20064_Simpson Gas_Limited Soil and Groundwater Assessment_20170518

Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
544 East Main Street
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002
Prepared for:
Mainspring Conservation Trust
577 East Main Street
Franklin, North Carolina 28734
Prepared by:
S&ME, Inc.
44 Buck Shoals Road, Ste C-3
Arden, NC 28704
May 18, 2017
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002
May 18, 2017 ii

Table of Contents
1.0 Project Information ............................................................................................... 1
1.1 Project Location ................................................................................................................. 1
1.2 Project Background .......................................................................................................... 1
1.2.1 Comprehensive Site Assessment (1999) .............................................................................. 1
1.2.2 UST Closure Testing (1999) ............................................................................................... 2
1.2.3 Sewer Line Installation (2010) ............................................................................................ 2
1.2.4 Soil and Groundwater Assessment (2015) .......................................................................... 2
1.2.5 Brownfields Assessment ...................................................................................................... 3
2.0 Work Plan Development ...................................................................................... 4
3.0 Permitting................................................................................................................ 4
4.0 Field Services .......................................................................................................... 4
4.1 Monitoring Well Installation ........................................................................................... 4
4.2 Soil Sampling Methodology ............................................................................................ 5
4.2.1 Near-Surface Soil Sampling ................................................................................................ 5
4.2.2 Sub-Surface Soil Samples .................................................................................................... 6
4.2.3 Heating Oil UST ................................................................................................................. 6
4.3 Groundwater Sampling Methodology .......................................................................... 7
4.4 Investigative Derived Waste (IDW) Management ....................................................... 7
5.0 Laboratory Results................................................................................................. 8
5.1 Soil Sampling Results ....................................................................................................... 8
5.1.1 Near-Surface Soil Sampling Results ................................................................................... 8
5.1.2 Sub-Surface Soil Sampling Results ..................................................................................... 8
5.1.3 Heating Oil UST Soil Sampling Results ............................................................................ 9
5.2 Groundwater Sampling Results ..................................................................................... 9
6.0 Quality Control Discussion ............................................................................... 10
6.1 Analytical Data Quality Review ................................................................................... 10
6.2 Quality Control Data ...................................................................................................... 10
6.2.1 Trip Blanks ........................................................................................................................ 10
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002
May 18, 2017 iii
6.2.2 Equipment Blanks ............................................................................................................. 10
6.2.3 Field Blanks ....................................................................................................................... 11
6.2.4 Duplicate Sample .............................................................................................................. 11
6.2.4.1 Soil Duplicate Sample .................................................................................................... 12
6.2.4.2 Groundwater Duplicate Sample ................................................................................... 12
6.2.5 Sampling Equipment ......................................................................................................... 12
7.0 Work Plan Deviations ......................................................................................... 12
8.0 Conclusions .......................................................................................................... 13
8.1 Groundwater ................................................................................................................... 13
8.2 Soil .................................................................................................................................... 13
9.0 Sole Use Statement .............................................................................................. 14
10.0 Limitations ............................................................................................................ 14
11.0 References ............................................................................................................. 15

List of Tables
Table 4-1: Summary of Near Surface PID Screening Results ................................................................ 6
Table 4-2: Summary of Sub-Surface PID Screening Results .................................................................. 6
Table 5-1: Near-Surface Sampling Results in Exceedance of Unrestricted PSRGs ............................ 8
Table 5-2: Sub-Surface Sampling Results in Exceedance of Unrestricted PSRGs ............................... 9

Appendices
Appendix I –Figures
Appendix II – Additional Tables
Appendix III – Work Plan Approval Letter
Appendix IV – Well Construction Permit Approval Letter
Appendix V – Site Photographs
Appendix VI – Well Construction Log and Record
Appendix VII – Soil Boring Logs
Appendix VIII – Field Sampling Forms
Appendix IX – Analytical Laboratory Report

Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 1
1.0 Project Information
1.1 Project Location
The subject property is located at the intersection of Northeast Main Street and Big Bear Lane on the
property addressed 544 East Main Street in Franklin, Macon County, North Carolina. Based on a review of
the Macon County Geographical Information System (GIS) website, the subject property consists of
parcels 6595318254 and 6595317214, totaling 0.67-acres in size. The property is developed with a vacant
single story structure formerly used as a fuel station. The vicinity of the subject property is mainly
commercial properties with a greenway to the north. A map depicting the location of the parcels is
included in Figure 1, Appendix I. An aerial photograph of the subject property is presented as Figure 3,
Appendix I.
1.2 Project Background
The subject property historically has been developed as a fuel station since the 1950s; selling kerosene,
fuel oil, gasoline, and diesel fuel. One fuel dispenser was located adjacent to the northeastern corner of
the building on the subject property, two dispensers were located near East Main Street, and heating oil
and kerosene was distributed via the overhead product lines connected to the former fueling rack on the
southwestern portion of the building. Based on an interview between Mr. Bob Simpson, the current
property owner, and S&ME, four 30,000-gallon ASTs were located on the subject property. Based on a
review of aerial photographs, the four 30,000-gallon ASTs were located on the subject property from the
1950s through 2005. According to the North Carolina Department of Environmental Quality (NCDEQ)
Underground Storage Tank (UST) Registered Tank Database, one 2,000-gallon gasoline UST was installed
on February 26, 1981 and one 550-gallon diesel UST was installed on February 26, 1984. The USTs were
permanently closed by removal in April 1994. The property is currently vacant and no longer operated as
a fuel station.
The subject property has been accepted into the North Carolina Brownfields Program. Mainspring.
Conservation Trust (Mainspring) was able to execute a contract with an option to purchase the subject
property and is moving forward with additional effort to obtain a BFA that would allow the property to be
used as greenspace.
Previous assessment activities are summarized in the following sections:
1.2.1 Comprehensive Site Assessment (1999)
In response to a Notice of Violation issued by NCDEQ in October 1998, Alpha Environmental Science, Inc.
(Alpha) was contracted by Mr. Doug Simpson (father of the current owner), the property owner and
former operator of Simpson Gas and Oil, to complete a Comprehensive Site Assessment (CSA) for the
subject property. The CSA activities included the collection of 11 groundwater samples from the shallow,
unconfined aquifer, three soil samples adjacent to the former AST area, and two soil samples at the
approximate depth of the former UST tank excavation. Based on a review of the analytical results
presented on Figure 2 of the 1999 Alpha CSA, groundwater contamination was detected in the vicinity of
the ASTs, dispensers, and in the vicinity of the eastern property boundary. Soil contamination was
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 2
detected in the samples collected near the ASTs and former USTs. It should be noted that a groundwater
sample was not collected near the former USTs.
1.2.2 UST Closure Testing (1999)
According the NCDEQ UST Registered Tank Database and the UST-2 forms found in Appendix B of the
Underground Storage Tank Closure Report written by Alpha and dated March 1999, the 2,000-gallon and
550-gallon USTs located on the Simpson Oil property were permanently closed in April 1994. To provide
proper UST closure sampling, Alpha collected two soil samples from beneath the former UST tank basin in
November 1998 and two in February 1999. Alpha summarized the analytical results by stating, “Based on
the analytical results reported, it appears that a release of petroleum has occurred from the USTs”. It is
documented in the UST-2 form of the March 1999 Alpha report that the 2,000-gallon UST was converted
to an AST and the 550-gallon UST was transferred to a farmers possession to be used as an AST.
1.2.3 Sewer Line Installation (2010)
Petroleum-impacted soil was encountered during installation of sewer line on the west side of the subject
property adjacent to NE Main Street. Approximately, 30 to 45 tons of petroleum-impacted soil was
excavated and transported off-site for disposal during installation of the sewer line.
1.2.4 Soil and Groundwater Assessment (2015)
S&ME performed soil and groundwater assessment activities on the subject property in July 2015 for the
NCDEQ Inactive Hazardous Site Branch (IHS). At the time of the 2015 assessment activities, the Land Trust
for the Little Tennessee (now known as Mainspring Conservation Trust) was in the process of obtaining a
contract with an option to purchase the subject property with tentative plans to redevelop the subject
property as green space under a BFA. The North Carolina Brownfields Program received a grant from the
United States Environmental Protection Agency (USEPA) to be used for assessment activities to move the
subject property along in the BFA process. The NCDEQ IHS was tasked with contracting the assessment
activities for completion.
In July 2015, S&ME installed eight temporary monitoring wells and collected groundwater samples for
analyses of volatile organic compounds (VOCs) by Method 8260LL (low level) and semi-volatile organic
compounds (SVOCs) by EPA Method 8270D. Target analytes were detected in two of the groundwater
samples at concentrations that exceed the respective NCDEQ UST Gross Contamination Levels (GCLs).
Target analytes were detected in the groundwater samples collected from monitoring wells TMW-1
through TMW-8 at concentrations that exceed the respective North Carolina Groundwater Quality
Standards (15A NCAC 2L .0202), herein identified as the 2L Standards. Target analytes were detected in
seven of the groundwater samples at concentration that exceeded the respective NCDEQ Division of
Waste Management (DWM) Vapor Intrusion Non-Residential Groundwater Screening Levels (GWSLs).
S&ME completed 20 soil borings ranging in depths from 10 to 20 feet below ground surface (ft-bgs) and
collected soil samples ranging in depths from 4 to 10 ft-bgs for analyses of VOCs by 8260B and SVOCs by
EPA Method 8270D. Target analytes were detected at concentrations in two of the soil samples that
exceeded the respective Industrial Preliminary Soil Remediation Goals (PSRGs), in three of the soil samples
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 3
that exceeded the respective Residential PSRGs1, and eight of the soil samples that exceeded the
respective Protection of Groundwater PSRGs. Based on the groundwater elevation figure, the
groundwater flows east towards the Little Tennessee River. During the assessment, groundwater was
encountered approximately 9 to 14 ft-bgs. The findings of the assessment activities were provided in the
Report of Environmental Services dated September 4, 2015. The report concluded that it appears that a
release of petroleum has occurred either from the former aboveground storage tanks (ASTs) or
underground (USTs) located on the eastern side of the retail store.
1.2.5 Brownfields Assessment
In general accordance with S&ME Proposal No. 43-1600872 dated November 7, 2016, S&ME completed a
Phase I Environmental Site Assessment (ESA) in association with the subject property. The February 2017
Phase I ESA revealed the following recognized environmental conditions in connection with the subject
property:
 The subject property historically operated as a fuel station with ASTs and USTs. Petroleum
contaminated soil and groundwater has been documented on the subject property.
 A heating oil UST was observed on the subject property, adjacent to and north of the northern
most structure located on the southwestern adjoining property.
 The former fuel station operation on the southwestern adjoining property addressed 522 East
Main Street.
On March 27, 2017, Mr. Bradley Keyse and Mr. Loftis, both with S&ME, attended a meeting with the
following individuals to present the historical assessment information related to the subject property and
make recommendations for additional assessment activities to address data gaps identified by S&ME:
 Ms. Sharon Taylor, Executive Director of Mainspring,
 Mr. Jordan Smith, Land Conservation Manager with Mainspring,
 Mr. Ben Laseter, Associate Director with Mainspring,
 Mr. Ken Murphy, member of the Mainspring Board of Directors,
 Mr. Ken Fromknecht, attorney representing Mainspring in the context of the real estate
transaction, and
 Ms. Jordan Thompson and Ms. Tracy Wahl, both with NCDEQ Division of Waste Management
(DWM) Brownfields Program.
On March 29, 2017, S&ME provided a proposal to Mr. Laseter to conduct a Limited Soil and Groundwater
Assessment on the subject property. On April 5, 2017, Ms. Taylor, authorized S&ME to perform the scope
of work outlined in S&ME Proposal No. 43-1600872 Change Order 01.

1 Now identified as the Unrestricted PSRGs
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 4
2.0 Work Plan Development
Prior to conducting the field services, a Work Plan was prepared to address requirements for conducting
work on NCDEQ Brownfield sites. The Work Plan addressed proposed additional soil and groundwater
assessment activities to further characterize the petroleum impacts documented at the site. The Work
Plan was submitted to Ms. Jordan Thompson with NCDEQ on April 4, 2017 and approved on April 5, 2017
on the condition that two comments provided by Ms. Thompson be addressed. The revised version of the
Work Plan was submitted to Ms. Thompson on April 11, 2017. On April 11, 2017, Ms. Thompson provided
a letter to Mainspring indicating that the Work Plan dated April 11, 2017 was approved by NCDEQ. The
approval letter is included in Appendix III.
3.0 Permitting
On April 7, 2017, in an effort to expedite the assessment activities, S&ME prepared and submitted a
monitoring well permit to Mr. Andrew W. Moore, P.G. with the NCDEQ Division of Water Resources. On
April 7, 2017, Mr. Moore informed S&ME via electronic mail that the proposed monitoring well on the
subject property was authorized for installation under well construction permit number WM0100403. On
April 11, 2017, Mr. Moore provided a well construction permit letter. The well construction permit is
provided in Appendix IV.
4.0 Field Services
S&ME contacted North Carolina One Call public utility locating service and retained the services of Utility
Specialist, Inc. (USI), a private utility locating service, to identify buried utilities that were in the work area.
A Site Specific Health and Safety Plan was prepared, following the requirements of CFR 1910.120
Hazardous Waste Operations and Emergency Response Standard (HAZWOPER) rule of the protection of
workers who are exposed or potentially exposed to hazardous substances. Site photographs taken during
field activities are presented in Appendix V.
4.1 Monitoring Well Installation
On April 12, 2017, S&ME installed permanent monitoring well as MW-1 on the northeastern portion of
the subject property near former temporary monitoring well TMW-4 installed during the July 2015
assessment. Mr. Bradley Keyse, with S&ME, was present on the subject property with Mr. Brian Ewing, a
North Carolina licensed well driller with South Atlantic Environmental Drilling and Construction Co. Inc.
(SAEDACCO). A 7822DT Geoprobe® drill rig was used with 4 ¼-inch inside diameter (ID) augers to
complete the soil boring for the installation of the monitoring well.
Prior to the installation of the monitoring well, S&ME collected soil profiles in 5 foot intervals using the
Geoprobe® Macro-Core® sampler to a depth of 20 ft-bgs. The soil profiles were contained in the
Macro-Core® sampler’s PVC sleeves and observed by S&ME personnel for soil lithology, the presence of
petroleum odors, staining, and groundwater. The soil profiles collected in the PVC sleeves were split into
5-foot samples and placed in sealed plastic bags. The collected soil samples were screened for the
presence of VOCs utilizing a calibrated MiniRAE 3000 PID meter. The PID readings ranged from 59.1 parts
per million (ppm) to 645.3 ppm.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 5
The well was installed for the collection of shallow groundwater located above consolidated material (i.e.
rock) at the site. No drilling within rock was performed. The permanent monitoring well consisted of 2-
inch diameter schedule 40, flush-thread, PVC pipe inserted into an approximate 8.5-inch diameter hole.
The lower portion of the pipe consists of manufactured well screen with 0.010-inch slots. The length of
the well screen pipe was determined based the depth of the apparent water table. Medium-to-fine
grained, washed sand was placed in the annular space of the well to a level approximately one foot above
the top of the well screen, with an approximate two foot thick bentonite seal positioned on top of the
sand pack. The annular space above the bentonite seal was grouted with Portland cement to the ground
surface. The new well was encased with a flush mount protective steel casing with a bolted manhole
cover.
Following installation, the monitoring well was developed with a decontaminated submersible pump and
new polyethylene tubing by evacuating groundwater from the well until the groundwater became
relatively clear. Well construction data is presented in Table 1, Appendix II. The well construction log
and construction record for the installation of monitoring MW-1 is presented in Appendix VI. A
photograph of the completed monitoring well is included as Photograph 7, Appendix V.
4.2 Soil Sampling Methodology
On April 13, 2017, twenty soil borings were completed on the subject property in the approximate
locations depicted on Figure 3, Appendix I. At each boring location, S&ME collected soil profiles via direct
push techniques with the Geoprobe® Macro-Core® sampler with the exception of soil samples SB-8 and
SB-12B that were completed with a decontaminated stainless steel hand auger.
The collected soil samples were containerized and submitted to Prism Laboratories, Inc. (Prism) a North
Carolina certified laboratory for analysis for VOCs by EPA Method 8260B, SVOCs by EPA Method 8270D,
and lead by EPA Method 6020B. After the soil samples were collected, the remaining soil from each soil
profile was field screened for concentrations of VOCs utilizing a calibrated MiniRAE 3000 PID. S&ME also
recorded the lithology of the soil as observed in the collected samples. The observed lithology and PID
screening results are included in the soil boring logs included in Appendix VII.
4.2.1 Near-Surface Soil Sampling
To identify areas of potential exposure from near-surface soil contamination, S&ME completed eighteen
shallow, near-surface soil borings on the subject property using a stainless steel hand auger or direct push
techniques. The soil boring locations are described as follows:
 Three soil borings (B-1 through B-3) were completed near the northwestern portion of the site by
Northeast Main Street,
 Three soil borings (B-4 through B-6) were completed just north of the building located on the
subject property in the vicinity of the suspected “truck washing area”.
 Three soil borings (B-12B, B-14, and B-15) were completed in the general vicinity the former
heating oil and kerosene fueling rack on the southwestern portion of the building,
 Nine soil borings (B-7 through B-9 and B-16 through B-21) were completed in the vicinity of the
former ASTs, product line, former USTs, and dispensers,
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 6
At each soil boring performed, S&ME collected a near-surface (0 to 2 feet bgs) soil sample2. The PID
readings measured in the collected soil samples are summarized below in Table 3-1.
Table 4-1: Summary of Near Surface PID Screening Results
Soil Boring ID Boring Area
PID Result
(ppm)
B-1 through B-3 Near Northeast Main Street 1.5 - 3.1
B-4 through B-6 The “Truck Wash Area” 3.8 – 24.8
B-7 through B-9 Former ASTs 0.0 – 15.4
B-12B, B-14, and B-15 Former Fueling Rack 1.3 – 6.3
B-16 and B-17 Former UST Tank Basin and Dispenser 18.8 – 528.4
B-18 and B-19 Existing Product Line 34.9 – 189.6
B-20 and B-21 Former Dispensers Near East Main Street 164.0 – 294.6
4.2.2 Sub-Surface Soil Samples
In addition to the near-surface soil samples, S&ME collected soil samples within two feet from the bottom
of the suspected former UST excavation basin located at 7 ft-bgs, the existing product lines located at 2
ft-bgs, and the piping associated with the former dispensers located at 2 ft-bgs. The PID readings
measured in the collected soil samples are summarized below in Table 3-2.
Table 4-2: Summary of Sub-Surface PID Screening Results
Soil Boring ID Boring Area
PID Result
(ppm)
B-16 and B-17 Former UST Tank Basin and Dispenser 331.3 – 332.6
B-18 and B-19 Existing Product Line 399.3 - 1042
B-20 and B-21 Former Dispensers Near East Main Street 515.6 – 700.1
4.2.3 Heating Oil UST
Two soil borings were completed adjacent the heating oil UST on the subject property, adjacent to and
north of the northern most structure located on the southwestern adjoining property. One boring was
completed on each end of the heating oil UST. One soil sample was collected from each soil boring at a
depth within two feet below the bottom elevation of the UST. Based on measurements obtained in the
field by measuring the bottom of the tank through the fill port of the heating oil UST, the bottom of the
tank is located at 4.5 ft-bgs. The PID readings measured in the collected soil samples ranged from 29.7
ppm to 76.5 ppm. Groundwater was not observed in the soil profiles.

2 Soil boring SB-8 was terminated at a depth of 1 ft-bgs due to encountering auger refusal.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 7
4.3 Groundwater Sampling Methodology
On April 13, 2017, a groundwater sample was collected from the permanent monitoring well MW-1 by Mr.
Keyse. Before purging and sampling of the monitoring well, the depth to groundwater was measured
relative to the top of casing using a decontaminated electric water level probe. S&ME also calibrated the
multi-parameter water quality and turbidity meters. Documentation of the instrument calibration is
provided in Appendix VIII. The location of monitoring well MW-1 is depicted on Figure 3, Appendix I.
The well was developed and purged for sampling using a variable speed, electric, peristaltic pump with
new polyethylene and silicon tubing. The purge water was monitored for temperature, dissolved oxygen,
pH, turbidity, and conductivity using a flow-through multi-meter. The well was considered sufficiently
purged when the temperature, dissolved oxygen, pH, and conductivity of the groundwater had stabilized
and the turbidity had either stabilized or was below 10 Nephelometric Turbidity Units (NTUs).
Stabilization occurred when dissolved oxygen, pH, conductivity, and turbidity varied no more than 10%
and the temperature was constant for three consecutive readings. If the dissolved oxygen concentration
was less than 1 milligram per liter, the dissolved oxygen concentration was deemed stabilized if the
subsequent changes in concentration were less than 0.1 milligram per liter. The stabilized field
parameters were recorded and are included with the field sampling summary sheets in Appendix VIII.
Once the groundwater monitoring well was sufficiently purged, a groundwater sample was collected from
monitoring well MW-1 using a new disposable polyethylene bailer. The collected groundwater sample
was identified as MW-1, placed into laboratory-prepared containers, and stored in a chilled cooler. The
sample was labeled to identify the sample identification, date, location, and analysis to be performed. The
sample collected from MW-1 was submitted to Prism under chain-of-custody for analysis for VOCs by EPA
Method 8260B, SVOCs by EPA Method 8270D, and lead by EPA Method 6020B. Following collection of
the groundwater sample, the total depth of the monitoring well was measured relative to the top of
casing using a decontaminated electric water level probe.
4.4 Investigative Derived Waste (IDW) Management
The contaminants of concern at the subject property are petroleum compounds. Investigative derived
waste (IDW) water generated during well development, decontamination procedures, and purging of the
existing monitoring wells was disposed of according to the following guidelines:
 Guidelines for Initial Response and Abatement, Assessment, and Corrective Action for Non-UST
Petroleum Releases developed by the NCDENR-DWM UST Section, effective July 1, 2012.
 Guidelines for Assessment and Corrective Action for UST Releases developed by the NCDENR-DWM
UST Section, Change 3, effective December 1, 2013.
According to the guidelines, the IDW water can be placed on the ground near the well in manner that will
prevent surface runoff, if hazardous waste is not likely present in the groundwater and if the uppermost
aquifer below land surface is contaminated with equal or higher concentrations than the waste water
being disposed. Historically solvents have not been detected during assessment activities on the subject
property. Soil cuttings generated during the installation of monitoring well MW-1 and the soil boring
activities was spread onsite in accordance with the guidelines reference above.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 8
5.0 Laboratory Results
5.1 Soil Sampling Results
The soil analytical data obtained from the soil borings was compared to the NCDEQ IHS Protection of
Groundwater PSRGS, NCDEQ IHS Unrestricted PSRGs, and the NCDEQ IHS Industrial/Commercial on
Figure 4, Appendix I and the tables provided in Appendix II. Due to the anticipated redevelopment of
the subject property as greenspace, the analytical data are discussed in relation to the NCDEQ IHS
Unrestricted PSRGs in the following sub-sections below. The analytical data of the target analytes
detected in the soil samples at concentrations exceeding the respective method detection limits are
summarized in Table 2A and Table 2B, Appendix II. The detected target analytes that exceed the
respective NCDEQ IHS Unrestricted PSRGs are shown in Figure 4, Appendix I and summarized below in
Table 5-1 and Table 5-2. The laboratory reports associated with the soil sampling event are included in
Appendix IX.
5.1.1 Near-Surface Soil Sampling Results
Target SVOCs and VOCs were detected in the soil sample collected from a depth of 0 to 2 ft-bgs at soil
borings B-17 at concentrations that exceeded the respective NCDEQ IHS Unrestricted PSRGs. Target
VOCs were detected in the soil sample collected from a depth of 0 to 2 ft-bgs at soil borings B-18 at
concentrations that exceeded the respective NCDEQ IHS Unrestricted PSRGs. Lead was not detected in
the near-surface soil samples at concentrations that exceeded the NCDEQ IHS Unrestricted PSRG for lead.
Table 5-1: Near-Surface Sampling Results in Exceedance of Unrestricted PSRGs
Soil Borings
Sample Depth
(ft-bgs)
Detected Target
Analytes Greater than
the Unrestricted PSRGs Collected Near
B-17 0 - 2
1-Meythlynaphthalene,
Benzene
Naphthalene
Suspected Former Diesel
UST Tank Basin
B-18 0 - 2
1,2,4-Trimethylbenzene
Ethylbenzene
Xylenes
Product Line
5.1.2 Sub-Surface Soil Sampling Results
Target VOCs were detected in the soil sample collected at a depth of 7 to 9 ft-bgs at soil boring B-16 at
concentrations that exceeded the respective NCDEQ IHS Unrestricted PSRGs. Target SVOCs and VOCs
were detected in the soil sample collected at a depth of 7 to 9 ft-bgs at soil boring B-17 at concentrations
that exceeded the respective NCDEQ IHS Unrestricted PSRGs. Target VOCs were detected in the soil
samples collected at a depth of 2 to 4 ft-bgs at soil borings B-18, B-20, and B-21 at concentrations that
exceeded the respective NCDEQ IHS Unrestricted PSRGs. Lead was not detected in the sub-surface soil
samples at concentrations that exceeded the NCDEQ IHS Unrestricted PSRG for lead.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 9
Table 5-2: Sub-Surface Sampling Results in Exceedance of Unrestricted PSRGs
Soil Borings
Sample Depth
(ft-bgs)
Detected Target
Analytes Greater than
the Unrestricted PSRGs Collected Near
B-16 7 - 9
1,2,4-Trimethylbenzene,
Benzene
Ethylbenzene
Naphthalene
Xylenes
Suspected Former
Gasoline UST Tank Basin
and Dispenser
B-17 7 - 9
1-Methylnaphthalene
2-Methylnapthalene
1,2,4-Trimethylbenzene
Benzene
Ethylbenzene
Naphthalene
Suspected Former Diesel
UST Tank Basin
B-18 2 – 4
1,2,4-Trimethylbenzene,
Benzene
Ethylbenzene
Naphthalene
Xylenes
Existing Product Line
B-20 and B-21 2 – 4
1,2,4-Trimethylbenzene,
Ethylbenzene (B-20 only)
Naphthalene
Former Dispensers
5.1.3 Heating Oil UST Soil Sampling Results
1,2,4-Trimethylbenzene, a target VOC, was detected in the soil sample collected from a depth of 5 to 6 ft-
bgs at soil boring B-23 at a concentration that exceeded the respective NCDEQ IHS Unrestricted PSRGs
for 1,2,4-trimethylbenzene. Lead was not detected in the sub-surface soil samples collected near the
heating oil UST at concentrations that exceeded the NCDEQ IHS Unrestricted PSRG for lead.
5.2 Groundwater Sampling Results
The groundwater analytical data obtained from the on-site monitoring well was compared to the current
2L Standards, the NCDEQ UST GCLs, and the NCDEQ DWM Residential and Non-Residential Vapor
Intrusion GWSLs. The analytical data of the target analytes detected in the groundwater sample collected
from monitoring well MW-1 at concentrations exceeding the respective method detection limits are
summarized on Table 3. The detected target analytes that exceed the respective 2L Standards are shown
in Figure 4, Appendix I. The analytical laboratory reports are included in Appendix IX.
Target SVOC and VOC analytes, including but not limited to, 1-methlynaphthalene, benzene, methyl-tert-
butyl ether (MTBE), naphthalene, and xylenes, were detected in the groundwater sample collected from
monitoring well MW-1 at concentrations that exceeded the respective 2L Standards.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 10
Target SVOC and VOC analytes, including but not limited to, naphthalene, benzene, 1,2,-
trimethylbenzene, and ethylbenzene, were detected in the groundwater sample collected from monitoring
well MW-1 at concentrations that exceeded the respective NCDEQ DWM Residential Vapor Intrusion
Groundwater Screening Levels (GWSLs).
Lead was not detected in the groundwater sample collected from monitoring well MW-1 at a
concentration that exceeded the 2L Standard for lead.
6.0 Quality Control Discussion
6.1 Analytical Data Quality Review
A qualitative review of the data was performed to verify that the detected concentrations in the laboratory
report were of known quality. A formal, quantitative data validation was not performed. Quality control
data provided in the laboratory reports were also reviewed. No rejected or otherwise unacceptable
quality data were reported from the laboratory.
6.2 Quality Control Data
6.2.1 Trip Blanks
One trip blank was placed in the each of the two coolers containing groundwater samples, the field blank
sample, and the equipment blanks during the shipment to the laboratory. The two trip blanks were
submitted to Prism for analysis of VOCs by EPA Method 8260B.
No target compounds were detected in trip blank samples Trip Blank-1 and Trip Blank-2. The results of
the trip blank analysis indicated that the collected soil groundwater samples, the field blank, and
equipment blanks were not subject to cross contamination during shipment. The laboratory results are
summarized in Table 3, Appendix II. The laboratory report is included in Appendix IX.
6.2.2 Equipment Blanks
The direct push tooling was decontaminated before each boring location using an Alconox®/water soap
mixture and water rinse. The hollow stem auger tooling was decontaminated prior to arrival to the
subject property. One equipment rinsate sample (Equipment Blank-1) was collected from the
decontaminated lead/cutting auger upon arrival to the subject property, one equipment rinsate sample
(Equipment Blank-2) was collected following the decontamination of the Macro-Core® sampler, and one
equipment rinsate sample (Equipment Blank-3) was collected following the decontamination of the
stainless steel hand auger. The rinsate sample was collected by pouring metals free deionized water
through the equipment into laboratory-prepared sampling containers.

The equipment rinsate samples were submitted to Prism under chain-of-custody for analyses for VOCs by
EPA Method 8260B, SVOCs by EPA Method 8270D, and lead by EPA Method 6020B. The results of the
rinsate sample analyses indicate that lead and 1,2,4-trichlorobenzene were detected in the equipment
rinsate samples (Equipment Blank-1) that was collected from the lead auger and methylene chloride was
detected in all three equipment rinsate samples.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 11
The lead and 1,2,4-trichlorobenzene detected in the equipment rinsate sample from the lead auger is
suspected to be from an off-site source that was not fully removed during decontamination activities prior
to site arrival. 1,2,4-Trichlorobenzene was not detected in the record or duplicate groundwater samples
collected from monitoring well MW-1 or in the soil samples collected throughout the site; therefore, it can
be concluded that the presence of 1,2,4-trichlorobenzene on the lead auger did not cause a detection in
the groundwater sample collected from monitoring well MW-1.
The lead concentrations detected in the rinsate sample collected from the lead auger likely represents
lead from an off-site source that was not fully removed during decontamination activities prior to site
arrival. Based on the distribution of lead concentrations detected in the collected soil samples, S&ME
concludes that the petroleum products released at the site were non-lead containing and the lead
detected throughout the soil and in the groundwater samples collected from monitoring well MW-1 is
likely naturally occurring.
The methylene chloride detected in all three equipment rinsate samples is a common laboratory
contaminant and is not suspected to be as a result of insufficient decontamination activities.
In summary, the laboratory results indicated that the decontamination procedures did not compromise
the integrity of the samples. The results for the rinsate sample are summarized in Table 3, Appendix II
and the laboratory report is included in Appendix IX.
6.2.3 Field Blanks
One field blank sample (Field Blank) was prepared by pouring laboratory supplied deionized water directly
into laboratory prepared containers at the location of monitoring well MW-1 and analyzed for VOCs by
EPA Method 8260B. No VOCs were detected in this sample above the laboratory reporting limits. The
laboratory results indicated that the groundwater water collection procedures did not contaminate or
otherwise compromise the integrity of the samples. The laboratory results are summarized in Table 3,
Appendix II. The laboratory report is included in Appendix IX.
6.2.4 Duplicate Sample
Duplicate samples were analyzed in association with the collected soil and groundwater samples. Relative
percent difference (RPD), a measure of precision, was used to compare analytical results between sample
and duplicate pair. RPD is calculated by
𝑅𝑃𝐷 (%) =(𝑋1 −𝑋2) / 𝑋𝑎𝑣𝑒 ∗ 100
where:
X1 = concentration of sample
X2 = concentration of duplicate pair
Xave = ((X1 + X2) / 2)
The RPD calculations were conducted only for the analytes detected in the record or corresponding
duplicate samples at concentrations exceeding the laboratory method detection limits. During
performance of the RPD calculations, for concentrations of analytes not detected by the laboratory
method, the concentrations were set equal to the laboratory reporting limit.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 12
6.2.4.1 Soil Duplicate Sample
A blind duplicate (Duplicate-1) was submitted for soil sample SB-18 (0’-2’) and analyzed for the same
parameters as the original sample. The laboratory results for Duplicate-1 are summarized in Table 2A
and Table 2B, Appendix II and the laboratory report is included in Appendix IX.

The laboratory results for the detected compounds submitted for soil sample SB-18 (0’-2’) and its blind
duplicate (Duplicate-1) had RPDs between 12% and 128%. However, a review of the laboratory data
quality information provided along with the analytical reports found no data to have been flagged as
rejected. Based on this observation, S&ME believes that the acquired data should be accepted. The
calculated RPDs for target analytes detected in both the record and duplicate samples are summarized in
Table 2A and Table 2B, Appendix II.
6.2.4.2 Groundwater Duplicate Sample
A blind duplicate (Duplicate-2) was submitted for groundwater sample MW-1 for the parameters as the
original sample. The laboratory results for Duplicate-2 are summarized in Table 3, Appendix II and the
laboratory report is included in Appendix IX.
The laboratory results for the detected compounds submitted for groundwater sample MW-1 and its
blind duplicate (Duplicate-2 had RPDs between 0% and 44%. However, a review of the laboratory data
quality information provided along with the analytical reports found no data to have been flagged as
rejected. Based on this observation, S&ME believes that the acquired data should be accepted. The
calculated RPDs for target analytes detected in both the record and duplicate samples are summarized in
Table 3, Appendix II.
6.2.5 Sampling Equipment
New silicone tubing (at the pump head) and polyethylene tubing (downwell) was used to purge each well.
A new disposable polyethylene bailer and twine was used to collect the groundwater sample from
monitoring well MW-1.
7.0 Work Plan Deviations
Four near-surface soil samples were not collected inside the building in the general vicinity of the former
heating oil and kerosene fueling rack as the concrete cores were not completed for two of the soil borings
and auger refusal was encountered at the remaining two soil boring locations. The soil borings not
completed are identified as B-10 through B-13 on Figure 3, Appendix I. The concrete cores for boring B-
12 and B-13 were not completed as the concrete coring machine would not adhere to the concrete due to
the uneven surface. Auger refusal was encountered in boring B-10 on stone and in boring B-11 on a
wooden object (Photo 8, Appendix V).
During the assessment activities on April 13, 2017, Mr. Keyse contacted Ms. Thompson to discuss the
deviations associated with the proposed near-surface soil sampling within the former fueling rack area.
Ms. Thompson suggested that S&ME obtain a soil sample from the southwest side of the building in lieu
of the interior soil samples. The soil boring is identified as B-12B on Figure 3, Appendix I. Ms.
Thompson also explained that the missed interior soil samples are not significant to the assessment as
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 13
near-surface soil sampling will be required once the building is removed and final grade site development
is completed.
8.0 Conclusions
8.1 Groundwater
On April 12, 2017, S&ME installed one 2-inch diameter permanent monitoring well identified as MW-1 on
the subject property. On April 13, 2017, S&ME collected a groundwater sample from newly installed
monitoring well for analyses of VOCs by Method 8260B, SVOCs by EPA Method 8270D, and lead by EPA
Method 6020B. The following is a summary of the analytical results:
 Several target analytes were detected in the groundwater sample collected from monitoring well
MW-1 at concentrations that exceed the respective 2L Standards.
 Several target analytes were detected in the groundwater samples collected from monitoring well
MW-1 at concentration that exceeded the respective NCDEQ DWM Residential Vapor Intrusion
GWSLs.
 Lead was not detected in the groundwater sample collected from monitoring well MW-1 at
concentration that exceeded the 2L Standard for lead.
 Free product was not detected in monitoring well MW-1.
Based on the historical data and the recent limited groundwater assessment activities, a dissolved
contaminant plume is likely present under the majority of the subject property and is likely migrating
easterly towards Big Bear Lane.
8.2 Soil
On April 13, 2017, twenty soil borings were completed on the subject property for the collection of soil
samples for analyses of VOCs by Method 8260B, SVOCs by EPA Method 8270D, and lead by EPA Method
6020B. The following summarizes the sampling locations and depths:
 Eighteen near surface soil samples were collected from a depth of 0 ft-bgs to 2 ft bgs3;
 Four soil samples were collected at a depth of 2 ft-bgs to 4 ft-bgs, directly below the depth of the
product line at the location of the existing product line and former dispenser islands;
 Two soil samples were collected at a depth of 7 ft-bgs to 9 ft-bgs, directly below the suspected
former UST excavation basin and a former dispenser; and
 Two soil samples were collected at a depth of 5 ft-bgs to 6 ft-bgs, within two feet below the
existing heating oil UST.

3 Soil boring SB-8 was terminated at a depth of 1 ft-bgs due to encountering auger refusal.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 14
The following is a summary of the analytical results:
 Target SVOCs and/or VOCs were detected at concentrations that exceed the respective NCDEQ
IHS Unrestricted PSRGs in two (B-17 and B-18) of the eighteen near-surface soil samples.
 Target SVOCs and/or VOCs were detected at concentrations that exceed the respective NCDEQ
IHS Unrestricted PSRGs in the two sub-surface soil samples collected beneath the suspected
former UST excavation basin.
 Target SVOCs and/or VOCs were detected at concentrations that exceed the respective NCDEQ
IHS Unrestricted PSRGs in the one (B-18) of the two sub-surface soil samples collected beneath
the existing product line.
 Target VOCs were detected at concentrations that exceed the respective NCDEQ IHS Unrestricted
PSRGs in the two sub-surface soil samples (B-20 and B-21) collected beneath the depth of the
product line at the former dispenser islands.
 A target VOC was detected at a concentration that exceed the respective NCDEQ IHS Unrestricted
PSRGs in one (B-23) of the two sub-surface soil samples collected within two feet below the
bottom of the existing heating oil UST.
 Lead was not detected in the soil samples collected from the twenty soil borings at concentration
that exceeded the NCDEQ IHS Unrestricted PSRGs for lead.
Based on historical data and the limited soil assessment, it appears that a release of petroleum has
occurred from the former USTs located on the northeastern side of the retail store, the existing product
line, the former dispensers near East Main Street, and the existing heating oil UST. Near-surface soil
contamination is currently present at concentration that exceed the NCDEQ IHS Unrestricted PSRGS in the
vicinity of soil borings B-17 and B-18.
9.0 Sole Use Statement
All materials and information used for this project were obtained by S&ME. This report is provided for the
sole use of the Mainspring Conservation Trust and the North Carolina Department of Environmental
Quality for this project. Use of this report by any parties other than Mainspring Conservation Trust and
the North Carolina Department of Environmental will be at such party's sole risk. S&ME disclaims liability
for any use of or reliance on this report by third parties.
10.0 Limitations
The assessment described herein represents the environmental conditions of the subject property and
associated properties at the date the groundwater and soil samples were collected for laboratory analyses.
The assessment data does not represent the future environmental conditions of the property and should
not be construed in this manner.

Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

May 18, 2017 15
11.0 References
Comprehensive Site Assessment for the Release of Petroleum Product at the Simpson Soil Company Facility.
Alpha Environmental Sciences, Inc. January 26, 1999.
Guidelines for Assessment and Cleanup. NCDEQ Inactive Hazardous Sites Program. October 2015.
Guidelines for Initial Response and Abatement, Assessment, and Corrective Action for Non-UST Petroleum
Releases. NCDENR-DWM UST Section. July 1, 2012.
Guidelines for Assessment and Corrective Action for UST Releases. NCDENR-DWM UST Section. December
1, 2013.
Macon County Sewer – Hydrocarbon Contaminated Soil. McGill & Associates. September 1, 2010.
Notice of Violation. North Carolina Department of Environment and Natural Resources. October 22, 1998.
Phase I Environmental Site Assessment. S&ME, Inc. February 13, 2017.
Report of Environmental Services, S&ME, Inc. September 4, 2015.
Underground Storage Tank Closure Report for Simpson Oil Company. Alpha Environmental Sciences, Inc.
March 1999.
Work Plan for Limited Soil and Groundwater Assessment. S&ME, Inc. April 11, 2017.

Appendices

Appendix I –Figures
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JOB NO.
SCALE:
DATE:
DRAWN BY:CHECKED BY:
FIGURE NO.
44 BUCK SHOALS ROAD
ARDEN, NC. 2874
PH. 828-687-9080
FAX. [phone]
WWW.SMEINC.COM
DRAWING PATH:Q:\4341\2017\17-002 - FORMER SIMPSON OIL AND GAS COMPANY (JH DUNCAN)\Former Simpson Oil & Ga
s

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SITE VICINITY MAP
FORMER SIMPSON OIL AND GAS PROPERTY
FRANKLIN, NORTH CAROLINA 28734
AS SHOWN RDM BSK
4341 17-002 Ph. 02 FEBRUARY 2017 1
SOURCE:FRANKLIN, NC QUADRANGLE, 7.5-MINUTE SERIES, USGS T
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CORBIN KNOB, NC QUADRANGLE, 7.5-MINUTE SERIES, USG
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FORMERSIMPSON OIL FACILITY SITE
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JOB NO.
SCALE:
DATE:
DRAWN BY:CHECKED BY:
FIGURE NO.
44 BUCK SHOALS ROAD
ARDEN, NC. 2874
PH. 828-687-9080
FAX. [phone]
WWW.SMEINC.COM
DRAWING PATH:Q:\4341\2017\17-002 - FORMER SIMPSON OIL AND GAS COMPANY (JH DUNCAN)\Former Simpson Oil & Ga
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USGS TOPOGRAPHIC MAP
FORMER SIMPSON OIL AND GAS PROPERTY
FRANKLIN, NORTH CAROLINA 28734
AS SHOWN RDM BSK
4341 17-002 Ph. 02 FEBRUARY 2017 2
SOURCE:FRANKLIN, NC QUADRANGLE, 7.5-MINUTE SERIES, USGS T
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CORBIN KNOB, NC QUADRANGLE, 7.5-MINUTE SERIES, USG
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FORMERSIMPSON OIL FACILITY SITE
Ð"C
Ð"CÐ"I
Ð"I
Ð"I
Ð"I
Ð"I
Ð"I
Ð"I
Ð"I Ð"I
Ð!G Ð!G
Ð!G
Ð!G
Ð!G
Ð!G
"Ð I
"Ð I
Ð"I
"Ð I
"Ð I
Ð"I
!A$
Ð"I
Former 2,000 gal.gasoline UST
Former dispensersFormer dispensersExisting product lines
Former ASTs
Former 550 gal.diesel UST
Heating oil UST
Concrete Slab
Former dispenser
Concrete Slab
SuspectedExisting USTs
E M A I N S T
E M A I N S T
BIG BEAR LN
N E M A I N S T
N E M A I N S T
B-22
B-23B-1
B-4
B-5
B-2
B-6
B-3
B-7
B-8 B-9
B-16 B-17
B-18
B-19
B-20
B-21
B-11
B-13
B-15
B-10
B-12
B-14
MW-1
B-12B
S I T E B A S E M A P
F O R M E R S I M P S O N G A S A N D O I L P R O P E R T Y
F R A N K L I N , M A C O N C O U N T Y , N O R T H C A R O L I N A
3
4 3 4 1 -1 7 -0 0 2
D D H
5 -5 -2 0 1 7
FIGURE NO.
S C A L E :
P R O J E C T N O .
D A T E :
D R A W N B Y :
REFERENCE:2015 AERIAL PHOTOGRAPHGIS DATA LAYERS WERE OBTAINED FROM NC ONEMAP AND MACON COUNTY. SITE FEATURES (EXCLUDING SAMPLE LOCATIONS) AND PROPERTY BOUNDARIESARE BASED OFF OF PRELIMINARY SURVEY DATA PROVIDED BY SMOKEY MOUNTAIN LAND SURVEYING, PA. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY.ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
³
1 " = 3 0 '
Q :\4 3 4 1 \1 7 \0 0 2 S i m p s o n O i l \3 _s i t e m a p .m x d p l o t t e d b y D H o m a n s 0 5 -0 5 -2 0 1 7
!A$Monitoring Well
Ð"C Soil Sample- Heating Oil Tank
Ð"I Soil Sample- Near Surface
"Ð I Soil Sample- Near Surface Not Collected
Ð!G Soil Sample- Near Surface and Subsurface
Project Parcel
0 30 60
(IN FEET)
Ð"C
Ð"CÐ"I
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B-16@7-9 feet BGS1,2,4-Trimethylbenzene : 49 Benzene: 1.2 Ethylbenzene: 21 Naphthalene: 5.9 Xylenes, total: 110
B-22
B-1
B-4
B-5
B-2
B-6
B-3
B-7
B-8 B-9
B-19
B-15
B-14
B-12BB-23@ 5­6 feet BGS1,2,4-Trimethylbenzene: 9.0
B-17@0-2 feet BGS1-Methylnaphthalene: 25 Benzene: 3.8 Naphthalene: 4.1 @7-9 feet BGS1-Methylnaphthalene: 382­Methylnaphthalene: 54 1,2,4-Trimethylbenzene: 31 Benzene: 15 Ethylbenzene: 21 Naphthalene: 5.9
B-18@0-2 feet BGS1,2,4-Trimethylbenzene: 59 Ethylbenzene: 23 Xylenes, total: 140 @2-4 feet BGS1,2,4-Trimethylbenzene: 97 Benzene: 1.2 Ethylbenzene: 39 Naphthalene : 9.9 Xylenes, total : 230
B-20@2-4 feet BGS1,2,4-Trimethylbenzene: 55 Ethylbenzene: 12 Naphthalene: 8.9
B-21@2-4 feet BGS1,2,4-Trimethylbenzene: 28 Naphthalene: 4.4
MW-11-Methylnaphthalene: 130 2-Methylnaphthalene: 200Naphthalene: 4701,2,4-Trimethylbenzene: 720Benzene: 7,200Ethylbenzene: 1,500Isopropyl Ether: 3,200Isopropylbenzene (Cumene): 71 Methyl-tert-Butyl Ether: 1,500Naphthalene: 450n-Propylbenzene: 160 Xylenes, total: 1,600
E M A I N S T
E M A I N S T
BIG BEAR LN
N E M A I N S T
N E M A I N S T
G R O U N D W A T E R A N D S O I L Q U A L I T Y M A P
F O R M E R S I M P S O N G A S A N D O I L P R O P E R T Y
F R A N K L I N , M A C O N C O U N T Y , N O R T H C A R O L I N A
4
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D D H
5 -5 -2 0 1 7
FIGURE NO.
S C A L E :
P R O J E C T N O .
D A T E :
D R A W N B Y :
GIS DATA LAYERS WERE OBTAINED FROM NC ONEMAP AND MACON COUNTY. SITE FEATURES(EXCLUDING SAMPLE LOCATIONS) AND PROPERTY BOUNDARIES ARE BASED OFF OF PRELIMINARYSURVEY DATA PROVIDED BY SMOKEY MOUNTAIN LAND SURVEYING, PA. THIS MAP IS FORINFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEYARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
³
1 " = 3 0 '
Q :\4 3 4 1 \1 7 \0 0 2 S i m p s o n O i l \4 _f i n d i n g s .m x d p l o t t e d b y D H o m a n s 0 5 -0 5 -2 0 1 7
!A$Monitoring Well - Groundwater Sample
Ð"C Soil Sample- Heating Oil Tank
Ð"I Soil Sample- Near Surface
Ð!G Soil Sample- Near Surface and Subsurface
Project Parcel
0 30 60
(IN FEET)
SOIL SAMPLES:Soil sample analytical results shown exceed theNCDEQ IHSB Unrestricted PSRGs. Results areshown in mg/kg.
Bolded values exceed the Commercial /Industrial PSRGs
GROUNDWATER SAMPLES:Groundwater results shown exceed the 2LStandards. Results are shown in µg/L.
Bold values exceed the DWM ResidentialVapor Intrusion Groundwater Screening Level
Underlined values exceed the GCL

