Cenco_Central Transport Annual RpT JUNE95-OCR

ANALYTICAL REPORT
PROJECT NO. 32278.000
CENTRAL TRANSPORT
KEN VOYLES
RUST ENVIRONMENT & INFRASTRUCT
QUANTERRA INCORPORATED
Certification Numl.>ers: E84059,HRS84297
FDEP CompQAP: 870270G
Chris Amstutz
Project Manager
January 4, 1995
EXECUTIVE SUMMARY -Detection Highlights
B4L2l0036
REPORTING
PARAMETER RESULT LIMIT UNIT METHOD
MW-6
bis(2-ethylhexyl)phthalate l40 lO ug/L SW846 8270A
TUX"bidity 175 2.5 NTU MCAWW 180.1
Aluminum 7,340 100 ug/L SWS46 6010A
Barium 112 10.0 ug/L SWS46 6010A
Calcium 37,300 500 ug/L SWB46 6010A
Cobalt 7.4 J 10.0 ug/L SWB46 6010A
ChX"omium 15.5 10.0 ug/L SWB46 6010A
Copper 32.8 10.0 ug/L SW846 6010A
Iron 6,580 100 ug/L SW846 6010A
Potassium 2,020 J 5,000 ug/L SW846 6010A
Magnesium 23,300 500 ug/L SW846 6010A
Manganese 125 10.0 ug/L SW846 6010A
Sodium 24,200 5,000 ug/L SWB46 6010A
Vanadium 27. 7 10.0 ug/L SW846 6010A
Zinc 23.8 20.0 ug/L SW846 6010A
Lead 6.8 5.0 ug/L SW846 H2l
MW-6-a
Di-n-butyl phthalate 40B 10 ug/L SWB46 8270A
TuX"bidity 200 5.0 NTU MCAWW 180.l
Aluminum 8,240 100 ug/L SW846 6010A
Barium 104 10.0 ug/L SW846 6010A
Calcium 36,300 500 ug/L SWB46 6010A
Cobalt 8.1 J 10.0 ug/L SW846 6010A
Chromium 17.0 10.0 ug/L SW846 6010A
CoppeX" 34.0 10.0 ug/L SWB46 6010A
Iron 7,550 100 ug/L SW846 6010A
Potassium 2,150 J 5,000 ug/L SWB46 6010A
Magnesium 22,400 500 ug/L SW846 6010A
Manganese 118 10.0 ug/L SWB46 6010A
Sodium 22,900 5,000 ug/L SWB46 6010A
Vanadium 12.8 10.0 ug/L SW846 6010A
Zinc 22 .l 20.0 ug/L SWB46 6010A
Lead 6.8 5.0 ug/L SWB46 7421
MW-7
Benzene 84 5.0 ug/L SW846 8240A
ChloX"obenzene 240 5.0 ug/L SW846 8240A
Ethylbenzene 47 5.0 ug/L SW846 8240A
Trichloroethene 4.6 J 5.0 ug/L SW846 8240A
EXECUTIVE SUMMARY -Detection Highlights
B4L210036
REPORTING
PARAMETER RESULT LlMIT UNIT METHOD
Vinyl chlo"ide 13 5.0 ug/L SW846 8240A
Xylenes, Total 190 5.0 ug/L SW846 82'>0A
cis-1,2-Dichloroethene 35 5.0 ug/L SWM6 8240A
Pi-n-buty1 phthalate 51B 10 ug/L SW846 8270A
1 1 4-Dichlorobenzene 28 10 ug/L SW846 8270A
2,4-Di~ethylphenol 8.6 J 10 ug/L SW846 8270A
Naphthalene 6.2 J 10 ug/L SW846 8270A
Turbidity 220 5.0 NTU MCAWW 180.l
Aluminum 10,400 100 ug/L SW846 6010A
Earium 239 10.0 ug/L SW846 6010A
Calcium 133,000 500 ug/L SW846 6010A
Cobalt 15.0 10.0 ug/L SW846 6010A
Chromium 17.l 10.0 ug/L SW846 6010A
Copper 44.4 10.0 ug/L SWM6 6010A
Iron 18,800 100 ug/L SW846 6010A
Potassium 10,000 5,000 ug/L SW846 6010A
Magnesium 69,600 500 ug/L SW8H 6010A
Manganese 2,';170 10.0 ug/L SW846 6010A
Sodium 157,000 5,000 ug/L SW846 60J.OA
Nickel 21.0 J 40.0 ug/L SWB46 6010A
Zinc 39.';I 20.0 ug/L SW846 6010A
Arsenic 2.0 J 5.0 ug/L SW846 7060
Lead 24 .6 5.0 ug/L SW846 7421
Selenium 4.8 J 5.0 ug/L SWB46 7740
MW-7-d
bis(2-ethylhexyllphthalate 11 10 ug/L SW846 8270A
Butyl benzyl phthalate 16 10 ug/L SW846 8270A
Pi-n-butyl phthalate 22B 10 ug/L SW846 8270A
Manganese 3 . ]. J J.0. 0 ug/L SWB46 60J.OA
Sodium 111 J 5,000 ug/L SW846 60J.0A
Zinc 13.3 J 20.0 ug/L SW846 6010A
MW-8
l,1-Dichloroechane 83 5.0 ug/L SW846 8240A
Tetrachloroethene 6.9 5.0 ug/L SW846 8240A
Trichloroethene 40 5.0 ug/L SW846 8240A
Vinyl chlo"ide 68 5.0 ug/L SW846 8240A
cis-l,2~Dichloroethene 540 5.0 ug/L SW846 8240A
Turbidity 1,600 25.0 NTU MCAWW J.80.1
Aluminum 117,000 100 ug/L SW846 6010A
Barium 863 10.0 ug/L SW846 60J.0A
Beryllium l.5 J 2.0 ug/L SW846 6010A
EXECUTIVE SUMMARY -Detection Highli~hts
B4L210036
REPORTING
PARAMETER RESULT LU!!IT UNlT METHOD
MW-8
Calcium 121,000 500 ug/L SW846 6010A
Cobalt 175 10.0 ug/L SWS46 6010A
Chromium 11140 10.0 ug/L SW846 6010A
copper 1,130 10.0 ug/L SW846 6010A
Iron 195, 000 100 ug/L SWB46 6010A
Potassium 15,500 S,000 ug/L SWS46 6010A
Magnesium 119' 000 500 ug/L SW846 60l0A
Manganese 4,850 10.0 Ug/L SW846 60l0A
Sodium 69,100 5,000 ug/L SW846 60l0A
Nickel 353 40.0 ug/L SW8H 6010A
Vanadium 450 10.0 ug/L SW846 6010A
Zinc 249 20.0 Ug/L SW846 60101'<
Arsenic 2.0 J 5.0 ug/L SW846 7060
Mercury 0.30 0.20 ug/L SWS46 7470
Lead ll.5 5.0 ug/L SWS46 7421
MW-9
Turbidity 17_0 0_50 NTU MCAWW J.80.1
Aluminum 213 100 ug/L SW846 6010A
Barium 6.0 J 10.0 ug/L SW846 6010A
Calcium 23' 300 500 ug/L SW846 60l-0A
I:i;on ';159 100 ug/L SWB46 6010A
Potassium 2,370 J 5,000 ug/L SW846 6010A
Magnesium 17,000 500 ug/L SWB46 6010A
Manganese 313 10_0 ug/L SWB46 6010A
Sodium 13,600 5,000 ug/L SWB46 6010A
MW-l-0
Turbidity 125 2.5 NTU MCA WW 190_1
Aluminum 6,190 100 ug/L SW8H 6010A
Ba.:ciurn 35.3 10.0 ug/L SW846 60l0A
Calcium 25,700 500 ug/L SW846 60l0A
Chromium 8.5 J 10_0 ug/L SW846 6010A
Copper 7.7 J 10.0 ug/L SW846 6010A
Iron 4,690 100 ug/L SWSH 6010A
Potassium 1,640 J 5,000 ug/L SW846 601011
Magnesium 13,900 500 ug/L SW846 6010A
Manganese 78.6 10.0 ug/L SW846 6010A
Sodium 13' 700 s.ooo ug/L SW846 6010A
Vanadirnn 11-4 10_0 ug/L SW846 6010A
EXECUTIVE SUMMARY -Detection Highlights
B4L210036
REPORTING
PARAMETER RESULT LIMIT !ill.IT METHOD
MW-10
Zinc 6_1 J 20.0 ug/L SW846 60]. 0.A
Lead 4_4 J 5.0 ug/L SWS46 742l
MW-13
Chlorobenzene 1-6 J 5.0 ug/L SWM6 8240.A
l 1 l·Dichloroethane 5.0 5_0 ug/L SW846 8240.A
l,lnDich1oroethene 2.4 J 5.0 ug/L SW846 8240.A
Trichloroethene 3.2 J 5_0 ug/L SW846 8240.A
Vinyl chloride 2.2 J 5.0 ug/L SW846 8240.A
cis-l,2-Dich1oroethene 16 5.0 ug/L SWS46 824 0.A
bis(2-ethylhexyl)phthalate l9 10 ug/L SW846 8270.A
Turbidity 48.0 1. 0 NTU MC.A.WW 180.1
.Aluminum 4,710 100 ug/L SWS46 6010.A
Barium l28 10.0 ug/L SW846 6010.A
Calcium 136,000 500 ug/L SW846 6010A
Cobalt U.l 10.0 ug/L SW846 6010.A
Chromium 41. 7 10.0 ug/L SWS46 6010A
Copper 20.8 10.0 ug/L SW846 6010A
Iron 6,900 100 ug/L SW846 6010A
Potassium 6,030 5,000 ug/L SWS46 6010.A
Magnesium 38,800 500 ug/L SWS46 6010.A
Manganese 1, 960 10.0 ug/L SWS46 6010A
Sodium 34,500 5,000 ug/L SWS46 6010.A
Nickel 21.0 J 40.0 ug/L SW846 6010.A
Vanadium S.l J 10_0 ug/L SW846 6010.A
Zinc 128 20.0 ug/L SW846 60J.OA
Arsenic 3.0 J 5.0 ug/L SW846 7060
Lead 3.0 J 5.0 ug/L SW846 H21
MW-16
Trichloroethene l.3 J 5.0 ug/L SW846 8240.A
cisMl,2-Dichloroethene 2.3 J 5.0 ug/L SW846 8240.A
Turbidity 8.0 0.50 NTU MC.A.WW 180.1
Aluminum 374 100 ug/L SW846 6010A
Barium 42.5 10.0 ug/L SW846 6010A
Calcium 76,500 500 ug/L SW846 6010.A
Chromium 5_5 J 10.0 ug/L SW846 6010A
Iron 608 100 ug/L SW846 6010.A
Pota.ssiwn 2,750 J 5,000 ug/L SWBH 6010.A
Magnesium 14,800 500 ug/L SW846 6010A
EXECUTIVE SUMMARY -Detection Highlights
B4L210036
REPORTING
PARAMETER RESULT LIMIT IlliII METHOD
MW-l6
Manganese 221 10.0 ug/L SW846 6010A
Sodium 15,400 5,000 ug/L SW$46 6010A
Lead 1.8 J 5.0 ug/L SW846 7421
ANALYTICAL METHODS SUMMARY
Para.meters
TCL Volatile Organics
TCL Semivo1atile Organics
Turbidity
Silver
Aluminum
Barium
Beryllium
Calcium
Cadmium
Cobalt
Chromium
Copper
Iron
Potassium
Magnesium
Manganese
Sodium
Nickel
Antimony
Vanadium
Zinc
Arsenic
Lead
11ercury
Selenium
Thallium
Cyanide, Total
11ethods
SW846 8240A
SW846 8270A
11CAWW 180.l
SW846 6010A
SW846 6010A
SW8H 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 7060
SW846 7';121
SW846 7470
SW846 7740
SW846 7841
SWS46 ~OlOA
References:
11CAWW
SW846
11ethods for Chemical Analysis of Water and Wastes, El1SL:
Cincinnati, OH: March 1983 and subsequent revisions
11 Test Methods for Evaluating Solid waste, Physical/Chemical
Methods", Third Edition1 September, 1986 and subsequent
:t""evisions
SAMPLE SUMMARY
The analytical results of the samples listed below are presented
en the following pages.
'.l'!Q_J!_ l.AEORATORY ID SAMPLE IDENTIFICATION
AlXRX B4L210036-00l MW-6
AlXT2 B4L210036-002 MW-6-a
AlXT7 B4L210036 -003 MW-7
AlXT9 B4L210036 • 004 MW-7-d
AlXTC B4L2l0036 -005 MW-8
AlXTE B4L210036-006 MW-9
AlXTG B4L210036-007 MW-10
AlXTK B4L210il36-008 MW-13
AlXTM B4L210036 • 009 MW-16
AlXTN B4L210036·010 MW-10-c
WO #: AlXRXlOR
LAB #: B4L210036-00l
MATRIX: WATER
PARAMETER
Benzo(a)pyrene
3,3 1 mDichlorobenzidine
Anthracene
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dirnethylphenol
Dimethyl phthalate
Di-n-octyl phthalate
4,6MDinitrc-
2·rnethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluorant:hene
Fluorene
Hexachlorobenzene
Hexachlorobut:adiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2·Methylphenol
4-Methylphenol
SURROGATE RECOVERY
Nitrobenzene-d5
2·Fluorobiphenyl
Terphenyl-dl4
2-Fluorophenol
Phenol-dS
2,4,6-Tribrornophenol
NOT~ AS RECEIVF ... D
RUST ENVIRONMEN'l' & INFRASTRUCT
DATE SAMPLED: 12/20/94
12/21/94 DATE .RECEIVED:
- -GC/MS Semi-Volatiles
2 OF 3
RESULT REPORTING
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
10
50
10
10
10
10
10
10
50
50
10
10
10
10
10
10
10
10
10
10
10
10
10
LIMIT METllOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWS46 8270A
SW846 B270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
68
71
52
68
56
82
26
27
10
10
10
10
131)
119)
165)
116)
175)
155)
EXTRACTION-
ANA.LYSIS DATE
QC
BATC!l
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
ND NOT DETF..CTRl) AT TUE STATED REPORTING LIMIT
RUST E!;VIRONMENT & INFRASTRUCT
WO #: AlXRXlOR
LAB #: B4L210036-00l
MATRIX: WATER
MW-6
DATE SAMPLED:
DATE )<ECEIVED:
12/20/94
12/21/94
- - - - - - - - - - - ---- - -GC/MS Semi-Volatiles - - - --- - - - - - -
PARAMETER
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
l,2,4-Trichlorobenzene
2,4,SMTrichlorophenol
2,4,6~Trichlorophenol
bis(2-chloroieopropyl)ether
SURROGATE RECOVERY
lli trobenzene -as
2-Fluorobiphenyl
Terphenyl-d14
2 -Fluorophenol
Phenol-dS
2 1 4,6-Tribromophenol
NOTF....; AS Rf..(:ElVED
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
68
7l
52
68
56
82
ND N<)l' Dl!';TECTED AT THE $'l'ATJ.ID REPORTING LfMl'J'
3 OF 3
REPORTING
LIMIT
10
50
50
50
10
10
50
10
10
50
10
10
10
10
10
10
10
METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW8H 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26 l31)
27 U9)
10 165)
10 116)
10 175)
10 155)
EXTRACTION-QC
AllALYSIS DATE BATCH
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRO!<IMENT & INFRASTRUCT
WO #: AlXRX
LAE #: B4L210036-001
MATRIX: WATER
MW-6
PATE SAMPLED:
DATE RECEIVED:
12/20/94
12/21/94
-- - - -· --- - -REQUESTED METALS - - - -· - - - -· - - - - -
PARAMETER
Silver
Alwninu:cn
Barium
Beryllium
Calcium
Cadmium
Cobalt
Chromium
Copper
Iron
Potassium
Magnesium
Manganese
Sodium
Nickel
Antimony
Vanadium
Zinc
Arsenic
Lead
Mercury
Selenium
Thallium
NOTE; AS RECEJ.VJ.i:I)
RESULT
ND
7.340
112
ND
37,300
ND
7.4 J
15.5
32.8
6,580
2,020 J
23,300
125
24,200
ND
ND
27.7
23.8
ND
6.8
ND
ND
ND
REPORTING
LIMIT
10.0
100
10.0
2_0
500
5.0
10.0
10.0
10.0
100
5,000
500
10.0
5,000
40.0
50.0
10.0
20.0
5_0
s.o
0.20
ND NOT IJl~F..CTIID AT Tiffi STATED REPOR1lNG LfMIT
ug/L
ug/L
ug/J'.,
ug/L
ug/L
ug/L
ug/L
ug/L
ug/I.
