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HomeMy WebLinkAboutCenco_Honbarrier Annual Sampling 2008December 19, 2008 LIMS USE: FR - JOHN REUSCHER LIMS OBJECT ID: 9233761 9233761 Project: Pace Project No.: RE: John Reuscher Delta Environmental Consultant 8008 Corp. Center Drive Suite 100 Charlotte, NC 28226 HONBARRIER ANNUAL SAMPLING Dear John Reuscher: Enclosed are the analytical results for sample(s) received by the laboratory on December 08, 2008. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Charlotte Certification IDsConnecticut Certification Number: PH-0104Pennsylvania Certification Number: 68-00784 West Virginia Certification Number: 357Virginia Certification Number: 00213Tennessee Certification Number: 04010South Carolina Drinking Water Cert. Number: 990060003South Carolina Certification Number: 990060001 North Carolina Field Services Certification Number: 5342North Carolina Wastewater Certification Number: 12 North Carolina Drinking Water Certification Number: 37706Louisiana/LELAP Certification Number: 04034Kentucky UST Certification Number: 84New Jersey Certification Number: NC012Florida/NELAP Certification Number: E87627 Asheville Certification IDs Connecticut Certification Number: PH-0106 Massachusetts Certification Number: M-NC030West Virginia Certification Number: 356Virginia Certification Number: 00072 Tennessee Certification Number: 2980South Carolina Bioassay Certification Number: 99030002 South Carolina Certification Number: 99030001 Pennsylvania Certification Number: 68-03578 North Carolina Bioassay Certification Number: 9North Carolina Wastewater Certification Number: 40North Carolina Drinking Water Certification Number: 37712 New Jersey Certification Number: NC011Louisiana/LELAP Certification Number: 03095 Florida/NELAP Certification Number: E87648 Eden Certification IDs Virginia Drinking Water Certification Number: 00424 North Carolina Wastewater Certification Number: 633 North Carolina Drinking Water Certification Number: 37738 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Lab ID Sample ID Matrix Date Collected Date Received 9233761001 MW-2 Water 12/06/08 12:15 12/08/08 14:30 9233761002 MW-13 Water 12/06/08 13:25 12/08/08 14:30 9233761003 MW-19 Water 12/06/08 14:30 12/08/08 14:30 9233761004 MW-7 Water 12/06/08 12:45 12/08/08 14:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Lab ID Sample ID Method Analytes ReportedAnalysts 9233761001 MW-2 EPA 601 31PPM 9233761002 MW-13 EPA 601 31PPM 9233761003 MW-19 EPA 601 31PPM 9233761004 MW-7 EPA 601/602 40PPM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Sample:MW-2 Lab ID:9233761001 Collected:12/06/08 12:15 Received:12/08/08 14:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 601 Volatiles Analytical Method: EPA 601 Bromodichloromethane ND ug/L 1.0 1 12/10/08 18:34 75-27-4 Bromoform ND ug/L 1.0 1 12/10/08 18:34 75-25-2 Bromomethane ND ug/L 1.0 1 12/10/08 18:34 74-83-9 Carbon tetrachloride ND ug/L 1.0 1 12/10/08 18:34 56-23-5 Chlorobenzene ND ug/L 1.0 1 12/10/08 18:34 108-90-7 Chloroethane ND ug/L 1.0 1 12/10/08 18:34 75-00-3 Chloroform ND ug/L 1.0 1 12/10/08 18:34 67-66-3 Chloromethane ND ug/L 2.0 1 12/10/08 18:34 74-87-3 Dibromochloromethane ND ug/L 1.0 1 12/10/08 18:34 124-48-1 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 12/10/08 18:34 106-93-4 1,2-Dichlorobenzene ND ug/L 1.0 1 12/10/08 18:34 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 12/10/08 