Appendix II – Additional Tables
Table 1
Well Construction and Groundwater Elevation Data
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002
Well ID Installation
Date
Well
Diameter
(inches)
Total Depth
(ft below TOC)
TOC Elevation1
(ft above datum)
Ground Surface
Elevation1
(ft above datum)
Top of Screen
Elevation
(ft above datum)
Bottom of Screen
Elevation
(ft above datum)
Date
Measured
Depth to Water
from TOC
(feet)
Groundwater
Elevation
(ft above datum)
MW-1 4-12-13 2 18 100.00 100.3 92.00 82.00 3/13/2014 12.18 87.82
Notes:
TOC = Top of Casing
ft = feet
1Assigned as 100.00 feet by S&ME
Table 2B
Summary of Groundwater Analytical Data
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002
6020
Date
Collected
Time
Collected
Sample
Depth
(ft bgs)
04/13/17 10:10 0-2 <0.076 <0.063 <0.051 <0.042 <0.046 <0.043 <0.049 <0.050 <0.056 <0.045 <0.063 <0.051 <0.052 15
04/13/17 10:05 0-2 <0.073 <0.061 <0.050 <0.041 <0.044 <0.042 <0.048 <0.049 <0.055 <0.044 <0.061 <0.050 <0.050 10
04/13/17 10:000 0-2 <0.073 <0.060 0.13 J 0.15 J 0.22 J 0.11 J 0.14 J 0.24 J <0.054 0.12 J <0.061 <0.049 0.21 J 13
04/13/17 9:55 0-2 <0.075 <0.062 <0.051 <0.042 <0.045 <0.043 <0.049 <0.050 <0.056 <0.045 <0.062 <0.050 <0.051 16
04/13/17 9:50 0-2 <0.078 <0.065 <0.053 <0.044 <0.047 <0.044 <0.051 <0.052 <0.058 <0.046 <0.065 <0.053 <0.054 14
04/13/17 9:45 0-2 <0.076 <0.063 <0.052 <0.043 <0.046 <0.043 <0.050 <0.050 <0.057 <0.045 <0.064 <0.051 <0.052 17
04/13/17 9:40 0-2 <0.079 <0.065 <0.053 <0.044 <0.047 <0.045 <0.051 <0.052 <0.059 <0.047 <0.066 <0.053 <0.054 13
04/13/17 11:45 0-1 <0.097 <0.080 <0.066 <0.054 <0.058 <0.055 <0.063 <0.064 <0.072 <0.058 <0.081 <0.065 <0.066 29
04/13/17 9:30 0-2 <0.077 <0.064 <0.053 <0.043 <0.047 <0.044 <0.051 <0.051 <0.058 <0.046 <0.065 <0.052 <0.053 19
04/13/17 14:40 0-2 <0.073 <0.061 <0.050 <0.041 <0.044 <0.042 <0.048 <0.048 <0.054 <0.043 <0.061 <0.049 <0.050 12
04/13/17 10:20 0-2 <0.071 <0.059 <0.048 <0.040 <0.043 <0.040 <0.046 <0.047 <0.053 <0.042 <0.059 <0.048 <0.049 12
04/13/17 10:25 0-2 <0.080 <0.066 <0.054 <0.045 <0.048 <0.045 <0.052 <0.053 <0.059 <0.047 <0.066 <0.054 <0.055 15
04/13/17 9:15 0-2 <0.072 <0.060 <0.049 <0.041 <0.044 <0.041 <0.047 <0.048 <0.054 <0.043 <0.060 <0.049 <0.050 17
04/13/17 9:20 7-9 1.1 2.1 <0.060 <0.050 <0.054 <0.051 <0.058 <0.059 <0.066 <0.053 2.4 0.12 J <0.061 5.6
04/13/17 9:00 0-2 25 32 <0.52 <0.43 <0.46 <0.43 <0.50 <0.50 9.1 <0.45 8.7 12 4.7 5.4
04/13/17 9:05 7-9 38 54 <0.58 <0.48 <0.51 <0.48 <0.55 <0.56 11 <0.51 17 16 4.8 5.6
04/13/17 8:40 0-2 0.34 J 0.65 <0.050 <0.042 <0.045 <0.042 <0.048 <0.049 <0.055 <0.044 0.51 0.16 J <0.051 5.3
04/13/17 8:40 2-4 4.3 6.6 <0.057 <0.047 <0.050 <0.047 <0.055 <0.055 0.33 J <0.050 6.6 0.58 <0.057 6.2
04/13/17 8:35 0-2 <0.085 <0.071 <0.058 <0.048 <0.051 <0.048 <0.056 <0.056 <0.063 <0.051 <0.071 <0.057 <0.059 0.46
04/13/17 8:35 2-4 <0.088 0.17 J <0.060 <0.050 <0.053 <0.050 <0.058 <0.059 <0.066 <0.053 0.13 J <0.060 <0.061 6.2
04/13/17 8:15 0-2 1.1 2.0 <0.056 <0.047 <0.050 <0.047 <0.054 <0.055 <0.062 <0.049 1.5 <0.056 <0.057 9.9
04/13/17 8:15 2-4 11 24 <0.054 <0.044 <0.048 <0.045 <0.052 <0.052 0.18 J <0.047 24 0.22 J 0.11 J 7.6
04/13/17 8:20 0-2 <0.078 <0.064 <0.053 <0.044 <0.047 <0.044 <0.051 <0.051 <0.058 <0.046 <0.065 <0.052 <0.053 6.3
04/13/17 8:20 2-4 2.0 4.2 <0.056 <0.046 <0.050 <0.047 <0.054 <0.055 <0.062 <0.049 2.1 <0.056 <0.057 6.4
04/13/17 10:50 5-6 <0.074 <0.062 <0.050 <0.042 <0.045 <0.042 <0.049 <0.049 0.21 J <0.044 <0.062 0.28 J <0.051 7.1
04/13/17 10:40 5-6 9.0 13 <0.052 <0.043 <0.046 <0.043 <0.050 <0.050 2.3 <0.045 3.3 3.4 <0.052 8.8
04/13/17 ---0-2 0.22 J 0.42 <0.049 <0.041 <0.044 <0.041 <0.048 <0.048 <0.054 <0.043 0.32 J <0.049 <0.050 4.7
0.055 1.6 0.18 0.059 0.6 7,800 18 330 56 2 0.21 68 220 270
18 48 0.16 0.016 0.16 NSE 16 480 480 0.16 3.8 NSE 360 400
73 600 2.9 0.29 0.29 NSE 290 600 600 2.9 17 NSE 4,600 800
Relative Percent Difference (RPD)42.9%43.0%N/A N/A N/A N/A N/A N/A N/A N/A 45.8%106.2%N/A 12.0%
Notes:
Analytes from the method suite that are not shown were not detected.Value Concentration exceeds the Laboratory Method Reporting Limit
Data presented in milligrams per kilograms (mg/kg)Value Concentration exceeds the respective Protection of Groundwater PSRGs
ft bgs = Feet Below Ground Surface Value Concentration exceeds the Unrestricted PSRGs
NA = Not Analyzed Value Concentration exceeds the Commercial / Industrial PSRGs
N/A = Not Applicable
SOCs = Volatile Organic Compounds
SVOCs = Semi-Volatile Organic Compounds
PSRGs = Preliminary Soil Remediation Goals
NCDEQ IHSB = North Carolina Department of Environmental Quality Inactive Hazardous Sites Branch
Duplicate-1 was collected with soil sample B-18 (0-2)
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration.
L e a d
P y r e n e
P h e n a n t h r e n e
B-7 (0-2)
B-8 (0-1)
B-2 (0-2)
B-3 (0-2)
B-4 (0-2)
B-5 (0-2)
B-17 (7-9)
B-18 (0-2)
SVOCs by 8270
B-15 (0-2)
B-16 (7-9)
B-9 (0-2)
B-12B (0-2)
B-14 (0-2)
B-21 (0-2)
B-21 (2-4)
B-22 (5-6)
Analytical Method
Sample ID
Contaminant of Concern
B e n z o (a )a n t h r a c e n e
B-18 (2-4)
B-19 (0-2)
B-19 (2-4)
B-20 (0-2)
B-20 (2-4)
B-6 (0-2)
B-16 (0-2)
B-17 (0-2)
NCDEQ IHSB Industrial/Commercial PSRGs
B-1 (0-2)
N a p h t h a l e n e
NCDEQ IHSB Unrestricted PSRGs
1 -M e t h y l n a p h t h a l e n e
2 -M e t h y l n a p h t h a l e n e
C h r y s e n e
F l u o r e n e
I n d e n o
(1 ,2 ,3 -c d )p y r e n e
B-23 (5-6)
Duplicate-1
B e n z o (b )f l u o r a n t h e n e
F l u o r a n t h e n e
B e n z o (a )p y r e n e
B e n z o (g ,h ,i )p e r y l e n e
NCDEQ IHSB Protection of Groundwater PSRGs
Table 2B
Summary of Groundwater Analytical Data
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002
Date
Collected
Time
Collected
Sample
Depth
(ft bgs)
B r o m o m e t h a n e
04/13/17 10:10 0-2 <0.00049 <0.00048 <0.00031 0.16 <0.00037 <0.00025 <0.00051 <0.00026 <0.00038 <0.00058 0.011 <0.00020 <0.00020 <0.00033 <0.00038 <0.00031 <0.00039 <0.00022 <0.00037 <0.0012
04/13/17 10:05 0-2 <0.00044 <0.00043 <0.00028 0.11 <0.00033 <0.00022 <0.00051 <0.00023 <0.00034 <0.00052 0.011 <0.00018 <0.00018 <0.00029 <0.00034 <0.00028 <0.00034 <0.00019 <0.00033 <0.0011
04/13/17 10:000 0-2 <0.00042 <0.00041 <0.00026 0.064 <0.00032 <0.00021 <0.00051 <0.00022 <0.00032 <0.00049 0.0074 <0.00017 <0.00017 <0.00028 <0.00032 <0.00026 <0.00033 <0.00018 <0.00031 <0.0010
04/13/17 9:55 0-2 <0.00045 <0.00045 <0.00029 0.16 <0.00035 <0.00023 <0.00051 <0.00024 <0.00035 <0.00054 0.011 <0.00019 <0.00019 <0.00030 <0.00035 <0.00029 <0.00036 <0.00020 <0.00034 <0.0011
04/13/17 9:50 0-2 <0.00045 <0.00045 <0.00028 0.23 <0.00034 <0.00023 <0.00051 <0.00024 <0.00035 <0.00053 0.010 <0.00019 <0.00019 <0.00030 <0.00035 <0.00029 <0.00036 <0.00020 <0.00034 <0.0011
04/13/17 9:45 0-2 0.0026 J <0.00042 <0.00027 0.18 <0.00032 0.0041 J <0.00051 <0.00023 <0.00033 <0.00050 <0.00031 <0.00018 <0.00018 <0.00028 <0.00033 <0.00027 <0.00034 <0.00019 0.011 0.015 J
04/13/17 9:40 0-2 <0.00045 <0.00044 <0.00028 0.055 J <0.00034 <0.00022 <0.00051 <0.00024 <0.00035 <0.00053 0.011 <0.00019 <0.00018 <0.00030 <0.00035 <0.00028 <0.00035 <0.00020 0.0028 J 0.0034 J
04/13/17 11:45 0-1 <0.00052 <0.00052 <0.00033 0.12 <0.00040 <0.00026 <0.00051 <0.00028 <0.00040 <0.00062 0.013 <0.00022 <0.00022 <0.00035 <0.00041 <0.00033 <0.00041 <0.00023 <0.00039 <0.0013
04/13/17 9:30 0-2 0.0046 J <0.00049 <0.00031 0.36 0.0056 0.0030 J 0.0049 J <0.00027 <0.00039 <0.00059 0.013 <0.00021 <0.00021 <0.00033 <0.00039 <0.00032 <0.00039 <0.00022 0.0063 J 0.020
04/13/17 14:40 0-2 <0.00032 <0.00031 0.015 0.11 <0.00024 <0.00016 <0.00051 <0.00017 <0.00025 <0.00038 0.0058 <0.00013 <0.00013 <0.00021 <0.00025 0.0026 J <0.00025 <0.00014 <0.00024 <0.00078
04/13/17 10:20 0-2 <0.00042 <0.00041 <0.00026 <0.0013 <0.00032 <0.00021 <0.00051 <0.00022 <0.00032 <0.00049 <0.00031 <0.00017 <0.00017 <0.00028 <0.00032 <0.00026 <0.00033 <0.00018 <0.00031 <0.0010
04/13/17 10:25 0-2 <0.00046 <0.00046 <0.00029 0.048 J <0.00035 <0.00023 <0.00051 <0.00025 <0.00036 <0.00055 0.011 <0.00019 <0.00019 <0.00031 <0.00036 <0.00029 <0.00037 <0.00021 <0.00035 <0.0011
04/13/17 9:15 0-2 <0.00039 <0.00038 <0.00024 0.17 <0.00029 <0.00019 <0.00051 <0.00021 <0.00030 <0.00046 <0.00028 <0.00016 <0.00016 <0.00026 <0.00030 <0.00024 <0.00030 <0.00017 0.0065 0.0051 J
04/13/17 9:20 7-9 49 15 0.36 <0.24 1.2 21 <0.00051 <0.065 2.2 0.49 J <0.067 0.22 J 5.9 1.5 7.8 0.78 0.49 <0.072 36 110
04/13/17 9:00 0-2 11 1.0 1.5 <0.23 3.8 5.4 <0.00051 0.41 0.72 <0.067 <0.064 1.3 4.1 2.1 1.8 1.9 <0.065 <0.069 1.5 11
04/13/17 9:05 7-9 31 3.3 3.8 <0.22 15 21 <0.00051 0.95 2.4 <0.064 <0.061 2.5 5.9 5.7 5.8 5.2 0.14 J <0.066 9.6 48
04/13/17 8:40 0-2 59 22 0.53 <0.21 0.18 J 23 <0.00051 <0.057 2.9 <0.062 <0.059 0.12 J 2.7 1.5 8.8 1.1 0.28 <0.064 25 140
04/13/17 8:40 2-4 97 31 0.71 <0.24 1.2 39 <0.00051 0.52 4.1 <0.071 <0.068 2.9 9.9 2.9 12 1.5 0.77 <0.073 76 230
04/13/17 8:35 0-2 0.023 0.0051 J <0.00030 0.088 0.0061 0.0068 <0.00051 0.0039 J <0.00037 <0.00057 0.0076 0.0036 J 0.0050 J <0.00032 0.0045 J <0.00030 <0.00038 <0.00021 <0.00036 0.0030 J
04/13/17 8:35 2-4 1.7 0.20 0.0065 0.071 0.25 LL 0.38 <0.00051 0.067 0.024 <0.00055 0.0079 0.067 0.18 0.027 0.068 0.0096 <0.00036 <0.00020 0.16 2.4
04/13/17 8:15 0-2 1.6 0.60 0.0073 0.042 J 0.064 0.41 <0.00051 <0.00023 0.033 <0.00052 <0.00032 <0.00018 0.22 0.017 0.10 0.010 <0.00035 <0.00019 0.43 0.66
04/13/17 8:15 2-4 55 15 0.50 <0.24 0.47 12 <0.00051 <0.066 1.6 <0.072 <0.068 <0.066 8.9 2.3 7.1 0.84 0.15 J <0.074 12 74
04/13/17 8:20 0-2 0.023 0.0062 <0.00029 0.24 <0.00035 0.0025 J <0.00051 <0.00025 <0.00036 <0.00055 0.0070 <0.00019 0.0025 J <0.00031 0.0040 J <0.00029 <0.00036 <0.00020 0.0028 J 0.0041 J
04/13/17 8:20 2-4 28 9.3 0.40 <0.21 0.33 1.8 <0.00051 <0.059 0.60 <0.064 <0.061 <0.059 4.4 2.3 3.1 0.71 <0.062 <0.066 0.53 6.0
04/13/17 10:50 5-6 <0.00040 <0.00039 0.011 <0.0013 <0.00030 0.0026 J <0.00051 <0.00021 0.025 <0.00047 0.0092 <0.00017 0.0076 J 0.0099 0.017 0.066 <0.00031 <0.00018 <0.00030 <0.00097
04/13/17 10:40 5-6 9.0 0.20 2.3 <0.0014 0.016 2.1 <0.00051 <0.00024 1.7 <0.00053 <0.00033 <0.00019 0.031 0.18 3.4 4.0 <0.00035 0.036 0.0099 0.34
04/13/17 ---0-2 25 8.5 0.21 J <0.21 <0.062 7.3 <0.00051 <0.058 1.0 <0.063 <0.060 <0.058 1.3 0.78 3.7 0.43 <0.061 <0.065 6.2 49
6.7 6.7 NSE 24 0.0073 8.1 NSE 0.32 1.3 0.17 0.023 0.085 0.21 2.4 NSE 2.2 0.92 1.7 5.5 6.1
11.6 156 NSE 12,200 1.2 5.8 1.36 440 268 40 57 14 3.8 108 NSE 145 867 183 818 116
48 182 NSE 100,000 5.1 25 6 1,880 268 260 640 210 17 108 NSE 145 867 183 818 260
Relative Percent Difference (RPD)81.0%88.5%86.5%N/A 97.5%103.6%N/A N/A 97.4%N/A N/A 69.7%70.0%63.2%81.6%87.6%128.4%N/A 120.5%96.3%
Notes:
Analytes from the method suite that are not shown were not detected.Value Concentration exceeds the Laboratory Method Reporting Limit
Data presented in milligrams per kilograms (mg/kg)Value Concentration exceeds the respective Protection of Groundwater PSRGs
ft bgs = Feet Below Ground Surface Value Concentration exceeds the Unrestricted PSRGs
NA = Not Analyzed Value Concentration exceeds the Commercial / Industrial PSRGs
N/A = Not Applicable
SOCs = Volatile Organic Compounds
SVOCs = Semi-Volatile Organic Compounds
PSRGs = Preliminary Soil Remediation Goals
NCDEQ IHSB = North Carolina Department of Environmental Quality Inactive Hazardous Sites Branch
Duplicate-1 was collected with soil sample B-18 (0-2)
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration.
Analytical Method VOCs by 8260
Sample ID
Contaminant of Concern
n -B u t y l b e n z e n e
n -P r o p y l b e n z e n e
4 -I s o p r o p y l t o l u e n e
A c e t o n e
B e n z e n e
E t h y l b e n z e n e
I s o p r o p y l E t h e r
I s o p r o p y l b e n z e n e
(C u m e n e )
s e c -B u t y l b e n z e n e
S t y r e n e
t e r t -B u t y l b e n z e n e
M e t h y l e n e C h l o r i d e
M e t h y l -t e r t -B u t y l E t h e r
N a p h t h a l e n e
1 ,2 ,4 -T r i m e t h y l b e n z e n e
1 ,3 ,5 -T r i m e t h y l b e n z e n e
T o l u e n e
X y l e n e s , t o t a l
B-16 (0-2)
B-2 (0-2)
B-3 (0-2)
B-4 (0-2)
B-5 (0-2)
B-6 (0-2)
B-7 (0-2)
B-8 (0-1)
B-9 (0-2)
B-12B (0-2)
B-14 (0-2)
B-15 (0-2)
B-1 (0-2)
M e t h y l B u t y l K e t o n e
(2 -H e x a n o n e )
B-22 (5-6)
B-16 (7-9)
B-17 (0-2)
B-17 (7-9)
B-18 (0-2)
B-18 (2-4)
B-19 (0-2)
B-19 (2-4)
B-20 (0-2)
B-20 (2-4)
B-21 (0-2)
B-21 (2-4)
B-23 (5-6)
Duplicate-1
NCDEQ IHSB Protection of Groundwater PSRGs
NCDEQ IHSB Unrestricted PSRGs
NCDEQ IHSB Industrial/Commercial PSRGs
Table 2B
Summary of Groundwater Analytical Data
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002
6020
Date
Collected
Time
Collected
04/13/17 16:25 130 200 7.0 J 470 8.6J 14 1.1 <6.6 720 86 7,200 1,500 3,200 71 <4.1 1,500 450 160 54 190 1,600
04/13/17 ---140 200 7.7 J 430 9.2J 22 1.3 <6.6 700 85 7,600 1,500 3,100 68 <4.1 1,400 410 150 52 190 1,500
04/12/17 11:00 <2.7 <2.5 <1.8 <2.7 <1.5 <1.0 1.4 0.58 J <0.054 <0.076 <0.048 <0.061 <0.050 <0.054 1.1 <0.042 <0.19 <0.087 <0.076 <0.044 <0.15
04/13/17 11:10 <2.7 <2.5 <1.8 <2.7 <1.5 <1.0 <0.061 <0.13 <0.054 <0.076 <0.048 <0.061 <0.050 <0.054 1.2 <0.042 <0.19 <0.087 <0.076 <0.044 <0.15
04/13/17 17:00 <2.6 <2.4 <1.7 <2.6 <1.5 <0.98 <0.061 <0.13 <0.054 <0.076 <0.048 <0.061 <0.050 <0.054 0.92 J <0.042 <0.19 <0.087 <0.076 <0.044 <0.15
04/13/17 17:35 NA NA NA NA NA NA NA <0.13 <0.054 <0.076 <0.048 <0.061 <0.050 <0.054 <0.083 <0.042 <0.19 <0.087 <0.076 <0.044 <0.15
04/13/17 17:35 NA NA NA NA NA NA NA <0.13 <0.054 <0.076 <0.048 <0.061 <0.050 <0.054 <0.083 <0.042 <0.19 <0.087 <0.076 <0.044 <0.15
04/13/17 17:30 NA NA NA NA NA NA NA <0.13 <0.054 <0.076 <0.048 <0.061 <0.050 <0.054 <0.083 <0.042 <0.19 <0.087 <0.076 <0.044 <0.15
1 30 300 6 200 30 15 70 400 400 1 600 70 70 5 20 6 70 70 600 500
1,000 12,500 990 6,000 410 30,000 15,000 70,000 28,500 25,000 5,000 84,500 70,000 25,000 5,000 20,000 6,000 30,000 8,500 260,000 85,500
NSE NSE NSE 34.8 NSE NSE NSE 7.19 5.8 NSE 15.9 34.9 1,390 177 942 4,500 34.8 NSE NSE 3,840 76.9
NSE NSE NSE 146 NSE NSE NSE 30.2 24.3 NSE 69.3 152 5,860 745 3,960 19,700 146 NSE NSE 16,100 323
Relative Percent Difference (RPD)7.4%0.0%9.5%8.9%6.7%44.4%16.7%0.0%2.8%1.2%5.4%0.0%3.2%4.3%0.0%6.9%9.3%6.5%3.8%0.0%6.5%
Notes:
Analytes from the method suite that are not shown were not detected.Value Concentration exceeds the Laboratory Method Detection Limits
Data presented in micrograms per liter (µg/L)Value Concentration exceeds the 2L Standards
NA = Not Analyzed Value Concentration exceeds the GCLs
NSE = No Standard Established Value Concentration exceeds the DWM Residential Vapor Intrusion Groundwater Screening Levels
VOCs = Volatile Organic Compounds Value Concentration exceeds the DWM Residential and Non-Residential Vapor Intrusion Groundwater Screening Levels
GWSL = Groundwater Screening Level
SVOCs = Semi-Volatile Organic Compounds
NCDEQ DWM = North Carolina Department of Environmental Quality, Division of Waste Management
Duplicate-2 was collected with groundwater sample MW-1
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration.
15A NCAC 2L .0202 (2L) Standards
NCDEQ DWM Residential Vapor Intrusion GWSL
Gross Contamination Levels (GCLs)
Equipment Blank-1 (Augers)
Duplicate-2
Trip Blank-1
Equipment Blank-3 (Hand Auger)
Equipment Blank-2 (Macro-Core)
T o l u e n e
X y l e n e s , t o t a l
MW-1
s e c -B u t y l b e n z e n e
VOCs by 8260SVOCs by 8270
M e t h y l -t e r t -B u t y l E t h e r
2 -M e t h y l n a p h t h a l e n e
F l u o r e n e
N a p h t h a l e n e
P h e n o l
L e a d
1 ,2 ,4 -T r i c h l o r o b e n z e n e
1 ,2 ,4 -T r i m e t h y l b e n z e n e
P h e n a n t h r e n e
NCDEQ DWM Non-Residential Vapor Intrusion GWSL
Analytical Method
Sample ID
Contaminant of Concern
1 -M e t h y l n a p h t h a l e n e
1 ,3 ,5 -T r i m e t h y l b e n z e n e
B e n z e n e
E t h y l b e n z e n e
I s o p r o p y l E t h e r
I s o p r o p y l b e n z e n e
(C u m e n e )
M e t h y l e n e C h l o r i d e
N a p h t h a l e n e
n -P r o p y l b e n z e n e
Field Blank
Trip Blank-2

Appendix III – Work Plan Approval Letter

State of North Carolina | Environmental Quality | Waste Management
1646 Mail Service Center | 217 West Jones Street | Raleigh, NC 27699-1646
919 707 8200 T

April 11, 2017
Sent Via Email

Mr. Benjamin Laseter
Mainspring Conservation Trust, Inc.
P.O. Box 1148
Franklin, North Carolina
[e-mail]

Subject: Work Plan Approval
Simpson Gas and Oil Property
544 East Main Street
Franklin, Macon County, North Carolina
Brownfields Project Number 20064-16-057

Dear Mr. Laseter:

The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received
and reviewed the Work Plan for Limited Soil and Groundwater Assessment dated April 4, 2017
and provided comments by e-mail on April 5, 2017. A revised Work Plan for Brownfields
Assessment dated April 11, 2017 was received and subsequently reviewed by DEQ. All comments
have been incorporated; therefore, the revised Work Plan for Limited Soil and Groundwater
Assessment is approved.

Be advised that this approval from the Brownfields Program does not waive any applicable
requirement to obtain any necessary permits, licenses, or certifications for the above listed
activities nor does it waive any requirement to comply with applicable law for such activities. If
you have any questions, please feel free to contact me at 704-235-2166, or via e-mail at
[e-mail].

Sincerely,
Jordan Thompson
Brownfields Project Manager

ec: David Loftis and Bradley Keyse, S&ME
Tracy Wahl, DEQ

Appendix IV – Well Construction Permit Approval Letter

Appendix V – Site Photographs

Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

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Location / Orientation 544 East Main Street / Looking West
Remarks Vacant building located on the subject property.

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Location / Orientation 544 East Main Street / Looking Northwest
Remarks Existing Product Line.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

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Location / Orientation 544 East Main Street
Remarks Geoprobe 7822DT

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Location / Orientation 544 East Main Street
Remarks Soil from Macro-Core sampler at MW-1.
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

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Location / Orientation 544 East Main Street
Remarks Soil from Macro-Core sampler at MW-1.

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Location / Orientation 544 East Main Street / Looking Southeast
Remarks Drilling of monitoring well MW-1
Limited Soil and Groundwater Assessment Report
Former Simpson Gas and Oil Property
Franklin, Macon County, North Carolina
S&ME Project No. 4341-17-002

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Location / Orientation 544 East Main Street / Looking North
Remarks Completed monitoring well MW-1

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Location / Orientation 544 East Main Street
Remarks View of the wood object located in boring B-11

Appendix VI – Well Construction Log and Record
Description
WITH MONITOR WELL CONSTRUCTION NOTES
DATE DRILLED:
PROJECT NAME:
DEPTH TO WATER:LATITUDE:
LONGITUDE:
DRILLING METHOD:
LOG OF SOIL BORING
Well
DEPTH (ft.)
PID (ppm)LITHOLOGY
TOC ELEVATION:
DRILLER:
LOGGED BY:
(ft.)
ELEVATION
Well
ConstructionDescription
44 Buck Shoals Road, Suite C-3
Arden, North Carolina 28704
NOTES:
0
-5
-10
-15
-20
0
-5
-10
-15
-20
Geoprobe/HSA
Former Simpson Gas & Oil
4/12/17
NM
12.18 ft.
SAEDACCO
B. Keyse
MW-1
59.1
146.4
645.3
497.2
Portland Grout
Sch. 40 PVC Casing
Bentonite
#2 Filter Sand
Sch. 40 0.010" SlottedPVC Screen
Gravel: ABC Stone; fill
Silty SAND: Brown; fill, with gravel
Silty SAND: Dark Brown; fill, petroleum odors
Sandy SILT: Dark Brownish Red; fill,
petroleum odors
moist
SAND: Dark Grayish Brown; fine to medium
grained, alluvium, petroleum odor, moist
very moist
wet
4
0
.
0
0
3
6
0
.
0
0
6
8
0
.
0
0
1
0
0
0
.
0
0
4
0
.
0
0
3
6
0
.
0
0
6
8
0
.
0
0
1
0
0
0
.
0
0
4
0
.
0
0
3
6
0
.
0
0
6
8
0
.
0
0
1
0
0
0
.
0
0
Brian Ewing
4240-B
SAEDACCO Inc
X
4-12-17 MW-1
544 East Main Street Franklin, NC 28734 Macon Coun, , ,
X
X
1
18
8
BORED
8 18 2 010 SCH-40 PVC
0 5 PORTLAND PORUED
7 18 FILTER SAND 2
0 18 gravel silt sand clay
Bentonite seal from 5 to 7
4/14/2017

Appendix VII – Soil Boring Logs
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-1
Silty SAND: Dark Brown; fill
Silty SAND: Brownish Red; fill 2.2
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-2
Gravel: ABC Stone; fill
Silty SAND: Brown; fill 3.1
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-3
Gravel: ABC Stone; fill
Silty SAND: Brownish Red; fill 1.5
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-4
Gravel: ABC Stone; fill
Silty SAND: Brown; fill 4.9
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-5
Silty SAND: Brownish Red; fill
3.8
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-6
Silty SAND: Reddish Brown; fill
24.8
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-7
Silty SAND: Reddish Brown; fill
4.5
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-8
Silty SAND: Reddish Tan; fill
Refusal at 1 ft-bgs
0.0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-9
Gravel: ABC Stone; fill
Silty SAND: Reddish Brown; fill, slight petroleum odor 15.4
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-12-B
Silty SAND: Light Brown; fill, with gravel
Silty SAND: Brown; fill, with rock fragments
NR
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-14
Gravel: ABC Stone; fill
SAND: Gray; fine to medium grained, fill, slight petroleum odor 6.3
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-15
Gravel: ABC Stone; fill
Silty SAND: Dark Brownish Red; fill, slight petroleum odor, staining 1.3
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-16
Silty SAND: Reddish Brown; fill
Silty SAND: Brownish Red; fill, petroleum odor
Silty SAND: Reddish Brown; fill, petroleum odor
Silty SAND: Reddish Brown; fill, petroleum odor, moist
SAND: Grayish Brown; alluvium, fine to medium grained, wet
528.4
332.6
0
.
0
1
8
7
.
5
3
7
5
.
0
5
6
2
.
5
7
5
0
.
0
0
.
0
1
8
7
.
5
3
7
5
.
0
5
6
2
.
5
7
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-17
Gravel: ABC Stone; fill
Silty SAND: Brown; fill, slight petroleum odor
Silty SAND: Dark Brownish Gray; fill, petroleum odor, staining
Sandy SILT: Brownish Red; fill, moist, petroleum odor
Silty SAND: Reddish Brown; fine to medium grained sand, fill, petroleum odor
18.8
331.3
1
0
.
0
1
3
2
.
5
2
5
5
.
0
3
7
7
.
5
5
0
0
.
0
1
0
.
0
1
3
2
.
5
2
5
5
.
0
3
7
7
.
5
5
0
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-18
Gravel: ABC Stone; fill
SAND: Brown; fill, fine to medium grained
Silty SAND: Brownish Red; fill, slight petroleum odor
Silty SAND: Brownish Red; fill, slight petroleum odor, staining
Silty SAND: Brownish Red; fill, petroleum odor
189.6
1042
1
0
0
.
0
7
0
0
.
0
1
3
0
0
.
0
1
9
0
0
.
0
2
5
0
0
.
0
1
0
0
.
0
7
0
0
.
0
1
3
0
0
.
0
1
9
0
0
.
0
2
5
0
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-19
Gravel: ABC Stone; fill
Silty SAND: Brownish Red; fill, slight petroleum odors
Silty SAND: Brownish Red; fill, petroleum odors, staining
Silty SAND: Brownish Red; fill, slight petroleum odors
34.9
399.3
2
0
.
0
1
4
0
.
0
2
6
0
.
0
3
8
0
.
0
5
0
0
.
0
2
0
.
0
1
4
0
.
0
2
6
0
.
0
3
8
0
.
0
5
0
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-20
Gravel: ABC Stone; fill, petroleum odor
Silty SAND: Reddish Brown; fill, petroleum odor 294.6
700.1
2
0
0
.
0
4
0
0
.
0
6
0
0
.
0
8
0
0
.
0
1
0
0
0
.
0
2
0
0
.
0
4
0
0
.
0
6
0
0
.
0
8
0
0
.
0
1
0
0
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-21
Gravel: ABC Stone; fill
Silty SAND: Reddish Brown; fill, with aggregrate
Silty SAND: Black and Red; fill, petroleum odor, staining
Silty SAND: Reddish Brown; fill, slight petroleum odor
164.0
515.6
1
0
0
.
0
3
2
5
.
0
5
5
0
.
0
7
7
5
.
0
1
0
0
0
.
0
1
0
0
.
0
3
2
5
.
0
5
5
0
.
0
7
7
5
.
0
1
0
0
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-22
Silty SAND: Brownish Orange; fill
Silty SAND: Brownish Orange; fill, petrolwum odor 29.7
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
0
.
0
1
2
.
5
2
5
.
0
3
7
.
5
5
0
.
0
ELEVATION
PROJECT NAME:LOGGED BY:
LATITUDE:
ELEVATION:LONGITUDE:
DRILLER:
LOG OF SOIL BORING
DEPTH
LITHOLOGY PIDSoil Description
PROJECT NUMBER:
44 Buck Shoals Road, Ste C-3
Arden, North Carolina 28704
(ppm)
DATE DRILLED:
DRILLING METHOD:
NOTES:
0
-5
-10
-15
0
5
10
15
B. Keyse
Hand Auger
Former Simpson Gas & Oil
4/12/17
NA
S&ME
NA
NA
4341-17-007
B-23
Silty SAND: Brownish Orange; fill
Silty SAND: Brownish Orange; fill, petroleum odor 76.5
0
.
0
2
5
.
0
5
0
.
0
7
5
.
0
1
0
0
.
0
0
.
0
2
5
.
0
5
0
.
0
7
5
.
0
1
0
0
.
0

Appendix VIII – Field Sampling Forms
Groundwater Sampling - Meter Calibration Form
Page 1
of 1
Time: 14:30
Unit:Reference:Reading:
Water Level Meter Feet (0.01 feet)NA NA
Submersible Pump NA NA NA
4.0 4.0
7.0 7.1
10.0 10.0
Temperature Degees Celcius
(0.1 °C)NA NA
100.0 100.0
1,000 999
Oxidation-Reduction Potential millivolts (1 mV)258 260
0.02 0.01
10.00 9.98
1,000 995
Name Signature Date
(1)Bradley Keyse 4/13/2017
(2)
Comments:
YSI / Professional Plus
Date of Calibration:
(MM/DD/YY)4/13/2017 4/13/2017Weather/Temperature:
Turbidity HF Scientific / MicroTPW
Nephelometric Turbidity Unit
(0.01 NTU ≤ 10.0 NTU,
0.1 NTU > 10.0 NTU and ≤ 100 NTU,
or 1 NTU >100 NTU)
Dissolved Oxygen milligrams per liter
(0.1 %)
Conductivity microSiemens per centimeter
(1 µS/cm)
Standard Unit
(0.1 s.u.)
Field Equipment, Meters, and Verifications
Equipment/Meter Make / Model
pH
Pegasus / Alexis
Heron / Water Tape
85
78
11.18 ft-TOC 2 inch
18.18 ft-TOC 1.1 Gal
7.00 feet 3.43 Gal
10 feet Stickup: -0.3 ft-GRD 5.71 Gal
Start Time:15:00 End Time:
On (sec):Off (sec):Pressure:psi
ft-TOC
feet 200 mL
ft-TOC
Gallons
mL/min
(Yes/No)
Field Parameters (Taken at time intervals ≥ 5 minutes and purge volumes ≥ 1 flow-through cell volume)
Time Volume Purged Flow Rate
Depth to
Water Temp pH Spec. Cond.
Dissolved
Oxygen ORP*Turbidity
(gal)(mL/min)(ft)(°C)(s.u.)(µS/cm)(mg/L)(mV)(NTU)
15:00 0.0 ------------------------
15:05 0.2 170 12.39 18.5 5.9 356 13.1 54 67.8
15:10 0.4 170 12.42 18.4 5.9 351 2.3 50 45.0
15:15 0.7 170 12.44 18.4 6.0 362 1.0 47 22.3
15:20 0.9 170 12.44 18.2 6.0 369 0.7 36 19.7
15:25 1.1 170 12.44 18.3 6.1 379 0.6 20 18.8
15:30 1.3 170 12.44 18.3 6.1 387 0.5 18 17.1
15:35 1.6 170 12.44 18.3 6.1 389 0.5 12 17.5
15:40 1.8 170 12.44 18.1 6.1 396 0.4 7 17.7
15:45 2.0 170 12.44 18.3 6.2 399 0.4 1 17.0
15:50 2.2 170 12.44 18.4 6.2 402 0.4 -4 14.8
15:55 2.5 170 12.44 18.3 6.2 404 0.3 -8 14.4
16:00 2.7 170 12.44 18.3 6.2 407 0.3 -10 12.3
16:05 2.9 170 12.44 18.2 6.2 408 0.3 -13 11.7
16:10 3.1 170 12.44 18.3 6.2 412 0.3 -15 10.9
16:15 3.4 170 12.44 18.2 6.2 413 0.3 -18 10.7
16:20 3.6 170 12.44 18.2 6.2 414 0.3 -20 10.5
16:25 3.8 170 12.44 18.2 6.2 417 0.3 -22 7.14
Final: 16:25 3.8 170 12.44 18.2 6.2 417 0.3 -22 7.1
Sample Method:16:25 16:35
Qty Container Qty Container
3 40mL VOAs
2 1L A
1 250mL P
Name Signature Date
(1)
(2)
Notes:
Form Revision Date:
Low Flow Groundwater Sampling Field Form
Project Name:Former Simpson Gas and Oil Property Purge Date:April 13, 2017
Source Well:MW-1 Sample Time:16:25
Locked?:Yes Weather:Sunny
Project Location:Franklin, North Carolina Purge Time: Minutes
Project Number:4341-17-002 Sample Date:April 13, 2017
Sampled By:Bradley Keyse Air Temp:° F
Flow Through Cell Serial No.:Pump Serial No.:Calibration Date:April 13, 2017
Total Well Depth:Water Volume
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Height of Water Column:3 * Well Volume
Screen Length:5 * Well Volume
Well Purging Information
Depth to Water:Well Diameter
Purge Method:Peristaltic Pump 16:25
(If Used)Bladder Pump Control Settings:
Pump Intake Depth from Top of Casing: 17.0
Water Column Above Pump Intake: 5.82 Flow Through Cell Vol:
DTW-TOC at 25% Drawdown of WC Above Pump: 12.64 Comments:
Comment
Final Volume Purged: 3.8 Used YSI Pro Plus
Final Volume Purge Rate: 170
Well Purged Dry?: No
Start Purging
Petroleum Odors
End of Purging
Bailer Sample Start Time:Sample End Time:
Analytical Data
Method Preservative Method Preservative
SVOCs 8270 Unpreserved
VOCs 8260 HCl
Metals 6020 (Total)HNO3
To convert ORP to Eh, add 205 mV to ORP.
Calibration: 4.04, 7.13, 10.01, 999 US/ cm, 260.2/257.6, 0.01, 9.98, 995.4
2/28/17 16:40
Bradley Keyse 4/13/17
Well ID
MW-1
S&ME Staff
Bradley Keyse
Drill Rig
Geoprobe 7822DT
Water Level at TOB (0.01 ft-BTOC)Land Surface Elev. (0.01 ft)
Unknown
Depth to Water (0.01 ft-BTOC)
Stickup Height - ft
TOC Relative to Ground -0.3 ft
-0.3 to 8.0
8.0 to 18.0
Top of Seal - 5.0 0.1 ft-bgs
Top of Filter Pack - 7.0 0.1 ft-bgs
-0.3 to 5.0
Top of Screen - 8.0 0.1 ft-bgs
5.0 to 7.0
Screened Interval -10.0 0.1 ft-bgs
7.0 to 18.0
Bottom of Screen - 18.0 0.1 ft-bgs
Bottom of Filter Pack - 18.0 0.1 ft-bgs
Cave In - 18.0 0.1 ft-bgs
Total Boring Depth - 18.0 0.1 ft-bgs
Form Revision Date:3/30/17 11:50 AM
TBD - To Be Determined
Notes:
Seal Interval (0.1 ft-bgs)
Filter Pack
Grout Interval (0.1 ft-bgs)
Development Volume (gal)
Development
Yes
For lithologic information
see attached boring log
15
BTOC - Below Top of Casing
Hollow Stem Auger
2' x 2' Concrete
Flush Vault (8" diam)
Seal Type
1-in Sch 40 PVC (0.010)
Quik-Grout®
2-in Sch 40 PVC
Casing Interval (0.1 ft-bgs)
Screen Type
Borehole Diameter (1 in)
8
Filter Pack Interval (0.1 ft-bgs)
Screen Interval (0.1 ft-bgs)
Grout Type
#2 Silica Sand
3/8 in. Holeplug®
Pad Type
Protective Casing
Casing Material
Depth Below Ground Surface (ft-bgs)
Well Construction Detail
Project Number
4341-17-007
Total Well Depth (0.1 ft-bgs)
18.0
Project Name
Former Simpson Gas and Oil Property
Unknown
12.50
Northing (0.1 ft)
55135.08
Date/Time
4/12/17 13:30
TOC Elev. (0.01 ft)
12.18 4/13/17 14:30 693887.2
SAEDACCO - Brian Ewing
Easting (0.1 ft)Date/Time
Installation Date
4/12/2017
County
Drilling Contractor
Drilling Method
Well Type / Use
City
Flush Monitor Well
Macon Franklin
License Number
4240B
Well Permit Number
WM0100403

