IDX GW Monitoring Rpt February 2001 (SF)-OCR

. *5981HSSF1066*
1111111111111111111111111111
DocumentlD NONCD0001814
Site Name HAMILTON BEACH/PROCTOR SILEX
oocumentType Progress/Monitoring Rpt {PRGMON)
RptSegment 1
DocDate
DocRcvd
Box
Access level
Division
Section
Program
DocCat
4/9/2001
2/20/2007
SF1066
PUBLIC
WASTE MANAGEMENT
SUPERFUND
IHS (IHS)
FACILITY
State of North Carolina
Department of Environment
and Natural Resources
Wasf.ington Regional Qffice
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Mr. Mario Kuhar
DIVISION OF WATER QUALITY
GROUNDWATER SECTION
April 9, 2001
Hamilton Beach<> Proctor-Silex, Inc.
442 Waterfront Drive
Glen Allen, Virginia 23060
RE: Quarterly Groundwater Sampling
Hamilton Beach<> Proctor-Silex, Inc.
Washington, Beaufort County, North Carol~na
Groundwater Incident Number -#14338
Dear Mr. Kuhar:
~A _•;~~ nm-~-----MCDEMR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
The Washington Regional Office received the above report, prepared by Radian
International, dated April 2001. We appreciate you submitting this report to our office.
Please continue to monitor groundwater quality until four consecutive quarterly monitoring
events reveal contaminant levels below the groundwater standards listed in Title 15A North Carolina
Administrative Code, Subchapter 2L (ISA NCAC 2L).
We appreciate your cooperation along with your effort to protect the state's groundwater
resources. Should you have any questions regarding this matter, please don't hesitate to call me at
252-946-6481, extension# 354.
Sincerely,
Michelle Volosin
Groundwater Section
cc: Radian International-Post Office Box 13000, Research Triangle Park, North Carolina 27709
WaRO
943 Washington Square Mall, Washington, North Carolina 27889 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer
April 4, 2001
Mr. Willie Hardison
North Carolina Department of Environment
and Natural Resources
934 Washington Square Mall
Washington, North Carolina 27889
RE: Groundwater Monitoring Report for February 2001
Groundwater Incident No. 14338
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Dear Mr. Hardison:
Mailing Address:
Post Office Box 13000
Research Triangle Park,
North Carolina 27709
Physical/ Shipping Address:
1600 Perimeter Park Drive
Morrisville, North Carolina 27560
919 461 1100 Tel
919 461 1415 Fax
APR - 5 2001
On behalf of Hamilton BeachOProctor-Silex, Inc., Radian International is submitting one
copy of the referenced report.
If you have any questions, please contact Mario Kuhar at [phone]
Sincerely,
RADIAN INTERNATIONAL
c52JL~
Craig L. Kennedy, L.G.
Geologist
CK: la.cvr _!tr.doc
Enclosure
\
cc: Mario Kuhar, Hamilton BeachOProctor-Silex
Bradford A. De Vore, Womble Carlyle Sandridge & Rice
Project File
Engineering Services in North Carolina are performed through Radian lntemational's wholly owned subsidiary, Radian Engineering, Inc.
Offices Worldwide
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1.
GROUNDWATER MONITORING REPORT
FOR FEBRUARY 2001
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
Prepared for:
Hamilton Beach<>Proctor-Silex, Inc.
4421 Waterfront Drove
Glen Allen, Virginia 23060
Prepared by:
Radian International
P.O. Box 13000
Research Triangle Park, North Carolina 27709
April2001
1 • · · APR -5 2001 __ 11 '
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CERTIFICATION PAGE
GROUNDWATER MONITORING REPORT
FOR FEBRUARY 2001
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater Incident No. 14338
Site Priority Ranking B
I, Craig L. Kennedy, a Licensed Geologist in the State of North Carolina, certify that
this report and its contents have been prepared under my direct control and personal
superv1s10n.
80396907.01 FebOl_GWRpt.doc (4/2/01) 11
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TABLE OF CONTENTS
Certification Page ................................................................................................................ ii
List of Figures .................................................................................................................... iv
List of Tables .................................................................................................................... vi
1.0 INTRODUCTION ........................................................................................................... 1-1
2.0 FIELD METHODS .......................................................................................................... 2-1
3.0 RESULTS ........................................................................................................................ 3-1
3 .1 Water Level Measurements ................................................... .' ............................. 3-1
3.2 Analytical Results ................................................................................................ 3-1
APPENDIX A GROUNDWATER SAMPLING ANALYTICAL REPORTS
APPENDIX B CONTAMINANT CONCENTRATIONS VERSUS TIME
80396907.01 FebOl_GWRpt.doc (4/2/01) 111
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LIST OF FIGURES
1-1 Topographic Map, Hamilton BeachOProctor-Silex, Inc.
2-1 Site Map, Washington Facility, Hamilton BeachOProctor-Silex, Inc.
3-1 Generalized Groundwater Flow Direction for Hydrogeologic Unit A,
Washington Facility
3-2 Generalized Groundwater Flow Direction for Hydrogeologic Unit B,
Washington Facility
3-3 Approximate Distribution ofTCE in Unit A
3-4 Approximate Distribution of TCE in Unit B
3-5 Approximate Distribution ofTrichloroethene, D-D'
3-6 Approximate Distribution ofTrichloroethene, E-E'
3-7 Approximate Distribution of cis-1,2-DCE in Unit A
3-8 Approximate Distribution of cis-1,2-DCE in Unit B
3-9 Approximate Distribution of cis-1,2-DCE, D-D'
3-10 Approximate Distribution of cis-1,2-DCE, E-E'
3-11 Approximate Distribution of 1,1-DCE in Unit A
3-12 Approximate Distribution of 1,1-DCE in Unit B
3-13 Approximate Distribution of 1,l-DCE, D-D'
3-14 Approximate Distribution of 1, 1-DCE, E-E'
3-15 Approximate Distribution of Vinyl Chloride in Unit A
3-16 Approximate Distribution of Vinyl Chloride in Unit B
3-17 Approximate Distribution ofVinyl Chloride, D-D'
3-18 Approximate Distribution of Vinyl Chloride, E-E'
3-19 Approximate Distribution of 1,1,1-TCA in Unit A
3-20 Approximate Distribution of 1,1,1-TCA in Unit B
80396907.0! FebOl_GWRpt.doc (4/2/01) iv
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LIST OF FIGURES (Continued)
3-21 Approximate Distribution of 1,1,1-TCA, D-D'
3-22 Approximate Distribution of 1,1,1-TCA, E-E'
3-23 Approximate Distribution of 1,2-DCA in Unit A
3-24 Approximate Distribution of 1,2-DCA in Unit B
3-25 Approximate Distribution of 1,2-DCA, D-D'
3-26 Approximate Distribution of 1,2-DCA, E-E'
3-27 Approximate Distribution of 1,1-DCA in Unit A
3-28 Approximate Distribution of 1,1-DCA in Unit B
3-29 Approximate Distribution of 1,1-DCA, D-D'
3-30 Approximate Distribution of 1,1-DCA, E-E'
3-31 Approximate Distribution of Toluene in Unit A
3-32 Cross-section Locations
3-33 Location of Surrounding Water Supply Wells
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2-1
3-1
3-2
LIST OF TABLES
Monitoring Well Construction Data for Sampled Wells
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
Water Level Measurements and Elevations, September 6, 2000
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
Historical Water Level Elevations at MW-213
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-3 Historical Water Level Elevations at MW-214
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-4 Historical Water Level Elevations at MW-215
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-5 Historical Water Level Elevations at MW-216
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-6 Historical Water Level Elevations at MW-220
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-7 Historical Water Level Elevations at MW-222
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-8 Historical Water Level Elevations at MW-224
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-9 Historical Water Level° Elevations at MW-225
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-10 Historical Water Level .Elevations at MW-226
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina .
3-11 Historical Water Level Elevations at MW-227
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-12 Historical Water Level Elevations at MW-228
Hamilton BeachOProctor-Silex, Inc., Washington, North Carolina
3-13 Historical Water Level Elevations at MW-230
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
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LIST OF TABLES (Continued)
3-14 Historical Water Level Elevations at MW-234
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-15 Field Measurements, September 6, and 7, 2000
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-16 Summary of Qualified Groundwater Analytical Results: September 2000
Volatile Organic Compounds by Method 8260B
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-17 Historical Analytical Results for MW-213
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-18 Historical Analytical Results for MW-214
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-19 Historical Analytical Results for MW-215
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-20 Historical Analytical Results for MW-216
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-21 Historical Analytical Results forMW-220
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-22 Historical Analytical Results for MW-222
Hamilton Beach<>Proctor-Silex, Inc., Washington; North Carolina
3-23 Historical Analytical Results forMW-224
Hamilton Beach<>Proctor-Silex, Inc., Washington, North CClrolina
3-24 Historical Analytical Results for MW-225
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-25 Historical Analytical Results for MW-226
Hamilton Beach<> Proctor-Silex, Inc., Washington, North Carolina
3-26 Historical Analytical Results for MW-227
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
3-27 Historical Analytical Results for MW-228
Hamilton Beach<>Proctor-Silex, Inc., Washington, North Carolina
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LIST OF TABLES (Continued)
3-28 Historical Analytical Results for MW-230
Hamilton Beach<'.> Proctor-Silex, Inc., Washington, North Carolina
3-29 Historical Analytical Results for MW-234
Hamilton Beach<'.>Proctor-Silex, Inc"., Washington, North Carolina
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1.0 INTRODUCTION
The Hamilton BeachOProctor-Silex (HBoPS) facility is located at 234 Springs
Road, north of the City of Washington, in Beaufort County, North Carolina (Figure 1-1). The
facility and surrounding land parcel are owned by the City of Washington and have been leased
by HBOPS since 1990 and previously leased by predecessor companies. The facility was
formerly involved in the final assembly, packaging, and warehousing of small electrical
household appliances.
Since 1992, when organic compounds. were initially detected in groundwater at
the site, several phases of investigation have been performed, including a comprehensive site
assessment (CSA). The results of the CSA indicated that a plume.of organic compounds is
present in groundwater underlying the site. The specific nature, volume, and time period of any
releases contributing to the plume are unknown. However, the principal constituents of the
plume are no longer lJ.Sed at the facility.
A plan for corrective action at the site has been proposed. Until corrective action
is implemented, groundwater will be sampled and analyzed on a quarterly schedule according to
a monitoring program requested and approved by the North Carolina Department of
Environment and Natural Resources, Groundwater Section. Quarterly groundwater .monitoring
is to be conducted in February, May, August, and November at seven wells: MW-220, -222,
-224, -225, -226, -230, and-234. These wells are located outside of the contaminant plume. In
February and August, the following six additional wells will be sampled: MW-213, -214, -215,
-216, -227, and-228. These wells are located within the contaminant plume. The purpose of the
monitoring program is to detect potential migration of the I?lume.
Radian International (Radian) conducted groundwater sampling at the facility in
February 2001. The sampling event included the measurement of water levels, temperature, pH,
and specific conductance; and the collection and analysis of samples from thirteen monitoring
wells. This report describes the sampling methods and presents the results for the quarterly
sampling event.
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. 2.0 FIELD METHODS
Groundwater was sampled on February 19 and 20, 2001 in general accordance
with the methods outlined in the Field Sampling and Analysis Plan prepared in April 1997 for
this site.
Thirteen monitoring wells were sampled. They included MW-213 through
MW-216, MW-220, MW-222, MW-224 through MW-228, MW-230, and MW-234. The
locations of the monitoring wells are shown in Figure 2-1. Details of well construction are
provided in Table 2-1.
Prior to sampling, the water level in each well was measured using an electric
water-level indicator. The wells were then purged using inertial foot-valve pumps, with the
exception of wells MW-213 and MW-228, which were purged with disposable hailers.
Temperature, pH, and specific conductance were measured and the data were recorded in a field
notebook. Purging continued until temperature, pH, and specific conductance stabilized; a
minimum of three well volumes was extracted; or the well was pumped dry. Each o~ the wells
was then sampled immediately f~llowing well purging using the inertial foot-valve pump or
bailer. For QA/QC purposes, duplicate samples were collected at wells MW-214 and-226; and,
a trip blank accompanied each sample shipment.
The groundwater samples were sent by o:vemight courier to STL in Austin, Texas,
for analysis of volatile organic compounds by EPA Method 8260B.
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3.0 RESULTS
3.1 Water Level Measurements
Table 3-1 presents the depth to groundwater and static water-level elevations
measured in the thirteen wells sampled and seven additional wells. Maps showing the
generalized direction of groundwater flow in hydrogeologic units A and B are included as
Figures 3-1 and 3-2, respectively. Historical water-level elevations in sampled wells are
included in Tables 3-2 to 3-14.
3.2 Analytical Results
Field measurements of water temperature, pH, and specific conductance are
summarized in Table 3-15. Qualified analytical results are summarized in Table 3-16. The
approximate extent of selected compounds that have been detected at concentrations exceeding
groundwater standards are illustrated in Figures 3-3 through 3-31. Cross-section locations are
shown in Figure 3-32. Both current and historical data were used to approximate the extent of
contaminants. Qualified data sheets and laboratory reports are included in Appendix A.
No analytes were detected above the ground'Yater standards.in samples fr~m
wells located near the perimeter of the site (MW-220, MW-222, MW-224, MW-225, MW-230,
and MW-234), nor were any analytes detected above the groundwater standards in the sample
from well MW-226, which is completed in the ~onfined Limestone Aquifer. Also, no analytes
were detected above groundwater standards in the sample collected from well MW-216 which is
located 350 feet from the source area. Concentrations of chemicals exceeding the standards were
detected in samples from wells MW-213, MW-214, MW-215, MW-227, and MW-228. These
five wells are located at, or within 150 feet of, the source area.
Historical analytical results for the sampled wells are presented in Tables 3-17 to
3-29, and in graphs included as Appendix B. A comparison of the record for wells located near
the perimeter of the site suggests that the plume remains on-site, at least 200 feet from potential
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receptors located north of Spring Road (Figure 3-33). The latest results for wells located at the
source area and other interior portions of the site are consistent with earlier results and indicate
no significant changes in chemical concentration and distribution have occurred.
80396907.01 FebOl_GWRpt.doc (4/2/01) 3-2
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FIGURES
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TABLES
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- - - -------.... -..,_ .. /_ - - - -
Table 2-1
Monitoring Well Construction Data for Sampled Wells
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Top of Casing
Installation Elevation Total Depth Screen Interval Filter Pack Bentonite Seal
Well No.· Date (ft. above MSL) (ft. bgs) (ft. bgs)
MW-213 1/14/98 28.44 7.5 3 -7.5
MW-214 1116/98 27.93 21 14.5 -21
MW-215 1116/98 28.06 10 8.5 -10
MW-216 5/5/98 32.82 35 26 -35
MW-220 5/5/98 31.50 34 25 -34
MW-222 5/6/98 35.11 40 31 -40
MW-224 11/13/98 33.43 34 25 -34
MW-225 11/13/98 33.43 10 4-10
MW-226 9/30/98 28.46 75 70-75
MW-227 10/1/98 28.47 25.5 20.5 -25.5
MW-228 9/23/98 28.71 10 3 -10
MW-230 10/26/98 33.47 14 8 -14
MW-234 6/23/99 35.03 26 17 -26
Monitoring wells 213 through 215 installed by Groundwater Management Associates, Inc.
Monitoring wells 216, 220, and 222 installed by Radian Mobile Field Services.
Monitoring wells 226 through 228 installed by Parratt Wolff, Inc.
Monitoring wells 224, 225, 230, and 234 installed by Probe Technology, Inc.
80396907.01 FebOl_GWRpt.doc (4/2/01)
(ft. bgs) (ft. bgs)
2.5 -7.5 1.5 -2.5
13.5 -21 12.5 -13.5
8 -10 7-8
25 -35 24-25
24-34 23 -24
30-40 29-30
24-34 23 -24
3 -10 2-3
69 -75 67 -69
19.5 25.5 17.5 -19.5
2-10 1 - 2
7 -14 5-7
16-26 13 -16
Grout Seal
(ft. bgs)
0-1.5
0 -12.5
0-7
0-24
0 23
0-29
0-23
0-2
0-67
0 -17.5
0 - 1
0-5
0-13
Table 3-1
Water Level Measurements and Elevations
February 19, 2001
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Measuring Point
Elevation Depth to Water
Well (ft above msl)) (ft)
MW-201S 29.74 1.70
MW-208 32.11 7.20
MW-213 28.44 3.96
MW-214 27.93 4.22
MW-215 28.06 7.12
MW-216 32.82 9.21
MW-217 32.75 8.06
MW-219 31.83 7.02
MW-220 31.50 8.05
MW-221 31.39 7.79
MW-222 35.11 13.77
MW-223 35.15 3.76
MW-224 33.43 8.20
MW-225 33.43 8.42
MW-226 28.46 19.26
MW-227 28.47 4.63
MW-228 28.71 4.20
MW-230 33.47 10.30
MW-233 34.55 10.57
MW-234 35.03 10.83
msl = mean sea level
80396907.01 FebOl_GWRpt.doc (4/2/01)
Water Level
Elevation
(ft above msl)
28.04
24.91
24.48
23.71
20.94
23.61
24.69
24.81
23.45
23.60
21.34
31.39
25.23
25.01
9.20
23.84
24.51
23.17
23.98
24.20
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Table 3-2
Historical Water Level Elevations at MW-213
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 25.54
November 16, 1998 24.21
February 2, 2000 26.41
Mav2, 2000 26.33
September 6, 2000 24.78
November 28, 2000 23.83
February 19, 2001 24.48
msl = mean sea level
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Table 3-3
Historical Water Level Elevations at MW-214
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
May 13, 1998 24.95
November 16, 1998 22.18
February 2, 2000 25.38
May2,2000 25.30
September 6, 2000 24.13
November 28, 2000 22.61
February 19, 2001 23.71
msl = mean sea level
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Table 3-5
Historical Water Level Elevations at MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
Mav 13, 1998 24.39
November 16, 1998 22.37
Februarv 2, 2000 24.84
May2, 2000 24.83
September 6, 2000 24.12
November 28, 2000 22.81
February 19, 2001 23.61
msl = mean sea level
•
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Table 3-9
Historical Water Level Elevations at MW-225
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 24.36
July 1, 1999 24.50
October 20, 1999 27.24
February 2, 2000 26.59
Mav2, 2000 26.40
September 6, 2000 27.22
November 28, 2000 24.38
Februarv 19, 2001 · 25.01
msl =: mean sea level
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Table 3-10
Historical Water Level Elevations at MW-226
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 8.43
July 1, 1999 8.54
October 20, 1999 11.11
Februii.ry 2, 2000 10.23
May 2, 2000 10.81
September 6, 2000 9.41
November 28, 2000 9.19
February 19, 2001 9.20
msl = mean sea level
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Table 3-11
Historical Water Level Elevations at MW-227
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 22.38
October 20, 1999 25.82
·February 2, 2000 25.88
Mav2, 2000 25.83
September 6, 2000 24.45
November 28, 2000 22.86
February 19, 2001 23.84
ms! = mean sea level
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Table 3-12
Historical Water Level Elevations at MW-228
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
November 16, 1998 23.01
f ebruarv 2, 2000 24.63
May2, 2000 26.36
September 6, 2000 25.44
November 28, 2000 23.74
February 19, 2001 24.51
msl = mean sea level
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Table 3-13
Historical Water Level Elevations at MW-230
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date ' (ft. above msl)
November 16, 1998 21.14
July 1, 1999 21.80
October 20, 1999 27.71
Februarv 2, 2000 27.44
May2, 2000 26.53
September 6, 2000 23.07
November 28, 2000 21.87
Februarv 19, 2001 23.17
msl = mean sea level
80396907.01 FebOl_GWRpt.doc (4/2/01)
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Table 3-14
Historical Water Level Elevations at MW-234
Hamilton BeachO Proctor-Silex, Inc.
Washington, North Carolina
Water Level Elevation
Date (ft. above msl)
July 1, 1999 23.24
October 20, 1999 25.71
February 2, 2000 25.67
Mav2,2000 25.56
September 6, 2000 25.04
November 28, 2000 23.23
February 19, 2001 24.20
msl = mean sea level
80396907.01 FebOl_GWRpt.doc (4/2/01)
Well Date Time
MW-213 2/20/01 09:00
MW-214 2/20/01 08:35
MW-215 2/20/01 08:05
MW-216 2/19/01 15:45
MW-220 2/19/01 14:30
MW-222 2/19/01 14:10
MW-224 2/19/01 15:05
MW-225 2/19/01 14:55
13:05
13:10
MW-226 2/19/01 13:15
13:20
13:25
13:30
MW-227 2/20/01 09:35
MW-228 2/20/01 09:40
MW-230 2/19/01 11:25
MW-234 2/19/01 13:50
80396907.0 I FebO I_ GWRpt.doc (4/2/0 I)
Table 3-15
Field Measurements
February 2001
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Volume Purged
(Gal) Pureine Criteria
2.6 3 well volumes
8.5 3 well volumes
1.4 3 well volumes
0.8 3 well volumes
0.8 3 well volumes
0.8 3 well volumes
0.8 3 well volumes
0.05 drv
9.0
11.5
15.0 Stabilized parameters
17.5
20.0
22.0
10.0 3 well volumes
3.0 3 well volumes
0.12 3 well volumes
0.5 3 well volumes
Specific
Temperature Conductance
(oC) (µS) pH
15.0 270 5.4
21.0 260 6.1
18.0 210 5.8
15.0 340 7.7
16.0 95 6.3
16.0 320 7.4
15.0 300 7.3
12.0 150 5.2
18.5 450 8.0
18.5 445 7.9
18.5 445 7.8
18.5 450 7.6
18.5 450 7.6
18.5 450 7.6
20.0 445 7.1
14.0 1100 4.0
12.5 150 4.5
16.0 140 6.6
---------~--~~~~~~-
.. _ .. _._ ......... '--· ... .. . ..: ....... -•.
Sample ID
Date of Sampling
Analyte (µg/L)
Benzene
2-Butanone (MEK)
n-Butylbenzene
sec-Butvlbenzene
Carbon Tetrachloride
Chloroethane
Chloroform
1, 1-Dichloroethane
1,2-Dichloroethane
l, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Ethvlbenzene
Isoproovlbenzene
Methyl t-butyl ether
Naphthalene
n-Proovlbenzene
Styrene
Tetrachloroethene
Tetrahvdrofuran
Toluene
I, 1, I -Trichloroethane
l, l ,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,4-Trimethvlbenzene
1,3,5-Trimethylbenzene
Vinvl chloride
m&o-Xvlene
o-Xylene
Table 3-16
Summary of Qualified Groundwater Analytical Results: February 2001
Volatile Organic Compounds by Method 8260B
Hamilton BeachOProctor-Silex, Washington, North Carolina
MW-213 MW-214 MW-215 MW-216 MW-220
2/20/01 2/20/0i 2/20/01 2/19/01 2119/01
0.465 J 0.396 J ND (0.0641) ND (0.0641) ND (0.0641)
ND (1.00) ND (LOO) ND (0.200) ND (0.200) ND (0.200)
ND <0.510) ND <0.510) ND (0.102) ND (0.102) ND (0.102)
ND (0.525) ND (0.525) ND (0.105) ND (0.105) ND (0.105)
ND (0.326) ND (0.326) ND (0.0652) ND (0.0652) ND (0.0652)
ND (0.462) ND <0.462) ND (0.0925) ND (0.0925) ND (0.0925)
ND (0.448) ND (0.448) ND (0.0896) ND (0.0896) ND (0.0896)
173 162 3.55 ND (0.124) 0.456 J
3.68 ND (0.510) ND (0.102) ND (0.102) ND (0.102)
433 16.8 2.38 ND (0.122) ND (0.122)
37.1 12.9 ND (0.112) ND (0.112) ND (0.112)
0.937 J 0.708 J ND (0.119) ND <0.119) ND (0.119)
0.170 J ND (0.680) ND (0.136) ND (0.136) ND (0.136)
ND (0.466) · ND (0.466) ND (0.0931) ND (0.0931) ND (0.0931)
ND (0.580) ND (0.580) 0.427 J ND (0.116) ND (0.116)
7.69J ND (0.400) UJ ND (0.0801) UJ ND (0.0801) UJ ND (0.0801) UJ
ND (0.700) ND (0.700) ND (0.140) ND (0.140) ND (0.140)
ND (0.488) ND (0.488) ND <0.0977) ND (0.0977) ND (0.0977)
28.8 ND(0.720) ND (0.144) UJ . ND (0.144) ND (0.144) UJ
ND (4.50) ND (4~50) 6.41 ND(0.900) ND (0.900)
ND (0.318) ND (0.318) ND (0.0637) ND (0.0637) ND <0.0637)
ND (0.845) ND (0.84'5) ND (0.169) ND (0.169) ND (0.169)
2.68 ND (0.410) ND (0.0821) ND (0.0821) ND (0.0821)
426 ND (0.685) ND (0.137) ND (0.137) ND (0.137)
ND (0.530) ND (0.530) ND (0.106) ND (0.106) ND (0.106)
ND (0.620) ND (0.620) NI) (0.124) ND (0.123) ND (0.123)
ND (0.452) ND (0.452) ND (0.0905) ND (0.0905) ND (0.0905)
19.2 11.8 ND (O.i 14) ND(0.114) ND (0.114)
0.363 u ND (0.835) ND (0.167) ND (0.167) ND (0.167)
0.815J ND (0.422) ND (0.0844) ND (0.0844) ND (0.0844)
J = Estimated value.
MW-222
2/19/01
ND (0.0641)
ND (0.200)
ND (0.102)
ND (0.105)
ND (0.0652)
ND.(0.0925)
. ND (0.0896)
0.589
ND (0.102)
0.102 J
0.222 J
ND (0.119)
ND (0.136)
ND (0.0931)
ND (0.116)
ND (0.0801) UJ
ND (0.140)
ND (0.0977)
ND (0.144) UJ
ND (0.900)
ND (0.0637)
ND (0.169)
ND (0.0821)
ND (0.137)
ND (0.106)
ND (0.123)
ND <0.0905)
ND (0.114)
ND (0.167)
ND (0.0844)
Target analytes not listed were not detected.
Bold values exceed Standards. U =Not present above the associated level, blank contamination present.
ND ( ) =Not detected at specified detection limit.
80396907.01 FebOl_GWRpt.doc (4/2/01)
SamulelD MW-224
Date of Sampling 2/19/01
Analyte (µWJ.,)
Benzene ND (0.0641)
2-Butanone (MEK) ND (0.200)
n-Butylbenzene ND (0.102)
sec-Butvlbenzene ND (0.105)
Carbon Tetrachloride ND (0.0652)
Chloroethane ND (0.0925)
Chloroform ND (0.0896)
1, 1-Dichloroethane ND (0.124)
1,2-Dichloroethane ND (0.102)
1, 1-Dichloroethene ND (0.122)
cis-1,2-Dichloroethene ND (0.112)
trans-1,2-Dichloroethene ND (0.119)
Ethvlbenzene ND (0.136)
Isopropylbenzene ND (0.0931)
Methyl t-butyl ether ND (0.116)
Naphthalene ND (0.0801) UJ
n-Proovlbenzene ND (0.140)
Styrene ND (0.0977)
Tetrachloroethene ND (0.144) UJ
Tetrahvdrofuran ND (0.900)
Toluene ND (0.0637)
1, 1, I-Trichloroethane ND (0.169)
1, 1,2-Trichloroethane ND (0.0821)
Trichloroethene ND (0.137)
Trichlorofluoromethane ND (0.106)
1,2,4-Trimethylbenzene ND (0.124)
1,3,5-Trimethvlbenzene ND (0.0905)
Vinvl chloride ND (0.114)
m&p-Xylene ND (0.167)
o-Xvlene ND (0.0844)
Target analytes not listed were not detected.
ND ( ) =Not detected at specified detection limit.
Bold values exceed Standards.
J = Estimated value.
Table J-16 (Continued)
MW-225 MW-226 MW-227
2/19/01 2/19/01 2/20/01
ND (0.0641) ND (0.0641) ND (0.0641)
ND (0.200) ND (0.200) 25.2J
ND (0.102) ND (0.102) ND (1.02)
ND (0.105) ND(0.105) ND (1.05)
ND (0.0652) ND (0.0652) ND (0.652)
ND (0.0925) ND (0.0925) 24.6
ND (0.0896) ND (0.0896) ND (0.896)
ND (0.124) ND (0.124) 2,300
ND (0.102) ND (0.102) 10.8
ND (0.122) ND (0.122) 332
ND (0.112) ND (0.112) 240
ND (0.119) ND (0.119) 5.48
ND (0.136) ND (0.136) ND (1.36)
ND (0.0931) ND (0.0931) ND (0.931)
ND (0.116) ND (0.116) ND (1.16)
ND (0.0801) UJ ND (0.0801) UJ ND (0.0801) UJ
ND (0.140) ND(0.140) ND(l.40)
ND (0:0977) ND(0.0977) ND (0.977)
ND (0.144) UJ ND (0.144) UJ ND (1.44)
ND (0.900) ND(0.900) ND (9.00)
ND (0.0637) ND (0.0637) 10.7
ND (0.169) ND (0.169) 1,760
ND (0.0821) ND (0.0821) ND (0.821)
ND (0.137) ND (0.137) 39.6
ND (0.106) ND (0.106) ND (1.06)
ND (0.124) ND (0.124) ND (1.24)
ND (0.0905) ND (0.0905) ND (0.905)
ND (0.114) ND (0.114) 4.73J
ND (0.167) ND (0.167) ND (1.67)
ND (0.0844) ND (0.0844) ND (0.844)
U =Not present above the associated level, blank contamination present.
80396907.01 FebOl_GWRpt.doc (4/2/01)
MW-228 MW-230 MW-234
2/20/01 2/19/01 2119/01
38.7 J ND (0.0641) ND (0.0641)
500J ND (0.200) ND(0.200)
28.9J ND (0.102) ND (0.102)
9.56J ND (0.105) ND (0.105)
23.0J ND (0.0652) ND(0.0652)
97.3 J ND (0.0925) ND(0.0925)
7.64J ND (0.0896) ND (0.0896)
10,200 ND (0.124) ND (0.124)
79.9J ND (0.102) ND (0.102)
29,800 ND (0.122) ND (0.122)
3,740 J 0.0969 J ND (0.112)
22.5 J ND (0.119) ND (0.119)
970J ND (0.136) ND (0.136)
63.8 J ND (0.0931) ND (0.0931)
ND (5.80) UJ. ND (0.116) ND (0.1J6)
973J ND (0.0801) UJ ND (0.0801) UJ
354J ND (0.140) ND(0.140)
28.3 J ND (0.0977) ND (0.0977)
18.6J ND (0.144) UJ ND (0.144) UJ
ND(45)UJ ND (0.900) ND(0.900)
1,610 J ND (0.0637) ND (0.0637)
50,500 ND (0.169) ND (0.169)
25.1 J ND (0.0821) ND (0.0821)
15,400 0.160 J ND (0.137)
28.2 ND (0.106) ND (0.106)
2,llOJ ND (0.124) ND (0.124)
530J ND (0.0905) ND (0.0905)
492 ND (0.114) ND (0.114)
2,530 J ND (0.167) ND (0.167)
2,150 J ND (0.0844) ND (0.0844)
~----~-~-~--~~-~---
Groundwater
AnaMe Standard
Benzene 1
Chloroethane 2800
1, 1-Dichloroethane 700
1,2-Dichloroethane 0.38
1, 1-Dichloroethene 7
cis-1,2-Dichloroefhene ,70
trans-1,2-Dichloroethene 70
p-lsopropyltoluene -
Trichloroethene 2.8
Vinyl chloride O.Q15
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
Table 3-18
Historical Analytical Results for MW-214
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
November February May
1998 2000 2000.
0.172 J 0.315 J 0.304 J
0.485 J 0.904 0.705
108 179 173
0.303 J 0.633 0.607
8.16 13.8 15.4
6.86 11.7 12.0
0.478 0.701 0.794
0.181 J ND (0.0452) ND (0.0452)
ND (0.587) U 0.289 J 0.494 J
8.84 11.5 9.73
U = Not present above the associated level; blank contamination is present.