18:34 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 12/10/08 18:34 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 12/10/08 18:34 75-71-8 1,1-Dichloroethane 6.6 ug/L 1.0 1 12/10/08 18:34 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 12/10/08 18:34 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 12/10/08 18:34 75-35-4 cis-1,2-Dichloroethene 33.5 ug/L 1.0 1 12/10/08 18:34 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 12/10/08 18:34 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 12/10/08 18:34 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 12/10/08 18:34 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 12/10/08 18:34 10061-02-6 Methylene Chloride ND ug/L 2.0 1 12/10/08 18:34 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 12/10/08 18:34 79-34-5 Tetrachloroethene ND ug/L 1.0 1 12/10/08 18:34 127-18-4 1,1,1-Trichloroethane ND ug/L 1.0 1 12/10/08 18:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 12/10/08 18:34 79-00-5 Trichloroethene ND ug/L 1.0 1 12/10/08 18:34 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 12/10/08 18:34 75-69-4 Vinyl chloride 1.7 ug/L 1.0 1 12/10/08 18:34 75-01-4 1-Chloro-3-fluorobenzene (S)94 %65-137 1 12/10/08 18:34 625-98-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 5 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Sample:MW-13 Lab ID:9233761002 Collected:12/06/08 13:25 Received:12/08/08 14:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 601 Volatiles Analytical Method: EPA 601 Bromodichloromethane ND ug/L 5.0 5 12/10/08 19:16 75-27-4 Bromoform ND ug/L 5.0 5 12/10/08 19:16 75-25-2 Bromomethane ND ug/L 5.0 5 12/10/08 19:16 74-83-9 Carbon tetrachloride ND ug/L 5.0 5 12/10/08 19:16 56-23-5 Chlorobenzene 10 ug/L 5.0 5 12/10/08 19:16 108-90-7 Chloroethane ND ug/L 5.0 5 12/10/08 19:16 75-00-3 Chloroform ND ug/L 5.0 5 12/10/08 19:16 67-66-3 Chloromethane ND ug/L 10.0 5 12/10/08 19:16 74-87-3 Dibromochloromethane ND ug/L 5.0 5 12/10/08 19:16 124-48-1 1,2-Dibromoethane (EDB)ND ug/L 5.0 5 12/10/08 19:16 106-93-4 1,2-Dichlorobenzene ND ug/L 5.0 5 12/10/08 19:16 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 5 12/10/08 19:16 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 5 12/10/08 19:16 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 5 12/10/08 19:16 75-71-8 1,1-Dichloroethane ND ug/L 5.0 5 12/10/08 19:16 75-34-3 1,2-Dichloroethane ND ug/L 5.0 5 12/10/08 19:16 107-06-2 1,1-Dichloroethene ND ug/L 5.0 5 12/10/08 19:16 75-35-4 cis-1,2-Dichloroethene 249 ug/L 5.0 5 12/10/08 19:16 156-59-2 trans-1,2-Dichloroethene 12.2 ug/L 5.0 5 12/10/08 19:16 156-60-5 1,2-Dichloropropane ND ug/L 5.0 5 12/10/08 19:16 78-87-5 cis-1,3-Dichloropropene ND ug/L 5.0 5 12/10/08 19:16 10061-01-5 trans-1,3-Dichloropropene ND ug/L 5.0 5 12/10/08 19:16 10061-02-6 Methylene Chloride ND ug/L 10.0 5 12/10/08 19:16 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 5.0 5 12/10/08 19:16 79-34-5 Tetrachloroethene ND ug/L 5.0 5 12/10/08 19:16 127-18-4 1,1,1-Trichloroethane ND ug/L 5.0 5 12/10/08 19:16 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 5 12/10/08 19:16 79-00-5 Trichloroethene ND ug/L 5.0 5 12/10/08 19:16 79-01-6 Trichlorofluoromethane ND ug/L 5.0 5 12/10/08 19:16 75-69-4 Vinyl chloride 27.8 ug/L 5.0 5 12/10/08 19:16 75-01-4 1-Chloro-3-fluorobenzene (S)96 %65-137 5 12/10/08 19:16 625-98-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 6 