Appendix IX – Analytical Laboratory Report

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
04/26/2017
S&ME, Inc. - Arden, NC
Bradley Keyse
44 Buck Shoals Rd. Suite C-3
Arden, NC 28704
Project: Former Simpson Gas & Oil Property
Lab Submittal Date: 04/17/2017
Prism Work Order: 7040298
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 207
Data Qualifiers Key Reference:
A Surrogate recovery below range due to sample matrix.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
LL Medium level analysis result below the RL. Low level analysis reported estimated above the calibration range.
M Matrix spike outside of the control limits.
SR Surrogate recovery outside the QC limits.
SR2 Re-analysis due to low surr. recovery resulted in similar recoveries. Matrix interference suspected. Initial result
reported.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 207
Sample Receipt Summary
04/26/2017
Prism Work Order: 7040298
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7040298-01 04/13/17B-1 (0-2)04/17/17Solid
7040298-02 04/13/17B-2 (0-2)04/17/17Solid
7040298-03 04/13/17B-3 (0-2)04/17/17Solid
7040298-04 04/13/17B-4 (0-2)04/17/17Solid
7040298-05 04/13/17B-5 (0-2)04/17/17Solid
7040298-06 04/13/17B-6 (0-2)04/17/17Solid
7040298-07 04/13/17B-7 (0-2)04/17/17Solid
7040298-08 04/13/17B-8 (0-1)04/17/17Solid
7040298-09 04/13/17B-9 (0-2)04/17/17Solid
7040298-10 04/13/17B-12B (0-2)04/17/17Solid
7040298-11 04/13/17B-14 (0-2)04/17/17Solid
7040298-12 04/13/17B-15 (0-2)04/17/17Solid
7040298-13 04/13/17B-16 (0-2)04/17/17Solid
7040298-14 04/13/17B-16 (7-9)04/17/17Solid
7040298-15 04/13/17B-17 (0-2)04/17/17Solid
7040298-16 04/13/17B-17 (7-9)04/17/17Solid
7040298-17 04/13/17B-18 (0-2)04/17/17Solid
7040298-18 04/13/17B-18 (2-4)04/17/17Solid
7040298-19 04/13/17B-19 (0-2)04/17/17Solid
7040298-20 04/13/17B-19 (2-4)04/17/17Solid
7040298-21 04/13/17B-20 (0-2)04/17/17Solid
7040298-22 04/13/17B-20 (2-4)04/17/17Solid
7040298-23 04/13/17B-21 (0-2)04/17/17Solid
7040298-24 04/13/17B-21 (2-4)04/17/17Solid
7040298-25 04/13/17B-22 (5-6)04/17/17Solid
7040298-26 04/13/17B-23 (5-6)04/17/17Solid
7040298-27 04/13/17Duplicate 1 04/17/17Solid
7040298-28 04/13/17Duplicate 2 04/17/17Water
7040298-29 04/13/17MW-1 04/17/17Water
7040298-30 04/12/17Equipment Blank 1 04/17/17Water
7040298-31 04/13/17Equipment Blank 2 04/17/17Water
7040298-32 04/13/17Equipment Blank 3 04/17/17Water
7040298-33 04/13/17Trip Blank 1 04/17/17Water
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 207
7040298-34 04/13/17Trip Blank 2 04/17/17Water
7040298-35 04/13/17Field Blank 04/17/17Water
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
15 mg/kg dry7040298-01 B-1 (0-2)Lead 6020B
0.16 mg/kg dry7040298-01 B-1 (0-2)Acetone 8260B
0.011 mg/kg dry7040298-01 B-1 (0-2)Methylene Chloride 8260B
10 mg/kg dry7040298-02 B-2 (0-2)Lead 6020B
0.11 mg/kg dry7040298-02 B-2 (0-2)Acetone 8260B
0.011 mg/kg dry7040298-02 B-2 (0-2)Methylene Chloride 8260B
0.13 J mg/kg dry7040298-03 B-3 (0-2)Benzo(a)anthracene 8270D
0.15 J mg/kg dry7040298-03 B-3 (0-2)Benzo(a)pyrene 8270D
0.22 J mg/kg dry7040298-03 B-3 (0-2)Benzo(b)fluoranthene 8270D
0.11 J mg/kg dry7040298-03 B-3 (0-2)Benzo(g,h,i)perylene 8270D
0.14 J mg/kg dry7040298-03 B-3 (0-2)Chrysene 8270D
0.24 J mg/kg dry7040298-03 B-3 (0-2)Fluoranthene 8270D
0.12 J mg/kg dry7040298-03 B-3 (0-2)Indeno(1,2,3-cd)pyrene 8270D
0.21 J mg/kg dry7040298-03 B-3 (0-2)Pyrene 8270D
13 mg/kg dry7040298-03 B-3 (0-2)Lead 6020B
0.064 mg/kg dry7040298-03 B-3 (0-2)Acetone 8260B
0.0074 mg/kg dry7040298-03 B-3 (0-2)Methylene Chloride 8260B
16 mg/kg dry7040298-04 B-4 (0-2)Lead 6020B
0.16 mg/kg dry7040298-04 B-4 (0-2)Acetone 8260B
0.011 mg/kg dry7040298-04 B-4 (0-2)Methylene Chloride 8260B
14 mg/kg dry7040298-05 B-5 (0-2)Lead 6020B
0.23 mg/kg dry7040298-05 B-5 (0-2)Acetone 8260B
0.010 mg/kg dry7040298-05 B-5 (0-2)Methylene Chloride 8260B
17 mg/kg dry7040298-06 B-6 (0-2)Lead 6020B
0.0026 J mg/kg dry7040298-06 B-6 (0-2)1,2,4-Trimethylbenzene 8260B
0.18 mg/kg dry7040298-06 B-6 (0-2)Acetone 8260B
0.0041 J mg/kg dry7040298-06 B-6 (0-2)Ethylbenzene 8260B
0.012 mg/kg dry7040298-06 B-6 (0-2)m,p-Xylenes 8260B
0.0032 J mg/kg dry7040298-06 B-6 (0-2)o-Xylene 8260B
0.011 mg/kg dry7040298-06 B-6 (0-2)Toluene 8260B
0.015 J mg/kg dry7040298-06 B-6 (0-2)Xylenes, total 8260B
13 mg/kg dry7040298-07 B-7 (0-2)Lead 6020B
0.055 J mg/kg dry7040298-07 B-7 (0-2)Acetone 8260B
0.0034 J mg/kg dry7040298-07 B-7 (0-2)m,p-Xylenes 8260B
0.011 mg/kg dry7040298-07 B-7 (0-2)Methylene Chloride 8260B
0.0028 J mg/kg dry7040298-07 B-7 (0-2)Toluene 8260B
0.0034 J mg/kg dry7040298-07 B-7 (0-2)Xylenes, total 8260B
29 mg/kg dry7040298-08 B-8 (0-1)Lead 6020B
0.12 mg/kg dry7040298-08 B-8 (0-1)Acetone 8260B
0.013 mg/kg dry7040298-08 B-8 (0-1)Methylene Chloride 8260B
19 mg/kg dry7040298-09 B-9 (0-2)Lead 6020B
0.0046 J mg/kg dry7040298-09 B-9 (0-2)1,2,4-Trimethylbenzene 8260B
0.36 mg/kg dry7040298-09 B-9 (0-2)Acetone 8260B
0.0056 mg/kg dry7040298-09 B-9 (0-2)Benzene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
0.0049 J mg/kg dry7040298-09 B-9 (0-2)Bromomethane 8260B
0.0030 J mg/kg dry7040298-09 B-9 (0-2)Ethylbenzene 8260B
0.014 mg/kg dry7040298-09 B-9 (0-2)m,p-Xylenes 8260B
0.013 mg/kg dry7040298-09 B-9 (0-2)Methylene Chloride 8260B
0.0063 J mg/kg dry7040298-09 B-9 (0-2)o-Xylene 8260B
0.0063 J mg/kg dry7040298-09 B-9 (0-2)Toluene 8260B
0.020 mg/kg dry7040298-09 B-9 (0-2)Xylenes, total 8260B
12 mg/kg dry7040298-10 B-12B (0-2)Lead 6020B
0.015 mg/kg dry7040298-10 B-12B (0-2)4-Isopropyltoluene 8260B
0.11 mg/kg dry7040298-10 B-12B (0-2)Acetone 8260B
0.0058 mg/kg dry7040298-10 B-12B (0-2)Methylene Chloride 8260B
0.0026 J mg/kg dry7040298-10 B-12B (0-2)sec-Butylbenzene 8260B
12 mg/kg dry7040298-11 B-14 (0-2)Lead 6020B
15 mg/kg dry7040298-12 B-15 (0-2)Lead 6020B
0.048 J mg/kg dry7040298-12 B-15 (0-2)Acetone 8260B
0.011 mg/kg dry7040298-12 B-15 (0-2)Methylene Chloride 8260B
17 mg/kg dry7040298-13 B-16 (0-2)Lead 6020B
0.17 mg/kg dry7040298-13 B-16 (0-2)Acetone 8260B
0.0051 J mg/kg dry7040298-13 B-16 (0-2)m,p-Xylenes 8260B
0.0065 mg/kg dry7040298-13 B-16 (0-2)Toluene 8260B
0.0051 J mg/kg dry7040298-13 B-16 (0-2)Xylenes, total 8260B
1.1 mg/kg dry7040298-14 B-16 (7-9)1-Methylnaphthalene 8270D
2.1 mg/kg dry7040298-14 B-16 (7-9)2-Methylnaphthalene 8270D
2.4 mg/kg dry7040298-14 B-16 (7-9)Naphthalene 8270D
0.12 J mg/kg dry7040298-14 B-16 (7-9)Phenanthrene 8270D
5.6 mg/kg dry7040298-14 B-16 (7-9)Lead 6020B
49 mg/kg dry7040298-14 B-16 (7-9)1,2,4-Trimethylbenzene 8260B
15 mg/kg dry7040298-14 B-16 (7-9)1,3,5-Trimethylbenzene 8260B
0.36 mg/kg dry7040298-14 B-16 (7-9)4-Isopropyltoluene 8260B
1.2 mg/kg dry7040298-14 B-16 (7-9)Benzene 8260B
21 mg/kg dry7040298-14 B-16 (7-9)Ethylbenzene 8260B
2.2 mg/kg dry7040298-14 B-16 (7-9)Isopropylbenzene (Cumene)8260B
81 mg/kg dry7040298-14 B-16 (7-9)m,p-Xylenes 8260B
0.49 J mg/kg dry7040298-14 B-16 (7-9)Methyl Butyl Ketone (2-Hexanone)8260B
0.22 J mg/kg dry7040298-14 B-16 (7-9)Methyl-tert-Butyl Ether 8260B
5.9 mg/kg dry7040298-14 B-16 (7-9)Naphthalene 8260B
1.5 mg/kg dry7040298-14 B-16 (7-9)n-Butylbenzene 8260B
7.8 mg/kg dry7040298-14 B-16 (7-9)n-Propylbenzene 8260B
32 mg/kg dry7040298-14 B-16 (7-9)o-Xylene 8260B
0.78 mg/kg dry7040298-14 B-16 (7-9)sec-Butylbenzene 8260B
0.49 mg/kg dry7040298-14 B-16 (7-9)Styrene 8260B
36 mg/kg dry7040298-14 B-16 (7-9)Toluene 8260B
110 mg/kg dry7040298-14 B-16 (7-9)Xylenes, total 8260B
25 mg/kg dry7040298-15 B-17 (0-2)1-Methylnaphthalene 8270D
32 mg/kg dry7040298-15 B-17 (0-2)2-Methylnaphthalene 8270D
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
9.1 mg/kg dry7040298-15 B-17 (0-2)Fluorene 8270D
8.7 mg/kg dry7040298-15 B-17 (0-2)Naphthalene 8270D
12 mg/kg dry7040298-15 B-17 (0-2)Phenanthrene 8270D
4.7 mg/kg dry7040298-15 B-17 (0-2)Pyrene 8270D
5.4 mg/kg dry7040298-15 B-17 (0-2)Lead 6020B
11 mg/kg dry7040298-15 B-17 (0-2)1,2,4-Trimethylbenzene 8260B
1.0 mg/kg dry7040298-15 B-17 (0-2)1,3,5-Trimethylbenzene 8260B
1.5 mg/kg dry7040298-15 B-17 (0-2)4-Isopropyltoluene 8260B
3.8 mg/kg dry7040298-15 B-17 (0-2)Benzene 8260B
5.4 mg/kg dry7040298-15 B-17 (0-2)Ethylbenzene 8260B
0.41 mg/kg dry7040298-15 B-17 (0-2)Isopropyl Ether 8260B
0.72 mg/kg dry7040298-15 B-17 (0-2)Isopropylbenzene (Cumene)8260B
9.8 mg/kg dry7040298-15 B-17 (0-2)m,p-Xylenes 8260B
1.3 mg/kg dry7040298-15 B-17 (0-2)Methyl-tert-Butyl Ether 8260B
4.1 mg/kg dry7040298-15 B-17 (0-2)Naphthalene 8260B
2.1 mg/kg dry7040298-15 B-17 (0-2)n-Butylbenzene 8260B
1.8 mg/kg dry7040298-15 B-17 (0-2)n-Propylbenzene 8260B
0.88 mg/kg dry7040298-15 B-17 (0-2)o-Xylene 8260B
1.9 mg/kg dry7040298-15 B-17 (0-2)sec-Butylbenzene 8260B
1.5 mg/kg dry7040298-15 B-17 (0-2)Toluene 8260B
11 mg/kg dry7040298-15 B-17 (0-2)Xylenes, total 8260B
38 mg/kg dry7040298-16 B-17 (7-9)1-Methylnaphthalene 8270D
54 mg/kg dry7040298-16 B-17 (7-9)2-Methylnaphthalene 8270D
11 mg/kg dry7040298-16 B-17 (7-9)Fluorene 8270D
17 mg/kg dry7040298-16 B-17 (7-9)Naphthalene 8270D
16 mg/kg dry7040298-16 B-17 (7-9)Phenanthrene 8270D
4.8 mg/kg dry7040298-16 B-17 (7-9)Pyrene 8270D
5.6 mg/kg dry7040298-16 B-17 (7-9)Lead 6020B
31 mg/kg dry7040298-16 B-17 (7-9)1,2,4-Trimethylbenzene 8260B
3.3 mg/kg dry7040298-16 B-17 (7-9)1,3,5-Trimethylbenzene 8260B
3.8 mg/kg dry7040298-16 B-17 (7-9)4-Isopropyltoluene 8260B
15 mg/kg dry7040298-16 B-17 (7-9)Benzene 8260B
21 mg/kg dry7040298-16 B-17 (7-9)Ethylbenzene 8260B
0.95 mg/kg dry7040298-16 B-17 (7-9)Isopropyl Ether 8260B
2.4 mg/kg dry7040298-16 B-17 (7-9)Isopropylbenzene (Cumene)8260B
43 mg/kg dry7040298-16 B-17 (7-9)m,p-Xylenes 8260B
2.5 mg/kg dry7040298-16 B-17 (7-9)Methyl-tert-Butyl Ether 8260B
5.9 mg/kg dry7040298-16 B-17 (7-9)Naphthalene 8260B
5.7 mg/kg dry7040298-16 B-17 (7-9)n-Butylbenzene 8260B
5.8 mg/kg dry7040298-16 B-17 (7-9)n-Propylbenzene 8260B
5.2 mg/kg dry7040298-16 B-17 (7-9)o-Xylene 8260B
5.2 mg/kg dry7040298-16 B-17 (7-9)sec-Butylbenzene 8260B
0.14 J mg/kg dry7040298-16 B-17 (7-9)Styrene 8260B
9.6 mg/kg dry7040298-16 B-17 (7-9)Toluene 8260B
48 mg/kg dry7040298-16 B-17 (7-9)Xylenes, total 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
0.34 J mg/kg dry7040298-17 B-18 (0-2)1-Methylnaphthalene 8270D
0.65 mg/kg dry7040298-17 B-18 (0-2)2-Methylnaphthalene 8270D
0.51 mg/kg dry7040298-17 B-18 (0-2)Naphthalene 8270D
0.16 J mg/kg dry7040298-17 B-18 (0-2)Phenanthrene 8270D
5.3 mg/kg dry7040298-17 B-18 (0-2)Lead 6020B
59 mg/kg dry7040298-17 B-18 (0-2)1,2,4-Trimethylbenzene 8260B
22 mg/kg dry7040298-17 B-18 (0-2)1,3,5-Trimethylbenzene 8260B
0.53 mg/kg dry7040298-17 B-18 (0-2)4-Isopropyltoluene 8260B
0.18 J mg/kg dry7040298-17 B-18 (0-2)Benzene 8260B
23 mg/kg dry7040298-17 B-18 (0-2)Ethylbenzene 8260B
2.9 mg/kg dry7040298-17 B-18 (0-2)Isopropylbenzene (Cumene)8260B
98 mg/kg dry7040298-17 B-18 (0-2)m,p-Xylenes 8260B
0.12 J mg/kg dry7040298-17 B-18 (0-2)Methyl-tert-Butyl Ether 8260B
2.7 mg/kg dry7040298-17 B-18 (0-2)Naphthalene 8260B
1.5 mg/kg dry7040298-17 B-18 (0-2)n-Butylbenzene 8260B
8.8 mg/kg dry7040298-17 B-18 (0-2)n-Propylbenzene 8260B
38 mg/kg dry7040298-17 B-18 (0-2)o-Xylene 8260B
1.1 mg/kg dry7040298-17 B-18 (0-2)sec-Butylbenzene 8260B
0.28 mg/kg dry7040298-17 B-18 (0-2)Styrene 8260B
25 mg/kg dry7040298-17 B-18 (0-2)Toluene 8260B
140 mg/kg dry7040298-17 B-18 (0-2)Xylenes, total 8260B
4.3 mg/kg dry7040298-18 B-18 (2-4)1-Methylnaphthalene 8270D
6.6 mg/kg dry7040298-18 B-18 (2-4)2-Methylnaphthalene 8270D
0.33 J mg/kg dry7040298-18 B-18 (2-4)Fluorene 8270D
6.6 mg/kg dry7040298-18 B-18 (2-4)Naphthalene 8270D
0.58 mg/kg dry7040298-18 B-18 (2-4)Phenanthrene 8270D
6.2 mg/kg dry7040298-18 B-18 (2-4)Lead 6020B
97 mg/kg dry7040298-18 B-18 (2-4)1,2,4-Trimethylbenzene 8260B
31 mg/kg dry7040298-18 B-18 (2-4)1,3,5-Trimethylbenzene 8260B
0.71 mg/kg dry7040298-18 B-18 (2-4)4-Isopropyltoluene 8260B
1.2 mg/kg dry7040298-18 B-18 (2-4)Benzene 8260B
39 mg/kg dry7040298-18 B-18 (2-4)Ethylbenzene 8260B
0.52 mg/kg dry7040298-18 B-18 (2-4)Isopropyl Ether 8260B
4.1 mg/kg dry7040298-18 B-18 (2-4)Isopropylbenzene (Cumene)8260B
160 mg/kg dry7040298-18 B-18 (2-4)m,p-Xylenes 8260B
2.9 mg/kg dry7040298-18 B-18 (2-4)Methyl-tert-Butyl Ether 8260B
9.9 mg/kg dry7040298-18 B-18 (2-4)Naphthalene 8260B
2.9 mg/kg dry7040298-18 B-18 (2-4)n-Butylbenzene 8260B
12 mg/kg dry7040298-18 B-18 (2-4)n-Propylbenzene 8260B
66 mg/kg dry7040298-18 B-18 (2-4)o-Xylene 8260B
1.5 mg/kg dry7040298-18 B-18 (2-4)sec-Butylbenzene 8260B
0.77 mg/kg dry7040298-18 B-18 (2-4)Styrene 8260B
76 mg/kg dry7040298-18 B-18 (2-4)Toluene 8260B
230 mg/kg dry7040298-18 B-18 (2-4)Xylenes, total 8260B
0.46 mg/kg dry7040298-19 B-19 (0-2)Lead 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
0.023 mg/kg dry7040298-19 B-19 (0-2)1,2,4-Trimethylbenzene 8260B
0.0051 J mg/kg dry7040298-19 B-19 (0-2)1,3,5-Trimethylbenzene 8260B
0.088 mg/kg dry7040298-19 B-19 (0-2)Acetone 8260B
0.0061 mg/kg dry7040298-19 B-19 (0-2)Benzene 8260B
0.0068 mg/kg dry7040298-19 B-19 (0-2)Ethylbenzene 8260B
0.0039 J mg/kg dry7040298-19 B-19 (0-2)Isopropyl Ether 8260B
0.0030 J mg/kg dry7040298-19 B-19 (0-2)m,p-Xylenes 8260B
0.0076 mg/kg dry7040298-19 B-19 (0-2)Methylene Chloride 8260B
0.0036 J mg/kg dry7040298-19 B-19 (0-2)Methyl-tert-Butyl Ether 8260B
0.0050 J mg/kg dry7040298-19 B-19 (0-2)Naphthalene 8260B
0.0045 J mg/kg dry7040298-19 B-19 (0-2)n-Propylbenzene 8260B
0.0030 J mg/kg dry7040298-19 B-19 (0-2)Xylenes, total 8260B
0.17 J mg/kg dry7040298-20 B-19 (2-4)2-Methylnaphthalene 8270D
0.13 J mg/kg dry7040298-20 B-19 (2-4)Naphthalene 8270D
6.2 mg/kg dry7040298-20 B-19 (2-4)Lead 6020B
0.20 mg/kg dry7040298-20 B-19 (2-4)1,3,5-Trimethylbenzene 8260B
0.0065 mg/kg dry7040298-20 B-19 (2-4)4-Isopropyltoluene 8260B
0.071 mg/kg dry7040298-20 B-19 (2-4)Acetone 8260B
0.25 LL mg/kg dry7040298-20 B-19 (2-4)Benzene 8260B
0.067 mg/kg dry7040298-20 B-19 (2-4)Isopropyl Ether 8260B
0.024 mg/kg dry7040298-20 B-19 (2-4)Isopropylbenzene (Cumene)8260B
0.0079 mg/kg dry7040298-20 B-19 (2-4)Methylene Chloride 8260B
0.067 mg/kg dry7040298-20 B-19 (2-4)Methyl-tert-Butyl Ether 8260B
0.18 mg/kg dry7040298-20 B-19 (2-4)Naphthalene 8260B
0.027 mg/kg dry7040298-20 B-19 (2-4)n-Butylbenzene 8260B
0.068 mg/kg dry7040298-20 B-19 (2-4)n-Propylbenzene 8260B
0.0096 mg/kg dry7040298-20 B-19 (2-4)sec-Butylbenzene 8260B
0.16 mg/kg dry7040298-20 B-19 (2-4)Toluene 8260B
1.7 mg/kg dry7040298-20 B-19 (2-4)1,2,4-Trimethylbenzene 8260B
0.38 mg/kg dry7040298-20 B-19 (2-4)Ethylbenzene 8260B
1.6 mg/kg dry7040298-20 B-19 (2-4)m,p-Xylenes 8260B
0.85 mg/kg dry7040298-20 B-19 (2-4)o-Xylene 8260B
2.4 mg/kg dry7040298-20 B-19 (2-4)Xylenes, total 8260B
1.1 mg/kg dry7040298-21 B-20 (0-2)1-Methylnaphthalene 8270D
2.0 mg/kg dry7040298-21 B-20 (0-2)2-Methylnaphthalene 8270D
1.5 mg/kg dry7040298-21 B-20 (0-2)Naphthalene 8270D
9.9 mg/kg dry7040298-21 B-20 (0-2)Lead 6020B
0.0073 mg/kg dry7040298-21 B-20 (0-2)4-Isopropyltoluene 8260B
0.042 J mg/kg dry7040298-21 B-20 (0-2)Acetone 8260B
0.064 mg/kg dry7040298-21 B-20 (0-2)Benzene 8260B
0.033 mg/kg dry7040298-21 B-20 (0-2)Isopropylbenzene (Cumene)8260B
0.45 mg/kg dry7040298-21 B-20 (0-2)m,p-Xylenes 8260B
0.22 mg/kg dry7040298-21 B-20 (0-2)Naphthalene 8260B
0.017 mg/kg dry7040298-21 B-20 (0-2)n-Butylbenzene 8260B
0.10 mg/kg dry7040298-21 B-20 (0-2)n-Propylbenzene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
0.21 mg/kg dry7040298-21 B-20 (0-2)o-Xylene 8260B
0.010 mg/kg dry7040298-21 B-20 (0-2)sec-Butylbenzene 8260B
0.66 mg/kg dry7040298-21 B-20 (0-2)Xylenes, total 8260B
1.6 mg/kg dry7040298-21 B-20 (0-2)1,2,4-Trimethylbenzene 8260B
0.60 mg/kg dry7040298-21 B-20 (0-2)1,3,5-Trimethylbenzene 8260B
0.41 mg/kg dry7040298-21 B-20 (0-2)Ethylbenzene 8260B
0.43 mg/kg dry7040298-21 B-20 (0-2)Toluene 8260B
11 mg/kg dry7040298-22 B-20 (2-4)1-Methylnaphthalene 8270D
24 mg/kg dry7040298-22 B-20 (2-4)2-Methylnaphthalene 8270D
0.18 J mg/kg dry7040298-22 B-20 (2-4)Fluorene 8270D
24 mg/kg dry7040298-22 B-20 (2-4)Naphthalene 8270D
0.22 J mg/kg dry7040298-22 B-20 (2-4)Phenanthrene 8270D
0.11 J mg/kg dry7040298-22 B-20 (2-4)Pyrene 8270D
7.6 mg/kg dry7040298-22 B-20 (2-4)Lead 6020B
55 mg/kg dry7040298-22 B-20 (2-4)1,2,4-Trimethylbenzene 8260B
15 mg/kg dry7040298-22 B-20 (2-4)1,3,5-Trimethylbenzene 8260B
0.50 mg/kg dry7040298-22 B-20 (2-4)4-Isopropyltoluene 8260B
0.47 mg/kg dry7040298-22 B-20 (2-4)Benzene 8260B
12 mg/kg dry7040298-22 B-20 (2-4)Ethylbenzene 8260B
1.6 mg/kg dry7040298-22 B-20 (2-4)Isopropylbenzene (Cumene)8260B
52 mg/kg dry7040298-22 B-20 (2-4)m,p-Xylenes 8260B
8.9 mg/kg dry7040298-22 B-20 (2-4)Naphthalene 8260B
2.3 mg/kg dry7040298-22 B-20 (2-4)n-Butylbenzene 8260B
7.1 mg/kg dry7040298-22 B-20 (2-4)n-Propylbenzene 8260B
22 mg/kg dry7040298-22 B-20 (2-4)o-Xylene 8260B
0.84 mg/kg dry7040298-22 B-20 (2-4)sec-Butylbenzene 8260B
0.15 J mg/kg dry7040298-22 B-20 (2-4)Styrene 8260B
12 mg/kg dry7040298-22 B-20 (2-4)Toluene 8260B
74 mg/kg dry7040298-22 B-20 (2-4)Xylenes, total 8260B
6.3 mg/kg dry7040298-23 B-21 (0-2)Lead 6020B
0.023 mg/kg dry7040298-23 B-21 (0-2)1,2,4-Trimethylbenzene 8260B
0.0062 mg/kg dry7040298-23 B-21 (0-2)1,3,5-Trimethylbenzene 8260B
0.24 mg/kg dry7040298-23 B-21 (0-2)Acetone 8260B
0.0025 J mg/kg dry7040298-23 B-21 (0-2)Ethylbenzene 8260B
0.0041 J mg/kg dry7040298-23 B-21 (0-2)m,p-Xylenes 8260B
0.0070 mg/kg dry7040298-23 B-21 (0-2)Methylene Chloride 8260B
0.0025 J mg/kg dry7040298-23 B-21 (0-2)Naphthalene 8260B
0.0040 J mg/kg dry7040298-23 B-21 (0-2)n-Propylbenzene 8260B
0.0028 J mg/kg dry7040298-23 B-21 (0-2)Toluene 8260B
0.0041 J mg/kg dry7040298-23 B-21 (0-2)Xylenes, total 8260B
2.0 mg/kg dry7040298-24 B-21 (2-4)1-Methylnaphthalene 8270D
4.2 mg/kg dry7040298-24 B-21 (2-4)2-Methylnaphthalene 8270D
2.1 mg/kg dry7040298-24 B-21 (2-4)Naphthalene 8270D
6.4 mg/kg dry7040298-24 B-21 (2-4)Lead 6020B
28 mg/kg dry7040298-24 B-21 (2-4)1,2,4-Trimethylbenzene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
9.3 mg/kg dry7040298-24 B-21 (2-4)1,3,5-Trimethylbenzene 8260B
0.40 mg/kg dry7040298-24 B-21 (2-4)4-Isopropyltoluene 8260B
0.33 mg/kg dry7040298-24 B-21 (2-4)Benzene 8260B
1.8 mg/kg dry7040298-24 B-21 (2-4)Ethylbenzene 8260B
0.60 mg/kg dry7040298-24 B-21 (2-4)Isopropylbenzene (Cumene)8260B
5.0 mg/kg dry7040298-24 B-21 (2-4)m,p-Xylenes 8260B
4.4 mg/kg dry7040298-24 B-21 (2-4)Naphthalene 8260B
2.3 mg/kg dry7040298-24 B-21 (2-4)n-Butylbenzene 8260B
3.1 mg/kg dry7040298-24 B-21 (2-4)n-Propylbenzene 8260B
1.0 mg/kg dry7040298-24 B-21 (2-4)o-Xylene 8260B
0.71 mg/kg dry7040298-24 B-21 (2-4)sec-Butylbenzene 8260B
0.53 mg/kg dry7040298-24 B-21 (2-4)Toluene 8260B
6.0 mg/kg dry7040298-24 B-21 (2-4)Xylenes, total 8260B
0.21 J mg/kg dry7040298-25 B-22 (5-6)Fluorene 8270D
0.28 J mg/kg dry7040298-25 B-22 (5-6)Phenanthrene 8270D
7.1 mg/kg dry7040298-25 B-22 (5-6)Lead 6020B
0.011 mg/kg dry7040298-25 B-22 (5-6)4-Isopropyltoluene 8260B
0.0026 J mg/kg dry7040298-25 B-22 (5-6)Ethylbenzene 8260B
0.025 mg/kg dry7040298-25 B-22 (5-6)Isopropylbenzene (Cumene)8260B
0.0092 mg/kg dry7040298-25 B-22 (5-6)Methylene Chloride 8260B
0.0076 J mg/kg dry7040298-25 B-22 (5-6)Naphthalene 8260B
0.0099 mg/kg dry7040298-25 B-22 (5-6)n-Butylbenzene 8260B
0.017 mg/kg dry7040298-25 B-22 (5-6)n-Propylbenzene 8260B
0.066 mg/kg dry7040298-25 B-22 (5-6)sec-Butylbenzene 8260B
9.0 mg/kg dry7040298-26 B-23 (5-6)1-Methylnaphthalene 8270D
13 mg/kg dry7040298-26 B-23 (5-6)2-Methylnaphthalene 8270D
2.3 mg/kg dry7040298-26 B-23 (5-6)Fluorene 8270D
3.3 mg/kg dry7040298-26 B-23 (5-6)Naphthalene 8270D
3.4 mg/kg dry7040298-26 B-23 (5-6)Phenanthrene 8270D
8.8 mg/kg dry7040298-26 B-23 (5-6)Lead 6020B
0.20 mg/kg dry7040298-26 B-23 (5-6)1,3,5-Trimethylbenzene 8260B
0.016 mg/kg dry7040298-26 B-23 (5-6)Benzene 8260B
0.17 mg/kg dry7040298-26 B-23 (5-6)m,p-Xylenes 8260B
0.031 mg/kg dry7040298-26 B-23 (5-6)Naphthalene 8260B
0.18 mg/kg dry7040298-26 B-23 (5-6)n-Butylbenzene 8260B
0.17 mg/kg dry7040298-26 B-23 (5-6)o-Xylene 8260B
0.036 mg/kg dry7040298-26 B-23 (5-6)tert-Butylbenzene 8260B
0.0099 mg/kg dry7040298-26 B-23 (5-6)Toluene 8260B
0.34 mg/kg dry7040298-26 B-23 (5-6)Xylenes, total 8260B
9.0 mg/kg dry7040298-26 B-23 (5-6)1,2,4-Trimethylbenzene 8260B
2.3 mg/kg dry7040298-26 B-23 (5-6)4-Isopropyltoluene 8260B
2.1 mg/kg dry7040298-26 B-23 (5-6)Ethylbenzene 8260B
1.7 mg/kg dry7040298-26 B-23 (5-6)Isopropylbenzene (Cumene)8260B
3.4 mg/kg dry7040298-26 B-23 (5-6)n-Propylbenzene 8260B
4.0 mg/kg dry7040298-26 B-23 (5-6)sec-Butylbenzene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
0.22 J mg/kg dry7040298-27 Duplicate 1 1-Methylnaphthalene 8270D
0.42 mg/kg dry7040298-27 Duplicate 1 2-Methylnaphthalene 8270D
0.32 J mg/kg dry7040298-27 Duplicate 1 Naphthalene 8270D
4.7 mg/kg dry7040298-27 Duplicate 1 Lead 6020B
25 mg/kg dry7040298-27 Duplicate 1 1,2,4-Trimethylbenzene 8260B
8.5 mg/kg dry7040298-27 Duplicate 1 1,3,5-Trimethylbenzene 8260B
0.21 J mg/kg dry7040298-27 Duplicate 1 4-Isopropyltoluene 8260B
7.3 mg/kg dry7040298-27 Duplicate 1 Ethylbenzene 8260B
1.0 mg/kg dry7040298-27 Duplicate 1 Isopropylbenzene (Cumene)8260B
35 mg/kg dry7040298-27 Duplicate 1 m,p-Xylenes 8260B
1.3 mg/kg dry7040298-27 Duplicate 1 Naphthalene 8260B
0.78 mg/kg dry7040298-27 Duplicate 1 n-Butylbenzene 8260B
3.7 mg/kg dry7040298-27 Duplicate 1 n-Propylbenzene 8260B
14 mg/kg dry7040298-27 Duplicate 1 o-Xylene 8260B
0.43 mg/kg dry7040298-27 Duplicate 1 sec-Butylbenzene 8260B
6.2 mg/kg dry7040298-27 Duplicate 1 Toluene 8260B
49 mg/kg dry7040298-27 Duplicate 1 Xylenes, total 8260B
140 ug/L7040298-28 Duplicate 2 1-Methylnaphthalene 8270D
200 ug/L7040298-28 Duplicate 2 2-Methylnaphthalene 8270D
7.7 J ug/L7040298-28 Duplicate 2 Fluorene 8270D
430 ug/L7040298-28 Duplicate 2 Naphthalene 8270D
9.4 J ug/L7040298-28 Duplicate 2 Phenanthrene 8270D
22 ug/L7040298-28 Duplicate 2 Phenol 8270D
1.3 ug/L7040298-28 Duplicate 2 Lead 6020B
700 ug/L7040298-28 Duplicate 2 1,2,4-Trimethylbenzene 8260B
85 ug/L7040298-28 Duplicate 2 1,3,5-Trimethylbenzene 8260B
7600 ug/L7040298-28 Duplicate 2 Benzene 8260B
1500 ug/L7040298-28 Duplicate 2 Ethylbenzene 8260B
3100 ug/L7040298-28 Duplicate 2 Isopropyl Ether 8260B
68 ug/L7040298-28 Duplicate 2 Isopropylbenzene (Cumene)8260B
1400 ug/L7040298-28 Duplicate 2 m,p-Xylenes 8260B
1400 ug/L7040298-28 Duplicate 2 Methyl-tert-Butyl Ether 8260B
410 ug/L7040298-28 Duplicate 2 Naphthalene 8260B
150 ug/L7040298-28 Duplicate 2 n-Propylbenzene 8260B
100 ug/L7040298-28 Duplicate 2 o-Xylene 8260B
52 ug/L7040298-28 Duplicate 2 sec-Butylbenzene 8260B
190 ug/L7040298-28 Duplicate 2 Toluene 8260B
1500 ug/L7040298-28 Duplicate 2 Xylenes, total 8260B
130 ug/L7040298-29 MW-1 1-Methylnaphthalene 8270D
200 ug/L7040298-29 MW-1 2-Methylnaphthalene 8270D
7.0 J ug/L7040298-29 MW-1 Fluorene 8270D
470 ug/L7040298-29 MW-1 Naphthalene 8270D
8.6 J ug/L7040298-29 MW-1 Phenanthrene 8270D
14 ug/L7040298-29 MW-1 Phenol 8270D
1.1 ug/L7040298-29 MW-1 Lead 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 207
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7040298
04/26/2017
Summary of Detections
720 ug/L7040298-29 MW-1 1,2,4-Trimethylbenzene 8260B
86 ug/L7040298-29 MW-1 1,3,5-Trimethylbenzene 8260B
7200 ug/L7040298-29 MW-1 Benzene 8260B
1500 ug/L7040298-29 MW-1 Ethylbenzene 8260B
3200 ug/L7040298-29 MW-1 Isopropyl Ether 8260B
71 ug/L7040298-29 MW-1 Isopropylbenzene (Cumene)8260B
1500 ug/L7040298-29 MW-1 m,p-Xylenes 8260B
1500 ug/L7040298-29 MW-1 Methyl-tert-Butyl Ether 8260B
450 ug/L7040298-29 MW-1 Naphthalene 8260B
160 ug/L7040298-29 MW-1 n-Propylbenzene 8260B
110 ug/L7040298-29 MW-1 o-Xylene 8260B
54 ug/L7040298-29 MW-1 sec-Butylbenzene 8260B
190 ug/L7040298-29 MW-1 Toluene 8260B
1600 ug/L7040298-29 MW-1 Xylenes, total 8260B
1.4 ug/L7040298-30 Equipment Blank 1 Lead 6020B
0.58 J ug/L7040298-30 Equipment Blank 1 1,2,4-Trichlorobenzene 8260B
1.1 ug/L7040298-30 Equipment Blank 1 Methylene Chloride 8260B
1.2 ug/L7040298-31 Equipment Blank 2 Methylene Chloride 8260B
0.92 J ug/L7040298-32 Equipment Blank 3 Methylene Chloride 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-1 (0-2)
Prism Sample ID: 7040298-01
Prism Work Order: 7040298
Time Collected: 04/13/17 10:10
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
82.4 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0611,2,4-Trichlorobenzene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0601,2-Dichlorobenzene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0551,3-Dichlorobenzene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0571,4-Dichlorobenzene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0761-Methylnaphthalene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0742,4,6-Trichlorophenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0762,4-Dichlorophenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0602,4-Dimethylphenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0552,4-Dinitrophenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0482,4-Dinitrotoluene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0522,6-Dinitrotoluene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0572-Chloronaphthalene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0562-Chlorophenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0632-Methylnaphthalene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0502-Methylphenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0712-Nitrophenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0773,3'-Dichlorobenzidine
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0483/4-Methylphenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0674-Bromophenyl phenyl ether
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0554-Chloro-3-methylphenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0474-Chloroaniline
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.0614-Nitrophenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.053Acenaphthene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.057Acenaphthylene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.063Anthracene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.052Azobenzene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.051Benzo(a)anthracene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.042Benzo(a)pyrene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.046Benzo(b)fluoranthene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.043Benzo(g,h,i)perylene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.051Benzo(k)fluoranthene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.033Benzoic Acid
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.052Benzyl alcohol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.068bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.055Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.067Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.058Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-1 (0-2)
Prism Sample ID: 7040298-01
Prism Work Order: 7040298
Time Collected: 04/13/17 10:10
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.056Butyl benzyl phthalate
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.049Chrysene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.060Dibenzofuran
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.054Diethyl phthalate
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.052Dimethyl phthalate
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.056Di-n-butyl phthalate
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.048Di-n-octyl phthalate
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.050Fluoranthene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.056Fluorene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.062Hexachlorobenzene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.070Hexachlorobutadiene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.070Hexachlorocyclopentadiene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.066Hexachloroethane
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.053Isophorone
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.063Naphthalene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.056Nitrobenzene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.060N-Nitrosodiphenylamine
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.046Pentachlorophenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.051Phenanthrene
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.058Phenol
BRL 8270D P7D027310.39 4/18/17 20:14 JMVmg/kg dry 0.052Pyrene
Surrogate Recovery Control Limits
39-13290 %2,4,6-Tribromophenol
44-11581 %2-Fluorobiphenyl
35-11575 %2-Fluorophenol
37-12271 %Nitrobenzene-d5
34-12175 %Phenol-d5
54-127106 %Terphenyl-d14
Total Metals
15 6020B P7D0257100.30 4/24/17 23:25 BGMmg/kg dry 0.057Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000531,1,1,2-Tetrachloroethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000311,1,1-Trichloroethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000431,1,2,2-Tetrachloroethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000571,1,2-Trichloroethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000281,1-Dichloroethylene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000351,1-Dichloropropylene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000361,2,3-Trichlorobenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000821,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-1 (0-2)
Prism Sample ID: 7040298-01
Prism Work Order: 7040298
Time Collected: 04/13/17 10:10
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000481,2,4-Trichlorobenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000491,2,4-Trimethylbenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000261,2-Dibromoethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000301,2-Dichlorobenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000381,2-Dichloroethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000401,2-Dichloropropane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000481,3,5-Trimethylbenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000421,3-Dichlorobenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000321,3-Dichloropropane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000332-Chlorotoluene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000384-Chlorotoluene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.000314-Isopropyltoluene
0.16 8260B P7D033710.064 4/20/17 17:32 ANGmg/kg dry 0.0016Acetone
BRL 8260B P7D033710.0038 4/20/17 17:32 ANGmg/kg dry 0.00037Benzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00053Bromobenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00035Bromochloromethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00036Bromodichloromethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00073Bromoform
BRL 8260B P7D033710.013 4/20/17 17:32 ANGmg/kg dry 0.00079Bromomethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00032Carbon Tetrachloride
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00034Chlorobenzene
BRL 8260B P7D033710.013 4/20/17 17:32 ANGmg/kg dry 0.00053Chloroethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00046Chloroform
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00043Chloromethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00027cis-1,2-Dichloroethylene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00029Dichlorodifluoromethane
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00025Ethylbenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00038Isopropylbenzene (Cumene)
BRL 8260B P7D033710.013 4/20/17 17:32 ANGmg/kg dry 0.00059m,p-Xylenes
BRL 8260B P7D033710.064 4/20/17 17:32 ANGmg/kg dry 0.00058Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D033710.13 4/20/17 17:32 ANGmg/kg dry 0.00058Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D033710.064 4/20/17 17:32 ANGmg/kg dry 0.00055Methyl Isobutyl Ketone
0.011 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00036Methylene Chloride
BRL 8260B P7D033710.013 4/20/17 17:32 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P7D033710.013 4/20/17 17:32 ANGmg/kg dry 0.00020Naphthalene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00033n-Butylbenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00038n-Propylbenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00026o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-1 (0-2)
Prism Sample ID: 7040298-01
Prism Work Order: 7040298
Time Collected: 04/13/17 10:10
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00031sec-Butylbenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00039Styrene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00022tert-Butylbenzene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00037Toluene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00038trans-1,2-Dichloroethylene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00034trans-1,3-Dichloropropylene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00041Trichloroethylene
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00041Trichlorofluoromethane
BRL 8260B P7D033710.032 4/20/17 17:32 ANGmg/kg dry 0.00088Vinyl acetate
BRL 8260B P7D033710.0064 4/20/17 17:32 ANGmg/kg dry 0.00031Vinyl chloride
BRL 8260B P7D033710.019 4/20/17 17:32 ANGmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12992 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-2 (0-2)
Prism Sample ID: 7040298-02
Prism Work Order: 7040298
Time Collected: 04/13/17 10:05
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
86.6 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0591,2,4-Trichlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0581,2-Dichlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0541,3-Dichlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0561,4-Dichlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0731-Methylnaphthalene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0712,4,6-Trichlorophenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0742,4-Dichlorophenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0582,4-Dimethylphenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0532,4-Dinitrophenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0462,4-Dinitrotoluene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0512,6-Dinitrotoluene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0552-Chloronaphthalene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0542-Chlorophenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0612-Methylnaphthalene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0492-Methylphenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0692-Nitrophenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0753,3'-Dichlorobenzidine
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0473/4-Methylphenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0574,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0654-Bromophenyl phenyl ether
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0534-Chloro-3-methylphenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0464-Chloroaniline
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0504-Chlorophenyl phenyl ether
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.0594-Nitrophenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.052Acenaphthene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.055Acenaphthylene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.061Anthracene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.050Azobenzene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.050Benzo(a)anthracene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.041Benzo(a)pyrene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.044Benzo(b)fluoranthene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.042Benzo(g,h,i)perylene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.050Benzo(k)fluoranthene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.032Benzoic Acid
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.050Benzyl alcohol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.066bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.054Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.065Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.057Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-2 (0-2)
Prism Sample ID: 7040298-02
Prism Work Order: 7040298
Time Collected: 04/13/17 10:05
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.054Butyl benzyl phthalate
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.048Chrysene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.046Dibenzo(a,h)anthracene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.058Dibenzofuran
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.053Diethyl phthalate
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.050Dimethyl phthalate
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.054Di-n-butyl phthalate
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.047Di-n-octyl phthalate
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.049Fluoranthene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.055Fluorene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.060Hexachlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.068Hexachlorobutadiene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.068Hexachlorocyclopentadiene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.064Hexachloroethane
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.044Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.052Isophorone
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.061Naphthalene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.054Nitrobenzene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.060N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.058N-Nitrosodiphenylamine
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.045Pentachlorophenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.050Phenanthrene
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.056Phenol
BRL 8270D P7D027310.38 4/18/17 20:36 JMVmg/kg dry 0.050Pyrene
Surrogate Recovery Control Limits
39-13283 %2,4,6-Tribromophenol
44-11574 %2-Fluorobiphenyl
35-11570 %2-Fluorophenol
37-12266 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-12796 %Terphenyl-d14
Total Metals
10 6020B P7D0257100.29 4/24/17 23:40 BGMmg/kg dry 0.054Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000471,1,1,2-Tetrachloroethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000281,1,1-Trichloroethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000391,1,2,2-Tetrachloroethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000511,1,2-Trichloroethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000731,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-2 (0-2)
Prism Sample ID: 7040298-02
Prism Work Order: 7040298
Time Collected: 04/13/17 10:05
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000431,2,4-Trichlorobenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000441,2,4-Trimethylbenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000341,2-Dichloroethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000431,3,5-Trimethylbenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000381,3-Dichlorobenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000291,3-Dichloropropane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000302-Chlorotoluene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000344-Chlorotoluene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.000284-Isopropyltoluene
0.11 8260B P7D033710.057 4/20/17 18:00 ANGmg/kg dry 0.0014Acetone
BRL 8260B P7D033710.0034 4/20/17 18:00 ANGmg/kg dry 0.00033Benzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00048Bromobenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00031Bromochloromethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00032Bromodichloromethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00065Bromoform
BRL 8260B P7D033710.011 4/20/17 18:00 ANGmg/kg dry 0.00071Bromomethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00030Chlorobenzene
BRL 8260B P7D033710.011 4/20/17 18:00 ANGmg/kg dry 0.00048Chloroethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00041Chloroform
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00038Chloromethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00026Dichlorodifluoromethane
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00022Ethylbenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00034Isopropylbenzene (Cumene)
BRL 8260B P7D033710.011 4/20/17 18:00 ANGmg/kg dry 0.00053m,p-Xylenes
BRL 8260B P7D033710.057 4/20/17 18:00 ANGmg/kg dry 0.00052Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D033710.11 4/20/17 18:00 ANGmg/kg dry 0.00052Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D033710.057 4/20/17 18:00 ANGmg/kg dry 0.00049Methyl Isobutyl Ketone
0.011 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00032Methylene Chloride
BRL 8260B P7D033710.011 4/20/17 18:00 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P7D033710.011 4/20/17 18:00 ANGmg/kg dry 0.00018Naphthalene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00029n-Butylbenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00034n-Propylbenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00023o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-2 (0-2)
Prism Sample ID: 7040298-02
Prism Work Order: 7040298
Time Collected: 04/13/17 10:05
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00028sec-Butylbenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00034Styrene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00033Toluene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00037Trichloroethylene
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00037Trichlorofluoromethane
BRL 8260B P7D033710.029 4/20/17 18:00 ANGmg/kg dry 0.00078Vinyl acetate
BRL 8260B P7D033710.0057 4/20/17 18:00 ANGmg/kg dry 0.00028Vinyl chloride
BRL 8260B P7D033710.017 4/20/17 18:00 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130111 %4-Bromofluorobenzene
84-123107 %Dibromofluoromethane
76-12992 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-3 (0-2)
Prism Sample ID: 7040298-03
Prism Work Order: 7040298
Time Collected: 04/13/17 10:00
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
87.6 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0591,2,4-Trichlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0571,2-Dichlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0531,3-Dichlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0551,4-Dichlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0731-Methylnaphthalene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0712,4,6-Trichlorophenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0732,4-Dichlorophenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0582,4-Dimethylphenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0532,4-Dinitrophenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0462,4-Dinitrotoluene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0502,6-Dinitrotoluene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0552-Chloronaphthalene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0532-Chlorophenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0602-Methylnaphthalene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0482-Methylphenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0692-Nitrophenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0743,3'-Dichlorobenzidine
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0463/4-Methylphenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0574,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0654-Bromophenyl phenyl ether
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0534-Chloro-3-methylphenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0454-Chloroaniline
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0494-Chlorophenyl phenyl ether
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.0584-Nitrophenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.051Acenaphthene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.055Acenaphthylene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.061Anthracene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.050Azobenzene
0.13 8270D P7D027310.38 4/18/17 20:59 JMVJmg/kg dry 0.049Benzo(a)anthracene
0.15 8270D P7D027310.38 4/18/17 20:59 JMVJmg/kg dry 0.041Benzo(a)pyrene
0.22 8270D P7D027310.38 4/18/17 20:59 JMVJmg/kg dry 0.044Benzo(b)fluoranthene
0.11 8270D P7D027310.38 4/18/17 20:59 JMVJmg/kg dry 0.041Benzo(g,h,i)perylene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.049Benzo(k)fluoranthene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.032Benzoic Acid
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.050Benzyl alcohol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.065bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.053Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.064Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.056Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-3 (0-2)
Prism Sample ID: 7040298-03
Prism Work Order: 7040298
Time Collected: 04/13/17 10:00
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.054Butyl benzyl phthalate
0.14 8270D P7D027310.38 4/18/17 20:59 JMVJmg/kg dry 0.048Chrysene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.046Dibenzo(a,h)anthracene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.057Dibenzofuran
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.052Diethyl phthalate
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.050Dimethyl phthalate
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.054Di-n-butyl phthalate
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.046Di-n-octyl phthalate
0.24 8270D P7D027310.38 4/18/17 20:59 JMVJmg/kg dry 0.048Fluoranthene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.054Fluorene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.060Hexachlorobenzene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.068Hexachlorobutadiene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.067Hexachlorocyclopentadiene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.063Hexachloroethane
0.12 8270D P7D027310.38 4/18/17 20:59 JMVJmg/kg dry 0.043Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.051Isophorone
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.061Naphthalene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.054Nitrobenzene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.059N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.057N-Nitrosodiphenylamine
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.045Pentachlorophenol
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.049Phenanthrene
BRL 8270D P7D027310.38 4/18/17 20:59 JMVmg/kg dry 0.056Phenol
0.21 8270D P7D027310.38 4/18/17 20:59 JMVJmg/kg dry 0.050Pyrene
Surrogate Recovery Control Limits
39-13284 %2,4,6-Tribromophenol
44-11570 %2-Fluorobiphenyl
35-11566 %2-Fluorophenol
37-12261 %Nitrobenzene-d5
34-12166 %Phenol-d5
54-12792 %Terphenyl-d14
Total Metals
13 6020B P7D0257100.29 4/24/17 23:45 BGMmg/kg dry 0.054Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000451,1,1,2-Tetrachloroethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000261,1,1-Trichloroethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000371,1,2,2-Tetrachloroethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000481,1,2-Trichloroethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000151,1-Dichloroethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000241,1-Dichloroethylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000301,1-Dichloropropylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000311,2,3-Trichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-3 (0-2)
Prism Sample ID: 7040298-03
Prism Work Order: 7040298
Time Collected: 04/13/17 10:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000701,2,3-Trichloropropane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000411,2,4-Trichlorobenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000421,2,4-Trimethylbenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000221,2-Dibromoethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000261,2-Dichlorobenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000331,2-Dichloroethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000341,2-Dichloropropane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000411,3,5-Trimethylbenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000361,3-Dichlorobenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000271,3-Dichloropropane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000262,2-Dichloropropane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000282-Chlorotoluene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000334-Chlorotoluene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.000264-Isopropyltoluene
0.064 8260B P7D033710.055 4/20/17 18:27 ANGmg/kg dry 0.0013Acetone
BRL 8260B P7D033710.0033 4/20/17 18:27 ANGmg/kg dry 0.00032Benzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00046Bromobenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00030Bromochloromethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00030Bromodichloromethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00062Bromoform
BRL 8260B P7D033710.011 4/20/17 18:27 ANGmg/kg dry 0.00067Bromomethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00027Carbon Tetrachloride
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00029Chlorobenzene
BRL 8260B P7D033710.011 4/20/17 18:27 ANGmg/kg dry 0.00046Chloroethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00039Chloroform
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00037Chloromethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00023cis-1,2-Dichloroethylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00018cis-1,3-Dichloropropylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00022Dibromochloromethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00025Dichlorodifluoromethane
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00021Ethylbenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00022Isopropyl Ether
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00032Isopropylbenzene (Cumene)
BRL 8260B P7D033710.011 4/20/17 18:27 ANGmg/kg dry 0.00050m,p-Xylenes
BRL 8260B P7D033710.055 4/20/17 18:27 ANGmg/kg dry 0.00049Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D033710.11 4/20/17 18:27 ANGmg/kg dry 0.00049Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D033710.055 4/20/17 18:27 ANGmg/kg dry 0.00047Methyl Isobutyl Ketone
0.0074 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00031Methylene Chloride
BRL 8260B P7D033710.011 4/20/17 18:27 ANGmg/kg dry 0.00017Methyl-tert-Butyl Ether
BRL 8260B P7D033710.011 4/20/17 18:27 ANGmg/kg dry 0.00017Naphthalene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00028n-Butylbenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00032n-Propylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-3 (0-2)
Prism Sample ID: 7040298-03
Prism Work Order: 7040298
Time Collected: 04/13/17 10:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00022o-Xylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00026sec-Butylbenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00033Styrene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00018tert-Butylbenzene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00026Tetrachloroethylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00031Toluene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00033trans-1,2-Dichloroethylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00029trans-1,3-Dichloropropylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00035Trichloroethylene
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00035Trichlorofluoromethane
BRL 8260B P7D033710.027 4/20/17 18:27 ANGmg/kg dry 0.00075Vinyl acetate
BRL 8260B P7D033710.0055 4/20/17 18:27 ANGmg/kg dry 0.00026Vinyl chloride
BRL 8260B P7D033710.016 4/20/17 18:27 ANGmg/kg dry 0.0010Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-129109 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-4 (0-2)
Prism Sample ID: 7040298-04
Prism Work Order: 7040298
Time Collected: 04/13/17 09:55
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
83.2 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0611,2,4-Trichlorobenzene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0591,2-Dichlorobenzene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0551,3-Dichlorobenzene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0571,4-Dichlorobenzene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0751-Methylnaphthalene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0732,4,6-Trichlorophenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0752,4-Dichlorophenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0592,4-Dimethylphenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0542,4-Dinitrophenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0472,4-Dinitrotoluene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0522,6-Dinitrotoluene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0562-Chloronaphthalene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0552-Chlorophenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0622-Methylnaphthalene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0502-Methylphenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0712-Nitrophenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0773,3'-Dichlorobenzidine
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0483/4-Methylphenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0584,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0674-Bromophenyl phenyl ether
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0544-Chloro-3-methylphenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0474-Chloroaniline
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0504-Chlorophenyl phenyl ether
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.0604-Nitrophenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.053Acenaphthene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.056Acenaphthylene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.063Anthracene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.051Azobenzene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.051Benzo(a)anthracene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.042Benzo(a)pyrene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.045Benzo(b)fluoranthene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.043Benzo(g,h,i)perylene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.051Benzo(k)fluoranthene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.033Benzoic Acid
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.051Benzyl alcohol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.067bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.055Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.066Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.058Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-4 (0-2)
Prism Sample ID: 7040298-04
Prism Work Order: 7040298
Time Collected: 04/13/17 09:55
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.055Butyl benzyl phthalate
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.049Chrysene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.047Dibenzo(a,h)anthracene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.059Dibenzofuran
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.054Diethyl phthalate
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.051Dimethyl phthalate
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.055Di-n-butyl phthalate
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.048Di-n-octyl phthalate
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.050Fluoranthene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.056Fluorene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.062Hexachlorobenzene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.070Hexachlorobutadiene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.069Hexachlorocyclopentadiene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.065Hexachloroethane
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.053Isophorone
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.062Naphthalene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.055Nitrobenzene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.061N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.059N-Nitrosodiphenylamine
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.046Pentachlorophenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.050Phenanthrene
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.057Phenol
BRL 8270D P7D027310.39 4/18/17 21:22 JMVmg/kg dry 0.051Pyrene
Surrogate Recovery Control Limits
39-13287 %2,4,6-Tribromophenol
44-11572 %2-Fluorobiphenyl
35-11572 %2-Fluorophenol
37-12267 %Nitrobenzene-d5
34-12170 %Phenol-d5
54-12799 %Terphenyl-d14
Total Metals
16 6020B P7D0257100.30 4/24/17 23:50 BGMmg/kg dry 0.057Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000491,1,1,2-Tetrachloroethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000291,1,1-Trichloroethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000531,1,2-Trichloroethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000261,1-Dichloroethylene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000331,1-Dichloropropylene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000761,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-4 (0-2)
Prism Sample ID: 7040298-04
Prism Work Order: 7040298
Time Collected: 04/13/17 09:55
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000451,2,4-Trimethylbenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000281,2-Dichlorobenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000351,2-Dichloroethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000371,2-Dichloropropane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000451,3,5-Trimethylbenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000391,3-Dichlorobenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000301,3-Dichloropropane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000282,2-Dichloropropane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000312-Chlorotoluene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000354-Chlorotoluene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.000294-Isopropyltoluene
0.16 8260B P7D033710.060 4/20/17 18:55 ANGmg/kg dry 0.0015Acetone
BRL 8260B P7D033710.0036 4/20/17 18:55 ANGmg/kg dry 0.00035Benzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00050Bromobenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00033Bromochloromethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00033Bromodichloromethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00068Bromoform
BRL 8260B P7D033710.012 4/20/17 18:55 ANGmg/kg dry 0.00073Bromomethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00030Carbon Tetrachloride
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00032Chlorobenzene
BRL 8260B P7D033710.012 4/20/17 18:55 ANGmg/kg dry 0.00050Chloroethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00043Chloroform
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00040Chloromethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00027Dichlorodifluoromethane
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00023Ethylbenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00024Isopropyl Ether
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene)
BRL 8260B P7D033710.012 4/20/17 18:55 ANGmg/kg dry 0.00055m,p-Xylenes
BRL 8260B P7D033710.060 4/20/17 18:55 ANGmg/kg dry 0.00054Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D033710.12 4/20/17 18:55 ANGmg/kg dry 0.00054Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D033710.060 4/20/17 18:55 ANGmg/kg dry 0.00051Methyl Isobutyl Ketone
0.011 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00033Methylene Chloride
BRL 8260B P7D033710.012 4/20/17 18:55 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P7D033710.012 4/20/17 18:55 ANGmg/kg dry 0.00019Naphthalene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00030n-Butylbenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00035n-Propylbenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00024o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-4 (0-2)
Prism Sample ID: 7040298-04
Prism Work Order: 7040298
Time Collected: 04/13/17 09:55
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00036Styrene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00028Tetrachloroethylene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00034Toluene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00036trans-1,2-Dichloroethylene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00039Trichloroethylene
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00038Trichlorofluoromethane
BRL 8260B P7D033710.030 4/20/17 18:55 ANGmg/kg dry 0.00082Vinyl acetate
BRL 8260B P7D033710.0060 4/20/17 18:55 ANGmg/kg dry 0.00029Vinyl chloride
BRL 8260B P7D033710.018 4/20/17 18:55 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130106 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-12994 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-5 (0-2)
Prism Sample ID: 7040298-05
Prism Work Order: 7040298
Time Collected: 04/13/17 09:50
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
81.2 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0631,2,4-Trichlorobenzene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0611,2-Dichlorobenzene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0591,4-Dichlorobenzene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0781-Methylnaphthalene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0762,4,6-Trichlorophenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0782,4-Dichlorophenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0572-Chlorophenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0652-Methylnaphthalene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0742-Nitrophenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0803,3'-Dichlorobenzidine
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.0624-Nitrophenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.065Anthracene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.053Azobenzene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.069Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-5 (0-2)
Prism Sample ID: 7040298-05
Prism Work Order: 7040298
Time Collected: 04/13/17 09:50
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.051Chrysene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.053Dimethyl phthalate
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.058Fluorene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.064Hexachlorobenzene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.073Hexachlorobutadiene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.072Hexachlorocyclopentadiene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.068Hexachloroethane
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.055Isophorone
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.065Naphthalene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.064N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.060Phenol
BRL 8270D P7D027310.40 4/18/17 21:44 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13288 %2,4,6-Tribromophenol
44-11573 %2-Fluorobiphenyl
35-11568 %2-Fluorophenol
37-12261 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-12799 %Terphenyl-d14
Total Metals
14 6020B P7D0257100.31 4/24/17 23:56 BGMmg/kg dry 0.058Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000491,1,1,2-Tetrachloroethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000291,1,1-Trichloroethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000521,1,2-Trichloroethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000261,1-Dichloroethylene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000321,1-Dichloropropylene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000751,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-5 (0-2)
Prism Sample ID: 7040298-05
Prism Work Order: 7040298
Time Collected: 04/13/17 09:50
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000451,2,4-Trimethylbenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000281,2-Dichlorobenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000351,2-Dichloroethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000371,2-Dichloropropane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000451,3,5-Trimethylbenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000391,3-Dichlorobenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000301,3-Dichloropropane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000282,2-Dichloropropane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000302-Chlorotoluene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000354-Chlorotoluene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.000284-Isopropyltoluene
0.23 8260B P7D033710.059 4/20/17 19:22 ANGmg/kg dry 0.0014Acetone
BRL 8260B P7D033710.0035 4/20/17 19:22 ANGmg/kg dry 0.00034Benzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00049Bromobenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00032Bromochloromethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00033Bromodichloromethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00067Bromoform
BRL 8260B P7D033710.012 4/20/17 19:22 ANGmg/kg dry 0.00073Bromomethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00029Carbon Tetrachloride
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00031Chlorobenzene
BRL 8260B P7D033710.012 4/20/17 19:22 ANGmg/kg dry 0.00049Chloroethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00043Chloroform
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00040Chloromethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00027Dichlorodifluoromethane
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00023Ethylbenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00024Isopropyl Ether
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene)
BRL 8260B P7D033710.012 4/20/17 19:22 ANGmg/kg dry 0.00054m,p-Xylenes
BRL 8260B P7D033710.059 4/20/17 19:22 ANGmg/kg dry 0.00053Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D033710.12 4/20/17 19:22 ANGmg/kg dry 0.00053Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D033710.059 4/20/17 19:22 ANGmg/kg dry 0.00050Methyl Isobutyl Ketone
0.010 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00033Methylene Chloride
BRL 8260B P7D033710.012 4/20/17 19:22 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P7D033710.012 4/20/17 19:22 ANGmg/kg dry 0.00019Naphthalene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00030n-Butylbenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00035n-Propylbenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00024o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-5 (0-2)
Prism Sample ID: 7040298-05
Prism Work Order: 7040298
Time Collected: 04/13/17 09:50
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00036Styrene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00028Tetrachloroethylene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00034Toluene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00035trans-1,2-Dichloroethylene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00038Trichloroethylene
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00038Trichlorofluoromethane
BRL 8260B P7D033710.030 4/20/17 19:22 ANGmg/kg dry 0.00081Vinyl acetate
BRL 8260B P7D033710.0059 4/20/17 19:22 ANGmg/kg dry 0.00029Vinyl chloride
BRL 8260B P7D033710.018 4/20/17 19:22 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12991 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-6 (0-2)
Prism Sample ID: 7040298-06
Prism Work Order: 7040298
Time Collected: 04/13/17 09:45
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
83.3 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0621,2,4-Trichlorobenzene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0601,2-Dichlorobenzene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0561,3-Dichlorobenzene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0581,4-Dichlorobenzene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0761-Methylnaphthalene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0742,4,6-Trichlorophenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0762,4-Dichlorophenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0612,4-Dimethylphenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0552,4-Dinitrophenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0482,4-Dinitrotoluene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0532,6-Dinitrotoluene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0572-Chloronaphthalene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0562-Chlorophenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0632-Methylnaphthalene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0512-Methylphenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0722-Nitrophenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0783,3'-Dichlorobenzidine
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0493/4-Methylphenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0684-Bromophenyl phenyl ether
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0554-Chloro-3-methylphenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.0614-Nitrophenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.054Acenaphthene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.057Acenaphthylene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.064Anthracene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.052Azobenzene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.052Benzo(a)anthracene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.043Benzo(a)pyrene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.046Benzo(b)fluoranthene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.043Benzo(g,h,i)perylene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.052Benzo(k)fluoranthene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.033Benzoic Acid
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.052Benzyl alcohol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.069bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.056Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.068Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.059Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-6 (0-2)
Prism Sample ID: 7040298-06
Prism Work Order: 7040298
Time Collected: 04/13/17 09:45
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.056Butyl benzyl phthalate
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.050Chrysene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.060Dibenzofuran
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.054Diethyl phthalate
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.052Dimethyl phthalate
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.056Di-n-butyl phthalate
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.050Fluoranthene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.057Fluorene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.063Hexachlorobenzene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.071Hexachlorobutadiene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.071Hexachlorocyclopentadiene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.066Hexachloroethane
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.054Isophorone
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.064Naphthalene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.056Nitrobenzene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.060N-Nitrosodiphenylamine
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.047Pentachlorophenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.051Phenanthrene
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.058Phenol
BRL 8270D P7D027310.40 4/18/17 22:07 JMVmg/kg dry 0.052Pyrene
Surrogate Recovery Control Limits
39-13289 %2,4,6-Tribromophenol
44-11572 %2-Fluorobiphenyl
35-11570 %2-Fluorophenol
37-12264 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-127100 %Terphenyl-d14
Total Metals
17 6020B P7D0257100.30 4/25/17 0:01 BGMmg/kg dry 0.056Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000461,1,1,2-Tetrachloroethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000271,1,1-Trichloroethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000381,1,2,2-Tetrachloroethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000491,1,2-Trichloroethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000151,1-Dichloroethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000711,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-6 (0-2)
