IDX GW Monitoring Rpt May 2000 (SF)-OCR

* 5971 HSSF1066*
1111111111111111111111111111
DocumentlD NONCD0001814
Site Name HAMILTON BEACH/PROCTOR SILEX
oocumentType Progress/Monitoring Rpt (PRGMON)
RptSegment 1
DocDate
DocRcvd
Box
Accesslevel
Division
Section
Program
DocCat
9/8/2000
2/20/2007
SF1066
PUBLIC
WASTE MANAGEMENT
SUPERFUND
IHS (IHS)
FACILITY
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ltf1 RADIAN INTERNATIONAL
~ A DAMES & MOORE GROUP COMPANY
GROUNDWATER
MONITORING REPORT
FORMAY2000
Hamilton Beach OJ>roctor-Silex, Inc.
Washington, North Carolina Facility
Prepared for:
Hamilton Beach <)Proctor-Silex, Inc.
4421 Wateifront Drive
Glen Allen, Virginia 23060
Prepared by:
Radian International
1600 Perimeter Park Drive
Morrisville, North CarolifJa 27709
September 2000
State of North Carolina
Department of Environment
and Natural Resources
Washington Regional Office
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Mr. Mario Kuhar
DIVISION OF WATER QUALITY
GROUNDWATER SECTION
September 8, 2000
NORTH CAROl.INA DEPARTMENT OF'
ENVIRONMENT AND NJ(TURAl. RESOURCES
Hamilton Beach/Proctor Silex, Inc.
4421 Waterfront Drive
Glen Allen, Virginia 23 060
RE: May 2000 Quarterly Groundwater Sampling Report
Hamilton Beach/Proctor Silex, Inc.
Dear Mr. Kuhar:
Washington, North Carolina -Beaufort County
Groundwater Incident Number -14338
The Washington Regional Office received the above report, prepared by Radian International,
dated September, 2000 (received September 6, 2000). We appreciate you submitting this report to
our office.
Please continue to monitor groundwater quality until a corrective action plan is approved. We
appreciate your cooperation along with your effort to protect the state1s groundwater resources.
Should you have any questions regarding this matter, please don't hesitate to call me at 252-
946-6481, extension 3 3 5.
cc: City of Washington
Radian International
WaRO/
Sincerely,
Willie Hardison, Groundwater Supervisor
Washington Regional Office
943 Washington Square Mall, Washington, North Carolina 27889 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer
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GROUNDWATER MONITORING REPORT
FORMAY2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
Prepared for:
Hamilton Beach<>Proctor-Silex, Inc.
4421 Waterfront Drove
Glen Allen, Virginia 23060 ,..
Prepared by:
Radian International
P.O. Box 13000
Research Triangle Park, North Carolina 27709
September 2000
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TABLE OF CONTENTS
Certification Page ................................................................................................................ ii
List of Figures .................................................................................................................... iv
List of Tables ................................................................................................................... vii
1.0 IN"TRODUCTION ........................................................................................................... 1-1
2.0 FIELD METHODS ...... .' ................................................................................................... 2-1
3.0 RESULTS ........................................................................................................................ 3-1
3 .1 Water Level Measurements ................................................................................. 3-1
3.2 Analytical Results ................................................................................................ 3-1
APPENDIX A
APPENDIXB
GROUNDWATER SAMPLIN"G ANALYTICAL REPORTS
CONTAMIN"ANT CONCENTRATIONS VERSUS TIME
650138.0901 May2000GW _Rpt.doc (09/05/00) 111
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LIST OF FIGURES
1-1 Topographic Map, Hamilton Beach<>Proctor-Silex, Inc.
2-1 Site Map, Washington Facility, Hamilton Beach<>Proctor-Silex, Inc.
3-1 Generalized Groundwater Flow Direction for Hydrogeologic Unit A,
Washington F·acility
3-2 Generalized Groundwater Flow Direction for Hydrogeologic Unit B,
Washington Facility
3-3 Approximate Distribution ofTCE in Unit A
3-4 Approximate Distribution ofTCE in Unit B
3-5 Approximate Distribution ofTrichloroethene, D-D'
3-6 Approximate Distribution ofTrichloroethene, E-E'
3-7 Approximate Distribution of cis-1,2-DCE in Unit A
3-8 Approximate Distribution of cis-1,2-DCE in Unit B
3-9 Approximate Distribution of cis-1,2-DCE, D-D'
3-10 Approximate Distribution of cis-1,2-DCE, E-E'
3-11 Approximate Distribution of 1,1-DCE in Unit A
3-12 Approximate Distribution of 1,1-DCE in Unit B
3-13 Approximate Distribution of 1,1-DCE, D-D'
3-14 Approximate Distribution of 1,1-DCE, E-E'
3-15 Approximate Distribution of Vinyl Chloride in Unit A
3-16 Approximate Distribution of Vinyl Chloride in Unit B
3-17 Approximate Distribution of Vinyl Chloride, D-D'
3-18 Approximate Distribution of Vinyl Chloride, E-E'
650138.0901 May2000GW _Rpt.doc (09/05/00) IV
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LIST OF FIGURES (Continued)
3-19 Approximate Distribution of 1, 1, 1-TCA in Unit A
3-20 Approximate. Distribution of 1, 1, 1-TCA in Unit B
3-21 Approximate Distribution of 1,1,1-TCA, D-D'
3-;22 Approximate Distribution of 1,1,1-TCA, E-E'
3-23 Approximate Distribution of 1,2-DCA in Unit A
3-24 Approximate Distribution of 1,2-DCA in Unit B
3-25 Approximate Distribution of 1,2-DCA, D-D'
3-26 Approximate Distribution of 1,2-DCA, E-E'
3-27 Approximate Distribution of 1,1-DCA in Unit A
3-28 Approximate Distribution of 1,1-DCA in Unit B
3-29 Approximate Distribution of 1,1-DCA, D-D'
3-30 Approximate Distribution of 1,1-DCA, E-E'
3-31 Approximate Distribution of Benzene in Unit A
3-32 Approximate Distribution of Chloroform in Unit A
3-33 Approximate Distribution ofEthylbenzene in Unit A
3-34 Approximate Distribution of Naphthalene in Unit A
3-35 Approximate Distribution ofTetrachloroethene in Unit A
3-36 Approximate Distribution of Toluene in Unit A
3-37 Approximate Distribution of 1,1,2-TCA in Unit A
3-38 Approximate Distribution of 1,2,4-TMB in Unit.A
3-39 Approximate Distribution of 1,3,5-TMB in Unit A
3-40 Approximate Distribution of Total Xylenes in Unit A
80396902.01 May2000GW _Rpt.doc (09/05/00) v
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LIST OF FIGURES (Continued)
3-41 Single Detection VOC Concentrations in Unit A
3-42 Single Detection VOC Concentrations in Unit B
3-43 Cross-section Locations
3-44 Location of Surrounding Water Supply Wells
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2-1
3-1
3-2
3-3
3-4
3-5
LIST OF TABLES
Monitoring Well Construction Data for Sampled Wells
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
Water Level Measurements and Elevations, May 2, 2000
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-213
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-214
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-215
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-216
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-6 Historical Water Level Elevations at MW-220
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-7 Historical Water Level Elevations at MW-222
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-8 Historical Water Level Elevations at MW-224
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-9 Historical Water Level Elevations at MW-225
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-10 Historical Water Level Elevations at MW-226
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-11 Historical Water Level Elevations at MW-227
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-12 Historical Water Level Elevations at MW-228
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-13 Historical Water Level Elevations at MW-230
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
80396902.0 I May2000GW _Rpt.doc (09/05/00) vii
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LIST OF TABLES (Continued)
3-14 Historical Water Level Elevations at MW-234
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-15 Field Measurements, May 2, and 3, 2000
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-16 Summary of Qualified Groundwater Analytical Results: May 2000
Volatile Organic Compounds by Method 8260B
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-17 Historical Analytical Results for MW-213
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-18 Historical Analytical Results for MW-214
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-19 Historical Analytical Results for MW-215
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-20 Historical Analytical Results for MW-216
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-21 Historical Analytical Results for MW-220
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-22 Historical Analytical Results for MW-222
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-23 Historical Analytical Results for MW-224
Hamilton Bea:chOProctor-Silex, Inc., Washington, North Carolina
3-24 Historical Analytical Results for MW-225
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-25 Historical Analytical Results for MW-226
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-26 Historical Analytical Results forMW-227
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-27 Historical Analytical Results for MW-228
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
80396902.01 May2000GW _Rpt.doc (09/05/00) viii
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LIST OF TABLES (Continued)
3-28 Historical Analytical Results for MW-230
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-29 Historical Analytical Results for MW-234
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
80396902.01 May2000GW _Rpt.doc (09/05/00) lX
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1.0 INTRODUCTION
The Hamilton Beach¢ Proctor-Silex (HBOPS) facility is located at 234 Springs
Road, north of the City of Washington, in Beaufort County, North Carolina (Figure 1-1). The
facility and surrounding land parcel are owned by the City of Washington and have been leased
by HBO PS since 1990 and previously leased by predecessor companies. The facility is involved
in the final assembly, packaging, and warehousing of small electrical household appliances.
Since 1992, when organic compounds were initially detected in groundwater at
the site, several phases of investigation have been performed, including a comprehensive site
assessment (CSA). The results of the CSA indicated that a plume of organic compounds is
present in groundwater underlying the site. The specific nature, volume, and time period of any
releases contributing to the plume are unknown. However, the principal constituents of the
plume are no longer used at the facility.
A plan for corrective action at the site has been proposed. Until corrective action
is implemented, groundwater will be sampled and analyzed on a quarterly schedule according to
a monitoring program requested and approved by the North Carolina Department of
Environment and Natural Resources, Groundwater Section. The purpose of the monitoring
program is to sample selected downgradient monitoring wells to detect potential migration of the
plume.
Radian International (Radian) conducted groundwater sampling at the facility in
May 2000. The sampling event included the measurement of water levels, temperature, pH, and
specific conductance; and the collection and analysis of samples from thirteen monitoring wells.
This report describes the sampling methods and presents the results for the fourth quarterly
sampling event.
80396902.0 I May2000GW _Rpt.doc (09/05/00) 1-1
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2.0 FIELD METHODS
Groundwater was sampled on May 2 and 3, 2000, in general accordance with the
methods outlined in the Field Sampling and Analysis Plan prepared in April 1997 for this site.
Thirteen monitoring wells were sampled. They included MW-213 through
.MW-216, MW-220, MW-222, MW-224 through MW-228, MW-230, and MW-234. The
locations of the monitoring wells are shown in Figure 2-1. Details of well construction are
provided in Table 2-1.
Prior to sampling, the water level in each well was measured using an electric
water-level indicator. The wells were then purged using inertial foot-valve pumps, with the
exception of well MW-228 which was purged with a bailer. Temperature, pH, and specific
conductance were measured and the data were recorded in a field notebook. Purging continued
until temperature, pH, and specific conductance stabilized; a minimum of three well volumes
was extracted; or the well was pumped dry. Each of the wells was then sampled immediately
following well purging· using the inertial foot-valve pump or bailer.
The groundwater samples were sent by overnight courier to STL (formerly
Radian Analytical Services) in Austin, Texas, for analysis of volatile organic compounds by
EPA Method 8260B.
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3.0 RESULTS
3.1 Water Level Measurements
Table 3-1 presents the depth to groundwater and static water-level elevations
measured in the thirteen wells sampled and seven additional wells. Maps showing the
generalized direction of groundwater flow in hydrogeologic units A and B are included as
Figures 3-1 and 3-2, respectively. Historical water-level elevations in sampled wells are
included in Tables 3-2 to 3-14.
3.2 {"\.nalytical Results
Field measurements of water temperature, pH, and specific conductance are
summarized in Table 3-15. Qualified analytical results are summarized in Table 3-16. The
approximate extent of selected compounds which have been detected at concentrations
exceeding groundwater standards are illusulated in Figures 3-3 through 3-42. Cross-section
· locations are shown in Figure 3-43. Both current and historical data were used to approximate
the extent of contaminants. Qualified data sheets and laboratory reports are included in
Appendix A.
No analytes were detected above the groundwater standards in samples from
wells located nearth'.e perimeter of the site (MW-220, MW-222, MW-224, MW-225, MW-230,
') 1 , ,,/
and MW-234), nor were any analytes detected above the groundwater standards in the sample
from well MW-22_6, which is completed in the confined Limestone Aquifer. Also, no analytes
were detected above groundwater standards in samples collected from wells M:V-21,5 and MW--..
216, which are located 120 feet and 350 feet from the source i:rea, respectively. Concentrations
of chemicals exceeding the standards were detected in samples from wells MW-213, MW-214,
MW-227, and MW-228. These four wells are located at, or within 150 feet of, the source area.
Historical analytical results for the sampled wells are presented in Tables 3-17 to
3-29, and in graphs included as Appendix B. A comparison of the record for wells located near
80396902.01 May2000GW _Rpt.doc (09/05/00) 3-1
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the perimeter of the site suggests that the plume remains on-site, at least 200 feet from potential
·receptors located north of Spring Road (Figure 3-44). The latest results for wells located at the
source area and other interior portions of the site are consistent with earlier results and indicate
no significant changes in chemical concentration and distribution haye occurred.
650138.0901 May2000GW _Rpt.doc (09/05/00) 3-2 Hamilton Beach<>Proctor-Silex, Inc.
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FIGURES
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TABLES
- - - -.. --· -.. - --: - - - - - - -
Table 2-1
Monitoring Well Construction Data for Sampled Wells
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Top of Casing -
Installation Elevation Total Depth Screen Interval Filter Pack Bentonite Seal
Well No. Date (ft. above MSL) (ft. bgs) (ft. b2s)
MW-213 1/14/98 28.44 7.5 3 -7.5
MW-214 1/16/98 27.93 21 14.5 -21
MW-215 1116/98 28.06 10 8.5 -10
MW-216 5/5/98 32.82 35 26-35
MW-220 5/5/98 31.50 34 25-34
MW-222 5/6/98 35.11 40 31 -40
MW-224 11113/98 33.43 34 25 -34
MW-225 11/13/98 33.43 10 4-10
MW-226 9/30/98 28.46 75 70-75
MW-227 10/1198 28.47 25.5 20.5 -25.5
MW-228 9/23/98 28.71 10 3 -10
MW-230 10/26/98 33.47 14 8 -14
MW-234 6123199 35.03 26 17 -26
Monitoring wells 213 through 215 installed by Groundwater Management Associates, Inc.
Monitoring wells 216, 220, and 222 installed by Radian Mobile Field Services.
Monitoring wells 226 through 228 installed by Parratt Wolff, Inc.
Monitoring wells 224, 225, 230, and 234 installed by Probe Technology, Inc.
80396902.01 May2000GW _Rpt.doc (09/05/00)
(ft. b2s) (ft. bgs)
2.5 -7.5 1.5 -2.5
13.5 -21 12.5 -13.5
8 -10 7-8
25 -35 24-25
24-34 23 -24
30 -40 29-30
24-34 23 -24
3 -10 2-3
69-75 67 -69
19.5 25.5 17.5 -19.5
2-10 1-2
7 -14 5-7
16-26 13 -16
Grout Seal
(ft. be;s)
0 -1.5
0-12.5
0-7
0-24
0 23
0-29
0-23
0-2
0-67
0 -17.5
0-1
0-5
0-13
Table 3-1
Water Level Measurements and Elevations
May2, 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Measuring Point Water Level
Elevation Elevation
Well (ft above msl)) Depth to Water (ft) (ft above msl)
MW-201S 29.74 1.97 27.77
MW-208 32.11 5.39 26.72
MW-213 28.44 2.11. 26.33
MW-214 27.93 2.63 25.30
MW-215 28.06 3.22 24.84
MW-216 32.82 7.99 24.83
MW-217 32.75 7.62 25.13
MW-219 31.83 6.90 24.93
MW-220 31.50 5.69 25.81
MW-221 31.39 7.05 24.34
MW-222 35.11 11.53 23.58
MW-223 35.15 3.21 31.94
MW-224 33.43 6.95 26.48
MW-225 33.43 7.03 26.40
MW-226 28.46 17.65 10.81
MW-227 28.47 2.64 25.83
MW-228 28.71 2.35 26.36
MW-230 33.47 6.94 26.53
MW-233 34.55 9.00 25.55
MW-234 35.03 9.47 25.56
msl = mean sea level
80396902.01 May2000GW _Rpt.doc (09105100)
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Table 3-2
Historical Water Level Elevations at MW-213
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina .
Date
Mav 13, 1998
November 16, .1998
July 1, 1999
October 20, 1999
February 2, 2000
Mav 2, 2000
msl = mean sea level
NM= Not measured
80396902.01 May2000GW _Rpt.doc (09/05/00)
Water Level Elevation
(ft. above msl)
25.54
24.21,.
NM
NM,
26.41.
26.33 J
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Table 3-4
Historical Water Level Elevations at MW-215
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
F ebruarv 2, 2000
May2, 2000
msl = mean sea level
NM =Not measured
Water Level Elevation
(ft. above msl)
24.97
24.19
NM
NM
25.23
24.84
I 80396902.0 I May2000GW _Rpt.doc (09/05/00)
Table 3-5
Historical Water Level Elevations at MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
May2, 2000
msl = mean sea level
NM =Not measured
80396902.01 May2000GW _Rpt.doc (09/05/00)
Water Level Elevation
(ft. above msl)
24.39
22.37
NM
NM
24.84
24.83.
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Table 3-9
Historical Water Level Elevations at MW-225
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
Mav2, 2000
msl = mean sea level
NM =Not measured
80396902.01 May2000GW _Rpt.doc (09/05/00)
Water Level Elevation
(ft. above msl)
NM
24.36
24.50
27.24
26.59
26.40
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Table 3-10
Historical Water Level Elevations at MW-226
Hamiltm1 BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July 1, 1999
October 20, 1999
February 2, 2000
May2, 2000
msl = mean sea level
NM =Not measured
80396902.01 May2000GW _Rpt.doc (09/05/00)
Water Level Elevation
(ft. above msl)
NM
8.43
8.54
11.11
10.23
10.81
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Table 3-12
Historical Water Level Elevations at MW-228
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16,.1998
July 1, 1999
October 20, 1999
February 2, 2000
May2, 2000
msl = mean sea level
NM =Not measured
80396902.01 May2000GW _Rpt.doc (09105100)
Water Level Elevation
(ft. above msl)
NM
23.01
NM
NM
24.63
26.36
Table 3-13
Historical Water Level Elevations at MW-230
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, .1998
July 1, 1999
October 20, 1999
F ebruarv 2, 2000
May 2, 2000
msl = mean sea level
NM =Not measured
80396902.01 May2000GW _Rpt.doc (09/05/00)
Water Level Elevation
(ft. above msl)
NM
21.14
21.80
27.71
27.44
26.53
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Table 3-14
Historical Water Level Elevations at MW-234
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Date
May 13, 1998
November 16, 1998
July l, 1999
October 20, 1999
February 2, 2000
Mav 2, 2000
msl = mean sea level
NM = Not measured
80396902.0 I May2000GW _Rpt.doc (09/05/00)
Water Level Elevation
(ft. above msl)
NM
NM
23.24
25.71
25.67
25.56
Well Date Time
MW-213 513100 08:16
MW-214 513100 08:40
MW-215 513100 08:48
MW-216 512100 13:25
MW-220 512100 13:05
MW-222 512100 13:50
MW-224 512100 12:20
MW-225 512100 12:12
MW-226 512100 11:05
11:10
11:15
11:17
11:20
MW-227 513100 09:20
MW-228 513100 09:34
MW-230 512100 14:15
MW-234 512100 12:50
Table 3-15
Field Measurements
May 2, 2000
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Volume Purged
(Gal) Purn:inl!: Criteria
2.8 3 well volumes
9.0 3 well volumes
1.7 Dry
0.85 3 well volumes
0.85 3 well volumes
0.9 3 well volumes
0.8 3 well volumes
0.15 3 well volumes
9.0 Stabilized parameters
11.0
14.0
17.0
20.0
11.0 3 well volumes
3.8 3 well volumes
0.5 3 well volumes
0.6 3 well volumes .
Specific
Temperature Conductance
(OC) (µS) oH
20.5 340 5.7
18.5 280 6.1
21.5 180 6.2
20.0 420 7.0
21.5 105 7.1
20.5 370 6.8
18.0 325 7.2
19.0 170 5.1
20.0 450 7.3
20.0 440 7.5
20.5 440 7.4
20.5 440 7.4
20.5 440 7.4
20.0 500 6.7
19.0 2100 3.6
19.0 265 4.5
20.0 170 6.6
-------------------
-------------------
Sample ID
Date of SampUng
Analyte {µg/L)
Acetone
Benzene
2-Butanone (MEK)
n=Butylbenzene
sec-Butyl benzene
Carbon tetrachloride
Chloroethane
Chloroform
Chloromethane
1,2-Dichlorobenzene
I, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
l, 1-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
p-Isopropyltoluene
Methyl t-butyl ether
4-Methyl-2-pentanone (MIBK)
Methylene chloride
Naphthalene
n-Propylbenzene
80396902.01 May2000GW _Rpt.doc (09/05/00)
Table 3-16
Summary of Qualified Groundwater Analytical Results: May 2000
Volatile Organic Compounds by Method 8260B
Hamilton BeachOProctor-Silex, Washington, North Carolina
MW-213 MW-214 MW-215 MW-216
513100 513100 513100 512100
ND (0.286) ND (0.286) ND (0.286) ND (0.286)
0.495 J 0.304 J ND (0.0492) ND (0.0492)
ND (0.179) UJ ND (0.179) UJ ND (0.179) UJ ND (0.179)
0.184 J ND (0.0642) ND (0.0642) ND (0.0642)
0.268 J ND (0.0745) ND (0.0745) ND (0.0745)
ND (0.0867) ND (0.0867) ND (0.0867) ND (0.0867)
ND(0.0756) 0.705 ND (0.0756) ND (0.0756)
0.577 ND (0.0670) ND (0.0670) ND (0.0670)
ND (0.0821) UJ ND (0.0821) UJ ND (0.0821) UJ ND (0.0821)
0.349 J ND (0.0920) ·ND (0.0920) -ND (0.0920)
178 173 3.43 ND (0.0487)
4.49 0.607 ND (0.0499) ND (0.0499)
4·01 15.4 1.93 ND (0.0706) U
·40.6 12.0 0.0409 J ND (0.0603)
1.41 0.794 ND (0.0813) ND (0.0813)
ND (0.0464) ND (0.0464) ND (0.0464) ND (0.0464)
0.727 ND (0.0552) ND (0.0552) ND (0.0552)
ND (0.167) UJ ND (0.167) UJ ND (0.167) UJ ND (0.167) UJ
0.400 J ND (0.0474) ND (0.0474) ND (0.0474)
0.182 J ND (0.0452) ND (0.0452) ND (0.0452)
ND (0.0469) ND (0.0469) 1.10 ND (0.0469)
ND (0.0845) UJ ND (0.0845) UJ ND (0.0845) UJ ND (0.0845)
ND (0.0796) ND (0.0796) ND (0.0796) ND (0.0796)
16.7 J ND (0.106) UJ ND (0.106) UJ ND (0.106)
ND (0.0886) ND (0.0886) ND (0.0886) ND (0.0886)
MW-220 MW-222
512100 512100
ND (0.286) ND (0.286)
ND (0.0492) ND (0.0492)
ND (0.179) ___ ND (0.179)
ND (0.0642) ----ND (0.0642)
ND (0.0745) ND (0.0745)
ND (0.0867) ND (0.0867)
ND (0.0756) ND (0.0756)
ND (0.0670) ND. (0.0670)
~ND (0.0821) ND (0.0821)
ND (0.0920) ND (0.0920)
ND (0.0487) -·· 0.338 J
ND (0.0499) ND (0.0499)
ND (0.0697) U ND (0.279) U
ND (0.0603) ND (0.0603)
ND (0.0813) ND (0.0813)
ND (0.0464) ND (0.0464)
ND (0.0552) ND (0.0552)
ND (0.167) UJ ND (0.167) UJ
ND (0.0474) ND.(0.0474)
ND (0.0452) ND (0.0452)
0.441 J ND (0.0469)
ND (0.0845) ND (0.0845)
ND (0.0796) ND (0.0796)
ND (0.106) ND (0.106)
ND (0.0886) ND (0.0886)
Sample ID MW-213
1, 1, 1,2-Tetrachloroethane ND (0.0948)
1, 1,2,2-Tetrachloroethane ND (0.0792)
Tetrachloroethene 34.4
Tetrahydrofuran ND (0.402) UJ
Toluene 0.335 J
1, 1, 1-Trichloroethane 0.928
1, 1,2-Trichloroethane 3.17
Trichloroethene 479
Trichlorofluoromethane 1.26 J
1, 1,2-Trichlorotrifluoroethane ND (0.0766)
1,2,4-Trimethylbenzene 0.509 J
1,3 ,5-Trimethylbenzene 0.248 J
Vinyl chloride 16.0
m&p-Xylene 0.935 J
o-Xylene 1.59
Target analytes not listed were not detected.
Bold values exceed Standards.
ND ( ) = Not detected at specified detection limit.
J = Estimated value.
la c:\hamilton\washington\csa-rpt (9/5/00)
Table 3-16 (Continued)
MW-214 MW-215 MW-216 MW-220 MW-222
ND (0.0948) ND (0.0948) ND (0.0948) ND (0.0948) ND (0.0948)
ND (0.0792) ND(0.0792) ND (0.0792) ND (0.0792) ND (0.0792)
ND (9.0568) ND (0.0568) ND (0.0568) ND (0.0568) ND (0.0568)
ND (0.402) UJ 15.0 ND (0.402) ND (0.402) ND (0.402)
ND (0.0680) ND (0.0680) ND (0.0680) ND (0.0680) ND (0.0680)
ND (0.0331) ND (0.0331) ND (0.0331) ND (0.0331) ND (0.0331)
ND (0.0952) ND (0.0952) ND (0.0952) ND (0.0952) ND (0.0952)
0.494 J 0.124 J ND (0.0905) ND (0.0905) ND (0.0905)
ND (0.208) ND (0.208) ND (0.208) ND (0.208) ND (0.208)
ND (0.0766) ND (0.0766) ND (0.0766) ND (0.0766) ND (0.0766)
ND (0.0749) ND (0.0749) ND (0.0749) ND (0.0749) ND (0.0749)
ND (0.0436) ND (0.0436) ND (0.0436) ND (0.0436) ND (0.0436)
9.73 ND (0.0574) ND (0.0574) ND (0.0574) ND (0.0574)
ND (0.137) ND (0.137) ND (0.137) ND (0.137) ND (0.137)
ND (0.0713) ND (0.0713) ND (0.0713) ND (0.0713) ND (0.0713)
------~------------
-------------------
Table 3-16 (Continued)
Sample ID MW-224 MW-225 MW-226 MW-227 MW-228 MW-230 MW-234
Date of Sampling 5/2/00 512100 512100 513100 513/00 512100 512100
Analyte (µg/L)
Acetone . ND (0.286) ND (0.286) ND (0.286) 19.1 J 360 J ND (0.286) ND (0.286)
Benzene ND (0.0492) ND (0.0492) ND (0.0492) 0.622 J 56.5J ND (0.0492) ND (0.0492)
2-Butanone (MEK) ND (0.179) ND (0.179) ND (0.179) 40.2J 382J ND (0.179) ND (0.179)
n-Butylbenzene ND (0.0642) ND (0.0642) ND (0.0642) ND (0.0642) UJ 9.88 J ND (0.0642) ND (0.0642)
sec-Butyl benzene ND (0.0745) ND (0.0745) ND (0.0745) ND (0.0745) UJ 7.96J ND (0.0745) ND (0.0745)
Carbon tetrachloride ND (0.0867) ND (0.0867) ND (0.0867) ND (0.0867) UJ 26.2J ND (0.0867) ND (0.0867)
Chloroethane ND (0.0756) ND (0.0756) ND (0.0756) 14.6 J 89.8 J ND (0.0756) ND (0.0756)
Chloroform ND (0.0670) ND (0.0670) ND (0.0670) 1.17 J 9.62J ND (0.0670) ND (0.0670)
Chloromethane ND (0.0821) ND (0.0821) ND (0.0821) ND (0.0821) UJ 1.33 J ND (0.0821) ND (0.0821)
1,2-Dichlorobenzene ND (0.0920) ND (0.0920) ND (0.0920) ND (0.0920) UJ ND (Q.0920) UJ ND (0.0920) ND (O.Q920)
1, 1-Dichloroethane ND (0.0487) ND (0.0487) ND~ (0.0487) ,_3,360 14,500 ND (0.348) U ND (0.0487)
1,2-Dichloroethane ND (0.0499) ND (0.0499) ND (0.0499) 20.2J ND (0.0499) UJ ND (0.0499) ND (0.0499)
1, 1-Dichloroethene ND (0.292)U NJ? (0.0697) ND (0.115) U 644 53,400 0.593 0.145 J
cis-1,2-Dichloroethene ND (0.0603) ND (0.0603) ND (0.0603) 381 2,360 0.573 ND (0.0603)
trans-1,2-Dichloroethene ND (0.0813) ND (0.0813) ND (0.0813) 7.93 J 17.0J ND (0.0813) ND (0.0813)
1, 1-Dichloropropene ND (0.0464) ND (0.0464) ND (0.0464) 0.182 J 1.51 J ND (0.0464) ND (0.0464)
Ethylbenzene ND (0.0552) ND (0.0552) ND (0.0552) 0.454J 555J ND (0.0552) ND (0.0552)
2-Hexanone ND (0.167) UJ ND (0.167) UJ ND (0.167) UJ ND (0.167) UJ 38.8J ND (0.167) UJ ND (0.167) UJ
Isopropylbenzene ND (0.0474) ND (0.0474) ND (0.0474) ND (0.0474) UJ 33.7 J ND (0.0474) ND (0.0474)
p-Isopropyltoluene ND (0.0452) ND (0.0452) ND (0.0452) ND (0.0452) UJ ND (0.0452) UJ ND (0.0452) ND (0.0452)
Methyl t-butyl ether ND (0.0469) ND (0.0469) ND (0.0469) 0.322 J 20.8 J ND (0.0469) _ ND (0.0469)
4-Methyl-2-pentanone (MIBK) ND (0.0845) ND (0.0845) ND (0.0845) ND (0.0845) UJ 17.5J ND (0.0845) ND (0.0845)
Methylene chloride ND (0.0796) ND (0.0796) ND (0.0796) 0.982 u ND (3.64) UJ ND (0.0796) ND (0.0796)
Naphthalene . ND (0.106) ND (0.106) ND (0.106) ND (0.982) UJ 246J ND (0.106) ND (0.106)
n-Propylbenzene ND (0.0886) ND (0.0886) ND (0.0886) ND (0.0886) UJ 302J ND (0.0886) NJ? (0.0886)
1, 1, 1,2-Tetrachloroethane ND (0.0948) ND (0.0948) ND (0.0948) ND (0.0948) UJ 0.844 J ND (0.0948) ND (0.0948)
1, 1,2,2-Tetrachloroethane ND (0.0792) ND (0.0792) ND (0.0792) 1.48J ND (0.0792) UJ ND (0.0792) ND (0.0792)
80396902.01 May2000GW _Rpt.doc (09/05/00)
Sample ID MW-224
Tetrachloroethene ND (0.0568)
Tetrahydrofuran ND (0.402)
Toluene 0.0542 J
1, 1, I -Trichloroethane ND (0.0331)
1, 1,2-Trichloroethane ND (0.0952)
Trichloroethene ND (0.0905)
Trichlorofluoromethane ND (0.208)
1, 1,2-Trichlorotrifluoroethane ND (0.0766)
1,2,4-Trimethylbenzene ND (0.0749)
1,3,5-Trimethylbenzene ND (0.0436)
Vinyl chloride ND (0.0574)
m&p-Xylene ND (0.137)
o-Xylene ND (0.0713)
Target analytes not listed were not detected.
ND ( ) = Not detected at specified detection limit.
Bold values exceed Standards.