ug/I.
ug/L
ug/L
ug/J;.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
J ESTJ.MATJ!:U VALlJF~ (Hl<:TECTED), BUT BELOW QUANTffAl'lON LIMIT,
METHOD
SW846 6010A
SW846 6010A
SW846 60l0A
SW846 6010A
SW846 6010A
SW8H 6010A
SW846 60l0A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 60l0A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 7060
SW846 7421
SW846 7470
SW846 7740
SW846 7Ml
PREPARATION -
ANALYSIS DATE
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/Z8-12/29 /94
12/28-12/29/94
12/28-12/29/94
12/;.!8-12/29/94
12/28-12/29/94
12/28-1;.l/29 /94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29 /94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28/94
12/27/94
12/28-12/29/94
12/28/94
QC
BATCH
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4360022
4362073
4362073
RUST Ell!VIRONMENT & INFRASTRUCT
WO #: AlXRX
LAB #: B4L21QQ36-00l
:MATRIX: WATER
-- -. -. .
PARAMETER
Turbidity
Cyanide, Total
NOT& AS RECEIVED
--
MW-6
- -. -INORGANIC ANALYTICAL
REPORTING
RESULT LIMIT UNIT
175 2,5 NTU
ND 0.010 rng/L
ND NOT DETECTll:lJ AT THE STATED REPORTING LIMIT
REPORT - -
DATE $A!dPLED:
DATE RECEIVED:
. -- -
. . --
12/20/94
12/21/94
PREPARATION QC
METHOD ANALYSIS DATE BATCH
MCAWW 180.1 12/21/94 4356088
SW846 9010A J./03/95 5003104
RUST ENVIRONMENT & lNFRASTRUCT
WO #: AlXT2lOQ
LAB #: B4L2l0036-002
l>IATRIX: WATER
MW-6-a
OATE SAMPLEO:
PATE RECEJ:VEO:
12/20/94
12/21/94
· -· · -· · -· · -· - -· - - -GC/MS Volatiles - --- - -· - -· -· --
PARAMETER
Acet.one
Benzene
Bromodichloromethane
Bromof orm
Bromornethane
Carbon disulfide
carbon tetrachloride
Chlorobenzene
Dibromochloromethane
Chloroethane
Cnloroform
Cnlorometnane
l,l-Dichloroethane
l,2-0icnloroetnane
1,1-Dichloroethene
cis-l,3-Dichloropropene
trans-1,3-Dicnloropropene
Ethylbenzene
2-Hexanone
1'letnylene cnloride
4-Metnyl-2-pentanone
Sty:i:;ene
1,1,2,2-Tetrachloroethane
SURROGATE RECOVERY
l,2-Dichloroethanewd4
Toluene-dB
Brornof1uorobenzene
Nora A.C;, RECEIVlol"J
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
100
100
99
NO NOT D!!71"F...CTED /\. T "fHE ST ATl~O REPOR'l'fNG LIM.lT
1 OF 2
REPORTING
LUUT
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
5.0
5.0
s.o
5.0
10
5.0
10
5.0
5.0
METHOD
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWM6 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
81
130)
109)
11 7)
EXTRACTION-
ANALYSIS DATE
12 /29 /94
12/29 /94
12/29/94
l2/29/94
u/n/94
l2/29/94
12/29/94
l2/29/94
l2 /29 /94
12/29/94
12/29/94
l2 /29 /94
12/29/94
l2/29/94
12/29/94
l2/29/94
12/29/94
l2/29/94
12/29/94
12/29/94
12/29/94
12/29/94
12/29/94
QC
BATCH
4364034
4364034
4364031
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
RUST ENVIRONMENT & INFRASTRUCT
WO #' AlXT210R
LAB #' B4L210036-002
MATRIX: WATER
"!W-6-a
DATE SM<IPLED:
DATE RECEIVED:
12/20/94
12/21/94
- - - - - - - - - - - - - - - - -GC/MS Semi-Volatiles - - - - - - - - - - - -
PARAMETER
A.cenaphthene
Acenai;>ht:hylene
B@nzo{a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(ghili;>erylene
bis(2-chloroethoxy)met:hane
bis(2-chloroethy1)ether
bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Diben~(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
l,2-Dichlorobenzene
1,3-Dichlcrobenzene
1,4-Dichlorobenzene
SURROGATE RECOVERY
Nitrcbenzene~d5
2-Fluorobiphenyl
Terph@nyl -d14
2-F1uoropheno1
Phenol-dS
2,4,6-Tribromophenol
N0'rt=;: AS RJXEIVF .. n
RESULT
lug/Ll
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
40B
ND
ND
ND
71
70
57
67
55
81
NJ) NOT DBTECTED A.'f Tiffi STATF.D U.l~PORTlNG LIMIT
1 OF 3
RE<>ORTING
LIMIT
10
10
10
lO
10
lO
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 6270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26
27
10
10
10
10
131)
ll9)
165)
116)
175)
155)
u (COMP'OUNl) OETEC'l'l:~U IN M1::1·noD RI,,A..NK ASSOCIATF ... n WlTH THlS SA.MPLF...)
EXTRACTION-
ANALYSIS DATE
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23 -12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
l2/23-l2/29/94
12/23-12/29/94
12/23 -12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12 /23-12/29/94
12/23-12/29/94
12/23-12/29/94
QC
BATCH
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #: A1XT210R
LAB #: B4L210036-002
MATRIX: WATER
MW-6-a
DATE Sl\MPLED:
DATE RECEIVED:
12/20/9-:<
12/21/94
---· -· -· -· - - - - - -· GC/MS Semi-Volatiles · - - -· -· -· -· -
PARAM!!TER
Naphthalene
2-Nitroaniline
3nNitroaniline
4-Nitroaniline
Nitroben.zene
2 -Ni trophenol
4-Nitrophenol
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
l,2,4~Trich1orobenzene
2,4,5~Trich1oropheno1
2,4,6-Trichlorophenol
bis(2·chloroisopropyl)ether
SURRoGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-d14
2-Fluoropnenol
Phenol-dS
2,4,6·Trib~ornopheno1
NOT}"'..: AS J{ECE.IV~l)
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
NP
NP
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
71
70
57
67
55
81
ND NOT OETF...CTBf> AT Tug ST ATJ<:n REP()ltTING LrMIT
3 OF 3
REPORTING
LIMIT
10
50
50
50
10
10
50
10
10
50
10
10
10
10
10
10
10
METflOD
SW846 8270A
SW846 B270A
SW846 8270A
SW846 8270A
SW846 8270A
SWM6 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 827QA
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26 131)
27 119)
10 165)
10 116)
10 175)
10 155)
EXTRACTION-QC
ANALYSIS DATE BATCfl
12/23-l2/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23·12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXT2
LAE #: B4L2l0036-002
MATRIX, WATER
MW-6-a
DATE SAMPLED:
DATE RECEIVED:
12/20/94
12/21/94
• - -• • • - - -• -REQUESTED METALS • • - -• • - -• • - - -• -
PARAMETER
Silver
Aluminum
Barium
Beryllium
Calcium
Cadmium
Cobalt
Chromium
Copper
I.ron
Potassium
Magnesium
Manganese
Sodium
Nickel
Antimony
Vanadiwn
Zinc
Arsenic
Lead
Mercury
Selenium
Thallium
NOTF....; AS RECElVllJ)
RESULT
ND
8,240
104
ND
36,300
ND
8.l J
17.0
34.0
7,550
2,150 J
22,400
118
22,900
ND
ND
12.8
22.1
ND
6.8
ND
ND
ND
REPORTING
LIMIT
10.0
100
10.0
2.0
500
5.0
10.0
10.0
10.0
100
5,000
500
10,0
5,000
40.0
50.0
10.0
20.0
5.0
5.0
0.20
5.0
s.o
ND NOl' l)F,l'F..CTED AT Tllli !ffATF.D REPORTlN<T L™IT
us/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
J ES'l'lJ\1A1'F.D VALUE. (Ul~Tlt .. C'f'f<:D). nuT UELOW QUANTITATJON i.IMIT.
MET!!QD
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 60101'
SW846 6010A
SW846 60101'
SW846 60101'
SW846 6010A
SW846 6010A
SW846 60101'
SW846 60101'
SW846 7060
SW846 7421
SW846 7470
SW846 7740
SW846 7841
PREPARATION -
ANALYSIS DATE
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/20-12;29 n4
12/28-12/29/94
l-2/28-12/29/94
12/28-12/29/94
12/28-l-2/29/94
12/28-12/29/94
12/28-12/29/94
12/28-l-2/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/9'1
12/28-12/29/94
l2/28/94
12/28/94
12/27 /94
12/28-12/29/94
12/28/94
QC
BATCH
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
<1362073
4362073
4360022
4362073
4362073
RUST ENVIROliMENT & INFRASTRUCT
WO jj, Al-XT2
LAB #: B4L210036-002
MATRJ:X: WATER
-. -. ---
PARAMETER
Turbidity
Cyanide, Total
NOTE: AS RECEIVED
-
MW-6-a
-. ---INORGANIC ANALYTICAL
REPORTING
RESULT LIMIT UNIT
200 s.o NTU
NP 0.010 rog/L
ND NOT DE"J.'ECTEP AT THE STATED REPORTING UlvflT
REl?ORT --
DATE SAMl?LEP:
DATE RECEJ:VED:
-----. --
12/20/94
l-2 /21/94
PREPARATION QC
METHOD ANALYSIS DATE BATCH
MC.II.WI\' 180.1 12/21/94 4356088
SW8H 9010A 1/03/95 5003104
WO #: 1'1XT710Q
Ll'B #: B4L210036-003
ldATRIX: WATER
RUST ENVIRONMENT & INFRASTRUCT
MW-7
DJ\ TE SAMPLED :
DllTE RECEIVED;
12/20/94
12/Zl/94
- - - - - - - - - - - --- - - - -GC/MS Volatiles - - - - - - - - - - --- - -
1 OF 2
RESULT REPORTING
PARAMSTER
Acetone
Benzene
Brotnodichloromethane
Bromoform
Brornomethane
Carbon disulfide
Carbon t@trachlo~ide
Chlorobe.nzene
Dibromochloromethane
Chloroethane
Chloroform
Chloromethane
1,1-Dichloroethane
1,2-Pichloroethane
1,1-Dichloroethene
cis~l,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
4-Methyl-2-pentanone
Styrene
1,1,2,2-Tetrachlo~oethane
SURROGATE RECOVERY
l,2-Dichloroethane-d4
Toluene-dB
Bromofluorobenzene
NOTE: AS RF...CE'JV"fl)
(ug/Ll
ND
84
ND
ND
NP
ND
ND
240
ND
ND
ND
ND
ND
ND
ND
ND
ND
47
ND
ND
ND
ND
ND
99
102
99
NJ.l NOT Uf.TECTEI) AT TlU'· STATEO RF..PORIING Ll)VflT
LIMIT
50
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
50
5.0
50
5.0
5.0
METHOD
SW846 824 OA
SW846 8240A
SW846 8240A
SWSH 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWS46 S240A
SW846 8240A
SW846 B240A
SW846 8240A
SWSH 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWSH 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
Bl
130)
109)
117)
EXTRACTION -
ANALYSIS DATE
12/29/94
12/29/94
12/29/94
12/29/94
12/29/94
12/29 n4
12/29/94
i2;29n4
12/29 /94
12/29/94
12/29/94
J.2 /29 /94
12/29/94
12/29 /94
12/29/94
12/29/94
12/29/94
12/29/94
12 /29 /94
12/29 /94
12/29 /94
12/29/94
12 /29 /94
QC
BATCH
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
WO #' AlXT7lOQ
LAB #' B4L210036-003
MATRIX, WATER
- - --- -
- -- --- -
-
RUST ENVIROl>lMENT & INFRASTRUCT
MW-7
- -- -Ge/Ms Volatiles - - -
2 OF 2
RESULT REPORTING
- -
!>.ATE S.AMl?LE!l'
!>.ATE RECEIVED,
- -
-- -- -
-
EXTRACTION-
-
12/20/94
12/21/94
QC
PARAMETER (ug/L) LIMIT METHOD ANALYSIS DATE BATCH
2~But.anone
1,2-Ilichloropropane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichlorcethane
Trichloroethene
Vinyl chloride
Xylene.st Total
cis-1,2-Dichloroethene
Vinyl acetate
SURROGATE RECOVERY
l,2-Dichloroethane-d4
Toluene-d8
Bromof luorobenzene
NOTI~ AS RECEIVED
NI>
ND
ND
ND
NI>
NI>
4.6
13
190
35
ND
1
99
102
99
J
NO NOT DETECTED AT TlU::.$TA'l'El) REPORTil"1G UMIT
50 SW846
5.0 SWS46
5.0 SW846
5.0 SW846
5.0 SW846
5.0 SW846
5.0 SW846
s.o SW846
5.0 SW846
s.o SW846
50 SW846
.l\CCEPTABLE LIMITS
78
90
81
no)
109)
117)
F~~TlMATF..D VALUE. (JJBTll.C'I'l~..l)). BUT BF.LOW QUANTITA'I'lON 1..Th!IT.