Prism Sample ID: 7040298-06
Prism Work Order: 7040298
Time Collected: 04/13/17 09:45
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000411,2,4-Trichlorobenzene
0.0026 8260B P7D033710.0056 4/20/17 19:50 ANGJmg/kg dry 0.000431,2,4-Trimethylbenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000221,2-Dibromoethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000261,2-Dichlorobenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000331,2-Dichloroethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000421,3,5-Trimethylbenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000371,3-Dichlorobenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000281,3-Dichloropropane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000334-Chlorotoluene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.000274-Isopropyltoluene
0.18 8260B P7D033710.056 4/20/17 19:50 ANGmg/kg dry 0.0014Acetone
BRL 8260B P7D033710.0033 4/20/17 19:50 ANGmg/kg dry 0.00032Benzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00046Bromobenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00031Bromochloromethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00031Bromodichloromethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00063Bromoform
BRL 8260B P7D033710.011 4/20/17 19:50 ANGmg/kg dry 0.00069Bromomethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00030Chlorobenzene
BRL 8260B P7D033710.011 4/20/17 19:50 ANGmg/kg dry 0.00046Chloroethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00040Chloroform
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00037Chloromethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00025Dichlorodifluoromethane
0.0041 8260B P7D033710.0056 4/20/17 19:50 ANGJmg/kg dry 0.00021Ethylbenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00033Isopropylbenzene (Cumene)
0.012 8260B P7D033710.011 4/20/17 19:50 ANGmg/kg dry 0.00051m,p-Xylenes
BRL 8260B P7D033710.056 4/20/17 19:50 ANGmg/kg dry 0.00050Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D033710.11 4/20/17 19:50 ANGmg/kg dry 0.00050Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D033710.056 4/20/17 19:50 ANGmg/kg dry 0.00047Methyl Isobutyl Ketone
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00031Methylene Chloride
BRL 8260B P7D033710.011 4/20/17 19:50 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P7D033710.011 4/20/17 19:50 ANGmg/kg dry 0.00018Naphthalene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00028n-Butylbenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00033n-Propylbenzene
0.0032 8260B P7D033710.0056 4/20/17 19:50 ANGJmg/kg dry 0.00023o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-6 (0-2)
Prism Sample ID: 7040298-06
Prism Work Order: 7040298
Time Collected: 04/13/17 09:45
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00027sec-Butylbenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00034Styrene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00027Tetrachloroethylene
0.011 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00032Toluene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00033trans-1,2-Dichloroethylene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00029trans-1,3-Dichloropropylene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00036Trichloroethylene
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00036Trichlorofluoromethane
BRL 8260B P7D033710.028 4/20/17 19:50 ANGmg/kg dry 0.00076Vinyl acetate
BRL 8260B P7D033710.0056 4/20/17 19:50 ANGmg/kg dry 0.00027Vinyl chloride
0.015 8260B P7D033710.017 4/20/17 19:50 ANGJmg/kg dry 0.0010Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-123101 %Dibromofluoromethane
76-12993 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-7 (0-2)
Prism Sample ID: 7040298-07
Prism Work Order: 7040298
Time Collected: 04/13/17 09:40
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
81.0 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0791-Methylnaphthalene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0762,4,6-Trichlorophenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0792,4-Dichlorophenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0652-Methylnaphthalene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0742-Nitrophenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0813,3'-Dichlorobenzidine
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.066Anthracene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-7 (0-2)
Prism Sample ID: 7040298-07
Prism Work Order: 7040298
Time Collected: 04/13/17 09:40
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.051Chrysene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.059Fluorene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.073Hexachlorobutadiene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.073Hexachlorocyclopentadiene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.068Hexachloroethane
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.055Isophorone
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.064N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.060Phenol
BRL 8270D P7D027310.41 4/18/17 22:29 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13287 %2,4,6-Tribromophenol
44-11573 %2-Fluorobiphenyl
35-11572 %2-Fluorophenol
37-12267 %Nitrobenzene-d5
34-12170 %Phenol-d5
54-12799 %Terphenyl-d14
Total Metals
13 6020B P7D0257100.31 4/25/17 0:06 BGMmg/kg dry 0.058Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000481,1,1,2-Tetrachloroethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000281,1,1-Trichloroethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000521,1,2-Trichloroethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000261,1-Dichloroethylene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000321,1-Dichloropropylene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000331,2,3-Trichlorobenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000751,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-7 (0-2)
Prism Sample ID: 7040298-07
Prism Work Order: 7040298
Time Collected: 04/13/17 09:40
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000451,2,4-Trimethylbenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000351,2-Dichloroethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000361,2-Dichloropropane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000441,3,5-Trimethylbenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000391,3-Dichlorobenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000291,3-Dichloropropane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000282,2-Dichloropropane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000302-Chlorotoluene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000354-Chlorotoluene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.000284-Isopropyltoluene
0.055 8260B P7D033710.058 4/20/17 20:17 ANGJmg/kg dry 0.0014Acetone
BRL 8260B P7D033710.0035 4/20/17 20:17 ANGmg/kg dry 0.00034Benzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00049Bromobenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00032Bromochloromethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00033Bromodichloromethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00066Bromoform
BRL 8260B P7D033710.012 4/20/17 20:17 ANGmg/kg dry 0.00072Bromomethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00029Carbon Tetrachloride
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00031Chlorobenzene
BRL 8260B P7D033710.012 4/20/17 20:17 ANGmg/kg dry 0.00049Chloroethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00042Chloroform
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00039Chloromethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00027Dichlorodifluoromethane
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00022Ethylbenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00024Isopropyl Ether
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene)
0.0034 8260B P7D033710.012 4/20/17 20:17 ANGJmg/kg dry 0.00054m,p-Xylenes
BRL 8260B P7D033710.058 4/20/17 20:17 ANGmg/kg dry 0.00053Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D033710.12 4/20/17 20:17 ANGmg/kg dry 0.00053Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D033710.058 4/20/17 20:17 ANGmg/kg dry 0.00050Methyl Isobutyl Ketone
0.011 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00033Methylene Chloride
BRL 8260B P7D033710.012 4/20/17 20:17 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P7D033710.012 4/20/17 20:17 ANGmg/kg dry 0.00018Naphthalene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00030n-Butylbenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00035n-Propylbenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00024o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-7 (0-2)
Prism Sample ID: 7040298-07
Prism Work Order: 7040298
Time Collected: 04/13/17 09:40
Time Submitted: 04/17/17 08:00
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00028sec-Butylbenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00035Styrene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00028Tetrachloroethylene
0.0028 8260B P7D033710.0058 4/20/17 20:17 ANGJmg/kg dry 0.00034Toluene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00035trans-1,2-Dichloroethylene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00038Trichloroethylene
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00038Trichlorofluoromethane
BRL 8260B P7D033710.029 4/20/17 20:17 ANGmg/kg dry 0.00080Vinyl acetate
BRL 8260B P7D033710.0058 4/20/17 20:17 ANGmg/kg dry 0.00028Vinyl chloride
0.0034 8260B P7D033710.018 4/20/17 20:17 ANGJmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130115 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12992 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-8 (0-1)
Prism Sample ID: 7040298-08
Prism Work Order: 7040298
Time Collected: 04/13/17 11:45
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
64.6 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0781,2,4-Trichlorobenzene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0761,2-Dichlorobenzene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0711,3-Dichlorobenzene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0731,4-Dichlorobenzene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0971-Methylnaphthalene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0942,4,6-Trichlorophenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0972,4-Dichlorophenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0772,4-Dimethylphenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0702,4-Dinitrophenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0612,4-Dinitrotoluene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0672,6-Dinitrotoluene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0732-Chloronaphthalene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0712-Chlorophenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0802-Methylnaphthalene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0642-Methylphenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0912-Nitrophenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0993,3'-Dichlorobenzidine
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0623/4-Methylphenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0754,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0864-Bromophenyl phenyl ether
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0704-Chloro-3-methylphenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0604-Chloroaniline
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0654-Chlorophenyl phenyl ether
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.0774-Nitrophenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.068Acenaphthene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.073Acenaphthylene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.081Anthracene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.066Azobenzene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.066Benzo(a)anthracene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.054Benzo(a)pyrene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.058Benzo(b)fluoranthene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.055Benzo(g,h,i)perylene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.066Benzo(k)fluoranthene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.042Benzoic Acid
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.066Benzyl alcohol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.087bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.071Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.086Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.074Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-8 (0-1)
Prism Sample ID: 7040298-08
Prism Work Order: 7040298
Time Collected: 04/13/17 11:45
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.071Butyl benzyl phthalate
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.063Chrysene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.061Dibenzo(a,h)anthracene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.076Dibenzofuran
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.069Diethyl phthalate
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.066Dimethyl phthalate
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.071Di-n-butyl phthalate
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.062Di-n-octyl phthalate
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.064Fluoranthene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.072Fluorene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.080Hexachlorobenzene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.090Hexachlorobutadiene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.089Hexachlorocyclopentadiene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.084Hexachloroethane
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.058Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.068Isophorone
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.081Naphthalene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.071Nitrobenzene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.079N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.076N-Nitrosodiphenylamine
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.059Pentachlorophenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.065Phenanthrene
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.074Phenol
BRL 8270D P7D027310.50 4/18/17 22:52 JMVmg/kg dry 0.066Pyrene
Surrogate Recovery Control Limits
39-13294 %2,4,6-Tribromophenol
44-11583 %2-Fluorobiphenyl
35-11579 %2-Fluorophenol
37-12275 %Nitrobenzene-d5
34-12178 %Phenol-d5
54-127107 %Terphenyl-d14
Total Metals
29 6020B P7D0257100.39 4/25/17 0:11 BGMmg/kg dry 0.073Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000561,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000331,1,1-Trichloroethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000461,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000611,1,2-Trichloroethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000871,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-8 (0-1)
Prism Sample ID: 7040298-08
Prism Work Order: 7040298
Time Collected: 04/13/17 11:45
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000511,2,4-Trichlorobenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000521,2,4-Trimethylbenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000421,2-Dichloropropane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000521,3,5-Trimethylbenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000451,3-Dichlorobenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.000334-Isopropyltoluene
0.12 8260B P7D036210.068 4/21/17 11:55 ANGmg/kg dry 0.0017Acetone
BRL 8260B P7D036210.0041 4/21/17 11:55 ANGmg/kg dry 0.00040Benzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00057Bromobenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00038Bromochloromethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00038Bromodichloromethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00078Bromoform
BRL 8260B P7D036210.014 4/21/17 11:55 ANGmg/kg dry 0.00084Bromomethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00034Carbon Tetrachloride
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00036Chlorobenzene
BRL 8260B P7D036210.014 4/21/17 11:55 ANGmg/kg dry 0.00057Chloroethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00049Chloroform
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00046Chloromethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00026Ethylbenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00040Isopropylbenzene (Cumene)
BRL 8260B P7D036210.014 4/21/17 11:55 ANGmg/kg dry 0.00063m,p-Xylenes
BRL 8260B P7D036210.068 4/21/17 11:55 ANGmg/kg dry 0.00062Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.14 4/21/17 11:55 ANGmg/kg dry 0.00062Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.068 4/21/17 11:55 ANGmg/kg dry 0.00058Methyl Isobutyl Ketone
0.013 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00038Methylene Chloride
BRL 8260B P7D036210.014 4/21/17 11:55 ANGmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P7D036210.014 4/21/17 11:55 ANGmg/kg dry 0.00022Naphthalene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00028o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-8 (0-1)
Prism Sample ID: 7040298-08
Prism Work Order: 7040298
Time Collected: 04/13/17 11:45
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00041Styrene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00039Toluene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00044Trichloroethylene
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00044Trichlorofluoromethane
BRL 8260B P7D036210.034 4/21/17 11:55 ANGmg/kg dry 0.00094Vinyl acetate
BRL 8260B P7D036210.0068 4/21/17 11:55 ANGmg/kg dry 0.00033Vinyl chloride
BRL 8260B P7D036210.021 4/21/17 11:55 ANGmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12992 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-9 (0-2)
Prism Sample ID: 7040298-09
Prism Work Order: 7040298
Time Collected: 04/13/17 09:30
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
80.8 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0631,2,4-Trichlorobenzene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0611,2-Dichlorobenzene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0591,4-Dichlorobenzene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0771-Methylnaphthalene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0752,4,6-Trichlorophenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0782,4-Dichlorophenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0562,4-Dinitrophenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0532,6-Dinitrotoluene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0582-Chloronaphthalene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0572-Chlorophenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0642-Methylnaphthalene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0512-Methylphenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0732-Nitrophenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0793,3'-Dichlorobenzidine
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0493/4-Methylphenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0694-Bromophenyl phenyl ether
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0564-Chloro-3-methylphenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.0624-Nitrophenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.058Acenaphthylene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.065Anthracene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.053Azobenzene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.043Benzo(a)pyrene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.069Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-9 (0-2)
Prism Sample ID: 7040298-09
Prism Work Order: 7040298
Time Collected: 04/13/17 09:30
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.057Butyl benzyl phthalate
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.051Chrysene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.061Dibenzofuran
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.055Diethyl phthalate
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.053Dimethyl phthalate
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.057Di-n-butyl phthalate
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.051Fluoranthene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.058Fluorene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.064Hexachlorobenzene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.072Hexachlorobutadiene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.072Hexachlorocyclopentadiene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.067Hexachloroethane
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.054Isophorone
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.065Naphthalene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.057Nitrobenzene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.061N-Nitrosodiphenylamine
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.047Pentachlorophenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.052Phenanthrene
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.059Phenol
BRL 8270D P7D027310.40 4/20/17 1:51 JMVmg/kg dry 0.053Pyrene
Surrogate Recovery Control Limits
39-13273 %2,4,6-Tribromophenol
44-11572 %2-Fluorobiphenyl
35-11572 %2-Fluorophenol
37-12267 %Nitrobenzene-d5
34-12173 %Phenol-d5
54-12793 %Terphenyl-d14
Total Metals
19 6020B P7D0257100.31 4/25/17 0:17 BGMmg/kg dry 0.058Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000541,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000321,1,1-Trichloroethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000441,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000581,1,2-Trichloroethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000291,1-Dichloroethylene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000361,1-Dichloropropylene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000371,2,3-Trichlorobenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000831,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-9 (0-2)
Prism Sample ID: 7040298-09
Prism Work Order: 7040298
Time Collected: 04/13/17 09:30
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000481,2,4-Trichlorobenzene
0.0046 8260B P7D036210.0065 4/21/17 12:23 ANGJmg/kg dry 0.000501,2,4-Trimethylbenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000261,2-Dibromoethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000311,2-Dichlorobenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000391,2-Dichloroethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000401,2-Dichloropropane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000491,3,5-Trimethylbenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000431,3-Dichlorobenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000331,3-Dichloropropane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000312,2-Dichloropropane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000342-Chlorotoluene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000394-Chlorotoluene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.000314-Isopropyltoluene
0.36 8260B P7D036210.065 4/21/17 12:23 ANGmg/kg dry 0.0016Acetone
0.0056 8260B P7D036210.0039 4/21/17 12:23 ANGmg/kg dry 0.00038Benzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00054Bromobenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00036Bromochloromethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00036Bromodichloromethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00074Bromoform
0.0049 8260B P7D036210.013 4/21/17 12:23 ANGJmg/kg dry 0.00080Bromomethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00032Carbon Tetrachloride
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00035Chlorobenzene
BRL 8260B P7D036210.013 4/21/17 12:23 ANGmg/kg dry 0.00054Chloroethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00047Chloroform
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00044Chloromethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00028cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00027Dibromochloromethane
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00030Dichlorodifluoromethane
0.0030 8260B P7D036210.0065 4/21/17 12:23 ANGJmg/kg dry 0.00025Ethylbenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00039Isopropylbenzene (Cumene)
0.014 8260B P7D036210.013 4/21/17 12:23 ANGmg/kg dry 0.00060m,p-Xylenes
BRL 8260B P7D036210.065 4/21/17 12:23 ANGmg/kg dry 0.00059Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.13 4/21/17 12:23 ANGmg/kg dry 0.00059Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.065 4/21/17 12:23 ANGmg/kg dry 0.00055Methyl Isobutyl Ketone
0.013 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00037Methylene Chloride
BRL 8260B P7D036210.013 4/21/17 12:23 ANGmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P7D036210.013 4/21/17 12:23 ANGmg/kg dry 0.00021Naphthalene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00033n-Butylbenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00039n-Propylbenzene
0.0063 8260B P7D036210.0065 4/21/17 12:23 ANGJmg/kg dry 0.00027o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-9 (0-2)
Prism Sample ID: 7040298-09
Prism Work Order: 7040298
Time Collected: 04/13/17 09:30
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00032sec-Butylbenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00039Styrene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00022tert-Butylbenzene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00031Tetrachloroethylene
0.0063 8260B P7D036210.0065 4/21/17 12:23 ANGJmg/kg dry 0.00037Toluene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00039trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00034trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00042Trichloroethylene
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00042Trichlorofluoromethane
BRL 8260B P7D036210.033 4/21/17 12:23 ANGmg/kg dry 0.00089Vinyl acetate
BRL 8260B P7D036210.0065 4/21/17 12:23 ANGmg/kg dry 0.00032Vinyl chloride
0.020 8260B P7D036210.020 4/21/17 12:23 ANGmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12992 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-12B (0-2)
Prism Sample ID: 7040298-10
Prism Work Order: 7040298
Time Collected: 04/13/17 14:40
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
85.7 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0591,2,4-Trichlorobenzene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0571,2-Dichlorobenzene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0531,3-Dichlorobenzene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0551,4-Dichlorobenzene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0731-Methylnaphthalene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0712,4,6-Trichlorophenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0732,4-Dichlorophenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0582,4-Dimethylphenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0532,4-Dinitrophenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0462,4-Dinitrotoluene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0502,6-Dinitrotoluene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0552-Chloronaphthalene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0542-Chlorophenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0612-Methylnaphthalene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0492-Methylphenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0692-Nitrophenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0753,3'-Dichlorobenzidine
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0473/4-Methylphenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0574,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0654-Bromophenyl phenyl ether
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0534-Chloro-3-methylphenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0464-Chloroaniline
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0494-Chlorophenyl phenyl ether
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.0584-Nitrophenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.052Acenaphthene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.055Acenaphthylene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.061Anthracene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.050Azobenzene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.050Benzo(a)anthracene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.041Benzo(a)pyrene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.044Benzo(b)fluoranthene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.042Benzo(g,h,i)perylene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.050Benzo(k)fluoranthene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.032Benzoic Acid
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.050Benzyl alcohol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.066bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.053Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.065Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.056Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-12B (0-2)
Prism Sample ID: 7040298-10
Prism Work Order: 7040298
Time Collected: 04/13/17 14:40
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.054Butyl benzyl phthalate
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.048Chrysene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.046Dibenzo(a,h)anthracene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.058Dibenzofuran
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.052Diethyl phthalate
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.050Dimethyl phthalate
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.054Di-n-butyl phthalate
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.047Di-n-octyl phthalate
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.048Fluoranthene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.054Fluorene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.060Hexachlorobenzene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.068Hexachlorobutadiene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.068Hexachlorocyclopentadiene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.063Hexachloroethane
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.043Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.051Isophorone
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.061Naphthalene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.054Nitrobenzene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.060N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.058N-Nitrosodiphenylamine
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.045Pentachlorophenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.049Phenanthrene
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.056Phenol
BRL 8270D P7D027310.38 4/20/17 2:14 JMVmg/kg dry 0.050Pyrene
Surrogate Recovery Control Limits
39-13272 %2,4,6-Tribromophenol
44-11568 %2-Fluorobiphenyl
35-11568 %2-Fluorophenol
37-12263 %Nitrobenzene-d5
34-12168 %Phenol-d5
54-12789 %Terphenyl-d14
Total Metals
12 6020B P7D0257100.29 4/25/17 0:22 BGMmg/kg dry 0.055Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000341,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000201,1,1-Trichloroethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000281,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000371,1,2-Trichloroethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000121,1-Dichloroethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000181,1-Dichloroethylene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000231,1-Dichloropropylene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000241,2,3-Trichlorobenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000531,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-12B (0-2)
Prism Sample ID: 7040298-10
Prism Work Order: 7040298
Time Collected: 04/13/17 14:40
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000311,2,4-Trichlorobenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000321,2,4-Trimethylbenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000171,2-Dibromoethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000201,2-Dichlorobenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000251,2-Dichloroethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000261,2-Dichloropropane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000311,3,5-Trimethylbenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000281,3-Dichlorobenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000211,3-Dichloropropane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000161,4-Dichlorobenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000202,2-Dichloropropane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000212-Chlorotoluene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000254-Chlorotoluene
0.015 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.000204-Isopropyltoluene
0.11 8260B P7D036210.042 4/21/17 12:50 ANGmg/kg dry 0.0010Acetone
BRL 8260B P7D036210.0025 4/21/17 12:50 ANGmg/kg dry 0.00024Benzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00035Bromobenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00023Bromochloromethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00023Bromodichloromethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00047Bromoform
BRL 8260B P7D036210.0083 4/21/17 12:50 ANGmg/kg dry 0.00051Bromomethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00021Carbon Tetrachloride
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00022Chlorobenzene
BRL 8260B P7D036210.0083 4/21/17 12:50 ANGmg/kg dry 0.00035Chloroethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00030Chloroform
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00028Chloromethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00018cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00014cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00017Dibromochloromethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00019Dichlorodifluoromethane
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00016Ethylbenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00017Isopropyl Ether
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00025Isopropylbenzene (Cumene)
BRL 8260B P7D036210.0083 4/21/17 12:50 ANGmg/kg dry 0.00038m,p-Xylenes
BRL 8260B P7D036210.042 4/21/17 12:50 ANGmg/kg dry 0.00038Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.083 4/21/17 12:50 ANGmg/kg dry 0.00038Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.042 4/21/17 12:50 ANGmg/kg dry 0.00035Methyl Isobutyl Ketone
0.0058 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00023Methylene Chloride
BRL 8260B P7D036210.0083 4/21/17 12:50 ANGmg/kg dry 0.00013Methyl-tert-Butyl Ether
BRL 8260B P7D036210.0083 4/21/17 12:50 ANGmg/kg dry 0.00013Naphthalene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00021n-Butylbenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00025n-Propylbenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00017o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-12B (0-2)
Prism Sample ID: 7040298-10
Prism Work Order: 7040298
Time Collected: 04/13/17 14:40
Time Submitted: 04/17/17 08:00
0.0026 8260B P7D036210.0042 4/21/17 12:50 ANGJmg/kg dry 0.00020sec-Butylbenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00025Styrene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00014tert-Butylbenzene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00020Tetrachloroethylene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00024Toluene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00025trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00022trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00027Trichloroethylene
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00027Trichlorofluoromethane
BRL 8260B P7D036210.021 4/21/17 12:50 ANGmg/kg dry 0.00057Vinyl acetate
BRL 8260B P7D036210.0042 4/21/17 12:50 ANGmg/kg dry 0.00020Vinyl chloride
BRL 8260B P7D036210.012 4/21/17 12:50 ANGmg/kg dry 0.00078Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12993 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-14 (0-2)
Prism Sample ID: 7040298-11
Prism Work Order: 7040298
Time Collected: 04/13/17 10:20
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
88.6 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0571,2,4-Trichlorobenzene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0561,2-Dichlorobenzene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0521,3-Dichlorobenzene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0541,4-Dichlorobenzene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0711-Methylnaphthalene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0692,4,6-Trichlorophenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0712,4-Dichlorophenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0562,4-Dimethylphenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0512,4-Dinitrophenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0452,4-Dinitrotoluene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0492,6-Dinitrotoluene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0532-Chloronaphthalene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0522-Chlorophenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0592-Methylnaphthalene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0472-Methylphenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0672-Nitrophenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0723,3'-Dichlorobenzidine
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0453/4-Methylphenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0554,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0634-Bromophenyl phenyl ether
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0514-Chloro-3-methylphenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0444-Chloroaniline
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0484-Chlorophenyl phenyl ether
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.0564-Nitrophenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.050Acenaphthene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.053Acenaphthylene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.059Anthracene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.048Azobenzene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.048Benzo(a)anthracene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.040Benzo(a)pyrene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.043Benzo(b)fluoranthene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.040Benzo(g,h,i)perylene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.048Benzo(k)fluoranthene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.031Benzoic Acid
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.048Benzyl alcohol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.064bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.052Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.063Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.054Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-14 (0-2)
Prism Sample ID: 7040298-11
Prism Work Order: 7040298
Time Collected: 04/13/17 10:20
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.052Butyl benzyl phthalate
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.046Chrysene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.045Dibenzo(a,h)anthracene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.056Dibenzofuran
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.051Diethyl phthalate
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.048Dimethyl phthalate
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.052Di-n-butyl phthalate
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.045Di-n-octyl phthalate
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.047Fluoranthene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.053Fluorene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.058Hexachlorobenzene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.066Hexachlorobutadiene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.065Hexachlorocyclopentadiene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.061Hexachloroethane
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.042Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.050Isophorone
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.059Naphthalene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.052Nitrobenzene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.058N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.056N-Nitrosodiphenylamine
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.043Pentachlorophenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.048Phenanthrene
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.054Phenol
BRL 8270D P7D027310.37 4/20/17 1:29 JMVmg/kg dry 0.049Pyrene
Surrogate Recovery Control Limits
39-13287 %2,4,6-Tribromophenol
44-11583 %2-Fluorobiphenyl
35-11583 %2-Fluorophenol
37-12277 %Nitrobenzene-d5
34-12184 %Phenol-d5
54-127107 %Terphenyl-d14
Total Metals
12 6020B P7D0257100.28 4/25/17 0:37 BGMmg/kg dry 0.053Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000451,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000261,1,1-Trichloroethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000371,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000481,1,2-Trichloroethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000151,1-Dichloroethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000241,1-Dichloroethylene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000301,1-Dichloropropylene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000311,2,3-Trichlorobenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000691,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-14 (0-2)
Prism Sample ID: 7040298-11
Prism Work Order: 7040298
Time Collected: 04/13/17 10:20
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000401,2,4-Trichlorobenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000421,2,4-Trimethylbenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000221,2-Dibromoethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000261,2-Dichlorobenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000321,2-Dichloroethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000341,2-Dichloropropane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000411,3,5-Trimethylbenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000361,3-Dichlorobenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000271,3-Dichloropropane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000211,4-Dichlorobenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000262,2-Dichloropropane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000282-Chlorotoluene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000324-Chlorotoluene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.000264-Isopropyltoluene
BRL 8260B P7D036210.054 4/21/17 13:18 ANGmg/kg dry 0.0013Acetone
BRL 8260B P7D036210.0033 4/21/17 13:18 ANGmg/kg dry 0.00032Benzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00045Bromobenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00030Bromochloromethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00030Bromodichloromethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00062Bromoform
BRL 8260B P7D036210.011 4/21/17 13:18 ANGmg/kg dry 0.00067Bromomethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00027Carbon Tetrachloride
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00029Chlorobenzene
BRL 8260B P7D036210.011 4/21/17 13:18 ANGmg/kg dry 0.00045Chloroethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00039Chloroform
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00037Chloromethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00023cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00018cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00022Dibromochloromethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00025Dichlorodifluoromethane
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00021Ethylbenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00022Isopropyl Ether
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00032Isopropylbenzene (Cumene)
BRL 8260B P7D036210.011 4/21/17 13:18 ANGmg/kg dry 0.00050m,p-Xylenes
BRL 8260B P7D036210.054 4/21/17 13:18 ANGmg/kg dry 0.00049Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.11 4/21/17 13:18 ANGmg/kg dry 0.00049Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.054 4/21/17 13:18 ANGmg/kg dry 0.00046Methyl Isobutyl Ketone
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00031Methylene Chloride
BRL 8260B P7D036210.011 4/21/17 13:18 ANGmg/kg dry 0.00017Methyl-tert-Butyl Ether
BRL 8260B P7D036210.011 4/21/17 13:18 ANGmg/kg dry 0.00017Naphthalene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00028n-Butylbenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00032n-Propylbenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00022o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 56 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-14 (0-2)
Prism Sample ID: 7040298-11
Prism Work Order: 7040298
Time Collected: 04/13/17 10:20
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00026sec-Butylbenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00033Styrene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00018tert-Butylbenzene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00026Tetrachloroethylene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00031Toluene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00032trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00029trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00035Trichloroethylene
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00035Trichlorofluoromethane
BRL 8260B P7D036210.027 4/21/17 13:18 ANGmg/kg dry 0.00074Vinyl acetate
BRL 8260B P7D036210.0054 4/21/17 13:18 ANGmg/kg dry 0.00026Vinyl chloride
BRL 8260B P7D036210.016 4/21/17 13:18 ANGmg/kg dry 0.0010Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12991 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 57 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-15 (0-2)
Prism Sample ID: 7040298-12
Prism Work Order: 7040298
Time Collected: 04/13/17 10:25
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
78.9 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0631,2-Dichlorobenzene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0801-Methylnaphthalene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0772,4,6-Trichlorophenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0802,4-Dichlorophenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0632,4-Dimethylphenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0582,4-Dinitrophenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0552,6-Dinitrotoluene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0602-Chloronaphthalene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0592-Chlorophenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0662-Methylnaphthalene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0532-Methylphenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0752-Nitrophenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0823,3'-Dichlorobenzidine
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0513/4-Methylphenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0714-Bromophenyl phenyl ether
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0584-Chloro-3-methylphenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0504-Chloroaniline
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.0644-Nitrophenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.060Acenaphthylene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.067Anthracene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.055Azobenzene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.045Benzo(a)pyrene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.072bis(2-Chloroethoxy)methane
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.071Bis(2-chloroisopropyl)ether
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 58 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-15 (0-2)
Prism Sample ID: 7040298-12
Prism Work Order: 7040298
Time Collected: 04/13/17 10:25
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.059Butyl benzyl phthalate
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.052Chrysene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.063Dibenzofuran
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.057Diethyl phthalate
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.055Dimethyl phthalate
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.059Di-n-butyl phthalate
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.051Di-n-octyl phthalate
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.053Fluoranthene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.059Fluorene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.066Hexachlorobenzene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.074Hexachlorobutadiene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.074Hexachlorocyclopentadiene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.069Hexachloroethane
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.056Isophorone
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.059Nitrobenzene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.063N-Nitrosodiphenylamine
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.049Pentachlorophenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.054Phenanthrene
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.061Phenol
BRL 8270D P7D027310.41 4/20/17 2:37 JMVmg/kg dry 0.055Pyrene
Surrogate Recovery Control Limits
39-13274 %2,4,6-Tribromophenol
44-11575 %2-Fluorobiphenyl
35-11576 %2-Fluorophenol
37-12270 %Nitrobenzene-d5
34-12177 %Phenol-d5
54-12797 %Terphenyl-d14
Total Metals
15 6020B P7D0257100.32 4/25/17 0:42 BGMmg/kg dry 0.060Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000501,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000291,1,1-Trichloroethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000411,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000541,1,2-Trichloroethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000331,1-Dichloropropylene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000771,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 59 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-15 (0-2)
Prism Sample ID: 7040298-12
Prism Work Order: 7040298
Time Collected: 04/13/17 10:25
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000451,2,4-Trichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000461,2,4-Trimethylbenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000361,2-Dichloroethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000461,3,5-Trimethylbenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000401,3-Dichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000301,3-Dichloropropane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000312-Chlorotoluene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000364-Chlorotoluene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.000294-Isopropyltoluene
0.048 8260B P7D036210.061 4/21/17 13:46 ANGJmg/kg dry 0.0015Acetone
BRL 8260B P7D036210.0036 4/21/17 13:46 ANGmg/kg dry 0.00035Benzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00051Bromobenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00033Bromochloromethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00069Bromoform
BRL 8260B P7D036210.012 4/21/17 13:46 ANGmg/kg dry 0.00075Bromomethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00030Carbon Tetrachloride
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00032Chlorobenzene
BRL 8260B P7D036210.012 4/21/17 13:46 ANGmg/kg dry 0.00051Chloroethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00044Chloroform
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00041Chloromethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00023Ethylbenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00036Isopropylbenzene (Cumene)
BRL 8260B P7D036210.012 4/21/17 13:46 ANGmg/kg dry 0.00056m,p-Xylenes
BRL 8260B P7D036210.061 4/21/17 13:46 ANGmg/kg dry 0.00055Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.12 4/21/17 13:46 ANGmg/kg dry 0.00055Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.061 4/21/17 13:46 ANGmg/kg dry 0.00052Methyl Isobutyl Ketone
0.011 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00034Methylene Chloride
BRL 8260B P7D036210.012 4/21/17 13:46 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P7D036210.012 4/21/17 13:46 ANGmg/kg dry 0.00019Naphthalene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00031n-Butylbenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00036n-Propylbenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00025o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 60 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-15 (0-2)
Prism Sample ID: 7040298-12
Prism Work Order: 7040298
Time Collected: 04/13/17 10:25
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00037Styrene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00029Tetrachloroethylene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00035Toluene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00036trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00032trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00039Trichloroethylene
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00039Trichlorofluoromethane
BRL 8260B P7D036210.030 4/21/17 13:46 ANGmg/kg dry 0.00083Vinyl acetate
BRL 8260B P7D036210.0061 4/21/17 13:46 ANGmg/kg dry 0.00029Vinyl chloride
BRL 8260B P7D036210.018 4/21/17 13:46 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-129106 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 61 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-16 (0-2)
Prism Sample ID: 7040298-13
Prism Work Order: 7040298
Time Collected: 04/13/17 09:15
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
85.4 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0591,2,4-Trichlorobenzene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0571,2-Dichlorobenzene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0531,3-Dichlorobenzene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0551,4-Dichlorobenzene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0721-Methylnaphthalene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0702,4,6-Trichlorophenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0732,4-Dichlorophenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0582,4-Dimethylphenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0522,4-Dinitrophenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0462,4-Dinitrotoluene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0502,6-Dinitrotoluene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0542-Chloronaphthalene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0532-Chlorophenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0602-Methylnaphthalene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0482-Methylphenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0682-Nitrophenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0743,3'-Dichlorobenzidine
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0463/4-Methylphenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0564,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0654-Bromophenyl phenyl ether
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0534-Chloro-3-methylphenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0454-Chloroaniline
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0494-Chlorophenyl phenyl ether
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.0584-Nitrophenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.051Acenaphthene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.054Acenaphthylene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.061Anthracene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.050Azobenzene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.049Benzo(a)anthracene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.041Benzo(a)pyrene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.044Benzo(b)fluoranthene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.041Benzo(g,h,i)perylene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.049Benzo(k)fluoranthene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.032Benzoic Acid
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.050Benzyl alcohol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.065bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.053Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.064Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.056Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 62 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-16 (0-2)
Prism Sample ID: 7040298-13
Prism Work Order: 7040298
Time Collected: 04/13/17 09:15
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.054Butyl benzyl phthalate
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.047Chrysene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.046Dibenzo(a,h)anthracene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.057Dibenzofuran
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.052Diethyl phthalate
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.050Dimethyl phthalate
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.053Di-n-butyl phthalate
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.046Di-n-octyl phthalate
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.048Fluoranthene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.054Fluorene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.060Hexachlorobenzene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.068Hexachlorobutadiene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.067Hexachlorocyclopentadiene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.063Hexachloroethane
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.043Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.051Isophorone
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.060Naphthalene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.053Nitrobenzene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.059N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.057N-Nitrosodiphenylamine
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.044Pentachlorophenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.049Phenanthrene
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.055Phenol
BRL 8270D P7D027410.38 4/19/17 19:49 JMVmg/kg dry 0.050Pyrene
Surrogate Recovery Control Limits
39-13279 %2,4,6-Tribromophenol
44-11572 %2-Fluorobiphenyl
35-11573 %2-Fluorophenol
37-12267 %Nitrobenzene-d5
34-12172 %Phenol-d5
54-12792 %Terphenyl-d14
Total Metals
17 6020B P7D0257100.29 4/25/17 0:48 BGMmg/kg dry 0.055Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000411,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000241,1,1-Trichloroethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000341,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000451,1,2-Trichloroethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000141,1-Dichloroethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000221,1-Dichloroethylene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000281,1-Dichloropropylene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000291,2,3-Trichlorobenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000641,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 63 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-16 (0-2)
Prism Sample ID: 7040298-13
Prism Work Order: 7040298
Time Collected: 04/13/17 09:15
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000381,2,4-Trichlorobenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000391,2,4-Trimethylbenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000201,2-Dibromoethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000241,2-Dichlorobenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000301,2-Dichloroethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000311,2-Dichloropropane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000381,3,5-Trimethylbenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000331,3-Dichlorobenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000251,3-Dichloropropane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000201,4-Dichlorobenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000242,2-Dichloropropane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000262-Chlorotoluene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000304-Chlorotoluene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.000244-Isopropyltoluene
0.17 8260B P7D036210.050 4/21/17 14:13 ANGmg/kg dry 0.0012Acetone
BRL 8260B P7D036210.0030 4/21/17 14:13 ANGmg/kg dry 0.00029Benzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00042Bromobenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00028Bromochloromethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00028Bromodichloromethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00057Bromoform
BRL 8260B P7D036210.010 4/21/17 14:13 ANGmg/kg dry 0.00062Bromomethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00025Carbon Tetrachloride
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00027Chlorobenzene
BRL 8260B P7D036210.010 4/21/17 14:13 ANGmg/kg dry 0.00042Chloroethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00036Chloroform
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00034Chloromethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00022cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00017cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00021Dibromochloromethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00023Dichlorodifluoromethane
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00019Ethylbenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00021Isopropyl Ether
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00030Isopropylbenzene (Cumene)
0.0051 8260B P7D036210.010 4/21/17 14:13 ANGJmg/kg dry 0.00047m,p-Xylenes
BRL 8260B P7D036210.050 4/21/17 14:13 ANGmg/kg dry 0.00046Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.10 4/21/17 14:13 ANGmg/kg dry 0.00046Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.050 4/21/17 14:13 ANGmg/kg dry 0.00043Methyl Isobutyl Ketone
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00028Methylene Chloride
BRL 8260B P7D036210.010 4/21/17 14:13 ANGmg/kg dry 0.00016Methyl-tert-Butyl Ether
BRL 8260B P7D036210.010 4/21/17 14:13 ANGmg/kg dry 0.00016Naphthalene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00026n-Butylbenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00030n-Propylbenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00021o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 64 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-16 (0-2)
Prism Sample ID: 7040298-13
Prism Work Order: 7040298
Time Collected: 04/13/17 09:15
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00024sec-Butylbenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00030Styrene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00017tert-Butylbenzene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00024Tetrachloroethylene
0.0065 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00029Toluene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00030trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00027trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00033Trichloroethylene
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00033Trichlorofluoromethane
BRL 8260B P7D036210.025 4/21/17 14:13 ANGmg/kg dry 0.00069Vinyl acetate
BRL 8260B P7D036210.0050 4/21/17 14:13 ANGmg/kg dry 0.00024Vinyl chloride
0.0051 8260B P7D036210.015 4/21/17 14:13 ANGJmg/kg dry 0.00095Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
84-123101 %Dibromofluoromethane
76-12992 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 65 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-16 (7-9)
Prism Sample ID: 7040298-14
Prism Work Order: 7040298
Time Collected: 04/13/17 09:20
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
69.2 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0721,2,4-Trichlorobenzene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0701,2-Dichlorobenzene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0651,3-Dichlorobenzene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0681,4-Dichlorobenzene
1.1 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0891-Methylnaphthalene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0872,4,6-Trichlorophenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0892,4-Dichlorophenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0712,4-Dimethylphenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0652,4-Dinitrophenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0562,4-Dinitrotoluene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0612,6-Dinitrotoluene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0672-Chloronaphthalene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0662-Chlorophenol
2.1 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0742-Methylnaphthalene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0592-Methylphenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0842-Nitrophenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0913,3'-Dichlorobenzidine
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0573/4-Methylphenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0694,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0794-Bromophenyl phenyl ether
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0654-Chloro-3-methylphenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0564-Chloroaniline
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0604-Chlorophenyl phenyl ether
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.0714-Nitrophenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.063Acenaphthene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.067Acenaphthylene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.075Anthracene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.061Azobenzene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.060Benzo(a)anthracene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.050Benzo(a)pyrene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.054Benzo(b)fluoranthene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.051Benzo(g,h,i)perylene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.061Benzo(k)fluoranthene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.039Benzoic Acid
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.061Benzyl alcohol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.080bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.065Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.079Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.069Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 66 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-16 (7-9)
Prism Sample ID: 7040298-14
Prism Work Order: 7040298
Time Collected: 04/13/17 09:20
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.066Butyl benzyl phthalate
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.058Chrysene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.056Dibenzo(a,h)anthracene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.070Dibenzofuran
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.064Diethyl phthalate
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.061Dimethyl phthalate
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.066Di-n-butyl phthalate
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.057Di-n-octyl phthalate
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.059Fluoranthene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.066Fluorene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.073Hexachlorobenzene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.083Hexachlorobutadiene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.082Hexachlorocyclopentadiene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.077Hexachloroethane
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.053Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.063Isophorone
2.4 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.074Naphthalene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.066Nitrobenzene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.073N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.070N-Nitrosodiphenylamine
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.055Pentachlorophenol
0.12 8270D P7D027410.46 4/19/17 20:12 JMVJmg/kg dry 0.060Phenanthrene
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.068Phenol
BRL 8270D P7D027410.46 4/19/17 20:12 JMVmg/kg dry 0.061Pyrene
Surrogate Recovery Control Limits
39-13282 %2,4,6-Tribromophenol
44-11573 %2-Fluorobiphenyl
35-11575 %2-Fluorophenol
37-12268 %Nitrobenzene-d5
34-12173 %Phenol-d5
54-12792 %Terphenyl-d14
Total Metals
5.6 6020B P7D0257100.36 4/25/17 0:53 BGMmg/kg dry 0.068Lead
Volatile Organic Compounds by GC/MS (Medium Level)
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0781,1,1,2-Tetrachloroethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0721,1,1-Trichloroethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0601,1,2,2-Tetrachloroethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0751,1,2-Trichloroethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0821,1-Dichloroethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0891,1-Dichloroethylene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0701,1-Dichloropropylene
BRL 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.0731,2,3-Trichlorobenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.111,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 67 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-16 (7-9)
Prism Sample ID: 7040298-14
Prism Work Order: 7040298
Time Collected: 04/13/17 09:20
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.0671,2,4-Trichlorobenzene
49 8260B P7D03945003.1 4/24/17 20:48 ANGmg/kg dry 0.681,2,4-Trimethylbenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0691,2-Dibromoethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0681,2-Dichlorobenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0661,2-Dichloroethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0621,2-Dichloropropane
15 8260B P7D03945003.1 4/24/17 20:48 ANGmg/kg dry 0.761,3,5-Trimethylbenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0741,3-Dichloropropane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0811,4-Dichlorobenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0702,2-Dichloropropane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0842-Chlorotoluene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0724-Chlorotoluene
0.36 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.0784-Isopropyltoluene
BRL 8260B P7D0394501.2 4/24/17 20:20 ANGmg/kg dry 0.24Acetone
1.2 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.069Benzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.073Bromobenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.081Bromochloromethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.070Bromodichloromethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.084Bromoform
BRL 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.081Bromomethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.075Carbon Tetrachloride
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.062Chlorobenzene
BRL 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.064Chloroethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.072Chloroform
BRL 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.069Chloromethane