J = Estimated value.
la c:\hamilton\washington\csa-rpt (9/5/00)
Table 3-16 (Continued)
MW-225 MW-226 MW-227
ND (0.0568) ND (0.0568) ND (0.0568) UJ
ND (0.402) ND (0.402) ND (0.402) UJ
ND (0.0680) ND (0.0680) 13.8J
ND (0.0331) ND (0.0331) 2,440 J
ND (0.0952) ND (0.0952) 2.95J
ND (0.0905) ND (0.0905) 48.9J
ND (0.208) ND (0.208) ND (0.208) UJ
ND (0.0766) ND (0.0766) ND (0.0766)
ND (0.0749) ND (0.0749) 0.720 J
ND (0.0436) ND (0.0436) 0.646 J
ND (0.0574) ND (0.0574) 5.51 J
ND (0.137) ND (0.137) 0.956 J
ND (0.0713) ND (0.0713) 0.995 J
MW-228 MW-230 MW-234
. 32.4 J ND (0.0568) ND (0.0568)
ND (0.402) UJ ND (0.402) ND (0.402)
1,520 0.0826 J ND (0.0680)
121,000 J ND (0.0331) ND (0.0331)
38.0J ND (0.0952) ND (0.0952)
13,300 1.11 ND (0.0905)
8.12 J ND (0.208) ND (0.208)
0.947 J ND (0.0766) ND (0.0766)
1,190 J ND (0.0749) ND (0.0749)
407J ND (0.0436) ND (0.0436)
194J ND (0.0574) ND (0.0574)
1,680 J ND (0.137) ND (0.137)
1,350 ND (0.0713) ND (0.0713)
-------------------
-------------------
Groundwater
Analyte Standard
Benzene 1
n-Butylbenzene 70
sec-Butylbenzene 70
Chloroform 0.19
1,2-Dichlorobenzene 620
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
Ethylbenzene 29
Isopropylbenzene 70
p-Isopropyltoluene -
Napthalene 21
Tetrachloroethene 0.7
Tetrahydrofuran -
Toluene 1000
1, 1, I-Trichloroethane 200
1, 1,2-Trichloroethane -
Trichloroethene 2.8
Trichlorofluoromethane 2100
Table 3-17
Historical Analytical Results for MW-213
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November
May 1998 1998 July 1999 October 1999
NS 0.724 NS NS
NS 0.240 NS NS
NS 0.315 NS NS
NS 0.793 NS NS
NS 0.642 NS NS
NS 351 NS NS
NS 7.02 NS NS
NS 867 NS NS
NS 39.3 NS NS
NS 2.22 NS NS
NS 2.03 NS NS
NS 0.618 NS NS
NS ND (0.106) NS NS
NS 15.7 J NS NS
NS 61.3 NS NS
·NS 7.63 J NS NS
NS 1.48 NS NS
NS 1.09 NS NS
NS 6.03 NS NS
NS 515 NS NS
NS 0.575 NS NS
February 2000 Mav2000
ND (0.984) 0.495 J,
ND (1.28) 0.184 j
ND (1.49) 0.268 J
ND (1.34) 0.577 --
ND (1.84) 0.349 J --
245 178 -
6.12 J 4.49 .-
492 401 .-
' 40.8 40.6 -F-
ND (1.63) -· 1.41 . -""'
ND (1.10) . .,.. 0.727 -
ND (0.948) 0.400 J -
ND (904) 0.182J ...,.,
ND (2.12) 16.7 +-
44.4 34.4 -
ND (8.4) ND (0.402) -
Nb {l.36) 0.335 J .,,
ND (0.662) 0.928
2.16 J 3.17
446 479
ND (4.16) 1.26
Groundwater
Analyte Standard Mav 1998
1,2, 4-Trimethylbenzene 350 NS
1,3 ,5-Trimethylbenzene 350 NS
Vinyl chloride 0.015 NS
m&p-Xylene 530 NS
o-Xylene 530 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
la c:\hamilton\washington\csa-rpt (9/5/00)
Table 3-17 (Continued)
November
1998 Julv 1999 October 1999 February 2000 May2000
ND (0.0952) NS NS ND (1.50) 0.509 J
ND (0.0800) NS NS ND (0.872) 0.248 J
38.7 NS NS 29.3 16.0
1.57 NS NS ND (2.74) 0.935 J
3.43 NS NS ND (1.43) 1.59
-------------------
-------------------
Groundwater
Table 3-18
Historical Analytical Results for MW-214
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November
Analyte Standard May 1998 1998 July 1999 October 1999
Benzene 1 NS
Chloroethane 2800 NS
1, 1-Dichloroethane 700 NS
1,2-Dichloroethane 0.38 NS
1, 1-Dichloroethene 7 NS
cis-1,2-Dichloroethene 70 NS
trans-1,2-Dichloroethene 70 NS
p-Isopropyltoluene -NS
Trichloroethene 2.8 NS
Vinyl chloride 0.015 NS
Target analytes_ not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND = Not detected at (detection limit).
NS = Not sampled.
0.172 J
0.485 J
108
0.303 J
8.16
6.86
0.478
0.181 J
ND (0.587) U
8.84
U = Not present above the associated level; blank contamination is present.
80396902.01 May2000GW _Rpt.doc (09/05/00)
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
February 2000 May2000
0.315 J 0.304 J
0.904 0.705
179 173
0.633 0.607
13.8 15.4
11.7 12.0
0.701 0.794
ND (0.0452) ND (0.0452)
0.289 J 0.494 J
11.5 9.73
Groundwater
Table 3-19
Historical. Analytical Results for MW-215
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November
Analyte Standard May 1998 1998 Julv 1999 October 1999
Benzene 1 NS
1, 1-Dichloroethane 700 NS
1, 1-Dichloroethene 7 NS
cis-1,2-Dichloroethene 70 NS
Ethylbenzene 29 NS
Methyl t-butyl ether 200 NS
Tetrahydrofuran -NS
Trichloroethene 2.8 NS
Vinyl chloride 0.015 NS
m&p-Xylene 530 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
0.0963 J
4.30
3.85
ND (0.104) U
0.0601 J
1.22
58.6
ND (0.322) U
0.381 J
0.0885 J
U = Not present above the associated level; blank contamination is present.
80396902.01 May2000GW _Rpt.doc (09/05/00)
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
Februarv 2000 Mav·2000
0.114 J Nb (0.0492)
4.07 3.43
3.02 1.93
0.0401 J 0.0409 J
ND (0.0552) ND (0.0552)
ND (0.0469) 1.10
19.1 15.0
0.138 J 0.124J
ND (0.0574) ND (0.0574)
ND (0.137) ND (0.137)
-------------------
-------------------
Groundwater
Table 3-20
Historical Analytical Results for MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November
Analvte Standard May 1998 1998 July 1999 October 1999
Toluene 1000 0.171
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
UJ = Not detected and the detection limit is estimated.
80396902.01 May2000GW _Rpt.doc (09/05/00)
ND (0.0522) UJ NS NS
February 2000 Mav2000
ND (0.0680) ND (0.0680)
Groundwater
Table 3-21
Historical Analytical Results for MW-220
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November
Analvte Standard Mavl998 1998 Julv 1999 October 1999
Carbon disulfide 700 ND (0.0547)
Methyl t-butyl ether 200 ND (0.0365)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
UJ = Not detected and the detection limit is estimated.
80396902.01 May2000GW_Rpt.doc (09/05/00)
ND (0.0547) 0.426 J 0.162
ND (0.0365) UJ ND (0.0334) ND (0.0512)
Februarv 2000 Mav2000
ND (0.0484) UJ ND (0.0484)
ND (0.0469) 0.441 J
-------------------
-------------------
Table 3-22
Historical Analytical Results for MW-222
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analyte Standard May 1998
Carbon disulfide 700 ND (0.0547)
I, 1-Dichloroethane 700 ND (0.0576)
1, 1-Dichloroethene 7 0.0908 J
Toluene 1,000 0.156 J
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND = Not detected at (detection limit).
Washington, North Carolina
November 1998 July 1999
ND (0.0547) 0.388 J
ND (0.0576) ND (0.0736)
ND (0.0715) ND (0.102)
ND (0.0522) ND (0.0766)
UJ = Not detected and the detection limit is estimated.
80396902.01 May2000GW _Rpt.doc (09/05/00)
October 1999
0.0944
ND (0.0588)
ND (0.0819)
ND (0.0645)
February 2000 May2000
ND (0.0484) UJ ND (0.0484)
ND (0.0487) 0.338 J
ND (0.0697) ND (0.279)U
ND (0.0680) ND (0.0680)
Table 3-23
Historical Analytical Results for MW-224
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analyte Standard May1998
Carbon disulfide 700 NS
Toluene 1,000 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
November 1998 July 1999
ND (0.0547) 2.22
ND (0.0522) ND (0.0766)
UJ = Not detected and the detection limit is estimated.
80396902.0 I May2000GW _ Rpt.doc (09/05/00)
October 1999
2.72
ND (0.0645)
February 2000 Mav2000
ND (1.05) UJ ND (0.334) U
(0.0680) 0.0542 J
-------------------
-------------------
Groundwater
Table 3-24
Historical Analytical Results for MW-225
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Analvte Standard Mav1998 November 1998 July 1999 October 1999
Carbon disulfide 700 NS
Chloroform 0.19 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
ND (0.0547)
ND (0.0480)
UJ = Not detected and the detection limit is estimated.
80396902.01 May2000GW _Rpt.doc (09705/00)
ND (0.864) 0.0691
ND (0.0424) 0.171
Februarv 2000 Mav2000
ND (0.0484) UJ ND (0.0484)
ND (0.0670) ND (0.0670)
Groundwater
Table 3-25
Historical Analytical Results for MW-226
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Analyte Standard May1998 November 1998 July 1999 October 1999
Carbon disulfide 700 NS
Target analytes not listed were not detected ..
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
ND (0.0547)
UJ = Not detected and the detection limit is estimated.
80396902.0 l May2000GW _Rpt.doc (09/05/00)
ND (0.864) 0.0950
February 200 May2000
ND (0.0484) UJ ND (0.0484) UJ
~------------------
-------------------
Groundwater
Analvte Standard
Acetone 700
Benzene 1
2-Butanone (MEK) 170
n-Butylbenzene 70
Carbon disulfide 700
Carbon tetrachloride 0.3
Chloroethane 2800
Chloroform 0.19
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
1, 1-Dichloropropene -
Ethyl benzene 29
Isopropylbenzene 70
p-Isopropyltoluene -
Methyl t-butyl ether 200
Methylene chloride 5
Napthalene 21
n-Propylbenzene 70
80396902.0 I May2000GW _Rpt.doc (09/05/00)
Table 3-26
Historical Analytical Results for MW-227
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November
May 1998 1998 July 1999 October 1999
NS 29.9 J NS NS
NS 0.668 J NS NS
NS 42.5 J NS NS
NS 0.437 J NS NS
NS 0.573 J NS NS
NS ND (0.0576) UJ NS NS
NS 2.14 J NS NS
NS 1.64 J NS NS
NS 4,620 NS NS
NS 19.5 J NS NS
NS 705 NS NS
NS 228 NS NS
NS 3.66 J NS NS
NS ND (0.0444) UJ NS NS
NS 3.58 J NS NS
NS 0.392 J NS NS
NS 0.194 J NS NS
NS ND (0.0365) UJ NS NS
NS ND (1.13) UJ NS NS
NS 3.73 J NS NS
NS 2.25 J NS NS
February 2000 May2000
ND (5.72) 19.1 J
ND (0.984) 0.622 J
ND (3.58) 40.2 J
ND (1.28) ND (0.0642) UJ
ND (0.968) ND (0.0484) UJ
ND (1.73) 26.2J
ND (1.51) 14.6 J
ND (1.34) 1.17 J -
844 3,360
4.40 J 20.2
'
108 644
105 381
ND (1.63) 7.93 J
ND (0.928) 0.182 J
I
ND (9.38) 0.454 J
ND (0.948) ND (0.0474) UJ
ND (0.904) ND (0.045f) UJ
ND (0.938) 0.322 J
ND (1.59) 0.982.U
ND (2.12) ND (0.982) UJ
ND (1.77) ND (0.0886) UJ
Groundwater
Analyte Standard May1998
1, 1,2,2-Tetrachloroethane 0.17 NS
Tetrachloroethene 0.7 NS
Toluene 1000 NS
I, 1, I -Trichloroethane 200 NS
1, 1,2-Trichloroethane -NS
Trichloroethene 2.8 NS
1,2,4-Trimethylbenzene 350 NS
1,3,5-Trimethylbenzene 350 NS
Vinyl chloride 0.15 NS
m&p-Xylene 530 NS
o-Xylene 530 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
80396902.0 l May2000GW _ Rpt.doc (09/05/00)
Table 3-26 (Continued)
November
1998 July 1999 October 1999 February 2000 May2000
ND (0.102) UJ NS NS ND (1.58) 1.48 J
1.41 J NS NS ND (1.14) ND (0.0568) UJ
29.6J NS NS 3.56 J 13.8J
3,200 NS NS 310 2,440J
3.20J NS NS ND (1.90) 2.95 J
810 NS NS 12.9 48.9 J
10.8 J NS NS ND (1.50) 0.720 J
3.37 J NS NS ND (0.872) 0.646 J
5.70 J NS NS ND (1.15) 5.51 J
8.78 J NS NS ND (2.74) 0.956 J
8.91 J NS NS ND (1.43) 0.995 J
~------------------
-------------------
Groundwater
Analvte Standard
Acetone 700
Benzene 1
2-Butanone (MEK) 170
n-Butylbenzene 70
sec-Butylbenzene 70
Carbon tetrachloride 0.3
Chloroethane 2800
Chloroform 0.19
Chloromethane 2.6
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
trans-1,2-Dichloroethene 70
1, 1-Dichloropropene -
Ethylbenzene 29
2-Hexanone -
Isopropylbenzene 70
p-Isopropyltoluene -
Methyl t-butyl ether 200
4-Methyl-2-pentanone (MIBK)
Napthalene 21
80396902.01 May2000GW _Rpt.doc (09/05/00)
Table 3-27
Historical Analytical Results for MW-228
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Mav 1998 November 1998 Julv 1999 October 1999
NS 307 J NS NS
NS 51.3 J NS NS
NS 21.3 J NS NS
NS 15.6 J NS NS
NS 5.27 J NS NS
NS 42.2J NS NS
NS 74.7 J NS NS
NS 12.8 J NS NS
NS ND (0.0521) UJ NS NS
NS 24,100 NS NS
NS 96,500 NS NS
NS 3,330 NS NS
NS 24.2 J NS NS
NS ND (0.0444) UJ NS NS
NS 544 NS NS
NS 45.1 J NS NS
NS 41.5 J NS NS
NS 6.80J NS NS
NS 5.21 J NS NS
NS 12.3 J NS NS
NS 608 NS NS
February 2000 Mav2000
ND (1,430) 360 J
ND (246) 56.5 J
ND (895) 382 J
ND (321) 9.88 J
ND (372) 7.96 J
ND (434) 26.2 J
ND (378) 89.8 J
ND (335) 9.62J
ND (410) 1.33 J
16,200 14,500
71,800 53,400
1,970 J 2,360
ND (406) 17.0 J
ND (232) 1.51 J
414 J 555 J
ND (835) 38.8 J
ND (237) 33.7 J
ND (226) ND (0.0452) UJ
ND (234) 20.8 J
ND (422) 17.5 J
ND (530) 246J
Groundwater
Analyte St~ndard May1998
n-Propylbenzene 70
1, 1, 1,2-Tetrachloroethane -
1, 1,2,2-Tetrachloroethane 0.17
Tetrachloroethene 0.7
Toluene 1000
1, 1, I-Trichloroethane 200
1, 1,2-Trichloroethane -
Trichloroethene 2.8
Trichlorofluoromethane 2100
l, 1,2-Trichlorotrifluoroethane 210,000
1,2,4-Trimethylbenzene 350
1,3,5-Trimethylbenzene 350
Vinyl chloride 0.15
m&p-Xylene 530
o-Xylene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
80396902.01 May2000GW _Rpt.doc (09/05/00)
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Table 3-27 (Continued)
November 1998 July 1999 October 1999 February 2000 May2000
200 NS .NS ND (443) 3021
0.810J NS NS ND (474) 0.844 J
0.688 J NS NS ND (396) ND (0.0792) UJ
30.5 J NS NS ND (284) 32.4J
1,460 NS NS 1,610 J 1,520
173,000 NS NS 135,000 121,000 J
49.3 J NS NS ND (476) 38.0J
22,800 NS NS 15,000 13,300
12.7 J NS NS ND (l,040) 8.12J
ND (0.0986) NS NS ND (383) 0.947 J
1,270 NS NS 1,220 J 1,190 J
309 NS NS ND (218) 407 J
314 NS NS ND (287) 194 J
1,540 NS NS 1,760 1,680 J
1,330 NS NS 1,370 1,350
-------------------
-------------------
Table 3-28
Historical Analytical Results for MW-230
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analvte Standard May 1998
1, 1-Dichloroethane 700 NS
1, 1-Dichloroethene · 7 NS
Cis-1,2-Dichloroethene 70 NS
Toluene 1,000 NS
Trichloroethene 2.8 NS·
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND = Not detected at (detection limit).
NS = Not samp~ed.
Washington, North Carolina
November
1998 July 1999
ND (0.0576) ND (0.0736)
ND (0.306) U ND (0.102)
ND (2.67) U ND (0.0595)
ND (0.0522) 0.286
ND(2.05)U ND (0.0929)
U = Not present above the associated level; blank contamination is present.
80396902.0 I May2000GW _Rpt.doc (09/05/00)
October 1999
0.265
0.133
0.304
ND (0.309) U
0.921
February 2000 May2000
0.189 J ND (0.348) U
0.148 J 0.593
0.354 J 0.573
0.284 J 0.0826 J
0.661 J --1.11
Table 3-29
Historical Analytical Results for MW-234
Hamilton BeachOProctor-Silex, Inc.
Groundwater
Analyte Standard Mav1998
Carbon disulfide 700 NS
1, 1-Dichloroethene 7 NS
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS = Not sampled.
Washington, North Carolina
November 1998 July 1999
NS ND (0.864)
NS ND (0.102)
U = Not present above the associated level; blank contamination is present.
UJ = Not detected and the detection limit is estimated.
80396902.01 May2000GW _Rpt.doc (09105100)
October 1999
0.0600
ND (0.0819)
February 2000 May2000
ND (0.0484) UJ ND (0.0484)
ND (0.0697) 0.145 J
'-------------------
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APPENDIX A
GROUNDWATER SAMPLING ANALYTICAL REPORTS
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QUALIFIED DATA
Date of
Continuing Associated
Calibration Results samples
butadiene (135%), 2-hexanone (78%), 5-isopropylbenzene (121 %), methyl
methacrylate (78%), 1,1,1-TCA (126%), 1,2,3-Trichloropropane (77%),
and 1, 1,2-trichlorotrifluoroethane ( 131 % ).
May8 Acetonitrile (74%), acrolein.(64%), acrylonitrile (78%), MEK (70%), Samples
@15:08 chloromethane (76%), l,2-dibromo-3-chloropropane (79%), trans-1,4-analyzed
dichloro-2-butene (74%), 2,2-dichloropropane (122%), hexachloro-1,3-5/8.
butadiene (137%), 2-hexanone (66%), methyl methacrylate (78%), MIBK
(67%), naphthalene (78%), tetrahydrofuran (73%), 1,2,3-trichlorobenzene
(73% ), trichlorofluoromethane ( 134% ), and 1, 1,2-trichlorotrifluoroethane
(126%).
May9 Acrolein (67%), bromomethane (39%), chloromethane (62%), trans-1,4-Samples
@16:49 dichloro-2-butene (57%), 2,2-dichloropropene (124%), hexachloro-1,3-analyzed 5/9
butadiene (138%), 1,2,3-trichlorobenzene (125%), 1,2,4-trichlorobenzene and 5/10.
(133%), 1,1,1-trichloroethane (123%), and trichlorofluoromethane (127%).
Results for these compounds where the recovery was less than 80% have been qualified as estimated (J,
UJ) in associated samples. Positive sample results were qualified as estimated (J) when the recovery
exceeded 120% in the continuing calibration.
Blank Contamination
Laboratory blanks are clean liquid and/or solid matrix samples prepared by the analytical laboratory and
analyzed in the same manner as the field samples. Laboratory blanks are used to ensure that the field
samples are not contaminated during the sample preparation, sample analysis, or from previous sample
(instrument carry-over). Trip blanks are analyte-free water samples that accompany volatile investigative
samples during all stages of shipment, storage, and analysis. The trip blanks are used to assess the potential
for artificial introduction of volatile compounds into the investigative samples during the transportation and
sample handling processes.
Methylene chloride, a common laboratory blank contaminant, was detected at a concentration ranging from
0.102 J to 0.347 J parts per billion (ppb) in the laboratory blanks. The trip blank contained carbon disulfide
at a concentration of 0.538 J ppb. Sample results that were not significantly greater (ten times for
methylene chloride, five times for carbon disulfide) than that detected in the blanks have been qualified due
to the presence of blank contamination. Affected results have been flagged "ND" and detection limits
elevated to the amount present in the sample and flagged with a "U".
The laboratory suspected carryover during VOA conducted on May 9 and 10th. Sample results suspected of
being affected by instrument carryover were qualified with a V-flag by the laboratory. Except for acetone,
2-butanone, and naphthalene, similar concentrations were obtained during the reanalysis of samples that
were conducted at similar dilutions. Acetone, 2-butanone, and naphthalene were not detected upon
reanalysis of 0500HBWD999 and 0500HBWW227 at higher dilutions. The original and reanalysis results
for these analytes have been qualified as estimated (J) in both samples because of the poor precision.
Surrogate Spikes
Surrogate compound percent recoveries are used to assess extraction efficiencies, possible matrix effects,
and overall analytical accuracy during organic analyses. Acceptable sample results were obtained for the
surrogate spikes during the VOA of all project samples, except 0500HBW -D999, -W227, and -W228. The
recovery for l ,2-dichloroethane-d4 was less than laboratory specification limits ( 61-143% ), but greater than
10%, during the undiluted analysis of these three samples. Acceptable recoveries were obtained for all
surrogate compounds during reanalysis. The volatile organic results from the undiluted analysis of samples
0500 HB-PS DE.doc
Page 2of3
06/09/00
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~~-~--~~~----~--~~­SECTION IV
Analytical Results
MS-VOA
SW8260B
''
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-l
75-05-8
l 07-02-8
107-13-l
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/30/200021:14
0500HBWW216
2000505106
Aaueous
Received
NA
05/02/2000 13 :30
05/04/2000 22:50
05/04/2000 22:50
l.0000
MSDA
ug/L
Cone Flag DL
ND 0.286
ND \;..-:S l.67
ND ~":) 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND \,\"} 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
I.IMS Workordcr: 756200.UA-Little Wa~hington, N [l000505 I] Hamilton Beach-Proctor Silex
STl.Auslin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW220 0500HBWW222
2000505105 2000505107
Aaueous Aaueous
Received Received
NA NA
05/02/2000 13: IO 0510212000 13:55
0510412000 22:22 05/04/2000 23: 18
05/04/2000 22:22 0510412000 23:18
l.0000 l.0000
MSDA MSDA
ug/L ug/L
Cone Flag DL RL Cone Flag DL
ND 0.286 0.000 ND 0.286
ND v..::5 l.67 0.000 ND \/\..:f l.67
ND IA..\ 0.983 0.000 ND \1""\ 0.983
ND 0.0901 0.000 ND 0.0901
ND 0.0492 0.000 ND 0.0492
ND 0.0622 0.000 ND 0.0622
ND 0.139 0.000 ND 0.139
ND 0.0683 0.000 ND 0.0683
ND V'-""S 0.136 0.000 ND vw 0.136
ND 0.106 0.000 ND 0.106
ND 0.179 0.000 ND 0.179
ND 0.0642 0.000 ND 0.0642
ND 0.0745 0.000 ND 0.0745
ND 0.0958 0.000 ND· 0.0958
ND 0.0484 0.000 ND 0.0484
ND 0.0867 0.000 ND 0.0867
ND 0.0839 0.000 ND 0.0839
ND 0.0473 0.000 ND 0.0473
ND 0.0756 0.000 ND 0.0756
ND 0.0670 0.000 ND 0.0670
ND 0.113 0.000 ND 0.113
Page 4
Sample result> Jun•e b<'l'll lfll/llijied by Rmlilm lnu·nwtiwwl bast-./ uu the l'l'itcrit1 aj Iii<' dt1W n·~·h•11• process. which;, 11111111·/,·cl 11//<'1 1/1<· Cimtrm·1 l.11/1111111my l'ro!/111111 N11tio1111/ F1111c1w1111/ <i11itl!'/i111•,
fur Org1111ic 11111l lllorg1111ic /111111 Rel'i<'ll' (11.S. F.l'A. October 199911111/ h·/Jrn111:1· /!NI. 1e1p1·c111•e/.rJ.
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
..
Continued
Parameter
Chloromethane
3-Chloroprooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
l .2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
1,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1,4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichlorodilluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
I 2-Dichloroorooane 78-87-5
I 3-Dichloroorooane 142-28-9
2 2-Dichlorooropane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-1,3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/30/200021:14
0500HBWW216
2000505106
Cone Flag DL
ND 0.0821
ND O.ll I
ND 0.113
ND 0.0762
ND ~ 1.05
ND \.I.\ 0.0564
ND \i..._'\ 0.152
ND ill..:\ 0.0939
ND l}...J 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND ·~ 0.113
ND 0.0487
ND 0.0499
0.0706\.\.. j t-0 ~
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND vw 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND \A.-S 0.167
LIMS Workorder: 756200.UA-Little Washington, N (20005051] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW220 0500HBWW222
2000505105 2000505107
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0762 0.000 ND 0.0762 0.000
ND V...'"3 1.05 0.000 ND u:! 1.05 0.000
ND 11'\ 0.0564 0.000 ND IL\ 0.0564 0.000
ND IA.'). 0.152 0.000 ND ~ 0.152 0.000
ND lk""S 0.0939 0.000 ND u..3' 0.0939 0.000
ND I A."! 0.390 0.000 ND \A.\ 0.390 0.000
ND 0.0587 0.000 ND 0.0587 0.000
ND 0.0920 0.000 ND 0.0920 0.000
ND 0.0591 0.000 ND 0.0591 0.000
ND V\.."3' 0.113 0.000 ND \,.Q 0.113 0.000
ND 0.0487 0.000 0.338 J 0.0487 0.000
ND 0.0499 0.000 ND 0.0499 0.000
4H3 ¥1~C> 0.06971h 0.000 0.279 v... f l'ID 0:fi69!1 0.000 . ND 0.0603 0.000 ND 0.0603 0.000
ND 0.0813 0.000 ND 0.0813 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.0451 0.000 ND 0.0451 0.000
ND 0.0714 0.000 ND 0.0714 0.000
ND 0.0464 0.000 ND 0.0464 0.000
ND 0.0366 0.000 ND 0.0366 0.000
ND I A.:J" 0.0658 0.000 ND l.t'-1" 0.0658 0.000
ND 0.0647. 0.000 ND 0.0647 0.000
ND 0.0552 0.000 ND 0.0552 0.000
ND 0.212 0.000 ND 0.212 0.000
ND \A.."J 0.167 0.000 ND vt.::r 0.167 0.000
Page 5 of 34
Sample result~· luu•i• been t/t1ttlifietl by Rmlian /11tenu1tioulll """""""tit<' 1 nit ·iw oj '"" t111w n·_i•i<•11• pron·IS, 11•/tich" 111otldnl 11/1<·1 1/1<· ( '0111mc1 [ 11/111mtmy /'rogt 11111 N111io111tl F1111< 11111111/ (i11id1'11111•,
... ---Jrgm-lt10141imtt111R--l.S.,.."lllb1·1~11/f ... /!i!l"'m'·111·e~-- - -·-· - ---- -
-~----~------~-~~-­SECTION IV
Analytical Results
MS-VOA
SW82608
.. Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4~Methvl-2-oentanone (MIBK) l 08-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
I, I I 2-Tetrachloroethane 630-20-6
I I 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
1.2 4-Trich lorobenzene 120-82-1
I ,I 1-Trich loroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
TrichloroOuoromethanc 75-69-4
1,2 3-Trichlorooropane 96-18-4
I. I 2-Trichlorotrifluoroethane 76-13-1
1.2.4-Trimethvlbenzene 95-63-6
1,3,5-TrimethYlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -05/30/2000 21 :14
0500HBWW216
2000505106
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND lA'.:J 0.114
ND 0.0469
ND 0.0845
ND 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND u:r 0.467
ND 0.118
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
+J.9-' R 0.9438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STL Austin
0500HBWW220 0500HBWW222
2000505105 2000505107
RL Cone Flaa DL RL Cone Flaa DL
0.000 ND 0.0616 0.000 ND 0.0616
0.000 ND 0.0474 0.000 ND 0.0474
0.000 ND 0.0452 0.000 ND 0.0452
0.000 ND \A_-:J 0.114 0.000 ND V-."! 0.114
0.000 0.441 J 0.0469 0.000 ND 0.0469
0.000 ND 0.0845 0.000 ND .0,0845
0.000 ND 0.0796 0.000 ND 0.0796
0.000 ND 0.106 0.000 ND 0.106
0.000 ND 0.688 0.000 ND 0.688
0.000 ND 0.0886 0.000 ND 0.0886
0.000 ND 0.0722 0.000 ND 0.0722
0.000 ND 0.0948 0.000 ND 0.0948
0.000 ND 0.0792 0.000 ND 0.0792
0.000 ND 0.0568 0.000 ND 0.0568
0.000 ND 0.402 0.000 ND 0.402
0.000 ND 0.0680 0.000 ND 0.0680
0.000 ND i>-:0 0.467 0.000 ND \.A.,,\ 0.467
0.000 ND 0.118 0.000 ND 0.118
0.000 ND 0.0331 0.000 ND 0.0331
0.000 ND 0.0952 0.000 ND 0.0952
0.000 ND 0.0905 0.000 ND 0.0905
0.000 ND 0.208 0.000 ND 0.208
0.000 ND 0.0543 0.000 ND 0.0543
0.000 ND 0.0766 0.000 ND 0.0766
0.000 ND 0.0749 0.000 ND 0.0749
0.000' ND 0.0436 0.000 ND 0.0436
Q.QQQ NB-R 0.9438 0.000 NB R 0.0438
0.000 ND 0.0574 0.000 ND 0.0574
Page 6
I I I lift I b R I. I · 11 .· I 11 t/J .. 1.1·1.,.1·1111.r111,. 11111t1 re1•il'll'l1roce1·5 which;, 1111111.·li·d 11/tc1 th<' ( umrnc1l11l111rt11111·r l'r111;r11111 N11tio11t1I Fw1C·tu111al (,"11itldiiu•, S'omp/e resu ll '"''e Jee11 'I'"' 1 1et y "' um 11tt•nwt1011t1 >mic1 u < ' < 'J . · • • . • ..
fur Orgm1ic m11i /11vrgw1ic I >altl Rni1•11· (11.S. £/'A. Octlllwr /999 1111.I I C'i1n1111T / l)l)-1, 1'<'1/U'C//l'<'(l J . .,
'·
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
e.ooo
0.000
of 34
-.. - -·-..... .... - --~ -.. .. .. ... - -
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
.. Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound .
l-Bromo-4-fluorobenzene
I' 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -05/30/2000 21: !4
0500HBWW216
2000505106
Aaueous
Received
NA
05/02/2000 13:30
0510412000 22:50
0510412000 22:50
I.0000
MSDA
U!!IL
% Recoverv Limits
100 77-117
lOI 6I-143
103 87-113
LIMS Workordcr: 756200.UA-Littlc Washington, N [2000505 lj Hamilton Beach-Proctor Silex
STLAustin
F
0500HBWW220 0500HBWW222
2000505105 2000505107
Aaueous Aaueous
Received Received
NA NA
0510212000 13: I 0 0510212000 13:55
0510412000 22:22 0510412000 23:I8
0510412000 22:22 0510412000 23:I8
l.0000 l.0000
MSDA MSDA
ug/L ul!IL
% Recoverv Limits F % Recoverv Limits
IOI 77-117 103 77-I I7
102 61-143 101 61-143
104 87-113 104 87-1I3
Page 8
Sample l'<'Slllts l1tll'<' b<'l'll lflllllijied by Rmlimi /11tcmatimwl Jmsl'd 011 rh1• 1·n11.,.111 of Jiu• d111t1 n•l'i<'ll' proc'·~s. 11•hid1 r~ m11d1·/,·tf 11/1<·1 ti(<' ( 'u11tmct 1-11bor111111:r l'rogr11111 N11tio1111/ /·i111<"1wmil U11idl'i1111•,
fur Orga11ic 11111/ ltrurg1111ic />11111 Rl'1•ii'1r (U.S. £1'.1. Octol>l'r 19991111,/ I l'l1m11rr l'J'J./, n·vp1·c111·1·l,1 J.
