0
NA 157
NA 15.4
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Hexachloropropene
Tndeno ( 1 -, 2, 3 -cd-)-pyrene
Isophorone
Isosafrole
Kepone
Methapyrilene
Methyl methanesulfonate
3-Methylcholanthrene
2-Methylnaphthalene
4-Methylphenol/3-Methylphenol
2-Methylphenol
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
Naphthalene
•
1198HBWW215
9811566-08A
X8335
11/18/98
11/20/98 11:25:00
11/24/98 22:02
1
Water
ug/L
received
Cone. DL
ND 0.806
ND -o. 0838
ND 0.280
ND 0.734
ND 2.42
ND 6.58
ND 0.753
ND 6.61
ND 0.284
ND 0.592
ND 0 .454
ND 0.894
ND 0.747
ND 1.46
ND 0.573
ND 1. 87
ND 0.653
ND 0.305
ND 0.751
ND 0.432
R B S UL T S S UM MARY (Cont'd)
1198HBWW227 1198HBWW228
9811566-lOA 9811566-llA
X8337 X8338
11/18/98 11/18/98
11/20/98 11:25:00 11/20/98 11:25:00
11/24/98 23:22 11/25/98 00:02
1 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.791 ND 0.806
ND 0.0822 ND -0. 08-38
ND 0.275 1.49 0.280
ND o. 721 ND 0.734
ND 2.37 ND 2.42
ND 6.46 ND 6.58
ND 0.739 ND 0.753
ND 6.49 ND 6.61
0.736 0.279 92.8 0.284
ND 0.581 30.4 F 0.592
ND 0.446 4.69 0.454
ND 0.878 ND 0.894
ND 0.733 ND 0.747
ND 1.43 ND 1.46
ND 0.563 ND 0.573
ND 1.83 ND 1. 87
ND 0. 641 ND 0.653
ND 0.299 ND 0.305
ND 0.737 ND 0.751
5.64 0.424 754 ER 0.432
•
Work Order # 9811566
Page lL
1198HBWW228
9811566-llA
X8356
11/18/98
11/20/98 11:25:00
11/25/98 17:14
20
Water
ug/L
received
Cone. DL
NA 16.1
-NA 1. 68
NA 5.60
NA 14.7
NA 48.4
NA 132
NA 15.1
NA 132
NA 5.68
NA 11.8
NA 9.09
NA 17.9
NA 14.9
NA 29.1
NA 11.5
NA 37.3
NA 13.1
NA 6.10
NA 15.0
720 8.65
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,4-Naphthoquinone
1-Naphthylamine
2-Naphthylamine
5-Nitro-o-toluidine
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-1-oxide
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
2-Picoline
Pronamide
1198HBWW215
9811566-08A
X8335
11/18/98
11/20/98 11:25:00
11/24/98 22:02
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.762
5.77
3.56
0. 713
0.251
0.522
1.39
0.811
0.916
7.83
3.95
0.456
0.829
1.53
6.33
0.375
0 .490
0.213
2.37
0 .213
• RBSULTS SUMMARY (Cont'd)
1198HBWW227
9811566-lOA
X8337
11/18/98
11/20/98 11:25:00
11/24/98 23:22
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.536
9. 72
ND
ND
DL
0.748
5.66
3.50
0.700
0.247
0.512
1.36
o,796
0.899
7.68
3.88
0.448
0.813
1.50
6.21
0.368
0.480
0.209
2.33
0.209
1198HBWW228
9811566-llA
X8338
11/18/98
11/20/98 11:25:00
11/25/98 00:02
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.77
27.5
ND
ND
DL
0.762
5. 77
3.56
0. 713
0.251
0.522
1.39
0.811
0.916
7.83
3.95
0.456
0.829
1.53
6.33
0.375
0.490
0.213
2.37
0.213
Work Order # 9811566
Page l!!._
1198HBWW228
•
9811566-llA
X8356
11/18/98
11/20/98 11:25:00
11/25/98 17: 14
20
Water
ug/L
received
Cone.
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
DL
15.2
115
71.2
14.3
5.03
10.4
27.8
16 .2.
18.3
157
79.0
9.12
16.6
30.7
127
7.50
9.79
4.27
47 .4
4.27
12/0l/98 15:28:21
Method Sernivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
·Pyridine --
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
o-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
syrn-Trinitrobenzene
•
ll98HBWW2l5
981l566-08A
X8335
ll/18/98
11/20/98 11:25:00
ll/24/98 22:02
l
Water
ug/L
received
Cone. DL
ND 0.308
---ND -2.50
ND 1.03
ND 0.369
ND 0.766
ND 0. 720
ND 0.379
ND 0. 345
ND 0.412
ND 0. 849
R B S ULT S S UM MARY (Cont'd)
ll98HBWW227 1198HBWW228
9811566-lOA 9811566-llA
X8337 X8338
11/18/98 11/18/98
11/20/98 11:25:00 ll/20/98 11:25:00
11/24/98 23:22 ll/25/98 00:02
1 l
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.302 ND 0. 308
ND 2.45 ND 2-.-50
ND 1.01 ND 1. 03
ND 0.362 ND 0.369
ND 0.751 ND 0.766
ND 0.707 ND 0. 720
ND 0.372 ND 0.379
ND 0.338 ND 0.345
ND 0.405 ND 0.412
ND 0.833 ND 0.849
•
Work Order # 9811566
Page 1,L
ll98HBWW228
9811566-llA
X8356
11/18/98
ll/20/98 11:25:00
ll/25/98 17:14
20
Water
ug/L
received
Cone. DL
NA 6.15
-NA 4_9. 9
NA 20.6
NA 7.37
NA 15.3
NA 14.4
NA 7.58
NA 6.90
NA 8.25
NA 17.0
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-dl4
2,4,6-Tribromophenol
1198HBWW215
9811566-08A
X8335
11/18/98
11/20/98 11:25:00
11/24/98 22:02
1
Water
ug/L
received
Cone.
Recovery
%
102
106
114
106
100
107
DL
• R B S UL T S S UM MARY (Cont'd)
1198HBWW227
9811566-lOA
X8337
11/18/98
11/20/98 11:25:00
11/24/98 23:22
1
Water
ug/L
received
Cone.
Recovery
%
99
98
106
104
106
113
DL
1198HBWW228
9811566-llA
X8338
11/18/98
11/20/98 11:25:00
11/25/98 00:02
1
Water
ug/L
received
Cone. DL
Recovery
%
103
103
115
NC
102
117
Work Order # 9811566
Page £Q_
1198HBWW228
9811566-llA
X8356
11/18/98
11/20/98 11:25:00
11/25/98 17:14
20
Water
ug/L
received
Cone. DL
Recovery
%
92
67
78
NC
78
84
•
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acenaphthene
'Acenaplitliylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Aniline
Anthracene
Benz(a)anthracene
Benz(a)pyrene
Benzidine
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
Carbazole
4-Chloro-3-methylphenol
p-Chloroaniline
•
ll98HBWW23l
9811566-09A
X8336
11/18/98
11/20/98 11:25:00
11/24/98 22:42
1
Water
ug/L
received
Cone. DL
ND 0.536
ND 0.4·95
ND 1.16
ND 0.570
ND 10.2
ND 2.30
ND 0.568
ND 0.412
ND 0.374
ND 13.6
ND 0.468
ND 0.210
ND 0.465
ND 45.2
ND 1.08
ND 0.301
ND 0.286
ND 0.332
ND 0.987
ND 1.58
R B S UL T S S UM MARY (Cont'd)
Cone. DL Cone.
-
•
DL
-
Work Order # 9811566
Page £L
Cone. DL
-
-
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Diallate
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,31 -Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
Diethylphthalate
1198HBWW231
9811566-09A
X8336
11/18/98
11/20/98 11:25:00
11/24/98 22:42
1
Water
ug/L
received
Cone. DL
ND 0.366
ND 0.421
ND 0.217
ND 0.266
ND 0.774
ND 0.469
ND 0.509
ND 0.529
ND 0.277
ND 0.317
ND 0.349
ND 0.238
ND 0.486
ND 0.871
ND 0.688
ND 0. 713
ND 1.35
ND 0.794
ND o. 732
ND 0.384
• RESULTS SUMMARY .(Cont'd)
-
Cone. DL Cone. DL
Work Order # 9811566
Page ~
Cone. DL
•
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
p-Dimethylaminoazobenzene
.. 7,12~Dimethylbenz(a)anthracene
3,3°-Dimethylbenzidine
Dimethylphenethylamine
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
1,3-Dinitrobenzene
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diphenylamine/N-NitrosoDPA
Ethyl methanesulfonate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
•
1198HBWW231
9811566-09A
X8336
11/18/98
11/20/98 11:25:00
11/24/98 22:42
1
Water
ug/L
received
Cone. DL
ND 0.895
Nb 2.10
ND 2.69
ND 38.7
ND 0. 647
ND 0.343
ND 1. 38
ND 0.901
ND 9.44
ND 0.508
ND 1.38
ND 0.843
ND 0.303
ND 5.83
ND 0.284
ND 0.487
ND 0.526
ND 0.818 .
ND 10.7
ND 1. 05
R. B S ULT S S UM MAR. Y (Cont'd)
Cone. DL Cone. DL
•
Work Order U 9811566
Page ll_
Cone. DL
. --
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Hexachloropropene
Indeno(l,2,3-cd)pyrene
Isophorone
Isosafrole
Ke pone
Methapyrilene
Methyl methanesulfonate
3-Methylcholanthrene
2-Methylnaphthalene
4-Methylphenol/3-Methylphenol
2-Methylphenol
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
Naphthalene
1198HBWW231
9811566-09A
X8336
11/18/98
11/20/98 11:25:00
11/24/98 22:42
1
Water
ug/L
received
Cone. DL
ND 1.10
ND 0.114
ND 0.382
ND 1.00
ND 3.30
ND 8.97
ND 1. 03
ND 9.01
ND 0.387
ND 0.808
ND 0.619
ND 1.22
ND 1.02
ND 1.99
ND 0.782
ND 2.55
ND 0.891
ND 0.416
ND 1. 02
ND 0.590
• R K S ULT S S UH HAR Y (Cont'd)
Cone. DL Cone.
:
DL
Work Order # 9811566
Page ~ •
Cone. DL
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,4-Naphthoquinone
-i-Naphthyl:amine
2-Naphthylamine
5-Nitro-o-toluidine
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-l-oxide
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
2-Picoline
Pronamide
••
ll98HBWW231
9811566-09A
X8336
11/18/98
11/20/98 11:25:00
11/24/98 22:42
l
Water
ug/L
received
Cone. DL
ND 1.04
ND 7.87
ND 4.86
ND 0.973
ND 0.343
ND 0.712
ND 1. 90
ND 1.11
ND 1.25
ND 10.7
ND 5.39
ND 0.622
ND 1.13
ND 2.09
ND 8.64
ND 0.512
ND 0.668
ND 0.291
ND 3.23
ND 0.291
R E S ULT S S UM MARY (Cont'd)
Cone. DL Cone. DL
•
Work Order # 9811566
Page ~
Cone. DL
~~ --
•
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Pyrene
Pyridine
Saf role
1,2,4,5-Tetraehlorobenzene
2,3,4,6-Tetraehlorophenol
o-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Triehlorophenol
sym-Trinitrobenzene
1198HBWW231
9811566-09A
X8336
11/18/98
11/20/98 11:25:00
11/24/98 22:42
1
Water
ug/L
received
Cone. DL
ND 0.419
ND 3.40
ND 1.40
ND 0.503
ND 1.04
ND 0.982
ND 0.517
ND 0.470
ND 0.562
ND 1.16
• RE S ULT S S UM MARY (Cont'd)
Cone. DL Cone.
•'
DL
Work Order # 9811566
Page~
Cone. DL
•
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBCM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-dl4
2,4,6-Tribromophenol
•
ll98HBWW23l
98ll566-09A
X8336
ll/18/98
11/20/98 11:25:00
ll/24/98 22:42
l
Water
ug/L
received
Cone. DL
Recovery
"
104
105
112
115
112
112
R B S ULT S S UM MARY (Cont'd)
Cone. DL Cone.
Recovery Recovery
" %
•
DL
Work Order # 9811566
Page '!:]_
Cone. DL
Recovery
"
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBOO
Initial Calibration # MSD1981121062400
Calibration Date ~11~/~2~1~/~9~8'--~~~-
Sequence/Analysis Time
1 11/24/98 08:35
2 11/24/98 08:59
3 11/24/98 09:39
4 11/24/98 1G:l9
5 11/24/98 11:02
6 11/24/98 11:42
7 11/24/98 12:22
8 11/24/98 13:03
9 11/24/98 13:43
10 11/24/98 14:23
11 11/24/98 14:43
12 11/24/98 15:24
13 11/24/98 17:23
14 11/24/98 18:03
15 11/24/98 18:42
16 11/24/98 19:22
17 11/24/98 20:02
18 11/24/98 20:42
. 19 11/24/98 21:22
20 11/24/98 22:02
21 11/24/98 22:42
22 11/24/98 23:22
23 11/25/98 00:02
24 11/25/98 00 :41
25 11/25/98 01:21
26 11/25/98 02:01
• ABALYSIS BATCH SUMMARY
Analysis Batch # MSMSD181124083501
Analysis Start Date/Time 11/24/98 08:35:00
Analysis Stop Date/Time 11/25/98 02:01:00
Work Order # 9811566
Page £1!_
Instrument !:!fil21____
Analyst !1f!!
Reviewer S~D~K,,_~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis File #
TUNE GC/MS tune files X8316
SSTD050 Continuing Calibration Verification X8317
LCS986251 Lab Control Sample X8318
LCSD986251 Lab Control Sample Duplicate X8319
BLK984092 Blank, Method X8320
9811612-07A Sample X8321
9811612-08A ·Matrix Spike X8322
9811612-09A Matrix Spike Duplicate X8323
9811579-0lA Sample X8324
TUNE GC/MS tune files X8325
SSTD050 Continuing Calibration Verification X8326
9811644-0lA Samp~e X8327
1198HBWW212 9811566-0lA Sample X8328
1198HBWW212 9811566-02A Matrix Spike X8329
1198HBWW212 9811566-03A Matrix Spike Duplicate X8330
1198HBWW213 9811566-04A Sample X8331
1198HBWW213 9811566-05A Matrix Spike X8332
1198HBWW213 9811566-06A Matrix Spike Duplicate X8333
1198HBWW214 9811566-07A Sample X8334
1198HBWW215 9811566-08A Sample X8335
1198HBWW231 9811566-09A Sample X8336
1198HBWW227 9811566-lOA Sample X8337
1198HBWW228 9811566-llA Sample X8338
1198HBWE02 9811566-12A Sample X8339
9811612-0lA Sample X8340
9811612-02A Sami:,>le X8341
•
12/01/98 15:28:21
Method Semivolatiles by SW8270C
Test Code 827SWBOO
Initial Calibration # MSD1981121062400
Calibration Date ~1~1~/~2~1~/9~8---~~~~
Sequence/Analysis Time
1 11/25/98 08:24
2 11/25/98 08:44
3 11/25/98 09:27
4 11/25/98 10:07
5 11/25/98 10:47
6 11/25/98 11:27
7 11/25/98 12:07
8 11/25/98 12:47
-· 9 ll/25/98 13 ,2-1
10 11/25/98 14:12
11 11/25/98 14:32
12 11/25/98 15:12
13 11/25/98 15:52
14 11/25/98 16:33
15 11/25/98 17:14
16 11/25/98 17:55
17 11/25/98 18:36
18 11/25/98 19:16
19 11/25/98 19:57
20 11/25/98 20:37
21 11/25/98 21:18
22 11/25/98 21:58
23 11/25/98 22:39
•
ABALYSIS BATCH SUMMARY
Analysis Batch # MSMSD181125082401
Analysis Start Date/Time 11/25/98 08:24:00
Analysis Stop Date/Time 11/25/98 22:39:00
Work Order # 9811566
Page~
Instrument ~
Analyst !:1£!!
Reviewer ~S~D=K~~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis· File #
TUNE GC/MS tune files X8342
SSTD050 Continuing Calibration Verification X8343
LCS986322 Lab Control Sample X8344
LCSD986322 Lab Control Sample Duplicate X8345
BLK984128 Blank, Method X8346
9811589-02A Sample X8347
9811589-03A Matrix Spike X8348
9811589-04A Matrix Spike Duplicate X8349
98l:l589~0l:A Sample --. ---X8350--
TUNE GC/MS tune files X8351
SSTD050 Continuing Calibration Verification X8352
9811589-05A Sample X8353
9811589-06A Sample X8354
9811589-08A Sample X8355
1198HBWW228 9811566-llA Sample X8356
9811612-03A Sample X8357
9811612-04A Sample X8358
9811574-07A Media Recovery Check X8359
9811574-08A Media Recovery Check Duplicate X8360
9811574-0lA Sample X8361
9811574-02A Sample X8362
9811574-03A Sample X8363
9811574-04A Sample X8364
• •
• 12/01/98 15:28:21
Method Semivolatiles by SW8270C Specification# ~~~~
Lab Sample ID
File ID
Project Sample
ID/Description Analyte
• ANALYTICAL PROTOCOL SUMMARY
COMMBBTS/BARRATIVB
Flag Comment/Narrative
9811566-llA
X833B
ll9BHBWW228 4-Methylphenol/3-Methylphenol F The F flag indicates that 3-methylphenol
coelutes with 4-methylphenol. The calibration
response factor is based on 4-methylphenol
only. Any identification for 4-methylphenol
should be regarded as a possible sum of the
two indistinguishable isomers.