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.065cis-1,2-Dichloroethylene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.068cis-1,3-Dichloropropylene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.066Dibromochloromethane
BRL 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.080Dichlorodifluoromethane
21 8260B P7D03945003.1 4/24/17 20:48 ANGmg/kg dry 0.70Ethylbenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.065Isopropyl Ether
2.2 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.072Isopropylbenzene (Cumene)
81 8260B P7D03945006.2 4/24/17 20:48 ANGmg/kg dry 1.5m,p-Xylenes
0.49 8260B P7D0394501.2 4/24/17 20:20 ANGJmg/kg dry 0.070Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0394501.2 4/24/17 20:20 ANGmg/kg dry 0.051Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0394501.2 4/24/17 20:20 ANGmg/kg dry 0.054Methyl Isobutyl Ketone
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.067Methylene Chloride
0.22 8260B P7D0394500.31 4/24/17 20:20 ANGJmg/kg dry 0.065Methyl-tert-Butyl Ether
5.9 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.047Naphthalene
1.5 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.062n-Butylbenzene
7.8 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.073n-Propylbenzene
32 8260B P7D03945003.1 4/24/17 20:48 ANGmg/kg dry 0.68o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 68 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-16 (7-9)
Prism Sample ID: 7040298-14
Prism Work Order: 7040298
Time Collected: 04/13/17 09:20
Time Submitted: 04/17/17 08:00
0.78 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.077sec-Butylbenzene
0.49 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.068Styrene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.072tert-Butylbenzene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.066Tetrachloroethylene
36 8260B P7D03945003.1 4/24/17 20:48 ANGmg/kg dry 0.66Toluene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.071trans-1,2-Dichloroethylene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.066trans-1,3-Dichloropropylene
BRL 8260B P7D0394500.31 4/24/17 20:20 ANGmg/kg dry 0.067Trichloroethylene
BRL 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.088Trichlorofluoromethane
BRL 8260B P7D0394501.2 4/24/17 20:20 ANGmg/kg dry 0.051Vinyl acetate
BRL 8260B P7D0394500.62 4/24/17 20:20 ANGmg/kg dry 0.086Vinyl chloride
110 8260B P7D03945009.3 4/24/17 20:48 ANGmg/kg dry 2.2Xylenes, total
Surrogate Recovery Control Limits
70-13096 %4-Bromofluorobenzene
70-13077 %Dibromofluoromethane
70-13090 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 69 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-17 (0-2)
Prism Sample ID: 7040298-15
Prism Work Order: 7040298
Time Collected: 04/13/17 09:00
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
83.5 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.611,2,4-Trichlorobenzene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.601,2-Dichlorobenzene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.551,3-Dichlorobenzene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.581,4-Dichlorobenzene
25 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.761-Methylnaphthalene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.742,4,6-Trichlorophenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.762,4-Dichlorophenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.602,4-Dimethylphenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.552,4-Dinitrophenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.482,4-Dinitrotoluene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.522,6-Dinitrotoluene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.572-Chloronaphthalene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.562-Chlorophenol
32 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.632-Methylnaphthalene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.502-Methylphenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.722-Nitrophenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.783,3'-Dichlorobenzidine
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.493/4-Methylphenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.594,6-Dinitro-2-methylphenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.684-Bromophenyl phenyl ether
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.554-Chloro-3-methylphenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.474-Chloroaniline
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.514-Chlorophenyl phenyl ether
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.614-Nitrophenol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.54Acenaphthene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.57Acenaphthylene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.63Anthracene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.52Azobenzene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.52Benzo(a)anthracene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.43Benzo(a)pyrene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.46Benzo(b)fluoranthene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.43Benzo(g,h,i)perylene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.52Benzo(k)fluoranthene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.33Benzoic Acid
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.52Benzyl alcohol
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.68bis(2-Chloroethoxy)methane
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.56Bis(2-Chloroethyl)ether
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.67Bis(2-chloroisopropyl)ether
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.58Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 70 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-17 (0-2)
Prism Sample ID: 7040298-15
Prism Work Order: 7040298
Time Collected: 04/13/17 09:00
Time Submitted: 04/17/17 08:00
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.56Butyl benzyl phthalate
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.50Chrysene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.48Dibenzo(a,h)anthracene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.60Dibenzofuran
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.54Diethyl phthalate
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.52Dimethyl phthalate
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.56Di-n-butyl phthalate
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.48Di-n-octyl phthalate
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.50Fluoranthene
9.1 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.57Fluorene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.63Hexachlorobenzene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.71Hexachlorobutadiene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.70Hexachlorocyclopentadiene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.66Hexachloroethane
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.45Indeno(1,2,3-cd)pyrene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.53Isophorone
8.7 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.63Naphthalene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.56Nitrobenzene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.62N-Nitroso-di-n-propylamine
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.60N-Nitrosodiphenylamine
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.47Pentachlorophenol
12 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.51Phenanthrene
BRL 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.58Phenol
4.7 8270D P7D0274103.9 4/21/17 12:04 JMVmg/kg dry 0.52Pyrene
Surrogate Recovery Control Limits
39-13288 %2,4,6-Tribromophenol
44-11589 %2-Fluorobiphenyl
35-11582 %2-Fluorophenol
37-122195 %Nitrobenzene-d5 SR
34-12187 %Phenol-d5
54-127105 %Terphenyl-d14
Total Metals
5.4 6020B P7D0257100.30 4/25/17 0:58 BGMmg/kg dry 0.056Lead
Volatile Organic Compounds by GC/MS (Medium Level)
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0751,1,1,2-Tetrachloroethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0691,1,1-Trichloroethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0571,1,2,2-Tetrachloroethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0721,1,2-Trichloroethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0781,1-Dichloroethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0851,1-Dichloroethylene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0671,1-Dichloropropylene
BRL 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.0701,2,3-Trichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 71 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-17 (0-2)
Prism Sample ID: 7040298-15
Prism Work Order: 7040298
Time Collected: 04/13/17 09:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.101,2,3-Trichloropropane
BRL 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.0641,2,4-Trichlorobenzene
11 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0651,2,4-Trimethylbenzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0661,2-Dibromoethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0641,2-Dichloroethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0591,2-Dichloropropane
1.0 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0731,3,5-Trimethylbenzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0711,3-Dichloropropane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0781,4-Dichlorobenzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0672,2-Dichloropropane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0812-Chlorotoluene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0694-Chlorotoluene
1.5 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.0744-Isopropyltoluene
BRL 8260B P7D0394501.2 4/24/17 19:25 ANGmg/kg dry 0.23Acetone
3.8 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.066Benzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.070Bromobenzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.078Bromochloromethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.067Bromodichloromethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.080Bromoform
BRL 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.077Bromomethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.072Carbon Tetrachloride
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.060Chlorobenzene
BRL 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.061Chloroethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.069Chloroform
BRL 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.066Chloromethane
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.062cis-1,2-Dichloroethylene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.065cis-1,3-Dichloropropylene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.063Dibromochloromethane
BRL 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.076Dichlorodifluoromethane
5.4 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.067Ethylbenzene
0.41 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.062Isopropyl Ether
0.72 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.069Isopropylbenzene (Cumene)
9.8 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.14m,p-Xylenes
BRL 8260B P7D0394501.2 4/24/17 19:25 ANGmg/kg dry 0.067Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0394501.2 4/24/17 19:25 ANGmg/kg dry 0.049Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0394501.2 4/24/17 19:25 ANGmg/kg dry 0.052Methyl Isobutyl Ketone
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.064Methylene Chloride
1.3 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.062Methyl-tert-Butyl Ether
4.1 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.045Naphthalene
2.1 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.059n-Butylbenzene
1.8 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.070n-Propylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 72 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-17 (0-2)
Prism Sample ID: 7040298-15
Prism Work Order: 7040298
Time Collected: 04/13/17 09:00
Time Submitted: 04/17/17 08:00
0.88 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.065o-Xylene
1.9 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.073sec-Butylbenzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.065Styrene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.069tert-Butylbenzene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.063Tetrachloroethylene
1.5 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.063Toluene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.068trans-1,2-Dichloroethylene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.063trans-1,3-Dichloropropylene
BRL 8260B P7D0394500.30 4/24/17 19:25 ANGmg/kg dry 0.064Trichloroethylene
BRL 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.084Trichlorofluoromethane
BRL 8260B P7D0394501.2 4/24/17 19:25 ANGmg/kg dry 0.049Vinyl acetate
BRL 8260B P7D0394500.59 4/24/17 19:25 ANGmg/kg dry 0.082Vinyl chloride
11 8260B P7D0394500.89 4/24/17 19:25 ANGmg/kg dry 0.21Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-13078 %Dibromofluoromethane
70-13092 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 73 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-17 (7-9)
Prism Sample ID: 7040298-16
Prism Work Order: 7040298
Time Collected: 04/13/17 09:05
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
75.0 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.691,2,4-Trichlorobenzene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.671,2-Dichlorobenzene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.621,3-Dichlorobenzene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.641,4-Dichlorobenzene
38 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.851-Methylnaphthalene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.832,4,6-Trichlorophenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.852,4-Dichlorophenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.672,4-Dimethylphenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.612,4-Dinitrophenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.532,4-Dinitrotoluene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.592,6-Dinitrotoluene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.642-Chloronaphthalene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.622-Chlorophenol
54 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.702-Methylnaphthalene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.562-Methylphenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.802-Nitrophenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.873,3'-Dichlorobenzidine
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.543/4-Methylphenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.664,6-Dinitro-2-methylphenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.764-Bromophenyl phenyl ether
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.624-Chloro-3-methylphenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.534-Chloroaniline
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.574-Chlorophenyl phenyl ether
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.684-Nitrophenol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.60Acenaphthene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.64Acenaphthylene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.71Anthracene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.58Azobenzene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.58Benzo(a)anthracene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.48Benzo(a)pyrene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.51Benzo(b)fluoranthene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.48Benzo(g,h,i)perylene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.58Benzo(k)fluoranthene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.37Benzoic Acid
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.58Benzyl alcohol
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.76bis(2-Chloroethoxy)methane
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.62Bis(2-Chloroethyl)ether
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.75Bis(2-chloroisopropyl)ether
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.65Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 74 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-17 (7-9)
Prism Sample ID: 7040298-16
Prism Work Order: 7040298
Time Collected: 04/13/17 09:05
Time Submitted: 04/17/17 08:00
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.63Butyl benzyl phthalate
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.55Chrysene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.54Dibenzo(a,h)anthracene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.67Dibenzofuran
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.61Diethyl phthalate
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.58Dimethyl phthalate
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.63Di-n-butyl phthalate
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.54Di-n-octyl phthalate
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.56Fluoranthene
11 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.63Fluorene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.70Hexachlorobenzene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.79Hexachlorobutadiene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.79Hexachlorocyclopentadiene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.74Hexachloroethane
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.51Indeno(1,2,3-cd)pyrene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.60Isophorone
17 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.71Naphthalene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.63Nitrobenzene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.69N-Nitroso-di-n-propylamine
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.67N-Nitrosodiphenylamine
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.52Pentachlorophenol
16 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.57Phenanthrene
BRL 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.65Phenol
4.8 8270D P7D0274104.4 4/21/17 12:49 JMVmg/kg dry 0.58Pyrene
Surrogate Recovery Control Limits
39-13278 %2,4,6-Tribromophenol
44-11591 %2-Fluorobiphenyl
35-11577 %2-Fluorophenol
37-12255 %Nitrobenzene-d5
34-12185 %Phenol-d5
54-127108 %Terphenyl-d14
Total Metals
5.6 6020B P7D0257100.33 4/25/17 1:03 BGMmg/kg dry 0.063Lead
Volatile Organic Compounds by GC/MS (Medium Level)
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0721,1,1,2-Tetrachloroethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0661,1,1-Trichloroethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0551,1,2,2-Tetrachloroethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0691,1,2-Trichloroethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0751,1-Dichloroethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0811,1-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0641,1-Dichloropropylene
BRL 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.0671,2,3-Trichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 75 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-17 (7-9)
Prism Sample ID: 7040298-16
Prism Work Order: 7040298
Time Collected: 04/13/17 09:05
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0991,2,3-Trichloropropane
BRL 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.0611,2,4-Trichlorobenzene
31 8260B P7D03945002.8 4/24/17 21:43 ANGmg/kg dry 0.631,2,4-Trimethylbenzene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0631,2-Dibromoethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0611,2-Dichloroethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0561,2-Dichloropropane
3.3 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0701,3,5-Trimethylbenzene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0561,3-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0681,3-Dichloropropane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0741,4-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0642,2-Dichloropropane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0772-Chlorotoluene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0664-Chlorotoluene
3.8 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.0714-Isopropyltoluene
BRL 8260B P7D0394501.1 4/24/17 21:15 ANGmg/kg dry 0.22Acetone
15 8260B P7D03945002.8 4/24/17 21:43 ANGmg/kg dry 0.63Benzene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.066Bromobenzene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.075Bromochloromethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.064Bromodichloromethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.076Bromoform
BRL 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.074Bromomethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.068Carbon Tetrachloride
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.057Chlorobenzene
BRL 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.058Chloroethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.065Chloroform
BRL 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.063Chloromethane
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.059cis-1,2-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.062cis-1,3-Dichloropropylene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.060Dibromochloromethane
BRL 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.073Dichlorodifluoromethane
21 8260B P7D03945002.8 4/24/17 21:43 ANGmg/kg dry 0.64Ethylbenzene
0.95 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.059Isopropyl Ether
2.4 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.066Isopropylbenzene (Cumene)
43 8260B P7D03945005.7 4/24/17 21:43 ANGmg/kg dry 1.4m,p-Xylenes
BRL 8260B P7D0394501.1 4/24/17 21:15 ANGmg/kg dry 0.064Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0394501.1 4/24/17 21:15 ANGmg/kg dry 0.046Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0394501.1 4/24/17 21:15 ANGmg/kg dry 0.050Methyl Isobutyl Ketone
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.061Methylene Chloride
2.5 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.059Methyl-tert-Butyl Ether
5.9 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.043Naphthalene
5.7 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.056n-Butylbenzene
5.8 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.067n-Propylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 76 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-17 (7-9)
Prism Sample ID: 7040298-16
Prism Work Order: 7040298
Time Collected: 04/13/17 09:05
Time Submitted: 04/17/17 08:00
5.2 8260B P7D03945002.8 4/24/17 21:43 ANGmg/kg dry 0.62o-Xylene
5.2 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.070sec-Butylbenzene
0.14 8260B P7D0394500.28 4/24/17 21:15 ANGJmg/kg dry 0.063Styrene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.066tert-Butylbenzene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.060Tetrachloroethylene
9.6 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.060Toluene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.065trans-1,2-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.060trans-1,3-Dichloropropylene
BRL 8260B P7D0394500.28 4/24/17 21:15 ANGmg/kg dry 0.061Trichloroethylene
BRL 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.080Trichlorofluoromethane
BRL 8260B P7D0394501.1 4/24/17 21:15 ANGmg/kg dry 0.047Vinyl acetate
BRL 8260B P7D0394500.57 4/24/17 21:15 ANGmg/kg dry 0.079Vinyl chloride
48 8260B P7D03945008.5 4/24/17 21:43 ANGmg/kg dry 2.0Xylenes, total
Surrogate Recovery Control Limits
70-13093 %4-Bromofluorobenzene
70-13065 %Dibromofluoromethane SR2
70-13091 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 77 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-18 (0-2)
Prism Sample ID: 7040298-17
Prism Work Order: 7040298
Time Collected: 04/13/17 08:40
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
84.0 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0601,2,4-Trichlorobenzene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0581,2-Dichlorobenzene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0541,3-Dichlorobenzene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0561,4-Dichlorobenzene
0.34 8270D P7D027410.38 4/19/17 20:57 JMVJmg/kg dry 0.0741-Methylnaphthalene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0722,4,6-Trichlorophenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0742,4-Dichlorophenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0592,4-Dimethylphenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0542,4-Dinitrophenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0472,4-Dinitrotoluene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0512,6-Dinitrotoluene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0562-Chloronaphthalene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0552-Chlorophenol
0.65 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0622-Methylnaphthalene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0492-Methylphenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0702-Nitrophenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0763,3'-Dichlorobenzidine
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0473/4-Methylphenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0584,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0664-Bromophenyl phenyl ether
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0544-Chloro-3-methylphenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0464-Chloroaniline
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0504-Chlorophenyl phenyl ether
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.0594-Nitrophenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.052Acenaphthene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.056Acenaphthylene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.062Anthracene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.051Azobenzene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.050Benzo(a)anthracene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.042Benzo(a)pyrene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.045Benzo(b)fluoranthene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.042Benzo(g,h,i)perylene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.050Benzo(k)fluoranthene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.032Benzoic Acid
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.051Benzyl alcohol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.067bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.054Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.066Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.057Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 78 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-18 (0-2)
Prism Sample ID: 7040298-17
Prism Work Order: 7040298
Time Collected: 04/13/17 08:40
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.055Butyl benzyl phthalate
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.048Chrysene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.047Dibenzo(a,h)anthracene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.059Dibenzofuran
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.053Diethyl phthalate
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.051Dimethyl phthalate
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.055Di-n-butyl phthalate
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.047Di-n-octyl phthalate
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.049Fluoranthene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.055Fluorene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.061Hexachlorobenzene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.069Hexachlorobutadiene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.069Hexachlorocyclopentadiene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.064Hexachloroethane
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.044Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.052Isophorone
0.51 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.062Naphthalene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.055Nitrobenzene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.061N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.059N-Nitrosodiphenylamine
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.045Pentachlorophenol
0.16 8270D P7D027410.38 4/19/17 20:57 JMVJmg/kg dry 0.050Phenanthrene
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.057Phenol
BRL 8270D P7D027410.38 4/19/17 20:57 JMVmg/kg dry 0.051Pyrene
Surrogate Recovery Control Limits
39-13272 %2,4,6-Tribromophenol
44-11567 %2-Fluorobiphenyl
35-11566 %2-Fluorophenol
37-12262 %Nitrobenzene-d5
34-12165 %Phenol-d5
54-12784 %Terphenyl-d14
Total Metals
5.3 6020B P7D0257100.30 4/25/17 1:09 BGMmg/kg dry 0.056Lead
Volatile Organic Compounds by GC/MS (Medium Level)
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0701,1,1,2-Tetrachloroethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0641,1,1-Trichloroethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0531,1,2,2-Tetrachloroethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0671,1,2-Trichloroethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0721,1-Dichloroethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0791,1-Dichloroethylene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0621,1-Dichloropropylene
BRL 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.0651,2,3-Trichlorobenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0961,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 79 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-18 (0-2)
Prism Sample ID: 7040298-17
Prism Work Order: 7040298
Time Collected: 04/13/17 08:40
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.0601,2,4-Trichlorobenzene
59 8260B P7D03945002.7 4/24/17 18:58 ANGmg/kg dry 0.611,2,4-Trimethylbenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0611,2-Dibromoethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0601,2-Dichlorobenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0591,2-Dichloroethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0551,2-Dichloropropane
22 8260B P7D03945002.7 4/24/17 18:58 ANGmg/kg dry 0.671,3,5-Trimethylbenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0541,3-Dichlorobenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0661,3-Dichloropropane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0721,4-Dichlorobenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0622,2-Dichloropropane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0752-Chlorotoluene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0644-Chlorotoluene
0.53 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.0694-Isopropyltoluene
BRL 8260B P7D0394501.1 4/24/17 18:30 ANGmg/kg dry 0.21Acetone
0.18 8260B P7D0394500.27 4/24/17 18:30 ANGJmg/kg dry 0.061Benzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.064Bromobenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.072Bromochloromethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.062Bromodichloromethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.074Bromoform
BRL 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.072Bromomethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.066Carbon Tetrachloride
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.055Chlorobenzene
BRL 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.057Chloroethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.063Chloroform
BRL 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.061Chloromethane
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.058cis-1,2-Dichloroethylene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.060cis-1,3-Dichloropropylene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.059Dibromochloromethane
BRL 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.071Dichlorodifluoromethane
23 8260B P7D03945002.7 4/24/17 18:58 ANGmg/kg dry 0.62Ethylbenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.057Isopropyl Ether
2.9 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.064Isopropylbenzene (Cumene)
98 8260B P7D03945005.5 4/24/17 18:58 ANGmg/kg dry 1.3m,p-Xylenes
BRL 8260B P7D0394501.1 4/24/17 18:30 ANGmg/kg dry 0.062Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0394501.1 4/24/17 18:30 ANGmg/kg dry 0.045Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0394501.1 4/24/17 18:30 ANGmg/kg dry 0.048Methyl Isobutyl Ketone
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.059Methylene Chloride
0.12 8260B P7D0394500.27 4/24/17 18:30 ANGJmg/kg dry 0.057Methyl-tert-Butyl Ether
2.7 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.042Naphthalene
1.5 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.055n-Butylbenzene
8.8 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.065n-Propylbenzene
38 8260B P7D03945002.7 4/24/17 18:58 ANGmg/kg dry 0.60o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 80 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-18 (0-2)
Prism Sample ID: 7040298-17
Prism Work Order: 7040298
Time Collected: 04/13/17 08:40
Time Submitted: 04/17/17 08:00
1.1 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.068sec-Butylbenzene
0.28 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.061Styrene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.064tert-Butylbenzene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.058Tetrachloroethylene
25 8260B P7D03945002.7 4/24/17 18:58 ANGmg/kg dry 0.58Toluene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.063trans-1,2-Dichloroethylene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.059trans-1,3-Dichloropropylene
BRL 8260B P7D0394500.27 4/24/17 18:30 ANGmg/kg dry 0.059Trichloroethylene
BRL 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.078Trichlorofluoromethane
BRL 8260B P7D0394501.1 4/24/17 18:30 ANGmg/kg dry 0.046Vinyl acetate
BRL 8260B P7D0394500.55 4/24/17 18:30 ANGmg/kg dry 0.076Vinyl chloride
140 8260B P7D03945008.2 4/24/17 18:58 ANGmg/kg dry 1.9Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-13056 %Dibromofluoromethane SR2
70-13091 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 81 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-18 (2-4)
Prism Sample ID: 7040298-18
Prism Work Order: 7040298
Time Collected: 04/13/17 08:40
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
74.6 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0661,2-Dichlorobenzene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0631,4-Dichlorobenzene
4.3 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0842,4-Dichlorophenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0532,4-Dinitrotoluene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0582,6-Dinitrotoluene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0632-Chloronaphthalene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0612-Chlorophenol
6.6 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0792-Nitrophenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0853,3'-Dichlorobenzidine
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0614-Chloro-3-methylphenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.0674-Nitrophenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.059Acenaphthene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.063Acenaphthylene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.070Anthracene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.057Benzo(a)anthracene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.057Benzyl alcohol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 82 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-18 (2-4)
Prism Sample ID: 7040298-18
Prism Work Order: 7040298
Time Collected: 04/13/17 08:40
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.062Butyl benzyl phthalate
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.055Chrysene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.053Dibenzo(a,h)anthracene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.066Dibenzofuran
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.060Diethyl phthalate
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.055Fluoranthene
0.33 8270D P7D027410.43 4/19/17 21:20 JMVJmg/kg dry 0.062Fluorene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.069Hexachlorobenzene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.078Hexachlorobutadiene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.072Hexachloroethane
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.050Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.059Isophorone
6.6 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.070Naphthalene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.061Nitrobenzene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.051Pentachlorophenol
0.58 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.064Phenol
BRL 8270D P7D027410.43 4/19/17 21:20 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13266 %2,4,6-Tribromophenol
44-11562 %2-Fluorobiphenyl
35-11551 %2-Fluorophenol
37-12260 %Nitrobenzene-d5
34-12159 %Phenol-d5
54-12778 %Terphenyl-d14
Total Metals
6.2 6020B P7D0257100.33 4/25/17 1:14 BGMmg/kg dry 0.063Lead
Volatile Organic Compounds by GC/MS (Medium Level)
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0791,1,1,2-Tetrachloroethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0731,1,1-Trichloroethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0611,1,2,2-Tetrachloroethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0761,1,2-Trichloroethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0831,1-Dichloroethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0901,1-Dichloroethylene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0711,1-Dichloropropylene
BRL 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.0741,2,3-Trichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 83 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-18 (2-4)
Prism Sample ID: 7040298-18
Prism Work Order: 7040298
Time Collected: 04/13/17 08:40
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.111,2,3-Trichloropropane
BRL 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.0681,2,4-Trichlorobenzene
97 8260B P7D03945003.1 4/25/17 11:50 ANGmg/kg dry 0.691,2,4-Trimethylbenzene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0701,2-Dibromoethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0691,2-Dichlorobenzene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0671,2-Dichloroethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0621,2-Dichloropropane
31 8260B P7D03945003.1 4/25/17 11:50 ANGmg/kg dry 0.771,3,5-Trimethylbenzene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0751,3-Dichloropropane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0821,4-Dichlorobenzene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0712,2-Dichloropropane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0852-Chlorotoluene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0734-Chlorotoluene
0.71 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.0794-Isopropyltoluene
BRL 8260B P7D0394501.2 4/24/17 17:07 ANGmg/kg dry 0.24Acetone
1.2 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.070Benzene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.073Bromobenzene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.082Bromochloromethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.071Bromodichloromethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.085Bromoform
BRL 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.082Bromomethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.076Carbon Tetrachloride
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.063Chlorobenzene
BRL 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.065Chloroethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.072Chloroform
BRL 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.070Chloromethane
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.066cis-1,2-Dichloroethylene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.069cis-1,3-Dichloropropylene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.067Dibromochloromethane
BRL 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.081Dichlorodifluoromethane
39 8260B P7D03945003.1 4/25/17 11:50 ANGmg/kg dry 0.71Ethylbenzene
0.52 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.065Isopropyl Ether
4.1 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.072Isopropylbenzene (Cumene)
160 8260B P7D03945006.2 4/25/17 11:50 ANGmg/kg dry 1.5m,p-Xylenes
BRL 8260B P7D0394501.2 4/24/17 17:07 ANGmg/kg dry 0.071Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0394501.2 4/24/17 17:07 ANGmg/kg dry 0.051Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0394501.2 4/24/17 17:07 ANGmg/kg dry 0.055Methyl Isobutyl Ketone
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.068Methylene Chloride
2.9 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.065Methyl-tert-Butyl Ether
9.9 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.048Naphthalene
2.9 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.062n-Butylbenzene
12 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.074n-Propylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 84 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-18 (2-4)
Prism Sample ID: 7040298-18
Prism Work Order: 7040298
Time Collected: 04/13/17 08:40
Time Submitted: 04/17/17 08:00
66 8260B P7D03945003.1 4/25/17 11:50 ANGmg/kg dry 0.69o-Xylene
1.5 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.078sec-Butylbenzene
0.77 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.069Styrene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.073tert-Butylbenzene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.066Tetrachloroethylene
76 8260B P7D03945003.1 4/25/17 11:50 ANGmg/kg dry 0.66Toluene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.072trans-1,2-Dichloroethylene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.067trans-1,3-Dichloropropylene
BRL 8260B P7D0394500.31 4/24/17 17:07 ANGmg/kg dry 0.068Trichloroethylene
BRL 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.089Trichlorofluoromethane
BRL 8260B P7D0394501.2 4/24/17 17:07 ANGmg/kg dry 0.052Vinyl acetate
BRL 8260B P7D0394500.62 4/24/17 17:07 ANGmg/kg dry 0.087Vinyl chloride
230 8260B P7D03945009.4 4/25/17 11:50 ANGmg/kg dry 2.2Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-13059 %Dibromofluoromethane SR2
70-13090 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 85 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-19 (0-2)
Prism Sample ID: 7040298-19
Prism Work Order: 7040298
Time Collected: 04/13/17 08:35
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
73.8 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0691,2,4-Trichlorobenzene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0671,2-Dichlorobenzene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0621,3-Dichlorobenzene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0651,4-Dichlorobenzene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0851-Methylnaphthalene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0832,4,6-Trichlorophenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0852,4-Dichlorophenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0682,4-Dimethylphenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0622,4-Dinitrophenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0542,4-Dinitrotoluene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0592,6-Dinitrotoluene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0642-Chloronaphthalene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0632-Chlorophenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0712-Methylnaphthalene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0572-Methylphenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0802-Nitrophenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0873,3'-Dichlorobenzidine
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0543/4-Methylphenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0664,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0764-Bromophenyl phenyl ether
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0624-Chloro-3-methylphenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0534-Chloroaniline
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0574-Chlorophenyl phenyl ether
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.0684-Nitrophenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.060Acenaphthene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.064Acenaphthylene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.071Anthracene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.058Azobenzene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.058Benzo(a)anthracene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.048Benzo(a)pyrene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.051Benzo(b)fluoranthene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.048Benzo(g,h,i)perylene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.058Benzo(k)fluoranthene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.037Benzoic Acid
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.058Benzyl alcohol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.077bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.062Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.076Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.066Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 86 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-19 (0-2)
Prism Sample ID: 7040298-19
Prism Work Order: 7040298
Time Collected: 04/13/17 08:35
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.063Butyl benzyl phthalate
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.056Chrysene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.054Dibenzo(a,h)anthracene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.067Dibenzofuran
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.061Diethyl phthalate
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.058Dimethyl phthalate
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.063Di-n-butyl phthalate
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.054Di-n-octyl phthalate
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.056Fluoranthene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.063Fluorene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.070Hexachlorobenzene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.079Hexachlorobutadiene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.079Hexachlorocyclopentadiene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.074Hexachloroethane
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.051Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.060Isophorone
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.071Naphthalene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.063Nitrobenzene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.070N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.067N-Nitrosodiphenylamine
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.052Pentachlorophenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.057Phenanthrene
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.065Phenol
BRL 8270D P7D027410.44 4/19/17 21:42 JMVmg/kg dry 0.059Pyrene
Surrogate Recovery Control Limits
39-13266 %2,4,6-Tribromophenol
44-11559 %2-Fluorobiphenyl
35-11558 %2-Fluorophenol
37-12253 %Nitrobenzene-d5
34-12159 %Phenol-d5
54-12778 %Terphenyl-d14
Total Metals
0.46 6020B P7D0257100.34 4/25/17 1:19 BGMmg/kg dry 0.064Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000521,1,1,2-Tetrachloroethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000301,1,1-Trichloroethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000431,1,2,2-Tetrachloroethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000561,1,2-Trichloroethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000281,1-Dichloroethylene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000361,2,3-Trichlorobenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000801,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 87 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-19 (0-2)
Prism Sample ID: 7040298-19
Prism Work Order: 7040298
Time Collected: 04/13/17 08:35
Time Submitted: 04/17/17 08:00
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000471,2,4-Trichlorobenzene
0.023 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000481,2,4-Trimethylbenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000301,2-Dichlorobenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000381,2-Dichloroethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000391,2-Dichloropropane
0.0051 8260B P7D038110.0063 4/24/17 13:54 ANGJmg/kg dry 0.000481,3,5-Trimethylbenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000421,3-Dichlorobenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000321,3-Dichloropropane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000384-Chlorotoluene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.000304-Isopropyltoluene
0.088 8260B P7D038110.063 4/24/17 13:54 ANGmg/kg dry 0.0015Acetone
0.0061 8260B P7D038110.0038 4/24/17 13:54 ANGmg/kg dry 0.00037Benzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00052Bromobenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00035Bromochloromethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00071Bromoform
BRL 8260B P7D038110.013 4/24/17 13:54 ANGmg/kg dry 0.00078Bromomethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00033Chlorobenzene
BRL 8260B P7D038110.013 4/24/17 13:54 ANGmg/kg dry 0.00052Chloroethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00045Chloroform
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00042Chloromethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00027cis-1,2-Dichloroethylene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00029Dichlorodifluoromethane
0.0068 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00024Ethylbenzene
0.0039 8260B P7D038110.0063 4/24/17 13:54 ANGJmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00037Isopropylbenzene (Cumene)
0.0030 8260B P7D038110.013 4/24/17 13:54 ANGJmg/kg dry 0.00058m,p-Xylenes
BRL 8260B P7D038110.063 4/24/17 13:54 ANGmg/kg dry 0.00057Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D038110.13 4/24/17 13:54 ANGmg/kg dry 0.00057Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D038110.063 4/24/17 13:54 ANGmg/kg dry 0.00054Methyl Isobutyl Ketone
0.0076 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00035Methylene Chloride
0.0036 8260B P7D038110.013 4/24/17 13:54 ANGJmg/kg dry 0.00020Methyl-tert-Butyl Ether
0.0050 8260B P7D038110.013 4/24/17 13:54 ANGJmg/kg dry 0.00020Naphthalene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00032n-Butylbenzene
0.0045 8260B P7D038110.0063 4/24/17 13:54 ANGJmg/kg dry 0.00037n-Propylbenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00026o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 88 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-19 (0-2)
Prism Sample ID: 7040298-19
Prism Work Order: 7040298
Time Collected: 04/13/17 08:35
Time Submitted: 04/17/17 08:00
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00038Styrene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00036Toluene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00038trans-1,2-Dichloroethylene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00041Trichloroethylene
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00041Trichlorofluoromethane
BRL 8260B P7D038110.031 4/24/17 13:54 ANGmg/kg dry 0.00086Vinyl acetate
BRL 8260B P7D038110.0063 4/24/17 13:54 ANGmg/kg dry 0.00030Vinyl chloride
0.0030 8260B P7D038110.019 4/24/17 13:54 ANGJmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-12389 %Dibromofluoromethane
76-12994 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 89 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-19 (2-4)
Prism Sample ID: 7040298-20
Prism Work Order: 7040298
Time Collected: 04/13/17 08:35
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
70.2 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0721,2,4-Trichlorobenzene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0701,2-Dichlorobenzene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0651,3-Dichlorobenzene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0671,4-Dichlorobenzene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0881-Methylnaphthalene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0862,4,6-Trichlorophenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0892,4-Dichlorophenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0702,4-Dimethylphenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0642,4-Dinitrophenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0562,4-Dinitrotoluene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0612,6-Dinitrotoluene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0662-Chloronaphthalene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0652-Chlorophenol
0.17 8270D P7D027410.46 4/19/17 22:05 JMVJmg/kg dry 0.0732-Methylnaphthalene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0592-Methylphenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0842-Nitrophenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0913,3'-Dichlorobenzidine
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0573/4-Methylphenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0694,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0794-Bromophenyl phenyl ether
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0644-Chloro-3-methylphenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0554-Chloroaniline
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0604-Chlorophenyl phenyl ether
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.0714-Nitrophenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.062Acenaphthene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.066Acenaphthylene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.074Anthracene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.061Azobenzene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.060Benzo(a)anthracene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.050Benzo(a)pyrene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.053Benzo(b)fluoranthene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.050Benzo(g,h,i)perylene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.060Benzo(k)fluoranthene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.039Benzoic Acid
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.060Benzyl alcohol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.080bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.065Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.078Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.068Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 90 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-19 (2-4)
Prism Sample ID: 7040298-20
Prism Work Order: 7040298
Time Collected: 04/13/17 08:35
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.065Butyl benzyl phthalate
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.058Chrysene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.056Dibenzo(a,h)anthracene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.070Dibenzofuran
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.063Diethyl phthalate
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.061Dimethyl phthalate
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.065Di-n-butyl phthalate
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.056Di-n-octyl phthalate
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.059Fluoranthene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.066Fluorene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.073Hexachlorobenzene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.082Hexachlorobutadiene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.082Hexachlorocyclopentadiene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.077Hexachloroethane
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.053Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.062Isophorone
0.13 8270D P7D027410.46 4/19/17 22:05 JMVJmg/kg dry 0.074Naphthalene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.065Nitrobenzene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.072N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.070N-Nitrosodiphenylamine
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.054Pentachlorophenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.060Phenanthrene
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.068Phenol
BRL 8270D P7D027410.46 4/19/17 22:05 JMVmg/kg dry 0.061Pyrene
Surrogate Recovery Control Limits
39-13265 %2,4,6-Tribromophenol
44-11559 %2-Fluorobiphenyl
35-11559 %2-Fluorophenol
37-12255 %Nitrobenzene-d5
34-12161 %Phenol-d5
54-12780 %Terphenyl-d14
Total Metals
6.2 6020B P7D0287100.36 4/25/17 2:11 BGMmg/kg dry 0.068Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000501,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000291,1,1-Trichloroethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000411,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000541,1,2-Trichloroethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000331,1-Dichloropropylene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000771,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 91 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-19 (2-4)
Prism Sample ID: 7040298-20
Prism Work Order: 7040298
Time Collected: 04/13/17 08:35
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000451,2,4-Trichlorobenzene
See 8260ML 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000461,2,4-Trimethylbenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000281,2-Dichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000361,2-Dichloroethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000381,2-Dichloropropane
0.20 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000461,3,5-Trimethylbenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000401,3-Dichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000301,3-Dichloropropane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000312-Chlorotoluene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000364-Chlorotoluene
0.0065 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.000294-Isopropyltoluene
0.071 8260B P7D036210.061 4/21/17 16:58 ANGmg/kg dry 0.0015Acetone
0.25 8260B P7D036210.0036 4/21/17 16:58 ANGLLmg/kg dry 0.00035Benzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00051Bromobenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00033Bromochloromethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00069Bromoform
BRL 8260B P7D036210.012 4/21/17 16:58 ANGmg/kg dry 0.00075Bromomethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00030Carbon Tetrachloride
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00032Chlorobenzene
BRL 8260B P7D036210.012 4/21/17 16:58 ANGmg/kg dry 0.00051Chloroethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00044Chloroform
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00041Chloromethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00028Dichlorodifluoromethane
See 8260ML 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00023Ethylbenzene
0.067 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00025Isopropyl Ether
0.024 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00036Isopropylbenzene (Cumene)
See 8260ML 8260B P7D036210.012 4/21/17 16:58 ANGmg/kg dry 0.00056m,p-Xylenes
BRL 8260B P7D036210.061 4/21/17 16:58 ANGmg/kg dry 0.00055Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.12 4/21/17 16:58 ANGmg/kg dry 0.00055Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.061 4/21/17 16:58 ANGmg/kg dry 0.00052Methyl Isobutyl Ketone
0.0079 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00034Methylene Chloride
0.067 8260B P7D036210.012 4/21/17 16:58 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether
0.18 8260B P7D036210.012 4/21/17 16:58 ANGmg/kg dry 0.00019Naphthalene
0.027 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00031n-Butylbenzene
0.068 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00036n-Propylbenzene
See 8260ML 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00025o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 92 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-19 (2-4)
Prism Sample ID: 7040298-20
Prism Work Order: 7040298
Time Collected: 04/13/17 08:35
Time Submitted: 04/17/17 08:00
0.0096 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00036Styrene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00029Tetrachloroethylene
0.16 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00035Toluene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00036trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00032trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00039Trichloroethylene
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00039Trichlorofluoromethane
BRL 8260B P7D036210.030 4/21/17 16:58 ANGmg/kg dry 0.00083Vinyl acetate
BRL 8260B P7D036210.0061 4/21/17 16:58 ANGmg/kg dry 0.00029Vinyl chloride
See 8260ML 8260B P7D036210.018 4/21/17 16:58 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-12384 %Dibromofluoromethane
76-12991 %Toluene-d8
Volatile Organic Compounds by GC/MS (Medium Level)
1.7 8260B P7D0394500.35 4/24/17 15:17 ANGmg/kg dry 0.0771,2,4-Trimethylbenzene
0.38 8260B P7D0394500.35 4/24/17 15:17 ANGmg/kg dry 0.079Ethylbenzene
1.6 8260B P7D0394500.70 4/24/17 15:17 ANGmg/kg dry 0.17m,p-Xylenes
0.85 8260B P7D0394500.35 4/24/17 15:17 ANGmg/kg dry 0.077o-Xylene
2.4 8260B P7D0394501.0 4/24/17 15:17 ANGmg/kg dry 0.24Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-13094 %Dibromofluoromethane
70-13092 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 93 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-20 (0-2)
Prism Sample ID: 7040298-21
Prism Work Order: 7040298
Time Collected: 04/13/17 08:15
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
76.2 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0631,4-Dichlorobenzene
1.1 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0612-Chlorophenol
2.0 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0782-Nitrophenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0853,3'-Dichlorobenzidine
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.0664-Nitrophenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.058Acenaphthene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.062Acenaphthylene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.069Anthracene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.056Benzo(k)fluoranthene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.057Benzyl alcohol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.073Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 94 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-20 (0-2)
Prism Sample ID: 7040298-21
Prism Work Order: 7040298
Time Collected: 04/13/17 08:15
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.054Chrysene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.065Dibenzofuran
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.059Diethyl phthalate
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.055Fluoranthene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.062Fluorene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.077Hexachlorobutadiene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.072Hexachloroethane
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.058Isophorone
1.5 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.069Naphthalene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.061Nitrobenzene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.065N-Nitrosodiphenylamine
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.051Pentachlorophenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.063Phenol
BRL 8270D P7D027410.43 4/19/17 22:27 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13276 %2,4,6-Tribromophenol
44-11569 %2-Fluorobiphenyl
35-11571 %2-Fluorophenol
37-12266 %Nitrobenzene-d5
34-12170 %Phenol-d5
54-12789 %Terphenyl-d14
Total Metals
9.9 6020B P7D0287100.33 4/25/17 2:16 BGMmg/kg dry 0.063Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000471,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000281,1,1-Trichloroethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000391,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000511,1,2-Trichloroethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000331,2,3-Trichlorobenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000731,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 95 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-20 (0-2)
Prism Sample ID: 7040298-21
Prism Work Order: 7040298
Time Collected: 04/13/17 08:15
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000431,2,4-Trichlorobenzene
See 8260ML 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000441,2,4-Trimethylbenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000341,2-Dichloroethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000361,2-Dichloropropane
See 8260ML 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000431,3,5-Trimethylbenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000381,3-Dichlorobenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000291,3-Dichloropropane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000302-Chlorotoluene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000344-Chlorotoluene
0.0073 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.000284-Isopropyltoluene
0.042 8260B P7D036210.057 4/21/17 17:25 ANGJmg/kg dry 0.0014Acetone
0.064 8260B P7D036210.0034 4/21/17 17:25 ANGmg/kg dry 0.00033Benzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00048Bromobenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00032Bromochloromethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00032Bromodichloromethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00065Bromoform
BRL 8260B P7D036210.011 4/21/17 17:25 ANGmg/kg dry 0.00071Bromomethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00029Carbon Tetrachloride
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00030Chlorobenzene
BRL 8260B P7D036210.011 4/21/17 17:25 ANGmg/kg dry 0.00048Chloroethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00041Chloroform
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00039Chloromethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00026Dichlorodifluoromethane
See 8260ML 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00022Ethylbenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00023Isopropyl Ether
0.033 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00034Isopropylbenzene (Cumene)
0.45 8260B P7D036210.011 4/21/17 17:25 ANGmg/kg dry 0.00053m,p-Xylenes
BRL 8260B P7D036210.057 4/21/17 17:25 ANGmg/kg dry 0.00052Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.11 4/21/17 17:25 ANGmg/kg dry 0.00052Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.057 4/21/17 17:25 ANGmg/kg dry 0.00049Methyl Isobutyl Ketone
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00032Methylene Chloride
BRL 8260B P7D036210.011 4/21/17 17:25 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether
0.22 8260B P7D036210.011 4/21/17 17:25 ANGmg/kg dry 0.00018Naphthalene
0.017 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00029n-Butylbenzene
0.10 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00034n-Propylbenzene
0.21 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00024o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 96 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-20 (0-2)
Prism Sample ID: 7040298-21
Prism Work Order: 7040298
Time Collected: 04/13/17 08:15
Time Submitted: 04/17/17 08:00
0.010 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00028sec-Butylbenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00035Styrene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00027Tetrachloroethylene
See 8260ML 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00033Toluene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00037Trichloroethylene
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00037Trichlorofluoromethane
BRL 8260B P7D036210.029 4/21/17 17:25 ANGmg/kg dry 0.00079Vinyl acetate
BRL 8260B P7D036210.0057 4/21/17 17:25 ANGmg/kg dry 0.00028Vinyl chloride
0.66 8260B P7D036210.017 4/21/17 17:25 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-12392 %Dibromofluoromethane
76-12989 %Toluene-d8
Volatile Organic Compounds by GC/MS (Medium Level)
1.6 8260B P7D0394500.30 4/24/17 15:45 ANGmg/kg dry 0.0681,2,4-Trimethylbenzene
0.60 8260B P7D0394500.30 4/24/17 15:45 ANGmg/kg dry 0.0751,3,5-Trimethylbenzene
0.41 8260B P7D0394500.30 4/24/17 15:45 ANGmg/kg dry 0.069Ethylbenzene
0.43 8260B P7D0394500.30 4/24/17 15:45 ANGmg/kg dry 0.065Toluene
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13093 %Dibromofluoromethane
70-13092 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 97 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-20 (2-4)
Prism Sample ID: 7040298-22
Prism Work Order: 7040298
Time Collected: 04/13/17 08:15
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
79.1 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0601,4-Dichlorobenzene
11 8270D P7D027452.0 4/20/17 12:28 JMVmg/kg dry 0.391-Methylnaphthalene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0772,4,6-Trichlorophenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0792,4-Dichlorophenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0632,4-Dimethylphenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0582-Chlorophenol
24 8270D P7D027452.0 4/20/17 12:28 JMVmg/kg dry 0.332-Methylnaphthalene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0752-Nitrophenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0813,3'-Dichlorobenzidine
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.066Anthracene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 98 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-20 (2-4)
Prism Sample ID: 7040298-22
Prism Work Order: 7040298
Time Collected: 04/13/17 08:15
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.052Chrysene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.052Fluoranthene
0.18 8270D P7D027410.41 4/19/17 22:50 JMVJmg/kg dry 0.059Fluorene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.074Hexachlorobutadiene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.073Hexachlorocyclopentadiene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.069Hexachloroethane
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.055Isophorone
24 8270D P7D027452.0 4/20/17 12:28 JMVmg/kg dry 0.33Naphthalene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.048Pentachlorophenol
0.22 8270D P7D027410.41 4/19/17 22:50 JMVJmg/kg dry 0.053Phenanthrene
BRL 8270D P7D027410.41 4/19/17 22:50 JMVmg/kg dry 0.060Phenol
0.11 8270D P7D027410.41 4/19/17 22:50 JMVJmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13263 %2,4,6-Tribromophenol
44-11561 %2-Fluorobiphenyl
35-11543 %2-Fluorophenol
37-1227 %Nitrobenzene-d5 A
34-12150 %Phenol-d5
54-12773 %Terphenyl-d14
Total Metals
7.6 6020B P7D0287100.31 4/25/17 2:22 BGMmg/kg dry 0.059Lead
Volatile Organic Compounds by GC/MS (Medium Level)
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0801,1,1,2-Tetrachloroethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0741,1,1-Trichloroethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0611,1,2,2-Tetrachloroethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0771,1,2-Trichloroethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0831,1-Dichloroethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0911,1-Dichloroethylene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0721,1-Dichloropropylene
BRL 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.0751,2,3-Trichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 99 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-20 (2-4)
Prism Sample ID: 7040298-22
Prism Work Order: 7040298
Time Collected: 04/13/17 08:15
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.111,2,3-Trichloropropane
BRL 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.0691,2,4-Trichlorobenzene