8240A 12/29/94 4364034
8240A 12/29/94 4364034
8240A n/29/94 4364034
8240A 12/29/94 4364034
8240A 12/29/94 4364034
8240.l\ 12/n/94 4364034
824'0.A 12/29/94 4364034
8240.A 12/29/94 4364034
8240.A 12/29/94 4364034
8240.A 12/29/94 4364034
8240A 12/29/94 4364034
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXT710R
LAB #: B4L210036-003
MATRIX: WATER
MW-7
DATE SAMI'LED:
DATE RECEIVED:
12/20/94
12/21/94
- - -· · · · -- - - - - -· -· GC/MS Semi-Volatiles - - -· -- - - - -· ·
PARAMETER
Acenaphthene
.Acenaphthylene
Benzo(a)anchracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(ghi)perylene
bis(2-chloroethoxy)methane
bis(2-chloroethyl)ether
bia(2·ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chryaene
Dibenz(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
l,2~Dich1orobenzene
l,3-Dichlorobenzene
l,4~Dichlorobenzene
SURROGATE RECOVERY
Nitrobenzene-d5
2·F1uorobiphenyl
Terpheny1-dl-4
2 • l'luorophenol
Phenol-d5
2,4,6mTribromophenol
NOTE: A~ R.EC1';IV1;-,n
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
51B
ND
ND
28
1
82
80
37
67
80
61
ND NOT DJ::"n~TEO Al' "fHESrATED REPORTING LIMIT
l-OF 3
REPORTING
LIMIT
10
lO
10
)_ 0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
lO
10
10
10
10
METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWS46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 S270A
SWS46 8270A
SW846 S270A
SW846 8270A
SW846 8270A
SW846 S270A
SW846 8270A
SW946 9270A
ACCEPTABLE LIMITS
26
27
10
10
10
10
131)
119)
l-65)
116)
175)
155)
6 (C()M.l•OOND DETECTED lli' :METHOD BLANK A.SS0ClA1'F..D WITH THIS SAM.l:'LB)
EXTRACTION-QC
ANALYSIS DATE BATC!J
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 435710l
l2/23-12/30/94 4357101
l2/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23·l2/30/94 435710l
12/23-12/30/94 4357101
l2/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357l0l
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 435710l
12/23-12/30/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #' A1XT710R
LJIB #: B4L210036·003
MATRIX: WATER
MW-7
PATE SAMPLED:
DATE RECEIVED:
12/20/94
12/21/94
- - - - - - - - - - - - - - -· -GC/MS Semi-Volatiles -· - - - - - - - - - -
PARAMETER
Benzo(a)pyrene
3,3'-Dichlorobenzidine
Anthracene
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
Di-n-octy1 phtha1ate
4,6-Dinitro-
2-rnethylphenol
214-Dinitrophenol
2,4-Dinicrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
lsophorone
2-Methylnaphthalene
2 ·Methylphenol
4-Methylphenol
SURROGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
Terpheny1 -d14
2-Fluorophenol
Phenol"d5
2,4,6-Tribromophenol
No·tr: AS R.ECr'lVF..D
RESULT
(ug/L)
ND
NP
ND
ND
ND
8.6 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
82
80
37
67
80
61
ND NOT DETJj.(:·fF..D AT TllF. S'fATED lU~>(>RTING Lfl\IOT
2 OF 3
REPORTING
LIMIT
10
50
10
10
10
10
10
10
50
so
10
10
10
10
10
10
10
10
10
10
10
10
10
METHOD
SWB46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A.
SW846 8270A
SW846 8270A
SW846 S270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW8% 8270A
SW846 8270A
ACCEPTABLE LJMITS
26
27
10
10
10
10
131)
119)
165)
116)
175)
155)
ESTIMA'l'F..D VALl)l~~ (DETECTl~l)), BUT UEl,O'W QUAN'11TATION l.fll.1:11'.
EXTRACTION-QC
ANALYSIS DATE BATCH
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #: A1XT710R
LAB #: B4L210036-003
MATRIX: WATER
MW-7
DATE S.l\MPLED:
DATE RECEIVED:
12/20/94
12/21/94
- - - - - - - - - - - - --- - -GC/MS Semi-Volatiles - - - - - - - - - - - -
PARJU<lETER
Naphthalene
2-Nitroaniline
3-Nitroanili:ne
4-Nit.roaniline
Nitrobe:nzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-T~ichlorophenol
2,4,6-Trichlorophenol
bis(2-chloroisopropyl)ether
SURROGATE RECOVERY
Nitrobe:nzene~d5
2-Fluorobiphenyl
Terphenyl-dl4
2 -Fluorophenol
Phenol-d5
2,4,6-Trib~omcphenol
NOTE; AS RF..Cl!lVED
RESULT
(ug/L)
6.2 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
82
80
37
67
80
61
ND NO'I" OETECTED AT '"flll:: STATED RF..POll'l'ING LlMIT
3 OF 3
REPORTING
LIMIT
lO
50
50
50
10
10
50
10
10
50
10
10
10
10
10
10
10
METHOD
SWS46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26 131)
27 119)
10 l.65)
10 116)
10 175)
10 155)
) ESTIMA rEn v /\LUE. (DETl<X::'flr,J)). UUT UF.J.()W QUAN'l'ITATION LIMIT.
EXTRACTION-
ANALYSIS DATE
12/23·12/30/94
12/23-12/30/94
12/23"12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
12/23-12/30/94
QC
BATCH
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
RUST E>IVIRONMENT & INFRASTRUCT
WO #: A1XT7
LAE #: B4L210036-003
MATRIX: WATER
MW·7
DATE .SAMPLED:
DATE RECEIVED:
12/20/94
12/21/94
- - - - - -• • • • -REQUESTED METALS • • • - - - -• • • - - - -•
l'ARAMETER
Silver
Alwninwn
Barium
Beryllium
Calcium
Cadmium
Cobalt
Chromium
Copper
Iron
Potaesiwn
Magnesium
Manganese
Sodium
Nickel
Antimony
Vanadium
Zinc
Arsenic
Lead
Me:rcu:t'y
selenium
Thallium
NOl'f..: AS RECEIVED
RESUL'l'
ND
10,400
239
ND
133,000
ND
15.0
17.l
44.4
18,800
10,000
69,600
2,470
157,000
21.0 J
ND
ND
39.4
2.0 J
24.6
ND
4.8 J
ND
REPORT!l'IG
LIMIT
lO.O
100
10.0
2.0
500
5.0
10.0
10.0
10.0
100
5,000
500
10.0
5,000
40.0
50.0
10.0
20.0
5.0
5.0
0.20
5.0
5.0
ND NOT DETECTED AT THE ST/\.Tl~I) RF.:PORTlNG LIMIT
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
J ESTIJ\1ATED VA..1_,UI"~ (l)J<'::rF..Cl'F..0). RUT BF.J..OW QUANTITATlON IJMl1'.
METHOD
SW8% 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 60l0A
SW846 6010.l\.
SW846 60H.l\.
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 7060
SW846 7421
SW846 7470
SW846 7740
SW846 7841
PREPARATION -
ANALYSIS DATE
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28·12/2S/94
12/28-12/29 /94
12/28-12/29 /94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28/94
12 /27 /94
12/28-12/29/94
12/28/94
QC
BATCH
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4360022
4362073
4362073
RUST ENVIRONMENT a INFRASTRUCT
WO #: A1XT7
L.IW #: B4L210036·003
MATRIX: WATER
-- - -- - -
PARMIETER
Tu:t"bidity
Cyanide, Tocal
NOTE: AS R.ECF";VED
- -
MW-7
-- - -INORGANIC ANALYTICAL
REPORTING
RESULT LIMIT !illll
220 5.0 llTU
ND 0.010 mg/L
ND Nol DETECTED AT 'fl(l~ STATED REPORTING UMIT
REPORT -.
DATE SAMPLED:
DATE RECEIVED:
. . - - -- - -
12/20/94
12/21/94
PREPARATION QC
METHOD ANALYSIS DATE BATCH
MCAWW 180.l 12/21/94 4356088
SW846 9010A 1/03/95 5003104
RUST ENVIROID<IENT & INFRASTRUCT
WO #: AlXT910Q
L.AB #: E4L210036-004
MATRIX, WATER
MW-7-d
DATE SAMPLED,
DATE RECEIVED:
12/20/94
12/21/94
- - - - - - ----------- -GC/MS Vola tJ.les - - - - - - -
PARAMETER
Acetone
Benzene
Bromodichloromethane
Bromof orrn
Bromornethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Dibrornochlorornethane
Chloroethane
Chloroform
Chloromethane
1 1 1-Dichloroethane
l,2~Dichloroethane
l,l~Dichloroethene
cis-l,3~Dichloropropene
trans-1,3-Dichloropropene
Echylbenzene
2-Hexanone
Methylene chloride
4-Methyl-2-pentanone
Styrene
111,2,2-Tetrachloroethane
SURROGATE RECOVERY
112-Dichloroethane-d4
Toluene-dB
Bromofluorobenzene
NOTE; AS RF...CEfVli:()
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
101
103
97
ND Nor n1;;1·1::.c·n~:n AT THE STATED REPORTlNG LIMIT
1 OF 2
REPORTING
LIMIT
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
METHOD
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWS46 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
81
130)
109)
ll 7)
EXTRACTION·
ANALYSIS OA'rE
12/29/94
12/29/94
12/29/94
12/29/94
12/29 /94
12 /29 /94
12/29/94
12/29/94
12/29/94
12/29/94
12/29/94
12/29/94
12/29 /94
12/29/94
12/29 /94
12/29 /94
12/29 /94
12/29/94
12/29/9<t
12/29/94
12/29/94
12/29/94
12/29/94
QC
EA'rCH
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
WO #: AlXT910Q
LAB #: B4L210036-004
MATRIX: WATER
PARAMETER
2-Butanone
l,2-0ich1oropropane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
cis-1,2-Dichloroethene
Vinyl acetate
SURROGATE RECOVERY
1,2-Dichloroethane-d4
Toluene-dB
Bromofluorobenzene
NOT~ AS RECFJVED
RUST ENVIRONMENT & INFRASTRUCT
MW-7-d
- - -GC/MS Volatiles
2 OF 2
RESULT REPORTING
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LIMIT
10
5_0
5_0
5.0
5.0
5.0
5.0
5,0
5.0
5.0
10
DATE SAMPLED:
DATE RECEIVED:
12/20/94
12/21/94
METHOD
EXTRACTION-
ANALYSIS DATE
QC
BATCH
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWSH 8240A
SW846 8240A
SWS46 8240A
SWS46 8240A
SWS46 S240A
12/29/94
12/n/94
12/29/94
12/29/94
12/29/94
12/29/94
12/29/94
12/29/94
12 /29 /94
12/29/94
12/29/94
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
43H034
4364034
4364034
ACCEPTABLE LIMITS
101
103
97
78
90
81
130)
109)
ll 7)
NI) NOT DETECTED AT THE STATED REPORTil'l'G LIMIT
RUST ENVIRONMENT & INFRASTRUCT
WO #: A1XT910R
LAB #: B4L210036-00~
MATRIX: WATER
MW·7-d
DATE SAMPLED:
DATE RECEIVED:
12/20/94
12/21/94
- - --· · - - -· - --- - - -GC/MS Semi-Volatiles - -· - - -· -· - --
PARAMETER
Benzo(a)py>;ene
3.3'~Dichlorobenzidine
Anthracene
2,4-Dichlorophenol
Diethyl phthalate
2,4·Dimethylphenol
Dimethyl phthalate
Oi-n-octyl phthalate
416-Dinitro~
2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2 1 6wOinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
rsophorone
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
SURROGATE RECOVERY
Nitrobenzene-dS
2·Fluorobiphenyl
Terphenyl · dl4
2 • Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
NOTE: i\S RECEM~H
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
70
69
117
64
60
79
ND N01· r>ETECTEO AT TllE STATi';I) REPORilNG 1.,JJ\.flT
2 OF 3
REPORTING
LIMIT
10
50
10
10
10
10
10
10
50
50
10
10
10
10
10
10
10
10
10
10
10
10
10
METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 82701'
SW846 8270A
SW846 82701'
SW846 8270A
SW846 8270A
SWS46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTA'BLE LIMITS
26
27
10
10
10
10
131)
119)
165)
116)
175)
155)
EXTRACTION· QC
ANALYSIS DATE BATCH
12/23-12/30/94 435710l
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
12/23-12/30/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #: JUXT9
LAB #: B4L210036-004
MATRIX: W,l<Tl<R
. . . --- -
PARAMETER
Turbidity
Cyanide, Total
NOTE: AS RECEIVED
.
MW-7-d
- - - --INORGANIC ANALYTICAL
REPORTING
RESULT LIMIT UNIT
ND 0.50 NTU
ND 0.010 mg/L
ND NOT DETECT£l> AT THE STATED REPORTING Utvnl
REPORT . -
DATE SAMPLED:
DATE RECEIVED:
- ---. . - -
12/20/94
J.2/21/94
PREPARATION QC
METHOD ANALYSIS DJ<TE BA.TCH
MCJ<WW 180.1 12/21/94 4356088
SWS46 9010A 1/03/95 5003104
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXTClOQ
LltJ> #: B4L210036-005
MATRIX: WATER
MW-8
DATE S.llMPLED:
DATE RECEIVED:
12/20/94
12/21/94
- - - - - - - - - - - - - - - - - -GC/MS Volatiles - --- - - -
PARJU1ETER
Acetone
Benzene
B~omodichloromethane
Bromof orm
Brornornethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Dibromochlorornethane
Chloroet.hane
Chloroform
Chlorornethane
l,l-Dichloroethane
lj2-Dichloroethane
1,1-Dichloroethene
cisrl,3~Dichloropropene
transrl,3-Dichloropropene
Et:hylbenzene
2~Hexanone
Methylene chloride
4-Methy1-2-pentanone
Styrene
l,l,2,2-Tetrach1oroethane
SURROGATE RECOVERY
l,2-Dich1oroethane-d4
Toluene-as
Bromofluorobenzene
N01"1~ AS Rl~.t:l!,lYI~.>
RESULT
(Uq/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
83
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
102
104
98
NU NOT DETECTED AT Tlll!: STATl.~l) R£l'0RtlNG l.(M:ll'
l OF 2
REPORTING
LIMIT
50
5.0
5.0
5.0
lO
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
50
5.0
50
5.0
5.0
METHOD
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWS46 8240A
SWS46 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWS46 8240A
SWS46 8240A
SWS46 8240A
SWS46 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
81
l30)
109)
117)
EXTRACT ION·
ANALYSIS DA'l'E
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
QC
BATCH
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
WO #' AlXTClOQ
LAB #' B4L210036-005
W\TRIX' WATER
. - -. . . . ---
PARAMETER
2-Butanone
1,2-Dichloropropane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1 1 2-Trichloroethane
Trichloroethene.