Corrective Action
• Work Order tt 9811566
Page l.Q_
12/01/98 15:28:21
•
Q U A L I T Y C 0 B T R 0 L B ][ C B P T I 0 B R B P 0 R T
SUMMARY
QCER # Analysis Batch Number
981125-15 MSD1981125082400
981124-12 MSD1981124083500
-
•
Work Order # 9811566
Page lL
•
12/07/98 15:00:34
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared --"R"'a"'d"'i"'a"'n'--"I""'n"'t"'e"'r-"n"'a"'t:.:ic:::o~n"'a"'l'"',_.L::L:>:C:....
By --=l-=4-=0-=4-=6-=S-"u"'m"'m"'i"'t-=D;.:r-'.-''-=B:.:l"'d"'q'-'._.B:....
P. O. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW212
1198HBWW213
1198HBWW214
1198HBWW215
1198HBWW227
1198HBWW228
•
ID/
-
WORK ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID WASHINGTON, NC
Case H MN.A-----~-~-~
SDG II .::N::..:A'---------
RAS # 80903AJAL
i.,ab Sample: ID I Test C.:>de{s)
OlA N23EWAOO
02A MS N23EWAOO
03A MSD N23EWAOO
04A N23EWAOO
05A MS N23EWAOO
06A MSD N23EWAOO
07A N23EWAOO
OBA N23EWAOO
09A N23EWAOO
lOA N23EWAOO
•
Work Order U 9811567
Page _1_
RCN 650138.0602
New York ELAP ID U: 10915
Method Desciption
Nitrate-Nitrite,Colorimetr
Nitrate-·Ni·tr"i t·e ,·Co·lorimet r -
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
Nitrate-Nitrite,Colorimetr
•
• 12/07/98 15:00:34
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB CBRTIPICATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order tt 9811567
Page L_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
12/07/98 15:00:34 ANALYTICAL PROTOCOL SUMMARY
FLAG DBPIHITIOHS
Flag Definition
< DL
NA
NC
ND
NR
NS
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A
B
c
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
--F
G
Interfer,ence or coe-lution suspected-. See .Narrative for explanat.ion.
Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Narrative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M Result modified from previous Report. See Narrative for explanation.
P Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Specification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
z See Narrative for explanation.
• •
Work Order U 9811567
Page _3_
•
• 12/07/98 15:00:34
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Nitrate-nitrite, EPA 353.1
Project Sample ID/Description
1198HBWW212
1198HBWW213
1198HBWW214
1198HBWW215
1198HBWW227
1198HBWW228
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch #
9811567-0lA N23EWAOO NA
9811567-04A N23EWAOO NA
9811567-07A N23EWAOO NA
9811567-08A N23EWAOO NA
9811567-09A N23EWAOO NA
9811567-lOA N23EWAOO NA
Work Order # 9811567
Page _4_
Analysis Batch #
WLTRAC81206115601
WLTRAC81206115601
WLTRAC81206115601
WLTRAC81206115601
WLTRAC81206115601
WLTRAC81206115601
•
12/07/98 15:00:34
Method Nitrate-nitrite, EPA 353.1
Test Code N23EWAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Nitrate-Nitrite as N
•
1198HBWW212
98ll567-01A
TRAC1206-18
ll/18/98
12/06/98 11:56:00
1
Water
mg/L
received
Cone.
0.0104
DL
0.00563
RESULTS SUMMARY
ll98HBWW213
98ll567-04A
TRAC1206-22
ll/18/98
12/06/98 11:56:00
1
Water
mg/L
received
Cone.
0.00970
•
DL
0.00563
ll98HBWW214
98ll567-07A
TRAC1206-26
ll/18/98
12/06/98 11:56:0~
1
Water
mg/L
received
Cone.
0.0166
DL
0.00563
Work Order U 9811567
Page _5_
1198HBWW215
98ll567-08A
TRAC12G6-27
ll/18/98
12/06/98 11:56:00
1
Water
mg/L
received
Cone. DL
0.0305 0.00563
•
• 12/07/98 15:00:34
Method Nitrate-nitrite, EPA 353.1
Test Code N23EWAOO
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Nitrate-Nitrite as N
l198HBWW227
9811567-09A
TRAC1206-28
11/18/98
12/06/98 11:56:00
1
Water
mg/L
received
Cone. DL
0. 04 85 0.00563
• R B S UL T S S U M MA R Y (Cont'd)
1198HBWW228
9811567-lOA
TRAC1206-29
11/18/98
12/06/98 11:56:00
l
Water
mg/L
received
Cone. DL
0.0824 0.00563
Cone. DL
Work Order # 9811567
Page _6_
Cone. DL
•
12/07/98 15:00:34
Method Nitrate-nitrite, EPA 353.1
Test Code N23EWAOO
Initial Calibration tt .N~A~------~
Calibration Date ---------
Sequence/Analysis Time
1 12/06/98 11:56:00
2 12/06/98 11:56:00
3 12/06/98 11:56:00
4 12/06/98 11:56:00
5 12/06/98 11:56:00
6 12/06/98 11:56:00
7 12/06/98 11:56:00
8 12/06/98 11:56:00
-9 12/06/98 1:1:56:00 --
10 12/06/98 11:56:00
11 12/06/98 11:56:00
12 12/06/98 11:56:00
13 12/06/98 11:56:00
14 12/06/98 11:56:00
15 12/06/98 11:56:00
"16 12/06/98 11:56:00
17 12/06/98 11:56:00
18 12/06/98 11:56:00
19 12/06/98 11:56:00
20 12/06/98 11:56:00
21 12/06/98 11:56:00
22 12/06/98 11:56:00
23 12/06/98 11:56:00
24 12/06/98 11:56:00
25 12/06/98 11:56:00
26 12/06/98 11:56:00
27 12/06/98 11:56:00
28 12/06/98 11:56:00
29 12/06/98 11:56:00
30 12/06/98 11:56:00
•
ANALYSIS BATCH SUMMARY
Analysis Batch tt WLTRAC81206115601
Analysis Start Date/Time 12/06/98 11:56:00
Analysi$ Stop Date/Time 12/06/98 11:56:00
work Order ff 9811567
Page _7_
Instrument ~
Analyst ~
Reviewer ~L~K~H'----------
Project Sample ID Lab Sample ID Sample Type Analysis·File tt
PRIMER TRAC1206-1
SYSBLK Blank, System TRAC1206-2
CALSTDl Initial Calibration Standard 1 TRAC1206-3
CALSTD2 Initial Calibration Standard 2 TRAC1206-4
CALSTD3 Initial Calibration Standard 3 TRAC1206-5
CALSTD4 Initial Calibration Standard 4 TRAC1206-6
CALSTD5 Initial Calibration Standard 5 TRACT206-7
CALSTD6 Initial Calibration Standard 6 TRAC1206-8
ICB Blank, lnitia-1 Ca-librat ion TAAC1.2Q6_-.9 -
ICV Initial Calibration Verification TRAC1206-10
N02REDCHECK Distilled Calibration Standard TRAC1206-ll
SYSBLK Blank, System TRAC1206-l2
DCS986518 Detectability Check Sample TRAC1206-l3
BLK984270 Blank, Method TRAC1206-14
LCS986517 Lab Control Sample TRAC1206-l5
LCSD986517 Lab Control Sample Duplicate TRAC1206-16
SYSBLK Blank, System TRAC1206-17
1198HBWW212 9811567-0lA Sample TRAC1206-18
1198HBWW21~ 9811567-02A Matrix Spike TRAC1206-19
1198HBWW212 9811567-03A Matrix Spike Duplicate TRAC1206-20
SYSBLK Blank, system TRAC1206-21
1198HBWW213 9811567-04A Sample TRAC1206-22
1198HBWW213 9811567-05A Matrix Spike TRAC1206-23
1198HBWW213 9811567-06A Matrix Spike Duplicate TRAC1206-24
SYSBLK Blank, System TRAC1206-25
1198HBWW214 9811567-07A Sample TRAC1206-26
1198HBWW215 9811567-08A Sample TRAC1206-27
1198HBWW227 9811567-09A Sample TRAC1206-28
1198HBWW228 9811567-lOA Sample TRAC1206-29
9811520-0lA Sample TRAC1206-30
• •
• 12/07/98 15:00:34
Method Nitrate-nitrite, EPA 353.1
Test Code N23EWAOO
Initial Calibration # ~N~A'---------~
Calibration Date ~--------
Sequence/Analysis Time
31 12/06/98 11:56:00
32 12/06/98 11:56:00
33 12/06/98 11:56:00
34 12/06/98 11:56:00
35 12/06/98 11:56:00
36 12/06/98 11:56:00
37 12/06/98 11:56:00
38 12/06/98 11:56:00
39 12/06/98 11:56:00
40 12/06/98 11:56:00
41 12/06/98 11:56:00
42 12/06/98 11:56:00
43 12/06/98 11:56:00
44 12/06/98 11:56:00
45 12/06/98 11:56:00
46 12/06/98 11:56:00
47 12/06/98 11:56:00
48 12/06/98 11:56:00
49 12/06/98 11:56:00
50 12/06/98 11:56:00
51 12/06/98 11:56:00
52 12/06/98 11:56:00
53 12/06/98 11:56:00
54 12/06/98 11:56:00
55 12/06/98 11:56:00
56 12/06/98 11:56:00
• A S A L Y S I S B AT C U S UM MAR Y (cont'd}
Analysis Batch # WLTRAC81206115601
Analysis Start Date/Time 12/06/98 11:56:00
Analysis Stop Date/Time 12/06/98 11:56:00
Project Sample ID Lab Sample ID Sample Type
9811618-0lA Sample
9811618-02A Sample
9811618-03A Sample
Work Order # 9811567
Page _8_
Instrument ~
Analyst [!£E
Reviewer ~L~K~H'----------
Analysis File #
TRAC1206-31
TRAC1206-32
TRAC1206-33
CCB Blank, Contiruing Calibration TRAC1206-34
CCV Continuing Calibration Verification TRAC1206-35
9811618-04A Sample TRAC1206-36
9811618-05A Sample TRAC1206-37
9811618-06A Sample TRAC1206-38
9811618-07A Matrix Spike TRAC1206-39
9811618-08A Matrix Spike Duplicate TRAC1206-40
SYSBLK Blank, System TRAC1206-41
9811618-09A Sample TRAC1206-42
9811618-lOA Sample TRAC120G-43
9811618-llA Sample TRAC1206-44
9811618-12A Sample TRAC1206-45
9811618-13A Sample TRAC1206-46
9811618-14A Sample TRAC1206-47 ,
9811618-15A Sample TRAC1206-48
SYSBLK Blank, System TRAC1206-49
CCB Blank, Continuing Calibration TRAC1206-50
CCV Continuing Calibration Verification TRAC1206-51
HIGHSTD Sample TRAC1206-52
LOWS TD Sample TRAC1206-53
LOW STD Sample TRAC1206-54
SYSBLK Blank, System TRAC1206-55
PRIMER Sample TRAC1206-56
•
12/07/98 15:00:34
Method Nitrate-nitrite, EPA 353.l Specification#~~-~
Lab Sample ID
File ID
•
Project Sample
ID/Description Analyte
ANALYTICAL PROTOCOL SUMMARY
COMMBHTS/HARRATIVB
Flag Comment/Narrative
•
Corrective Action
Work Order # 9811567
Page _9_
•
12/03/98 16:43:13
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared --=-R"'a"'d"'i"'a~n'-"I"'n"'t"'e"'r"'n"'a"'t"'i"'o"'n"'a"'l'-''-=L"'L"'C'­
By -~1-4_0_4_6_.s_u"'m'"'m"'i"'t:...;:;D"'r'"'._.,~B-l"'d"'g'""._.B.__
P. O. Box 201088
Austin, TX 78720-10~8
CSC JALINDSEY
'
Project Sample
Description
1198HBWW225
·119·aHBWW212
1198HBWW213
1198HBWW214
1198HBWW215
1198HBWW227
1198HBWW228
•
ID/
NORK ORDBR SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID WASHINGTON, NC
Case # -N-A..__~~-----
SDG # _NA.._ _______ _
RAS # 80903AJAL
Lab Sample ID Test Code(s)
OlA ALKEWACP
0211: -. ALKEWACP --·
03A MS ALKEWACP
04A MSD ALKEWACP
05A ALKEWACP
06A MS ALKEWACP
07A MSD ALKEWACP
OBA ALKEWACP
09A ALKEWACP
lOA ALKEWACP
llA ALKEWACP
•
Work Order # 9811568
Page 1._
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Alkalinity
A·lka·Hn±ty· --
.Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
Alkalinity
•
• 12/03/98 16:43:13
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
• STATB CBRTIPICATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order # 9811568
Page ;L_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
12/03/98 16:43:13 ANALYTICAL PROTOCOL SUMMARY
Flag
< DL
NA
NC
ND
NR
NS
A
8
c
D
E -
F
G
H
I
J
K
M
p
Q
R
s
T
x
y
z
•
FLAG DEFINITIONS
Definition
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this a~alysis.
RPD and/or % Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
Confirming data obta~ned using second GC-column or GCMS.
Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
Analyte concentration exceeded calibration range.
Interference or coelution suspected. See Narrative for explanation.
Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
Presence of analyte previously confirmed by historical data.
Analyte identification suspect. See Narrative for explanation.
Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
Peak did not meet method identification criteria. Analyte not detected on other GC column.
Result modified from previous Report. See Narrative for explanation.
Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
QC result does not meet tolerance in Protocol Specification.
Result reported elsewhere.
Analyte concentration obtained using Method of Standard Additions (MSA) .
Second column confirma.tional analysis not performed.
See Narrative for explanation.
See Narrative for explanation.
See Narrative for explanation.
•
Work Order # 9811568
Page _3_
•
• 12/03/98 16:43:13
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method Alkalinity by E310.1
Project Sample ID/Description
1198HBWW212
1198HBWW213
1198HBWW214
1198HBWW215
1198HBWW225
1198HBWW227
1198HBWW228
• ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch U
9811568-02A ALKEWACP NA
9811568-05A ALKEWACP NA
9811568-08A ALKEWACP NA
9811568-09A ALKEWACP NA
9811568-0lA ALKEWACP NA
9811568-lOA ALKEWACP NA
9811568-llA ALKEWACP NA
Work Order U 9811568
Page _4_
Analysis Batch #
WLOTT081123104601
WLOTT081123104601
WLOTT081123104601
WLOTT081123104601
WLOTT081123104601
WLOTT081123104601
WLOTT081123104601
•
12/03/98 16:43:13
Method Alkalinity by E310.l
Test Code ALKEWACP
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Bicarbonate
Carbonate --
Hydroxide
Total Alkalinity
•
1198HBWW212
9811568-02A
OTT01123-5
11/18/98
11/23/98 10:46:00
1
Water
mg/L
received
Cone. --OL
100 B
0
0
100 B 0.358
RESULTS SUMMARY
1198HBWW213 1198HBWW214
9811568-05A 9811568-08A
OTT01123-8 OTT01123-12
11/18/98 11/18/98
11/23/98 10:46:00 11/23/98 10:46:00
1 1
Water Water
mg/L mg/L
received received
Cone. DL Cone. DL
51.l B 102 B
0 -o--
0 0
51. l B 0.358 102 B 0.358
•
- -
Work Order # 9811568
Page L
1198HBWW215
9811568-09A
OTT01123-13
11/18/98
11/23/98 10:46:00
l
Water
mg/L
received
Cone. DL
14.4 B
0
0
14 .4 B 0.358
•
• 12/03/98 16:43:13
Method Alkalinity by E310.1
Test Code ALKEWACP
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Bicarbonate
Carbonate
Hydroxide
Total Alkalinity
1198HBWW225
9811568-0lA
OTT0112 3-11
11/18/98
11/23/98 10:46:00
1
Water
mg/L
received
Cone. DL
1. 08 B
0
0
1. 08 B 0.358
• RBS ULT S S UM MARY (Cont'd)
1198HBWW227 1198HBWW228
9811568-lOA 9811568-llA
OTT01123-14 OTT01123-15
11/18/98 11/18/98
11/23/98 10:46:00 11/23/98 10:46:00
1 1
Water Water
mg/L mg/L
received received
Cone. DL Cone. DL
216 B 0 B
0 0
0 0
216 B 0.358 0 BJ 0.358
Work Order ff 9811568
Page _6_
Cone. DL
•
12/03/98 16:43:13
Method Alkalinity by E310.l
Test Code ALKEWACP
Initial Calibration # ~N~A'-----~~~~­
Calibration Date -~--~~-~
Sequence/Analysis Time
1 11/23/98 10:46:00
2 11/23/98 10:46:00
3 11/23/98 10:46:00
4 11/23/98 10:46:00
5 11/23/98 10:46:00
6 11/23/98 rn:4§:oo
7 11/23/98 10:46:00
8 11/23/98 10:46:00
9 11/23/98 lff:46:00
10 11/23/98 10:46:00
11 ll/23/98 10:46:00
12 11/23/98 10:46:00
13 ll/23/98 10:46:00
14 11/23/98 10:46:00
15 ll/23/98 10:46:00
16 ll/23/98 10:46:00
17 11/23/98 10:46:00
18 11/23/98 10:46:00
19 11/23/98 10 :46: oo.