55 8260B P7D03945003.2 4/24/17 22:38 ANGmg/kg dry 0.701,2,4-Trimethylbenzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0711,2-Dibromoethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0691,2-Dichlorobenzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0681,2-Dichloroethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0631,2-Dichloropropane
15 8260B P7D03945003.2 4/24/17 22:38 ANGmg/kg dry 0.781,3,5-Trimethylbenzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0621,3-Dichlorobenzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0761,3-Dichloropropane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0831,4-Dichlorobenzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0722,2-Dichloropropane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0862-Chlorotoluene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0744-Chlorotoluene
0.50 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.0794-Isopropyltoluene
BRL 8260B P7D0394501.3 4/24/17 22:10 ANGmg/kg dry 0.24Acetone
0.47 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.071Benzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.074Bromobenzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.083Bromochloromethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.071Bromodichloromethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.085Bromoform
BRL 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.083Bromomethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.076Carbon Tetrachloride
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.064Chlorobenzene
BRL 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.065Chloroethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.073Chloroform
BRL 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.071Chloromethane
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.066cis-1,2-Dichloroethylene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.070cis-1,3-Dichloropropylene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.067Dibromochloromethane
BRL 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.081Dichlorodifluoromethane
12 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.072Ethylbenzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.066Isopropyl Ether
1.6 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.073Isopropylbenzene (Cumene)
52 8260B P7D03945006.3 4/24/17 22:38 ANGmg/kg dry 1.5m,p-Xylenes
BRL 8260B P7D0394501.3 4/24/17 22:10 ANGmg/kg dry 0.072Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0394501.3 4/24/17 22:10 ANGmg/kg dry 0.052Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0394501.3 4/24/17 22:10 ANGmg/kg dry 0.055Methyl Isobutyl Ketone
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.068Methylene Chloride
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.066Methyl-tert-Butyl Ether
8.9 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.048Naphthalene
2.3 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.063n-Butylbenzene
7.1 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.074n-Propylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 100 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-20 (2-4)
Prism Sample ID: 7040298-22
Prism Work Order: 7040298
Time Collected: 04/13/17 08:15
Time Submitted: 04/17/17 08:00
22 8260B P7D03945003.2 4/24/17 22:38 ANGmg/kg dry 0.69o-Xylene
0.84 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.078sec-Butylbenzene
0.15 8260B P7D0394500.32 4/24/17 22:10 ANGJmg/kg dry 0.070Styrene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.074tert-Butylbenzene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.067Tetrachloroethylene
12 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.067Toluene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.073trans-1,2-Dichloroethylene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.068trans-1,3-Dichloropropylene
BRL 8260B P7D0394500.32 4/24/17 22:10 ANGmg/kg dry 0.068Trichloroethylene
BRL 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.090Trichlorofluoromethane
BRL 8260B P7D0394501.3 4/24/17 22:10 ANGmg/kg dry 0.053Vinyl acetate
BRL 8260B P7D0394500.63 4/24/17 22:10 ANGmg/kg dry 0.088Vinyl chloride
74 8260B P7D03945009.5 4/24/17 22:38 ANGmg/kg dry 2.2Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
70-13080 %Dibromofluoromethane
70-13091 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 101 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-21 (0-2)
Prism Sample ID: 7040298-23
Prism Work Order: 7040298
Time Collected: 04/13/17 08:20
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
79.9 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0631,2,4-Trichlorobenzene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0611,2-Dichlorobenzene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0591,4-Dichlorobenzene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0781-Methylnaphthalene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0752,4,6-Trichlorophenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0782,4-Dichlorophenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0562,4-Dinitrophenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0582-Chloronaphthalene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0572-Chlorophenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0642-Methylnaphthalene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0732-Nitrophenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0793,3'-Dichlorobenzidine
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0694-Bromophenyl phenyl ether
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0564-Chloro-3-methylphenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.0624-Nitrophenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.058Acenaphthylene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.065Anthracene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.053Azobenzene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.069Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 102 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-21 (0-2)
Prism Sample ID: 7040298-23
Prism Work Order: 7040298
Time Collected: 04/13/17 08:20
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.057Butyl benzyl phthalate
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.051Chrysene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.061Dibenzofuran
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.055Diethyl phthalate
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.053Dimethyl phthalate
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.057Di-n-butyl phthalate
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.051Fluoranthene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.058Fluorene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.064Hexachlorobenzene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.072Hexachlorobutadiene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.072Hexachlorocyclopentadiene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.067Hexachloroethane
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.054Isophorone
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.065Naphthalene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.057Nitrobenzene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.061N-Nitrosodiphenylamine
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.052Phenanthrene
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.059Phenol
BRL 8270D P7D027410.40 4/20/17 2:59 JMVmg/kg dry 0.053Pyrene
Surrogate Recovery Control Limits
39-13269 %2,4,6-Tribromophenol
44-11575 %2-Fluorobiphenyl
35-11576 %2-Fluorophenol
37-12272 %Nitrobenzene-d5
34-12177 %Phenol-d5
54-12794 %Terphenyl-d14
Total Metals
6.3 6020B P7D0287100.32 4/25/17 2:27 BGMmg/kg dry 0.060Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000501,1,1,2-Tetrachloroethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000291,1,1-Trichloroethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000411,1,2,2-Tetrachloroethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000531,1,2-Trichloroethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000331,1-Dichloropropylene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000771,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 103 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-21 (0-2)
Prism Sample ID: 7040298-23
Prism Work Order: 7040298
Time Collected: 04/13/17 08:20
Time Submitted: 04/17/17 08:00
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000451,2,4-Trichlorobenzene
0.023 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000461,2,4-Trimethylbenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000281,2-Dichlorobenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000361,2-Dichloroethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000371,2-Dichloropropane
0.0062 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000461,3,5-Trimethylbenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000401,3-Dichlorobenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000301,3-Dichloropropane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000312-Chlorotoluene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000364-Chlorotoluene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.000294-Isopropyltoluene
0.24 8260B P7D038110.060 4/24/17 14:22 ANGmg/kg dry 0.0015Acetone
BRL 8260B P7D038110.0036 4/24/17 14:22 ANGmg/kg dry 0.00035Benzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00050Bromobenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00033Bromochloromethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00069Bromoform
BRL 8260B P7D038110.012 4/24/17 14:22 ANGmg/kg dry 0.00074Bromomethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00030Carbon Tetrachloride
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00032Chlorobenzene
BRL 8260B P7D038110.012 4/24/17 14:22 ANGmg/kg dry 0.00050Chloroethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00044Chloroform
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00041Chloromethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00027Dichlorodifluoromethane
0.0025 8260B P7D038110.0060 4/24/17 14:22 ANGJmg/kg dry 0.00023Ethylbenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00036Isopropylbenzene (Cumene)
0.0041 8260B P7D038110.012 4/24/17 14:22 ANGJmg/kg dry 0.00056m,p-Xylenes
BRL 8260B P7D038110.060 4/24/17 14:22 ANGmg/kg dry 0.00055Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D038110.12 4/24/17 14:22 ANGmg/kg dry 0.00055Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D038110.060 4/24/17 14:22 ANGmg/kg dry 0.00051Methyl Isobutyl Ketone
0.0070 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00034Methylene Chloride
BRL 8260B P7D038110.012 4/24/17 14:22 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether
0.0025 8260B P7D038110.012 4/24/17 14:22 ANGJmg/kg dry 0.00019Naphthalene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00031n-Butylbenzene
0.0040 8260B P7D038110.0060 4/24/17 14:22 ANGJmg/kg dry 0.00036n-Propylbenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00025o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 104 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-21 (0-2)
Prism Sample ID: 7040298-23
Prism Work Order: 7040298
Time Collected: 04/13/17 08:20
Time Submitted: 04/17/17 08:00
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00036Styrene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00029Tetrachloroethylene
0.0028 8260B P7D038110.0060 4/24/17 14:22 ANGJmg/kg dry 0.00035Toluene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00036trans-1,2-Dichloroethylene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00032trans-1,3-Dichloropropylene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00039Trichloroethylene
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00039Trichlorofluoromethane
BRL 8260B P7D038110.030 4/24/17 14:22 ANGmg/kg dry 0.00083Vinyl acetate
BRL 8260B P7D038110.0060 4/24/17 14:22 ANGmg/kg dry 0.00029Vinyl chloride
0.0041 8260B P7D038110.018 4/24/17 14:22 ANGJmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-12396 %Dibromofluoromethane
76-12992 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 105 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-21 (2-4)
Prism Sample ID: 7040298-24
Prism Work Order: 7040298
Time Collected: 04/13/17 08:20
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
76.8 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0601,3-Dichlorobenzene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0631,4-Dichlorobenzene
2.0 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0802,4,6-Trichlorophenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0612-Chlorophenol
4.2 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0782-Nitrophenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0853,3'-Dichlorobenzidine
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0644,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.0664-Nitrophenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.058Acenaphthene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.062Acenaphthylene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.069Anthracene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.046Benzo(a)pyrene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.056Benzo(k)fluoranthene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.056Benzyl alcohol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.074bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.073Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 106 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-21 (2-4)
Prism Sample ID: 7040298-24
Prism Work Order: 7040298
Time Collected: 04/13/17 08:20
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.054Chrysene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.065Dibenzofuran
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.059Diethyl phthalate
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.055Fluoranthene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.062Fluorene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.077Hexachlorobutadiene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.076Hexachlorocyclopentadiene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.072Hexachloroethane
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.058Isophorone
2.1 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.069Naphthalene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.061Nitrobenzene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.067N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.065N-Nitrosodiphenylamine
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.051Pentachlorophenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.063Phenol
BRL 8270D P7D027410.43 4/19/17 23:13 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13279 %2,4,6-Tribromophenol
44-11577 %2-Fluorobiphenyl
35-11581 %2-Fluorophenol
37-12274 %Nitrobenzene-d5
34-12181 %Phenol-d5
54-12794 %Terphenyl-d14
Total Metals
6.4 6020B P7D0287100.33 4/25/17 2:32 BGMmg/kg dry 0.061Lead
Volatile Organic Compounds by GC/MS (Medium Level)
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0711,1,1,2-Tetrachloroethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0661,1,1-Trichloroethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0551,1,2,2-Tetrachloroethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0681,1,2-Trichloroethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0741,1-Dichloroethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0811,1-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0641,1-Dichloropropylene
BRL 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.0661,2,3-Trichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0981,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 107 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-21 (2-4)
Prism Sample ID: 7040298-24
Prism Work Order: 7040298
Time Collected: 04/13/17 08:20
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.0611,2,4-Trichlorobenzene
28 8260B P7D03945002.8 4/25/17 11:22 ANGmg/kg dry 0.621,2,4-Trimethylbenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0631,2-Dibromoethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0601,2-Dichloroethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0561,2-Dichloropropane
9.3 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0691,3,5-Trimethylbenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0551,3-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0671,3-Dichloropropane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0741,4-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0642,2-Dichloropropane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0772-Chlorotoluene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0664-Chlorotoluene
0.40 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.0714-Isopropyltoluene
BRL 8260B P7D0394501.1 4/24/17 16:12 ANGmg/kg dry 0.21Acetone
0.33 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.063Benzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.066Bromobenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.074Bromochloromethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.063Bromodichloromethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.076Bromoform
BRL 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.073Bromomethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.068Carbon Tetrachloride
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.057Chlorobenzene
BRL 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.058Chloroethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.065Chloroform
BRL 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.063Chloromethane
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.059cis-1,2-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.062cis-1,3-Dichloropropylene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.060Dibromochloromethane
BRL 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.072Dichlorodifluoromethane
1.8 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.064Ethylbenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.059Isopropyl Ether
0.60 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.065Isopropylbenzene (Cumene)
5.0 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.14m,p-Xylenes
BRL 8260B P7D0394501.1 4/24/17 16:12 ANGmg/kg dry 0.064Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0394501.1 4/24/17 16:12 ANGmg/kg dry 0.046Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0394501.1 4/24/17 16:12 ANGmg/kg dry 0.049Methyl Isobutyl Ketone
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.061Methylene Chloride
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.059Methyl-tert-Butyl Ether
4.4 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.043Naphthalene
2.3 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.056n-Butylbenzene
3.1 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.066n-Propylbenzene
1.0 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.062o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 108 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-21 (2-4)
Prism Sample ID: 7040298-24
Prism Work Order: 7040298
Time Collected: 04/13/17 08:20
Time Submitted: 04/17/17 08:00
0.71 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.070sec-Butylbenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.062Styrene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.066tert-Butylbenzene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.060Tetrachloroethylene
0.53 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.060Toluene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.065trans-1,2-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.060trans-1,3-Dichloropropylene
BRL 8260B P7D0394500.28 4/24/17 16:12 ANGmg/kg dry 0.061Trichloroethylene
BRL 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.080Trichlorofluoromethane
BRL 8260B P7D0394501.1 4/24/17 16:12 ANGmg/kg dry 0.047Vinyl acetate
BRL 8260B P7D0394500.56 4/24/17 16:12 ANGmg/kg dry 0.078Vinyl chloride
6.0 8260B P7D0394500.84 4/24/17 16:12 ANGmg/kg dry 0.20Xylenes, total
Surrogate Recovery Control Limits
70-13096 %4-Bromofluorobenzene
70-13086 %Dibromofluoromethane
70-13091 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 109 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-22 (5-6)
Prism Sample ID: 7040298-25
Prism Work Order: 7040298
Time Collected: 04/13/17 10:50
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
83.2 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0601,2,4-Trichlorobenzene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0581,2-Dichlorobenzene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0541,3-Dichlorobenzene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0561,4-Dichlorobenzene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0741-Methylnaphthalene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0722,4,6-Trichlorophenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0742,4-Dichlorophenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0592,4-Dimethylphenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0542,4-Dinitrophenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0472,4-Dinitrotoluene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0512,6-Dinitrotoluene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0562-Chloronaphthalene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0552-Chlorophenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0622-Methylnaphthalene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0492-Methylphenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0702-Nitrophenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0763,3'-Dichlorobenzidine
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0473/4-Methylphenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0584,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0664-Bromophenyl phenyl ether
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0544-Chloro-3-methylphenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0464-Chloroaniline
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0504-Chlorophenyl phenyl ether
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.0594-Nitrophenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.052Acenaphthene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.056Acenaphthylene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.062Anthracene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.051Azobenzene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.050Benzo(a)anthracene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.042Benzo(a)pyrene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.045Benzo(b)fluoranthene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.042Benzo(g,h,i)perylene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.051Benzo(k)fluoranthene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.032Benzoic Acid
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.051Benzyl alcohol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.067bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.054Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.066Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.057Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 110 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-22 (5-6)
Prism Sample ID: 7040298-25
Prism Work Order: 7040298
Time Collected: 04/13/17 10:50
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.055Butyl benzyl phthalate
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.049Chrysene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.047Dibenzo(a,h)anthracene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.059Dibenzofuran
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.053Diethyl phthalate
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.051Dimethyl phthalate
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.055Di-n-butyl phthalate
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.047Di-n-octyl phthalate
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.049Fluoranthene
0.21 8270D P7D027410.39 4/19/17 23:35 JMVJmg/kg dry 0.055Fluorene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.061Hexachlorobenzene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.069Hexachlorobutadiene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.069Hexachlorocyclopentadiene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.065Hexachloroethane
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.044Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.052Isophorone
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.062Naphthalene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.055Nitrobenzene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.061N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.059N-Nitrosodiphenylamine
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.046Pentachlorophenol
0.28 8270D P7D027410.39 4/19/17 23:35 JMVJmg/kg dry 0.050Phenanthrene
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.057Phenol
BRL 8270D P7D027410.39 4/19/17 23:35 JMVmg/kg dry 0.051Pyrene
Surrogate Recovery Control Limits
39-13272 %2,4,6-Tribromophenol
44-11569 %2-Fluorobiphenyl
35-11570 %2-Fluorophenol
37-12267 %Nitrobenzene-d5
34-12170 %Phenol-d5
54-12789 %Terphenyl-d14
Total Metals
7.1 6020B P7D0287100.30 4/25/17 2:37 BGMmg/kg dry 0.057Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000431,1,1,2-Tetrachloroethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000251,1,1-Trichloroethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000351,1,2,2-Tetrachloroethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000461,1,2-Trichloroethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000141,1-Dichloroethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000231,1-Dichloroethylene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000281,1-Dichloropropylene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000291,2,3-Trichlorobenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000661,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 111 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-22 (5-6)
Prism Sample ID: 7040298-25
Prism Work Order: 7040298
Time Collected: 04/13/17 10:50
Time Submitted: 04/17/17 08:00
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000391,2,4-Trichlorobenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000401,2,4-Trimethylbenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000211,2-Dibromoethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000241,2-Dichlorobenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000311,2-Dichloroethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000321,2-Dichloropropane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000391,3,5-Trimethylbenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000341,3-Dichlorobenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000261,3-Dichloropropane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000201,4-Dichlorobenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000252,2-Dichloropropane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000272-Chlorotoluene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000314-Chlorotoluene
0.011 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.000254-Isopropyltoluene
BRL 8260B P7D038110.052 4/24/17 14:49 ANGmg/kg dry 0.0013Acetone
BRL 8260B P7D038110.0031 4/24/17 14:49 ANGmg/kg dry 0.00030Benzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00043Bromobenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00029Bromochloromethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00029Bromodichloromethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00059Bromoform
BRL 8260B P7D038110.010 4/24/17 14:49 ANGmg/kg dry 0.00064Bromomethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00026Carbon Tetrachloride
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00027Chlorobenzene
BRL 8260B P7D038110.010 4/24/17 14:49 ANGmg/kg dry 0.00043Chloroethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00037Chloroform
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00035Chloromethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00022cis-1,2-Dichloroethylene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00017cis-1,3-Dichloropropylene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00021Dibromochloromethane
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00024Dichlorodifluoromethane
0.0026 8260B P7D038110.0052 4/24/17 14:49 ANGJmg/kg dry 0.00020Ethylbenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00021Isopropyl Ether
0.025 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00031Isopropylbenzene (Cumene)
BRL 8260B P7D038110.010 4/24/17 14:49 ANGmg/kg dry 0.00048m,p-Xylenes
BRL 8260B P7D038110.052 4/24/17 14:49 ANGmg/kg dry 0.00047Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D038110.10 4/24/17 14:49 ANGmg/kg dry 0.00047Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D038110.052 4/24/17 14:49 ANGmg/kg dry 0.00044Methyl Isobutyl Ketone
0.0092 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00029Methylene Chloride
BRL 8260B P7D038110.010 4/24/17 14:49 ANGmg/kg dry 0.00017Methyl-tert-Butyl Ether
0.0076 8260B P7D038110.010 4/24/17 14:49 ANGJmg/kg dry 0.00016Naphthalene
0.0099 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00026n-Butylbenzene
0.017 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00031n-Propylbenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00021o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 112 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-22 (5-6)
Prism Sample ID: 7040298-25
Prism Work Order: 7040298
Time Collected: 04/13/17 10:50
Time Submitted: 04/17/17 08:00
0.066 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00025sec-Butylbenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00031Styrene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00018tert-Butylbenzene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00025Tetrachloroethylene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00030Toluene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00031trans-1,2-Dichloroethylene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00027trans-1,3-Dichloropropylene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00034Trichloroethylene
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00034Trichlorofluoromethane
BRL 8260B P7D038110.026 4/24/17 14:49 ANGmg/kg dry 0.00071Vinyl acetate
BRL 8260B P7D038110.0052 4/24/17 14:49 ANGmg/kg dry 0.00025Vinyl chloride
BRL 8260B P7D038110.016 4/24/17 14:49 ANGmg/kg dry 0.00097Xylenes, total
Surrogate Recovery Control Limits
70-13091 %4-Bromofluorobenzene
84-12396 %Dibromofluoromethane
76-12990 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 113 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-23 (5-6)
Prism Sample ID: 7040298-26
Prism Work Order: 7040298
Time Collected: 04/13/17 10:40
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
81.8 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0621,2,4-Trichlorobenzene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0601,2-Dichlorobenzene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0561,3-Dichlorobenzene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0581,4-Dichlorobenzene
9.0 8270D P7D027452.0 4/20/17 12:50 JMVmg/kg dry 0.381-Methylnaphthalene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0742,4,6-Trichlorophenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0762,4-Dichlorophenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0612,4-Dimethylphenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0552,4-Dinitrophenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0482,4-Dinitrotoluene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0532,6-Dinitrotoluene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0572-Chloronaphthalene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0562-Chlorophenol
13 8270D P7D027452.0 4/20/17 12:50 JMVmg/kg dry 0.322-Methylnaphthalene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0512-Methylphenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0722-Nitrophenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0783,3'-Dichlorobenzidine
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0493/4-Methylphenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0684-Bromophenyl phenyl ether
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0554-Chloro-3-methylphenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.0614-Nitrophenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.054Acenaphthene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.057Acenaphthylene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.064Anthracene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.052Azobenzene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.052Benzo(a)anthracene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.043Benzo(a)pyrene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.046Benzo(b)fluoranthene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.043Benzo(g,h,i)perylene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.052Benzo(k)fluoranthene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.033Benzoic Acid
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.052Benzyl alcohol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.069bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.056Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.068Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.059Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 114 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-23 (5-6)
Prism Sample ID: 7040298-26
Prism Work Order: 7040298
Time Collected: 04/13/17 10:40
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.056Butyl benzyl phthalate
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.050Chrysene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.060Dibenzofuran
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.055Diethyl phthalate
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.052Dimethyl phthalate
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.056Di-n-butyl phthalate
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.050Fluoranthene
2.3 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.057Fluorene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.063Hexachlorobenzene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.071Hexachlorobutadiene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.071Hexachlorocyclopentadiene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.066Hexachloroethane
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.054Isophorone
3.3 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.064Naphthalene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.056Nitrobenzene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.060N-Nitrosodiphenylamine
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.047Pentachlorophenol
3.4 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.051Phenanthrene
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.058Phenol
BRL 8270D P7D027410.40 4/19/17 23:58 JMVmg/kg dry 0.052Pyrene
Surrogate Recovery Control Limits
39-13284 %2,4,6-Tribromophenol
44-11581 %2-Fluorobiphenyl
35-11564 %2-Fluorophenol
37-122129 %Nitrobenzene-d5 SR
34-12166 %Phenol-d5
54-12795 %Terphenyl-d14
Total Metals
8.8 6020B P7D0287100.30 4/25/17 2:43 BGMmg/kg dry 0.056Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000481,1,1,2-Tetrachloroethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000281,1,1-Trichloroethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000521,1,2-Trichloroethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000261,1-Dichloroethylene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000321,1-Dichloropropylene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000331,2,3-Trichlorobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 115 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-23 (5-6)
Prism Sample ID: 7040298-26
Prism Work Order: 7040298
Time Collected: 04/13/17 10:40
Time Submitted: 04/17/17 08:00
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000751,2,3-Trichloropropane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene
See 8260ML 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000451,2,4-Trimethylbenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000281,2-Dichlorobenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000351,2-Dichloroethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000361,2-Dichloropropane
0.20 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000441,3,5-Trimethylbenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000391,3-Dichlorobenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000291,3-Dichloropropane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000282,2-Dichloropropane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000302-Chlorotoluene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000354-Chlorotoluene
See 8260ML 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.000284-Isopropyltoluene
BRL 8260B P7D036210.059 4/21/17 19:15 ANGmg/kg dry 0.0014Acetone
0.016 8260B P7D036210.0035 4/21/17 19:15 ANGmg/kg dry 0.00034Benzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00049Bromobenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00032Bromochloromethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00033Bromodichloromethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00067Bromoform
BRL 8260B P7D036210.012 4/21/17 19:15 ANGmg/kg dry 0.00072Bromomethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00029Carbon Tetrachloride
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00031Chlorobenzene
BRL 8260B P7D036210.012 4/21/17 19:15 ANGmg/kg dry 0.00049Chloroethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00042Chloroform
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00039Chloromethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00027Dichlorodifluoromethane
See 8260ML 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00023Ethylbenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00024Isopropyl Ether
See 8260ML 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene)
0.17 8260B P7D036210.012 4/21/17 19:15 ANGmg/kg dry 0.00054m,p-Xylenes
BRL 8260B P7D036210.059 4/21/17 19:15 ANGmg/kg dry 0.00053Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D036210.12 4/21/17 19:15 ANGmg/kg dry 0.00053Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D036210.059 4/21/17 19:15 ANGmg/kg dry 0.00050Methyl Isobutyl Ketone
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00033Methylene Chloride
BRL 8260B P7D036210.012 4/21/17 19:15 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether
0.031 8260B P7D036210.012 4/21/17 19:15 ANGmg/kg dry 0.00019Naphthalene
0.18 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00030n-Butylbenzene
See 8260ML 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00035n-Propylbenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 116 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: B-23 (5-6)
Prism Sample ID: 7040298-26
Prism Work Order: 7040298
Time Collected: 04/13/17 10:40
Time Submitted: 04/17/17 08:00
0.17 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00024o-Xylene
See 8260ML 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00028sec-Butylbenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00035Styrene
0.036 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00028Tetrachloroethylene
0.0099 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00034Toluene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00035trans-1,2-Dichloroethylene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00038Trichloroethylene
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00038Trichlorofluoromethane
BRL 8260B P7D036210.029 4/21/17 19:15 ANGmg/kg dry 0.00080Vinyl acetate
BRL 8260B P7D036210.0059 4/21/17 19:15 ANGmg/kg dry 0.00028Vinyl chloride
0.34 8260B P7D036210.018 4/21/17 19:15 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130195 %4-Bromofluorobenzene SR
84-12373 %Dibromofluoromethane SR
76-129122 %Toluene-d8
Volatile Organic Compounds by GC/MS (Medium Level)
9.0 8260B P7D0394500.30 4/24/17 16:40 ANGmg/kg dry 0.0671,2,4-Trimethylbenzene
2.3 8260B P7D0394500.30 4/24/17 16:40 ANGmg/kg dry 0.0764-Isopropyltoluene
2.1 8260B P7D0394500.30 4/24/17 16:40 ANGmg/kg dry 0.069Ethylbenzene
1.7 8260B P7D0394500.30 4/24/17 16:40 ANGmg/kg dry 0.070Isopropylbenzene (Cumene)
3.4 8260B P7D0394500.30 4/24/17 16:40 ANGmg/kg dry 0.071n-Propylbenzene
4.0 8260B P7D0394500.30 4/24/17 16:40 ANGmg/kg dry 0.075sec-Butylbenzene
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
70-13088 %Dibromofluoromethane
70-13093 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 117 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: Duplicate 1
Prism Sample ID: 7040298-27
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
General Chemistry Parameters
86.5 *SM2540 G P7D035910.100 4/20/17 14:40 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0591,2,4-Trichlorobenzene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0571,2-Dichlorobenzene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0531,3-Dichlorobenzene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0551,4-Dichlorobenzene
0.22 8270D P7D027410.38 4/20/17 0:21 JMVJmg/kg dry 0.0731-Methylnaphthalene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0712,4,6-Trichlorophenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0732,4-Dichlorophenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0582,4-Dimethylphenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0532,4-Dinitrophenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0462,4-Dinitrotoluene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0502,6-Dinitrotoluene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0552-Chloronaphthalene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0542-Chlorophenol
0.42 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0602-Methylnaphthalene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0482-Methylphenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0692-Nitrophenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0753,3'-Dichlorobenzidine
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0473/4-Methylphenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0574,6-Dinitro-2-methylphenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0654-Bromophenyl phenyl ether
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0534-Chloro-3-methylphenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0454-Chloroaniline
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0494-Chlorophenyl phenyl ether
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.0584-Nitrophenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.051Acenaphthene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.055Acenaphthylene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.061Anthracene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.050Azobenzene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.049Benzo(a)anthracene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.041Benzo(a)pyrene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.044Benzo(b)fluoranthene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.041Benzo(g,h,i)perylene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.050Benzo(k)fluoranthene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.032Benzoic Acid
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.050Benzyl alcohol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.066bis(2-Chloroethoxy)methane
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.053Bis(2-Chloroethyl)ether
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.065Bis(2-chloroisopropyl)ether
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.056Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 118 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: Duplicate 1
Prism Sample ID: 7040298-27
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.054Butyl benzyl phthalate
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.048Chrysene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.046Dibenzo(a,h)anthracene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.057Dibenzofuran
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.052Diethyl phthalate
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.050Dimethyl phthalate
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.054Di-n-butyl phthalate
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.046Di-n-octyl phthalate
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.048Fluoranthene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.054Fluorene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.060Hexachlorobenzene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.068Hexachlorobutadiene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.067Hexachlorocyclopentadiene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.063Hexachloroethane
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.043Indeno(1,2,3-cd)pyrene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.051Isophorone
0.32 8270D P7D027410.38 4/20/17 0:21 JMVJmg/kg dry 0.061Naphthalene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.054Nitrobenzene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.060N-Nitroso-di-n-propylamine
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.057N-Nitrosodiphenylamine
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.045Pentachlorophenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.049Phenanthrene
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.056Phenol
BRL 8270D P7D027410.38 4/20/17 0:21 JMVmg/kg dry 0.050Pyrene
Surrogate Recovery Control Limits
39-13266 %2,4,6-Tribromophenol
44-11563 %2-Fluorobiphenyl
35-11564 %2-Fluorophenol
37-12259 %Nitrobenzene-d5
34-12163 %Phenol-d5
54-12780 %Terphenyl-d14
Total Metals
4.7 6020B P7D0287100.29 4/25/17 2:48 BGMmg/kg dry 0.055Lead
Volatile Organic Compounds by GC/MS (Medium Level)
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0701,1,1,2-Tetrachloroethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0641,1,1-Trichloroethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0541,1,2,2-Tetrachloroethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0671,1,2-Trichloroethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0731,1-Dichloroethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0791,1-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0631,1-Dichloropropylene
BRL 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.0651,2,3-Trichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0971,2,3-Trichloropropane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 119 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: Duplicate 1
Prism Sample ID: 7040298-27
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.0601,2,4-Trichlorobenzene
25 8260B P7D03945002.8 4/24/17 18:02 ANGmg/kg dry 0.611,2,4-Trimethylbenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0621,2-Dibromoethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0611,2-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0591,2-Dichloroethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0551,2-Dichloropropane
8.5 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0681,3,5-Trimethylbenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0541,3-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0661,3-Dichloropropane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0721,4-Dichlorobenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0632,2-Dichloropropane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0762-Chlorotoluene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.0644-Chlorotoluene
0.21 8260B P7D0394500.28 4/24/17 17:35 ANGJmg/kg dry 0.0704-Isopropyltoluene
BRL 8260B P7D0394501.1 4/24/17 17:35 ANGmg/kg dry 0.21Acetone
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.062Benzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.065Bromobenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.073Bromochloromethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.062Bromodichloromethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.075Bromoform
BRL 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.072Bromomethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.067Carbon Tetrachloride
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.056Chlorobenzene
BRL 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.057Chloroethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.064Chloroform
BRL 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.062Chloromethane
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.058cis-1,2-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.061cis-1,3-Dichloropropylene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.059Dibromochloromethane
BRL 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.071Dichlorodifluoromethane
7.3 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.063Ethylbenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.058Isopropyl Ether
1.0 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.064Isopropylbenzene (Cumene)
35 8260B P7D03945005.5 4/24/17 18:02 ANGmg/kg dry 1.3m,p-Xylenes
BRL 8260B P7D0394501.1 4/24/17 17:35 ANGmg/kg dry 0.063Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0394501.1 4/24/17 17:35 ANGmg/kg dry 0.045Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0394501.1 4/24/17 17:35 ANGmg/kg dry 0.048Methyl Isobutyl Ketone
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.060Methylene Chloride
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.058Methyl-tert-Butyl Ether
1.3 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.042Naphthalene
0.78 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.055n-Butylbenzene
3.7 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.065n-Propylbenzene
14 8260B P7D03945002.8 4/24/17 18:02 ANGmg/kg dry 0.61o-Xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 120 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Solid
Client Sample ID: Duplicate 1
Prism Sample ID: 7040298-27
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
0.43 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.069sec-Butylbenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.061Styrene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.065tert-Butylbenzene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.059Tetrachloroethylene
6.2 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.059Toluene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.064trans-1,2-Dichloroethylene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.059trans-1,3-Dichloropropylene
BRL 8260B P7D0394500.28 4/24/17 17:35 ANGmg/kg dry 0.060Trichloroethylene
BRL 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.079Trichlorofluoromethane
BRL 8260B P7D0394501.1 4/24/17 17:35 ANGmg/kg dry 0.046Vinyl acetate
BRL 8260B P7D0394500.55 4/24/17 17:35 ANGmg/kg dry 0.077Vinyl chloride
49 8260B P7D03945008.3 4/24/17 18:02 ANGmg/kg dry 1.9Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
70-13073 %Dibromofluoromethane
70-13092 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 121 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Duplicate 2
Prism Sample ID: 7040298-28
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.81,2,4-Trichlorobenzene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.71,2-Dichlorobenzene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.01,3-Dichlorobenzene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.71,4-Dichlorobenzene
140 8270D P7D02511104/18/17 16:05 JMVug/L 2.71-Methylnaphthalene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.72,4,5-Trichlorophenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.92,4,6-Trichlorophenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.72,4-Dichlorophenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 3.62,4-Dimethylphenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.82,4-Dinitrophenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.52,4-Dinitrotoluene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.22,6-Dinitrotoluene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.82-Chloronaphthalene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.02-Chlorophenol
200 8270D P7D02511104/18/17 16:05 JMVug/L 2.52-Methylnaphthalene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.92-Methylphenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.52-Nitroaniline
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.52-Nitrophenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.53,3'-Dichlorobenzidine
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.63/4-Methylphenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.43-Nitroaniline
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.44,6-Dinitro-2-methylphenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.34-Bromophenyl phenyl ether
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.54-Chloro-3-methylphenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.64-Chloroaniline
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.44-Chlorophenyl phenyl ether
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 0.974-Nitroaniline
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 0.624-Nitrophenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.9Acenaphthene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.1Acenaphthylene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.5Aniline
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.5Anthracene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.9Azobenzene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.5Benzo(a)anthracene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.5Benzo(a)pyrene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.2Benzo(b)fluoranthene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.4Benzo(g,h,i)perylene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.5Benzo(k)fluoranthene
BRL 8270D P7D025111004/18/17 16:05 JMVug/L 4.9Benzoic Acid
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.2Benzyl alcohol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.7bis(2-Chloroethoxy)methane
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.4Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 122 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Duplicate 2
Prism Sample ID: 7040298-28
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.1Bis(2-chloroisopropyl)ether
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.4Bis(2-Ethylhexyl)phthalate
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.4Butyl benzyl phthalate
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.5Chrysene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.2Dibenzo(a,h)anthracene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.8Dibenzofuran
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 3.5Diethyl phthalate
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.5Dimethyl phthalate
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.8Di-n-butyl phthalate
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.4Di-n-octyl phthalate
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.8Fluoranthene
7.7 8270D P7D02511104/18/17 16:05 JMVJug/L 1.8Fluorene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.3Hexachlorobenzene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.2Hexachlorobutadiene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.8Hexachlorocyclopentadiene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.8Hexachloroethane
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 4.1Indeno(1,2,3-cd)pyrene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.6Isophorone
430 8270D P7D02515524/19/17 8:45 JMVug/L 13Naphthalene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.7Nitrobenzene
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 2.3N-Nitroso-di-n-propylamine
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.4N-Nitrosodiphenylamine
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.3Pentachlorophenol
9.4 8270D P7D02511104/18/17 16:05 JMVJug/L 1.5Phenanthrene
22 8270D P7D02511104/18/17 16:05 JMVug/L 1.0Phenol
BRL 8270D P7D02511104/18/17 16:05 JMVug/L 1.5Pyrene
Surrogate Recovery Control Limits
43-140113 %2,4,6-Tribromophenol
44-11993 %2-Fluorobiphenyl
19-11953 %2-Fluorophenol
44-12087 %Nitrobenzene-d5
11-5232 %Phenol-d5
50-134113 %Terphenyl-d14
Total Metals
1.3 6020B P7D032111.0 4/21/17 21:19 BGMug/L 0.061Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 5.61,1,1,2-Tetrachloroethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.11,1,1-Trichloroethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 1.81,1,2,2-Tetrachloroethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.31,1,2-Trichloroethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 4.21,1-Dichloroethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 4.11,1-Dichloroethylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 123 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Duplicate 2
Prism Sample ID: 7040298-28
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.61,1-Dichloropropylene
BRL 8260B P7D0349501004/21/17 21:32 KDMug/L 201,2,3-Trichlorobenzene
BRL 8260B P7D034950504/21/17 21:32 KDMug/L 6.81,2,3-Trichloropropane
BRL 8260B P7D034950504/21/17 21:32 KDMug/L 6.61,2,4-Trichlorobenzene
700 8260B P7D034950254/21/17 21:32 KDMug/L 2.71,2,4-Trimethylbenzene
BRL 8260B P7D0349501004/21/17 21:32 KDMug/L 8.41,2-Dibromo-3-chloropropane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.51,2-Dibromoethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.81,2-Dichlorobenzene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.31,2-Dichloroethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 5.51,2-Dichloropropane
85 8260B P7D034950254/21/17 21:32 KDMug/L 3.81,3,5-Trimethylbenzene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.71,3-Dichlorobenzene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.21,3-Dichloropropane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.51,4-Dichlorobenzene
BRL 8260B P7D0349501004/21/17 21:32 KDMug/L 5.62,2-Dichloropropane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.32-Chlorotoluene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.54-Chlorotoluene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 4.44-Isopropyltoluene
BRL 8260B P7D0349502504/21/17 21:32 KDMug/L 16Acetone
BRL 8260B P7D03495010004/21/17 21:32 KDMug/L 10Acrolein
BRL 8260B P7D03495010004/21/17 21:32 KDMug/L 10Acrylonitrile
7600 8260B P7D034910005004/21/17 22:06 KDMug/L 48Benzene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.8Bromobenzene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 7.2Bromochloromethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.1Bromodichloromethane
BRL 8260B P7D034950504/21/17 21:32 KDMug/L 2.0Bromoform
BRL 8260B P7D034950504/21/17 21:32 KDMug/L 9.0Bromomethane
BRL 8260B P7D0349502504/21/17 21:32 KDMug/L 3.7Carbon disulfide
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 5.4Carbon Tetrachloride
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.1Chlorobenzene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 11Chloroethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.8Chloroform
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.9Chloromethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.8cis-1,2-Dichloroethylene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.9cis-1,3-Dichloropropylene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 4.0Dibromochloromethane
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.3Dibromomethane
BRL 8260B P7D034950504/21/17 21:32 KDMug/L 5.7Dichlorodifluoromethane
1500 8260B P7D034950254/21/17 21:32 KDMug/L 3.1Ethylbenzene
BRL 8260B P7D0349501004/21/17 21:32 KDMug/L 7.8Hexachlorobutadiene
3100 8260B P7D034950254/21/17 21:32 KDMug/L 2.5Isopropyl Ether
68 8260B P7D034950254/21/17 21:32 KDMug/L 2.7Isopropylbenzene (Cumene)
1400 8260B P7D034950504/21/17 21:32 KDMug/L 5.8m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 124 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Duplicate 2
Prism Sample ID: 7040298-28
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0349502504/21/17 21:32 KDMug/L 3.2Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0349502504/21/17 21:32 KDMug/L 12Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0349502504/21/17 21:32 KDMug/L 3.9Methyl Isobutyl Ketone
BRL 8260B P7D034950504/21/17 21:32 KDMug/L 4.1Methylene Chloride
1400 8260B P7D034950254/21/17 21:32 KDMug/L 2.1Methyl-tert-Butyl Ether
410 8260B P7D034950504/21/17 21:32 KDMug/L 9.6Naphthalene
BRL 8260B P7D034950504/21/17 21:32 KDMug/L 3.8n-Butylbenzene
150 8260B P7D034950254/21/17 21:32 KDMug/L 4.3n-Propylbenzene
100 8260B P7D034950254/21/17 21:32 KDMug/L 2.2o-Xylene
52 8260B P7D034950254/21/17 21:32 KDMug/L 3.8sec-Butylbenzene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 2.4Styrene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 4.4tert-Butylbenzene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 4.9Tetrachloroethylene
190 8260B P7D034950254/21/17 21:32 KDMug/L 2.2Toluene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 4.7trans-1,2-Dichloroethylene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.5trans-1,3-Dichloropropylene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.9Trichloroethylene
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 3.1Trichlorofluoromethane
BRL 8260B P7D0349501004/21/17 21:32 KDMug/L 3.0Vinyl acetate
BRL 8260B P7D034950254/21/17 21:32 KDMug/L 4.8Vinyl chloride
1500 8260B P7D0349100015004/21/17 22:06 KDMug/L 150Xylenes, total
Surrogate Recovery Control Limits
80-12496 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-12393 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 125 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: MW-1
Prism Sample ID: 7040298-29
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.81,2,4-Trichlorobenzene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.71,2-Dichlorobenzene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.01,3-Dichlorobenzene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.71,4-Dichlorobenzene
130 8270D P7D02511104/18/17 16:28 JMVug/L 2.71-Methylnaphthalene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.72,4,5-Trichlorophenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.92,4,6-Trichlorophenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.72,4-Dichlorophenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 3.62,4-Dimethylphenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.82,4-Dinitrophenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.52,4-Dinitrotoluene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.22,6-Dinitrotoluene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.82-Chloronaphthalene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.02-Chlorophenol
200 8270D P7D02511104/18/17 16:28 JMVug/L 2.52-Methylnaphthalene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.92-Methylphenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.52-Nitroaniline
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.52-Nitrophenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.53,3'-Dichlorobenzidine
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.63/4-Methylphenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.43-Nitroaniline
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.44,6-Dinitro-2-methylphenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.34-Bromophenyl phenyl ether
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.54-Chloro-3-methylphenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.64-Chloroaniline
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.44-Chlorophenyl phenyl ether
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 0.974-Nitroaniline
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 0.624-Nitrophenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.9Acenaphthene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.1Acenaphthylene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.5Aniline
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.5Anthracene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.9Azobenzene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.5Benzo(a)anthracene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.5Benzo(a)pyrene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.2Benzo(b)fluoranthene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.4Benzo(g,h,i)perylene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.5Benzo(k)fluoranthene
BRL 8270D P7D025111004/18/17 16:28 JMVug/L 4.9Benzoic Acid
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.2Benzyl alcohol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.7bis(2-Chloroethoxy)methane
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.4Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 126 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: MW-1
Prism Sample ID: 7040298-29
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.1Bis(2-chloroisopropyl)ether
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.4Bis(2-Ethylhexyl)phthalate
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.4Butyl benzyl phthalate
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.5Chrysene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.2Dibenzo(a,h)anthracene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.8Dibenzofuran
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 3.5Diethyl phthalate
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.5Dimethyl phthalate
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.8Di-n-butyl phthalate
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.4Di-n-octyl phthalate
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.8Fluoranthene
7.0 8270D P7D02511104/18/17 16:28 JMVJug/L 1.8Fluorene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.3Hexachlorobenzene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.2Hexachlorobutadiene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.8Hexachlorocyclopentadiene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.8Hexachloroethane
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 4.1Indeno(1,2,3-cd)pyrene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.6Isophorone
470 8270D P7D02515524/19/17 9:07 JMVug/L 13Naphthalene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.7Nitrobenzene
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 2.3N-Nitroso-di-n-propylamine
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.4N-Nitrosodiphenylamine
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.3Pentachlorophenol
8.6 8270D P7D02511104/18/17 16:28 JMVJug/L 1.5Phenanthrene
14 8270D P7D02511104/18/17 16:28 JMVug/L 1.0Phenol
BRL 8270D P7D02511104/18/17 16:28 JMVug/L 1.5Pyrene
Surrogate Recovery Control Limits
43-140109 %2,4,6-Tribromophenol
44-11988 %2-Fluorobiphenyl
19-11949 %2-Fluorophenol
44-12086 %Nitrobenzene-d5
11-5232 %Phenol-d5
50-134106 %Terphenyl-d14
Total Metals
1.1 6020B P7D032111.0 4/21/17 21:34 BGMug/L 0.061Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 5.61,1,1,2-Tetrachloroethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.11,1,1-Trichloroethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 1.81,1,2,2-Tetrachloroethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.31,1,2-Trichloroethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 4.21,1-Dichloroethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 4.11,1-Dichloroethylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 127 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: MW-1
Prism Sample ID: 7040298-29
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.61,1-Dichloropropylene
BRL 8260B P7D0349501004/21/17 22:40 KDMug/L 201,2,3-Trichlorobenzene
BRL 8260B P7D034950504/21/17 22:40 KDMug/L 6.81,2,3-Trichloropropane
BRL 8260B P7D034950504/21/17 22:40 KDMug/L 6.61,2,4-Trichlorobenzene
720 8260B P7D034950254/21/17 22:40 KDMug/L 2.71,2,4-Trimethylbenzene
BRL 8260B P7D0349501004/21/17 22:40 KDMug/L 8.41,2-Dibromo-3-chloropropane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.51,2-Dibromoethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.81,2-Dichlorobenzene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.31,2-Dichloroethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 5.51,2-Dichloropropane
86 8260B P7D034950254/21/17 22:40 KDMug/L 3.81,3,5-Trimethylbenzene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.71,3-Dichlorobenzene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.21,3-Dichloropropane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.51,4-Dichlorobenzene
BRL 8260B P7D0349501004/21/17 22:40 KDMug/L 5.62,2-Dichloropropane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.32-Chlorotoluene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.54-Chlorotoluene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 4.44-Isopropyltoluene
BRL 8260B P7D0349502504/21/17 22:40 KDMug/L 16Acetone
BRL 8260B P7D03495010004/21/17 22:40 KDMug/L 10Acrolein
BRL 8260B P7D03495010004/21/17 22:40 KDMug/L 10Acrylonitrile
7200 8260B P7D034910005004/21/17 23:13 KDMug/L 48Benzene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.8Bromobenzene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 7.2Bromochloromethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.1Bromodichloromethane
BRL 8260B P7D034950504/21/17 22:40 KDMug/L 2.0Bromoform
BRL 8260B P7D034950504/21/17 22:40 KDMug/L 9.0Bromomethane
BRL 8260B P7D0349502504/21/17 22:40 KDMug/L 3.7Carbon disulfide
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 5.4Carbon Tetrachloride
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.1Chlorobenzene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 11Chloroethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.8Chloroform
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.9Chloromethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.8cis-1,2-Dichloroethylene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.9cis-1,3-Dichloropropylene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 4.0Dibromochloromethane
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.3Dibromomethane
BRL 8260B P7D034950504/21/17 22:40 KDMug/L 5.7Dichlorodifluoromethane
1500 8260B P7D034950254/21/17 22:40 KDMug/L 3.1Ethylbenzene
BRL 8260B P7D0349501004/21/17 22:40 KDMug/L 7.8Hexachlorobutadiene
3200 8260B P7D034950254/21/17 22:40 KDMug/L 2.5Isopropyl Ether
71 8260B P7D034950254/21/17 22:40 KDMug/L 2.7Isopropylbenzene (Cumene)
1500 8260B P7D034950504/21/17 22:40 KDMug/L 5.8m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 128 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: MW-1
Prism Sample ID: 7040298-29
Prism Work Order: 7040298
Time Collected: 04/13/17 00:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D0349502504/21/17 22:40 KDMug/L 3.2Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D0349502504/21/17 22:40 KDMug/L 12Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D0349502504/21/17 22:40 KDMug/L 3.9Methyl Isobutyl Ketone
BRL 8260B P7D034950504/21/17 22:40 KDMug/L 4.1Methylene Chloride
1500 8260B P7D034950254/21/17 22:40 KDMug/L 2.1Methyl-tert-Butyl Ether
450 8260B P7D034950504/21/17 22:40 KDMug/L 9.6Naphthalene
BRL 8260B P7D034950504/21/17 22:40 KDMug/L 3.8n-Butylbenzene
160 8260B P7D034950254/21/17 22:40 KDMug/L 4.3n-Propylbenzene
110 8260B P7D034950254/21/17 22:40 KDMug/L 2.2o-Xylene
54 8260B P7D034950254/21/17 22:40 KDMug/L 3.8sec-Butylbenzene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 2.4Styrene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 4.4tert-Butylbenzene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 4.9Tetrachloroethylene
190 8260B P7D034950254/21/17 22:40 KDMug/L 2.2Toluene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 4.7trans-1,2-Dichloroethylene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.5trans-1,3-Dichloropropylene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.9Trichloroethylene
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 3.1Trichlorofluoromethane
BRL 8260B P7D0349501004/21/17 22:40 KDMug/L 3.0Vinyl acetate
BRL 8260B P7D034950254/21/17 22:40 KDMug/L 4.8Vinyl chloride
1600 8260B P7D034950754/21/17 22:40 KDMug/L 7.4Xylenes, total
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-12999 %Dibromofluoromethane
