IDX GW Monitoring Rpt May 2002 (SF)-OCR

*5841HSSF1065*
1111111111111111111111111111
DocumentlD NONCD0001814
Site Name HAMILTON BEACH/PROCTOR SILEX
DocumentType Progress/Monitoring Rpt (PRGMON)
RptSegment 1
DocDate
DocRcvd
Box
Accesslevel
Division
Section
Program
DocCat
6/5/2002
2/20/2007
SF1065
PUBLIC
WASTE MANAGEMENT
SUPERFUND
IHS {IHS)
FACILITY
URS
June 5, 2002
Ms. Michele Volosin
North Carolina Department of Environment
and Natural Resources
934 Washington Square Mall
Washington, North Carolina 27889
RE: Groundwater Monitoring Report for May 2002
Groundwater Incident No. 14338
Hamilton Beach<>Proctor-Silex, Inc.
Washington, North Carolina
Dear Ms. Volosin:
On behalf of Hamilton Beach<> Proctor-Silex, Inc., URS is submitting one copy of the
referenced report.
If you have any questions, please contact Mario Kuhar at [phone].
Sincerely,
~?~
Craig L. Kennedy, L.G.
Geologist
CK: la
Enclosure
cc: R. L. Willoughby, City of Washington
Mario Kuhar, Hamilton BeachOProctor-Silex
Bradford A. De Vore, Womble Carlyle Sandridge & Rice
Project File
URS Corporation
1600 Perimeter Park Drive, Suite 100
Morrisville, NC 27560
Tel: [phone]
Fax: [phone]
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GROUNDWATER MONITORING REPORT
FORMAY2002
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
Prepared for:
Hamilton BeachOProctor-Silex, Inc.
4421 Waterfront Drove
Glen Allen, Virginia 23060
Prepared by:
URS Corporation
1600 Perimeter Park Drive
Morrisville, North Carolina 27560
June 2002
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CERTIFICATION PAGE
GROUNDWATER MONITORING REPORT
FORMAY2002
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
I, Craig L. Kennedy, a Licensed Geologist in the State of North Carolina, certify that
this report and its contents have been prepared under my direct control and personal
superv1s10n.
80396914.01 May2002GW _Rpt.doc (06/05/02) 1
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TABLE OF CONTENTS
Certification Page ................................................................................................................. i
List of Figures .................................................................................................................... iii
List of Tables .................................................................................................................... iv
1.0 IN"TRODUCTION ........................................................................................................... 1-1
2.0 FIELD METHODS .......................................................................................................... 2-1
3.0 RESULTS ........................................................................................................................ 3-1
3.1 Water Level Measurements ................................................................................. 3-1
3.2 Analytical Results ................................................................................................ 3-1
APPENDIX A GROUNDWATER SAMPLIN"G ANALYTICAL REPORTS
80396914.01 May2002GW _Rpt.doc (06/05/02) 11
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LIST OF FIGURES
1-1 Topographic Map, Hamilton BeachOProctor-Silex, Inc.
2-1 Site Map, Washington Facility, Hamilton BeachOProctor-Silex, Inc.
3-1 Generalized Groundwater Flow Direction for Hydrogeologic Unit A,
Washington Facility
3-2 Generalized Groundwater Flow Direction for Hydro geologic Unit B,
Washington Facility
3-3 Location of Surrounding Water Supply Wells
80396914.01 May2002GW _Rpt.doc (06/05/02) iii
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LIST OFT ABLES
2-1 Monitoring Well Construction Data for Sampled Wells
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina·
3-1 Water Level Measurements and Elevations, May 8, 2002
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-2 Historical Water Level Elevations at MW-220
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-3 Historical Water Level Elevations at MW-222
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-4 Historical Water Level Elevations at MW-224
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-5 Historical Water Level Elevations at MW-225
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-6 Historical Water Level Elevations at MW-226
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-7 Historical Water Level Elevations at MW-230
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-8 Historical Water Level Elevations at MW-234
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-9 Field Measurements, May 8, 2002
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-10 Summary of Qualified Groundwater Analytical Results: May 2002
Volatile Organic Compounds by Method 8260B
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-11 Historical Analytical Results for MW-220
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-12 Historical Analytical Results for MW-222
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-13 Historical Analytical Results for MW-224
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
80396914.01 May2002GW _Rpt.doc (06/05/02) IV
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LIST OF TABLES (Continued)
3-14 Historical Analytical Results for MW-225
Hamilton Beach<> Proctor-Silex, fuc., Washington, North Carolina
3-15 Historical Analytical Results for MW-226
Hamilton Beach<> Proctor-Silex, fuc., Washington, North Carolina
3-16 Historical Analytical Results for MW-230
Hamilton Beach<> Proctor-Silex, fuc., Washington, North Carolina
3-17 Historical Analytical Results for MW-234
Hamilton Beach<> Proctor-Silex, fuc., Washington, North Carolina
80396914.01 May2002GW _Rpt.doc (06/05/02) v
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1.0 INTRODUCTION
The Hamilton BeachOProctor-Silex (HBOPS) facility is located at 234 Springs
Road, north of the City of Washington, in Beaufort County, North Carolina (Figure 1-1). The
facility and surrounding land parcel are owned by the City of Washington and have been leased
by HBO PS since 1990 and previously leased by predecessor companies. The facility was
formerly involved in the final assembly, packaging, and warehousing of small electrical
household appliances.
Since 1992, when organic compounds were initially detected in groundwater at
the site, several phases of investigation have been performed, including a comprehensive site
assessment (CSA). The results of the CSA indicated that a plume of organic compounds is
present in groundwater underlying the site. The specific nature, volume, and time period of any
releases contributing to the plume are unknown. However, the principal constituents of the
plume are no longer used at the facility.
A plan for corrective action at the site has been proposed. Until corrective action
is implemented, groundwater will be sampled and analyzed on a quarterly schedule according to
a monitoring program requested by the North Carolina Department of Environment and Natural
Resources, Groundwater Section. Quarterly groundwater monitoring is being conducted in
February, May, August, and November at seven wells: MW-220, -222, -224, -225, -226, -230,
and-234. These monitoring wells are located outside of the contaminant plume. In August, six
additional wells: MW-213, -214, -215, -216, -227, and-228 are sampled. These wells are
located within the contaminant plume. The purpose of the monitoring program is to detect
potential migration of the plume.
URS Corporation (URS) conducted groundwater sampling at the facility on
May 8, 2002. The sampling event included the measurement of water levels, temperature, pH,
and specific conductance; and the collection and analysis of samples from seven monitoring
wells. Water levels were measured in ten additional wells. This report describes the sampling
methods and presents the results for the quarterly sampling event.
80396914.0 l May2002GW _Rpt.doc(06/05/02) 1-2
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2.0 FIELD METHODS
Groundwater was sampled on May 8, 2002 in general accordance with the
methods outlined in the Field Sampling and Analysis Plan prepared in April 1997 for this site.
Seven monitoring wells were sampled. They included MW-220, MW-222,
MW-224, MW-225, MW-226, MW-230, and MW-234. The locations of the monitoring wells
are shown in Figure 2-1. Details of well construction are provided in Table 2-1.
Prior to sampling, the water level in each well was measured using an electric
water-level indicator. The wells were then purged using inertial foot-valve pumps. Temperature,
specific conductance, and pH were measured and the data were recorded in a field notebook.
Purging continued until temperature, specific conductance, and pH stabilized; a minimum of
three well volumes was extracted; or the well was pumped dry. Each of the wells was then
sampled immediately following well purging using the inertial foot-valve pump. For QA/QC
purposes, a duplicate sample was collected at well MW-226.
The groundwater samples were sent by overnight courier to STL in Austin, Texas,
for analysis of volatile organic compounds by EPA Method 8260B.
80396914.01 May2002GW _ Rpt.doc(06/05/02)
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3.0 RESULTS
3.1 Water Level Measurements
Table 3-1 presents the depth to groundwater and static water-level elevations
measured in the seven wells sampled, and in ten additional monitoring wells. Maps showing the
generalized direction of groundwater flow in hydrogeologic units A and B are included as
Figures 3-1and3-2, respectively. Historical water-level elevations in sampled wells are
included in Tables 3-2 to 3-8.
3.2 Analytical Results
Field measurements of water temperature, specific conductance, and pH are
summarized in Table 3-9. Qualified analytical results are summarized in Table 3-10. Qualified
data sheets and laboratory reports are included in Appendix A.
No analytes were detected above the groundwater standards in samples from
wells located near the perimeter of the site (MW-220, MW-222, MW-224, MW-225, MW-230,
and MW-234), nor were any analytes detected above the groundwater standards in the sample
from well MW-226, which is completed in the confined Limestone Aquifer.
Historical analytical results for the sampled wells are presented in Tables 3-17 to
3-23. A comparison of the record for wells located near the perimeter of the site suggests that
the plume remains on-site. Locations of surrounding water-supply wells are shown in
Figure 3-3.
80396914.01 May2002GW _Rpt.doc(06/0S/02) 3-1
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FIGURES
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TABLES
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LABORATORY REPORTS
SECTION I
Table of Contents
Section
I.
MS-VOA
II.
III.
IV.
v.
VI.
VII.
Form
Cover Page -laboratory Analytical Report
Table of Contents • . . . . . . . . . . .
Report Surrmaries . . . . .
Workorder Surrmary
Protocol Surrmary
Carments and Flag Definitions . . . . .
Standard Flag Definitions .
Analyst Carments . . . . .
Sarrple Condition Carments
Analytical Results . . . . . . . . . .
SW8260B . . . . . . . . . .
calibration and Quality Control Results
SW8260B . . . . . . . . . . .
Batch Surrmaries . .
SW8260B
Certifications . . .
calibration Verification Results
Mass Spectrometer Tune
Method Blank Results
Control Sarrple Results . . . .
Extraction/Digestion Batch Surrmary
Analysis Batch Surrmary
Section I -Table of Contents -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Page
. i
1
. 1
1
1
3
• 3
3
3
. . . . . . 4
. . . . . 4
19
. 19
. . 19
27
29
. . 33
37
37
37
39
. 41
-------------------
-------------------SECTION 11
Report Summaries
MS-VOA
Client Name: Hamilton Beach-Proctor Silex
Client Code: HB-PS
Workorder Summary
: < < ("b' <
',,, ', ,',, ;
, , ' ' , > ~ ,, < Jl .; ~,'
,Clierit-Sama:>leill::> ,',:,A, · Sample:iD
0502HBWW220 2020505401
0502HBWW222 2020505402
0502HBWW224 2020505403
0502HBWW225 2020505404
0502HBWW226 2020505405
0502HBWW230 2020505406
0502HBWW234 2020505407
0502HBWD999 2020505408
TRIP BLANK 2020505409
Protocol Summary
,, < < ¥ -" ' ' '• /< ,, . ' ~ : ,"', ;. -, <' ,, -, '',,: ka,b ,,
" • <
:'cnetits~mor•-la~ _ ,, --, -·samole ID " . -
Method: SW8260B
0502HBWW220 2020505401
0502HBWW222 2020505402
0502HBWW224 2020505403
0502HBWW225 2020505404
0502HBWW226 2020505405
SECTlON II-Report Summaries -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Project Name: 80396913 [20205054] Hamilton Beach-Proctor Silex
Facility Name: NC
,,
sample· Matrix Method Citation • Method Descriotiort _
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B . Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles by GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
< --Hold.Time Spec
·Qate ~ Tjoj(I Dat<t&Tim' Pr~p b•te & Time Ana!ysi$ · P~te.&Time .Preo Analvsis
·Collected < Received -B_atchlD _ Pte'oared .B.atch 10 _Analvzed. ·spec ·Actual _Spec Actual
05/08/02 12:50 05/09/02 11:01 27619 05/13/02 21 :20 27619 05/13/02 21 :20 7D 5D 7D 5D
05/08/02 13:55 05/09/02 11:01 27619 05/13/02 21:49 27619 05/13/02 21:49 7D 5D 7D 5D
05/08/02 13:15 05/09/02 11:01 27619 05/13/02 22:17 27619 05/13/02 22:17 7D 5D 7D 5D
05/08/02 13 :25 05/09/02 11:01 27619 05/13/02 22:46 27619 05/13/02 22:46 7D 5D 7D 5D
05/08/02 11 :45 05/09/02 11:01 27619 05/13/02 23:14 27619 05/13/02 23:14 7D 5D 7D 5D
Page I of 41
SECTION II
Report Summaries
MS-VOA
Protocol Summary continued -
. ' ;bfb .
Client Samole ID .· ,,: . sYrfii.18.rD
Method: SW8260B continued -
0502HBWW230 2020505406
0502HBWW234 2020505407
0502HBWD999 2020505408
TRIP BLANK 2020505409
SECTION II -Report Summaries -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
DCJte&Time Date& Time Prep
Collected Received Batch.ID
05/08/02 11: 10 05/09/02 11:01 27619
05/08/02 13:40 05/09/02 11:01 27619
05/08/02 11:50 05/09/02 11:01 27619
05/08/02 00:00 05/09/02 11:01 27619
Hoid Time S >ec
Date& Time Analysis Pate & Time Preo .Analvsis
Preo.ared Batch ID Analvzed Soec Aetua: ·Spec· Actual
05/13/02 23:43 27619 05/13/02 23 :43 7D 5D 7D 5D
05/14/02 00: 11 27619 05/14/0200:11 7D 6D 7D 6D
05/14/02 00:39 27619 05/14/02 00:39 7D 6D 7D 6D
05/13/02 19:24 27619 05/13/02 19:24 7D 5D 7D 5D
Page 2 of 41
-------------------
------------SECTION Ill
Comments and Flag Definitions
MS-VOA
Standard Data Qualifiers
Flaa Definition ','
" ' J Result > or = MDL and <POL
NA Not analvzed/Not available
ND Not detected at the specified reporting limit
0 Result does not meet tolerance in Protocol Snecification
u Result less than sample specific method detection limit
Analyst Comments
-Affected Sam le Method __
0502HBWW220 SW8260B
Sample Condition Comments
I Affecfe<f,,sample --, _ I ,Comment_
SECTION III -Comments and Flag Definitions -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
Comment
See CER 5247.
- -- - -- -
:1
Page 3 of 41
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone fMRK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results-05/14/2002 15:49
0502HBWD999
2020505408
Aaueous
Received
NA
05/08/2002 11:50
05/14/2002 00:39
05/14/2002 00:39
1.0000
MSDA
ug/L
.. Cone Flaa .