•
A !ii A L Y S I S B A T C ll S U M M A R Y
Analysis Batch # WLOTT081123104601
Analysis Start Date/Time 11/23/98 10:46:00
Analysis Stop Date/Time 11/23/98 17:15:00
Project Sample ID Lab Sample ID Sample Type
csv Second Source Standard
BLK984217 Blank, Method
LCS986436 Lab Control Sample
LCSD986436 Lab Control Sample Duplicate
1198HBWW212 9811568-02A Sample
ll98HBWW212 9811568-03A Matrix Spike
l198HBWW212 9811568-04A Matrix Spike Duplicate
1198HBWW2l3 9811568-05A Sample
1T98HBWW213 98-ll56·8·-06A -Matrix -Spike
1198HBWW213 9811568-0?A Matrix Spike Duplicate
1198HBWW225 9811568-0lA Sample
ll98HBWW214 98ll568-08A Sample
ll98HBWW215 9811568-09A Sample
ll98HBWW227 9811568-lOA Sample
ll98HBWW228 9811568-llA Sample
csv Second Source Standard
ll98HBWW228 9811568-llA Sample
ll98HBWW228 9811568-llA Sample
csv Second Source Standard
•
Work Order # 9811568
Page _7 _
Instrument Q!!Q...__
Analyst Jg&
Reviewer ~A~C~R _______ _
Analysis File #
OTT01123-l
OTT01123-2
OTT01123-3
OTT01l23-4
OTT01123-5
OTT01123-6
OTTOli23-7 -
OTT01123-8
9TT01123-9
OTT01123-l0
OTT01123-ll
OTT01123-l2
OTT01123-l3
OTT01123-l4
OTT0ll23-l5
OTT01123-l6
OTT01123-l7
OTT01123-l8
OTT01123-l9
•
• 12/03/98 16:43:13
Method Alkalinity by E310.l
Lab Sample ID
File ID
Project Sample
ID/Description
Specification# A:..:::L~K __ _
Analyte
• ANALYTICAL PROTOCOL SUMMARY
COMMEHTS/HARRATIVB
Flag Comment/Narrative Corrective Action
• Work Order # 9811568
Page _s_
12/03/98 16:43:13
•
QUALITY C 0 Ii TR 0 L B lC CB PT I o·N RB P 0 RT
SUMMARY
QCER # Analysis Batch Number
981123-19 OTT0981123104600
•
Work Order # 9811568
Page _9 _
•
• 11/30/98 12:49:55
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ _...,R~a~d~i~a~n'--"'I~n~t~e~r~n~a~t~i~o~n~a~l~,'--"'L~L~C'-­
By --=1~4~0~4~6.....,,,S~u~m~m~i~t_.:::D~r~·~r_.:::B~l~d~q~.-"B'-­
P. 0. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWW225
1198HBWW212
1198HBWW213
1198HBWW214
1198HBWW215
1198HBWW227
1198HBWW228
ID/
• WORK ORDER SUMMARY
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON NC
Work ID WASHINGTON, NC
Case # _N_A.._ _______ _
SDG # ~N~A'---------­
RAS # 80903AJAL
Lab Sample ID Test Code (s)
OlA XXIEWASF
02A XXIEWASF
03A MS XXIEWASF
04A MSD XXIEWASF
05A XXIEWASF
06A MS XXIEWASF
07A MSD XXIEWASF
OBA XXIEWASF
09A XXIEWASF
lOA XXIEWASF
llA XXIEWASF
Anions
Anions
Anions
Anions
Anions
Anions
Anions
Anions
Anions
Anions
Anions
by
by
by
by
by
Work Order # 9811569
Page _1_
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
IC
IC
IC
IC
IC
by IC
by IC
by IC
by IC
by IC
by IC
•
11/30/98 12:49:55
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
SO\lth Ca]'."olina
Utah
Wisconsin
-----
•
STATE CBRTIPICATIOHS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
•
Work Order # 9811569
Page L
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
-
•
I
• • 11/30/98 12:49:55 ANALYTICAL PROTOCOL SUMMARY
Flag
< DL
NA
NC
ND
NR
NS
A
B
c
D
E
F
G
H
I
J
K
M
p
Q
R
S·
T
x
y
z
FLAG DEFINITIONS
Definition
Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis.
RPD and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
Presence of hyprocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
Confirming data obtained using second GC column or GCMS.
Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
Analyte concentration exceeded calibration range.
Interference or coelution suspected. See Narrative for explanation.
Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match tbat of Jet Fuel.
Presence of analyte previously confirmed by historical data.
Analyte identification suspect. See Narrative for explanation.
Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
Peak did not meet method identification criteria. Analyte not detected on other GC column.
Result modified from previous Report. See Narrative for explanation.
Analyte not confirmed. Results from primary and secondary GC columns differ by greater than a factor of 3.
QC result does not meet tolerance in Protocol Specification.
Result reported elsewhere.
Analyte concentration obtained using Method of Standard Additions (MSA) .
Second column confirmational analysis not performed.
See Narrative for explanatfon.
See Narrative for explanation.
See Narrative for explanation.
Work Order # 9811569
Page _3_ •
11/30/98 12:49:55
Client HAMILTON BEACH
Facility WASHINGTON.NC
Client Code HAM BEACH NC
Method IC EPA 300.0
Project Sample ID/Description
1198HBWW212
1198HBWW213
1198HBWW214
1198HBWW215
1198HBWW225
1198HBWW227
1198HBWW228
•
AHALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code (s) Batch #
9811569-02A XXIEWASF NA
9811569-0SA XXIEWASF NA
9811569-08A XXIEWASF NA
9811569-09A XXIEWASF NA
9811569-0lA XXIEWASF NA
9811569-lOA XXIEWASF NA
9811569-llA XXIEWASF NA
•
Work Order # 9811569
Page _4 _
Analysis Batch-#
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
WLX10081123091701
•
• 11/30/98 12:49:55
Method IC EPA 300.0
Test Code XXIEWASF
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Sulfate
1198HBWW212
9811569-02A
Xl001123-28
11/18/98
11/23/98 16:22:05
l
Water
mg/L
received
Cone.
0 J
DL
0.0421
• RESULTS SUMMARY
1198HBWW213
9811569-05A
Xl001123-31
11/18/98
11/23/98 17:09:15
1.
Water
mg/L
received
Cone.
41.1
DL
0.0421
1198HBWW214
9811569-08A
Xl001123-34
11/18/98
11/23/98 17:56:03
l
Water
mg/L
received
Cone. DL
3.13 0.0421
Work Order # 9811569
Page L
1198HBWW215
9811569-09A
Xl001.123-35
11/18/98
11/23/98 18:11:42
l
Water
mg/L
received
Cone.
7.77
DL
0.0421
•
11/30/98 12:49:55
Method IC EPA 300.0
Test Code XXIEWASF
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Sulfate
•
1198HBWW225
9811569-0lA
X1001123-27
11/18/98
11/23/98 16:06:25
1
Water
mg/L
received
Cone .. .DL
19.4 0.0421
R R S U L T S S U H H A R Y (Cont'd)
1198HBWW227 1198HBWW228
9811569-lOA 9811569-llA
X1001123-36 X1001123-37
11/18/98 11/18/98
11/23/98 18:27:22 11/23/98 18:43:00
1 1
Water Water
mg/L mg/L
received received
Cone. DL Cone. DL
15.2 0.0421 26.6 0.0421
..
•
Work Order # 9811569
Page _6_
Cone. DL
•
• 11/30/98 12:49:55
Method IC EPA 300.0
Test Code XXIEWASF
Initial Calibration # ~N~A=--~~~~~~~
Calibration Date ~~~~~~~~
Sequence/Analysis Time
1 11/23/98 09:17:38
2 11/23/98 09:33:08
3 11/23/98 09:49:25
4 11/23/98 10:05:05
5 11/23/98 10:20:27
6 11/23/98 10:37:50
7 11/23/98 10:53:28
8 11/23/98 11:09:06
9 11/23/98 11:24:45
10 11/23/98 11:40:24
11 11/23/98 11:56:03
12 11/23/98 12:11:42
13 11/23/98 12:27:22
14 11/23/98 12:43:00
15 11/23/98 12:58:22
16 11/23/98 13:13:48
17 11/23/98 13:29:17
18 11/23/98 13:45:38
19 11/23/98 14:01:16
20 11/23/98 14:16:56
21 11/23/98 14:32:36
22 11/23/98 14:48:17
23 11/23/98 15:03:55
24 11/23/98 15:19:29
25 11/23/98 15:35:08
26 11/23/98 15:50:46
27 11/23/98 16:06:25
28 11/23/98 16:22:05
29 11/23/98 16:37:42
30 11/23/98 16:53:35
• ANALYSIS BATCH SUMMARY
Analysis Batch # WLX10081123091701
Analysis Start Date/Time 11/23/98 09:17:00
Analysis Stop Date/Time 11/23/98 18:58:39
Work Order # 9811569
Pagel_
Instrument K1QQ..__
Analyst m&
Reviewer ~A=C~R~~~~~~~~
Project Sample ID Lab Sample ID Sample Type Analysis File #
sysblk Blank, System Xl001123-l
!CV Initial Calibration Verification Xl001123-2
BLK984146 Blank, Method Xl001123-3
LCS986339 Lab Control Sample Xl001123-4
LCSD986339 Lab Control Sample Duplicate Xl001123-5
9811249-0lA Sample X1001123-6
9811249-02A Sample X1001123-7
9811249-0lA Sample X1001123-8
9811249-0lA Matrix Spike X1001123-9
9811249-0lA Matrix Spike Duplicate X1001123-10
9811249-02A Sample X1001123-11
9811497-0lA Sample Xl001123-12
9811497-02A Sample Xl001123-13
9811497-03A Sample X1001123-14
9811497-0lA Matrix Spike X1001123-15
9811497-0lA Matrix Spike Duplicate X1001123-16
CCV Continuing Calibration Verification Xl001123-17
9811553-0lA Sample Xl001123-18
9811553-02A Sample Xl001123-19
9811553-03A Sample Xl001123-20.
9811553-04A Sample X1001123-21
9811553-05A Sample X1001123-22
9811553-06A Sample Xl001123-23
9811553-07A Sample Xl001123-24
9811553-08A Sample Xl001123-25
CCV Continuing Calibration Verification X1001123-26
1198HBWW225 9811569-0lA Sample X1001123-27
1198HBWW212 9811569-02A Sample Xl001123-28
1198HBWW212 9811569-03A Matrix Spike Xl001123-29
1198HBWW212 9811569-04A Matrix Spike Duplicate X1001123-30
•
11/30/98 12:49:55
Method IC EPA 300.0
Test Code XXIEWASF
Initial Calibration # ~N~A~~~~~~~­
Calibration Date ~~~~~~~~
Sequence/Analysis Time
31 11/23/98 17:09:15
32 11/23/98 17:24:53
33 11/23/98 17:40:20
34 11/23/98 17:56.:03
35 11/23/98 18:11:42
36 11/23/98 18:27:22
37 11/23/98 18:43:00
38 11/23/98 18:58:39
--
•
Project Sample
ll98HBWW213
1198HBWW213
1198HBWW213
1198HBWW214
ll98HBWW215
J.l98HJ:lWW;!?7
ll98HBWW228
A Ji ALYS I S BAT CB SUMMA R'Y (cont'd)
Analysis Batch# WLX10081123091701
Analysis Start Date/Time 11/23/98 09:17:00
Analysis Stop Date/Time 11/23/98 18:58:39
ID Lab Sample ID Sample Type
9811569-05A Sample
9811569-06A Matrix Spike
9811569-07A Matrix Spike
9811569-08A Sample
9811569-09A Sample
9811569-lOA Sample
9811569-llA Sample
Duplicate
Work Order # 9811569
Page _8 _
Instrument li!.QQ__
Analyst .Qg;
Reviewer A~C~R~~~~~~~~
Analysis File II
X1001123-31
Xl001123-32
Xl001123-33
X1001123-34
Xl001123-35
Xl001123-36
Xl001123-37
CCV Continuing Calibration Verification Xl001123-38
• •
• ll/30/98 12:49:55
Method IC EPA 300.0
Lab Sample ID
File ID
Project Sample
ID/Description
Specification# ~X~X=I=E-~
Analyte
• AHALYTICAL PROTOCOL SUMMARY
COMMBHTS/H.ARRATIVB
Flag Comment/Narrative Corrective Action
• Work Order # 9811569
Page _9_
11/30/98 12:49:55
••
QUALITY CORTROL BJ:CBPTIOR RB PORT
SUMMARY
QCER # Analysis Batch Number
981123-12 Xl00981123091700
- -
•
Work Order # 9811569
Page lQ_
•
• # 981123-12
QUALITY CONTROL EXCEPTION REPORT
LEVEL 2 -ANALYTICAL
REPORT COPY 9811569
Revised: 11/25/98
Analyst: DAVID CARRUTHERS
Batch #: X100981123091700
Prot Spec: AL/SPC034
Instrument: =D=X=l=O=O~-­
Matrix: Water ~...-...,...-.---
Date Analyzed: 11/23/98
Status: .Q
Analyte: S04 An al y sis File #:
Lab Sample ID:
9811569
Client ID: CSC:
9811553
9811497
HAM BEACH NC
HAM BEACH NC
HAM BEACH NC
JAL
JAL
JAL
9811249
SAMPLE PREPARATION:
PROBLEM IDENTIFICATION
Sample Went Dry
Loss of %
of Sample
Emulsion Formed
Blank Contamination
Instrument
Hold Time
MS/MSD Not Available
Instrument
Other (Describe) ·-----Comments:
SAMPLE ANALYSIS:
PROBLEM IDENTIFICATION
Surrogate Recovery
MS/MSD Recovery X
LCS/LCSD Recovery
MS/MSD Precision
LCS/LCSD Precision
Standard
Blank Contamination
Instrument
Hold Time
No MS/MSD Available
for Batch
Sample pH
Dil. Due to Hi-Level
Non-Target Analytes
Serial Dilution
Analytical Spike
Internal Standard
•
Other (Describe)
---
PROBABLE CAUSE
Matrix Effect
Instrument
Spiking Error
Contamination
Coelution
Unknown X
Other(Describe)
Project Sample ID:
CORRECTIVE ACTION TAKEN
Reprepare Sample
Sample Sent for Analysis _
Resample _
Other (Describe) ·-
CORRECTIVE ACTION TAKEN
Reprepare Sample
Reanalyze Sample
Reanalyze LCS/LCSD
Recalibrate Instrument
Analyze Out of Hold Time
Prepare New Standard
Flag Data X
Resample
Analyze by MSA
Perform Analytical Spike
No Action Required X
Level 3 QCER to Follow
Other (Describe)
Comments: The MS and MSD (9811497-0lAS and 9811497-0lASD) recoveries of
109% each are outside of tolerance. The LCS/LCSD recoveries
of 101% and 99% are acceptable. No action taken per protocol
specification.
T""'I...! -1---..! , ___ .&,_ ..! ---l""fl"'1r1 T _,_ T"'I __ -"'"-""'"
12/03/98 14:49:28
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STATE CERTIFICATIONS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma Water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
--
•
Work Order fl 9811570
Page _2_
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
12/03/98 14:49:28
Client HAMILTON BEACH
Facility WASHINGTON NC
Client Code HAM BEACH NC
Method TDS El60.l
Project Sample ID/Description
1198HBWW225
ll98HBWW225
ll98HBWW227
ll 98HBWW228 -
•
ANALYTICAL PROTOCOL SUMMARY
Extraction/Digestion
Lab Sample ID Test Code(s) Batch II
9811570-0lA TDSEWAOO NA
9811570-0lA TDSEWAOO NA
9811570-02A TDSEWAOO NA
9 8115 7 0-03A TDSEWAOO NA
•
Work Order tt 9811570
Page 4_
Analysis Batch II
WLTDS_81123120001
WLTDS_81123120001
WLTDS_81123120001
WLTDS_8112312000l
•
12/03/98 14:49:28
Method TDS E160.1
Test Code TDSEWAOO
Initial Calibration # ~N~A'--------~
Calibration Date ~--------
Sequence/Analysis Time
1 11/23/98 12:00:00
2 11/23/98 12:00:00
3 11/23/98 12:00:00
4 11/23/98 12:00:00
5 11/23/98 12:00:00
6 11/23/98 12:00:00
7 11/23/98 12:00:00
•
ANALYSIS BATCH SUMMARY
Analysis Batch # WLTDS 81123120001
Analysis Start Date/Time 11/23/98 12:00:00
Analysis Stop Date/Time 11/26/98 12:00:00
Project Sample ID Lab Sample ID Sample Type
BLK984150 Blank, Method
LCS986344 Lab Control Sample
LCSD986344 Lab Control Sample
1198HBWW2·25 9811570-0lA Sample
1198HBWW227 9811570-02A Sample
1198HBWW228 9811570-03A Sample
1198HBWW225 9811570-0lA Sample Duplicate
•
Duplicate
Work Order # 9811570
Page _6_
Instrument IQ§.___
Analyst ~
Reviewer ACR
Analysis File #
TDS1123-1
TDS1123-2
TDS1123-3
TDS1123-4
TDS1123-5
TDS1123-6
TDS1123-7
•
12/03/98 14:~
Method TDS El60.l
Lab Sample ID
File ID
Project Sample
ID/Description
Specif icationU TDSE
Analyte
ANALYTICAL .TOCOL SUMMARY
COHHBNTS/NARRATIVB
Flag Comment/Narrative Corrective Action
Work Order I~
Page _7_
12/01/98 13:31:01
Report RADIAN INTERNATIONAL
To 3200 E. CHAPEL HILL RD.
