20070_Scottish Rite Temple_Brownfields Assessment Report_20170104

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Brownfields Assessment Report Scottish Rite Temple Site
4640 and 4740 Randolph Road
Charlotte, North Carolina H&H Job GSL-002 Table of Contents

1.0 Introduction and Background .............................................................................................. 1
2.0 Groundwater Assessment ....................................................................................................... 4
2.1 Sampling Methodology ........................................................................................................ 4
2.2 Well Abandonment and IDW ............................................................................................... 6
2.3 Groundwater Sampling Results ............................................................................................ 6
3.0 Soil Assessment........................................................................................................................ 7
3.1 Sampling Methodology ........................................................................................................ 7
3.2 Soil Assessment Results ....................................................................................................... 8
4.0 Hydraulic Oil Sampling .......................................................................................................... 9
4.1 Sampling Methodology ........................................................................................................ 9
4.2 Hydraulic Oil Assessment Results ....................................................................................... 9
5.0 Laboratory QA/QC ............................................................................................................... 10
6.0 Summary ................................................................................................................................ 10

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List of Tables
Table 1 Summary of Groundwater Analytical Data
Table 2 Summary of Soil Analytical Data
Table 3 Summary of Hydraulic Oil Analytical Data

List of Figures
Figure 1 Site Location Map
Figure 2 Sample Location Map

List of Appendices
Appendix A Boring Logs
Appendix B Laboratory Analytical Reports

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Brownfields Assessment Report Scottish Rite Temple Site
4640 and 4740 Randolph Road
Charlotte, North Carolina H&H Job GSL-002
1.0 Introduction and Background
On behalf of prospective developer (PD) Greystar GP II, LLC, Hart & Hickman, PC (H&H) has
prepared this report summarizing Brownfields assessment activities conducted at the Scottish
Rite Temple site located at 4640 to 4740 Randolph Road in Charlotte, Mecklenburg County,
North Carolina (see Figure 1). The subject site consists of two contiguous parcels of land (Parcel
#s 18502136 and 18502134) of approximately 6.4 acres and are developed with the following
structures:

 4640 Randolph Road – one-story single-family residence (2,127 square ft) built in
1953; and
 4740 Randolph Road – split-level institutional building (40,596 square ft) built in
1978/1979.

The residence is currently vacant and the Jamgotch residence property is partially over-grown
with vegetation. The institutional building is utilized by the Scottish Rite Masonic organization
as an office/meeting facility.

During recent Phase I ESA activities, H&H identified the following environmental issues
associated with the subject site:

Jamgotch Residence - Water Supply Well
The vacant residential property (previously owned be Mr. Nish Jamgotch) is located in the
northern portion of the site. The Environmental Database Resources (EDR) environmental
database report reviewed during previous Phase I Environmental Site Assessment (ESA)
activities listed the following databases under the name the Jamgotch Well: Recovered
Government Archive (RGA) Hazardous Waste Site (HWS), Incident Management Database

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(IMD), and State Hazardous Waste Site (SHWS). According to information provided in the
databases, methyl tert-butyl ether (MTBE) was detected in a groundwater sample collected from
a water supply well located adjacent to the residence. The water supply well was sampled during
a January 2002 groundwater assessment event associated with an off-site leaking underground
storage tank (LUST) incident reported at a Unocal service station located approximately 950 ft
north-northwest and topographically cross-gradient of the subject site. According to the
databases, the status of the Jamgotch Well incident has not been determined. The water supply
well was reportedly located southwest of the residence. However, H&H did not located the
water supply well during our site reconnaissance of the residential property.

H&H reviewed previous reports from the North Carolina Department of Environmental Quality
(DEQ) CARA³ (currently Laserfiche) web-portal to obtain additional information regarding the
Jamgotch Well incident. According to information obtained during our review of environmental
reports, Mecklenburg County Division of Water Quality (DWQ) collected groundwater samples
from the Jamgotch well between January 2002 and April 2006. 1,2-Dichloropropane (1,2-DCP)
was identified in groundwater samples collected from the water supply well at concentrations of
1.3 micrograms per liter (µg/L) to 2.7 µg/L, which are above the NC Groundwater Quality
Standard (2L Standard) of 0.6 µg/L. 1,2-DCP is a volatile organic compound (VOC) historically
used as a fumigant and in paint strippers. The VOCs 1,1-dichloroethene (1,1-DCE, <0.25 to 0.41
µg/L) and chloroform (<0.25 to 0.34 µg/L) were also detected in groundwater samples collected
from the Jamgotch well at concentrations below their 2L Standards of 7 µg/L (for a private well)
and 70 µg/L, respectively. MTBE was not detected above laboratory detection limits in
groundwater samples collected from the Jamgotch well after April 2002.

State toxicologist Mr. Ken Rudo with the Occupational and Environmental Epidemiology
Branch of NC Department of Health and Human Services (DHHS) last reviewed groundwater
data from the Jamgotch well in January 2006. He reported that lab results were not conclusive
and he recommended conducting additional sampling. The last Jamgotch well groundwater
sampling event was conducted in April 2006.

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H&H interviewed Ms. Shawna Caldwell with Mecklenburg County Groundwater Services, and
Mr. Dave Ramey and Mr. Vincent Antrilli with the DEQ Inactive Hazardous Sites Branch
(IHSB) to determine the current status of the Jamgotch Well release incident. Ms. Caldwell, Mr.
Ramey, and Mr. Antrilli confirmed that the incident has not been closed by either Mecklenburg
County or NC DEQ and the source of the release has not been identified. Ms. Caldwell checked
Mecklenburg County records and reported that the property was connected to a municipal water
supply in 2005. She also noted that Mecklenburg County does not have a record that the
Jamgotch well was abandoned. However, H&H was not able to locate the water supply well
during recent assessment activities.

Hydraulic Elevators
H&H identified two hydraulic elevators located in the southern and eastern portions of the
Scottish Rite Temple building. The elevators were installed during construction of the building
in 1978/1979. The elevators are constructed with in-ground pistons and are equipped with
mechanical system and reservoir tanks located in adjacent storage rooms. Site contact Mr. DC
Heilman with the Scottish Rite Temple reported that the elevators are serviced on a routine basis
by Otis Elevator Company (Otis).

H&H contacted Mr. Steve Verta with Otis who confirmed that they service the elevators located
in the Scottish Rite Temple building. Mr. Verta reported that there have not been any reported
issues regarding elevator failure or unexplained lack of hydraulic fluid. The hydraulic fluid
reservoirs were observed to be in good condition in the nearby elevator equipment rooms with
only minor oil staining observed to the concrete floor below the mechanical system associated
with the southern elevator. Based on the age of the elevators (installed in 1978/1979), it is
possible that hydraulic fluid utilized in the elevators may contain polychlorinated biphenyls
(PCBs). It is also possible that a hydraulic oil release could have occurred to the in-ground
pistons below the elevators.

Underground Storage Tank
H&H identified a fill port and vent cap associated with an approximate 1,000-gallon
underground storage tank (UST) located southwest of the Scottish Rite Temple building. Site

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contact Mr. Heilman reported that the building is currently heated with natural gas. He reported
that the UST was installed to store fuel oil for use as a backup fuel supply in the late 1970s.
However, he reported that the UST was currently empty and had never contained fuel oil or other
petroleum product. The UST is not identified on environmental databases in the EDR report and
H&H did not locate a record of the UST during our review of DEQ Division of Waste
Management (DWM) UST regulatory databases, documents, and files. Because the UST
reportedly never contained fuel oil and due to the lack of a reported release incident, the potential
for impact to the subject site appears low.

As discussed with DEQ during the recent Kick-Off/Data Gap meeting, H&H proposed to
conduct soil sampling at the site to determine if VOCs, Semi-VOCs (SVOCs), and Resource
Conservation and Recovery Act (RCRA) metals are present in soil on the Jamgotch and Scottish
Rite Temple properties prior to redevelopment. H&H also proposed to sample shallow soil
below the drip lines of both onsite structures for lead and shallow groundwater near the former
Jamgotch residence for VOCs, SVOCs, and RCRA Metals. Hydraulic oil within the reservoir of
the Scottish Rite Temple elevators was also sampled for polychlorinated biphenyls (PCBs). The
assessment activities were conducted in general accordance with the methods stated in the DEQ
IHSB Guidance documents field procedures and US Environmental Protection Agency (EPA)
Region 4 Standard Operating Procedures. Details concerning these activities are provided
below.

2.0 Groundwater Assessment

Prior to the assessment activities, H&H obtained a Subsurface Investigation Permit (SIP No.
70002397) from the Mecklenburg County Land Use and Environmental Services Agency
(LUESA).
2.1 Sampling Methodology

On December 6, 2016, H&H contracted Environmental Drilling and Probing Services. (EDPS) to
install one temporary groundwater monitoring well (TMW-1) at the site. The temporary well
location is depicted on Figure 2 and was installed near the existing residential water supply well.

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TMW-1 was advanced using direct push technology (DPT) and hollow stem auger drilling
techniques. Soil cuttings were logged for lithologic purposes, inspected for the presence of
staining and odors, and field-screened for the presence of organic vapors with a calibrated photo-
ionization detector (PID). The temporary well boring log is included as Appendix A.

TMW-1 was advanced to 35 ft below ground surface (bgs) and installed with 2-inch diameter
PVC with a 10 ft of well screen with a sand filtered pre-packed screen set to bracket the water
table. The remaining portion of the borehole was completed with a hydrated bentonite seal that
extended to the ground surface. Due to the temporary nature of the well, grout was not placed
above the bentonite seal. Following installation, a locking expansion plug was secured to the
temporary well.

After installation, the monitoring well was developed by purging a minimum of three well
volumes. Development was considered complete when field parameters of temperature, pH,
conductivity, and oxidation reduction potential (ORP) stabilized, and purge water was visually
clear.

On December 7, 2016, H&H gauged the depth to the water table utilizing a decontaminated
electronic water level indicator. The water level in the well was measured at a depth of 28.0 ft
below top of casing (TOC) in TMW-1.