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
DL
1.26
5.34
2.85
0.290
0.0465
0.0643
0.0449
0.0528
0.106
0.0454
2.83
0.0888
0.104
0.0934
0.0415
0.0553
0.0596
0.0404
0.0755
0.0338
0.0798
0502HBWW220 0502HBWW222
2020505401 2020505402
Aaueous Aaueous
Received Received
NA NA
05/08/2002 12:50 05/08/2002 13:55
05/13/2002 21 :20 05/13/2002 21 :49
05/13/2002 21 :20 05/13/2002 21 :49
1.0000 1.0000
MSDA MSDA
ug/L ug/L
. RL Coric Flaa DL RL Cone Flaa DL RL
0.00 ND 1.26 0.00 ND 1.26 0.00
0.00 ND 5.34 0.00 ND 5.34 0.00
0.00 ND 2.85 0.00 ND 2.85 0.00
0.00 ND 0.290 0.00 ND 0.290 0.00
0.00 ND 0.0465 0.00 ND 0.0465 0.00
0.00 ND 0.0643 0.00 ND 0.0643 0.00
0.00 ND 0.0449 0.00 ND 0.0449 0.00
0.00 ND 0.0528 0.00 ND 0.0528 0.00
0.00 ND 0.106 0.00 ND 0.106 0.00
0.00 ND 0.0454 0.00 ND 0.0454 0.00
O.OQ ND 2.83 0.00 ND 2.83 0.00
0.00 ND 0.0888 0.00 ND 0.0888 0.00
0.00 ND 0.104 0.00 ND 0.104 0.00
0.00 ND 0.0934 0.00 ND 0.0934 0.00
0.00 ND 0.0415 0.00 ND 0.0415 0.00
0.00 ND 0.0553 0.00 ND 0.0553 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0404 0.00 ND 0.0404 0.00
0.00 ND 0.0755 0.00 ND 0.0755 0.00
0.00 ND 0.0338 0.00 ND 0.0338 0.00
0.00 ND 0.0798 0.00 ND 0.0798 0.00
Page 4 of 41
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
: · Parameter : ·
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
.. GAS ..
74-87-3
107-05-1
95-49-8
106-43-4
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1,2-Dichlorobenzene 95-50-1
1,3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloropronane 78-87-5
1,3-Dichloroorooane 142-28-9
2,2-Dichloropropane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1 3-Dichlorooropene 10061-01-5
trans-I 3-Dichlorooronene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -0511412002 15 :49
0502HBWD999
2020505408
··•Cone .Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.0509 0.00
0:0785 0.00
0.0359 0.00
0.0684 0.00
0.777 0.00
0.0946 0.00
0.0895 0.00
0.0550 0.00
0.0596 0.00
0.0495 0.00
0.0596 0.00
0.0591 0.00
0.0930 0.00
0.0445 0.00
0.0632 0.00
0.0492 0.00
0.0353 0.00
0.0430 o.oo.
0.0519 0.00
0.0401 0.00
0.0492 0.00
0.0374 0.00
0.0526 0.00
0.0486 0.00
0.0822 0.00
0.0469 0.00
0.155 0.00
0.838 0.00
0502HBWW220 0502HBWW222
2020505401 2020505402
. Cone Flaa.· DL RL Cone Flaa DL RL ..
' ND 0.0509 0.00 ND 0.0509 0.00
ND 0.0785 0.00 ND 0.0785 0.00
ND 0.0359 0.00 ND 0.0359 0.00
ND 0.0684 0.00 NO 0.0684 0.00
ND 0.777 0.00 ND 0.777 0.00
ND 0.0946 0.00 ND . 0.0946 0.00
ND 0.0895 0.00 ND 0.0895 0.00
ND 0.0550 0.00 ND 0.0550 0.00
ND 0.0596 0.00 ND 0.0596 0.00
ND 0.0495 0.00 ND 0.0495 0.00
ND 0.0596 0.00 ND 0.0596 0.00
ND 0.0591 0.00 ND 0.0591 0.00
ND 0.0930 0.00 ND 0.0930 0.00
0.917 0.0445 0.00 ND 0.0445 0.00
ND 0.0632 0.00 ND . 0.0632 0.00
ND 0.0492 0.00 0.139 J 0.0492 0.00
ND 0.0353 0.00 ND 0.0353 0.00
ND 0.0430 0.00 ND 0.0430 0.00
ND 0.0519 0.00 ND 0.0519 0.00
ND 0.0401 0.00 ND 0.0401 0.00
ND 0.0492 0.00 ND 0.0492 0.00
ND 0.0374 0.00 ND 0.0374 0.00
ND 0.0526 0.00 ND 0.0526 0.00
ND 0.0486 0.00 ND 0.0486 0.00
ND 0.0822 0.00 ND 0.0822 0.00
ND 0.0469 0.00 ND 0.0469 0.00
ND 0.155 0.00 ND 0.155 0.00
.. ND 0.838 0.00 ND 0.838 0.00
Page 5 of 41
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter OAS:
Iodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isourouvltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Propanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 1.1.2-Tetrachloroethane 630-20-6
1.1.2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2 3-Trichlorobenzene 87-61-6
1,2,4-Trichlorobenzene 120-82-1
1.1.1-Trichloroethane 71-55-6
1. 1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2.3-Trichloroorooane 96-18-4
1. 1,2-Trichlorotrifluoroethane 76-13-1
1 2.4-Trimethvlbenzene 95-63-6
1 3,5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/I4/2002 I5:49
0502HBWD999
2020505408
·Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
DL
0.0452
0.0769
0.0899
0.175
0.0619
0.473
0.0210
0.0708
0.652
0.0698
0.0295
0.0578
0.109
0.103
1.28
0.0236
0.110
0.140
0.0511
0.0489
0.0506
0.0495
0.117
0.0529
0.0744
0.0616
0.172
0.0501
0502HBWW220 0502HBWW222
2020505401 2020505402
RL Cone Flaa DL RL Cone Flaa DL RL ..
-
0.00 ND 0.0452 0.00 ND 0.0452 0.00
0.00 ND 0.0769 0.00 ND 0.0769 0.00
0.00 ND 0.0899 0.00 ND 0.0899 0.00
0.00 ND 0.175 0.00 ND 0.175 0.00
0.00 ND 0.0619 0.00 ND 0.0619 0.00
0.00 ND 0.473 0.00 ND 0.473 0.00
0.00 ND 0.0210 0.00 ND 0.0210 0.00
0.00 ND 0.0708 0.00 ND 0.0708 0.00
0.00 ND 0.652 0.00 ND 0.652 0.00
0.00 ND 0.0698 0.00 ND 0.0698 0.00
0.00 ND 0.0295 0.00 ND 0.0295 0.00
0.00 ND 0.0578 0.00 ND 0.0578 0.00
0.00 ND 0.109 0.00 ND 0.109 0.00
0.00 ND 0.103 0.00 ND 0.103 0.00
0.00 ND 1.28 0.00 ND 1.28 0.00
0.00 ND 0.0236 0.00 ND 0.0236 0.00
0.00 ND 0.110 0.00 ND 0.110 0.00
0.00. ND 0.140 0.00 ND 0.140 0.00
0.00 ND 0.0511 0.00 ND 0.0511 0.00
0.00 ND 0.0489 0.00 ND 0.0489 0.00
0.00 ND 0.0506 0.00 ND 0.0506 0.00
0.00 ND 0.0495 0.00 ND 0.0495 0.00
0.00 ND 0.117 0.00 ND 0.117 0.00
0.00 ND 0.0529 0.00 ND 0.0529 0.00
0.00 ND 0.0744 0.00 ND 0.0744 0.00
0.00 ND 0.0616 0.00 ND 0.0616 0.00
0.00 ND 0.172 0.00 ND 0.172 0.00
0.00 ND 0.0501 0.00 ND 0.0501 0.00
Page 6 of 41
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
: Parameter<
-.
',,~
p-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
... ,·,._:cAS~" ...
106-42-3
95-47-6
SECTION IV -Analytical Results-05/14/2002 15:49
0502HBWD999
2020505408
, ' ',', -~~ .·cone· . Flaa
ND
ND
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
.. DL RL
0.0869 0.00
0.0409 0.00
0502HBWW220 0502HBWW222
2020505401 2020505402
Cone Flaa DL RL. Cone Flaa DL RL ..
ND 0.0869 0.00 ND 0.0869 0.00
ND 0.0409 0.00 ND 0.0409 0.00
Page 7 of 41
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate eomoound
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWD999
2020505408
Aaueous
Received
NA
05/08/2002 11:50
05/14/2002 00:39
05/14/2002 00:39
1.0000
MSDA
u{!fL
%RecoveN
89
119
108
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
. Limits f
77-117
61-143
87-113
0502HBWW220 0502HBWW222
2020505401 2020505402
Aaueous Aaueous
Received Received
NA NA
05/08/2002 12:50 05/08/2002 13 :55
05/13/2002 21:20 05/13/2002 21 :49
05/13/2002 21 :20 05/13/2002 21:49
1.0000 1.0000
MSDA MSDA
Ul!IL u{!/L
% Recoverv Limits F %Recoverv Limits F
87 77-117 89 77-117
112 61-143 118 61-143
106 87-113 109 87-113
Page 8 of 41
-------------------
---------------~--­SECTION IV
Analytical Results
MS-VOA
SW8260B
: Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
,' -'· ..
Bromochloromethane
'
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
. . .: OAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW224
2020505403
Aqueous
Received
NA
05/08/2002 13:15
05/13/2002 22:17
05/13/2002 22:17
1.0000
MSDA
ug/L
·Cone ··Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.740 J
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
_:DL .RL
1.26 0.00
5.34 0.00
2.85 0.00
0.290 0.00
0.0465 0.00
0.0643 0.00
0.0449 0.00
0.0528 0.00
0.106 0.00
0.0454 0.00
2.83 o.oo.
0.0888 0.00
0.104 0.00
0.0934 0.00
0.0415 0.00
0.0553 0.00
0.0596 0.00
0.0404 0.00
0.0755 0.00
0.0338 0.00
0.0798 0.00
0502HBWW225 0502HBWW226
2020505404 2020505405
Aqueous Aqueous
Received Received
NA NA
05/08/2002 13 :25 05/08/2002 11 :45
05/13/2002 22:46 05/13/2002 23:14
05/13/2002 22:46 05/13/2002 23:14
1.0000 1.0000
MSDA MSDA
u11/T ug/L
·.Cone Fla·a. Dl:. RL cone Flaa DL . RL
ND 1.26 0.00 ND 1.26 0.00
ND 5.34 0.00 ND 5.34 0.00
ND 2.85 0.00 ND 2.85 0.00
ND 0.290 0.00 ND 0.290 0.00
ND 0.0465 0.00 ND 0.0465 0.00
ND 0.0643 0.00 ND 0.0643 0.00
ND 0.0449 0.00 ND 0.0449 0.00
ND 0.0528 0.00 ND :·0.0528 0.00
ND 0.106 0.00 ND 0.106 0.00
ND 0.0454 0.00 ND 0.0454 0.00
ND 2.83 0.00 ND 2.83 0.00
ND 0.0888 0.00 ND 0.0888 0.00
ND 0.104 0.00 ND 0.104 0.00
ND 0.0934 0.00 ND 0.0934 0.00
ND 0.0415 0.00 ND 0.0415 0.00
ND 0.0553 0.00 ND 0.0553 o:oo
ND 0.0596 0.00 ND 0.0596 0.00
ND 0.0404 0.00 ND 0.0404 0.00
ND 0.0755 0.00 ND 0.0755 0.00
ND 0.0338 0.00 ND 0.0338 0.00
ND 0.0798 0.00 ND 0.0798 0.00
Page 9 of 41
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
OAS ..
74-87-3
107-05-1
95-49-8
106-43-4
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
1,1-Dichloroprooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-1 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results-05/14/2002 15:49
0502HBWW224
2020505403
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.118 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396913 (20205054] Hamilton Beach-Proctor Silex
STLAustin
DL
0.0509
0.0785
0.0359
0.0684
0.777
0.0946
0.0895
0.0550
0.0596
0.0495
0.0596
0.0591
0.0930
0.0445
0.0632
0.0492
0.0353
0.0430
0.0519
0.0401
0.0492
0.0374
0.0526
0.0486
0.0822
0.0469
0.155
0.838
0502HBWW225 0502HBWW226
2020505404 2020505405
RL Cone Flaa DL RL Cone Flaa DL RL -
0.00 ND 0.0509 0.00 ND 0.0509 0.00
0.00 ND 0.0785 0.00 ND 0.0785 0.00
0.00 ND 0.0359 0.00 ND 0.0359 0.00
0.00 ND 0.0684 0.00 ND 0.0684 0.00
0.00 ND 0.777 0.00 ND 0.777 0.00
0.00 ND 0.0946 0.00 ND 0.0946 0.00
0.00 ND 0.0895 0.00 ND 0.0895 0.00
0.00 ND 0.0550 0.00 ND 0.0550 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0495 0.00 ND 0.0495 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0591 0.00 ND 0.0591 0.00
0.00 ND 0.0930 0.00 ND 0.0930 0.00
0.00 ND 0.0445 0.00 ND 0.0445 0.00
0.00 ND 0.0632 0.00 ND 0.0632 0.00
0.00 ND 0.0492 0.00 ND 0.0492 0.00
0.00 ND 0.0353 0.00 ·ND 0.0353 0.00
0.00. ND 0.0430 0.00 ND 0.0430 0.00
0.00 ND 0.0519 0.00 ND 0.0519 0.00
0.00 ND 0.0401 0.00 ND 0.0401 0.00
0.00 ND 0.0492 0.00 ND 0.0492 0.00
0.00 ND 0.0374 0.00 ND 0.0374 0.00
0.00 ND 0.0526 0.00 ND 0.0526 0.00
0.00 ND 0.0486 0.00 ND 0.0486 0.00
0.00 ND 0.0822 0.00 ND 0.0822 0.00
0.00 ND 0.0469 0.00 ND 0.0469 0.00
0.00 ND 0.155 0.00 ND 0.155 0.00
0.00 ND 0.838 0.00 ND 0.838 0.00
Page 10 of 41
--------------------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
.. ,Parameter .
n-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS.
106-42-3
95-47-6
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW224
2020505403
Cone. Flaa
ND
ND
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.0869 0.00
0.0409 0.00
0502HBWW225 0502HBWW226
2020505404 2020505405
Cone Flaa Dl RL Cone Flaa DL RL ..
ND 0.0869 0.00 ND 0.0869 0.00
ND 0.0409 0.00 ND 0.0409 0.00
Page 12 of 41
-------------------
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
0502HBWW224
2020505403
Aaueous
Received
NA
05/08/2002 13:15
05/13/2002 22: 17
05/13/2002 22:17
1.0000
MSDA
ug/L
· Surroaate::comoound %Recbverv .. ·•Limits
l-Bromo-4-fluorobenzene 87
1 2-Dichloroethane-d4 118
Toluene-dB 107
SECTION IV -Analytical Results -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
77-117
61-143
87-113
_f
0502HBWW225 0502HBWW226
2020505404 2020505405
Aaueous Aqueous
Received Received
NA NA
05/08/2002 13 :25 05/08/2002 11 :45
05/13/2002 22:46 05/13/2002 23:14
05/13/2002 22:46 05/13/2002 23:14
1.0000 1.0000
MSDA MSDA
ug/L ug/L
%:Recoverv :Limits F ·. %. Recoverv · Limits f,
87 77-117 89 77-117
116 61-143 115 61-143
106 87-113 107 87-113
Page 13 of 41
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene .
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAs··
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/14/2002 15 :49
0502HBWW230
2020505406
Aqueous
Received
NA
05/08/2002 11: 10
05/13/2002 23:43
05/13/2002 23:43
1.0000
MSDA
u!!IL
cone· ·p1aa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
DL.