P.O. BOX 13000
Attention JIM NARKUNAS
Prepared _ __,,R.:::a.:::d""i"'a""n'"-"I""n"'t"'e::r~n~ac:::t:.:!io!::o~n~a~l'"',__:L!:L:::C,_
By --"'1~4~0~4~6._.:;:S.:::u~m~m~i~t'-"D~r~·~·'-"B~l~d~q~.'-"B'­
P. O. Box 201088
Austin, TX 78720-1088
CSC JALINDSEY
Project Sample
Description
1198HBWE02
TRIP BLANK
•
ID/
II 0 R I: 0 R. D B R. S UM MAR Y (Cont'd)
Client Code HAM BEACH NC
Client HAMILTON BEACH
Facility WASHINGTON,NC
Work ID WASHINGTON, NC
Case # ~N-A'---------­
SDG # ~N-A'--~~~~~~~
RAS # 80903AJAL
Lab Sample ID Test Code(s)
llB SPAREBOO
llC SPAREBOO
12A 826SWACM
12B SPAREBOO
•
Work Order # 9811619
Page L
RCN 650138.0602
New York ELAP ID #: 10915
Method Desciption
Spare Sample
Spare Sample -~ -
Volatile Organics by GC/MS
Spare Sample
•
12/01/98 13:~ if 0 R I: 0 R D B R C .B H T S
The standard Method 8260A surrogate tolerances are laboratory derived from
historical data. Project specific tolerances may differ.
Work Order II ~ Page _3_
12/01/98 13:31:01
State
Arkansas
California
Kansas
Louisiana
North Carolina
New Jersey
New York
Oklahoma
South Carolina
Utah
Wisconsin
•
STATB CBRTIPICATIORS
Agency
Department of Pollution Control and Ecology
California Environmental Laboratory Accreditation Program
Kansas Department of Health and Environment
Louisiana Department of Health and Hospitals
Department of Environment, Health and Natural Resources
New Jersey Department of Environmental Protection
New York State Department of Health
Oklahoma water Resources Board
Department of Health and Environmental Control
Utah Department of Health
Wisconsin Department of Natural Resources
Work Order U 9811619
Page i.._
Certification ID
2257
E-10165
LA 97-29
302
82005
10915
8720
82003001
RADC
99885260
•
12/01/.:31:01 ARALYTICAL .OCOL SUMMARY
FLAG DEFIRITIORS
Flag Definition
< DL Result less than stated Detection Limit and greater than or equal to zero.
Analyte concentration not available for this analysis. NA
NC
ND
NR
NS
RPD and/or \ Recovery not calculated. See Narrative for explanation.
Not detected. No instrument response for analyte or result less than zero.
Not reported. Result greater than or equal to stated Detection Limit and less than specified Reporting Limit.
Analyte not spiked.
A Presence of hydrocarbon mix eluting in the Lube Oil range. The pattern does not match that of Lube Oil.
B Analyte detected in method blank at concentration greater than the Reporting Limit (and greater than zero) .
C Confirming data obtained using second GC column or GCMS.
D Presence of hydrocarbon mix eluting in the Diesel range. The pattern does not match that of Diesel.
E Analyte concentration exceeded calibration range.
F Interference or coelution suspected. See Narrative for explanation.
G Presence of hydrocarbon mix eluting in the Jet Fuel range. The pattern does not match that of Jet Fuel.
H Presence of analyte previously confirmed by historical data.
I Analyte identification suspect. See Na~rative for explanation.
J Result is less than stated Detection Limit but greater than or equal to specified Reporting Limit.
K Peak did not meet method identification criteria. Analyte not detected on other GC column.
M
p
Result modified from previous Report.
Analyte not confirmed. Results from
See Narrative for explanation.
primary and secondary GC columns differ by greater than a factor of 3.
Q QC result does not meet tolerance in Protocol Spe.cification.
R Result reported elsewhere.
S Analyte concentration obtained using Method of Standard Additions (MSA) .
T Second column confirmational analysis not performed.
X See Narrative for explanation.
Y See Narrative for explanation.
Z See Narrative for explanation.
Work Order # 9811619
Page L •
12/01/98 13:31:01
Client HAMILTON BEACH
Facility WASHINGTON.NC
Client Code HAM BEACH NC
Method Volatile Organics SW8260B
Project Samplf: ID/Descripticn
1198HBWE02
1198HBWW212
1198HBWW213
1198HBWW213
1198HBWW214
1198HBWW214
1198HBWW215
1198HBWW215
1198HBWW227
1198HBWW227
1198HBWW228
1198HBWW228
1198HBWW228
1198HBWW228
TRIP BLANK
•
!.ab
-
9811619-llB
9811619-0lA
9811619-04A
9811619-04B
9811619-0?A
9811619-0?B
9811619-08A
9811619-08B
9811619-09A
9811619-09B
9811619-lOA
9811619-lOB
9811619-lOC
9811619-lOC
9811619-126
AHALYT:CCAL PROTOCOL SUMMARY
Extraction/Digestion
Samrle IC Test Code(s) Batch #
-------·-----
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
826SWACM NA
•
Work Order # 9811619
Page _6 _
Analysis Batch #
MSMSDC81123170401
MSMSDB81121035401
MSMSDB81121035401
MSMSDC81123170401
MSMSDB81121035401
MSMSDC81123170401
MSMSDB81121035401
MSMSDC81123170401
MSMSDBa-112~035401
MSMSDC81123170401
MSMSDB81121035401
MSMSDC81123170401
MSMSDC81123170401
MSMSDC81124183801
MSMSDC81123170401
·-
•
12/01/98 13:31:01
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
l,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-l,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodif luoromethane
1,1-Dichloroethane
1,2-Dichloroethane
l,l-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
•
1198H8WE02
9811619-llB
Cl123822
11/18/98 13:30
00:00:00
11/24/98 02:12:00
1
Water
ug/L
received
Cone. DL
ND 0.0933
ND 0.157
ND 0.0876
ND 0.0905
ND 0.297
ND 0.312
ND 1.43
ND 0.0762
ND 0.0875
ND 0.205
ND 0.286
ND 0.334
ND 0.328
ND 0.352
ND 0.0675
ND 0.0363
ND 0.0989
ND 0.127
ND 0.0465
ND 0.0835
R. B S ULT S S UM MAR Y (Cont'd)
1198H8WW212 1198H8WW213
9811619-0lA 9811619-04A
81121816 81121819
11/18/98 09:00 11/18/98 09:30
00:00:00 00:00:00
11/21/98 10:34:00 11/21/98 11:59:00
l l
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.0480 0.793 0.0480
-
ND 0.0605 ND 0.0605
ND 0.0521 ND 0.0521
ND 0.0605 ND 0.0605
ND 0.0881 ND 0.0881
ND 0.0538 ND 0.0538
ND 0.194 ND 0.194
ND 0.0769 ND 0.0769
ND 0.0435 ND 0.0435
ND 0.118 ND 0 .118
ND 0.412 ND 0.412
ND 0.0733 0.642 0.0733
ND 0.0469 ND 0.0469
ND 0.0466 ND 0.0466
ND 0.176 ND 0.176
2.56 ' 0.0576 241 ER 0.0576
0.698 0.0348 7.02 0.0348
14.3 0.0715 436 ER 0. 0715
0.188 0.0383 39.3 0.0383
ND 0. 0618 2.22 0.0618
•
Work Order # 9811619
Page _8_
1198H8WW213
9811619-048
Cll23824
11/18/98 09:30
00:00:00
11/24/98 03:08:00
20
Water
ug/L
received
Cone. DL
ND 1. 87
ND 3.14
ND 1. 75
ND 1. 81
ND 5.94
ND 6.24
ND 28.6
ND 1. 52
ND 1. 75
ND 4.10
ND 5. 72
ND 6.68
ND 6.56
ND 7.04
ND 1.35
351 o. 726
8.37 l. 98
867 2.54
43.8 0.930
ND 1.67
•
12/01/98 13:31:01
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
a-Xylene
•
1198HBWE02
9811619-llB
Cll23822
11/18/98 13:30
00:00:00
11/24/98 02:12:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.194
0.158
0.0970
0.340
o. 920
0.141
0.350
0.333
0.0965
0.0881
0.219
0.182
0.253
0.113
0.205
0.205
0.0749
0.162
0.500
0.259
RBS ULT S SUMMARY (Cont'd)
1198HBWW212
9811619-0lA
Bll21816
11/18/98 09:00
00:00:00
11/21/98 10:34:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.579
ND
ND
ND
ND
ND
ND
4.48
ND
ND
•
DL
0.0578
0. 0848
0.102
0.0515
0.489
0.0522
0.0896
0.113
0.0658
0.0602
0. 0892
0.0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0. 0414.
1198HBWW213
9811619-04A
Bll21819
11/18/98 09:30
00:00:00
11/21/98 11:59:00
l
Water
ug/L
received
Cone.
ND
ND
ND
61.3
7.63
1.48
ND
ND
1.09
6.03
407 ER
0.575
ND
ND
ND
ND
ND
38.7
1. 57
3.43
DL
0.0578
0.0848
0.102
0.0515
0 .489
0.0522
0.0896
0.113
0.0658
0.0602
0. 0892
0.0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0. 0414
Work Order # 9811619
Page 1.Q._
1198HBWW213
9811619-04.B
Cll23824
11/18/98 09:30
00:00:00
11/24/98 03:08:00
20
Water
ug/L
received
Cone.
ND
ND
ND
52.l
ND
ND
ND
ND
ND
5.25
515
ND
ND
ND
ND
ND
ND
47.2
ND
3.43 J
DL
3.88
3-.16
1. 94
6.80
18.4
2.82
7.00
6.66
1. 93
1. 76
4.38
3.64
5.06
2.26
4.10
4.10
1.50
3.24
10.0
5.18
•
12/01/98 13:31:01
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
A:t:etonitrile
Acrolein
Acrylonitrile
Benzene
l-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
•
1198HBWW214
9811619-07A
81121822
11/18/98 10:15
00:00:00
11/21/98 13:24:00
1 .
Water
ug/L
received
Cone. DL
ND 0.413
'ND 5. 72
ND 7.17
ND 0.333
ND 0.0375
ND 0.0928
ND 0.0624
ND 0.0828
ND 0.0634
ND 0.0547
ND 0. 0467
ND 0.222
ND 0.116
ND 0.0782
ND 0.0823
ND 0.0547
ND 0.0576
ND 0.0719
ND 0.0453
ND 0.0441
R B S ULT S S UM MAR Y (Cont'd)
1198H8WW214 ll 98H8WW215
9811619-078 9811619-08A
Cll23820 81121823
11/18/98 10:15 11/18/98 10 :40
00:00:00 00:00:00
11/24/98'01:17:00 11/21/98 13:52:00
l 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.809 ND 0.413
·ND 4.57 -ND 5.n
ND 4 .14 ND 7.17
ND 0.780 ND 0.333
0.172 0.0647 ND 0.0375
ND 0.104 ND 0. 0928
ND 0.382 ND 0.0624
ND 0.0935 ND 0.0828
ND 0.104 ND 0.0634
ND 0.178 ND 0.0547
ND 0.124 ND 0.0467
ND 0.231 ND 0.222
ND 0.113 ND 0.116
ND 0.156 ND 0.0782
ND 0.164 ND 0.0823
ND 0.132 ND 0.0547
ND 0.143 ND 0.0576
ND 0.0420 ND 0.0719
ND 0.189 ND 0.0453
0.485 0.0977 ND 0. 0441
•
Work Order # 9811619
Page g_
1198HBWW215
9811619-088
Cl123821
11/18/98 10:40
00:00:00
11/24/98 01:44:00
1
Water
ug/L
received
Cone. DL
ND 0.809
ND 4.57
ND 4.14
ND 0.780
0.0963 0.0647
ND 0.104
ND 0.382
ND 0.0935
ND 0 .104
ND 0.178
ND 0.124
ND 0.231
ND 0.113
ND 0.156
ND 0.164
ND 0.132
ND 0.143
ND. 0.0420
ND 0.189
ND 0.0977
•
12/01/98 13:31:01
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBKJ
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
•
1198HBWW214
9811619-07A
Bll21822
11/18/98 10:15
00:00:00
11/21/98 13:24:00
1
Water
ug/L
received
Cone. DL
ND 0.0631
ND 0.0397
ND 0.0769
ND 0.0444
ND 0.0421
ND 0.0643
ND 0.0361
ND 0. 0928
ND 0.115
ND 0.232
ND 0.0291
ND 0.0661
ND 0.106
ND 0.130
ND 0.0365
ND 0.160
0.255 B 0.137
ND 0.578
ND 0.390
ND 0.0577
RESULTS SUMMARY (Cont'd)
1198HBWW214 1198HBWW215
9811619-07B 9811619-08A
C1123820 Bll21823
11/18/98 10:15 11/18/98 10 :40
00:00:00 00:00:00
11/24/98 01:17:00 11/21/98 13:52:00
1 l
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 0.146 ND 0.0631
ND o-. 0"618 ND 0.0397
ND 0.0699 ND 0.0769
ND 0.159 ND 0.0444
ND 0.116 ND 0.0421
ND 0.0400 ND 0.0643
ND 0.0612 ND 0.0361
ND 0.234 ND 0.0928
ND 0.554 ND 0.115
ND 0.737 ND 0.232
ND 0.119 ND 0.0291
ND 0.255 ND 0.0661
0.181 0.136 ND 0.106
ND 0.124 ND 0.130
ND 0.0646 0.895 0.0365
ND 0.137 ND 0.160
0.289 B 0.218 0.219 B 0.137
ND 0.234 ND 0.578
ND 0.580 ND 0.390
ND 0.239 ND 0.0577
·• I.~ I
•
Work Order # 9811619
Page !!_
1198HBWW215
9811619-08B
Cll23821
11/18/98 10 :40
00:00:00
11/24/98 01:44:00
1
Water
ug/L
received
Cone. DL
ND 0.146
ND 0-.-0618
ND 0.0699
ND 0.159
ND 0.116
ND 0.0400
ND 0.0612
0.0601 J 0.234
ND 0.554
ND 0.737
ND 0.119
ND 0.255
ND 0.136
ND 0.124
1.22 0.0646
ND 0.137
0.212 BJ 0.218
ND 0.234
ND 0.580
ND 0.239
•
l2/0l~3:3l:Ol
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
l,l,l,2-Tetrachloroethane
l,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
m&p-Xylene
a-Xylene
ll98HBWW214
98ll619-07A
81121822
ll/18/98 10:15
00:00:00
11/21/98 13:24:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.587 R
ND
ND
ND
ND
ND
ND
7.04
ND
ND
DL
0.0578
0.0848
0.102
0.0515
0.489
0.0522
0.0896
0.113
0.0658
0.0602
0.0892
0.0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0.0414
R B S ULT S • MARY (Cont'd)
ll98HBWW214
9811619-078
Cll23820
11/18/98 10:15
00:00:00
11/24/98 01:17:00
l
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.169 J
ND
ND
ND
ND
ND
ND
8.84
ND
ND
DL
0.194
0.158
0.0970
0.340
0. 920
0.141
0.350
0.333
0.0965
0.0881
0.219
0.182
0.253
0.113
0.205
0.205
0.0749
0.162
0.500
0.259
1198HBWW215
9811619-08A
81121823
11/18/98 10:40
00:00:00
11/21/98 13:52:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
45.9
ND
ND
ND
ND
ND
0.322 R
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
0.0578
0. 0848
0.102
0.0515
0.489
0.0522
0.0896
0.113
0.0658
0.0602
0.0892
0. 0473
0.0514
0.0986
0.0952
0.0800
0.0929
0.0639
0.115
0. 0414
Work Order # 9811619
Page 12_
ll98H8WW215
9811619-088
Cll23821
11/18/98 10:40
00: 00.: 00
11/24/98 01:44:00
1
Water
ug/L
received
Cone.
ND
ND
ND
ND
58.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.381
0.0885 J
ND
DL
0.194
0.158
0.0970
0.340
0.920
0.141
0.350
0.333
0.0965
o.000i
0.219
0.182
0.253
0.113
0.205
0.205
0.0749
0.162
0.500
0.259
12/01/98 13:31:01
Method Volati J ,. Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
Fil!'l ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
•
1198HBWW214
9811619-07A
81121822
11/18/98 10:15
00:00:00
11/21/98 13:24:00
1
Water
ug/L
received
Cone.
Recovery
%
95
94
96
DL
R B S U L T S S U M M A R Y (Cont'd)
119BHBWW214
9811619-078
Cl123820
11/18/98 10:15
00:00:00
11/24/98 01:17:00
1
Water
ug/L
received
Cone.
Recovery
%
96
104
100
•
DL
1198H8WW215
9811619-08A
81121823
11/18/98 10:40
00:00:00
11/21/98 13:52:00
1
Water
ug/L
received
Cone.
Recovery
\
96
96
98
DL
Work Order # 9811619
Page 1.§_
1198H8WW215
9811619-088
Cl123821
11/18/98 10:40
00:00:00
11/24/98 01:44:00
1
Water
ug/L
received
Cone.
Recovery
%
96
106
101
DL
•
12/01~:31:01
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Al_lalyte
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Benzene
1-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
ll98HBWW227
98ll619-09A
81121824
11/18/98 13:00
00:00:00
11/21/98 14:21:00
1
Water
ug/L
received
Cone.