After the depth to groundwater measurement was collected, a groundwater sample was collected
from the temporary monitoring well utilizing low flow/low stress purging methods with a
peristaltic pump and dedicated Teflon lined polyethylene tubing. The well was purged until
readings of pH and specific conductivity stabilized for three consecutive measurements.
Because the sample from TMW-1 was analyzed for metals, TMW-1 was purged until turbidity
readings were below 10 nephelometric turbidity units (NTUs). The groundwater sample was
then collected directly into laboratory supplied glassware, and labeled with the sample
identification, site name, date, time, and requested analyses.

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The sample was placed in a laboratory supplied cooler, covered with ice, and delivered under
standard chain of custody protocol to Test America for analysis of VOCs by EPA Method
8260B, SVOCs by EPA Method 8270D, and RCRA metals by EPA Methods 6010/7470. The
laboratory analytical report is provided in Appendix B.

2.2 Well Abandonment and IDW

On December 13, 2016, following groundwater sample collection the temporary monitoring well
was abandoned by EDPS with hydrated bentonite and the surface was repaired to match pre-
drilling conditions. The well abandonment records were subsequently uploaded to Mecklenburg
County’s MAPS system in order to close the SIP.

Soil investigation derived waste (IDW) produced during the assessment activities was placed
back into the soil boring to the extent possible and extra soil was thin spread on the site parcels
to which access was provided because evidence of significant impacts was not observed during
the field screening of the soil cuttings. Water IDW produced during the assessment activities
was released on the site parcels to which access was provided in the vicinity of where the water
originated.

2.3 Groundwater Sampling Results

A summary of the groundwater laboratory analytical results is presented on Table 1. The
laboratory analytical data report is included in Appendix B. The groundwater analytical data
were compared to 2L groundwater standards.

The groundwater analytical results indicate that VOCs or SVOCs were not detected in the
groundwater sample in concentrations at or above laboratory detection limits. The metal barium
was detected in the groundwater sample at a concentration of 61.8 µg/L which is well below the
standard of 700 µg/L. No other metals were detected above 2L groundwater standards in the
groundwater sample collected at the site.

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3.0 Soil Assessment

On December 7, 2016, H&H collected 18 soil samples from nine soil borings installed at the site.
The methods and results of the soil assessment activities are provided in the following sections.

3.1 Sampling Methodology

On December 7, 2016, H&H advanced nine soil borings (SS-1 through SS-9) at locations on the
Brownfields property near the Jamgotch residence and on the Scottish Rite Temple property to
determine if 1,2-DCP or other VOCs, SVOCs, and RCRA metals are present in soil. The soil
borings were advanced to a depth of 4 ft bgs using a decontaminated hand auger and soil from
the borings were field screened for the presence of odor, staining, and elevated PID readings. A
shallow soil sample (0.5 to 1.5 ft bgs) and a deeper soil sample (3 to 4 ft bgs) from each soil
boring were collected and submitted to the laboratory for analysis of VOCs by EPA Method
8260B, SVOCs by EPA Method 8270D, and RCRA metals by EPA Methods 6010/7470. Soil
sample locations are depicted on Figure 2. Soil boring logs are included as Appendix A. The
laboratory analytical data report is included in Appendix B.

On December 7, 2016, H&H also advanced eight shallow soil borings along the drip line of the
Jamgotch residence and Scottish Rite Temple building located on the Brownfields property to
characterize soil for lead prior to redevelopment. The soil borings were advanced to a depth of 2
ft bgs on each side of the residence and Scottish Rite Temple using a decontaminated hand
auger. H&H observed the soils for visual evidence of paint chips. At each structure location,
one composite soil sample from the drip line (two composite soil samples total [DL-1 and DL-
2]) were submitted for laboratory analysis for lead by EPA Method 6020B. Drip line composite
sample locations are depicted on Figure 2. The laboratory analytical data report is included in
Appendix B.

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3.2 Soil Assessment Results

A tabular summary of the laboratory analytical results of the soil samples collected at the site is
presented on Table 2. The soil sample results were compared to the DEQ IHSB Residential
Preliminary Soil Remediation Goals (PSRGs). In addition, the metals data were compared to
typical naturally occurring concentrations of metals in soil.

The compounds acetone (SB-1 through SB-9 and DUP-1), bromomethane (SB-1, SB-2, SB-3,
SB-4, SB-8, and SB-9), toluene (SB-3 and SB-9), 2-butanone (SB-1, SB-2, SB-3, SB-4, SB-7,
SB-8, SB-9, and DUP-1), 1,2,3-trichlorobenzene (DUP-1), and 1,2,4-trimethylbenzene (SB-1,
SB-2, SB-3, SB-4, and SB-8) were detected in soil samples below established Residential PSRGs
of 12,200 milligrams per kilogram (mg/kg), 1.36 mg/kg, 818 mg/kg 5,400 mg/kg, 12.6 mg/kg,
and 11.6 mg/kg, respectively. P-isopropyltoluene (SB-3 and SB-5) was also detected; however,
a PSRG has not been established for this compound. No SVOCs were detected in the soil
samples collected.

Detected metals concentrations are consistent with typical background levels. The metals
arsenic, barium, cadmium, chromium, lead, selenium, and mercury were detected in soil samples
collected at the site in concentrations below the Residential PSRG. Arsenic concentrations
detected in five soil samples exceeded the Residential PSRG of 0.68 mg/kg and the Industrial
PSRG of 3.0 mg/kg. However, arsenic concentrations are within the typical background ranges
in North Carolina soil as indicated in Table 2.

Results for the drip line composite samples (DL-1 and DL-2) analyzed for lead indicated that
lead concentrations in both composite soil samples were within typical background levels for
North Carolina as indicated in Table 2. In addition, the concentrations of lead detected in drip
line samples DL-1 and DL-2 did not exceed the Residential PSRG of 400 mg/kg.

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QA/QC Soil Samples
As requested by DEQ, H&H collected a shallow (0.5 to 1.5 ft bgs) and deeper (3 to 4 ft bgs)
duplicate soil sample (DUP-1) from the SB-7 soil boring location advanced southeast of the
Scottish Rite Temple building for quality assurance/quality control (QA/QC) purposes. Similar
to the other soil samples, the shallow and deeper duplicate DUP-1 soil samples were submitted
for laboratory analysis for VOCs by EPA Method 8260B. The shallow and deeper duplicate
samples collected from sample location SB-7 had similar compounds detected that were
generally within the same order of magnitude concentration as the parent samples. Lab
repeatability of the analysis was considered acceptable.

4.0 Hydraulic Oil Sampling

On December 7, 2016, H&H collected two hydraulic oil samples from the site. The methods and
results of the soil assessment activities are provided in the following sections.

4.1 Sampling Methodology

On December 7, 2015, H&H collected two hydraulic oil samples (HO-1 and HO-2) from the two
on-site hydraulic oil reservoirs utilizing laboratory supplied glassware and nitrile gloves. The
hydraulic oil samples were analyzed for PCBs by EPA Method 8020A.

4.2 Hydraulic Oil Assessment Results
A tabular summary of the laboratory analytical results of the hydraulic oil samples collected at
the site is presented in Table 3. Hydraulic oil samples HO-1 and HO-2 were not found to contain
PCBs above laboratory detection limits.

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5.0 Laboratory QA/QC

Soil, groundwater, and hydraulic oil samples were shipped in sealed coolers on ice and
accompanied by a signed chain-of-custody to TestAmerica Laboratories, Inc. (TestAmerica)
located in Nashville, Tennessee for laboratory analysis in compliance with the requirements of a
Level II QA/QC data package. As requested by DEQ, TestAmerica reported estimated
concentrations (J values) above the laboratory method detection limit (MDL) but below the
laboratory Reporting Limit (RL).

Information included in the job narrative of the lab report indicates that TestAmerica ran
laboratory control samples (LCS)/LCS duplicates (LCSD) on the batches analyzed for VOCs by
EPA Method 8260 and SVOCs by EPA Method 8270 that included samples collected from the
subject site to meet US Environmental Protection Agency (EPA) requirements. The job
narrative from the lab report also indicates that a matrix spike/matrix spike duplicate (MS/MSD)
was performed for metals run on the same batches analyzed by EPA Methods
6010D/6020B/7470A/7471B that included samples collected from the subject site to meet EPA
requirements.

6.0 Summary

H&H has completed groundwater and soil assessment activities at the Scottish Rite Temple site
located at 4640 and 4670 Randolph Road in Charlotte, Mecklenburg County, North Carolina.
The assessment activities included the collection of a groundwater sample from one temporary
monitoring well installed at the site, collection of 18 soil samples from nine soil borings,
collection of two composite drip line samples, and collection of two hydraulic oil samples from
the site. Based upon the results of our Phase II ESA sampling activities, H&H determined the
following:

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Groundwater
• The laboratory analytical results indicate that no VOCs or SVOCs were detected in the
groundwater sample collected from TMW-1 in concentrations at or above laboratory
detection limits.
• Barium was detected in the groundwater sample below the 2L groundwater standard.

Soil

• The compounds acetone (SB-1 through SB-9 and DUP-1), bromomethane (SB-1, SB-2,
SB-3, SB-4, SB-8, and SB-9), p-isopropyltoluene (SB-3 and SB-5), toluene (SB-3 and
SB-9), 2-butanone (SB-1, SB-2, SB-3, SB-4, SB-7, SB-8, SB-9, and DUP-1), 1,2,3-
trichlorobenzene (DUP-1), and 1,2,4-trimethylbenzene (SB-1, SB-2, SB-3, SB-4, and SB-
8) were detected in soil samples below established Residential PSRGs.
• No SVOCs were detected in the soil samples collected.
• Metals concentrations in the samples (SB-1 through SB-9) were generally within the
typical background ranges for metals in soil.
• The concentrations of lead detected in the drip line samples (DL-1 and DL-2) did not
exceed the Residential PSRG of 400 mg/kg and were consistent with background
concentrations.

Hydraulic Oil
• The hydraulic oil analytical results indicate that PCBs were not detected in hydraulic oil
samples (HO-1 and HO-2).