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Sample:MW-19 Lab ID:9233761003 Collected:12/06/08 14:30 Received:12/08/08 14:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 601 Volatiles Analytical Method: EPA 601 Bromodichloromethane ND ug/L 1.0 1 12/10/08 19:58 75-27-4 Bromoform ND ug/L 1.0 1 12/10/08 19:58 75-25-2 Bromomethane ND ug/L 1.0 1 12/10/08 19:58 74-83-9 Carbon tetrachloride ND ug/L 1.0 1 12/10/08 19:58 56-23-5 Chlorobenzene ND ug/L 1.0 1 12/10/08 19:58 108-90-7 Chloroethane ND ug/L 1.0 1 12/10/08 19:58 75-00-3 Chloroform ND ug/L 1.0 1 12/10/08 19:58 67-66-3 Chloromethane ND ug/L 2.0 1 12/10/08 19:58 74-87-3 Dibromochloromethane ND ug/L 1.0 1 12/10/08 19:58 124-48-1 1,2-Dibromoethane (EDB)ND ug/L 1.0 1 12/10/08 19:58 106-93-4 1,2-Dichlorobenzene ND ug/L 1.0 1 12/10/08 19:58 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 12/10/08 19:58 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 12/10/08 19:58 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 12/10/08 19:58 75-71-8 1,1-Dichloroethane 3.5 ug/L 1.0 1 12/10/08 19:58 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 12/10/08 19:58 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 12/10/08 19:58 75-35-4 cis-1,2-Dichloroethene 15.3 ug/L 1.0 1 12/10/08 19:58 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 12/10/08 19:58 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 12/10/08 19:58 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 12/10/08 19:58 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 12/10/08 19:58 10061-02-6 Methylene Chloride ND ug/L 2.0 1 12/10/08 19:58 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 12/10/08 19:58 79-34-5 Tetrachloroethene ND ug/L 1.0 1 12/10/08 19:58 127-18-4 1,1,1-Trichloroethane ND ug/L 1.0 1 12/10/08 19:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 12/10/08 19:58 79-00-5 Trichloroethene ND ug/L 1.0 1 12/10/08 19:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 12/10/08 19:58 75-69-4 Vinyl chloride 1.9 ug/L 1.0 1 12/10/08 19:58 75-01-4 1-Chloro-3-fluorobenzene (S)98 %65-137 1 12/10/08 19:58 625-98-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 7 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Sample:MW-7 Lab ID:9233761004 Collected:12/06/08 12:45 Received:12/08/08 14:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 601/602 Volatiles Analytical Method: EPA 601/602 Benzene 96.4 ug/L 5.0 5 12/10/08 12:36 71-43-2 Bromodichloromethane ND ug/L 5.0 5 12/10/08 12:36 75-27-4 Bromoform ND ug/L 5.0 5 12/10/08 12:36 75-25-2 Bromomethane ND ug/L 5.0 5 12/10/08 12:36 74-83-9 Carbon tetrachloride ND ug/L 5.0 5 12/10/08 12:36 56-23-5 Chlorobenzene 214 ug/L 5.0 5 12/10/08 12:36 108-90-7 Chloroethane ND ug/L 5.0 5 12/10/08 12:36 75-00-3 Chloroform ND ug/L 5.0 5 12/10/08 12:36 67-66-3 Chloromethane ND ug/L 10.0 5 12/10/08 12:36 74-87-3 Dibromochloromethane ND ug/L 5.0 5 12/10/08 12:36 124-48-1 1,2-Dibromoethane (EDB)ND ug/L 5.0 5 12/10/08 12:36 106-93-4 1,2-Dichlorobenzene ND ug/L 5.0 5 12/10/08 12:36 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 5 12/10/08 12:36 541-73-1 1,4-Dichlorobenzene 10.4 ug/L 5.0 5 12/10/08 12:36 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 5 12/10/08 12:36 75-71-8 1,1-Dichloroethane ND ug/L 5.0 5 12/10/08 12:36 75-34-3 1,2-Dichloroethane ND ug/L 5.0 5 12/10/08 12:36 107-06-2 1,1-Dichloroethene ND ug/L 5.0 5 12/10/08 12:36 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 5 12/10/08 