29.9
ND
ND
ND
0.668
ND
ND
ND
ND
ND
ND
42.5
0.437
ND
ND
0.573
ND
ND
ND
2.14
DL
0.413
5.72
7.17
0.333
0.0375
0. 0928
0.0624
0.0828
0.0634
0.0547
0.0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0. 0719
0. 0453
0. 0441
RESULTS .MARY
ll98HBWW227
9811619-098
Cll23825
11/18/98 13:00
00:00:00
11/24/98 03:37:00
100
Water
ug/L
received
Cone.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DL
80.9
457
414
78.0
6.47
10.4
38.2
9.35
10.4
17.8
12.4
23.1
11.3
15.6
16.4
13.2
14.3
4.20
18.9
9.77
(Cont'd)
1198HBWW228
9811619-lOA
81121825
11/18/98 13:20
00:00:00
11/21/98 14:49:00
1
Water
ug/L
received
Cone.
307 EY
ND
ND
ND
51.3
ND
ND
ND
ND
ND
ND
21. 3
15.6
5.27
ND
ND
42.2
ND
ND
74.7
DL
0 .413
5. 72
7.17
0.333
0.0375
0.0928
0.0624
0.0828
0.0634
0.0547
0. 0467
0.222
0.116
0.0782
0.0823
0.0547
0.0576
0. 0719
0.0453
0. 0441
Work Order # 9811619
Page ll_
1198HBWW228
•
9811619-lOB
Cll23826
11/18/98 13:20
00:00:00
11/24/98 04:04:00
500
Water
ug/L
received
Cone.
ND
ND
ND
ND
71.2
ND
ND
ND
ND
ND
ND
806
ND
ND
ND
ND
ND
ND
ND
ND
DL
404
2280
2070
390
32.4
52.0
191
46.8
52. o.
89.0
62.0
116
56.5
78.0
82.0
66.0
71.5
21. 0
94.5
48.8
12/01/98 13:31:01
Method Volatile Organics SW82608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
---
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1, 4-Dichl~:;;o-2-l..mtene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
•
1198H8WW227
9811619-09A
81121824
11/18/98 13:00
00:00:00
11/21/98 14:21:00
l
Water
ug/L
received
Cone. DL
1.64 0.0480
ND 0.0605
ND 0.0521
ND 0.0605
ND 0.0881
ND 0.0538
ND 0.194
ND 0.0769
ND 0.0435
ND 0.118
ND 0.412
ND 0.0733
ND 0.0469
ND 0.0466
ND 0.176
1070 ER 0.0576
19.5 0.0348
373 ER 0. 0715
147 ER 0.0383
3.66 0.0618
R B S ULT S S U M MAR Y (Cont'd)
1198H8WW227 1198H8WW228
9811619-098 9811619-lOA
Cll23825 81121825
11/18/98 13:00 11/18/98 13 :20
00:00:00 00:00:00
11/24/98 03:37:00 11/21/98 14:49:00
100 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 9.33 12.8 0. 0480
ND 15.7 ND 0. 06"05
ND 8.76 ND 0.0521
ND 9.05 ND 0.0605
ND 29. 7 ND 0.0881
ND 31.2 ND 0.0538
ND 143 ND 0.194
ND 7.62 ND 0.0769
ND 8.75 ND 0.0435
ND 20.5 ND 0.118
ND 28.6 ND 0.412
NI/ 33.4 ND 0.0733
ND 32.8 ND 0.0469
ND 35.2 ND 0.0466
ND 6.75 ND 0.176
4620 3.63 3490 ER 0.0576
31.l 9.89 ND 0,0348
705 12.7 4530 ER 0.0715
228 4.65 1390 ER 0.0383
ND 8.35 24.2 0.0618
•
Work Order tt 9811619
Page 1:.!L
1198H8WW228
9811619-108
C1123826
11/18/98 13:20
00:00:00
11/24/98 04:04:00
500
Water
ug/L
received
Cone. DL
ND 46.6
ND 78.5
ND 43.8
ND 45.2
ND 148
ND 156
ND 715
ND 38.1
ND 43.8
ND 102
ND 143
ND 167
ND 164
ND 176
ND 33.8
24100 18.2
203 49 .4
78000 ER 63.5
3330 23.2
ND 41. 8
•
12/01/98 13:31:01
Method Volatile. urqa1:.ics SWB2608
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Styrene
-r~ 1, 1, 2-Tetrach-l:oroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorornethane
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trirnethylbenzene
1,3,5-Trirnethylbenzene
Vinyl acetate
Vinyl chloride
rn&p-Xylene
a-Xylene
•
1198H8WW227
9811619-09A
81121824
11/18/98 13:00
00:00:00
11/21/98 14:21:00
1
Water
ug/L
received
Cone. DL
ND 0.0578
ND-0-. 0848
ND 0.102
1.41 0.0515
ND 0.489
29.6 0.0522
ND 0.0896
ND 0.113
1050 ER 0.0658
3.20 0.0602
458 ER 0.0892
ND 0. 0473
ND 0.0514
ND 0.0986
10.8 0.0952
3.37 0,0800
ND 0.0929
5. 70 0.0639
8.78 0.115
8.91 0. 0414
R B S ULT S S U MM AR Y (Cont'd)
1198H8WW227 1198H8WW228
9811619-098 9811619-lOA
Cl123825 81121825
11/18/98 13:00 11/18/98 13 :20
00:00:00 00:00:00
11/24/98 03:37:00 11/21/98 14:49:00
100 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 19.4 ND 0.0578
ND 15.8 --0.810 0.0848
ND 9.70 0.688 0.102
ND 34.0 30.5 0.0515
ND 92.0 ND 0.489
38.8 14.l 626 ER 0.0522
ND 35.0 ND 0. 0896
ND 33.3 ND 0.113
3200 9.65 12600 ER 0.0658
ND 8.81 49.3 0.0602
810 21. 9 4200 ER 0.0892
ND 18.2 12.7 0.0473
ND 25.3 ND 0.0514
ND 11.3 ND 0.0986
14.6 J 20.5 607 ER 0.0952
ND 20.5 226 ER 0.0800
ND 7.49 ND 0.0929
ND 16.2 258 ER 0.0639
8.86 J 50.0 753 ER 0.115
ND 25.9 700 ER 0.0414
Work Order # 9811619
Page a9-
--
1198H8WW228
9811619-108
Cll23826
11/18/98 13:20
00:00,00
11/24/98 04:04:00
500
Water
ug/L
received
Cone. DL
ND 97.0
ND 79.0 ---
ND 48.5
ND 170
ND 460
1460 70.5
ND 175
ND 166
146000 ER 48.2
ND 44.0
22800 110
ND 91.0
ND 126
ND 56.5
1270 102
309 102
ND 37.4
314 81. 0
1540 250
1330 130
•
12/01/98 13:31:01
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Acetone
Acetonitrile -
Acrolein
Acrylonitrile
Benzene
1-Bromo-2-chloroethane
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromof orm
Bromomethane
2-Butanone(MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
•
1198HBWW228
9811619-lOC
Cll23830
11/18/98 13:20
00:00:00
11/24/98 15:24:00
1000
Water
ug/L
received
Cone. DL
ND 809
ND 4570
ND 4140
ND 780
76.6 64.7
ND 104
ND 382
ND 93.5
ND 104
ND 178
ND 124
ND 231
ND 113
ND 156
ND 164
46. 5 BJ 132
ND 143
ND 42.0
ND 189
ND 97.7
R B S ULT S S UM MAR Y (Cont'd)
1198HBWW22B TRIP BLANK
9811619-lOC 9Bll619-12B
Cll24806 Cll23823
11/18/98 13:20
00:00:00 00:00:00
11/24/98 20:28:00 11/24/98 02:39:00
5000 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 4040 ND 0.809
--ND 22800 ND --4.57
ND 20700 ND 4.14
ND 3900 ND 0.780
ND 324 ND 0.0647
ND 520 ND 0.104
ND 1910 ND 0.382
ND 468 ND 0.0935
ND 520 ND 0.104
ND 890 ND 0.178
ND 620 ND 0.124
ND 1160 ND 0.231
ND 565 ND 0.113
ND 780 ND 0.156
ND 820 ND 0.164
ND 660 ND 0.132
ND 715 ND 0.143
ND 210 ND 0. 0420
ND 945 ND 0.189
ND 488 ND 0.0977
•
Work Order U 9811619
Page ~
Cone. DL
------
•
12/01/.31:01
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1198HBWW228
9811619-lOC
Cll23830
11/18/98 13:20
00:00:00
11/24/98 15:24:00
1000
Water
ug/L
received
Cone. DL
ND 93.3
ND 157
ND 87.6
ND 90.5
ND 297
ND 312
ND 1430
Nb 76.2
ND 87.5
ND 205
ND 286
ND 334
ND 328
ND 352
ND 67.5
25900 36.3
246 98.9
96500 127
3510 46.5
ND 83.5
RESULTS S.ARY
1198HBWW228
9811619-lOC
Cll24806
11/18/98 13:20
00:00:00
11/24/98 20:28:00
5000
Water
ug/L
received
Cone. DL
ND 466
ND 785
ND 438
ND 452
ND 1480
ND 1560
ND 7150
ND 381
ND 438
ND 1020
ND 1430
ND 1670
ND 1640
ND 1760
ND 338
25300 182
ND 494
102000 635
3470 232
ND 418
(Cont'd)
TRIP BLANK
9811619-128
C1123823
00:00:00
11/24/98 02:39:00
1
Water
ug/L
received
Cone. DL
ND 0.0933
ND 0.157
ND 0.0876
ND 0.0905
ND 0.297
ND 0.312
ND 1.43
ND 0.0762
ND 0.0875
ND 0.205
ND 0.286
ND 0.334
ND 0.328
ND 0.352
ND 0.0675
ND 0.0363
ND 0.0989
ND 0.127
ND 0.0465
ND 0.0835
Work Order# 9811619
Page ll_
Cone.
•
--
DL
12/01/98 13:31:01
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl methacrylate
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
Iodomethane
Isopropylbenzene
p-Isopropyltoluene
Methyl methacrylate
Methyl t-butyl ether
4-Methyl-2-pentanone(MIBK)
Methylene chloride
Naphthalene
Propanenitrile
n-Propylbenzene
•
1198HBWW228
9811619-lOC
Cll23830
11/18/98 13:20
00:00:00
11/24/98 15:24:00
1000
Water
ug/L
received
Cone. DL
ND 146
ND 61.8-
ND 69.9
ND 159
ND 116
ND 40.0
ND 61.2
608 234
ND 554
ND 737
ND 119
ND 255
ND 136
ND 124
ND 64.6
ND 137
212 BJ 218
ND 234
ND 580
206 J 239
R E S U L T S S U M M A R Y (Cont'd)
1198HBWW228 TRIP BLANK
9811619-lOC 9811619-128
Cll24806 Cll23823
11/18/98 13:20
00:00:00 00:00:00
11/24/98 20:28:00 11/24/98 02:39:00
5000 1
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
ND 730 ND 0.146
ND 309 ND 0-.-061-0
ND 350 ND 0.0699
ND 795 ND 0.159
ND 580 ND 0.116
ND 200 ND 0.0400
ND 306 ND 0.0612
446 J 1170 ND 0.234
ND 2770 ND 0.554
ND 3680 ND 0.737
ND 595 ND 0.119
ND 1280 ND 0.255
ND 680 ND 0.136
ND 620 ND 0.124
ND 323 ND 0.0646
ND ' 685 ND 0.137
1100 B 1090 0.423 B 0.218
ND 1170 ND 0.234
ND 2900 ND 0.580
ND 1200 ND 0.239
•
Work Order # 9811619
Page .£1._
Cone. DL
-----
•
12/01/98 13:31:01
Method Volatile Organics SW8260B
Test Code 826SWACM
Project Sample ID:
Lab ID:
File ID:
Date Collected:
Date Prepared:
Date Analyzed:
Dilution Factor:
Matrix:
Units:
Report as:
Column:
Analyte
Surrogate(s)
1,4-Bromofluorobenzene
l,2-Dichloroethane-d4
Toluene-dB
•
ll98HBWW228
9811619-lOC
Cll23830
11/18/98 13:20
00:00:00
11/24/98 15:24:00
1000
Water
ug/L
received
Cone. DL
Recovery
\
96
100
103
RBS ULT S SUH HAR Y (Cont'd)
ll98HBWW228 TRIP BLANK
9811619-lOC 9811619-128
Cll24806 Cll23823
11/18/98 13:20
00:00:00 00:00:00
11/24/98 20:28:00 11/24/98 02:39:00
5000 l
Water Water
ug/L ug/L
received received
Cone. DL Cone. DL
Recovery Recovery
\ %
97 95
103 105
103 102
•
Work Order tt 9811619
Page ~
.
Cone.