80396907.01 FebOl_GWRpt.doc (4/2/01)
September February
2000 2001
0.280 J 0.396 J
0.649 J ND (0.462)
159 162
0.576 J ND (0.51Q)
13.7 16.8
11.6 12.9
0.683 J 0.708 J
ND (0.0904) ND (0.575)
ND (0.489) U ND (0.685)
9.35 11.8
-----~~--~~--~-~---
Groundwater
Analyte Standard
Toluene 1000
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
Table 3-20
Historical Analytical Results for MW-216
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
May November February May
1998 1998 2000 2000
0.171 ND (0.0522) UJ ND (0.0680) ND (0.0680)
UJ =Not detected and the detection limit is estimated.
80396907.01 FcbOl_GWRpt.doc (4/2/01)
September February
2000 2001
ND (0.0680) ND (0.0637)
---------~--~~--~~~
Groundwater
Analvte Standard
Carbon disulfide 700
1, 1-Dichloroethane 700
l, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
Toluene 1,000
Groundwater
Analyte Standard
Carbon disulfide 700
1, 1-Dichloroethane 700
1, 1-Dichloroethene 7
cis-1,2-Dichloroethene 70
Toluene 1,000
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
Table 3-22
Historical Analytical Results for MW-222
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
May November July October
1998 1998 1999 1999
ND (0.0547) ND (0.0547) 0.388 J 0.0944
ND (0.0576) ND (0.0576) ND (0.0736) ND (0.0588)
0.0908 J ND (0.0715) ND (0.102) ND (0.0819)
ND (0.0383) ND (0.223)U ND (0.0595) ND (0.0407)
0.156 J ND (0.0522) ND (0.0766) ND (0.0645)
November February
2000 2001
ND (0.0684) ND (0.0684) UJ
ND (0.124) 0.589
0.0668 J 0.102 J
0.124 J 0.222 J
ND (0.137) ND (0.0637)
UJ = Not detected and the detection limit is estimated.
U =Not present above the associated level, blank contamination present.
80396907.01 FebOl_GWRpt.doc (4/2/01)
February May September
2000 2000 2000
ND (0.0484) UJ ND (0.0484) ND (0.0484) UJ
ND (0.0487) 0.338 J 0.328 J
ND (0.0697) ND (0.279) U 0.0766 J
ND (0.0603) ND (0.0603) 0.139 J
ND (0.0680) ND (0.0680) ND (0.0680)
- ----- -;--.. - - -.... - -..... -
Groundwater November
Analyte Standard 1998
Carbon disulfide 700 ND (0.0547)
Chloroform 0.19 ND (0.0480)
Analyte Groundwater February
Standard 2001
Carbon disulfide 700 ND (0.511) UJ
Chloroform 0.19 ND (0.0896)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
ND= Not detected at (detection limit).
NS = Not sampled.
UJ = Not detected and the detection limit is estimate~.
80396907.01 FebOl_GWRpt.doc (4/2/01)
Table 3-24
Historical Analytical Results for MW-225
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
July October February May2000
1999 1999 2000
ND (0.864) 0.0691 ND (0.0484) UJ ND (0.0484)
ND (0.0424) 0.171 ND (0.0670) ND (0.0670)
September November
2000 2000
ND (0.0484) UJ ND (0.0684)
ND (0.0670) ND (0.0896)
-----------~~~-----
--~--------~-~----~
Groundwater November
Analvte Standard 1998
Carbon disulfide 700 ND (0.0547)
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND = Not detected at (detection limit).
UJ =Not detected and the detection limit is estimated.
80396907.01 FebOl_GWRpt.doc (4/2/01)
Table 3-25
Historical Analytical Results for MW-226
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
July October February May
1999 1999 2000 2000
ND (0.864) 0.0950 ND (0.0484) UJ ND (0.0484) UJ
September November February
2000 2000 2001
0.210 J ND (0.0684) ND (0.0684) UJ
Analyte
Acetone
Benzene
2-Butanone (MEK)
n-Butylbenzene ·
Carbon disulfide
Carbon tetrachloride
Chloroethane
Chloroform
l, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1, 1-Dichloropropene
Ethylbenzene
Isopropylbenzene
p-lsopropyltoluene
Methyl t-butvl ether
Methylene chloride
Napthalene
n-Propylbenzene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1, I-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
1,2,4-Trimethylbenzene
1,3,5-Trimethvlbenzene
80396907.01 FebOl_GWRpt.doc (4/2/01)
Table 3-26
Historical Analytical Results for MW-227
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater November February May
Standard 1998 2000 2000
700 29.9J ND (5.72) 19.1 J
1 0.668 J ND (0.984) 0.622 J
170 42.5 J ND (3.58) 40.2J
70 0.437 J ND (1.28) ND (0.0642) VJ
700 0.573 J ND (0.968) ND (0.0484) VJ
0.3 ND (0.0576) UJ ND (1.73) 26.2J
2800 2.14 J ND (1.51) 14.6 J
0.19 1.64 J ND (1.34) 1.17 J
700 4,620 844 3,360
0.38 19.5 J 4.40 J 20.2
7 705 108 644
70 228 105 381
70 3.66 J ND (1.63) 7.93 J
-ND (0.0444) UJ . ND (0.928) 0.182 J
29 3.58 J ND (9.38) 0.454 J
70 0.392 J ND (0.948) ND (0.0474) VJ
-0.194 J ND (0.904) ND (0.0452) UJ
200 ND (0.0365) UJ ND (0.938) 0.322 J
5 ND (1.13) UJ ND (1.59) 0.982 u
21 3.73 J ND (2.12) ND (0.982) UJ
70 2.25 J ND (1.77) ND (0.0886) VJ
0.17 ND (0.102) VJ ND (1.58) 1.48 J
0.7 1.41 J ND (1.14) ND (0.0568) UJ
1000 29.6·J 3.56 J 13.8J
200 3,200 310 2,440 J
-3.20J ND 0.90) 2.95 J
2.8 810 12.9 48.9 J
350 10.8 J ND (1.50) 0.720 J
350 3.37 J ND (0.872) 0.646 J
September February
2000 2001
ND (14.3) UJ ND (4.38)
ND (2.46) ND (0.0641)
ND (8.95) 25.2
ND (3.21) ND (1.02)
ND (2.42) UJ ND (0.684) UJ
ND (4.34) UJ ND (0.652)
26.3 24.6
ND (3.35) ND (0.896)
1,340 2,300
ND (2.50) 10.8
249 332
211 240
ND (4.06) 5.48
ND (2.32) ND (0.994)
ND (2.76) ND (1.36)
ND (2.37) ND (0.931)
ND (2.26) ND (1.15)
ND (2.34) ND (1.16)
ND (3.98)U ND (1.26) U
ND (5.30) ND (0.0801) UJ
ND (4.43) ND (1.40)
ND (4.74) ND (0.870)
ND (2.84) UJ ND (1.44)
8.92 J 10.7
1,220 1,760
ND (4.76) ND (0.821)
ND (36.9) U 39.6
ND (3.74) ND (l.24)
ND (2.18) ND (0.905)
-----------~---~---
--------------------
Table 3-26 (Continued)
Groundwater
Analyte Standard
Vinyl chloride .015
m&p-Xylene 530
o-Xvlene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND =Not detected at (detection limit).
November
1998
5.70 J
8.78 J
8.91 J
U =Not present above the associated level, blank contamination present.
UJ = Not detected and the detection limit is estimated.
80396907.01 drft_Feb_OIGW _Rpt.doc (4/4/01)
February
2000
ND (1.15)
ND (2.74)
ND (1.43)
May September February
2000 2000 2001
5.51 J ND (I 15) 4.73
0.956 J 1,520 J ND (1.67)
0.995 J 1,240 ND (0.844)
Analyte
Acetone
Benzene
2-Butanone (MEK)
n-Butylbenzene
sec-Butvlbenzene
Carbon tetrachloride
Chloroethane
Chloroform
Chloromethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1, 1-Dichloropropene
Ethvlbenzene
2-Hexanone
Isopropylbenzene
p-lsopropyltoluene
Methyl t-butvl ether
4-Methyl-2-pentanone (MIBK)
Napthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1, I-Trichloroethane
80396907 .0 I FebO l _ GWRpt.doc (4/2/0 I)
Table 3-27
Historical Analytical Results for MW-228
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
Groundwater November February .May
Standard 1998 2000 2000
700 307 J ND (1,430) 360J
l 51.3 J ND (246) 56.5 J
170 21.3 J ND (895) 382J
70 15.6 J ND (321) 9.88 J
70 .. 5.27 J ND (372) 7.96J
0.3 42.2J ND (434) 26.2J
2800 74.7 J ND (378) 89.8 J
0.19 12.8 J ND (335) 9.62J
2.6 ND (0.0521) UJ ND (410) 1.33 J
700 24,100 16,200 14,500
0.38 ND (0.0348) UJ ND (250) ND (0.0499) UJ
7 96,500 71,800 53,400
70 3,330 1,970 J 2,360
70 24.2J ND (406) 17.0 J
-ND (0.0444) UJ ND (232) 1.51 J
29 544 414J 555 J
-45.1 J ND (835) 38.8 J
70 41.5 J ND (237) 33.7 J
-6.80 J ND (226) ND (0.0452) UJ
200 5.21 J ND (234) 20.8 J
-12.3 J ND (422) 17.5 J
21 608 ND (530) 246J
70 200 ND (443) 302 J
100 ND (0.0578) UJ ND (361) ND (0.0722) UJ
-0.810 J ND (474) 0.844 J
0.17 0.688 J ND (396) ND (0.0792) UJ
0.7 30.5 J ND (284) 32.4 J
1000 1,460 1,610 J 1,520
200 173,000 135,000 121,000 J
September February
2000 2001
ND (572) UJ ND (87.6)
ND (98.4) 38.7 J
ND (358) 5001
ND (128) 28.9J
ND 049) 9.56 J.
ND (173) UJ 23.0J
ND (151) 97.3 J
ND {134) 7.64J
ND (164) UJ ND (6.35) UJ
11,900 10,200
ND (99.8) 79.9J
31,200 29,800
2,380 3,740 J
ND (163) 22.5 J
ND (92.8) ND (4.97) UJ
506 J 970J
ND (334) ND (8.45) UJ
ND (94.8) 63.8 J
ND (90.4) ND (5.75) UJ
ND (93.8) ND (5.80) UJ
ND (169) ND (8.90) UJ
ND (212) 973 J
ND (177) 354 J
ND (144) 28.3 J
ND (190) ND (5.55) UJ
ND (158) ND (4.35) UJ
ND (114) 18.6 J
1,340 1,610
64,400 50,500
-------------------
-------------------
Groundwater
Analvte Standard
J, 1,2-Trichloroethane -
Trichloroethene 2.8
Trichlorofluoromethane 2100
1, 1,2-Trichlorotrifluoroethane 210,000
1,2,4-Trimethylbenzene 350
1,3,5-Trimethvlbenzene 350
Vinyl chloride .015
m&p-Xvlene 530
o-Xvlene 530
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
UJ = Not detected and the detection limit is estimated.
80396907.01 drft_Feb_OlGW _Rpt.doc (4/4/01)
Table 3-27 (Continued)
November February
1998 2000
49.3 J ND (476)
22,800 15,000
12.7 J ND (1,040)
ND (0.0986) ND (383)
1,270 1,220 J
309 ND (218)
314 ND (287)
1,540 1,760
1,330 1,370
May September February
2000 2000 2001
38.0 J ND (190) 25.l J
13,300 11,500 15,400
8.12 J ND (416) 28.2
0.947 J ND (153) UJ ND (6.15) UJ
1,190 J 933 J 2,110 J
407 J ND (87.2) 530 J
194 J ND (115) 492
1,680 J 1,520 J 2,530
1,350 1,240 2,150J
Groundwater November
Analvte Standard 1998
1, 1-Dichloroethane 700 ND (0.0576)
1, 1-Dichloroethene 7 ND(0.306)U
Cis-1,2-Dichloroethene 70
Toluene 1,000
Trichloroethene 2.8
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
ND(2.67)U
ND (0.0522)
ND (2.05)U
Table 3-28
Historical Analytical Results for MW-230
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
July October February May
1999 1999 2000 2000
ND (0.0736) 0.265 0.189 J ND (0.348) U
ND (0.102) 0.133 0.148 J 0.593
ND (0.0595) 0.304 0.354 J 0.573
0.286 ND (0.309) U 0.284 J 0.0826 J
ND (0.0929) 0.921 0.661 J 1.11
U =Not present above the associated level; blank contamination is present.
80396907.01 FebOl_GWRpt.doc (412/01)
September November February
2000 2000 2001
ND (0.0487) ND (0.124) ND (0.124)
ND (0.0697) ND (0.122) ND(0.122)
0.102 J 0.142 J 0.0969 J
0.126 J ND (0.0637) ND (0.0637)
ND (0.355) U 0.235 J 0.160 J
-------------------
_ .. _________ _ - - - - -- -
Groundwater November
Analvte Standard 1998
Carbon disulfide 700
1, 1-Dichloroethene 7
Target analytes not listed were not detected.
All samples reported in micrograms per liter.
J = Estimated value.
ND= Not detected at (detection limit).
NS
NS
UJ =Not detected and the detection limit is estimated.
80396907.01 FebOl_GWRpt.doc (4/2/01)
Table 3-29
Historical Analytical Results for MW-234
Hamilton BeachOProctor-Silex, Inc.
Washington, North Carolina
July October February May
1999 1999 2000 2000
ND (0.864) 0.0600 ND (0.0484) UJ ND (0.0484)
ND (0.102) ND (0.0819) ND (0.0697) 0.145 J
September November February 2000 2000 2001
ND (0.0484) UJ ND (0.0684) ND (0.0684) UJ
ND (0.0697) ND (0.122) ND (0.122)
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APPENDIX A
GROUNDWATER SAMPLING ANALYTICAL REPORTS
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QUALIFIED DATA ·
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Introduction
Hamilton Beach<>Proctor-Silex, Washington, NC
Data Validation Report
URS-Radian, March 2001
URS-Radian collected thirteen groundwater samples (0201HBWW-213 through-216, -220, -222, -224
through -228, -230, and -234) and two field duplicates at the Hamilton Beach<>Proctor Silex facility in
Washington, NC on February 19 and 20, 2001. The samples were submitted to Severn Trent Laboratories
(STL) in Austin, Texas for the determination of volatile organic compounds (VOC) by SW-846 Method
8260B. A trip blank was included with each shipment of samples to the laboratory for the analysis of
voe.
URS-Radian reviewed the analytical results, which were reported by the laboratory under work order
number 20102134. ·The data evaluation was modeled after the National Functional Guide.lines for Organic
Data Review (EPA, October 1999). Accuracy was determined from the review of holding times, spike
recov~ries, tuning result, continuing calibration results, and.blank contamination. Precision was based on
the evaluation of field and laboratory duplicate results. Sample results have been appropriately qualified
based on the criteria of the data review process. The results of the data review are summarized below.
Sample Condition upon Receipt and Holding Times
All samples were received intact and in good condition by STL on February 21, 2001. It should be noted
that samples shipped February 19 were not received by the laboratory until the 21 because the air bill was
misplaced during transit. The carrier, Federal Express, opened the cooler to determine the destination of
the samples. Custody seals placed on sample containers by the field team were iptact upon receipt at the
laboratory. The Chain-of-Custody (COC) record included in the cooler by the field team for samples
collected February 19 was lost during shipment. A copy of the original COC record was faxed to the
laboratory by the field team leader. The temperature of sample containers upon receipt at the laboratory
was within laboratory specification limits of 1-4°C. Air bubbles were not observed in any volatile organic
analysis (VOA) vials.
Technical hold times were assessed by comparing the sampling dates with that of the analysis date.
Samples were analyzed for VOC within EPA-established holding times of seven days for unpreserved
samples.
Calibration
Gas chromatograph/mass spectrometer (GC/MS) instrument tuning and performance checks are performed
to ensure the instrument's ability to provide appropriate mass-resolution, identification, and sensitivity. All
samples were analyzed for voe within twelve hours of the performance check standard. The tuning
compound mass-ion abundance criteria for the VOA were reported within control limits.
Control limits for initial and continuing calibrations are established to ensure that the instrument is capable
of producing accurate quantitative and qualitative data at the beginning and throughout each of the
analyses. Since the results of the initial calibration were not included in the laboratory report, the
evaluation was based on the n~view of the February 23 and 26 continuing calibration data. Laboratory
specifications were met during the volatile organic continuing calibration conducted on instrument MSDA.
The recovery of the continuing calibration standard, however, was not within 80-120% recovery of the true
value for the following target analytes:
0201 HB-PS Wash DE.doc
Page I of3
03/22/01
• Continuing calibration of February 23 at 08:12 -acetonitrile (79%), acrolein (68%), bromoform
(79%), bromomethane (79%), carbon disulfide (78%), chloromethane (75%), 1,2-dibromo3-
chloropropane (69%), hexachlorobutadiene (66%), 2-hexanone (78%), naphthalene (68%), 1,2,3-
trichlorobenzene (63%), 1,1,2,2-tetrachloroethane (79%), tetrachloroethene (79%), 1,2,4-
trichlorobenzene (70%), and vinyl acetate (79%).
• Continuing calibration ofFebruary 26 at 10:46-carbon disulfide (79%), chloromethane (79%),
hexachlorobutadiene (75%), naphthalene (74%), 1,2,3-trichlorobenzene (72%), 1,2,4-trichlorobenzene
(76%), and 1,1,2-trichlorotrifluoroethane (124%).
Results for compounds where the recovery was less than 80% during the continuing calibration have been
qualified as estimated (J, UJ) in associated samples. Positive sample results were qualified as estimated (J)
when the recovery exceeded 120% in the continuing calibration.
Laboratory Control Samples
Laboratory control samples (LCS) are blallk samples fortified (spiked) with known concentrations of
analyte of interest. The percent recoveries and/or duplicate results of the LCS and their duplicates are used
to assess extraction efficiencies and overall analytical accuracy and precision.
Laboratory and project1 specifications' were met during the LCS/LCS duplicate analysis of February 23.
Blank Contamination
Laboratory blanks are clean liquid and/or solid matrix samples prepared by the analytical laboratory and
analyzed in the same manner as the field samples. Laboratory blanks are used to ensure that the field
samples are not contaminated during the sample preparation, sample analysis, or from previous samples
(instrument carry-over). Trip blanks are analyte-free water samples that accompany volatile investigative
samples during all stages of shipment, storage, and analysis. The trip blanks are used to assess the potential
for artificial introd1,1ction of volatile compounds into the investigative samples during the transportation and
sample handling processes.
Methylene chloride, a common laboratory blank contaminant, was detected at a concentration of 0.153 J
parts per billion in the method blank. Carbon disulfide was also detected in the method blank at a
concentration of 0.234 J parts per billion. VOC were not detected in the trip blanks. Sample results that
were not significantly greater (ten times for methylene chloride, five times for carbon disulfide) than that
detected in the blanks have been qualified due to the presence of blank contamination. Affected sample
results have been flagged "ND" and detection limits elevated to the amount present in the sample and
flagged with a U.
Surrogate Spikes
Surrogate compound percent recoveries are used to assess extraction efficiencies, possible matrix effects,
and overall analytical accuracy during organic analyses.
Acceptable sample results were obtained for the surrogate spikes during the VOA of all samples, except
0201HBWW228. During the February 26 analysis of sample 0201HBWW228 at 18:37, the surrogate
recovery for l,2-dichloroethane-d4 was 60%, which is less than the laboratory control limits of61-143%.
The volatile organic results associated with this sample analysis were qualified as estimated (J, UJ).
1 The recovery of either the LCS or LCSD must be within 60-140%.
0201 HB-PS Wash DE.doc
Page2 of3
03/22/01
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Matrix Spikes
Matrix spikes (MS) are samples spiked with known concentrations of analytes of interest. MS percent
recoveries and duplicate results are used to assess extraction efficiencies, possible matrix effects, and
overall analytical accuracy and precision.
The criteria for precision were met during the MS and MS duplicate (MSD) analysis of sample
0201HBWW2 l 5 for VOC. Recoveries fell within QC limits during the MS/MSD analysis of sample
0201HBWW215 for all target analytes, except acrolein and 1,2,3-trichlorobenzene. Recoveries for acrolein
(67 and 69%) and 1,2,3-trichlorobenzene (58 and 62%) were less than control limits (70-130% and 66-
140%, respectively). The non-detect acrolein and 1,2,3-trichlorobenzene results in sample
02010HBWW215 have been qualified as estimated (UJ).
Field Duplicates
Fie1d duplicate samples are used to demonstrate acceptable precision during the sample collection process.
Acceptable precision was observed during the analysis of field duplicate samples 0201HBWW226 and
0201HBWWD998, and 0201HBWW214 and 0201HBWWD999.
Sample Results
The laboratory provided volatile organic results for all North Carolina groundwater quality standards
presented in 15A NCAC 2L.0202. Detection limits were less than or equal to Class GA standard or
practical quantitation limits.
The laboratory flagged sample results less than the practical quantitation limit and sample detection limit
with a J and U, respectively. All positive sample results that are less than these limits are considered
estimated (J).
0201 HB-PS Wash DE.doc
Page 3 of3
03/22/01
HB<>PS Washington ATTACHMENT A
Absolute 2x's
Analyte 214 0999 DL DL*5 Criteria RPO Difference DL Comments/Action
benzene 0.396 0.362 0.32 1.6 Abs Oiff 9 0.034 0.64 None
1,1-DCA 162 164 0.62 3.1 RPO 1 2 1.24 None
1, 1-DCE 16.8 16.7 0.61 3.05 RPO 1 0.1 1.22 None
cis-1,2-DCE 12.9 11.9 0.56 2.8 RPO 8 1 1.12 None
trans-1,2-DCE 0.708 0.424 0.595 2.975 Abs Diff 50 0.284 1.19 None
vmyl chloride 11.8 11.6 0.57 2.85 RPO 2 0.2 1.14 None
Criteria: If both sample results are greater than 5xs' the average DL, then evaluate precision based on the RPD between field duplicate
results. If either sample result is less than 5x's the average DL, then evaluate precision based on the absolute difference between results.
Flag results J/UJ, if RPO between sample results is greater than 50% or the absolute difference between sample results is greater than 2 the
average DL. If one sample result is ND and the other is positive, qualify results as estimated (J/UJ).
DL Detection Limit
E Exceeded calibration range (lab flag)
J Estimated value
R Reported elsewhere (lab flag)
RPD Relative percent difference
V Carryover suspected (lab flag)
B Detected in method blank.
0201 HB-PS Wash VOA-Field Dup.xls, 214-d999
3/8/2001, 1 :53 PM
2 of2 -------------------
-------------------
HB<>.PS -Washington
Absolute 2x's
Analyte 226 0998 DL DL*5 Criteria RPD Difference DL Comments/Action
0 ##### 0 0 None
0 ##### 0 0
Criteria: If both sample results are greater than 5xs' the average DL, then evaluate precision based on the RPO between field duplicate
results. If either sample result is less than 5x's the average DL, then evaluate precision based on the absolute difference between results.
Flag results J/UJ, if RPD between sample results is greater than 50% or the absolute difference between sample results is greater than 2 the
average DL. If one sample result is ND and the other is positive, qualify results as estimated (J/UJ).
DL Detection Limit
E Exceeded calibration range (lab flag)
J Estimated value
R Reported elsewhere (lab flag)
RPO Relative percent difference
V Carryover suspected (lab flag)
After taking blank contamination into account, target analytes were not detected in either sample.
0201 HB-PS Wash VOA-Field Dup.xls, 226-d998
3/8/2001, 1 :53 PM
1of2
ATTACHMENT A
- - - - - - - - - - - - ---- - - - -
SECTION IV
Analytical Results
MS-VOA
SW8260B·
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
I -Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
· «· .. CAS ..
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWD998
2010213416
Aaueous
Received
NA
02/19/2001 13:35
02/26/2001 12:12
02/26/2001 12:12
1.0000
MSDA
ul!/L.
.cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.322U.1NI> ,._
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 (f.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
&.6684' 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0;000
0.0896 0.000
0.0938 0.000
0201HBWD999 0201HBWD999
2010213403 2010213403
Aoueous Aaueous
Received Received
NA NA
02/20/2001 08:45 02/20/2001 08:45
02/26/2001 13:39 02/26/2001 17:34 ..
02/26/2001 13:39 02/26/2001 17:34
50.0000 5.0000
MSDA MSDA
ul!/L ug/L
.. Cone Flaa DL "; ",·>RC -.. " ·_: :.ccu1c·1,, .. :· Flaa ··: .. nL: ~ RL
N') R 2!.: ~-~~o ND 2.19 0.00'0
N) 341 o.obo ND 34.1 0.000
N) 190 OJ 100 ND 19.0 0.000
ND 22.3 oA:>oo ND 2.23 0.000
l' n 3.20 d.ooo 0.362 J 0.320 0.000
l'D 4.99 ~.ooo. ND 0.499 0.000
l D 6.55 /o.000 ND 0.655 0.000
D 5.90 /0.000 ND 0.590 0.000 m 8.50 I o.ooo ND 0.850 0.000 m 9.95 I o.ooo ND 0.995 0.000
.JD 10.0 I o.ooo ND l.00 0.000
>JD 5.10 I o.ooo ND 0.510 0.000 m 5.25 I 0.000 ND 0.525 0.000
D -4.56 I 0.000 ND 0.456 0.000
m I! 3.42 / 0.000 ND l'-:S s 0.342 0.000
JO 3.26/ ·. 0.000 ND 0.326 0.000
1'10 5.7d 0.000 ND 0.570 0.000
l D 4.'l/I 0.000 ND 0.421 0.000
10 4.,2 0.000 ND 0.462 0.000
l.D 4/48 0.000 ND 0.448 0.000
l !D I[/ J rn {\ {\{\{\ ND 0.469 0.000
Page 4 of
Sample results have been qualified by URS-Radian based on the results of the da1a review process, which is modeled after th<' Nllli1J1111l l-i111cticm11/ U11itle/111<'sfvr Orgm1ic 11111/ lnorg1111ic.Data Rt•i•if'w
(US EPA, October 1999 and February 1994, respcc11vely).
66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS:..·: ;'",
Chloromethane 74-87-3
3-Chloroaroaene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
l 2-Dibromo-3-chlorooroaane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1 4-Dichlorobenzene 106-46-7
l 2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichloroditluoromethane 75-71-8
l 1-Dichloroethane 75-34-3
1.2-Dich loroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
l 2-Dichlorooronane 78-87-5
1 3-Dichloroorooane 142-28-9
2 2-Dichloronrooane 594-20-7
1.1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-I 3-Dichloronronene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWD998
2010213416
Cone Flaa
ND t.A.1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND \A. "3'
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL RL .
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 0.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
020IHBWD999 0201HBWD999
2010213403 2010213403,
Cone Flaa·. DL RL' . . . . Cone·· Fla if ·,01.:,.;· RL
N' ~ R 6.:;.'; v .... ND \.A-:1 0.635. 0.000
N~ 3.88 0.0 0 l ND 0.388 0.000
N'> 8.90 0.0 0) ND 0.890 0.000
N> 4.87 0.01 ) ND 0.487 0.000
N) 27.4. 0.0 0 ND 2.74 0.000
N> 7.00 0.0 10 ND 0.700 0.000
N) 6.85 . 0.1 10 ND 0.685 0.000
N) 7.40 0. oo· ND 0.740 0.000
.N) 39.0 0. 00 ND 3.90 0.000
N) 7.50 omoo ND 0.750 0.000
NG 4.82 « 000 ND 0.482 0.000
1' [) 4.23 1.000 ND 0.423 0.000
l' [) 11.8 I .000 ND 1.18 0.000
2 15 6.20 hooo 164 0.620 o.ooo·
1' n 5.10 ./o.ooo ND 0.510 0.000
l '.3 t 6.10 I o.ooo 16.7 0.6-10 0.000
l .6 'J 5.60 I o.ooo 11.9 0.560 0.000
l' D 5.95 I o.ooo· 0.424 :r J1 0.595 0.000
l\D 4.34 I 0.000 ND 0.434 0.000
l\D 6.75 0.000 ND 0.675 0.000
1'D 8.00 I 0.000 ND 0.800 0.000
l\ [) 4.97 I 0.000 ND 0.497 0.000
Nn 4.09/ 0.000 ND 0.409 0.000
1' D 4.5tf 0.000 ND 0.454 0.000
1' D 5.M 0.000 ND 0.505 0.000
D 6.to 0.000 ND 0.680 0.000
HD lb.6 0.000 ND \A.J l.66 0.000
ff') ,V --ND 0.845 0.000 o.-+ u. JVU
Page 5 of
Sample rc,ults have been qualified by URS-Radian based on the results of lhc daia review prnccss, which is modeled afler th<' N111io1111/ F1111c111m11/ G11iile/111esfur Organic 11111/ lnorg1111ic JJ11111 R.:1·i1·11·
66
--USEPA:Octoberiiidfcbruafll994,resrec1ivcly)-- - - - - - - - - - - -
-------------------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter . CAS'
Iodomethane 74-88-4
lsoorooylbenzene 98-82-8
4-IsoorooYltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methyl tert-butvl ether <MTBE) · 1634-04-4
4-Methvl-2-oentanone (MIBK) l 08-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Propanenitrile 107-12-0
n-Propylbenzene 103-65-1
Stvrene 100-42-5
1.1.1.2-Tetrachloroethane 630-20-6
l l.2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahydrofuran 109-99-9
Toluene 108-88-3
l 2 3-Trichlorobenzene 87-61-6
1.2 4-Trichlorobenzene 120-82-1
l l I -Trichloroethane 71-55-6
1.1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2.3-Trichloroorooane 96-18-4
1, l ,2-Trichlorotritluoroethane 76-13-1
1.2.4-Trimethylbenzene 95-63-6
1.3.5-Trimethvlbenzene 108-67-8
Vinyl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -03/05/2001 13:42
020 l HBWD998
2010213416
... . . ·cone Ftaa
ND
ND
ND
ND
ND
ND
ND s
ND \,\~
ND
.ND
ND
ND
ND
ND
ND
ND
ND \.A.3
ND I k '.\
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STL Austin
DL RL ..
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 6.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123. 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114. 0.000
020 IHBWD999 020IHBWD999
2010213403 2010213403
.. Cone Flaa· DL .. "· RL: , ~' cone ;-.filici~"';Dl{1.~·.;. ·. RL '
-NI R. ~o ND 0.545 0.000
NI 4.66 0.0 ~o ND 0.466 0.000
NI) 5.75 o.c [)0 ND 0.575 0.000
NI > 6.55 0.( 00 ND 0.655 0.000
N> 5.80 o.boo ND -0.580 0.000
N> 8.90 olooo ND :_o.890 0.000
NI:> a 6.30 ".000 ND ~ .:~-0.630 0.000
N) 4.00 .O.ooo ND \I\_\ 0.400 0.000
N) 79.5 /0.000 ND 7.95 0.000
Nb 7.00 I o.ooo ND 0.700 0.000
ND 4.88 I o.ooo ND 0.488 0.000
ND 5.55 I 0.000 ND 0.555 0.000
ND 4.35 I 0.000 ND 0.435 0.000
N) 1.20 I 0.000 ND ...,... 0.720 0.000
]\ I) 45.0/ 0.000 ND 4.50 0.000
1'.D 3.1&' 0.000 ND 0.318 0.000
1'D 27.~ 0.000 ND u:r 2.76 0.000
1' [) 6.'Z#, 0.000 ND 1.)..:\ 0.675 0.000
1' n 8.• 5 0.000 ND 0.845 0.000
l\D 4. 0 0.000 ND 0.410 0.000
1' D 61&5 0.000 ND 0.685 0.000
l D 'i/.30 0.000 ND 0.530 0.000
1 D '4.4 0.000 ND 1.44 0.000
JD >.15 0.000 ND 0.615 0.000
1 D t>.20 0.000 ND 0.620 0.000
l'D U2 0.000 ND 0.452 0.000
l D 4.74 0.000 ND 0.474 0.000
1 !4..2 Ji ll( 7(\ I\ 1\1\0 11.6 0.570 0.000
Page 6 of·
Sample results have been qualilicd by URS-Radian based on the results of the data review process, which is modeled after 1/w Nt11io1111/ F1111c11011al G11ide/111esfor Org1111ic 1111d lt10rg1111ic /)a111 Re1•iew
(US EPA, October 1999 and February 1994, respectively).