77-12396 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 129 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 1
Prism Sample ID: 7040298-30
Prism Work Order: 7040298
Time Collected: 04/12/17 11:00
Time Submitted: 04/17/17 08:00
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.81,2,4-Trichlorobenzene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.71,2-Dichlorobenzene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.01,3-Dichlorobenzene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.71,4-Dichlorobenzene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.71-Methylnaphthalene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.72,4,5-Trichlorophenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.92,4,6-Trichlorophenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.72,4-Dichlorophenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 3.62,4-Dimethylphenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.82,4-Dinitrophenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.52,4-Dinitrotoluene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.22,6-Dinitrotoluene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.82-Chloronaphthalene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.02-Chlorophenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.52-Methylnaphthalene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.92-Methylphenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.52-Nitroaniline
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.52-Nitrophenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.53,3'-Dichlorobenzidine
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.63/4-Methylphenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.43-Nitroaniline
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.44,6-Dinitro-2-methylphenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.34-Bromophenyl phenyl ether
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.54-Chloro-3-methylphenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.64-Chloroaniline
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.44-Chlorophenyl phenyl ether
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 0.974-Nitroaniline
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 0.624-Nitrophenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.9Acenaphthene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.1Acenaphthylene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.5Aniline
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.5Anthracene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.9Azobenzene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.5Benzo(a)anthracene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.5Benzo(a)pyrene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.2Benzo(b)fluoranthene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.4Benzo(g,h,i)perylene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.5Benzo(k)fluoranthene
BRL 8270D P7D025111004/18/17 16:50 JMVug/L 4.9Benzoic Acid
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.2Benzyl alcohol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.7bis(2-Chloroethoxy)methane
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.4Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 130 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 1
Prism Sample ID: 7040298-30
Prism Work Order: 7040298
Time Collected: 04/12/17 11:00
Time Submitted: 04/17/17 08:00
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.1Bis(2-chloroisopropyl)ether
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.4Bis(2-Ethylhexyl)phthalate
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.4Butyl benzyl phthalate
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.5Chrysene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.2Dibenzo(a,h)anthracene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.8Dibenzofuran
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 3.5Diethyl phthalate
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.5Dimethyl phthalate
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.8Di-n-butyl phthalate
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.4Di-n-octyl phthalate
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.8Fluoranthene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.8Fluorene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.3Hexachlorobenzene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.2Hexachlorobutadiene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.8Hexachlorocyclopentadiene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.8Hexachloroethane
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 4.1Indeno(1,2,3-cd)pyrene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.6Isophorone
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.7Naphthalene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.7Nitrobenzene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 2.3N-Nitroso-di-n-propylamine
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.4N-Nitrosodiphenylamine
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.3Pentachlorophenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.5Phenanthrene
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.0Phenol
BRL 8270D P7D02511104/18/17 16:50 JMVug/L 1.5Pyrene
Surrogate Recovery Control Limits
43-140104 %2,4,6-Tribromophenol
44-11981 %2-Fluorobiphenyl
19-11951 %2-Fluorophenol
44-12071 %Nitrobenzene-d5
11-5234 %Phenol-d5
50-134113 %Terphenyl-d14
Total Metals
1.4 6020B P7D032111.0 4/21/17 21:39 BGMug/L 0.061Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0511,1-Dichloropropylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 131 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 1
Prism Sample ID: 7040298-30
Prism Work Order: 7040298
Time Collected: 04/12/17 11:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034912.0 4/21/17 20:24 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7D034911.0 4/21/17 20:24 KDMug/L 0.141,2,3-Trichloropropane
0.58 8260B P7D034911.0 4/21/17 20:24 KDMJug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7D034912.0 4/21/17 20:24 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7D034912.0 4/21/17 20:24 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7D034915.0 4/21/17 20:24 KDMug/L 0.31Acetone
BRL 8260B P7D03491204/21/17 20:24 KDMug/L 0.20Acrolein
BRL 8260B P7D03491204/21/17 20:24 KDMug/L 0.20Acrylonitrile
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.048Benzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.057Bromobenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.14Bromochloromethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7D034911.0 4/21/17 20:24 KDMug/L 0.040Bromoform
BRL 8260B P7D034911.0 4/21/17 20:24 KDMug/L 0.18Bromomethane
BRL 8260B P7D034915.0 4/21/17 20:24 KDMug/L 0.075Carbon disulfide
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.062Chlorobenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.22Chloroethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.076Chloroform
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.079Chloromethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.081Dibromochloromethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.065Dibromomethane
BRL 8260B P7D034911.0 4/21/17 20:24 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.061Ethylbenzene
BRL 8260B P7D034912.0 4/21/17 20:24 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7D034911.0 4/21/17 20:24 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7D034915.0 4/21/17 20:24 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 132 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 1
Prism Sample ID: 7040298-30
Prism Work Order: 7040298
Time Collected: 04/12/17 11:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034915.0 4/21/17 20:24 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D034915.0 4/21/17 20:24 KDMug/L 0.078Methyl Isobutyl Ketone
1.1 8260B P7D034911.0 4/21/17 20:24 KDMug/L 0.083Methylene Chloride
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7D034911.0 4/21/17 20:24 KDMug/L 0.19Naphthalene
BRL 8260B P7D034911.0 4/21/17 20:24 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.044o-Xylene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.047Styrene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.044Toluene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.078Trichloroethylene
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7D034912.0 4/21/17 20:24 KDMug/L 0.060Vinyl acetate
BRL 8260B P7D034910.50 4/21/17 20:24 KDMug/L 0.097Vinyl chloride
BRL 8260B P7D034911.5 4/21/17 20:24 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12496 %4-Bromofluorobenzene
75-129109 %Dibromofluoromethane
77-12395 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 133 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 2
Prism Sample ID: 7040298-31
Prism Work Order: 7040298
Time Collected: 04/13/17 11:10
Time Submitted: 04/17/17 08:00
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.81,2,4-Trichlorobenzene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.71,2-Dichlorobenzene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.01,3-Dichlorobenzene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.71,4-Dichlorobenzene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.71-Methylnaphthalene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.72,4,5-Trichlorophenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.92,4,6-Trichlorophenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.72,4-Dichlorophenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 3.62,4-Dimethylphenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.82,4-Dinitrophenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.52,4-Dinitrotoluene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.22,6-Dinitrotoluene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.82-Chloronaphthalene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.02-Chlorophenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.52-Methylnaphthalene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.92-Methylphenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.52-Nitroaniline
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.52-Nitrophenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.53,3'-Dichlorobenzidine
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.63/4-Methylphenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.43-Nitroaniline
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.44,6-Dinitro-2-methylphenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.34-Bromophenyl phenyl ether
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.54-Chloro-3-methylphenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.64-Chloroaniline
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.44-Chlorophenyl phenyl ether
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 0.974-Nitroaniline
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 0.624-Nitrophenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.9Acenaphthene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.1Acenaphthylene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.5Aniline
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.5Anthracene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.9Azobenzene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.5Benzo(a)anthracene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.5Benzo(a)pyrene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.2Benzo(b)fluoranthene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.4Benzo(g,h,i)perylene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.5Benzo(k)fluoranthene
BRL 8270D P7D025111004/18/17 17:13 JMVug/L 4.9Benzoic Acid
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.2Benzyl alcohol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.7bis(2-Chloroethoxy)methane
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.4Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 134 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 2
Prism Sample ID: 7040298-31
Prism Work Order: 7040298
Time Collected: 04/13/17 11:10
Time Submitted: 04/17/17 08:00
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.1Bis(2-chloroisopropyl)ether
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.4Bis(2-Ethylhexyl)phthalate
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.4Butyl benzyl phthalate
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.5Chrysene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.2Dibenzo(a,h)anthracene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.8Dibenzofuran
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 3.5Diethyl phthalate
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.5Dimethyl phthalate
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.8Di-n-butyl phthalate
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.4Di-n-octyl phthalate
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.8Fluoranthene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.8Fluorene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.3Hexachlorobenzene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.2Hexachlorobutadiene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.8Hexachlorocyclopentadiene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.8Hexachloroethane
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 4.1Indeno(1,2,3-cd)pyrene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.6Isophorone
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.7Naphthalene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.7Nitrobenzene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 2.3N-Nitroso-di-n-propylamine
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.4N-Nitrosodiphenylamine
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.3Pentachlorophenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.5Phenanthrene
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.0Phenol
BRL 8270D P7D02511104/18/17 17:13 JMVug/L 1.5Pyrene
Surrogate Recovery Control Limits
43-14099 %2,4,6-Tribromophenol
44-11980 %2-Fluorobiphenyl
19-11953 %2-Fluorophenol
44-12071 %Nitrobenzene-d5
11-5235 %Phenol-d5
50-134111 %Terphenyl-d14
Total Metals
BRL 6020B P7D032111.0 4/21/17 21:45 BGMug/L 0.061Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0511,1-Dichloropropylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 135 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 2
Prism Sample ID: 7040298-31
Prism Work Order: 7040298
Time Collected: 04/13/17 11:10
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034912.0 4/21/17 19:51 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7D034912.0 4/21/17 19:51 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7D034912.0 4/21/17 19:51 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7D034915.0 4/21/17 19:51 KDMug/L 0.31Acetone
BRL 8260B P7D03491204/21/17 19:51 KDMug/L 0.20Acrolein
BRL 8260B P7D03491204/21/17 19:51 KDMug/L 0.20Acrylonitrile
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.048Benzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.057Bromobenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.14Bromochloromethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.040Bromoform
BRL 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.18Bromomethane
BRL 8260B P7D034915.0 4/21/17 19:51 KDMug/L 0.075Carbon disulfide
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.062Chlorobenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.22Chloroethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.076Chloroform
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.079Chloromethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.081Dibromochloromethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.065Dibromomethane
BRL 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.061Ethylbenzene
BRL 8260B P7D034912.0 4/21/17 19:51 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7D034915.0 4/21/17 19:51 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 136 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 2
Prism Sample ID: 7040298-31
Prism Work Order: 7040298
Time Collected: 04/13/17 11:10
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034915.0 4/21/17 19:51 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D034915.0 4/21/17 19:51 KDMug/L 0.078Methyl Isobutyl Ketone
1.2 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.083Methylene Chloride
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.19Naphthalene
BRL 8260B P7D034911.0 4/21/17 19:51 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.044o-Xylene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.047Styrene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.044Toluene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.078Trichloroethylene
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7D034912.0 4/21/17 19:51 KDMug/L 0.060Vinyl acetate
BRL 8260B P7D034910.50 4/21/17 19:51 KDMug/L 0.097Vinyl chloride
BRL 8260B P7D034911.5 4/21/17 19:51 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12496 %4-Bromofluorobenzene
75-129107 %Dibromofluoromethane
77-12395 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 137 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 3
Prism Sample ID: 7040298-32
Prism Work Order: 7040298
Time Collected: 04/13/17 17:00
Time Submitted: 04/17/17 08:00
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.81,2,4-Trichlorobenzene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.61,2-Dichlorobenzene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.91,3-Dichlorobenzene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.61,4-Dichlorobenzene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.61-Methylnaphthalene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.62,4,5-Trichlorophenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.82,4,6-Trichlorophenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.62,4-Dichlorophenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 3.42,4-Dimethylphenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.72,4-Dinitrophenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.42,4-Dinitrotoluene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.12,6-Dinitrotoluene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.72-Chloronaphthalene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.92-Chlorophenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.42-Methylnaphthalene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.82-Methylphenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.42-Nitroaniline
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.42-Nitrophenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.43,3'-Dichlorobenzidine
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.53/4-Methylphenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.43-Nitroaniline
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.44,6-Dinitro-2-methylphenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.34-Bromophenyl phenyl ether
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.44-Chloro-3-methylphenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.44-Chloroaniline
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.34-Chlorophenyl phenyl ether
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 0.934-Nitroaniline
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 0.604-Nitrophenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.8Acenaphthene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.0Acenaphthylene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.4Aniline
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Anthracene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.8Azobenzene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Benzo(a)anthracene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Benzo(a)pyrene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.1Benzo(b)fluoranthene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Benzo(g,h,i)perylene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Benzo(k)fluoranthene
BRL 8270D P7D025111004/18/17 17:36 JMVug/L 4.7Benzoic Acid
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.1Benzyl alcohol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.6bis(2-Chloroethoxy)methane
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.3Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 138 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 3
Prism Sample ID: 7040298-32
Prism Work Order: 7040298
Time Collected: 04/13/17 17:00
Time Submitted: 04/17/17 08:00
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.0Bis(2-chloroisopropyl)ether
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.3Bis(2-Ethylhexyl)phthalate
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Butyl benzyl phthalate
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Chrysene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.2Dibenzo(a,h)anthracene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.8Dibenzofuran
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 3.3Diethyl phthalate
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Dimethyl phthalate
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.7Di-n-butyl phthalate
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.3Di-n-octyl phthalate
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.7Fluoranthene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.7Fluorene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.3Hexachlorobenzene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.1Hexachlorobutadiene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.7Hexachlorocyclopentadiene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.7Hexachloroethane
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 3.9Indeno(1,2,3-cd)pyrene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.5Isophorone
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.6Naphthalene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.6Nitrobenzene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 2.2N-Nitroso-di-n-propylamine
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.3N-Nitrosodiphenylamine
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.2Pentachlorophenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.5Phenanthrene
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 0.98Phenol
BRL 8270D P7D02511104/18/17 17:36 JMVug/L 1.4Pyrene
Surrogate Recovery Control Limits
43-140103 %2,4,6-Tribromophenol
44-11982 %2-Fluorobiphenyl
19-11949 %2-Fluorophenol
44-12071 %Nitrobenzene-d5
11-5232 %Phenol-d5
50-134112 %Terphenyl-d14
Total Metals
BRL 6020B P7D032111.0 4/21/17 21:50 BGMug/L 0.061Lead
Volatile Organic Compounds by GC/MS
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0511,1-Dichloropropylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 139 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 3
Prism Sample ID: 7040298-32
Prism Work Order: 7040298
Time Collected: 04/13/17 17:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034912.0 4/21/17 19:17 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7D034911.0 4/21/17 19:17 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7D034911.0 4/21/17 19:17 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7D034912.0 4/21/17 19:17 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7D034912.0 4/21/17 19:17 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7D034915.0 4/21/17 19:17 KDMug/L 0.31Acetone
BRL 8260B P7D03491204/21/17 19:17 KDMug/L 0.20Acrolein
BRL 8260B P7D03491204/21/17 19:17 KDMug/L 0.20Acrylonitrile
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.048Benzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.057Bromobenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.14Bromochloromethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7D034911.0 4/21/17 19:17 KDMug/L 0.040Bromoform
BRL 8260B P7D034911.0 4/21/17 19:17 KDMug/L 0.18Bromomethane
BRL 8260B P7D034915.0 4/21/17 19:17 KDMug/L 0.075Carbon disulfide
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.062Chlorobenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.22Chloroethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.076Chloroform
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.079Chloromethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.081Dibromochloromethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.065Dibromomethane
BRL 8260B P7D034911.0 4/21/17 19:17 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.061Ethylbenzene
BRL 8260B P7D034912.0 4/21/17 19:17 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7D034911.0 4/21/17 19:17 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7D034915.0 4/21/17 19:17 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 140 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Equipment Blank 3
Prism Sample ID: 7040298-32
Prism Work Order: 7040298
Time Collected: 04/13/17 17:00
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034915.0 4/21/17 19:17 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D034915.0 4/21/17 19:17 KDMug/L 0.078Methyl Isobutyl Ketone
0.92 8260B P7D034911.0 4/21/17 19:17 KDMJug/L 0.083Methylene Chloride
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7D034911.0 4/21/17 19:17 KDMug/L 0.19Naphthalene
BRL 8260B P7D034911.0 4/21/17 19:17 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.044o-Xylene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.047Styrene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.044Toluene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.078Trichloroethylene
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7D034912.0 4/21/17 19:17 KDMug/L 0.060Vinyl acetate
BRL 8260B P7D034910.50 4/21/17 19:17 KDMug/L 0.097Vinyl chloride
BRL 8260B P7D034911.5 4/21/17 19:17 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12497 %4-Bromofluorobenzene
75-129109 %Dibromofluoromethane
77-12395 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 141 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Trip Blank 1
Prism Sample ID: 7040298-33
Prism Work Order: 7040298
Time Collected: 04/13/17 17:35
Time Submitted: 04/17/17 08:00
Volatile Organic Compounds by GC/MS
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7D034912.0 4/21/17 18:43 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7D034912.0 4/21/17 18:43 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7D034912.0 4/21/17 18:43 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7D034915.0 4/21/17 18:43 KDMug/L 0.31Acetone
BRL 8260B P7D03491204/21/17 18:43 KDMug/L 0.20Acrolein
BRL 8260B P7D03491204/21/17 18:43 KDMug/L 0.20Acrylonitrile
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.048Benzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.057Bromobenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.14Bromochloromethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.040Bromoform
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.18Bromomethane
BRL 8260B P7D034915.0 4/21/17 18:43 KDMug/L 0.075Carbon disulfide
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.062Chlorobenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.22Chloroethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.076Chloroform
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.079Chloromethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 142 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Trip Blank 1
Prism Sample ID: 7040298-33
Prism Work Order: 7040298
Time Collected: 04/13/17 17:35
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.065Dibromomethane
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.061Ethylbenzene
BRL 8260B P7D034912.0 4/21/17 18:43 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7D034915.0 4/21/17 18:43 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D034915.0 4/21/17 18:43 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D034915.0 4/21/17 18:43 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.083Methylene Chloride
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.19Naphthalene
BRL 8260B P7D034911.0 4/21/17 18:43 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.044o-Xylene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.047Styrene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.044Toluene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.078Trichloroethylene
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7D034912.0 4/21/17 18:43 KDMug/L 0.060Vinyl acetate
BRL 8260B P7D034910.50 4/21/17 18:43 KDMug/L 0.097Vinyl chloride
BRL 8260B P7D034911.5 4/21/17 18:43 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12496 %4-Bromofluorobenzene
75-129111 %Dibromofluoromethane
77-12396 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 143 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Trip Blank 2
Prism Sample ID: 7040298-34
Prism Work Order: 7040298
Time Collected: 04/13/17 17:35
Time Submitted: 04/17/17 08:00
Volatile Organic Compounds by GC/MS
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7D034912.0 4/21/17 18:09 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7D034912.0 4/21/17 18:09 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7D034912.0 4/21/17 18:09 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7D034915.0 4/21/17 18:09 KDMug/L 0.31Acetone
BRL 8260B P7D03491204/21/17 18:09 KDMug/L 0.20Acrolein
BRL 8260B P7D03491204/21/17 18:09 KDMug/L 0.20Acrylonitrile
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.048Benzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.057Bromobenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.14Bromochloromethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.040Bromoform
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.18Bromomethane
BRL 8260B P7D034915.0 4/21/17 18:09 KDMug/L 0.075Carbon disulfide
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.062Chlorobenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.22Chloroethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.076Chloroform
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.079Chloromethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 144 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Trip Blank 2
Prism Sample ID: 7040298-34
Prism Work Order: 7040298
Time Collected: 04/13/17 17:35
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.065Dibromomethane
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.061Ethylbenzene
BRL 8260B P7D034912.0 4/21/17 18:09 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7D034915.0 4/21/17 18:09 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D034915.0 4/21/17 18:09 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D034915.0 4/21/17 18:09 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.083Methylene Chloride
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.19Naphthalene
BRL 8260B P7D034911.0 4/21/17 18:09 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.044o-Xylene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.047Styrene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.044Toluene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.078Trichloroethylene
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7D034912.0 4/21/17 18:09 KDMug/L 0.060Vinyl acetate
BRL 8260B P7D034910.50 4/21/17 18:09 KDMug/L 0.097Vinyl chloride
BRL 8260B P7D034911.5 4/21/17 18:09 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129110 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 145 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Field Blank
Prism Sample ID: 7040298-35
Prism Work Order: 7040298
Time Collected: 04/13/17 17:30
Time Submitted: 04/17/17 08:00
Volatile Organic Compounds by GC/MS
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P7D034912.0 4/21/17 17:35 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P7D034912.0 4/21/17 17:35 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P7D034912.0 4/21/17 17:35 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P7D034915.0 4/21/17 17:35 KDMug/L 0.31Acetone
BRL 8260B P7D03491204/21/17 17:35 KDMug/L 0.20Acrolein
BRL 8260B P7D03491204/21/17 17:35 KDMug/L 0.20Acrylonitrile
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.048Benzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.057Bromobenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.14Bromochloromethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.062Bromodichloromethane
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.040Bromoform
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.18Bromomethane
BRL 8260B P7D034915.0 4/21/17 17:35 KDMug/L 0.075Carbon disulfide
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.062Chlorobenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.22Chloroethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.076Chloroform
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.079Chloromethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 146 of 207
Laboratory Report
04/26/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Sample Matrix: Water
Client Sample ID: Field Blank
Prism Sample ID: 7040298-35
Prism Work Order: 7040298
Time Collected: 04/13/17 17:30
Time Submitted: 04/17/17 08:00
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.065Dibromomethane
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.061Ethylbenzene
BRL 8260B P7D034912.0 4/21/17 17:35 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.050Isopropyl Ether
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.12m,p-Xylenes
BRL 8260B P7D034915.0 4/21/17 17:35 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P7D034915.0 4/21/17 17:35 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P7D034915.0 4/21/17 17:35 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.083Methylene Chloride
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.19Naphthalene
BRL 8260B P7D034911.0 4/21/17 17:35 KDMug/L 0.076n-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.087n-Propylbenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.044o-Xylene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.047Styrene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.044Toluene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.078Trichloroethylene
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P7D034912.0 4/21/17 17:35 KDMug/L 0.060Vinyl acetate
BRL 8260B P7D034910.50 4/21/17 17:35 KDMug/L 0.097Vinyl chloride
BRL 8260B P7D034911.5 4/21/17 17:35 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129108 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 147 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0337 - 5035
Blank (P7D0337-BLK1)Prepared & Analyzed: 04/20/17
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 148 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0337 - 5035
Blank (P7D0337-BLK1)Prepared & Analyzed: 04/20/17
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 12663.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10251.0
ug/L 50.00 76-129Surrogate: Toluene-d8 9246.2
LCS (P7D0337-BS1)Prepared & Analyzed: 04/20/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0516 0.0050 0.05000 72-115103
1,1,1-Trichloroethane mg/kg wet0.0605 0.0050 0.05000 67-131121
1,1,2,2-Tetrachloroethane mg/kg wet0.0436 0.0050 0.05000 56-12687
1,1,2-Trichloroethane mg/kg wet0.0468 0.0050 0.05000 70-13394
1,1-Dichloroethane mg/kg wet0.0518 0.0050 0.05000 74-127104
1,1-Dichloroethylene mg/kg wet0.0540 0.0050 0.05000 67-149108
1,1-Dichloropropylene mg/kg wet0.0555 0.0050 0.05000 71-130111
1,2,3-Trichlorobenzene mg/kg wet0.0451 0.0050 0.05000 68-13090
1,2,3-Trichloropropane mg/kg wet0.0452 0.0050 0.05000 60-13790
1,2,4-Trichlorobenzene mg/kg wet0.0455 0.0050 0.05000 66-12591
1,2,4-Trimethylbenzene mg/kg wet0.0461 0.0050 0.05000 69-12992
1,2-Dibromoethane mg/kg wet0.0492 0.0050 0.05000 70-13298
1,2-Dichlorobenzene mg/kg wet0.0424 0.0050 0.05000 72-12385
1,2-Dichloroethane mg/kg wet0.0499 0.0050 0.05000 68-128100
1,2-Dichloropropane mg/kg wet0.0525 0.0050 0.05000 73-130105
1,3,5-Trimethylbenzene mg/kg wet0.0469 0.0050 0.05000 69-12894
1,3-Dichlorobenzene mg/kg wet0.0464 0.0050 0.05000 71-12093
1,3-Dichloropropane mg/kg wet0.0470 0.0050 0.05000 75-12494
1,4-Dichlorobenzene mg/kg wet0.0462 0.0050 0.05000 71-12392
2,2-Dichloropropane mg/kg wet0.0591 0.0050 0.05000 50-142118
2-Chlorotoluene mg/kg wet0.0468 0.0050 0.05000 67-12494
4-Chlorotoluene mg/kg wet0.0472 0.0050 0.05000 71-12694
4-Isopropyltoluene mg/kg wet0.0468 0.0050 0.05000 68-12994
Acetone mg/kg wet0.0852 0.050 0.1000 29-19885
Benzene mg/kg wet0.0520 0.0030 0.05000 74-127104
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 149 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0337 - 5035
LCS (P7D0337-BS1)Prepared & Analyzed: 04/20/17
Bromobenzene mg/kg wet0.0454 0.0050 0.05000 73-12591
Bromochloromethane mg/kg wet0.0531 0.0050 0.05000 72-134106
Bromodichloromethane mg/kg wet0.0598 0.0050 0.05000 75-122120
Bromoform mg/kg wet0.0509 0.0050 0.05000 66-135102
Bromomethane mg/kg wet0.0548 0.010 0.05000 20-180110
Carbon Tetrachloride mg/kg wet0.0733 0.0050 0.05000 LH64-143147
Chlorobenzene mg/kg wet0.0493 0.0050 0.05000 74-11899
Chloroethane mg/kg wet0.0549 0.010 0.05000 33-149110
Chloroform mg/kg wet0.0524 0.0050 0.05000 73-127105
Chloromethane mg/kg wet0.0416 0.0050 0.05000 45-14383
cis-1,2-Dichloroethylene mg/kg wet0.0516 0.0050 0.05000 76-134103
cis-1,3-Dichloropropylene mg/kg wet0.0604 0.0050 0.05000 71-125121
Dibromochloromethane mg/kg wet0.0515 0.0050 0.05000 73-122103
Dichlorodifluoromethane mg/kg wet0.0410 0.0050 0.05000 26-14682
Ethylbenzene mg/kg wet0.0495 0.0050 0.05000 74-12899
Isopropyl Ether mg/kg wet0.0478 0.0050 0.05000 59-15996
Isopropylbenzene (Cumene)mg/kg wet0.0473 0.0050 0.05000 68-12695
m,p-Xylenes mg/kg wet0.0997 0.010 0.1000 75-124100
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0404 0.050 0.05000 J61-15781
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0389 0.10 0.05000 J63-14978
Methyl Isobutyl Ketone mg/kg wet0.0451 0.050 0.05000 J57-16290
Methylene Chloride mg/kg wet0.0482 0.0050 0.05000 74-12996
Methyl-tert-Butyl Ether mg/kg wet0.0516 0.010 0.05000 70-130103
Naphthalene mg/kg wet0.0413 0.010 0.05000 57-15783
n-Butylbenzene mg/kg wet0.0439 0.0050 0.05000 65-13588
n-Propylbenzene mg/kg wet0.0483 0.0050 0.05000 67-13097
o-Xylene mg/kg wet0.0485 0.0050 0.05000 74-12697
sec-Butylbenzene mg/kg wet0.0463 0.0050 0.05000 66-13193
Styrene mg/kg wet0.0494 0.0050 0.05000 77-12199
tert-Butylbenzene mg/kg wet0.0471 0.0050 0.05000 67-13294
Tetrachloroethylene mg/kg wet0.0540 0.0050 0.05000 68-130108
Toluene mg/kg wet0.0523 0.0050 0.05000 71-129105
trans-1,2-Dichloroethylene mg/kg wet0.0543 0.0050 0.05000 73-132109
trans-1,3-Dichloropropylene mg/kg wet0.0535 0.0050 0.05000 68-123107
Trichloroethylene mg/kg wet0.0547 0.0050 0.05000 75-133109
Trichlorofluoromethane mg/kg wet0.0549 0.0050 0.05000 44-146110
Vinyl acetate mg/kg wet0.0535 0.025 0.05000 85-161107
Vinyl chloride mg/kg wet0.0389 0.0050 0.05000 48-14778
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 76-129Surrogate: Toluene-d8 9145.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 150 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0337 - 5035
LCS Dup (P7D0337-BSD1)Prepared & Analyzed: 04/20/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0523 0.0050 0.05000 2072-115105 1
1,1,1-Trichloroethane mg/kg wet0.0593 0.0050 0.05000 2067-131119 2
1,1,2,2-Tetrachloroethane mg/kg wet0.0432 0.0050 0.05000 2056-12686 1
1,1,2-Trichloroethane mg/kg wet0.0473 0.0050 0.05000 2070-13395 1
1,1-Dichloroethane mg/kg wet0.0506 0.0050 0.05000 2074-127101 2
1,1-Dichloroethylene mg/kg wet0.0530 0.0050 0.05000 2067-149106 2
1,1-Dichloropropylene mg/kg wet0.0536 0.0050 0.05000 2071-130107 4
1,2,3-Trichlorobenzene mg/kg wet0.0448 0.0050 0.05000 2068-13090 0.6
1,2,3-Trichloropropane mg/kg wet0.0437 0.0050 0.05000 2060-13787 3
1,2,4-Trichlorobenzene mg/kg wet0.0458 0.0050 0.05000 2066-12592 0.6
1,2,4-Trimethylbenzene mg/kg wet0.0460 0.0050 0.05000 2069-12992 0.3
1,2-Dibromoethane mg/kg wet0.0489 0.0050 0.05000 2070-13298 0.7
1,2-Dichlorobenzene mg/kg wet0.0467 0.0050 0.05000 2072-12393 10
1,2-Dichloroethane mg/kg wet0.0494 0.0050 0.05000 2068-12899 1
1,2-Dichloropropane mg/kg wet0.0524 0.0050 0.05000 2073-130105 0.1
1,3,5-Trimethylbenzene mg/kg wet0.0454 0.0050 0.05000 2069-12891 3
1,3-Dichlorobenzene mg/kg wet0.0460 0.0050 0.05000 2071-12092 0.8
1,3-Dichloropropane mg/kg wet0.0468 0.0050 0.05000 2075-12494 0.4
1,4-Dichlorobenzene mg/kg wet0.0466 0.0050 0.05000 2071-12393 0.7
2,2-Dichloropropane mg/kg wet0.0578 0.0050 0.05000 2050-142116 2
2-Chlorotoluene mg/kg wet0.0453 0.0050 0.05000 2067-12491 3
4-Chlorotoluene mg/kg wet0.0455 0.0050 0.05000 2071-12691 4
4-Isopropyltoluene mg/kg wet0.0461 0.0050 0.05000 2068-12992 2
Acetone mg/kg wet0.0847 0.050 0.1000 2029-19885 0.5
Benzene mg/kg wet0.0515 0.0030 0.05000 2074-127103 1
Bromobenzene mg/kg wet0.0442 0.0050 0.05000 2073-12588 3
Bromochloromethane mg/kg wet0.0544 0.0050 0.05000 2072-134109 2
Bromodichloromethane mg/kg wet0.0599 0.0050 0.05000 2075-122120 0.2
Bromoform mg/kg wet0.0514 0.0050 0.05000 2066-135103 0.9
Bromomethane mg/kg wet0.0560 0.010 0.05000 2020-180112 2
Carbon Tetrachloride mg/kg wet0.0718 0.0050 0.05000 20 LH64-143144 2
Chlorobenzene mg/kg wet0.0495 0.0050 0.05000 2074-11899 0.4
Chloroethane mg/kg wet0.0532 0.010 0.05000 2033-149106 3
Chloroform mg/kg wet0.0518 0.0050 0.05000 2073-127104 1
Chloromethane mg/kg wet0.0458 0.0050 0.05000 2045-14392 10
cis-1,2-Dichloroethylene mg/kg wet0.0512 0.0050 0.05000 2076-134102 0.8
cis-1,3-Dichloropropylene mg/kg wet0.0601 0.0050 0.05000 2071-125120 0.5
Dibromochloromethane mg/kg wet0.0520 0.0050 0.05000 2073-122104 1
Dichlorodifluoromethane mg/kg wet0.0397 0.0050 0.05000 2026-14679 3
Ethylbenzene mg/kg wet0.0491 0.0050 0.05000 2074-12898 0.8
Isopropyl Ether mg/kg wet0.0477 0.0050 0.05000 2059-15995 0.1
Isopropylbenzene (Cumene)mg/kg wet0.0457 0.0050 0.05000 2068-12691 3
m,p-Xylenes mg/kg wet0.0987 0.010 0.1000 2075-12499 1
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0400 0.050 0.05000 20 J61-15780 1
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0393 0.10 0.05000 20 J63-14979 1
Methyl Isobutyl Ketone mg/kg wet0.0444 0.050 0.05000 20 J57-16289 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 151 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0337 - 5035
LCS Dup (P7D0337-BSD1)Prepared & Analyzed: 04/20/17
Methylene Chloride mg/kg wet0.0482 0.0050 0.05000 2074-12996 0.1
Methyl-tert-Butyl Ether mg/kg wet0.0522 0.010 0.05000 2070-130104 1
Naphthalene mg/kg wet0.0414 0.010 0.05000 2057-15783 0.4
n-Butylbenzene mg/kg wet0.0466 0.0050 0.05000 2065-13593 6
n-Propylbenzene mg/kg wet0.0467 0.0050 0.05000 2067-13093 3
o-Xylene mg/kg wet0.0485 0.0050 0.05000 2074-12697 0.02
sec-Butylbenzene mg/kg wet0.0470 0.0050 0.05000 2066-13194 2
Styrene mg/kg wet0.0496 0.0050 0.05000 2077-12199 0.4
tert-Butylbenzene mg/kg wet0.0456 0.0050 0.05000 2067-13291 3
Tetrachloroethylene mg/kg wet0.0532 0.0050 0.05000 2068-130106 1
Toluene mg/kg wet0.0514 0.0050 0.05000 2071-129103 2
trans-1,2-Dichloroethylene mg/kg wet0.0528 0.0050 0.05000 2073-132106 3
trans-1,3-Dichloropropylene mg/kg wet0.0536 0.0050 0.05000 2068-123107 0.1
Trichloroethylene mg/kg wet0.0527 0.0050 0.05000 2075-133105 4
Trichlorofluoromethane mg/kg wet0.0533 0.0050 0.05000 2044-146107 3
Vinyl acetate mg/kg wet0.0556 0.025 0.05000 2085-161111 4
Vinyl chloride mg/kg wet0.0471 0.0050 0.05000 2048-14794 19
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.9
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9848.8
ug/L 50.00 76-129Surrogate: Toluene-d8 9245.8
Batch P7D0349 - 5030B
Blank (P7D0349-BLK1)Prepared & Analyzed: 04/21/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 152 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0349 - 5030B
Blank (P7D0349-BLK1)Prepared & Analyzed: 04/21/17
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
Methyl-tert-Butyl Ether ug/LBRL0.50
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL1.0
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 153 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0349 - 5030B
Blank (P7D0349-BLK1)Prepared & Analyzed: 04/21/17
Xylenes, total ug/LBRL1.5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9849.0
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10854.1
ug/L 50.00 77-123Surrogate: Toluene-d8 9547.3
LCS (P7D0349-BS1)Prepared & Analyzed: 04/21/17
1,1,1,2-Tetrachloroethane ug/L20.5 0.50 20.00 79-134103
1,1,1-Trichloroethane ug/L22.3 0.50 20.00 75-136112
1,1,2,2-Tetrachloroethane ug/L19.1 0.50 20.00 62-12796
1,1,2-Trichloroethane ug/L21.2 0.50 20.00 70-140106
1,1-Dichloroethane ug/L20.0 0.50 20.00 78-130100
1,1-Dichloroethylene ug/L21.4 0.50 20.00 70-154107
1,1-Dichloropropylene ug/L20.3 0.50 20.00 71-136101
1,2,3-Trichlorobenzene ug/L18.8 2.0 20.00 58-14494
1,2,3-Trichloropropane ug/L19.7 1.0 20.00 71-12798
1,2,4-Trichlorobenzene ug/L18.4 1.0 20.00 66-13992
1,2,4-Trimethylbenzene ug/L19.0 0.50 20.00 75-13395
1,2-Dibromo-3-chloropropane ug/L19.5 2.0 20.00 63-13498
1,2-Dibromoethane ug/L20.3 0.50 20.00 77-135102
1,2-Dichlorobenzene ug/L20.1 0.50 20.00 78-128101
1,2-Dichloroethane ug/L20.7 0.50 20.00 68-131103
1,2-Dichloropropane ug/L19.9 0.50 20.00 77-13099
1,3,5-Trimethylbenzene ug/L20.4 0.50 20.00 75-131102
1,3-Dichlorobenzene ug/L20.2 0.50 20.00 77-125101
1,3-Dichloropropane ug/L20.1 0.50 20.00 76-132100
1,4-Dichlorobenzene ug/L19.4 0.50 20.00 75-12697
2,2-Dichloropropane ug/L21.9 2.0 20.00 29-149110
2-Chlorotoluene ug/L19.0 0.50 20.00 74-12695
4-Chlorotoluene ug/L19.6 0.50 20.00 78-12998
4-Isopropyltoluene ug/L19.2 0.50 20.00 69-13296
Acetone ug/L34.9 5.0 40.00 40-16687
Acrolein ug/L50.9 20 40.00 70-130127
Acrylonitrile ug/L42.5 20 40.00 81-127106
Benzene ug/L19.9 0.50 20.00 77-12899
Bromobenzene ug/L18.5 0.50 20.00 78-12992
Bromochloromethane ug/L19.6 0.50 20.00 78-13598
Bromodichloromethane ug/L20.7 0.50 20.00 76-138104
Bromoform ug/L20.2 1.0 20.00 71-135101
Bromomethane ug/L16.3 1.0 20.00 41-16881
Carbon disulfide ug/L21.6 5.0 20.00 59-135108
Carbon Tetrachloride ug/L21.3 0.50 20.00 72-142106
Chlorobenzene ug/L19.9 0.50 20.00 78-119100
Chloroethane ug/L20.6 0.50 20.00 57-142103
Chloroform ug/L19.1 0.50 20.00 77-13096
Chloromethane ug/L15.7 0.50 20.00 47-14579
cis-1,2-Dichloroethylene ug/L19.9 0.50 20.00 76-141100
cis-1,3-Dichloropropylene ug/L20.5 0.50 20.00 65-140102
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 154 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0349 - 5030B
LCS (P7D0349-BS1)Prepared & Analyzed: 04/21/17
Dibromochloromethane ug/L20.6 0.50 20.00 75-134103
Dibromomethane ug/L20.8 0.50 20.00 76-138104
Dichlorodifluoromethane ug/L17.2 1.0 20.00 28-16386
Ethylbenzene ug/L20.2 0.50 20.00 80-127101
Hexachlorobutadiene ug/L20.8 2.0 20.00 61-134104
Isopropyl Ether ug/L19.2 0.50 20.00 60-15496
Isopropylbenzene (Cumene)ug/L20.7 0.50 20.00 70-130103
m,p-Xylenes ug/L42.5 1.0 40.00 77-133106
Methyl Butyl Ketone (2-Hexanone)ug/L17.9 5.0 20.00 64-13790
Methyl Ethyl Ketone (2-Butanone)ug/L16.7 5.0 20.00 71-13483
Methyl Isobutyl Ketone ug/L19.7 5.0 20.00 69-13498
Methylene Chloride ug/L19.5 1.0 20.00 73-13198
Methyl-tert-Butyl Ether ug/L21.3 0.50 20.00 68-135107
Naphthalene ug/L17.2 1.0 20.00 64-13686
n-Butylbenzene ug/L19.2 1.0 20.00 68-13496
n-Propylbenzene ug/L20.1 0.50 20.00 72-132101
o-Xylene ug/L20.0 0.50 20.00 78-128100
sec-Butylbenzene ug/L18.8 0.50 20.00 71-13194
Styrene ug/L18.9 0.50 20.00 78-12994
tert-Butylbenzene ug/L20.4 0.50 20.00 70-132102
Tetrachloroethylene ug/L21.3 0.50 20.00 80-129106
Toluene ug/L20.3 0.50 20.00 76-131102
trans-1,2-Dichloroethylene ug/L21.3 0.50 20.00 76-135107
trans-1,3-Dichloropropylene ug/L21.0 0.50 20.00 67-140105
Trichloroethylene ug/L21.1 0.50 20.00 77-133105
Trichlorofluoromethane ug/L23.2 0.50 20.00 62-148116
Vinyl acetate ug/L21.0 2.0 20.00 34-167105
Vinyl chloride ug/L19.4 0.50 20.00 57-14197
Xylenes, total ug/L62.4 1.5 60.00 77-133104
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9547.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 77-123Surrogate: Toluene-d8 9547.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 155 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0349 - 5030B
LCS Dup (P7D0349-BSD1)Prepared & Analyzed: 04/21/17
1,1,1,2-Tetrachloroethane ug/L20.3 0.50 20.00 2079-134102 1
1,1,1-Trichloroethane ug/L22.0 0.50 20.00 2075-136110 2
1,1,2,2-Tetrachloroethane ug/L18.1 0.50 20.00 2062-12790 5
1,1,2-Trichloroethane ug/L19.8 0.50 20.00 2070-14099 7
1,1-Dichloroethane ug/L20.0 0.50 20.00 2078-130100 0.3
1,1-Dichloroethylene ug/L22.6 0.50 20.00 2070-154113 5
1,1-Dichloropropylene ug/L20.6 0.50 20.00 2071-136103 1
1,2,3-Trichlorobenzene ug/L19.2 2.0 20.00 2058-14496 2
1,2,3-Trichloropropane ug/L20.9 1.0 20.00 2071-127104 6
1,2,4-Trichlorobenzene ug/L18.9 1.0 20.00 2066-13994 2
1,2,4-Trimethylbenzene ug/L19.7 0.50 20.00 2075-13399 4
1,2-Dibromo-3-chloropropane ug/L18.8 2.0 20.00 2063-13494 4
1,2-Dibromoethane ug/L20.6 0.50 20.00 2077-135103 2
1,2-Dichlorobenzene ug/L20.4 0.50 20.00 2078-128102 1
1,2-Dichloroethane ug/L20.6 0.50 20.00 2068-131103 0.2
1,2-Dichloropropane ug/L19.6 0.50 20.00 2077-13098 2
1,3,5-Trimethylbenzene ug/L20.8 0.50 20.00 2075-131104 2
1,3-Dichlorobenzene ug/L20.3 0.50 20.00 2077-125101 0.2
1,3-Dichloropropane ug/L20.2 0.50 20.00 2076-132101 0.4
1,4-Dichlorobenzene ug/L19.6 0.50 20.00 2075-12698 1
2,2-Dichloropropane ug/L21.6 2.0 20.00 2029-149108 2
2-Chlorotoluene ug/L19.5 0.50 20.00 2074-12697 3
4-Chlorotoluene ug/L20.5 0.50 20.00 2078-129103 4
4-Isopropyltoluene ug/L20.2 0.50 20.00 2069-132101 5
Acetone ug/L36.3 5.0 40.00 2040-16691 4
Acrolein ug/L47.2 20 40.00 2070-130118 7
Acrylonitrile ug/L38.1 20 40.00 2081-12795 11
Benzene ug/L20.0 0.50 20.00 2077-128100 0.4
Bromobenzene ug/L18.8 0.50 20.00 2078-12994 2
Bromochloromethane ug/L19.3 0.50 20.00 2078-13596 2
Bromodichloromethane ug/L20.4 0.50 20.00 2076-138102 2
Bromoform ug/L19.7 1.0 20.00 2071-13598 3
Bromomethane ug/L17.2 1.0 20.00 2041-16886 6
Carbon disulfide ug/L21.8 5.0 20.00 2059-135109 1
Carbon Tetrachloride ug/L22.0 0.50 20.00 2072-142110 3
Chlorobenzene ug/L20.4 0.50 20.00 2078-119102 2
Chloroethane ug/L21.1 0.50 20.00 2057-142105 2
Chloroform ug/L19.4 0.50 20.00 2077-13097 1
Chloromethane ug/L16.3 0.50 20.00 2047-14582 4
cis-1,2-Dichloroethylene ug/L19.9 0.50 20.00 2076-14199 0.3
cis-1,3-Dichloropropylene ug/L20.7 0.50 20.00 2065-140103 1
Dibromochloromethane ug/L21.0 0.50 20.00 2075-134105 2
Dibromomethane ug/L20.8 0.50 20.00 2076-138104 0.3
Dichlorodifluoromethane ug/L16.9 1.0 20.00 2028-16384 2
Ethylbenzene ug/L20.8 0.50 20.00 2080-127104 3
Hexachlorobutadiene ug/L21.8 2.0 20.00 2061-134109 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 156 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0349 - 5030B
LCS Dup (P7D0349-BSD1)Prepared & Analyzed: 04/21/17
Isopropyl Ether ug/L19.1 0.50 20.00 2060-15496 0.4
Isopropylbenzene (Cumene)ug/L21.5 0.50 20.00 2070-130108 4
m,p-Xylenes ug/L43.2 1.0 40.00 2077-133108 2
Methyl Butyl Ketone (2-Hexanone)ug/L17.6 5.0 20.00 2064-13788 2
Methyl Ethyl Ketone (2-Butanone)ug/L18.8 5.0 20.00 2071-13494 12
Methyl Isobutyl Ketone ug/L18.8 5.0 20.00 2069-13494 5
Methylene Chloride ug/L19.5 1.0 20.00 2073-13198 0
Methyl-tert-Butyl Ether ug/L20.3 0.50 20.00 2068-135102 5
Naphthalene ug/L17.6 1.0 20.00 2064-13688 2
n-Butylbenzene ug/L19.9 1.0 20.00 2068-134100 4
n-Propylbenzene ug/L20.6 0.50 20.00 2072-132103 2
o-Xylene ug/L20.8 0.50 20.00 2078-128104 4
sec-Butylbenzene ug/L19.7 0.50 20.00 2071-13199 5
Styrene ug/L19.4 0.50 20.00 2078-12997 3
tert-Butylbenzene ug/L21.3 0.50 20.00 2070-132107 5
Tetrachloroethylene ug/L22.7 0.50 20.00 2080-129113 6
Toluene ug/L20.5 0.50 20.00 2076-131103 1
trans-1,2-Dichloroethylene ug/L21.2 0.50 20.00 2076-135106 0.7
trans-1,3-Dichloropropylene ug/L20.6 0.50 20.00 2067-140103 2
Trichloroethylene ug/L21.6 0.50 20.00 2077-133108 2
Trichlorofluoromethane ug/L23.6 0.50 20.00 2062-148118 2
Vinyl acetate ug/L22.2 2.0 20.00 2034-167111 6
Vinyl chloride ug/L20.2 0.50 20.00 2057-141101 4
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9647.9
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9547.5
ug/L 50.00 77-123Surrogate: Toluene-d8 9547.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 157 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0362 - 5035
Blank (P7D0362-BLK1)Prepared & Analyzed: 04/21/17
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 158 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0362 - 5035
Blank (P7D0362-BLK1)Prepared & Analyzed: 04/21/17
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10351.3
ug/L 50.00 76-129Surrogate: Toluene-d8 9246.0
LCS (P7D0362-BS1)Prepared & Analyzed: 04/21/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0506 0.0050 0.05000 72-115101
1,1,1-Trichloroethane mg/kg wet0.0592 0.0050 0.05000 67-131118
1,1,2,2-Tetrachloroethane mg/kg wet0.0439 0.0050 0.05000 56-12688
1,1,2-Trichloroethane mg/kg wet0.0478 0.0050 0.05000 70-13396
1,1-Dichloroethane mg/kg wet0.0515 0.0050 0.05000 74-127103
1,1-Dichloroethylene mg/kg wet0.0529 0.0050 0.05000 67-149106
1,1-Dichloropropylene mg/kg wet0.0540 0.0050 0.05000 71-130108
1,2,3-Trichlorobenzene mg/kg wet0.0437 0.0050 0.05000 68-13087
1,2,3-Trichloropropane mg/kg wet0.0455 0.0050 0.05000 60-13791
1,2,4-Trichlorobenzene mg/kg wet0.0444 0.0050 0.05000 66-12589
1,2,4-Trimethylbenzene mg/kg wet0.0456 0.0050 0.05000 69-12991
1,2-Dibromoethane mg/kg wet0.0494 0.0050 0.05000 70-13299
1,2-Dichlorobenzene mg/kg wet0.0456 0.0050 0.05000 72-12391
1,2-Dichloroethane mg/kg wet0.0497 0.0050 0.05000 68-12899
1,2-Dichloropropane mg/kg wet0.0523 0.0050 0.05000 73-130105
1,3,5-Trimethylbenzene mg/kg wet0.0451 0.0050 0.05000 69-12890
1,3-Dichlorobenzene mg/kg wet0.0455 0.0050 0.05000 71-12091
1,3-Dichloropropane mg/kg wet0.0475 0.0050 0.05000 75-12495
1,4-Dichlorobenzene mg/kg wet0.0452 0.0050 0.05000 71-12390
2,2-Dichloropropane mg/kg wet0.0589 0.0050 0.05000 50-142118
2-Chlorotoluene mg/kg wet0.0449 0.0050 0.05000 67-12490
4-Chlorotoluene mg/kg wet0.0449 0.0050 0.05000 71-12690
4-Isopropyltoluene mg/kg wet0.0453 0.0050 0.05000 68-12991
Acetone mg/kg wet0.0937 0.050 0.1000 29-19894
Benzene mg/kg wet0.0513 0.0030 0.05000 74-127103
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 159 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0362 - 5035
LCS (P7D0362-BS1)Prepared & Analyzed: 04/21/17
Bromobenzene mg/kg wet0.0433 0.0050 0.05000 73-12587
Bromochloromethane mg/kg wet0.0539 0.0050 0.05000 72-134108
Bromodichloromethane mg/kg wet0.0585 0.0050 0.05000 75-122117
Bromoform mg/kg wet0.0494 0.0050 0.05000 66-13599
Bromomethane mg/kg wet0.0627 0.010 0.05000 20-180125
Carbon Tetrachloride mg/kg wet0.0698 0.0050 0.05000 64-143140
Chlorobenzene mg/kg wet0.0486 0.0050 0.05000 74-11897
Chloroethane mg/kg wet0.0602 0.010 0.05000 33-149120
Chloroform mg/kg wet0.0516 0.0050 0.05000 73-127103
Chloromethane mg/kg wet0.0484 0.0050 0.05000 45-14397
cis-1,2-Dichloroethylene mg/kg wet0.0514 0.0050 0.05000 76-134103
cis-1,3-Dichloropropylene mg/kg wet0.0594 0.0050 0.05000 71-125119
Dibromochloromethane mg/kg wet0.0507 0.0050 0.05000 73-122101
Dichlorodifluoromethane mg/kg wet0.0403 0.0050 0.05000 26-14681
Ethylbenzene mg/kg wet0.0493 0.0050 0.05000 74-12899
Isopropyl Ether mg/kg wet0.0474 0.0050 0.05000 59-15995
Isopropylbenzene (Cumene)mg/kg wet0.0449 0.0050 0.05000 68-12690
m,p-Xylenes mg/kg wet0.0994 0.010 0.1000 75-12499
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0446 0.050 0.05000 J61-15789
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0424 0.10 0.05000 J63-14985
Methyl Isobutyl Ketone mg/kg wet0.0486 0.050 0.05000 J57-16297
Methylene Chloride mg/kg wet0.0486 0.0050 0.05000 74-12997
Methyl-tert-Butyl Ether mg/kg wet0.0521 0.010 0.05000 70-130104
Naphthalene mg/kg wet0.0420 0.010 0.05000 57-15784
n-Butylbenzene mg/kg wet0.0457 0.0050 0.05000 65-13591
n-Propylbenzene mg/kg wet0.0461 0.0050 0.05000 67-13092
o-Xylene mg/kg wet0.0486 0.0050 0.05000 74-12697
sec-Butylbenzene mg/kg wet0.0461 0.0050 0.05000 66-13192
Styrene mg/kg wet0.0489 0.0050 0.05000 77-12198
tert-Butylbenzene mg/kg wet0.0455 0.0050 0.05000 67-13291
Tetrachloroethylene mg/kg wet0.0526 0.0050 0.05000 68-130105
Toluene mg/kg wet0.0514 0.0050 0.05000 71-129103
trans-1,2-Dichloroethylene mg/kg wet0.0523 0.0050 0.05000 73-132105
trans-1,3-Dichloropropylene mg/kg wet0.0533 0.0050 0.05000 68-123107
Trichloroethylene mg/kg wet0.0522 0.0050 0.05000 75-133104
Trichlorofluoromethane mg/kg wet0.0599 0.0050 0.05000 44-146120
Vinyl acetate mg/kg wet0.0582 0.025 0.05000 85-161116
Vinyl chloride mg/kg wet0.0443 0.0050 0.05000 48-14789
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9849.0
ug/L 50.00 76-129Surrogate: Toluene-d8 9246.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 160 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0362 - 5035
LCS Dup (P7D0362-BSD1)Prepared & Analyzed: 04/21/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0490 0.0050 0.05000 2072-11598 3
1,1,1-Trichloroethane mg/kg wet0.0567 0.0050 0.05000 2067-131113 4
1,1,2,2-Tetrachloroethane mg/kg wet0.0437 0.0050 0.05000 2056-12687 0.5
1,1,2-Trichloroethane mg/kg wet0.0469 0.0050 0.05000 2070-13394 2
1,1-Dichloroethane mg/kg wet0.0493 0.0050 0.05000 2074-12799 4
1,1-Dichloroethylene mg/kg wet0.0496 0.0050 0.05000 2067-14999 6
1,1-Dichloropropylene mg/kg wet0.0523 0.0050 0.05000 2071-130105 3
1,2,3-Trichlorobenzene mg/kg wet0.0451 0.0050 0.05000 2068-13090 3
1,2,3-Trichloropropane mg/kg wet0.0448 0.0050 0.05000 2060-13790 2
1,2,4-Trichlorobenzene mg/kg wet0.0455 0.0050 0.05000 2066-12591 2
1,2,4-Trimethylbenzene mg/kg wet0.0448 0.0050 0.05000 2069-12990 2
1,2-Dibromoethane mg/kg wet0.0486 0.0050 0.05000 2070-13297 2
1,2-Dichlorobenzene mg/kg wet0.0461 0.0050 0.05000 2072-12392 1
1,2-Dichloroethane mg/kg wet0.0494 0.0050 0.05000 2068-12899 0.8
1,2-Dichloropropane mg/kg wet0.0504 0.0050 0.05000 2073-130101 4
1,3,5-Trimethylbenzene mg/kg wet0.0445 0.0050 0.05000 2069-12889 1
1,3-Dichlorobenzene mg/kg wet0.0456 0.0050 0.05000 2071-12091 0.3
1,3-Dichloropropane mg/kg wet0.0474 0.0050 0.05000 2075-12495 0.2
1,4-Dichlorobenzene mg/kg wet0.0453 0.0050 0.05000 2071-12391 0.2
2,2-Dichloropropane mg/kg wet0.0571 0.0050 0.05000 2050-142114 3
2-Chlorotoluene mg/kg wet0.0445 0.0050 0.05000 2067-12489 0.8
4-Chlorotoluene mg/kg wet0.0451 0.0050 0.05000 2071-12690 0.4
4-Isopropyltoluene mg/kg wet0.0446 0.0050 0.05000 2068-12989 2
Acetone mg/kg wet0.0895 0.050 0.1000 2029-19890 5
Benzene mg/kg wet0.0495 0.0030 0.05000 2074-12799 4
Bromobenzene mg/kg wet0.0436 0.0050 0.05000 2073-12587 0.6
Bromochloromethane mg/kg wet0.0524 0.0050 0.05000 2072-134105 3
Bromodichloromethane mg/kg wet0.0575 0.0050 0.05000 2075-122115 2
Bromoform mg/kg wet0.0491 0.0050 0.05000 2066-13598 0.4
Bromomethane mg/kg wet0.0557 0.010 0.05000 2020-180111 12
Carbon Tetrachloride mg/kg wet0.0679 0.0050 0.05000 2064-143136 3
Chlorobenzene mg/kg wet0.0484 0.0050 0.05000 2074-11897 0.5
Chloroethane mg/kg wet0.0552 0.010 0.05000 2033-149110 9
Chloroform mg/kg wet0.0497 0.0050 0.05000 2073-12799 4
Chloromethane mg/kg wet0.0450 0.0050 0.05000 2045-14390 7
cis-1,2-Dichloroethylene mg/kg wet0.0503 0.0050 0.05000 2076-134101 2
cis-1,3-Dichloropropylene mg/kg wet0.0580 0.0050 0.05000 2071-125116 2
Dibromochloromethane mg/kg wet0.0505 0.0050 0.05000 2073-122101 0.4
Dichlorodifluoromethane mg/kg wet0.0383 0.0050 0.05000 2026-14677 5
Ethylbenzene mg/kg wet0.0478 0.0050 0.05000 2074-12896 3
Isopropyl Ether mg/kg wet0.0468 0.0050 0.05000 2059-15994 1
Isopropylbenzene (Cumene)mg/kg wet0.0444 0.0050 0.05000 2068-12689 1
m,p-Xylenes mg/kg wet0.0962 0.010 0.1000 2075-12496 3
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0438 0.050 0.05000 20 J61-15788 2
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0410 0.10 0.05000 20 J63-14982 3
Methyl Isobutyl Ketone mg/kg wet0.0473 0.050 0.05000 20 J57-16295 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 161 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0362 - 5035
LCS Dup (P7D0362-BSD1)Prepared & Analyzed: 04/21/17
Methylene Chloride mg/kg wet0.0470 0.0050 0.05000 2074-12994 3
Methyl-tert-Butyl Ether mg/kg wet0.0519 0.010 0.05000 2070-130104 0.5
Naphthalene mg/kg wet0.0426 0.010 0.05000 2057-15785 1
n-Butylbenzene mg/kg wet0.0454 0.0050 0.05000 2065-13591 0.8
n-Propylbenzene mg/kg wet0.0456 0.0050 0.05000 2067-13091 1
o-Xylene mg/kg wet0.0469 0.0050 0.05000 2074-12694 3
sec-Butylbenzene mg/kg wet0.0456 0.0050 0.05000 2066-13191 1
Styrene mg/kg wet0.0484 0.0050 0.05000 2077-12197 1
tert-Butylbenzene mg/kg wet0.0450 0.0050 0.05000 2067-13290 1
Tetrachloroethylene mg/kg wet0.0506 0.0050 0.05000 2068-130101 4
Toluene mg/kg wet0.0499 0.0050 0.05000 2071-129100 3
trans-1,2-Dichloroethylene mg/kg wet0.0507 0.0050 0.05000 2073-132101 3
trans-1,3-Dichloropropylene mg/kg wet0.0526 0.0050 0.05000 2068-123105 1
Trichloroethylene mg/kg wet0.0506 0.0050 0.05000 2075-133101 3
Trichlorofluoromethane mg/kg wet0.0582 0.0050 0.05000 2044-146116 3
Vinyl acetate mg/kg wet0.0572 0.025 0.05000 2085-161114 2
Vinyl chloride mg/kg wet0.0443 0.0050 0.05000 2048-14789 0.09
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.4
ug/L 50.00 76-129Surrogate: Toluene-d8 9246.0
Matrix Spike (P7D0362-MS1)Prepared & Analyzed: 04/21/17 Source: 7040298-08
1,1,1,2-Tetrachloroethane mg/kg dry0.0517 0.0081 0.08076 BRL 60-12064
1,1,1-Trichloroethane mg/kg dry0.0720 0.0081 0.08076 BRL 52-13989
1,1,2,2-Tetrachloroethane mg/kg dry0.0416 0.0081 0.08076 BRL 39-13552
1,1,2-Trichloroethane mg/kg dry0.0521 0.0081 0.08076 BRL 44-14065
1,1-Dichloroethane mg/kg dry0.0605 0.0081 0.08076 BRL 59-13775
1,1-Dichloroethylene mg/kg dry0.0656 0.0081 0.08076 BRL 54-16281
1,1-Dichloropropylene mg/kg dry0.0656 0.0081 0.08076 BRL 55-13781
1,2,3-Trichlorobenzene mg/kg dry0.0238 0.0081 0.08076 BRL M34-12030
1,2,3-Trichloropropane mg/kg dry0.0443 0.0081 0.08076 BRL 45-13955
1,2,4-Trichlorobenzene mg/kg dry0.0243 0.0081 0.08076 BRL M35-11630
1,2,4-Trimethylbenzene mg/kg dry0.0518 0.0081 0.08076 BRL 38-14264
1,2-Dibromoethane mg/kg dry0.0529 0.0081 0.08076 BRL 49-13266
1,2-Dichlorobenzene mg/kg dry0.0395 0.0081 0.08076 BRL 42-13049
1,2-Dichloroethane mg/kg dry0.0541 0.0081 0.08076 BRL 51-13167
1,2-Dichloropropane mg/kg dry0.0579 0.0081 0.08076 BRL 55-13872
1,3,5-Trimethylbenzene mg/kg dry0.0477 0.0081 0.08076 BRL 44-14059
1,3-Dichlorobenzene mg/kg dry0.0394 0.0081 0.08076 BRL 41-12949
1,3-Dichloropropane mg/kg dry0.0513 0.0081 0.08076 BRL 53-12964
1,4-Dichlorobenzene mg/kg dry0.0391 0.0081 0.08076 BRL 44-13448
2,2-Dichloropropane mg/kg dry0.0787 0.0081 0.08076 BRL 30-14797
2-Chlorotoluene mg/kg dry0.0439 0.0081 0.08076 BRL 46-13254
4-Chlorotoluene mg/kg dry0.0415 0.0081 0.08076 BRL 44-13551
4-Isopropyltoluene mg/kg dry0.0409 0.0081 0.08076 BRL 32-14451
Acetone mg/kg dry0.0773 0.081 0.1615 0.121 M, J34-143NR
Benzene mg/kg dry0.0604 0.0048 0.08076 BRL 60-13575
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 162 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0362 - 5035
Matrix Spike (P7D0362-MS1)Prepared & Analyzed: 04/21/17 Source: 7040298-08
Bromobenzene mg/kg dry0.0424 0.0081 0.08076 BRL 45-13552
Bromochloromethane mg/kg dry0.0630 0.0081 0.08076 BRL 55-13678
Bromodichloromethane mg/kg dry0.0601 0.0081 0.08076 BRL 55-12774
Bromoform mg/kg dry0.0440 0.0081 0.08076 BRL 40-13654
Bromomethane mg/kg dry0.0497 0.016 0.08076 BRL 30-13762
Carbon Tetrachloride mg/kg dry0.0783 0.0081 0.08076 BRL 48-15397
Chlorobenzene mg/kg dry0.0538 0.0081 0.08076 BRL 57-12567
Chloroethane mg/kg dry0.0655 0.016 0.08076 BRL 16-17781
Chloroform mg/kg dry0.0604 0.0081 0.08076 BRL 56-13775
Chloromethane mg/kg dry0.0519 0.0081 0.08076 BRL 40-14564
cis-1,2-Dichloroethylene mg/kg dry0.0599 0.0081 0.08076 BRL 58-14074
cis-1,3-Dichloropropylene mg/kg dry0.0566 0.0081 0.08076 BRL 42-13570
Dibromochloromethane mg/kg dry0.0501 0.0081 0.08076 BRL 49-12762
Dichlorodifluoromethane mg/kg dry0.0488 0.0081 0.08076 BRL 25-15160
Ethylbenzene mg/kg dry0.0561 0.0081 0.08076 BRL 44-14470
Isopropyl Ether mg/kg dry0.0513 0.0081 0.08076 BRL 51-15564
Isopropylbenzene (Cumene)mg/kg dry0.0479 0.0081 0.08076 BRL 41-14059
m,p-Xylenes mg/kg dry0.112 0.016 0.1615 BRL 36-14869
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0175 0.081 0.08076 BRL M, J30-14722
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0292 0.16 0.08076 BRL M, J24-16036
Methyl Isobutyl Ketone mg/kg dry0.0353 0.081 0.08076 BRL J25-16344
Methylene Chloride mg/kg dry0.0533 0.0081 0.08076 0.0129 M53-14450
Methyl-tert-Butyl Ether mg/kg dry0.0601 0.016 0.08076 BRL 49-13574
Naphthalene mg/kg dry0.0342 0.016 0.08076 BRL 32-12742
n-Butylbenzene mg/kg dry0.0362 0.0081 0.08076 BRL 23-14845
n-Propylbenzene mg/kg dry0.0465 0.0081 0.08076 BRL 35-14458
o-Xylene mg/kg dry0.0575 0.0081 0.08076 BRL 43-14371
sec-Butylbenzene mg/kg dry0.0437 0.0081 0.08076 BRL 34-14454
Styrene mg/kg dry0.0424 0.0081 0.08076 BRL 42-13252
tert-Butylbenzene mg/kg dry0.0468 0.0081 0.08076 BRL 36-15058
Tetrachloroethylene mg/kg dry0.0616 0.0081 0.08076 BRL 47-14276
Toluene mg/kg dry0.0625 0.0081 0.08076 BRL 57-13577
trans-1,2-Dichloroethylene mg/kg dry0.0634 0.0081 0.08076 BRL 58-14179
trans-1,3-Dichloropropylene mg/kg dry0.0551 0.0081 0.08076 BRL 41-12468
Trichloroethylene mg/kg dry0.0656 0.0081 0.08076 BRL 38-16481
Trichlorofluoromethane mg/kg dry0.0742 0.0081 0.08076 BRL 30-15792
Vinyl acetate mg/kg dryBRL0.040 0.08076 BRL M61-154
Vinyl chloride mg/kg dry0.0616 0.0081 0.08076 BRL 40-15676
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.5
ug/L 50.00 76-129Surrogate: Toluene-d8 9045.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 163 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0362 - 5035
Matrix Spike Dup (P7D0362-MSD1)Prepared & Analyzed: 04/21/17 Source: 7040298-08
1,1,1,2-Tetrachloroethane mg/kg dry0.0554 0.0078 0.07767 BRL 1560-12071 7
1,1,1-Trichloroethane mg/kg dry0.0758 0.0078 0.07767 BRL 2152-13998 5
1,1,2,2-Tetrachloroethane mg/kg dry0.0403 0.0078 0.07767 BRL 2239-13552 3
1,1,2-Trichloroethane mg/kg dry0.0522 0.0078 0.07767 BRL 2144-14067 0.2
1,1-Dichloroethane mg/kg dry0.0626 0.0078 0.07767 BRL 2159-13781 3
1,1-Dichloroethylene mg/kg dry0.0675 0.0078 0.07767 BRL 2254-16287 3
1,1-Dichloropropylene mg/kg dry0.0682 0.0078 0.07767 BRL 1955-13788 4
1,2,3-Trichlorobenzene mg/kg dry0.0248 0.0078 0.07767 BRL 41 M34-12032 4
1,2,3-Trichloropropane mg/kg dry0.0429 0.0078 0.07767 BRL 2545-13955 3
1,2,4-Trichlorobenzene mg/kg dry0.0271 0.0078 0.07767 BRL 6235-11635 11
1,2,4-Trimethylbenzene mg/kg dry0.0489 0.0078 0.07767 BRL 2438-14263 6
1,2-Dibromoethane mg/kg dry0.0531 0.0078 0.07767 BRL 1549-13268 0.3
1,2-Dichlorobenzene mg/kg dry0.0405 0.0078 0.07767 BRL 2142-13052 3
1,2-Dichloroethane mg/kg dry0.0548 0.0078 0.07767 BRL 1351-13171 1
1,2-Dichloropropane mg/kg dry0.0586 0.0078 0.07767 BRL 1655-13875 1
1,3,5-Trimethylbenzene mg/kg dry0.0462 0.0078 0.07767 BRL 2944-14060 3
1,3-Dichlorobenzene mg/kg dry0.0411 0.0078 0.07767 BRL 2441-12953 4
1,3-Dichloropropane mg/kg dry0.0523 0.0078 0.07767 BRL 1553-12967 2
1,4-Dichlorobenzene mg/kg dry0.0401 0.0078 0.07767 BRL 2144-13452 2
2,2-Dichloropropane mg/kg dry0.0821 0.0078 0.07767 BRL 2030-147106 4
2-Chlorotoluene mg/kg dry0.0429 0.0078 0.07767 BRL 2946-13255 2
4-Chlorotoluene mg/kg dry0.0412 0.0078 0.07767 BRL 2344-13553 0.7
4-Isopropyltoluene mg/kg dry0.0430 0.0078 0.07767 BRL 2232-14455 5
Acetone mg/kg dry0.0806 0.078 0.1553 0.121 49 M34-143NR 4
Benzene mg/kg dry0.0618 0.0047 0.07767 BRL 2060-13580 2
Bromobenzene mg/kg dry0.0410 0.0078 0.07767 BRL 2545-13553 3
Bromochloromethane mg/kg dry0.0627 0.0078 0.07767 BRL 1855-13681 0.5
Bromodichloromethane mg/kg dry0.0631 0.0078 0.07767 BRL 1755-12781 5
Bromoform mg/kg dry0.0473 0.0078 0.07767 BRL 3540-13661 7
Bromomethane mg/kg dry0.0593 0.016 0.07767 BRL 3030-13776 18
Carbon Tetrachloride mg/kg dry0.0862 0.0078 0.07767 BRL 2348-153111 10
Chlorobenzene mg/kg dry0.0556 0.0078 0.07767 BRL 1457-12572 3
Chloroethane mg/kg dry0.0690 0.016 0.07767 BRL 4716-17789 5
Chloroform mg/kg dry0.0620 0.0078 0.07767 BRL 1856-13780 3
Chloromethane mg/kg dry0.0553 0.0078 0.07767 BRL 2640-14571 6
cis-1,2-Dichloroethylene mg/kg dry0.0617 0.0078 0.07767 BRL 2858-14079 3
cis-1,3-Dichloropropylene mg/kg dry0.0576 0.0078 0.07767 BRL 3242-13574 2
Dibromochloromethane mg/kg dry0.0530 0.0078 0.07767 BRL 2449-12768 6
Dichlorodifluoromethane mg/kg dry0.0496 0.0078 0.07767 BRL 3725-15164 2
Ethylbenzene mg/kg dry0.0579 0.0078 0.07767 BRL 1944-14475 3
Isopropyl Ether mg/kg dry0.0522 0.0078 0.07767 BRL 1351-15567 2
Isopropylbenzene (Cumene)mg/kg dry0.0477 0.0078 0.07767 BRL 2741-14061 0.5
m,p-Xylenes mg/kg dry0.111 0.016 0.1553 BRL 2036-14871 1
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0174 0.078 0.07767 BRL 42 M, J30-14722 0.3
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0278 0.16 0.07767 BRL 42 M, J24-16036 5
Methyl Isobutyl Ketone mg/kg dry0.0327 0.078 0.07767 BRL 44 J25-16342 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 164 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0362 - 5035
Matrix Spike Dup (P7D0362-MSD1)Prepared & Analyzed: 04/21/17 Source: 7040298-08
Methylene Chloride mg/kg dry0.0550 0.0078 0.07767 0.0129 1453-14454 3
Methyl-tert-Butyl Ether mg/kg dry0.0603 0.016 0.07767 BRL 2249-13578 0.3
Naphthalene mg/kg dry0.0328 0.016 0.07767 BRL 4432-12742 4
n-Butylbenzene mg/kg dry0.0377 0.0078 0.07767 BRL 3923-14849 4
n-Propylbenzene mg/kg dry0.0453 0.0078 0.07767 BRL 2735-14458 3
o-Xylene mg/kg dry0.0580 0.0078 0.07767 BRL 1743-14375 0.8
sec-Butylbenzene mg/kg dry0.0461 0.0078 0.07767 BRL 2834-14459 5
Styrene mg/kg dry0.0435 0.0078 0.07767 BRL 2842-13256 3
tert-Butylbenzene mg/kg dry0.0490 0.0078 0.07767 BRL 2936-15063 5
Tetrachloroethylene mg/kg dry0.0633 0.0078 0.07767 BRL 2647-14282 3
Toluene mg/kg dry0.0626 0.0078 0.07767 BRL 2257-13581 0.09
trans-1,2-Dichloroethylene mg/kg dry0.0654 0.0078 0.07767 BRL 1858-14184 3
trans-1,3-Dichloropropylene mg/kg dry0.0554 0.0078 0.07767 BRL 2041-12471 0.6
Trichloroethylene mg/kg dry0.0673 0.0078 0.07767 BRL 1838-16487 3
Trichlorofluoromethane mg/kg dry0.0769 0.0078 0.07767 BRL 2730-15799 3
Vinyl acetate mg/kg dryBRL0.039 0.07767 BRL 35 M61-154
Vinyl chloride mg/kg dry0.0639 0.0078 0.07767 BRL 3540-15682 4
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9647.9
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.7
ug/L 50.00 76-129Surrogate: Toluene-d8 9145.6
Batch P7D0381 - 5035
Blank (P7D0381-BLK1)Prepared & Analyzed: 04/24/17
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 165 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0381 - 5035
Blank (P7D0381-BLK1)Prepared & Analyzed: 04/24/17
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10452.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 76-129Surrogate: Toluene-d8 9145.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 166 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0381 - 5035
LCS (P7D0381-BS1)Prepared & Analyzed: 04/24/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0534 0.0050 0.05000 72-115107
1,1,1-Trichloroethane mg/kg wet0.0606 0.0050 0.05000 67-131121
1,1,2,2-Tetrachloroethane mg/kg wet0.0428 0.0050 0.05000 56-12686
1,1,2-Trichloroethane mg/kg wet0.0483 0.0050 0.05000 70-13397
1,1-Dichloroethane mg/kg wet0.0510 0.0050 0.05000 74-127102
1,1-Dichloroethylene mg/kg wet0.0552 0.0050 0.05000 67-149110
1,1-Dichloropropylene mg/kg wet0.0546 0.0050 0.05000 71-130109
1,2,3-Trichlorobenzene mg/kg wet0.0460 0.0050 0.05000 68-13092
1,2,3-Trichloropropane mg/kg wet0.0449 0.0050 0.05000 60-13790
1,2,4-Trichlorobenzene mg/kg wet0.0470 0.0050 0.05000 66-12594
1,2,4-Trimethylbenzene mg/kg wet0.0466 0.0050 0.05000 69-12993
1,2-Dibromoethane mg/kg wet0.0507 0.0050 0.05000 70-132101
1,2-Dichlorobenzene mg/kg wet0.0471 0.0050 0.05000 72-12394
1,2-Dichloroethane mg/kg wet0.0504 0.0050 0.05000 68-128101
1,2-Dichloropropane mg/kg wet0.0511 0.0050 0.05000 73-130102
1,3,5-Trimethylbenzene mg/kg wet0.0456 0.0050 0.05000 69-12891
1,3-Dichlorobenzene mg/kg wet0.0464 0.0050 0.05000 71-12093
1,3-Dichloropropane mg/kg wet0.0484 0.0050 0.05000 75-12497
1,4-Dichlorobenzene mg/kg wet0.0462 0.0050 0.05000 71-12392
2,2-Dichloropropane mg/kg wet0.0679 0.0050 0.05000 50-142136
2-Chlorotoluene mg/kg wet0.0455 0.0050 0.05000 67-12491
4-Chlorotoluene mg/kg wet0.0458 0.0050 0.05000 71-12692
4-Isopropyltoluene mg/kg wet0.0458 0.0050 0.05000 68-12992
Acetone mg/kg wet0.0920 0.050 0.1000 29-19892
Benzene mg/kg wet0.0518 0.0030 0.05000 74-127104
Bromobenzene mg/kg wet0.0436 0.0050 0.05000 73-12587
Bromochloromethane mg/kg wet0.0546 0.0050 0.05000 72-134109
Bromodichloromethane mg/kg wet0.0591 0.0050 0.05000 75-122118
Bromoform mg/kg wet0.0520 0.0050 0.05000 66-135104