Vinyl chloride
Xylenee, Total
-
oia~l,2-Dichloroethene
Vinyl acetate
SURROGATE RECOVERY
1,2-Dichloroethane-d4
Toluene-d8
Bromof1uorobenzene
NOTE; AS RECF.JVED
-. -
RUST ENVIRO:mdENT & INl'RASTRUCT
----GC/MS Volatiles -- - -
2 OF 2
RESULT REPORTING
-
DATE SAMPLED'
DATE RECEIVED'
- ---. . . -
EXTRACTION-
-
12/20/94
12 /21 /94
QC
(ug/L) LIMIT METHOD ANALYSIS DATE BATCH
ND
ND
6.9
ND
ND
ND
40
68
ND
540
ND
102
104
98
50 SW846 s_o SW846
5.0 SW846
s_o SW846 s_o SW846
5.0 SW846
5.0 SW846
5.0 SW846
5.0 SW846
5.0 SW846
so SW846
ACCEPTABLE LIMITS
78
90
81
130)
109)
117)
8240A 12/30/94 4364093
8240A 12/30/94 4364093
8240A 12/30/94 4364093
82-:!0A 12/30/94 4364093
8240A 12/30/94 4364093
8240A 12/30/94 4364093
8240A 12/30/9'\I 4364093
8240A 12/30/94 4364093
8240A 12/30/94 4364093
8240A 12/30/94 4364093
8240A 12/30/94 4364093
ND NOT OETF.CTF,.O A 'l' l'fl)<;. $'1' A 'l'F..O Rf~))()~TlNC LlMIT
ROST ENVIR01'ME11'l' & INFRASTRUCT
WO #: AlXTClOR
LAB #' B4L210036-005
MllTRIX: WATER
MW·S
DATE SAMPLED:
DATE RECEIVED'
12/20/94
12/21/94
- - - - - - - - - - - - - - - - -Ge/MS Semi -Volatiles - - - - - - - - - - - -
1 OF 3
RESULT REPORTING EXTRACTION-QC
PARAMETER (ug/Ll LIMIT METHOD ANALYSIS DATE BATCH
Acenaphthene ND 10 SW846 8270A 12/23 -12/29 /94 4357101
Acenaphthylene ND 10 SW846 8270A 12 /23 -12 /29 /94 4357l0l
Benzo(a)anthracene ND 10 SW846 8270A 12/23-12/29/94 4357101
Benzo(b)fluoranthene ND 10 SW846 8270A 12/23-12/29 /94 4357101
Benzo(k)fluoranthene ND 10 SW846 8270A 12/23-12/29/94 4357101
Benzo(ghi)perylene ND 10 SW846 8270A 12/23-12/29/94 4357101
bis(2-chloroethoxy)methane ND 10 SW846 8270A 12/23-12/29/94 4357101
bis(2-chloroethyl)ether ND 10 SW846 8270A 12 /23 -12 /29 /94 4357101
bis(2-ethylhexyl)phthalate ND 10 SW846 8270A 12 /23 -12 /29 /94 4357101
4-Bromophenyl phenyl ether ND 10 SWB46 8270A 12/23-12/29/S4 4357101
Butyl ben•yl phthalate ND 10 SW846 8270A 12/23-12/29/94 4357101
4~Chloroani1ine ND 10 SW846 8270A 12/23-12/29/94 4357101
4-Chloro-3-methylphenol ND 10 SW846 8270A 12/23 -12 /29 /94 4357101
2-Chloronaphthalene ND 10 SW846 8270A 12/23-12/29/94 4357101
2-Chlorophenol ND 10 SW846 8270A 12/23-12/29/94 4357101
4-Chlorophenyl phenyl ether ND 10 SW846 8270A 12/23 -12/29 /94 4357101
Chrysene ND 10 SW846 8270A 12/23-12/29/94 4357101
Dibenz(a,h)anthracene ND 10 SWS46 8270A 12/23-12/29/94 4357101
Dibenzofuran ND 10 SW846 8270A 12/23-12/29/94 4357101
Di-n-butyl phthalate ND 10 SW846 8270A 12/23-12/29/94 4357101
l,2-Dichlorobenzene ND 10 SW846 8270A 12/23-12/29/94 4357101
1,3-Dichlorobenzene ND 10 SW846 8270A 12/23-12/29/94 4357101
1,4-Dichlorobenzene ND 10 SW846 8270A 12/23-12/29/94 4357101
SURROGATE RECOVERY i ACCEPTABLE LIMITS
NitrobenzenewdS 80 26 131)
2-Fluorobiphenyl 83 27 119)
Terphenyl -dl4 95 10 165)
2-Fluorophenol 21 10 116)
Phenol-d5 58 10 175)
2,4,6-Tribromophenol 2t J.0 155)
NOTE; AS R.IOC EJVF.J)
Nl> NOT DETF...Crl<:l> AT THE STA'l'l~n IU~PORTING LlMIT
RUST EllVIRO~NT & INFRl>.STRUCT
WO #: AlXTClOR
L,l\E #: B4L210036·005
MATRIX: WATER
MW-8
DATE SAMPLED:
DATE RECEIVED:
12/20/94
12/2l/94
- - - - - - - - - - - - - - - - -GC/1'!S Semi-Volatiles - - - --- - - - - - -
PARAMETER
Benzo(a)pyrene
3,3'-Dichlorobenzidine
Anthracene
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
Di-n-octyl phthalate
4,6-Dinitro-
2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluorant.hene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
SURROGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
2-Fluorophenol
Phenol-d5
2,4 1 6-Tribrornophenol
Nc)·n~ AS RECF.JVr;;u
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
80
83
95
21
58
21
ND NO'f Ol~TBCTED AT 'flll::~TATED REPOltTIJ'llG LIMIT
2 OF 3
REPORTING
LIMIT
10
50
10
10
10
10
10
10
50
50
10
10
10
10
10
10
10
10
10
10
10
10
10
METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWS46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26
27
10
10
10
10
131)
119)
165)
116)
175)
155)
EXTRACTION-QC
ANALYSlS DATE BATCH
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23·12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23"12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23"12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXTCl-OR
LAB #: B4L2l0036-005
ldATRIX: WATER
DATE SAMl?LED:
DATE RECEIVED:
12/20/94
12/"11/94
- - - --- - --- - - --- --GC/MS Semi-Volatiles - - - - - - - - ----
PARAMETER
Naphthalene
2-Nitroaniline
3rNitroaniline
4-Nitroaniline
Nitrcbenzene
2-Nitrophenol
4 -Ni t:<ophenol
N-Nitrosodi-n-propylamine
N~Nitrosodiphsnylaroine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5·T~ichlorophenol
2,4,6-Trichlorophenol
bis(2-chloroisopropyl)ether
SURROGATE RECOVERY
Nitrobenzene-dS
2-Fluorobiphenyl
Terpheny1-d14
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
NOTE; AB lU<:CFJVF.J)
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
80
83
95
21
58
21
ND NOT DETEC'J'gl) A"l' 'fHE STAT~I) Rl<:l'ORTING Lll\11.IT
3 OF 3
REPORTING
LIMIT
10
50
50
50
10
10
50
10
)_ 0
50
10
10
10
10
10
10
10
)'!ETHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWS46 8270A
SWS46 8270A
SWB46 8270A
SW846 82701'
SWB46 82701'
SW846 8270A
SWB46 8270A
SW846 8270A
SWB46 82701'
SW846 82701'
SW846 82701'
SW846 82701'
ACCEPTABLE LIMITS
26 131)
27 119)
10 165)
lO ll6)
10 175)
10 155)
E:XTRACTION-
l>NJ>,LYSIS Dl>TE
12/23-l2/29/94
12/23-l2/29/94
12/23-U/29/94
12/23-l2/29/94
l-2/23-12/29/94
12/23-12/29/94
12/23·12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-n/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
QC
BATCH
4357101
4357101
435710l
4357l01
4357101
4357101
4357101
4357101
4357101
4357l01
4357101
4357;!_01
435710).
4357101
4357l01
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXTC
LAB #: B4L210036-005
MATRIX: WATER
MW-8
DATE SAMPLED:
DATE RECEIVED:
12/20/94
12/21/94
· · · - - - -· · · -REQUESTED METALS - - - --· - - - - - - -· -
PARAMETER
Silver
Aluminum
Barium
Beryllium
Calcium
Cadmium
Cobalt
Chromium
Copper
I:ron
l?otaaaium
Magnesium
Manganese
Sodium
Nickel
Antimony
Vanadium
Zinc
Arsenic
Lead
Me:r:cury
Selenium
Thallium
NOTI'.,.! AS RECF.JVf:.U
RESULT
ND
117,000
863
l.5 J
121,000
ND
175
1,140
1,130
195,000
15,500
119,000
4.850
69,100
353
ND
450
249
2.0 J
11.5
0.30
ND
ND
REPORTING
LIMIT
10_0
100
10.0
2.0
500
s_o
10.0
10.0
10.0
100
5,000
500
10.0
5,000
40.0
50.0
10,0
20.0
s.o
s.o
0.20
10.0
lO_Q
ND NOT DE"l'l~l'ED AT THES1'A'l'ED REPOR'flNG J.J.MIT
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
u1;1/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
J F.STIMAl'l-~I,) VALUE. {l)E.Tt;c·l'r~n). BUT BF..LOW QUANTITATION LIMl'f.
METHOD
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
8W846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW646 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 7060
SW846 7421
SW846 7470
SW846 7740
SW846 7841
PREPARATION -
ANALYSIS DATE
12/28-12/29/94
12/28-12/29/94
12/28-12/29 /94
12/28-12/29 /94
12/28·12/29/94
12/28-12/29/94
12/28-12/29 /94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29 /94
12/28-12/29/94
12/28·12/29 /94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28/94
12/27/94
12/28-12/29/94
12/28/94
QC
BATCH
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4360022
4362073
4362073
RUST ENVIRONMENT & INFRASTRUCT
WO # : JUXTC
LAB #: B4L210036-005
MATRIX: WATER
- - - - - - -
P~TER
Turbidity
Cyanide, Total
NOTE. AS RECEIVED
- -
MW-8
- - - -INORGANIC ANALYTICAL
REPORTING
RESULT LI!HT UNIT
1,600 25.0 NTU
ND 0.010 mg/L
ND NOT DETECTED AT TI-fE SLA'tfb Rl1l'Olrl"ING J..iMIT
REPORT --
DATE SAMPLED:
DATE RECEIVED:
-- - - - - - -
12/20/94
12/21/94
PREPARATION QC
METHOD ANALYSIS DATE BATCH
MCAWW 180.1 12/21/94 4356088
SW846 9010A 1/03/95 5003104
RUST ENVIROl'IMENT & INFRASTRUCT
MW-9
WO #: AlXTElOQ DATE S~FLED: 12/20/94
12/21/94 LAB #: B4L210036-006
MATRIX: WATER
DATE RECEIVED:
- - --- - - - - - - - - - - - --GC/MS Vela tiles - - - - - - -
2 01' 2
RESULT REPORTING
PARAMETER (ug/L) LIMIT METHOD
2-Butanone
1,2-Dichloropropane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
vinyl chloride
Xylenes, Total
cia-1,2-Dichloroethene
Vinyl acetate
SURROGATE RECOVERY
1,2-Dichloroethane-d4
Toluene-dB
Bromof luorobenzene
NOTE: AS RECEIVED
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
99
101
100
ND NOT DETECTED AT THE STATED REPORTING LIMIT
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
81
130)
109)
117)
E:XTRACTION-
ANALYSIS DATE
12/29/94
12/29/94
12/29/94
12 /29 /94
12 /29 /94
U/29/94
12/29/94
12/29/94
12/29/94
12/29/94
lZ/29/94
QC
BATCH
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXTElOR
LNl #: B4L210036-006
MATRIX: WATER
MW-9
PATE SAMPLEP:
PATE RECEIVEP:
12/20/94
12/21/94
- ---- --- ---- ---- -GC/MS Semi-Volatiles -- --- -------
PbRAMETER
Acenapnchene
Acenapnthylene
Benzo(a)anthracene
Benzo(b)fluorantnene
Benzo(K)fluorantnene
Benzo(9ni)perylene
bis(2·chloroethoxy)rnethane
bis(2-chloroethyl)ether
bis(2-ethylhexyl)phthalate
4-Brornophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
4-Chloro-3-rnethylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenz{a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4~Dichlorobenzene
SURROGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
Terpnenyl-dl4
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
NOTl!l AS RECEJVfill
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
74
78
113
30
41
26
Nn NOT DETI::.CTF.D AT Tllli ::iTATED REPORTING LIMIT
l OF 3
REPORTING
Ll))[IT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J)[ETHQD
SW846 8270A
SW846 8270A
SW846 8270A
SWB46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWM6 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 B270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26
27
10
10
10
10
l31)
119)
165)
116)
175)
155)
EXTAACTION· QC
ANALYSIS DATE BATCH
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
l2/23·l2/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
l2/23·12/29/94 4357l01
12/23-12/29/94 4357101
12/23-l2/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #: )UXTElOR
LAB #: E4L210036·006
MATRIX: WATER
MW-9
DATE SAMPLED:
DATE RECEIVED:
12/20/94
12/21/94
- - - - - - - ----- --- - -GC/MS Semi-Volatiles - - - - --- -----
PARAME:TER
Eenzo(a)pyrene
3,3'-Dichlorobenzidine
Arlthracene
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
Di-n-octyl phthalate
4,6-Dinitro-
2-methylphenol
2,4~Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Meehylphenol
4-Methylphenol
SURROGATE RECOVERY
Nitrobenzene~d5
2-Fluorobiphenyl
Terphenyl-dl4
2-Fluorophenol
Phenol-d5
2 1 4,6-Tribromophenol
NOTE: AS R.l~l;:lVF.J'.J
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
74
78
113
30
41
26
ND NOT DETECTED J\T Tiff.. STATED REPORT.l.NG LrMIT
2 OF 3
REPOR'UNG
LildIT
10
50
10
10
10
10
10
10
50
50
10
10
10
10
10
10
10
10
10
10
10
10
10
METHOD
SWB46 8270A
SW846 8270A
SWB46 8270A
SW8H 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWB46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 B270A
SW846 8270A
ACCEPTABLE LIMITS
26
27
10
10
10
10
131)
119)
165)
116)
175)
155)
EXTRACTION-QC
ANALYSIS DATE !lliIQ!
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23'12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRO"™ENT & INFRASTRUCT
WO #' AlXTElOR
LAfl #: S4L210036-006
!dATRIX: WATER
DATE SAMPLED:
DATE ;<ECEIVED:
12/20/94
12/21/94
- - - -· - - - - - - - - - - --GC/MS Semi-Volatiles --- - - - - - - - - -
PARAMETER
Naphchalene
2-Nitroa;niline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanth:rene
Phenol
Pyre:ne
l,2,4~Trichlorobenzene
2,4,SwTrichlorophenol
2,4,6-Trichlorophenol
bis(2-chloroieopropyl)ether
SURROGATE RECOVERY
Nitrobenzene-ds
2-Fluorobiphenyl
Terphenyl·d14
2-Fluorophenol
Phenol-dS
2,4 1 6-Tribrorncphenol
NOTE: AS RECEJ.VfJ)
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
74
78
113
30
41
26
ND NOT OETECTl!:h AT THE S'fATED ltl<:.l'•ORTING tlMI'I'
3 OF 3
REPORTING
LIMIT
10
50
50
50
10
10
50
10
10
50
10
10
10
10
10
10
10
METHOD
SW846 8270A
SWS46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWS46 8270A
SWB46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWSH 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26 131)
27 119)
J_ 0 165)
10 116)
10 175)
10 155)
EXTRACTION-QC
ANAJ:.YSIS DATE BATCH
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357l01
12/23-12/29/94 4357101
l2/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357l0l
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXTE
L1'B #: B4L210036-006
MATRIX: WATER
PATE SAM:PLED:
DATE RECEIVED:
12/20/94
12/2l/94
- - -• - - -• - - -REQUESTED METALS • -- -• - -• • - - -• - -
PARAMETER
Silver
Alwninwn
Barium
Beryllium
Ca.lciwn.