12:36 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 5 12/10/08 12:36 156-60-5 1,2-Dichloropropane ND ug/L 5.0 5 12/10/08 12:36 78-87-5 cis-1,3-Dichloropropene ND ug/L 5.0 5 12/10/08 12:36 10061-01-5 trans-1,3-Dichloropropene ND ug/L 5.0 5 12/10/08 12:36 10061-02-6 Diisopropyl ether ND ug/L 5.0 5 12/10/08 12:36 108-20-3 Ethylbenzene 53.8 ug/L 5.0 5 12/10/08 12:36 100-41-4 Methylene Chloride ND ug/L 10.0 5 12/10/08 12:36 75-09-2 Methyl-tert-butyl ether ND ug/L 5.0 5 12/10/08 12:36 1634-04-4 Naphthalene ND ug/L 10.0 5 12/10/08 12:36 91-20-3 1,1,2,2-Tetrachloroethane ND ug/L 5.0 5 12/10/08 12:36 79-34-5 Tetrachloroethene ND ug/L 5.0 5 12/10/08 12:36 127-18-4 Toluene 10.1 ug/L 5.0 5 12/10/08 12:36 108-88-3 1,1,1-Trichloroethane ND ug/L 5.0 5 12/10/08 12:36 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 5 12/10/08 12:36 79-00-5 Trichloroethene ND ug/L 5.0 5 12/10/08 12:36 79-01-6 Trichlorofluoromethane ND ug/L 5.0 5 12/10/08 12:36 75-69-4 Vinyl chloride ND ug/L 5.0 5 12/10/08 12:36 75-01-4 Xylene (Total)40.7 ug/L 10.0 5 12/10/08 12:36 1330-20-7 m&p-Xylene 40.7 ug/L 10.0 5 12/10/08 12:36 1330-20-7 o-Xylene ND ug/L 5.0 5 12/10/08 12:36 95-47-6 1-Chloro-3-fluorobenzene (S)96 %65-137 5 12/10/08 12:36 625-98-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 8 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING QC Batch: QC Batch Method: Analysis Method: Analysis Description: GCV/2735 EPA 601/602 EPA 601/602 601/602 GCV Water Associated Lab Samples:9233761004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:209680 Associated Lab Samples:9233761004 Matrix:Water Analyzed 1,1,1-Trichloroethane ug/L ND 1.0 12/09/08 17:52 1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/09/08 17:52 1,1,2-Trichloroethane ug/L ND 1.0 12/09/08 17:52 1,1-Dichloroethane ug/L ND 1.0 12/09/08 17:52 1,1-Dichloroethene ug/L ND 1.0 12/09/08 17:52 1,2-Dibromoethane (EDB)ug/L ND 1.0 12/09/08 17:52 1,2-Dichlorobenzene ug/L ND 1.0 12/09/08 17:52 1,2-Dichloroethane ug/L ND 1.0 12/09/08 17:52 1,2-Dichloropropane ug/L ND 1.0 12/09/08 17:52 1,3-Dichlorobenzene ug/L ND 1.0 12/09/08 17:52 1,4-Dichlorobenzene ug/L ND 1.0 12/09/08 17:52 Benzene ug/L ND 1.0 12/09/08 17:53 Bromodichloromethane ug/L ND 1.0 12/09/08 17:52 Bromoform ug/L ND 1.0 12/09/08 17:52 Bromomethane ug/L ND 1.0 12/09/08 17:52 Carbon tetrachloride ug/L ND 1.0 12/09/08 17:52 Chlorobenzene ug/L ND 1.0 12/09/08 17:52 Chloroethane ug/L ND 1.0 12/09/08 17:52 Chloroform ug/L ND 1.0 12/09/08 17:52 Chloromethane ug/L ND 2.0 12/09/08 17:52 cis-1,2-Dichloroethene ug/L ND 1.0 12/09/08 17:52 cis-1,3-Dichloropropene ug/L ND 1.0 12/09/08 17:52 Dibromochloromethane ug/L ND 1.0 12/09/08 17:52 Dichlorodifluoromethane ug/L ND 1.0 12/09/08 17:52 Diisopropyl ether ug/L ND 1.0 12/09/08 17:53 Ethylbenzene ug/L ND 1.0 12/09/08 17:53 m&p-Xylene ug/L ND 2.0 12/09/08 17:53 Methyl-tert-butyl ether ug/L ND 1.0 12/09/08 17:53 Methylene Chloride ug/L ND 2.0 12/09/08 17:52 Naphthalene ug/L ND 2.0 12/09/08 17:53 o-Xylene ug/L ND 1.0 12/09/08 17:53 Tetrachloroethene ug/L ND 1.0 12/09/08 17:52 Toluene ug/L ND 1.0 12/09/08 17:53 trans-1,2-Dichloroethene ug/L ND 1.0 12/09/08 17:52 trans-1,3-Dichloropropene ug/L ND 1.0 12/09/08 17:52 Trichloroethene ug/L ND 1.0 12/09/08 17:52 Trichlorofluoromethane ug/L ND 1.0 12/09/08 17:52 Vinyl chloride ug/L ND 1.0 12/09/08 17:52 Xylene (Total)ug/L ND 2.0 12/09/08 17:53 1-Chloro-3-fluorobenzene (S)%103 65-137 12/09/08 17:52 