Recovery
%
DL
•
12/01/.:31:01
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDB981003000000
Calibration Date ~l~0~/~0~3~/~9~8---~
Sequence/Analysis Time
1 11/21/98 03:26:00
2 11/21/98 03:54:00
3 11/21/98 03:54:00
4 11/21/98 04:22:00
5 11/21/98 04:50:00
6 11/21/38 05:18:00
7 11/21/98 05:46:00
8 11/21/98 06:14:00
9 11/21/98 06:43:00
10 11/21/98 07:11:00
11 11/21/98 07:39:00
12 11/21/98 08:08:00
13 11/21/98 08:38:00
14 11/21/98 09:07:00
15 11/21/98 09:37:00
16 11/21/98 10:06:00
17 11/21/98 10:34:00
18 11/21/98 11:03:00
19 11/21/98 11:3l:OQ
20 11/21/98 11:59:00
21 11/21/98 12:27:00
22 11/21/98 12:55:00
23 11/21/98 13:24:00
24 11/21/98 13:52:00
25 11/21/98 14:21:00
26 11/21/98 14:49:00
27 11/21/98 15:18:00
28 11/21/98 15:46:00
AlllALJ:SIS ii.A.SUMMARY
Analysis Batch # MSMSDB81121035401
Analysis Start Date/Time 11/21/98 03:54:00
Analysis Stop Date/Time 11/21/98 15:46:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
Work Order tt 98J1619
Page TI_
Instrument !:l§!2!!..__
Analyst ~
Reviewer ~A;.;.P.=S ____ _
Analysis
Bll21801
Bll21802
File #
VSTDCAL Continuing Calibration Verification Bll21802
LCS986017 Lab Control Sample Bll21803
LCSD986018 Lab Control Sample Duplicate Bll21804
BLK983943 Blank, Method Bll21805
9811583-0lA Sample Bll21806
9811583-02A Sample . Bll21807
9811555-05A Sample Bll21808
9811555-07B Sample Bll21809
9811555-08B Sample Bll21810
9811555-02B Sample Bll21811
9811555-04B Sample Bll21812
9811555-03B Sample Bll21813
9811555-06B Sample Bll21814
9811414-06B Sample Bll21815
1198HBWW212 9811619-0lA Sample Bll21816
1198HBWW212 9811619-02A Matrix Spike Bl121817
1198HBWW212 9811619-03A Matrix Spike Duplicate Bl121818
1198HBWW213 9811619-04A Sample Bll21819
1198HBWW213 9811619-05A Matrix Spike Bl121820
1198HBWW213 9811619-06A Matrix Spike Duplicate Bll21821
1198HBWW214 9811619-07A Sample Bl121822
1198HBWW215 9811619-08A ' Sample Bl121823
1198HBWW227 9811619-09A Sample Bl121'824
1198HBWW228 9811619-lOA Sample Bll21825
1198HBWE02 9811619-llA Sample Bll21826
TRIP BLANK 9811619-l2A Sample 81121827
•
12/01/98 13:31:01
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDC980921000000
Calibration Date -0~9~/~2~1~/~98""-~~~~
Sequence/Analysis Time
l 11/23/98 16:36:00
2 11/23/98 17:04:00
3 11/23/98 17:04:00
4 11/23/98 17:31:00
5 11/23/98 17:59:00
6 11/23/98 18:26:00
7 11/23/98 18:53:00
8 11/23/98 19:21:00
-
9 11/23/98 19:48:00
10 11/23/98 20:15:00
11 11/23/98 2'0:43:00
12 11/23/98 21:10:00
13 11/23/98 21:38:00
14 11/23/98 22:05:00
15 11/23/98 22:33:00
16 11/23/98 23:00:00
17 11/23/98 23:27:00
18 11/23/98 23:55:00
19 11/24/98 00:22:00
20 11/24/98 00:49:00
21 11/24/98 01:17:00
22 11/24/98 01:44:00
23 11/24/98 02:12:00
24 11/24/98 02:39:00
25 11/24/98 03:08:00
26 11/24/98 03:37:00
27 11/24/98 04:04:00
28 11/24/98 14:02:00
29 11/24/98 14:29:00
30 11/24/98 14:29:00
•
Project ~ample
1198HBWW214
1198HBWW215
ll98HBWE02
TRIP BLANK
1198HBWW213
1198HBWW227
1198HBWW228
ANALYSIS BATCH SUMMARY
Analysis Batch # MSMSDC81123170401
Analysis Start Date/Time 11/23/98 17:04:00
Analysis Stop Date/Time 11/24/98 15:24:00
ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
VSTDCAL Continuing Calibration
LCS985987 Lab Control Sample
Work Order # 9811619
Page £L
Instrument !1§!2f..._
Analyst !:1JIB
Reviewer -A~P~S~~~~~~~~
Analysis File #
Cll23801
Cll23802
Verification Cll23802
Cll23803
LCSD985988 Lab Control Sample Duplicate Cll23804
BLK983928 Blank, Method Cl123805
9811342-0lA Sample Cll23806
9811342-02A Sample Cll23807
9811342-03A Matrix Spike C1123808
9811342-04A Matrix Spike Duplicate Cll23809
9811342-05A Sample Cll23810
9811342-06A Sample Cll23811
9811342-07A Sample C1123812
9811342-08A Sample Cll23813
9811342-09A Sample Cll23814
9811342-lOA Sample C1123815
9811555-08C Sample Cll23816
9811555-03C Sample C1123817
9811555-0GC Sample Cll23818
9811423-02B Sample Cll23819
9811619-07B Sample Cll23820
9811619-08B Sample Cll23821
9811619-llB Sample Cll23822
9811619-12B Sample Cll23823
9811619-04B Sample Cll23824
9811619-09B Sample C1123825
9811619-lOB Sample Cll23826
SB Blank, System Cll23827
BFB GC/MS tune files Cll23828
VSTDCAL Continuing Calibration Verification Cll23828
• •
12/01~:31:01
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDC980921000000
Calibration Date ~0~9·/~2~1./~9~8~~~~-
Sequence/Analysis Time
31 11/24/98 14:56:00
32 11/24/98 15:24:00
AR ALY S I S BA. S UM MAR y (cont'd)
Analysis Batch # MSMSDC81123170401
Analysis Start Date/Time 11/23/98 17:04:00
Analysis Stop Date/Time 11/24/98 15:24:00
Project Sample ID Lab Sample ID Sample Type
9811555-06C Sample
1198HBWW228 9811619-lOC Sample
Work Order # 9811619
Page £2.._
Instrument !::12!2f__
~alyst !:1§B
Reviewer ~A~P~S~~~~~~~~-
Analysis File #
Cl123829
Cll23830
•
12/01/98 13:31:01
Method Volatile Organics SW8260B
Test Code 826SWAOO
Initial Calibration # MSDC980921000000
Calibration Date ~0~9~/~2=1~/~9~8~~~~
Sequence/Analysis Time
l 11/24/98 18:10:00
2 11/24/98 18:38:00
3 11/24/98 18:38:00
4 11/24/98 19:06:00
5 11/24/98 19:33:00
6 11/24/98 20:01:00
7 11/24/98 20:28:00
8 11/24/98 20:56:00
9 11/24/98 21:23:00
10 11/24/98 21:50:00
11 11/24/98 22:18:00
12 11/24/98 22:45:00
13 11/24/98 23:13:00
14 11/24/98 23:40:00
15 11/25/98 00:07:00
16 11/25/98 00:35:00
17 11/25/98 01:02:00
18 11/25/98 01:29:00
19 11/25/98 01:57:00
20 11/25/98 02:24:00
21 11/25/98 02:52:00
22 11/25/98 03:19:00
23 11/25/98 03:46:00
24 11/25/98 04:14:00
25 11/25/98 04:41:00
26 11/25/98 05:08:00
27 11/25/98 05:36:00
28 11/25/98 06:03:00
•
A Jll A L Y S I S B A T C H S U M M A R Y
Analysis Batch # MSMSDC81124183801
Analysis Start Date/Time 11/24/98 18:38:00
Analys~s Stop Date/Time 11/25/98 06:03:00
Project Sample ID Lab Sample ID Sample Type
SB Blank, System
BFB GC/MS tune files
Work Order # 9811619
Page 1Q_
Instrument ~
Analyst !:!!IB
Reviewer ~A~PS:;_~~~~~~~-
Analysis. File #
C1124801
C1124802
VSTDCAL Continuing Calibration Verification C1124802
LCS985989 Lab Control Sample Cll24803
LCSD985990 Lab Control Sample Duplicate Cl124804
BLK983929 Blank, Method Cll24805
1198HBWW228 9811619-lOC Sample C1124806
9811681-0lA Sample Cll24807
98116.81-02A Sample C:Ll24.8.0 8
9811681-03A Sample C1124809
9811631-0lA Sample C1124810
9811631-02A Sample C1124811
9811631-03A Sample Cll24812
9811715-0lA Sample Cll24813
9Bll715-02A Sample Cl124814
98ll 715-03A Sample Cll24815
98ll 715-04A Sample Cll24816
9811615-0lA Sample Cll24817
9811615-02A Sample Cll24818
9811615-03A Sample Cll24819
9811615-04A Sample Cll24820
9811615-05A Sample Cll24821
9811615-06A Sample Cll24822
9811615-07A Sample Cll24823
9811615-08A Matrix Spike Cll24824
9811615-09A Matrix Spike Duplicate Cll24825
9811615-lOA Sample C1124826
9811615-llA Sample Cll24827
• .,
12/01/98 1~1
Method Volatile Organics SW82608
Lab Sample ID
File ID
9811619-0?A
81121822
9811619-0?A
81121822
9811619-08A
81121823
9811619-08A
81121823
9811619-lOA
81121825
9811619-078
C1123820
Project Sample
ID/Description
1198H8WW214
1198HBWW214
1198HBWW215
1198HBWW215
1198H8WW228
1198H8WW214
ABALYTICAL ~TOCOL SUMMARY COMMBB~BARRATIVB
Specification#
Analyte
Trichloroethene
1,1-Dichloroethene & llDCA
Trichloroethene
1,1-Dichloroethene & llDCA
Acetone
1,1-Dichloroethane
Flag Comment/Narrative
R
z
R
z
y
E
The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these results.
The results indicated the possible presence
of instrument carryover. The sample was
reanalyzed and the reanalysis confirmed the
original results. No measurable carryover
was present.
The results indicate the possible presence
of instrument carryover. The sample was
reanalyzed to verify these results.
The results indicated the possible presence
of instrument carryover. The sample was
reanalyzed and the reanalysis confirmed the
original results. No measurable carryover
was present.
This analyte is outside of the calibration
range. The sample was reanalyzed at a higher
dilution but acetone was
diluted out. Due to high concentrations of
other target analytes, the sample could not
be reanalyzed at an intermediate dilution.
The E flag indicates that this analyte is
outside of the range of calibration but well
within the linear range. The concentration
is outside of the rang.e of calibration by
less than 10%, so the sample was not
reanalyzed.
Work Order~1619 ~
Corrective Action
12/01/98 13:31:01
•
QUALITY CORTROL BJ:CBPTIOH RBPORT
SUMMARY
QCER # Analysis Batch Number
981124-14 MSMSDC81124183801
981123-14 MSMSDC81123170401
981121-03 MSMSDB981121035400
'
•
Work Order # 9811619
Page R_
•
CHAIN OF CUSTODY FORMS
4.0 CONDITION OF SAMPLES VERIFIED BY: _Am_· .............. l....._ __ _
Samples received match COC : 15YEs ONO Bottles received intact : ~YES
Samples screened for radioactivity : D YES ~o Samples received from USDA restricted area : DYES
See additional discrepancies/comments section : O YES 0'No
5.0 ADDITIONAL DISCREP AJ.'fCIES
Appears. on COC Appears on Label
Sample ID Date/Time Analysis Sample ID Date/Time Analysis Comments
i
6.0 SHIPPING DOCUMENTATION
Freight bill is available and attached to COC : ~S D NO Carrier: __ Fe.?( __ £ __ y__=---
Freight bill numbers : &'5.3JGf lJ f D:2)... q D
7.0 COMMENTS
Client chain-of-custody is signed, dated with time of receipt, and:addendum number is noted in the comments section.
Sample Coritrol Addendwn Verified By: J{J~ . Date: I{ 1 ll / q£)
Page 2 Of2
ONO
~o
..
(revision 1.0 03(26/97)
•
•
•
•
APPENDIXH
MONITORING WELL CONSTRUCTION REPORTS
•
•
•
APPENDIX I
HYDRAULIC TESTING PROCEDURES AND CALCULATIONS
•
•
•
•
•
APPENDIX I
HYDRAULIC TESTING PROCEDURES AND CALCULATIONS
This appendix describes procedures used to conduct a pumping test and four
"bail-down" tests at the facility. The appendix includes the recorded field measur~ments and the
calculations performed in analyzing the data.
1.1 Pumping Test
1.1.1 Introduction
A constant-rate pumping test was conducted at well PW-1 located in the area east
of the employee parking lot. The objective of the tests was to determine hydraulic
characteristics ofhydrogeologic unit B. The test site was selected based on its location outside
any chemical plume, which allowed the water generated by the test to be discharged without
treatment.
PW-1 was pumped using an electric-powered submersible pump. Well yield was
monitored using a calibrated bucket and stop watch and regulated, as necessary, by adjusting the
pump's impeller speed. The discharge was diverted from the pumping well through a water hose
and released to a drainage ditch. Drawdown in the pumping and observation wells was
measured using an electric water-level indicator and recorded manually.
I.1.2 Pumping Test Description
The well network for the pumping test included wells PW-1, OW-10, OW-20,
and MW-220. Well PW-1 served as the pumping well and wells OW-10, OW-20, and MW-220,
served as the observations wells. Wells OW-10 and OW-20 are located 10 feet and 20 feet west
of PW-1, respectively. Well MW-220 is located 48.5 feet south of PW-I. All wells are screened
in hydrogeologic unit B. A constant-rate test was started at 7:34 a.m. on November 5, 1998.
PW-1 was pliroped at an average rate of 1.6 gallons per minute (0.214 ft3/min) and drawdown
la c:\hamilton\washington\csa-rpt ( 12/16/98) I-1
was measured in all wells in the test network. Pumping continued uninterrupted until terminated
after 480 minutes. Results of the test are discussed in Section Ll.3.2.
1.1.3 Pumping Test Analysis
This section describes the analytical procedure used to evaluate the data from the
pumping test and presents the results. Tables and graphs of water-level drawdown
measurements utilized in the analyzing the test are included at the end of the discussion.
1.1.3.1 Analytical Procedure
The conceptual model used to analyze the pumping test is that of a semi-confined
(leaky) aquifer with no storage effects in t4e confining layer. Governing equations and type
curves are those presented by Hantush andiJacobs (1955) with a correction applied for partial
penetration of the observation wells (Hantush, 1961). Type curves were initially fit to measured
drawdown data by nonlinear least-squares parameter estimation and, subsequently, matched
visually using AQTESOL V software developed by Geraghty and Miller Modeling Group
(Duffield, 1991). Input to the aquifer model, in addition to the measured drawdown, included
discharge rate (Q); distance from the pumping well to the observation well (r); well casing radius
(re); borehole radius (rw); and, aquifer thickness (b). Specific input values for these parameters
are listed under "Test Data" on the accompanying graphs.
1.1.3.2 Pumping Test Results
Transmissivity calculated for hydrogeologic unit B ranges from 0.044 ft2/min
(63.4 ft2/day) to 0.045 ft2/min (64.9 ft2/day). These values equate to hydraulic conductivity
values between 3.0 ft/day and 3.1 ft/day .. The range of hydraulic conductivity values is
consistent with an aquifer comprised of fine-grained silty sand. The coefficient of storage ranges ..
from 0.0003 to 0.0006, which is typical of semi-confined aquifers.
la c:\hamilton\washington\csa·rpt ( 12/ 16/98) 1-2
•
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V
A Program for
Automatic Estimation of Aquifer Coefficients
Fro.m Aquifer Test Data
By:
Glenn M. Duffield
and
James O. Rumbaugh, III
Geraghty & Miller Modeling Group
1895 Preston White Drive, Suite 301
Reston, VA 22091
(703) 476 -0335
A Q T E S 0 L V is a user-friendly program designed to
analyze data from ~quifer·tests automatically. Aquifer
coefficients for a variety of aquifer test conditions can
be estimated by A Q T E S O L V , including the following:
o confined aquifers, unconfined aquifers,
and leaky aquifers
'
o pumping tests, injection tests, recovery tests,
and slug test:s
Features:
o Interactive, menu-driven program design
o Nonlinear least-squares estimation of aquifer coefficients
o Statistical analysis of results
o Complete graphical display of results
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
•
•
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V R E S U L T S
Version 1.10
12/15/98 14:10:40
==================================================?=============================
TEST DESCRIPTION
Data set ........... owlO.dat
Data set title ..... Pumping Test OW-10
Company ............ Radian International
Project ............ 650138.0601
Client ............. Hamilton Beach<>Proctor-Silex
Location ........... Washington, NC
Test date .......... 11/5/98
Test well .......... PW-1
Obs. well .......... OW-10
Knowns and Constants:
No. of data points .................. 47
Pumping rate ........................ 0. 214
Radius (distance) to obs. well ...... 10
Radius of pumped well casing ........ 0.083
Radius of pumped wellbore ........... 0.25
Partial Penetration Data:
Depth of top of well screen ......... 1
Depth of bottom of well screen ...... 21
Depth of top of obs. well screen ..... 1
Depth of bottom of obs. well screen .. 21
Hyd. conductivity ratio (Kz/Kr) ..... 1
================================================================================ ANALYTICAL METHOD
Hantush (Leaky Aquifer)
================================================================================
RESULTS FROM STATISTI~ CURVE MATCHING
STATISTICAL MATCH PARAMETER ESTIMATES
T
s
r/B=
Estimate
4.4017E-002 +/-
6.4284E-004 +/-
1.0000E-005 +/-
ANALYSIS OF MODEL RESIDUALS
Std. Error
1.2682E-003
4.3263E-OOS
2.4364E+001
residual = calculated -observed
weighted residual = residual * weight
Weighted Residual Statistics:
Number of residuals ............... 47
Number of estimated parameters .... 3
Degrees of freedom ................ 44
Residual mean ..................... 0.002898 • Residual standard deviation ....... 0.05422
Residual variance ................. 0.00294
Model Residuals:
Time Observed Calculated Residual Weight ------------- ------------- ---------------------------------------1 0.4 0.29583 0.10417 1
1. 5 0.54 0.4121 0.1279 1
2 0.62 0.50219 0.11781 1
2.5 0.68 0.5755 0.1045 1
3 0.72 0.63722 0.082776 1
4 0.79 0.73736 0.052641 1
5 0.85 0.81691 0.033089 1
6 0.91 0.88289 0.027105 1
7 0.94 0.93926 0.000736 1
8 0.98 0.98846 -0.0084643 1
9 1. 01 1.0321 -0.022113 1
10 1. 02 1. 0713 -0.051336 1
11 1. 07 1.1069 -0.036949 l··
12 1. 09 1.1396 -0.04956 1
13 1.12 1.1696 -0.049635 1
14 1.15 1". 1975 -0.047541 1
15 1.18 1.2236 -0.043569 1
16 1.2 1.248 -0.047957 1
18 1.24 1. 2926 -0.052556 1
20 1.26 1.3325 -0.072542 1 • 22 1.31 1.3688 -0.05878 1
24 1. 35 1.4019 -0.051913 1
26 1.38 1. 4324 -0.052431 1
28 1.41 1.4607 -0.050717 1
30 1.44 1.4871 -0.047076 1
35 1.49 1.546 -0.056046 1
40 1.54 1.5972 -0.057206 1
50 1. 64 1.6828 -0.042835 1
60 1. 72 1. 7529 -0.032904 1
70 1. 8 1.8122 -0.012209 1
80 1. 86 1.8636 -0.003619 1
90 1.91 1. 909 0.0010076 1
100 1. 95 1. 9496 0.00040124 1
120 2.02 2.0199 9.7744E-005 1
140 2.09 2.0794 0.010626 1
160 2.14 2.1309 0.0090901 1
180 2.2 2.1764 0.023619 1
200 2.24 2.2171 0.022934 1
220 2.28 2.2539 0.026124 1
240 2.31 2.2875 0.022513 1
260 2.34 2.3184 0.021591 1
280 2.38 2.347 0.032958 1
300 2.41 2.3737 0.036299 1
330 2.45 2.4105 0.039467 1
360 2.5 2.4442 0.055839 1
420 2.56 2.5037 0.056255 1
480 2.63 2.5554 0.074635 1 •
================================================================================ • RESULTS FROM VISUAL CURVE MATCHING
VISUAL MATCH PARAMETER ESTIMATES
Estimate
T 4.4017E-002
S 6.4284E-004
r/B= l.OOOOE-005
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
TYPE CURVE DATA
T = 4.40165E-002 s 6.42844E-004
r/B= 1.00000E-005
Time Drawdown Time Drawdown Time Drawdown ------------------------------------------------------------1.000E+OOO 2.958E-001 1.122E+OOO 3.274E-001 1.259E+OOO 3.601E-001
1.413E+OOO 3.940E-001 1.585E+OOO 4.289E-001 l.778E+OOO 4.647E-001
1.995E+OOO 5.014E-001 2.239E+OOO 5.389E-001 2.512E+OOO 5.771E-001
2.818E+OOO 6.159E-001 3.162E+OOO 6.553E-001 3.548E+OOO 6.953E-001
3.981E+OOO 7.357E-001 4.467E+OOO 7.765E-001 5.012E+OOO 8.178E-001
5.623E+OOO 8.593E-001 6.310E+OOO 9.012E-001 7.079E+OOO 9.434E-001
7.943E+OOO 9.858E-001 8.913E+OOO 1.028E+OOO 1.000E+OOl l.071E+OOO • 1.122E+001 1.114E+OOO 1.259E+001 1.158E+OOO 1.413E+001 1. 201E+OOO
1.585E+001 1.244E+OOO 1.778E+001 1.288E+OOO l.995E+001 l.332E+OOO
2.239E+001 l.375E+OOO 2.512E+001 1~419E+OOO 2.818E+001 1.463E+OOO
3.162E+001 1.507E+OOO 3.548E+001 1.SSlE+OOO 3.981E+001 1.595E+OOO
4.467E+001 1.640E+OOO 5.012E+001 1.684E+OOO 5.623E+001 1.728E+OOO
6.310E+001 l.772E+OOO 7.079E+001 1. 817E+OOO 7.943E+001 l.861E+OOO
8.913E+001 1.905E+OOO 1.000E+002 1. 950E+OOO l.122E+002 l.994E+OOO
1.259E+002 2.038E+OOO 1.413E+002 2.083E+OOO 1.585E+002 2.127E+OOO
1.778E+002 2.172E+OOO 1.995E+002 2.216E+OOO 2.239E+002 2.261E+OOO
2.512E+002 2 :30SE+OOO 2.818E+002 2.350E+OOO 3.162E+002 2.394E+OOO
3.548E+002 2.439E+OOO 3.981E+002 2.483E+OOO 4.467E+002 2.528E+OOO
5.012E+002 2.572E+OOO 5.623E+002 2.617E+OOO 6.310E+002 2.661E+OOO
7.079E+002 2.706E+OOO 7.943E+002 2.'.i'SOE+OOO 8.913E+002 2.795E+OOO
1.000E+003 2.839E+OOO
•
•
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V
A Program for
Automatic Estimation of Aquifer Coefficients
From Aquifer Test Data
By:
Glenn M. Duffield
and
James o. Rumbaugh, III
Geraghty & Miller Modeling Group
1895 Preston White Drive, Suite 301
Rest9n, VA 22091
(703) 476 -0335
A Q T E s O L V is a user-friendly program designed to
analyze data from aquifer tests automatically. Aquifer
coefficients for a variety of aquifer test conditions·can
be estimated by A Q T E S 0 L V , including the following:
o confined aquifers, unconfined aquifers,
and leaky aquifers
o pumping tests, injection tests, recovery tests,
and slug tests
Features:
o Interactive, menu-driven program design
o Nonlinear least-squares estimation of aquifer coefficients
o Statistical analysis of results
o Complete graphical display of results
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V R E S U L T S
Version 1.10 • 14:11:53 12/15/98
I ================================================================================ TEST DESCRIPTION
Data set ........... ow20.dat
Data set title ..... Pumping Test, OW-20
Company ............ Radian Inter'national
Project ............ 650138. 0601
Client ............. Hamilton Beach<>Proctor-Silex
Location ........... Washington, ,NC
Test date .......... 11/5/98
Test well .......... PW-1
Obs. well .......... OW-20
Knowns and Constants:
No. of data points ................... 47
Pumping rate ................. '. . . . . . . O. 214
Radius (distance) to obs. well ...... 20
Radius of pumped well casing ........ 0.083
Radius of pumped wellbore ........... 0.25
Partial Penetration Data:
Depth of top of well screen.; ....... 1
Depth of bottom of well screen ...... 21
Depth of top of obs. well screen ..... 1
Depth of bottom of obs. well screen .. 21
Hyd. conductivity ratio (Kz/1J<r) ..... 1 •
================================================================================
Hantush (Leaky Aquifer)
ANALYTICAL METHOD I
================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING
STATISTICAL MATCH PARAMETER ESTIMATES
T = s
r/B=
Estimate
4.4765E-002 +/-
3 .1534E-004 +/-
1. OOOOE-005 +/-
ANALYSIS OF MODEL RESIDUALS
Std. Error
1.4800E-003
1.9386E-005
5.0262E+001
residual = calculated -observed
weighted residual = residual * weight
•
Weighted Residual Statistics:
Number of residuals ............... 47
Number of estimated parameters .... 3 • Degrees of freedom ................ 44
Residual mean ..................... 0.0106
Residual standard deviation ....... 0.05344
Residual variance ................. 0.002856
Model Residual.s:
Time Observed Calculated Residual Weight -----------------------------------------------------------------
1 0.24 0.141 0.098999 1
1. 5 0.33 0.22764 0.10236 1
2 0.39 0.30045 0.089551 1
2.5 0 .45 0.36237 0.087629 1
3 0.49 0.41599 0.074015 1
4 0.56 0.50524 0.054762 1
5 0.62 0.57774 0.042264 1
6 0.66 0.63872 0.021284 1
7 0.71 0.69131 0.018687 1
8 0.75 0.73755 0.012455 1
9 0.78 0.77878 0.0012185 1
10 0.82 0.81599 0.0040063 1
11 0.85 0.8499 0.00010403 1 ..