Cadmium
Cobalt
chromium
copper
'Iron
Potassium
Magnesium
Manganese
Sodiwn
Nickel
Antimony
vanadium
Zinc
Arsenic
Lead
Mercury
Selenium
Thallium
N()TF....; AS RECJ1JWD
RESULT
ND
213
6.0 J
ND
23,300
ND
ND
ND
ND
459
2,370 J
17,000
313
13,600
ND
ND
ND
ND
ND
ND
ND
ND
ND
REPORTING
LIMIT
10.0
lOO
10.0
2.0
500
5.0
10.0
10.0
10.0
100
5,000
500
10.0
5,000
40.0
50.0
10.0
20.0
5.0
5.0
0.20
5.0
5.0
ND NOT nf.;ff..CTED AT Tllli8TAi1ID REPORllN<~ LfMIT
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 E5TIMA.'l''l<'D VALUE. (DETl£(:·1'ED). ntrr BEJ.,()W QUANTITATJON 11MIT.
METliQD
SW84'6 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 60'tOA
SW846 60l0A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 7060
SW846 7421
SW846 7470
SW846 7740
SW846 78"1
PREPARATION -
ANALYSIS DATE
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29 /94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/H
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28/94
12/27/94
12/28-12/29/94
12/28/94
QC
BATCli
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
B62073
4362073
4362073
4362073
4362073
4362073
4360022
4362073
4362073
RUST ENVIRONMENT & INF~S'l'RUCT
WO #: AlXTE
L.i<B #: B4L210036-006
MATRlX: WATER
-- -----
PARAMETER
Turbidity
Cyanide, Total
NOTf.;. AS RECE.lVED
--
MW'-9
----INORGANIC ANALYTICAL
REPORTING
RESULT LIMIT UNIT
17.0 0.50 NTU
ND 0.010 mg/L
ND NOT DETECTED AT THE STATED REl'ORTINO LlM"fT
REPORT " -
DATE S.llMPLED:
DATE RECEIVED:
----- ---
12/20/94
12/21/94
PREPARATION QC
METH OP ANALYSIS DATE BATCll
MCAWW 160.1 12/21/94 4356088
SWB46 9010A 1/03/95 5003104
RUST ENVIRONMENT & INFRl'STRUCT
WO #: AlXTGlOQ
LAB #: B4L210036-007
MATRIX: WATER
MW-10
DATE S.l\MJ!l'..ED :
DATE RECEIVED:
12/20/94
12/21/94
- - - - - -. ----- - - - - --GC/MS Vol a tiles ---- - - ------- -
PARAMETER
Acetone
Benzene
Brornodichloromethane
l!romof o:on
B:romomethane
Carbon disulfide
Carbon tetrachloride
Ch1orobenzene
Oibromochlorornethane
Chloroethan€
Chloroform
Chloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2~Hexanone
Methylene chloride
4-Methyl-2-pentanone
Styrene
l,l,2,2~Tetrachloroethane
SURROGATE RECOVERY
1,2-Dichloroethane~d~
Toluene-dB
Bromofluorobenzene
N<)l"1'""..! AS RF..CF.JVED
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
101
103
98
ND NCYf oi:.:rt:Cl'l<"'l) AT l'HF.. STATF.J) REPORTING LIMIT
1 OF 2
REPORTING
LIMIT
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
METHOD
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A,
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
81
130)
109)
117)
EXTRACTION-QC
ANALYSIS DATE BATCH
12/29"12/30/94 4364034
12/29-12/30/94 4364034
12/29"12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
,-
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXTGlOQ
LAB #: B4L2l0036-007
MATRIX: WATER
MW-10
PATE S.llMPLEP:
PATE RECEIVED:
12/20/94
12/21/94
- - - - - --- - - - - - - - - - -GC/MS Volatiles - - - - - - - - - - - - --
PAAJ\METER
2-Butanone
1,2-Dichloropropane
Tetrachloroethene
Toluene
l,l,1-Trichloroethane
l,112-Trichloroethane
Trichl.oroethene
Vinyl chloride
Xylenes, Total
cis-l,2~Dichlo~o€thene
Vinyl acetate
SURROG.1'.TE RECOVERY
l,2-Dichloroethane-d4
Toluene-dB
Brornofluorobenzene
NOT~ A.$ R.F..CF.IVED
RESULT
!ug/Ll
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
101
103
98
ND NOT Dh"TE<.~'n;'.l) AT 111E ~l'Al'F.D REPO&'flNG LIMIT
2 OF 2
REPORTING
LIMIT
10
5.0
5_0
5.0
5.0
5.0
5_0
5.0
s.o
5.0
10
METllOD
SW846 B240A
SWB46 B240A
SWB46 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWB46 8240A
SWB46 8240A
SWB46 8240.1'.
SW846 8240A
SW846 8240.1'.
ACCEPTABLE LIMITS
78 130)
90 109)
Bl 117)
EXTRACTION-QC
ANALYSIS DATE BATCH
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
WO #: AlXTGlQR
LAB #: B4L210036-007
Ml\TRIX: WATER
PARAMETER
Acenaphthene
Acenaphthylene
Ben•o(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(ghi)perylene
bis(2·chloroethoxy)methane
bis(2·chloroethyl)ether
bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
l,2-Dichlorobenzene
l.3~Dichlorobenzene
114~Dich1orobenzene
SURROGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dl4
2-Fluorophenol
Phenol·dS
2,4,6-Tribromophenol
NOTE~ AS RECEJVF.J)
RUST ENVIRONMENT & INFRASTRUCT
MW-10
DATE SAMPLED: 12/20/94
12/21/94 DATE RECEIVED:
- -GC/MS Semi-Volatiles
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
50
54
41
53
41
61
1 OF 3
REPORTING
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWS46 S270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26
27
10
10
10
10
131)
11~)
165)
116)
175)
155)
EXTRACTION-
ANALYSIS DATE
12/23·12 /29 /94
12/23-12/29/94
12/23-12/29/94
12/23"12 /29 /94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23 -12 /29 /S4
12/23-12/29/94
12/23-12/29/~4
12/23-12/29/94
12 /23 -12 /29 /94
12/23 -12/29 /94
12/23-12/29/94
12/23-12/29/94
12/23 -12/29 /94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
QC
BATCH
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
ND NOT DETF..c1·~-:n AT TllE STATED RF.PORTrNG l,rMrr
RUST ENVIROl'lMENT & INFRASTRUCT
WO #: AlXTGlOR
I.JIB #: B4L2l0036-007
MATRIX: WATER
MW-H
DATE SAMPLED:
DATE RECEIVED:
12/20/94
1-2/21/94
---- - --· - - --· - - - -GC/MS Semi-Volatiles - ---- ---- - --
PARAMETER
8enzo(a)pyrene
3 1 3 1 -Dichlorobenziditle
AAthracene
2,4-Dichlorophenol
Diethyl phthalate
2,4-Diroethylphenol
Dimethyl phthalate
Di-n-octyl phthalate
4,6~Dinitro-
2-methylphenol
2,4-Dinicrophenol
2,4~Dinitrotoluene
2 1 ~-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlo~obenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone
2-l1ethylnaphthalene
2-Methylphenol
4-Methylphenol
SURROGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-dH
2-Fluorophenol
Phenol-d5
214 1 6-Trib~omophenol
NOTE: AS Rl!X~l?,lVFD
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
50
54
41
53
41
61
ND NOT DJ~rt<"..CIF.D AT Tiffi STAT~U R'f..l'(>RTING LlMl'l'
2 OF 3
REPORTING
LIMIT
10
50
10
10
10
10
10
10
50
50
10
10
10
10
10
10
10
10
10
10
10
10
10
METHOD
SW846 8270A
SW8'16 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWS46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26
27
10
10
10
10
l31)
119)
165)
ll.6)
175)
155)
EXTRACTION-QC
ANALYSIS DATE BATCH
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
WO #: A1XTG10R
LAB #: B4L210036-007
MATRIX: WATER
PARAMETER
Naphthalene
:2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4 -Nitrophenol
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylrunine
Pentach1orophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
bis(2-chloroisopropyl)ether
SURROGATE RECOVERY
Nit:robenzene-d5
2-Fluorobiphenyl
Terpnenyl-d14
2 -Fluorophenol
Pl1enol-d5
2,4,6-Tribromopnenol
NOTE: /\.S Rl::.CflVF.D
RUST ENVIRONMENT & INFRASTRUCT
MW·lO
DATE SAMPLED: 12/20/94
12/21/9~ DATE RECEIVED:
- -GC/MS Semi-Volatiles
3 OF 3
RESULT REPORTlNG
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
50
54
41
53
41
61
10
50
50
so
10
10
50
10
10
50
10
10
10
10
10
10
10
LlMlT METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWM6 8270A
SW846 8270A
SWB46 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26 131)
27 119)
10 165)
10 116)
10 175)
10 155)
EXTRACTION-
ANALYSlS DATE
QC
BATCH
12/23-12/29/94 4357101
12/23·12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
NU t'il<)"f fJETF..CTF..D AT THE ST1\'n~o U.f<~'P<)RTING LThfiT
RUST ENVIRONMENT & INFl<ASTRUCT
WO #: .1<1XTG
LAB #: B4L210036·007
MATRIX: WJ<TER
MW-10
DATE SAMPLED:
DATE RECEIVED;
12/20/94
12/21/94
- - - - - - - - - - -REQUESTED METALS - - - - - - - -· - -· - - -
PJ.Ul.AMETER
Silver
Aluminu:m
Barium
Beryllium
Calciwn
Cadmium
Cobalt
Chromium
Copper
I:ron
Potassium
Magnesium
Manganese
Sodium
Nickel
Antimony
Vanadium
Zinc
Arsenic
Lead
Mercury
Selenium
Thallium
NOl'F...:; AB RECl:JVF.D
RESULT
ND
6,190
35.3
ND
25,700
ND
ND
8.5 J
7.7 J
4,690
1,640 J
13,900
78 ,6
13,700
ND
ND
11.4
6.1 J
ND
4.4 J
ND
ND
ND
REPORTING
LIMIT
10.0
100
10.0
2.0
500
5.0
10.0
10.0
10.0
100
5,000
500
10.0
5,000
40.0
50.0
10.0
20.0
5.0
5.0
0.20
5.0
5.0
ND NOT I)).::l'ECTED A 1" llfli: ST A 1'J~) RF..PORTlNG lJMIT
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/J:,
ug/L
ug/L
ug/L
ug/I>
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 ESTll\11'.ATF..D VALlJI•;. (OF..TECTEU). nUT BF.LOW QUANTITA"l'lON LIM.l"f.
METHOD
SW846 6010.1<
SW846 6010A
SW846 6010A
SW846 6010.1<
SW846 6010A
SW846 6010.1<
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010.1<
SW846 6010A
SW846 6010A
SW846 7060
SW846 H2l
SW846 7470
SW846 7740
SW846 7841
PREPARATION -
J<NALYSlS DATE
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28 -12/29 /94
12/28-12/29/94
12/28-12/29/94
12/28-12/29 /94
l.2/28-12/29 /94
12/28/94
12/28/94
12/27 /94
12/28-l-2/2$1/94
12/28/94
QC
BATCH
4362073
4362073
4362073
'1362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4360022
4362073
4362073
RUST ENVIRO!ndENT & INFRASTRUCT
WO #: AlXTG
L.AB #: B4L2l0036-007
MATRIX: WATER
- -" -. --
PARAMETER
Turbidity
Cyanide, Total
NO'fF.n AS RECEIVJ:~:O
--
MW-lO
" - --INORGANIC ANALY'l'ICAL
REPORTING
RESULT LIMIT UNIT
125 2.5 NTU
ND 0.010 mg/L
ND NOT DETECTED AT IBE SIA TED REPORTING LIWT
REPOR'l' --
DATE SAMPLED:
DA'l'E RECEIVED:
---- -- --
12/20/94
12/2l-/94
PREPARATION QC
METHOD ANALYSIS DATE BATC!l
MCAWW 180.1 12/21/94 4356088
SWS46 9010A 1/03/95 5003l04
RUST ENVIRONMENT & INFRASTRUCT
WO # : AlXTKl OQ
LAB #: B4L210036·008
MATRIX: WATER
PARAMETER
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Dibromochloromethane
Chloroethane
Chloroform
Chlorornethane
1,1-Dichlo~oethane
1,2-Dichloroethane
1.1-Dichloroethene
cis-1,3-Dichloropropene
trans-1,3-Dichlo~opropene
Ethylbenzene
2-Hexanone
Methylene chloride
4-Methyl-2-pentanone
Styrene
l11,2,2~Tetrach1oroethane
MW-B
- - -GC/MS Volatiles
1 OF 2
RESULT REPORTING
(ug/L)
ND
ND
ND
ND
ND
ND
ND
1.6 J
ND
ND
ND
ND
5.0
ND
2.4 J
ND
ND
ND
ND
ND
ND
ND
ND
LIMIT
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
DATE SAMPLED'
DATE RECEIVED,
12/20/94
12/21/94
METHOD
SW846 8240A
SW846 S:240A
SW846 824.0A
SW846 8240A
SW846 8240A
SW846 8240A
SWS46 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWS46 8240A
SWS46 8240A
SW846 8240A
SW846 8240A
SW846 8240A
EXTRACTION -
ANALYSIS DATE
QC
BATCH
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29·12/30/94 4364034
12/29-12/30/94 4.364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
SURROGATE RECOVERY ACCEPTABLE LIMITS
l,2-Dichloroethane-d4
Toluene-d8
Bromofluorobenzene
N01'& A,$ R.l'.i(.':EJ:VED
n
100
98
NO NOT DETECTF.D A'l' THJi: $TATJ.ID REPORTING LIMIT
J ESTIMATED VALUJ<"~ (U1£:TECTED). BUf BE.LOW QUANTli'Al'ION LIMlT.