Future site redevelopment activities will be addressed in an Environmental Management Plan
(EMP) that will be prepared for the site. The EMP will include a requirement to field screen soil
during the potential removal of the hydraulic elevator in-ground pistons and removal of the
empty UST identified on the Scottish Rite Temple property. If obvious evidence of petroleum-
impacted soil is identified during closure of the hydraulic elevator in-ground pistons, one soil
sample from each hydraulic elevator excavation will be submitted to the laboratory for analysis

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of SVOCs by EPA Method 8270D and extractable petroleum hydrocarbons (EPH) by the
Massachusetts Department of Environmental Protection (MADEP) Method.

If obvious evidence of petroleum-impacted soil is identified during removal of the UST, two soil
samples from the tank excavation will be submitted to the laboratory for analysis of VOCs by
EPA Method 8260B, SVOCs by EPA Method 8270D, and volatile petroleum hydrocarbons
(VPH) and EPH by the MADEP Method.
Table 1
Summary of Groundwater Analytical Data
Scottish Rite Temple Site
Charlotte, North Carolina
H&H Job No. GSL-002
Location TMW Adjacent to Former
Jamgotch Water Supply Well
NCAC 2L
Groundwater Standard(1)
Sample ID TMW-1
Sample Date 12/6/2016
Units µg/L µg/L
ALL VOCs (8260B)ND
ALL SVOCs (8270D)ND
RCRA Metals (6010/7470)
Barium 61.8 700
Notes:
1) North Carolina Administrative Code 15A 2L Groundwater Standard
Only those compounds detected in at least one sample shown above
Bold indicates concentration exceeds NCAC 15A 2L Groundwater Standard
Method number follows parameter in parenthesis
VOCs = volatile organic compounds
µg/L = micrograms per liter
ND = not detected above
TMW=Temporary Monitoring Well
Table 2
Summary of Soil Analytical DataScottish Rite Temple Site
Charlotte, North CarolinaH&H Job No. GSL-002
(Revised 1-4-17)
S:\AAA-Master Projects\Greystar, LLC (GSL)\GSL-002 Overture Cotswold Site\Brownfields Sampling\Tables\Soil Sampling Tables.xlsx1/6/2017
Table 2Hart & Hickman, PC
Sample ID DL-1 DL-2
Sample Location
Composite from Jamgotch
Residence
Composite from Scottish Rite
Temple
Sample Depth 0.5-1.5'3-4'0.5-1.5'3-4'0.5-1.5'3-4'0.5-1.5'3-4'0.5-1.5'3-4'0.5-1.5'3-4'0.5-1.5'3-4'0.5-1.5'3-4'0.5-1.5'3-4'0-2'0-2'0.5-1.5'3-4'
Sample Date 12/6/2016 12/6/2016
Units (mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)
VOCs (8260B)
Acetone 0.183 0.213 0.298 0.245 0.286 0.0875 0.171 0.0923 0.161 0.0743 J 0.123 <0.0106 0.209 0.0520 J 0.225 0.178 0.327 0.197 NA NA 0.233 0.0757 J 12,200 100,000 ----
Bromomethane <0.00165 0.00151 J 0.00163 J 0.00164 J 0.00199 J <0.00121 0.00239 <0.00169 <0.00137 <0.00188 <0.00162 <0.00152 <0.00158 <0.00157 0.00261 <0.00127 0.00236 J <0.00180 NA NA <0.00153 <0.00182 1.36 6 ----
2-Butanone (MEK)<0.00703 0.0146 J 0.0189 J 0.0121 J 0.0193 J <0.00512 0.0108 <0.00717 <0.00583 <0.00800 <0.00687 <0.00645 0.00716 J <0.00669 0.0173 J 0.0119 J 0.0201 J <0.00764 NA NA 0.00859 J <0.00774 5400 28,400
p-Isopropyltoluene <0.000923 <0.000735 <0.000680 <0.000829 0.00137 J 0.00954 <0.000912 <0.000942 0.00461 <0.00105 <0.000903 <0.000848 <0.000884 <0.000879 <0.000735 <0.000709 <0.00104 <0.00100 NA NA <0.000855 <0.00102 NE NE ----
1,2,3-Trichlorobenzene <0.000524 <0.000417 <0.000386 <0.000470 <0.000438 <0.000382 <0.000517 <0.000535 <0.000434 <0.000596 <0.000512 <0.000481 <0.000501 <0.000498 <0.000417 <0.000402 <0.000589 <0.000569 NA NA 0.000638 J 0.00123 J 12.6 186
1,2,4-Trimethylbenzene <0.00138 0.00196 J 0.00165 J 0.00243 J 0.00198 J <0.00100 0.00193 J <0.00141 <0.00114 <0.00157 <0.00135 <0.00127 <0.00132 <0.00131 0.00121 J <0.00106 <0.00155 <0.00150 NA NA <0.00128 <0.00152 J 11.6 48
Toluene <0.00102 <0.000812 <0.000751 <0.000915 <0.000853 0.00269 <0.00101 <0.00104 <0.000846 <0.00116 <0.000997 <0.000936 <0.000977 <0.000971 <0.000812 <0.000783 0.00131 J <0.00111 NA NA <0.000945 <0.00112 818 818 ----
SVOCs (8270D)ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA --------
RCRA Metals (6010/7471)
Arsenic 4.06 3.82 4.27 4.00 3.75 <1.47 <1.50 <1.56 <1.42 <1.55 <1.49 <1.48 <1.55 <1.60 <1.38 <1.47 1.61 J <1.44 NA NA NA NA 0.680 3.00 1.0 - 18 4.8
Barium 33.0 34.3 45.1 56.2 59.5 13.3 70.8 14.9 33.7 13.8 14.4 5.12 20.1 12.0 37.6 15.3 81.4 57.5 NA NA NA NA 3,000 44,000 50 - 1000 356
Cadmium <0.125 <0.125 <0.115 <0.120 <0.119 2.60 1.68 2.13 1.58 2.72 2.71 1.78 2.92 7.96 1.06 J 1.81 1.25 1.99 NA NA NA NA 14.2 196 1.0 - 10 4.30
Chromium, total 79.7 52.3 38.3 37.0 28.6 27.9 32.9 29.4 38.9 75.3 37.9 20.1 30.2 73.3 17.4 23.5 22.0 37.3 NA NA NA NA NE NE 7 - 300 65
Lead 24.1 19.2 19.1 20.8 17.7 22.5 20.5 19.0 18.4 23.7 28.9 21.2 32.2 13.6 17.3 22.7 16.9 17.1 23.8 9.1 NA NA 400 800 ND - 50 16
Selenium 6.83 3.82 3.81 3.95 2.92 <1.35 <1.38 <1.43 <1.30 <1.42 <1.37 <1.36 <1.42 8.92 J B <1.27 <1.35 <1.32 <1.32 NA NA NA NA 78 1,160 <0.1 - 0.8 0.42
Silver <0.508 <0.485 <0.471 <0.489 <0.472 <0.491 <0.501 <0.519 <0.472 <0.518 <0.497 <0.494 <0.517 <0.532 <0.461 <0.490 <0.481 <0.480 NA NA NA NA 78 1,160 ND - 5.0 --
Mercury 0.0564 J <0.0360 <0.0350 <0.0358 <0.0343 <0.0369 <0.0367 <0.0384 <0.0367 <0.0375 <0.0382 <0.0367 0.0484 J <0.0396 <0.0333 0.0371 J <0.0358 <0.0377 NA NA NA NA 4.60 70.0 0.03 - 0.52 0.121
Notes:
1. NC DENR Inactive Hazardous Sites Branch (IHSB) Preliminary Industrial Health Based Soil Remediation Goals - October 2016
2. NC DENR Inactive Hazardous Sites Branch (IHSB) Preliminary Residential Health Based Soil Remediation Goals - October 2016
3. Range and Mean background values for North Carolina or Southeast soils taken from Elements in North American Soils by Dragun and Chekiri, 2005
Bold indicates an exceedance of the Protection of Groundwater PSRGGrey and underlined values indicate laboratory reporting limit exceeds Protection of Groundwater PSRGOnly those compounds detected in at least one sample shown aboveEPA Method follows parameter in parenthesis; -- = Not Applicable; ND = not detected above laboratory reporting limitsVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act
NA= not analyzed, NE= not established; mg/kg = milligrams per kilogram
"J -flag" represents an apprroximate value that is less than the laboratory reporting limit (RL) but that is greater than or equal to the laboratory's method detection limit (MDL)
Screening Criteria
IHSB Industrial
PSRG1
IHSB
Residential
PSRG2
Background Metals
Range4 Background Metals
Mean4
SB-1
Southeast of Jamogotch
Residence
SB-2
East of Jamogotch
Residence
SB-3
South of Jamogotch
Residence
SB-9
Southwest of Scottish
Rite Temple
SB-4
Southwest of
Jamogotch Residence
SB-5
Within Greenhouse
SB-6
North of Jamogotch
Residence
DUP-1
Collected from SB-7
12/6/2016 12/6/2016 12/6/2016 12/6/2016 12/6/2016 12/6/2016 12/6/2016 12/6/2016 12/6/2016 12/6/2016
SB-7
Southeast of Scottish
Rite Temple
SB-8
Northeast of Scottish
Rite Temple
Table 3
Summary of Hydraulic Oil Analytical Data
Scottish Rite Temple
Charlotte, North Carolina
H&H Job No. GSL-002
Location
Eastern Elevator Hydraulic Oil
Reservoir
Southern Elevator Hydraulic Oil
Reservoir
Sample ID HO-1 HO-2
Sample Date 12/6/2016 12/6/2016
Units mg/kg mg/5g
PCBs (8082A)
PCB-1016 <2.36 <2.23
PCB-1221 <2.36 <2.23
PCB-1232 <2.36 <2.23
PCB-1242 <2.36 <2.23
PCB-1248 <2.36 <2.23
PCB-1254 <2.36 <2.23
PCB-1260 <2.36 <2.23
Notes:
PCBs = polychlorinated biphenyls
mg/kg = milligrams per kilogram
ND = not detected above laboratory reporting limits
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
TITLE
PROJECT
SITE LOCATION MAP
4640-4740 RANDOLPH ROAD
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
3-28-16 0
1GSL-002
CHARLOTTE EAST, NORTH CAROLINA (1991)
2923 S. Tryon Street, Suite 100Charlotte, NC 28203704.586.0007(p) 704.586.0373(f)
SITE
GS
L
-00
2
JAMGOTCH RESIDENCE
(4640 RANDOLPH ROAD)
SB-8
SB-7
SB-9
SB-2
SB-6
SB-5
SB-1
SB-4
SB-3
DL-1
DL-1
DL-1
DL-1
DL-2
DL-2
DL-2
DL-2
TMW-1
HO-1
HO-2
GREENHOUSE
SCOTTISH RITE TEMPLE
(4740 RANDOLPH ROAD)
REVISION NO. 0
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
JOB NO. GSL-002
DATE: 12-14-16
FIGURE NO. 2
4640-4740 RANDOLPH ROAD
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAPLEGEND
SITE PROPERTY BOUNDARY
SHALLOW SOIL BORING LOCATION
DRIP LINE COMPOSITE SAMPLE LOCATION
TEMPORARY MONITORING WELL LOCATION
HYDRAULIC OIL SAMPLE LOCATION
JAMGOTCH WATER SUPPLY WELL
ELEVATOR
EMPTY UNDERGROUND STORAGE TANK
S:\
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Appendix A
Boring Logs
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
1.6
1.2
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-01
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
R
I
N
G