F
of 34
-~-~--~~~--------~­SECTION IV
Analytical Results
MS-VOA
SW82608
Continued
Parameter
Ch loromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1'
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromoch loromethane 124-48-1
1,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Di ch lorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1,2-Dichloroprooane 78-87-5
I 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1 3-Dichloropropene 10061-01-5
trans-1.3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/30/2000 21 :14
0500HBWW224
2000505103
Cone Flaa DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND \.>-, ",.} 1.05
ND IA'.T 0.0564
ND A.'.\ 0.152
ND IA.:i' 0.0939
ND I)._""\' 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND ' V\'.:\ 0.113
ND 0.0487
ND 0.0499
0.292 IA Y 1-lD O.Og9:;?
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND u.. . .'.) 0.0366
ND 'A--\ 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND lA -s 0.167
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-l;roclor Silex
STL Austin
0500HBWW225 0500HBWW226
2000505102 2000505101
RL· Cone Flaa DL RL Cone Flag DL
0.000 ND 0.0821 0.000 ND 0.0821
0.000 ND 0.111 0.000 ND 0.111
0.000 ND 0.113' 0.000 ND 0.113
0.000 ND 0.0762 0.000 ND 0.0762
0.000 ND IA""\ 1.05 0.000 ND I.>-.-:.\ 1.05
0.000 ND I.I.,:\ 0.0564 0.000 ND 1.A,3 0.0564
0.000 ND \/\.0° 0.152 0.000 ND LI:\ o·.152
0.000 ND IA,:) 0.0939 0.000 ND \A.:\ 0.0939
0.000 ND \;.:,S 0.390 0.000 ND \A.-:\ 0.390
0.000 ND 0.0587 0.000 ND 0.0587
0.000 ND 0.0920 0.000 ND 0.0920
0.000 ND 0.0591 0.000 ND 0.0591
0.000 ND \A.-S-0.113 0.000 ND LA . .:...i 0.113
0.000 ND 0.0487 0.000 ND 0.0487
0.000 ND 0.0499 0.000 ND 0.0499
6.666 ND 0.0697 0.000 0.115 "'-· 1 r-tD 0.969il
0.000 ND 0~0603 0.000 ND 0.0603
0.000 ND 0.0813 0.000 ND 0.0813
0.000 ND 0.0670 0.000 ND 0.0670
0.000 ND 0.0451 0.000 ND 0.0451
0.000 ND 0.0714 0.000 ND 0.0714
0.000 ND 0.0464 0.000 ND 0.0464
0.000 ND \M 0.0366 0.000 ND ~ 0.0366
0.000 ND iA\ 0.0658 0.000 ND i!.\ 0.0658
0.000 ND 0.0647 0.000 ND 0.0647
0.000 ND 0.0552 0.000 ND 0.0552
0.000 ND 0.212 0.000 ND 0.212
0.000 ND \AJ' 0.167 0.000 ND iA.,":l" 0.167
Page IO
Sample results hm•e been t/1ttdified by Raditm //l/C'mtlTicmal basetl 011 !ht' in1t·iw oj !Ill' dt11t1 re~·it·w proceH. wliicli fa 111tJ1/d.-d ,~f/t't th<' ( 'u11/nt<'i l.11/wrntc>1:i· l'rog1w11 N111im1ttl V.11111101111/ liuidcli11n
for Organic mu/ "1orgt111ic l>t11t1 Re1•ieir (tl.S. F.l'.1. Ocwlwr 1999 awl I d1n1111:r / '.)l).J. reVpC'c 111'£'/J ).
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 .
0.000
0.000
0.000
0.000
0.000
0.000
0.000
e.ooo
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
''
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsopropyltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Prooylbenzene 103-65-1
Styrene 100-42-5
1. I. I 2-Tetrachloroethane 630-20-6
I, 1,2 i-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2J-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
I 1 I-Trichloroethane 71-55-6
I, 1,2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorotluoromethane 75-69-4
I 2.3-Trichloroorooane 96-18-4
I 1,2-Trichlorotritluoroethane 76-13-1
l 2.4-Trimethvlbenzene 95-63-6
I 3 5-Trimethylbenzene 108-67-8
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -05/30/2000 21: 14
0500HBWW224
2000505103
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND ~ 0.114
ND 0.0469
ND 0.0845
ND 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
0.0542 'S" 0 0.0680
ND \It..:} 0.467
ND 0.118
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
Nfr K. 0.9438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N (2000505 I] Hamilton Bcach-P~octor Silex
STLAustin
0500HBWW225 0500HBWW226
2000505102 2000505101
RL Cone Flag DL RL Cone Flaa DL RL
0.000 ND 0:0616 0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.000 ND 0.045i 0.000 ND 0.0452 0.000
0.000 ND u...--s 0.114 0.000 ND \,/\.'"J 0.114 0.000
0.000 ND 0.0469 0.000 ND 0.0469 0.000
0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.000 ND 0.0796 0.000 ND 0.0796 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.688 0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.000 ND 0.0568 0.000 ND 0.0568 0.000
0.000 ND 0.402 0.000 ND 0.402 0.000
0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.000 ND iA-:l 0.467 0.000 ND \;\:5 0.467 0.000
0.000 ND 0.118 0.000 ND 0.118 0.000
0.000 ND 0.0331 0.000 ND 0.0331 0.000
0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.000 ND 0.0905 0.000 ND 0.0905 ·o.ooo
0.000 ND 0.208 0.000 ND 0.208 0.000
0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.000 ND 0.0766 0.000 ND 0.0766 0.000
0.000 ND 0.0749 0.000 ND 0.0749 0.000
0.000 ND 0.0436 0.000 ND 0.0436 0.000
Q.006 ND' R. 6.0438 0.000 ND K 6.6lfj8 67000
0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page II of 34
-
....Jf!e!.!.pll' result~ /un•i• /J<'t'll <Jlllllijied by Rmlimi llllt'nurticnwl bme1/ u11 rhc, rtlC'l'ltl of //w dat11 n·~·it'1t' Jll"OC<'l.\', 11·/iic/i il 111oddnl a/1c1 th<' ( 'u111mct /.abort//Ol'I' l'rogra111 Nati01111/ f-111111101111/ (i11idl'i11w'
--Jrgm-fllor~1tc1R-l.S.~-robc·-1111/J-·1!)9~·111•£•l---- --· -·-__ -
-------~-~-----~---­SECTION IV
Analytical Results
MS-VOA
SW82608
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Ch loro-1 3-butadiene
Ch lorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/30/2000 21 :14
0500HBWW230
2000505108
Aaueous
Received
NA
05/02/2000 14:20
05/04/2000 23:46
05/04/2000 23 :46
l.0000
MSDA
ug/L
Cone Flag DL
ND 0.286
ND \A:\ 1.67
ND IA."3 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND \A:::5 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workordcr: 756200.UA·Littlc Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
0500HBWW234
2000505104
Aaueous
Received
NA
05/02/2000 12:55
05/04/2000 21 :54
05/04/2000 21 :54
1.0000
MSDA
ug/L
RL Cone Flag
0.000 ND
0.000 ND 1A-r
0.000 ND tA.-:5
0.000 ND
0.000 ND
0.000 ND
0.000 ND
0.000 ND
0.000 ND Vw
0.000 ND
0.000 ND
0.000 ND
0.000 ND
0.000 ND
0.000 ND
0.000 ND
0.000 ND
0.000 ND
.0.000 ND
0.000 ND
0.000 ND
TRIP BLANK
2000505109
Aaueous
Received
NA
05/02/2000 00:00
05/05/2000 00: 13
0510512000 00: 13
1.0000
MSDA
_ug/L
DL RL Cone Flaa DL RL
0.286 0.000 ND 0.286 0.000
1.67 0.000 ND u;r l.67 0.000
0.983 0.000 ND I.A\ 0.983 0.000
0.0901 0.000 ND 0.0901 0.000
0.0492 0.000 ND 0.0492 0.000
0.0622 0.000 ND 0.0622 0.000
0.139 0.000 ND 0~139 6.ooo
0.0683 0.000 ND 0.0683 0.000
0.136 0.000 ND iA.~ 0.136 0.000
0.106 0.000 ND 0.106 0.000
0.179 0.000 ND 0.179 0.000
0.0642 0.000 ND 0.0642 0.000
0.0745 0.000 ND 0.0745 0.000
0.0958 0.000 ND 0.0958 0.000
0.0484 0.000 0.538 j 0.0484 0.000
0.0867 0.000 ND 0.0867 0.000
0.0839 0.000 ND 0.0839 0.000
0.0473 0.000 ND 0.0473 0.000
0.0756 0.000 ND 0.0756 0.000
0.0670 0.000 ND 0.0670 0.000
0.113 0.000 ND 0.113 0.000
Page 14 of
Smupl<' n•sull' Jww b£'<'ll 1[1tlllijied by Rllllillu /u/C'l"ll1tli111111/ b11sl'd 011f/11·1"1"11<·n11 oj 1/w d111t1 /"!'l'it'll' Jll"lll"<'H. which ;, 11101"'/.·d <(/1<·1 1hc ( iJ111tm 1 / aborwmy !'l"tl.~mm N111im111/ J-"11111"/1tJ11til (11iiddin1•,
fur Orga11ic m11/ illorg1111ic /J11w Re1•il'll' (11.S. F.l'.1. Ocw/>i•r !999 11111/ / l'imu11:r llJIJ./. 11•.\pcct11·<·(1 J.
34
SECTION IV
Analytical Results
MS-VOA
SW8260B
..
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I ,2-Dibromo-3-chloroorooane 96-12-8
Dibromoch loromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1,4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
l 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1,2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
I 2-Dichloroorooane 78-87-5
1 3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
I, 1-Dichloropropene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexach loro-1,3-butad iene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/30/2000 21: 14
0500HBWW230
2000505108
Cone Flag DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND \A'.::f l.05
ND V\\ 0.0564
ND l.k""\ 0.152
ND \.\., \ 0.0939
ND i,f\,J 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND \A."J 0.113
0.348 \A. Y r~h Q.,Q4B]
ND , 0.0499
0.593 0.0697
0.573 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND IA.3° 0.0366
ND IA.\ 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND \A,J 0.167
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STL.Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
.0.000
0.000
0.000
0500HBWW234 TRIP BLANK
2000505104 2000505109
Cone Flag DL Rl Cone Flaa DL RL
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.111 0.000 ND 0.11 l 0.000
ND O.ll3 0.000 ND 0.113 0.000
ND 0.0762 0.000 ND 0.0762 0.000
ND \1--:I l.05 0.000 ND w 1.05 0.000
ND iA. :s 0.0564 0.000 ND V\..3 0.0564 0.000
ND iA.::S 0.152 0.000 ND iA..} 0.152 0.000
ND ~ .. :::r 0.0939 0.000 ND IA.:f 0.0939 0.000
ND V....-:\ 0.390 0.000 ND ,A :f 0.390 0.000
ND 0.0587 0.000 ND 0.0587 0.000
ND 0.0920 0.000 ND 0.0920 0.000
ND 0.0591 0.000 ND 0.0591 0.000
ND lA.:r 0.113 0.000 ND l,,A.:":S 0.113 0.000
ND 0.0487 0.000 ND 0.0487 0.000
ND 0.0499 Ci.000 ND 0.0499 0.000
0.145 J 0.0697 0.000 ND 0.0697 0.000
ND 0.0603 0.000 ND 0.0603 0.000
ND 0.0813 0.000 ND 0.0813 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.0451 0.000 ND 0.0451 0.000
ND 0.0714 0.000 ND 0.0714 0.000
ND 0.0464 0.000 ND 0.0464 0.000
ND ~ 0.0366 0.000 ND IA3" 0.0366 0.000
ND \A:J 0.0658 0.000 ND 11-:\ 0.0658 0.000
ND 0.0647 0.000 ND 0.0647 0.000
ND 0.0552 0.000 ND 0.0552 0.000
ND 0.212 0.000 ND 0.212 0.000
ND vcr 0.167 0.000 ND \.).:f 0.167 0.000
Page 15 of 34
Smrrple l'l'l1tlts 11111.,. been ,111atijied by Ratlimi /menwticmal bmC'd 011 tlw 1 r11c1w of tilt' daw n•1•it•w /Jl'{)Cl'.H, which Cl 11wd..t,·d 1~/tc1 tll<' ( 'v111r111·1 l 11/wnt1cu:1· l'rogrum N11ti1m11/ Fwu·twmil <i11idf'iitt•·'
-.-it:'Jrgll-l11or~11t1R-l.S.~wbc·im.1111/J .. ·/l)l) .... clll'<'llilll - - - - - - - - -
------~---------~-~ SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Iodomethane
Isooropylbenzene
4-Isooroovltoluene
Methyl methacrvlate
Client Sample ID
Lab Sample ID
CAS
74-88-4
98-82-8
99-87-6
80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) I 08-10-1
Methylene chloride 75-09-2.
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I 1.1.2-Tetrachloroethane 630-20-6
I 1,2 2-Tetrachloroethane 79-34-5
Tetrach loroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2,3-Trichlorobenzene 87-61-6
I 2,4-Trich lorobenzene 120-82-1
I I.I-Trichloroethane 71-55-6
0500HBWW230
2000505108
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND IA::) 0.114
ND 0.0469
ND 0.0845
ND 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
0.0826 J 0.0680
ND \A:\ 0.467
ND 0.118
ND 0.0331
0500HBWW234 TRIP BLANK
2000505104 2000505109
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 .ND 0.0616 0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.000 ND i.A.,~ 0.114 0.000 ND f..A."S 0.114 0.000
0.000 ND 0.0469 0.000 ND 0.0469 0.000
0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.000 ND 0.0796 0.000 ND 0.0796 0.000
0.000 ND 0.106 0.000 ND 0.106 . 0.000
0.000 ND 0.688 0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.000 ND 0.0568 0.000 ND .0.0568 0.000
0.000 ND 0.402 0.000 ND ·0.402 0.000
0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.000 ND ~...) 0.467 0.000 ND IJ-_.""J' 0.467 0.000
0.000 ND 0.118 0.000 ND 0.118. 0.000
0.000 ND 0.0331 0.000 ND 0.0331 0.000
I 1.2-Trichloroethane 79-00-5 ND 0.0952 0.000 ND 0.0952 0.000 ND 0.0952 .0.000
Trichloroethene 79-01-6 1.11 0.0905
Trichlorofluoromethane 75-69-4 ND 0.208
I 2 3-Trichloropropane 96-18-4 ND 0.0543
I I 2-Trichlorotrifluoroethane 76-13-1 ND 0.0766
I 2 4-Trimethylbenzene 95-63-6 ND 0.0749
1,3 5-Trimethvlbenzene 108-67-8 ND 0.0436
Vinvl acetate 108-05-4 cNtt--K 0 04J8
Vinyl chloride 75-01-4 ND. 0.0574
SECTION IV -Analytical Results -05/30/2000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N (20005051] Hamilton Beach-Proctor Silex
STLAustin
0.000 ND 0.0905 0.000 ND 0.0905
0.000 ND 0.208 0.000 ND 0.208
0.000 ND 0.0543 0.000 ND 0.0543
0.000 ND 0.0766 0.000 ND 0.0766
0.000 ND 0.0749 0.000 ND 0.0749
0.000 ND 0.0436 0.000 ND 0.0436
9.999. NB-f-9.(}438 6.000 ND-f2_ '6-:t)zt38
0.000 ND 0.0574 0.000 ND 0.0574
Page 16
Sampll' rl'sults /un•I' bl'ell ,11111/ijieti by Radiwi /ull'fllllficuw/ basl'd u111/11" ,., ll<'rlll of lit<' t/11111 rc·~·i,•11• procl'.H. ll'iticlt 1~ 11111,/,·/,·d 11/1,·1 tlil' ( !J111mc1 /.11b1w111cn:i-l'm~r11111 N111io1111/ Fw1c1w1ut! (;11idc·/1111"'
for Organic a11d /J10Q~1111ic /Jm11 R"1·i1·11 (11.S. El'A. Ocwbl'f" /9!.19 mu// 1·hm111:i /1)9.J. n·1pc·c111·e~1 J.
0.000
0.000
0.000
0.000
0.000
0.000
0.006-
0.000
of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
p-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -05/30/2000 21 :14
0500HBWW230
2000505108
Cone Flaa DL
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-LiUle Washington, N [20005051] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0500HBWW234 TRIP BLANK
2000505104 2000505109
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND 0.0713 0.000 ND 0.0713 0.000
Page 17 of 34
-Smuple re~ultl lilll'<' beC'll lflllllijietl by Rmlillll //ll('rllilliomtl b11sc1J 011 the1 nt1·r111oj1111• t/11111 n•1•iell' proce.1s. which il 111mll'/nl 11fti·1 the ( ·01111twt l.11/wrntm:I' l'rugr.1111 N11tio1111/ J-"1111<·11111111/ Ci11itldi111''
.... Jrgt11-Jnor41!91tllR--l.S.~wfu•1-111tl/-... /!J!J~c111·c•~ .. -·--·--;--- -
-- -
- - -... SECTION IV
Analytical Results
Surrogates
MS-VOA
SW82608
Surroaate Compound
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results-05/30/2000 21:14
0500HBWW230
2000505108
AQueous
Received
NA
05/02/2000 14:20
05/04/2000 23 :46
05/04/2000 23:46
1.0000
MSDA
ug/L
% Recoverv Limits
IOI 77-117
IOI 61-143
103 87-113
LIMS Workorder: 756200.UA-Little Washington, N (20005051] Hamilton Beach-Proctor Silex
STLAustin
-- ----- - -
0500HBWW234 TRIP BLANK
2000505104 2000505109
AQueous AQueous
Received Received
NA NA
05/02/2000 12:55 05/02/2000 00:00
05/04/2000 21 :54 05/05/2000 00: I 3
05/04/2000 21 :54 05/05/2000 00:13
1.0000 1.0000
MSDA MSDA
u12:/L ug/L
F % Recoverv Limits F % Recoverv Limits
103 77-117 100 77-117
102 61-143 IOI 61-143
102 87-113 103 87-113
Page 18
Smuple result;"""" been q1talified by /fodit1J1 /ntl'ri1tllim1til bml'tl 0111/Jc1'11/c/'ltl 11} 1/ie du111 r£'1'it-11· proce.1s. 1d1id1 i; 111odc!t·d 11/1e1 the l 0111111< I l.11bo11u111y l'ro-~ra111 N111i111111/ h11w1w1111/ <i11itldi111•,
/111· Organic· m11/ /11orgc111ic I Iara Rei•il'W (I l.S. F./'.1. Octo/wr 1999 11111/ / d1rn111T /9<J.J. 11'\[Jl'Cli1-e~1 J.
- -
F
of 34
-------------------SECTION IV
Analytical Results
MS-VOA
SW82608
Continued
Parameter
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1 4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1,2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1,2-Dichloroorooane 78-87-5
1.3-Dichlorooropane 142-28-9
2 2-Dichloroprooane 594-20-7
1, 1-Dichloroorooene 563-58-6
cis-1 3-Dichloropropene 10061-01-5
trans-I 3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethylbenzene I 00-41-4
Hexachloro-1,3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWD999
200050570 1-
Cone Flaa DL
ND v.:s-0.0821
ND 0.111
ND 0.113
ND 0.0762
ND I 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND I 0.0920
ND I 0.0591
ND ~ 0.113
~36 £R 0,041!'.7
23.7 ·:r 0.0499
-4%6 ER 0.0697
349 ~R n -~~
·~
9.11 ::J' . 0.0813
ND IA:f 0.0670
ND v.:r 0.0451
ND I.A\ 0.0714
0.181 J 0.0464
ND ID 0.0366
ND VIJ' 0.0658
ND IA J 0.0647
0.810 )/~ 0.0552
ND l• !.r 0.212
ND V-v"\ 0.167
LIMS Workorder: 756200.UA-Littlc Washington, N [20005057) Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Q.QOO
0.000
~000
v ......
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWD999 0500HBWW213
2000505706@ 2000505701 i
Cone Flaa DL RL Cone Flaa DL RL
Nfl ' i2 . -ND IA"".\ 0.0821 0.000 "T.IV v.vilU
N[ 5.55 o.too ND 0.111 0.000
NI 5.65 ctooo ND 0.113 0.000
NI• 3.81 J>.000 ND 0.0762 0.000
N' 52.5 /0;000 ND IA.-:\ J.05 0.000
NP 2.82 I o.ooo ND 0.0564 0.000
N' 1.60 I 0.000 ND 0.152 0.000
NP 4.10 I 0.000 ND 0.0939 0.000
N ~ 19.5/ 0.000 ND \A,-:\ 0.390 0.000
N) 2.94 0.000 ND 0.0587 0.000
1J11 4.00 0.000 0.349 J 0.0920 0.000
lllD 2.1>6 0.000 ND 0.0591 0.000
&-lf dt=i: ~.~~o ND 0.113 0".000
3560 2.44 0.000 468 .. IBR ~.6487 6.66()•
~ J' " ~-~Q (l.()00 4.49 0.0499 0.000
684 3.48 0.000 -3-64 ~R G-:e697 6.600
394 3.02 0.000 40.6 0.0603 0.000
"9:6t j R.. -1.41 0.0813 0.000 .JU v::UW
ND 3.35 0.000 ND 0.0670 0.000
ND 2.26 o.~oo ND 0.0451 0.000
ND 3.57 Qlooo ND V& 0.0714 0.000
ND 2.32 D.ooo ND -0.0464 0.000
ND 1.83 /0.000 ND 0.0366 0.000
NI 3.29 I o.ooo ND 0.0658 0.000
N'> 3.24 I 0.000 ND 0.0647 0.000
ND 2.16 I 0.000 0.727 0.0552 0.000
N b. IO.fl 0.000 ND 0.212 0.000
NB' I" 8.:.~ ~:000 ND LLJ 0.167 0.000
(!) µ•"'Lu.-iu ( "i I 2..6lr0 n~-~ t(IVi Y
Page~ of 60
Swuple resultl hm•<' been ,11wtijietl by Rmliim lutenwticmal bmecl 011 1/i,· l'l'll<"l"lll of th<' cla/ll n·~·i,•11• process. which i> 1111,,/1·/n/ <!/In th<' ( "v111rnc1l11bon11111:i· l'rogmm N11tio1111/ f-"11111'/101111/ li11itll"iu11.,
{'or Organic amt /11org1111ic /la/ti Re1•il'1r (U.S. EPA. Octobl'r 1999mu/1-<'brnarr l':J'J-1. n·1p<'cli1'e~1J.
' '·
,'
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Iodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methyl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
I. I, 1,2-Tetrachloroethane 630-20-6
I I 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
I 2 3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
I. I I-Trichloroethane 71-55-6
I.I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloroorooane 96-18-4
I I 2-Trichlorotrifluoroethane 76-13-1
I 2 4-Trimethvlbenzene 95-63-6
I 3 5-Trimethylbenzene 108-67-8
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWD999
2000505706 i
Cone Flaa DL
ND IA.:f 0.0616
ND 0.0474
ND 0.0452
ND I( 0.114
0.538 J 0.0469
ND u:r 0.0845
1.00lA.J" XrS.D~
25.0 J"i 0.106
ND il\..:f 0.688
0.302 JN 0.0886
ND vs 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND ~ 0.402
16.3 :r :y' 0.0680
ND v-....1 0.467
ND i/\.\l° 0.118
,.J.§IQ ~R 0.0331
3.44 :r 0.0952
60.7 :s>I 0.0905
ND ~\ 0.208
ND i 0.0543
ND \'ii 0.0766
2.01 3")l 0.0749
0.500 JW 0.0436
-WB-rz .QJIB8
4.42 :r~ 0.0574
LIMS Workordcr: 756200.UA-Littlc Washington, N [20005057] Hamilton Beach-Proctor Silex
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.666
0.000
0.000
0.000
0.000
0.000
0.000
0.000
O.OOU
0.000
0500HBWD999 0500HBWW213
2000505706 200050570 I :z
Cone Flaa DL RL Cone Flaa DL RL
~ I ~ ~~ ~,llflfl ND 0.0616 0.000 Jo
ND/ 2.37 O.MO 0.400 J 0.0474 0.000
NI 2.26 <Y.tioo 0.182 J 0.0452 0.000
N 5.70 /0.000 ND I 1 "'1 0.114 0.000
1' ) 2.34 / 0.000 ND 0.0469 0.000
llD 4.22/ 0.000 ND Ll'.S 0.0845 0.000
!. lD-HIP 3~ u.uuu ND it 0.0796 0.000
ND l.A.°"3" 5.30 0.000 16.7 :3 .. 0.106 0.000
~ iz... ~. {\ n..n.n. ND 0.688 0.000 -. -·-
ND 4.43 0.000 ND 0.0886 0.000
ND 3.61 o.A>oo ND 0.0722 0.000
NC 4.74 J).ooo ND 0.0948 0.000
N 3.96 /o.ooo ND 0.0792 0.000
N > 2.84 / 0.000 34.4 0.0568 0.000
ND 20.I I 0.000 ND I.A.'! 0.402 0.000
I .2 i 3.4<1 0.000 0.335 J 0.0680 0.000
1' D 2¥'4 0.000 ND Ll-:f 0.467 0.000
1'I U}. . , -.Ion .0..000 ND 0.118 0.000
2570 1.66 0.000 0.928 0.0331 0.000
~. . i1.. 4 --.v v:uw 3.17 0.0952 0.000
59.l 4.52 0.9'00 A A ~R {l.Q9()~ Q.000
ND 10.4 ct.ooo 1.26 :::r 0.208 0.000
NDJ 2.72 ;0.000 ND 0.0543 0.000
Nd 3.83 / 0.000 ND 0.0766 0.000
Nrh 3.74 / 0.000 0.509 J 0.0749 0.000
NO 2.1$" 0.000 0.248 J 0.0436 0.000
~ . ' 2:: ': --{\ ,.,,,.. Ne--~ Q.IH~8 0.09Q -·
ND 2.87 0.000 16.0 0.0574 0.000
STL Auslin Page 6 of 60
Sump/e resultl '"""'been ,11utlified by Radit111 /l//enurtio1111/ bm·ctl u111h.-, n/1"1"11/ oj 1/11• t/11111 rc•1•it•11• profl'lS. wlric Ir;, 11wddnl 1!fln tire ( Ulll/"/lct l 11bo/"/l/Of"I l'mgn1111 N111iou11/ J-"1111111111111/ Ci11id1'1111n
-lilli·gani<mii°':g"'iilll'R"'iliilS.El'llllifbe1·1iil"'''".S'Nl.r•·rc111·e(11.. - - - - - - - - -
--SECTION IV
Analytical Results
MS-VOA
SW82608
Continued
Parameter
n-Xvlene/m-Xvlene
o-Xvlene
-· -· -
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
---
0500HBWD999
2000505706
Cone Flaa DL
1.97 :J fl 0.137
1.83 :r II 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
---- --- -
0500HBWD999 0500HBWW2 I 3
2000505706 2000505701
RL Cone Flaa DL RL Cone Flaa DL
0.000 ND 6.85 0.000 0.935 J 0.137
0.000 ND 3.56 0.000 1.59 0.0713
Pago.: 7
Sample n•s1t//~ /1tll'<' bee11 </1tt1lified by Radiw1 /uu•m111imw/ based 011 the r ri1cria of f/w t/111<1 ffl'i<'ll' /l/'O('(•n·. wlii«h i~ 1111nl1·/1 «i <(/l«r rhe ( 'u11tmc1I11/wnuo1T l'rogr11111 N111iona/ l-'1111< llon11/ Ci11ult·/1111·1
for Org11nk mu/ /1101~i:1mic /l111t1 Re1•ic1r (U.S. EPA, Ocwber /9!)911111/ l-l'iw1111rr llJ'N. re.1pcc111•el.1 ).
' '·
--
RL
0.000
0.000
or 60
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
l-Bromo-4-fluorobenzene
I .2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -05/25/2000 01 :00
0500HBWD999
2000505706
Aaueous
Received
NA
05/03/2000 09:45
05/08/2000 23 :23
05/08/2000 23:23
1.0000
MSDA
ue:/L
% Recoverv Limits
107 77-117
55 61-143
103 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20005057) Hamilton Beach-Proctor Silex
F
0
0500HBWD999 0500HBWW213
2000505706 2000505701
Aqueous Aqueous
Received Received
NA NA
05/03/2000 09:45 05/03/2000 08:20
05/09/2000 23:53 05/08/2000 2 t :03
05/09/2000 23:53 05/08/2000 21 :03
50.0000 1.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recoverv Limits F
107 77-117 103 77-117
90 61-143 92 61-143
103 87-113 IOI 87-113
STL Austin Page 8 of 60
•'
Sample resultl· luwe been qualified by Riu/imi /nwm111icm11/ bill<'cl u11 th<', nt.-rw of the c/11111 rc·.1•it•11• proCL'lS, which il m<1ddnl <(/1<·1 the ( 'u11tr11c1 l.i1/wrnto1y l'roi,:n1111 N11tio1111/ F1111< t1<11111/ (iwdl'l1111·'
-.w·ganic.org11n{"l>11111Re1•i<·11·fll.S:El'-'berl-ll1·/i-Y!i./.~«·.1pec111·e(r1-·---------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Aceton itri le
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Brom om ethane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
0500HBWW213
2000505701
Aaueous
Received
NA
0510312000 08:20
05/09/2000 22:54
05/09/2000 22:5~
10.0000
MSDA
U!!/L
Cone Flag DL RL
•-* ~ R. ..... ~ ~ ~ -· v.u"•••
N) 16.7 o.o('o
N> 9.83 OjV O
N> 0.901 OJ loo
N~ 0.492 oA JOO
NI> 0.622 tJ.ooo
NI 1.39 b.ooo
NC 0.683 /0.000
NI 1.36 I o.ooo
NC 1.06 I 0.000
2-Butanone (MEK) 78-93-3 NI 1.19 I 0.000
n-Butvlbenzene 104-51-8 N > 0.642/
sec-Butvlbenzene 135-98-8 ND 0.745/
tert-Butvlbenzene 98-06-6 ND 0.95
Carbon disulfide 75-15-0 ND 0.4~ i
Carbon tetrachloride· 56-23-5 ND 0.8 7
2-Chloro-1 3-butadiene 126-99-8 1'D O.! 19
Ch lorobenzene 108-90-7 l'D O.• 73
Chloroethane 75-00-3 l'D O.J' 56.
Chloroform 67-66-3 l'D o/.670
1-Chlorohexane 544-10-5 l\lll., ;/ I '~ 1. 1.J
SECTION IV -Analytical Results -0512512000 0 I :00
LIMS Workordcr: 756200.UA-Littlc Washington, N (20005057] llamilton Beach-Proctor Silex
STLAustin
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
a:ouo
0500HBWW214 0500HBWW214
2000505702 2000505702
Aaueous Aaueous
Received Received
NA NA
05/03/2000 08:45 05/03/2000 08:45
05/08/2000 21 :31 05/09/2000 22:24
05/08/2000 21 :31@ 05/09/2000 22:24(~
1.0000 2.0000
MSDA MSDA
Ul!/L ug/L
Cone Flag DL RL Cone Flaa DL RL
ND 0.286 ' 0.000 Nt7 e. ~ -..,,.,-.,,, ... U.UI .XJ
ND lA3 1.67 0.000 N) 3.34 0.01 lo
ND u:r 0.983 0.000 N) 1.97 o.ol ~o
ND IA\ 0.0901 0.000 N) 0.180 OJ 100
0.304 J 0.0492 0.000 0. 136 ' 0.0984 oboo
ND 0.0622 0.000 N) 0.124 i:tooo
ND 0.139 0.000 N > ~ 0.278 D.ooo
ND 0.0683 o:ooo NU 0.137 /0.000
ND 0.136 0.000 N ~ 0.272 I o.ooo
ND 0.106 0.000 N > 0.212 I 0.000
ND vw 0.179 0.000 N) 0.358 / 0.000
ND 0.0642 0.000 ND 0.128/ 0.000
ND 0.0745 0.000 ND 0.14</ ·0.000
ND 0.0958 0.000 Ni) 0.19/2 0.000
ND 0.0484 0.000 N) 0.0</68 0.000
ND 0.0867 0.000 l\b 0.1!73 0.000
ND 0.0839 0.000 ]\ ) O.i68 0.000
ND 0.0473 0.000 ND 0/0946 0.000
0.705 0.0756 0.000 0. B3 I ,d 0'.151 0.000
ND 0.0670 0.000 ]\ ) I U34 0.000
ND 0.113 0.000 1\~ ~ I ) ?"' (\ """
Page 9 of
Sm11ple results hm•e bee11111wlifled by Rmli1111 //l/en1111io1111/ ba;cd 011 the <'l"lt<'l'ia of till' daw n•.1•it•11· prO£'('H, which i; 111odt'l1·d '!/ft·l' tl1e ( 'u11tmct l.1il><1mto1:i· l'roJ,!l'lllll Natimwl i"lu11 t1111111l <iuul<'IJJll''
for Organic 11111/ /11org1111ic 1111111 Rel'i1•11· (11.S. El'A. Ocwber /999111u/ /'1·/i,.11111:r IY'J.J. n•1pfflll'<'~l J.
' '·
60
--- ----- -SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surrogate Comoound
1-Bromo-4-tluorobenzene
I ,2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Dateffime Collected
Dateffime Prepared
Dateffime Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWW213
2000505701
Aaueous
Received
NA
05/03/2000 08:20
0510912000 22:54
05/09/2000 22:54
10.0000
MSDA
ug/L
% Recoverv Limits
105 77-117
91 61-143
103 87-113
LIMS Workordcr: 756200.UA-Littlc Washington, .N (20005057] Hamilton Beach-Proctor Silex
STLAustin
-
F
- -- - ---
0500HBWW214 0500HBWW214
2000505702 2000505702
Aaueous Aaueous
Received Received
NA NA
05/03/2000 08:45 05/03/2000 08:45
05/08/2000 21:31 05/09/2000 22:24
05/08/2000 21 :3 1 05/09/2000 22:24
1.0000 2.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recovery Limits
105 77-117 106 77-117
90 61-143 92 61-143
102 87-113 103 87-113
Page 13
Sampll' n·su/tl· iim•e b<"l'll IJlllliijied by lladiall bttcmational bmnl 011 1/i,·, n11·1w of the daw n•1•il'll' proc1·ss. ll'liiclr fa 1111u/..f,·d 1!/11·1 Iii<" ( '0111rnct / 11/wrn111rr l'rogram Natio1111/ F1111< 11111111/ <i111dd1111'I
for Organic m11/ /11org1111ic /J11111 Re1•i""' (I l.S. El'A. Oc10bl'r 19991111.t I 1•/1111111:r /91J./. l'<'l/'<'C'ti1·£"~1 J.