78
90
81
130)
109)
117)
RUST ENVIRO!<IMENT & INFRASTRUCT
WO #: AlXTKlOQ
LAB #: B4L210036-008
MATRIX: WATER
MW-13
DATE SAMPLED:
DATE RECEIVED:
12/20/94
12 /2l/94
- - - - - - - - - - - - - -· - - -GC/MS Volatiles - - - - --- - - - - - - -
PARAMETER
2-Butanone
1,2-Dichloropropane
Tetrachloroethene
Toluene
l,l,l-Trichloroethane
1,1 1 2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
cis-1,2-Dichlo~oethene
Vinyl acetate
SURROGATE RECOVERY
l,2-0ichloroethane-d4
Toluene-dB
Bromofluorobenzene
NOli':.: AS Rf..CtlVEO
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
3.2 J
2.2 J
ND
16
ND
1
98
100
98
NI) NOT Df..TF..CTED AT THE STATED RE.PORTING LIJ\.11T
2 OF 2
REPORTING
LIMIT
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
s.o
10
METHOD
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWS46 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
81
130)
109)
117)
1;:s"I'IMA'J.'l<)) VALUE. (lJETF..Cl'F.D). BUT BELOW QUANTITATJON l,IMl"L
EXTRACTION-QC
ANALYSIS DATE BATCH
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29·12/30/94 4364034
12/29-12/30/94 4364034
RUST ENVIROW>IENT & INFRASTRUCT
WO #: AlXTKlOR
LAB #: B4L210036-008
MATRIX: WATER
MW-13
DATE SAMP:LED:
DATE RECEIVED:
12/20/94
12/21/94
- - - - - - - - - - - - - - - - -GC/MS Semi-Volatiles - - - - - - - - - - - -
1 OF 3
RESUL'l' REPORTING EXTRACTION· QC
PARAMETER (ug/:L) :LIMIT METHOD ANALXSIS DATE BATCH
Acenaphthene ND 10 SW846 8270A 12/23-12/29/94 4357101
Acenaphthylene ND 10 SW846 8270A 12/23-12/29/94 4357101
Bento(a)anthracene ND 10 SW846 8270A 12/23-12/29/94 4357101
Benzo(b)fluoranthene ND 10 SW846 8270A 12/23-12/29/94 4357101
Benzo(~)fluoranthene ND 10 SW846 8270A 12/23-12/29/94 4357101
Benzo(ghilperylene ND 10 SW846 8270A 12 /23 -12 /29 /94 4357101
bis(2-chloroechoxy)rnethane ND 10 SW846 8270A 12/23-12/29/94 4357101
bis(2-chloroethy1)ether ND 10 SW846 8270A 12/23-12/29/94 4357101
bis(2-ethylhexyl)phtha1ate 19 10 SW846 8270A 12/23-12/29/94 4357101
4-Bromophenyl phenyl ether ND 10 SW846 8270A 12/23-U/29/94 4357101
Butyl benzyl phthalate ND 10 SW846 8270A 12/23-12/29/94 4357101
4-Chloroaniline ND 10 SW846 8270A 12/23 -12/29 /94 4357101
4·Chloro-3-methylphenol ND 10 SW846 8270A 12/23·12/29/94 4357101
2-Chloronaphthalene ND 10 SW846 8270A 12/23-12/29/94 4357101
2-Chlorophenol ND 10 SW846 8270A 12 /23 -12 /29 /94 4357101
4-Chlorophenyl phenyl ether ND 10 SW846 8270A 12/23-12/29/94 4357101
Chrysene ND 10 SW846 8270A 12/23-12/29/94 4357101
Dibenz(a,h)anthracene ND 10 SW846 8270A 12/23-12/29/94 4357101
Dibenzofuran ND 10 SW846 8270A 12/23 -12/29 /94 4357101
Di-n-butyl phthalate ND 10 SW846 8270A 12/23-12/29/94 4357101
1,2-Dichlorobenzene ND 10 SW846 8270A 12/23-12/29/94 4357101
1,3-Dichlorobenzene ND 10 SW846 S270A 12/23 -12/29 /94 4357101
1,4-Dichlorobenzene ND 10 SWS46 8270A 12/23-12/29/94 4357101
SURROGATE RECOVERX !_ ACCEPTAB:LE :LIMITS
Nitrobenzene-ds 73 26 131)
2-Fluorobiphenyl 72 27 119)
Terph@nyl-dl4 90 10 165)
2 -Fl uorophenol 27 10 116)
Phenol-dS 51 10 175)
2,4 1 6-Tribromophenol 14 10 155)
NOTE: AS RF..CEIVl:;J)
ND NOT DETECTEn AT TlIESTATEn RJ~P()RTING l.fMl:'f
RUST ENVIRONME:NT & INFRASTRUCT
WO II: AlXTIClOR
LAB II: B4L210036·008
!dATRil!'.: WATER
MW-13
PATE SAMl'LEP:
DATE RECEJ:VEP:
12/20/94
12/21/94
-- ---- - - - - - --- - - -GC/MS Semi-Volatiles -- - - - - - - --- -
PARAMETER
Benzo(a)pyrene
3,3'-Dichlorobenzidine
Anth:cacene
2,4-Diohlorophenol
Diethyl pnthalate
2,4-Dimechylphenol
Dimethyl phthalate
Di-n-octyl phthalate
4,6-Dinitro-
2-mE!thyJ.phenoJ.
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyolopentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthal-ene
2-Methylphenol
4-Methylpnenol
SURROGATE RECOVERY
Nitrobenzene-dS
2-Fluorobiphenyl
Terphenyl·d14
2 -Fluoropnenol
Phenol-dS
2 1 4,6-Tribromophenol
NOTI~ J\S R.ECl~.D
RESULT
(uq/Ll
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NP
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
73
72
90
27
51
14
ND NO'I' OETECTl~O AT TUB $'1'ATE.J.) Rl~l'ORTING J .l"MIT
2 OF 3
REPORTING
LIMIT
10
50
10
10
10
10
10
10
50
50
10
10
10
10
10
10
10
10
10
10
10
10
10
METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SWB46 8270A
SWS46 8270A
SW846 8270A
SW846 B270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26
27
10
10
10
10
131)
119)
165)
116)
175)
155)
EXTRACTION·
ANALYSIS DATE
12/23-12/n/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12 /23 -12/29 /94
12/23"12/29/94
12/23-12/29/94
12 /23 -12/29 /94
12 /23 -12 /29 /9'1
12/23-12/29/94
12/23-12/29 /94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/29 /94
12/23-12/29/94
12/23-12/29/94
12/23-12/29/94
12/23-12/n/94
QC
BATCH
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357101
4357Hl
4357101
4357101
4357101
4357101
4357101
4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
RUST ENVIRONMENT & INFRASTRUCT
WO II• AlXTK
r.AB #' B4L210036-008
ldATRIX' WATER
MW-13
Il!l.TE SAMPLED '
DATE RECEIVED:
12/20/94
l2/2l/94
-· -· - -· -· -· REQUESTED METALS · -· - - - - - -· -· - -·
PARAMETER
Silver
Aluminum
Earium
Beryllium
Calcium
Cadmium
Cobalt
Chromillil\
Copper
Iron
Potassium
Magnesium
Manganese
Sodiwn
Nickel
Antimony
Vanadium
Zinc
Arsenic
Lead
Mercury
Selenium
Thallium
NOTE.? AS RECl!:l:VFJ)
RESULT
ND
4,710
128
ND
136,000
ND
14.1
41.7
20.8
6,900
6' 030
38,800
l, 960
34,500
21.0 J
ND
8.1 J
128
3.0 J
3.0 J
ND
ND
ND
REPORTING
LIMIT
10.0
100
10.0
2.0
500
5.0
10.0
10.0
10.0
100
5,000
500
10.0
5,000
40.0
50.0
10.0
20.0
5.0
s.o
0.20
5.0
5.0
ND NOl' l"JETECTJ::'D AT Tllli SIATE.D R.€.PORTING cmnT
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
J F.STIJ\1.A:I't.:J> VAJ...tJt<:.. (l)ETE<;Tt-"l)), BUT BELOW QUAN11T/\.1l0N LlJ\1.ff.
METHOD
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010!1.
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW8M 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW8'\\6 6010A
SW846 6010A
SW846 6010A
SW846 7060
SW846 7'\\;.ll
SW846 H70
SW8H 7740
SW846 7841
PREPARATION -
ANALYSIS DATE
12/28-12/29/94
1:2/28-12/29/94
12/28-12/29/94
l2/2s-12/n/9'>
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/:29 /94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29 /94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/20-12/n/94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28/94
12/27/94
12/28-12/29/94
12/28/94
QC
BATCH
4362073
4362073
4362073
4362073
4362073
4362073
4362073
'\\362073
4362073
'!362073
'\\362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4360022
4362073
4362073
RUST ENVIRONMENT & IN~RASTRUCT
WO #' AlXTK
LAB#' B4L2l0036-008
MATRIX' WATER
-------
PARAMETER
Turbidity
Cyanide, Total
NOTE: AS REC~IVED
--
MW-13
- -" -INORGANIC ANALYTICAL
REPORTING
RESULT LIMIT !lliIT
'l;6' 0 1.0 NTU
ND 0.010 mg/L
ND NOL OETECTED AT THE STA JED REPORTING UMTf
REPORT --
DATE SAMPLEO:
PATE RECEIVEO:
- ---- - --
12/2on4
12/21/94
PREPARATION QC
METHOO ANALYSIS DATE BATCH
MCAWW 180.l 12/21/94 4356088
SW846 9010A 1/03/95 5003104
RUST ENVIRONMENT ~ lNFRASTRuCT
WO #: AlXTMlOQ
LAE #: B4L210036·009
MATRIX: WATER
MW-16
Dl\.TE Sl\.MPLED:
Dl\.TE RECEIVED:
12/20/94
12/2l/S4
- - - - - - - - - - - -· - - - - -GC/MS Volatiles - - - - - - - - - - - - - -
PARAMETER
Acetone
Benzene
Bromodichloromethane
Brornoform
Brornomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Dibromochloromethane
Chloi::oethane
Chloi::of orm
Chloi::ornethane
l,lnDichloroethane
l,2-Dichloroethane
l,1-Dich1oroethene
cis~l,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2uHexanone
Methylene chloi::ide
4-Methyl-2-pentanone
Styrene
1,l,2,2-Tetrachloroethane
SURROGATE RECOVERY
l,2-Dichloi::oethane-d4
Toluene-de
Bromcfluorobenzene
NOTE; A.$ RECF.JVEI)
RESUL'l'
(uq/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
102
104
SS
NI) NOT Dh""l'l::c·rr.n AT THE 8TA 'fF..D REPOR'l'fNG LII'vllT
1 OF 2
REPORTING
LIMIT
10
5_0
5_0
5.0
10
5_0
5.0
5.0
5_0
10
5_0
10
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
METHOD
SWB46 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWB46 8240A
SWB46 8240A
SWB46 8240A
SW846 8240A
SW846 8240A
SWSH 8240A
SW8'.16 92401'
SW846 8240A
SW8'<6 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
81
130)
109)
117)
EXTRACTION-QC
ANALYSIS DATE BATCH
12/29-12/30/94 4364034
12/29-12/30/94 436403'<
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29"12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 436'<034
12/29-12/30/94 4364034
12/29-12/30/S4 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/S4 4364034
12/29-12/30/S4 4364034
l2/2S-12/30/94 '<364034
l2/2S-12/30/94 '<36403'<
l2/2S-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 '<364034
l2/2S-12/30/94 4364034
12/2S-l2/30/94 4364034
l2/2S-12/30/94 4364034
RUST E>IVIROm.IENT & INFRASTRUCT
WO #: ;nXTMlOQ
LAB #: B4L210036-009
MATRIX: WATER
MW-16
PATE SAMPLEP:
DATE RECEIVED:
12/20/94
12/21/94
- - - - - - - - - - - - - - - - -· GC/MS Volatiles - - -· - -· - -· - - - -
PARAMETER
2-Butanone
l,2-Dichloropropane
Tetrachloroethene
Toluene
l,l,1-Trichloroethane
l,1,2-Trichloroechane
Trichloroethene
vinyl chloride
Xylenes, Total
cie-1,2-Dichloroethene
vinyl acetate
SURROGATE RECOVERY
1,2-Dichloroethane-d4
Toluene-dB
Bromofluorobenzene
NOTf.: AS RECl'.lVF..D
RESULT
(ug/L)
ND
ND
ND
ND
NP
ND
1.3 J
ND
ND
2. 3 J
ND
102
104
99
ND NOT OETECTED Al' 1'HE STATJ'tl) RF..POR'l'lNG LIMIT
2 OF 2
REPORTING
LIMIT
10
5_0
5_0
5.0
5.0
5.0
s.o
5.0
5.0
5.0
10
METH OP
SW846 8240A
SW846 8240A
SWS46 8240A
SW846 S240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
ACCEPTABLE LIMITS
78
90
81
130)
109)
H7)
ESTIJ\!l.l\'ff..D V ALU& (flETECTED). 8UT BELOW QUANTITA'I'lON LIMI'f,
EXTRl<CTION-
ANALYSlS PATE
12/29-12/30/94
12/29-12/30/94
12/29-12/30/94
l2/29-l2/30/94
12/29-12/30/94
12/29-12/30/94
12/29-12/30/94
l2 /29-12/30/94
12/29-12/30/94
QC
BATCH
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
RUST ENVIRONMENT & INFRASTRUCT
WO #: AlXTMlOR
L!Ul #: B4L210036-009
MATRIX: WATER
MW-l6
DATE SAMl't.ED:
DA'J'E RECEIVED'
12/20/94
12/21/94
- - - - - - - - --- - - - - - -GC/MS Semi-Volatilea - - - - - - --- - - -
1 OF 3
RESULT REPORTING EXTRACTION-QC
PARAMETER {ug/L) Lii.UT METHOD ANALYSIS DATE BJ\.TCH
Acenaphthene ND 10 SWB46 B270A 12/23-12/29/94 4357101
Acenaphthylene ND 10 SWS46 8270A l.2/23-12/29/94 4357101
Benzo(a)anthracene ND 10 SW846 8270A 12/23-12/29/94 4357101
Benzo(b)fluoranthene ND 10 SW846 8270A 12/23-12/29/94 4357101
Benzo(k)fluoranthene ND 10 SWB46 827 OJI. 12/23-12/29/94 4357101
Benzo(ghi)perylene ND 10 SW846 8270A 12/23-12/29/94 4357101
bis(2-chloroethoxy)methane ND 10 SW846 8270A 12/23-12/29/94 4357101
bis(2-chloroethyl)ether ND 10 SWM6 8270A 12/23·12/2~/94 4357101
bis(2-ethylhexyl)phthalate ND 10 SW846 8270A 12 /23 -12 /29 N4 4357101
4-Brornophenyl phenyl ether ND 10 SW846 8270A 12/23-12/29/94 4357101
Butyl benzyl phthalate ND 10 SWB46 8270A 12/23-12/29/H 4357101
4-Chloroaniline ND 10 SW846 B270A 12/23-12/29/94 4357101
4-Chloro-3-rnethylphenol ND 10 SWS46 B270A 12/23-12/29/94 4357101
2-Chloronaphthalene ND 10 SWS46 8270)1. 12/23-12/29/94 4357101
2-Chlorophenol ND 10 SWS46 B270A 12/23-J.2/29/94 4357101
4-Chlorophenyl phenyl ether ND 10 SWS46 S270A 12/23-12/29/94 4357101
Ch:rysene ND 10 SWS46 S270A 12/23-12/29/94 4357101
Dibenz(a,h)anthracene ND 10 SWS46 S270A 12/23-12/29/94 4357101
Dibenzofuran ND 10 SW846 8270A 12/23-12/29/94 4357101
Di-n"butyl phchalate ND 10 SW846 8270)1. 12/23-lZ/29/94 4357101
l,2-Dichlorobenzene ND 10 SW846 8270A 12/23-12/29/94 4357101
l,3-Dichlorobenzene ND 10 SW846 8270A 12/23-12/29/94 4357101
l,4-Dichlorobenzene ND 10 SW846 8270)1. 12/23-12/29/94 4357101
SURROGATE RECOVERY i ACCEPTABLE LIMITS
Nitrobenzenerd5 86 26 131)
2-Fluorobiphenyl 87 27 119)
Te:<phenyl-d14 83 10 165)
2-Fluorophenol 66 10 116)
Phenol-as 56 10 175)
2,4,6-Tribromophenol 72 10 155)
NOTE; A$ RF...CEfVED
ND NOT 0ETEC1'F..D Al' Tiffi S'fATED RE.POJfflNG 1.JMIT
WO #' AlXTMlOR
LAB #' B4L210036-009
MATRIX: WATER
PARAMETER
Benzo(a)pyrene
3,3'-Dichlorobenzidine
Anthracene
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
Di-n-octyl phthalate
4,6-Dinitro-
2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyc1opentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
SURROGATE RECOVERY
Nitrobenzene-d5
2-Fluorobiphenyl
Terphenyl-d14
2-Fluorophenol
Phenol-dS
2,4,6-Tribromophenol
NOTE. AS Rf...CJ::Jvgn
RUST ENVIRONMENT & INFRASTRUCT
MW-16
DATE SAMPLED,
DATE RECEIVED,
12/20/94
12/21/94
--GC/MS Semi-Volatiles
RESULT
(uq/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
86
87
83
66
56
72
2 OF 3
REPORTING
LIMIT
10
50
10
10
10
10
10
10
50
50
10
10
10
10
10
10
10
10
10
10
10
10
10
MET!lOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270.A
SW846 8270.A
SW846 8270.A
SW846 8270.A
SW846 8270.A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270.A
SW846 8270.A
SW846 8270.A
SW846 8270.A
SW846 8270.A
SW846 8270.A
SW846 8270A
SW8'16 8 2 7 OA
SW846 8270.A
SW846 8270A
SW846 8270.A
.ACCEPTABLE LIMITS
26
27
10
10
10
10
131)
119)
165)
116)
175)
155)
EXTRACTION-
ANALYSIS DATE
QC
BATC!l
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
NU NOT l)h"'TECTED AT 1llE S'fATl~D l.f..~l"ORTING L[M]T
WO #: A1XTl:'JlOR
LJUI #: E4L210036-009
MATRIX: WATER
PARAMETER
Naphthalene
2-Nitroa.niline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2 -Ni trophenol
4-Nitrophenol
N-Nitrosodi-n~p~opylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
l,2,4~Trichlorobenzene
2,4,SrTrichlorophencl
2,4,6-Trichlorophenol
bis(2-ohloroisopropyl)ether
SURROGATE RECOVERY
Nitrobenzene-dS
2-Fluorobiphenyl
Terphenyl-d14
2 -Fluorophenol
Phenol-as
2,4,6-Tribromophenol
NOl'f..: AS RECEJVl:;Jl
RUST ENVIROl'IMENT & INFRASTRUCT
MW-16
DATE SAMPLED: 12/20/94
12/21/94 DATE RECEIVED:
· -GC/MS Semi-Volatiles
3 OF 3
RESULT REPORTING
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
86
87
83
66
56
72
10 so
50
50
10
10
50
10
10
50
10
10
10
10
10
10
10
LIMIT METHOD
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW846 8270A
SW8i\6 8270A
SW846 8270A
SW846 8270A
SW8i!6 B270A
SW8i!6 8270A
SW846 8270A
SW8i\6 B270A
SW846 8270A
SW846 8270A
SW846 8270A
ACCEPTABLE LIMITS
26 131)
27 119)
10 165)
10 116)
10 175)
10 155)
EXTRACTION-
ANALYSIS DATE
QC
BATCH
12/23-12/29/9'!; 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/9'!; 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23"12/29/94 4357101
12/23"12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
12/23·12/29/94 4357101
12/23-12/29/94 4357101
12/23-12/29/94 4357101
ND NOT DET~i::IF.D AT THE STA.TfJ) REPORTING .,rMIT
RUST ENVIRO~NT & INFRASTRUCT
WO #' AlXTM
LAB #: B4L210036-009
MATRIX, WATER
MW-H
PATE ,SAMPLEP:
DATE RECEIVED:
12/20/94
12/21/94
- -REQUESTEP ~TALS · · · · · - -
PARAMETER
Silver
Aluminum
Barium
Beryllium
calcium
cadmium
cobalt
Chro:nium
copper
Iron
Potassium
Magnesium
Manganese
Sodium
Nickel
Antimony
Vanadium
zinc
Arsenic
Lead
Mercury
Selenium
Thallium
NOTE: AS RECEIVED
RESULT
ND
374
42.S
ND
76.500
ND
ND
5.5 J
NP
608
2,750 J
14. 800
221
15,400
ND
ND
ND
ND
ND
l.8 J
ND
ND
ND
REPORTING
LIMIT UNIT
10.0 ug/L
100 ug/L
10.0 ug/L
2. 0 ug/L
500 ug/L
5.0 ug/L
10.0 ug/L
10.0 ug/L
10.0 ug/L
100 ug/L
5, 000 ug/L
500 ug/L
10.0 ug/L
5,000 ug/L
40.0 ug/L
50.0 ug/L
10.0 ug/L
20.0 ug/L
5. 0 ug/L
5.0 ug/L
0.20 ug/L
5. 0 ug/L
5. O ug/L
ND NOT DETECTED AT THE 8TATF..H ltgl'<'>R"fl:NG l~lMJT
J ESTIMATED VALUE. (DETECTF.D), nm' 8El,OW Ql.JAN'lTl'A'l'lON LfMli'.