12 0.87 0.88103 -0.011028 1
13 0.87 0.90981 -0.039808 1
14 0.92 0.93657 -0.016566 1
15 0.94 0.96157 -0.021567 1
16 0.97 0.98503 -0.015027 1 • 18 0.99 1. 028 -0.038012 1
20 1 1.0666 -0.066633 1
22 1. 03 1.1017 -0.071693 1
24 1.07 1.1338 -0.063795 1
26 1.1 1.1634 -0.063398 1
28 1.12 1.1909 -0.070864 1
30 1.15 1. 2165 -0.06648 1
35 1.21 1.2739 -0.063861 1
40 1.27 1.3237 -0.053711' 1
50 1.37 1. 4073 -0.037271 1
60 1.43 1.4757 -0.045743 1
70 l.'52 1.5338 -0.013751 1
80 1.57 1. 5841 -0.014074 1
90 1. 63 1. 6285 0.0014893 1
100 1. 68 1. 6683 0.011704 1
120 1. 75 1.7372 0.01279 1
140 1. 82 1.7955 0.024465 1
160 1. 87 1. 8461 0.023905 1
180 1. 92 1.8907 0.029283 1
200 1. 96 1. 9306 0.02935 1
220 2.01 1.9668 0.043213 1
240 2.04 1.9998 0.040213 1
260 2.08 2.0302 b.049849 1
280 2.12 2.0583 0.06173 1
300 2.14 2.0845 0.055547 1
330 2.18 2.1206 0.05937 t
360 2.21 2.1537 0.056336 1
420 2.29 2.2122 0.0778 1 • ·480 2.35 2.2629 0.087081 1
================================================================================
RESULTS FROM VISUAL CURVE MATCHING • VISUAL MATCH PARAMETER ESTIMATES
Estimate
T 4.4765E-002
S 3.1534E-004
r/B= l.OOOOE-005
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
TYPE CURVE DATA
T 4.47646E-002 s 3.15337E-004
r/B= l.OOOOOE-005
Time Drawdown Time Drawdown Time Drawdown ------------------------------------------------------------l.OOOE+OOO 1. 410E-001 l.122E+OOO l.635E-001 l.259E+OOO l.877E-001
l.413E+OOO 2.136E-001 l.585E+OOO 2.409E-001 l.778E+OOO 2.697E-001
l.995E+OOO 2.998E-001 2.239E+OOO 3.312E-001 2.512E+OOO 3.637E-001
2.818E+OOO 3.973E-001 3.162E+OOO 4.319E-001 3.548E+OOO 4.674E-001
3.981E+OOO 5.037E-001 4.467E+OOO 5.408E-001 5.012E+OOO 5.785E-001
5.623E+OOO 6.169E-001 6.310E+OOO 6.558E-001 7.079E+OOO 6.952E-001
7.943E+OOO 7 ."351E-001 8.913E+OOO 7.753E-001 l.OOOE+OOl 8.160E-001
l.122E+001 8.570E-001 l.259E+001 8.982E-001 l.413E+001 9.398E-001 • l.585E+001 9.816E-001 1.778E+001 l.024E+OOO l.995E+001 l.066E+OOO
2.239E+001 l.108E+OOO 2.512E+001 l.lSlE+OOO 2.818E+001 1.193E+OOO
3.162E+001 1.236E+OOO 3.548E+001 l.279E+OOO 3.981E+001 l.322E+OOO
4.467E+001 1.365E+OOO S.012E+001 l.408E+OOO 5.623E+001 l.451E+OOO
6.310E+001 l.495E+OOO 7.079E+001 1.538E+OOO 7.943E+001 l.581E+OOO
8.913E+001 1.625E+OOO l.OOOE+002 1.668E+OOO l.122E+002 l.712E+OOO
l.259E+002 l.755E+OOO l.413E+002 l.799E+OOO l.585E+002 l.843E+OOO
l.778E+002 l.886E+OOO l.995E+002 l.930E+OOO 2.239E+002 l.973E+OOO
2.512E+002 2.017E+OOO 2.818E+002 2.061E+OOO 3.162E+002 2.104E+OOO
3.548E+002 2.148E+OOO 3.981E+002 2.192E+OOO 4.467E+002 2.236E+OOO
5.012E+002 2.279E+OOO 5.623E+002 2.323E+OOO 6.310E+002 2.367E+OOO
7.079E+002 2.411E+OOO 7. 943E+'002 2.454E+OOO 8.913E+002 2.498E+OOO
l.OOOE+003 2.542E+OOO
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V
A Program for
I
Automatic Estimation of Aquifer Coefficients
From Aquifer Test Data
By:
Glenn M. Duffield
and
James o. Rumbaugh, III
Geraghty & Miller Modeling Group
1895 Preston White Drive, Suite 301
Reston, VA 22091
(703) 476 -0335
A Q T E S O L V is a user-friendly program designed to
analyze data from ~quifer.tests automatically. Aquifer
coefficients for a variety of aquifer test conditions can
be estimated by A Q T E S 0 L V , including the following:
o confined aquifers, unconfined aquifers,
and leaky aquifers
o pumping tests, injection tests, recovery tests,
and slug tes~s
Features:
o Interactive, menu-driven program design
o Nonlinear least-squares estimation of aquifer coefficients
o Statistical analy~is of results
o Complete graphical display of results
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
•
•
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V R E S U L T S
Version 1.10
12/15/98 14:13:22
=============~==================================================================
TEST DESCRIPTION
Data set ........... mw220.dat
Data set title ..... Pumping Test MW-220
Company ............ Radian International
Project ............ 650138.0601
Client ............. Hamilton Beach<>Proctor-Silex
Location ........... Washington, NC
Test date .......... 11/5/98
Test well .......... PW-1
Obs. well .......... MW-220
Knowns and Constants:
No. of data points .................. 40
Pumping rate ........................ O. 214
Radius (distance) to obs. well ...... 48.5
Radius of pumped well casing ........ 0.083
Radius of pumped wellbore ........... 0.25
Partial Penetration Data:
Depth of top of well screen ......... 1
Depth of bottom of well screen ...... 21
Depth of top of obs. well screen ..... 1
Depth of bottom of obs. well screen .. 21
Hyd. conductivity ratio (Kz/Kr) ..... 1
================================================================================
ANALYTICAL METHOD
Hantush (Leaky Aquifer)
================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING
STATISTICAL MATCH PARAMETER ESTIMATES
T s
r/B=
Estimate
4.5056E-002 +/-
3 .2553E-004 +/-
l.OOOOE-005 +/-
ANALYSIS OF MODEL RESIDUALS
Std. Error
1. 7333E-003
1.1315E-005
2.5352E+002
residual = calculated -observed
weighted residual = residual * weight
Weighted Residual Statistics:
Number of residuals ............... 40
Number of estimated parameters .... 3
Degrees of freedom ................ 37
Residual mean ..................... 0.006571 • Residual standard deviation .•..... 0.03199
Residual variance ................. 0.001023
Model Residuals:
Time Observed ' Calculateci Residual Weight --------------------------, _____________ --------------------------
1 0.05 0.0010582 0.048942 1
2 0.08 0.015579 0.064421 1
2.5 0.08 0.028237 0.051763 1
3 0.1 0.04286 0.05714 1
5.5 0.18 0.12342 0.056582 1
6 0.18 0.13911 0.040886 1
7 0.2 0.16935 0.030646 1
8 0.22 0.19796 0.022045 1
10.5 0.28 0.26256 0.017442 1
11 0.29 0.2744 0.015601 1
12 0.31 0.29712 0.012881 1
13 0.32 0.31865 0.0013528 1
14 0.33 0.33909 -0.0090891 1 ..
15 0.35 0.35854 -0.0085386 1
16 0.36 0.37708 -0.01708 1
18 0. 39 0.41173 -0.021735 1
20 0.42 0.44357 -0.023565 1
30 0.56 0.57229 -0.012287 1
35.5 0.63 0.62814 0.0018627 1
40 0.67 0.66843 0.0015658 1 • 50 0.72 0.74512 -0.025117 1
60 0.77 0.80888 -0.038879 1
70 0.83 0.86344 -0.033442 1
80 0.88 0.91113 -0.031125 1
90 0.93 0.95347 -0.023468 1
100 0.98 0.99155 -0.011546 1
120 1 1.0578 -0.057832 1
140 1.14 1.1142 0.025784 1
160 1.17 1.1633 0.0067275 1
180 1.22 1. 2067 0.013311 1
200 1.28 1. 2456 0.03437 1
220 1.28 1.2809 -0.00093139 1
240 1.28 1. 3132 -0.033216 1
260 1.31 1. 343 -0.032959 1
280 1. 38 1.3705 0.0094681 1
300 1.41 1.3962 0.013771 1
330 1.45 1.4318 0.01823 1
363 1. 51 1. 4674 0.042645 1
420 1. 56 1.5219 0.038115 1
480 1. 59 1. 5719 0.018121 1
================================================================================
RESULTS FROM VISUAL CURVE MATCHING
VISUAL MATCH PARAMETER ESTIMATES •
•
•
•
T = s
r/B=
Estimate
4.5056E-002
3.2553E-004
l.OOOOE-005
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<~<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
TYPE CURVE DATA
T 4.50557E-002
s 3.25529E-004
r/B= l.OOOOOE-005
Time Drawdown Time Drawdown Time Drawdown
-------------------------------------------------- ----------l.OOOE+OOO l.058E-003 l.122E+OOO l.852E-003 l.259E+OOO 3.077E-003
l.413E+OOO 4.883E-003 l.585E+OOO 7.433E-003 l.778E+OOO l.090E-002
l.995E+OOO l.547E-002 2.239E+OOO 2.131E-002 2.512E+OOO 2.857E-002
2.818E+OOO 3.738E-002 3.162E+OOO 4.787E-002 3.548E+OOO 6.0llE-002
3.981E+OOO 7.417E-002 4.467E+OOO · 9.005E-002 5.012E+OOO l.078E-001
5.623E+OOO l.273E-001 6.310E+OOO l.486E-001 7.079E+OOO l.717E-001
7.943E+OOO l.964E-001 8.913E+OOO 2.226E-001 l.OOOE+OOl 2.504E-001
l.122E+001 2.795E-001 l.259E+001 3.099E-Q01 l.413E+001 3.416E-001
l.585E+001 3.743E-001 l.778E+001 4.081E-001 l.995E+001 4.428E-001
2.239E+001 4.784E-001 2.512E+001 5.148E-001 2.818E+001 5.519E-001
3.162E+001 5.896E-001 3.548E+001 6.280E-001 3.981E+001 6.668E-001
4.467E+001 7.062E-001 5.012E+001 7.459E-001 5.623E+001 7.861E-001
6.310E+001 8.266E-001 7.079E+001 8.675E-001 7.943E+001 9.086E-001
8.913E+001 9.499E-001 1.000E+002 9.915E-001 1.122E+002 1.033E+OOO
l.259E+002 1.075E+OOO l.413E+002 1.117E+OOO 1.585E+002 l.160E+OOO
1.778E+.002 1.202E+OOO 1.995E+002 1.245E+OOO 2.239E+002 l.287E+OOO
2.512E+002 1.330E+OOO 2.818E+002 1. 373E+OOO 3.162E+002 1.416E+OOO
3.548E+002 1.459E+OOO 3.981E+002 1.502E+OOO 4.467E+002 l.545E+OOO
5.012E+002 1.588E+OOO 5.623E+002 1.631E+OOO 6.310E+002 1.674E+OOO
7.079E+002 1.718E+OOO 7.943E+002 1.761E+OOO 8.913E+002 1.804E+OOO
1.000E+003 1.848E+.OOO
1.2 Bail-down Tests
1.2.1 Introduction
Bail-down tests were condudted at wells MW-217, MW-219, MW-223, and MW-
231. The objective of the tests was to determine the hydraulic conductivity of the hydrogeologic
I
unit A at the facility. The test sites were selected based on their locations in different parts of the
facility. A secondary consideration was each well's location outside any chemical plume, which
allowed water generated during the test to be disposed without treatment.
1.2.2 Bail-down Test Description
All wells tested are screened in hydrogeologic unit A. Instantaneous removal of
water to effect the initial drawdown was performed using an electric-powered peristaltic pump.
Immediately after withdrawal, water-level recovery in each well was measured using an electric
•
water-level indicator and recorded manually. Measurement continued at regular intervals until •
the water level recovered to within at least 95 percent of equilibrium. Results of the tests are
discussed in Section I.1.3.2.
1.2.3 Bail ... down Test Analysis
This section describes the analytical procedure used to evaluate the data from
each bail-down test and presents the results. Tables and graphs of water-level recovery
measurements utilized in the analysis of each test are included at the end of the discussion.
1.2.3.1 Analytical Procedure
The conceptual model used to analyze each bail-down test is that of an
unconfined aquifer with completely or partially penetrating wells . Governing equations and type
curves are those presented by Bouwer and Rice (1976). Type curves were initially fit to
measured drawdown data by nonlinear least-squares parameter estimation and, subsequently,
matched visually using AQTESOL V software developed by Geraghty and Miller Modeling
I
la c:\hamilton\washington\csa-rpt ( 12/16/98) I-3
•
• Group (Duffield, 1991 ). Input to the aquifer model, in addition to the measured water levels,
included initial drawdown (H0); well casing radius (re); borehole radius (rw); saturated length of
well screen (L); aquifer thickness (b); and height of water in the well. Specific input values for
these parameters are listed under "Test Data" on the accompanying graphs.