66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
.CAS··
106-42-3
95-47-6
SECTION IV -Analytical Results -03/05/2001 13:42
020 l HB WD998
2010213416
Cone Flaa
ND
ND
LIMS Workorder: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STL Austin
DL RL
0.167 0.000
0.0844 0.000
0201HBWD999 020 l HB WD999
2010213403 2010213403
Cone Flaa DL RL "Cone . F.li 1ci't-''·'Dt:'l'l : · .. a . .. . ... RL
Mi> g,_ Q ""' ~:UOO ND 0.835 0.000
Nb-. f-_ A.A.-< ~-~00 ND 0.422 0.000
Page 7 of
Sample results have been 4ualilie<l by URS-Radian based on the 1esul1s of the <lala review process, which is modeled after rlw N111io1111/ Fr111crim111/ <J11ide/111esfor Org11111c 11111/ bwrg1111u· [)11111 Rel'iew --USEPA.Octobcr.ndFdilil994,resetivcly-- - - - - - - - - - -
66 -
-------------------
SECTION IV·
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
0201HBWD998
2010213416
Aaueous
Received
NA
02/19/2001 13:35
02/26/2001 12:12
02/26/2001 12:12
1.0000
MSDA
u!!IL
. 020 l HBWD999 020 lHBWD999
2010213403 2010213403
Aaueous Aaueous
Received Received
NA NA
02/20/200 l 08:45 02/20/200 l 08:45
02/26/200113:39 02/26/2001 17:34
02/26/2001 13:39 02/26/2001 17:34
50.0000 5.0000
MSDA MSDA
u!!IL ul?/L
Surroaate Corrlhfturid · .. · %''Recoveni LlinitS .. ~-· >'.' ;.F·~· ! % ReeovaiY :., ;:· ·_ · LlrlilfS~<J'..<sJ~-~1;~'1'~.~f.R) . i:%:'.R.Covervt~·;;~~: um1& · · --: •:·.· ,· .. :-: .. :
l-Bromo-4-fluorobenzene 97
l .2-Dichloroethane-d4 98
Toluene-dB 106
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] llamilton Beach-Proctor Silex
STLAustin
77-117 98
61-143 100
87-113 102
77-117 99 77-117
61-143 96 61-143
87-113 104 87-113
Page 8
Sample results have been qualified by URS-Radian based on the results ofthc data review process, which is modeled atier 1he Nmio1111/ F1111c1w11al G11ide/i11esfor Organic 11111l bw1:ir,1111ic Daw Re1•11•11•
(US EPA, October 1999 and February 1994, respectively).
of
F
66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
., CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW213
2010213404
Aqueous
Received
NA
02/20/200 I 09:05
02/26/2001 13:09
02/26/200 I 13 :09
5.0000
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
0.465 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND l,\.:S B
ND
ND
ND
ND
ND
ND
LIMS Workordcr: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL RL
2.19 0.000
34.1 0.000
19.0 0.000
2.23 0.000
0.320 0.000
0.499 0.000
0.655 0.000
0.590 0.000
0.850 0.000
0.995 0.000
1.00 0.000
0.510 0.000
0.525 0.000
0.456 0.000
0.342 0.000
0.326 0.000
0.570 0.000
0.421 0.000
0.462 0.000
0.448 0.000
0.469 0.000
0201HBWW214 0201HBWW215
2010213402 2010213401
Aaueous Aaueous
Received Received
NA NA
02/20/200 I 08:40 02/20/200 I 08:20
02/26/2001 12:41 02/23/200 I I 0:20
02/26/2001 12:41 02/23/200 I l 0:20
5.0000 1.0000
MSDA MSDA
U!!/L ul!.!L
.. Cone Flaa , ,,·DI:.· :i.~:~" "' Rt:·,:·::,: :,, ::·cdricf · ·:Flaa,. DL:· RL
ND 2.19 0.000 ND 0.438 0.000
ND 34.l 0.000 ND (A-S 6.82 0.000
ND 19.0 0.000 ND (Aj 3.79 0.000
ND· 2.23 0.000 ND 0.446 0.000
0.396 J 0.320 0.000 ND 0.0641 0.000
ND 0.499 0.000 ND 0.0998 0.000
ND 0.655 0.000 ND 0.131 0.000
ND 0.590 0.000 ND 0.118 0.000
ND 0.850 0.000 ND l.A'l 0.170 0.000
ND 0.995 0.000 ND lA.::r 0.199 0.000
ND 1.00 0.000 ND 0.200 0.000
ND 0.510 0.000 ND 0.102 0.000
ND 0.525 0.000 ND 0.105 0.000
ND . 0.456 0.000 ND 0.0911 0.000
ND IA.J It 0.342 0.000 1.13 L-l~ l'JD B ().;Q684 6.000
ND 0.326 0.000 ND 0.0652 0.000
ND 0.570 0.000 ND 0.114 0.000
ND 0.421 0.000 ND 0.0842 0.000
ND 0.462 0.000 ND 0.0925 0.000
ND 0.448 0.000 ND 0.0896 0.000
ND 0.469 0.000 ND 0.0938 0.000
Page 9 of 66
-Sample results have been qualified by URS-Radian based on the results of the dala 1cv1cw process, which is modeled alicr 111<' N111i111111/ F1111c1i111111/ G11ide/111esfur Org1111ic 11111/ /Jwrg11111c l>altl Rel'i•·11·
... USE .. l<:ber-dFcbruaryl994,-ivcly)-- - - - - - - -· - - - -
-------------------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0201HBWW213
2010213404
.' >sParameter :.: . ·· , : . 't~ ~-. ~ .';f· ,;.;t,>~C'AS'£fftfl~?:: ;~conc:'.~:.IFlacf :'. Dl!'~!,: .. :;!\RL:·:v.:''.ifri:Oi
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
I 2-Dibromo-3-chloroorooane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
I 2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-I 4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 ND
1.2-Dichlorobenzene 95-50-1 ND
1.3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 ND
1.1-Dichloroethane 75-34-3 173
1.2-Dichloroethane 107-06-2 3.68
1.1-Dichloroethene 75-35-4 433
cis-l .2-Dichloroethene 156-59-2 37.1
trans-I 2-Dichloroethene 156-60-5 0.937
1.2-Dichloronrooane 78-87-5 ND
1.3-Dichloroorooane 142-28-9 ND
2.2-Dichloroorooane 594-20-7 ND
Ll-Dichloroorooene 563-58-6 ND
cis-1 3-Dichlorooronene 10061-01-5 ND
trans-1.3-Dichloroorooene 10061-02-6 ND
Ethvl methacrvlate 97-63-2 ND
Ethvlbenzene 100-41-4 0.170
Hexachloro-1 3-butadiene 87-68-3 ND
2-Hexanone 591-78-6 ND
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907 .0 I (20102134) Hamilton Beach-Proctor Silex
STLAuslin
LA::S 0.635 0.000
0.388 0.000
0.890 0.000
0.487· 0.000
2.74 0.000
0.700 0.000
0.685 0.000
0.740 0.000
3.90 0.000
0.750 0.000
0.482 0.000
0.423 0.000
l.18 0.000
0.620 0.000
0.510 0.000
0.610 0.000
0.560 0.000
J 0.595 0.000
0.434 0.000
0.675 0.000
0.800 0.000
0.497 0.000
0.409 0.000
0.454 0.000
0.505 0.000
:j"' li'.1' 0.680 0.000
lA.."S 1.66 0.000
0.845' 0.000
0201HBWW214 0201HBWW215
2010213402 2010213401
:cone:~ ·: ·:·F1aa·;;·1,·~oa.::);~~\r~~:~~~~f!£ ~~«::<iric"\~ :\:J~e1r~ol!~st:1~.;Rl:·>·
ND l,\. "3" 0.635 0.000 ND lJ-. '! 0.127 0.000
ND 0.388 0.000 ND 0.0777 0.000
ND 0.890 0.000 ND 0.178 0.000
ND 0.487 0.000 ND 0.0974 0.000
ND 2.74 0.000 ND \;\.J .0.548 0.000
ND 0.700 0.000 ND ~.0.140 0.000
ND 0.685 0.000 ND _,_0.137 0.000
ND 0.740 0.000 ND 0.148 0.000
ND 3.90 0.000 ND 0.780 0.000
ND 0.750 0.000· ND 0.150 0.000
ND 0.482 0.000 ND 0.0965 0.000
ND 0.423 0.000 ND 0.0846 0.000
ND Us 0.000 ND 0.237 0.000
162 0.620 0.000 3.55 -~,_0.124 0.000.
ND 0.510 0.000 ND ,.0.102 0.000
16.8 0.610 0.000 '2.38 0.122 0.000
12.9 0.560 0.000 ND 0.112 0.000
0.708 J 0.595 0.000 ND 0.119 0.000
ND 0.434 0.000 ND 0.0869 0.000
ND 0.675 0.000 ND 0.135 0.000
ND 0.800 0.000 ND 0.160 0.000
ND 0.497 0.000 ND 0.0994 0.000
ND 0.409 0.000 ND 0.0818 0.000
ND 0.454 0.000 ND 0.0908 0.000
ND 0.505 0.000 ND 0.101 0.000
ND 0.680 0.000 ND 0.136 0.000
ND IA "J' 1.66 0.000 ND lA"l 0.331 0.000
ND 0.845 0.000 ND lA.J 0.169 0.000
Page 10 of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is mudded a lier rlw N111i111111/ F111wtiu1111/ G11ide/i11esjur Org1111ic mui /11org1111ic JJ11111 Re1•ie11•
(US EPA, October 1999 and February 1994, respectively).
bb
SECTION IV
Analytical Results
MS·VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CA$
Iodomethane 74-88-4
Isonroovlbenzene 98-82-8
4-lsooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-oentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Pronanenitrile 107-12-0
n-Proov lbenzene 103-65-1
Stvrene 100-42-5
1. l. l .2-Tetrachloroethane 630-20-6
l. l 2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2.3-Trichlorobenzene 87-61-6
1.2.4-Trichlorobenzene 120-82-1
LI I-Trichloroethane 71-55-6
l. l 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2 3-Trichloronrooane 96-18-4
l. l .2-Trichlorotrifluoroethane 76-13-1
l 2.4-Trimethv !benzene 95-63-6
I 3.5-Trimethv !benzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW213
2010213404
.... (·) Cone Flaa .
ND
ND
ND
ND
ND
ND
ND B
7.69 ":\
ND
ND
ND
ND
ND
24.8
ND
ND
ND IA-°'S
ND \A-:\
ND
2.68
426
ND
ND
ND
ND
ND
ND
19.2
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.545 0.000
0.466 0.000
0.575 0.000
0.655. 0.000
0.580 0.000
0.890 0.000
0.630 0.000
0.400 0.000
7.95 0.000
0.700 0.000
0.488 0.000
0.555 0.000
0.435 0.000
0.720 0.000
4.50 0.000
0.318 0.000
2.76 0.000
0.675 0.000
0.845 0.000
0.410 0.000
0.685 0.000
0.530 0.000
1.44 0.000
0.615 0.000
0.620 0.000
0.452 0.000
0.474 0.000
0.570 . 0.000
0201HBWW214 0201HBWW215
2010213402 2010213401
Cone Flaa ot: · ·Rt-· Cone Fl~::·{'Dll1~?·,,v1R('
ND 0.545 0.000 ND 0.109 0.000
ND 0.466 0.000 ND 0.0931 0.000
ND 0.575 0.000 ND 0.115 0.000
ND 0.655 0.000 ND 0.131 0.000
ND 0.580 0.000 0.427 J 0.116 0.000
ND 0.890 0.000 ND 0.178 0.000
ND 8 0.630 0.000 ND Ji 0.126 0.000
ND \A.J 0.400 0.000 ND I '-'\ 0.0801 0.000
ND 7.95 0.000 ND 1.59 0.000
ND 0.700 o.ooo· ND 0.140 0.000
ND 0.488 0.000 ND 0.0977 : 0.000
ND 0.555 0.000 ND 0.111 0.000
ND 0.435 0.000 ND l.1..1 0.0870 0.000
ND 0.720 0.000 ND I A J 0.144 0.000
ND 4.50 0.000 6.41 0.900 0.000
ND 0.318 0.000 ND 0.0637 0.000
ND \J\ :r 2.76 0.000 ND l.A.J 0.551 0.000
ND \A,:S-0.675 0.000 ND IA.-:\ 0.135 0.000
ND 0.845 0.000 ND 0.169 0.000
ND 0.410 o.ooo. ND 0.0821 0.000
ND 0.685 0.000 ND 0.137 0.000
ND 0.530 0.000 ND 0.106 0.000
ND l.44 0.000 ND 0.288 0.000
ND 0.615 0.000 ND 0.123 0.000
ND 0.620 0.000 ND 0.124 0.000
ND 0.452 0.000 ND 0.0905 0.000
ND 0.474 0.000 ND Ll..:f 0.0948 0.000
11.8 0.570 0.000 ND 0.114 0.000
Page 11 of 66
Sanipk results have been qualified by URS-Radian based on the results of the data review process, which is mudded after //It' N111io1111/ F1111rno1111/ G11ide/1111•sfur Organic 11111l /11org1111ic D111t1 Re1•11•w
-... USElliiobcriifdFe~994,.ively ... - - - -~ - - - - - - -
-- --- - - ---
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
'.Parameter
o-Xvlene/m-Xvlene
o-Xvlene
,'
Client Sample ID
Lab Sample ID
. :;:;t:As· t{~i!.~f-~:' ·_"r•
106-42-3
95-47-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW213
2010213404
Cone ·~·Flaa·
0.363 u
0.815 j
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAusti11
DL -RC/ ... r
0.835 0.000
0.422 0.000
-- --- - - -
0201HBWW214 0201HBWW215
2010213402 2010213401
cone· Flicf~_i ~DI!·~;·/ ~'.;~~Rl:;i~:}~r~:·~~ .'C-onc '~ ·:, :~.filin~l'kllHil'.i~~.I:l1k'"RL
ND 0.835 0.000 ND 0.167 0.000
ND 0.422 0.000 ND 0.0844 0.000
Page 12 of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled aticr f/w Na1io1111/ F1111c1io1111/ <i11ide/i11esfor Org1111ic 1111d /11arg1111ic /)11//1 Re1•iew
(US EPA, October 1999 and February 1994, respectively). ,
-
66
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Datefflme Collected
Dateffime Prepared
Dateffime Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
1-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-dB
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW213
2010213404
Aaueous
Received
NA
02/20/200 l 09:05
02/26/2001 13:09
02/26/200 l 13 :09
5.0000
MSDA
ul!!L.
·% Reeoverv
100
100
104
LIMS Workorder: 80396907.~l [20102134) Hamilton Beach-Proctor Silex
STLAustin
Llmit8 .. , F
77-117
61-143
87-113
0201HBWW214 020IHBWW215
2010213402 2010213401
Aaueous Aaueous
Received Received
NA NA
02/20/200 l 08:40 02/20/200 l 08:20
02/26/2001 12:41 02/23/200 l 10:20
02/26/2001 12:41 02/23/200 l 10:20
5.0000 l.0000
MSDA MSDA
ul!/L ue:/L
:% Recoverv , Umlt8 -f .. ' ... \ ·"f,.'' -.-.c. Ra.-.nvaw:i ·~ · , · umtta·.: : ..:,,, !'
99 77-117 96 77-117
96 61-143 96 61-143
102 87-113 102 87-113
Page 13
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled alicr 1/w N111imw/ F1111c1io1111/ G11ide/111esji>r Org1111ic 1111d /11org1111ic D11111 Re1•it•11·
F
of 66
--USE-tobcr-ndFcbru3Jl994,respectively .. - - - - - - - - - - - -
-.. - - - - - --:-- --·' - - - - ----
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
·---CAs· -
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW216
2010213415
Aaueous
Received
NA
02/19/2001 15:45
02/26/200 I 11 :44
02/26/2001 11 :44
1.0000
MSDA
ug/L.
. cone·. ·Flaa
ND
ND
ND
ND
ND
ND·
ND
ND
ND
ND
ND
ND
ND
ND
ND \A.~ It
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20!02134) Hamilton Beach-Proctor Silex
STLAuslin
DL ... RC-
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0;000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938. 0.000
0201HBWW220 0201HBWW222
2010213414 2010213409
Aaueous Aaueous
Received Received
NA NA
02/19/2001 14:35 02/19/2001 14:15
02/23/2001 15:45 02/23/200 I 13 :23
02/23/2001 15:45 02/23/2001 13:23
1.0000 1.0000
MSDA MSDA
ul!/L ul!/L
--'CO'nc-~~ · ~:·~,:F.18U1-; ~lo1r~::l t~~~:tr~ ... r:~Li ~ f:conc:s.: :::~~.Elaa:~ ~-ot.: ·~;. ,:·RL'·.
ND 0.438 0.000 ND 0.438 0.000
ND l,\, ..\ 6.82 0.000 ND iA. -:r 6.82 0.000
ND \>..::s .3.79 0.000 ND \.t _"':\ 3.79 0.000
ND 0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.118 0.000 ND -0.118 0.000
ND l.1.."J 0.170 0.000 ND \,I.,;.) 0.170 0.000
ND lA 'J 0.199 0.000 ND u .. :r 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND ·0.0911 0.000 ND 0.0911 0.000
ND \A:S H 0.0684 0.000 ND ~'-3 :H 0.0684 0.000
ND 0.0652. 0.000 ND 0.0652 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND _0.0925 0:000.
ND 0.0896 0.000 ND 0.0896 0.000
ND. 0.0938 0.000 ND 0.0938 0.000
Page 14 of
Sample rcsulls have been qualified by URS-Radian based on the results ul' the data review process, "".hich is 111oddcd after till' N11tio1111/ F1111ctio1111/ <i11uleli11esji11· 01 g1111ic and Jnorg1111ic 1>11111 R1·1·11·11·
(US EPA, October 1999 and February 1994, respectively).
66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter ; ~ CAs··Vi?o-c;~1~~;
Chloromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
1.2-Dibromo-3-chloronronane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-l.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
l.2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
l 2-Dichloroethane 107-06-2
t .1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
l 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
1 1-Dichloroorooene 563-58-6
cis-1 3-Dichloroorooene l 0061-01-5
trans-1.3-Dichlorooronene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -03/05/2001 I3:42
0201HBWW216
2010213415
·cone Flaa
ND L"-.3
ND
ND
ND
ND
ND
ND
ND
ND
·ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND l A '3
ND
LIMS Workorder: 80396907.01 [20!02134] Hamilton Beach-Proctor Silex
STLAustin
DL· ··" RL''·''
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 0:000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
. 0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
0201HBWW220 0201HBWW222
2010213414 2010213409
Cone··:· Flaa·· ·oa:. , ~:·. R.l.t'.;_', '· " 'Con'c "Flan5.~Jn~~'r·~ :' RL
ND \A.J 0.127 0.000 ND \A..":S 0.127 0.000
ND 0.0777 0.000 ND 0.0777 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 0.0974 0.000 ND 0.0974 0.000
ND 1.J,.:3 0.548 0.000 ND \.\ \ 0.548 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.148 0.000 ND 0.148 0.000
ND 0.780 0.000 ND 0.780 0.000
ND 0.150 0.000 ND 0.150 0.000
ND. 0.0965 0.000 ND 0.0965 0.000
ND 0.0846 0.000 ND 0.0846 0.000
ND 0.237 0.000 ND 0.237 0.000 .
0.456 J 0.124 0.000 0.589 0.124 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.122 0.000 0.102 ;:f ~ 0.122 0.000
ND 0.112 0.000 0.222 J 0.112 0.000
ND 0.119 0.000 ND 0.119 0.000
ND 0.0869 0.000 ND 0.0869 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.160 0.000 ND 0.160 0.000
ND 0.0994 0.000 ND 0.0994 0.000
ND 0.0818 0.000 ND 0.0818 0.000
ND 0.0908 0.000 ND 0.0908 0.000
ND 0.101 0.000 ND 0.101 0.000
ND 0.136 0.000 ND 0.136 0.000
ND l ~:) 0.331 0.000 ND \),. 'Y 0.331 0.000
ND \A3 0.169 0.000 ND IA\ 0.169 0.000
Page 15 of 66
Sample icsults have been qualified by URS-Radian based on the rcsulb ul' the data review process, which is mudded aflcr th<' N11111m11/ F1111cti111111/ G11ide/11w~for Org1111ic 1111d /11~1-g1111il' /)tlfa R1•1w11·
-111EUSliilif.lubcr ... ndF.:-1994-·tivcly ... ---> W --·· - - - - - - -
--------~--~-------
SECTION IV
Analytical Results
MS-VOA.
SW8260B
Continued
Client Sample ID
Lab Sample ID
0201HBWW216
2010213415 .
'·."Paranietei"i"P:··~' · c· "'· '-~~: \r'£7:exs:,N:~~-;torfoY-~" 1::·,F1ac.·i-. -'ttL'~~i;;f..·_, "RL:'ii,:;~~r: ~:·
lodomethane 74-88-4 ND
lsooroovlbenzene 98-82-8 ND
4-lsooroovltoluene 99-87-6 ND
Methvl methacrvlate 80-62-6 ND
Methvl tert-butvl ether (MTBE) 1634-04-4 ND
4-Methvl-2-oentanone (MIBK) 108-10-1 ND
Methvlene chloride 75-09-2 ND
Naohthalene 91-20-3 ND
Prooanenitrile 107-12-0 ND
n-Proovlbenzene 103-65-1 ND
Stvrene 100-42-5 ND
1.1 1.2-Tetrachloroethane 630-20-6 ND
1.1.2 2-Tetrachloroethane 79-34-5 ND
Tetrachloroethene 127-18-4 ND
Tetrahvdrofuran 109-99-9 ND
Toluene 108-88-3 ND
1 2.3-Trichlorobenzene 87-61-6 ND
1.2 4-Trichlorobenzene 120-82-1 ND
1.1 I -Trichloroethane 71-55-6 ND
1.1 2-Trichloroethane 79-00-5 ND
Trichloroethene 79-01-6 ND
Trichlorofluoromethane 75-69-4 ND
1.2 3-Trichlorooronane 96-18-4 ND
l. l .2-Trichlorotrifluoroethane 76-13-1 ND
1.2.4-Trimethv lbenzene 95-63-6 Nb
1.3.5-Trimethv I benzene 108-67-8 ND
Vinvl acetate 108-05-4 ND
Vinvl chloride 75-01-4 ND
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STL Austin
0:109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
B 0.126 0.000
I A-:f 0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 0:000
0.0637 0.000
\A."::S 0.551 0.000
IA .. -:\ 0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114 . 0.000
020 I HBWW220 0201HBWW222
2010213414 2010213409
...-con&:;_·,~·-:FtaatJ'ti;l>L~~s~i~~~~~r~r. tCCfniVi:ifi'.-lil!•I : ~~Rt.1·
ND 0.109 0.000 ND 0.109 0.000
ND 0.0931 0.000 ND 0.0931 0.000
ND 0.115 0.000 ND 0.115 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.116 0.000 ND 0.116 0.000
ND 0.178 0.000 ND ·0.118 0.000
ND B 0.126 0.000 ND B' "''0.126 0.000
ND (.I. --:r 0.0801 0.000 ND u..-:r 0.0801 0.000
ND 1.59 0.000 ND 1.59 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.0977 0.000 ND 0.0977 .·0.000
ND 0.111 0.000 ND 0.111 0.000
ND \,)\.~ 0.0870 0.000 ND iA.1 0.0870 0.000
ND \A.-S 0.144 0.000 ND l,\, 'J 0.144 0.000
ND 0.900 0.000 ND ·0.900 0.000
ND 0.0637 0.000 ND 0.0637 0.000
ND IA~ 0.551 0.000 ND \A"! 0.551 0.000
ND \A.3 0.135 0.000 ND I,\~ 0.135 0.000
ND 0.169 0.000 ND 0.169 0.000
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.288 . 0.000 ND 0.288 0.000
ND 0.123 0.000 ND 0.123 0.000
ND 0.124 0.000 ND 0.124 0.000
ND 0.0905 0.000 ND 0.0905 0.000
ND \J\.0° 0.0948 0.000 ND lA. :::5 0.0948 0.000
ND 0.114 0.000 ND 0.114 0.000
Page 16 of
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled after rlt<' N111im111/ F1111crio11a/ G11ideli11l'sfor Vrga11ic t111tl /norg1111ic /)11/t1 Re1•i1'l1·
(US EPA, October 1999 and February 1994, respectively).
66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter·
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAS ·,
106-42-3
95-47-6
SECTION JV -Analytical Results -03/05/2001 13:42
0201HBWW216
2010213415
Cone. Flaa
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.167 0.000
0.0844 0.000
020 l HBWW220 0201HBWW222
2010213414 2010213409
Cone Flaa· 'DL •,•RL:' ·:,· ., Cone Fl'lilr."~·?o~~l' . 'RL
ND 0.167 0.000 ND 0.167 0.000
ND 0.0844 0.000 ND 0.0844 0.000
Page 17 of 66
Sample results have been qualified by URS-Radian based on the results of the daw review process, which is modeled a tier th<' N111io1111/ F1111c1io1111/ G11ule/u1esfur Orgmuc 11111/ bwrgm1ic 1>11111 Ht•1•ie11·
-... USE~.ubcriiifdFcw.'994,.ivcly ... --1 ·----------
------------------ - -..
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
°lo Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surtoaate Comoound
1-Bromo-4-fluorobenzene
I .2-Dichloroethane-d4
Toluene-dB
0201HBWW216
2010213415
Aoueous
Received
NA
02/19/2001 15:45
02/26/200 l 11 :44
02/26/200 l 11 :44
1.0000
MSDA
ug/L
% Recover\t'
98
98
103
SECTION IV -Analytical Results -03/05/2001 13:42 .
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAustin
Limits -F
77-117
61-143
87-113
0201HBWW220 0201HBWW222
2010213414 2010213409
Aoueous Aaueous
Received Received
NA NA
02/19/2001 14:35 02/19/2001 14:15
02/23/2001 15:45 02/23/2001 13 :23
02/23/2001 15:45 02/23/2001 13 :23
1.0000 1.0000
MSDA MSDA
ug/L ug/L
: % Recovarv · · :;; :(lriiftSJ:n;1~~ .. ::·; .. '. F.. .:~iffecoveni · : .. ·:.t:1m1ts ·
96 77-117 96 77-117
102 61-143 97 61-143
101 87-113 103 87-113
Page 18
Sample results have been qualified by URS-Radian based on the results of the data review process, which is mudded after th<' National F1111ctio11a/ G11idt:lill<'Sfor Org1111ic and Inorg1111k l>alil Re1•it'11·
(US EPA, October 1999 and February 1994, respectively).
;: .. · F
of
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrv lonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chioro-l .3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
°lo Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-l
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW224
2010213412
Aaueous
Received
NA
02/19/2001 15:10
02/2312001 14:47
02/23/2001 14:47
1.0000
MSDA
ug/L··
Cone Flaa
ND
ND \A.J
ND LA..'\
ND
ND
ND
ND
ND
ND \J\3
ND \/\ 'J
ND
ND
ND
ND
0.571 U.1 rtD J8'
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STL Austin
DL RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 6.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.08M' 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
020 I HBWW225 0201HBWW226
2010213413 2010213410
Aaueous Aaueous
Received Received
NA NA
02/19/2001 15:15 02/19/2001 13:30
02/23/2001 15:15 02/23/2001 13:51
02/23/2001 15:15 02/23/2001 13:51
1.0000 l.0000
MSDA MSDA
uf!!L uf!!L
~,. ' Cone· Flltl ''OL". ~: ''Rt ~ ·.' ·· "Coric .. _; .. "Fliii ... :; DL " RL· ..
ND 0.438 0.000 ND 0.438 0.000
ND vJ 6.82 0.000 ND lA:J 6.82 0.000
ND lA--:l" 3.79 0.000 ND tA::S 3.79 0.000
ND 0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.118 0.000 ND 0.118 0.000
ND I.A. J 0.170 0.000 ND H-:T 0.170 0.000
ND \A'S 0.199 0.000 ND t,\..3 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND . 0.0911 0.000 ND 0.0911 0.000 0.511\.l~ND .18' o~ 0.000 ND IA."\: JI{ 0.0684 0.000
ND 0.0652· 0.000 ND 0.0652 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND 0.0925 0.000
ND 0.0896 0.000 ND 0.0896 0.000
ND. 0.0938 0.000 ND 0.0938 0.000
Page 19 of 6b
Sample results have been qualified by URS-Ra1han based on 1he results uf lhc dala 1cvicw process, which is mudded atkr Iii<' N11111111ttl F1111c1ic11111/ <.l11idl'l111L'sfur Organic mu/ ltwrg1111ic /)l//11 Re1•it'11·
-lllllJ..ISE-tubcriii11dFc .. 994, .. ivcly .. --- -~ ---- -- -
------~--------~-~-
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
·-Parameter .. .. ':: •::rtcAs· :.:;~.rt!€~~: ;. ...
Chloromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
I 2-Dibromo-3-chlorooronane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane . 74-95-3
trans-l .4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
l.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
l .1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
l 1-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichloroorooane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
l 1-Dichloroorooene 563-58-6
cis-1 3-Dichlorooronene 10061-01-5
trans-1.3-Dichloronrooene 10061-02-6
Ethv I methacrv late 97-63-2
Ethv lbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW224
2010213412
~cone" "! ·Flaa·
ND \f\. '"S
ND
ND
ND
ND \A 1°
ND
ND
ND
ND
·ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND \A:S
ND \,\\
LIMS Workorder: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STLAustin
: DL"f. "': · '.'RI.;/ :~ ·'.!.& •
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 {)'.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169. 0.000
0201HBWW225 020IHBWW226
2010213413 2010213410
coricf'"~ ··:Flaa··. ·01S·'.i::'7:-'.(.;RJtf~~f: ·;?;,·~ '.'bone"'.·; ~Ffi'n~f>ll~l~f~~RL
ND v...s 0.127 0.000 ND v":r 0.127 0.000
ND 0.0777 0.000 ND 0.0777 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 0.0974 0.000 ND 0.0974 0.000
ND IA.J 0.548 0.000 ND \AT 0.548 0.000 . -· ND 0.140 0.000 ND 0.140 0.000 ...
ND 0.137 0.000 ND 0.137 0.000
ND 0.148 0.000 ND 0.148 0.000
ND 0.780 0.000 ND 0.780 0.000
ND 0.150 0.000 ND 0.150 0.000
ND' 0.0965 0.000 ND 0.0965 0.000
ND 0.0846 0.000 ND 0.0846 0.000
ND 0.237 0.000 ND 0.237 0.000.
ND 0.124 0.000 ND 0.124 0.000 . ...
ND 0.102 0.000 ND 0.102 0.000
ND 0.122 0.000 ND 0.122 0.000
ND 0.112 0.000 ND 0.112 0.000
ND 0.119 0.000 ND 0.119 0.000
ND 0.0869 0.000 ND 0.0869 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.160 0.000 ND 0.160 0.000
ND 0.0994 0.000 ND 0.0994 0.000
ND 0.0818 0.000 ND 0.0818 0.000
ND 0.0908 0.000 ND 0.0908 0.000
ND 0.101 0.000 ND 0.101 0.000
ND 0.136 0.000 ND 0.136 0.000
ND Ll. J 0.331 0.000 ND \/\\ 0.331 0.000
ND \A..'S 0.169 0.000 ND IA I 0.169 0.000
Page 20 of
Sample results have been 41.alificd by URS-Radian based on the results of thc data rc,·icw process, which is mudded after the N111io11a/ F111u·1io111rl G11ideli11cs fur Organic and /11u1go11ic 0/1/a Rc1•i1'11·
(US EPA, October 1999 and February 1994, respectivdy).