Bromomethane mg/kg wet0.0734 0.010 0.05000 20-180147
Carbon Tetrachloride mg/kg wet0.0736 0.0050 0.05000 L164-143147
Chlorobenzene mg/kg wet0.0505 0.0050 0.05000 74-118101
Chloroethane mg/kg wet0.0662 0.010 0.05000 33-149132
Chloroform mg/kg wet0.0519 0.0050 0.05000 73-127104
Chloromethane mg/kg wet0.0526 0.0050 0.05000 45-143105
cis-1,2-Dichloroethylene mg/kg wet0.0516 0.0050 0.05000 76-134103
cis-1,3-Dichloropropylene mg/kg wet0.0612 0.0050 0.05000 71-125122
Dibromochloromethane mg/kg wet0.0533 0.0050 0.05000 73-122107
Dichlorodifluoromethane mg/kg wet0.0627 0.0050 0.05000 26-146125
Ethylbenzene mg/kg wet0.0503 0.0050 0.05000 74-128101
Isopropyl Ether mg/kg wet0.0464 0.0050 0.05000 59-15993
Isopropylbenzene (Cumene)mg/kg wet0.0455 0.0050 0.05000 68-12691
m,p-Xylenes mg/kg wet0.102 0.010 0.1000 75-124102
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0432 0.050 0.05000 J61-15786
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0419 0.10 0.05000 J63-14984
Methyl Isobutyl Ketone mg/kg wet0.0462 0.050 0.05000 J57-16292
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 167 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0381 - 5035
LCS (P7D0381-BS1)Prepared & Analyzed: 04/24/17
Methylene Chloride mg/kg wet0.0470 0.0050 0.05000 74-12994
Methyl-tert-Butyl Ether mg/kg wet0.0555 0.010 0.05000 70-130111
Naphthalene mg/kg wet0.0433 0.010 0.05000 57-15787
n-Butylbenzene mg/kg wet0.0460 0.0050 0.05000 65-13592
n-Propylbenzene mg/kg wet0.0462 0.0050 0.05000 67-13092
o-Xylene mg/kg wet0.0501 0.0050 0.05000 74-126100
sec-Butylbenzene mg/kg wet0.0463 0.0050 0.05000 66-13193
Styrene mg/kg wet0.0504 0.0050 0.05000 77-121101
tert-Butylbenzene mg/kg wet0.0460 0.0050 0.05000 67-13292
Tetrachloroethylene mg/kg wet0.0532 0.0050 0.05000 68-130106
Toluene mg/kg wet0.0521 0.0050 0.05000 71-129104
trans-1,2-Dichloroethylene mg/kg wet0.0535 0.0050 0.05000 73-132107
trans-1,3-Dichloropropylene mg/kg wet0.0564 0.0050 0.05000 68-123113
Trichloroethylene mg/kg wet0.0547 0.0050 0.05000 75-133109
Trichlorofluoromethane mg/kg wet0.0692 0.0050 0.05000 44-146138
Vinyl acetate mg/kg wet0.0618 0.025 0.05000 85-161124
Vinyl chloride mg/kg wet0.0561 0.0050 0.05000 48-147112
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.8
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9648.0
ug/L 50.00 76-129Surrogate: Toluene-d8 9145.4
LCS Dup (P7D0381-BSD1)Prepared & Analyzed: 04/24/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0504 0.0050 0.05000 2072-115101 6
1,1,1-Trichloroethane mg/kg wet0.0574 0.0050 0.05000 2067-131115 5
1,1,2,2-Tetrachloroethane mg/kg wet0.0424 0.0050 0.05000 2056-12685 1
1,1,2-Trichloroethane mg/kg wet0.0470 0.0050 0.05000 2070-13394 3
1,1-Dichloroethane mg/kg wet0.0489 0.0050 0.05000 2074-12798 4
1,1-Dichloroethylene mg/kg wet0.0518 0.0050 0.05000 2067-149104 6
1,1-Dichloropropylene mg/kg wet0.0510 0.0050 0.05000 2071-130102 7
1,2,3-Trichlorobenzene mg/kg wet0.0446 0.0050 0.05000 2068-13089 3
1,2,3-Trichloropropane mg/kg wet0.0443 0.0050 0.05000 2060-13789 1
1,2,4-Trichlorobenzene mg/kg wet0.0451 0.0050 0.05000 2066-12590 4
1,2,4-Trimethylbenzene mg/kg wet0.0440 0.0050 0.05000 2069-12988 6
1,2-Dibromoethane mg/kg wet0.0497 0.0050 0.05000 2070-13299 2
1,2-Dichlorobenzene mg/kg wet0.0452 0.0050 0.05000 2072-12390 4
1,2-Dichloroethane mg/kg wet0.0490 0.0050 0.05000 2068-12898 3
1,2-Dichloropropane mg/kg wet0.0491 0.0050 0.05000 2073-13098 4
1,3,5-Trimethylbenzene mg/kg wet0.0429 0.0050 0.05000 2069-12886 6
1,3-Dichlorobenzene mg/kg wet0.0442 0.0050 0.05000 2071-12088 5
1,3-Dichloropropane mg/kg wet0.0472 0.0050 0.05000 2075-12494 3
1,4-Dichlorobenzene mg/kg wet0.0444 0.0050 0.05000 2071-12389 4
2,2-Dichloropropane mg/kg wet0.0634 0.0050 0.05000 2050-142127 7
2-Chlorotoluene mg/kg wet0.0426 0.0050 0.05000 2067-12485 6
4-Chlorotoluene mg/kg wet0.0433 0.0050 0.05000 2071-12687 6
4-Isopropyltoluene mg/kg wet0.0429 0.0050 0.05000 2068-12986 7
Acetone mg/kg wet0.0937 0.050 0.1000 2029-19894 2
Benzene mg/kg wet0.0493 0.0030 0.05000 2074-12799 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 168 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7D0381 - 5035
LCS Dup (P7D0381-BSD1)Prepared & Analyzed: 04/24/17
Bromobenzene mg/kg wet0.0415 0.0050 0.05000 2073-12583 5
Bromochloromethane mg/kg wet0.0529 0.0050 0.05000 2072-134106 3
Bromodichloromethane mg/kg wet0.0569 0.0050 0.05000 2075-122114 4
Bromoform mg/kg wet0.0508 0.0050 0.05000 2066-135102 2
Bromomethane mg/kg wet0.0621 0.010 0.05000 2020-180124 17
Carbon Tetrachloride mg/kg wet0.0688 0.0050 0.05000 2064-143138 7
Chlorobenzene mg/kg wet0.0473 0.0050 0.05000 2074-11895 6
Chloroethane mg/kg wet0.0613 0.010 0.05000 2033-149123 8
Chloroform mg/kg wet0.0497 0.0050 0.05000 2073-12799 4
Chloromethane mg/kg wet0.0508 0.0050 0.05000 2045-143102 4
cis-1,2-Dichloroethylene mg/kg wet0.0495 0.0050 0.05000 2076-13499 4
cis-1,3-Dichloropropylene mg/kg wet0.0599 0.0050 0.05000 2071-125120 2
Dibromochloromethane mg/kg wet0.0512 0.0050 0.05000 2073-122102 4
Dichlorodifluoromethane mg/kg wet0.0559 0.0050 0.05000 2026-146112 11
Ethylbenzene mg/kg wet0.0467 0.0050 0.05000 2074-12893 7
Isopropyl Ether mg/kg wet0.0450 0.0050 0.05000 2059-15990 3
Isopropylbenzene (Cumene)mg/kg wet0.0424 0.0050 0.05000 2068-12685 7
m,p-Xylenes mg/kg wet0.0949 0.010 0.1000 2075-12495 7
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0438 0.050 0.05000 20 J61-15788 1
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0427 0.10 0.05000 20 J63-14985 2
Methyl Isobutyl Ketone mg/kg wet0.0470 0.050 0.05000 20 J57-16294 2
Methylene Chloride mg/kg wet0.0458 0.0050 0.05000 2074-12992 3
Methyl-tert-Butyl Ether mg/kg wet0.0548 0.010 0.05000 2070-130110 1
Naphthalene mg/kg wet0.0437 0.010 0.05000 2057-15787 1
n-Butylbenzene mg/kg wet0.0430 0.0050 0.05000 2065-13586 7
n-Propylbenzene mg/kg wet0.0429 0.0050 0.05000 2067-13086 7
o-Xylene mg/kg wet0.0468 0.0050 0.05000 2074-12694 7
sec-Butylbenzene mg/kg wet0.0430 0.0050 0.05000 2066-13186 7
Styrene mg/kg wet0.0481 0.0050 0.05000 2077-12196 5
tert-Butylbenzene mg/kg wet0.0426 0.0050 0.05000 2067-13285 8
Tetrachloroethylene mg/kg wet0.0496 0.0050 0.05000 2068-13099 7
Toluene mg/kg wet0.0493 0.0050 0.05000 2071-12999 6
trans-1,2-Dichloroethylene mg/kg wet0.0504 0.0050 0.05000 2073-132101 6
trans-1,3-Dichloropropylene mg/kg wet0.0550 0.0050 0.05000 2068-123110 3
Trichloroethylene mg/kg wet0.0510 0.0050 0.05000 2075-133102 7
Trichlorofluoromethane mg/kg wet0.0637 0.0050 0.05000 2044-146127 8
Vinyl acetate mg/kg wet0.0621 0.025 0.05000 2085-161124 0.6
Vinyl chloride mg/kg wet0.0518 0.0050 0.05000 2048-147104 8
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 76-129Surrogate: Toluene-d8 9145.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 169 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P7D0394 - 5035
Blank (P7D0394-BLK1)Prepared & Analyzed: 04/24/17
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.010
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.010
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.020
Benzene mg/kg wetBRL0.0050
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.010
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.010
Ethylbenzene mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 170 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P7D0394 - 5035
Blank (P7D0394-BLK1)Prepared & Analyzed: 04/24/17
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.020
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020
Methyl Isobutyl Ketone mg/kg wetBRL0.020
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.0050
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.010
Vinyl acetate mg/kg wetBRL0.020
Vinyl chloride mg/kg wetBRL0.010
Xylenes, total mg/kg wetBRL0.015
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10452.0
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10452.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 70-130Surrogate: Toluene-d8 9145.6
ug/L 50.00 70-130Surrogate: Toluene-d8 9145.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 171 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P7D0394 - 5035
LCS (P7D0394-BS1)Prepared & Analyzed: 04/24/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0534 0.0050 0.05000 72-115107
1,1,1-Trichloroethane mg/kg wet0.0606 0.0050 0.05000 72-123121
1,1,2,2-Tetrachloroethane mg/kg wet0.0428 0.0050 0.05000 62-12786
1,1,2-Trichloroethane mg/kg wet0.0483 0.0050 0.05000 73-12397
1,1-Dichloroethane mg/kg wet0.0510 0.0050 0.05000 73-119102
1,1-Dichloroethylene mg/kg wet0.0552 0.0050 0.05000 59-157110
1,1-Dichloropropylene mg/kg wet0.0546 0.0050 0.05000 70-129109
1,2,3-Trichlorobenzene mg/kg wet0.0460 0.010 0.05000 59-13392
1,2,3-Trichloropropane mg/kg wet0.0449 0.0050 0.05000 52-13790
1,2,4-Trichlorobenzene mg/kg wet0.0470 0.010 0.05000 66-12394
1,2,4-Trimethylbenzene mg/kg wet0.0466 0.0050 0.05000 69-12693
1,2,4-Trimethylbenzene mg/kg wet0.0466 0.0050 0.05000 69-12693
1,2-Dibromoethane mg/kg wet0.0507 0.0050 0.05000 69-127101
1,2-Dichlorobenzene mg/kg wet0.0471 0.0050 0.05000 70-12194
1,2-Dichloroethane mg/kg wet0.0504 0.0050 0.05000 69-125101
1,2-Dichloropropane mg/kg wet0.0511 0.0050 0.05000 75-124102
1,3,5-Trimethylbenzene mg/kg wet0.0456 0.0050 0.05000 69-12491
1,3,5-Trimethylbenzene mg/kg wet0.0456 0.0050 0.05000 69-12491
1,3-Dichlorobenzene mg/kg wet0.0464 0.0050 0.05000 70-12193
1,3-Dichloropropane mg/kg wet0.0484 0.0050 0.05000 70-12497
1,4-Dichlorobenzene mg/kg wet0.0462 0.0050 0.05000 71-11992
2,2-Dichloropropane mg/kg wet0.0679 0.0050 0.05000 46-154136
2-Chlorotoluene mg/kg wet0.0455 0.0050 0.05000 70-12191
4-Chlorotoluene mg/kg wet0.0458 0.0050 0.05000 72-12692
4-Isopropyltoluene mg/kg wet0.0458 0.0050 0.05000 71-12692
4-Isopropyltoluene mg/kg wet0.0458 0.0050 0.05000 71-12692
Acetone mg/kg wet0.0920 0.020 0.1000 12-19692
Benzene mg/kg wet0.0518 0.0050 0.05000 74-123104
Bromobenzene mg/kg wet0.0436 0.0050 0.05000 66-12287
Bromochloromethane mg/kg wet0.0546 0.0050 0.05000 73-128109
Bromodichloromethane mg/kg wet0.0591 0.0050 0.05000 76-123118
Bromoform mg/kg wet0.0520 0.0050 0.05000 71-124104
Bromomethane mg/kg wet0.0734 0.010 0.05000 L156-145147
Carbon Tetrachloride mg/kg wet0.0736 0.0050 0.05000 L167-140147
Chlorobenzene mg/kg wet0.0505 0.0050 0.05000 74-121101
Chloroethane mg/kg wet0.0662 0.010 0.05000 64-142132
Chloroform mg/kg wet0.0519 0.0050 0.05000 75-125104
Chloromethane mg/kg wet0.0526 0.010 0.05000 54-132105
cis-1,2-Dichloroethylene mg/kg wet0.0516 0.0050 0.05000 68-132103
cis-1,3-Dichloropropylene mg/kg wet0.0612 0.0050 0.05000 75-128122
Dibromochloromethane mg/kg wet0.0533 0.0050 0.05000 71-121107
Dichlorodifluoromethane mg/kg wet0.0627 0.010 0.05000 39-178125
Ethylbenzene mg/kg wet0.0503 0.0050 0.05000 69-125101
Ethylbenzene mg/kg wet0.0503 0.0050 0.05000 69-125101
Isopropyl Ether mg/kg wet0.0464 0.0050 0.05000 77-12393
Isopropylbenzene (Cumene)mg/kg wet0.0455 0.0050 0.05000 68-12991
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 172 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P7D0394 - 5035
LCS (P7D0394-BS1)Prepared & Analyzed: 04/24/17
Isopropylbenzene (Cumene)mg/kg wet0.0455 0.0050 0.05000 68-12991
m,p-Xylenes mg/kg wet0.102 0.010 0.1000 64-125102
m,p-Xylenes mg/kg wet0.102 0.010 0.1000 64-125102
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0432 0.020 0.05000 54-13986
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0419 0.020 0.05000 34-16584
Methyl Isobutyl Ketone mg/kg wet0.0462 0.020 0.05000 63-13092
Methylene Chloride mg/kg wet0.0470 0.0050 0.05000 65-13594
Methyl-tert-Butyl Ether mg/kg wet0.0555 0.0050 0.05000 62-123111
Naphthalene mg/kg wet0.0433 0.010 0.05000 58-12987
n-Butylbenzene mg/kg wet0.0460 0.0050 0.05000 71-12692
n-Propylbenzene mg/kg wet0.0462 0.0050 0.05000 68-12892
n-Propylbenzene mg/kg wet0.0462 0.0050 0.05000 68-12892
o-Xylene mg/kg wet0.0501 0.0050 0.05000 69-121100
o-Xylene mg/kg wet0.0501 0.0050 0.05000 69-121100
sec-Butylbenzene mg/kg wet0.0463 0.0050 0.05000 71-12893
sec-Butylbenzene mg/kg wet0.0463 0.0050 0.05000 71-12893
Styrene mg/kg wet0.0504 0.0050 0.05000 67-129101
tert-Butylbenzene mg/kg wet0.0460 0.0050 0.05000 71-12692
Tetrachloroethylene mg/kg wet0.0532 0.0050 0.05000 71-124106
Toluene mg/kg wet0.0521 0.0050 0.05000 74-122104
Toluene mg/kg wet0.0521 0.0050 0.05000 74-122104
trans-1,2-Dichloroethylene mg/kg wet0.0535 0.0050 0.05000 69-129107
trans-1,3-Dichloropropylene mg/kg wet0.0564 0.0050 0.05000 74-127113
Trichloroethylene mg/kg wet0.0547 0.0050 0.05000 68-133109
Trichlorofluoromethane mg/kg wet0.0692 0.010 0.05000 60-138138
Vinyl acetate mg/kg wet0.0618 0.020 0.05000 14-179124
Vinyl chloride mg/kg wet0.0561 0.010 0.05000 69-135112
Xylenes, total mg/kg wet0.152 0.015 0.1500 74-126101
Xylenes, total mg/kg wet0.152 0.015 0.1500 74-126101
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.8
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9648.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9648.0
ug/L 50.00 70-130Surrogate: Toluene-d8 9145.4
ug/L 50.00 70-130Surrogate: Toluene-d8 9145.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 173 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P7D0394 - 5035
LCS Dup (P7D0394-BSD1)Prepared & Analyzed: 04/24/17
1,1,1,2-Tetrachloroethane mg/kg wet0.0504 0.0050 0.05000 2072-115101 6
1,1,1-Trichloroethane mg/kg wet0.0574 0.0050 0.05000 2072-123115 5
1,1,2,2-Tetrachloroethane mg/kg wet0.0424 0.0050 0.05000 2062-12785 1
1,1,2-Trichloroethane mg/kg wet0.0470 0.0050 0.05000 2073-12394 3
1,1-Dichloroethane mg/kg wet0.0489 0.0050 0.05000 2073-11998 4
1,1-Dichloroethylene mg/kg wet0.0518 0.0050 0.05000 2059-157104 6
1,1-Dichloropropylene mg/kg wet0.0510 0.0050 0.05000 2070-129102 7
1,2,3-Trichlorobenzene mg/kg wet0.0446 0.010 0.05000 2059-13389 3
1,2,3-Trichloropropane mg/kg wet0.0443 0.0050 0.05000 2052-13789 1
1,2,4-Trichlorobenzene mg/kg wet0.0451 0.010 0.05000 2066-12390 4
1,2,4-Trimethylbenzene mg/kg wet0.0440 0.0050 0.05000 2069-12688 6
1,2,4-Trimethylbenzene mg/kg wet0.0440 0.0050 0.05000 2069-12688 6
1,2-Dibromoethane mg/kg wet0.0497 0.0050 0.05000 2069-12799 2
1,2-Dichlorobenzene mg/kg wet0.0452 0.0050 0.05000 2070-12190 4
1,2-Dichloroethane mg/kg wet0.0490 0.0050 0.05000 2069-12598 3
1,2-Dichloropropane mg/kg wet0.0491 0.0050 0.05000 2075-12498 4
1,3,5-Trimethylbenzene mg/kg wet0.0429 0.0050 0.05000 2069-12486 6
1,3,5-Trimethylbenzene mg/kg wet0.0429 0.0050 0.05000 2069-12486 6
1,3-Dichlorobenzene mg/kg wet0.0442 0.0050 0.05000 2070-12188 5
1,3-Dichloropropane mg/kg wet0.0472 0.0050 0.05000 2070-12494 3
1,4-Dichlorobenzene mg/kg wet0.0444 0.0050 0.05000 2071-11989 4
2,2-Dichloropropane mg/kg wet0.0634 0.0050 0.05000 2046-154127 7
2-Chlorotoluene mg/kg wet0.0426 0.0050 0.05000 2070-12185 6
4-Chlorotoluene mg/kg wet0.0433 0.0050 0.05000 2072-12687 6
4-Isopropyltoluene mg/kg wet0.0429 0.0050 0.05000 2071-12686 7
4-Isopropyltoluene mg/kg wet0.0429 0.0050 0.05000 2071-12686 7
Acetone mg/kg wet0.0937 0.020 0.1000 2012-19694 2
Benzene mg/kg wet0.0493 0.0050 0.05000 2074-12399 5
Bromobenzene mg/kg wet0.0415 0.0050 0.05000 2066-12283 5
Bromochloromethane mg/kg wet0.0529 0.0050 0.05000 2073-128106 3
Bromodichloromethane mg/kg wet0.0569 0.0050 0.05000 2076-123114 4
Bromoform mg/kg wet0.0508 0.0050 0.05000 2071-124102 2
Bromomethane mg/kg wet0.0621 0.010 0.05000 2056-145124 17
Carbon Tetrachloride mg/kg wet0.0688 0.0050 0.05000 2067-140138 7
Chlorobenzene mg/kg wet0.0473 0.0050 0.05000 2074-12195 6
Chloroethane mg/kg wet0.0613 0.010 0.05000 2064-142123 8
Chloroform mg/kg wet0.0497 0.0050 0.05000 2075-12599 4
Chloromethane mg/kg wet0.0508 0.010 0.05000 2054-132102 4
cis-1,2-Dichloroethylene mg/kg wet0.0495 0.0050 0.05000 2068-13299 4
cis-1,3-Dichloropropylene mg/kg wet0.0599 0.0050 0.05000 2075-128120 2
Dibromochloromethane mg/kg wet0.0512 0.0050 0.05000 2071-121102 4
Dichlorodifluoromethane mg/kg wet0.0559 0.010 0.05000 2039-178112 11
Ethylbenzene mg/kg wet0.0467 0.0050 0.05000 2069-12593 7
Ethylbenzene mg/kg wet0.0467 0.0050 0.05000 2069-12593 7
Isopropyl Ether mg/kg wet0.0450 0.0050 0.05000 2077-12390 3
Isopropylbenzene (Cumene)mg/kg wet0.0424 0.0050 0.05000 2068-12985 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 174 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P7D0394 - 5035
LCS Dup (P7D0394-BSD1)Prepared & Analyzed: 04/24/17
Isopropylbenzene (Cumene)mg/kg wet0.0424 0.0050 0.05000 2068-12985 7
m,p-Xylenes mg/kg wet0.0949 0.010 0.1000 2064-12595 7
m,p-Xylenes mg/kg wet0.0949 0.010 0.1000 2064-12595 7
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0438 0.020 0.05000 2054-13988 1
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0427 0.020 0.05000 2034-16585 2
Methyl Isobutyl Ketone mg/kg wet0.0470 0.020 0.05000 2063-13094 2
Methylene Chloride mg/kg wet0.0458 0.0050 0.05000 2065-13592 3
Methyl-tert-Butyl Ether mg/kg wet0.0548 0.0050 0.05000 2062-123110 1
Naphthalene mg/kg wet0.0437 0.010 0.05000 2058-12987 1
n-Butylbenzene mg/kg wet0.0430 0.0050 0.05000 2071-12686 7
n-Propylbenzene mg/kg wet0.0429 0.0050 0.05000 2068-12886 7
n-Propylbenzene mg/kg wet0.0429 0.0050 0.05000 2068-12886 7
o-Xylene mg/kg wet0.0468 0.0050 0.05000 2069-12194 7
o-Xylene mg/kg wet0.0468 0.0050 0.05000 2069-12194 7
sec-Butylbenzene mg/kg wet0.0430 0.0050 0.05000 2071-12886 7
sec-Butylbenzene mg/kg wet0.0430 0.0050 0.05000 2071-12886 7
Styrene mg/kg wet0.0481 0.0050 0.05000 2067-12996 5
tert-Butylbenzene mg/kg wet0.0426 0.0050 0.05000 2071-12685 8
Tetrachloroethylene mg/kg wet0.0496 0.0050 0.05000 2071-12499 7
Toluene mg/kg wet0.0493 0.0050 0.05000 2074-12299 6
Toluene mg/kg wet0.0493 0.0050 0.05000 2074-12299 6
trans-1,2-Dichloroethylene mg/kg wet0.0504 0.0050 0.05000 2069-129101 6
trans-1,3-Dichloropropylene mg/kg wet0.0550 0.0050 0.05000 2074-127110 3
Trichloroethylene mg/kg wet0.0510 0.0050 0.05000 2068-133102 7
Trichlorofluoromethane mg/kg wet0.0637 0.010 0.05000 2060-138127 8
Vinyl acetate mg/kg wet0.0621 0.020 0.05000 2014-179124 0.6
Vinyl chloride mg/kg wet0.0518 0.010 0.05000 2069-135104 8
Xylenes, total mg/kg wet0.142 0.015 0.1500 20074-12694 7
Xylenes, total mg/kg wet0.142 0.015 0.1500 20074-12694 7
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.1
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.1
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 70-130Surrogate: Toluene-d8 9145.5
ug/L 50.00 70-130Surrogate: Toluene-d8 9145.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 175 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0251 - 3510C MS
Blank (P7D0251-BLK1)Prepared & Analyzed: 04/18/17
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1-Methylnaphthalene ug/LBRL10
2,4,5-Trichlorophenol ug/LBRL10
2,4,6-Trichlorophenol ug/LBRL10
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL10
2,4-Dinitrotoluene ug/LBRL10
2,6-Dinitrotoluene ug/LBRL10
2-Chloronaphthalene ug/LBRL10
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Methylphenol ug/LBRL10
2-Nitroaniline ug/LBRL10
2-Nitrophenol ug/LBRL10
3,3'-Dichlorobenzidine ug/LBRL10
3/4-Methylphenol ug/LBRL10
3-Nitroaniline ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL10
4-Bromophenyl phenyl ether ug/LBRL10
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL10
4-Nitroaniline ug/LBRL10
4-Nitrophenol ug/LBRL10
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL10
Aniline ug/LBRL10
Anthracene ug/LBRL10
Azobenzene ug/LBRL10
Benzo(a)anthracene ug/LBRL10
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzoic Acid ug/LBRL100
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chrysene ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 176 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0251 - 3510C MS
Blank (P7D0251-BLK1)Prepared & Analyzed: 04/18/17
Dibenzo(a,h)anthracene ug/LBRL10
Dibenzofuran ug/LBRL10
Diethyl phthalate ug/LBRL10
Dimethyl phthalate ug/LBRL10
Di-n-butyl phthalate ug/LBRL10
Di-n-octyl phthalate ug/LBRL10
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Hexachlorobenzene ug/LBRL10
Hexachlorobutadiene ug/LBRL10
Hexachlorocyclopentadiene ug/LBRL10
Hexachloroethane ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isophorone ug/LBRL10
Naphthalene ug/LBRL10
Nitrobenzene ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL10
N-Nitrosodiphenylamine ug/LBRL10
Pentachlorophenol ug/LBRL10
Phenanthrene ug/LBRL10
Phenol ug/LBRL10
Pyrene ug/LBRL10
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 9898.5
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8140.7
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5453.6
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7437.2
ug/L 100.0 11-52Surrogate: Phenol-d5 3434.0
ug/L 50.00 50-134Surrogate: Terphenyl-d14 10954.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 177 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0251 - 3510C MS
LCS (P7D0251-BS1)Prepared & Analyzed: 04/18/17
1,2,4-Trichlorobenzene ug/L30.9 10 50.00 29-12662
1,2-Dichlorobenzene ug/L32.0 10 50.00 32-11164
1,3-Dichlorobenzene ug/L30.7 10 50.00 28-11061
1,4-Dichlorobenzene ug/L30.6 10 50.00 29-11261
1-Methylnaphthalene ug/L35.6 10 50.00 41-11971
2,4,5-Trichlorophenol ug/L44.7 10 50.00 53-12389
2,4,6-Trichlorophenol ug/L43.6 10 50.00 50-12587
2,4-Dichlorophenol ug/L36.3 10 50.00 47-12173
2,4-Dimethylphenol ug/L40.0 10 50.00 31-12480
2,4-Dinitrophenol ug/L66.2 10 50.00 23-143132
2,4-Dinitrotoluene ug/L47.8 10 50.00 57-12896
2,6-Dinitrotoluene ug/L47.3 10 50.00 57-12495
2-Chloronaphthalene ug/L41.2 10 50.00 40-11682
2-Chlorophenol ug/L38.0 10 50.00 38-11776
2-Methylnaphthalene ug/L35.1 10 50.00 40-12170
2-Methylphenol ug/L36.8 10 50.00 30-11774
2-Nitroaniline ug/L41.9 10 50.00 55-12784
2-Nitrophenol ug/L37.0 10 50.00 47-12374
3,3'-Dichlorobenzidine ug/L48.8 10 50.00 27-12998
3/4-Methylphenol ug/L31.1 10 50.00 29-11062
3-Nitroaniline ug/L42.1 10 50.00 41-12884
4,6-Dinitro-2-methylphenol ug/L47.0 10 50.00 44-13794
4-Bromophenyl phenyl ether ug/L43.8 10 50.00 55-12488
4-Chloro-3-methylphenol ug/L39.4 10 50.00 52-11979
4-Chloroaniline ug/L34.2 10 50.00 33-11768
4-Chlorophenyl phenyl ether ug/L42.0 10 50.00 53-12184
4-Nitroaniline ug/L42.1 10 50.00 45-13584
4-Nitrophenol ug/L21.3 10 50.00 10-7743
Acenaphthene ug/L43.3 10 50.00 47-12287
Acenaphthylene ug/L42.5 10 50.00 41-13085
Aniline ug/L48.4 10 50.00 12-19797
Anthracene ug/L46.0 10 50.00 57-12392
Azobenzene ug/L41.2 10 50.00 61-11682
Benzo(a)anthracene ug/L47.0 10 50.00 58-12594
Benzo(a)pyrene ug/L46.1 10 50.00 54-12892
Benzo(b)fluoranthene ug/L46.0 10 50.00 53-13192
Benzo(g,h,i)perylene ug/L42.2 10 50.00 50-13484
Benzo(k)fluoranthene ug/L46.2 10 50.00 57-12992
Benzoic Acid ug/L13.0 100 50.00 J10-12526
Benzyl alcohol ug/L36.7 10 50.00 31-11273
bis(2-Chloroethoxy)methane ug/L34.6 10 50.00 48-12069
Bis(2-Chloroethyl)ether ug/L34.8 10 50.00 43-11870
Bis(2-chloroisopropyl)ether ug/L37.3 10 50.00 37-13075
Bis(2-Ethylhexyl)phthalate ug/L47.3 10 50.00 55-13595
Butyl benzyl phthalate ug/L44.2 10 50.00 53-13488
Chrysene ug/L47.8 10 50.00 59-12396
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 178 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0251 - 3510C MS
LCS (P7D0251-BS1)Prepared & Analyzed: 04/18/17
Dibenzo(a,h)anthracene ug/L47.8 10 50.00 51-13496
Dibenzofuran ug/L43.7 10 50.00 53-11887
Diethyl phthalate ug/L44.2 10 50.00 56-12588
Dimethyl phthalate ug/L44.1 10 50.00 45-12788
Di-n-butyl phthalate ug/L44.1 10 50.00 59-12788
Di-n-octyl phthalate ug/L47.5 10 50.00 51-14095
Fluoranthene ug/L45.8 10 50.00 57-12892
Fluorene ug/L44.1 10 50.00 52-12488
Hexachlorobenzene ug/L46.2 10 50.00 53-12592
Hexachlorobutadiene ug/L29.7 10 50.00 22-12459
Hexachlorocyclopentadiene ug/L11.9 10 50.00 L32-11724
Hexachloroethane ug/L27.2 10 50.00 21-11554
Indeno(1,2,3-cd)pyrene ug/L44.3 10 50.00 52-13489
Isophorone ug/L35.8 10 50.00 42-12472
Naphthalene ug/L34.3 10 50.00 40-12169
Nitrobenzene ug/L32.4 10 50.00 45-12165
N-Nitroso-di-n-propylamine ug/L37.1 10 50.00 49-11974
N-Nitrosodiphenylamine ug/L55.1 10 50.00 51-123110
Pentachlorophenol ug/L63.1 10 50.00 35-138126
Phenanthrene ug/L45.6 10 50.00 59-12091
Phenol ug/L20.0 10 50.00 12-5840
Pyrene ug/L47.2 10 50.00 57-12694
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 9897.9
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8040.0
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5150.9
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6431.8
ug/L 100.0 11-52Surrogate: Phenol-d5 3333.4
ug/L 50.00 50-134Surrogate: Terphenyl-d14 10251.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 179 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0251 - 3510C MS
LCS Dup (P7D0251-BSD1)Prepared & Analyzed: 04/18/17
1,2,4-Trichlorobenzene ug/L28.9 10 50.00 2029-12658 7
1,2-Dichlorobenzene ug/L28.5 10 50.00 2032-11157 12
1,3-Dichlorobenzene ug/L27.4 10 50.00 2028-11055 11
1,4-Dichlorobenzene ug/L26.8 10 50.00 2029-11254 13
1-Methylnaphthalene ug/L34.3 10 50.00 2041-11969 4
2,4,5-Trichlorophenol ug/L43.6 10 50.00 2053-12387 3
2,4,6-Trichlorophenol ug/L43.2 10 50.00 2050-12586 1
2,4-Dichlorophenol ug/L35.3 10 50.00 2047-12171 3
2,4-Dimethylphenol ug/L39.2 10 50.00 2031-12478 2
2,4-Dinitrophenol ug/L64.2 10 50.00 2023-143128 3
2,4-Dinitrotoluene ug/L47.3 10 50.00 2057-12895 1
2,6-Dinitrotoluene ug/L47.7 10 50.00 2057-12495 0.7
2-Chloronaphthalene ug/L39.9 10 50.00 2040-11680 3
2-Chlorophenol ug/L35.4 10 50.00 2038-11771 7
2-Methylnaphthalene ug/L33.8 10 50.00 2040-12168 4
2-Methylphenol ug/L34.6 10 50.00 2030-11769 6
2-Nitroaniline ug/L41.0 10 50.00 2055-12782 2
2-Nitrophenol ug/L35.8 10 50.00 2047-12372 3
3,3'-Dichlorobenzidine ug/L48.0 10 50.00 2027-12996 2
3/4-Methylphenol ug/L29.6 10 50.00 2029-11059 5
3-Nitroaniline ug/L39.3 10 50.00 2041-12879 7
4,6-Dinitro-2-methylphenol ug/L47.1 10 50.00 2044-13794 0.1
4-Bromophenyl phenyl ether ug/L44.4 10 50.00 2055-12489 1
4-Chloro-3-methylphenol ug/L38.0 10 50.00 2052-11976 4
4-Chloroaniline ug/L31.4 10 50.00 2033-11763 9
4-Chlorophenyl phenyl ether ug/L42.5 10 50.00 2053-12185 1
4-Nitroaniline ug/L41.4 10 50.00 2045-13583 2
4-Nitrophenol ug/L20.1 10 50.00 2010-7740 6
Acenaphthene ug/L43.1 10 50.00 2047-12286 0.5
Acenaphthylene ug/L41.2 10 50.00 2041-13082 3
Aniline ug/L43.1 10 50.00 2012-19786 12
Anthracene ug/L46.3 10 50.00 2057-12393 0.6
Azobenzene ug/L40.8 10 50.00 2061-11682 1
Benzo(a)anthracene ug/L46.6 10 50.00 2058-12593 0.8
Benzo(a)pyrene ug/L45.9 10 50.00 2054-12892 0.3
Benzo(b)fluoranthene ug/L46.5 10 50.00 2053-13193 1
Benzo(g,h,i)perylene ug/L42.4 10 50.00 2050-13485 0.6
Benzo(k)fluoranthene ug/L45.9 10 50.00 2057-12992 0.7
Benzoic Acid ug/L7.49 100 50.00 20 D, J10-12515 54
Benzyl alcohol ug/L34.1 10 50.00 2031-11268 7
bis(2-Chloroethoxy)methane ug/L33.0 10 50.00 2048-12066 5
Bis(2-Chloroethyl)ether ug/L31.7 10 50.00 2043-11863 9
Bis(2-chloroisopropyl)ether ug/L35.0 10 50.00 2037-13070 6
Bis(2-Ethylhexyl)phthalate ug/L46.4 10 50.00 2055-13593 2
Butyl benzyl phthalate ug/L43.9 10 50.00 2053-13488 0.7
Chrysene ug/L47.7 10 50.00 2059-12395 0.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 180 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0251 - 3510C MS
LCS Dup (P7D0251-BSD1)Prepared & Analyzed: 04/18/17
Dibenzo(a,h)anthracene ug/L45.6 10 50.00 2051-13491 5
Dibenzofuran ug/L43.2 10 50.00 2053-11886 1
Diethyl phthalate ug/L43.7 10 50.00 2056-12587 1
Dimethyl phthalate ug/L44.0 10 50.00 2045-12788 0.3
Di-n-butyl phthalate ug/L44.1 10 50.00 2059-12788 0.1
Di-n-octyl phthalate ug/L47.0 10 50.00 2051-14094 1
Fluoranthene ug/L45.6 10 50.00 2057-12891 0.5
Fluorene ug/L43.5 10 50.00 2052-12487 1
Hexachlorobenzene ug/L46.2 10 50.00 2053-12592 0.02
Hexachlorobutadiene ug/L27.5 10 50.00 2022-12455 8
Hexachlorocyclopentadiene ug/L11.1 10 50.00 20 L32-11722 7
Hexachloroethane ug/L24.2 10 50.00 2021-11548 12
Indeno(1,2,3-cd)pyrene ug/L44.2 10 50.00 2052-13488 0.2
Isophorone ug/L34.7 10 50.00 2042-12469 3
Naphthalene ug/L32.4 10 50.00 2040-12165 6
Nitrobenzene ug/L30.2 10 50.00 2045-12160 7
N-Nitroso-di-n-propylamine ug/L33.4 10 50.00 2049-11967 11
N-Nitrosodiphenylamine ug/L54.8 10 50.00 2051-123110 0.6
Pentachlorophenol ug/L62.9 10 50.00 2035-138126 0.3
Phenanthrene ug/L45.8 10 50.00 2059-12092 0.3
Phenol ug/L18.3 10 50.00 2012-5837 9
Pyrene ug/L47.0 10 50.00 2057-12694 0.4
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 9797.0
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7738.7
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 4645.8
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6130.4
ug/L 100.0 11-52Surrogate: Phenol-d5 3130.9
ug/L 50.00 50-134Surrogate: Terphenyl-d14 10351.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 181 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0273 - 3546
Blank (P7D0273-BLK1)Prepared: 04/18/17 Analyzed: 04/19/17
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 182 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0273 - 3546
Blank (P7D0273-BLK1)Prepared: 04/18/17 Analyzed: 04/19/17
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 923.05
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 871.44
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 852.83
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 791.31
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 842.81
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 1081.80
LCS (P7D0273-BS1)Prepared: 04/18/17 Analyzed: 04/19/17
1,2,4-Trichlorobenzene mg/kg wet1.11 0.33 1.667 34-11867
1,2-Dichlorobenzene mg/kg wet1.16 0.33 1.667 33-11770
1,3-Dichlorobenzene mg/kg wet1.14 0.33 1.667 30-11569
1,4-Dichlorobenzene mg/kg wet1.14 0.33 1.667 31-11568
1-Methylnaphthalene mg/kg wet1.22 0.33 1.667 40-11973
2,4,6-Trichlorophenol mg/kg wet1.39 0.33 1.667 39-12683
2,4-Dichlorophenol mg/kg wet1.21 0.33 1.667 40-12273
2,4-Dimethylphenol mg/kg wet1.30 0.33 1.667 30-12778
2,4-Dinitrophenol mg/kg wet1.74 0.33 1.667 27-129104
2,4-Dinitrotoluene mg/kg wet1.48 0.33 1.667 48-12689
2,6-Dinitrotoluene mg/kg wet1.47 0.33 1.667 46-12488
2-Chloronaphthalene mg/kg wet1.35 0.33 1.667 41-11481
2-Chlorophenol mg/kg wet1.37 0.33 1.667 34-12182
2-Methylnaphthalene mg/kg wet1.19 0.33 1.667 38-12271
2-Methylphenol mg/kg wet1.40 0.33 1.667 32-12284
2-Nitrophenol mg/kg wet1.17 0.33 1.667 36-12370
3,3'-Dichlorobenzidine mg/kg wet1.44 0.33 1.667 22-12187
3/4-Methylphenol mg/kg wet1.26 0.33 1.667 34-11976
4,6-Dinitro-2-methylphenol mg/kg wet1.59 0.33 1.667 29-13296
4-Bromophenyl phenyl ether mg/kg wet1.37 0.33 1.667 46-12482
4-Chloro-3-methylphenol mg/kg wet1.31 0.33 1.667 45-12278
4-Chloroaniline mg/kg wet1.14 0.33 1.667 17-10668
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 183 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0273 - 3546
LCS (P7D0273-BS1)Prepared: 04/18/17 Analyzed: 04/19/17
4-Chlorophenyl phenyl ether mg/kg wet1.35 0.33 1.667 45-12181
4-Nitrophenol mg/kg wet1.45 0.33 1.667 30-13287
Acenaphthene mg/kg wet1.46 0.33 1.667 40-12388
Acenaphthylene mg/kg wet1.42 0.33 1.667 32-13285
Anthracene mg/kg wet1.53 0.33 1.667 47-12392
Azobenzene mg/kg wet1.47 0.33 1.667 39-12588
Benzo(a)anthracene mg/kg wet1.53 0.33 1.667 49-12692
Benzo(a)pyrene mg/kg wet1.52 0.33 1.667 45-12991
Benzo(b)fluoranthene mg/kg wet1.52 0.33 1.667 45-13291
Benzo(g,h,i)perylene mg/kg wet1.38 0.33 1.667 43-13483
Benzo(k)fluoranthene mg/kg wet1.53 0.33 1.667 47-13292
Benzoic Acid mg/kg wet0.931 0.33 1.667 10-8356
Benzyl alcohol mg/kg wet1.33 0.33 1.667 29-12280
bis(2-Chloroethoxy)methane mg/kg wet1.17 0.33 1.667 36-12170
Bis(2-Chloroethyl)ether mg/kg wet1.12 0.33 1.667 31-12067
Bis(2-chloroisopropyl)ether mg/kg wet1.24 0.33 1.667 33-13174
Bis(2-Ethylhexyl)phthalate mg/kg wet1.58 0.33 1.667 51-13395
Butyl benzyl phthalate mg/kg wet1.57 0.33 1.667 48-13294
Chrysene mg/kg wet1.55 0.33 1.667 50-12493
Dibenzo(a,h)anthracene mg/kg wet1.51 0.33 1.667 45-13490
Dibenzofuran mg/kg wet1.42 0.33 1.667 44-12085
Diethyl phthalate mg/kg wet1.44 0.33 1.667 50-12486
Dimethyl phthalate mg/kg wet1.40 0.33 1.667 48-12484
Di-n-butyl phthalate mg/kg wet1.47 0.33 1.667 51-12888
Di-n-octyl phthalate mg/kg wet1.59 0.33 1.667 45-14095
Fluoranthene mg/kg wet1.53 0.33 1.667 50-12792
Fluorene mg/kg wet1.45 0.33 1.667 43-12587
Hexachlorobenzene mg/kg wet1.42 0.33 1.667 45-12285
Hexachlorobutadiene mg/kg wet1.15 0.33 1.667 32-12369
Hexachlorocyclopentadiene mg/kg wet0.420 0.33 1.667 L32-11725
Hexachloroethane mg/kg wet1.10 0.33 1.667 28-11766
Indeno(1,2,3-cd)pyrene mg/kg wet1.43 0.33 1.667 45-13386
Isophorone mg/kg wet1.21 0.33 1.667 30-12273
Naphthalene mg/kg wet1.20 0.33 1.667 35-12372
Nitrobenzene mg/kg wet1.13 0.33 1.667 34-12268
N-Nitroso-di-n-propylamine mg/kg wet1.26 0.33 1.667 36-12076
N-Nitrosodiphenylamine mg/kg wet1.80 0.33 1.667 38-127108
Pentachlorophenol mg/kg wet1.72 0.33 1.667 25-133103
Phenanthrene mg/kg wet1.52 0.33 1.667 50-12191
Phenol mg/kg wet1.40 0.33 1.667 34-12184
Pyrene mg/kg wet1.56 0.33 1.667 47-12793
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 862.86
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 791.31
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 792.62
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 641.07
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 782.60
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 184 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0273 - 3546
LCS (P7D0273-BS1)Prepared: 04/18/17 Analyzed: 04/19/17
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 981.63
LCS Dup (P7D0273-BSD1)Prepared: 04/18/17 Analyzed: 04/19/17
1,2,4-Trichlorobenzene mg/kg wet1.15 0.33 1.667 2034-11869 3
1,2-Dichlorobenzene mg/kg wet1.21 0.33 1.667 2033-11773 4
1,3-Dichlorobenzene mg/kg wet1.18 0.33 1.667 2030-11571 3
1,4-Dichlorobenzene mg/kg wet1.20 0.33 1.667 2031-11572 5
1-Methylnaphthalene mg/kg wet1.25 0.33 1.667 2040-11975 2
2,4,6-Trichlorophenol mg/kg wet1.43 0.33 1.667 2039-12686 3
2,4-Dichlorophenol mg/kg wet1.25 0.33 1.667 2040-12275 3
2,4-Dimethylphenol mg/kg wet1.34 0.33 1.667 2030-12781 3
2,4-Dinitrophenol mg/kg wet1.72 0.33 1.667 2027-129103 1
2,4-Dinitrotoluene mg/kg wet1.52 0.33 1.667 2048-12691 3
2,6-Dinitrotoluene mg/kg wet1.52 0.33 1.667 2046-12491 3
2-Chloronaphthalene mg/kg wet1.40 0.33 1.667 2041-11484 3
2-Chlorophenol mg/kg wet1.40 0.33 1.667 2034-12184 3
2-Methylnaphthalene mg/kg wet1.24 0.33 1.667 2038-12275 4
2-Methylphenol mg/kg wet1.41 0.33 1.667 2032-12285 0.8
2-Nitrophenol mg/kg wet1.23 0.33 1.667 2036-12374 5
3,3'-Dichlorobenzidine mg/kg wet1.43 0.33 1.667 2022-12186 0.8
3/4-Methylphenol mg/kg wet1.29 0.33 1.667 2034-11978 2
4,6-Dinitro-2-methylphenol mg/kg wet1.63 0.33 1.667 2029-13298 2
4-Bromophenyl phenyl ether mg/kg wet1.42 0.33 1.667 2046-12485 4
4-Chloro-3-methylphenol mg/kg wet1.32 0.33 1.667 2045-12279 1
4-Chloroaniline mg/kg wet1.17 0.33 1.667 2017-10670 3
4-Chlorophenyl phenyl ether mg/kg wet1.39 0.33 1.667 2045-12183 2
4-Nitrophenol mg/kg wet1.46 0.33 1.667 2030-13287 0.4
Acenaphthene mg/kg wet1.50 0.33 1.667 2040-12390 3
Acenaphthylene mg/kg wet1.48 0.33 1.667 2032-13289 4
Anthracene mg/kg wet1.56 0.33 1.667 2047-12394 2
Azobenzene mg/kg wet1.53 0.33 1.667 2039-12592 4
Benzo(a)anthracene mg/kg wet1.53 0.33 1.667 2049-12692 0.2
Benzo(a)pyrene mg/kg wet1.50 0.33 1.667 2045-12990 1
Benzo(b)fluoranthene mg/kg wet1.49 0.33 1.667 2045-13290 2
Benzo(g,h,i)perylene mg/kg wet1.38 0.33 1.667 2043-13483 0.2
Benzo(k)fluoranthene mg/kg wet1.54 0.33 1.667 2047-13292 0.07
Benzoic Acid mg/kg wet0.963 0.33 1.667 2010-8358 3
Benzyl alcohol mg/kg wet1.36 0.33 1.667 2029-12282 3
bis(2-Chloroethoxy)methane mg/kg wet1.20 0.33 1.667 2036-12172 3
Bis(2-Chloroethyl)ether mg/kg wet1.12 0.33 1.667 2031-12067 0.7
Bis(2-chloroisopropyl)ether mg/kg wet1.28 0.33 1.667 2033-13177 3
Bis(2-Ethylhexyl)phthalate mg/kg wet1.56 0.33 1.667 2051-13394 1
Butyl benzyl phthalate mg/kg wet1.57 0.33 1.667 2048-13294 0.2
Chrysene mg/kg wet1.55 0.33 1.667 2050-12493 0.1
Dibenzo(a,h)anthracene mg/kg wet1.48 0.33 1.667 2045-13489 2
Dibenzofuran mg/kg wet1.46 0.33 1.667 2044-12088 3
Diethyl phthalate mg/kg wet1.46 0.33 1.667 2050-12488 1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 185 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0273 - 3546
LCS Dup (P7D0273-BSD1)Prepared: 04/18/17 Analyzed: 04/19/17
Dimethyl phthalate mg/kg wet1.43 0.33 1.667 2048-12486 2
Di-n-butyl phthalate mg/kg wet1.49 0.33 1.667 2051-12890 2
Di-n-octyl phthalate mg/kg wet1.59 0.33 1.667 2045-14095 0.2
Fluoranthene mg/kg wet1.56 0.33 1.667 2050-12794 2
Fluorene mg/kg wet1.49 0.33 1.667 2043-12589 2
Hexachlorobenzene mg/kg wet1.47 0.33 1.667 2045-12288 3
Hexachlorobutadiene mg/kg wet1.20 0.33 1.667 2032-12372 4
Hexachlorocyclopentadiene mg/kg wet0.442 0.33 1.667 20 L32-11727 5
Hexachloroethane mg/kg wet1.16 0.33 1.667 2028-11769 5
Indeno(1,2,3-cd)pyrene mg/kg wet1.46 0.33 1.667 2045-13388 2
Isophorone mg/kg wet1.24 0.33 1.667 2030-12274 2
Naphthalene mg/kg wet1.26 0.33 1.667 2035-12376 5
Nitrobenzene mg/kg wet1.17 0.33 1.667 2034-12270 4
N-Nitroso-di-n-propylamine mg/kg wet1.31 0.33 1.667 2036-12078 3
N-Nitrosodiphenylamine mg/kg wet1.85 0.33 1.667 2038-127111 3
Pentachlorophenol mg/kg wet1.80 0.33 1.667 2025-133108 4
Phenanthrene mg/kg wet1.56 0.33 1.667 2050-12194 3
Phenol mg/kg wet1.41 0.33 1.667 2034-12185 0.5
Pyrene mg/kg wet1.55 0.33 1.667 2047-12793 0.3
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 892.98
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 811.35
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 802.67
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 681.13
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 802.65
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 981.63
Matrix Spike (P7D0273-MS1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-04
1,2,4-Trichlorobenzene mg/kg dry0.934 0.39 1.970 BRL 34-11847
1,2-Dichlorobenzene mg/kg dry0.965 0.39 1.970 BRL 33-11749
1,3-Dichlorobenzene mg/kg dry0.944 0.39 1.970 BRL 30-11548
1,4-Dichlorobenzene mg/kg dry0.938 0.39 1.970 BRL 31-11548
1-Methylnaphthalene mg/kg dry1.07 0.39 1.970 BRL 40-11954
2,4,6-Trichlorophenol mg/kg dry1.18 0.39 1.970 BRL 39-12660
2,4-Dichlorophenol mg/kg dry1.03 0.39 1.970 BRL 40-12252
2,4-Dimethylphenol mg/kg dry0.812 0.39 1.970 BRL 30-12741
2,4-Dinitrophenol mg/kg dry1.30 0.39 1.970 BRL 27-12966
2,4-Dinitrotoluene mg/kg dry1.25 0.39 1.970 BRL 48-12663
2,6-Dinitrotoluene mg/kg dry1.24 0.39 1.970 BRL 46-12463
2-Chloronaphthalene mg/kg dry1.15 0.39 1.970 BRL 41-11458
2-Chlorophenol mg/kg dry1.14 0.39 1.970 BRL 34-12158
2-Methylnaphthalene mg/kg dry1.04 0.39 1.970 BRL 38-12253
2-Methylphenol mg/kg dry1.10 0.39 1.970 BRL 32-12256
2-Nitrophenol mg/kg dry1.00 0.39 1.970 BRL 36-12351
3,3'-Dichlorobenzidine mg/kg dry0.148 0.39 1.970 BRL M, J22-1218
3/4-Methylphenol mg/kg dry1.03 0.39 1.970 BRL 34-11952
4,6-Dinitro-2-methylphenol mg/kg dry1.14 0.39 1.970 BRL 29-13258
4-Bromophenyl phenyl ether mg/kg dry1.18 0.39 1.970 BRL 46-12460
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 186 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0273 - 3546
Matrix Spike (P7D0273-MS1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-04
4-Chloro-3-methylphenol mg/kg dry1.13 0.39 1.970 BRL 45-12257
4-Chloroaniline mg/kg dry0.836 0.39 1.970 BRL 17-10642
4-Chlorophenyl phenyl ether mg/kg dry1.13 0.39 1.970 BRL 45-12157
4-Nitrophenol mg/kg dry1.23 0.39 1.970 BRL 30-13262
Acenaphthene mg/kg dry1.23 0.39 1.970 BRL 40-12363
Acenaphthylene mg/kg dry1.23 0.39 1.970 BRL 32-13262
Anthracene mg/kg dry1.33 0.39 1.970 BRL 47-12367
Azobenzene mg/kg dry1.30 0.39 1.970 BRL 39-12566
Benzo(a)anthracene mg/kg dry1.33 0.39 1.970 BRL 49-12667
Benzo(a)pyrene mg/kg dry1.27 0.39 1.970 BRL 45-12964
Benzo(b)fluoranthene mg/kg dry1.32 0.39 1.970 BRL 45-13267
Benzo(g,h,i)perylene mg/kg dry1.12 0.39 1.970 BRL 43-13457
Benzo(k)fluoranthene mg/kg dry1.24 0.39 1.970 BRL 47-13263
Benzoic Acid mg/kg dry0.854 0.39 1.970 BRL 10-8343
Benzyl alcohol mg/kg dry1.15 0.39 1.970 BRL 29-12259
bis(2-Chloroethoxy)methane mg/kg dry1.03 0.39 1.970 BRL 36-12152
Bis(2-Chloroethyl)ether mg/kg dry1.01 0.39 1.970 BRL 31-12051
Bis(2-chloroisopropyl)ether mg/kg dry1.11 0.39 1.970 BRL 33-13156
Bis(2-Ethylhexyl)phthalate mg/kg dry1.43 0.39 1.970 BRL 51-13373
Butyl benzyl phthalate mg/kg dry1.44 0.39 1.970 BRL 48-13273
Chrysene mg/kg dry1.32 0.39 1.970 BRL 50-12467
Dibenzo(a,h)anthracene mg/kg dry1.24 0.39 1.970 BRL 45-13463
Dibenzofuran mg/kg dry1.20 0.39 1.970 BRL 44-12061
Diethyl phthalate mg/kg dry1.21 0.39 1.970 BRL 50-12461
Dimethyl phthalate mg/kg dry1.19 0.39 1.970 BRL 48-12460
Di-n-butyl phthalate mg/kg dry1.31 0.39 1.970 BRL 51-12867
Di-n-octyl phthalate mg/kg dry1.47 0.39 1.970 BRL 45-14074
Fluoranthene mg/kg dry1.28 0.39 1.970 BRL 50-12765
Fluorene mg/kg dry1.24 0.39 1.970 BRL 43-12563
Hexachlorobenzene mg/kg dry1.20 0.39 1.970 BRL 45-12261
Hexachlorobutadiene mg/kg dry0.980 0.39 1.970 BRL 32-12350
Hexachlorocyclopentadiene mg/kg dry0.263 0.39 1.970 BRL M, J32-11713
Hexachloroethane mg/kg dry0.931 0.39 1.970 BRL 28-11747
Indeno(1,2,3-cd)pyrene mg/kg dry1.21 0.39 1.970 BRL 45-13361
Isophorone mg/kg dry1.06 0.39 1.970 BRL 30-12254
Naphthalene mg/kg dry1.06 0.39 1.970 BRL 35-12354
Nitrobenzene mg/kg dry0.979 0.39 1.970 BRL 34-12250
N-Nitroso-di-n-propylamine mg/kg dry1.05 0.39 1.970 BRL 36-12053
N-Nitrosodiphenylamine mg/kg dry1.49 0.39 1.970 BRL 38-12775
Pentachlorophenol mg/kg dry1.38 0.39 1.970 BRL 25-13370
Phenanthrene mg/kg dry1.31 0.39 1.970 BRL 50-12167
Phenol mg/kg dry1.13 0.39 1.970 BRL 34-12158
Pyrene mg/kg dry1.38 0.39 1.970 BRL 47-12770
mg/kg dry 3.940 39-132Surrogate: 2,4,6-Tribromophenol 562.21
mg/kg dry 1.970 44-115Surrogate: 2-Fluorobiphenyl 561.11
mg/kg dry 3.940 35-115Surrogate: 2-Fluorophenol 522.07
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 187 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0273 - 3546
Matrix Spike (P7D0273-MS1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-04
mg/kg dry 1.970 37-122Surrogate: Nitrobenzene-d5 480.939
mg/kg dry 3.940 34-121Surrogate: Phenol-d5 552.17
mg/kg dry 1.970 54-127Surrogate: Terphenyl-d14 721.41
Matrix Spike Dup (P7D0273-MSD1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-04
1,2,4-Trichlorobenzene mg/kg dry1.05 0.38 1.942 BRL 2034-11854 12
1,2-Dichlorobenzene mg/kg dry1.12 0.38 1.942 BRL 2033-11758 15
1,3-Dichlorobenzene mg/kg dry1.08 0.38 1.942 BRL 2030-11556 14
1,4-Dichlorobenzene mg/kg dry1.07 0.38 1.942 BRL 2031-11555 13
1-Methylnaphthalene mg/kg dry1.19 0.38 1.942 BRL 2040-11961 10
2,4,6-Trichlorophenol mg/kg dry1.36 0.38 1.942 BRL 2039-12670 15
2,4-Dichlorophenol mg/kg dry1.17 0.38 1.942 BRL 2040-12260 12
2,4-Dimethylphenol mg/kg dry0.917 0.38 1.942 BRL 2030-12747 12
2,4-Dinitrophenol mg/kg dry1.50 0.38 1.942 BRL 2027-12977 14
2,4-Dinitrotoluene mg/kg dry1.42 0.38 1.942 BRL 2048-12673 13
2,6-Dinitrotoluene mg/kg dry1.40 0.38 1.942 BRL 2046-12472 13
2-Chloronaphthalene mg/kg dry1.32 0.38 1.942 BRL 2041-11468 14
2-Chlorophenol mg/kg dry1.29 0.38 1.942 BRL 2034-12167 13
2-Methylnaphthalene mg/kg dry1.16 0.38 1.942 BRL 2038-12260 11
2-Methylphenol mg/kg dry1.24 0.38 1.942 BRL 2032-12264 12
2-Nitrophenol mg/kg dry1.15 0.38 1.942 BRL 2036-12359 13
3,3'-Dichlorobenzidine mg/kg dry0.262 0.38 1.942 BRL 20 D, M, J22-12113 55
3/4-Methylphenol mg/kg dry1.16 0.38 1.942 BRL 2034-11960 12
4,6-Dinitro-2-methylphenol mg/kg dry1.37 0.38 1.942 BRL 2029-13270 18
4-Bromophenyl phenyl ether mg/kg dry1.34 0.38 1.942 BRL 2046-12469 13
4-Chloro-3-methylphenol mg/kg dry1.28 0.38 1.942 BRL 2045-12266 13
4-Chloroaniline mg/kg dry0.957 0.38 1.942 BRL 2017-10649 13
4-Chlorophenyl phenyl ether mg/kg dry1.31 0.38 1.942 BRL 2045-12167 15
4-Nitrophenol mg/kg dry1.43 0.38 1.942 BRL 2030-13273 15
Acenaphthene mg/kg dry1.41 0.38 1.942 BRL 2040-12373 13
Acenaphthylene mg/kg dry1.39 0.38 1.942 BRL 2032-13272 12
Anthracene mg/kg dry1.52 0.38 1.942 BRL 2047-12378 14
Azobenzene mg/kg dry1.48 0.38 1.942 BRL 2039-12576 13
Benzo(a)anthracene mg/kg dry1.51 0.38 1.942 BRL 2049-12678 13
Benzo(a)pyrene mg/kg dry1.45 0.38 1.942 BRL 2045-12975 13
Benzo(b)fluoranthene mg/kg dry1.50 0.38 1.942 BRL 2045-13277 13
Benzo(g,h,i)perylene mg/kg dry1.28 0.38 1.942 BRL 2043-13466 13
Benzo(k)fluoranthene mg/kg dry1.43 0.38 1.942 BRL 2047-13273 14
Benzoic Acid mg/kg dry0.992 0.38 1.942 BRL 2010-8351 15
Benzyl alcohol mg/kg dry1.31 0.38 1.942 BRL 2029-12267 12
bis(2-Chloroethoxy)methane mg/kg dry1.14 0.38 1.942 BRL 2036-12159 11
Bis(2-Chloroethyl)ether mg/kg dry1.16 0.38 1.942 BRL 2031-12060 14
Bis(2-chloroisopropyl)ether mg/kg dry1.28 0.38 1.942 BRL 2033-13166 14
Bis(2-Ethylhexyl)phthalate mg/kg dry1.62 0.38 1.942 BRL 2051-13383 12
Butyl benzyl phthalate mg/kg dry1.63 0.38 1.942 BRL 2048-13284 12
Chrysene mg/kg dry1.51 0.38 1.942 BRL 2050-12478 13
Dibenzo(a,h)anthracene mg/kg dry1.40 0.38 1.942 BRL 2045-13472 12
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 188 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0273 - 3546
Matrix Spike Dup (P7D0273-MSD1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-04
Dibenzofuran mg/kg dry1.39 0.38 1.942 BRL 2044-12071 14
Diethyl phthalate mg/kg dry1.39 0.38 1.942 BRL 2050-12471 14
Dimethyl phthalate mg/kg dry1.35 0.38 1.942 BRL 2048-12469 13
Di-n-butyl phthalate mg/kg dry1.48 0.38 1.942 BRL 2051-12876 12
Di-n-octyl phthalate mg/kg dry1.68 0.38 1.942 BRL 2045-14087 14
Fluoranthene mg/kg dry1.47 0.38 1.942 BRL 2050-12776 13
Fluorene mg/kg dry1.43 0.38 1.942 BRL 2043-12574 14
Hexachlorobenzene mg/kg dry1.37 0.38 1.942 BRL 2045-12271 13
Hexachlorobutadiene mg/kg dry1.10 0.38 1.942 BRL 2032-12357 12
Hexachlorocyclopentadiene mg/kg dry0.290 0.38 1.942 BRL 20 M, J32-11715 10
Hexachloroethane mg/kg dry1.05 0.38 1.942 BRL 2028-11754 12
Indeno(1,2,3-cd)pyrene mg/kg dry1.34 0.38 1.942 BRL 2045-13369 10
Isophorone mg/kg dry1.18 0.38 1.942 BRL 2030-12261 11
Naphthalene mg/kg dry1.17 0.38 1.942 BRL 2035-12360 11
Nitrobenzene mg/kg dry1.10 0.38 1.942 BRL 2034-12257 12
N-Nitroso-di-n-propylamine mg/kg dry1.17 0.38 1.942 BRL 2036-12060 11
N-Nitrosodiphenylamine mg/kg dry1.75 0.38 1.942 BRL 2038-12790 16
Pentachlorophenol mg/kg dry1.65 0.38 1.942 BRL 2025-13385 18
Phenanthrene mg/kg dry1.48 0.38 1.942 BRL 2050-12176 12
Phenol mg/kg dry1.29 0.38 1.942 BRL 2034-12166 13
Pyrene mg/kg dry1.55 0.38 1.942 BRL 2047-12780 12
mg/kg dry 3.884 39-132Surrogate: 2,4,6-Tribromophenol 672.62
mg/kg dry 1.942 44-115Surrogate: 2-Fluorobiphenyl 651.26
mg/kg dry 3.884 35-115Surrogate: 2-Fluorophenol 612.38
mg/kg dry 1.942 37-122Surrogate: Nitrobenzene-d5 551.06
mg/kg dry 3.884 34-121Surrogate: Phenol-d5 632.46
mg/kg dry 1.942 54-127Surrogate: Terphenyl-d14 831.61
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 189 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0274 - 3546
Blank (P7D0274-BLK1)Prepared: 04/18/17 Analyzed: 04/19/17
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 190 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0274 - 3546
Blank (P7D0274-BLK1)Prepared: 04/18/17 Analyzed: 04/19/17
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 802.66
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 771.29
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 792.62
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 721.20
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 772.55
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 961.59
LCS (P7D0274-BS1)Prepared: 04/18/17 Analyzed: 04/19/17
1,2,4-Trichlorobenzene mg/kg wet0.956 0.33 1.667 34-11857
1,2-Dichlorobenzene mg/kg wet1.02 0.33 1.667 33-11761
1,3-Dichlorobenzene mg/kg wet1.01 0.33 1.667 30-11561
1,4-Dichlorobenzene mg/kg wet0.997 0.33 1.667 31-11560
1-Methylnaphthalene mg/kg wet1.09 0.33 1.667 40-11966
2,4,6-Trichlorophenol mg/kg wet1.28 0.33 1.667 39-12677
2,4-Dichlorophenol mg/kg wet1.07 0.33 1.667 40-12264
2,4-Dimethylphenol mg/kg wet1.26 0.33 1.667 30-12776
2,4-Dinitrophenol mg/kg wet1.65 0.33 1.667 27-12999
2,4-Dinitrotoluene mg/kg wet1.41 0.33 1.667 48-12684
2,6-Dinitrotoluene mg/kg wet1.42 0.33 1.667 46-12485
2-Chloronaphthalene mg/kg wet1.22 0.33 1.667 41-11473
2-Chlorophenol mg/kg wet1.19 0.33 1.667 34-12172
2-Methylnaphthalene mg/kg wet1.08 0.33 1.667 38-12265
2-Methylphenol mg/kg wet1.25 0.33 1.667 32-12275
2-Nitrophenol mg/kg wet1.02 0.33 1.667 36-12361
3,3'-Dichlorobenzidine mg/kg wet1.40 0.33 1.667 22-12184
3/4-Methylphenol mg/kg wet1.15 0.33 1.667 34-11969
4,6-Dinitro-2-methylphenol mg/kg wet1.52 0.33 1.667 29-13291
4-Bromophenyl phenyl ether mg/kg wet1.30 0.33 1.667 46-12478
4-Chloro-3-methylphenol mg/kg wet1.23 0.33 1.667 45-12274
4-Chloroaniline mg/kg wet1.08 0.33 1.667 17-10665
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 191 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0274 - 3546
LCS (P7D0274-BS1)Prepared: 04/18/17 Analyzed: 04/19/17
4-Chlorophenyl phenyl ether mg/kg wet1.28 0.33 1.667 45-12177
4-Nitrophenol mg/kg wet1.36 0.33 1.667 30-13281
Acenaphthene mg/kg wet1.36 0.33 1.667 40-12382
Acenaphthylene mg/kg wet1.32 0.33 1.667 32-13279
Anthracene mg/kg wet1.45 0.33 1.667 47-12387
Azobenzene mg/kg wet1.43 0.33 1.667 39-12586
Benzo(a)anthracene mg/kg wet1.46 0.33 1.667 49-12688
Benzo(a)pyrene mg/kg wet1.41 0.33 1.667 45-12984
Benzo(b)fluoranthene mg/kg wet1.39 0.33 1.667 45-13283
Benzo(g,h,i)perylene mg/kg wet1.28 0.33 1.667 43-13477
Benzo(k)fluoranthene mg/kg wet1.43 0.33 1.667 47-13286
Benzoic Acid mg/kg wet0.813 0.33 1.667 10-8349
Benzyl alcohol mg/kg wet1.18 0.33 1.667 29-12271
bis(2-Chloroethoxy)methane mg/kg wet1.05 0.33 1.667 36-12163
Bis(2-Chloroethyl)ether mg/kg wet0.966 0.33 1.667 31-12058
Bis(2-chloroisopropyl)ether mg/kg wet1.10 0.33 1.667 33-13166
Bis(2-Ethylhexyl)phthalate mg/kg wet1.49 0.33 1.667 51-13389
Butyl benzyl phthalate mg/kg wet1.51 0.33 1.667 48-13290
Chrysene mg/kg wet1.46 0.33 1.667 50-12487
Dibenzo(a,h)anthracene mg/kg wet1.39 0.33 1.667 45-13484
Dibenzofuran mg/kg wet1.33 0.33 1.667 44-12080
Diethyl phthalate mg/kg wet1.37 0.33 1.667 50-12482
Dimethyl phthalate mg/kg wet1.34 0.33 1.667 48-12481
Di-n-butyl phthalate mg/kg wet1.42 0.33 1.667 51-12885
Di-n-octyl phthalate mg/kg wet1.50 0.33 1.667 45-14090
Fluoranthene mg/kg wet1.44 0.33 1.667 50-12787
Fluorene mg/kg wet1.38 0.33 1.667 43-12583
Hexachlorobenzene mg/kg wet1.35 0.33 1.667 45-12281
Hexachlorobutadiene mg/kg wet0.985 0.33 1.667 32-12359
Hexachlorocyclopentadiene mg/kg wet0.347 0.33 1.667 L32-11721
Hexachloroethane mg/kg wet0.992 0.33 1.667 28-11759
Indeno(1,2,3-cd)pyrene mg/kg wet1.32 0.33 1.667 45-13379
Isophorone mg/kg wet1.11 0.33 1.667 30-12267
Naphthalene mg/kg wet1.05 0.33 1.667 35-12363
Nitrobenzene mg/kg wet1.00 0.33 1.667 34-12260
N-Nitroso-di-n-propylamine mg/kg wet1.16 0.33 1.667 36-12070
N-Nitrosodiphenylamine mg/kg wet1.73 0.33 1.667 38-127104
Pentachlorophenol mg/kg wet1.67 0.33 1.667 25-133100
Phenanthrene mg/kg wet1.44 0.33 1.667 50-12187
Phenol mg/kg wet1.24 0.33 1.667 34-12174
Pyrene mg/kg wet1.45 0.33 1.667 47-12787
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 812.69
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 701.16
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 692.30
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 570.943
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 682.28
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 192 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0274 - 3546
LCS (P7D0274-BS1)Prepared: 04/18/17 Analyzed: 04/19/17
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 921.53
LCS Dup (P7D0274-BSD1)Prepared: 04/18/17 Analyzed: 04/19/17
1,2,4-Trichlorobenzene mg/kg wet1.05 0.33 1.667 2034-11863 10
1,2-Dichlorobenzene mg/kg wet1.14 0.33 1.667 2033-11768 10
1,3-Dichlorobenzene mg/kg wet1.12 0.33 1.667 2030-11567 10
1,4-Dichlorobenzene mg/kg wet1.12 0.33 1.667 2031-11567 11
1-Methylnaphthalene mg/kg wet1.18 0.33 1.667 2040-11971 8
2,4,6-Trichlorophenol mg/kg wet1.38 0.33 1.667 2039-12683 7
2,4-Dichlorophenol mg/kg wet1.18 0.33 1.667 2040-12271 9
2,4-Dimethylphenol mg/kg wet1.32 0.33 1.667 2030-12779 5
2,4-Dinitrophenol mg/kg wet1.66 0.33 1.667 2027-12999 0.3
2,4-Dinitrotoluene mg/kg wet1.46 0.33 1.667 2048-12688 4
2,6-Dinitrotoluene mg/kg wet1.48 0.33 1.667 2046-12489 4
2-Chloronaphthalene mg/kg wet1.32 0.33 1.667 2041-11479 8
2-Chlorophenol mg/kg wet1.33 0.33 1.667 2034-12180 11
2-Methylnaphthalene mg/kg wet1.15 0.33 1.667 2038-12269 6
2-Methylphenol mg/kg wet1.37 0.33 1.667 2032-12282 9
2-Nitrophenol mg/kg wet1.14 0.33 1.667 2036-12369 11
3,3'-Dichlorobenzidine mg/kg wet1.30 0.33 1.667 2022-12178 7
3/4-Methylphenol mg/kg wet1.27 0.33 1.667 2034-11976 10
4,6-Dinitro-2-methylphenol mg/kg wet1.47 0.33 1.667 2029-13288 3
4-Bromophenyl phenyl ether mg/kg wet1.33 0.33 1.667 2046-12480 2
4-Chloro-3-methylphenol mg/kg wet1.28 0.33 1.667 2045-12277 4
4-Chloroaniline mg/kg wet1.12 0.33 1.667 2017-10667 3
4-Chlorophenyl phenyl ether mg/kg wet1.33 0.33 1.667 2045-12180 4
4-Nitrophenol mg/kg wet1.42 0.33 1.667 2030-13285 5
Acenaphthene mg/kg wet1.42 0.33 1.667 2040-12385 4
Acenaphthylene mg/kg wet1.41 0.33 1.667 2032-13284 6
Anthracene mg/kg wet1.47 0.33 1.667 2047-12388 1
Azobenzene mg/kg wet1.43 0.33 1.667 2039-12586 0.3
Benzo(a)anthracene mg/kg wet1.47 0.33 1.667 2049-12688 0.7
Benzo(a)pyrene mg/kg wet1.43 0.33 1.667 2045-12986 2
Benzo(b)fluoranthene mg/kg wet1.44 0.33 1.667 2045-13286 4
Benzo(g,h,i)perylene mg/kg wet1.31 0.33 1.667 2043-13478 2
Benzo(k)fluoranthene mg/kg wet1.45 0.33 1.667 2047-13287 2
Benzoic Acid mg/kg wet0.897 0.33 1.667 2010-8354 10
Benzyl alcohol mg/kg wet1.29 0.33 1.667 2029-12277 9
bis(2-Chloroethoxy)methane mg/kg wet1.14 0.33 1.667 2036-12169 9
Bis(2-Chloroethyl)ether mg/kg wet1.07 0.33 1.667 2031-12064 10
Bis(2-chloroisopropyl)ether mg/kg wet1.21 0.33 1.667 2033-13173 10
Bis(2-Ethylhexyl)phthalate mg/kg wet1.52 0.33 1.667 2051-13391 2
Butyl benzyl phthalate mg/kg wet1.52 0.33 1.667 2048-13291 0.6
Chrysene mg/kg wet1.49 0.33 1.667 2050-12489 2
Dibenzo(a,h)anthracene mg/kg wet1.43 0.33 1.667 2045-13486 3
Dibenzofuran mg/kg wet1.40 0.33 1.667 2044-12084 5
Diethyl phthalate mg/kg wet1.42 0.33 1.667 2050-12485 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 193 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0274 - 3546
LCS Dup (P7D0274-BSD1)Prepared: 04/18/17 Analyzed: 04/19/17
Dimethyl phthalate mg/kg wet1.39 0.33 1.667 2048-12483 3
Di-n-butyl phthalate mg/kg wet1.41 0.33 1.667 2051-12885 0.7
Di-n-octyl phthalate mg/kg wet1.52 0.33 1.667 2045-14091 2
Fluoranthene mg/kg wet1.46 0.33 1.667 2050-12788 1
Fluorene mg/kg wet1.44 0.33 1.667 2043-12586 4
Hexachlorobenzene mg/kg wet1.36 0.33 1.667 2045-12282 0.9
Hexachlorobutadiene mg/kg wet1.11 0.33 1.667 2032-12366 12
Hexachlorocyclopentadiene mg/kg wet0.407 0.33 1.667 20 L32-11724 16
Hexachloroethane mg/kg wet1.08 0.33 1.667 2028-11765 9
Indeno(1,2,3-cd)pyrene mg/kg wet1.36 0.33 1.667 2045-13382 3
Isophorone mg/kg wet1.19 0.33 1.667 2030-12271 7
Naphthalene mg/kg wet1.17 0.33 1.667 2035-12370 10
Nitrobenzene mg/kg wet1.09 0.33 1.667 2034-12266 9
N-Nitroso-di-n-propylamine mg/kg wet1.24 0.33 1.667 2036-12075 7
N-Nitrosodiphenylamine mg/kg wet1.77 0.33 1.667 2038-127106 2
Pentachlorophenol mg/kg wet1.72 0.33 1.667 2025-133103 3
Phenanthrene mg/kg wet1.49 0.33 1.667 2050-12189 3
Phenol mg/kg wet1.38 0.33 1.667 2034-12183 11
Pyrene mg/kg wet1.49 0.33 1.667 2047-12789 2
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 832.76
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 761.26
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 762.53
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 621.03
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 752.49
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 931.55
Matrix Spike (P7D0274-MS1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-23
1,2,4-Trichlorobenzene mg/kg dry1.33 0.41 2.085 BRL 34-11864
1,2-Dichlorobenzene mg/kg dry1.42 0.41 2.085 BRL 33-11768
1,3-Dichlorobenzene mg/kg dry1.39 0.41 2.085 BRL 30-11566
1,4-Dichlorobenzene mg/kg dry1.39 0.41 2.085 BRL 31-11566
1-Methylnaphthalene mg/kg dry1.49 0.41 2.085 BRL 40-11972
2,4,6-Trichlorophenol mg/kg dry1.57 0.41 2.085 BRL 39-12675
2,4-Dichlorophenol mg/kg dry1.47 0.41 2.085 BRL 40-12270
2,4-Dimethylphenol mg/kg dry1.66 0.41 2.085 BRL 30-12780
2,4-Dinitrophenol mg/kg dry1.21 0.41 2.085 BRL 27-12958
2,4-Dinitrotoluene mg/kg dry1.69 0.41 2.085 BRL 48-12681
2,6-Dinitrotoluene mg/kg dry1.74 0.41 2.085 BRL 46-12484
2-Chloronaphthalene mg/kg dry1.65 0.41 2.085 BRL 41-11479
2-Chlorophenol mg/kg dry1.67 0.41 2.085 BRL 34-12180
2-Methylnaphthalene mg/kg dry1.47 0.41 2.085 BRL 38-12271
2-Methylphenol mg/kg dry1.70 0.41 2.085 BRL 32-12282
2-Nitrophenol mg/kg dry1.32 0.41 2.085 BRL 36-12363
3,3'-Dichlorobenzidine mg/kg dry1.14 0.41 2.085 BRL 22-12155
3/4-Methylphenol mg/kg dry1.55 0.41 2.085 BRL 34-11974
4,6-Dinitro-2-methylphenol mg/kg dry1.23 0.41 2.085 BRL 29-13259
4-Bromophenyl phenyl ether mg/kg dry1.63 0.41 2.085 BRL 46-12478
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 194 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0274 - 3546
Matrix Spike (P7D0274-MS1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-23
4-Chloro-3-methylphenol mg/kg dry1.60 0.41 2.085 BRL 45-12277
4-Chloroaniline mg/kg dry1.20 0.41 2.085 BRL 17-10657
4-Chlorophenyl phenyl ether mg/kg dry1.61 0.41 2.085 BRL 45-12177
4-Nitrophenol mg/kg dry1.72 0.41 2.085 BRL 30-13283
Acenaphthene mg/kg dry1.71 0.41 2.085 BRL 40-12382
Acenaphthylene mg/kg dry1.74 0.41 2.085 BRL 32-13283
Anthracene mg/kg dry1.81 0.41 2.085 BRL 47-12387
Azobenzene mg/kg dry1.81 0.41 2.085 BRL 39-12587
Benzo(a)anthracene mg/kg dry1.77 0.41 2.085 BRL 49-12685
Benzo(a)pyrene mg/kg dry1.73 0.41 2.085 BRL 45-12983
Benzo(b)fluoranthene mg/kg dry1.85 0.41 2.085 BRL 45-13289
Benzo(g,h,i)perylene mg/kg dry1.57 0.41 2.085 BRL 43-13475
Benzo(k)fluoranthene mg/kg dry1.69 0.41 2.085 BRL 47-13281
Benzoic Acid mg/kg dry0.468 0.41 2.085 BRL 10-8322
Benzyl alcohol mg/kg dry1.66 0.41 2.085 BRL 29-12280
bis(2-Chloroethoxy)methane mg/kg dry1.44 0.41 2.085 BRL 36-12169
Bis(2-Chloroethyl)ether mg/kg dry1.50 0.41 2.085 BRL 31-12072
Bis(2-chloroisopropyl)ether mg/kg dry1.59 0.41 2.085 BRL 33-13176
Bis(2-Ethylhexyl)phthalate mg/kg dry1.95 0.41 2.085 BRL 51-13394
Butyl benzyl phthalate mg/kg dry1.97 0.41 2.085 BRL 48-13294
Chrysene mg/kg dry1.80 0.41 2.085 BRL 50-12486
Dibenzo(a,h)anthracene mg/kg dry1.64 0.41 2.085 BRL 45-13478
Dibenzofuran mg/kg dry1.72 0.41 2.085 BRL 44-12082
Diethyl phthalate mg/kg dry1.70 0.41 2.085 BRL 50-12482
Dimethyl phthalate mg/kg dry1.66 0.41 2.085 BRL 48-12480
Di-n-butyl phthalate mg/kg dry1.75 0.41 2.085 BRL 51-12884
Di-n-octyl phthalate mg/kg dry2.07 0.41 2.085 BRL 45-14099
Fluoranthene mg/kg dry1.76 0.41 2.085 BRL 50-12785
Fluorene mg/kg dry1.74 0.41 2.085 BRL 43-12583
Hexachlorobenzene mg/kg dry1.66 0.41 2.085 BRL 45-12280
Hexachlorobutadiene mg/kg dry1.39 0.41 2.085 BRL 32-12366
Hexachlorocyclopentadiene mg/kg dryBRL0.41 2.085 BRL M32-117
Hexachloroethane mg/kg dry0.890 0.41 2.085 BRL 28-11743
Indeno(1,2,3-cd)pyrene mg/kg dry1.65 0.41 2.085 BRL 45-13379
Isophorone mg/kg dry1.48 0.41 2.085 BRL 30-12271
Naphthalene mg/kg dry1.49 0.41 2.085 BRL 35-12371
Nitrobenzene mg/kg dry1.42 0.41 2.085 BRL 34-12268
N-Nitroso-di-n-propylamine mg/kg dry1.53 0.41 2.085 BRL 36-12073
N-Nitrosodiphenylamine mg/kg dry2.20 0.41 2.085 BRL 38-127106
Pentachlorophenol mg/kg dry1.59 0.41 2.085 BRL 25-13376
Phenanthrene mg/kg dry1.82 0.41 2.085 BRL 50-12187
Phenol mg/kg dry1.67 0.41 2.085 BRL 34-12180
Pyrene mg/kg dry1.90 0.41 2.085 BRL 47-12791
mg/kg dry 4.169 39-132Surrogate: 2,4,6-Tribromophenol 642.66
mg/kg dry 2.085 44-115Surrogate: 2-Fluorobiphenyl 771.60
mg/kg dry 4.169 35-115Surrogate: 2-Fluorophenol 753.12
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 195 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0274 - 3546
Matrix Spike (P7D0274-MS1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-23
mg/kg dry 2.085 37-122Surrogate: Nitrobenzene-d5 651.35
mg/kg dry 4.169 34-121Surrogate: Phenol-d5 763.18
mg/kg dry 2.085 54-127Surrogate: Terphenyl-d14 931.93
Matrix Spike Dup (P7D0274-MSD1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-23
1,2,4-Trichlorobenzene mg/kg dry1.35 0.41 2.084 BRL 2034-11865 1
1,2-Dichlorobenzene mg/kg dry1.42 0.41 2.084 BRL 2033-11768 0.1
1,3-Dichlorobenzene mg/kg dry1.38 0.41 2.084 BRL 2030-11566 0.3
1,4-Dichlorobenzene mg/kg dry1.38 0.41 2.084 BRL 2031-11566 0.4
1-Methylnaphthalene mg/kg dry1.49 0.41 2.084 BRL 2040-11972 0.03
2,4,6-Trichlorophenol mg/kg dry1.63 0.41 2.084 BRL 2039-12678 4
2,4-Dichlorophenol mg/kg dry1.42 0.41 2.084 BRL 2040-12268 3
2,4-Dimethylphenol mg/kg dry1.71 0.41 2.084 BRL 2030-12782 3
2,4-Dinitrophenol mg/kg dry1.21 0.41 2.084 BRL 2027-12958 0.2
2,4-Dinitrotoluene mg/kg dry1.71 0.41 2.084 BRL 2048-12682 1
2,6-Dinitrotoluene mg/kg dry1.74 0.41 2.084 BRL 2046-12483 0.2
2-Chloronaphthalene mg/kg dry1.66 0.41 2.084 BRL 2041-11479 0.3
2-Chlorophenol mg/kg dry1.64 0.41 2.084 BRL 2034-12179 2
2-Methylnaphthalene mg/kg dry1.47 0.41 2.084 BRL 2038-12270 0.6
2-Methylphenol mg/kg dry1.73 0.41 2.084 BRL 2032-12283 1
2-Nitrophenol mg/kg dry1.33 0.41 2.084 BRL 2036-12364 1
3,3'-Dichlorobenzidine mg/kg dry1.32 0.41 2.084 BRL 2022-12163 15
3/4-Methylphenol mg/kg dry1.56 0.41 2.084 BRL 2034-11975 0.4
4,6-Dinitro-2-methylphenol mg/kg dry1.22 0.41 2.084 BRL 2029-13259 0.8
4-Bromophenyl phenyl ether mg/kg dry1.60 0.41 2.084 BRL 2046-12477 2
4-Chloro-3-methylphenol mg/kg dry1.59 0.41 2.084 BRL 2045-12276 0.8
4-Chloroaniline mg/kg dry1.27 0.41 2.084 BRL 2017-10661 6
4-Chlorophenyl phenyl ether mg/kg dry1.60 0.41 2.084 BRL 2045-12177 0.7
4-Nitrophenol mg/kg dry1.71 0.41 2.084 BRL 2030-13282 1
Acenaphthene mg/kg dry1.72 0.41 2.084 BRL 2040-12382 0.1
Acenaphthylene mg/kg dry1.75 0.41 2.084 BRL 2032-13284 0.7
Anthracene mg/kg dry1.78 0.41 2.084 BRL 2047-12386 2
Azobenzene mg/kg dry1.79 0.41 2.084 BRL 2039-12586 0.8
Benzo(a)anthracene mg/kg dry1.73 0.41 2.084 BRL 2049-12683 2
Benzo(a)pyrene mg/kg dry1.71 0.41 2.084 BRL 2045-12982 2
Benzo(b)fluoranthene mg/kg dry1.80 0.41 2.084 BRL 2045-13286 3
Benzo(g,h,i)perylene mg/kg dry1.51 0.41 2.084 BRL 2043-13473 4
Benzo(k)fluoranthene mg/kg dry1.65 0.41 2.084 BRL 2047-13279 2
Benzoic Acid mg/kg dry0.357 0.41 2.084 BRL 20 D, J10-8317 27
Benzyl alcohol mg/kg dry1.68 0.41 2.084 BRL 2029-12281 1
bis(2-Chloroethoxy)methane mg/kg dry1.43 0.41 2.084 BRL 2036-12168 0.8
Bis(2-Chloroethyl)ether mg/kg dry1.51 0.41 2.084 BRL 2031-12073 0.8
Bis(2-chloroisopropyl)ether mg/kg dry1.65 0.41 2.084 BRL 2033-13179 3
Bis(2-Ethylhexyl)phthalate mg/kg dry1.89 0.41 2.084 BRL 2051-13391 3
Butyl benzyl phthalate mg/kg dry1.92 0.41 2.084 BRL 2048-13292 2
Chrysene mg/kg dry1.74 0.41 2.084 BRL 2050-12483 4
Dibenzo(a,h)anthracene mg/kg dry1.60 0.41 2.084 BRL 2045-13477 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 196 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7D0274 - 3546
Matrix Spike Dup (P7D0274-MSD1)Prepared: 04/18/17 Analyzed: 04/20/17 Source: 7040298-23
Dibenzofuran mg/kg dry1.71 0.41 2.084 BRL 2044-12082 0.3
Diethyl phthalate mg/kg dry1.68 0.41 2.084 BRL 2050-12480 2
Dimethyl phthalate mg/kg dry1.65 0.41 2.084 BRL 2048-12479 0.9
Di-n-butyl phthalate mg/kg dry1.73 0.41 2.084 BRL 2051-12883 1
Di-n-octyl phthalate mg/kg dry2.04 0.41 2.084 BRL 2045-14098 2
Fluoranthene mg/kg dry1.75 0.41 2.084 BRL 2050-12784 0.8
Fluorene mg/kg dry1.76 0.41 2.084 BRL 2043-12584 1
Hexachlorobenzene mg/kg dry1.61 0.41 2.084 BRL 2045-12277 3
Hexachlorobutadiene mg/kg dry1.40 0.41 2.084 BRL 2032-12367 1
Hexachlorocyclopentadiene mg/kg dryBRL0.41 2.084 BRL 20 M32-117
Hexachloroethane mg/kg dry1.10 0.41 2.084 BRL 20 D28-11753 21
Indeno(1,2,3-cd)pyrene mg/kg dry1.61 0.41 2.084 BRL 2045-13377 2
Isophorone mg/kg dry1.48 0.41 2.084 BRL 2030-12271 0.2
Naphthalene mg/kg dry1.49 0.41 2.084 BRL 2035-12372 0.5
Nitrobenzene mg/kg dry1.42 0.41 2.084 BRL 2034-12268 0.5
N-Nitroso-di-n-propylamine mg/kg dry1.57 0.41 2.084 BRL 2036-12075 3
N-Nitrosodiphenylamine mg/kg dry2.17 0.41 2.084 BRL 2038-127104 1
Pentachlorophenol mg/kg dry1.58 0.41 2.084 BRL 2025-13376 0.2
Phenanthrene mg/kg dry1.77 0.41 2.084 BRL 2050-12185 3
Phenol mg/kg dry1.72 0.41 2.084 BRL 2034-12183 3
Pyrene mg/kg dry1.85 0.41 2.084 BRL 2047-12789 3
mg/kg dry 4.168 39-132Surrogate: 2,4,6-Tribromophenol 692.88
mg/kg dry 2.084 44-115Surrogate: 2-Fluorobiphenyl 761.59
mg/kg dry 4.168 35-115Surrogate: 2-Fluorophenol 753.13
mg/kg dry 2.084 37-122Surrogate: Nitrobenzene-d5 651.36
mg/kg dry 4.168 34-121Surrogate: Phenol-d5 773.21
mg/kg dry 2.084 54-127Surrogate: Terphenyl-d14 901.88
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 197 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0257 - 3050B
Blank (P7D0257-BLK1)Prepared: 04/18/17 Analyzed: 04/24/17
Lead mg/kg wetBRL0.25
LCS (P7D0257-BS1)Prepared: 04/18/17 Analyzed: 04/24/17
Lead mg/kg wet27.3 0.25 25.00 80-120109
Matrix Spike (P7D0257-MS1)Prepared: 04/18/17 Analyzed: 04/24/17 Source: 7040298-01
Lead mg/kg dry49.1 0.30 30.35 14.8 75-125113
Matrix Spike Dup (P7D0257-MSD1)Prepared: 04/18/17 Analyzed: 04/24/17 Source: 7040298-01
Lead mg/kg dry48.5 0.30 30.35 14.8 2075-125111 1
Batch P7D0287 - 3050B
Blank (P7D0287-BLK1)Prepared: 04/19/17 Analyzed: 04/25/17
Lead mg/kg wetBRL0.25
LCS (P7D0287-BS1)Prepared: 04/19/17 Analyzed: 04/25/17
Lead mg/kg wet27.4 0.25 25.00 80-120110
Batch P7D0321 - 3005A
Blank (P7D0321-BLK1)Prepared: 04/20/17 Analyzed: 04/21/17
Lead ug/L0.103 1.0 J
LCS (P7D0321-BS1)Prepared: 04/20/17 Analyzed: 04/21/17
Lead ug/L1091.0 100.0 80-120109
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 198 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0321 - 3005A
Matrix Spike (P7D0321-MS1)Prepared: 04/20/17 Analyzed: 04/21/17 Source: 7040298-28
Lead ug/L1121.0 100.0 1.28 75-125110
Matrix Spike Dup (P7D0321-MSD1)Prepared: 04/20/17 Analyzed: 04/21/17 Source: 7040298-28
Lead ug/L1051.0 100.0 1.28 2075-125104 6
Post Spike (P7D0321-PS1)Prepared: 04/20/17 Analyzed: 04/21/17 Source: 7040298-28
Lead ug/L106 100.0 1.28 80-120104
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 199 of 207
4/26/17
Level II QC Report
44 Buck Shoals Rd. Suite C-3
Project: Former Simpson Gas & Oil
Property
S&ME, Inc. - Arden, NC
Arden, NC 28704
Attn: Bradley Keyse
Prism Work Order: 7040298
Time Submitted: 4/17/2017 8:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7D0359 - Solids, Dry Weight
Duplicate (P7D0359-DUP2)Prepared & Analyzed: 04/20/17 Source: 7040298-01
% Solids % by Weight83.6 0.100 82.4 201
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 200 of 207
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P7D03597040298-01 04/20/17 14:4030 30g g
P7D03597040298-02 04/20/17 14:4030 30g g
P7D03597040298-03 04/20/17 14:4030 30g g
P7D03597040298-04 04/20/17 14:4030 30g g
P7D03597040298-05 04/20/17 14:4030 30g g
P7D03597040298-06 04/20/17 14:4030 30g g
P7D03597040298-07 04/20/17 14:4030 30g g
P7D03597040298-08 04/20/17 14:4030 30g g
P7D03597040298-09 04/20/17 14:4030 30g g
P7D03597040298-10 04/20/17 14:4030 30g g
P7D03597040298-11 04/20/17 14:4030 30g g
P7D03597040298-12 04/20/17 14:4030 30g g
P7D03597040298-13 04/20/17 14:4030 30g g
P7D03597040298-14 04/20/17 14:4030 30g g
P7D03597040298-15 04/20/17 14:4030 30g g
P7D03597040298-16 04/20/17 14:4030 30g g
P7D03597040298-17 04/20/17 14:4030 30g g
P7D03597040298-18 04/20/17 14:4030 30g g
P7D03597040298-19 04/20/17 14:4030 30g g
P7D03597040298-20 04/20/17 14:4030 30g g
P7D03597040298-21 04/20/17 14:4030 30g g
P7D03597040298-22 04/20/17 14:4030 30g g
P7D03597040298-23 04/20/17 14:4030 30g g
P7D03597040298-24 04/20/17 14:4030 30g g
P7D03597040298-25 04/20/17 14:4030 30g g
P7D03597040298-26 04/20/17 14:4030 30g g
P7D03597040298-27 04/20/17 14:4030 30g g
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P7D02517040298-28 04/18/17 8:079601mL mL
P7D02517040298-28 04/18/17 8:079601mL mL
P7D02517040298-29 04/18/17 8:079601mL mL
P7D02517040298-29 04/18/17 8:079601mL mL
P7D02517040298-30 04/18/17 8:079601mL mL
P7D02517040298-31 04/18/17 8:079601mL mL
P7D02517040298-32 04/18/17 8:071000 1mL mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7D02737040298-01 04/18/17 10:3030.63 1g mL
P7D02737040298-02 04/18/17 10:3030.03 1g mL
P7D02737040298-03 04/18/17 10:3030 1g mL
P7D02737040298-04 04/18/17 10:3030.68 1g mL
P7D02737040298-05 04/18/17 10:3030.13 1g mL
P7D02737040298-06 04/18/17 10:3030.08 1g mL
P7D02737040298-07 04/18/17 10:3030 1g mL
P7D02737040298-08 04/18/17 10:3030.55 1g mL
P7D02737040298-09 04/18/17 10:3030.52 1g mL
P7D02737040298-10 04/18/17 10:3030.51 1g mL
P7D02737040298-11 04/18/17 10:3030.49 1g mL
P7D02737040298-12 04/18/17 10:3030.4 1g mL
P7D02747040298-13 04/18/17 12:4530.86 1g mL
P7D02747040298-14 04/18/17 12:4530.97 1g mL
P7D02747040298-15 04/18/17 12:4530.11 1g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 201 of 207
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P7D02747040298-16 04/18/17 12:4530.01 1g mL
P7D02747040298-17 04/18/17 12:4530.63 1g mL
P7D02747040298-18 04/18/17 12:4530.67 1g mL
P7D02747040298-19 04/18/17 12:4530.35 1g mL
P7D02747040298-20 04/18/17 12:4530.74 1g mL
P7D02747040298-21 04/18/17 12:4530.22 1g mL
P7D02747040298-22 04/18/17 12:4530.58 1g mL
P7D02747040298-22 04/18/17 12:4530.58 1g mL
P7D02747040298-23 04/18/17 12:4530.81 1g mL
P7D02747040298-24 04/18/17 12:4530.11 1g mL
P7D02747040298-25 04/18/17 12:4530.89 1g mL
P7D02747040298-26 04/18/17 12:4530.59 1g mL
P7D02747040298-26 04/18/17 12:4530.59 1g mL
P7D02747040298-27 04/18/17 12:4530.29 1g mL
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7D03217040298-28 04/20/17 8:0550 50mL mL
P7D03217040298-29 04/20/17 8:0550 50mL mL
P7D03217040298-30 04/20/17 8:0550 50mL mL
P7D03217040298-31 04/20/17 8:0550 50mL mL
P7D03217040298-32 04/20/17 8:0550 50mL mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P7D02577040298-01 04/18/17 9:102 50g mL
P7D02577040298-02 04/18/17 9:102 50g mL
P7D02577040298-03 04/18/17 9:102 50g mL
P7D02577040298-04 04/18/17 9:102 50g mL
P7D02577040298-05 04/18/17 9:102 50g mL
P7D02577040298-06 04/18/17 9:102 50g mL
P7D02577040298-07 04/18/17 9:102 50g mL
P7D02577040298-08 04/18/17 9:102 50g mL
P7D02577040298-09 04/18/17 9:102 50g mL
P7D02577040298-10 04/18/17 9:102 50g mL
P7D02577040298-11 04/18/17 9:102 50g mL
P7D02577040298-12 04/18/17 9:102 50g mL
P7D02577040298-13 04/18/17 9:102 50g mL
P7D02577040298-14 04/18/17 9:102 50g mL
P7D02577040298-15 04/18/17 9:102 50g mL
P7D02577040298-16 04/18/17 9:102 50g mL
P7D02577040298-17 04/18/17 9:102 50g mL
P7D02577040298-18 04/18/17 9:102 50g mL
P7D02577040298-19 04/18/17 9:102 50g mL
P7D02877040298-20 04/19/17 8:051.96 50g mL
P7D02877040298-21 04/19/17 8:051.97 50g mL
P7D02877040298-22 04/19/17 8:052.02 50g mL
P7D02877040298-23 04/19/17 8:051.97 50g mL
P7D02877040298-24 04/19/17 8:052 50g mL
P7D02877040298-25 04/19/17 8:051.98 50g mL
P7D02877040298-26 04/19/17 8:052.05 50g mL
P7D02877040298-27 04/19/17 8:051.98 50g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 202 of 207
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7D03497040298-28 04/21/17 12:1610 10mL mL
P7D03497040298-28 04/21/17 12:1610 10mL mL
P7D03497040298-29 04/21/17 12:1610 10mL mL
P7D03497040298-29 04/21/17 12:1610 10mL mL
P7D03497040298-30 04/21/17 12:1610 10mL mL
P7D03497040298-31 04/21/17 12:1610 10mL mL
P7D03497040298-32 04/21/17 12:1610 10mL mL
P7D03497040298-33 04/21/17 12:1610 10mL mL
P7D03497040298-34 04/21/17 12:1610 10mL mL
P7D03497040298-35 04/21/17 12:1610 10mL mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P7D03377040298-01 04/20/17 10:434.74 5g mL
P7D03377040298-02 04/20/17 10:435.05 5g mL
P7D03377040298-03 04/20/17 10:435.23 5g mL
P7D03377040298-04 04/20/17 10:435.05 5g mL
P7D03377040298-05 04/20/17 10:435.21 5g mL
P7D03377040298-06 04/20/17 10:435.39 5g mL
P7D03377040298-07 04/20/17 10:435.28 5g mL
P7D03627040298-08 04/21/17 9:085.66 5g mL
P7D03627040298-09 04/21/17 9:084.75 5g mL
P7D03627040298-10 04/21/17 9:087.01 5g mL
P7D03627040298-11 04/21/17 9:085.19 5g mL
P7D03627040298-12 04/21/17 9:085.22 5g mL
P7D03627040298-13 04/21/17 9:085.8 5g mL
P7D03817040298-19 04/24/17 8:225.38 5g mL
P7D03627040298-20 04/21/17 9:085.88 5g mL
P7D03627040298-21 04/21/17 9:085.71 5g mL
P7D03817040298-23 04/24/17 8:225.19 5g mL
P7D03817040298-25 04/24/17 8:225.79 5g mL
P7D03627040298-26 04/21/17 9:085.21 5g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P7D03947040298-14 04/24/17 8:075.85 5g mL
P7D03947040298-14 04/24/17 8:075.85 5g mL
P7D03947040298-15 04/24/17 8:075.06 5g mL
P7D03947040298-16 04/24/17 8:075.9 5g mL
P7D03947040298-16 04/24/17 8:075.9 5g mL
P7D03947040298-17 04/24/17 8:075.43 5g mL
P7D03947040298-17 04/24/17 8:075.43 5g mL
P7D03947040298-18 04/24/17 8:075.36 5g mL
P7D03947040298-18 04/24/17 8:075.36 5g mL
P7D03947040298-20 04/24/17 8:075.11 5g mL
P7D03947040298-21 04/24/17 8:075.38 5g mL
P7D03947040298-22 04/24/17 8:075.01 5g mL
P7D03947040298-22 04/24/17 8:075.01 5g mL
P7D03947040298-24 04/24/17 8:075.8 5g mL
P7D03947040298-24 04/24/17 8:075.8 5g mL
P7D03947040298-26 04/24/17 8:075.06 5g mL
P7D03947040298-27 04/24/17 8:075.23 5g mL
P7D03947040298-27 04/24/17 8:075.23 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 203 of 207
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