L
O
G

-

H
A
R
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H
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K
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A
N
.
G
D
T

-

1
2
/
7
/
1
6

1
5
:
1
6

-

S
:
\
B
B
B

M
A
S
T
E
R

G
I
N
T

P
R
O
J
E
C
T
S
\
G
S
L
-
0
0
2

S
C
O
T
T
I
S
H

R
I
T
E

T
E
M
P
L
E
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
1.9
6.1
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-02
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
R
I
N
G

L
O
G

-

H
A
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T

H
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K
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A
N
.
G
D
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-

1
2
/
7
/
1
6

1
5
:
1
6

-

S
:
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B
B
B

M
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S
T
E
R

G
I
N
T

P
R
O
J
E
C
T
S
\
G
S
L
-
0
0
2

S
C
O
T
T
I
S
H

R
I
T
E

T
E
M
P
L
E
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
33.0
7.8
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-03
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
R
I
N
G

L
O
G

-

H
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H
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A
N
.
G
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-

1
2
/
7
/
1
6

1
5
:
1
6

-

S
:
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B
B

M
A
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T
E
R

G
I
N
T

P
R
O
J
E
C
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S
\
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0
0
2

S
C
O
T
T
I
S
H

R
I
T
E

T
E
M
P
L
E
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
2.1
2.3
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-04
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
R
I
N
G

L
O
G

-

H
A
R
T

H
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K
M
A
N
.
G
D
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-

1
2
/
7
/
1
6

1
5
:
1
6

-

S
:
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B
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M
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I
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P
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O
J
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C
T
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\
G
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-
0
0
2

S
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O
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T
I
S
H

R
I
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E

T
E
M
P
L
E
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
3.8
6.9
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-05
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
R
I
N
G

L
O
G

-

H
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H
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A
N
.
G
D
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-

1
2
/
7
/
1
6

1
5
:
1
6

-

S
:
\
B
B
B

M
A
S
T
E
R

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I
N
T

P
R
O
J
E
C
T
S
\
G
S
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-
0
0
2

S
C
O
T
T
I
S
H

R
I
T
E

T
E
M
P
L
E
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
1.6
0.8
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-06
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
R
I
N
G

L
O
G

-

H
A
R
T

H
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C
K
M
A
N
.
G
D
T

-

1
2
/
7
/
1
6

1
5
:
1
6

-

S
:
\
B
B
B

M
A
S
T
E
R

G
I
N
T

P
R
O
J
E
C
T
S
\
G
S
L
-
0
0
2

S
C
O
T
T
I
S
H

R
I
T
E

T
E
M
P
L
E
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
1.6
0.8
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-07
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
R
I
N
G

L
O
G

-

H
A
R
T

H
I
C
K
M
A
N
.
G
D
T

-

1
2
/
7
/
1
6

1
5
:
1
6

-

S
:
\
B
B
B

M
A
S
T
E
R

G
I
N
T

P
R
O
J
E
C
T
S
\
G
S
L
-
0
0
2

S
C
O
T
T
I
S
H

R
I
T
E

T
E
M
P
L
E
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
1.3
1.3
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
OV
A

(
p
p
m
)
BORING DIAGRAM
BK
G
.
SA
M
P
.
Sheet 1 of 1
BORING NUMBER SB-08
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
R
I
N
G

L
O
G

-

H
A
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T

H
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K
M
A
N
.
G
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1
2
/
7
/
1
6

1
5
:
1
6

-

S
:
\
B
B
B

M
A
S
T
E
R

G
I
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T

P
R
O
J
E
C
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S
\
G
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-
0
0
2

S
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T
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G
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Slightly moist, slightly soft, red brown, silty CLAY
Bottom of borehole at 4.0 feet.
0.0
0.0
27.0
2.8
DRAWN BY:GES
BORING COMPLETED:12/6/16
DRILLING CONTRACTOR:H&H Remarks:
DRILL RIG/ METHOD:Hand Auger / N/A
SAMPLING METHOD:Grab Soil samples collected from 0.5'-1.5'and 3'-4' for laboratory analysis.
BORING STARTED:12/6/16
LOGGED BY:RDM
TOTAL DEPTH: 4 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
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T
H
(f
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)
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O
L
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MATERIAL DESCRIPTION
RE
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BORING DIAGRAM
BK
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Sheet 1 of 1
BORING NUMBER SB-09
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
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-

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2
/
7
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1
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1
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:
1
6

-

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R

G
I
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T

P
R
O
J
E
C
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\
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-
0
0
2

S
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T
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R
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E
M
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L
E
.
G
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2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
4
5
0
1
2
3
4
5
Moist, stiff, red brown, silty CLAY
Slightly moist, slightly soft, red brown, silty CLAY
Slightly moist, slightly soft, red brown with tan mottling, silty CLAY
Moist, slightly soft, red brown with tan mottling, silty CLAY
Moist, slightly soft, red brown with white/black mottling, silty CLAY
Saturated, slightly soft, red brown with white/black mottling, siltyCLAY
Saturated, slightly soft, red brown with black mottling, silty CLAY
Moist, slightly soft, red brown with black mottling, silty CLAY
Bottom of borehole at 35.0 feet.
Bentonite
2" PVC Riser
Filter Sand
2" Pre-pack
Screen
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
3.2
1.1
1.2
1.6
1.5
7.6
1.5
1.6
4.5
1.9
2.0
2.5
1.9
2.1
1.5
1.7
DRAWN BY:GES
BORING COMPLETED:12/5/16
DRILLING CONTRACTOR:EDPS Remarks:
DRILL RIG/ METHOD:Geoprobe 54DT / Direct Push
SAMPLING METHOD:Macro-Core
BORING STARTED:12/5/16
LOGGED BY:RDM
TOTAL DEPTH: 35 ft.
TOP OF CASING ELEV:
DEPTH TO WATER: 28 ft.
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
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G
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MATERIAL DESCRIPTION
RE
C
O
V
E
R
Y

(
%
)
SA
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P
L
E

T
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BORING DIAGRAM
BK
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Sheet 1 of 1
BORING NUMBER TMW-1
PROJECT:Scottish Rite Temple
JOB NUMBER:GSL-002
LOCATION:4740 Randolph Road, Charlotte, North Carolina
BO
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L
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1
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1
6

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R

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I
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T

P
R
O
J
E
C
T
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S
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-
0
0
2

S
C
O
T
T
I
S
H

R
I
T
E

T
E
M
P
L
E
.
G
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J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
30
35
0
5
10
15
20
25
30
35