00
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter · ;, ·cAS-~T.
lodomethane 74-88-4
lsooronvlbenzene 98-82-8
4-lsooroov !toluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) '· 1634-04-4
4-Methvl-2-oentanone lMIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
L 1.1 2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Tri ch lorobenzene 87-61-6
I 2.4-Trichlorobenzene 120-82-1
1.1 I-Trichloroethane 71-55-6
1.1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
I 2 3-Trichlorooronane 96-18-4
1.1.2-Trichlorotrifluoroethane 76-13-1
1.2.4-Trimethv !benzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -03/05/2001 13:42
0201 HBWW224
2010213412
. ~' Cone Flaa
ND
ND
ND
ND
ND
ND
ND B
ND ~
ND
ND
ND
ND
ND \A-"3
ND IA-:S·
ND
ND
ND lA.:5
ND I.A.-:\
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STL Austin
DL RL
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 ·<>.ooo
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114. 0.000
0201HBWW225 0201 HBWW226
2010213413 2010213410
Cone Flaa· ·Dl· RL',. Cone ' :•F.IA~ .. ·r~1.oi;:.,1; RL
ND 0.109 0.000 ND 0.109 0.000
ND 0.0931 0.000 ND 0.0931 0.000
ND 0.115 0.000 ND 0.115 0.000
ND 0.131 0.000 ND : 0.131 0.000
ND 0.116 0.000 ND 0.116 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 8 0.126 0.000 ND If 0.126 0.000
ND IA."S 0.0801 0.000 ND IA."T 0.0801 0.000
ND 1.59 0.000 ND 1.59 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.0977 0.000 ND 0.0977 . 0.000
ND 0.111 0.000 ND 0.111 0.000
ND \.,\,0 0.0870 0.000 ND IA J 0.0870 0.000
ND \A. '"S 0.144 0.000 ND IA\ 0.144 0.000
ND 0.900 0.000 ND 0.900 0.000
ND 0.0637 0.000 ND 0.0637 0.000
ND '" '3 0.551 0.000 ND \J\, J 0.551 0.000
ND I II. -:S 0.135 0.000 ND lA.:S-0.135 0.000
ND 0.169 0.000 ND 0.169 0.000
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.288 0.000 ND 0.288 0.000
ND 0.123 0.000 ND 0.123 0.000
ND 0.124 0.000 ND 0.124 0.000
ND 0.0905 0.000 ND 0.0905 0.000
ND 0.0948 0.000 ND 0.0948 0.000
ND 0.114 0.000 ND 0.114 0.000
Page 21 of 66
Sample results have been qualified by URS-Radian based on the results of thi: data review process, which is modeled a tier the N111io1111/ F1111c1io1111/ (i11ide/111esfor Organic muf lnorga11ic /)11111 Re1•it'11•
-... USE'MtoberiifdFc'llfl994,.ivcly-- -- -·-- -... -·-- -
-.. -- -
-.. - --
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0201HBWW224
2010213412
··:parameter'·· "·. ' . ' ~·: · ;tf~fc.As ~~i-l!~·:#.{$: !'Con·c .· Flaa :: .. DL: · .: ..
p-Xvlene/m-Xvlene 106-42-3 ND
o-Xvlene 95-47-6 ND
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAuslin
0.167
0.0844
. · . '"RC 'i .: ·" :_;:.-.
0.000
0.000
-- ---- --
0201HBWW225 020 IHBWW226
2010213413 2010213410
1:Coric~;~~:-~ Flia~~Dll'.?'.~;~~t~RE~it~~~~ 1~~6nct~;. :;:~;eta~~" D~i}RC;
ND 0.167 0.000 ND 0.167 0.000
ND 0.0844 0.000 ND 0.0844 0.000
Page 22 of
Sample results have been qualified by URS-Radian based on the results ufthc data review process, which is modeled after 1/w N111io11al F1111c1iv1111/ G11ideli11esfor Org1111ic 11ml ltwrg1111ic 1>11111 Re1•ie11•
(US El' A, Octqbcr 1999 and February 1994, respectively).
-
66
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTlme Prepared
DatefTlme Analyzed
Dilution Factor
Instrument
·Units
· · Surrnnate:comnnund ' · ~\~J ",: ~~
l-Bromo-4-fluorobenzene
l .2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW224
2010213412
Aoueous
Received
NA
02/19/2001 15:10
02/23/2001 14:47
02/23/2001 14:47
1.0000
MSDA
u!!IL
.% Recoveri
96
100
102
LIMS Workorder: 80396907.01 (20102134) Hamilton Beach-Proctor Silex
STl.Austin
Limits· J' .. ·. · ff?
77-117
61-143
87-113
0201HBWW225 0201HBWW226
2010213413 2010213410
Aoueous Aaueous
Received Received
NA NA
02/19/2001 15:15 02/19/2001 13:30
02/23/2001 15: 15 02/23/2001 13 :51
02/23/2001 15: 15 02/23/2001 13:51
1.0000 1.0000
MSDA MSDA
U!!IL u!!IL
%·Recoven,.,J', Umlti~-l':t~,,., .-. 3':e; ,.~ ·R~v•fti" .. -, Tfimh" .•. ·-· F ~""'•:4-• ,•,,.,,~,a'-ot• f ~ ~ ' -•i.:t •I
97 77-117 98 77-117
98 61-143 100 61-143
103 87-113 100 87-113
Page 23 of 66
Sample results have been qualified by URS-Radian based on the results of the data review process, which is modeled after rh<' N111w1111/ F111u·1w11lll G11ide/111e~Jor Orgmuc 1111d Jiwrgm1ic l>lllll Re1•1t'll'
-~USE-tober-1dFc-1994,-tivcly-- -- - -·-- - - - - -
-------------~-----SECTION IV
Analytical Results
MS-VOA
SW8260B
-Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chlorofonn
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTlme Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
-CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
020 I HBWW227
2010213405
Aaueous
Received
NA
02/20/200 I 09:35
02/26/2001 14:09
02/26/2001 14:09
50.0000
MSDA
ug/L·
·:cone Flaa
Mt R
N[
NI
NI D
NI ~
N >
N~
N~
N>
ND
ND
ND
Nb
ND
!'lb 8
} 0
1' D
1 D
: ru
lD
]LU;}. II/
LIMS Workordcr: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STLAuslin
Dl' ~;::"·". R(. ·:; '.'::·.'
-,,.. """'"" .G 1.::> v. JVW'
341 0.01 h
190 0.01 0
22.3 o.ono
3.20 O.DOO
4.99 <Y.ooo
6.55 6.ooo
5.90 /6.000
8.50 I o.ooo
9.95 I o.ooo
10.0 I o.ooo
5.10 I 0.000
5.25 I 0.000
4.56 I 0.000
3.42 / 0.000
3.26/ 0.000
5.7d 0.000
4_2j 0.000
4~lh 0.000
4.lt8 0.000 ,i ,.n n ,,,.,,,..,,,,.
0201HBWW227 0201HBWW228
2010213405 2010213406
Aaueous Aaueous
Received Received
NA NA
02/20/200 I 09:35 02120/200 I 09:45
02/26/2001 18:07 02/26/2001 14:37
02/26/2001 18:07 02/26/2001 14:37
10.0000 200.0000
MSDA MSDA
U!!/L ul!/L
cone· Flaa·' "':DL ·.; ' . RL:·.(-.' . . ~·cone:'.· ·"Flaa. Di.' ' RL
ND 4.38 0.000 ND 87.6 0.000
ND 68.2 0.000 Mt Q -----·-v. " u
ND 37.9 0.000 N£ 758 0.0 0
ND 4.46 0.000 N[ 89.2 o.c JO
ND 0.641 0.000 30. 1 12.8 0.1 00
ND 0.998 0.000 ND 20.0 0.1 00
ND l.31 0.000 ND -26.2 0. ~00
ND 1.18 0.000 N[ -· 23.6 0 000
ND l.70 0.000 NI 34.0 O,O 00
ND l.99 0.000 NI 39.8 <i.ooo
25.2 "J 2.00 0.000 41 y 40.0 I .000
ND l.02 0.000 31 5 ,_.,. 20.4 j}.000
ND l.05 0.000 Nib I 21.0 /0.000
ND . 0.911 0.000 N~ 18.2 I o.ooo
ND IA.1 B 0.684 0.000 ND g 13.7 I o.ooo
ND 0.652." 0.000 Nl 13.0 I 0.000
ND 1.14 0.000 ND 22.8 I 0.000
ND 0.842 0.000 Nb 16.8/ 0.000
24.6 0.925 0.000 6ti.3 -, 18.1 0.000
ND 0.896 0.000 ~D l 7FJ 0.000
ND 0.938 0.000 &o ,,, 1~;; \J.UUU
Page 24 of
Sample results have been qualified by URS-Radian based on the results of 1hc dala review process, which is modeled alicr the No1w1111/ F1111criomtl G11idelme~'for Org1111ic 111111 /11org1111ic Oa111 Rc:1•iew
(US EPA, October 1999 and February 1994, respectively).
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter ·: :. CAS ''~:·:·>:.·.
Chloromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
I .2-Dibromo-3-chloronronane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1 4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
1 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
I 2-Dichloronrooane 78-87-5
I 3-Dichlorooronane 142-28-9
2.2-Dichloroorooane 594-20-7
1.1-Dichloronrooene 563-58-6
cis-1.3-Dichloronronene 10061-01-5
trans-I 3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -03/05/200I I3:42
0201HBWW227
2010213405
Cone Flaa
NtJr ~
NT
Nr
NI
NII
N >
N)
1' n
1 D
. ] D
D
'm
~ ~;
2300
~· J R
39£
281
4.1 1:: l1
ND
ND
ND
ND
NI::
NI
N
N '>
N)
~ '
LIMS Workorder: 80396907.01 [20!02134) Hamilton Beach-Proctor Silex
STLAustin
DL RL·;
£ ,.,, 1110 or.:r.: u.
3.88 0.0 ho
8.90 o.~ 00
4.87 11.ooo
27.4 .O.ooo
7.00 /0.000
6.85 I o.ooo
7.40 I 0.000
39.o I 0.000
7.5f/ 0.000
4.82 0.000
4h3 0.000 "' -,,. ---
& .-.u v.
6.20 0.000
"' "' ,,,,. -- --· .. -v.
6.10 o.ot'lo
5.60 oA>oo
5.95 0.000
4.34 /o.ooo
6.75 I o.ooo
8.00 I o.ooo
4.97 I 0.000
4.09 I 0.000
4.54/ 0.000
5.0t 0.000
6.tO 0.000
Y6.6 0.000
lo ·~ u . .00
0201HBWW227 0201HBWW228
2010213405 2010213406
·Cone·· Flaa ··oL "RL ; .. Cone " ··t:lia;~.f. DL:.(~: : RL
ND \;\. --:s , 1.27 0.000 NH , 2.; • ..;. ~.;;oo ' ND 0.777 0.000 N' 15.5 <Y.ooo
ND 1.78 0.000 N> 35.6 l>.ooo
ND 0.974 0.000 N) 19.5 /o.ooo
ND 5.48 0.000 ND 110 I o.ooo
ND 1.40 0.000 1\ D 28.0 I o.ooo
ND 1.37 0.000 1'D 27.4 I 0.000
ND 1.48 0.000 lD 29.6/ 0.000
ND 7.80 0.000 1' D 156/ 0.000
ND 1.50 0.000 D 30.-0 0.000
ND' 0.965 0.000 ~D 14'.3 0.000
ND 0.846 0.000 ~D '16.9 0.000
ND 2.37 0.000 blQ 1.-I'( ~;-. 0.UUll
H89 ~R 1.2!4 '8.860 10200 24.8 0.000.
10.8 1.02 . 0.000 ~~ J I( --L\l."t U.•ur•O
332 1.22 0.000 28• 00 RR 24.4 o.hoo
240 1.12 0.000 28' 0 22.4 <f.ooo
5.48 1.19 0.000 NI: 23.8 lt.000
ND 0.869 0.000 ND 17.4 j).000
ND 1.35 0.000 ND 27.0 /0.000
ND 1.60 0.000 ND 32.0 I o.ooo
ND 0.994 0.000 NC 19.9 I 0.000
ND 0.818 0.000 NI:: 16.4 I 0.000
ND 0.908 0.000 Nl 18.2 I 0.000
ND 1.01 0.000 N > 20.2/ 0.000
ND 1.36 0.000 7'9 27.'i 0.000
ND \A.-:l 3.31 0.000 ND 66/l. 0.000
ND 1.69 0.000 Ne 'V 3.,/0 --U •. nl\J
Page 25 of 66
Sample icsults have been 4ualilicd by URS-Radian based on the results of the data review process, which is modeled after rht• N111w111il Fz111c1w1111/ G1111/e/111esfor Org1111ic 111111 /lwrg11111c Daw Re1·i<'w
-.. USE .. _tober .. ndFe .. 1994,-tivelrlm - - - - - -.. - - - - -
------~--~---------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0201HBWW227
2010213405
· · : Parainele·r ,.. · · ... ~ ..... t', ·'l~~~0As::.:~~:1r'.i~ ·cone 1;·· 'Flaa"'!"' DL;''''i' '~:·RL.
lodomethane 74-88-4 +ff
lsoproov !benzene 98-82-8 N[
4-Isooroov I toluene 99-87-6 NI
Methvl methacrvlate 80-62-6 NI
Methvl tert-butvl ether <MTBE) · 1634-04-4 Nr
4-Methvl-2-oentanone <MIBK) 108-10-1 NI
Methvlene chloride 75-09-2 NI•
Naohthalene 91-20-3 N!>
Prooanenitrile 107-12-0 N >
n-Proovlbenzene 103~65-l ND
Stvrene 100-42-5 N)
I. 1 .1.2-Tetrachloroethane 630-20-6 ND
1.1.2.2-Tetrachloroethane 79-34-5 ND
Tetrachloroethene 127-18-4 JI,()
Tetrahvdrofuran 109-99-9 1' D
Toluene 108-88-3 P.3
1.2 3-Trichlorobenzene 87-61-6 lm
I 2.4-Trich lorobenzene 120-82-1 .J It)
I I 1 -Trichloroethane 71-55-6 1760
1 1 .2-Trichloroethane 79-00-5 -Nf
Trichloroethene 79-01-6 38. ~
Trichlorofluoromethane 75-69-4 N[
1 2 3-Trichloroorooane 96-18-4 N[
1 1 2-Trichlorotrifluoroethane 76-13-1 NI
124-Trimethvlbenzene 95-63-6 NI
I 3 5-Trimethvlbenzene 108-67-8 N
Vinvl acetate 108-05-4 ND
Vinvl chloride 75-01-4 Ni:T
SECTION IV -Analytical Results -03/05/200I I3:42
LIMS Workorder: 80396907.01 [20I02134] Hamilton Beach-Proctor Silex
STLAustin
12 &: A&: ::.;oo . ·~
4.66 o.boo
5.75 oJooo
6.55 ~.000
5.80 ,.000
8.90 J~.000 g 6.30 /o.ooo
4.00 I o.ooo
79.5 J 0.000
7.00 I 0.000
4.88 I 0.000
5.55 I 0.000
4.35 / 0.000
7.20/ 0.000
45.d 6.000
1 3.te 0.000
21.6 0.000
~,,. f/.!15 6.006
8.45 0.000
lZ A ' ----.,.-.-.:v v ......
6.85 o.Hoo
5.30 .O.ooo
14.4 I o.ooo
6.15 I 0.000
6.20/ 0.000
4.51 0.000
4/?4 0.000
I/ " --.J./V • V.v1n
.. , .
0201HBWW227 020 IHBWW228
2010213405 2010213406
Cone'"~",·· Flia'"r~oi:~~--... .;!,;··!~Rl'.'.if$,~;r~Efl: r..comf"'~'~HiiW'l~~D~"t,~·i:;.Rt:
ND 1.09 0.000 Mt ~ -. ;;:UQU ~·.o
ND 0.931 0.000 51. t .f 18.6 o. lllo
ND 1.15 0.000 N[ 23.0 0. 00
ND 1.31 0.000 NC 26.2 0. 100
ND 1.16 0.000 NI 23.2 0.000
ND 1.78 0.000 N '"'35.6 0000
o~ ~DUH' . l.261A 0.000 2J. ~ND UH--" . :...25.21.A <J.ooo
ND IA"J 0.801 0.000 10 0 16.0 A:>.000
ND 15.9 0.000 NI 318 I o.ooo
ND 1.40 0.000 28• 28.0 I 0.000
ND 0.977 0.000 19.17 -1 19.5 / .. 0.000
ND I.I I 0.000 N[ 22.2 7 0.000
ND 0.870 0.000 N[ 17.4 f 0.000
ND 1.44 0.000 10.0 ..lJ' 28.8/ 0.000
ND 9.00 0.000 N[ 18cY 0.000
10.7 0.637 0.000 12 0 1in 0.000
ND \A"J 5.51 0.000 N 1 VO 0.000
ND \A.:5 1.35 0.000 N'i> 2t.o 0.000
l~O 'f:R 1.69 9.998 4< 700 ..F.fl ~ l.8 0.000
ND 0.821 0.000 Ni~ ~/ !.:-~ v.uuu
39.6 1.37 0.000 15400 27.4 0.000
ND 1.06 0.000 NO R. --I\ ,. .... .,..
£1.£--· ND 2.88 0.000 N 57.6 {Y.d'oo
ND 1.23 0.000 ND 24.6 /o.ooo
ND 1.24 0.000 1 40 24.8 J 0.000
ND 0.905 0.000 4, 0 18.V 0.000
ND 0.948 0.000 ~D l lt.O 0.000
4.73 J 1.14 0.000 tu;) '1 ,..,;~ a.vuO
Page 26 of
Sample results have been qualified by URS-Radian based on the results or the data review process, which is modeled after the N111io1111/ F111ll'lio1111/ Guide/iuesfor Organic and /11orga11ic D11111 Re1•1e11·
(US EPA, October 1999 and February 1994, respectively).
66
----~--------~-----SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Datefflme Collected
Dateffime Prepared
Dateffime Analyzed
Dilution Factor
Instrument
Units
Surronate Comoound ''
l-Bromo-4-fluorobenzene
I 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW227
2010213405
Aoueous
Received
NA
02/20/2001 09:35
02/26/2001 14:09
02/26/2001 14:09
50.0000
MSDA
ug/L
%'R8coverv
99
97
103
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STI. Austin
Limits F
77-117
61-143
87-113
020 l HBWW227 0201HBWW228
2010213405 2010213406
Aoueous Aaueous
Received Received
NA NA
02/20/2001 09:35 02/20/200 l 09:45
02/26/200 I 18:07 02/26/2001 14:37
02/26/2001 18:07 02/26/2001 14:37
10.0000 200.0000
MSDA MSDA
ug/L ug/L
, % 'Reeoverv :. • :-· Llmlta~:·)t : : .,, ,; F.:. ·'%:Recover.1:·· "'·:um1ta · ...... ·
96 77-117 98 77-117
96 61-143 87 61-143
103 87-113 102 87-113
Page 28
Sample results have been qualified by URS-Radian hascd on the results uf the data review prncess, which is modeled at'icr the Natio1111/ F1111ctio1wl G11ideli11esfor Org1111ic 11111/ fllorg1111ic 1>11/ll Re1•iew
(US EPA, October 1999 and February 1994, respectively),
F
of 66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butv I benzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTlme Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/200 I 13:42
020IHBWW228
2010213406
Aaueous
Received
NA
02/20/200 l 09:45
02/26/200 l 16:43
02/26/2001 16:43
1000.0000
MSDA
u"'/L.
Cone Flaa
N61 R
ND
Nn
NI:
Nr
NI:
Nr
Nr
N
N>
N>
N>
N>
Nn
1' D $
l\n
lD
lD
1D m
~ W'
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAustin
DL RL·1·.
.. ,0 U.IHI ..
6820 o.oob
3790 o.obo
446 o.doo
64.1 o.boo
99.8 1iooo
131 11.000
118 J).000
170 /0.000
199 I o.ooo
200 I o.ooo
102 I o.ooo
105 I 0.000
91.1 I 0.000
68.4 I 0.000
65.21 0.000
114/ 0.000
84/l 0.000
9-1_5 0.000
8JJ.6 0.000
""' 0 I\ '""'
020 I HBWW228 020IHBWW230
2010213406 2010213408
Aaueous Aaueous
Received Received
NA NA
02/20/2001 09:45 02/ 19/200 l 11 :30
02/26/2001 18:37 02/23/2001 12:55
02/26/2001 18:37 02/23/2001 12:55
50.0000 1.0000
MSDA MSDA
ul!/L ul!/L
·.cone : ·. Flaa ·. '. ·oL· '::::::·~RL:-:::. * ·~ ~·,i.\ :·cone-'::' ··flan·. · DL · ·RL·
~· -/: ~ ~1.9 0.000 ND 0.438 ·o.ooo
ND \.\.:r 341 0.000 ND iA."J 6.82 0.000
ND IA."T 190 0.000 ND IA:\ 3.79 0.000
ND ll.. -:s 22.3 0.000 ND 0.446 0.000
38.7 3 3.20 0.000 ND 0.0641 0.000
ND \A, "S 4.99 0.000 ND 0.0998 0.000
ND 6.55 0.000 ND 0.131 0.000
ND 5.90 0.000 ND 0.118 0.000
ND 8.50 0.000 ND I>.. ""S 0.170 0.000
ND 'r 9.95 0.000 ND L\-:\ 0.199 0.000
500 ::r 10.0 0.000 ND 0.200 0.000
28.9 J 5.10 0.000 ND 0.102 0.000
9.56 J 5.25 0.000 ND 0.105 0.000
ND \.;\...'°S' . 4.56 0.000 ND 0.091 I 0.000
ND lr..J g 3.42 0.000 ND iA~ H 0.0684 0.000
23.0 J 3.26 .. 0.000 ND 0.0652 0.000
ND iA.'3" 5.70 0.000 ND 0.114 0.000
ND \J\,J 4.21 0.000 ND 0.0842 0.000
97.3 :s 4.62 0.000 ND 0.0925 o.ooo.
7.64 J 4.48 0.000 ND 0.0896 0.000
ND V\.'S 4.69 0.000 ND 0.0938 0.000
Page 29 of 66
Sample results have been qualified by URS-Radian based on the results uf the data review process, which is modeled a lier 1/11• N111io1111/ F1111c1io1111/ G11ide/111es jor Org1111ic 1111d /11org1111ic /J111t1 Re1•11•w
-... USElfllitobcrlilrdF~ .. 1994, .. !lvcly ... -1-----------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
lodomethane
lsooroov I benzene
4-lsooroovltoluene
Methvl methacrvlate
Client Sample ID
Lab Sample ID
CAS
74-88-4
98-82-8
99-87-6
80-62-6
Methvl tert-butvl ether <MTBE) 1634-04-4
4-Methvl-2-oentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I. I.I 2-Tetrachloroethane 630-20-6
1.1.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
...
,
0201HBWW228
2010213406
Cone Flaa DL RL
]lftr g_ 1-~ -.. v.-
NI 93.l 0.060
NP 115 0.600
N> 131 <Y.ooo
N~ 116 b.ooo
tn 178 /0.000
l'D K 126 I o.ooo
8 '5 J 80.l I o.ooo
l'D 1590 I o.ooo , 34 J 140 I 0.000 • ~D 91.1 I 0.000
~D 111 / 0.000
m 87./J 0.000
m ' 14'4 0.000
m <lbo 0-.000
220 63.7 0.000
lD /551 0.000
l 2.4-Trichlorobenzene 120-82-I HB-, / lt ~ ~ ----
I I. I -Trichloroethane 71-55-6 50500
1 1.2-Trichloroethane 79-00-5 bill
Trichloroethene 79-01-6 15 00
Trichlorofluoromethane 75-69-4 NI
1 2 3-Trichloronronane 96-18-4 N)
I.I 2-Trichlorotrifluoroethane 76-13-1 N}
1.2 4-Trimethvlbenzene 95-63-6 1170
l 3.5-Trimethvlbenzene 108-67-8 .4 ~ l
Vinvl acetate 108-05-4 l D
Vinvl chloride 75-0I-4 iul9
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STL Austin
,_,_, v.uuu
169 0.000
R ---0..:..1 v:uou
I37 0.9'00
106 t.ooo
288 /0.000
I23 I o.ooo
I24 I 0.000
i 90.'/ 0.000
94.8 0.000
iw ,/, ...... ...,. __ .. -·
0201HBWW228 0201HBWW230
2010213406 2010213408
cone Flaa· DL .. · :: :RL/·'., ·.: ·.cone ... Fli'"' .... ·or:·'""" " . . .. aa1 ;~ · ?d ·· ·RL
ND l,\..J 5.45 0.000 ND 0.109 0.000
63.8 J 4.66 0.000 ND 0.0931 0.000
ND IA J 5.75 0.000 ND 0.115 0.000
ND 6.55 0.000 ND 0.131 0.000
ND 5.80 0.000 ND 0.116 0.000
ND .v' 8.90 0.000 ND 0.178 0.000
4..fo"" ND Ulf 6.301.A.'3 0.000 ND ;fj' 0.126 0.000
973 :T 4.00 0.000 ND lA."3' 0.0801 0.000
ND i.x:r 79.5 0.000 ND 1.59 0.000
354 3 7.00 0.000 ND 0.140 0.000
28.3 }' 4.88 0.000 ND 0.0977 : . 0.000
ND \..l'J 5.55 0.000 ND 0.111 0.000
ND l)\.j 4.35 0.000 ND lA 'J 0.0870 0.000
18.6 J 7.20 0.000 ND \A\ 0.144 0.000
ND !A.'3' 45.0 0.000 ND 0.900 0.000
1610 'T 3.18 0.000 ND 0.0637 0.000
ND \,,\""\ 27.6 0.000 ND V\. "3' 0.551 0.000
ND v-.:S 6.75 0.000 ND iA.~ 0.135 0.000
~9QQ ER 8.45 8.666 ND O.I69 0.000
25.l -:r 4.10 0.000 ND 0.0821 0.000
l;tQ99 ER &:85 6.000 0.160 J 0.137 0.000
28.2 J 5.30 0.000 ND 0.106 0.000
ND IA...1 14.4 '0.000 ND 0.288 0.000
ND IA:\" 6.15 0.000 ND 0.123 0.000
2110 J 6.20 0.000 ND 0.124 0.000
530 :r 4.52 0.000 ND 0.0905 0.000
ND \A.1' 4.74 0.000 ND \.~'J 0.0948 0.000
492 :T 5.70 0.000 ND 0.114 0.000
Page 31 of 66
Sample results have been qualified by URS· Radian based on the n:sults of the data review process, which is modeled after th<' N111i01111/ Fu11ctio1111/ G11ideli11<·sfur Organic mid ltwrg1111ic Dt11a Re1·it·w
-.. USE-tober~dFc: .. 1994,-tivel}'. .. - - - - - - - - - -~ -
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surtoaate Comnnund -~,.;:·/: ·' · · ...
1-Bromo-4-fluorobenzene
l .2-Dichloroethane-d4
Toluene-d8
0201HBWW228
2010213406
Aaueous
Received
NA
02/20/2001 09:45
02/26/200 l 16:43
02/26/2001 16:43
1000.0000
MSDA
ul!/L
%RecoveN
97
99
IOO
SECTION IV -Analytical Results -03/05/2001 13:42 .
LIMS Workorder: 80396907.01 (20102134) Hamilton Beach-Proctor Silex
STI. Austin
Limits : ; ' •'''.l:f"
77-117
61-143
87-113
0201HBWW228 0201HBWW230
2010213406 2010213408
Aaueous Aaueous
Received Received
NA NA
02/20/2001 09:4·5 02/19/200 l 11 :30
02/26/2001 18:37 02/23/2001 12:55
02/26/2001 18:37 02/23/2001 12:55
50.0000 1.0000
MSDA MSDA
Ui!/L Ui!IL
% Recovar1·:-~'r ·Llmltii~ · .. ' 1:1>~,~t~1:ff'f:~; ·::~1Rtlcbvenll . •'Wmltil" · ~,:._~;. F
100 77-117 97 77-117
60 61-143 0 95 61-143
102 87-113 IOO 87-113
Page 33 ot 66
Sample results have been qualified by URS-Radian based on the results of the data review process, which is moddcd aticr r/w N111io1111/ Fu11c1w1111/ Gu11/e/i11elfvr Orgmuc 11111/ /norgmuc l>11lll Rel'ie11·
--USEPA1 0c1ober ... ndFe-1994,respectivcly .... -·-- - ---- -- --
-------------------
SECTION IV
Analytical Results
MS-VOA
SW8260B
., ·Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofonn
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chlorofonn
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Daterrime Collected
Datefrime Prepared
Daterrime Analyzed
Dilution Factor
Instrument
Units
.. .. CAS . . .. ~ .
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
020lHBWW234
201021341 l
Aaueous
Received
NA
02/19/200 l 13:55
02/23/200 l 14: 19
02/23/2001 14: 19
1.0000
MSDA
ug/L··
·Cone ... · · · Flaa
ND
ND \A.::S
ND I A-:\
ND
ND
ND·
ND
ND
ND \J\.:J
ND IA\
ND
ND
ND
ND
ND (A,1 g
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.~I [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL
0.438
6.82
3.79
0.446
0.0641
0.0998
0.131
0.118
0.170
0.199
0.200
0.102
0.105
0.0911
0.0684
0.0652
0.114
0.0842
0.0925
0.0896
0.0938-
TRIP BLANK TRIP BLANK
2010213407 2010213417
Aaueous Aaueous
Received Received
NA NA
02/20/2001 00:00 02/19/200 l 00:00
02/23/2001 11 :58 02/23/2001 12:27
02/23/200 l 11 :58 02/23/2001 12:27
1.0000 1.0000
MSDA MSDA
uir/L ug/L
RL. '.Coric:.-··· · Flaa ;·:·ol!.· .. '1.;:_hRC::.-~-~-'.r~·: ~Concf; ··,i Flaa· ~:.DL} · RL.
0.000 ND 0.438 0.000 ND 0.438 0.000
0.000 ND lLI 6.82 0.000 ND IA.:J' 6.82 0.000
0.000 ND 11\::\ 3.79 0.000 ND L-l.1 3.79 0.000
0.000 ND 0.446 0.000 ND 0.446 0.000
0.000 ND 0.0641 0.000 ND 0.0641 0.000
0.000 ND 0.0998 0.000 ND 0.0998 0.000
0.000 ND 0.131 0.000 ND 0.131 0.000
6.000 ND 0.118 0.000 ND ~ 0.118 0.000
0.000 ND \A.~ 0.170 0.000 ND . l A".\ 0.170 0.000
0.000 ND lA.""\ 0.199 0.000 ND LLI 0.199 0.000
0.000 ND 0.200 0.000 ND 0.200 0.000
0.000 ND 0.102 0.000 ND 0.102 0.000
0.000 ND 0.105 0.000 ND , 0.105 0.000
0.000 ND . 0.09ll 0.000 ND 0.091 l 0.000
0.000 ND IA-\ .8' 0.0684 0.000 ND u:s B 0.0684 0.000
0.000 ND 0.0652. 0.000 ND 0.0652 0.000
0.000 ND 0.114 0.000 ND 0.114 0.000
0.000 ND 0.0842 0.000 ND 0.0842 0.000
0.000 ND 0.0925 0.000 ND 0.0925 0.000·
0.000 ND 0.0896 0.000 ND 0.0896 0.000
0.000 ND-0.0938 0.000 ND 0.0938 0.000
Page 34 of
Sample results have been qualified by URS-Radian based on the results uf the dala review process, which is modded after 1'11· N111im111/ F1111ctio11al G11idl!/i11esfor Orgm1ic m11i ltwrga11ic Data Re1•11·w
(US EPA, October 1999 and February 1994, respectively).
66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter CAS
Chloromethane 74-87-3
3-Chlorooroaene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
1.2-Dibromo-3-chloronroaane 96-12-8
Dibromochloromethane 124-48-1
1.2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1 2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1 1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
U-Dichloroethene 75-35-4
cis-1.2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichlorooronane 78-87-5
1.3-Dichloroorooane 142-28-9
2.2-Dichloroorooane 594-20-7
l .1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-I 3-Dichloronrooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW234
2010213411
Cone. Flaa
ND \A.:S
ND
ND
ND
ND \/\. :s
ND
ND
ND
ND
"ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND Iii. j
ND LA.-:I
LIMS Workorder: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 ct.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.33 l 0.000
0.169 . 0.000
TRIP BLANK TRIP BLANK
2010213407 2010213417
Cone Flaa DL RL: . ·'. cone· · l!laa···. ·:.:oL .. ~' ·· ·· RL ,,··
ND t ... .) 0.127 0.000 ND IA::! 0.127 0.000
ND 0.0777 0.000 ND 0.0777 0.000
ND 0.178 0.000 ND 0.178 0.000
ND 0.0974 0.000 ND 0.0974 0.000
ND i ... -:s 0.548 0.000 ND I 1-."°S 0.548 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.148 0.000 ND 0.148 0.000
ND 0.780 0.000 ND 0.780 0.000
ND 0.150 0.000 ND 0.150 0.000
ND 0.0965 0.000 ND 0.0965 0.000
ND 0.0846 0.000 ND 0.0846 0.000
ND 0.237 0.000 ND 0.237 0.000.