- -
F
of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrv Ion itrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-I 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
t 08-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/25/2000 0!:00
0500HBWW2 I 5
2000505703
AQueous
Received
NA
05/03/2000 08:55
05/08/2000 2 I :59
05/08/2000 2 I :59('2;)
1.0000
MSDA
ug/L
Cone Flaa DL
ND 0.286
ND \.\~ 1.67
ND \A:J 0.983
ND \ \,".)° 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND IA'.) 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workordcr: 756200.UA-Littlc Washington, N [20005057) Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW215 0500HBWW227
2000505703 2000505704
Aaueous Aaueous
Received Received
NA NA
05/03/2000 08:55 05/03/2000 09:30
05/09/2000 2 I :56 05/08/2000 22:27
05/09/2000 2 I :56(~ 05/08/2000 22:27 {7-)
1.0000 l.0000
MSDA MSDA
ug/L ug/L
Cone Flaa DL RL Cone Flaa DL
ND 0.286 0.000 19. I '3 0.286
ND 1.67 0.000 ND v3 1.67
ND \,\, ... ""\ 0.983 0.000 ND I 0.983
ND 0.0901 0.000 ND ~. 0.0901
ND 0.0492 0.000 0.622 s 0.0492
ND 0.0622 0.000 ND v..:r 0.0622
ND 0.139 0.000 ND 0.139
ND 0.0683 0.000 ND 0.0683
ND 0.136 0.000 ND 0.136
NI)-12._ D.IQ6 0.000 ND 1 !t 0.106
ND 0.179 0.000 40.2 \ 0.179
ND 0.0642 0.000 ND lJ\.::f 0.0642
ND 0.0745 0.000 ND 0.0745
ND 0.0958 0.000 ND 0.0958
ND 0.0484 0.000 ND 0.0484
ND 0.0867 0.000 ND 0.0867
ND 0.0839 0.000 ND 0.0839
ND 0.0473 0.000 ND ·I 0.0473 ,,
ND 0.0756 0.000 14.6 c;-0.0756
ND 0.0670 0.000 1.17 J 0.0670
ND 0.113 0.000 ND \,\::.\ 0.113
Page 14
Sample res11/b hm•e bee11 q11a/ified by R111/iw1 illtem11tic11111/ bmed 011 till' inti -rw oj tlw t/11111 re1•h•11• 11r11ce1s, 11'/iicli "' motld.-d <!fin tile ( ""''"'"' I 11/wuuorl' l'm.~ri1111 Nt1tio11t1/ /-um 11111111/ < i111tll'i1111·1
RL
0.000
0.000
0.000
0.000
0.000
. 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 ..
0.000
0.000
0.000
of 60
-llliilliirg1millllijwrg11tlliil"R"'ilj·S.Elllif'"('l"iii"t11'111it!i9-l.rc·\fL·c1i1·eJ.11illl - - - - - - - - -
----~--------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloropropene
2-Ch lorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I .4-Dichloro-2-butene I 10-57-6
1.4-Dich lorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichloropropane 78-87-5
1 3-Dichloropropane 142-28-9
2.2-Dichloroorooane 594-20-7
I 1-Dichloropropene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-I 3-Dichloropropene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/25/2000 01:00
0500HBWW2 l 5
2000505703 1)1
Cone Flaa DL
ND i.l :\' 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND \A.'X 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND \A'S° 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
3.43 y 0.0487
ND 0.0499
1.87 'i 0.0697
0.0409 <l 11 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND \A'J 0.167
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW215 0500HBWW227
2000505703 2000505704 z_")
Cone Flaa DL RL Cone Flaa DL
~ R Q.()!!;! I 6.000 ND w 0.0821
ND 0.111 0.000 ND 0.111
ND 0.113 0.000 ND 0.113
ND 0.0762 0.000 ND 0.0762
ND 1.05 0.000 ND 1.05
ND 0.0564 0.000 ND 0.0564
ND 0.152 0.000 ND --0.152
ND 0.0939 0.000 ND 0.0939
ND tA.\.f 0.390 0.000 ND 0.390
ND 0.0587 0.000 ND 0.0587
ND 0.0920 0.000 ND 0.0920
ND 0.0591 0.000 ND 0.0591
ND 0.113 0.000 ND iv 0.113
3.16 0.0487 0.000 ',.n I""' ~-Q..9487 v ~R
ND 0.0499 0.000 20.2 :r· 0.0499
1.93 0.0697 0.000 4~9 !R 11.66~7
ND 0.0603 0.000 """' -~R 6.6663
ND 0.0813 0.000 7.93 '3' 0.0813
ND 0.0670 0.000 ND \>.-:I 0.0670
ND 0.0451 0.000 ND I 0.0451
ND 0.0714 0.000 ND J, 0.0714
ND 0.0464 0.000 0.182 j 0.0464
ND 0.0366 0.000 ND IA "T 0.0366
ND 0.0658 0.000 ND \ 0.0658
ND 0.0647 0.000 ND ir 0.0647
ND 0.0552 0.000 0.454 j 0.0552
ND 0.212 0.000 ND \.<.\ 0.212
ND 0.167 0.000 ND IA "J 0.167
Page 15
Swuple i'<'SlllH full't' bee11 qua/ified by Rtulit1u /llterllt1timwl bt1sed "" thi· n 11,·rw <'./the d11w re1'it'll' proceH, which fa 11wdd, ·d <~ft er the ( i.J11tmct l.11bo1111ori· I 'rog1<1111 N111io1111/ hou tw1111f <i11iildi111 .,
for 01~~ank and /lwrg1111ic /111111 Re1•it·1r (11.S. F.l'.1. October JW9 11111/ I 1•/w1111rr /YY./. n•1pt·ctil'e~1 J.
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.886'
0.000
6.600
e.0ee
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
or 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsoproovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-pentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanen itri le 107-12-0
n-Proovlbenzene 103-65-l
Stvrene 100-42-5
1.1 l 2-Tetrachloroethane 630-20-6
l, l 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2 3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
l LI-Trichloroethane 71-55-6
l, l 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1,2 3-Trichloroorooane 96-18-4
1.1 2-Trichlorotrifluoroethane 76-13-l
I 2 4-Trimethvlbenzene 95-63-6
l 3.5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
. Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/25/2000 01:00
0500HBWW215
2000505703
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND U3 0.114
l.10 0.0469
ND \A :J 0.0845
ND B 0.0796
ND \A'\ 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
12.8 :s-0.402
ND 0.0680
ND \A.:\ 0.467
ND 0.118
ND 0.033 l
ND 0.0952
0.113 w 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
Nf}-~ 0.9438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N [20005057) Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
O.OQO
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.QQ9-
0.000
0500HBWW215 0500HBWW227
2000505703 2000505704
Cone Flaa DL RL Cone Flaa DL
ND 0.0616 0.000 ND I A •::f 0.0616
ND 0.0414 0.000 ND 0.0474
ND 0.0452 0.000 ND 0.0452
ND 0.114 0.000 ND ii/ 0.114
1.09 0.0469 0.000 0.322 J 0.0469
ND 0.0845 0.000 ND \..LJ 0.0845
ND H 0.0796 0.000 0.982 u.JB 0.09~6
ND ( 0.106 0.000
..
ND 0.106
ND 0.688 0.000 ND 0.688
ND 0.0886 0.000 ND 0.0886
ND 0.0722 0.000 ND 0.0722
ND 0.0948 0.000 ND I 0.0948
ND 0.0792 0.000 1.48 ::-r 0.0792
ND 0.0568 0.000 ND u.-:r 0.0568
15.0 0.402 0.000 ND IA:! 0.402
ND 0.0680 0.000 13.8 ~ 0.0680
ND 0.467 0.000 ND IA.\ 0.467
ND 0.118 0.000 ND w 0.118
ND 0.033 l 0.000 ..L'Ll {\ ~R 1l.e:3j t >J -
ND 0.0952 0.000 2.95 ~I" 0.0952.
0.124 J 0.0905 0.000 48.9 :T 0.0905
ND 0.208 0.000 ND l.A.S 0.208
ND 0.0543 0.000 ND l 0.0543
ND 0.0766 0.000 ND '!}' 0.0766
ND 0.0749 0.000 0.720 J 0.0749
ND 0.0436 0.000 0.646 J 0.0436
Ne--µ._ 0.0•B8 6.600 ~ !i2--.Q.9438
ND 0.0574 0.000 5.51 _1_ 0.0574
Page 16
Samp/£' r£'~·11/1s hm•e bce11 qmilifietl by Rmliw1 l111<•rnt11im111/ bmcil u11 thc c rucrw of tltc i/111t1re1•it•w1n·on'lS, whi1 Ii il 111111/1·/,·d <!fl•'' 1/1<' ( 'u11tr<1ct l <1/>cm11m r l'rog1e1111 N<11io1111/ hem 1w11a/ (,"wc/du11•,
RL
0.000
0.000
0.000
0.000
0.000
0.000
O.OUO . 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.00Q.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.600
0.000
of 60
---ganic-01:g111 .. 1 Re1•i111ii\' El'illll'ber '1111'' ""111!1!1./, 'm'''e(1J._ - - - - - - - - -
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
Daterrime Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
l-Bromo-4-tluorobenzene
I ,2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWW215
2000505703
Aaueous
Received
NA
05/03/2000 08:55
05/08/2000 21 :59
05/08/2000 21 :59
1.0000
MSDA
ug/L
% Recoverv Limits
105 77-117
92 61-143
101 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
F
0500HBWW215 0500HBWW227
2000505703 2000505704
Aqueous Aaueous
Received Received
NA NA
05/03/2000 08:55 05/03/2000 09:30
05/09/2000 21 :56 0510812000 22:27
0510912000 21 :56 05/08/2000 22:27
1.0000 1.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recoverv Limits F
107 77-117 106 77-117
91 61-143 57 61-143 Q
104 87-113 101 87-113
STL. Austin Page 18 of 60
::;11111p/e re~u/ts /wi•e been 111111/ified by R111/i11111tui•m111im111/ b"'"'' 011tit<"11111·1111 oj tlw d11111 re1•i<•11• process, 11·/iicli 1~ 111od.-/, ti 1(/11·1 rlw ( untrtwt / 11/>0111101 r l'ro~111111 N111w1111/ /·1111< 1w111il C.1111/d111n
mlll!' mrga11illllii101x111ii1111Re1illl(l .. \'.£/llllr'"'',.ill'"'..t•t!Wl.mr11·e(1.. - - - - - - - - -
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromoch loromethane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
0500HBWW227
2000505704
Aqueous
Received
NA
05/03/2000 09:30
05/09/2000 23:24
05/09/2000 23:24 {'f>.
50.0000 \V
MSDA
ug/L
Cone Flaa DL RL
ND \,'-"S 14.3 0.000
W0-t-" nn -""'"'~ ..... v .. l\IJ
N D' 49.2 0.000
NC 4.50 o,()oo
NH 2.46 li.ooo
N) 3.11 /0.000
l\ D 6.95 I o.ooo
Bromodichloromethane 75-27-4 ? D 3.42 I 0.000
Bromoform 75-25-2 lD 6.8o/
Brom om ethane 74-83-9 WO -n/...
' I _,,JV
2-Butanone (MEK) 78-93-3 ND \.A.':5 8.95
n-Butvlbenzene 104-51-8 wa R ,, '" -·-· sec-Butvlbenzene 135-98-8 N t 3.72
tert-Butv I benzene 98-06-6 N) 4.79
Carbon disulfide 75-15-0 1' ) 2.42
Carbon tetrachloride 56-23-5 }'.D 4.34 /
2-Chloro-I 3-butadiene 126-99-8 l'D 4.W
Chlorobenzene 108-90-7 '~ '
_..,,,,,,.
Chloroethane 75-00-3 NG-K trl-~..;ig.
Chloroform 67-66-3 NP R n n-J,JJ
1-Chlorohexane 544-10-5 MD. R_ "~ -
SECTION IV -Analytical Results -05/25/2000 01 :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
0.000
n n v.vJU
0.000
n "'"''"' -· .,
0,.600
..-0.ooo
/ 0.000
0.000
0.000
n. .......... ,... -· 6.990..C
~o· ----v.vvu
0500HBWW228 0500HBWW228
2000505705 2000505705
Aaueous Aaueous
Received Received
NA NA
05/03/2000 09:35 05/03/2000 09:35
05/08/2000 22:55 05110/2000 00:21
05/08/2000 22:55/]:') 05/10/2000 00:21(:;))
1.0000 -2000.0000
MSDA MSDA
ue./L ue.IL
Cone Flaa DL RL Cone Flaa DL RL
360 J~ 0.286 0.000 m:l '/.. C"l"I A "'"',,... -· ·~
ND l,,-W" 1.67 0.000 NC 3340 0.01/0
ND I 0.983 0.000 NC 1970 o.doo
ND ~ 0.0901 0.000 NC 180 0~00
56.5 ::r 0.0492 0.000 NC 98.4 <l.ooo
ND rJ-;J 0.0622 0.000 N[ 124 ~.000
ND 0.139 0.000 N[ 278 /0.000
ND 0.0683 o:ooo NI 137 I o.ooo
ND 0.136 0.000 Nl 272 I o.ooo
ND .v 0.106 0.000 NI 212 I o.ooo
382 0 ~ 0.179 0.000 NI I 358 I 0.000
9.88 .:r 0.0642 0.000 NI> ' 128 I 0.000
7.96
"""
0.0745 0.000 N) 149 I .o.ooo
ND lJW 0.0958 0.000 ND 192 I 0.000
1.96 \;1.-:S r-:iP ~ 0.000 N) 96.8/ 0.000
26.2 ·r 0.0867 0.000 ND 173/ 0.000
ND v..::s 0.0839 0.000 }.D 168/ 0.000
ND iA'J 0.0473 0.000 l'D 94,4) 0.000
89.8 :.\ 0.0756 0.000 }D 111 0.000
9.62 d 0.0670 0.000 ? D IB4 0.000
ND \A.~ 0.113 0.000 H9 " ~~-v:UUU
Page 19 of
Smuple results hm•e bel'l11Jll1tlified by Rmliim lmemlllicm11/ b1t~l'd ul/ 1'1", rl/t'l'ia oj th<' da/ll n•1•i<'ll' pmcen', which i> 1111)(/t'/,'tl <!fil'1 1/ic ( 'u111mc1 /.alwrn1m:i· l'rogrn111 N111io1111/ /"um 11mwl (i11icll'iill"1
fur Organic anti /11org11nic /)11111 Re1•it·11· (U.S. £1'.4. Ocwbl'r 199911111/ I l'lw11w·r 199./. '""~p,.c1i1•e(1 J.
60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1,2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichloroditluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 ·2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1,3-Dichloroorooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/25/2000 01 :00
0500HBWW227
2000505704
Cone Flaa DL RL
+If• !?-. n l'oo -----...... &..., v.vvy
NC 5.55 o.olfo
N[ 5.65 o . .tfoo
NI• 3.81 11.000
ND 52.5 A>.ooo
N > 2.82 I o.ooo
ND 7.60 I o.ooo
ND 4.10 I 0.000
N) 19.5 I 0.000
N > 2.94/ 0.000
N) 4.6.n 0.000
ND 2/J6 0.000
NJ.. I?' ,J ., .. v ..........
3360 2.44 0.000
~ .Y12 2.~9 6.666
644 3.48 0.000
381 3.02 0.000
~~ I e... ---n "\'". Jl Ve'J'-IVI
NC
,
3.35 0.000
Nr 2.26 0.000
NC 3.57 o.-Ooo
NC 2.32 n.ooo
Nf 1.83 /0.000
NI> 3.29 I o.ooo
Nh 3.24/ 0.000
l'){D 2.1t 0.000
~D la':6 0.000
I~ 3.:::iJ --~ r , v.uuu
LIMS Workorder: 756200.UA-Little Washington, N [20005057) Hamilton Beach-Proctor Silex
0500HBWW228 0500HBWW228
200050570 2000505705 3'
Cone Flag DL RL Cone Flaa DL RL
1.33 ~T 0.0821 0.000 Nf)'t" ~ 1.r• n --v.
ND i;,::r 0.111 o:ooo ND 222 o.ol>o
ND 0.113 0.000 Nr 226 0.~00
ND 0.0762 0.000 NC 152 0/000
ND 1.05 0.000 N1 2100 ~.000
ND 0.0564 0.000 N,> 113 ftl.000
ND 0.152 0.000 N) 304 I o.ooo
ND 0.0939 0.000 N) 188 I o.ooo
ND 0.390 0.000 1' ) 780 I 0.000
ND 0.0587 0.000 1'D 117 I 0.000
ND 0.0920 0.000 l D 184{ 0.000
ND 0.0591 0.000 ]JD Iii 0.000
ND .,v 0.113 0.000 HT-~ r; _J, ---1 v 0 ...,.J\J
-1716 ~R Q.Q48+ 0.660 14500 97.4 0.000
ND IA...} 0.0499 0.000 -+fB-~ 99.8 9.009
i:LS~O ER Q.969:jl 0.600-53400 139 0.000
"'4926 -f:R ..Q.9693 9.980 .2360 121 0.000
17.0 ~ 0.0813 0.000 ~ R I~ U.UU!I
ND IA.:; \ 0.0670 0.000 ND' 134 0.000
ND \.A-:1 0.0451 0.000 NC 90.2 .o..doo
ND \;.._":\ 0.0714 0.000 N[ 143 tf.000
1.51 :\ 0.0464 0.000 NI 92.8 /0.000
ND L<\ 0.0366 0.000 N > 73.2 / 0.000
ND \Al 0.0658 0.000 N) 137/ 0.000
ND \)~ 0.0647 0.000 ·l'of Er .., / I~ u.uuu
40~ iR G.9§:§~ 9.9Q9-555 J 110 0.000
ND \A_\ 0.212 0.000 'Ntr R. ·~ "T.<. ... IJ,..00\J
38.8 ... T 0.167 0.000 14tr r: 33A __.,,.,,---r. n.n......o..
V.JVV
STL Austin Page 20 of 60
Sample results /u11•e bee11 lflllllijied by Rmlicm lmematicmal b11l't•d 011 tlw, rt11Tict oj tltl' c/111t1 r<"l'il'll' proc·eu', wlticlt ;, 111c11/l'inl c!flc1 tltc l ·u1111e1c1 l al>cu utorr /'1C1gra111 N11ti111111/ /-1111< 1w11al (11111/d1m·'
---ganic .. 01-g11'iliil1 Re1·11i1~· El'tliibe1· /·I I 1'111 .. !l!I./. ('('\§('"111•c•(1J._ - - - - - - - - -
- ----SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Comoound
I -Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -05/25/2000 01 :09
---
0500HBWW227
2000505704
Aaueous
Received
NA
05/03/2000 09:30
05/09/2000 23:24
05/09/2000 23 :24
50.0000
MSDA
ug/L
% Recovery Limits
106 77-117
90 61-143
99 87-113
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STL Austin
- - -- --- --
0500HBWW228 0500HBWW228
2000505705 2000505705
Aaueous Aaueous
Received Received
NA NA
05/03/2000 09:35 05/03/2000 09:35
05/08/2000 22:55 05/10/2000 00:21
05/08/2000 22:55 05/10/2000 00:21
1.0000 2000.0000
MSDA MSDA
ug/L ug/L
F % Recovery Limits F % Recoverv Limits
92 77-117 106 77-117
22 61-143 0 90 61-143
113 87-113 101 87-113
Page 23
Smnple results lull'<' bt'l'll IJIW/ifii:d by Rmti1111 /111i:rut1tim111/ bmecl u11 1/1, ·, ,.,,, ·na oj tht' d111t1 l"l'_i·iew f""""'lS, ll'hich il 111odd, "' '!fla the ( u1111m·1 I 11bornto1:r l'ro!!,1'<1111 N11tio1111/ F1111< tw1111/ ( i11i1i< ·/11w'
for Organic m11/ /11org1111ic /J11111 Rl'l'iC'll' (l ! . .\'. EPA. October 1999 w1d f'<'l>ruw:r /!NI. n•.1p1·1111•1:(1 J.
--
F
"
of 60
--SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroprooene
2-Chlorotoluene
4-Chlorotoluene
---
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
1 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
J ,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I A-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
1,3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1,2-Dichloroethene 156-60-5
1.2-Dich loropropane 78-87-5
I 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
1 1-Dichloropropene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-I 3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hex·anone 591-78-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
-- -
I TRIP BLANK 2
2000505707 ~)
Cone Flaa
ND lA :_\
ND
ND
ND
ND \>..:\
ND
ND
ND
ND I A""\
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND i.A:S
DL
0.0821
0.111
0.113
0.0762
1.05
0.0564
0.152
0.0939
0.390
0.0587
0.0920
0.0591
0.113
0.0487
0.0499
0.0697
0.0603
0.0813
0.0670
0.0451
0.0714
0.0464
0.0366
0.0658
0.0647
0.0552
0.212
0.167
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STLAustin
----- - - - -
RL Cone Flag DL RL Cone Flaa DL
0.000
0.000
0.000
0.000
0.000 -
0.000 ----
0.000 ··-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 -·
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 25
Sample re~·u/ts /ull'e beeu q11a/ijied by Rmlitm Jmerut11iont1/ bmetl u11 tit<" a11,·ri11 of tlte t/11111 rei•h•w prot«'lS. 11•/iiclt 1; 1111Jl/l'/,·d 11/ter the ( "u111ruct /.11bornw1:i• l'ro.~rn111 N11tio1111/ /:11111 '"""'' (i11id..ti111'I
fur Organic mu/ Jiwrg1111ir l>t1111 Rei•il·w (11.S. El'il. Octolwr /l)<J91111d /-,•/>r11111)' /<J<J-1. rc.1p1Ttil-e(rJ. .
--
RL
or 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsopropylbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butyl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Propvlbenzene 103-65-1
Styrene 100-42-5
I. I. I 2-Tetrachloroethane 630-20-6
I. I 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene I 08-88-3
1.2 3-Trichlorobenzene 87-61-6
1.2.4-Trich lorobenzene 120-82-1
I l, 1-Trich loroethane 71-55-6
I l.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2,3-Trichloroprooane 96-18-4
1.1.2-Trichlorotrifluoroethane 76-13-1
l 2 4-Trimethvlbenzene 95-63-6
1.3 5-Trimethvlbenzene 108-67-8
Vinyl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/25/2000 0 I :00
I TRIP BLANK 2
2000505707 @)
Cone Flaa
ND
ND
ND
ND u:s
ND
ND IA\
ND Jf
ND (A'\"
ND
ND
ND
ND
ND
ND
ND l;\.:J
ND
ND \;\..""S
ND
ND
ND
ND
ND
ND
ND
ND
ND
~ ~
ND
DL
0.0616
0.0474
0.0452
0.114
0.0469
0.0845
0.0796
0.106
0.688
0.0886
0.0722
0.0948
0.0792
0.0568
0.402
0.0680
0.467
0.118
0.0331
0.0952
0.0905
0.208
0.0543
0.0766
0.0749
0.0436
G.0438
0.0574
LIMS Workorder: 756200.UA-Little Washington, N (20005057) Hamilton Beach-Proctor Silex
RL Cone Flaa DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.QOO
0.000
STL Austin Page 26 of 60
Sample results hm•e be<'ll l/llliiijied by Rmlimi lutenwtimwl b11S1•cl uu th<" cntcri11 oj the 1/11/tl re1'i<'w /J11JC<'S.I", which i~ modd1·d '!/1.-1 the ( iJ11tmc1 l.11b1J11llotT l'rogram N11ti1J1111/ 1-"11111 tw1111/ C,11idt"/111n
.. mrgtmi .. 10rg11-11Re111ii·~·.£1Mi11b1·r•l"'1-e1-t!/ll.l.ffT'c1il·e(1J-- - - - - - - - -
- -SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
---
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
- --
TRIP BLANK2
2000505707
Cone Flaa DL
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
- --- - - - --
RL Cone Flaa DL RL Cone FlaQ DL
0.000
0.000
Page 27
!:Jiuuple rl'su//s luwe b<'l'll t/1tt1lifled by Radian /memaiional based uu 111<' ffi/i"l"ia of /ht' da/11 re1•h•11• proce,s, which i' 11111dl'inl 1!flc1 tlte ( 'u111ruc1 l.alwm1ot:i• l'm.~m111 Na1io11al l-"1111< t1eJ11al Ci11itll'l111c•,
for Organic mu/ illorg1111ic l >11/(/ Re1•ie1r (l l.S. El'A. ( Jc-111/ler 1999 mu/ /·d•rnm:r / IJIJ-1. respeC111•e(1 J.
--
RL
"
of 60
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW82608
Client Sample ID
'Lab Sample ID
Matrix .
Reported As
% Moisture
Dateffime Collected
Dateffime Prepared
Dateffime Analyzed
Dilution Factor
Instrument
Units
Surroaate Compound
l-Bromo-4-fluorobenzene
1.2-Dich loroethane-d4
Toluene-d8
SECTION IV -Analytical Results -05/25/2000 01 :00
TRIPBLANK2
2000505707
Aaueous
Received
NA
05/03/2000 00:00
05/08/2000 20:35
05/08/2000 20:35
1.0000
MSDA
ug/L
% Recovery Limits
105 77-1I7
90 61-143
JOI 87-113
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
F % Recovery Limits F % Recoverv Limits
STL Austin Page 28 of
Sample /"l'l"llill flill'I' beell Cflllllijieil by Rmiiw1 /111enw1imwl based u11 th<' tT//crt11 oj the d111t1 ffl'it'll' proc-t·~s. which fa 11wd<'h ii •!/lei th<' ( 0u11tr11c1 l.11/wmtmy l'r11!J111111 N111101111/ f-"11"' tw1111l (i111d..!111n
...... rgani.101;gai11111Re1·i<·11·v1.s.E11illi°"",.lili"'''''iii1'YY./.liJiiiii';,."(1-- - - - - - - -
F.
60 -
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
RAW DATA
SECTION I
Table of Contents
Section
I.
MS-VOA
II.
III.
IV.
v.
VI.
VII.
Form
Cover Page -Laboratory Analytical Report
Table of Contents .
Report Surrma.ries . . . . .
Workorder Surrmary
Protocol Surrmary
Corrments and Flag Definitions .
Standard Flag Definitions .
Analyst Corrments . . . . .
Sample Condition Corrments
Analytical Results . . . . . . . . .
SW8260B . . . . . • . . .
Calibration and Quality Control Results
SW8260B • . . . . . . . . . .
Batch Surrmaries .
SW8260B •.
Certifications . . .
Calibration Verification Results
Mass Spectrometer Tune . . . .
Method Blank Results
Control Sample Results
Extraction/Digestion Batch Surrmary
Extraction/Digestion Batch Surrmary
Analysis Batch Surrmary
Analysis Batch Surrmary
Section I -Table of Contents -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
Page
i
1
1
. 1
1
• 3
• 3
• 3
. 3
4
• 4
29
. . ·29
29
41
• • • • • 44
. 48
. 56
. . . . . . . 56
56
56
58
• 58
60
--··-------------------
--· - -.. , ---.. - - - _ ... -... _ - -
SECTION II
. Report Summaries
MS-VOA
Client Name: Hamilton Beach-Proctor Silex Project Name: 7S6200.UA-Little Washington, N (2000SOS7] Hamilton Beach-Proctor Silex
Client Code: HB-PS Facility Name: NC
Workorder Summary
Lab
Client Samele ID Samele ID Sample Matrix
OSOOHBWW213 200050S701 Aaueous
OSOOHBWW214 2000SOS702 Aqueous
OSOOHBWW2 JS 2000SOS103 Aaueous
OSOOHBWW227 2000SOS104 Aqueous
OSOOHBWW228 2000SOS10S Aaueous
OSOOHBWD999 2000SOS106 Aqueous
TRIP BLANK2 2000SOS707 Aqueous
Protocol Summary
L,.ab Date & Time
Client Samele ID Sample ID Collected
Method: SW8260B
OSOOHBWW213 2000SOS701 OS/03100 08:20
OSOOHBWW213 2000SOS701 OS/03/00 08:20
OSOOHBWW214 2000SOS702 OS/03100 08:4S
OSOOHBWW214 2000SOS702 OS/03100 08:4S
OSOOHBWW21S 2000SOS103 OS/03100 08:SS
0500HBWW2IS 2000SOS103 OS/03100 08:SS
SECTION II -Report Summaries -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex ·
STLAustin
Method Citation
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
Date& Time Prep
Received Batch ID
OS/04100 08:30 4862
OS/04/00 08:30 4881
OS/04100 08:30 4862
OS/04100 08:30 4881
OS/04100 08:30 4862
OS/04100 08:30 4881
Method Description
Volatiles by GC/MS
Volatiles bv GC/MS
Volatiles bv GC/MS
Volatiles by GC/MS
Volatiles bv GC/MS
Volatiles by GC/MS
Volatiles bv GC/MS
Hold Time S :>ec
Date & Time Analysis Date& Time Preo Analvsis
Pre eared Batch ID Analvzed Spec Actual Spec Actua
OS/08/00 21 :03 4862 OS/08/00 21 :03 70 so 7D so
OS/09/00 22:S4 4881 OS/09100 22:S4 70 60 70 6D
OS/08/00 21 :31 4862 OS/08/00 21 :31 70 SD 70 SD
OS/09100 22:24 4881 OS/09100 22:24 70 6D 70 60
OS/08/00 21 :S9 4862. OS/08/00 21 :S9 70 so 70 so
OS/09100 21 :S6 4881 OS/09100 21 :S6 70 60 70 60
Page I of 60
SECTION II
Report Summaries
MS-VOA
Protocol Summary continued -
Hold Time Spee
Lab Date&Time Date&Time Prep Date & Time Analysis Date&Time Prep Analvsis
Client Samole ID SamolelD Collected Received Batch ID Preoared Batch ID Analvzed Soec Actua Soec Actua
Method· SW8260B continued -
0500HBWW227 2000505704 05/03/00 09:30 05/04/00 08:30 4862 05/08/00 22:27 4862 05/08/00 22:27 70 50 70 50
0500HBWW227 2000505704 05/03/00 09:30 05104100 08:30 4881 05109100 23:24 4881 05109100 23 :24 70 60 70 60
0500HBWW228 2000505705 05/03/00 09:35 05/04/00 08:30 4862 05/08/00 22:55 4862 05108100 22:55 70 50 70 50
0500HBWW228 2000505705 05/03/00 09:35 05/04/00 08:30 4881 05/l 0/00 00:21 4881 05/l 0/00 00:21 70 70 70 70
0500HBW0999 2000505706 05/03/00 09:45 05/04/00 08:30 4862 05108100 23:23 4862 05/08/00 23:23 70 50 70 50
0500HBW0999 2000505706 05/03/00 09:45 05/04/00 08:30 4881 05109100 23:53 4881 05109100 23:53 7D 6D 7D 6D
TRIP BLANK2 2000505707 05/03/00 00:00 05/04/00 08:30 4862 05/08/00 20:35 4862 05/08/00 20:35 7D SD 7D SD
SECTION II -Report Summaries -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin Page 2 of 60
·---~-~-~----~-~---
-----~------~------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1,2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
I 2-Dichloropropane 78-87-5
I 3~Dichloroorooane 142-28-9
2 2-Dichloropropane 594-20-7
I, 1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-1,3-Dichloropropene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68~3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWD999
2000505706
Cone Flaa DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
936 ER 0.0487
23.7 0.0499
426 ER 0.0697
349 ER 0.0603
9.11 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
0.181 J 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
0.810 v 0.0552
ND 0.212
ND 0.167
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWD999 0500HBWW213
2000505706 2000505701
Cone Flaa DL RL Cone Flaa DL RL
ND 4.10 0.000 ND 0.0821 0.000
ND 5.55 0.000 ND 0.111 0.000
ND 5.65 0.000 ND 0.113 0.000
ND 3.81 0.000 ND 0.0762 0.000
ND 52.5 0.000 ND .~-1.05 0.000
ND 2.82 0.000 ND -.0.0564 0.000 -.
ND 7.60 0.000 ND 0.152 0.000
ND 4.70 0.000 ND 0.0939 0.000 .
ND 19.5 0.000 ND 0.390 0.000
ND 2.94 0.000 ND 0.0587 0.000
ND 4.60 0.000 0.349 J 0.0920 0.000
ND 2.96 0.000 ND 0.0591 0.000
ND 5.65 0.000 ND 0.113 0.000
3560 2.44 0.000 168 ER ~0.0487 0.000 ..