Appendix B
Laboratory Analytical Reports
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-117643-1
TestAmerica Sample Delivery Group: GSL-002
Client Project/Site: Scottish Rite Temple
Revision: 1
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: Ryan Mayette
Authorized for release by:
12/22/2016 4:50:09 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: Scottish Rite Temple
TestAmerica Job ID: 490-117643-1
SDG: GSL-002
Page 2 of 159 TestAmerica Nashville12/22/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .91
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .135
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .143
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .152
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .153
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .154
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .159
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Sample Summary
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-117643-1 SB-1 (0.5-1.5)Soil 12/06/16 09:55 12/07/16 09:40
490-117643-2 SB-1 (3-4)Soil 12/06/16 09:55 12/07/16 09:40
490-117643-3 SB-2 (0.5-1.5)Soil 12/06/16 12:00 12/07/16 09:40
490-117643-4 SB-2 (3-4)Soil 12/06/16 12:00 12/07/16 09:40
490-117643-5 SB-3 (0.5-1.5)Soil 12/06/16 12:05 12/07/16 09:40
490-117643-6 SB-3 (3-4)Soil 12/06/16 12:05 12/07/16 09:40
490-117643-7 SB-4 (0.5-1.5)Soil 12/06/16 12:40 12/07/16 09:40
490-117643-8 SB-4 (3-4)Soil 12/06/16 12:40 12/07/16 09:40
490-117643-9 SB-5 (0.5-1.5)Soil 12/06/16 12:15 12/07/16 09:40
490-117643-10 SB-5 (3-4)Soil 12/06/16 12:15 12/07/16 09:40
490-117643-11 SB-6 (0.5-1.5)Soil 12/06/16 12:45 12/07/16 09:40
490-117643-12 SB-6 (3-4)Soil 12/06/16 12:45 12/07/16 09:40
490-117643-13 SB-7 (0.5-1.5)Soil 12/06/16 15:15 12/07/16 09:40
490-117643-14 SB-7 (3-4)Soil 12/06/16 15:15 12/07/16 09:40
490-117643-15 SB-8 (0.5-1.5)Soil 12/06/16 15:30 12/07/16 09:40
490-117643-16 SB-8 (3-4)Soil 12/06/16 15:30 12/07/16 09:40
490-117643-17 SB-9 (0.5-1.5)Soil 12/06/16 15:50 12/07/16 09:40
490-117643-18 SB-9 (3-4)Soil 12/06/16 15:50 12/07/16 09:40
490-117643-19 DUP-1 (0.5-1.5)Soil 12/06/16 01:01 12/07/16 09:40
490-117643-20 DUP-1 (3-4)Soil 12/06/16 01:01 12/07/16 09:40
490-117643-21 DL-1 Soil 12/06/16 16:55 12/07/16 09:40
490-117643-22 DL-2 Soil 12/06/16 17:00 12/07/16 09:40
490-117643-23 HO-1 Oil 12/06/16 09:30 12/07/16 09:40
490-117643-24 HO-2 Oil 12/06/16 09:35 12/07/16 09:40
490-117643-25 TMW-1 Water 12/06/16 11:30 12/07/16 09:40
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Job ID: 490-117643-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-117643-1
Comments
All analyses in the following report have been performed in compliance with all requirements of a Level II QA/QC data deliverable.
No additional comments.
Receipt
The samples were received on 12/7/2016 9:40 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 2 coolers at receipt time were 0.5º C and 3.1º C.
GC/MS VOA
Method 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with soil analytical batch 490-392730. However, an LCS and LCSD were performed on this batch to meet
EPA requirements. These results are listed in the QC Sample Results pages 92 thru 95.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-392749 and analytical batch 490-392931. However, an LCS and LCSD were performed on this batch to meet
EPA requirements. These results are listed in the QC Sample Results pages 110 thru 113.
Method 8270D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 490-392774 and analytical batch
490-393298 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated
laboratory control sample (LCS) recovery was within acceptance limits. These were not samples specific to this sample set an do not
reflect matrix issues with the samples from this site.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method 8082A: The following samples was diluted due to the nature of the sample matrix: HO-1 (490-117643-23), HO-2 (490-117643-24)
and (490-117643-A-24-B DU). Elevated reporting limits (RLs) are provided.
Method 8082A: Surrogate recovery for the following samples was outside control limits: HO-1 (490-117643-23), HO-2 (490-117643-24)
and (490-117643-A-24-B DU). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.
Method 8082A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-392824 and analytical batch 490-392908. However, an LCS and Client Sample Duplicate were performed on this
batch to meet EPA requirements. These results are listed in the QC Sample Results page 127.
Method 8082A: The %RPD between the primary and confirmation column exceeded 40% for DCB Decachlorobiphenyl (Surr) for the
following method blank (MB): (MB 490-392824/1-A). The lower value(s) has been reported and qualified in accordance with the
laboratory's SOP.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 6010D: The continuing calibration verification (CCV) associated with batch 490-393847 recovered above the upper control limit for
Arsenic. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The
following sample is impacted: TMW-1 (490-117643-25).
Method 6010D/6020B/7470A/7471B: An MS/MSD was performed for metals in all prep and analytical batches, but most were on
samples not from this site. Only Prep batch 490-393053 and analytical batch 490-393847 for 6010D metals were performed on a
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Job ID: 490-117643-1 (Continued)
Laboratory: TestAmerica Nashville (Continued)
sample from this sample set.
Method 6010D: The low level check standard recovery associated with batch 490-393847 is outside the acceptance criteria for the
following analyte(s): Selenium.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
GC Semi VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
B Compound was found in the blank and sample.
F1 MS and/or MSD Recovery is outside acceptance limits.
^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-1Client Sample ID: SB-1 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.183 0.0689 0.0116 mg/Kg ☼12/06/16 08:55 12/08/16 21:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Benzene <0.000923
0.00276 0.000992 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Bromobenzene <0.000992
0.00276 0.000758 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Bromochloromethane <0.000758
0.00276 0.000758 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Bromodichloromethane <0.000758
0.00276 0.000758 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Bromoform <0.000758
0.00276 0.00165 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Bromomethane <0.00165
0.0689 0.00703 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼2-Butanone (MEK)<0.00703
0.00689 0.00496 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Carbon disulfide <0.00496
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Carbon tetrachloride <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Chlorobenzene <0.000923
0.00276 0.000469 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Chlorodibromomethane <0.000469
0.00689 0.00262 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Chloroethane <0.00262
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Chloroform <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Chloromethane <0.000923
0.00276 0.00123 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼2-Chlorotoluene <0.00123
0.00276 0.00116 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼4-Chlorotoluene <0.00116
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼cis-1,2-Dichloroethene <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼cis-1,3-Dichloropropene <0.000923
0.00689 0.000965 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2-Dibromo-3-Chloropropane <0.000965
0.00276 0.00138 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2-Dibromoethane (EDB)<0.00138
0.00276 0.000772 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Dibromomethane <0.000772
0.00276 0.000469 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2-Dichlorobenzene <0.000469
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,3-Dichlorobenzene <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,4-Dichlorobenzene <0.000923
0.00276 0.00138 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Dichlorodifluoromethane <0.00138
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,1-Dichloroethane <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2-Dichloroethane <0.000923
0.00276 0.000786 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,1-Dichloroethene <0.000786
0.00276 0.000648 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2-Dichloroethene, Total <0.000648
0.00276 0.00130 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2-Dichloropropane <0.00130
0.00276 0.00130 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,3-Dichloropropane <0.00130
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼2,2-Dichloropropane <0.000923
0.00276 0.000703 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,1-Dichloropropene <0.000703
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Diisopropyl ether <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Ethylbenzene <0.000923
0.00689 0.00157 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Hexachlorobutadiene <0.00157
0.0689 0.0230 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼2-Hexanone <0.0230
0.00276 0.000565 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Isopropylbenzene <0.000565
0.0138 0.00119 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Methylene Chloride <0.00119
0.0689 0.00262 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼4-Methyl-2-pentanone (MIBK)<0.00262
0.00276 0.00132 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Methyl tert-butyl ether <0.00132
0.00689 0.00234 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Naphthalene <0.00234
0.00276 0.00135 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼n-Butylbenzene <0.00135
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼N-Propylbenzene <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼p-Isopropyltoluene <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼sec-Butylbenzene <0.000923
0.00276 0.00152 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Styrene <0.00152
0.00276 0.00124 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼tert-Butylbenzene <0.00124
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-1Client Sample ID: SB-1 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000923 0.00276 0.000923 mg/Kg ☼12/06/16 08:55 12/08/16 21:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00276 0.00138 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,1,2,2-Tetrachloroethane <0.00138
0.00276 0.00101 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Tetrachloroethene <0.00101
0.00276 0.00102 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Toluene <0.00102
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼trans-1,2-Dichloroethene <0.000923
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼trans-1,3-Dichloropropene <0.000923
0.00276 0.000524 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2,3-Trichlorobenzene <0.000524
0.00276 0.000923 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2,4-Trichlorobenzene <0.000923
0.00276 0.00127 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,1,1-Trichloroethane <0.00127
0.00689 0.00193 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,1,2-Trichloroethane <0.00193
0.00276 0.00132 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Trichloroethene <0.00132
0.00276 0.00138 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Trichlorofluoromethane <0.00138
0.00276 0.000758 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2,3-Trichloropropane <0.000758
0.00276 0.00138 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,2,4-Trimethylbenzene <0.00138
0.00276 0.00103 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼1,3,5-Trimethylbenzene <0.00103
0.00276 0.00152 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Vinyl chloride <0.00152
0.00827 0.00170 mg/Kg 12/06/16 08:55 12/08/16 21:09 1☼Xylenes, Total <0.00170
4-Bromofluorobenzene (Surr)87 70-130 12/06/16 08:55 12/08/16 21:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)121 12/06/16 08:55 12/08/16 21:09 170-130
1,2-Dichloroethane-d4 (Surr)113 12/06/16 08:55 12/08/16 21:09 170-130
Toluene-d8 (Surr)88 12/06/16 08:55 12/08/16 21:09 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0397 0.0832 0.0397 mg/Kg ☼12/08/16 11:04 12/09/16 20:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0832 0.0360 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Acenaphthylene <0.0360
0.0832 0.0360 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Anthracene <0.0360
0.0832 0.0372 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Benzo[a]anthracene <0.0372
0.0832 0.0335 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Benzo[a]pyrene <0.0335
0.0832 0.0348 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Benzo[b]fluoranthene <0.0348
0.0832 0.0410 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Benzo[g,h,i]perylene <0.0410
0.0832 0.0335 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Benzo[k]fluoranthene <0.0335
0.413 0.248 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Bis(2-chloroethoxy)methane <0.248
0.413 0.264 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Bis(2-chloroethyl)ether <0.264
0.413 0.246 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼bis (2-chloroisopropyl) ether <0.246
0.413 0.257 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Bis(2-ethylhexyl) phthalate <0.257
0.413 0.254 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼4-Bromophenyl phenyl ether <0.254
0.413 0.267 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Butyl benzyl phthalate <0.267
0.413 0.257 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Carbazole <0.257
0.413 0.282 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼4-Chloroaniline <0.282
0.413 0.209 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼4-Chloro-3-methylphenol <0.209