ND 0.124 0.000 ND 0.124 0.000.
ND 0.102 0.000 ND 0.102 0.000
ND 0.122 0.000 ND 0.122 0.000
ND 0.112 0.000. ND 0.112 0.000
ND 0.119 0.000 ND 0.119 0.000
ND 0.0869 0.000 ND 0.0869 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.160 0.000 ND 0.160 0.000
ND 0.0994 0.000 ND 0.0994 0.000
ND 0.0818 0.000 ND 0.0818 0.000
ND 0.0908 0.000 ND 0.0908 0.000
ND 0.101 0.000 ND 0.101 0.000
ND 0.136 0.000 ND 0.136 0.000
ND \JLoJ 0.331 0.000 ND 1.A-:X-0.331 0.000
ND IA. 'J 0.169 0.000 ND l l'J 0.169 0.000
Page 35 of 66
Sanipk results have bct:n qualified by URS-Radian based on the ri:sulls of the data review process, which is modeled aitcr 1he N11ti111111/ F1111ctiu1111/ Guu/e/mesfur Org1111ic 1111d brorgm1ic 011111 Rt·1·1e11•
--USE-·tobcr~dFc .. 1994,-ively .. - - - - - - - -·-- - -
-------------------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
·parameter
lodomethane
lsoaroov I benzene
4-lsoaroovltoluene
Methvl methacrvlate
"
Client Sample ID
Lab Sample ID
·CAS
74-88-4
98-82-8
99-87-6
80-62-6
~" .... , ~": .•: ',
Methvl tert-butvl ether <MTBE) 1634-04-4
4-Methvl-2-oentanone <MJBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 1.1 2-Tetrachloroethane 630-20-6
I 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
I 2.3-Trichlorobenzene 87-61-6
1 2.4-Trichlorobenzene 120-82-1
1 I.J-Trichloroethane 71-55-6
LI 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2 3-Trichloroorooane 96-18-4
I .. I 2-Trichlorotrifluoroethane 76-13-1
1.2 4-Trimethvlbenzene 95-63-6
1.3 .5-Trimethv !benzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride -75-01-4
SECTION IV -Analytical Results -03/05/2001 13:42
020IHBWW234
2010213411
Cone Flaa
ND
ND
ND
ND
ND
ND
ND "Fi
ND ·Id
ND
ND
ND
ND
ND lA::r
ND l A-:\.
ND
ND
ND \;'\,"5
ND I A-:\
ND
ND
ND
ND
ND
ND
ND
ND
ND \!v"S,.
ND
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAuslin
DL
0.109
0.0931
0.115
0.131
0.116
0.178
0.126
0.0801
1.59
0.140
0.0977
0.111
0.0870
0.144
0.900
0.0637
0.551
0.135
0.169
. 0.0821
0 .. 137
0.106
0.288
0.123
0.124
0.0905
0.0948
0.114.
TRIP BLANK TRIP BLANK
2010213407 2010213417
·RL ,.. .... -,, . Coric'·-'.~· Flaa', ... cl ., .··Ra;:: . .:'·:"~::;.,·.; ~cone · . ··F.:lacl.ti.'D~:i? ::Rt:: .
0.000 ND 0.109 0.000 ND 0.109 0.000
0.000 ND 0.0931 0.000 ND 0.0931 0.000
0.000 ND 0.115 o.ooo. ND 0.115 0.000
0.000 ND 0.131 0.000 ND 0.131 0.000
0.000 ND 0.116 0.000 ND __ 0.116 0.000
0.000 ND 0.178 0.000 ND 0.178 0.000
0.000 ND pi' 0.126 0.000 ND ~· 0.126 0.000
0.000 ND IA\' 0.0801 0.000 ND lk-f 0.0801 0.000
0.000 ND 1.59 0.000 ND 1.59 0.000
0.000 ND 0.140 0.000 ND 0.140 0.000
0.000 ND 0.0977 0.000 ND 0.0977 .. 0.000
0.000 ND 0.111 0.000 ND 0.111 0.000
0.000 ND vU 0.0870 0.000 ND ll~ 0.0870 0.000
0.000 ND \,A • ..) 0.144 0.000 ND V-.,\ _., 0.144 0.000
0.000 ND 0.900 0.000 ND .. 0.900 0.000
0.000 ND 0.0637 0.000 ND 0.0637 0.000
0.000 ND lA..J 0.551 0.000 ND [A,:\" 0.551 0.000
0.000 ND \J,..j 0.135 0.000 ND LA.\ 0.135 0.000
0.000 ND 0.169 0.000 ND 0.169 0.000
0.000 ND 0.0821 0.000 ND 0.0821 0.000
0.000 ND 0.137 0.000 ND 0.137 0.000
0.000 ND 0.106 0.000 ND 0.106 0.000
0.000 ND 0.288 . 0.000 ND 0.288 0.000
0.000 ND 0.123 0.000 ND 0.123 0.000
0.000 ND 0.124 0.000 ND 0.124 0.000
0.000 ND 0.0905 0.000 ND 0.0905 0.000
0.000 ND IA.\ 0.0948 0.000 ND \A,::\ 0.0948 0.000
0.000 ND 0.114 0.000 ND 0.114 0.000
Page 36 of
Sample results have been qualified by URS-Radian based on \he results of the data review process, which is modeled aftcr Ihl' Nmio1111/ F1111c1io1111/ G11ide/i11esfor Vrg1111it' mid fllorg1111ic D11111 Re1•iew
(US EPA, October 1999 and February 1994, respectively).
66
SECTION 1v·
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
0201HBWW234
2010213411
Continued
CAS' ·."
.. Cone. Parameter
o-Xvlene/m-Xvlene 106-42-3 ND
o-Xvlene 95-47-6 ND
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.01 (20102134) Hamilton Beach-Proctor Silex
STLAustin
Flaa DL RL
0.167 0.000
0.0844 0.000
TRIP BLANK TRIP BLANK
2010213407 2010213417
Cone Flaa DL· RL ·.·. _;~· cone .''Rfi'ft'I~ ·;tJL:~/. . RL
ND 0.167 0.000 ND 0.167 0.000
ND 0.0844 0.000 ND 0.0844 0.000
Page 37 of 66
Sample results have been qualified by URS-Radian based on the results of the dala review process, which is modeled after 1/w Nlllimud F1111c1iu1111/ G1111/e/111esfur Org11111c 1111d ltwrg11111c D11111 Re1•i1•11•
-~USlif:toberiiillndF .. 1994 .. tivcl.. - - - -·-- - -__ - - -
------------------ -
SECTION IV
Analytical Results
Surrogates
MS-VOA.
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
I-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW234
20 I02 I341 I
Aaueous
Received
NA
02/I9/200I 13:55
02/23/2001 14:19
02/23/2001 14:19
1.0000
MSDA
ul!/L.
'lo Recoverv ·
97
IOI
IOI
LIMS Workorder: 8039690?.0l (20102134] llamilton Beach-Proctor Silex
STLAuslin
Limit& '"• .. ,.F.:
77-I I 7
6I-143
87-113
TRIP BLANK TRIP BLANK
2010213407 2010213417
Aoueous Aaueous
Received Received
NA NA
02/20/2001 00:00 02/19/2001 00:00
02/23/2001 11 :58 02/23/2001 12:27
02/23/2001 11 :58 02/23/2001 12:27
1.0000 1.0000
MSDA MSDA
Ul!IT. ul!!L
·'" Reeovirv· . .;_ :. UmltS\ -: ··,:~\hit.,\ ~F..i '% Reeove..v· · · L1in11s
95 77-117 97 77-117
100 61-143 100 6I-I43
100 87-I I3 102 87-113
Page 38
Sample results have been qualified by URS-Radian based on the results uf the data review proct!SS, which is modeled after 1/it' N111io1111/ F111w1io1111/ G11ideli11esfor Org1111ii' 11111{ illorg1111ic D11111 Re1•it•11•
(US EPA, Oc1ober 1999 and February 1994, respectively).
F
of 66
I
I
I
I
I
I
I
I
I
I
·1
I
I
I
I
I
I
I
I
LABORATORY REPORTS
SECTION I
Table of Contents
Section
I.
MS-VOA
II.
III.
IV.
v.
VI.
VII.
Form
Cover Page -Laboratory Analytical Report
Table of Contents
Report Surrmaries . • . . • . .
Workorder Surrmary .
Protocol Surrmary
Corrments and Flag Definitions
Standard Flag Definitions .
Analyst Corrments . . . .
Sarrple Condition Corrments . . • . •
Analytical Results . . • . . • . . . .
SW8260B . . . . . . . . . .
Calibration and Quality Control Results
SW8260B . . . . . . . . . . .
Batch Surrmaries . .
SW8260B .
Certifications . . .
Calibration Verification Results
Mass Spectrometer Tune
~ethod Blank Results
Spiked Sarrple Results .
Control Sarrple Results
Extraction/Digestion Batch Surrmary
Analysis Batch Surrmary
Section I -Table of Contents -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Page
i
. 1
1
1
2
• 3
• 3
. 3
• 3
4
. 4
39
39
39
47
49
. 53
58
62
62
62
• 64
. 66
-------------------
-------------------SECTION II .
Report Summaries
MS-VOA
Client Name: Hamilton Beach-Proctor Silex
Client Code: HB-PS
Workorder Summary
. , ,., . : -~. •\ _'.; ·., -. ..
Project Name: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
Facility Name: NC
'·. .. :;:; ~ . '•'' ~ . -.. .. ' •'" ' -;J.;.aa>:~./~; .. '::. ·?: ,.: ': . .':. <:: ~-f'.f,f;:~ ;,' : :·-: . .:;. :. ":"· .~;··: ;: ....... '.! '. ~ ~::t~;i~~ .. :> .. ... :·<_·;1 ;::Ni~it.&J.:o'e&'~ti~tion::{ ·?::::.'.:_: ;:; .• , .. Clierit:sarrlnie ID .,sam·ohit-ID · . · ·samole Matrix · · ' .,. ~ . ·r.nethod Citatio·n . , · .,.,. .-I: .~ -. .,
020IHBWW215 2010213401
0201HBWW214 2010213402
0201HBWD999 2010213403
0201HBWW213 2010213404
0201HBWW227 2010213405
0201HBWW228 2010213406
TRIP BLANK 2010213407
0201HBWW230 2010213408
0201HBWW222 2010213409
0201 HBWW226 2010213410
0201HBWW234 2010213411
0201HBWW224 2010213412
0201HBWW225 2010213413
0201HBWW220 2010213414
0201HBWW216 2010213415
0201HBWD998 2010213416
TRIP BLANK 2010213417
SECTION II -Report Summaries -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS ·
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous ~W8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Aaueous SW8260B Volatiles bv GC/MS
Page I of 66
SECTION II
Report Summaries
MS-VOA
Protocol Summary
,,
';· ·' '• •, ,, ,<
·Lab'"·• Date & :nrrie
Client Samole ID ;• ·.~ .. ;·,~ : sanuillt 10 .. Collected
Method· SW8260B .
0201HBWW215 2010213401 02/20/01 08:20
0201HBWW2l4 2010213402 02/20/01 08:40
0201HBWD999 2010213403 02/20/01 08:45
0201HBWD999 2010213403 02/20/01 08:45
0201HBWW213 2010213404 02/20/01 09:05
0201HBWW227 2010213405 02/20/01 09:35
0201HBWW227 2010213405 02/20/01 09:35
0201HBWW228 2010213406 02/20/0 I 09:45
0201HBWW228 2010213406 02/20/01 09:45
0201HBWW228 2010213406 02/20/01 09:45
TRIP BLANK 2010213407 02/20/0 I 00:00
0201HBWW230 2010213408 02/I 9/01 11 :30
0201 HBWW222 2010213409 02/19/01 14:15
0201HBWW226 2010213410 02/19/01 13:30
0201HBWW234 2010213411 02/19/01 13:55
0201HBWW224 2010213412 02/19/01 15:10
0201HBWW225 2010213413 02/19/01 15:15
0201HBWW220 2010213414 02/19/01 14:35
0201HBWW216 2010213415 02/19/01 15:45
0201HBWD998 2010213416 02/19/01 13:35
TRIP BLANK 2010213417 02/19/01 00:00
SECTION II -Report Summaries -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STLAustin
''
Date·& Time·· Prep
Received:· ·· · · Batch ID'
02/21101 11:15 10778
02/21/01 11:15 10778
02/21/01 11: 15 10778
02/21/01 l l:i 5 10778
02/21/01 11:15 10778
02/21/01 11 :15 10778
02/21101 11:15 10778
02/21/01 11: 15 10778
02/21/01 11:15 10778
02/21/01 11: 15 10778
02/21/61 11:15 10778
02/21/01 11: 15 10778
02/21/01 11:15 10778
02/21/01 11:15 10778
02/21/01 11:15 10778
02/21/01 11:15 10778
02/21/01 11:15 10778
02/21/01 11:15 10778
02/21/01 11:15 10778
02/21/01 11:15 10778
02/21/01 11: 15 10778
.. •!',· ~-., ,,
' 'Hold.Timct:•S >ac ,• ,,
A_n~ly~J~ 'Date$ Time J>ren ·.--. 'A.nalvsis Date & Time ,,'-,
' '
Preoared ·Batch· ID .Ana~ed: :· :;sn.tc. Adtua· isoec Actual
02/23/01 10:20 10778 02/23/01 10:20 7D 3D 7D 3D
02/26/01 12:41 10778 02/26/01 12:41 7D 6D 7D 6D
02/26/01 13:39 10778 02/26/01 13:39 7D 6D 7D 6D
02/26/01 17:34 10778 02/26/01 17:34 7D 6D 7D 6D
02/26/01 13 :09 10778 02/26/01 13:09 7D 6D 7D 6D
02/26/01 14:09 10778 02/26/01 14:09 7D 6D 7D 6D
02/26/01 18:07 10778 02/26/01 18:07 7D 6D 7D 6D
02/26/01 14:37 10778 02/26/01 14:37 7D 6D 7D 6D
02/26/01 16:43 10778 02/26/01 16:43 7D 6D 7D 6D
02/26/01 18:37 10778 02/26/01 18:37 7D 6D 7D 6D
02/23/01 11 :58 10778 02/23/0 I 11 :58 7D 3D 7D 3D
02/23/01 12:55 10778 02/23/01 12:55 7D 4D 7D 4D
02/23/01 13:23 10778 02/23/01 13:23 7D 4D 7D 4D
0212310113:51 10778 02/23/01 13:51 7D 4D 7D 4D
02/23/01 14:19 10778 02/23/01 14: 19 7D 4D 7D 4D
02/23/01 14:47 10778 02/23/0114:47 7D 4D 7D 4D
02/23/01 15:15 10778 02/23/01 15:15 7D 4D 7D 4D
02/23/01 15:45 10778 02/23/01 15:45 7D 4D 7D 4D
02/26/01 11 :44 10778 02/26/01 11 :44 7D 7D 7D 70
02/26/01 12:12 10778 02/26/01 12:12 7D 7D 7D 70
02/23/01 12:27 10778 02/23/01 12:27 7D 4D 7D 40
Page 2 of 66 - --· - - - - - - - - - - - - - - - -
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWD998
2010213416
Aqueous
Received
NA
02/19/2001 13:35
02/26/2001 12:12
02/26/2001 12:12
1.0000
MSDA
u!!IL.
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.322 JB
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL Rl
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0:000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0201HBWD999 0201HBWD999
2010213403 2010213403
Aaueous Aaueous
Received Received
NA NA
02/20/2001 08:45 02/20/2001 08:45
02/26/2001 13:39 02/26/2001 17:34
02/26/2001 13:39 02/26/2001 17:34
50.0000 5.0000
MSDA MSDA
ul!.IL u!!IL
Cone Flaa " DL, ; RL ·cone-Flaa:· bl· RL
ND 21.9 0.000 ND 2.19 0.000
ND 341 0.000 ND 34.1 0.000
ND 190 0.000 ND 19.0 0.000
ND 22.3 0.000 ND 2.23 0.000
ND 3.20 0.000 0.362 J 0.320 0.000
ND 4.99 0.000 ND 0.499 0.000
ND 6.55 0.000 ND 0.655 0.000
ND 5.90 0.000 ND 0.590 0.000
ND 8.50 0.000 ND 0.850 0.000
ND 9.95 0.000 ND 0.995 0.000
ND 10.0 0.000 ND 1.00 0.000
ND 5.10 0.000 ND 0.510 0.000
ND 5.25 0.000 ND 0.525 0.000
ND 4.56 0.000 ND 0.456 0.000
ND B 3.42 0.000 ND B 0.342 0.000
ND 3.26 0.000 ND 0.326 0.000
ND 5.70 0.000 ND 0.570 0.000
ND 4.21 0.000 ND 0.421 0.000
ND 4.62 0.000 ND 0.462 0.000
ND 4.48 0.000 ND 0.448 0.000
ND 4.69 0.000 ND 0.469 0.000
Page 4 of 66
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
:Parameter -. -··-c ·CAS'. ,.: ::·-
Chloromethane 74-87-3
3-Chloroorooene 107-05-I
2-Chlorotoluene 95-49-8
4-Chlorotoluene I06-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-I
1.2-Dibromoethane I06-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene 110-57-6
I 4-Dichlorobenzene I06-46-7
I ,2-Dichlorobenzene 95-50-I
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-7I-8
1. I-Dichloroethane 75-34-3
I .2-Dichloroethane 107-06-2
I. I-Dichloroethene 75-35-4
cis-1,2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloroprooane 78-87-5
I 3-Dichloroorooane 142-28-9
2 2-Dichloroprooane 594-20-7
1 1-Dichloroorooene 563-58-6
cis-I .3-Dichloronrooene 1006I-OI-5
trans-I .3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-4I-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 59I-78-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWD998
20102134I6
:cone:_ Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.0I (20102134] Hamilton Beach-Proctor Silex
STLAustin
DL "·-·. '-RL'·· '··:
0.127 0.000
0.0777 0.000
O.I78 0.000
0.0974 0.000
0.548 0.000
0.140 0.000
0.137 0.000
O.I48 0.000
0.780 0.000
O.I50 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 0.000
0.122 0.000
O.l I2 0.000
0.119 0.000
0.0869 0.000
0.135 0.000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
O.lOI 0.000
0.136 0.000
0.331 0.000
0.169 0.000
0201HBWD999 0201HBWD999
20102I3403 20I0213403
Cone_, · Flaa_ .. ·.Dl·. · • .: R.C' ')·'·; -.cone· __ : -ftaa:::_~DB::-' ·._ _ RL ~ '_..._
ND 6.35 0.000 ND 0.635 0.000
ND 3.88 0.000 ND 0.388 0.000
ND 8.90 0.000 ND 0.890 0.000
ND 4.87 0.000 ND 0.487 0.000
ND 27.4 0.000 ND 2.74 0.000
ND 7.00 0.000 ND 0.700 0.000
ND 6.85 0.000 ND -·~ 0.685 0.000
ND 7.40 0.000 ND ... 0.740 0.000
ND 39.0 0.000 ND 3.90 0.000
ND 7.50 0.000 ND 0.750 0.000
ND 4.82 0.000 ND 0.482 0.000
ND 4.23 0.000 ND 0.423 0.000
ND 11.8 0.000 ND 1.18 0.000
205 6.20 0.000 164 0.620 0.000
ND 5.10 0.000 ND ·-0.510 0.000
19.3 J 6.10 0.000 16.7 0.610 0.000
I4.6 J 5.60 0.000 11.9 0.560 0.000
ND 5.95 0.000 0.424 u 0.595 0.000
ND 4.34 0.000 ND 0.434 0.000
ND 6.75 0.000 ND 0.675 0.000
ND 8.00 0.000 ND 0.800 0.000
ND 4.97 0.000 ND 0.497 0.000
ND 4.09 0.000 ND 0.409 0.000
ND 4.54 0.000 ND 0.454 0.000
ND 5.05 0.000 ND 0.505 0.000
ND 6.80 0.000 ND 0.680 0.000
ND 16.6 0.000 ND 1.66 0.000
ND 8.45 0.000 ND 0.845 0.000
Page 5 of 66
SECTION.IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
·Parameter cAs
Iodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether <MTBE) · 1634-04-4
4-Methvl-2-oentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
LI l 2-Tetrachloroethane 630-20-6
l 12 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
l 2 3-Trichlorobenzene 87-61-6
1.2 4-Trichlorobenzene 120-82-l
1.1. l-Trichloroethane 71-55-6
l 1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2.3-Trichloroorooane 96-18-4
1 1 2-Trichlorotrifluoroethane 76-13-1
1.2 4-Trimethvlbenzene 95-63-6
1.3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWD998
2010213416
. '. ·cone · Flaa
ND
ND
ND
ND
ND
ND
ND B
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL . RL
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
l.59 0.000
0.140 0.000
0.0977 0.000
O.ll l 0.000
0.0870 0.000
0.144 0.000
0.900 6.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114 0.000
0201HBWD999 0201HBWD999
2010213403 2010213403
Cone Flaa· DL "RL ··cone· · . ,filarf ·· 01.:· ·: . .· RL
ND 5.45 0.000 ND 0.545 0.000
ND 4.66 0.000 ND 0.466 0.000
ND 5.75 0.000 ND 0.575 0.000
ND 6.55 0.000 ND 0.655 0.000
ND 5.80 0.000 ND 0.580 0.000
ND 8.90 0.000 ND 0.890 0.000
ND B 6.30 0.000 ND B 0.630 0.000
ND 4.00 0.000 ND 0.400 0.000
ND 79.5 0.000 ND 7.95 0.000
ND 7.00 0.000 ND 0.700 0.000
ND 4.88 0.000 ND 0.488 0.000
ND 5.55 0.000 ND 0.555 0.000
ND 4.35 0.000 ND 0.435 0.000
ND 7.20 0.000 ND 0.720 0.000
ND 45.0 0.000 ND 4.50 0.000
ND 3.18 0.000 ND 0.318 0.000
ND 27.6 0.000 ND 2.76 0.000
ND 6.75 0.000 ND 0.675 0.000
ND 8.45 0.000 ND 0.845 0.000
ND 4.10 0.000 ND 0.410 0.000
ND 6.85 0.000 ND 0.685 0.000
ND 5.30 0.000 ND 0.530 0.000
ND 14.4 0.000 ND 1.44 0.000
ND 6.15 0.000 ND 0.615 0.000
ND 6.20 0.000 ND 0.620 0.000
ND 4.52 0.000 ND 0.452 0.000
ND 4.74 0.000 ND 0.474 0.000
14.2 J 5.70 0.000 11.6 0.570 0.000
Page 6 of 66
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
·,'.Parameter "
o-Xvlene/m-Xvlene
o-Xvlene
'
i ..
Client Sample ID
Lab Sample ID
'•· '._:.-GAS:>·:·:-::
106-42-3
95-47-6
SECTION IV -Analytical Results -0310512001 13:42
0201HBWD998
2010213416
':.cone Flaa,
ND
ND
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAustin
'DL" ',
0.167
0.0844
0201HBWD999 020 IHBWD999
2010213403 2010213403
RL ' 'Cone Flaa~;' .DL , , :i:u:.. . ~~¥: > --~·::. '.G.oric: . . . ::;'f.laa':·:_~<Dfi';5:~~; :< ::RL
0.000 ND 8.35 0.000 ND 0.835 0.000
0.000 ND 4:22 0.000 ND 0.422 0.000
Page 7 of 66
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
Surroaate Comcound
l-Bromo-4-fluorobenzene
1.2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWD998
2010213416
Aaueous
Received
NA
02/19/2001 13:35
02/26/2001 12:12
02/26/2001 12:12
1.0000
MSDA
ug/L
·3 RecoveN
97
98
106
LIMS Workorder: 80396907.0I [20102134] Hamilton Beach-Proctor Silex
STLAustin
Limits '.f
77-117
61-143
87-113
0201HBWD999 0201HBWD999
2010213403 2010213403
Aaueous Aaueous
Received Received
NA NA
02/20/200 I 08:45 02/20/2001 08:45
02/26/2001 13:39 02/26/2001 17:34
02/26/2001 13:39 02/26/2001 17:34
50.0000 5.0000
MSDA MSDA
U!!IL u!!IL
%Recoveftl. . Limits" F .% Recoverv . um1ta. · F
98 77-117 99 77-117
100 61-143 96 61-143
102 87-113 104 87-113
Page 8 of 66
-------------------
-------------------SECTION IV
Analytical Results
MS-VOA
SW8260B
. ·: Parameter'·
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
< ~ ~-.; '
Bromochloromethane
Bromodichloromethane
Bromoform
Brom om ethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butv !benzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
... :·:·,·cAS· · '••
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/200I 13:42
0201HBWW213
2010213404
Aqueous
Received
NA
02/20/200 l 09:05
02/26/200 l 13 :09
02/26/200 l 13 :09
5.0000
MSDA
ug/L
·Cone·· Flaa
ND
ND
ND
ND
0.465 J
Nb
ND
ND
ND
ND
ND
ND
ND
ND
ND B
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.0I [20102134] Hamilton Beach-Proctor Silex
STLAustin
:OL · ·Rl" .·>.:';
2.19 0.000
34.1 0.000
19.0 0.000
2.23 0.000
0.320 0.000
0.499 0.000
0.655 0.000
0.590 e.ooo
0.850 0.000
0.995 0.000
1.00 0.000
0.510 0.000
0.525 0.000
0.456 0.000
0.342 0.000
0.326 0.000
0.570 0.000
0.421 0.000
0.462 0.000
0.448 0.000
0.469 0.000
0201HBWW214 0201HBWW215
2010213402 2010213401
Aoueous Aoueous
Received Received
NA NA
02/20/2001 08:40 02/20/2001 08:20
02/26/2001 12:41 02/23/2001 10:20
02/26/2001 12:41 02/23/2001 10:20
5.0000 1.0000
MSDA MSDA
U!!/L u!!IL
·cone . :: Flaa:.-·· DL)/~;:'~ ::,RL>: :.'; ,._ ,::cone:~;. · '.,, ··F1aa·: ·.·: DL :., ·'. · :.RL
ND 2.19 0.000 ND 0.438 0.000
ND 34.1 0.000 ND 6.82 0.000
ND 19.0 0.000 ND 3.79 0.000
ND 2.23 0.000 ND 0.446 0.000
0.396 J 0.320 0.000 ND 0.0641 0.000
ND 0.499 0.000 ND 0.0998 0.000
ND 0.655 0.000 ND 0.131 0.000
ND 0.590 0.000 ND -· 0.118 0.000
ND 0.850 0.000 ND --0.170 0.000
ND 0.995 0.000 ND 0.199 0.000
ND 1.00 0.000 ND 0.200 0.000
ND 0.510 0.000 ND 0.102 0.000
ND 0.525 0.000 ND 0.105 0.000
ND 0.456 0.000 ND 0.0911 0.000
ND B 0.342 0.000 1.13 B 0.0684 0.000
ND 0.326 0.000 ND 0.0652 0.000
ND 0.570 0.000 ND 0.114 0.000
ND 0.421 0.000 ND 0.0842 0.000.
ND 0.462 0.000 ND 0.0925 0.000
ND 0.448 0.000 ND 0.0896 0.000
ND 0.469 0.000 ND 0.0938 0.000
Page 9 of 66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0201HBWW213
2010213404
Parameter.· ; ""· CAs·· ' ... :~ ··· :.cone'' Flaa . DL
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
I 2-Dibromo-3-chlorooronane 96-12-8 ND
Dibromochloromethane 124-48-1 ND
I 2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-I 4-Dichloro-2-butene 110-57-6 ND
1.4-Dichlorobenzene 106-46-7 . ND
I 2-Dichlorobenzene 95-50-1 ND
I 3-Dichlorobenzene 541-73-1 ND
Dichlorodifluoromethane 75-71-8 ND
1.1-Dichloroethane 75-34-3 173
I 2-Dichloroethane 107-06-2 3.68
1.1-Dichloroethene 75-35-4 433
cis-1 2-Dichloroethene f56-59-2 37.1
trans-I 2-Dichloroethene 156-60-5 0.937
I 2-Dichloroorooane 78-87-5 ND
I 3-Dichlorooronane 142-28-9 ND
2 2-Dichloroorooane. 594-20-7 ND
1.1-Dichloronronene 563-58-6 ND
cis-1 3-Dichloroorooene 10061-01-5 ND
trans-1.3-Dichloronronene 10061-02-6 ND
Ethvl methacrvlate 97-63-2 ND
Ethvlbenzene 100-41-4 0.170
Hexachloro-1 3-butadiene 87-68-3 ND
2-Hexanone 591-78-6 ND
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20!02134] Hamilton Beach-Proctor Silex
STLAustin
0.635
0.388
0.890
0.487
2.74
0.700
0.685
0.740
3.90
0.750
0.482
0.423
l.18
0.620
0.510
0.610
0.560
J 0.595
0.434
0.675
0.800
0.497
0.409
0.454
0.505 u 0.680
1.66
0.845
0201HBWW214 0201HBWW215
2010213402 2010213401
·.RL· .,: cone· ' Flaa··. Bl..·:.·.:). RL'·.' .: .. : .. :.cone' .. : :• 'flao '.>OL .. · .. :-RL .
0.000 ND 0.635 0.000 ND 0.127 0.000
0.000 ND 0.388 0.000 ND 0.0777 0.000
0.000 ND 0.890 0.000 ND 0.178 0.000
0.000 ND 0.487 0.000 ND 0.0974 0.000
0.000 ND 2.74 0.000 ND 0.548 0.000
0.000 ND 0.700 0.000 ND 0.140 0.000
0.000 ND 0.685 0.000 ND 0.137 0.000
0.000 ND 0.740 0.000 ND 0.148 0.000
0.000 ND 3.90 0.000 ND 0.780 0.000
0.000 ND 0.750 0.000 ND 0.150 0.000
0.000 ND 0.482 0.000 ND 0.0965 0.000
0.000 ND 0.423 0.000 ND 0.0846 0.000
0.000 ND l.18 0.000 ND 0.237 0.000
0.000 162 0.620 0.000 3.55 0.124 0.000
tl.000 ND 0.510 0.000 ND 0.102 0.000
0.000 16.8 0.610 0.000 2.38 0.122 0.000
0.000 12.9 0.560 0.000 ND 0.112 0.000
0.000 0.708 J 0.595 0.000 ND 0.119 0.000
0.000 ND 0.434 0.000 ND 0.0869 0.000
0.000 ND 0.675 0.000 ND 0.135 0.000
0.000 ND 0.800 0.000 ND 0.160 0.000
0.000 ND 0.497 0.000 ND 0.0994 0.000
0.000 ND 0.409 0.000 ND 0.0818 0.000
0.000 ND 0.454 0.000 ND 0.0908 0.000
0.000 ND 0.505 0.000 ND 0.101 0.000
0.000 ND 0.680 0.000 ND 0.136 0.000
0.000 ND 1.66 0.000 ND 0.331 0.000
0.000 ND 0.845 0.000 ND 0.169 0.000
Page IO of 66 - - - - - - -·-- - - - - - - - - - -
__________ !!m _______ _
SECTION IV.