24.7 J 2.50 0.000 4.49 0.0499 0.000
684 3.48 0.000 364 ER 0.0697 0.000
394 3.02 0.000 40.6 0.0603 0.000
9.68 J 4.06 0.000 1.41 0.0813 0.000
ND 3.35 0.000 ND 0.0670 0.000
ND 2.26 0.000. ND 0.0451 0.000
ND 3.57 0.000 ND 0.0714 0.000
ND 2.32 0.000 ND 0.0464 0.000
ND 1.83 0.000 ND 0.0366 0.000
ND 3.29 0.000 ND 0.0658 0.000
ND 3.24 0.000 ND 0.0647 0.000
ND 2.76 0.000 0.727 0.0552 0.000
ND 10.6 0.000 ND 0.212 0.000
ND 8.35 0.000 ND 0.167 0.000
Page 5 . of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsopropylbenzene 98-82-8
4-lsooronvltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methyl tert-butyl ether (MTBE) I634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naphthalene 9I-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-I
Stvrene 100-42-5
I l, I ,2-Tetrachloroethane 630-20-6
I I 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I ,2.3-Trichlorobenzene 87-61-6
I .2 4-Trichlorobenzene 120-82-1
I. I 1-Trichloroethane 7I-55-6
I. I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2 3-Trichloropropane 96-I8-4
I 1,2-Trichlorotrifluoroethane 76-I3-l
1 2.4-Trimethvlbenzene 95-63-6
1 3.5-Trimethvlbenzene 108-67-8
Vinyl acetate 108-05-4
Vinvl chloride 75-0I-4
SECTION IV -Analytical Results -05/25/2000 01 :00
0500HBWD999
2000505706
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
0.538 J 0.0469
ND 0.0845
l.00 JB 0.0796
25.0 v 0.106
ND 0.688
0.302 JV 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
16.3 v 0.0680
ND 0.467
ND 0.118
I510 ER 0.0331
3.44 0.0952
60.7 v 0.0905
ND 0.208
ND 0.0543
ND 0.0766
2.01 v 0.0749
0.500 JV 0.0436
ND 0.0438
4.42 v 0.0574
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STLAustin
0500HBWD999 0500HBWW213
2000505706 2000505701
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 3.08 0.000 ND 0.0616 0.000
0.000 ND 2.37 0.000 0.400 J 0.0474 0.000
0.000 ND 2.26 0.000 0.182 J 0.0452 0.000
0.000 ND 5.70 0.000 ND O. I 14 0.000
0.000 ND 2.34 0.000 ND 0.0469 0.000
0.000 ND 4.22 0.000 ND 0.0845 0.000
0.000 ND B 3.98 0.000 ND B 0.0796 0.000
0.000 ND 5.30 0.000 16.7 0.106 0.000
0.000 ND 34.4 0.000 ND 0.688 0.000
0.000 ND 4.43 0.000 ND 0.0886 0.000
0.000 ND 3.6I 0.000 ND 0.0722 0.000
0.000 ND 4.74 0.000 ND 0.0948. 0.000
0.000 ND 3.96 0.000 ND 0.0792 0.000
0.000 ND 2.84 0.000 34.4 0.0568 0.000
0.000 ND 20.1 0.000 ND 0.402 0.000
0.000 I5.2 J 3.40 0.000 0.335 J 0.0680 0.000
0.000 ND 23.4 0.000 ND 0.467 0.000
0.000 ND 5.90 0.000 ND O. I 18 0.000
0.000 2570 l.66 0.000 0.928 0.033I 0.000
0.000 ND 4.76 0.000 3.I7 0.0952 0.000
0.000 59.I 4.52 0.000 444 ER 0.0905 0.000
0.000 ND 10.4 0.000 l.26 0.208 0.000
0.000 ND 2.72 0.000 ND 0.0543 0.000
0.000 ND 3.83 0.000 ND 0.0766 0.000
0.000 ND 3.74 0.000 0.509 J 0.0749 0.000
0.000 ND 2.I8 0.000 0.248 J 0.0436 0.000
0.000 ND 2.I9 0.000 ND 0.0438 0.000
0.000 ND 2.87 0.000 16.0 0.0574 0.000
Page 6 of 60
-------------~-~---
-~----------~-~----
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
p-X ylene/m-X v lene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWD999
2000505706
Cone Flag DL
1.97 v 0.137
1.83 v 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0500HBWD999 0500HBWW213
2000505706 2000505701
Cone Flaa DL RL Cone Flag DL RL
ND 6.85 0.000 0.935 J 0.137 0.000
ND 3.56 0.000 1.59 0.0713 0.000
Page 7 of 60
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surroaate Comoound
1-Bromo-4-fluorobenzene
l ,2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWD999
2000505706
Aaueous
Received
NA
05/03/2000 09:45
05/08/2000 23:23
05/08/2000 23:23
1.0000
MSDA
ue:/L
% Recoverv Limits
107 77-117
55 61-143
103 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
F
0
0500HBWD999 0500HBWW213
2000505706 2000505701
Aaueous Aaueous
Received Received
NA NA
05/03/2000 09:45 05/03/2000 08:20
05/09/2000 23:53 05/08/2000 21 :03
05/09/2000 23:53 05/08/2000 21 :03
50.0000 1.0000
MSDA MSDA
ug/L ue:/L
% Recoverv Limits F % Recoveav Limits F
107 77-117 103 77-117 .
90 61-143 92 61-143
103 87-113 101 87-113
Page 8 of 60
--------------~----
------~------------SECTION IV
Analytical Results
MS-VOA
SW82608
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-I 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
l 07-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/25/2000 01:00
0500HBWW213
2000505701
Aaueous
Received
NA
05/03/2000 08:20
05/09/2000 22:54
05/09/2000 22:54
10.0000
MSDA
U!!/L
Cone Flaa DL
ND 2.86
ND 16.7
ND 9.83
ND 0.901
ND 0.492
ND 0.622
ND 1.39
ND 0.683
ND 1.36
ND 1.06
ND 1.79
ND 0.642
ND 0.745
ND 0.958
ND 0.484
ND 0.867
ND 0.839
ND 0.473
ND 0.756
ND 0.670
ND 1.13
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
0500HBWW214 0500HBWW214
2000505702 2000505702
Aaueous Aaueous
Received Received
NA NA
05/03/2000 08:45 05/03/2000 08:45
05/08/2000 21 :31 05/09/2000 22:24
05/08/2000 21 :31 0510912000 22:24
1.0000 2.0000
MSDA MSDA
Ull'/L ug/L
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.286 0.000 ND 0.572 0.000
0.000 ND 1.67 0.000 ND 3.34 0.000
0.000 ND 0.983 0.000 ND 1.97 0.000
0.000 ND 0.0901 0.000 ND 0.180 0.000.
0.000 0.304 J 0.0492 0.000 0.336 J 0.0984 0.000
0.000 ND 0.0622 0.000 ND 0.124 0.000
0.000 ND 0.139 0.000 ND -0.278 0.000
0.000 ND 0.0683 0.000 ND 0.137 0.000
0.000 ND 0.136 0.000 ND 0.272 0.000
0.000 ND 0.106 0.000 ND 0.212 0.000
0.000 ND 0.179 0.000 ND 0.358 0.000
0.000 ND 0.0642 0.000 ND 0.128 0.000
0.000 ND 0.0745 0.000 ND 0.149 0.000
0.000 ND 0.0958 0.000 ND 0.192 0.000
0.000 ND 0.0484 0.000 ND 0.0968 0.000
0.000 ND 0.0867 0.000 ND 0.173 0.000
0.000 ND 0.0839 0.000 ND 0.168 0.000
0.000 ND 0.0473 0.000 ND 0.0946 0.000
0.000 0.705 0.0756 0.000 0.831 J 0.151 0.000
0.000 ND 0.0670 0.000 ND 0.134 0.000
0.000 ND 0.113 0.000 ND o.226 0.000
Page 9 of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Chloromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1,2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1,2-Dichlorobenzene 95-50-1
l 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I. 1-Dichloroethane 75-34-3
I .2-Dichloroethane 107-06-2
l, 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichloropropane 78-87-5
1 3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
l, 1-Dichloropropene 563-58-6
cis-1 3-Dichloroorooene I 0061-01-5
trans-1,3-Dichloronronene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone . 591-78-6
SECTION IV -Analytical Results -0512512000 01:00
0500HBWW213
2000505701
Cone Flaa DL
ND 0.821
ND 1.11
ND 1.13
ND 0.762
ND 10.5
ND 0.564
ND 1.52
ND 0.939
ND 3.90
ND 0.587
ND 0.920
ND 0.591
ND 1.13
178 0.487
4.32 J 0.499
401 0.697
41.4 0.603
ND 0.813
ND 0.670
ND 0.451
ND 0.714
ND. 0.464
ND 0.366
ND 0.658
ND 0.647
ND 0.552
ND 2.12
ND 1.67
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW214 0500HBWW214
2000505702 2000505702
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0821 0.000 ND 0.164 0.000
ND 0.111 0.000 ND 0.222 0.000
ND 0.113 0.000 ND 0.226 0.000
ND 0.0762 0.000 ND 0.152 0.000
ND 1.05 0.000 ND 2.10 0.000
ND 0.0564 0.000 ND 0.113 0.000
ND 0.152 0.000 ND 0.304 0.000
ND 0.0939 0.000 ND 0.188 0.000
ND 0.390 0.000 ND 0.780 0.000
ND 0.0587 0.000 ND 0.117 0.000
ND 0.0920 0.000 ND 0.184 0.000
ND 0.0591 0.000 ND 0.118 0.000
ND 0.113 0.000 ND 0.226 0.000
172 ER 0.0487 0.000 173 0.0974 0.000
0.607 0.0499 0.000 0.635 J 0.0998 0.000
15.4 v 0.0697 0.000 15.4 0.139 0.000
12.0 0.0603 0.000 11.4 0.121 0.000
0.794 0.0813 0.000 0.690 J 0.163 0.000
ND 0.0670 0.000 ND 0.134 0.000
ND 0.0451 0.000 ND 0.0902 0.000
ND 0.0714 0.000 ND 0.143 0.000
ND 0.0464 0.000 ND 0.0928 0.000
ND 0.0366 0.000 ND 0.0732 0.000
ND 0.0658 0.000 ND 0.132 0.000
ND 0.0647 0.000 ND ·0.129 0.000
ND 0.0552 0.000 ND 0.110 0.000
ND 0.212 0.000 ND 0.424 0.000
ND 0.167 0.000 ND 0.334 0.000
Page 10 of 60
---·-----·-----------
------~------~-----SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsopropyltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methyl-2-pentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Propanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Styrene 100-42-5
LI 1 2-Tetrachloroethane 630-20-6
1, 1,2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2 3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
1 1 1 ~Trichloroethane 71-55-6
1 1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2 3-Trichloroorooane 96-18-4
1 1 2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethylbenzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/25/2000 01 :00
0500HBWW213
2000505701
Cone Flaa Dl
ND 0.616
ND 0.474
ND 0.452
ND 1.14
ND. 0.469
ND 0.845
ND B 0.796
ND 1.06
ND 6.88
ND 0.886
ND 0.722
ND 0.948
ND 0.792
31.7 0.568
ND 4.02
ND 0.680
ND 4.67
ND 1.18
ND 0.331
2.59 J 0.952
479 0.905
ND 2.08
ND 0.543
ND 0.766
ND 0.749
ND 0.436
ND 0.438
15.3 0.574
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
0500HBWW214 0500HBWW214
2000505702 2000505702
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0616 0.000 ND 0.123 0.000
0.000 ND 0.0474 0.000 ND 0.0948 0.000
0.000 ND 0.0452 0.000 ND 0.0904 0.000
0.000 ND 0.114 0.000 ND 0.228 0.000
0.000 ND 0.0469 0.000 ND 0.0938 0.000
0.000 ND 0.0345 0.000 ND . 0.169 0.000
0.000 ND B 0.0796 0.000 ND B 0.159 0.000
0.000 ND 0.106 0.000 ND 0.212 0.000
0.000 ND 0.688 0.000 ND 1.38 0.000
0.000 ND 0.0886 0.000 ND 0.177 0.000
0.000 ND 0.0722 0.000 ND 0.144 0.000
0.000 ND 0.0948 0.000 ND 0.190 0.000
0.000 ND 0.0792 0.000 ND 0.158 0.000
0.000 ND 0.0568 0.000 ND 0.114 0.000
0.000 ND 0.402 0.000 ND -· 0.804 0.000
0.000 ND 0.0680 0.000 ND 0.136 0.000
0.000 ND 0.467 0.000 ND 0.934 0.000
0.000 ND 0.118 0.000 ND 0.236 0.000
0.000 ND 0.0331 0.000 ND 0.0662 0.000
0.000 ND 0.0952 0.000 ND 0.190 0.000
0.000 0.494 JV 0.0905 0.000 0.355 J 0.18 l 0.000
0.000 ND 0.208 0.000 ND 0.416 0.000
0.000 ND 0.0543 0.000 ND 0.109 0.000
0.000 ND 0.0766 0.000 ND 0.153 0.000
0.000 ND 0.0749 0.000 ND 0.150 0.000
0.000 ND 0.0436 0.000 ND 0.0872 0.000
0.000 ND 0.0438 0.000 ND 0.0876 0.000
0.000 9.73 0.0574 0.000 9.65 0.115 0.000
Page II of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWW213
2000505701
Cone Flaa DL
ND 1.37
ND 0.713
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0500HBWW214 0500HBWW214
2000505702 2000505702
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.274 0.000
ND 0.0713 0.000 ND 0.143 0.000
Page 12 of 60
---------------~---
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surronate Compound
1-Bromo-4-fluorobenzene
I ,2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWW213
2000505701
Aaueous
Received
NA
05/03/2000 08:20
05/09/2000 22:54
05/09/2000 22:54
10.0000
MSDA
ug/L
% Recoverv Limits
105 77-117
91 61-143
103 87-113
LIMS Workordcr: 756200.UA-Littlc Washington, N [200050S7] Hamilton Beach-Proctor Silex
STL Austin
F
0500HBWW214 0500HBWW214
2000505702 2000505702
Aaueous Aaueous
Received Received
NA NA
05/03/2000 08:45 05/03/2000 08:45
05/08/2000 21 :31 05/09/2000 22:24
05/08/2000 21 :31 05/09/2000 22:24
1.0000 2.0000
MSDA MSDA
U!!:/L ug/L
% Recoverv Limits F % Recoverv Limits F
105 77-117 106 77-117
90 61-143 92 61-143
102 87-1I3 103 87-113
Page 13 of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
I -Ch lorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
I 04-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -0512512000 01 :00
0500HBWW215
2000505703
Aaueous
Received
NA
05/03/2000 08:55
05/08/2000 21 :59
05/08/2000 21 :59
1.0000
MSDA
ug/L
Cone Flaa DL
ND 0.286
ND l.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW215 0500HBWW227
2000505703 2000505704
Aaueous Aaueous
Received Received
NA NA
05/03/2000 08:55 05/03/2000 09:30
05/09/2000 21 :56 05/08/2000 22:27
05/09/2000 21 :56 05/08/2000 22:27
l.0000 1.0000
MSDA MSDA
ug/L ug/L
Cone Flag DL RL Cone Flaa DL RL
ND 0.286 0.000 19. l 0.286 0.000
ND l.67 0.000 ND l.67 0.000
ND 0.983 0.000 ND 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 0.622 0.0492 0.000
ND 0.0622 0.000 ND 0.0622 0.000
ND 0.139 0.000 ND 0.139 0.000
ND 0.0683 0.000 ND 0.0683 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.179 0.000 40.2 0.179 0.000
ND 0.0642 0.000 ND· 0.0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
ND 0.0484 0.000 ND 0.0484 0.000
ND 0.0867 0.000 ND 0.0867 0.000
ND 0.0839 0.000 ND 0.0839 0.000
ND 0.0473 0.000 ND 0.0473 0.000
ND 0.0756 0.000 14.6 0.0756 0.000
ND 0.0670 0.000 l.17 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
Page 14 of 60
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Ch loroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
l 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichloroditluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
l 2-Dichloroethane 107-06-2
l 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
1 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1 3-Dichloropropene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 J-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWW215
2000505703
Cone Flaa DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
3.43 v 0.0487
ND 0.0499
1.87 v 0.0697
0.0409 u 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND 0.167
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
0500HBWW215 0500HBWW227
2000505703 2000505704
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0821 0.000 ND 0.0821 0.000
0.000 ND 0.111 0.000 ND 0.111 0.000
0.000 ND 0.113 0.000 ND 0.113 . 0.000
0.000 ND 0.0762 0.000 ND 0.0762 0.000
0.000 ND 1.05 0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000 ND .. 0.0564 0.000
0.000 ND 0.152 0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000 ND 0.0587 0.000
0.000 ND 0.0920 0.000 ND 0.0920 0.000
0.000 ND 0.0591 0.000 ND 0.0591 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 3.16 0.0487 0.000 847 ER 0.0487 0.000
0.000 ND 0.0499 0.000 20.2 0.0499 0.000
0.000 1.93 0.0697 0.000 459 ER 0.0697 0.000
0.000 ND 0.0603 0.000 307 ER 0.0603 0.000
0.000 ND 0.0813 0.000 7.93 0.0813 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.0451 0.000 ND 0.0451 0.000
0.000 ND 0.0714 0.000 ND 0.0714 0.000
0.000 ND 0.0464 0.000 0.182 J 0.0464 0.000
0.000 ND 0.0366 0.000 ND 0.0366 0.000
0.000 ND 0.0658 0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000 0.454 J 0.0552 0.000
0.000 ND 0.212 0.000 ND 0.212 0.000
0.000 ND 0.167 0.000 ND 0.167 0.000
Page 15 of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Iodomethane 74-88-4
lsopropylbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Propylbenzene 103-65-1
Stvrene 100-42-5
I, 1 I 2-Tetrachloroethane 630-20-6
I 1.2.2-Tetrachloroethane 79-34-5
Tetrachloroethene i27-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2.3-Trichlorobenzene 87-61-6
I 2.4-Trichlorobenzene 120-82-1
I I I-Trichloroethane 71-55-6
1, l 2-Trichloroethane 79-00-5
Trich loroethene 79-01-6
Trichlorofluoromethane 75-69-4
1,2 3-Trichloroorooane 96-18-4
1. 1 2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
1,3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/25/2000 01:00
0500HBWW215
2000505703
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND O.ll4
1.10 0.0469
ND 0.0845
ND B 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
12.8 0.402
ND 0.0680
ND 0.467
ND 0.118
ND 0.0331
ND 0.0952
0.113 JV 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW215 0500HBWW227
2000505703 2000505704
Cone Flaa DL Rl Cone Flaa DL RL
ND 0.0616 0.000 ND 0.0616 0.000
ND 0.0474 0.000 ND 0.0474 0.000
ND 0.0452 0.000 ND 0.0452 0.000
ND 0.114 0.000 ND 0.114 0.000
1.09 0.0469 0.000 0.322 J 0.0469 0.000
ND 0.0845 0.000 ND 0.0845 0.000
ND B 0.0796 0.000 0.982 JB 0.0796 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.688 0.000 ND 0.688 0.000
ND 0.0886 0.000 ND 0.0886 0.000
ND 0.0722 0.000 ND 0.0722 0.000
ND 0.0948 0.000 ND 0.0948 0.000
ND 0.0792 0.000 1.48 0.0792 0.000
ND 0.0568 0.000 ND 0.0568 0.000
15.0 0.402 0.000 ND 0.402 0.000
ND 0.0680 0.000 13.8 0.0680 0.000
ND 0.467 0.000 ND 0.467 0.000
ND 0.118 0.000 ND 0.118 0.000
ND 0.0331 0.000 1310 ER 0.0331 0.000
ND 0.0952 0.000 2.95 0.0952 0.000
0.124 J 0.0905 0.000 48.9 0.0905 0.000
ND 0.208 0.000 ND 0.208 0.000
ND 0.0543 0.000 ND 0.0543 0.000
ND 0.0766 0.000 ND 0.0766 0.000
ND 0.0749 0.000 0.720 J 0.0749 0.000
ND 0.0436 0.000 0.646 J 0.0436 0.000
ND 0.0438 0.000 ND 0.0438 0.000
ND 0.0574 0.000 5.51 0.0574 0.000
Page 16. of 60
--------------·-----
______ , ____________ _
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
p-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWW215
2000505703
Cone Flaa DL
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0500HBWW215 0500HBWW227
2000505703 2000505704
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 0.956 J 0.137 0.000
ND 0.0713 0.000 0.995 0.0713 0.000
Page 17 of 60
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW82608
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
1-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -05/25/2000 0 I :00
0500HBWW215
2000505703
Aqueous
Received
NA
05/03/2000 08:55
05/08/2000 21 :59
05/08/2000 21 :59
1.0000
MSDA
u!!IL
% Recoverv Limits
105 77-117
92 61-143
101 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
F
0500HBWW215 0500HBWW227
2000505703 2000505704
Aqueous Aaueous
Received Received
NA NA
05/03/2000 08:55 05/03/2000 09:30
05/09/2000 21 :56 05/08/2000 22:27
05/09/2000 21 :56 05/08/2000 22:27
l.0000 1.0000
MSDA MSDA
ug/L u!!IL
% Recoverv Limits F % Recoverv Limits F
107 77-117 106 77-117 .
91 61-143 57 61-143 0
104 87-113 101 87-113
Page 18 of 60
-------------------
- - - ----- - - - - - - - - - - - -
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Ch lorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time· Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -0512512000 OJ :00
0500HBWW227
2000505704
Aaueous
Received
NA
05/03/2000 09:30
0510912000 23 :24
05/09/2000 23:24
50.0000
MSDA
ug/L
Cone Flaa DL
ND 14.3
ND 83.5
ND 49.2
ND 4.50
ND 2.46
ND 3.11
ND 6.95
ND 3.42
ND 6.80
ND 5.30
ND 8.95
ND 3.21
ND 3.72
ND 4.79
ND 2.42
ND 4.34
ND 4.20
ND 2.36
ND 3.78
ND 3.35
ND 5.65
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
.0.000
0.000
0.000
0500HBWW228 0500HBWW228
2000505705 2000505705
Aaueous Aaueous
Received Received
NA NA
05/03/2000 09:35 05/03/2000 09:35
05/08/2000 22:55 05/10/2000 00:21
05/08/2000 22:55 05/10/2000 00:21
1.0000 2000.0000
MSDA MSDA
u2/L u2/L
Cone Flaa DL RL Cone Flaa DL RL
360 XE 0.286 0.000 ND 572 0.000
ND 1.67 0.000 ND 3340 0.000
ND 0.983 0.000 ND 1970 0.000
ND 0.0901 0.000 ND 180 0.000
56.5 0.0492 0.000 ND 98.4 0.000
ND 0.0622 0.000 ND 124 0.000
ND 0.139 0.000 ND 278 0.000
ND 0.0683 0.000 ND 137 0.000
ND 0.136 0.000 ND 272 0.000
ND 0.106 0.000 ND 212 0.000
382 XE 0.179 0.000 ND 358 0.000
9.88 0.0642 0.000 ND 128 0.000
7.96 0.0745 0.000 ND 149 0.000
ND 0.0958 0.000 ND 192 0.000
1.96 0.0484 0.000 ND 96.8 0.000
26.2 0.0867 0.000 ND 173 0.000
ND 0.0839 0.000 ND 168 0.000
ND 0.0473 0.000 ND 94.6 0.000
89.8 0.0756 0.000 ND 151 0.000
9.62 0.0670 0.000 ND 134 0.000
ND 0.113 0.000 ND 226 0.000
Page 19 of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroprooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
1.2-Dibromo-3-chloropropane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1,2-Dichloroorooane 78-87-5
I 3-Dichloroprooane 142-28-9
2 2-Dichloroorooane 594-20-7
1 1-Dichloroorooene 563-58-6
cis-1.3-Dichloropropene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone . 591-78-6
SECTION IV -Analytical Results -05/25/2000 01 :00
0500HBWW227
2000505704 .
Cone Flaa DL
ND 4.10
ND 5.55
ND 5.65
ND 3.81
ND 52.5
ND 2.82
ND 7.60
ND 4.70
ND 19.5
ND 2.94
ND 4.60
ND 2.96
ND 5.65
3360 2.44
22.2 J 2.50
644 3.48
381 3.02
8.01 J 4.06
ND· 3.35
ND 2.26
ND 3.57
ND 2.32
ND 1.83
ND 3.29
ND 3.24
ND 2.76
ND 10.6
ND 8.35
LIMS Workorder: 756200.UA-Little Washington, N [20005057) Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW228 0500HBWW228
2000505705 2000505705
Cone Flaa DL RL Cone Flaa DL RL
1.33 0.0821 0.000 ND 164 0.000
ND 0.111 0.000 ND 222 0.000
ND 0.113 0.000 ND 226 0.000
ND 0.0762 0.000 ND 152 0.000
ND 1.05 0.000 ND 2100 0.000
ND 0.0564 0.000 ND 113 0.000
ND 0.152 0.000 ND 304 0.000
ND 0.0939 0.000 ND 188 0.000
ND 0.390 0.000 ND 780 0.000
ND 0.0587 0.000 ND 117 0.000
ND 0.0920 0.000 ND 184 0.000
ND 0.0591 0.000 ND I 18 0.000
ND 0.113 0.000 ND 226 0.000
1710 ER 0.0487 0.000 14500 97.4 0.000
ND 0.0499 0.000 ND 99.8 0.000
4840 ER 0.0697 0.000 53400 139 0.000
1320 ER 0.0603 0.000 2360 121 0.000
17.0 0.0813 0.000 ND 163 0.000
ND 0.0670 0.000 ND 134 0.000
ND 0.0451 0.000 ND 90.2 0.000
ND 0.0714 0.000 ND 143 0.000
1.51 0.0464 0.000 ND 92.8 0.000
ND 0.0366 0.000 ND 73.2 0.000
ND 0.0658 0.000 ND 132 0.000
ND 0.0647 0.000 ND 129 0.000
492 ER 0.0552 0.000 555 J 110 0.000
ND 0.212 0.000 ND 424 0.000
38.8 0.167 0.000 ND 334 0.000
Page 20 of 60
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6 . Methvl methacrvlate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I I I 2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
1,2.4-Trichlorobenzene 120-82-1
I 1, I-Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloroorooane 96-18-4
l 1,2-Trichlorotrifluoroethane 76-13-1
I 2.4-Trimethvlbenzene 95-63-6
1 3,5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -0512512000 0 I :00
0500HBWW227
2000505704
Cone Flag DL
ND 3.08
ND 2.37
ND 2.26
ND 5.70
ND 2.34
ND 4.22
ND B 3.98
ND 5.30
ND 34.4
ND 4.43
ND 3.61
ND 4.74
ND 3.96
ND 2.84
ND 20.1
15.7 J 3.40
ND 23.4
ND 5.90
2440 1.66
ND 4.76
58.6 4.52
ND 10.4
ND 2.72
ND 3.83
ND 3.74
ND 2.18
ND 2.19
ND 2.87
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW228 0500HBWW228
2000505705 2000505705
Cone Flag DL RL Cone Flaa DL RL
ND 0.0616 0.000 ND 123 0.000
33.7 0.0474 0.000 ND 94.8 0.000
ND 0.0452 0.000 ND 90.4 0.000
ND 0.114 0.000 ND 228 0.000
20.8 0.0469 0.000 ND -93.8 0.000
17.5 0.0845 0.000 ND 169 0.000
3.64 B 0.0796 0.000 ND B 159 0.000
246 XE 0.106 0.000 ND 212 0.000
ND 0.688 0.000 ND 1380 0.000
302 XE 0.0886 0.000 ND 177 0.000
ND 0.0722 0.000 ND 144 0.000
0.844 0.0948 0.000 ND 190 0.000
ND 0.0792 0.000 ND 158 0.000
32.4 0.0568 0.000 ND 114 0.000
ND 0.402 0.000 ND 804 0.000
972 ER 0.0680 0.000 1520 136 0.000
ND 0.467 0.000 ND 934 0.000
ND 0.118 0.000 ND 236 0.000
6990 ER 0.0331 0.000 121000 66.2 0.000
38.0 0.0952 0.000 ND 190 0.000
3550 ER 0.0905 0.000 13300 181 0.000
8.12 0.208 0.000 ND 416 0.000
ND 0.0543 0.000 ND 109 0.000
0.947 0.0766 0.000 ND 153 0.000
1220 ER 0.0749 0.000 1190 J 150 0.000
407 XE 0.0436 0.000 ND 87.2 0.000
ND 0.0438 0.000 ND 87.6 0.000
194 XE 0.0574 0.000 ND 115 0.000
Page 21 of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analyti~al Results -05/25/2000 0 I :00
0500HBWW227
2000505704
Cone Flaa DL
ND 6.85
ND 3.56
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
RL
0.000
0.000
0500HBWW228 0500HBWW228
2000505705 2000505705
Cone Flaa DL RL Cone Flaa DL RL
1120 ER 0.137 0.000 1680 J 274 0.000
930 ER 0.0713 0.000 1350 143 0.000
Page 22 of 60
- - - - - - - - - - - - - -·-- - - -
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surrogate Compound
1-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -0512512000 01 :_DO
0500HBWW227
2000505704
Aqueous
Received
NA
05/03/2000 09:30
05/09/2000 23:24
0510912000 23:24
50.0000
MSDA
ug/L
% Recovery Limits
106 77-117
90 61-143
99 87-113
LIMS Workorder: 756200.UA-Littlc Washington, N [20005057) Hamilton Beach-Proctor Silex
STLAustin
F
0500HBWW228 0500HBWW228
2000505705 2000505705
Aqueous Aqueous
Received Received
NA NA
05/03/2000 09:35 05/03/2000 09:35
05/08/2000 22:55 05/10/2000 00:21
05/08/2000 22:55 05/10/2000 00:21
1.0000 2000.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recoverv Limits F
92 77-117 ·106 77-117
22 61-143 0 90 61-143
113 87-113 JOI 87-113
Page 23 of 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Ch loro-1.3-butadiene
Chlorobenzene
Chloroethane
Chlorofonn
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/25/2000 0 I :00
TRIP BLANK2
2000505707
Aaueous
Received
NA
05/03/2000 00:00
05/08/2000 20:35
05/08/2000 20:35
1.0000
MSDA
ue:/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flag DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 24 of 60
~------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW82608
Continued
Parameter
Ch loromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1,3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
I. 1-Dichloroethene 75-35-4
cis-1,2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
1 2-Dichloropropane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
I, 1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-1,3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/25/2000 01 :00
I TRIP BLANK 2
2000505707
Cone Flaa DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND 0.167
LIMS Wbrkorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flaa DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 .