•
•
I.2.3.2 Bail-down Test Results
Hydraulic conductivity values calculated for hydrogeologic unit A range from
3.9 x io-7 ft/min (5.7 x 10-4 ft/day) to 5.1x10-5 ft/min (7.4 x io-2 ft/day). The range of hydraulic
conductivity values are representative of clay, sandy silt, and clayey sand .
la c:\hamilton\washington\csa-rpt (12/16/98) I-4
•
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V
A Program for
Automatic Estimation of Aquifer Coefficients
From Aquifer Test Data
By:
Glenn M. Duffield
and
James 0. Rumbaugh, III
Geraghty & Miller Modeling Group
1895 Preston White Drive, Suite 301
Reston, VA 22091
(703) 476 -0335
A Q T E S O L V is a user-friendly program designed to
analyze data from aquifer tests automatically. Aquifer
coefficients for a variety of aquifer test conditions can
be estimated by A Q T E S 0 L V , including the following:
o confined aquifers, unconfined aquifers,
and leaky aquifers
o pumping tests, injection tests, recovery tests,
and slug tests
Features:
o Interactive, menu-driven program design
o Nonlinear least-squares estimation of aquifer coefficients
o Statistical analysis of results
o Complete graphical display of results
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V R E S U L T S
Version 1.10 • 12/15/98 13:50:27
================================================================================
TEST DESCRIPTION
Data set ........... rnw217.dat
Data set title ..... MW-217 Bail-down Test
Company ............ Radian International
Project ............ 650138.0601
Client ............. Hamilton Beach<>Proctor-Silex
Location ........... Washington, ,NC
Test date .......... 10/04/98
Test well .......... MW-217
Knowns and Constants:
No. of data points ................. .
Radius of well casing .............. .
Radius of well .............. , ...... .
Aquifer saturated thickness.r ...... .
Well screen length .......... •··· ... .
Static height of water in well ..... .
Log (Re/Rw) ......................... .
A, B, C ...•......................•.•
28
0.02
0.083
4.42
4.42
4.42
3.045
0.000, 0.000, 2.954
============================================================================• ANALYTICAL METHOD I
Bouwer-Rice (Unconfined Aquifer Slug Test)
================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING
STATISTICAL MATCH PARAMETER ESTIMATES
K
yo
Estimate
1. 5276E-005 +/-
4. 3333E+OOO +/-
ANALYSIS OF MODEL RESIDUALS
Std. Error.
8.6034E-007
1. 2,807E-001
residual = calculated -observed
weighted residual = residual * weight
Weighted Residual Statistics:
Number of residuals ............... 28
Number of estimated paramet~rs .... 2
Degrees of freedom ................ 26
Residual mean. . . . . . . . . . . . . . . . . . . . . -0. 05019
Residual standard deviation ....... 0.2284 •
•
•
•
Residual variance ................. 0.05216
Model Residuals:
Time Observed Calculated Residual Weight -------------------------- ---------------------------------------0.5 3.84 4.0996 -0.25959 1
1 3.64 3.8785 -0.23849 1
1. 5 3.49 3.6693 -0.17931 1
2 3.36 3.4714 -0.11142 1
2.5 3.25 3.2842 -0.034197 1
3 3 .13 3 .1071 . 0.022927 1
3.5 3.01 2.9395 0.070498 1
4 2.93 2.781 0.14903 1
4.5 2.8 2.631 0.16902 l
5 2.69 2.4891 ·0.20091 1
5.5 2.61 2.3548 0.25515 1
6 2.5 2.2278 0.27215 1
7 2.26 1. 994 0.26598 l
8 2.04 1.7847 0.25526 l
9 1. 8 1.5974 0.20258 l
10 1. 57 1. 4298 0.14024 1
11 1.32 1. 2797 0.0403 1
12 1. 08 1.1454 -0.065388 l
14 0.7 0.91758 -0.21758 1 ..
16 0.38 0.73507 -0.35507 l
18 0.19 0.58887 -0.39887 l
20 0.1 o."47175 -0.37175 l
22 0.06 0.37792 -0.31792 1
24 0.04 0.30275 -0.26275 l
26 0.03 0.24254 -0.21254 1
28 0.02 0.1943 -0.1743 1
30 0.02 0.15565 -0.13565 l
32 0.01 0.12469 -0.11469 1
================================================================================
RESULTS FROM VISUAL CURVE MATCHING
VISUAL MATCH PARAMETER ESTIMATES
K =
yo
Estimate
1. 5276E-005
4.3333E+OOO
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
TYPE CURVE DATA
K 1.52764E-005
yO = 4.33329E+OOO
Time Drawdown Time Drawdown Time Drawdown
O.OOOE+OOO 4.333E+OOO 3.200E+001 1.247E-001
•
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V
A Program for
Automatic Estimation of Aquifer Coefficients
From Aquifer Test Data
By:
Glenn M. Duffield
and
James 0. Rumbaugh, III
Geraghty & Miller Modeling Group
1895 Preston White Drive, Suite 301
Reston, VA 22091
(703) "476 -0335
A Q T E S 0 L V is a user-friendly program designed to
analyze data from aquifer tests automatically. Aquifer
coefficients for a variety of aquifer test conditions can
be estimated by A Q T E S O L V , including the following:
o confined aquifers, unconfined aquifers,
and leaky aquifers
o pumping tests, injection tests, recovery tests,
and slug. tests
Features:
o Interactive, menu-driven program design
o Nonlinear least-squares estimation of aquifer coefficients
o Statistical analysis of results
o Complete graphical display of results
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V R E S U L T S
Version 1.10 14:02:~ 12/15/98
================================================================================
TEST DESCRIPTION
I
Data set ........... mw219.dat
Data set title ..... MW-219 Bail-down Test
Company ............ Radian International
Project ............ 650138.0601
Client ............. Hamilton Beach<>Proctor-Silex
Location ........... Washington, NC
Test date .......... 10/04/98
Test well .......... MW-219
Knowns and Constants:
No. of data points ................. .
Radius of well casing .............. .
Radius of well ..................... .
Aquifer saturated thickness ........ .
Well screen length ................. .
Static height of water in well ..... .
Log (Re/Rw) ................... : ...... .
A, B, C •........•............ : ...... .
28
0.02
0.083
3.86
3.86
3.86
2.936
0.000, 0.000, 2.519
ANALYTICAL. METHOD
=============================================================================-·
Bouwer-Rice (Unconfined Aquifer Slug Test)
I ================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING
STATISTICAL MATCH PARAMETER ESTIMATES
K =
yo =
Estimate
3.1333E-005 +/-
3.7101E+OOO +/-
ANALYSIS OF MODEL RESIDUALS
Stdi Error.
8.3575E-007
6.2539E-002
residual = calculated -observed
weighted residual = residual * weight
Weighted Residual Statistics:
Number of residuals ............... 28
Number of estimated parameters .... 2
Degrees of freedom ................ 26
Residual mean ..................... 0.00792
Residual standard deviation ....... 0.08102 •
•
•
•
Residual variance ................. 0.006564
Model Residuals:
Time Observed Calculated Residual Weight -----------------------------------------------------------------0.5 3.22 3.3469 -0.12694 1
1 3.01 3.0194 -0.0093585 1
1. 5 2.79 2.7238 0.066159 1
2 2.47 2.4572 0.012753 1
2.5 2.3 2.2167 0.083254 1
3 2.08 1.9998 0.080216 1
3.5 2.04 1. 8041 0.23594 1
4 1.47 1. 6275 -0.15749 1
4.5 1.46 1. 4982 -0.008197 1
5 1. 37 1.3245 0.045502 1
5.5 1. 06 1.1949 -0.13486 1
6 1. 04 1. 0779 -0.037918 1
7 0.81 0.87724 -0.067243 1
8 0.63 0.71393 -0.083927 1
9 0.52 0.58102 -0.061016 1
10 0.45 0.47285 -0.022849 1
11 0.39 0.38482 0.005181 1
12 0.35 0.31318 0.036822 1
14 0.27 0.20742 0.062576 l··
16 0.2 0.13738 0.062619 1
18 0.15 0.09099 0.05901 1
20 0.1 0.060265 0.039735 1
22 0.08 0.039915 0.040085 1
24 0.06 0.026436 0.033564 1
26 0.04 0.017509 0.022491 1
28 0.04 0.011597 0.028403 1
30 0.02 0.0076808 0.012319 1
32 0.01 0.0050871 0.0049129 1
================================================================================
RESULTS FROM VISUAL CURVE MATCHING
VISUAL MATCH PARAMETER ESTIMATES
K
yo =
Estimate
3.1333E-005
3.7101E+OOO
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
TYPE CURVE DATA
K 3.13328E-005
yO 3.71006E+OOO
Time Drawdown · Time Drawdown Time Drawdown
O.OOOE+OOO 3.710E+OOO 3.200E+001 5.087E-003
•
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>~>>>>>
A Q T E S 0 L V
A Program for
Automatic Estimation of Aquifer Coefficients
From Aquifer Test Data
By:
Glenn M. Duffield
and
James 0. Rumbaugh, III
Geraghty & Miller Modeling Group
1895 Preston White Drive, Suite 301
Reston, VA 22091
A Q T E S 0 L
analyze data
coefficients
be estimated
(703) 476 -0335
V is
from
for
a user-friendly program designed to
aquifer tests automatically. Aquifer
a variety of aquifer test conditions can
Q T E S O L V , including the following: by A
o confined aquifers, unconfined aquifers,
and leaky aquifers
o pumping tests, injection tests, recovery tests,
and slug tests
Features:
o Interactive, menu-driven program design
o Nonlinear least-squares estimation of aquifer coefficients
o Statistical analysis of results
o Complete graphical display of results
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V R E S U L T S
Version 1.10 • 14:03:44 12/15/98
================================================================================
TEST DESCRIPTION
Data set ........... mw223.dat
Data set title ..... MW-223 Bail-down Test
Company ............ Radian International
Project ............ 650138. 0601
Client ............. Hamilton Beach<>Proctor-Silex
Location ........... Washington, NC
Test date .......... 10/04/98
Test well .......... MW-223
Knowns and Constants:
No. of data points .................. 18
Radius of well casing ............... 0.02
Radius of well ...................... 0.083
Aquifer saturated thickness ......... 5.47
Well screen length .................. 5.47
Static height of water in well ...... 5.47
Log (Re/Rw) .......................... 3. 214
A, B, C ............................. 0.000, 0.000, 3.195
===============================;~~~;~;~=~;;~;~============================•
Bouwer-Rice (Unconfined Aquifer: Slug Test)
================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING
STATISTICAL MATCH PARAMETER EST.IMATES
K
yo =
Estimate
5.1014E-OOS +/-
4.7431E+OOO +/-
ANALYSIS OF MODEL RESIDUALS
Std. Error.
l.6398E-006
1.1671E-001
residual = calculated -observed
weighted residual = residual * w.eight
Weighted Residual Statistics:
Number of residuals ............... 18
Number of estimated paramet~rs .... 2
Degrees of freedom ......... I ...... 16
Residual mean ..................... O. 04066
Residual standard deviation ....... 0.09684 •
•
•
•
Residual variance ................. 0.009377
Model Residuals:
Time Observed Calculated Residual.• Weight --------------------------------------- --------------------------0.5 3.87 3.8177 0.05229 1
1 3.08 3.0729 0.0071428 1
1.5 2.53 2.4733 0.056671 1
2 1. 91 1.9908 -0.080771 1
2.5 1. 5 1.6024 -0.10236 1
3 1. 22 1. 2897 -0.069734 1
3.5 0.97 1. 0381 -0.068101 1
4 0.81 0.83556 -0.025563 1
4.5 0.68 0.67254 0.007459 1
5 0.58 0.54133 0.038675 1
5.5 0.49 0.43571 0.05429 1
6 0.43 0.3507 0.079299 1
7 0.32 0.2272 0.092796 1
8 0.26 0.1472 0.1128 1
9 0.21 0.095362 0.11464 1
10 0.2 0.061781 0.13822 1
11 0.2 0.040025 0.15997 1
12 0.19 0.025931 0.16407 1
================================================================================
RESULTS FROM VISUAL CURVE MATCHING
VISUAL MATCH PARAMETER ESTIMATES
K =
yo =
Estimate
5.1014E-005
4.7431E+OOO
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
TYPE CURVE DATA
K 5.10138E-005
yo 4.74311E+OOO
Time Drawdown Time Drawdown Time Drawdown
O.OOOE+OOO 4.743E+OOO l.200E+001 2.593E-002
•
•
•
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V
A Program for
Automatic Estimation of Aquifer Coefficients
From Aquifer Test Data
By:
Glenn M. Duffield
and
James 0. Rumbaugh, III
Geraghty & Miller Modeling Group
1895 Preston White Drive, Suite 301
Reston, VA 22091
(703) 476 -0335
A Q T E S O L V is a user-friendly program designed to
analyze data from aquifer ·tests automatically. Aquifer
coefficients for a variety of aquifer test conditions can
be estimated by A Q T E S O L V , including the following:
o confined aquifers, unconfined aquifers,
and leaky aquifers
o pumping tests, injection tests, recovery tests,
and slug tests
Features:
o Interactive, menu-driven program design
o Nonlinear least-squares estimation of aquifer coefficients
o Statistical analysis of results
o Complete graphical display of results
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>.>>>>>>>>>>>>>>>>>>>>>>>>>>>
J
I
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
A Q T E S 0 L V R E S U L T S
Version 1.10 • 12/15/98 14:07:56
================================================================================
TEST DESCRIPTION
Data set ........... mw231.dat
Data set title .. : .. MW-231 Bail-down Test
Company ............ Radian International
Project ............ 650138.0601
Client ............. Hamilton Beach~>Proctor-Silex
Location ........... Washington, NC
Test date .......... 10/04/98
Test well .......... MW-231
Knowns and Constants:
No. of data points ................. .
Radius of well casing .............. .
Radius of well ..................... .
Aquifer saturated thickness ........ .
Well screen length ................. .
Static height of water in well ..... .
Log (Re/Rw) ......................... ·.
A, B, C •..•....•.......•....•.......
41
0.02
0.083
3.67
3.67
3.67
2.894
0.000, 0.000, 2.440
====================================~========================================•
ANALYTICAL METHOD
Bouwer-Rice (Unconfined Aquifer Slug Test)
================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING
STATISTICAL MATCH PARAMETER ESTIMATES
K
yo
Estimate
3.9322E-007 it-/-
7.9715E-001 +/-
ANALYSIS OF MODEL RESIDUALS
Std. Error
3.5856E-008
5.2288E-003
residual = calculated -observed
weighted residual = residual * weight
Weighted Residual Statistics:
Number of residuals ................ 41
Number of estimated parameters .... 2
Degrees of freedom ................ 39
Residual mean ..................... 1. 024E-005
Residual standard deviation ....... 0.02034 •
•
•
•
Residual variance ................. 0.0004135
Model Residuals:
Time Observed Calculated Residual Weight ------------- ----------------------------------------------------0.5 0.88 0.79616 O.Q83845 1
1 0.85 0.79516 0.054837 1
1. 5 0.82 0.79417 0.025827 1
2 0.82 0.79318 0.026816 1
2.5 0.79 0. 7922 -0.0021955 1
3 0.79 0.79121 -0.0012086 1
3.5 0.79 0.79022 -0.00022301 1
4 0.78 0.78924 -0.0092386 1
4.5 0.78 0.78826 -0.0082555 1
5 0.77 0.78727 -0.017274 1
6 0.77 0.78531 -0.015313 1
7 0.77 0.78336 -0.013358 1
8 0.77 0.78141 -0.011408 1
9 0.77 0.77946 -0.009462 1
10 0.77 0.77752 -0.0075213 1
11 0.76 0.77559 -0.015585 1
12 0.76 0.77365 -0.013654 1
14 0.75 0.76981 -0.019807 1
16 0.75 0.76598 -0.015978 1 ..
18 0.74 0.76217 -0.022168 1
20 0.74 0.75838 -0.018378 1
22 0.74 0.75461 -0.014606 1
24 0.74 0.75085 -0.010853 1
26 0.74 0.74712 -0.0071185 1
28 0.73 0.7434 -0.013403 1
30 0.73 0.73971 -0.0097054 1
32 0.73 0.73603 -0.0060265 1
34 0.73 0.73237 -0.0023658 1
36 0.73 0.72872 0.0012766 1
38 0.72 0.7251 -0.0050991 1
40 0.72 0.72149 -0.0014928 1
42 0.72 0.7179 0.0020955 1
44 0.72 0.71433 0.005666 1
46 0.71 0.71078 -0.00078128 1
48 0.71 0.70725 0.0027538 1
so 0.71 0.70373 0.0062713 1
52 0.71 0.70023 0.0097713 1
54 0.71 0.69675 0.013254 1
56 0.71 0.69328 0.016719 1
58 0.7 0.68983 0.010167 1
60 0.7 0.6864 0.013598 1
================================================================================
RESULTS FROM VISUAL CURVE MATCHING
VISUAL MATCH PARAMETER ESTIMATES
Estimate
K 3.9322E-007
yo = 7.9715E-001
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
TYPE CURVE DATA
K 3.93222E-007
yo 7.97148E-001
Time Drawdown Time Drawdown
O.OOOE+OOO 7.971E-001 6.000E+OOl 6.864E-001
•
Time Drawdown
•
•