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter· ' :cAS· "'
lodomethane 74-88-4
lsooroovlbenzene 98-82-8
4-lsoproovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methyl tert-butvl ether (MTBE) 1634-04-4
4-Methvl-2-pentanone <MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile 107-12-0
n-Propylbenzene 103-65-1
Stvrene 100-42-5
1.1 1 2-Tetrachloroethane 630-20-6
I l.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2.3-Trichlorobenzene 87-61-6
I 2 4-Trichlorobenzene 120-82-1
1 I I-Trichloroethane 71-55-6
I I 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2.3-Trichloroorooane 96-18-4
1 1 2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
I 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -03/05/2001 I3:42
0201HBWW213
2010213404
.~ ~~ · ... ~ .. , cone Flaa
ND
ND
ND
ND
ND
ND
ND B
7.69
ND
ND
ND
ND
ND
24.8
ND
ND
ND
ND
ND
2.68
426
ND
ND
ND
ND
ND
ND
19.2
LIMS Workorder: 80396907.01 [20102I34] Hamilton Beach-Proctor Silex
STLAustin
DL
0.545
0.466
0.575
0.655
0.580
0.890
0.630
0.400
7.95
0.700
0.488
0.555
0.435
0.720
4.50
0.318
2.76
0.675
0.845
0.410
0.685
0.530
1.44
0.615
0.620
0.452
0.474
0.570
0201HBWW214 0201HBWW215
2010213402 2010213401
. :Rt: . ·-cone. : .. Flaa· . DL · --:::-.'.Rl!.: J • cone·:· . t=hict:· :;:oc:;rc::·:' RL . .,,,
0.000 ND 0.545 0.000 ND 0.109 0.000
0.000 ND 0.466 0.000 ND 0.0931 0.000
0.000 ND 0.575 0.000 ND 0.115 0.000
0.000 ND 0.655 0.000 ND 0.131 0.000
0.000 ND 0.580 0.000 0.427 J 0.116 0.000
0.000 ND 0.890 0.000 ND 0.178 0.000
0.000 ND B 0.630 0.000 ND B .. ,,, . 0.126 0.000
0.000 ND 0.400 0.000 ND 0.0801 0.000
0.000 ND 7.95 0.000 ND 1.59 0.000
0.000 ND 0.700 0.000 ND 0.140 0.000
0.000 ND 0.488 0.000 ND 0.0977 0.000
0.000 ND 0.555 0.000 ND 0.111 0.000
0.000 ND 0.435 0.000 ND 0.0870 0.000
0.000 ND 0.720 0.000 ND "' 0.144 0.000
0.000 ND 4.50 0.000 6.41 0.900 0.000
0.000 ND 0.318 0.000 ND 0.0637 0.000
0.000 ND 2.76 0.000 ND 0.551 0.000
0.000 ND 0.675 0.000 ND 0.135 0.000
0.000 ND 0.845 0.000 ND 0.169 0.000
0.000 ND 0.410 0.000 ND 0.0821 0.000
0.000 ND 0.685 0.000 ND 0.137 0.000
0.000 ND 0.530 0.000 ND 0.106 0.000
0.000 ND 1.44 0.000 ND 0.288 0.000
0.000 ND 0.615 0.000 ND 0.123 0.000
0.000 ND 0.620 0.000 ND 0.124 0.000
0.000 ND 0.452 0.000 ND 0.0905 0.000
0.000 ND 0.474 0.000 ND 0.0948 0.000
0.000 11.8 0.570 0.000 ND 0.114 0.000
Page II of 66
SECTION IV.
Analytical Results
MS-VOA
SW8260B
Continued
· : Parameter·
n-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
.. ·-<·OAS· '"':.: .-: :
106-42-3
95-47-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW213
2010213404
Cone 'Flaa
0.363 u
0.815 J
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STL Austin
DL --RL
0.835 0.000
0.422 0.000
0201HBWW214 0201HBWW2 l 5
2010213402 2010213401
' Cone· ·Flaa·. ·ol " • ·o.· RL::·: ,_. ·: :cone··'-. --... :':·Flaa'.;'.·,, ot::·. · Ri.. .·
ND 0.835 0.000 ND 0.167 0.000
ND 0.422 0.000 ND 0.0844 0.000
Page 12 of 66 - --· - - - - - - -~ - - - - - - - -
-------------------SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
surro·nate c6mt>ound " .. .. . ..
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW213
2010213404
Aaueous
Received
NA
02/20/200 I 09:05
02/26/2001 13:09
02/26/2001 13:09
5.0000
MSDA
ug/L
·%::Recoverv.
100
100
104
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Llm·1~: .. '" .'. ''.\;"·f·
77-117
61-143
87-113
0201HBWW214 0201HBWW215
2010213402 2010213401
Aqueous Aqueous
Received Received
NA NA
02/20/2001 08:40 02/20/200 I 08:20
02/26/2001 12:41 02/23/2001 10:20
02/26/2001 12:41 02/23/2001 10:20
5.0000 1.0000
MSDA MSDA
ug/L ug/L
:·.% ·RecovefV: :· ·. · . LimitS. ~, : : · ·:-..:, .. y. ~ ''; ~F.: :.%:.t'~_e-c:oveiV/r;::,. t::1mits:; ~: 1'' F :
99 77-117 96 77-117
96 61-143 96 61-143
102 87-113 102 87-113
Page 13 of 66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrv Ion itrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
CA$:
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
020 IHBWW2 l 6
2010213415
Aaueous
Received
NA
02/19/2001 15:45
02/26/2001 11 :44
02/26/2001 11 :44
1.0000
MSDA
ul!IL
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND B
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0201HBWW220 0201HBWW222
2010213414 2010213409
Aaueous Aaueous
Received Received
NA NA
02/19/2001 14:35 02/19/2001 14:15
02/23/2001 15:45 02/23/2001 13:23
02/23/2001 15:45 02/23/2001 13:23
l.0000 1.0000 .
MSDA MSDA
UPIL UQ/L
Cone . Flaa. · DL'· · ·-·~Rt. .. ·cone · f laa·: · 't:>t RL
ND 0.438 0.000 ND 0.438 0.000
ND 6.82 0.000 ND 6.82 0.000
ND 3.79 0.000 ND 3.79 0.000
ND 0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.118 0.000 ND 0.118 0.000
ND 0.170 0.000 ND 0.170 0.000
ND 0.199 0.000 ND 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND 0.0911 0.000 ND 0.0911 0.000
ND B 0.0684 0.000 ND B 0.0684 0.000
ND 0.0652 . 0.000 ND 0.0652 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND 0.0925 0.000
ND 0.0896 0.000 ND 0.0896 0.000
ND 0.0938 0.000 ND 0.0938 0.000
Page 14 of 66
-------------------
- - - -Im; - - -.... - --· -- -.. -- -
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0201HBWW2I6
2010213415
. ·:Parameter· '• ~ :cAs>-<-~-;·, ·cone · · Flaa ·, DL', . '
Chloromethane 74-87-3 ND
3-Chloroorooene 107-05-1 ND
2-Chlorotoluene 95-49-8 ND
4-Chlorotoluene 106-43-4 ND
I.2-Dibromo-3-chloroorooane 96-I2-8 ND
Dibromochloromethane I24-48-l ND
I 2-Dibromoethane 106-93-4 ND
Dibromomethane 74-95-3 ND
trans-I .4-Dichloro-2-butene I 10-57-6 ND
I .4-Dichlorobenzene 106-46-7 .ND
I 2-Dichlorobenzene 95-50-I ND
l 3-Dichlorobenzene 54I-73-I ND
Dichlorodifluoromethane 75-7I-8 ND
I. I-Dichloroethane 75-34-3 ND
I 2-Dichloroethane 107-06-2 ND
l, I-Dichloroethene 75-35-4 ND
cis-1 2-Dichloroethene 156-59-2 ND
trans-I 2-Dichloroethene I56-60-5 ND
I 2-Dichloroorooane 78-87-5 ND
1 3-Dichloroorooane I42-28-9 ND
2 2-Dichloroorooane 594-20-7 ND
I .1-Dichloroorooene 563-58-6 ND
cis-1 3-Dichloroorooene 1006I-OI-5 ND
trans-I 3-Dichloroorooene 10061-02-6 ND
Ethvl methacrvlate 97-63-2 ND
Ethvlbenzene 100-41-4 ND
Hexachloro-I 3-butadiene 87-68-3 ND
2-Hexanone 59I-78-6 ND
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
0.127
0.0777
0.178
0.0974
0.548
0.140
0.137
O.I48
0.780
0.150
0.0965
0.0846
0.237
0.124
0.102
O.I22
O.I 12
0.1 I9
0.0869
0.135
0.160
0.0994
0.0818
0.0908
O.lOI
0.136
0.33I
0.169
0201HBWW220 0201HBWW222
20I02I34I4 2010213409
'···''RI.:' : , . co·nc'• 'f.lacL .. DL :···" ·.,RL'~'-':.·. . ·:cone·· · · · :i;1aa;f:l5fi'~'-~:_:-:;'· RL . '.
0.000 ND 0.127 0.000 ND 0.127 0.000
0.000 ND 0.0777 0.000 ND 0.0777 0.000
0.000 ND 0.178 0.000 ND 0.178 0.000
0.000 ND 0.0974 0.000 ND 0.0974 0.000
0.000 ND 0.548 0.000 ND 0.548 0.000
0.000 ND 0.140 0.000 ND . 0.140 0.000
0.000 ND 0.137 0.000 ND .. O.I37 0.000
0.000 ND O.I48 0.000 ND O.I48 0.000
0.000 ND 0.780 0.000 ND 0.780 0.000
0.000 ND 0.150 0.000 ND O.i50 0.000
0.000 ND 0.0965 0.000 ND 0.0965 o~ooo
0.000 ND 0.0846 0.000 ND 0.0846 0.000
0.000 ND 0.237 0.000 ND 0.237 0.000
0.000. 0.456 J O.I24 0.000 0.589 0.124 0.000
0:000 ND 0.102 0.000 ND 0.102 0.000
0.000 ND 0.122 0.000 0.102 u O.I22 0.000
0.000 ND O.I 12 0.000 0.222 J O.I 12 0.000
0.000 ND 0.1I9 0.000 ND O.I 19 0.000
0.000 ND 0.0869 0.000 ND 0.0869 0.000
0.000 ND 0.135 0.000 ND 0.135 0.000
0.000 ND 0.160 0.000 ND 0.160 0.000
0.000 ND 0.0994 '0.000 ND 0.0994 0.000
0.000 ND 0.08I8 0.000 ND 0.0818 0.000
0.000 ND 0.0908 0.000 ND 0.0908 0.000
0.000 ND 0.101 0.000 ND O.lOI 0.000
0.000 ND 0.136 0.000 ND 0.136 0.000
0.000 ND 0.33 I 0.000 ND 0.331 0.000
0.000 ND 0.169-0.000 ND O.I69 0.000
Page 15 of 66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Client Sample ID
Lab Sample ID
0201HBWW216
2010213415
· · Pararrtetei<' · ,., ... . /, ·".!~?~ ~ ;"~~·~:cAs~·'_'.!~~ .:.1-.i "Ccn1c'"' ~'>:Flaa ... DL r::. ,:·RL>'-:· .• ~:·
lodomethane 74-88-4 ND
lsonronvlbenzene 98-82-8 ND
4-lsooronvltoluene 99-87-6 ND
Methvl methacrvlate 80-62-6 ND
Methvl tert-butvl ether (MTBE\ 1634-04-4 ND
4-Methvl-2-oentanone CMIBK) 108-10-1 ND
Methvlene chloride 75-09-2 ND
Nanhthalene 91-20-3 ND
Pronanenitrile 107-12-0 ND
n-Proovlbenzene 103-65-1 ND
Stvrene 100-42-5 ND
1.1.l 2-Tetrachloroethane 630-20-6 ND
I 1.2.2-Tetrachloroethane 79-34-5 ND
Tetrachloroethene 127-18-4 ND
Tetrahvdrofuran 109-99-9 ND
Toluene 108-88-3 ND
l .2 3-Trichlorobenzene 87-61-6 ND
1.2.4-Trichlorobenzene 120-82-1 ND
1.1.1-Trichloroethane 71-55-6 ND
I 1.2-Trichloroethane 79-00-5 ND
Trichloroethene 79-01-6 ND
Trichlorofluoromethane 75-69-4 ND
I 2 3-Trichloronronane 96-18-4 ND
1.1 2-Trichlorotrifluoroethane 76-13-1 ND
1.2 4-Trimethv I benzene 95-63-6 ND
1.3 5-Trimethv !benzene 108-67-8 ND
Vinvl acetate 108-05-4 ND
Vinvl chloride 75-01-4 ND
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
0:109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
B 0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 0:000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114 0.000
0201HBWW220 0201HBWW222
2010213414 2010213409
· '.·Concf · . Flaa: :· ot; · '.: :·:·:} Rt:::. : ·" :· · ·" · ·cone:-::,:·· .. :F1aa·~:1~ou~r_;.;;:: ~u
ND 0.109 0.000 ND 0.109 0.000
ND 0.0931 0.000 ND 0.0931 0.000
ND 0.115 0.000 ND 0.115 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.116 0.000 ND 0.116 0.000
ND 0.178 0.000 ND 0.178 0.000
ND B 0.126 0.000 ND B 0.126 0.000
ND 0.0801 0.000 ND 0.0801 0.000
ND 1.59 0.000 ND 1.59 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.0977 0.000 ND 0.0977 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.0870 0.000 ND 0.0870 0.000
ND 0.144 0.000 ND 0.144 0.000
ND 0.900 0.000 ND 0.900 0.000
ND 0.0637 0.000 ND 0.0637 0.000
ND 0.551 0.000 ND 0.551 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.169 0.000 ND 0.169 0.000
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.288 0.000 ND 0.288 0.000
ND 0.123 0.000 ND 0.123 0.000
ND 0.124 0.000 ND 0.124 0.000
ND 0.0905 0.000 ND 0.0905 0.000
ND 0.0948 0.000 ND 0.0948 0.000
ND 0.114 0.000 ND 0.114 0.000
Page 16 of 66
----~---~·---~--~---
--- - - -.. -... - -•. -·---' - - -
SECTION IV"
Analytical Results
MS-VOA
SW8260B
Continued
Param·eter-. · ·
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
r. " :CAS • r ':•r
106-42-3
95-47-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW216
2010213415
.. ·: ~: ·cone· Flaa ..
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL ,
0.167
0.0844
0201HBWW220 0201HBWW222
2010213414 2010213409
:RL ~· , ·Cone·; Flaa :oc ;·:::;RL' .":.'. . .'Cone .
> ~Flaa'-·;. !:bLX ·'.'., RL
0.000 ND 0.167 0.000 ND 0.167 0.000
0.000 ND 0.0844 0.000 ND 0.0844 0.000
Page 17 of 66
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW82608
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW216
2010213415
Aaueous
Received
NA
02/19/2001 15:45
02/26/2001 11 :44
02/26/2001 11 :44
1.0000
MSDA
ug/L
% Recoveni
98
98
103
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Limits F
77-117
61-143
87-113
0201HBWW220 0201HBWW222
2010213414 2010213409
Aoueous Aaueous
Received Received
NA NA
02/19/2001 14:35 02/19/2001 14:15
02/23/2001 15:45 02/23/2001 13:23
02/23/2001 15:45 02/23/2001 13:23
1.0000 1.0000
MSDA MSDA
u!!IL u!!IL
-%' Recoverv · · limit$''. " .F , % Recoverv · um its F
96 77-117 96 77-117
102 61-143 97 61-143
101 87-113 103 87-113
Page 18 of 66
------~-~---------~
------~~----~------
SECTION IV
Analytical Results
MS-VOA
SW8260B
·Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chioro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
,-
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
_, -CAS.
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/200I 13:42
0201HBWW224
2010213412
Aaueous
Received
NA
02119/2001 15: 10
02/23/2001 14:47
02/23/2001 14:47
1.0000
MSDA
ug/L
·:_Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.571 JB
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102I34] Hamilton Beach-Proctor Silex
STLAustin
DL :_ RL-,. --·,
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 6.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0201 HBWW225 0201HBWW226
2010213413 2010213410
Aaueous Aaueous
Received Received
NA NA
02/19/2001 15:15 02/19/200113:30
02/23/2001 15: 15 02/23/2001 13:51
02/23/2001 15:15 02/23/2001 13:51
1.0000 1.0000
MSDA MSDA
ug/L ug/L
cone. Flaa·. ~DL'':-':~·-:· Rt:.,, : ·cone._,. r J~iaa, . -:ot::·· .. -: ,·Rt.· ,, ,,
ND 0.438 0.000 ND 0.438 0.000
ND 6.82 0.000 ND 6.82 0.000
ND 3.79 0.000 ND 3.79 0.000
ND 0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND -0.131 0.000
ND 0.118 0.000 ND 0.118 0.000
ND 0.170 0.000 ND 0.170 0.000
ND 0.199 0.000 ND 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND 0.0911 0.000 ND 0.0911 0.000
0.511 JB 0.0684 0.000 ND B 0.0684 0.000
ND 0.0652 0.000 ND 0.0652 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND 0.0925 0.000
ND 0.0896 0.000 ND 0.0896 0.000
ND 0.0938 0.000 ND 0.0938 0.000
Page I9 of 66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter ',<. ', '• .··".:CAS':· '1'/1;t.
Chloromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
l .2-Dibromo-3-chlorooronane 96-12-8
Dibromochloromethane 124-48-1
1 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
I 1-Dichloroethane 75-34-3
1 2-Dichloroethane 107-06-2
1 1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-1.2-Dichloroethene 156-60-5
I 2-Dichloroorooane 78-87-5
1 3-Dichloroorooane 142-28-9
2 2-Dichloroorooane 594-20-7
I 1-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-1.3-Dichloronronene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW224
2010213412
.·Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Di.' .... ,
0.127
0.0777
0.178
0.0974
0.548
0.140
0.137
0.148
0.780
0.150
0.0965
0.0846
0.237
0.124
0.102
0.122
0.112
0.119
0.0869
0.135
0.160
0.0994
0.0818
0.0908
0.101
0.13,6
0.331
0.169
0201HBWW225 0201HBWW226
2010213413 2010213410
RL, ···, cone · : . Fiaa, 'DL: ·: :· Rt>-c : :cone ·,~Flaa· ·ai::.;, > ,RL
0.000 ND 0.127 0.000 ND 0.127 0.000
0.000 ND 0.0777 0.000 ND 0.0777 0.000
0.000 ND 0.178 0.000 ND 0.178 0.000
0.000 ND 0.0974 0.000 ND 0.0974 0.000
0.000 ND 0.548 0.000 ND 0.548 0.000
0.000 ND 0.140 0.000 ND 0.140 0.000
0.000 ND 0.137 0.000 ND 0.137 0.000
0.000 ND 0.148 0.000 ND 0.148 0.000
0.000 ND 0.780 0.000 ND 0.780 0.000
0.000 ND 0.150 0.000 ND 0.150 0.000
0.000 ND 0.0965 0.000 ND 0.0965 0.000
0.000 ND 0.0846 0.000 ND 0.0846 0.000
0.000 ND 0.237 0.000 ND 0.237 0.000
0.000 ND 0.124 0.000 ND 0.124 0.000
0-.000 ND 0.102 0.000 ND 0.102 0.000
0.000 ND 0.122 0.000 ND 0.122 0.000
0.000 ND 0.112 0.000 ND 0.112 0.000
0.000 ND 0.119 0.000 ND 0.119 0.000
0.000 ND 0.0869 0.000 ND 0.0869 0.000
0.000 ND 0.135 0.000 ND 0.135 0.000
0.000 ND 0.160 0.000 ND 0.160 0.000
0.000 ND 0.0994 0.000 ND 0.0994 0.000
0.000 ND 0.0818 0.000 ND 0.0818 0.000
0.000 ND 0.0908 0.000 ND 0.0908 0.000
0.000 ND 0.101 0.000 ND 0.101 0.000
0.000 ND 0.136 0.000 ND 0.136 0.000
0.000 ND 0.331 0.000 ND 0.331 0.000
0.000 ND 0.169 0.000 ND 0.169 0.000
Page 20 of 66
------~-----~------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
'' ,parameter
n-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
.._'; '::CAS"; ',:>., ~-"
106-42-3
95-47-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW224
2010213412
~Cone " Flaa':
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL ·-
0.167
0.0844
0201HBWW225 0201HBWW226
2010213413 2010213410
'RL"··~y :cone'-':~·· , Flaa7· DC';·, " ;,Rt;;','< ' -~'Cone·· : F.lad(~·EC.~ ;·;-.:" :.Rt'
0.000 ND 0.167 0.000 ND 0.167 0.000
0.000 ND 0.0844 0.000 ND 0.0844 0.000
Page 22 of 66
-----~~~----~------
~-~-~--~----~~--~--
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
Date/Time Collected
Date/Time Prepared
Date/Time Analyzed
Dilution Factor
Instrument
Units
:~ surrociate:.comoound ' ~ < ,~ ! ,~ "'.:. ~w•; " ~'.;
"
.. ~/ ~_,., ' l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -0310512001 13:42
0201,HBWW224
2010213412
Aaueous
Received
NA
02/19/2001 15:10
02/23/2001 14:47
02/23/2001 14:47
1.0000
MSDA
ug/L
'.%Recoven( "
.,
96
100
102
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
l.irhitS '-,.:;
77-117
61-143
87-113
0201HBWW225 0201HBWW226
2010213413 2010213410
Aaueous Aaueous
Received Received
NA NA
02/19/2001 15:15 02/19/2001 13:30
02/23/2001 15:15 02/23/2001 13:51
02/23/2001 15:15 02/23/2001 13:51
1.0000 1.0000
MSDA MSDA
UQ-/f. ug/L
. ":~ __ .-'\i;'!; '. ·%'·Recovani::?~~ J.ir.nit8t<-,:;:t1·~:::: :: r. ·fF: .·%··aecoieiY'· :.<limits· .. ::·;· ~, ... P;~·--F '· .
97 77-117 98 77-117
98 61-143 100 61-143
103 87-113 100 87-113
Page 23 of 66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units·
0201 HBWW227
2010213405
Aaueous
Received
NA
02/20/2001 09:35
02/26/2001 14:09
02/26/2001 14:09
50.0000
MSDA
ug/L
Parameter CAS Cone Flaa;·· DL
Acetone 67-64-1 ND
Acetonitrile 75-05-8 ND
Acrolein 107-02-8 ND
Acrvlonitrile 107-13-1 ND
Benzene 71-43-2 ND
Bromobenzene 108-86-1 ND
Bromochloromethane 74-97-5 ND
Bromodichloromethane 75-27-4 ND
Bromoform 75-25-2 ND
Bromomethane 74-83-9 ND
2-Butanone (MEK) 78-93-3 ND
n-Butvlbenzene 104-51-8 ND
sec-Butvlbenzene 135-98-8 ND
tert-Butvlbenzene 98-06-6 ND
Carbon disulfide 75-15-0 ND
Carbon tetrachloride 56-23-5 ND
2-Chloro-1 3-butadiene 126-99-8 ND
Chlorobenzene 108-90-7 ND
Chloroethane 75-00-3 27.3
Chloroform 67-66-3 ND
1-Chlorohexane 544-10-5 ND
SECTION IV -Analytical Results -03/05/2001 13:42
LIMS Workorder: 80396907.0l [20102134] Hamilton Beach-Proctor Silex
STLAustin
21.9
341
190
22.3
3.20
4.99
6.55
5.90
8.50
9.95
10.0
5.10
5.25
4.56
B 3.42
3.26
5.70
4.21
4.62
4.48
4.69
. 'RL."
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0201HBWW227 0201HBWW228
2010213405 2010213406
Aaueous Aaueous
Received Received
NA NA
02/20/2001 09:35 02/20/2001 09:45
02/26/2001 18:07 02/26/2001 14:37
02/26/2001 18:07 02/26/2001 14:37
10.0000 200.0000
MSDA MSDA
u~/L U!!IL
·cone Flaa .DL
.. ,
RL Cone. -Flaa· DL RL
ND 4.38 0.000 ND 87.6 0.000
ND 68.2 0.000 ND 1360 0.000
ND 37.9 0.000 ND 758 0.000
ND 4.46 0.000 ND 89.2 0.000
ND 0.641 0.000 30.8 J 12.8 0.000
ND 0.998 0.000 ND 20.0 0.000
ND 1.31 0.000 ND 26.2 0.000
ND 1.18 0.000 ND 23.6 0.000
ND 1.70 0.000 ND 34.0 0.000
ND 1.99 0.000 ND 39.8 0.000
25.2 J 2.00 0.000 413 J 40.0 0.000
ND 1.02 0.000 31.5 J 20.4 0.000
ND 1.05 0.000 ND 21.0 0.000
ND 0.911 0.000 ND 18.2 0.000
ND B 0.684 0.000 ND B 13.7 0.000
ND 0.652 0.000 ND 13.0 0.000
ND 1.14 0.000 ND 22.8 0.000
ND 0.842 0.000 ND 16.8 0.000
24.6 0.925 0.000 66.3 J 18.5 0.000
ND 0.896 0.000 ND 17.9 0.000
ND 0.938 0.000 ND 18.8 0.000
Page 24 of 66
...... _ --··· --- -·--- - - - - - - -.,... -
/
~-~~---~--~---~-~--
SECTION IV
Analytical Results
MS-VOA
SW82608
Client Sample ID
Lab Sample ID
Continued
. Parameter~ ·· ·--·. ''CAS !;.:i /' '.·:--~
Chioromethane 74-87-3
3-Chloroorooene 107-05-I
2-Chlorotoluene 95-49-8
4-Chlorotoiuene 106-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-I
1 2-Dibromoethane I06-93-4
Dibromomethane 74-95-3
trans-I 4-Dichioro-2-butene I 10-57-6
1.4-Dichlorobenzene 106-46-7
1,2-Dichlorobenzene 95-50-1
1.3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
I ,2-Dichloroethane I07-06-2
I .1-Dichloroethene 75-35-4
cis-I 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1 2-Dichloroorooane 78-87-5
1 3-Dichloroprooane 142-28-9
2 2-Dichloroorooane 594-20-7
U-Dichloroprooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-I 3-Dichloroorooene 1006I-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene I00-4I-4
Hexachloro-13-butadiene 87-68-3
2-Hexanone 59I-78-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW227
20102I3405
.Cone Flaa:
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2300
I2.9 J
394
281
4.10 u
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
oL· > ·,:-RL":'.: ... '·
6.35 0.000
3.88 0.000
8.90 0.000
4.87 0.000
27.4 0.000
7.00 0.000
6.85 0.000
7.40 0.000
39.0 0.000
7.50 0.000
4.82 0.000
4.23 0.000
I 1.8 0.000
6.20 0.000
5.10 0-.000
6.IO 0.000
5.60 0.000
5.95 0.000
4.34 0.000
6.75 0.000
8.00 0.000
4.97 0.000
4.09 0.000
4.54 0.000
5.05 0.000
6.80 0.000
16.6 0.000
8.45 0.000
0201HBWW227 0201HBWW228
20102I3405 20102I3406
·cone·.;.• Flaa. · oa.; ..... -.RE.:; .'i . cone··: · :· ·f:1aa·1.1.:ot:;. :·>: <Rt
ND 1.27 0.000 ND 25.4 0.000
ND 0.777 0.000 ND I5.5 0.000
ND 1.78 0.000 ND 35.6 0.000
ND 0.974 0.000 ND I9.5 0.000
ND 5.48 0.000 ND I 10 0.000
ND 1.40 0.000 ND 28.0 0.000
ND 1.37 0.000 ND ' . 27.4 0.000
ND 1.48 0.000 ND 29.6 0.000
ND 7.80 0.000 ND 156 0.000
ND 1.50 0.000 ND 30.0 0.000
ND 0.965 0.000 ND 19.3 0.000
ND 0.846 0.000 ND 16.9 0.000
ND 2.37 0.000 ND 47.4 0.000
I780 ER 1.24 0.000 10200 24.8 0.000
10.8 1.02 0.000 59.5 J --20.4 0.000
332 1.22 0.000 28400 ER 24.4 0.000
240 1.12 0.000 2870 22.4 0.000
5.48 1.19 0.000 ND 23.8 0.000
ND 0.869 0.000 ND 17.4 0.000
ND 1.35 0.000 ND 27.0 0.000
ND 1.60 0.000 ND 32.0 0.000
ND 0.994 0.000 ND 19.9 0.000
ND 0.818 0.000 ND 16.4 0.000
ND 0.908 0.000 ND I8.2 0.000
ND l.OI 0.000 ND 20.2 0.000
ND 1.36 0.000 729 27.2 0.000
ND 3.3 I 0.000 ND 66.2 0.000
ND 1.69 0.000 ND 33.8 0.000
Page 25 of 66
SECTION IV
Analytical Results
MS-VOA
SW82608
Client Sample ID
Lab Sample ID
Continued
Parameter' : · · · ... ·.·-'':,,-cAs·:: ...-·~ :~.
Iodomethane 74-88-4
Isooroov !benzene 98-82-8
4-lsooroovltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether <MTBE) 1634-04-4
4-Methvl-2-pentanone (MIBK) 108-10-1
Methylene chloride 75-09-2
Naohthalene 91-20-3
Propanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
I.I 1.2-Tetrachloroethane 630-20-6
IJ.2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
1.2.4-Trichlorobenzene 120-82-1
I.I I-Trichloroethane 71-55-6
1.1.2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2.3-Trichloroorooane 96-18-4
1 1 2-Trichlorotrifluoroethane 76-13-1
I 2 4-Trimethvlbenzene 95-63-6
I 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW227
2010213405
·'Cone! :-Fiao:
ND
ND
ND
ND
ND
ND.
ND B
ND
ND
ND
ND
ND
ND
ND
ND
12.3 J
ND
ND
1760
ND
38.7
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL ·" .. RL .,
5.45 0.000
4.66 0.000
5.75 0.000
6.55 0.000
5.80 0.000
8.90 0.000
6.30 0.000
4.00 0.000
79.5 0.000
7.00 0.000
4.88 0.000
5.55 0.000
4.35 0.000
7.20 0.000
45.0 6.000
3.18 0.000
27.6 0.000
6.75 0.000
8.45 0.000
4.10 0.000
6.85 0.000
5.30 0.000
14.4 0.000
6.15 0.000
6.20 0.000
4.52 0.000
4.74 0.000
5.70 0.000
0201HBWW227 0201HBWW228
2010213405 2010213406
tone:-Flaa." D~: <' "'RL ... ..::. ' :·cone ... '. '.·'Fl ta' ··ot::.:.:.: ... ,ff.l. . , a . .. ....
ND 1.09 0.000 ND 21.8 0.000
ND 0.931 0.000 51.4 J 18.6 0.000
ND 1.15 0.000 ND 23.0 0.000
ND 1.31 0.000 ND 26.2 0.000
ND 1.16 0.000 ND 23.2 0.000
ND 1.78 0.000 ND 35.6 0.000
0.628 UB 1.26 0.000 21.5 UB 25.2 0.000
ND 0.801 0.000 1020 16.0 0.000
ND 15.9 0.000 ND 318 0.000
ND 1.40 0.000 284 28.0 0.000
ND 0.977 0.000 19.7 J 19.5 0.000
ND 1.11 0.000 ND 22.2 0.000
ND 0.870 0.000 ND 17.4 0.000
ND 1.44 0.000 10.0 u 28.8 0.000
ND 9.00 0.000 ND 180 0.000
10.7 0.637 0.000 1250 12.7 0.000
ND 5.51 0.000 ND llO 0.000
ND l.35 0.000 ND 27.0 0.000
1430 ER 1.69 0.000 44700 ER 33.8 0.000
ND 0.821 0.000 ND 16.4 0.000
39.6 l.37 0.000 15400 27.4 0.000
ND 1.06 0.000 ND 21.2 0.000
ND 2.88 0.000 ND 57.6 0.000
ND 1.23 0.000 ND 24.6 0.000
ND 1.24 0.000 1740 24.8 0.000
ND 0.905 0.000 430 18.1 0.000
ND 0.948 0.000 ND 19.0 0.000
4.73 J 1.14 0.000 337 22.8 0.000
Page 26 of 66
-------~-----------
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
Daterrime Analyzed
Dilution Factor
Instrument
Units
Surroaate ComDound
l -Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW227
2010213405
Aaueous
Received
NA
02/20/2001 09:35
02/26/2001 14:09
02/26/2001 14:09
50.0000
MSDA
ug/L
% Recoverv
99
97
103
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAustin
" Limits F
77-117
61-143
87-113
0201HBWW227 0201HBWW228
2010213405 2010213406
Aaueous Aaueous
Received Received
NA NA
02/20/2001 09:35 02/20/2001 09:45
02/26/2001 18:07 02/26/2001 14:37
02/26/2001 18:07 02/26/2001 14:37
10.0000 200.0000
MSDA MSDA
ug/L U!!:IL
% Reeove..V Limits·. · F %R~cc>velY •> Limits .. F
96 77-117 98 77-117
96 61-143 87 61-143
103 87-113 102 87-113
Page 28 of 66
-----~~-----~---~--
--~-----~~-~~---~~-
SECTION IV
Analytical Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone <MEK)
n-Butv !benzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTirne Analyzed
Dilution Factor
Instrument
Units
. CAS -:
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW228
2010213406
Aaueous
Received
NA
021201200 I 09:45
02/26/2001 16:43
02/26/2001 16:43
1000.0000
MSDA
ug/L
Cone Flaa .