1.26
5.34
2.85
0.290
0.0465
0.0643
0.0449
0.0528
0.106
0.0454
2.83
0.0888
0.104
0.0934
0.0415
0.0553
0.0596
0.0404
0.0755
0.0338
0.0798
0502HBWW234 TRIP BLANK
2020505407 2020505409
Aqueous Aqueous
Received Received
NA NA
05/08/2002 13 :40 05/08/2002 00:00
05/14/2002 00:11 05/13/2002 19:24
05/14/2002 00: 11 05/13/2002 19:24
1.0000 1.0000
MSDA MSDA
u!!IL u!!IL
RL Cone· Flaa DL Rl.. Cone Flaa DL RL.
0.00 ND 1.26 0.00 ND 1.26 0.00
0.00 ND 5.34 0.00 ND 5.34 0.00
0.00 ND 2.85 0.00 ND 2.85 0.00
0.00 ND 0.290 0.00 ND 0.290 0.00
0.00 ND 0.0465 0.00 ND 0.0465 0.00
0.00 ND 0.0643 0.00 ND 0.0643 0.00
0.00 ND 0.0449 0.00 ND 0.0449 0.00
0.00 ND 0.0528 0.00 ND 0.0528 0.00
0.00 ND 0.106 0.00 ND 0.106 0.00
0.00 ND 0.0454 0.00 ND 0.0454 0.00
o.oo. ND 2.83 0.00 ND 2.83 0.00
0.00 ND 0.0888 0.00 ND 0.0888 0.00
0.00 ND 0.104 0.00 ND 0.104 0.00
0.00 ND 0.0934 0.00 ND 0.0934 0.00
0.00 ND 0.0415 0.00 ND 0.0415 0.00
0.00 ND 0.0553 0.00 ND 0.0553 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0404 0.00 ND 0.0404 0.00
0.00 ND 0.0755 0.00 ND 0.0755 0.00
0.00 ND 0.0338 0.00 ND 0.0338 0.00
0.00 ND 0.0798 0.00 ND 0.0798 0.00
Page 14 of 41
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter .
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
" "
Client Sample ID
Lab Sample ID
" · , _ :b'ASi' •··
74-87-3
107-05-1
95-49-8
106-43-4
1,2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1,3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1,1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-1,2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1,3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
1.1-Dichloroorooene 563-58-6
c
,,,.,,
cis-1 3-Dichloroorooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1,3-butadiene 87-68-3
2-Hexanone , 591-78-6
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW230
2020505406
:cone'. :• Flaa·
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
DL -~
0.0509
0.0785
0.0359
0.0684
0.777
0.0946
0.0895
0.0550
0.0596
0.0495
0.0596
0.0591
0.0930
0.0445
0.0632
0.0492
0.0353
0.0430
0.0519
0.0401
0.0492
0.0374
0.0526
0.0486
0.0822
0.0469
0.155
0.838
0502HBWW234 TRIP BLANK
2020505407 2020505409
.RL. ., cone··. i=1aa· .DL Rf Cone Flaa .. bl -·.RL . , -.
0.00 ND 0.0509 0.00 ND 0.0509 0.00
0.00 ND 0.0785 0.00 ND 0.0785 0.00
0.00 ND 0.0359 0.00 ND 0.0359 0.00
0.00 ND 0.0684 0.00 ND 0.0684 0.00
0.00 ND 0.777 0.00 ND 0.777 0.00
0.00 ND 0.0946 0.00 ND ·0.0946 0.00
0.00 ND 0.0895 0.00 ND ···0.0895 0.00
0.00 ND 0.0550 0.00 ND 0.0550 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0495 0.00 ND 0.0495 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0591 0.00 ND 0.0591 0.00
0.00 ND 0.0930 0.00 ND 0.0930 0.00
0.00 ND 0.0445 0.00 ND _0.0445 0.00
0.00 ND 0.0632 0.00 ND :t>.0632 0.00
0.00 ND 0.0492 0.00 ND 0.0492 0.00
0.00 ND 0.0353 0.00 ND 0.0353 0.00
o.oo. ND 0.0430 0.00 ND 0.0430 0.00
0.00 ND 0.0519 0.00 ND 0.0519 0.00
0.00 ND 0.0401 0.00 ND 0.0401 0.00
0.00 ND 0.0492 0.00 ND 0.0492 0.00
0.00 ND 0.0374 0.00 ND 0.0374 0.00
0.00 ND 0.0526 0.00 ND 0.0526 0.00
0.00 ND 0.0486 0.00 ND 0.0486 0.00
0.00 ND 0.0822 0.00 ND 0.0822 0.00
0.00 ND 0.0469 0.00 ND 0.0469 0.00
0.00 ND 0.155 0.00 ND 0.155 0.00
0.00 ND 0.838 0.00 ND 0.838 0.00
Page 15 of 41
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter OAS
lodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 1 1.2-Tetrachloroethane 630-20-6
1 1 2,2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-61-6
1.2.4-Trichlorobenzene 120-82-1
1 1.1-Trichloroethane 71-55-6
1 1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2.3-Trichloropropane 96-18-4
1 1 2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW230
2020505406
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LJMS Workorder: 80396913 (20205054] Hamilton Beach-Proctor Silex
STLAustin
DL
0.0452
0.0769
0.0899
0.175
0.0619
0.473
0.0210
0.0708
0.652
0.0698
0.0295
0.0578
0.109
0.103
1.28
0.0236
0.110
0.140
0.0511
0.0489
0.0506
0.0495
0.117
0.0529
0.0744
0.0616
0.172
0.0501
0502HBWW234 TRIP BLANK
2020505407 2020505409
Rt Cone. Flaa DL RL Cone Flaa bl RL ..
0.00 ND 0.0452 0.00 ND 0.0452 0.00
0.00 ND 0.0769 0.00 ND 0.0769 0.00
0.00 ND 0.0899 0.00 ND 0.0899 0.00
0.00 ND 0.175 0.00 ND 0.175 0.00
0.00 ND 0.0619 0.00 ND 0.0619 0.00
0.00 ND 0.473 0.00 ND 0.473 0.00
0.00 ND 0.0210 0.00 0.114 J 0.0210 0.00
0.00 ND 0.0708 0.00 ND 0.0708 0.00
0.00 ND 0.652 0.00 ND 0.652 0.00
0.00 ND 0.0698 0.00 ND 0.0698 0.00
0.00 ND 0.0295 0.00 ND 0.0295 0.00
0.00 ND 0.0578 0.00 ND 0.0578 0.00
0.00 ND 0.109 0.00 ND 0.109 0.00
0.00 ND 0.103 0.00 ND 0.103 0.00
0.00 ND 1.28 0.00 ND 1.28 0.00
0.00 ND 0.0236 0.00 ND 0.0236 0.00
0.00 ND 0.110 0.00 ND 0.110 0.00 o.oo. ND 0.140 0.00 ND 0.140 0.00
0.00 ND 0.0511 0.00 ND 0.0511 0.00
0.00 ND 0.0489 0.00 ND 0.0489 0.00
0.00 ND 0.0506 0.00 ND 0.0506 0.00
0.00 ND 0.0495 0.00 ND 0.0495 0.00
0.00 ND 0.117 0.00 ND 0.117 0.00
0.00 ND 0.0529 0.00 ND 0.0529 0.00
0.00 ND 0.0744 0.00 ND 0.0744 0.00
0.00 ND 0.0616 0.00 ND 0.0616 0.00
0.00 ND 0.172 0.00 ND 0.172 0.00
0.00 ND 0.0501 0.00 ND 0.0501 0.00
Page 16 of 41
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
'' ·Parameter :. · · :. ·
o-Xvlene/m-Xvlene
o-Xvlene
• <
Client Sample ID
Lab Sample ID
. -_:. :.ex~:~:> :'. ~ ..
106-42-3
95-47-6
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW230
2020505406
J~onc· ffaa '
ND
ND
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
DL' RL
0.0869 0.00
0.0409 0.00
0502HBWW234 TRIP BLANK
2020505407 2020505409
·cone Fiaa DL · RL Cone Flaa DL RL
ND 0.0869 0.00 ND 0.0869 0.00
ND 0.0409 0.00 ND 0.0409 0.00
Page 17 of 41
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Comnound
1-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-dB
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW230
2020505406
Aaueous
Received
NA
05/08/2002 11: 10
05/13/2002 23:43
05/13/2002 23:43
1.0000
MSDA
ut!IL
% Recoverv
86
115
106
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0502HBWW234 TRIP BLANK
2020505407 2020505409
Aaueous Aaueous
Received Received
NA NA
05/08/2002 13:40 05/08/2002 00:00
05/14/2002 00:11 05/13/2002 19:24
05/14/2002 00: 11 05/13/2002 19:24
1.0000 1.0000
MSDA MSDA
ul?/L ut!IL
%Recovery Limits F % Recovery Limits F
86 77-117 87 77-117
116 61-143 115 61-143
106 87-113 109 87-113
Page 18 of 41
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 27619 Instrument Data File: A0513202.D
Instrument ID: MSDA Analyst: BJP
Parameter. ,,, Reference Value
Acetone 20
Acetonitrile 100
Acrolein 100
Acrvlonitrile 100
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone (MEK) 20
n-Butylbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
2-Chloro-1 3-butadiene 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
1-Chlorohexane 20
Chloromethane 20
3-Chloroorooene 20
2-Chlorotoluene 20
4-Chlorotoluene 20
l .2-Dibromo-3-chloropropane 20
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [2'0205054] Hamilton Beach-Proctor Silex
STLAustin
Measured· Cone Flaa .
18.6
132
53.8
97.0
19.4
20.4
20.0
21.5
17.7
21.0
18.2
21.0
20.5
20.9
19.9
22.2
20.8
18.8
21.5
21.3
18.4
21.3
22.5
20.6
20.5
17.4
.. '
Dateffime Analyzed:05/13/2002 11:O1
Units: ug/L
. %Recove..V · Flad · QC Limits %Recoverv
93
132
54
97
97
102
100
108
89
105
91
105
102
105
100
111
104
94
108
107 80-120
92
107
113
103
102
87
Page 19 of 41
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 27619 Instrument Data File: A0513202.D
Instrument ID: MSDA Analyst: BJP
Continued
Parameter ~eterence Value
Dibromochloromethane 20
1 2-Dibromoethane 20
Dibromomethane 20
trans-1.4-Dichloro-2-butene 20
1.4-Dichlorobenzene 20
1,2-Dichlorobenzene 20
1 3-Dichlorobenzene 20
Dichlorodifluoromethane 20
1 1-Dichloroethane 20
1 2-Dichloroethane 20
1 1-Dichloroethene 20
cis-1.2-Dichloroethene 20
trans-1 2-Dichloroethene 20
1 2-Dichloropropane 20
1 3-Dichlorooronane 20
2 2-Dichloropropane 20
1 1-Dichloronronene 20
cis-1 3-Dichloronrooene 20
trans-1.3-Dichloropropene 20
Ethvl methacrvlate 20
Ethvlbenzene 20
Hexachloro-1 3-butadiene 20
2-Hexanone 20
Iodomethane 20
Isooroovlbenzene 20
4-Isopronvltoluene 20
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
Measured Cone Flag
20.1
19.6
20.5
24.3
19.0
19.2
19.3
18.1
22.7
23.7
20.0
19.6
20.7
19.8
18.5
20.1
20.5
19.2
18.2
17.5
18.8
20.0
17.7
19.5
18.9
20.8
Dateffime Analyzed:05/13/2002 11:01
Units: ug/L
%Recoveni Flag QC Limits %Recoverv
101
98
103
122
95
96
96
91
113
118
100 80-120
98
104
99 80-120
92
100
103
96
91
88
94 80-120
100
89
98
94
104
Page 20 of 41 ----·---------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 27619 Instrument Data File: A0513202.D
Instrument ID: MSDA Analyst: BJP
Continued
Parameter ·Reference,Value .·
Methyl methacrvlate 20
Methvl tert-butvl ether (MTBE) 20
4-Methyl-2-oentanone (MIBK) 20
Methylene chloride 20
Naohthalene 20
Prooanenitrile 100
n-ProoYlbenzene 20
Stvrene 20
1 1 1,2-Tetrachloroethane 20
1 1.2.2-Tetrachloroethane 20
Tetrachloroethene 20
Tetrahvdrofuran 20
Toluene 20
1 2.3-Trichlorobenzene 20
1 2 4-Trichlorobenzene 20
1 1.1-Trichloroethane 20
1 1,2-Trichloroethane 20
Trichloroethene 20
Trichlorofluoromethane 20
1 2,3-Trichloropropane 20
I 1.2-Trichlorotrifluoroethane 20
I 2.4-Trimethylbenzene 20
I 3.5-Trimethvlbenzene 20
Vinyl acetate 20
Vinvl chloride 20
o-Xylene/m-Xylene 40
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
. Measured Cone .ffaa.