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 9 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 209681LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1-Trichloroethane ug/L 21.620 108 41-138 1,1,2,2-Tetrachloroethane ug/L 21.220 106 8-184 1,1,2-Trichloroethane ug/L 20.420 102 39-136 1,1-Dichloroethane ug/L 20.120 101 47-132 1,1-Dichloroethene ug/L 20.520 102 28-167 1,2-Dibromoethane (EDB)ug/L 20.420 102 50-150 1,2-Dichlorobenzene ug/L 21.820 109 1-208 1,2-Dichloroethane ug/L 23.620 118 51-147 1,2-Dichloropropane ug/L 20.120 100 44-156 1,3-Dichlorobenzene ug/L 20.420 102 7-187 1,4-Dichlorobenzene ug/L 21.520 107 42-143 Benzene ug/L 22.120 110 39-150 Bromodichloromethane ug/L 21.820 109 42-172 Bromoform ug/L 20.620 103 13-159 Bromomethane ug/L 18.220 91 1-144 Carbon tetrachloride ug/L 23.020 115 43-143 Chlorobenzene ug/L 22.120 111 38-150 Chloroethane ug/L 20.420 102 46-137 Chloroform ug/L 15.720 78 49-133 Chloromethane ug/L 22.920 114 1-193 cis-1,2-Dichloroethene ug/L 21.820 109 38-155 cis-1,3-Dichloropropene ug/L 23.220 116 22-178 Dibromochloromethane ug/L 20.620 103 24-191 Dichlorodifluoromethane ug/L 22.120 110 48-157 Diisopropyl ether ug/L 19.220 96 89-108 Ethylbenzene ug/L 20.720 103 32-160 m&p-Xylene ug/L 38.840 97 82-115 Methyl-tert-butyl ether ug/L 21.120 106 88-110 Methylene Chloride ug/L 21.020 105 25-162 Naphthalene ug/L 17.220 86 50-150 o-Xylene ug/L 19.820 99 91-110 Tetrachloroethene ug/L 21.020 105 26-162 Toluene ug/L 21.520 107 46-148 trans-1,2-Dichloroethene ug/L 22.820 114 38-155 trans-1,3-Dichloropropene ug/L 20.720 103 22-178 Trichloroethene ug/L 20.320 102 35-146 Trichlorofluoromethane ug/L 21.820 109 21-156 Vinyl chloride ug/L 21.220 106 28-163 Xylene (Total)ug/L 58.760 98 50-150 1-Chloro-3-fluorobenzene (S)%99 65-137 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 10 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING QC Batch: QC Batch Method: Analysis Method: Analysis Description: GCV/2736 EPA 601 EPA 601 601 GCV Water Associated Lab Samples:9233761001, 9233761002, 9233761003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:209917 Associated Lab Samples:9233761001, 9233761002, 9233761003 Matrix:Water Analyzed 1,1,1-Trichloroethane ug/L ND 1.0 12/10/08 17:11 1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/10/08 17:11 1,1,2-Trichloroethane ug/L ND 1.0 12/10/08 17:11 1,1-Dichloroethane ug/L ND 1.0 12/10/08 17:11 1,1-Dichloroethene ug/L ND 1.0 12/10/08 17:11 1,2-Dibromoethane (EDB)ug/L ND 1.0 12/10/08 17:11 1,2-Dichlorobenzene ug/L ND 1.0 12/10/08 17:11 1,2-Dichloroethane ug/L ND 1.0 12/10/08 17:11 1,2-Dichloropropane ug/L ND 1.0 12/10/08 17:11 1,3-Dichlorobenzene ug/L ND 1.0 12/10/08 17:11 1,4-Dichlorobenzene ug/L ND 1.0 12/10/08 17:11 Bromodichloromethane ug/L ND 1.0 12/10/08 17:11 Bromoform ug/L ND 1.0 12/10/08 17:11 Bromomethane ug/L ND 1.0 12/10/08 17:11 Carbon tetrachloride ug/L ND 1.0 12/10/08 17:11 Chlorobenzene ug/L ND 1.0 12/10/08 17:11 Chloroethane ug/L ND 1.0 12/10/08 17:11 Chloroform ug/L ND 1.0 12/10/08 17:11 Chloromethane ug/L ND 2.0 12/10/08 17:11 cis-1,2-Dichloroethene ug/L ND 1.0 12/10/08 17:11 cis-1,3-Dichloropropene ug/L ND 1.0 12/10/08 17:11 Dibromochloromethane ug/L ND 1.0 12/10/08 17:11 Dichlorodifluoromethane ug/L ND 1.0 12/10/08 17:11 Methylene Chloride ug/L ND 2.0 12/10/08 17:11 Tetrachloroethene ug/L ND 1.0 12/10/08 17:11 trans-1,2-Dichloroethene ug/L ND 1.0 12/10/08 17:11 