0.413 0.259 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2-Chloronaphthalene <0.259
0.413 0.237 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2-Chlorophenol <0.237
0.413 0.250 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼4-Chlorophenyl phenyl ether <0.250
0.0832 0.0459 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Chrysene <0.0459
0.827 0.140 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Cresols <0.140
0.0832 0.0397 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Dibenz(a,h)anthracene <0.0397
0.413 0.261 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Dibenzofuran <0.261
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-1Client Sample ID: SB-1 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.236 0.413 0.236 mg/Kg ☼12/08/16 11:04 12/09/16 20:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.413 0.236 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼1,3-Dichlorobenzene <0.236
0.413 0.243 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼1,4-Dichlorobenzene <0.243
0.832 0.253 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼3,3'-Dichlorobenzidine <0.253
0.413 0.217 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2,4-Dichlorophenol <0.217
0.413 0.263 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Diethyl phthalate <0.263
0.832 0.416 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2,4-Dimethylphenol <0.416
0.413 0.257 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Dimethyl phthalate <0.257
0.413 0.262 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Di-n-butyl phthalate <0.262
0.413 0.284 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼4,6-Dinitro-2-methylphenol <0.284
0.413 0.312 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2,4-Dinitrophenol <0.312
0.413 0.258 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2,4-Dinitrotoluene <0.258
0.413 0.277 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2,6-Dinitrotoluene <0.277
0.413 0.221 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Di-n-octyl phthalate <0.221
0.0832 0.0422 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Fluoranthene <0.0422
0.0832 0.0360 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Fluorene <0.0360
0.413 0.310 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Hexachlorobenzene <0.310
0.413 0.207 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Hexachlorobutadiene <0.207
0.413 0.186 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Hexachlorocyclopentadiene <0.186
0.413 0.225 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Hexachloroethane <0.225
0.0832 0.0360 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Indeno[1,2,3-cd]pyrene <0.0360
0.413 0.233 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Isophorone <0.233
0.0832 0.0348 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼1-Methylnaphthalene <0.0348
0.0832 0.0323 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2-Methylnaphthalene <0.0323
0.413 0.268 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2-Methylphenol <0.268
0.413 0.252 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼3 & 4 Methylphenol <0.252
0.0832 0.0360 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Naphthalene <0.0360
0.413 0.257 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2-Nitroaniline <0.257
0.832 0.286 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼3-Nitroaniline <0.286
0.832 0.295 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼4-Nitroaniline <0.295
0.413 0.250 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Nitrobenzene <0.250
0.413 0.302 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2-Nitrophenol <0.302
0.832 0.474 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼4-Nitrophenol <0.474
0.413 0.241 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼N-Nitrosodi-n-propylamine <0.241
0.413 0.0658 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0658
0.832 0.330 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Pentachlorophenol <0.330
0.0832 0.0422 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Phenanthrene <0.0422
0.413 0.252 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Phenol <0.252
0.0832 0.0422 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼Pyrene <0.0422
0.413 0.225 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼1,2,4-Trichlorobenzene <0.225
0.413 0.271 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2,4,5-Trichlorophenol <0.271
0.413 0.238 mg/Kg 12/08/16 11:04 12/09/16 20:25 1☼2,4,6-Trichlorophenol <0.238
2-Fluorobiphenyl (Surr)65 29-120 12/08/16 11:04 12/09/16 20:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)59 12/08/16 11:04 12/09/16 20:25 110-120
Nitrobenzene-d5 (Surr)63 12/08/16 11:04 12/09/16 20:25 127-120
Phenol-d5 (Surr)60 12/08/16 11:04 12/09/16 20:25 110-120
Terphenyl-d14 (Surr)66 12/08/16 11:04 12/09/16 20:25 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-1Client Sample ID: SB-1 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)69 10-120 12/08/16 11:04 12/09/16 20:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic 4.06 2.49 1.49 mg/Kg ☼12/08/16 12:08 12/08/16 21:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.49 1.25 mg/Kg 12/08/16 12:08 12/08/16 21:37 1☼Barium 33.0
1.25 0.125 mg/Kg 12/08/16 12:08 12/08/16 21:37 1☼Cadmium <0.125
1.25 1.12 mg/Kg 12/08/16 12:08 12/08/16 21:37 1☼Chromium 79.7
1.25 0.623 mg/Kg 12/08/16 12:08 12/08/16 21:37 1☼Lead 24.1
2.49 1.37 mg/Kg 12/08/16 12:08 12/08/16 21:37 1☼Selenium 6.83
1.27 0.508 mg/Kg 12/09/16 15:11 12/10/16 05:17 1☼Silver <0.508
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0564 J 0.122 0.0367 mg/Kg ☼12/08/16 12:01 12/09/16 09:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 78.5 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-2Client Sample ID: SB-1 (3-4)
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.213 0.0549 0.00922 mg/Kg ☼12/06/16 08:55 12/08/16 20:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Benzene <0.000735
0.00220 0.000790 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Bromobenzene <0.000790
0.00220 0.000604 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Bromochloromethane <0.000604
0.00220 0.000604 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Bromodichloromethane <0.000604
0.00220 0.000604 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Bromoform <0.000604
0.00220 0.00132 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Bromomethane 0.00151 J
0.0549 0.00560 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼2-Butanone (MEK)0.0146 J
0.00549 0.00395 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Carbon disulfide <0.00395
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Carbon tetrachloride <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Chlorobenzene <0.000735
0.00220 0.000373 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Chlorodibromomethane <0.000373
0.00549 0.00209 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Chloroethane <0.00209
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Chloroform <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Chloromethane <0.000735
0.00220 0.000977 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼2-Chlorotoluene <0.000977
0.00220 0.000922 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼4-Chlorotoluene <0.000922
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼cis-1,2-Dichloroethene <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼cis-1,3-Dichloropropene <0.000735
0.00549 0.000768 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2-Dibromo-3-Chloropropane <0.000768
0.00220 0.00110 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2-Dibromoethane (EDB)<0.00110
0.00220 0.000615 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Dibromomethane <0.000615
0.00220 0.000373 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2-Dichlorobenzene <0.000373
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,3-Dichlorobenzene <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,4-Dichlorobenzene <0.000735
0.00220 0.00110 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Dichlorodifluoromethane <0.00110
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,1-Dichloroethane <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2-Dichloroethane <0.000735
0.00220 0.000626 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,1-Dichloroethene <0.000626
0.00220 0.000516 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2-Dichloroethene, Total <0.000516
0.00220 0.00103 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2-Dichloropropane <0.00103
0.00220 0.00103 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,3-Dichloropropane <0.00103
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼2,2-Dichloropropane <0.000735
0.00220 0.000560 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,1-Dichloropropene <0.000560
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Diisopropyl ether <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Ethylbenzene <0.000735
0.00549 0.00125 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Hexachlorobutadiene <0.00125
0.0549 0.0183 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼2-Hexanone <0.0183
0.00220 0.000450 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Isopropylbenzene <0.000450
0.0110 0.000944 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Methylene Chloride <0.000944
0.0549 0.00209 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼4-Methyl-2-pentanone (MIBK)<0.00209
0.00220 0.00105 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Methyl tert-butyl ether <0.00105
0.00549 0.00187 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Naphthalene <0.00187
0.00220 0.00108 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼n-Butylbenzene <0.00108
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼N-Propylbenzene <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼p-Isopropyltoluene <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼sec-Butylbenzene <0.000735
0.00220 0.00121 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Styrene <0.00121
0.00220 0.000988 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼tert-Butylbenzene <0.000988
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-2Client Sample ID: SB-1 (3-4)
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000735 0.00220 0.000735 mg/Kg ☼12/06/16 08:55 12/08/16 20:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00220 0.00110 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,1,2,2-Tetrachloroethane <0.00110
0.00220 0.000801 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Tetrachloroethene <0.000801
0.00220 0.000812 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Toluene <0.000812
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼trans-1,2-Dichloroethene <0.000735
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼trans-1,3-Dichloropropene <0.000735
0.00220 0.000417 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2,3-Trichlorobenzene <0.000417
0.00220 0.000735 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2,4-Trichlorobenzene <0.000735
0.00220 0.00101 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,1,1-Trichloroethane <0.00101
0.00549 0.00154 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,1,2-Trichloroethane <0.00154
0.00220 0.00105 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Trichloroethene <0.00105
0.00220 0.00110 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Trichlorofluoromethane <0.00110
0.00220 0.000604 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2,3-Trichloropropane <0.000604
0.00220 0.00110 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,2,4-Trimethylbenzene 0.00196 J
0.00220 0.000823 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼1,3,5-Trimethylbenzene <0.000823
0.00220 0.00121 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Vinyl chloride <0.00121
0.00659 0.00135 mg/Kg 12/06/16 08:55 12/08/16 20:40 1☼Xylenes, Total <0.00135
4-Bromofluorobenzene (Surr)89 70-130 12/06/16 08:55 12/08/16 20:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)121 12/06/16 08:55 12/08/16 20:40 170-130
1,2-Dichloroethane-d4 (Surr)114 12/06/16 08:55 12/08/16 20:40 170-130
Toluene-d8 (Surr)90 12/06/16 08:55 12/08/16 20:40 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0396 0.0829 0.0396 mg/Kg ☼12/08/16 11:04 12/09/16 20:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0829 0.0359 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Acenaphthylene <0.0359
0.0829 0.0359 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Anthracene <0.0359
0.0829 0.0371 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Benzo[a]anthracene <0.0371
0.0829 0.0334 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Benzo[a]pyrene <0.0334
0.0829 0.0347 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Benzo[b]fluoranthene <0.0347
0.0829 0.0408 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Benzo[g,h,i]perylene <0.0408
0.0829 0.0334 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Benzo[k]fluoranthene <0.0334
0.412 0.248 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Bis(2-chloroethoxy)methane <0.248
0.412 0.264 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Bis(2-chloroethyl)ether <0.264
0.412 0.245 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼bis (2-chloroisopropyl) ether <0.245
0.412 0.256 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Bis(2-ethylhexyl) phthalate <0.256
0.412 0.254 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼4-Bromophenyl phenyl ether <0.254
0.412 0.266 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Butyl benzyl phthalate <0.266
0.412 0.256 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Carbazole <0.256
0.412 0.281 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼4-Chloroaniline <0.281
0.412 0.208 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼4-Chloro-3-methylphenol <0.208