18.0
22.4
19.0
20.8
16.2
109
21.1
18.3
18.2
17.4
18.9
21.2
18.8
15.4
17.l
22.6
18.8
20.l
31.0
18.6
21.7
22.l
21.8
18.2
21.0
36.4
Dateffime Analyzed:05/13/2002 11:01
Units: ug/L
.%Recover.1 Flaa QC Limits %Recoverv
90
112
95
104
81
109
106
92
91
87
95
106
94 80-120
77
85
113
94
101
155
93
108
111
109
91
105 80-120
91
Page 21 of 41
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 27619 Instrument Data File: A0513214.D
Instrument ID: MSDA Analyst: BJP
Parameter :: ,, '· .. ' Jteferenc:& Value· . ·
Acetone 20
Acetonitrile 100
Acrolein 100
Acrvlonitrile 100
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Bromomethane 20
2-Butanone (MEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
2-Chloro-1.3-butadiene 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
1-Chlorohexane 20
Chloromethane 20
3-Chloroorooene 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1.2-Dibromo-3-chloroorooane 20
SECTION V -Calibration and QC Infonnation -0511412002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Measured Cone. Flag
17.1
117
52.0
95.4
18.7
18.8
19.7
20.3
14.1
20.3
17.2
19.2
19.0
19.5
16.7
19.7
20.3
18.0
20.9
20.9
17.3
20.4
18.8
19.4
19.l
14.9
Dateffime Analyzed:05/13/2002 16:57
Units: ug/L
%Recoverv Flag . QC Limits %Recoverv
86
117
52
95
94
94
99
101
71
102
86
96
95
98
83
99
102
90
105
105 80-120
87
102
94
97
96
75
Page 23 of 41
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 27619 Instrument Data File: A0513214.D
Instrument ID: MSDA Analyst: BJP
Continued
Parameter ··Reference Value
Dibroinochloroinethane 20
1.2-Dibromoethane 20
Dibroinoinethane 20
trans-1.4-Dichloro-2-butene 20
1.4-Dichlorobenzene 20
1.2-Dichlorobenzene 20
1.3-Dichlorobenzene 20
Dichlorodifluoroinethane 20
1.1-Dichloroethane 20
1,2-Dichloroethane 20
1.1-Dichloroethene 20
cis-1 2-Dichloroethene 20
trans-1 2-Dichloroethene 20
l 2-Dichloropropane 20
1 3-Dichloroorooane 20
2.2-Dichloropropane 20
1.1-Dichloroprooene 20
cis-1.3-Dichloropropene 20
trans-1,3-Dichloroorooene 20
Ethvl methacrvlate 20
Ethvlbenzene 20
Hexachloro-1.3-butadiene 20
2-Hexanone 20
Iodoinethane 20
lsopropvlbenzene 20
4-Isooroovltoluene 20
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Measured Cone ·Flaa
16.8
18.7
20.0
21.9
17.7
17.4
17.8
18.0
22.2
23.0
19.8
19.0
20.5
19.0
18.2
18.3
19.7
17.4
16.1
15.9
17.5
17.8
16.0
18.8
17.9
18.9
Datetrime Analyzed:05/13/2002 16:57
Units: ug/L
%Recoverv Flaa ·QC Limits %Recoverv
84
93
100
110
89
87
89
90
111
115
99 80-120
95
103
95 80-120
91
92
99
87
81
79
88 80-120
89
80
94
90
95
Page 24 of 41
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 27619 Instrument Data File: A0513214.D
Instrument ID: MSDA Analyst: BJP
Continued
/Parameter Reference Value
Methvl methacrvlate 20
Methvl tert-butvl ether (MTBE) 20
4-Methvl-2-oentanone (MIBK) 20
Methvlene chloride 20
Naohthalene 20
Propanenitrile 100
n-Proovlbenzene 20
Stvrene 20
I 1 l.2-Tetrachloroethane 20
I I 2,2-Tetrachloroethane 20
Tetrachloroethene 20
Tetrahvdrofuran 20
Toluene 20
I 2 3-Trichlorobenzene 20
I 2.4-Trichlorobenzene 20
1 I. I -Trichloroethane 20
1 I 2-Trichloroethane 20
Trichloroethene 20
Trichlorofluoromethane 20
I 2.3-Trichloroorooane 20
I I 2-Trichlorotrifluoroethane 20
I 2.4-Trimethvlbenzene 20
1 3.5-Trimethvlbenzene 20
Vinyl acetate 20
Vinvl chloride 20
o-Xvlene/m-Xvlene 40
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Measured. Cone flaa
I5.9
21.2
I7.7
20.3
13.5
98.8
I9.6
I7.I
I6.6
I7.3
18.0
20.1
I7.9
I2.5
14.5
21.0
I8.6
I9.2
28.0
17.9
20.6
20.7
20.5
16.8
20.5
35.l
Dateffime Analyzed:05/13/2002 16:57
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
80
106
88
lOI
67
99
98
85
83
86
90
IOl
90 80-I20
63
73
105
93
96
140
90
103
104
103
84
102 80-I20
88
Page 25 of 41
-------------------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW82608
BFB
Analysis Batch ID: 27619
Instrument ID: MSDA
Instrument Data File: A0513202.D
Injection Time: 05/13/2002 11:01
-Ion Abundance Criteria_
MassLEnerov , '" · •. Lower limit · ·
50 15
75 30
95 100
96 5
173 0
174 50
175 5
176 95
177 5
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Unner Limit
40
60
100
9
2
9
IOI
9
Date Analyzed: 05/13/2002 11 :0 I
Analyst: BJP
· % Relative Abundance ·
25.I
46.1
100
6.8
0
78.4
7.1
98.2
6.6
Page 27 of 41
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 27619
Instrument ID: MSDA
Instrument Data File: A0513214.D
Injection Time: 05/13/2002 16:57
Ion Abundance Criteria
Mass/Enerav . .lower Limit ..
50 15
75 30
95 100
96 5
173 0
174 50
175 5
176 95
177 5
SECTION V -Calibration and QC Infonnation -05/14/2002 15:49
LIMS Workorder: 80396913 (20205054] Hamilton Beach-Proctor Silex
STLAustin
Unnerlimit
40
60
100
9
2
9
101
9
Date Analyzed: 05/13/2002 16:57
Analyst: BJP
% Relative Abundance
24.6
47.2
100
6.7
0
53.5
7.5
99.1
6.4
Page 28 of 41
-------------------
-------------------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone rMEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1,3-butadiene
Chlorobenzene
· Chloroethane
Chloroform
1-Chlorohexane
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chloroto luene
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
.OAS, .. ''' ~, '
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
95-49-8
106-43-4
1038317
Method Blank
Aaueous
05/13/2002 13:01
05/13/2002 13:01
MSDA
ug/L
Gone .. Flaa·
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
DL RL · Cone Flag DL Rl ·Cone Flaa DL, 'RL.
1.26 0.00
5.34 0.00
2.84 0.00
0.290 0.00
0.0465 0.00
0.0643 0.00
0.0449 0.00
0.0528 0.00
0.106 0.00
0.0454 0.00
2.83 0.00
0.0888 0.00
0.104 0.00
0.0934 0.00
0.0415 0.00
0.0553 0.00
0.0596 0.00
0.0404 0.00
0.0755 0.00
0.0338 0.00
0.0798 0.00
0.0509 0.00
0.0785 0.00
0.0359 0.00
0.0684 0.00
Page 29 of 41
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS.
l .2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1,2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1 2-Dichloropropane 78-87-5
1 3-Dichloroprooane 142-28-9
2,2-Dichloropropane 594-20-7
1.1-Dichloroprooene 563-58-6
cis-1 3-Dichloroprooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
Iodomethane 74-88-4
Isopropvlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
1038317
Cone
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
Flaa DL RL Cone Flag DL RL Cone Fla'a · DL RL
0.777 0.00
0.0946 0.00
0.0895 0.00
0.0550 0.00
0.0596 0.00
0.0495 0.00
0.0596 0.00
0.0591 0.00
0.0930 0.00
0.0445 0.00
0.0632 0.00
0.0492 0.00
0.0353 0.00
0.0430 0.00
0.0519 0.00
0.0401 0.00
0.0492 0.00
0.0374 0.00
0.0526 0.00
0.0486 0.00
0.0822 0.00
0.0469 0.00
0.155 0.00
0.838 0.00
0.0452 0.00
0.0769 0.00
0.0899 0.00
0.175 0.00
0.0619 0.00
Page 30 of 41
-------------------
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Surroaate Comoound
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
1038317
Method Blank
Aqueous
05/13/2002 13:01
05/13/2002 13:01
MSDA
ul!IL
'" %Recoverv
85
110
104
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Limits F % Recoverv Limits F % Recoverv Limits F
77-117
61-143
87-113
Page 32 of 41
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
LCS for HBN 27619 [MSV/1852]
27619
Analysis Batch ID: 27619
; ,, ,, :_ > t ',.,,, ,, . -~ ' ' ', ·~ ~ ' .,
:-f '':: :<:
Rarameter': , , ,I,,, ,' ~;' <'.• , ·, "/,r, , ,
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
l ,2-Dibromo-3-chloropropane
Dibromochloromethane
l ,2-Dibromoethane
Dibromomethane
1,4-Dichlorobenzene
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
Contro IS amne
·Lab ID; · to·aa3ts
, FileJD: A0513203.D
. SPk'Amt. Cone , •' %Rec Fla·
20 23.5 117
20 22.0 110
20 20.8 104
20 19.9 99
20 21.8 109
20 19.2 96
20 17.2 86
20 20.6 103
20 21.9 110
20 21.3 107
20 21.5 108
20 18.7 94
20 22.7 114
20 20.2 101
20 21.8 109
20 22.l 110
20 18.7 93
20 21.4 107
20 21.1 106
20 17.8 89
20 21.2 106
20 21.0 105
20 21.5 107
20 19.9 99
Lab ID:.
FileU):
.SPkAmt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture:
Analyst:
NA
BJP
c ontro amne un 1cate IS 1 D r
1038316.
A0513204.D
.cone . 0ioRec Fla
24.5 123
22.7 114
21.2 106
20.7 103
22.3 111
19.5 97
16.7 84
17.9 90
21.7 108
21.4 107
21.8 109
18.9 95
22.8 114
20.7 103
22.2 111
22.6 113
18.5 93
21.5 108
21.6 108
19.2 96
22.1 111
21.7 109
22.5 113
20.7 104
QC Limits
RPO Fla %Rec . RPO
5 0.1-240 71
3.6 71-133 17
1.9 67-127 12
4 61-145 21
1.8 57-135 19
1 23-151 17
2.4 34-128 25
13 0.1-214 39
1.8 28-184 30
0 45-160 31
0.9 65-148 27
1 29-223 23
0 46-150 23
2 77-129 14
1.8 39-133 27
2.7 64-146 16
0 18-140 26
0.9 70-136 24
1.9 74-132 23
7.6 39-171 25
4.6 45-137 15
3.7 19-187 19
5.4 52-138 21
4.9 70-132 13
Page 33 of 41
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Parameter
1.2-Dichlorobenzene
1,3-Dichlorobenzene
Dichlorodifluoromethane
1.1-Dichloroethane
1,2-Dichloroethane
1.1-Dichloroethene
cis-1.2-Dichloroethene
trans-1 2-Dichloroethene
1 2-Dichloroorooane
1 3-Dichloropropane
2.2-Dichloroorooane
1 1-Dichloropropene
cis-1.3-Dichloroorooene
trans-I 3-Dichloroorooene
Ethvlbenzene
Hexachloro-1 3-butadiene
2-Hexanone
Iodomethane
lsoproovlbenzene
4-Isooroovltoluene
4-Methvl-2-oentanone (MlBK)
Methylene chloride
Naohthalene
n-Proovlbenzene
Stvrene
1.1 1 2-Tetrachloroethane
1.1.2 2-Tetrachloroethane
Tetrachloroethene
Toluene
1 2,3-Trichlorobenzene
1 2.4-Trichlorobenzene
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
C t IS on ro amo e contmue d
1038315 Lab ID:
A0513203.D File ID:
Cone %Rec Fla Sok Amt
19.4 97 20
19.4 97 20
14.3 71 20
23.1 116 20
23.7 119 20
20.4 102 20
20.0 100 20
21.7 109 20
20.1 101 20
19.4 97 20
21.1 106 20
21.0 105 20
19.2 96 20
18.2 91 20
20.0 100 20
19.9 100 20
18.8 94 20
19.2 96 20
20.0 100 20
22.0 110 20
19.0 95 20
20.8 104 20
16.9 85 20
22.0 110 20
19.0 95 20
18.7 94 20
17.8 89 20
21.0 105 20
19.7 99 20
16.3 82 20
17.0 85 20
c ontro amo.e uo 1cate continued IS I D r
1038316
A0513204.D QC Limits
Cone %Rec Fla RPD Fla %Rec. RPO
20.0 100 3 67-135 14
20.1 101 4 68-134 14
15.8 79 11 0.1-166 26
23.7 119 2.6 66-138 19
24.6 123 3.3 48-152 23
21.0 105 2.9 47-175 25
20.5 102 2 66-144 18
22.0 110 0.9 62-146 22
20.8 104 2.9 61-133 17
20.3 101 4 70-128 16
21.0 105 0.9 40-168 30
21.5 107 1.9 71-155 31
20.0 100 4.1 36-142 16
18.9 95 4.3 34-138 21
20.4 102 2 75-131 14
19.6 98 2 46-150 34
20.4 102 8.2 22-164 34
19.8 99 3.1
19.6 98 2 54-152 26
21.9 109 0.9 41-165 28
21.8 109 14 27-149 36
21.2 106 1.9 36-166 23
18.7 94 IO 32-172 22
21.6 108 1.8 61-143 28
20.l 100 5.1 68-136 14
19.0 95 1 63-141 20
18.5 93 4.4 47-143 20
25.7 129 20 0 69-137 16
19.9 99 0 70-132 17
17.0 85 3.6 66-140 20
18.2 91 6.8 66-144 22
Page 34 of 41
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Parameter
1 LI -Trichloroethane
1 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1 2.3-Trichloroorooane
1 2 4-Trimethvlbenzene
1 3 5-Trimethvlbenzene
Vinvl acetate
Vinvl chloride
o-Xvlene/m-Xylene
o-Xvlene
, ,
--~ ', .,
SECTION V -Calibration and QC Infonnation -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Control Samole continued
. Lab ID: 1'038~15
File Ilk A0513203.D
Sok Amt Cone %Rec :Flci. ·
20 22.8 114
20 18.6 93
20 20.9 104
20 28.0 140
20 19.2 96
20 22.3 112
20 22.4 112
20 3.20 16
20 17.5 87
40 39.0 97
20 19.2 96
Control Sample Duplicate continued
L~bJD: 1038316
. File ID: A0513204.D QC Limit~
Sok Amt tone .%Rec Fla RPO Fla %Rec. RPO
20 23.4 117 2.6 49-155 24
20 19.7 99 6.2 67-135 17
20 21.6 108 3.8 71-129 17
20 27.7 139 0.7 39-147 29
20 19.8 99 3.1 64-140 18
20 22.5 113 0.9 54-156 25
20 22.8 114 '1.8 62-144 25
20 2.91 15 6.4 0.1-164 31
20 17.6 88 1.1 24-138 27
40 39.6 99 2 76-134 15
20 19.4 97 1 77-131 15
Page 35 of 41
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Surroaate Comoounds
1-Bromo-4-fluorobenzene
l .2-Dichloroethane-d4
Toluene-d8
SECTION V -Calibration and QC Information -05/14/2002 15:49
LIMS Workorder: 803969 I 3 [20205054] Hamilton Beach-Proctor Silex
STLAustin
lab ID: 1038315
%Recoverv Flaas
90
108
105
Lab ID: 1038316
%Recoverv Fla as QC RecovelV Limits
90 77-117
110 61-143
109 87-113
Page 36 of 41
-------------------
-------------------SECTIONVI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 27619
" ~' ~ '{, '', ' ' ,,
· Clittnt Samole :io ' "' " ' ' A! ¥ ~' ~ ; ; ) :tab~·sam~1e io ·
INSTRUMENT QC 1000
INSTRUMENT QC 1406
LCS for HBN 27619 rMSV/18521 1038315
LCSD for HBN 27619 fMSV/18521 1038316
MB for HBN 27619 rMSV/18521 1038317 zzzzzzzzzz 2020501501 zzzzzzzzzz 2020506001 zzzzzzzzzz 2020505801 zzzzzzzzzz 2020506101 zzzzzzzzzz 2020505901 zzzzzzzzzz 2020501501
INSTRUMENT QC 1000
INSTRUMENT QC 1406 zzzzzzzzzz 1038318 zzzzzzzzzz 1038319 zzzzzzzzzz 2020503801
TRIP BLANK 2020505409 zzzzzzzzzz 2020506101 zzzzzzzzzz 2020504202 zzzzzzzzzz 2020504201
0502HBWW220 2020505401
0502HBWW222 2020505402
0502HBWW224 2020505403
0502HBWW225 2020505404
0502HBWW226 2020505405
0502HBWW230 2020505406
0502HBWW234 2020505407
0502HBWD999 2020505408
SECTION VI -Batch Summaries -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Start Date/Time: 05/13/2002 11:01 Analyst: BJP
Stop Date/Time: 05/14/2002 02:05
-Samole Size
·. Samole Tvoe Matrix Initial . Final Preoaration Method ' .