METH OP
SWS46 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SWB46 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SwS46 6010A
SW846 6010A
SW846 6010A
SW846 7060
SW846 7421
SW846 7470
SW846 7740
SWB46 7841
PREPARATION -
ANALYSIS DATE
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12 /28 · 12 /29 /94
12/28-12/29/94
12/28-12 /29 /94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/:.l8·12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28/94
12/27/94
12/28-12/29/94
12/28/94
QC
BATCH
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4362073
4360022
4362073
4362073
RUST ENVIRONMENT & INFRASTRUCT
WO #: A1XTM
Ll'B #: B4L210036-009
MATRIX: WATER
. --. --.
l?AR.1\METER
Turbidity
Cyanide, Total
NOTE: AS RECElV£D
- -
MW-16
. - -. INORGANIC ANALYTICAL
REJ?ORTING
RESULT LIMIT UNIT
8.0 o.so NTU
ND 0.010 mg/L
ND NOT DETECTJ!D AT THE STATED RE.?ORTING LlrvtlT
REPORT -.
DATE SAMPLED:
DATE RECEIVED:
-. -----.
12/20/94
12/21/94
PREl?ARATION QC
MET!lOD ANALYSIS DATE BATCH
MCAWW 180.1 12/21/94 4356088
SW846 9010J'< 1/03/95 5003104
RUST ENVIRONMENT & INFR/<STRUCT
WO #: AlXTNlOQ
LAB #: B4L210036-010
!o!ATRIX: WJ<TER
MW·lO-c
Dl<TE SAMPLED:
DATE jl.ECElVED:
12/20/94
12/21/94
-· - - -· · - - -· - -· · - - -GC/MS Volatiles --· · - -· - - -· - -·
Pl<FJ\METER
Acetone:
Benzene
Bromodichloromethane
Bromof orm
Brornomethane
Carbon disulfide
Carbon tetrachlo~ide
Chlorobenzene
Dibromochloromethane
Chloroethane
Chloroform
Chloromethane
1,1~oichloroethane
l,2-Dichloroethane
1,1-Dichloroethene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
4-Methyl-2-pentanone
Styrene
l,1,2,2-Tetrachloroethane
SURROGATE RECOVERY
l,2-Dichloroethane~d4
Toluene-dB
Bromofluorobenzene
NOT1~ AS RF...CEIVBU
RESULT
(uq/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
100
102
101
NO NOT DETl!X:'l1ID AT THE Sl'/\'l'F.J) REPORTJN(• l.lMIT
1 OF 2
REPORTING
LIMIT
10
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
10
5.0
5.0
METHOD
SW846 8240A
SW846 8240A
SWM6 B240A
SW846 8240A
SWB46 8240A
SW846 8240A
SW846 8240A
SW846 B240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SW846 8240A
SWS46 8240A
SW846 8240A
SWB46 8240A
ACCEPTABLE LIMITS
78
90
81
130)
109)
117)
EXTRACTION-QC
ANALYSIS DATE BATCH
12/29·12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
RUST ENVIROl'IMENT & INFRASTRUCT
WO #' AlXTNlOQ
LAB #' B4L210036-010
MATRIX' WATER
MW-10-c
DATE SAMPLED:
DATE RECEIVED,
12/20/94
12/2l/94
--- ----- - - - - - - --- -GC/MS Volatiles - --- - - - - - - - - - -
PARAMETER
2-Butanone
1 1 2-Dichloropropane
Tetrach1oroethene
Toluene
1,1,l~Trichloroethane
l,l,2-Trichlo~oethane
Trichloroethene
Vinyl chloride
Xy1enes, Total
cis-l,2-Dichloroethene
Vinyl acetate
SURROGATE RECOVERY
l 1 2-Dich1oroethane-d4
Toluene-as
Brornofluorobenzene
NO'fE; AS RECElVl::n
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
100
102
101
ND NOT n1~rr:cTF.J) AT THE STATl~1) ltF...PORTING l.JMlT
2 OF 2
REPORTING
LIMIT
10
5.0
5.0
5.0
5_0
5.0
5.0
5.0
5.0
5.0
10
METHOD
SW846 82401'
SW846 82401'
SW846 8240!'\
SW846 8240A
SWM6 8240A
SW846 8240A
SW846 8240A
SW846 8240J<
SW846 8240A
SW846 8240A
SW846 8240A
J<CCEPTABLE LIMITS
78
90
81
130)
109)
117)
EXTAAC'rION-QC
ANALYSIS DATE BATCH
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
12/29-12/30/94 4364034
INTRA-LAB BLANK RE~ORT
LAB #: B4L300000-034
· · · - - - -· · · · - - - -· · · GC/MS Volatiles - - -
PARAMETER
1,1,2,2-Tetrachloroethane
Tetrach1oroethene
Toluene
1,1,1-Trichlo~oethane
111,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
Xylenes, Total
SURROGATE RECOVERY
l,2rDichloroethane~d4
Toluene-d8
Bromofluorobenzene
Nb (NONE DETECTED)
RESULT
(uq/Ll
ND
ND
ND
ND
ND
ND
ND
ND
ND
l
103
102
101
REPORTING
LIMIT
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
ACCEPTABLE LIMITS
( 78 130)
( 90 109)
( 81 117)
PREPARATION -
ANALYSlS DATE
12/n/94
J.2/29/:;>4
12/29/94
12/29/94
12/29/94
12/lS /94
12/29/94
12/29/94
l2/29/94
QC
BATCH
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
4364034
INTRA-LAB BLANK REPORT
LAB #• B4L300000-093
· · - - - - - - - - - - - - - - - -GC/MS Volatiles · · ·
PARAMETER
Acetone
Benzene
Bromodichloromethane
E:i::-omoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Dibrornochlorornethane
Chloroethane
Chloroform
Chlorornethane
1,1-Dichloroethane
1,2-Dichloroethane
l,l-Dich1oroethene
cis·l,2~Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene chloride
l11 1212-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
l,l,2-Trichloroethane
SURROGATE RECOVERY
l,2-Dichloroethane·d4
Toluene-dB
Bromofluorobenzene
NOTE;
ND (NON!i DETECTf:P)
RESULT
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1
101
103
99
REPORTING
LIMIT
10
l.O
1.0
1.0
1.0
1.0
1. 0
1. 0
1. 0
1.0
1. 0
1.0
1.0
1.0
1. 0
1.0
1.0
1.0
1.0
1.0
1.0
1. 0
1.0
1.0
1. 0
ACCEPTABLE LIMITS
( 78 l.30)
( 90 109)
( 81 117)
PREPARATION -
ANALYSIS DATE
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
12/30/94
l2/30/94
QC
BATCH
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
4364093
INTR.A-LAB BLANI< REPORT
LAB #' B4L230000-10l
- - - - - - - - - - - - - - - - -GC/MS Semi-Volatiles - -
RESULT REPORTING PREPAAATION QC
PARA.lfilTER {ug/L) Lll>[IT ANJ'.LYSIS DATE BATCH
Acenaphthene ND 10 12/23-12/28/94 435710).
Acenaphthylene ND 10 12/23-12/28/94 435710).
Anthracene ND 10 12/23-l-2/28/94 4357101
Benzc(a)anthracene ND 10 l2 /23 -12 /28 /94 4357101
Benzo(b)fluoranthene ND 10 12/23-12/28/94 435710).
Benzo(k)fluoranthene ND 10 l-2/23-12/28/94 4357101
Benzo(ghi)perylene ND 10 12/23-12/28/94 4357101
Benzo(a)pyrene ND 10 12/23-12/28/94 4357101
bis(2-chloroethoxy)rnethane ND 10 12/23-12/28/94 4357101
bis(2-ch1oroethyl)ether ND 10 12/23-12/28/94 435710).
bis(2-chloroisopropyl)ether ND 10 12/23-12/28/94 4357101
bis(2-ethylhexyl)phthalate ND 10 12/23-12/28/94 4357101
4-Brornophenyl phenyl ether ND 10 12/23-12/28/94 435710).
Butyl benzyl phthalate ND 10 12/23-12/28/94 4357101
4-Chloroaniline ND 10 12/23-12/28/94 4357101
4-Chloro-3-rnethylphenol ND 10 12/23-12/28/94 4357101
2-Chloronaphthalene ND 10 12/23-12/28/94 4357101
2-Chlorophenol ND 10 12/23-12/28/94 4357).01
4-Chlorophenyl phenyl ether' ND 10 12/23 -12/28/94 4357101
Chrysene ND 10 12/23-12/28/94 4357101
Dibenz(a,h)anthracene ND 10 12/23-12/28/94 4357101
Dibenzofuran ND 10 12/23-12/28/94 4357101
Di-n·butyl phthalate 44 10 12/23-12/28/94 4357101
l,2·Dichlorobenzene ND 10 l-2/23-12/28/94 4357101
l,3-Dichlo~obenzene ND 10 12/23-12/28/94 4357101
SURROGATE RECOVERY 1 ACCEPTJillLE LIMITS
Nitrobenzene-d5 63 26 131)
2-Fluorobiphenyl 58 27 119)
Terphenyl-d14 85 10 165)
2-Fluorophenol 55 10 116)
Phenol-d5 61 10 175)
2,4,6-Tribromophenol 74 10 155)
NOTE:
ND (NONE D~"l"ECTED)
LAB #: B4L210036
PARAMETER
Mercury
Silver
Aluminum
Arsenic
Barium
Beryllium
Calciwn
Cadmium
Cobalt
chromium
Copper
Iron
Potassium
Magnesium
Manganese
Sodium
Nickel
NOTE!
RESULT
ND
ND
ND
ND
ND
ND
35 .9 J
ND
ND
ND
ND
ND
ND
ND
ND
102 J
ND
INTRA-LAB BLANK REPORT
METALS • • - -• • -• • • -• • - -• • - - -
REPORTING
LIMIT
BATCH:4360022
0.20 ug/L
BATCII;4362073
10.0 ug/L
100 ug/L
5.0 ug/L
10.0
2.0
500
5.0
10.0
10.0
10.0
100
5,000
500
10.0
5,000
40.0
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
METHOD
SWS46 7470
SW846 6010A
SW846 6010A
SW846 7060
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW84;6 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 6010A
SW846 60lOA
SW846 6010A
PREPARATION
ANALYSIS DATE
12/27/94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28-12/n/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
l2/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/29-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28 -12/29 /94
12/28-12/29/94
ND NOT DEToCrED AT THE STATED REPORTING UMJ'f
lNTRA-LAB BLAl<K REPORT
LA:a #: B4L210036
METALS " --- ---- - - --• - - ---• -
REPORTING PREPARATION
PARAMETER RESULT LIMIT UNIT METHOD ANALYSIS DATE
BATCH:4362073
Lead 2.1 J 5.0 ug/L SWS46 7421 12/28/94
Antimony ND 50.0 ug/L SW846 6010A 12/28-12/n/94
Selenium ND 5.0 ug/L SW846 7740 12/28"12/29/94
Thallium ND 5.0 ug/L SW846 7841 12/28/94
Vanadium ND 10.0 ug/L SW846 6010A 12/28-12/29/94
zinc ND 20.0 ug/L SW846 6010A 12/28-12/29/94
NOTE.