trans-1,3-Dichloropropene ug/L ND 1.0 12/10/08 17:11 Trichloroethene ug/L ND 1.0 12/10/08 17:11 Trichlorofluoromethane ug/L ND 1.0 12/10/08 17:11 Vinyl chloride ug/L ND 1.0 12/10/08 17:11 1-Chloro-3-fluorobenzene (S)%103 65-137 12/10/08 17:11 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 209918LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1-Trichloroethane ug/L 21.220 106 41-138 1,1,2,2-Tetrachloroethane ug/L 22.020 110 8-184 1,1,2-Trichloroethane ug/L 21.220 106 39-136 1,1-Dichloroethane ug/L 21.320 106 47-132 1,1-Dichloroethene ug/L 22.320 112 28-167 1,2-Dibromoethane (EDB)ug/L 21.420 107 50-150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 11 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 209918LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dichlorobenzene ug/L 22.020 110 1-208 1,2-Dichloroethane ug/L 23.020 115 51-147 1,2-Dichloropropane ug/L 20.820 104 44-156 1,3-Dichlorobenzene ug/L 24.020 120 7-187 1,4-Dichlorobenzene ug/L 19.820 99 42-143 Bromodichloromethane ug/L 21.320 107 42-172 Bromoform ug/L 21.620 108 13-159 Bromomethane ug/L 21.220 106 1-144 Carbon tetrachloride ug/L 19.820 99 43-143 Chlorobenzene ug/L 20.320 102 38-150 Chloroethane ug/L 21.020 105 46-137 Chloroform ug/L 15.720 79 49-133 Chloromethane ug/L 26.220 131 1-193 cis-1,2-Dichloroethene ug/L 21.820 109 38-155 cis-1,3-Dichloropropene ug/L 22.920 114 22-178 Dibromochloromethane ug/L 21.620 108 24-191 Dichlorodifluoromethane ug/L 22.420 112 48-157 Methylene Chloride ug/L 21.920 110 25-162 Tetrachloroethene ug/L 20.820 104 26-162 trans-1,2-Dichloroethene ug/L 23.520 117 38-155 trans-1,3-Dichloropropene ug/L 21.420 107 22-178 Trichloroethene ug/L 21.220 106 35-146 Trichlorofluoromethane ug/L 21.620 108 21-156 Vinyl chloride ug/L 20.520 103 28-163 1-Chloro-3-fluorobenzene (S)%98 65-137 Parameter Units Dup Result Max RPD QualifiersRPDResult 9233928001 209919SAMPLE DUPLICATE: 1,1,1-Trichloroethane ug/L ND 30ND 1,1,2,2-Tetrachloroethane ug/L ND 30ND 1,1,2-Trichloroethane ug/L ND 30ND 1,1-Dichloroethane ug/L ND 30ND 1,1-Dichloroethene ug/L ND 30ND 1,2-Dibromoethane (EDB)ug/L ND 30ND 1,2-Dichlorobenzene ug/L ND 30ND 1,2-Dichloroethane ug/L ND 30ND 1,2-Dichloropropane ug/L ND 30ND 1,3-Dichlorobenzene ug/L ND 30ND 1,4-Dichlorobenzene ug/L ND 30ND Bromodichloromethane ug/L ND 30ND Bromoform ug/L ND 30ND Bromomethane ug/L ND 30ND Carbon tetrachloride ug/L ND 30ND Chlorobenzene ug/L ND 30ND Chloroethane ug/L ND 30ND Chloroform ug/L ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 12 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING Parameter Units Dup Result Max RPD QualifiersRPDResult 9233928001 209919SAMPLE DUPLICATE: Chloromethane ug/L ND 30ND cis-1,2-Dichloroethene ug/L 3.4 .2 303.4 cis-1,3-Dichloropropene ug/L ND 30ND Dibromochloromethane ug/L ND 30ND Dichlorodifluoromethane ug/L ND 30ND Methylene Chloride ug/L ND 30ND Tetrachloroethene ug/L 7.6 4 307.3 trans-1,2-Dichloroethene ug/L ND 30ND trans-1,3-Dichloropropene ug/L ND 30ND Trichloroethene ug/L 3.9 5 303.7 Trichlorofluoromethane ug/L ND 30ND Vinyl chloride ug/L ND 30ND 1-Chloro-3-fluorobenzene (S)%115 6109 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 13 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Pace Project No.: Project: 9233761 HONBARRIER ANNUAL SAMPLING DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 12/19/2008 10:18 AM Page 14 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176