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND B
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL· .. ·RL:~/ . '
438 0.000
6820 0.000 -
3790 0.000
446 0.000
64.1 0.000
99.8 0.000
131 0.000
118 '0.000
170 0.000
199 0.000
200 0.000
102 0.000
105 0.000
91.1 0.000
68.4 0.000
65.2 0.000
114 0.000
84.2 0.000
92.5 0.000
89.6 0.000
93.8 0.000
0201HBWW228 020 IHBWW230
2010213406 2010213408
Aaueous Aaueous
Received Received
NA NA
0212012001 09:45 02/19/200i 11:30
02/26/2001 18:37 02/23/2001 12:55
02/26/2001 18:37 02/23/2001 12:55
50.0000 1.0000
MSDA MSDA
ug/L U!!IL
·-Coric . >· Flaa'.,· 'i:>L·;. -;;~. 'RL:·;·; .·/ -~:: : Conc~·.:_;:,':)flaa· DL ... ·,Rl
364 21.9 0.000 ND 0.438 0.000
ND 341 0.000 ND 6.82 0.000
ND 190 0.000 ND 3.79 0.000
ND 22.3 0.000 ND 0.446 0.000
38.7 3.20 0.000 ND 0.0641 0.000
ND 4.99 0.000 ND 0.0998 0.000
ND 6.55 0.000 ND . 0.131 0.000
Nb 5.90 0.000 ND -~ 0.118 0.000
ND 8.50 0.000 ND 0.170 0.000
ND 9.95 0.000 ND 0.199 0.000
500 10.0 0.000 ND 0.200 0.000
28.9 J 5.10 0.000 ND 0.102 0.000
9.56 J 5.25 0.000 ND 0.105 0.000
ND 4.56 0.000 ND 0.0911 0.000
ND B 3.42 0.000 ND B 0.0684 0.000
23.0 J 3.26. 0.000 ND 0.0652 0.000
ND 5.70 0.000 ND 0.114 0.000
ND 4.21 0.000 ND 0.0842 0.000
97.3 4.62 0.000 ND 0.0925 0.000
7.64 J 4.48 0.000 ND 0.0896 0.000
ND 4.69 0.000 ND 0.0938 0.000
Page 29 of 66
SECTION IV·
Analytical Results
MS-VOA
SW82608
Client Sample ID
Lab Sample ID
Continued
·Parameter .. .. . .. · ,:c.As: . .-_::~;;: . ·.
Chloromethane 74-87-3
3-Chloroorooene 107-05-I
2-Chlorotoluene 95-49-8
4-Chlorotoluene I06-43-4
I 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-I
I .2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-I 4-Dichloro-2-butene I 10-57-6
I 4-Dichlorobenzene I06-46-7
I 2-Dichlorobenzene 95-50-I
I 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
I 2-Dichloroethane 107-06-2
I. I-Dichloroethene 75-35-4
cis-I .2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene I56-60-5
I 2-Dichloroorooane 78-87-5
I .3-Dichloroorooane I42-28-9
2.2-Dichloroorooane 594-20-7
I. I-Dichloroorooene 563-58-6
cis-1.3-Dichloroorooene l006I-Ol-5
trans-I 3-Dichloroorooene l006I-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene I00-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW228
2010213406
~·cone: . Flaa·
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
10500
ND
29800
2790
ND
ND
ND
ND
ND
ND
ND
ND
729
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL '··RL ."'· ·:.
I27 0.000
77.7 0.000
I78 0.000
97.4 0.000
548 0.000
I40 0.000
I37 0.000
I48 0.000
780 0.000
I50 0.000
96.5 0.000
84.6 0.000
237 0.000
124 0.000
102 0:000
I22 0.000
112 0.000
119 0.000
86.9 0.000
135 0.000
160 0.000
99.4 0.000
81.8 0.000
90.8 0.000
101 0.000
136 0.000
331 0.000
169 0.000
0201HBWW228 0201HBWW230
2010213406 2010213408
·Cone ... ··.Flaa. · oL: · . ·: ···.' Rl:i .. {· ..: ·•:cone-: · : .. ?ffali'.,:ot:~·:·;, -..Rt
ND 6.35 0.000 ND 0.127 0.000
ND 3.88 0.000 ND 0.0777 o.ono
ND 8.90 0.000 ND 0.178 0.000
ND 4.87 0.000 ND 0.0974 0.000
ND 27.4 0.000 ND 0.548 0.000
ND 7.00 0.000 ND 0.I40 0.000
ND 6.85 0.000 ND O.I37 0.000
ND 7.40 0.000 ND 0.148 0.000
ND 39.0 0.000 ND 0.780 0.000
ND 7.50 0.000 ND O.I50 0.000
ND 4.82 0.000 ND 0.0965 0.000
ND 4.23 0.000 ND 0.0846 0.000
ND 11.8 0.000 ND 0.237 0.000
I I700 ER 6.20 0.000 ND 0.I24 0.000
79.9 5.10 0.000 ND 0.102 0.000
25900 ER 6.10 0.000 ND 0.122 0.000
3740 5.60 0.000 0.0969 u 0.I 12 0.000
22.5 J 5.95 0.000 ND 0.119 0.000
ND 4.34 0.000 ND 0.0869 0.000
ND 6.75 0.000 ND 0.135 0.000
ND 8.00 0.000 ND 0.160 0.000
ND 4.97 0.000 ND 0.0994 0.000
ND 4.09 0.000 ND 0.0818 0.000
ND 4.54 0.000 ND 0.0908 0.000
ND 5.05 0.000 ND 0.101 0.000
970 6.80 0.000 ND 0.136 0.000
ND 16.6 0.000 ND 0.331 0.000
ND 8.45 0.000 ND 0.169 0.000
Page 30 of 66
~-~-~---~---~---~--
-----~--~--~~--~~--
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
. Parameter · : "" ·cAS : '; :,::.
Iodomethane 74-88-4
Isopropylbenzene 98-82-8
4-Isoorooyltoluene 99-87-6
Methyl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) I634-04-4
4-Methyl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naphthalene 91-20-3
Prooanenitrile l07-I2-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1.1.1 2-Tetrachloroethane 630-20-6
1 1,2 2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-I8-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1 2 3-Trichiorobenzene 87-61-6
1,2 4-Trichlorobenzene I20-82-l
1.1 I -Trichloroethane 71-55-6
lJ 2-Trichloroethane 79-00-5
Trichloroethene 79-0I-6
Trichlorofluoromethane 75-69-4
1 2,3-Trichloroorooane 96-18-4
l, 1 2-Trichlorotrifluoroethane 76-13-1
1 2 4-Trimethvlbenzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinyl chloride 75-01-4
SECTION IV -Analytical Results -03/05/2001 13:42
020 IHBWW228
2010213406
. Cone. Flaa
ND
ND
ND
ND
ND
ND
ND B
875 J
ND
234 J
ND
ND
ND
ND
ND
1220
ND
ND
50500
ND
15600
ND
ND
ND
1570
431 J
ND
299 J
LIMS Workorder: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STLAustin
DL ·.-
109
93.l
II5
13I
116
178
126
80.l
I590
140
97.7
I 11
87.0
I44
900
63.7
551
135
169
82.1
137
106
288
123
124
90.5
94.8
114
0201HBWW228 0201HBWW230
2010213406 2010213408
RL Cone~·.: ..• Flaa; .. _ DL <· ,. : RL·;,:> ,: . '. /:Cone··. :.:;_f.faa::~·fol!.~:~::: · .... ·RL
0.000 ND 5.45 0.000 ND 0.109 0.000
0.000 63.8 4.66 0.000 ND 0.093I 0.000
0.000 ND 5.75 0.000 ND O.I I5 0.000
0.000 ND 6.55 0.000 ND O.I31 0.000
0.000 ND 5.80 0.000 ND O.I I6 0.000
0.000 ND 8.90 0.000 ND ... 0.178 0.000
0.000 4.40 UB 6.30 0.000 ND B .. 0.126 0.000
0.000 973 4.00 0.000 ND 0.0801 0.000
0.000 ND 79.5 0.000 ND 1.59 0.000
0.000 354 7.00 0.000 ND O.I40 0.000
0.000 28.3 4.88 0.000 ND 0.0977 0.000
0.000 ND 5.55 0.000 ND 0.111 0.000
0.000 ND 4.35 0.000 ND 0.0870 0.000
0.000 I8.6 J 7.20 0.000 ND -0.144 0.000
0-.000 ND 45.0 0.000 ND . 0.900 0.000
0.000 I6IO 3.I8 0.000 ND 0.0637 0.000
0.000 ND 27.6 0.000 ND 0.551 0.000
0.000 ND 6.75 0.000 ND 0.135 0.000
0.000 39900 ER 8.45 0.000 ND 0.169 0.000
0.000 25.l 4.10 0.000 ND 0.082I 0.000
0.000 17000 ER 6.85 0.000 0.160 J 0.137 0.000
0.000 28.2 J 5.30 0.000 ND 0.106 0.000
. 0.000 ND 14.4 0.000 ND 0.288 0.000
0.000 ND 6.15 0.000 ND 0.123 0.000
0.000 2110 6.20 0.000 ND 0.124 0.000
0.000 530 4.52 0.000 ND 0.0905 0.000
0.000 ND 4.74 0.000 ND 0.0948 0.000
0.000 492 5.70 0.000 ND 0.114 0.000
Page 31 of 66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Continued
Parameter
o-Xvlene/m-Xvlene
o-Xvlene
Client Sample ID
Lab Sample ID
CAs·.
106-42-3
95-47-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW228
2010213406
'' ~ >' :i. Cone· ··Flaa
1860
1550
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL ·RL·.
167 0.000
84.4 0.000
0201HBWW228 0201HBWW230
2010213406 2010213408
... Cone ' . Flaa ·OL ·Re·:· . . cone · , :flacf · · ol·· RL
2530 8.35 0.000 ND 0.167 0.000
2150 4.22 0.000 ND 0.0844 0.000
Page 32 of 66
--------~---~------
SECTION IV
Analytical Results
MS-VOA
SW82608
Parameter
Acetone
Acetonitrile
Acrolein
Acrv lonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butv lbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-l 3-butadiene
Chlorobenzene
Chloroethane
Chloroform
1-Chlorohexane
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
lnstr~ment
Units
CAS
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW234
2010213411
Aaueous
Received
NA
02/19/2001 13:55
02/23/2001 14:19
02/23/2001 14:19
1.0000
MSDA
ug/L
Cone Flaa
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND B
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000
0.102 0.000
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
TRIP BLANK TRIP BLANK
2010213407 2010213417
Aaueous Aaueous
Received Received
NA NA
02/20/2001 00:00 02/19/2001 00:00
02/23/2001 11 :58 02/23/2001 12:27
02/23/2001 11 :58 02/23/2001 12:27
1.0000 1.0000 .
MSDA MSDA
ug/L ug/L
Cone. Flaa ·DL . RL · Cone · · · · Flaa · · DL RL
ND 0.438 0.000 ND 0.438 0.000
ND 6.82 0.000 ND 6.82 0.000
ND 3.79 0.000 ND 3.79 0..000
ND 0.446 0.000 ND 0.446 0.000
ND 0.0641 0.000 ND 0.0641 0.000
ND 0.0998 0.000 ND 0.0998 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.118 0.000 ND 0.118 0.000
ND 0.170 0.000 ND 0.170 0.000
ND 0.199 0.000 ND 0.199 0.000
ND 0.200 0.000 ND 0.200 0.000
ND 0.102 0.000 ND 0.102 0.000
ND 0.105 0.000 ND 0.105 0.000
ND 0.0911 0.000 ND 0.0911 0.000
ND B 0.0684 0.000 ND B 0.0684 0.000
ND 0.0652 . 0.000 ND 0.0652 0.000
ND 0.114 0.000 ND 0.114 0.000
ND 0.0842 0.000 ND 0.0842 0.000
ND 0.0925 0.000 ND 0.0925 0.000
ND 0.0896 0.000 ND 0.0896 0.000
ND 0.0938 0.000 ND 0.0938 0.000
Page 34 of 66
-~--------------~~-
-~----------~------
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Param·eter , , .. CAS·\··.· ·
Chloromethane 74-87-3
3-Chloroorooene 107-05-1
2-Chlorotoluene 95-49-8
4-Chlorotoluene 106-43-4
1.2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
l 2-Dibromoethane 106-93-4
Dibromomethane 74-95-3
trans-1 4-Dichloro-2-butene 110-57-6
1 4-Dichlorobenzene 106-46-7
l 2-Dichlorobenzene 95-50-1
l 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
· 1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichlorooronane 78-87-5
l 3-Dichloroorooane 142-28-9
2 2-Dichlorooronane 594-20-7
1 1-Dichloroorooene 563-58-6
cis-1.3-Dichloronronene 10061-01-5
trans-1.3-Dichloroorooene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethv !benzene 100-41-4
Hexachloro-1.3-butadiene 87-68-3
2-Hexanone 591-78-6
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW234
201021341 l
Coric Flaa.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL
0.127
0.0777
0.178
0.0974
0.548
0.140
0.137
0.148
0.780
0.150
0.0965
0.0846
0.237
0.124
0.102
0.122
0.112
0.119
0.0869
0.135
0.160
0.0994
0.0818
0.0908
0.101
0.136
0.331
0.169
TRIP BLANK TRIP BLANK
2010213407 2010213417
... RL" . cone· FJaa~ ·oL:.-.. ·:Rt.:·,.,' , ,. ·caner .: . ::: '1t1aa-:t~:Ol(~ ', : .·RL' ,, ', ,;,,
0.000 ND 0.127 0.000 ND 0.127 0.000
0.000 ND 0.0777 0.000 ND 0.0777 0.000
0.000 ND 0.178 0.000 ND 0.178 0.000
0.000 ND 0.0974 0.000 ND 0.0974 0.000
0.000 ND 0.548 0.000 ND 0.548 0.000
0.000 ND 0.140 0.000 ND :-:A 0.140 0.000
0.000 ND 0.137 0.000 ND ~ 0.137 0.000
0.000 ND 0.148 0.000 ND 0.148 0.000
0.000 ND 0.780 0.000 ND 0.780 0.000
0.000 ND 0.150 0.000 ND 0.150 0.000
0.000 ND 0.0965 0.000 ND 0.0965 0.000
0.000 ND 0.0846 0.000 ND 0.0846 0.000
0.000 ND 0.237 0.000 ND 0.237 0.000
0.000 ND 0.124 0.000 ND ... 0.124 0.000
0'.000 ND 0.102 0.000 ND -·· 0.102 0.000
0.000 ND 0.122 0.000 ND 0.122 0.000
0.000 ND 0.112 0.000 ND 0.112 0.000
0.000 ND 0.119 0.000 ND 0.119 0.000
0.000 ND 0.0869 0.000 ND 0.0869 0.000
0.000 ND 0.135 0.000 ND 0.135 0.000
0.000 ND 0.160 0.000 ND 0.160 0.000
0.000 ND 0.0994 0.000 ND 0.0994 0.000
0.000 ND 0.08i8 0.000 ND 0.0818 0.000
0.000 ND 0.0908 0.000 ND 0.0908 0.000
0.000 ND 0.101 0.000 ND 0.101 0.000
0.000 ND 0.136 0.000 ND 0.136 0.000
0.000 ND 0.331 0.000 ND 0.331 0.000
0.000 ND 0.169 0.000 ND 0.169 0.000
Page 35 of 66
SECTION IV
Analytical Results
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Continued
Parameter -.-.CAS
Iodomethane 74-88-4
Isooronvlbenzene 98-82-8
4-Isooroovltoluene 99-87-6
Methv I methacrvlate 80-62-6
Methvl tert-butvl ether <MTBE) 1634-04-4
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 l, 1.2-Tetrachloroethane 630-20-6
l 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
l ,2,3-Trichlorobenzene 87-61-6
1 2.4-Trichlorobenzene 120-82-1
l 1 I-Trichloroethane 71-55-6
1.1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1.2.3-Trichlorooronane 96-18-4
l l ,2-Trichlorotrifluoroethane 76-13-1
l 2.4-Trimethv I benzene 95-63-6
1.3,5-Trimethv !benzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW234
2010213411
, ... ·,· Cone Flaa , , .
ND
ND
ND
ND
ND
ND
ND B
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAustin
DL . RL
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
0.178 0.000
0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000
0.111 0.000
0.0870 0.000
0.144 0.000
0.900 (t.000
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114 0.000
TRIP BLANK TRIP BLANK
2010213407 2010213417
~ ·Coric ,-Flaa -,bl' ·-. RL:-· 'Cone; Fliia: _ DL ~ ::_ . RL
ND 0.109 0.000 ND 0.109 0.000
ND 0.0931 0.000 ND 0.0931 0.000
ND 0.115 o.ooo. ND 0.115 0.000
ND 0.131 0.000 ND 0.131 0.000
ND 0.116 0.000 ND 0.116 0.000
ND 0.178 0.000 ND 0.178 0.000
ND B 0.126 0.000 ND B 0.126 0.000
ND 0.0801 0.000 ND 0.0801 0.000
ND l.59 0.000 ND 1.59 0.000
ND 0.140 0.000 ND 0.140 0.000
ND 0.0977 0.000 ND 0.0977 0.000
ND 0.111 0.000 ND 0.111 0.000
ND 0.0870 0.000 ND 0.0870 0.000
ND 0.144 0.000 ND 0.144 0.000
ND 0.900 0.000 ND 0.900 0.000
ND 0.0637 0.000 ND 0.0637 0.000
ND 0.551 0.000 ND 0.551 0.000
ND 0.135 0.000 ND 0.135 0.000
ND 0.169 0.000 ND 0.169 0.000
ND 0.0821 0.000 ND 0.0821 0.000
ND 0.137 0.000 ND 0.137 0.000
ND 0.106 0.000 ND 0.106 0.000
ND 0.288 0.000 ND 0.288 0.000
ND 0.123 0.000 ND 0.123 0.000
ND 0.124 0.000 ND 0.124 0.000
ND 0.0905 0.000 ND 0.0905 0.000
ND 0.0948 0.000 ND 0.0948 0.000
ND 0.114 0.000 ND 0.114 0.000
Page 36 of 66
-~-----~-----------
SECTION IV
Analytical Results
Surrogates
MS-VOA
SW8260B
Client Sample ID
Lab Sample ID
Matrix
Reported As
% Moisture
DatefTime Collected
DatefTime Prepared
DatefTime Analyzed
Dilution Factor
Instrument
Units
Surroaate Comoound
l-Bromo-4-fluorobenzene
I.2-Dichloroethane-d4
Toluene-d8
SECTION IV -Analytical Results -03/05/2001 13:42
0201HBWW234
2010213411
Aaueous
Received
NA
02/19/2001 13:55
02/23/2001 14:19
02/23/2001 14:19
1.0000
MSDA
ui!IL
% Recoverv
97
101
101
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAustin
LlmltS F
77-117
61-143
87-113
TRIP BLANK TRIP BLANK
2010213407 2010213417
Aaueous Aaueous
Received Received
NA NA
02/20/2001 00:00 02/19/2001 00:00
02/23/2001 11 :58 02/23/2001 12:27
02/23/2001 ll :58 02/23/2001 12:27
1.0000 1.0000
MSDA MSDA
u!!IL u!!IL
•1o Recovery Limits·· ''•' F % Recovery Limits F
95 77-117 97 77-117
100 61-143 100 61-143
100 87-113 102 87-113
Page 38 of 66
-------------------
- -------~----------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 10778 Instrument Data File: A0222102.D
Instrument ID: MSDA Analyst: BJP
:Parameter -:R.eference:Value. · Measured Coric
Acetone 20 18.5
Acetonitrile 100 79.l
Acrolein 100 68.2
Acrv lonitrile 20 16.4
Benzene 20 17.0
Bromobenzene 20 18.3
Bromochloromethane 20 16.8
Bromodichloromethane 20 16.3
Bromofonn 20 15.8
Brom om ethane 27.8 21.8
2-Butanone (MEK) 20 18.8
n-Butvlbenzene 20 17.9
sec-Butvlbenzene 20 '16.5
tert-Butvlbenzene 20 17.4
Carbon disulfide 20 15.6
Carbon tetrachloride 20 19.2
2-Chloro-l 3-butadiene 20 18.0
Chlorobenzene 20 17.4
Chloroethane 20 17.6
Chlorofonn 20 17.7
1-Chlorohexane 20 17.9
Chloromethane 20 14.9
3-Chloroorooene 20 16.8
2-Chlorotoluene 20 18.0
4-Chlorotoluene 20 17.6
1 2-Dibromo-3-chloronronane 20 13.9
SECTION V -Calibration and QC Infonnation -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
··Flaa·.·
-
·'
Dateffime Analyzed:02/23/2001 08: 12
Units: ug/L
o/oRecoverv .Flaa;~ .. . " "Qc.:1.:11n1ts'.:%Recoveni:·~. ·· .
92
79
68
82
85
91
84
82
79
79
94
89
83
87
78
96
90
87
88
89 80-120
90
75
84
90
88
69
Page 39 of 66
SECTIONV.
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 10778 Instrument Data File: A0222102.D
Instrument ID: MSDA Analyst: BJP
Continued
· Parameter Reference Valu·e Measured Cone
Dibromochloromethane 20 16.1
I 2-Dibromoethane 20 16.9
Dibromomethane 20 17.4
trans-1.4-Dichloro-2-butene 20 16.7
1.4-Dichlorobenzene 20 16.9
1.2-Dichlorobenzene 20 16.8
l 3-Dichlorobenzene 20 17.3
Dichlorodifluoromethane 20 18.8
I 1-Dichloroethane 20 17.9
1.2-Dichloroethane 20 16.2
I 1-Dichloroethene 20 17.1
cis-1 2-Dichloroethene 20 17.2
trans-I 2-Dichloroethene 20 18.3
1.2-Dichlorooronane 20 17.4
1.3-Dichloroorooane 20 16.6
2.2-Dichloroorooane 20 19.8
1 1-Dichloroorooene 20 18.8
cis-1 3-Dichloroorooene 20 17.7
trans-1.3-Dichloroorooene 20 16.9
Ethvl methacrvlate 20 16.9
Ethvlbenzene 20 17.5
Hexachloro-1 3-butadiene 20 13.3
2-Hexanone 20 15.6
Iodomethane 20 17.8
lsooroov !benzene 20 16.8
4-Isooroovltoluene 20 17.6
SECTION V -Calibration and QC Infonnation -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Flaa
~
Dateffime Analyzed:02/23/2001 08:12
Units: ug/L
%Recovel"4 Flaa. QC Llmlts %Recovatv
80
84
87
84
84
84
86
94
89
81
85 80-120
86
92
87 80-120
83
99
94
88
85
84
88 80-120
66
78
89
84
88
Page 40 of 66
- --· - -
---.. -----------
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Cpntinuing Calibration Check
Analysis Batch ID: 10778 Instrument Data File: A0222102.D
Instrument ID: MSDA Analyst: BJP
Continued
Parameter. ., ·-Reference .Value. ·Measured Cone
Methvl methacrvlate 20 16.2
Methvl tert-butvl ether <MTBE) 20 18.l
4-Methvl-2-oentanone <MIBK) 20 16.4
Methvlene chloride 20 }6.9
Naohthalene 20 13.5
Prooanenitrile 100 93.9
n-Pronvlbenzene 20 17.8
Stvrene 20 16.9
1 I L2-Tetrachloroethane 20 16.9
1.1 2.2-Tetrachloroethane 20 15.7
Tetrachloroethene 20 15.9
Tetrahvdrofuran 20 16.8
Toluene 20 17.3
1.2 3-Trichlorobenzene 20 12.6
1.2 4-Trichlorobenzene 20 13.9
1.1 I-Trichloroethane 20 19.3
1 1.2-Trichloroethane 20 16.6
Trichloroethene 20 18.4
Trichlorofluoromethane 20 19.l
1 2 3-Trichloronronane 20 16.3
1 1.2-Trichlorotrifluoroethane 20 21.3
1 2.4-Trimethvlbenzene 20 17.3
1 3.5-Trimethvlbenzene 20 16.9
Vinvl acetate 20 15.8
Vinvl chloride 20 17.8
o-Xvlene/m-Xvlene 40 34.8
SECTION V -Calibrati~n and QC Information -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
.Fiaa
-
Dateffime Analyzed:02/23/2001 08: 12
Unjts: ug/L
%Recoveril Flaa -. QC Limit&'%Recovenl.
81
91
82
84
68
94
89
84
85
79
79
84
87 80-120
63
70
96
83
92
96
81
106
87
85
79
89 80-120
87
Page 41 of 66
- -- - - - -- -----------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Continuing Calibration Check Sample Type:
Analysis Batch ID: 10778 Instrument Data File: A0222119.D
Instrument ID: MSDA Analyst: BJP
·Parameter Reference Value. Measured Coric ·
Acetone 20 22.2
Acetonitrile 100 91.1
Acrolein 100 86.4
Acrv lonitrile 20 19.4
Benzene 20 20.4
Bromobenzene 20 20.7
Bromochloromethane 20 19.9
Bromodichloromethane 20 19.0
Bromoform 20 16.1
Bromomethane 27.8 27.2
2-Butanone <MEK) 20 21.5
n-Butvlbenzene 20 19.6
sec-Butvlbenzene 20 19.4
tert-Butvlbenzene 20 19.4
Carbon disulfide 20 15.8
Carbon tetrachloride 20 21.3
2-Chloro-l 3-butadiene 20 21.6
Chlorobenzene 20 19.5
Chloroethane 20 20.l
Chloroform 20 20.2
1-Chlorohexane 20 20.2
Chloromethane 20 15.8
3-Chlorooronene 20 19.4
2-Chlorotoluene 20 20.7
4-Chlorotoluene 20 20.6
1 2-Dibromo-3-chloronrooane 20 16.l
SECTION V -Calibration and QC Infonnation -03/05/2001 13:42
LIMS Workorder: 80396907.0 I (20I02134] Hamilton Beach-Proctor Silex
STL Austin
Flaa·
~
-
Dateffime Analyzed:02/26/2001 10:46
Units: ug/L
· %Recovehi Flaa'·:--· .. ac. t1m1t5 _%Recov&n1~ .;;
111
91
86
97
102
104
100
95
81
98
108
98
97
97
79
107
108
97
101
101 80-120
101
79
97
103
103
80
Page 43 of 66
SECTIONV
Calibration· and QC Information
Calibration Verification Results
MS-VOA
SW82608
Continuing Calibration Check Sample Type:·
Analysis Batch ID: 10778 Instrument Data File: A0222119.D
Instrument ID: MSDA Analyst: BJP
Continued
Parameter Reference Value Measured Cone
Dibromochloromethane 20 17.4
l .2-Dibromoethane 20 19.3
Dibromomethane 20 20.3
trans-l.4-Dichloro-2-butene 20 19.4
l 4-Dichlorobenzene 20 19.6
1.2-Dichlorobenzene 20 18.7
l.3-Dichlorobenzene 20 19.5
Dichlorodifluoromethane 20 19.0
1.1-Dichloroethane 20 20.9
1.2-Dichloroethane 20 19.3
l. l-Dichloroethene 20 21.0
cis-1 2-Dichloroethene 20 20.5
trans-l .2-Dichloroethene 20 21.4
l 2-Dichloronronane 20 20.l
I 3-Dichlorooronane 20 19.2
2.2-Dichloronrooane 20 22.4
1.1-Dichlorooronene 20 21.3
cis-1.3-Dichloroorooene 20 20.5
trans-1.3-Dichloronronene 20 19.5
Ethvl methacrvlate 20 19.4
Ethvlbenzene 20 19.8
Hexachloro-1.3-butadiene 20 15.0
2-Hexanone 20 18.0
Iodomethane 20 17.4
Isooronv I benzene 20 19.4
4-Isooroov Ito I uene 20 19.7
SECTION V -Calibration and QC lnfonnation -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Flaa
-
Dateffime Analyzed:02/26/200 l l 0:46
Units: ug/L
%Recoverv Flaa QC Limlts.%Recoverv
87
97
102
97
98
94
97
95
105
97
105 80-120
102
107
IOI 80-120
96
112
107
103
97
97
99 80-120
75
90
87
97
99
- -
---------------Page 44 of 66 -- -
-------------------SECTIONV
Calibration and QC Information
Calibration Verification Results
MS-VOA
SW8260B
Sample Type: Continuing Calibration Check
Analysis Batch ID: 10778 Instrument Data File: A0222 l l 9 .D
Instrument ID: MSDA Analyst: BJP
Continued
Parameter · Reference Value Measured Cone
Methvl methacrvlate 20 19.4
Methvl tert-butvl ether (MTBE) 20 21.7
4-Methvl-2-pentanone (MIBK) 20 20.4
Methvlene chloride 20 20.3
Naphthalerie 20 14.8
Pronanenitrile 100 108
n-Proovlbenzene 20 20.5
Stvrene 20 19.4
1, 1, 1 2-Tetrachloroethane 20 19.4
I 1.2 2-Tetrachloroethane 20 18.3
Tetrachloroethene 20 20.8
Tetrahvdrofuran 20 18.8
Toluene 20 19.8
1.2 3-Trichlorobenzene 20 14.5
1,2 4-Trichlorobenzene 20 15.2
1.1.1-Trichloroethane 20 22.2
l, l 2-Trichloroethane 20 19.0
Ttichloroethene 20 21.l
Trichlorofluoromethane 20 21.7
1.2.3-Trichloroorooane 20 18.4
l, 1,2-Trichlorotrifluoroethane 20 24.7
1.2.4-Trimethvlbenzene 20 19.7
1,3,5-Trimethvlbenzene 20 19.9
Vinvl acetate 20 18.4
Vinyl chloride 20 19.3
n-X vlene/m-Xvlene 40 39.1
SECTION V -Calibration and QC Information -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Flaa
-
Dateffime Analyzed:02/26/2001 10:46
Units: ug/L
%Recoverv Flaa QC Limit&<o/ciRecover\r ·.
97
109
102
101
74
108
103
97
97
92
104
94
99 80-120
72
76
111
95
105
108
92
124 .
99
100
92
97 80-120
98
Page 45 of 66
-------------------SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW82608
BFB
Analysis Batch ID: 10778
Instrument ID: MSDA
· Mass/Enerav,
50
75
95
96
173
174
175
176
177
Instrument Data File: A0222102.D
Injection Time: 02/23/2001 08:12
-~~ ~ i/ y. •• Ion Abundance Criteria -· _.
: _. -; · ·: ·) :·Lower Limit Uooer Limit :·· : ·.-:-' -~ · ' ·
15 40
30 60
100 100
5 9
-o 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC Infonnation -03/05/2001 13:42
LIMS Workorder: 80396907.01 (20102134] Hamilton Beach-Proctor Silex
STLAustin
Date Analyzed: 02/23/2001 08:12
Analyst: BJP
~-• •• 1
-.3 Rei•t1~& -Ab~ndimce' -
23.8
40.4
100
6.8
0
64.7
6.6
96.5
6
Page 47 of 66
SECTIONV
Calibration and QC Information
Mass Spectrometer Tune
MS-VOA
SW8260B
BFB
Analysis Batch ID: 10778
Instrument ID: MSDA
Mass/Enernv
50
75
95
96
173
174
175
176
177
Instrument Data File: A0222l 19.D
Injection Time: 02/26/2001 10:46
· Ion Abundance Criteria
. Lower Limit Unner Limit
15 40
30 60
100 100
5 9
0 2
50
5 9
95 101
5 9
SECTION V -Calibration and QC lnfonnation -03/05/200 I 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Date Analyzed: 02/26/2001 10:46
Analyst: BJP
% Relative Abundance
25.4
42.7
100
6.5
0
66.4
7.1
95.7
6.2
Page 48 of 66
-------------------
-------------------SECTIONV··
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Parameter
Acetone
Acetonitrile
Acrolein
Acrvlonitrile
Benzene
Bromobenzene
Bromothloromethane
Bromodichloromethane
Bromofonn
Bromomethane
2-Butanone (MEK)
n-Butvlbenzene
sec-Butvlbenzene
tert-Butvlbenzene
Carbon disulfide
Carbon tetrachloride
2-Chloro-1.3-butadiene
Chlorobenzene
Chloroethane
Chlorofonn
1-Chlorohexane
Chloromethane
3-Chloroorooene
2-Chlorotoluene
4-Chlorotoluene
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
· ·•:cAS,·-.··.