0.412 0.259 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2-Chloronaphthalene <0.259
0.412 0.236 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2-Chlorophenol <0.236
0.412 0.249 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼4-Chlorophenyl phenyl ether <0.249
0.0829 0.0458 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Chrysene <0.0458
0.824 0.140 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Cresols <0.140
0.0829 0.0396 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Dibenz(a,h)anthracene <0.0396
0.412 0.260 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Dibenzofuran <0.260
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-2Client Sample ID: SB-1 (3-4)
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.235 0.412 0.235 mg/Kg ☼12/08/16 11:04 12/09/16 20:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.412 0.235 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼1,3-Dichlorobenzene <0.235
0.412 0.243 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼1,4-Dichlorobenzene <0.243
0.829 0.253 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼3,3'-Dichlorobenzidine <0.253
0.412 0.217 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2,4-Dichlorophenol <0.217
0.412 0.262 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Diethyl phthalate <0.262
0.829 0.415 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2,4-Dimethylphenol <0.415
0.412 0.256 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Dimethyl phthalate <0.256
0.412 0.261 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Di-n-butyl phthalate <0.261
0.412 0.283 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼4,6-Dinitro-2-methylphenol <0.283
0.412 0.311 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2,4-Dinitrophenol <0.311
0.412 0.257 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2,4-Dinitrotoluene <0.257
0.412 0.276 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2,6-Dinitrotoluene <0.276
0.412 0.220 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Di-n-octyl phthalate <0.220
0.0829 0.0421 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Fluoranthene <0.0421
0.0829 0.0359 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Fluorene <0.0359
0.412 0.309 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Hexachlorobenzene <0.309
0.412 0.207 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Hexachlorobutadiene <0.207
0.412 0.186 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Hexachlorocyclopentadiene <0.186
0.412 0.224 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Hexachloroethane <0.224
0.0829 0.0359 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Indeno[1,2,3-cd]pyrene <0.0359
0.412 0.233 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Isophorone <0.233
0.0829 0.0347 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼1-Methylnaphthalene <0.0347
0.0829 0.0322 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2-Methylnaphthalene <0.0322
0.412 0.267 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2-Methylphenol <0.267
0.412 0.251 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼3 & 4 Methylphenol <0.251
0.0829 0.0359 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Naphthalene <0.0359
0.412 0.256 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2-Nitroaniline <0.256
0.829 0.285 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼3-Nitroaniline <0.285
0.829 0.295 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼4-Nitroaniline <0.295
0.412 0.249 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Nitrobenzene <0.249
0.412 0.301 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2-Nitrophenol <0.301
0.829 0.473 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼4-Nitrophenol <0.473
0.412 0.240 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼N-Nitrosodi-n-propylamine <0.240
0.412 0.0656 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0656
0.829 0.329 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Pentachlorophenol <0.329
0.0829 0.0421 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Phenanthrene <0.0421
0.412 0.251 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Phenol <0.251
0.0829 0.0421 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼Pyrene <0.0421
0.412 0.224 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼1,2,4-Trichlorobenzene <0.224
0.412 0.270 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2,4,5-Trichlorophenol <0.270
0.412 0.238 mg/Kg 12/08/16 11:04 12/09/16 20:43 1☼2,4,6-Trichlorophenol <0.238
2-Fluorobiphenyl (Surr)60 29-120 12/08/16 11:04 12/09/16 20:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)57 12/08/16 11:04 12/09/16 20:43 110-120
Nitrobenzene-d5 (Surr)57 12/08/16 11:04 12/09/16 20:43 127-120
Phenol-d5 (Surr)57 12/08/16 11:04 12/09/16 20:43 110-120
Terphenyl-d14 (Surr)70 12/08/16 11:04 12/09/16 20:43 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-2Client Sample ID: SB-1 (3-4)
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)70 10-120 12/08/16 11:04 12/09/16 20:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic 3.82 2.49 1.50 mg/Kg ☼12/08/16 12:08 12/08/16 21:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.49 1.25 mg/Kg 12/08/16 12:08 12/08/16 21:43 1☼Barium 34.3
1.25 0.125 mg/Kg 12/08/16 12:08 12/08/16 21:43 1☼Cadmium <0.125
1.25 1.12 mg/Kg 12/08/16 12:08 12/08/16 21:43 1☼Chromium 52.3
1.25 0.623 mg/Kg 12/08/16 12:08 12/08/16 21:43 1☼Lead 19.2
2.49 1.37 mg/Kg 12/08/16 12:08 12/08/16 21:43 1☼Selenium 3.82
1.21 0.485 mg/Kg 12/09/16 15:11 12/10/16 05:22 1☼Silver <0.485
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0360 0.120 0.0360 mg/Kg ☼12/08/16 12:01 12/09/16 09:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 80.4 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-3Client Sample ID: SB-2 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.298 0.0508 0.00853 mg/Kg ☼12/06/16 11:00 12/08/16 20:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Benzene <0.000680
0.00203 0.000731 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Bromobenzene <0.000731
0.00203 0.000558 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Bromochloromethane <0.000558
0.00203 0.000558 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Bromodichloromethane <0.000558
0.00203 0.000558 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Bromoform <0.000558
0.00203 0.00122 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Bromomethane 0.00163 J
0.0508 0.00518 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼2-Butanone (MEK)0.0189 J
0.00508 0.00366 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Carbon disulfide <0.00366
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Carbon tetrachloride <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Chlorobenzene <0.000680
0.00203 0.000345 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Chlorodibromomethane <0.000345
0.00508 0.00193 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Chloroethane <0.00193
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Chloroform <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Chloromethane <0.000680
0.00203 0.000904 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼2-Chlorotoluene <0.000904
0.00203 0.000853 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼4-Chlorotoluene <0.000853
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼cis-1,2-Dichloroethene <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼cis-1,3-Dichloropropene <0.000680
0.00508 0.000711 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2-Dibromo-3-Chloropropane <0.000711
0.00203 0.00102 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2-Dibromoethane (EDB)<0.00102
0.00203 0.000569 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Dibromomethane <0.000569
0.00203 0.000345 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2-Dichlorobenzene <0.000345
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,3-Dichlorobenzene <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,4-Dichlorobenzene <0.000680
0.00203 0.00102 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Dichlorodifluoromethane <0.00102
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,1-Dichloroethane <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2-Dichloroethane <0.000680
0.00203 0.000579 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,1-Dichloroethene <0.000579
0.00203 0.000477 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2-Dichloroethene, Total <0.000477
0.00203 0.000954 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2-Dichloropropane <0.000954
0.00203 0.000954 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,3-Dichloropropane <0.000954
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼2,2-Dichloropropane <0.000680
0.00203 0.000518 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,1-Dichloropropene <0.000518
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Diisopropyl ether <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Ethylbenzene <0.000680
0.00508 0.00116 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Hexachlorobutadiene <0.00116
0.0508 0.0170 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼2-Hexanone <0.0170
0.00203 0.000416 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Isopropylbenzene <0.000416
0.0102 0.000873 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Methylene Chloride <0.000873
0.0508 0.00193 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼4-Methyl-2-pentanone (MIBK)<0.00193
0.00203 0.000975 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Methyl tert-butyl ether <0.000975
0.00508 0.00173 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Naphthalene <0.00173
0.00203 0.000995 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼n-Butylbenzene <0.000995
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼N-Propylbenzene <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼p-Isopropyltoluene <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼sec-Butylbenzene <0.000680
0.00203 0.00112 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Styrene <0.00112
0.00203 0.000914 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼tert-Butylbenzene <0.000914
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-3Client Sample ID: SB-2 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000680 0.00203 0.000680 mg/Kg ☼12/06/16 11:00 12/08/16 20:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00203 0.00102 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,1,2,2-Tetrachloroethane <0.00102
0.00203 0.000741 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Tetrachloroethene <0.000741
0.00203 0.000751 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Toluene <0.000751
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼trans-1,2-Dichloroethene <0.000680
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼trans-1,3-Dichloropropene <0.000680
0.00203 0.000386 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2,3-Trichlorobenzene <0.000386
0.00203 0.000680 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2,4-Trichlorobenzene <0.000680
0.00203 0.000934 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,1,1-Trichloroethane <0.000934
0.00508 0.00142 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,1,2-Trichloroethane <0.00142
0.00203 0.000975 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Trichloroethene <0.000975
0.00203 0.00102 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Trichlorofluoromethane <0.00102
0.00203 0.000558 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2,3-Trichloropropane <0.000558
0.00203 0.00102 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,2,4-Trimethylbenzene 0.00165 J
0.00203 0.000762 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼1,3,5-Trimethylbenzene <0.000762
0.00203 0.00112 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Vinyl chloride <0.00112
0.00609 0.00125 mg/Kg 12/06/16 11:00 12/08/16 20:10 1☼Xylenes, Total <0.00125
4-Bromofluorobenzene (Surr)89 70-130 12/06/16 11:00 12/08/16 20:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)122 12/06/16 11:00 12/08/16 20:10 170-130
1,2-Dichloroethane-d4 (Surr)119 12/06/16 11:00 12/08/16 20:10 170-130
Toluene-d8 (Surr)90 12/06/16 11:00 12/08/16 20:10 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0376 0.0787 0.0376 mg/Kg ☼12/08/16 11:04 12/09/16 21:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0787 0.0341 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Acenaphthylene <0.0341
0.0787 0.0341 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Anthracene <0.0341
0.0787 0.0352 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Benzo[a]anthracene <0.0352
0.0787 0.0317 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Benzo[a]pyrene <0.0317
0.0787 0.0329 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Benzo[b]fluoranthene <0.0329
0.0787 0.0388 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Benzo[g,h,i]perylene <0.0388
0.0787 0.0317 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Benzo[k]fluoranthene <0.0317
0.391 0.235 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Bis(2-chloroethoxy)methane <0.235
0.391 0.250 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Bis(2-chloroethyl)ether <0.250
0.391 0.233 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼bis (2-chloroisopropyl) ether <0.233
0.391 0.243 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Bis(2-ethylhexyl) phthalate <0.243
0.391 0.241 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼4-Bromophenyl phenyl ether <0.241
0.391 0.253 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Butyl benzyl phthalate <0.253
0.391 0.243 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Carbazole <0.243
0.391 0.267 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼4-Chloroaniline <0.267
0.391 0.197 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼4-Chloro-3-methylphenol <0.197
0.391 0.245 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2-Chloronaphthalene <0.245