GC/MS Tune Aaueous 15mL 15mL SW8260B
Continuing Calibration Check Aaueous 15mL 15mL SW8260B
Lab Control Sample Aaueous 15mL 15mL SW8260B
Lab Control Sample Duplicate Aaueous 15mL 15mL SW8260B
Method Blank Aaueous 15mL 15mL SW8260B
Field Sample Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Sample Aaueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Sample Aqueous 15mL 15mL SW8260B
Field Sample Aqueous 15mL 15mL SW8260B
GC/MS Tune Aaueous 15mL 15mL SW8260B
Continuing Calibration Check Aaueous 15mL 15 mL SW8260B
Matrix Soike Aqueous 15mL 15 mL SW8260B
Matrix Spike Duplicate Aaueous l5mL 15mL SW8260B
Field Sample Aqueous 15mL 15mL SW8260B
Field Sample Aaueous 15mL 15mL SW8260B
Field Sample Aqueous 15mL 15mL SW8260B
Field Sample Aaueous 15mL 15mL SW8260B
Field Sample Aqueous 15mL 15mL SW8260B
Field Sample Aaueous 15mL 15mL SW8260B
Field Sample Aqueous 15mL 15mL SW8260B
Field Samole Aaueous 15mL 15mL SW8260B
Field Sample Aaueous 15mL 15mL SW8260B
Field Sample Aqueous 15mL 15mL SW8260B
Field Sample Aaueous 15 mL 15mL SW8260B
Field Sample Aqueous 15mL 15mL SW8260B
Field Samole .Aqueous 15mL 15mL SW8260B
Page 37 of 41
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 27619 continued
..
Client Sample ID ' Lab Sample ID zzzzzzzzzz 2020503802
zzzzzzzzzz 2020503803 zzzzzzzzzz 2020503804
SECTION VI -Batch Summaries -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Sample Size
SamoleTvoe Matrix Initial Final Preoa·ration Method
Field Samole Aaueous 15mL 15mL SW8260B
Field Sample Aaueous 15 mL 15mL SW8260B
Field Sample Aqueous 15 mL 15mL SW8260B
Page 38 of 41
-------------------
-------------------SECTIONVI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 27619
··sequence . Client Samofo ID_
1 INSTRUMENT QC
2 INSTRUMENT OC
•'
'" i-,-'
' '
3 LCS for HBN 27619 fMSV/18521
4 LCSD for HBN 27619 fMSV/18521
5 MB for HBN 27619 fMSV/18521
6 zzzzzzzzzz
7 zzzzzzzzzz
8 zzzzzzzzzz
9 zzzzzzzzzz
10 zzzzzzzzzz
11 zzzzzzzzzz
12 INSTRUMENT QC
13 INSTRUMENT OC
14 zzzzzzzzzz
15 zzzzzzzzzz
16 zzzzzzzzzz
17 TRIP BLANK
18 zzzzzzzzzz
19 zzzzzzzzzz
20 zzzzzzzzzz
21 0502HBWW220
22 0502HBWW222
23 0502HBWW224
24 0502HBWW225
25 0502HBWW226
26 0502HBWW230
27 0502HBWW234
28 0502HBWD999
29 zzzzzzzzzz
SECTION VI -Batch Summaries -05/14/2002 15:49
LIMS Workorder: 80396913 (20205054] Hamilton Beach-Proctor Silex
STLAustin
Instrument ID: MSDA Analyst: BJP
Anal vs is . Sub-
.Lab Samole ID bate Time SamoleTvoe Analvsis File -ID Batch ID
1000 05/13/2002 11:01:00 GC/MS Tune A0513202.D 0
1406 05/13/2002 11:01:00 Continuing Calibration Check A0513202.D 0
1038315 05/13/2002 11:34:00 Lab Control Samole A0513203.D 0
1038316 05/13/2002 12:03:00 Lab Control Samole Duolicate A0513204.D 0
1038317 05/13/2002 13:01:00 Method Blank A0513206.D 0
2020501501 05/13/2002 13:30:00 Field Samole A0513207.D 0
2020506001 05/13/2002 14:00:00 Field Sample A0513208.D 0
2020505801 05/13/2002 14:30:00 Field Samole A0513209.D 0
2020506101 05/13/2002 15:00:00 Field Sample A0513210.D. 0
2020505901 05/13/2002 15:30:00 Field Sample A0513211.D 0
2020501501 05/13/2002 16:00:00 Field Sample A0513212.D 0
1000 05/13/2002 16:57:00 GC/MSTune A0513214.D 0
1406 05/13/2002 16:57:00 Continuing Calibration Check A0513214.D 0
1038318 05/13/2002 17:27:00 Matrix Soike A0513215.D 0
1038319 05/13/2002 17:57:00 Matrix Spike Duplicate A0513216.D 0
2020503801 05/13/2002 18:55:00 Field Samole A0513218.D 0
2020505409 05/13/2002 19:24:00 Field Samole A0513219.D 0
2020506101 05/13/2002 19:53:00 Field Sample A0513220.D 0
2020504202 05/13/2002 20:22:00 Field Samole A0513221.D 0
2020504201 05/13/2002 20:51:00 Field Sample A0513222.D 0
2020505401 05/13/2002 21:20:00 Field Samole A0513223.D 0
2020505402 05/13/2002 21:49:00 Field Sample A0513224.D· 0
2020505403 05/13/2002 22:17:00 Field Samole A0513225.D 0
2020505404 05/13/2002 22:46:00 Field Samole A0513226.D 0
2020505405 05/13/2002 23:14:00 Field Sample A0513227.D 0
2020505406 05/13/2002 23:43:00 Field Sample A0513228.D 0
2020505407 05/14/2002 00:11:00 Field Sample A0513229.D 0
2020505408 05/14/2002 00:39:00 Field Sample A0513230.D 0
2020503802 05/14/2002 01:08:00 Field Sample A0513231.D 0
Page 39 of 41
SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 27619
Seauence Client Samole ID
30 zzzzzzzzzz
31 zzzzzzzzzz
SECTION VI -Batch Summaries -05/14/2002 15:49
continued
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
Lab Samole ID
2020503803
2020503804
Analvsis . Sub_.
Date·. Time SamoleTvoe Analvsis File ID Batch ID
05/14/2002 01:36:00 Field Sample A0513232.D 0
05/14/2002 02:05:00 Field Sample A0513233.D 0
Page 40 of 41
-------------------
- - -SECTION VII - - - - ------------
Certifications
State/Aaencv· .. <.
c ... -'--·
Arkansas Deoartment of Environmental Oualitv
California Environmental Laboratory Accreditation Program I Waste Water/Hazardous Waste
Connecticut Deoartment ofHealth/Waste Water/Trade Waste. Sewage/Effluent Soil
Kansas Deoartment of Health and Environment I Solid and Hazardous Waste
Louisiana Department of Environmental Qualitv. ELAP I Waste Water/Hazardous Waste/Air Emissions
Montana Deoartment of Environmental Oualitv/Petroleum Release Section
New York State Department of Health /Waste Water/Hazardous Waste/ Air
North Carolina Deot. ofNatural Resources & Communitv Develooment I Waste Water
Oklahoma Department of Environmental Quality/General Water Qualitv/Sludge
South Carolina Deot. of Health & Environmental Control
Texas(TNRCC)
Texas Deoartment of Public Safety/Precursor Chemical and Lab Aooaratus
Wisconsin Deoartment of Natural Resources
US Air Force/AFCEE
US Armv Corns ofEneineers t'MRD.ACE)
US Department of Agriculture I Restricted Soils Permit
US Navv<NFESC)
SECTION VII -Certifications -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054] Hamilton Beach-Proctor Silex
STLAustin
.ID.·.#
2411
PH-0761
E-10165
30736
Particioating Laboratory
10915
302
8720
82003
Participating Laboratory
3039
999885260
Participating Laboratory
Participating Laboratorv
S-42350
Particioatine Laboratory
Page 41 of 41
-------------------
Table 2-1
Monitoring Well Construction Data for Sampled Wells
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
. Top of Casing
Installation Elevation Total Depth Screen Interval Filter Pack Bentonite Seal
Well No. Date (ft. above MSL) (ft. bes)
MW-220 515198 31.50 34
MW-222 5/6/98 35.11 40
MW-224 11/13/98 33.43 34
MW-225 11113/98 33.43 10
MW-226 9/30/98 28.46 75
MW-230 10/26/98 33.47 14
MW-234 6/23/99 35.03 26
Monitoring wells 220 and 222 installed by Radian Mobile Field Services.
Monitoring wells 226 was installed by Parratt Wolff, Inc.
(ft. b2sl
25-34
31-40
25-34
4-10
70-75
8-14
17 -26
Monitoring wells 224, 225, 230, and 234 installed by Probe Technology, Inc.
80396914.01 May2002GW _ Rpt.doc(06/0S/02}
(ft. bl?S) (ft. bi's)
24-34 23-24
30-40 29-30
24-34 23-24
3 -10 2-3
69-75 67-69
7 -14 5-7
16-26 13 -16
Grout Seal
(ft. bl?S)
0 [] 23
0-29
0-23
0-2
0-67
0-5
0-13
Well
MW-2018
MW-213
MW-214
MW-216
MW-217
MW-220
MW-221
MW-222
MW-223
MW-224
MW-225
MW-226
MW-227
MW-228
MW-230
MW-233
MW-234
Table 3-1
Water Level Measurements and Elevations
May 8, 2002
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North ·carolina
Measuring Point
Elevation Water Level Elevation
(ft above msm Deoth to Water (ft) (ft above msll
29.74 3.30 26.44
28.44 4.15 24.29
27.93 4.13 23.80
32.82 9.20 23.62
32.75 8.37 24.38
31.50 8.60 22.90
31.39 8.15 23.24
35.11 13.41 21.70
35.15 5.52 29.63
33.43 8.66 24.77
33.43 8.66 24.77
28.46 18.85 9.61
28.47 4.45 24.02
28.71 3.60 25.11
33.47 10.20 23.27
34.55 10.60 23.95
35.03 10.60 24.43
msl = mean sea level
80396914.01 May2002GW _Rpt:doc(06/05/02)
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
' .....
,. ·.'];.
Table 3-2
Historical Water Level Elevations at MW-220
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
Mav 13, 1998 25.13
November 16, 1998 20.55
Julv 1, 1999 21.50
October 20, 1999 25.63
Februarv 2, 2000 25.85
May2, 2000 25.81
Sentember 6, 2000 22.90
November 28, 2000 21.71
February 19, 2001 23.45
Mav 16, 2001 21.95
August 14, 2001 21.80
November 26, 2001 18.46
February 12, 2002 22.43
Mav8,2002 22.90
msl =mean sea level
80396914.01 May2002GW_Rpldoc(06/05/02)
Table 3-3
Historical Water Level Elevations at MW-222
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 22.34
November 16, 1998 19.99
July l, 1999 20.61
October 20, 1999 24.22
Februarv 2, 2000 23.34
May2, 2000 23.58
September 6, 2000 21.50
November 28, 2000 20.52
Februarv 19, 2001 21.34
May 16, 2001 20.91
Au1n1st 14, 2001 20.89
November 26, 2001 18.53
Februarv 12, 2002 20.84
.Mav8,2002 21.70
msl = mean sea level
80396914.01 May2002GW _Rpt.doc(06/05/02)
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-4
Historical Water Level Elevations at MW-224
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
May2,2000
Seotember 6, 2000
November 28, 2000
Februarv 19, 2001
May 16, 2001
August 14, 2001
November 26, 2001
Februarv 12, 2002
MayS,2002
msl = mean sea level
NM =Not measured
80396914.01 May2002GW _Rptdoc(06/05/02)
Water Level Elevation
m.abovemsn
NM
23.64
24.39
26.88
26.73
26.48
25.99
24.36
25.23
24.23
24.01
21.59
25.63
24.77
Table 3-5
Historical Water Level Elevations at MW-225
Hamilton JJeach¢Proctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
Februarv 2, 2000
May2,2000
September 6, 2000
November 28, 2000
Februarv 19, 2001
May 16, 2001
Au1rust 14, 2001
November 26, 2001
Februarv 12, 2002
Mav8,2002
msl = mean sea level
NM= Not measured
80396914.01 May2002GW _Rpt.doc(06/0S/02}
Water Level Elevation.
(ft. above ms))
NM
24.36
24.50
27.24
26.59
26.40
27.22
24.38
25.01
24.21
24.57
22.55
26.48
24.77
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 3-6
Historical Water Level Elevations at MW-226
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
Februarv 2, 2000
May2,2000
September 6, 2000
November 28, 2000
Februarv 19, 2001
May 16, 2001
Aul!USt 14, 2001
November 26, 2001
Februarv 12, 2002
May8,2002
msl = mean sea level
NM= Not measured
80396914.01 May2002GW_Rptdoc(06/05/02)
Water Level Elevation
(ft. above msll
NM
8.43
8.54
11.11
10.23
10.81
9.41
9.19
9.20
9.31
8.71
8.04
8.88
9.61 --
Table 3-7
Historical Water Level Elevations at MW-230
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
Date
Mav 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
Mav2, 2000
September 6, 2000
November 28, 2000
Februarv 19, 2001
Mav 16, 2001
August 14, 2001
November 26, 2001
Februarv 12, 2002
May8,2002
msl = mean sea level
NM =Not measured
80396914.01 May2002GW _Rptdoc(06/05/02)
Water Level Elevation
(Ct. above msl)
NM
21.14
21.80
27.71
27.44
26.53
23.07
21.87
23.17
22.17
22.20
18.89
22.16
23.27
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I·-
I
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I
I
Table 3-8
Historical Water Level Elevations at MW-234
Hamilton Beacb¢Proctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
Mav2, 2000
September 6, 2000
November 28, 2000
Februarv 19, 2001
May 16, 2001
Aul!USt 14, 2001
November 26, 2001
Februarv 12, 2002
May8, 2002
msl = mean sea level
NM =Not measured
80396914.01 May2002GW_Rptdoc(06/05/02)
Water Level Elevation
(ft. above msll
NM
NM
23.24
25.71
25.67
25.56
25.04
23.23
24.20
23.53
23.94
21.29
26.34
24.43
Well Date Time
MW-220 5/8/02 12:45
MW-222 5/8/02 13:50
MW-224 5/8/02 13:10
MW-225 5/8/02 13:05
11:25
MW-226 5/8/02 11:30
11:35
11:40
MW-230 5/8/02 10:55
MW-234 5/8/02 13:35
80396914.01 May2002GW _Rpt.doc(06/05/02)
Table 3-9
Field Measurements
May 8, 2002
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Volume Purged
(Gal) Purelne Criteria .