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 25 or 60
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsooroov Ito I uene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-lO-l
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I I, 1.2-Tetrachloroethane 630-20-6
I 1.2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2 3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
I I I-Trichloroethane 71-55-6
I. I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichloroorooane 96-18-4
1 1.2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
1,3,5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/25/2000 01 :00
I TRIP BLANK 2
2000505707
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
ND 0.0845
ND B 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND 0.467
ND 0.118
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flaa DL RL Cone Flag DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 -0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 26 of 60
·------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -0512512000 01 :00
I TRIP BLANK 2
2000505707
Cone Flaa DL
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flaa DL RL. Cone Flaa DL RL
0.000
0.000
Page 27 of 60
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Compound
I-Bromo-4-tluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -05/25/2000 01 :00
TRIPBLANK2
2000505707
Aoueous
Received
NA
05/03/2000 00:00
05/08/2000 20:35
05/08/2000 20:35
1.0000
MSDA
ug/L
% Recoverv Limits
105 77-117
90 61-143
101 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
F 0/o Recoverv Limits F % Recoverv Limits F
Page 28 of 60
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4862 Instrument Data File: A0508002.D
Instrument ID: MSDA Analyst: MER
Parameter Reference Value Measured Cone
Acetone 20 17.1
Acetonitrile 100 74.0
Acrolein 100 63.9
Acrvlonitrile 20 15.5
Benzene 20 19.6
Bromobenzene 20 19.9
Bromochloromethane 20 22.5
Bromodichloromethane 20 18.7
Bromoform 20 19.l
Bromomethane 20 20.2
2-Butanone (MEK) 20 14.0
n-Butvlbenzene 20 22.4
sec-Butvlbenzene 20 21.9
tert-Butvlbenzene 20 21.4
Carbon disulfide 20 22.1
Carbon tetrachloride 20 22.7
2-Chloro-1.3-butadiene 20 23.2
Chlorobenze"ne 20 20.7
Chloroethane 20 20.6
Chloroform 20 22.1
1-Chlorohexane 20 22.5
Chloromethane 20 15.3
3-Chloroorooene 20 18.9
2-Chlorotoluene 20 20.8
4-Chlorotoluene 20 20.2
l 2-Dibromo-3-chloroorooane 20 15.9
SECTION V -Calibration and QC Information -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Date/Time Analyzed:05/08/2000 15:08
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
85
74
64
78
98
100
112
93
95
101
70
112
109
107
110
113
116
104
103
110 80-120
112
76
95
104
101
79
Page 29 of 60
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4862 Instrument Data File: A0508002.D
Instrument ID: MSDA Analyst: MER
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 19.1
I 2-Dibromoethane 20 17.9
Dibromomethane 20 17. l
trans-I .4-Dichloro-2-butene 20 14.8
I .4-Dichlorobenzene 20 19.5
1.2-Dichlorobenzene 20 19.3
1.3-Dichlorobenzene 20 19.6
Dichlorodifluoromethane 20 19.3
1 1-Dichloroethane 20 21.4
1 2-Dichloroethane 20 19.5
1.1-Dichloroethene 20 23.6
cis-1.2-Dichloroethene 20 21.7
trans-1.2-Dichloroethene 20 22.4
I 2-Dichloroorooane 20 18.2
I 3-Dichloroorooane 20 17.3
2 2-Dichloroorooane 20 24.3
l 1-Dichloroorooene 20 20.0
cis-1 3-Dichloroorooene 20 · 18.4
trans-I 3-Dichloroorooene 20 17.4
Ethyl methacrvlate 20 16.0
Ethvlbenzene 20 20.9
Hexachloro-1 3-butadiene 20 27.4
2-Hexanone 20 13.2
lodomethane 20 22.7
lsooroovlbenzene 20 22.0
4-lsooroovltoluene 20 22.1
SECTION V -Calibration and QC lnfonnation -0512512000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Dateffime Analyzed:05/08/2000 15:08
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
95
89
86
74
98
97
98
97
107
98
118 80-120
109
112
91 80-120
86
122
100
92
87
80
105 80-120
137
66
113
110
110
Page 30 of 60
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4862 Instrument Data File: A0508002.D
Instrument ID: MSDA Analyst: MER
Continued
Parameter Reference Value Measured Cone
Methyl methacrylate 20 15.7
Methvl tert-butvl ether (MTBE) 20 18.6
4-Methvl-2-pentanone (MIBK) 20 13.4
Methvlene chloride 20 19.9
Naphthalene 20 15.5
Prooanenitrile 100 80.9
n-Propyfbenzene 20 21.2
Stvrene 20 20.7
I. I I 2-Tetrachloroethane 20 21.3
I.I 2 2-Tetrachloroethane 20 I6.9
Tetrachloroethene 20 23.0
Tetrahvdrofuran 20 14.6
Toluene 20 20.0
I 2 3-Trichlorobenzene 20 14.6
1,2 4-Trichlorobenzene 20 21.3
I I I-Trichloroethane 20 23.2.
l 1.2-Trichloroethane 20 I7.6
Trichloroethene 20 22.1
Trichlorotluoromethane 20 26.7
1.2 3-Trichloroorooane 20 16.7
1 1,2-Trichlorotrifluoroethane 20 25.2
1.2 4-Trimethvlbenzene 20 20.4
I 3 5-Trimethvlbenzene 20 20.7
Vinyl acetate 20 I7.0
Vinvl chloride 20 19.3
p-Xvlene/m-Xvlene 40 43.2
SECTION V -Calibration and QC Information -05/25/2000 0 I :00
UMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Dateffime Analyzed:05/08/2000 15 :08
Units: ug/L
%Recoverv Flaa QC limits %Recoverv
78
93
67
99
78
8I
106
I03
107
84
l I5
73
100 80-120
73
106
116
88
111
134
84
126
102
103
85
96 80-I20
108
Page 31 of 60
------------SECTIONV -------
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW82608
Sample Type: Continuing Calibration Check
Analysis ),latch ID: 4862 Instrument Data File: A0508028.D
Instrument ID: MSDA Analyst: MER
Parameter Reference Value Measured Cone
Acetone 20 15.3
Acetonitrile 100 68.2
Acrolein 100 67.4
Acrvlonitrile 20 16.6
Benzene 20 18.3
Bromobenzene 20 18.9
Bromoch loromethane 20 22.0
Bromodichloromethane 20 18.1
Bromoform 20 17.3
Bromomethane 20 7.10
2-Butanone (MEK) 20 19.3
n-Butvlbenzene 20 20.1
sec-Butvlbenzene 20 19.7
tert-Butvlbenzene 20 19.2
Carbon disulfide 20 16.5
Carbon tetrachloride 20 20.0
2-Chloro-1.3-butadiene 20 20.8
Chlorobenzene 20 19.8
Chloroethane 20 18.2
Chloroform 20 21.0
1-Chlorohexane 20 21.0
Chloromethane 20 12.2
3-Chloroorooene 20 16.6
2-Chlorotoluene 20 19.0
4-Chlorotoluene 20 18.7
I 2-Dibromo-3-chloroorooane 20 19.1
SECTION V -Calibration and QC Information -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [2000505'7] Hamillon Beach-Proctor Silex
STLAustin
Flaa
Dateffime Analyzed:05/09/2000 13:33
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
77
68
67
83
92
94
110
91
87
35
96
101
98
96
83
100
104
99
91
105 80-120
105
61
83
95
94
96
Page 33 of 60
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4862 Instrument Data File: A0508028.D
Instrument ID: MSDA Analyst: MER
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 18. l
I 2-Dibromoethane 20 19.4
Dibromomethane 20 18.7
trans-1.4-Dichloro-2-butene 20 9.50
l 4-Dichlorobenzene 20 18.4
l .2-Dichlorobenzene 20 19.3
1 3-Dichlorobenzene 20 18.6
Dichlorodifluoromethane 20 17.0
I 1-Dichloroethane 20 19.6
1.2-Dichloroethane 20 19.9
1.1-Dichloroethene 20 20.3
cis-1.2-Dichloroethene 20 20.6
trans-1.2-Dichloroethene 20 20.6
1 2-Dichlorooronane 20 17.9
1 3-Dichloroorooane 20 18.3
2.2-Dichlorooronane 20 24.l
1.1-Dichloroorooene 20 19.4
cis-1 3-Dichloroorooene 20 17.6
trans-I 3-Dichloroorooene 20 17.3
Ethvl methacrvlate 20 18.7
Ethvlbenzene 20 19.8
Hexachloro-1.3-butadiene 20 27.2
2-Hexanone 20 16.8
lodomethane 20 20.3
Isooroovlbenzene 20 20.5
4-lsooroovltoluene 20 19.7
SECTION V -Calibration and QC Information -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Dateffime Analyzed:05/09/2000 13:33
Units: ug/L
%Recoveni Flaa QC Limits %Recoverv
91
97
94
47
92
96
93
85
98
100
102 80-120
103
103
89 80-120
92
120
97
88
86
94
99 80-120
136
84
101
102
99
Page 34 of 60
-------------------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4862 Instrument Data File: A0508028.D
Instrument ID: MSDA Analyst: MER
Continued
Parameter Reference Value Measured Cone
Methvl methacrvlate 20 17.9
Methvl tert-butyl ether (MTBE) 20 20.9
4-Methvl-2-oentanone (MlBK) 20 16.3
Methylene chloride 20 19.7
Naohthalene 20 24.7
Propanenitrile 100 84.0
n-Propy !benzene 20 19.4
Stvrene 20 19.7
1.1 1.2-Tetrachloroethane 20 20.5
1,122-Tetrachloroethane 20 19.8
Tetrachloroethene 20 21.6
Tetrahydrofuran 20 15.9
Toluene 20 18.7
I 2,3-Trichlorobenzene 20 . 27.9
1.2 4-Trichlorobenzene 20 26.8
I, I I -Trichloroethane 20 23.9
1.1.2-Trichloroethane 20 19.1
Trichloroethene 20 21.4
Trichlorofluoromethane 20 25.5
1.2 3-Trichloroorooane 20 18.9
I I 2-Trichlorotrifluoroethane 20 22.9
1.2.4-Trimethvlbenzene 20 18.6
1.3.5-Trimethylbenzene 20 18.5
Vinvl acetate 20 18.2
Vinyl chloride 20 17.3
o-Xylene/m-Xylene 40 40.0
SECTION V -Calibration and QC Information -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Date/Time Analyzed:05/09/2000 13:33
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
90
105
82
98
124
84
97
99
103
99
108
80
94 80-120
139
134
120 *
96
107
128
95
114
93
93
91
86 80-120
JOO
Page 35 of 60
--·------------------SECTION V
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4881 Instrument Data File: A0509001.D
Instrument ID: MSDA Analyst: MER
Parameter Reference Value Measured Cone Flaa
Acetone 20 16.3
Acetonitrile 100 70.3
Acrolein 100 67.4
Acrvlonitrile 20 17.2
Benzene 20 19.1
Bromobenzene 20 19.7
Bromoch loromethane 20 23.0
Bromodich1oromethane 20 19.2
Bromoform 20 18.1
Bromomethane 20 7.74
2-Butanone (MEK) 20 16.3
n-Butvlbenzene 20 20.8
sec-Buty1benzene 20 20.5
tert-Butvlbenzene 20 20.4
Carbon disulfide 20 17.3
Carbon tetrachloride 20 21.3
2-Chloro-1 3-butadiene 20 21.7
Chlorobenzene 20 20.5
Chloroethane 20 19.0
Chloroform 20 21.5
1-Chlorohexane 20 21.9
Chloromethane 20 12.4
3-Chloroorooene 20 17.3
2-Chlorotoluene 20 20.0
4-Chlorotoluene 20 19.5
I 2-Dibromo-3-chloroorooane 20 19.2
SECTION V -Calibration and QC Information -05/25/2000 ~I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAuslin
Dateffime Analyzed:05/09/2000 16:49
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
81
70
67
86
95
98
115
96
91
39
81
104
103
102
87
106
109
102
95
107 80-120
109
62
87
100
98
96
Page 37 of 60
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4881 Instrument Data File: A050900 l.D
Instrument ID: MSDA Analyst: MER
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 19.0
I 2-Dibromoethane 20 19.9
Dibromomethane 20 19.1
trans-I 4-Dichloro-2-butene 20 11.5
1.4-Dichlorobenzene 20 19.6
1,2-Dichlorobenzene 20 19.9
1.3-Dichlorobenzene 20 19.4
Dichlorodifluoromethane 20 16.0
1.1-Dichloroethane 20 20.5
I 2-Dichloroethane 20 20.7
I 1-Dichloroethene 20 21.3
cis-1 2-Dichloroethene 20 21.4
trans-1.2-Dichloroethene 20 21.7
1 2-Dichloroorooane 20 18.7
1.3-Dichloroorooane 20 18.4
2 2-Dichloroorooane 20 24.7
I 1-Dichloroprooene 20 20.4
cis-1 3-Dichloroorooene 20 ·18.8
trans-I 3-Dichloroorooene 20 17.9
Ethvl methacrvlate 20 18.2
Ethvlbenzene 20 20.4
Hexachloro-1.3-butadiene 20 27.5
2-Hexanone 20 16.2
lodomethane 20 21.0
Isooroovlbenzene 20 21.3
4-Isooroovltoluene 20 20.4
SECTION V -Calibration and QC Information -0512512000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Dateffime Analyzed:05/09/2000 16:49
Units: ug/L
%Recoveni Flaa QC Limits %Recoverv
95
100
96
57
98
99
97
80
102
103
107 80-120
107
109
93 80-120
92
124
102
94
90
91
102 80-120
138
81
105
106
102
Page 38 of 60
·~--~--------------
-----SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
- - -
Sample Type: Continuing Calibration Check
- --- - - - -
Analysis Batch ID: 4881 Instrument Data File: A0509001 .D Date!fime Analyzed:05/09/2000 16:49
Instrument ID: MSDA Analyst: MER
Continued
Parameter Reference Value Measured Cone
Methvl methacrvlate 20 18.3
Methvl tert-butvl ether (MTBE) 20 18.7
4-Methyl-2-oentanone (MIBK) 20 17.1
Methylene chloride 20 19.9
Naohthalene 20 23.2
ProoaAenitrile 100 81.0
n-Proovlbenzene 20 20.4
Stvrene 20 20.6
I. I I 2-Tetrachloroethane 20 20.8
1.1.2 2-Tetrachloroethane 20 19.7
Tetrachloroethene 20 22.4
Tetrahydrofuran 20 19.6
Toluene 20 19.4
I 2 3-Trichlorobenzene 20 25.0
I 2 4-Trichlorobenzene 20 26.6
I. I. I -Trichloroethane 20 24.7
1.1.2-Trichloroethane 20 19.4
Trichloroethene 20 22.2
Trichlorofluoromethane 20 25.4
I 2 3-Trichloroorooane 20 19. I
I I 2-Trichlorotrifluoroethane 20 23.6
I 2.4-Trimethylbenzene 20 19.6
1,3 ,5-Trimethvlbenzene 20 19.3
Vinvl acetate 20 17.8
Vinyl chloride 20 17.6
o-Xylene/m-Xylene 40 41.7
SECTION V -Calibration and QC Information • 0512512000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
' .
Flaa
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
91
93
85
100
116
81
102
103
104
99
112
98
97 80-120
125
133
123
97
II I
127
96
118
98
96
89
88 80-120
104
- - - -
Page 39 of 60
-------------------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 4862
Instrument ID: MSDA
Mass/Enerav
50
75
95
96
173
174
175
176
177
Instrument Data File: A0508002.D
Injection Time: 05/08/2000 15:08
Ion Abundance Criteria
Lower limit Unner limit
15 40
30 60
100 100
5 9
0 2
50
5 .. 9
95 IOI
5 9
SECTION V -Calibration and QC Information -0512512000 01:00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
Date Analyzed: 05/08/2000 1·5:08
Analyst: MER
% Relative Abundance
27
45.9
100
6.5
0
82.2
7.4
96.2
6.1
Page 41 of 60
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS· VOA
SW8260B
BFB
Analysis Batch ID: 4862
Instrument ID: MSDA
Instrument Data File: A0508028.D
Injection Time: 05/09/2000 13:33
Ion Abundance Criteria
Mass/Enerav Lower limit Uooerlimit
50 15 40
75 30 60
95 100 100
96 5 9
173 0 2
174 50
175 5 9
176 95 101
177 5 9
SECTION V -Calibration and QC Information -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STL Austin
Date Analyzed: 05/09/2000 13:33
Analyst: MER
o/o Relative Abundance
23.7
46.9
100
6.2
0
80.1
7. l
96.4
6
Page 42 of 60
-------------------
-------------------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW82608
BFB
Analysis Batch ID: 4881
Instrument ID: MSDA
Instrument Data File: A0509001.0
Injection Time: 05/09/2000 16:49
Ion Abundance Criteria
Mass/Enerav Lower limit Uooer Limit
50 15 40
75 30 60
95 100 JOO
96 5 9
173 0 2 -174 50
175 5 9
176 95 IOI
177 5 9
SECTION V -Calibration and.QC lnfonnation -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
Date Analyzed: 05/09/2000 16:49
Analyst: MER
% Relative Abundance
30.8
46.5
JOO
6.9
0
88.8
6.9
97.8
6.6
Page 43 of 60
SECTION V
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Buty I benzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Ch loromethane
3-Chloroprooene
2-Chlorotoluene
4-Chlorotoluene
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
95-49-8
106-43-4
SECTION V -Calibration and QC Information -05/25/2000 0 \ :00
1007230
Method Blank
Aaueous
05/08/2000 17: 18
05/08/2000 17:18
MSDA
m1/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
LIMS Workorder: 756200.UA-Little Washington, N. [20005057] Hamilton Beach-Proctor Silex
STLAustin
1007341
Method Blank
Aaueous
05/09/2000 18: 13
0510912000 18: 13
MSDA
U!!/L
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.286 0.000
0.000 ND 1.67 0.000
0.000 ND 0.983 0.000
0.000 ND 0.0901 0.000
0.000 ND 0.0492 0.000
0.000 ND 0.0622 0.000
0.000 ND 0.139 0.000
0.000 ND 0.0683 0.000
0.000 ND 0.136 -0.000
0.000 ND 0.106 0.000
0.000 ND 0.179 0.000
0.000 ND 0.0642 0.000
0.000 ND 0.0745 0.000
0.000 ND 0.0958 0.000
0.000 ND 0.0484 0.000
0.000 ND 0.0867 0.000
0.000 ND 0.0839 0.000
0.000 ND 0.0473 0.000
0.000 ND 0.0756 0.000
0.000 ND 0.0670 0.000
0.000 ND 0.113 0.000
0.000 ND 0.0821 0.000
0.000 ND 0.111 0.000
0.000 ND 0.113 0.000
0.000 ND 0.0762 0.000
Page 44 of 60 ________ , __________ _
-------------------SECTl9NV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-l .4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-l
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3"
1.2-Dichioroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-l .2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
I 2-Dichloroorooane 78-87-5
I 3-Dichloronronane 142-28-9
2.2-Dichloroorooane 594-20-7
l. l-Dichloronronene 563-58-6
cis-1 3-Dichloronrooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
Iodomethane 74-88-4
lsonronvlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
SECTION V -Calibration and QC Information -05/25/2000 01 :00
1007230
Cone Flaa DL
ND 1.05 .
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND 0.167
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
1007341
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000
0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000 -
0.000 ND 0.0920 0.000 -~-
0.000 ND 0.0591 0.000
0.000 ND 0.113 0.000
0.000 ND 0.0487 0.000
0.000 ND 0.0499 0.000
0.000 ND 0.0697 0.000
0.000 ND 0.0603 0.000
0.000 ND 0.0813 0.000
0.000 ND 0.0670 0.000 --
0.000 ND 0.0451 0.000 -
0.000 ND 0.0714 0.000
0.000 ND 0.0464 0.000
0.000 ND 0.0366 0.000
0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000
0.000 ND 0.212 0.000
0.000 ND 0.167 0.000
0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000
0.000. ND 0.0452 0.000
0.000 ND 0.114 0.000
0.000 ND 0.0469 0.000
Page 45 of 60
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
4-Methvl-2-oentanone fMIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Pronanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 1 1.2-Tetrachloroethane 630-20-6
I 1 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2-3-Trichlorobenzene 87-61-6
1 2 4-Trichlorobenzene 120-82-l
1 1 I-Trichloroethane 71-55-6
1.1 2-Trichloroethane 79-00-5
Trichlbroethene 79-01-6
Trichlorotluoromethane 75-69-4
1 2 3-Trichloroorooane 96-18-4
1.1 2-Trichlorotrifluoroethane 76-13-1
1 2.4-Trimethvlbenzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
n-Xvlene/m-Xvlene 106-42-3
o-Xvlene 95-47-6
SECTION V -Calibration and QC lnfonnation -05/25/2000 0 I :00
1007230
Cone Flaa DL
ND 0.0845
0.347 J 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND 0.467
ND 0.118
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005057) Hamilton Beach-Proctor Silex
STLAustin
1007341
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0845 0.000
0.000 0.102 J 0.0796 0.000
0.000 ND 0.106 0.000
0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000
0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000
0.000 ND 0.0568 0.000
0.000 ND 0.402 0.000
0.000 ND 0.0680 0.000
0.000 ND 0.467 0.000
0.000 ND 0.118 0.000
0.000 ND 0.0331 0.000
0.000 ND 0.0952 0.000
0.000 ND 0.0905 0.000
0.000 ND 0.208 Q.000
0.000 ND 0.0543 0.000
0.000 ND 0.0766 0.000
0.000 ND 0.0749 0.000
0.000 ND 0.0436 0.000
0.000 ND 0.0438 0.000
0.000 ND 0.0574 0.000
0.000 ND 0.137 0.000
0.000 ND 0.0713 0.000
Page 46 of 60
-------------------
-------------------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
. SW8260B
Surroaate Comoound
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
SECTION V -Calibration and QC Information -05~25/2000 0.1 :00
1007230
Method Blank
Aaueous
0510812000 17: 18
05/08/2000 17: 18
MSDA
mdL
% Recoverv Limits
106 77-117
90 62-143
100 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20005057) Hamilton Beach-Proctor Silex
STLAustin
100734 l
Method Blank
Aqueous
0510912000 18: l 3
.) 0510912000 18: 13
MSDA
ug/L
F % Recoverv Limits F % Recoverv Limits F
106 77-117
90 62-143
102 87-113 ·-
Page 47 of 60
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
LCS for HBN 4862 [MSV/1134]
4862
4862
Instrument ID:
Units:
Matrix:
MSDA
ug/L
Aqueous
c ontrol Samole
Lab ID: 1007228
File ID: A0508003.D
Parameter Sok Amt Cone
Acetone 20 16.4
Benzene 20 18.8
Bromobenzene 20 19.7
Bromoch loromethane 20 23.2
Bromodichloromethane 20 20.1
Bromoform 20 22.7
Bromomethane 20 19.5
2-Butanone (MEK) 20 18.5
n-Butvlbenzene 20 19.6
sec-Butvlbenzene 20 20.1
tert-Butvlbenzene 20 19.2
Carbon disulfide 20 16.7
Carbon tetrachloride 20 21.3
Chlorobenzene 20 19.9
Chloroethane 20 17.5
Chloroform 20 21.0
Chloromethane 20 12.6
2-Chlorotoluene 20 19.2
4-Chlorotoluene 20 19.5
I ,2-Dibromo-3-chloroorooane 20 20.7
Dibromochloromethane 20 21.8
1,2-Dibromoethane 20 20.7
Dibromomethane 20 19.6
1.4-Dichlorobenzene . 20 19.1
SECTION V -Calibration and QC Information -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
82
94
99
116
101
113
97
93
98
100
96
83
106
100
87
105
63
96
98
104
109
104
98
96
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture: NA
MER Analyst:
Control Sample Duplicate
1007229
A0508004.D
Cone %Rec Fla
15.4 77
18. I 90
18.8 94
22.8 114
19.6 98
21.1 105
19.3 96
15.9 80
19.1 96
19.6 98
18.5 93
16.5 82
20.3 101
19.6 98
17.0 85
20.7 103
12.0 60
18.7 94
18.9 94
18.4 92
20.8 104
19.4 97
18.7 93
18.3 91
QC Limits
RPO Fla %Rec RPO
6.3 0.1-240 71
4.3 71-133 17
5.2 67-127 12
1.7 61-145 21
3 57-135 19
7.3 23-151 17
I 34-128 25
15 0.1-214 39
2.1 28-184 30
2 45-160 31
3.2 65-148 27
1.2 29-223 23
4.8 46-150 23
2 77-129 14
2.3 39-133 27
1.9 64-146 16
4.9 18-140 26
2.1 70-136 24
4.2 74-132 23
12 39-171 25 -4.7 45-137 15
7 19-187 19
5.2 52-138 21
5.3 70-132 13
Page 48 of 60
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Lab ID:
c ontro IS amn e contmue
1007228
File ID: A0508003.D
Parameter Sok Amt Cone
1.2-Dichlorobenzene 20 I9.9
I 3-Dichlorobenzene 20 I8.7
Dichlorodifluoromethane 20 I3.3
I. I-Dichloroethane 20 I9.3
1,2-Dichloroethane 20 20.3
I I-Dichloroethene 20 21.0
cis-I 2-Dichloroethene 20 20.5
trans-1,2-Dichloroethene 20 21.6
I 2-Dichloroorooane 20 I8.4
I 3-Dichloroorooane 20 . I9.2
2.2-Dichloroorooane 20 23.8
I. I-Dichloroorooene 20 I8.9
cis-1 3-Dichloroprooene 20 I8.5
trans-I 3-Dichloroorooene 20 I8. I
Ethvlbenzene 20 I9.9
Hexachloro-I 3-butadiene 20 25.7
2-Hexanone 20 I7.4
lodomethane 20 I9.7
Isopropylbenzene 20 20.9
4-Isooroovltoluene 20 19.2
4-Methvl-2-pentanone (MIBK) 20 16.7
Methvlene chloride 20 19.9
Naphthalene 20 24.9
n-Proovlbenzene 20 19.3
Stvrene 20 20.0
I, I I ,2-Tetrachloroethane 20 21.7
1 I 2.2-Tetrachloroethane 20 21.5
Tetrachloroethene 20 21.6
Toluene 20 I9.0
I 2 3-Trichlorobenzene 20 26.8
I .2 4-Trichlorobenzene 20. 27.5
SECTION V -Calibration and QC Information -05/25/2000 01 :00
LIMS Workorder: 756200.UA-Littie Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
100
93
67
96
102
105
103
108
92
96
I I 9
95
92
90
100
I29
87
99
105
96
84
100
125
97
100
109
107
108
95
I34
I37
d
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Contro IS am vie Duolicate contmue d
1007229
A0508004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
I9. I 95 5. I 67-135 I4
I8.3 92 1.l 68-I34 I4
I3.6 68 1.5 O.I-166 26
19.3 96 0 66-I38 I9
20.0 100 2 48-I52 23
2I .4. 107 l.9 47-I75 25
20.3 IOI 2 66-I44 I8
21.6 108 0 62-I46 22
I8.3 9I 1.l --61-I33 I7
I8.9 94 2. I 70-I28 I6
22.8 ll4 4.3 40-I68 30
18.2 91 4.3 71-I 55 3I
I8.3 92 0 36-I42 16
17.7 89 I.I 34-I38 2I
I9.2 96 4.1 75-I3 I I4
25.2 I26 2.4 46-I50 34
I6.2 8I 7.! . -· 22-I64 34
19.7 99 0 -
20.4. 102 2.9 54-152 26
18.7 94 2.1 41-165 28
I7.0 85 l.2 27-I49 36
21.0 105 4.9 36-I66 23
23.8 ll9 4.9 32-172 22
19.3 96 1 61-143 28
I9.6 98 2 68-136 14
20.9 105 3.7 63-14I 20
I9.9 100 6.8 47-I43 20
21.4 107 0.9 69-I37 16
I8.6 93 2. I 70-132 17
26.4 I32 l.5 66-I40 20
25.9 I29 6 66-I44 22
Page 49 of 60
SECTIONV
Calibration and QC Information
Control Sample Results .
MS-VOA
SW8260B
Lab ID:
C t IS on ro f d ampe con mue
1007228
File ID: A0508003.D
Parameter Sok Amt Cone
I 1.1-Trich loroethane 20 21.7
I, 1,2-Trichloroethane 20 19.9
Trichloroethene 20 21.2
Trichlorofluoromethane 20 21.1
I 2 3-Trichloropropane 20 20.6
1 2 4-Trimethvlbenzene 20 18.7
I 3 5-Trimethvlbenzene 20 18.6
Vinvl acetate 20 7.56
Vinvl chloride 20 15.6
p-Xvlene/m-Xvlene 40 40.5
o-Xvlene 20 19.9
SECTION V -Calibration and QC Information -05/25/2000 OJ :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
' 109
99
106
106
103
94
93
38
78
101
JOO
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
40
20
c ontro IS ampe up 1cate con mue I D r f d
1007229
A0508004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
21.0 105 3.7 49-155 24
19.1 95 4.1 67-135 17
20.8 104 1.9 71-129 17
21.4 107 0.9 39-147 29
19.4 97 6 64-140 18
18.2 91 3.2 54-156 25
18.1 91 2.2 62-144 25
7.80 39 2.6 0.1-164 31
15.8 79 1.3 24-138 27
39.5 99 2 76-134 15
19.6 98 2 77-131 15
Page 50 of 60
~------------------
-·-- --·-----SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Surroaate Comoounds
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
SECTION V -Calibration and QC Information -05/25/2000 01:00
Lab ID: 1007228
%Recoverv
110
91
102
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STLAustin
Flaas
------- - -
Lab ID: 1007229
%Recoverv Flaas QC Recoverv Limits
106 77-117
90 62-143
101 87-113
Page 51 of 60
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
LCS for HBN 4881 [MSV/1137]
4881
4881
Lab ID:
Fiie ID:
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
C t IS on ro amoe
1007339
A0509002.D
Parameter Sok Amt Cone %Rec Fla
Acetone 20 15.9
Benzene 20 19.0
Bromobenzene 20 19.5
Bromochloromethane 20 23.2
Bromodichloromethane 20 19.8
Bromoform 20 18.9
Bromomethane 20 8.86
2-Butanone (MEK) 20 17.2
n-Butvlbenzene 20 20.0
sec-Butvlbenzene 20 20.0
tert-Butvlbenzene 20 19.3
Carbon disulfide 20 17.1
Carbon tetrachloride 20 21.3
Chlorobenzene 20 20.1
Chloroethane 20 17.9
Chloroform 20 21.6
Chloromethane 20 10.9
2-Chlorotoluene 20 19.5
4-Chlorotoluene 20 19.2
1 2-Dibromo-3-chloroorooane 20 18.6
Dibromochloromethane 20 19.7
1,2-Dibromoethane 20 19.7
Dibromomethane 20 19.6
I 4-Dichlorobenzene 20 18.8
SECTION V -Calibration and QC Information -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STL Austin
80
95
98
116
99 ~
95
44
86
100
100
97
86
106
100
89
108
54
98
96
93
98
99
98
94
Lab ID:
Fiie ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture: NA
MER Analyst:
c ontro IS ampe up:1ca e I D r t
1007340
A0509003.D
Cone %Rec Fla
15.3 77
18.4 92
19.2 96
22.5 113
19.2 96
19.4 97
8.69 43
16.2 81
19.7 98
19.9 100
19.0 95
18.1 90
21.0 105
19.7 99
17.0 85
20.8 104
10.5 52
19.1 95
19.l 96
18.8 94
20.4 102
19.4 97
18.8 94
18.5 92
QC Limits
RPO Fla %Rec RPO
3.8 0.1-240 71
3.2 71-133 17
2.1 67-127 12
2.6 61-145 21
3.1 57-135 19
2.1 23-151 17
2.3 34-128 25
6 O.l-214 39
2 28-184 30
0 45-160 31
2.1 65-148 27
4.5 29-223 23
0.9 46-150 23
1 77~129 14
4.6 39-133 27
3.8 64-146 16
3.8 18-140 26
3.1 70-136 24
0 74-132 23
I. I 39-171 25
4 45-137 15
2 19-187 19
4.2 52-138 21
2.2 70-132 13
Page 52 of 60
~------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Lab ID:
C t IS on ro f d amo econ mue
1007339
File ID: A0509002.D
Parameter SpkAmt Cone
I 2-Dichlorobenzene 20 19.6
1.3-Dichlorobenzene 20 18.9
Dichlorodifluoromethane 20 14.2
1 1-Dichloroethane 20 20.0
I 2-Dichloroethane 20 20.4
I 1-Dichloroethene 20 22.0
cis-1.2-Dichloroethene 20 21.I
trans-I 2-Dichloroethene 20 22.2
1,2-Dichloropropane 20 18.7
I 3-Dichloroorooane 20 18.8
2,2-Dichloropropane 20 24.2
I 1-Dichloroorooene 20 19.3
cis-1 3-Dichloropropene 20 18.3
trans-I 3-Dichloropropene 20 17.1
Ethylbenzene 20 19.8
Hexachloro-1,3-butadiene 20 26.8
2-Hexanone 20 16.6
lodomethane 20 21.4
lsoproovlbenzene 20 21.0
4-lsopropyltoluene 20 19.6
4-Methyl-2-pentanone (MIBK) 20 17.3
Methvlene chloride 20 20.5
Naphthalene 20 24.9
n-Proovlbenzene 20 19.7
Stvrene 20 19.9
I I I 2-Tetrachloroetharie 20 20.8
I I 2 2-Tetrachloroethane 20 19.4
Tetrachloroethene 20 21.7
Toluene 20 19. l
1.2 3-Trichlorobenzene 20 28.1
l 2.4-Trichlorobenzene 20 27.3
SECTION V -Calibration and QC Information -0512512000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
98
94
71
100
102
110
105
i 11
93
94
121
97
92
86
99
134
83
107
105
98
87
102
124
99
99
104
97
109
96
140
137
Lab ID:
File ID:
SpkAmt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
·20
20
20
20
20
20
20
20
20
20
C t IS on ro amp e up 1cate con mue I D I' f d
1007340
A0509003.D QC Limits
Cone %Rec Fla RPDFla %Rec RPO
19.5 97 I 67-135 14
18.2 91 3.2 68-134 14
13.6 68 4.3 0.1-166 26
19.3 97 3 66-138 19
19.6 98 4 48-152 23
21.3 107 2.8 47-175 25
20.2 101 3.9 66-144 18
21.2 106 4.6 62-146 22
18.3 91 2.2 -·· 61-133 17
18.7 93 I.I 70-128 16
23.0 115 5.1 40-168 30
18.5 92 5.3 71-155 31
18.2 91 I.I 36-142 16
17.1 85 1.2 34-138 21
19.4 97 2 75-131 14
25.7 128 4.6 46-150 34
16.3 82 1.2 -22-164 34
21.2 106 0.9 ·-
20.8 104 I 54-152 26
19.2 96 2.1 41-165 28
17. l 86 1.2 27-149 36
19.7 98 4 36-166 23
24.2 121 2.4 32-172 22
19.5 97 2 61-143 28
20.I 101 2 68-136 14
20.7 103 I 63-141 20
19.5 98 1 47-143 20
21.3 107 1.9 69-137 16
18.8 94 2.1 70-132 17
27.1 135 3.6 66-140 20
27.1 . 136 0.7 66-144 22
Page 53 of 60
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Control Samole continued
Lab ID: 1007339
File ID: A0509002.D
Parameter Sok Amt Cone
I I I-Trichloroethane 20 23.5
I I 2-Trichloroethane 20 19. J
Trichloroethene 20 21.8
Trichlorofluoromethane 20 23.6
1 2 3-Trichloroorooane 20 19.0
1.2 4-Trimethvlbenzene 20 18.8
1,3 5-Trimethvlbenzene 20 18.8
Vinvl acetate 20 7.87
Vinvl chloride 20 16.7
o-Xvlene/m-Xylene 40 39.7
o-Xvlene 20 20.l
SECTION V -Calibration and QC Information -05/25/2000 OJ :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
117
96
109
118
95
94
94
39
83
99
100
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
40
20
Control Samole Duolicate continued
1007340
A0509003.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
22.8 114 2.6 49-155 24
19.0 95 l 67-135 17
21.2 106 2.8 71-129 17
23.0 115 2.6 39-147 29
18.6 93 2.1 64-140 18
18.7 93 l.1 54-156 25
18.3 91 3.2 62-144 25
7.51 38 2.6 0.1-164 31
15.7 78 6.2 24-138 27
39.7 99 0 76-134 15
19.6 98 2 77-131 15
Page 54 of 60
-------------------
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Surroaate Comoounds
l-Bromo-4-fluorobenzene
1-2-Dichloroethane-d4
Toluene-d8
SECTION V -Calibration and QC Information -05/25/2000 01 :00
Lab ID: 1007339
%Recoverv
106
91
102
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
Lab ID: ~007340
Flans %Recoverv Fla as QC Recoverv Limits
106 77-117
89 62-143
103 87-113
Page 55 of 60
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 4862
Client Sample ID
INSTRUMENT OC
INSTRUMENT OC
LCS for HBN 4862 fMSV/11341
LCSD for HBN 4862 rMSV/11341
MB for HBN 4862 fMSV/11341
MB for HBN 4862 rMSV/11341 zzzzzzzzzz zzzzzzzzzz
TRIP BLANK2
0500HBWW213
0500HBWW2l4
0500HBWW215
0500HBWW227
0500HBWW228
0500HBWD999 zzzzzzzzzz
INSTRUMENT OC
INSTRUMENT QC zzzzzzzzzz zzzzzzzzzz
Extraction Batch ID: 4881
Client Samele ID
INSTRUMENT QC
INSTRUMENT OC
SECTION VI -Batch Summaries -05/25/2000 0 I :00
Lab Sample ID
1000
1406
1007228
1007229
1007230
1007231
2000420104
2000420601
2000505707
2000505701
2000505702
2000505703
2000505704
2000505705
2000505706
2000508130
1000
1406
2000420103
2000420102
Lab Sample ID
1000
1406
Start Dateffime:
Stop Dateffime:
SampleTvpe
GC/MS Tune
05/08/2000 15:08
05/09/2000 14:54
Matrix
Aaueous
Continuing Calibration Check Aaueous
Lab Control Sample Aaueous
Lab Control Samole Duolicate Aaueous
Method Blank Aaueous
Method Blank Aaueous
Field Samole Aaueous
Field Sample Aaueous
Field Samole Aaueous
Field Sample Aaueous
Field Samole Aaueous
Field Sample Aaueous
Field Sample Aqueous
Field Sample Aaueous
Field Samole Aaueous
Field Sample Aaueous
GC/MSTune Aaueous
Continuing Calibration Check Aaueous
Field Samole Aqueous
Field Sample Aaueous
Start Dateffime:
Stop Dateffime:
05/09/2000 16:49
05/10/2000 0I:17
SampleTvoe Matrix
GC/MS Tune Aqueous
Continuing Calibration Check Aaueous
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
Analyst: MER
Sample Size
Initial Final Preparation Method
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15mL SW8260B
15mL 15 mL SW8260B
15 mL 15 mL· SW8260B
15mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
Analyst: MER
Sample Size
Initial Final Preparation Method
15 mL 15mL SW8260B
15 mL 15mL SW8260B
Page 56 of 60
-------------------
-------------------SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 4881 continued
.