67-64-1
75-05-8
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
126-99-8
108-90-7
75-00-3
67-66-3
544-10-5
74-87-3
107-05-1
95-49-8
106-43-4
1021300
Method Blank
Aaueous
02/23/2001 09:51
02/23/200 I 09:51
MSDA
u!?/L
-·.con·c Flaa:.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.284 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SECTION V -Calibration and QC Information -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
DL ·RC:. .Cone · Flaa · DL ... ·~ .. Rl. ~ · ~ :·.· .cone ··<'=' 1=1aa· ·· oc < : RL
0.438 0.000
6.82 0.000
3.79 0.000
0.446 0.000
0.0641 0.000
0.0998 0.000
0.131 0.000
0.118 0.000
0.170 0.000
0.199 0.000
0.200 0.000 ,.
0.102 6.000 -..
0.105 0.000
0.0911 0.000
0.0684 0.000
0.0652 0.000
0.114 0.000
0.0842 0.000
0.0925 0.000
0.0896 0.000
0.0938 0.000
0.127 0.000
0.0777 0.000
0.178 0.000
0.0974 0.000
Page 49 of 66
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
Parameter CAS
l 2-Dibromo-3-chloroorooane 96-12-8
Dibromochloromethane 124-48-1
I 2-Dibromoethime 106-93-4
Dibromomethane 74-95-3
trans-1.4-Dichloro-2-butene 110-57-6
1.4-Dichlorobenzene 106-46-7
1.2-Dichlorobenzene 95-50-1
1 3-Dichlorobenzene 541-73-1
Dichlorodifluoromethane 75-71-8
1.1-Dichloroethane 75-34-3
1.2-Dichloroethane 107-06-2
1.1-Dichloroethene 75-35-4
cis-1 2-Dichloroethene 156-59-2
trans-I 2-Dichloroethene 156-60-5
1.2-Dichloronropane 78-87-5
1 3-Dichloronrooane 142-28-9
2 2-Dichloroorooane 594-20-7
1.1-Dichloronrooene 563-58-6
cis-1.3-Dichloroorooene 10061-01-5
trans-1 3-Dichloropropene 10061-02-6
Ethvl methacrvlate 97-63-2
Ethvlbenzene 100-41-4
Hexachloro-1 3-butadiene 87-68-3
2-Hexanone 591-78-6
lodomethane 74-88-4
Isooroovlbenzene 98-82-8
4-Isonronvltoluene 99-87-6
Methvl methacrvlate 80-62-6
Methvl tert-butvl ether (MTBE) 1634-04-4
SECTION V -Calibration and QC Infonnation -03/05/2001 13:42
1021300
Cone
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STLAustin
Flaa DL RL Cone· Flaa OL RL Cone Flaa DL ·.· RL
0.548 0.000
0.140 0.000
0.137 0.000
0.148 0.000
0.780 0.000
0.150 0.000
0.0965 0.000
0.0846 0.000
0.237 0.000
0.124 0.000
0.102 0.000
0.122 0.000
0.112 0.000
0.119 0.000
0.0869 0.000
0.135 0:000
0.160 0.000
0.0994 0.000
0.0818 0.000
0.0908 0.000
0.101 0.000
0.136 0.000
0.331 0.000
0.169 0.000
0.109 0.000
0.0931 0.000
0.115 0.000
0.131 0.000
0.116 0.000
Page 50 of 66 - --· - - - - - - - -·-- - - - - - -
-------------------SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Continued
.Parameter CAS ·
4-Methvl-2-oentanone (MIBK) 108-10-1
Methvlene chloride 75-09-2
Naohthalene 91-20-3
Prooanenitrile 107-12-0
n-Proovlbenzene 103-65-1
Stvrene 100-42-5
1 1 1.2-Tetrachloroethane 630-20-6
1 1 2.2-Tetrachloroethane 79-34-5
Tetrachloroethene 127-18-4
Tetrahvdrofuran 109-99-9
Toluene 108-88-3
1.2 3-Trichlorobenzene 87-61-6
1.2 4-Trichlorobenzene 120-82-1
I I.I-Trichloroethane 71-55-6
1.1 2-Trichloroethane 79-00-5
Trichloroethene 79-01-6
Trichlorofluoromethane 75-69-4
1 2.3-Trichloroorooane 96-18-4
1 1 2-Trichlorotrifluoroethane 76-13-1
I 2 4-Trimethvlbenzene 95-63-6
1 3 5-Trimethvlbenzene 108-67-8
Vinvl acetate 108-05-4
Vinvl chloride 75-01-4
n-Xvlene/m-Xvlene 106-42-3
o-Xvlene 95-47-6
·. -'
SECTION V -Calibration and QC Information -03/05/:iOOl 13:42
1021300
Cone
ND
0.153
ND
ND
ND
ND.
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMS Workorder: 80396907.0l [20102134] Hamilton Beach-Proctor Silex
STLAustin
Flaa DL RL Cone.· Flaa .:oL ... RL,,::·.· .; >Cone · . ;.Flaa:,.:_ ~oL;,. · · RL
0.178 0.000
J 0.126 0.000
0.0801 0.000
1.59 0.000
0.140 0.000
0.0977 0.000 .
0.111 0.000 -~.
0.0870 0.000 ~--
0.144 0.000
0.900 0.000 .
0.0637 0.000
0.551 0.000
0.135 0.000
0.169 0.000
0.0821 0.000
0.137 0.000 _...,,o:,
0.106 0.000
0.288 0.000
0.123 0.000
0.124 0.000
0.0905 0.000
0.0948 0.000
0.114 0.000
0.167 0.000
0.0844 0.000
Page 51 of 66
SECTIONV
Calibration and QC Information
Method Blank Results
MS-VOA
SW8260B
Method Blank ID
Sample Type
Matrix
Date/Time Prepared
Date/Time Analyzed
Instrument
Units
Surroaate Comoouild
l-Bromo-4-fluorobenzene
1 2-Dichloroethane-d4
Toluene-d8
SECTION V -Calibration and QC Information -03/05/2001 13:42
1021300.
Method Blank
Aaueous
02/23/200 I 09:51
02/23/2001 09:51
MSDA
U!!/L
% Recoverv
98
98
103
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Limits F % Recoverv Limits .F % Recove..V • · um its F
77-1'17
61-143
87-113
Page 52 of 66 -------------------
-------------------
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
Client Sample ID:
Sample Type:
Prep Batch ID:
Analysis Batch ID:
0201HBWW215
Matrix Spike
10778
10778
Parent Samnle
; ',' ·:20102~3401 , .
' '. , Pil ·a:ac:. "'
,< ' ... :-!;
• ' ~' :.• 1 1,0000 . " ,,
,, ' ~~ .,. •'f' , .. ..
: ;Parame'ter . ; ')"~·,, , ' .·cone: Flci -~ .. "· .·
Acetone ND
Acetonitrile ND
Acrolein ND
Acrv Ion itrile ND
Benzene ND
Bromobenzene ND
Bromochloromethane ND
Bromodichloromethane ND
Bromoform ND
Bromomethane ND
2-Butanone (MEK) ND
n-Butvlbenzene ND
sec-Butvlbenzene ND
tert-Butvlbenzene ND
Carbon disulfide 1.13 B
Carbon tetrachloride ND
2-Chloro-1.3-butadiene ND
Chlorobenzene ND
Chloroethane ND
Chloroform ND
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
Sniked Samnle
J..ab 10:·· · ·102130'1 """'. ¥'\' . ,, .
', " Pilfac_:. :1.0_0QQ.,; .. :__:: ":·.> · .....
-File ID: ... '-~Ad222-~07 .. D,·:,;· .. _.;o;r :·:A -·
. ·sok cone · :conc:-.·,·r~~;:. :·;%Rec'Fla,.,
20 17.2 86
100 75.4 75
100 67.1 67 0
20 15.3 77
20 18.6 93
20 19.4 97
20 17.5 87
20 17.7 89
20 16.3 ~ 82
27.8 24.2 87
20 14.8 74
20 19.3 97
20 18.2 91
20 19.2 96
20 19.6 92
20 20.9 105
20 19.3 97
20 18.9 94
20 20.0 100
20 19.1 96
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Jnfonnation -03/05/200 I 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
% Moisture: NA
BJP Analyst:
Spiked Sample Duplicate
·Cab ID:' .. 1021302 .··~:" . ._, ::,:·: , :~ ·: · : .. ·~ · .. ·;'.w;:;,;~1::<. -..... ·' .. on Fae: .. ·1~ooocr · ~.-... • ' '. <;,.~'I • >, ,: <>
• -_ , ~ • _.,.. t, , r,. • .. "i > .. ,, / } < ~ • "
'Fila ID:· .... A0222:108.0," :;. · ·'.-:·:.,;;r~.;, '-•;1:~·:;.iv. ::: . .,· -. ::»·
·'Snk'C"' ..... ·c·J'" "·)'':·i-''%~:r·-~'f.if:I' '''RRl:t151ii ·'•' . one-, .. one,. : ..... ~,, ac .. :.· .. , •.. ;_.,,
20 18.0 90 4.5
100 78.5 78 3.9
100 68.7 69 0 2.9
20 15.8 79 2.6
20 18.5 93 0
20 19.0 95 2.1
20 17.1 86 1.2
20 17.6 88 1.1
20 16.5 82 0 ·.,;;.-
27.8 23.2 84 --3.5
20 16.4 82 10
20 18.3 92 5.3
20 17.8 89 2.2
20 18.2 91 5.3
20 18.3 86 6.7
20 21.1 106 0.9
20 19.9 100 3
20 18.0 90 4.3
20 19.3 96 4.1
20 18.3 91 5.3
Pf>• . r ~ ,
:·:~Qq '.'-hnits
" ,:; i·~~; .~. '. ··~:.· ,· ' .. .'·,
'-%Rec ' " RPt»
0.1-240 71
70-130 25
70-130 25
70-130 25
71-133 17
67-127 12
61-145 21
57-135 19
23-151 17
34-128 25
0.1-214 39
28-184 30
45-160 31
65-148 27
29-223 23
46-150 23
70-130 25
77-129 14
39-133 27
64-146 16
Page 53 of 66
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
'.'·'
·parameter
1-Chlorohexane
Chloromethane
3-Chloronronene
2-Chlorotoluene
4-Chlorotoluene
l.2-Dibromo-3-chloronrooane
Dibromochloromethane
l 2-Dibromoethane
Dibromomethane
trans-l .4-Dichloro-2-butene
1.4-Dichlorobenzene
1.2-Dichlorobenzene
1.3-Dichlorobenzene
Dichlorodifluoromethane
l 1-Dichloroethane
1.2-Dichloroethane
1 1-Dichloroethene
cis-1 2-Dichloroethene
trans-I 2-Dichloroethene
1 2-Dichloronronane
1 3-Dichloronrooane
2 2-Dichloronronane
1.1-Dichloronronene
cis-1 3-Dichloronrooene
trans-I 3-Dichloronrooene
"
Parent continue d
201'0213401
on Fae:
1.0000
Cone Fla
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.55
ND
2.38
ND
ND
ND
ND
ND
ND
ND
ND
Soiked Samole contmued
Lab ID: 1021'301
Oil Fae: 1.0000
File ID: A0222107.D
Sok Cone Cone %Rec Fla
20 20.0 IOO
20 16.5 82
20 19.4 97
20 19.9 99
20 19.3 96
20 11.9 60
20 16.7 83
20 16.7 84
20 17.3 86
20 17.5 87
20 17.7 89
20 16.8 84
20 18.3 91
20 20.8 ~ l04
20 23.2 98
20 16.4 82
20 21.0 93
20 19.3 96
20 20.3 101
20 18.0 90
20 16.5 83
20 19.4 97
20 20.8 l04
20 18.3 92
20 18.0 90
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
Spiked Samnle Dunlicate continued
'La~. ID: . 1021302 , '.'. , ,~ .. ; . ,, ~.;$'~'!• ... , . ' , , ·" , , •,
DH Fae: ~.9000 ',
.QC Limits ,, ,
File ID: . · A0222108.D · ·:.~ , " . ; •• ;i_.
•' •• '\'<
Sok Cone~. .Cone. '%RecFia · RPD'Fla · %·Rec: RPO
20 19.1 95 5.1 70-130 25
20 16.2 81 1.2 18-140 26
20 18.9 95 2.1 70-130 25
20 19.2 96 3.1 70-136 24
20 18.9 94 2.1 74-132 23
20 12.5 62 3.3 39-171 25
20 16.5 82 1.2 45-137 15
20 16.6 83 1.2 19-187 19
20 17.7 88 2.3 52-138 21
20 18.2 91 4.5 70-130 25
20 17.6 88 l.l 70-132 13
20 16.7 84 0 67-135 14
20 18.0 90 l.l 68-134 14
20 19.6 98 5.9 O.l-166 26
20 22.8 96 2.1 66-138 19
20 16.8 84 2.4 48-152 23
20 20.3 90 3.3 47-175 25
20 18.8 94 2.1 66-144 18
20 19.8 99 2 62-146 22
20 18.5 93 3.3 61-133 17
20 16.6 83 0 70-128 16
20 21.0 l05 7.9 40-168 30
20 20.4 102 1.9 71-155 31
20 18.8 94 2.2 36-142 16
20 17. l 85 5.7 34-138 21
Page 54 of 66
-------------------
-------------------
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
Parent continued
.. 201021$401 '
. bil Fae:.· f" . 1.0000 .
Sniked Samo e contmued Soiked Samole Duolicate continued
Lab ID:
Oil Fae:
File ID:
1021301' .,. ·.··. ·_ ., Lal?.1.D: : . .10~1:~0~:::· .... ,. )_ >-; .·:-::. '.:·:/~:· , .. <.~~::.-:~~::
··1.0000 <. • '' Dil'Fa<;:.'.:topo.o";,, .·.'.':::, ,, , ·:::-.: '., "" ' ;~'GCLiinits
Ao222107:0:· ,_ " File ID:'.-,. A0222t08.Q;'_ ', . :;· . . ,'" '• '.(' '.:"
Parameter . Cone Fla Sok Coric Coric >. · --· %Rec.Fla Snk·conc ·· ccin'c· : < "<%Rec:Ela . ..RPD'.·Fla " -~R~~ RPO
Ethvl methacrvlate ND 20 15.8 79 20 16.5 82 3.7 70-130 25
Ethvlbenzene ND 20 19.4 97 20 18.4 92 5.3 75-131 14
Hexachloro-1 .3-butadiene ND 20 14.1 71 20 13.5 67 5.8 46-150 34
2-Hexanone ND 20 14.3 72 20 14.6 73 1.4 22-164 34
lodomethane ND 20 20.3 101 20 20.0 100 1 70-130 25
Isooroovlbenzene ND 20 18.7 93 20 17.6 88 5.5 ~·-54-152 26
4-Isoproovltoluene ND 20 19.3 96 20 18.6 93 3.2 41-165 28
Methvl methacrvlate ND 20 15.3 76 20 15.9 79 3.9 70-130 25
Methvl tert-butvl ether (MTBE) 0.427 J 20 15.6 76 20 17.6 86 12 70-130 25
4-Methvl-2-oentanone (MIBK) ND 20 15.2 76 20 16.1 80 5.1 27-149 36
Methvlene chloride ND B 20 18.4 92 20 17.9 90 2.2 36-166 23
Naphthalene ND 20 11.8 59 20 12.1 60 1.7 32-172 22
Prooanenitrile ND 100 110 110 100 105 105 4.7 70-130 25
n-Proovlbenzene ND 20 19.8 -99 20 18.9 95 4.1 -· . 61-143 28
Stvrene ND 20 17.9 90 20 17.3 86 4.5 -68-136 14
1 I. 1.2-Tetrachloroethane ND 20 18.2 91 20 17.4 87 4.5 63-141 20
I, I 2 2-Tetrachloroethane ND 20 14.7 74 20 15.3 76 2.7 47-143 20
Tetrachloroethene ND 20 16.5 82 20 15.5 78 5 69-137 16
Tetrahvdrofuran 6.41 20 23.2 84 20 25.0 93 10
Toluene ND 20 19.1 95 20 18.3 91 4.3 70-132 17
1.2 3-Trichlorobenzene ND 20 11.5 58 0 20 12.4 62 0 6.7 66-140 20
1.2.4-Trichlorobenzene ND 20 13.4 67 20 13.6 68 1.5 66-144 22
l, l, I-Trichloroethane ND 20 20.2 101 20 20.7 104 2.9 49-155 24
1.1.2-Trichloroethane ND 20 16.3 82 20 16.7 83 1.2 67-135 17
Trichloroethene ND 20 19.8 99 20 19.2 96 3.1 71-129 17
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -03/05/2001 13:42
LIMS Workorder: 80396907 .0 I (20 I 02134) Hamilton Beach-Proctor Silex
STLAustin Page 55 of 66
SECTIONV
Calibration and QC Information
Spiked Sample Results
MS-VOA
SW8260B
p t f d aren con mue
201Q213401
Oil Fae:· ·
S 'k dS iPI e amp e contmued
Lab ID: 1021391 -'•
Oil Fae: 1.QOOO: ·
1.0000 File ID: A0222107.D
" Parameter Cone Fla Sok Cone· .cone
Trichlorofluoromethane ND 20 21.8
1.2 3-Trichloronronane ND 20 15.5
1.1 2-Trichlorotrifluoroethane ND 20 22.9
1.2 4-Trimethvlbenzene ND 20 19.0
I 3.5-Trimethvlbenzene ND 20 18.9
Vinvl acetate ND 20 16.0
Vinvl chloride ND 20 20.1
o-Xvlene/m-Xvlene ND 40 37.8
o-Xvlene ND 20 18.9
Note: Spike Concentration for solid matrices not adjusted for percent moisture.
SECTION V -Calibration and QC Information -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134) Hamilton Beach-Proctor Silex
STLAustin
%Rec Fla
109
78
115
95
95
80
100
95
95
Lab ID: ·on Fae:.·
File ID:
Sok Coric_
20
20
20
20
20
20
20
40
20
Spiked Sample Duolicate continued
1021~02 " >
'• " -{. ,:,,,. .. , -: , :~! , " ,_ ' 1 '. 1.0000, " >
.-, ' ,. "', ~ , ', •' 'J~CL.lmit$ , .
: A0222108.o ', :: . ~ , •' ', > ,, ., , .. ,,
> > • cone;· '%RecFla· RPD·Fla _·. ·%Rec· . RPO
20.8 104 4.7 39-147 29
15.6 78 0 64-140 18
23.3 116 0.9
18.3 92 3.2 54-156 25
18.5 92 3.2 62-144 25
16.0 80 0 0.1-164 31
19.5 98 2 24-138 27
36.5 91 4.3 76-134 15
18.0 90 5.4 77-131 15
Page 56 of 66
-------------------
SECTIONV
Calibration and QC Information
Control Sample Results
MS-VOA
SW8260B
Client Sample ID:
Prep Batch ID:
Analysis Batch ID:
LCS for HBN 10778 [MSV/1473]
10778
10778
.,
Instrument ID: MSDA
Units: ug/L
Matrix: Aqueous
Control s amnle
.Lab ID: 1021298
File ID: . A0222103.D
Parameter
'. Sok Amt'
Acetone 20
Benzene 20
Bromobenzene 20
Bromochloromethane 20
Bromodichloromethane 20
Bromoform 20
Brom om ethane 20
2-Butanone (MEK) 20
n-Butvlbenzene 20
sec-Butvlbenzene 20
tert-Butvlbenzene 20
Carbon disulfide 20
Carbon tetrachloride 20
Chlorobenzene 20
Chloroethane 20
Chloroform 20
Chloromethane 20
2-Chlorotoluene 20
4-Chlorotoluene 20
1 2-Dibromo-3-chloroorooane 20
Dibromochloromethane 20
I 2-Dibromoethane 20.
Dibromomethane 20
1 4-Dichlorobenzene 20
SECTION V -Calibration and QC Information -03/05/200 I 13 :42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
cone %Rec Flo
20.9 104
18.5 93
20.9 105
19.5 97
18.9 94
18.9 94
22.8 114
20.2 101
19.8 99
19.0 95
19.3 ~ 97
16.4 82
20.4 102
19.4 97
19.9 100
20.0 100
17.8 89
20.2 101
19.9 100
13.8 69
19.5 97
19.2 96
19.4 97
19.1 96
Lab tD:
File ID:
Sok.Amt
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
% Moisture: NA
BJP Analyst:
Control Samnle Dunlicate
'·10212.99:., '• -..
A0222104.D .,.
Cone -.%Rec Fla"
22.l llO
19.7 99
21.5 107
20.0 100
19.7 99
19.7 98
23.3 117
19.7 99
20.4 102
19.9 99
20.0 100
17.6 88
22.2 111
20.l 101
20.9 105
20.3 102
19.0 95
21.l 106
20.5 102
15.2 76
20.0 100
19.9 100
20.4 102
19.7 99
> -~'' , .. · , .. !; :
: .. ;·QC Limits -..,· ,, . --'',,
. RPO:Ffa: ·. '%Ree· RPO
5.6 0.1-240 71
6.3 71-133 17
l.9 67-127 12
3 61-145 21
5.2 57-135 19
4.2 23-151 17
2.6 34-128 25
2 0.1-214 39
3 28-184 30
4.1 45-160 31
3 65-148 27
7.1 29-223 23
8.5 46-150 23
4 77-129 14
4.9 39-133 27
2 64-146 16
6.5 18-140 26
4.8 70-136 24
2 74-132 23
9.7 39-171 25
3· 45-137 15
4.1 19-187 19
5 52-138 21
3.1 70-132 13
Page 58 of 66
~------------------
SECTION VI
Batch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 10778
-
Client Samole ID
INSTRUMENT OC
INSTRUMENT OC
LCS for HBN 10778 fMSV/14731
LCSD for HBN 10778 fMSV/14731
MB for HBN 10778 fMSV/14731
0201HBWW215
0201HBWW215
020IHBWW215
TRIP BLANK
TRIP BLANK
0201HBWW230
0201HBWW222
0201HBWW226
0201 HBWW234
0201HBWW224
0201 HBWW225
020lHBWW220
INSTRUMENT OC
INSTRUMENT OC
0201HBWW216
0201HBWD998
0201HBWW214
0201HBWW213
0201HBWD999
020lHBWW227
0201HBWW228
0201HBWW228
020 l HBWD999
SECTION VI -Batch Summaries -03/05/2001 13:42
Lab Samole ID
1000
1406
1021298
1021299
1021300
2010213401
1021301
1021302
2010213407
2010213417
2010213408
2010213409
2010213410
2010213411
2010213412
2010213413
2010213414
1000
1406
2010213415
2010213416
2010213402
2010213404
2010213403
2010213405
2010213406
2010213406
2010213403
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STL Austin
Start Dateffime: 02/23/2001 08: 12
Stop Dateffime: 02/26/2001 18:37
SamoleTvoe Matrix
GC/MS Tune Aaueous
Continuing Calibration Check Aaueous
Lab Control Samnle Aaueous
Lab Control Samnle Dunlicate Aaueous
Method Blank Aaueous
Field Samnle Aaueous
Matrix Snike Aaueous
Matrix Snike Dunlicate Aaueous
Field Samole Aaueous
Field Sample Aaueous
Field Samole Aaueous
Field Samnle Aaueous
Field Samole Aaueous
Field Samole Aaueous
Field Samnle ~ Aaueous
Field Samnle Aaueous
Field Sample Aaueous
GC/MS Tune Aaueous
Continuing Calibration Check Aaueous
Field Samnle Aaueous
Field Sample Aaueous
Field Samnle Aaueous
Field Sample Aaueous
Field Samole Aaueous
Field Samnle Aaueous
Field Sample Aaueous
Field Samole Aaueous
Field Samole Aaueous
Analyst: BJP
samole 'Slztt' · , .-,,', '·, 'J,-' <" '.-· Initial ·Final Preo~ratlon: Method
15mL 15mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15mL 15mL SW8260B
15mL 15 mL SW8260B
15 mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15 mL 15mL SW8260B
15mL 15mL SW8260B
l5mL l5mL SW8260B
15 mL 15 mL SW8260B
15mL 15 mL SW8260B
15 mL 15mL SW8260B
15 mL 15mL SW8260B
15 mL 15 mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15 mL 15 mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15mL 15mL SW8260B
15 lnL 15mL SW8260B
15mL 15mL SW8260B
15 mL 15mL SW8260B
15 mL 15mL SW8260B
15 mL 15mL SW8260B
l5mL 15 mL SW8260B
Page 62 of 66
-------------------
-------------------SECTION VI
6atch Summaries
Extraction/Digestion Batch Summary
MS-VOA
SW8260B
Extraction Batch ID: 10778 continued
..
Client Sample ID Lab Samele ID .
020 I HBWW227 2010213405
0201HBWW228 2010213406
SECTION VI -Batch Summaries -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin.
.. '·. '
SamoleTvoe ,.Matrix:.
Field Samole Aaueous
Field Sample Aqueous
: ·:_·0.: Sams:>1e:sb~a:.::;-_·: , '. :.-. --~~~~}~~?/~---~ ~u:~:?:~:-l>" ~ -:
' " ,,,, -:·1n1t1a.r . : --: Flnar::· _.:, · .Preoaratlon.Method ..
15 mL 15mL SW8260B
l5mL 15mL SW8260B
Page 63 of 66
SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW82608
Analysis Batch ID: 10778 Instrument ID: MSDA
..
Seauence Client Samele ID Lab Samele ID .
1 INSTRUMENT OC 1000
2 INSTRUMENT OC 1406
3 LCS for HBN 10778 fMSV/14731 1021298
4 LCSD for HBN 10778 IMSV/14731 1021299
5 MB for HBN 10778 fMSV/14731 1021300
6 0201HBWW215 2010213401
7 0201HBWW215 1021301
8 0201HBWW2 l 5 1021302
9 TRIP BLANK 2010213407
IO TRIP BLANK 2010213417
11 0201HBWW230 2010213408
12 0201HBWW222 2010213409
13 0201HBWW226 2010213410
14 0201HBWW234 201021341 l
15 0201HBWW224 2010213412
16 0201HBWW225 2010213413
17 0201HBWW220 2010213414
18 INSTRUMENT OC 1000
19 INSTRUMENT OC 1406
20 0201HBWW216 2010213415
21 020 lHBWD998 2010213416
22 0201HBWW214 2010213402
23 0201HBWW213 2010213404
24 0201HBWD999 2010213403
25 0201HBWW227 2010213405
26 0201HBWW228 2010213406
27 0201HBWW228 2010213406
28 0201HBWD999 2010213403
29 0201HBWW227 2010213405
SECTION VI -Batch Summaries -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STLAustin
,' Analvsis
Date Time·
02/23/2001 08:12:00
02/23/2001 08:12:00
02/23/2001 08:55:00
02/23/2001 09:23:00
02/23/2001 09:51:00
02/23/2001 10:20:00
02/23/2001 11:02:00
02/23/2001 11:30:00
02/23/2001 11:58:00
02/23/2001 12:27:00
02/23/2001 12:55:00
02/23/2001 13:23:00
02/23/2001 13:51:00
02/23/2001 14:19:00
02/23/2001 14:47:00
02/23/2001 15:15:00
02/23/2001 15:45:00
02/26/2001 10:46:00
02/26/2001 10:46:00
02/26/2001 11:44:00
02/26/2001 12:12:00
02/26/2001 12:41:00
02/26/2001 13:09:00
02/26/2001 13:39:00
02/26/2001 14:09:00
02/26/2001 14:37:00
02/26/2001 16:43:00
02/26/2001 17:34:00
02/26/2001 18:07:00
Analyst: BJP
., . . ' _,., ,,,.,. ... . ·' ,•,, .. ,, •, ' !'>
samoleTvoe 'Analvsls :F·lla 11>· · Sub .. Batch ID
GC/MS Tune A0222102.D 0
Continuing Calibration Check A0222102.D 0
Lab Control Samnle A0222103.D 0
Lab Control Samole Dunlicate A0222104.D 0
Method Blank A0222105.D 0
Field Sample A0222106.D 0
Matrix Soike A0222107.D 0
Matrix Spike Duplicate A0222108.D 0
Field Samnle A0222109.D 0
Field Sample A0222110.D 0
Field Sample A0222111.D 0
Field Sample A0222112.D 0
Field Sample A0222113.D 0
Field Samnle A0222114.D 0
Field Sample A0222115.D 0
Field Sample A0222116.D 0
Field Samnle A0222117.D 0
GC/MSTune A0222119.D 0
Continuing Calibration Check A0222119.D 0
Field Samnle A0222120.D 0
Field Sample A0222121.D 0
Field Samnle A0222122.D 0
Field Sample A0222123.D 0
Field Samnle A0222124.D 0
Field Sample A0222125.D 0
Field Sample A0222126.D 0
Field Sample A0222128.D 0
Field Sample A0222129.D 0
Field Samnle A0222130.D 0
Page 64 of 66
-------------------
-------------------SECTION VI
Batch Summaries
Analysis Batch Summary
MS-VOA
SW8260B
Analysis Batch ID: 10778 continued
Seauence Client Sam Die ID,
30 0201 HBWW228
SECTION VI -Batch Summaries -03/05/2001 13:42
Analvsis
Lab Samole ID , Date I Time
2010213406 02/26/2001 18:37:00
LIMS Workorder: 80396907,01 [20102134] Hamilton Beach-Proctor Silex
STLAuslin
• ~' :::'; , ''; ! ~ .. : k ,_: O' ', ~ <. ~ ,_ , <A : ~ ~: "_'./;r:,:-.. 'if ':, ~ ; F:> ,
SamDleTvDe :,, ,,_, -.L ,,,·'·· , :Analvsls Flle]D::: ; Sub~Batch·ID
Field Samnle A0222 l 3 l .D 0
Page 65 of 66
SECTION VII
Certifications
·state/Aaencv
Arkansas Denartment of Pollution Control and Ecolo!!v
California Environmental Laboratorv Accreditation Proe.ram I Waste Water/Hazardous Waste
Kansas Department of Health and Environment I Solid and Hazardous Waste/Drinkin!! Water
Louisiana Deoartment of Environmental Oualitv. ELAP I Waste Water/Hazardous Waste/Air/Emissions
New Jersey Deoartment of Environmental Protection
New York State Denartment of Health I Waste Water/Hazardous Waste
North Carolina Dent. of Natural Resources & Communitv Develonment I Waste Water
Oklahoma Water Resources Board I Waste Water
South Carolina Dent. of Health & Environmental Control
Utah Deoartment of Health I Solid and Hazardous Waste
Wisconsin Denartment of Natural Resources
US Air Force/AFCEE
US Army Corns ofEne.ineers (ACE)
US Deoartment of Ae.riculture I Restricted Soils Permit
SECTION VII -Certifications -03/05/2001 13:42
LIMS Workorder: 80396907.01 [20102134] Hamilton Beach-Proctor Silex
STL Austin
-- - - ---- -- -
'' ID#' ,. " ' "'
' -" ''
2257
E-10165
82005
10915
302
8720
82003002
RADC-
999885260
Particioatini:!: Laboratorv
S-42350
Page 66 of 66 ----- - --
Page 2 of 2
.i.o CONDITION OF BOTTLES/CONTAINE~ ~~ERIFIED BY . .c:.;~ __ s.__._1_..,,. ______ --r-----
Samples received match' COC· ~,~e; g::o ;ottles received intact: d YES 0jNO
Sec additional discrepanci~'lomments section: Gf YES 'tt,_O Samples received from USDA restricted area: 0 YES QNO
VOA trip blanks included: rsiJ YES D NO Q N/ A
5.0 ADDITIONAL DISCREPANCIES
Appears on COC . Appears on Label
Sample ID Dateffime Sample ID Date!fime Comments
5.0 SHIPPING DOCUMENTATION J YES 0 NO Air bill#:--'-'---------------<\ir/freight bill is available and attached to COC:
Hand-delivered Carrier:. _________________ _ Date: _______ Time:------
7.0 OTHER COMMENTS:
v\.\\%)~~ CQC ffOM I epD/~ ~ 6ZS=t:·?-'57o·!J5t/i)
Client COC is signed. dated with time of receipt, and addendum number"is noted in the comments section. DYES
CORRECTIVE ACTION:
Client's Name: ----------Informed verbally on: -------By: ----------
Client's Name: ----------Informed verbally on: -------By: ---------
Sample(s) processed "as is" comments: -------------------------------
Samples(s) on hold until: --------------If released. notify: ------------
REVIEW:
Project Management: ------------------------Date: ----------
SIGNED ORIGINAL MUST BE RETAINED IN THE PROJECT FILE
:vised 12/8//2000
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APPENDIXB
CONTAMINANT CONCENTRATIONS VERSUS TIME
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