0.85 3 well volumes
0.80 3 well volumes
0.75 3 well volumes
0.01 Dry
9.00
13.00 Stabilized parameters
15.00
17.00
0.10 Dry
0.50 3 well volumes
Specific
Temperature Conductance
(OC) luS) PH
19.0 110 6.1
20.0 350 7.1
20.0 330 7.1
26.0 200 4.8
20.0 440 7.3
20.0 440 7.4
20.0 440 7.4
20.0 440 7.4
20.0 150 4.5
20.0 140 6.2
-------------------
-------------------i
Table 3-10
Summary of Qualified Groundwater Analytical Results: May 2002
Volatile Organic Compounds by Method 8260B
Hamilton Beach¢Proctor-Silex, Washington, North Carolina . I
Sample ID MW-~20
Date of Sampling 51812 02
Analyte (µg/L) ''
Carbon Disulfide ND (0.0415)
1, 1-Dichloroethane 0.917
1, 1-Dichloroethene ND(0.0492)
Target analytes not listed were not detected.
Bold values exceed Standards.
MW-222
5/8/2002
ND (0.0415)
ND (0.0445)
0.139 J
ND ( ) =Not detected at specified detection limit.
J = Estimated value.
1 { I ~
I'
80396914.01 May2002GW _Rpt.doc(06/05/02)
MW-224 MW-225 MW-226
5/8/2002 5/8/2002 5/8/2002
0.7401 ND (0.0415) ND (0.0415)
ND (0.0445) ND(0.0445) ND(0.0445)
0.118 J ND (0.0492) ND (0.0492)
MW-230 MW-234
5/8/2002 5/8/2002
ND (0.0415) ND (0.0415)
ND (0.0445) ND (0.0445)
ND (0.0492) ND (0.0492)
Groundwater May
Analvte Standard 1998
Carbon disulfide 700 ND (0.0547)
1, 1-Dichloroethane 700 ND (0.0576)
Methyl t-butyl ether 200 ND (0.0365)
-. Groundwater November
Analyte Standard 2000
Carbon disulfide 700 ND (0.0684)
1, 1-Dichloroethane 700 0.426 J
Methyl t-butyl ether 200 ND (0.116)
Target analytes not-listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value·.
ND= Not detected at (detection limit).
UJ =Not detected and the detection limit is estimated.
80396914.01 May2002GW _ Rpt.doc(06/05/02)
Table 3-11
Historical Analytical Results for MW-220
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
November July October
1998 1999 1999
ND (0.0547) 0.426J 0.162
ND (0.0576) ND (0.0736) ND (0.0588)
ND (0.0365) UJ ND(0.0334) ND(0.0512)
February May August
2001 2001 2001
ND (0.0684) UJ ND (0.0684) ND (0.0684) UJ
0.456 J ND (0.124) 0.530
ND (0.116) ND (0.116) ND (0.116)
February May September
2000 2000 2000
ND (0.0484) UJ ND (0.0484) ND (0.0484)UJ
ND (0.0487) ND (0.0487) ND (0.0487)
ND (0.0469) 0.441 J ND (0.0469)
November February May
2001 2002 2002
ND (0.0415) ND (0.0415) ND (0.0415)
0.550 0.607 0.917
ND(0.0619) ND (0.0619) ND (0.0619)
-------------------
-------------~-----
Groundwater
ADalyte Standard
Carbon disulfide 700
1,1-Dichloroethane 700
l, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
Toluene 1,000
. Groundwater
Analyte Standard
Carbon disulfide 700
1, 1-Dichloroethane 700
l, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
Toluene 1,000
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
May
'1998
ND (0.0547)
ND (0.0576)
0.09081
ND (0.0383)
0.1561
November
2000
ND (0.0684)
ND (0.124)
0.06681
0.1241
ND (0.137)
U1 =Not detected and the detection limit is estimated.
. '.fable 3-12 ;
Historical Analytical Results for MW-222
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
November July October
1998 1999 1999
ND (0.0547) 0.3881 0.0944
ND(0.0576) ND (0.0736) ND (0.0588)
ND(0.0715) ND (0.102) ND(0.0819)
ND(0.223)U ND (0.0595) ND(0.0407)
ND (0.0522) ND (0.0766) ND (0.0645)
February May August
2001 2001 2001
ND (0.0684) U1 ND (0.0684) ND (0.0684) UJ
0.589 0.536 ND(0.124)
0.1021 0.07931 ND(0.122)
0.2221 0.2601 0.157 J
ND (0.0637) ND (0.0637) ND(0.0637)
U =Not present above the associated level, blank contamination present.
. 80396914.01 May2002GW_Rpt.doc(06/05/02)
February May September 2000 2000 2000
ND (0.0484) U1 ND (0.0484) ND (0.0484) U1
ND (0.0487) 0.3381 0.3281
ND (0.0697) ND(0.279)U 0.0766J
ND(0.0603) ND (0.0603) 0.1391
ND(0.0680) ND (0.0680) ND (0.0680)
November February May
2001 2002 2002
ND(0.0415) ND (0.0415) ND (0.0415)
0.375 J ND (0.0445) ND (0.0445)
0.1301 ND(0.0492) 0.1391
0.1261 ND(0.0353) ND (0.0353)
ND (0.0236) ND (0.0236) ND (0.0236)
Table 3-13
Historical Analytical Results for MW-224
Hamilton Beach¢Proctor-Silex, Inc.
Groundwater November
Analvte Standard 1998
Carbon disulfide 700 ND (0.0547)
Toluene 1,000 ND(0.0522)
Groundwater February
Analvte Standard 2001
Carbon disulfide 700 ND (0.571) UJ
Toluene 1.000 ND(0.0637)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
UJ =Not detected and the detection limit is estimated.
80396914.01 May2002GW _ Rpt.doc(06/05/02)
Washington, North Carolina
July October February
1999 1999 2000
2.22 2.72 ND (1.05)UJ
ND (0.0766) ND (0.0645) ND (0.0680)
May August November
2001 2001 2001
0.715 J 0.515 J 0.531 J
ND <0.0637) ND(0.0637) ND (0.0236)
May September November
2000 2000 2000
ND<0.334lU 0.350 J 0.697 J
0.0542 J ND(0.0680) ND (0.0637)
February May
2002 2002
0.640J 0.740 J
ND <0.0236) ND(0.0236)
-------------------
-------------------
Table 3-14
Historical Analytical Results for MW-225
Hamilton Beach¢Proctor-Silex, Inc.
Groundwater November
Analyte Standard 1998
Carbon disulfide 700 ND (0.0547)
Chloroform 0.19 ND(0.0480)
Groundwater February
Analyte Standard 2001
Carbon disulfide 700 ND (0.511) UJ
Chloroform 0.19 ND(0.0896)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
UJ =Not detected and the detection limit is estimated.
80396914.0 I May2002GW _Rpt.doc(06/05/02)
Washington, North Carolina
July October February
1999 1999 2000
ND (0.864) 0.0691 ND (0.0484) UJ
ND (0.0424) 0.171 ND (0.0670)
May August November
2001 2001 2001
ND (0.0684) ND (0.0684) ND (0.0415)
ND (0.0896) ND (0.0896) ND (0.0338)
May2000 September November
2000 2000
ND (0.0484) ND (0.0484) UJ ND (0.0684)
ND (0.0670) ND (0.0670) ND (0.0896)
February May
2002 2002
ND (0.0415) ND (0.0415)
ND (0.0338) ND(0.0338)
Groundwater November
Analvte Standard 1998
Carbon disulfide 700 ND(0.0547)
Groundwater February
Analvte Standard. 2001
Table 3-15
Historical Analytical Results for MW-226
Hamilton Beach¢Proctor-Silex, Inc.
Washington, North Carolina
July October February
1999 1999 200
ND (0.864) 0.0950 ND (0.0484) UJ
May August November
2001 2001 2001
Carbon disulfide 700 ND (0.0684) UJ ND(0.0684) ND (0.0684) UJ ND (0.0415)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
UJ =Not detected and the detection limit is estimated.
80396914.01 May2002GW _Rpt.doc(06/05/02)
May September November
2000 2000 2000
ND (0.0484) UJ 0.210 J ND (0.0684)
February . May
2002 2002
ND <0.0415) ND (0.0415)
-------------------
-------------------
Groundwater
Analyte Standard
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
Cis-1,2-Dichloroethene 70
Methvl methacrvlate POL
Toluene 1,000
Trichloroethene 2.8
Groundwater
Analyte Standard
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
Cis-1,2-Dichloroethene 70
Methyl methacrvlate POL
Toluene 1,000
Trichloroethene 2.8
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
!
Table 3-16
Historical Analytical Results for MW-230
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November July October February
1998 1999 1999 2000
ND (0.0576) ND (0.0736) 0.265 0.189 J
ND (0.306)U ND (0.102) 0.133 0.148 J
ND(2.67)U ND (0.0595) 0.304 0.354 J
ND (0.130) ND (0.156) ND(0.0916) ND (0.114)
ND (0.0522) 0.286 ND(0.309)U 0.284 J
ND(2.05)U ND (0.0929) 0.921 0.661 J
February May August November
2001 2001 2001 ' 2001
ND (0.124) ND(0.124) ND (0.124) ND (0.0445)
ND (0.122) ND (0.122) ND (0.122) ND (0.0492)
0.0969J 0.288 J 0.119 J ND (0.0353)
ND (0.131) ND (0.131) ND (0.131) 0.148 J
ND (0.0637) ND (0.0637) ND (0.0637) ND (0.0236)
0.160 J 0.292 J 0.140J ND (0.0506)
U =Not present above the associated level; blank contamination is present.
80396914.01 May2002GW _Rpt.doc(06/05/02)
May September November
2000 2000 2000
ND(0.348)U ND (0.0487) ND (0.124)
0.593 ND (0.0697) ND (0.122)
0.573 0.102 J 0.142 J
ND (0.114) UJ ND (0.114) ND (0.131)
0.0826J 0.126J ND (0.0637)
1.11 ND (0.355)U 0.235 J
February May
2002 2002
ND (0.0445) ND(0.0445)
ND (0.0492) ND (0.0492)
ND (0.0353) ND (0.0353)
ND (0.175) ND (0.175)
ND (0.0236) ND (0.0236)
ND (0.0506) ND (0.0506)
Table 3-17
Historical Analytical Results for MW-234
Hamilton BeachOProctor-Silex, Inc.
Groundwater July
Analvte Standard 1999
Carbon disulfide 700 ND(0.864)
1, 1-Dichloroethene 7 ND (0.102)
Groundwater February
Analyte Standard 2001
Carbon disulfide 700 ND (0.0684) UJ
1, 1-Dichloroethene 7
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
ND (0.122)
UJ =Not detected and the detection limit is estimated.
80396914.01 May2002GW_Rpt.doc(06/05/02)
Washington, North Carolina
October February May
1999 2000 2000
0.0600 ND (0.0484) UJ ND (0.0484)
ND (0.0819) ND (0.0697) 0.145 J
May August November
2001 2001 2001
ND (0.0684) ND (0.0684) ND (0.0415)
ND (0.122) ND (0.122) ND (0.0492)
September November
2000 2000
ND l0.0484) UJ ND(0.0684)
ND (0.0697) ND(0.122)
February May
2002 2002
ND (0.0415) ND (0.0415)
ND (0.0492) ND (0.0492)
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
0502HBWD999
2020505408
Aaueous
0502HBWW220 0502HBWW222
2020505401 2020505402
Aaueous Aaueous
Reported As Received Received Received I
% Moisture
Dateffime Collected
Daterrime Prepared
Dateffime Analyzed
Dilution Factor
Instrument
Units
NA
05/08/2002 11:50
05/14/2002 00:39
05/14/2002 00:39
1.0000
MSDA
Ui!IL
·,/ ;,'.'-·~:·.'; .• f···:.· .:,:. . ;'f'E:'®::. ;(;;; : '\: :1?i•; ~~:~:Ke'•,,,;, .. ,.· ;;11 :.·conas• .. 1 ··',filan~;1,.DL ·
Acetone 67-64-1 ND
Acetonitrile 75-05-8 ND
Acrolein 107-02-8 ND
Acrvlonitrile 107-13-1 ND
Benzene 71-43-2 ND
Bromobenzene 108-86-1 ND
Bromochloromethane 74-97-5 ND
Bromodichloromethane 75-27-4 ND
Bromoform 75-25-2 ND
Bromomethane 74-83-9 ND
2-Butanone (MEK) 78-93-3 ND
n-Butvlbenzene 104-51-8 ND
sec-Butvlbenzene 135-98-8 ND
tert-Butvlbenzene 98-06-6 ND
Carbon disulfide 75-15-0 ND
Carbon tetrachloride 56-23-5 ND
2-Chloro-1.3-butadiene 126-99-8 ND
Chlorobenzene 108-90-7 ND
Chloroethane 75-00-3 ND
Chloroform 67-66-3 ND
1-Chlorohexane 544-10-5 ND
SECTION IV -Analytical Results -05/14/2002 15:49
LIMS Workorder: 80396913 (20205054] Hamilton Beach-Proctor Silex
STL Austin
1.26
5.34
~ 2.85
0.290
0.0465
0.0643
0.0449
0.0528
IA:\ 0.106
0.0454
2.83
0.0888
0.104
0.0934
0.0415
0.0553
0.0596
0.0404
0.0755
0.0338
0.0798
.. ···.RL
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
NA NA
05/08/2002 12:50 05/08/2002 13:55
05113/2002 21 :20 05/13/2002 21 :49
05/13/2002 21:20 05/13/2002 21 :49
1.0000 1.0000
MSDA MSDA
U!!II. ug/L
· .. :.cone:. ; Flaa DL RL Cone Flaa DL
ND 1.26 0.00 ND 1.26
ND 5.34 0.00 ND 5.34
ND IJVJ 2.85 0.00 ND lA, --s 2.85
ND 0.290 0.00 ND 0.290
ND 0.0465 0.00 ND 0.0465
ND 0.0643 0.00 ND 0.0643
ND 0.0449 0.00 ND 0.0449
ND 0.0528 0.00 ND 0.0528
ND IA.::5 0.106 0.00 ND \A:S-0.106
ND 0.0454 0.00 ND 0.0454
ND 2.83 0.00 ND 2.83
ND 0.0888 0.00 ND 0.0888
ND 0.104 0.00 ND 0.104
ND 0.0934 0.00 ND 0.0934
ND 0.0415 0.00 ND 0.0415
ND 0.0553 0.00 ND 0.0553
ND 0.0596 0.00 ND 0.0596
ND 0.0404 0.00 ND 0.0404
ND 0.0755 0.00 ND 0.0755
ND 0.0338 0.00 ND 0.0338
ND 0.0798 0.00 ND 0.0798
Page 4
Sample results have been qua lilied by URS-Radian based on the results uf the data review process, winch is modeled alicr the Natio1111/ Fimctw1111/ G11itle/i11es fur V1gt11111· 11111l /11urg11111c 0111t1 Henn"
111c i::PA ,.,.,,..,.., tQ<lQ :mil Frhruarv 1994. resoeclivelv)
RL
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
of 41
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
0502HBWD999
2020505408
Continued
'. Rarameter .. ~fiinc·
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
I 2-Dibromo-3-chloroorooane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
1.2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-1.4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
I 2-Dichlorobenzene 95-50-1 ND
I 3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 ND
l, 1-Dichloroethane 75-34-3 ND
1.2-Dichloroethane 107-06-2 ND
I 1-Dichloroethene 75-35-4 ND
cis-1.2-Dichloroethene 156-59-2 ND
trans-1.2-Dichloroethene 156-60-5 ND
1,2-Diohloropropane 78-87-5 ND
1.3-Dichloroorooane 142-28-9 ND
2.2-Dichloropropane 594-20-7 ND
I l-Dichloroorooene 563-58-6 ND
cis-1 3-Dichloropropene 10061-01-5 ND
trans-1.3-Dichloroorooene 10061-02-6 ND
Ethyl methacrvlate 97-63-2 ND
Ethvlbenzene 100-41-4 ND
Hexachloro-1 3-butadiene 87-68-3 ND
2-Hexanone 591-78-6 ND
SECTION IV -Analytical Results -05/14/2002 15:49
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
·· Flan
(..1.\
1.A..S
DL
0.0509
0.0785
0.0359
0.0684
0.777
0.0946
0.0895
0.0550
0.0596
0.0495
0.0596
0.0591
0.0930
0.0445
0.0632
0.0492
0.0353
0.0430
0.0519
0.0401
0.0492
0.0374
0.0526
0.0486
0.0822
0.0469
0.155
0.838
0502HBWW220 0502HBWW222
2020505401 2020505402
RL Cone Flan· DL RL Cone Flaa >ot:. RL
0.00 ND 0.0509 0.00 ND 0.0509 0.00
0.00 ND 0.0785 0.00 ND 0.0785 0.00
0.00 ND 0.0359 0.00 ND 0.0359 0.00
0.00 ND 0.0684 0.00 ND 0.0684 0.00
0.00 ND \,l :T 0.777 0.00 ND ll\ \ 0.777 0.00
0.00 ND 0.0946 0.00 ND 0.0946 0.00
0.00 ND 0.0895 0.00 ND 0.0895 0.00
0.00 ND 0.0550 0.00 ND 0.0550 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0495 0.00 ND 0.0495 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0591 0.00 ND 0.0591 0.00
0.00 ND 0.0930 0.00 ND 0.0930 0.00
0.00 0.917 0.0445 0.00 ND 0.0445 0.00
0.00 ND 0.0632 0.00 ND 0.0632 0.00
0.00 ND 0.0492 0.00 0.139 J 0.0492 0.00
0.00 ND 0.0353 0.00 ND 0.0353 0.00
0.00 ND 0.0430 0.00 ND 0.0430 0.00
0.00 ND 0.0519 0.00 ND 0.0519 0.00
0.00 ND 0.0401 0.00 ND 0.0401 0.00
0.00 ND 0.0492 0.00 ND 0.0492 0.00
0.00 ND 0.0374 0.00 ND 0.0374 0.00
0.00 ND 0.0526 0.00 ND 0.0526 0.00
0.00 ND 0.0486 0.00 ND 0.0486 0.00
0.00 ND \X'.l" 0.0822 0.00 ND (A:\ 0.0822 0.00
0.00 ND 0.0469 0.00 ND 0.0469 0.00
0.00 ND 0.155 0.00 ND 0.155 0.00
0.00 ND 0.838 0.00 ND 0.838 0.00
Page 5 of -Sample results have been r~ahfied by lJ~S-Radian based on the results of the data ICVICW process, wluch is modeled a lier '"'' N111101111/ fi111rno1111/ Gw1/e/111,·s for Org111uc 11111/ lrrorg1mu· 011111 Hatt'»" -JSE~berl Feb 4.r-vcly)------------
41 -
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
P'animitar:. : .· . c: ..
lodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Propylbenzene 103-65-1
Stvrene 100-42-5
1 l 1.2-Tetrachloroethane 630-20-6
I l 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2 3-Trichlorobenzene 87-61-6
1.2 4-Trichlorobenzene 120-82-1
1.1.1-Trichloroethane 71-55-6
1.1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2 3-Trichloroorooane 96-18-4
1.1.2-Trichlorotrifluoroethane 76-13-1
1.2.4-Trimethvlbenzene 95-63-6
1.3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWD999
2020505408
··~one f laa
ND
ND
ND
ND
ND
ND
ND
ND tM
ND
ND
ND
ND
ND
ND ll~
ND
ND
ND \A:\
ND IA°S
ND
ND
ND
ND
ND
ND
ND
ND
ND
-Nil-f<_
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STL Austin
DL RL
0.0452 0.00
0.0769 0.00
0.0899 0.00
0.175 0.00
0.0619 0.00
0.473 0.00
0.0210 0.00
0.0708 0.00
0.652 0.00
0.0698 0.00
0.0295 0.00
0.0578 0.00
0.109 0.00
0.103 0.00
1.28 0.00
0.0236 0.00
0.110 0.00
0.140 0.00
0.0511 0.00
0.0489 0.00
0.0506 0.00
0.0495 0.00
0.117 0.00
0.0529 0.00
0.0744 0.00
0.0616 0.00
0.172 0.00
0.0501 ('),00
0502HBWW220 0502HBWW222
2020505401 2020505402
Cone Flaa DL RL Cone Flaa DL
ND 0.0452 0.00 ND 0.0452
ND 0.0769 0.00 ND 0.0769
ND 0.0899 0.00 ND 0.0899
ND 0.175 0.00 ND 0.175
ND 0.0619 0.00 ND 0.0619
ND 0.473 0.00 ND 0.473
ND 0.0210 0.00 ND 0.0210
ND IA.:\ 0.0708 0.00 ND lA::I 0.0708
ND 0.652 0.00 ND 0.652
ND 0.0698 0.00 ND 0.0698
ND 0.0295 0.00 ND 0.0295
ND 0.0578 0.00 ND 0.0578
ND 0.109 0.00 ND 0.109
ND \AS 0.103 0.00 ND \A.:~ 0.103
ND 1.28 0.00 ND 1.28
ND 0.0236 0.00 ND 0.0236
ND \A:3 0.110 0.00 ND 1A:1 0.110
ND I A"\ 0.140 0.00 ND i A:\ 0.140
ND 0.0511 0.00 ND 0.0511
ND 0.0489 0.00 ND 0.0489
ND 0.0506 0.00 ND 0.0506
ND 0.0495 0.00 ND 0.0495
ND 0.117 0.00 ND 0.117
ND 0.0529 0.00 ND 0.0529
ND 0.0744 0.00 ND 0.0744
ND 0.0616 0.00 ND 0.0616
ND 0.172 0.00 ND 0.172
NI} R 0.0:'.501 (J.{JO -NB f?._ 0.0:'.501
Page 6
Sample results have bct:n qualified by URS-Radian based on the results of the data review process, wh1d1 is modeled a lier the N"/101111/ F1111ctim111/ G11i1/e/i11es for U1g11111c 1111il /11org11111c 1>11111 Rnu·.,.
111" l'l'A October 1999 and F.:bruarv 19'J4, rcspec1ivt:ly)
RL
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
'6.00
of 41
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
0502HBWW224
2020505403
Aaueous
Received
NA
05/08/2002 13: 15
05/13/2002 22:17
05/13/2002 22:17
1.0000
MSDA
ug/L
.... ,. ..
''i '· . ;;'' :~{':\<> ' ;. ;·'.c•S;i;{;;·:~.fr1 ''t'!t\n~r;~· \~«llAa' ·ot .. ' ; ...
Acetone 67-64-1 ND
Acetonitrile 75-05-8 ND
Acrolein 107-02-8 ND
Acrvlonitrile 107-13-1 ND
Benzene 71-43-2 ND
Bromobenzene 108-86-1 ND
Bromochloromethane 74-97-5 ND
Bromodichloromethane 75-27-4 ND
Bromofonn 75-25-2 ND
Bromomethane 74-83-9 ND
2-Butanone (MEK) 78-93-3 ND
n-Butvlbenzene 104-51-8 ND
sec-Butylbenzene 135-98-8 ND
tert-Butvlbenzene 98-06-6 ND
Carbon disulfide 75-15-0 0.740
Carbon tetrachloride 56-23-5 ND
2-Chloro-l 3-butadiene 126-99-8 ND
Chlorobenzene 108-90-7 ND
Chloroethane 75-00-3 ND
Chlorofonn 67-66-3 ND
1-Chlorohexane 544-10-5 ND
SECTION IV -Analytical Results -05/14/2002 15:49
LIMS Workorder: 80396913 (20205054] Hamilton Beach-Proctor Silex
STLAustin
l.26
5.34
IA.:\ 2.85
0.290
0.0465
0.0643
0.0449
0.0528
lA.-1' 0.106
0.0454
2.83
0.0888
0.104
0.0934
J 0.0415
0.0553
0.0596
0.0404
0.0755
0.0338
0.0798
0502HBWW225 0502HBWW226
2020505404 2020505405
Aaueous Aaueous
Received Received I
NA NA
05/08/2002 13:25 05/08/2002 11 :45
05/13/2002 22:46 05/13/200223:14
05/13/2002 22:46 05/ 13/2002 23: 14
1.0000 l.0000
MSDA MSDA
ug/L ug/L
RL .. Cone ·Flaa DL ' RL Cone Flaa OL RL
0.00 ND l.26 0.00 ND l.26 0.00
0.00 ND 5.34 0.00 ND 5.34 0.00
0.00 ND \ )\ "'.\ 2.85 0.00 ND l~\ 2.85 0.00
0.00 ND 0.290 0.00 ND 0.290 0.00
0.00 ND 0.0465 0.00 ND 0.0465 0.00
0.00 ND 0.0643 0.00 ND 0.0643 0.00
0.00 ND 0.0449 0.00 ND 0.0449 0.00
0.00 ND 0.0528 0.00 ND 0.0528 0.00
0.00 ND l A".\ 0.106 0.00 ND \A:\ 0.106 0.00
0.00 ND 0.0454 0.00 ND 0.0454 0.00
0.00 ND 2.83 0.00 ND 2.83 0.00
0.00 ND 0.0888 0.00 ND 0.0888 0.00
0.00 ND 0.104 0.00 ND 0.104 0.00
0.00 ND 0.0934 0.00 ND 0.0934 0.00
0.00 ND 0.0415 0.00 ND 0.0415 0.00
0.00 ND 0.0553 0.00 ND 0.0553 0.00
0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.00 ND 0.0404 0.00 ND 0.0404 0.00
0.00 ND 0.0755 0.00 ND 0.0755 0.00
0.00 ND 0.0338 0.00 ND 0.0338 0.00
0.00 ND 0.0798 0.00 ND 0.0798 0.00
Page 9 of 41 -Sample rcsuhs have been qualified by URS-Radian based un 1hc rc:mhs of 1hc da1a review process, wlm:h is modeled a lier the N111w1111/ F11111·1w1111/ G111de/111es fur Vrg1111u· 111ul liwrg11n1c 011111 Nauw
-JSE~bcr-dfc~994,.-vely)-- - - - - -.. - - - - -
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter··
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
74-87-3
107-05-1
95-49-8
106-43-4
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
l 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-l ,4-Dichloro-2-butene ll0-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1,3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
l 1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichloropropane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloropropane 594-20-7
l, 1-Dichloroorooene 563-58-6
A•
cis-1 3-Dichloropropene 10061-01-5
trans-1,3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW224
2020505403
')11••' •.tone Flaa
ND
ND
ND
ND
ND IX.~
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.118 J
ND
ND
ND
ND
ND
ND
ND
ND
ND IA:\
ND
ND
ND
LIMS Workorder: 80396913 (20205054) Hamilton Beach-Proctor Silex
STLAustin
0502HBWW225 0502HBWW226
2020505404 2020505405
DL RL Cone Flaa DL RL Cone Flaa DL
0.0509 0.00 ND 0.0509 0.00 ND 0.0509
0.0785 0.00 ND 0.0785 0.00 ND 0.0785
0.0359 0.00 ND 0.0359 0.00 ND 0.0359
0.0684 0.00 ND 0.0684 0.00 ND 0.0684
0.777 0.00 ND \A...T 0.777 0.00 ND IM 0.777
0.0946 0.00 ND 0.0946 0.00 ND 0.0946
0.0895 0.00 ND 0.0895 0.00 ND 0.0895
0.0550 0.00 ND 0.0550 0.00 ND 0.0550
0.0596 0.00 ND 0.0596 0.00 ND 0.0596
0.0495 0.00 ND 0.0495 0.00 ND 0.0495
0.0596 0.00 ND 0.0596 0.00 ND 0.0596
0.0591 0.00 ND 0.0591 0.00 ND 0.0591
0.0930 0.00 ND 0.0930 0.00 ND 0.0930
0.0445 0.00 ND 0.0445 0.00 ND 0.0445
0.0632 0.00 ND 0.0632 0.00 ND 0.0632
0.0492 0.00 ND 0.0492 0.00 ND 0.0492
0.0353 0.00 ND 0.0353 0.00 ND 0.0353
0.0430 0.00 ND 0.0430 0.00 ND 0.0430
0.0519 0.00 ND 0.0519 0.00 ND 0.0519
0.0401 0.00 ND 0.0401 0.00 ND 0.0401
0.0492 0.00 ND 0.0492 0.00 ND 0.0492
0.0374 0.00 ND 0.0374 0.00 ND 0.0374
0.0526 0.00 ND 0.0526 0.00 ND 0.0526
0.0486 0.00 ND 0.0486 0.00 ND 0.0486
0.0822 0.00 ND IA\ 0.0822 0.00 ND ~;\.. \ 0.0822
0.0469 0.00 ND 0.0469 0.00 ND 0.0469
0.155 0.00 ND 0.155 0.00 ND 0.155
0.838 0.00 .ND 0.838 0.00 ND 0.838
Page 10
Sample n:sulls have been qualified by URS-Radian based on 1hc u:sulls uf 1hc da1a review process, wluch is nllldclcd afler the N111w1111/ F111u·1w1111/ G11i1/e/i11es fu1· V1g111111· 11111/ lnurg11111c 011111 Nt•1·1•'"'
(US EPA, October 19'J') and Fi:brnary 19')4, n:speclivdy)
RL
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
of 41
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
0502HBWW230
2020505406
Aaueous
Received
NA
05/08/2002 11: 10
05/13/2002 23:43
05/13/2002 23:43
1.0000
MSDA
ul!!L
-,,,, la'··o-.-.,, __ ?<->:' w?bi;>,, > '/>t'.'!.''., -'''?V'. o~U';!CfAS:'.1~;;+, ';t:2i ':""'~ %:;,, (:' ''Pl80;'-~\;!~f: .. ,,,
Acetone 67-64-1 ND
Acetonitrile 75-05-8 ND
Acrolein 107-02-8 ND
Acrvlonitrile 107-13-1 ND
Benzene 71-43-2 ND
Bromobenzene 108-86-1 ND
Bromochloromethane 74-97-5 ND
Bromodichloromethane 75-27-4 ND
Bromoform 75-25-2 ND
Bromomethane 74-83-9 ND
2-Butanone (MEK) 78-93-3 ND
n-Butvlbenzene 104-51-8 ND
sec-Butvlbenzene 135-98-8 ND
tert-Butvlbenzene 98-06-6 ND
Carbon disulfide 75-15-0 ND
Carbon tetrachloride 56-23-5 ND
2-Chloro-l 3-butadiene 126-99-8 ND
Chlorobenzene 108-90-7 ND
Chlo roe thane 75-00-3 ND
Chloroform 67-66-3 ND
1-Chlorohexane 544-10-5 ND
SECTION IV -Analytical Results -05/14/2002 15:49
LIMS Workorder: 80396913 (20205054] Hamilton Beach-Proctor Silex
STLAustin
1.26
5.34
I>..\ 2.85
0.290
0.0465
0.0643
0.0449
0.0528
IA;S° 0.106
0.0454
2.83
0.0888
0.104
0.0934
0.0415
0.0553
0.0596
0.0404
0.0755
0.0338
0.0798
li'it>
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0502HBWW234 TRIP BLANK
2020505407 2020505409
Aaueous Aqueous
Received Received I
NA NA
05/08/2002 13:40 05/08/2002 00:00
05/14/200200:11 05/13/2002 19:24
05/14/200200:11 05/13/2002 19:24
1.0000 1.0000
MSDA MSDA
U!!/L ul!/L
:•:,, 1'tonc. . flan :':'DL :c, , , flt. .· :,' Cone Flaa DL
ND 1.26 0.00 ND 1.26
ND 5.34 0.00 ND 5.34
ND ~ 2.85 0.00 ND Ii..~ 2.85
ND 0.290 0.00 ND 0.290
ND 0.0465 0.00 ND 0.0465
ND 0.0643 0.00 ND 0.0643
ND 0.0449 0.00 ND 0.0449
ND 0.0528 0.00 ND 0.0528
ND lA\ 0.106 0.00 ND I~'""\ 0.106
ND 0.0454 0.00 ND 0.0454
ND 2.83 0.00 ND 2.83
ND 0.0888 0.00 ND 0.0888
ND 0.104 0.00 ND 0.104
ND 0.0934 0.00 ND 0.0934
ND 0.0415 0.00 ND 0.0415
ND 0.0553 0.00 ND 0.0553
ND 0.0596 0.00 ND 0.0596
ND 0.0404 0.00 ND 0.0404
ND 0.0755 0.00 ND 0.0755
ND 0.0338 0.00 ND 0.0338
ND 0.0798 0.00 ND 0.0798
Page 14
Sample results have been qualified by URS-Radian based on 1hc results of lhc da1a review process, wluch is modeled a tier the Na11011a/ F1111ctio1wl G11ule/iiws for V1g1111ic mu/ ltwrg11mc I la111 Nt·1·1""'
111<;; !'PA 0.-t<iher 191}9 and Fcbrnarv 1994. rc:soectivdy)
RL
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
of 41
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
, "'Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
''
Client Sample ID
Lab Sample ID
',,, ..