Client Sample ID Lab Sample ID
LCS for HBN 4881 fMSV/11371 1007339
LCSD for HBN 4881 rMSV/11371 1007340
MB for HBN 4881 fMSV/11371 1007341
LB for HBN 4881 rMSV/11371 1007342
zzzzzzzzzz 2000418605
zzzzzzzzzz 2000418606 zzzzzzzzzz 1007343 zzzzzzzzzz 1007344 zzzzzzzzzz 2000418607 zzzzzzzzzz 2000418608
0500HBWW215 2000505703
0500HBWW214 2000505702
0500HBWW213 2000505701
0500HBWW227 2000505704
0500HBWD999 2000505706
0500HBWW228 2000505705
zzzzzzzzzz 2000508711
zzzzzzzzzz 2000508710
SECTION VI -Batch Summaries -0512512000 0 I :00
Sample Type
Lab Control Sample
Lab Control Sample Duplicate
Method Blank
Leachate Blank
Field Sample
Field Sample
Matrix SPike
Matrix Spike Duplicate
Field Sample
Field Sample
Field Sample
Field Sample
Field Sample
Field Sample
Field Sample
Field Sample
Field Sample
Field Sample
LIMS Workorder: 756200.UA-Littie Washington, N °[20005057] Hamilton Beach-Proctor Silex
STL Austin
Sample Size
Matrix Initial Final Preparation Method
Aqueous 15mL 15mL SW8260B
Aqueous 15mL 15 mL SW8260B
Aaueous 15 mL 15 mL SW8260B
Leachate 15 mL 15 mL SW8260B
Leachate 15 mL 15 mL SW8260B
Leachate 15mL 15mL SW8260B·,.-
Leachate 15mL 15 mL SW8260B--
Leachate 15 mL 15 mL SW8260B
Leachate 15 mL 15 mL SW8260B
Leachate 15mL 15 mL SW8260B
Aqueous 15mL 15 mL SW8260B
Aqueous 15 mL 15 mL SW8260B
Aqueous 15 mL 15 mL· SW8260B
Aqueous 15mL 15mL SW8260B
Aqueous 15mL 15 mL SW8260B,
Aqueous 15mL 15 mL SW8260B--
Aqueous 15 mL 15 mL SW8260B
Aqueous 15mL 15mL SW8260B
Page 57 of 60
SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 4862
Seauence Client Samole ID
I INSTRUMENT QC
2 INSTRUMENT QC
3 LCS for HBN 4862 fMSV/11341
4 LCSD for HBN 4862 rMSV/11341
5 MB for HBN 4862 fMSV/11341
6 MB for HBN 4862 rMSV/11341
9 zzzzzzzzzz
11 zzzzzzzzzz
12 TRIPBLANK2
13 0500HBWW213
14 0500HBWW214
15 0500HBWW2 l 5
16 0500HBWW227
17 0500HBWW228
18 0500HBWD999
26 zzzzzzzzzz
27 INSTRUMENT QC
28 INSTRUMENT QC
29 zzzzzzzzzz
30 zzzzzzzzzz
Analysis Batch ID: 4881
Seauence Client Samele ID
I INSTRUMENT QC
2 INSTRUMENT QC
3 LCS for HBN 4881 fMSV/11371
4 LCSD for HBN 4881 rMSV/11371
SECTION VI -Batch Summaries -05/25/2000 0 I :00
Instrument ID: MSDA
Analvsis
Lab Samole ID Date Time
1000 05/08/2000 15:08:00
1406 05/08/2000 15:08:00
1007228 05/08/2000 16:22:00
1007229 05/08/2000 16:50:00
1007230 05/08/2000 17:18:00
1007231 05/08/2000 17:46:00
2000420104 05/08/2000 18:42:00
2000420601 05/08/2000 20:08:00
2000505707 05/08/2000 20:35:00
2000505701 05/08/2000 21 :03:00
2000505702 05/08/2000 21 :31 :00
2000505703 05/08/2000 21 :59:00
2000505704 05/08/2000 22:27:00
2000505705 05/08/2000 22:55:00
2000505706 05/08/2000 23:23:00
2000508130 05/09/2000 03:15:00
1000 05/09/2000 13:33:00
1406 05/09/2000 13:33:00
2000420103 05/09/2000 14:24:00
2000420102 05/09/2000 14:54:00
Instrument ID: MSDA
Analvsis
Lab Samole ID Date Time
1000 05/09/2000 16:49:00
1406 05/09/2000 16:49:00
1007339 05/09/2000 17:17:00
1007340 05/09/2000 17:45:00
LIMS Workordcr: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
Analyst: MER
SamoleTvoe Analvsis File ID Sub-Batch ID
GC/MSTune A0508002.D 0
Continuing Calibration Check A0508002.D 0
Lab Control Sample A0508003.D 0
Lab Control Samole Duolicate A0508004.D 0
Method Blank A0508005.D 0
Method Blank A0508006.D 0
Field Sample A0508008.D 0
Field Sample A05080l l.D 0
Field Sample A0508012.D 0
Field Samole A0508013.D 0
Field Sample A0508014.D 0
Field Sample A0508015.D 0
Field Sample A0508016.D 0
Field SamPle A0508017.D 0
Field Sample A0508018.D 0
Field Sample A0508026.D 0
GC/MS Tune A0508028.D 0
Continuing Calibration Check A0508028.D 0
Field Sample A0508029.D 0
Field Sample A0508030.D 0
Analyst: MER
SampleTvoe Analvsis File ID Sub-Batch ID
GC/MS Tune A0509001.D 0
Continuing Calibration Check A050900l.D 0
Lab Control Sample A0509002.D 0
Lab Control Sample Duolicate A0509003.D 0
Page 58 of 60
·------------------
-------------------SECTIONVI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 4881
Seauence Client Samele ID
continued
5 MB for HBN 4881 fMSV/11371
6 LB for HBN 4881 rMSV/I 1371
7 zzzzzzzzzz
8 zzzzzzzzzz
9 zzzzzzzzzz
10 zzzzzzzzzz
11 zzzzzzzzzz
12 zzzzzzzzzz
13 0500HBWW215
14 0500HBWW214
15 0500HBWW2 l 3
16 0500HBWW227
17 0500HBWD999
18 0500HBWW228
19 zzzzzzzzzz
20 zzzzzzzzzz
SECTION VI -Batch Summaries -05/25/2000 0 I :00
Lab Samele ID
1007341
1007342
2000418605
2000418606
1007343
1007344
2000418607
2000418608
2000505703
2000505702
2000505701
2000505704
2000505706
2000505705
2000508711
2000508710
LIMS Workorder: 756200.UA-Little Washington, N (20005057] Hamilton Beach-Proctor Silex
STLAustin
' "
Analvsis
Date Time SameleTvee Analvsis File ID Sub-Batch ID
05/09/2000 18:13:00 Method Blank A0509004.D 0
05/09/2000 18:41:00 Leachate Blank A0509005.D 0
05/09/2000 19:09:00 Field Samnle A0509006.D 0
05/09/2000 19:37:00 Field Samnle A0509007.D 0
05/09/2000 20:04:00 Matrix Snike A0509008.D 0
05/09/2000 20:32:00 Matrix Snike Dunlicate A0509009.D 0
05/09/2000 21:00:00 Field Samole A0509010.D " 0
05/09/2000 21:28:00 Field Samnle A0509011.D 0
05/09/2000 21:56:00 Field Samole A0509012.D 0
05/09/2000 22:24:00 Field Samnle A0509013.D 0
05/09/2000 22:54:00 Field Samole A0509014.D 0
05/09/2000 23:24:00 Field Samnle A0509015.D 0
05/09/2000 23:53:00 Field Samole A0509016.D 0
05/10/2000 00:21:00 Field Samnle A0509017.D 0
05/10/2000 00:49:00 Field Samole A0509018.D 0
05/10/2000 01:17:00 Field Samnle A0509019.D 0
Page 59 of 60
SECTION VII
Certifications
State/Aaencv
Arkansas Department of Pollution Control and Ecology
California Environmental Laboratorv Accreditation Program I Waste Water/Hazardous Waste
Kansas Department of Health and Environment I Solid and Hazardous Waste/Drinking Water
Louisiana Department of Environmental Quality, ELAP I Waste Water/Hazardous Waste/Air/Emissions
New Jersey Department of Environmental Protection
New York State Department of Health I Waste Water/Hazardous Waste
North Carolina Dept. of Natural Resources & Communitv Development I Waste Water
Oklahoma Water Resources Board I Waste Water
South Carolina Dept. of Health & Environmental Control
Utah Department of Health I Solid and Hazardous Waste
Wisconsin Department of Natural Resources
US Air Force/ AFCEE
US Army Corns of Engineers (ACE)
US Deoartment of Agriculture I Restricted Soils Permit
SECTION VII -Certifications -05/25/2000 0 I :00
LIMS Workorder: 756200.UA-Little Washington, N [20005057] Hamilton Beach-Proctor Silex
STLAustin
------ - -- - -
ID#
2257
E-10165
82005
10915
302
8720
82003002
RADC
999885260
Participating Laboratory
S-42350
Page 60 of 60
- ---- ---
SECTION I
Table of Contents
Section
I.
MS-VOA
II.
III.
IV.
v.
VI.
VII.
Form
Cover Page -Laboratory Analytical Report
Table of Contents . . . .
Report Sumnaries . . . . .
Workorder Surrmary
Protocol Surrmary
Corrments and Flag Definitions
Standard Flag Definitions .
Analyst Corrments . . . .
Sarrple Condition Corrments
Analytical Results . . . . . . . . .
SW8260B ........ .
Calibration and Quality Control Results
SW8260B . . . . . . . . . .
Batch Surrmaries .
SW8260B
Certifications . . .
Calibration Verification Results
Mass Spectrometer Tune
Method Blank Results
Control Sarrple Results
Extraction/Digestion Batch Surrmary
Analysis Batch Surrmary
Section I -Table of Contents -0513012000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
Page
i
. . 1
1
. . 1
1
3
• 3
. 3
• • 3
4
4
. 19
. . 19
19
. 23
. 24
. 28
32
32
. . 32
33
34
-------------------"
-------------------SECTION II
Report Summaries
MS-VOA
Client Name: Hamilton Beach-Proctor Silex Project Name: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
Client Code: HB-PS Facility Name: NC
Workorder Summary
Lab
Client Sample ID Sample ID Sample Matrix
0500HBWW226 2000505101 Aaueous
0500HBWW225 2000505i02 Aqueous
0500HBWW224 2000505103 Aqueous
0500HBWW234 2000505104 Aqueous
0500HBWW220 2000505105 Aqueous
0500HBWW216 2000505106 Aaueous
0500HBWW222 2000505107 Aqueous
0500HBWW230 2000505108 Aqueous
TRIP BLANK 2000505109 Aqueous
Protocol Summary
Lab Date&Time
Client Sample ID Sample ID Collected
Method: SW8260B
0500HBWW226 2000505101 05/02/00 11 :25
0500HBWW225 2000505102 05/02/00 12:25
0500HBWW224 2000505103 05/02/00 12:30
0500HBWW234 2000505104 05/02/00 12:55
SECTION II -Report Summaries -0513012000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STL Austiu
"·
Method Citation
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
Date & Time Prep
Received Batch ID
05103100 09:08 4837
05/03/00 09:08 4837
05103100 09:08 4837
05103100 09:08 4837
Method Descriotion
Volatiles by GC/MS
Volatiles by GC/MS
Volatiles by GC/MS
Volatiles bv GC/MS
Volatiles by GC/MS
Volatiles by GC/MS
Volatiles by GC/MS
Volatiles by GC/MS
Volatiles by GC/MS
Hold Time S1:>ec
Date& Time Analysis Date& Time Preo Analysis
Prepared Batch ID Analyzed Spec Actua Spec Actua
05104100 20:30 4837 05104100 20:30 7D 2D 7D 2D
05104/00 20:58 4837 05/04/00 20:58 7D 2D 7D 2D
05104100 21 :26 4837 05104100 21 :26 7D 2D 7D 2D
05104100 21 :54 4837 05104100 21 :54 7D 2D 7D 2D
Page I of 34
SECTION II
Report Summaries
MS-VOA
Protocol Summary continued -
Hold Time S >ec
Lab Date&Time Date& Time Prep Date&Time Analysis Date& Time Preo Analvsis
Client Samole ID Sample ID Collected Received Batch ID Prepared Batch ID Analyzed Soec Actua Soec Actual
Method· SW8260B continued -
0500HBWW220 2000505105 05/02/00 13: 10 05/03/00 09:08 4837 05/04/00 22:22 4837 05/04/00 22:22 7D 2D 7D 2D
0500HBWW216 2000505106 05/02/00 13:30 05103100 09:08 4837 05/04/00 22:50 4837 05104/00 22:50 7D 2D 7D 2D
0500HBWW222 2000505107 05/02/00 13:55 05/03/00 09:08 4837 05/04/00 23:18 4837 05104100 23:18 7D 2D 7D 2D
0500HBWW230 2000505108 05/02/00 14:20 05/03/00 09:08 4837 05/04/00 23:46 4837 05/04/00 23:46 7D 2D 7D 2D
TRIP BLANK 2000505109 05/02/00 00:00 05/03/00 09:08 4837 05105100 00: 13 4837 05105100 00:13 7D 3D 7D 3D
SECTION II -Report Summaries -05/30/2000 2 I: I 4
LIMS Workorder: 756200.UA-Little Washington, N [200050SI] Hamilton Beach-Proctor Silex
STLAustin Page 2 of 34
-------------------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/30/2000 21: 14
0500HBWW216
2000505106
Aaueous
Received
NA
05/02/2000 13:30
0510412000 22:50
05/04/2000 22:50
1.0000
MSDA
U!!/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N [l000505 I] Hamilton Beach-Proctor Silex
STLAustin
0500HBWW220 0500HBWW222
2000505105 2000505107
Aaueous Aaueous
Received Received
NA NA
05/02/2000 13: IO 05/02/2000 13:55
0510412000 22:22 05/04/2000 23: 18
05/04/2000 22:22 05/04/2000 23:18
1.0000 1.0000
MSDA MSDA
U!!/L ug/L
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.286 0.000 ND 0.286 0.000
0.000 ND 1.67 0.000 ND 1.67 0.000
0.000 ND 0.983 0.000 ND 0.983 0.000
0.000 ND 0.0901 0.000 ND 0.0901 0.000
0.000 ND 0.0492 0.000 ND 0.0492 0.000
0.000 ND 0.0622 0.000 ND 0.0622 0.000
0.000 ND 0.139 0.000 ND 0.139 0.000
0.000 ND 0.0683 0.000 ND 0.0683 0.000
0.000 ND 0.136 0.000 ND 0.136 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.179 0.000 ND 0.179 0.000
0.000 ND 0.0642 0.000 ND 0.0642 0.000
0.000 ND 0.0745 0.000 ND 0.0745 0.000
0.000 ND 0.0958 0.000 ND 0.0958 0.000
0.000 ND 0.0484 0.000 ND 0.0484 0.000
0.000 ND 0.0867 0.000 ND 0.0867 0.000
0.000 ND 0.0839 0.000 ND 0.0839 0.000
0.000 ND 0.0473 0.000 ND 0.0473 0.000
0.000 ND 0.0756 0.000 ND 0.0756 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
Page 4 of 34
·------------------
-·-- - - - - - - - - - - - - - - - -SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-4978
106-43-4
I .2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I .2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene I 10-57-6
I ,4-Dichlorobenzene 106-46-7
I .2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1 .2-Dichloroethane 107-06-2
I. 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I ,2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
I 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1 3-Dichlotoorooene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrylate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-I 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/30/2000 2 I: I 4
0500HBWW216
2000505106
Cone Flaa DL
ND 0.0821
ND 0. I I I
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
0.0706 J 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND 0.167
LIMS Workorder: 756200.UA-Little Washington, N [200050°5 I] Hamilton Beach-Proctor Silex
STLAustin
.,
'·
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW220 0500HBWW222
2000505105 2000505107
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.1 I I 0.000 ND 0. I 1 I 0.000
ND 0.113 0.000 ND 0. I 13 0.000
ND 0.0762 0.000 ND . 0.0762 0.000
ND 1.05 0.000 ND -1.05 0.000
ND 0.0564 0.000 ND ·--0.0564 0.000
ND 0.152 0.000 ND .. 0.152 0.000 .
ND 0.0939 0.000 ND 0.0939 0.000
ND 0.390 0.000 ND 0.390 0.000
ND 0.0587 0.000 ND 0.0587 0.000
ND 0.0920 0.000 ND 0.0920 0.000
ND 0.0591 0.000 ND 0.0591 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0487 0.000 0.338 J ~ 0.0487 0.000
ND 0.0499 0.000 ND -0.0499 0.000
0.153 J 0.0697 0.000 0.279 J 0.0697 0.000
ND 0.0603 0.000 ND 0.0603 0.000
ND 0.0813 0.000 ND 0.0813 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.0451 0.000 ND 0.0451 0.000
ND 0.0714 0.000 ND 0.0714 0.000
ND 0.0464 0.000 ND 0.0464 0.000
ND 0.0366 0.000 ND 0.0366 0.000
ND 0.0658 0.000 ND 0.0658 0.000
ND 0.0647 0.000 ND 0.0647 0.000
ND 0.0552 0.000 ND 0.0552 0.000
ND 0.212 0.000 ND 0.212 0.000
ND 0.167 0.000 ND 0.167 0.000
Page 5 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-Isopropyltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Propylbenzene 103-65-1
Stvrene 100-42-5
1 1 1,2-Tetrachloroethane 630-20-6
1 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
1,2 4-Trichlorobenzene 120-82-1
1.1 I-Trichloroethane 71-55-6
l, 1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorotluoromethane 75-69-4
1.2 3-Trichloroorooane 96-18-4
1 1,2-Trichlorotritluoroethane 76-13-1
I 2.4-Trimethvlbenzene 95-63-6
1 3,5-Trimethylbenzene 108-67-8
Vinyl acetate 108-05-4
Vinyl chloride . 75-01-4
SECTION IV -Analytical Results -05/30/200021:14
0500HBWW216
2000505106
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
ND 0.0845
ND 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND 0.467
ND 0.118
NO. 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
0500HBWW220 0500HBWW222
2000505105 2000505107
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0616 0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.000 ND 0.114 0.000 ND 0.114 0.000
0.000 0.441 J 0.0469 0.000 ND 0.0469 0.000
0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.000 ND 0.0796 0.000 ND 0.0796 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.688 0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000 ND 0.0792 0.000.
0.000 ND 0.0568 0.000 ND 0.0568 0.000
0.000 ND 0.402 0.000 ND 0.402 0.000
0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.000 ND 0.467 0.000 ND 0.467 0.000
0.000 ND 0.118 0.000 ND 0.118 0.000
0.000 ND 0.0331 0.000 ND 0.0331 0.000
0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.000 ND 0.0905 0.000 ND 0.0905 0.000
0.000 ND 0.208 0.000 ND 0.208 0.000
0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.000 ND 0.0766 0.000 ND 0.0766 0.000
0.000 ND 0.0749 0.000 ND 0.0749 0.000
0.000 ND 0.0436 0.000 ND 0.0436 0.000
0.000 ND 0.0438 0.000 ND 0.0438 0.000
0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page 6 of 34
... ·-- - - - - - - - - - - - - - - - -
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
n-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -0513012000 21: 14
0500HBWW216
2000505106
Cone Flaa DL
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005051 J Hamilton Beach-P.roctor Silex
STL Austin
RL
0.000
0.000
0500HBWW220 0500HBWW222
2000505105 2000505107
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND 0.0713 0.000 ND 0.0713 0.000
Page 7 of 34
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Surrogate Comoound
l-Bromo-4-fluorobenzene
1.2-Dichloroethane-d4
Toluene-dB
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -05/30/2000 2I:I4
0500HBWW216
2000505106
Aaueous
Received
NA
05/02/2000 13 :30
05/04/2000 22:50
05/04/2000 22:50
1.0000
MSDA
ug/L
% Recoverv Limits
100 77-117
101 61-143
103 87-113
LIMS Workorder: 756200.UA-Little Washington, N [2000505 I] Hamilton Beach-Proctor Silex
STL Austin
F
0500HBWW220 0500HBWW222
2000505105 2000505107
Aaueous Aaueous
Received Received
NA NA
05/02/2000 13: 10 05/02/2000 13:55
05/04/2000 22:22 0510412000 23: 18
05/04/2000 22:22 05/04/2000 23: 18
1.0000 1.0000
MSDA MSDA
ug/L ue:/L
% Recoverv Limits F % Recoverv Limits F
101 77-117 103 77-117
102 61-143 101 61-143
104 87-113 104 87-113
Page 8 of 34
·------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec.:Butvlbenzene
tert-Butv !benzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3 . 544-10-5
SECTION IV -Analytical Results -05/30/200021:14
0500HBWW224
2000505103
Aqueous
Received
NA
05/02/2000 12:30
0510412000 21 :26
0510412000 21 :26
1.0000
MSDA
ug/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
0.334 J 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
" l
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW225 0500HBWW226
2000505102 2000505101
Aqueous Aaueous
Received Received
NA NA
0510212000 12:25 0510212000 11 :25
0510412000 20:58 0510412000 20:30
05/04/2000 20:58 05/04/2000 20:30
1.0000 1.0000
MSDA MSDA
ug/L ug/L
Cone Flaa DL RL Cone Flaa DL RL
ND 0.286 0.000 ND 0.286 0.000
ND 1.67 0.000 ND 1.67 0.000
ND 0.983 0.000 ND 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 ND 0.0492 0.000
ND 0.0622 0.000 ND 0.0622 0.000
ND 0.139 0.000 ND -:-0.139 0.000
ND 0.0683 0.000 ND -0.0683 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.179 0.000 ND 0.179 0.000
ND 0.0642 0.000 ND 0.0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
ND 0.0484 0.000 ND 0.0484 0.000
ND 0.0867 0.000 ND 0.0867 0.000
ND 0.0839 0.000 ND 0.0839 0.000 -ND 0.0473 0.000 ND 0.0473 0.000
ND 0.0756 0.000 ND 0.0756 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
Page 9 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1,4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
I 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1,2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1,2-Dichloroprooane 78-87-5
1.3-Dichloroorooane 142-28-9
2,2-Dichloroprooane 594-20-7
l 1-Dichloroorooene 563-58-6
cis-1,3-Dichlorooropene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 J-butaaiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/30/2000 21 :14
0500HBWW224
2000505103
Cone Flag DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
0.292 J 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND 0.167
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STL Austin
0500HBWW225 0500HBWW226
2000505102 2000505101
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0821 0.000 ND 0.0821 0.000
0.000 ND 0.111 0.000 ND 0.111 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 0.0762 0.000 ND' 0.0762 0.000
0.000 ND 1.05 0.000 ND 1.05 0.000
0.000 ND 0.0564 0.000 ND 0.0564 0.000
0.000 ND 0.152 0.000 ND 0.152 0.000
0.000 ND 0.0939 0.000 ND 0.0939 0.000
0.000 ND 0.390 0.000 ND 0.390 0.000
0.000 ND 0.0587 0.000 ND 0.0587 0.000
0.000 ND 0.0920 0.000 ND 0.0920 0.000
0.000 ND 0.0591 0.000 ND 0.0591 0.000
0.000 ND 0.113 0.000 ND 0.113 0.000
0.000 ND 0.0487 0.000 ND 0.0487 0.000
0.000 ND 0.0499 0.000 ND 0.0499 0.000
0.000 ND 0.0697 0.000 0.115 J 0.0697 0.000
0.000 ND 0.0603 0.000 ND 0.0603 0.000
0.000 ND 0.0813 0.000 ND 0.0813 0.000
0.000 ND 0.0670 0.000 ND 0.0670 0.000
0.000 ND 0.0451 0.000 ND 0.0451 0.000
0.000 ND 0.0714 0.000 ND 0.0714 0.000
0.000 ND 0.0464 0.000 ND 0.0464 0.000
0.000 ND 0.0366 0.000 ND 0.0366 0.000
0.000 ND 0.0658 0.000 ND 0.0658 0.000
0.000 ND 0.0647 0.000 ND 0.0647 0.000
0.000 ND 0.0552 0.000 ND 0.0552 0.000
0.000 ND 0.212 0.000 ND 0.212 0.000
0.000 ND 0.167 0.000 ND 0.167 0.000
Page 10 of 34
-------------------
·-.. - - - -mm; - - - - - - - - - - - -SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample 10
Continued
Parameter CAS
Iodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methyl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1.1.1 2-Tetrachloroethane 630-20-6
l, 1,2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
1.2.4-Trichlorobenzene 120-82-1
1.1.1-Trichloroethane 71-55-6
l, 1,2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Tri ch lorofluoromethane 75-69-4
1 2 3-Trichloroorooane 96-18-4
1.1.2-Trichlorotrifluoroethane 76-13-1
1.2 4-Trimethvlbenzene 95-63-6
1,3.5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -05/30/20002I:14
0500HBWW224
2000505103
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
ND 0.0845
ND 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
0.0542 u 0.0680
ND 0.467
ND 0.118
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N (2000505 I] Hamilton Beach-Proctor Silex
STLAustiu
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
·o.ooo
0.000
0500HBWW225 0500HBWW226
2000505102 2000505101
Cone Flaa DL RL Cone Flaa DL RL
ND 0.0616 0.000 ND 0.0616 0.000
ND 0.0474 0.000 ND 0.0474 0.000
ND 0.0452 0.000 ND 0.0452 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0469 0.000 ND -0.0469 0.000
ND 0.0845 0.000 ND ··0.0845 0.000
ND 0.0796 0.000 ND 0.0796 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.688 0.000 ND 0.688 0.000
ND 0.0886 0.000 ND 0.0886 0.000
ND 0.0722 0.000 ND 0.0722 0.000
ND 0.0948 0.000 ND 0.0948 0.000
ND 0.0792 0.000 ND 0.0792 0.000
ND 0.0568 0.000 ND :· 0.0568 0.000
ND 0.402 0.000 ND . 0.402 0.000
ND 0.0680 0.000 ND 0.0680 0.000
ND 0.467 0.000 ND 0.467 0.000
ND 0.118 0.000 ND 0.118 0.000
ND 0.0331 0.000 ND 0.0331 0.000
ND 0.0952 0.000 ND 0.0952 0.000
ND 0.0905 0.000 ND 0.0905 0.000
ND 0.208 0.000 ND 0.208 0.000
ND .0.0543 0.000 ND 0.0543 0.000
ND 0.0766 0.000 ND 0.0766 0.000
ND 0.0749 0.000 ND 0.0749 0.000
ND 0.0436 0.000 ND 0.0436 0.000
ND 0.0438 0.000 ND 0.0438 0.000
ND 0.0574 0.000 ND 0.0574 0.000
Page 11 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -05/30/200021:14
0500HBWW224
2000505103
Cone Flaa DL
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0500HBWW225 0500HBWW226
2000505102 2000505101
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND 0.0713 0.000 ND 0.0713 0.000
Page 12 of 34
-------------------
--· - -.. - - --· - - - - - - - - - -SECTION IV
Analytical Results
SurrQgates
MS-VOA
SW8260B
Surrogate Compound
1-Bromo-4-fluorobenzene
l 2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -05/30/2000 21:14
0500HBWW224
2000505103
Aqueous
Received
NA
05/02/2000 12:30
05/04/2000 21 :26
05/04/2000 21 :26
1.0000
MSDA
ug/L
% Recoverv Limits
102 77-117
102 61-143
105 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
F
0500HBWW225 0500HBWW226
2000505102 2000505101
Aqueous Aqueous
Received Received
NA NA
05/02/2000 12:25 05/02/2000 11 :25
0510412000 20:58 0510412000 20:30
05/04/2000 20:58 05/04/2000 20:30
1.0000 1.0000
MSDA MSDA
ug/L ug/L
% Recoverv Limits F % Recoverv Limits F
102 77-117 101 77-117
102 61-143 100 61-143
102 87-113 103 87-113
Page 13 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butv !benzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units ·
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -05/30/200021:14
0500HBWW230
2000505108
AQueous
Received
NA
05/02/2000 14:20
05/04/2000 23:46
05/04/2000 23:46
1.0000
MSDA
ug/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW234 TRIP BLANK
2000505104 2000505109
AQueous Aaueous
Received Received
NA NA
05/02/2000 12:55 05/02/2000 00:00
05/04/2000 21 :54 05/05/2000 00: 13
05/04/2000 21 :54 05/05/2000 00: 13
l.0000 l.0000
MSDA MSDA
ug/L ug/L
Cone Flaa DL RL Cone Flaa DL RL
ND 0.286 0.000 ND 0.286 0.000 .
ND 1.67 0.000 ND 1.67 0.000
ND 0.983 0.000 ND 0.983 0.000
ND 0.0901 0.000 ND 0.0901 0.000
ND 0.0492 0.000 ND 0.0492 0.000
ND 0.0622 0.000 ND 0.0622 0.000
ND 0.139 0.000 ND 0.139 0.000
ND 0.0683 0.000 ND 0.0683 0.000
ND 0.136 0.000 ND 0.136 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.179 0.000 ND 0.179 0.000
ND 0.0642 0.000 ND 0.0642 0.000
ND 0.0745 0.000 ND 0.0745 0.000
ND 0.0958 0.000 ND 0.0958 0.000
ND 0.0484 0.000 0.538 J 0.0484 0.000
ND 0.0867 0.000 ND 0.0867 0.000
ND 0.0839 0.000 ND 0.0839 0.000
ND 0.0473 0.000 ND 0.0473 0.000
ND 0.0756 0.000 ND 0.0756 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.113 0.000 ND 0.113 0.000
Page 14 of 34
-·---~---~----------
----~--------------SECTION IV
Analytical Results
MS-VOA
SW8260B
.