ND NOT DETECll~D AT THE STATED REP'(JRTiNG Ul\fJT
INTRA-LAa llLANK REPORT
t.AB #' ll4L220000-088
· -· -· -· -· -· -· - -INORGANIC ANALYTICAL REPORT
PARAMETER
Turbidity
Cyanide
NOTE:
ND (NONI?: DETECIED)
ND
ND
RESUI.T
REPORTING
I.IMIT
0.50
0.010
UNIT
NTU
mg/L
PREPARATION -
ANALYSIS DATE
12/21/94
1/03/95
QC
llATCH
4356088
5003104
CHECK SJIMPLE REPORT
LAB #' B4L210036
METALS · --------. . -. . -. . . _ . .
SPrKE
PERCEN'l' Q/C PREPAll..l'<TION ·
COMPOUND RECOVERY LIMITS ANALYSIS DATE
BATCHo4360022
Mercut:y 97 (75-121) 12/27/94
EATCH:4362073
Si1ve:r 100 (84-113) 12/28-12/29/94
Aluminum 104 (83-117) l2/28-12/29/94
Arsenic 105 (77-118) 12/28/94
Barium 103 (90-113) 12/28-12/29/94
Beryllium 103 (81-112) 12/28-12/n/94
Calcium 108 (85-121) 12/28-12/29/94
Cadmium 99 (83-117) 12/28-12/29/94
Cobalt 100 (87-115) 12/28-12/29/94
Chromium 102 (89-J.17) 12/28-12/29/94
Copper 101 (88-112) 12/28-12/29/94
Iron 110 (86-124) 12/28-12/29/94
Potassium 104 (69-131) 12/28-12/29/94
Magnesium 106 (81-118) 12/28-12/29/94
Manganese 100 (86-114) 12/28-12/29/94
Sodium 105 (83-117) 12/28-12/29/94
Nickel 99 (86-ll4) 12/28-12/29/94
Lead 93 (83-ll9) 12/28/94
Antimony 97 (73-118) 12/28-12/29/94
selenium 92 (57-127) 12/28-12/29/94
Thallium 102 (79-126) 12 /28/94
Vanadium 99 (90-113) 12/28-12/29/94
Zinc 103 (75-110) 12/28-12/29/94
CHEC~ S.AMJ?LE REJ?ORT
LAS #: B4L210036
- - - - --· - ---· - - -INORGANIC ANALYTICAL REPORT - - -· · · - -· · - - -· ·
COMPOUND
Cyanide
SPIKE
PERCENT
RECOVERY
102
).,IMITS
(56-128)
PREPARATION -
ANALYSIS DATE
1/03/95
Q/C
BATCll
5003104
:c.AB #: B4L210036-001
MATRIX: WATER
- --. . - - -- -
PARAMETER
Turbidity
SAMPLE -SAMPLE DUP
--- --. INORGANIC ANJU,YTICAL
RESULT
SMP PUP
175 185
WO #o AJ.XRX
REPORT -" ---- -
RPD EXTRACTION / QC
RPD l#fil1'. ANALYSIS DATE BATCH
6 (0·20) 12/2l/94 4356088
QC BATCH: 4364034
LAB #: B4L210036-001 S
MATRIX: WATER
MATRIX SPIKE REPORT
WO #: AlXRX
PREPARi'TION DATE: 12/29/94
DATE ANALYZED: 12/29/94
- - --- - - - - - --- --- - -GC/MS Volatiles -- - - --- - - - - - --- - - -
SPIKE SPIKE/DUP
PERCENT PERCENT Q/C RPD
COMPOUND RECOVERY RECOVERY LIMITS RPD LIMIT
111-Dichloroethene 99 100 (63-123) 1. 5 (0-19)
Benzene 106 106 (76-126) 0.12 (0-16)
Trichloroethene 96 99 (75-115) 3.3 (0-10)
Toluene 107 108 (75-122) 0.48 ( 0-23)
Chloroben2ene 104 105 (74-113) 1. 7 (0-13)
C(l\.::1,1!11tion~ 11ru p1::.rfonntd b\:.foie iOUndin~ to (IV0id rQ1md-off ~rror~ i11 cak:ulatOO H'-'!\llll!
QC BATCH: ~357101
LAB #: B4L200008·001 S
MATRIX: WATER
------- -----
COMPOUND
Phenol
2-Chlorophenol
l,4-Dichlorobenzene
-
N-Nitrosodi-n-propylamine
l,2,4~Trichlorobenzene
4-Chloro-3-methylphenol
Acenaphthene
4-Nitrophenol
2,4-Dinitrotoluene
Pentachlorophenol
Pyrene
MATRIX SPIKE REPORT
-- --GC/MS Semi-Volatiles
SPIKE SPIKE/DUP
PERCENT PERCENT
RECOVERY RECOVERY
46 37
51 40
42 33
56 46
45 36
55 52
58 57
46 51
40 55
62 63
55 57
-
WO #: AlWP5
PREPARATION DATE: 12/23/94
DATE ANALYZED: 12/29/94
----- -
---------
Q/C RPD
LIMITS RPD LIMIT
(15-97) 23 (0-23)
(17-89) 24 (0-21)
(l-6-56) 25 (0-20)
(40-127) 20 (0-29)
(27-65) 21 ( 0 -15)
(8.0-101) 4.5 (0-36)
(57-104) 1.8 (0-24)
(13-99) 10 (0-34)
(22-81) 31 (0-22)
(13-96) 2.1 (0-42)
(58-148) 3.0 (0-30)
-
COMPOUND
Silver
Aluminum
Arsenic
Ba:r-ium
Beryllium
calcium
cadmium
Cobalt
Chromium
Copper
Iron
Potassium
Magnesium
Manganeee
Sodium
Nickel
Lead
Antimony
Selenium
Thallium
Vanadium
Zinc
NOTE~
ldATRIX SPIKE REPORT
METALS -· - -· - - - - - - - - - - - - - - - -
SPIKE SPIKE/DUP
PERCENT PERCENT
RECOVERY RECOVERY
BATCH:4362073
100 99
l04 lM
106 103
101 102
102 102
111 110
100 99
100 100
102 102
98 99
110 no
103 102
105 105
99 99
103 105
100 99
98 99
96 98
98 97
108 107
98 98
104 103
Q/C
LIMITS
MATRIX: WATER
(80-120)
(80-120)
(48-Hl)
(80·120)
(80·l20)
(80-120)
(80-120)
(80-120)
(80-120)
(80-120)
(80-120)
(80-120)
(80-120)
(80-120)
(80-120)
(80-120)
(55·137)
(80-120)
(30-171)
(30-162)
(80-120)
(80-120)
RPD
0.77
0.28
2.6
1.1
0.39
1.2
). . 2
0.38
0.49
O.M
0.18
1.2
0.28
0.12
1. 7
1.2
1.5
1.6
0.51
0.70
0.34
0.67
RPD
LIMITS
( 0 -20)
(0-20)
(0-18)
(0-20)
(0-20)
(0-20)
(0-20)
(0-20)
(0-20)
(0-20)
(0-20)
(0-20)
(0-20)
(0·20)
(0-20)
(0·20)
(0-11)
(0-20)
(0-22)
(0-21)
(0-20)
(0-20)
PREPARATION ·
ANALYSIS DATE
J.2/28-12/29/94
12/28-J.2/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28-12/29/H
12/28-12/29/94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28-12/29/94
12/28-12/29/94
12/28/94
12/28-12/29/94
12/28-12/29/94
-·-··-----
Page _/_ ol _L RI.KT ENVIRONMENT & Custody Chain and Analytical Request RUST E&I Project No. 'J 7). 7'j, <!o 0
INFRASTRUCTURE RUST E&I Projecl Name ('&l'772AL '""'""'·
Custody No./LIMS No.
Project/Lo-callon: f't:""IJ T /l.4L rll.14//f l'61LT -t! II I/ /lL " TTL SAMPLE ANALYSIS (SP EClFY METH OD)
Client Name: Cet\/lJ/4/ /)7!/1n'5 ,t'ottr .:TNC. ~ '"' t' ~ ~ VI ,] <:. ~ w !e c
Co llecled By: TU lJl > te_ /?70/tbit/\J ~ ::5 g. ll "' Ci ~ .. "~ ~~ J
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(Min.imlze Characlers) Date 0. ~ 1l " a ie: ~~ ~~ u (24·HO\Jr) E tillered, elc.) 0 "' ;: u mw-(> 12--J-<J-01 //30 x 3 3 A = Aqueous., S == Solid. M -= Aqueous J A
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12.-· i-" 1)'" J/30 x 1 3 ~
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I 'i.t~ ;:' a1-,q.,J1L I /f m /?GJl/1-ru 12. € A
Custody Transfers Prior to Receipt By Laboratory Sample Dell very Details/Laboratory Receipt
Relinquished b.,.l(Signed]-Received byl(Signed) D.a1e Tome Delivered Directly to Lab 0 Shipped [2i CXc' ~°):'"""1,&,, f-e tr
{01"921nizarion}
1. ; z_~ j.() ''i( ;?iio Method of Shipment ,C,.:t -t.K Airbill #: :; 1 l-L 0 -Ft. -V .S:. -~
2. Analytical .Lab: = !j704 Location: 77,,,,4 ,rl. ,4, F?
3. Date: / l-2/ 1i Time (/Vo Lab Rec1p1 en!: U X,
(Signature)
A-ddilion.al Remarks:
(Co~dition Upon lab Receipt, Elc.)
Rev. 09/()1/93 White • Laboratory: Yellow · RU ST E&I: Pin~ · P roj eel Files
I'll -..ENVIRONMENT& 1'-U> I INFRASTRUCTURE Custody Chain and Analytical Request
PagB __f___ of _L
3;;iz.7 g. 000
((. fy,,.Z y;;;,,~ RUST E& I Pro jecl No.
RUST E&I Project Name
Custody N o./L I MS No.
Project/Location: (! eN'T12#<.... ~ S /JM.r _ ~ ,4.4 /Z,t.. 6 ff ;C SAMPLE ANALYSlS (SPECIFY METHOD)
c1;en!Nam9' {t:Ju/nAL TIZA/1/5/'on.r ::z::""' c.
Collected By' /«CL'>", /?lo IL 6 #-A..J
Soo ;j
I Commeri1s Sa mp le Information S;;:impre ID Date I Time <>. I> ~1 (loca1iQn. dep,h, (Minimize Cha r;icter:s.) {2-4·Hour} c ~ 1ille red, etc.) 0 ~ 0 Cl ~ ---·
0 ~ :;-':] ~ ~ §' ~ ~ -.:. 0'
0 "'~"' <::i ~ u ·t'" ' '
Ci" '"'""~'"' ~~" ..:i,t·" ~('.2.i~~\J ~~
COMMENTS
(8dd preserv,11ive ~niormaLion)
2 ;.; _,
• 0 0 u
l/:2.·1-0 ·~v /ff vi/-/& /3/0 ,I ---x ;nw-1 :3 fl· U·1'1 /306 v 'VI'-'' u I I I ~1 15" I~ I/ I / I ' I I I I I I I A=Aqueous S
0
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fr1 IV-7-d /2.. Z.• -1'1 1-;;1 '.l-xi SI ~ I / I / I 1 I I I I I I l.5#11<-r ttvcD IC
/YJW-7 /2· ZC·?y !Zt> x G' I ~I / I / I / I I I I I I TN11£ av Jl<1•6101ryl c
/
'{[111 f' /?,l //·Ill I(. I Ti#ff' c
Custody Transfers Prior to Receipt By Laboratory Sample Delivery Details/Laboratory Receipt
Relin.e:uished byl(Slgried) R'BD!!(..,ed bylf~ried) Date Time 1.CA 7rz;;.1 ,t,,ir~ 10,,00;,.,;001 ;;.,)~· ?/ avti Del ive red Di reclly to Lab D Shi pp eel ill
Method of Shipmenl: (;_,( l /( Airbill #: 2 3 ~( 0 -FL-~ W$_
~
-~~-~~~~~~~~
3.
Addllional Remarks:
(Condi1ioo llpon Lab Receipt. Elc.)
Rev. 09101193
Analylical Lab: ~I'~ t;;;;i Localion: 77,fo/ Ft.A.
Lab Recipient ::(1 { ] = Date: IC -!t-9'{Time: //Ct'\
(Signature)
While · laboratory; Yellow · RUST E& I: Pink · Project Files
y-
Page_/_ of _L__
mJn'ENVIRONMENT& Custody Chain and Analytical Request RUST E&I Project No. 3Jl-7'i'· 000
INFRASTRUCTURE RUST E& I Pro jecl Na me {' (: "1 rl7!~'-/ll "'. s
Custody No.IUMS No.
Projectlloca•ion: C&Til/4<._ T/ftfN.f !'Wt r-OIA-~TT'£ SAMPLE ANALYSIS (SPEC I FY METHOD)
Client Name: Ca.'11lt4L T £4 A.IS ;:!Jr1.-T ::TNC. 11 "' ~ ~ " ;), s Collected Sy: 'luc1l>_ft. /1'/o llt~l'!-/V !i ~ ~ "' ~ " c " )t: ~ ' -' ' "" 0 ~~ "' COMMENTS S.am ple ln!o rmatio n u '<. ...... ~ • Commenls 0 ?. ;,.. 0 Sample ID Tlm-e
0. " (location, depth, ~~ ' "" (ac..td preservative inforrna li-oci l 0 (Minimize Characters) Date (24-HoLrr) ~ " ~~ ~~ ~~ u 5 ~ fil1ered. etc.) i\l u "' 111w-'7 I ,l'•)O • 1'( 1/30 I 5 ) I I I A= Aqueous, S "" SrniO. M "" A-c:;_ueo1.1s I 6
rnw-C,,-ci J( ' I Solid ti.tixture. ·w "" ~"'/<1sl-c () lrl.· JO·f</ 1/.30 .;i I I
M/AJ -8 /J..· ~·'ti 1100 J( 5" ;; I I I 5·rro/!.r Ho<.-l> B
(';/ITG' t>H
ru !2. /J 1 o 1 T"1 ,
'
l)/11 f !2iL/1N\L I 711 .. I'. A
Custody Transfers Prior to Receipt By Laboratory Sam p I e Delivery De ta i Is/Laboratory Re cei pl
Relinquished ls~J{S1gned) Re-:::eive<li byl(Signed-) Dace Time De I ivered Di reclly to Lab D Shipped igj 1{/L_ c;p'"';'Zrf g IT (Organ'izatlon~
t~·:>o.'J{ /fDO Method of Shipment: fi/ f X Airbill #: ~di c;Yjf?} Ot;/,)-
2. Analylical Lab: !il!Jvltf(f X tp Location; 1j'}[ti / r:-t,t/ ·
3. Lab Rec;pienl: ' Md~' ' l<l, Date: I -r I r Time: II a::_)
(Signalure)
Addi1tonal Remarks:
(Condilio-n Upon Lab Aeceip1, Etc.)
Rev. 0 9101193 While -Laboratory: Yellow - R LIST E & I: Pink -Project Files
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l
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