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW230
2020505406
·;~{&~; " :",.;.;.;._or, ..... , Flan. ,' '<
ND
ND
ND
ND
ND IA-J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND vs
ND
ND
ND
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
0502HBWW234 TRIP BLANK
2020505407 2020505409
DL RL Cone flan DL RL Cone Flaa <DL· RL
0.0509 0.00 ND 0.0509 0.00 ND 0.0509 0.00
0.0785 0.00 ND 0.0785 0.00 ND 0.0785 0.00
0.0359 0.00 ND 0.0359 0.00 ND 0.0359 0.00
0.0684 0.00 ND 0.0684 0.00 ND 0.0684 0.00
0.777 0.00 ND vw 0.777 0.00 ND lk::S 0.777 0.00
0.0946 0.00 ND 0.0946 0.00 ND 0.0946 0.00
0.0895 0.00 ND 0.0895 0.00 ND 0.0895 0.00
0.0550 0.00 ND 0.0550 0.00 ND 0.0550 0.00
0.0596 0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.0495 0.00 ND 0.0495 0.00 ND 0.0495 0.00
0.0596 0.00 ND 0.0596 0.00 ND 0.0596 0.00
0.0591 0.00 ND 0.0591 0.00 ND 0.0591 0.00
0.0930 0.00 ND 0.0930 0.00 ND 0.0930 0.00
0.0445 0.00 ND 0.0445 0.00 ND 0.0445 0.00
0.0632 0.00 ND 0.0632 0.00 ND 0.0632 0.00
0.0492 0.00 ND 0.0492 0.00 ND 0.0492 0.00
0.0353 0.00 ND 0.0353 0.00 ND 0.0353 0.00
0.0430 0.00 ND 0.0430 0.00 ND 0.0430 0.00
0.0519 0.00 ND 0.0519 0.00 ND 0.0519 0.00
0.0401 0.00 ND 0.0401 0.00 ND 0.0401 0.00
0.0492 0.00 ND 0.0492 0.00 ND 0.0492 0.00
0.0374 0.00 ND 0.0374 0.00 ND 0.0374 0.00
0.0526 0.00 ND 0.0526 0.00 ND 0.0526 0.00
0.0486 0.00 ND 0.0486 0.00 ND 0.0486 0.00
0.0822 0.00 ND IA.-1 0.0822 0.00 ND lA.S 0.0822 0.00
0.0469 0.00 ND 0.0469 0.00 ND 0.0469 0.00
0.155 0.00 ND 0.155 0.00 ND 0.155 0.00
0.838 0.00 .ND 0.838 0.00 ND 0.838 0.00
Page 15 of 41 -Sample resuhs have been qualified by URS-Radian based on 1hc results uf lhe dala 1cv1cw process, winch is modeled aflcr Iii<' N111iom1/ F1111c1wm1/ G11ule/i1wsjor U1gt111K mul ln01g11111c /J11111 Ne1·1n•'
-ISEJ'9mllberl~Feb-~l94,r-vely)------------ -
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
'"' ·Parameter.· · · .. ' •·
lodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methyl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Propylbenzene 103-65-1
Stvrene 100-42-5
1 1 1.2-Tetrachloroethane 630-20-6
1 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1 2.3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
1 1 1-Trichloroethane 71-55-6
1 I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloropropane 96-18-4
1 1 2-Trichlorotrifluoroethane 76-13-1
1,2 4-Trimethylbenzene 95-63-6
I 3 5-Trimethvlbenzene 108-67-8
Vinyl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/14/2002 15:49
0502HBWW230
2020505406
··one ··Flaa ·
ND
ND
ND
ND
ND
ND
ND
ND \A~
ND
ND
ND
ND
ND
ND IA 3
ND
ND
ND l.A:S
ND v..:j
ND
ND
ND
ND
ND
ND
ND
ND
ND
NB--R._
LIMS Workorder: 80396913 [20205054) Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.0452 0.00
0.0769 0.00
0.0899 0.00
0.175 0.00
0.0619 0.00
0.473 0.00
0.0210 0.00
0.0708 0.00
0.652 0.00
0.0698 0.00
0.0295 0.00
0.0578 0.00
0.109 0.00
0.103 0.00
l.28 0.00
0.0236 0.00
0.110 0.00
0.140 0.00
0.0511 0.00
0.0489 0.00
0.0506 0.00
0.0495 0.00
0.117 0.00
0.0529 0.00
0.0744 0.00
0.0616 0.00
0.172 0.00
0.0~01 8.09
0502HBWW234 TRIP BLANK
2020505407 2020505409
Cone Flaa DL RL Cone Flaa DL
ND 0.0452 0.00 ND 0.0452
ND 0.0769 0.00 ND 0.0769
ND 0.0899 0.00 ND 0.0899
ND 0.175 0.00 ND 0.175
ND 0.0619 0.00 ND 0.0619
ND 0.473 0.00 ND 0.473
ND 0.0210 0.00 0.114 J 0.0210
ND \.10 0.0708 0.00 ND iA.-S 0.0708
ND 0.652 0.00 ND 0.652
.ND 0.0698 0.00 ND 0.0698
ND 0.0295 0.00 ND 0.0295
ND 0.0578 0.00 ND 0.0578
ND 0.109 0.00 ND 0.109
ND \A.:S-0.103 0.00 ND w 0.103
ND 1.28 0.00 ND 1.28
ND 0.0236 0.00 ND 0.0236
ND ~ 0.110 0.00 ND \A3" 0.110
ND 1A:\ 0.140 0.00 ND I A:\ 0.140
ND 0.0511 0.00 ND 0.0511
ND 0.0489 0.00 ND 0.0489
ND 0.0506 0.00 ND 0.0506
ND 0.0495 0.00 ND 0.0495
ND 0.117 0.00 ND 0.117
ND 0.0529 0.00 ND 0.0529
ND 0.0744 0.00 ND 0.0744
ND 0.0616 0.00 ND 0.0616
ND 0.172 0.00 ND -0.172
-NB ~ t).(')jt)t 6.66 N£r j-<.._ 9.0581
Page 16
Sample n:sulls have been qualified by URS-Radian based on lhc rcsul&s of &he dala review process, wtm:h is modded aflcr th<" N111im111/ F1111ctw1111/ G1111/eli11t"s fur U1g11111t· 11nil /norg11n1t· /)11111 }{,.,.,. • .,.
111-. !'PA 0.-toher 1999 and Fo:bruarv 1994, respectively).
RL
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
e.oo
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Sample Results
The laboratory provided volatile organic results for all North Carolina groundwater quality standards
presented in ISA NCAC 2L.0202. Detection limits were less than or equal to Class GA standard or
practical quantitation limits for undiluted :satpple analyses.
The laboratory flagged sample results less than the practical quantitation limit and sample detection limit
with a J and U, respectively. All positive sample results that are less than these limits are considered
estimated (J).
0502 HB-PS Wash DE.doc
Page 3 of3
05/23/02
Laboratory Control Samples
Laboratory control samples (LeS) are blank samples fortified (spiked) with known concentrations of
analyte of interest. The percent recoveries and/or duplicate results of the Les and their duplicates are used
to assess extraction efficiencies and overall analytical accuracy and precision.
The laboratory criteria for accuracy and precision were met during Les and Les duplicate (LeSD)
analyses for all target analytes, except tetrachloroethene. The relative percent difference (20%) between
the Les and LeSD result for tetrachloroethene was greater than the laboratory control limit of 16%.
Tetrachloroethene sample results have been qualified as estimated (J, UJ) due to analytical imprecision.
Although laboratory specifications were met for accuracy, non-detect results for vinyl chloride were
qualified as unusable (R) because the percent recovery (15-16%) of the Les and LeSD was less than 60%
of the true value.
Blank Contamination
Laboratory blanks are clean liquid and/or solid matrix samples prepared by the analytical laboratory and
analyzed in the same manner as the field samples. Laboratory blanks are used to ensure that the field
samples are not contaminated during the sample preparation, sample analysis, or from previous samples
(instrument carry-over). Trip blanks are analyte-free water samples that accompany volatile investigative
samples during all stages of shipment, storage, and analysis. The trip blanks are used to assess the potential
for artificial introduction of volatile compounds into the investigative samples during the transportation and
sample handling processes.
Methylene chloride, a common laboratory blank contaminant, was detected at a concentration of 0.114 J
micrograms per liter (µg/L) in the trip blank. voe were not detected in the method blank. Methylene
chloride was not detected in any of the samples. Therefore, qualification of the data due to the presence of
blank contamination was not required.
Surrogate Spikes
Surrogate compound percent recoveries are used to assess extraction efficiencies, possible matrix effects,
and overall analytical accuracy during organic analyses.
Surrogate recoveries met laboratory control limits during all volatile organic sample analyses.
Matrix Spikes
Matrix spikes (MS) are samples spiked with known concentrations of analytes of interest. MS percent
recoveries and duplicate results are used to assess extraction efficiencies, possible matrix effects, and
overall analytical accuracy and precision.
A batch sample was selected for the volatile organic MS and matrix spike duplicate (MSD) analysis. An
evaluation of matrix interference is not possible since the batch sample results, which were not included in
the analytical report by the laboratory, may not be representative of conditions at the site.
Field Duplicates
Field duplicate samples are used to demonstrate acceptable precision during the sample collection process.
voes were not detected in field duplicate samples 0502HBWW226 and 0502HBWWD999.
0502 HB-PS Wash DE.doc
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Introduction
Hamilton Beach<>Proctor-Silex, Washington, NC
May 2002 Sampling Event, Data Evaluation Report
URS Corporation, May 2002
URS Corporation collected eight groundwater samples (0502HBWW-220, 222, 224 through 226, 230,
234, and D999), including one field duplicate sample, at the Hamilton Beach<>Proctor Silex facility in
Washington, NC on May 8, 2002. The samples were submitted to Severn Trent Laboratories (STL) in
Austin, Texas for the determination of volatile organic compounds (VOC) by SW-846 Method 8260B. A
trip blank was included with the shipment of samples to the laboratory for the analysis of VOC.
URS Corporation reviewed the analytical results, which were reported by the laboratory under work order
number 20205054. The data evaluation was modeled after the National Functional Guidelines for Organic
Data Review (EPA, October 1999). Qualitative and quantitative limitations associated with the analytical
results were identified and defined based on the results of specific quality control (QC) criteria. Accuracy
was determined from the review of spike recoveries. Precision was based on the evaluation of laboratory
duplicate results. Sensitivity was evaluated by comparing reported detection limits to project-specific
maximum reporting limits. Representativeness was evaluated from the review of holding time and blank
data. Sample results have been appropriately qualified based on the criteria of the data review process.
The results of the data review are summarized below.
Sample Condition upon Receipt and Holding Times
All samples were received intact and in good condition by STL on May 9, 2002. The temperature of
sample containers upon receipt at the laboratory met EPA-established storage requirements of 4 ± 2°C. Air
bubbles were not observed any volatile organic analysis (VOA) vials.
Technical hold times were assessed from a comparison of the sampling and analysis dates. Samples were
analyzed for VOC within EPA-established holding times of seven days for unpreserved samples.
Calibration
Gas chromatograph/mass spectrometer (GC/MS) instrument tuning and performance checks are performed
to ensure the instrument's ability to provide appropriate mass-resolution, identification, and sensitivity. All
samples were analyzed for voe within twelve hours of the performance check standard. The tuning
compound mass-ion abundance criteria for the VOA were reported within control limits.
Control limits for initial and continuing calibrations are established to ensure that the instrument is capable
of producing accurate quantitative and qualitative data at the beginning and throughout each of the
analyses. Since the results of the initial calibration were not included in the laboratory report, the
evaluation was based on the review of continuing calibration data. Laboratory specifications were met
during the volatile organic continuing calibration conducted on May 13, 2002 at 16:57 on instrument
MSDA. The recovery of the continuing calibration standard, however, was not within 80-120% recovery
of the true value for the following target analytes: acrolein (52%), bromoform (71 %), l,2-dibromo-3-
chloropropene (75%), ethyl methacrylate (79%), naphthalene (67%), 1,2,3-trichlorobenzene (63%), 1,2,4-
trichlorobenzene (73%), trichlorofluoromethane (140%). Results for compounds where the recovery was
less than 80% during the continuing calibration have been qualified as estimated (J, UJ) in associated
samples. Positive sample results were qualified as estimated (J) when the recovery exceeded 120% in the
continuing calibration.
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APPENDIX A
GROUNDWATER SAMPLING ANALYTICAL REPORTS