Continued
Parameter
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Client Sample ID
Lab Sample ID
CAS
74-87-3
107-05-1
95-49-8
106-43-4
l .2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1,4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichloroditluoromethane 75-71-8
I, 1-Dichloroetliane 15-34-3
1.2-Dichloroethane 107-06-2
1, 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichloropropane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloropropane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1 3-Dichloropropene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethyl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -05/30/2000 21: 14
0500HBWW230
2000505108
Cone Flag DL
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND ·0.0591
ND 0.113
0.348 J 0.0487
ND 0.0499
0.593 0.0697
0.573 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND 0.167
LIMS Workordcr: 756200.UA-Little Washington, N (20005051] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0500HBWW234 TRIP BLANK
2000505104 2000505109
Cone Flag DL RL Cone Flaa DL RL
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0762 0.000 ND 0.0762 0.000
ND 1.05 0.000 ND . 1.05 0.000
ND 0.0564 0.000 ND ~ ... 0.0564 0.000
ND 0.152 0.000 ND ·--0.152 0.000
ND 0.0939 0.000 ND 0.0939 0.000
ND 0.390 0.000 ND 0.390 0.000
ND 0.0587 0.000 ND 0.0587 0.000
ND 0.0920 0.000 .ND 0.0920 0.000
ND 0.0591 0.000 ND 0.0591" 0.000
ND 0.113 0.000 ND 0.113 0.000
ND 0.0487 0.000 ND :c-0.0487 0.000
ND 0.0499 0.000 ND ·'-0.0499 0.000
0.145 J 0.0697 0.000 ND 0.0697 0.000
ND 0.0603 0.000 ND 0.0603 0.000
ND 0.0813 0.000 ND 0.0813 0.000
ND 0.0670 0.000 ND 0.0670 0.000
ND 0.0451 0.000 ND 0.0451 0.000
ND 0.0714 0.000 ND 0.0714 0.000
ND 0.0464 0.000 ND 0.0464 0.000
ND 0.0366 0.000 ND 0.0366 0.000
ND 0.0658 0.000. ND 0.0658 0.000
ND 0.0647 0.000 ND 0.0647 0.000
ND 0.0552 0.000 ND 0.0552 0.000
ND 0.212 0.000 ND 0.212 0.000
ND 0.167 0.000 ND 0.167 0.000
Page 15 of 34
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
lodomethane 74-88-4
Isoorooylbenzene 98-82-8
4-1 sopropy ltol uene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butyl ether (MTBE) 1634-04-4
4-MethYl-2-oentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-ProoYlbenzene 103-65-1
Styrene 100-42-5
I, I 1.2-Tetrachloroethane 630-20-6
1.1.2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
l 2,4-Trichlorobenzene 120-82-1
l l ."1-Trichloroethane 71-55-6
l l ,2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
l 2.3-Trichloroorooane 96-18-4
l l 2-Trichlorotrifluoroethane 76-13-1
1.2 4-Trimethylbenzene 95-63-6
1,3 5-Trimethylbenzene 108-67-8
Vinyl acetate 108-05-4
Vinvl chloride . 75-01-4
SECTION IV -Analytical Results -05/30/2000 21 :14
0500HBWW230
2000505108
Cone Flaa DL
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
ND 0.0845
ND 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
0.0826 J 0.0680
ND 0.467
ND 0.118
ND 0.0331
ND 0.0952
1.11 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
0500HBWW234 TRIP BLANK
2000505104 2000505109
RL Cone Flaa DL RL Cone Flaa DL RL
0.000 ND 0.0616 0.000 ND 0.0616 0.000
0.000 ND 0.0474 0.000 ND 0.0474 0.000
0.000 ND 0.0452 0.000 ND 0.0452 0.000
0.000 ND 0.114 0.000 ND 0.114 0.000
0.000 ND 0.0469 0.000 ND 0.0469 0.000
0.000 ND 0.0845 0.000 ND 0.0845 0.000
0.000 ND 0.0796 0.000 ND 0.0796 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.688 0.000 ND 0.688 0.000
0.000 ND 0.0886 0.000 ND 0.0886 0.000
0.000 ND 0.0722 0.000 ND 0.0722 0.000
0.000 ND 0.0948 0.000 ND 0.0948 0.000
0.000 ND 0.0792 0.000 ND 0.0792 0.000
0.000 ND 0.0568 0.000 ND 0.0568 0.000
0.000 ND 0.402 0.000 ND 0.402 0.000
0.000 ND 0.0680 0.000 ND 0.0680 0.000
0.000 ND 0.467 0.000 ND 0.467 0.000
0.000 ND 0.118 0.000 ND 0.118 0.000
0.000 ND 0.0331 0.000 ND 0.0331 0.000
0.000 ND 0.0952 0.000 ND 0.0952 0.000
0.000 ND 0.0905 0.000 ND 0.0905 0.000
0.000 ND 0.208 0.000 ND 0.208 0.000
0.000 ND 0.0543 0.000 ND 0.0543 0.000
0.000 ND 0.0766 0.000 ND 0.0766 0.000
0.000 ND 0.0749 0.000 ND 0.0749 0.000
0.000 ND 0.0436 0.000 ND 0.0436 0.000
0.000 ND 0.0438 0.000 ND 0.0438 0.000
0.000 ND 0.0574 0.000 ND 0.0574 0.000
Page 16 of 34
----~--------------
____ mm; _____________ _
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
n-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS
106-42-3
95-47-6
SECTION IV -Analytical Results -05/30/2000 21 :14
0500HBWW230
2000505108
Cone Flaa DL
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
RL
0.000
0.000
0500HBWW234 TRIP BLANK
2000505104 2000505109
Cone Flaa DL RL Cone Flaa DL RL
ND 0.137 0.000 ND 0.137 0.000
ND. 0.0713 0.000 ND 0.0713 0.000
Page 17 of 34
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW82608
Surrogate Compound
1-Bromo-4-fluorobenzene
I ,2-Dichloroethane-d4
Toluene-d8
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
SECTION IV -Analytical Results -05/30/2000 21:14
0500HBWW230
2000505108
Aaueous
Received
NA
05/02/2000 14:20
05/04/2000 23 :46
05/04/2000 23 :46
1.0000
MSDA
ug/L
% Recovery Limits
101 77-117
101 61-143
103 87-113
LIMS Workorder: 756200.UA-Little Washington, N (20005051] Hamilton Beach-Proctor Silex
STLAustin
.
F
0500HBWW234 TRIP BLANK
2000505104 2000505109
Aaueous Aaueous
Received Received
NA NA
05/02/2000 12:55 05/02/2000 00:00
05/04/2000 21 :54 05/05/2000 00: 13
05/04/2000 21 :54 05/05/2000 00: 13
1.0000 1.0000
MSDA MSDA
ug/L ug/L
% Recovery Limits F % Recovery Limits F
103 77-117 100 77-117
102 61-143 101 61-143
102 87-113 103 87-113
Page 18 of 34
----~--------------
- - -
_________ .. _____ _
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis.Batch ID: 4837 Instrument Data File: A0504002.D
Instrument ID: MSDA · Analyst: JEC
Parameter Reference Value Measured Cone Flaa
Acetone 20 16.9
Acetonitrile 100 77.7
Acrolein 100 61.4
Acrvlonitrile 20 16.5
Benzene 2.0 20.9
Brornobenzene 20 18.3
Brornochlorornethane 20 19.8
Brornodichlorornethane 20 16.7
Brornoform 20 11.4
Brom om ethane 20 20.9
2-Butanone (MEK) 20 19.6
n-Butylbenzene 20 25.8
sec-Butvlbenzene 20 24.8
tert-Butvlbenzene 20 23.6
Carbon disulfide 20 17.3
Carbon tetrachloride 20 19.8
2-Chloro-l 3-butadiene 20 25.2
Chlorobenzene 20 . 19.0
Chloroethane 20 24.0
Chloroform 20 23.4
1 -Chlorohexane 20 23.3
Chlorornethane 20 19.3
3-Chloropropene 20 18.9
2-Chlorotoluene 20 22.6
4-Chlorotoluene 20 21.3
I 2-Dibromo-3-chloroorooane 20 14.6
SECTION V -Calibration and QC Information -05/30/2000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
Dateffime Analyzed:05/04/2000 17:14
Units: ug/L
%Recoverv Flaa QC Limits %Recoverv
85
78
61
82
104
91
99
84
57
105
98
129
124
118
86
99
126
95
120
117 80-120
116
97
94
113
106
73
Page 19 of 34
SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4837 Instrument Data File: A0504002.D
Instrument ID: MSDA Analyst: JEC
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 13.7
1 2-Dibromoethane 20 15.1
Dibromomethane 20 15.8
trans-I .4-Dichloro-2-butene 20 12.3
1 4-Dichlorobenzene 20 19.0
1 2-Dichlorobenzene 20 18.7
I 3-Dichlorobenzene 20 19.4
Dichlorodifluoromethane 20 15.7
l l-Dichloroethane 20 25.5
1 2-Dichloroethane 20 20.3
1. l-Dichloroethene 20 23.6
cis-1 2-Dichloroethene 20 23.1
trans-l .2-Dichloroethene 20 23.8
1 2-Dichloroorooane 20 20.3
1.3-Dichloroorooane 20 16.3
2.2-Dichloroorooane 20 27.5
1.1-Dichloropropene 20 21.6
cis-l .3-Dichloroorooene 20 16. l
trans-I 3-Dichloropropene 20 14.4
Ethvl methacrvlate 20 16.4
Ethvlbenzene 20 20.4
Hexachloro-l .3-butadiene 20 27.0
2-Hexanone 20 15.6
Iodomethane 20 21.3
lsooroovlbenzene 20 21.5
4-lsooroov Ito luene 20 24.l
SECTION V -Calibration and QC Information -05/30/2000 21:14
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STL Austin
Flaa
Dateffime Analyzed:05/04/2000 17: 14
Units: ug/L
o/oRecoverv Flaa QC Limits o/oRecoverv
69
76
79
61
95
93
97
78
128
101
118 80-120
115
119
102 80-120
81
137
108
81
72
82
102 80-120
135
78
106
108
121
Page 20 of 34
-------------------
___ .. ___ _ ----------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 4837 Instrument Data File: A0504002.D
Instrument ID: MSDA Analyst: JEC
Continued
Parameter Reference Value Measured Cone
Methyl methacrvlate 20 15.5
Methyl tert-butvl ether (MTBE) 20 17.5
4-Methyl-2-pentanone (MIBK) 20 16.2
Methylene chloride 20 20.2
Naphthalene 20 18.5
Prooanenitrile 100 82.3
n-Propylbenzene 20 23.9
Stvrene 20 18.9
1, l, 1,2-Tetrachloroethane 20 17.8
1.1.2.2-Tetrachloroethane 20 . I6.0
Tetrachloroethene 20 I 9.4
Tetrahydrofuran 20 I7.4
Toluene 20 20.0
I .2.3-Trichlorobenzene 20 18.9
1,2,4-Trichlorobenzene 20 21.8
I. I I -Trichloroethane 20 25.2
1 1.2-Trichloroethane 20 I5.9
Trichloroethene 20 21.4
Trichlorofluoromethane 20 25.2
I 2,3-Trichloropropane 20 I5.4
I I .2-Trichlorotrifluoroethane 20 26.3
I 2,4-Trimethylbenzene 20 22.8
I 3.5-Trimethylbenzene 20 22.8
Vinyl acetate 20 I9.8
Vinyl chloride 20 21.3
p-Xylene/m-Xylene 40 42.I
SECTION V -Calibration and QC Information -0513012000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N (20005051] Hamilton Beach-Proctor Silex
STLAustin
Flaa
Date/Time Analyzed:05/04/2000 17: 14
Units: ug/L
%Recoverv Flaa QC Limits %Recovery
78
88
81
101
93
82
120
94
89
80
97
87
100 80-I20
94
I09
126
79
I07
I26
77
13 I
II4
Il4
99
I06 80-I20
105
Page 21
- -
of 34
-------------------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW82608
BFB
Analysis B!!tch ID: 4837
Instrument ID: MSDA
Mass/Enerav
50
75
95
96
173
174
175
176
177
Instrument Data File: A0504002.D
Injection Time: 05/04/2000 17:14
Ion Abundance Criteria
Lower Limit Unner Limit
15 40
30 60
100 100
5 9
0 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC Information -05/30/2000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
" '·
Date Analyzed: 05/04/2000 17: 14
An.alyst: JEC
% Relative Abundance
28.6
46.9
100
6.1
0
61.9
7.3
96.5
6.9
Page 23 of 34
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrv lonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Chloromethane
3-Chloropropene
2-Chlorotoluene
4-Chlorotoluene
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
95-49-8
106-43-4
SECTION V -Calibration and QC Information -05/30/2000 21 :14
1007150
Method Blank
Aaueous
0510412000 18:38
05/04/2000 18:38
MSDA
ue:/L
Cone Flaa DL
ND 0.286
ND 1.67
ND 0.983
ND 0.0901
ND 0.0492
ND 0.0622
ND 0.139
ND 0.0683
ND 0.136
ND 0.106
ND 0.179
ND 0.0642
ND 0.0745
ND 0.0958
ND 0.0484
ND 0.0867
ND 0.0839
ND 0.0473
ND 0.0756
ND 0.0670
ND 0.113
ND 0.0821
ND 0.111
ND 0.113
ND 0.0762
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STL Austin
RL Cone Flaa DL · RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000 .
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 24 of 34
-------------------
-------------------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromoch1oromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1,4-Dichlorobenzene 106-46-7
I 2-Dichlorobenzene 95-50-1
1,3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
1 2-bichloroethane 107-06-2
I 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1,2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1,3-Dichloropronane 142-28-9
2.2-Dichloroorooane 594-20-7
l, 1-Dichloropropene 563-58-6
cis-1 3-Dichloroorooene 10061-01-5
trans-1.3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
Iodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isopropvltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
SECTION V -Calibration and QC Information -0513012000 21:14
1007150
Cone Flaa DL
ND 1.05
ND 0.0564
ND 0.152
ND 0.0939
ND 0.390
ND 0.0587
ND 0.0920
ND 0.0591
ND 0.113
ND 0.0487
ND 0.0499
ND 0.0697
ND 0.0603
ND 0.0813
ND 0.0670
ND 0.0451
ND 0.0714
ND 0.0464
ND 0.0366
ND 0.0658
ND 0.0647
ND 0.0552
ND 0.212
ND 0.167
ND 0.0616
ND 0.0474
ND 0.0452
ND 0.114
ND 0.0469
LIMS Workorder: 756200.UA-Little Washington, N (20005051] Hamilton Beach-Proctor Silex
STLAustin
,
"
RL Cone Flag DL RL Cone Flag DL RL
0.000
0.000
0.000
0.000
0.000
0.000 -·-
0.000 --
0.000 -
0.000
0.000
0.000
0.000
0.000
0.000
0.000 --
0.000 -
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 25 of 34
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
4-Methvl-2-oentanone (MIBK) 108-10-I
Methylene chloride 75-09-2
Naohthalene 9I-20-3
Propanenitrile 107-I2-0
n-Proovlbenzene I03-65-1
Styrene I00-42-5
I. I I 2-Tetrachloroethane 630-20-6
I. I 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene I27-I8-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-61-6
I ,2,4-Trichlorobenzene 120-82-1
I 1.1-Trichloroethane 71-55-6
l l ,2-Trichloroethane 79-00-5
Trichloroethene 79-0I-6
Trichlorofluoromethane 75-69-4
l 2.3-Trichloroorooane 96-18-4
1 I ,2-Trichlorotrifluoroethane 76-I3-l
I 2.4-Trimethvlbenzene 95-63-6
I 3 5-Trimethylbenzene 108-67-8
Vinvl acetate I08-05-4
Vinyl chloride 75-0I-4
o-Xvlene/m-Xvlene 106-42-3
o-Xvlene 95-47-6
SECTION V -Calibration and QC Information -05/30/2000 21:14
1007I50
Cone Flaa DL
ND 0.0845
O.I64 J 0.0796
ND 0.106
ND 0.688
ND 0.0886
ND 0.0722
ND 0.0948
ND 0.0792
ND 0.0568
ND 0.402
ND 0.0680
ND 0.467
ND O. I 18
ND 0.0331
ND 0.0952
ND 0.0905
ND 0.208
ND 0.0543
ND 0.0766
ND 0.0749
ND 0.0436
ND 0.0438
ND 0.0574
ND 0.137
ND 0.0713
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
RL Cone Flaa DL RL Cone Flaa DL RL
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Page 26 of 34
------·-----------·--
-------------------SECTION V
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Surronate Compound
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
SECTION V -Calibration and QC Information -05/30/2000 21:14
1007150
Method Blank
Aqueous
05/04/2000 18:38
05/04/2000 18:38
MSDA
ug/L
% Recoverv Limits
102 77-117
102 61-143
103 87-113
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
F % Recoverv .Limits F % Recoverv Limits F
~
L-"
Page 27 of 34
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
LCS for HBN 4837 [MSV/1133)
4837
4837
Instrument ID:
Units:
Matrix:
MSDA
ug/L
Aqueous
Control Samole
Lab ID: 1007148
File ID: A0504003.D
Parameter Sok Amt Cone
Acetone 20 21.3
Benzene 20 19.8
Bromobenzene 20 18.4
Bromochloromethane 20 21.4
Bromodichloromethane 20 18.7
Bromoform 20 13.5
Brom om ethane 20 19.6
2-Butanone (MEK) 20 22.5
n-Butvlbenzene 20 22.7
sec-Butvlbenzene 20 21.9
tert-Butv !benzene 20 20.3
Carbon disulfide 20 14.9
Carbon tetrachloride 20 19.1
Chlorobenzene 20 17.5
Chloroethane 20 19.9
Chloroform 20 21.8
Chloromethane 20 15.4
2-Chlorotoluene 20 19.9
4-Chlorotoluene 20 20.0
1.2-Dibromo-3-chloroorooane 20 17.2
Dibromochloromethane 20 15.6
1 2-Dibromoethane 20 17.6
Dibromomethane 20 19.0
I 4-Dichlorobenzene 20 17.8
SECTION V -Calibration and QC Information -05/30/2000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
106
99
92
107
93
67
98
113
113
110
101
74
95
87
100
109
77
99
100
86
78
88
95
89
Lab ID:
File ID:
Sok Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture: NA
JEC Analyst:
Control Sample Duolicate
1007149
A0504004.D
Cone %Rec Fla
22.3 112
20.9 104
19.4 97
22.8 114
20.9 104
16.6 83
20.7 103
25.4 127
23.2 116
22.8 114
20.8 104
18.2 91
21.1 105
18.9 94
21.2 ' 106
23.4 117
16.l 80
20.9 105
20.5 103
17.9 89
18.3 91
18.5 93
20.4 102
18.9 94
QC Limits
RPO Fla %Rec RPO
5.5 0.1-240 71
4.9 71-133 17
5.3 67-127 12
6.3 61-145 21
11 57-135 19
21 0 23-151 17
5 34-128 25
12 0.1-214 39
2.6 28-184 30
3.6 45-160 31
2.9 65-148 27
21 29-223 23
10 46-150 23
7.7 77-129 14
5.8 39-133 27
7.1 64-146 16
3.8 18-140 26
5.9 70-136 24
3 74-132 23
3.4 39-171 25
15 45-137 15
5.5 19-187 19
7.1. 52-138 21
5.5 70-132 13
Page 28 of 34
------~------------
--------~---------­SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW82608
Lab ID:
C t IS on ro f d amo. econ mue
1007148
File ID: A0504003.D
Parameter $pk Amt Cone
1 2-Dichlorobenzene 20 18.4
1 3-Dichlorobenzene 20 18.4
Dichlorodifluoromethane 20 13.8
I I-Dichioroethane 20 22.8
I 2-Dichloroethane 20 22.2
I I-Dichloroethene 20 22.0
cis-I .2-Dichloroethene 20 20.7
trans-I 2-Dichloroetherie 20 21.8
1.2-Dichloroorooane 20 20.7
1.3-Dichloroorooane 20 I 8. I
2,2-Dichloropropane 20 24.0
I .1-Dichloroorooene 20 20.3
cis-I ,3-Dichloropropene 20 I 7.3
trans-I 3-Dichloroorooene 20 I5.0
Ethylbenzene 20 I 8.1
Hexachloro-1.3-butadiene 20 23.4
2-Hexanone 20 19.9
Iodomethane 20 I9. I
Isopropylbenzene 20 I8.8
4-Isooroovltoluene 20 20.4
4-Methvl-2-oentanone (MIBK) 20 22.4
Methvlene chloride 20 20.6
Naphthalene .. 20 22.9
n-Proovlbenzene 20 20.6
Stvrene 20 17.8
I, I 1 2-Tetrachloroethane 20 17.3
I. I 2 2-Tetrachloroethane 20 I8.7
Tetrachloroethene 20 I7.4
Toluene 20 I7.7
I ,2 3-Trichlorobenzene 20 23.I
I .2 4-Trichlorobenzene -20 23.3
SECTION V -Calibration and QC Information -0513012000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
92
92
69
114
I 11
110
I03
I09
103
9I
120
IOI
86
75
90
l I7
IOO
95
94
102
112
103
115
103
89
87
94
87
89
I15
117
Lab ID:
File ID:
SpkAmt
20
20
20
20
20
20
20.
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
C t IS on ro amoe uo 1ca e con mue I D r t f d
1007149
A0504004.D QC Limits
Cone %Rec Fla RPO Fla %Rec RPO
19.3 97 5.3 67-135 14
18.9 95 3.2 68-134 14
14.8 74 7 0.1-166 26
24.2 121 6 66-138 I9
23.5 117 5.3 48-152 23
23.I 116 5.3 47-I75 25
22.4 II2 8.4 66-144 18
23.3 I17 7.1 . 62-146 22
22.4 112 8.4 . . 61-133 17
19.l 96 5.3 70-128 16
24.9 124 3.3 40-I68 30
21.1 105 3.9 7I-155 3I
20.4 I02 I7 0 36-I42 16
I7.8 89 I7 34-I38 2I
I9.I 96 6.5 75-131 14
24.3 121 3.4 46-150 34
20.2 101 I ~ 22-164 34
I8.6 93 2. I ··.
20.I lOI 7.2 54-I52 26
21.2 106 3.8 4 I-165 28
22.0 I 10 1.8 27-149 36
21.9 110 6.6 36-I66 23
24.6 123 6.7 32-I72 22
21.8 109 5.7 6I-I43 28
19.1 95 6.5 68-136 14
18.8 94 7.7 63-141 20
20.0 100 6.2 47-143 20
I 8.3 9I 4.5 . 69-137 16
18.9 94 5.5 70-132 I7
24.8 124 7.5 66-140 20
25.3 127 8.2 66-I44 22
Page 29 of 34
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B c ontrol Samnle continue
Lab ID: 1007148
File ID: A0504003.D
Parameter Sok Amt Cone
1 I I -Trichloroethane 20 22.I
1 I 2-Trichloroethane 20 17.4
Trichloroethene 20 20.0
Trichlorofluoromethane 20 20.9
I 2 3-Trichlorooronane 20 18.7
I 2 4-Trimethvlbenzene 20 20.1
I 3 5-Trimethylbenzene 20 20.1
Vinvl acetate 20 11.0
Vinyl chloride 20 18.4
n-Xvlene/m-Xvlene 40 36.5
o-Xvlene 20 17.8
SECTION V -Calibration and QC lnfonnation -05130120002I:14
LIMS Workorder: 756200.UA-Little Washington, N (2000505 I] Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
110
87
100
104
93
100
101
55
92
91
89
d Control Sample Duplicate continued
Lab ID: 1007149
File ID: A0504004.D QC Limits
Sok Amt Cone %Rec Fla RPO Fla %Rec RPO
20 23.3 117 6.2 49-155 24
20 18.7 93 6.7 67-135 17
20 21.0 105 4.9 71-129 17
20 22.5 113 8.3 39-147 29
20 19.6 98 5.2 64-140 18
20 20.6 103 3 54-156 25
20 21.0 105. 3.9 62-144 25
20 10.7 54 1.8 0.1-164 31
20 19.7 98 6.3 24-138 27
40 38.8 97 6.4 76-134 15
20 19.2 96 7.6 77-131 15
Page 30 of 34
'1111!11 - - - - - - - - - - - - - - - - - -
-------------------SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Surroaate Comoounds
l-Bromo-4-tluorobenzene
l .2-Dichloroethane-d4
Toluene-d8
SECTION V -Calibration and QC Information -05/30/200021:14
Lab ID: 1007148
%Recovery
100
97
104
LIMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STLAustin
~ I.
Lab ID: 1007149
Flags %Recovery Flaas QC Recoverv Limits
100 77-117
100 61-143
104 87-113
Page 31 of 34
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 4837
Client Samole ID
INSTRUMENT QC
INSTRUMENT QC
LCS for HBN 4837 rMSV/11331
LCSD for HBN 4837fMSV/11331
MB for HBN 4837 rMSV/11331 zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz
0500HBWW226
0500HBWW225
0500HBWW224
0500HBWW234
0500HBWW220
0500HBWW216
0500HBWW222
0500HBWW230
TRIP BLANK
zzzzzzzzzz
zzzzzzzzzz
zzzzzzzzzz
zzzzzzzzzz
zzzzzzzzzz
zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz zzzzzzzzzz
SECTION VI -Batch Summaries -05/30/200021:14
Lab Samole ID
1000
1406
1007148
1007149
1007150
2000422411
1007151
1007152
2000505101
2000505102
2000505103
2000505104
2000505105
2000505106
2000505107
2000505108
2000505109
2000422402
2000422403
2000422404
2000422405
2000422406
2000422407
2000422408
2000422409
2000422410
2000422401
Start Dateffime:
Stop Dateffime:
0510412000 17: 14
0510512000 04:54
SamoleTvoe Matrix
GC/MS Tune AQueous
Continuin2 Calibration Check Aaueous
Lab Control Sample AQueous
Lab Control Sample Duplicate AQueous
Method Blank AQueous
Field Sample AQueous
Matrix Soike AQueous
Matrix Spike Duplicate AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Samnle AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
Field Sample AQueous
LIMS Workorder: 756200.UA-Little Washington, N (200050Sl] Hamilton Beach-Proctor Silex
STLAustin
Analyst: JEC
SamoleSize
Initial Final Preoaration Method
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15mL 15 mL SW8260B
15mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15mL l5mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15mL SW8260B
15mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15 mL 15 mL SW8260B
Page 32 of 34
-------------------
- - - - ----- - - - - - - - - - - -SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 4837 Instrument ID: MSDA
Sequence Client Sample ID Lab Samole ID
1 INSTRUMENT OC !000
2 INSTRUMENT QC I406
3 .LCS for HBN 4837 fMSV/11331 1007148
4 LCSD for HBN 4837 fMSV/11331 !007149
5 MB for HBN 4837 fMSV/11331 !007150
6 zzzzzzzzzz 2000422411
7 zzzzzzzzzz !007151
8 zzzzzzzzzz !007152
9 0500HBWW226 2000505101
10 0500HBWW225 2000505102
I 1 0500HBWW224 2000505103
12 0500HBWW234 2000505104
13 0500HBWW220 2000505105
14 0500HBWW2 l 6 2000505!06
15 0500HBWW222 2000505107
16 0500HBWW230 2000505108
17 TRIP BLANK 2000505109
18 zzzzzzzzzz 2000422402
19 zzzzzzzzzz 2000422403
20 zzzzzzzzzz 2000422404
21 zzzzzzzzzz 2000422405
22 zzzzzzzzzz 2000422406
23 zzzzzzzzzz 2000422407
24 zzzzzzzzzz 2000422408
25 zzzzzzzzzz 2000422409
26 zzzzzzzzzz 2000422410
27 zzzzzzzzzz 2000422401
SECTION VI -Batch Summaries -0513012000 21: I4
I.IMS Workorder: 756200.UA-Little Washington, N [20005051] Hamilton Beach-Proctor Silex
STL Austin
, '
Analvsis
Date Time
05/04/2000 17:14:00
05/04/2000 17:14:00
05/04/2000 17:42:00
05/04/2000 18:10:00
05/04/2000 18:38:00
05/04/2000 19:06:00
05/04/2000 19:34:00
05/04/2000 20:02:00
05/04/2000 20:30:00
05/04/2000 20:58:00
05/04/2000 21:26:00
05/04/2000 21:54:00
05/04/2000 22:22:00
05/04/2000 22:50:00
05/04/2000 23:18:00
05/04/2000 23:46:00
05/05/2000 00:13:00
05/05/2000 00:41:00
05/05/2000 01:09:00
05/05/2000 01:37:00
05/05/2000 02:05:00
05/05/2000 02:33:00
05/05/2000 03:01:00
05/05/2000 03:29:00
05/05/2000 03:57:00
05/05/2000 04:25:00
0510512000 04:54:00
Analyst: JEC
SamoleTvoe Analvsis File ID Sub-Batch ID
GC/MSTune A0504002.D 0
Continuing Calibration Check A0504002.D 0
Lab Control Sample A0504003.D 0
Lab Control Samole Duolicate A0504004.D 0
Method Blank A0504005.D 0
Field Samole A0504006.D . 0
Matrix Spike A0504007.D 0
Matrix Spike Duplicate A0504008.D 0
Field Samole A0504009.D 0
Field Sample A0504010.D 0
Field Samole A050401 l.D 0
Field Sample A0504012.D 0
Field Samole A0504013.D. 0
Field Sample A0504014.D 0
Field Samole A0504015.D 0
Field Sample A0504016.D 0
" Field Samole A0504017.D 0
Field Sample A0504018.D 0
Field Sample A0504019.D 0
Field Samole A0504020.D 0
Field Sample A0504021.D 0
Field Samole A0504022.D 0
Field Sample A0504023.D 0
Field Sample A0504024.D 0
Field Sample A0504025.D 0
Field Samole A0504026.D 0
Field Sample A0504027.D 0
Page 33 of 34
SECTION VII ,
Certifications
State/Aaencv
Arkansas Department of Pollution Control and Ecolo!!v
California Environmental Laboratorv Accreditation Program I Waste Water/Hazardous Waste
Kansas Department of Health and Environment I Solid and Hazardous Waste/Drinking Water
ID#
2257
E-10165
Louisiana Deoartment of Environmental Quality ELAP I Waste Water/Hazardous Waste/Air/Emissions
New Jersey Department of Environmental Protection
New York State Department of Health I Waste Water/Hazardous Waste
North Carolina Dept. of Natural Resources & Community Development I Waste Water
Oklahoma Water Resources Board I Waste Water
South Carolina Dept. of Health & Environmental Control
Utah Department of Health I Solid and Hazardous Waste
Wisconsin Department of Natural Resources
US Air Force/AFCEE
US Armv Coros of Engineers (ACE)
US Department of Agriculture I Restricted Soils Permit
SECTION Vil -Certifications -05/30/2000 21: 14
LIMS Workorder: 756200.UA-Little Washington, N [20005051) Hamilton Beach-Proctor Silex
STL Austin
-- ----- - -
82005
10915
302
8720
82003002
RADC
999885260
Participating Laboratorv
S-42350
-- -- -
Page 34 of 34 - ----
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APPENDIXB
CONTAMINANT CONCENTRATIONS VERSUS TIME
-------------------
1000
900
800
·~
-
700
-..J -600 C> ::s -c 0 ;; 500 ca ... -c Cl)
(.) c 400 0 -
0
300 -
200
100
0
Nov-98
MW-213
~
~
Feb-99 May-99
~
Aug-99
Sample Date
Dec-99
~ ...
---
" "' "7'
Mar-00 Jun-00
-+-1, 1-Dichloroethene
-Tetrachloroethene
_....._ Trichloroethene
~Vinyl chloride
'•
200,000
180,000
160,000
jr--------___
140,000 -
:::J -120,000 C> -
:I -c 0 +:; 100,000 I! IL -c Q)
(,) c 80,000 0 -
0
60,000
40,000
20,000
0
·Nov-98 Feb-99 May-99
MW-228
~
Aug-99
Sample Date
Dec-99
~
"-.
--.. ..
Mar-00 Jun-00
_._ 1, 1-Dichloroethane
--1. 1-Dichloroethene
--ats--1, 1, 1-Trichloroethane
-*-Trichloroethene
-------------------
-...J -C) ::s -c 0 ~ -c Q)
(.) c
0 0
MW-228
0-t--.....-.....-.....-.....--,.........-.....-.....-.....--,-.....-.....-.....-.....---,.....-.....-.....-.....-.....-.....-.....-.....-.....-.....-.....-.....-.....-.....-.....-~
Nov-98 Feb-99 May-99 Aug-99
Sample Date
Dec-99 Mar-00 Jun-00
l-+-1, 1,2,2-Tetrachloroethane I
-------------------
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