0.391 0.224 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2-Chlorophenol <0.224
0.391 0.236 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼4-Chlorophenyl phenyl ether <0.236
0.0787 0.0435 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Chrysene <0.0435
0.782 0.133 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Cresols <0.133
0.0787 0.0376 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Dibenz(a,h)anthracene <0.0376
0.391 0.247 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Dibenzofuran <0.247
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-3Client Sample ID: SB-2 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.223 0.391 0.223 mg/Kg ☼12/08/16 11:04 12/09/16 21:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.391 0.223 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼1,3-Dichlorobenzene <0.223
0.391 0.230 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼1,4-Dichlorobenzene <0.230
0.787 0.240 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼3,3'-Dichlorobenzidine <0.240
0.391 0.206 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2,4-Dichlorophenol <0.206
0.391 0.249 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Diethyl phthalate <0.249
0.787 0.393 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2,4-Dimethylphenol <0.393
0.391 0.243 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Dimethyl phthalate <0.243
0.391 0.248 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Di-n-butyl phthalate <0.248
0.391 0.269 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼4,6-Dinitro-2-methylphenol <0.269
0.391 0.295 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2,4-Dinitrophenol <0.295
0.391 0.244 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2,4-Dinitrotoluene <0.244
0.391 0.262 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2,6-Dinitrotoluene <0.262
0.391 0.209 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Di-n-octyl phthalate <0.209
0.0787 0.0399 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Fluoranthene <0.0399
0.0787 0.0341 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Fluorene <0.0341
0.391 0.294 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Hexachlorobenzene <0.294
0.391 0.196 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Hexachlorobutadiene <0.196
0.391 0.176 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Hexachlorocyclopentadiene <0.176
0.391 0.213 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Hexachloroethane <0.213
0.0787 0.0341 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Indeno[1,2,3-cd]pyrene <0.0341
0.391 0.221 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Isophorone <0.221
0.0787 0.0329 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼1-Methylnaphthalene <0.0329
0.0787 0.0305 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2-Methylnaphthalene <0.0305
0.391 0.254 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2-Methylphenol <0.254
0.391 0.238 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼3 & 4 Methylphenol <0.238
0.0787 0.0341 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Naphthalene <0.0341
0.391 0.243 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2-Nitroaniline <0.243
0.787 0.270 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼3-Nitroaniline <0.270
0.787 0.280 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼4-Nitroaniline <0.280
0.391 0.236 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Nitrobenzene <0.236
0.391 0.285 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2-Nitrophenol <0.285
0.787 0.449 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼4-Nitrophenol <0.449
0.391 0.228 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼N-Nitrosodi-n-propylamine <0.228
0.391 0.0622 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0622
0.787 0.312 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Pentachlorophenol <0.312
0.0787 0.0399 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Phenanthrene <0.0399
0.391 0.238 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Phenol <0.238
0.0787 0.0399 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼Pyrene <0.0399
0.391 0.213 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼1,2,4-Trichlorobenzene <0.213
0.391 0.256 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2,4,5-Trichlorophenol <0.256
0.391 0.226 mg/Kg 12/08/16 11:04 12/09/16 21:02 1☼2,4,6-Trichlorophenol <0.226
2-Fluorobiphenyl (Surr)63 29-120 12/08/16 11:04 12/09/16 21:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)61 12/08/16 11:04 12/09/16 21:02 110-120
Nitrobenzene-d5 (Surr)64 12/08/16 11:04 12/09/16 21:02 127-120
Phenol-d5 (Surr)63 12/08/16 11:04 12/09/16 21:02 110-120
Terphenyl-d14 (Surr)69 12/08/16 11:04 12/09/16 21:02 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-3Client Sample ID: SB-2 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)72 10-120 12/08/16 11:04 12/09/16 21:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic 4.27 2.30 1.38 mg/Kg ☼12/08/16 12:08 12/08/16 21:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.30 1.15 mg/Kg 12/08/16 12:08 12/08/16 21:48 1☼Barium 45.1
1.15 0.115 mg/Kg 12/08/16 12:08 12/08/16 21:48 1☼Cadmium <0.115
1.15 1.03 mg/Kg 12/08/16 12:08 12/08/16 21:48 1☼Chromium 38.3
1.15 0.574 mg/Kg 12/08/16 12:08 12/08/16 21:48 1☼Lead 19.1
2.30 1.26 mg/Kg 12/08/16 12:08 12/08/16 21:48 1☼Selenium 3.81
1.18 0.471 mg/Kg 12/09/16 15:11 12/10/16 05:27 1☼Silver <0.471
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0350 0.117 0.0350 mg/Kg ☼12/08/16 12:01 12/09/16 09:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 84.2 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-4Client Sample ID: SB-2 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.245 0.0618 0.0104 mg/Kg ☼12/06/16 11:00 12/08/16 19:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Benzene <0.000829
0.00247 0.000890 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Bromobenzene <0.000890
0.00247 0.000680 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Bromochloromethane <0.000680
0.00247 0.000680 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Bromodichloromethane <0.000680
0.00247 0.000680 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Bromoform <0.000680
0.00247 0.00148 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Bromomethane 0.00164 J
0.0618 0.00631 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼2-Butanone (MEK)0.0121 J
0.00618 0.00445 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Carbon disulfide <0.00445
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Carbon tetrachloride <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Chlorobenzene <0.000829
0.00247 0.000420 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Chlorodibromomethane <0.000420
0.00618 0.00235 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Chloroethane <0.00235
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Chloroform <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Chloromethane <0.000829
0.00247 0.00110 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼2-Chlorotoluene <0.00110
0.00247 0.00104 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼4-Chlorotoluene <0.00104
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼cis-1,2-Dichloroethene <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼cis-1,3-Dichloropropene <0.000829
0.00618 0.000866 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2-Dibromo-3-Chloropropane <0.000866
0.00247 0.00124 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2-Dibromoethane (EDB)<0.00124
0.00247 0.000693 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Dibromomethane <0.000693
0.00247 0.000420 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2-Dichlorobenzene <0.000420
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,3-Dichlorobenzene <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,4-Dichlorobenzene <0.000829
0.00247 0.00124 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Dichlorodifluoromethane <0.00124
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,1-Dichloroethane <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2-Dichloroethane <0.000829
0.00247 0.000705 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,1-Dichloroethene <0.000705
0.00247 0.000581 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2-Dichloroethene, Total <0.000581
0.00247 0.00116 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2-Dichloropropane <0.00116
0.00247 0.00116 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,3-Dichloropropane <0.00116
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼2,2-Dichloropropane <0.000829
0.00247 0.000631 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,1-Dichloropropene <0.000631
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Diisopropyl ether <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Ethylbenzene <0.000829
0.00618 0.00141 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Hexachlorobutadiene <0.00141
0.0618 0.0207 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼2-Hexanone <0.0207
0.00247 0.000507 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Isopropylbenzene <0.000507
0.0124 0.00106 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Methylene Chloride <0.00106
0.0618 0.00235 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼4-Methyl-2-pentanone (MIBK)<0.00235
0.00247 0.00119 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Methyl tert-butyl ether <0.00119
0.00618 0.00210 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Naphthalene <0.00210
0.00247 0.00121 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼n-Butylbenzene <0.00121
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼N-Propylbenzene <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼p-Isopropyltoluene <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼sec-Butylbenzene <0.000829
0.00247 0.00136 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Styrene <0.00136
0.00247 0.00111 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼tert-Butylbenzene <0.00111
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-4Client Sample ID: SB-2 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000829 0.00247 0.000829 mg/Kg ☼12/06/16 11:00 12/08/16 19:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00247 0.00124 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,1,2,2-Tetrachloroethane <0.00124
0.00247 0.000903 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Tetrachloroethene <0.000903
0.00247 0.000915 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Toluene <0.000915
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼trans-1,2-Dichloroethene <0.000829
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼trans-1,3-Dichloropropene <0.000829
0.00247 0.000470 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2,3-Trichlorobenzene <0.000470
0.00247 0.000829 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2,4-Trichlorobenzene <0.000829
0.00247 0.00114 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,1,1-Trichloroethane <0.00114
0.00618 0.00173 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,1,2-Trichloroethane <0.00173
0.00247 0.00119 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Trichloroethene <0.00119
0.00247 0.00124 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Trichlorofluoromethane <0.00124
0.00247 0.000680 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2,3-Trichloropropane <0.000680
0.00247 0.00124 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,2,4-Trimethylbenzene 0.00243 J
0.00247 0.000927 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼1,3,5-Trimethylbenzene <0.000927
0.00247 0.00136 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Vinyl chloride <0.00136
0.00742 0.00152 mg/Kg 12/06/16 11:00 12/08/16 19:41 1☼Xylenes, Total <0.00152
4-Bromofluorobenzene (Surr)89 70-130 12/06/16 11:00 12/08/16 19:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)116 12/06/16 11:00 12/08/16 19:41 170-130
1,2-Dichloroethane-d4 (Surr)110 12/06/16 11:00 12/08/16 19:41 170-130
Toluene-d8 (Surr)87 12/06/16 11:00 12/08/16 19:41 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0395 0.0828 0.0395 mg/Kg ☼12/08/16 11:04 12/09/16 21:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0828 0.0358 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Acenaphthylene <0.0358
0.0828 0.0358 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Anthracene <0.0358
0.0828 0.0371 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Benzo[a]anthracene <0.0371
0.0828 0.0334 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Benzo[a]pyrene <0.0334
0.0828 0.0346 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Benzo[b]fluoranthene <0.0346
0.0828 0.0408 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Benzo[g,h,i]perylene <0.0408
0.0828 0.0334 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Benzo[k]fluoranthene <0.0334
0.411 0.247 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Bis(2-chloroethoxy)methane <0.247
0.411 0.263 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Bis(2-chloroethyl)ether <0.263
0.411 0.245 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼bis (2-chloroisopropyl) ether <0.245
0.411 0.256 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Bis(2-ethylhexyl) phthalate <0.256
0.411 0.253 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼4-Bromophenyl phenyl ether <0.253
0.411 0.266 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Butyl benzyl phthalate <0.266
0.411 0.256 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Carbazole <0.256
0.411 0.280 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼4-Chloroaniline <0.280
0.411 0.208 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼4-Chloro-3-methylphenol <0.208
0.411 0.258 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2-Chloronaphthalene <0.258
0.411 0.236 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2-Chlorophenol <0.236
0.411 0.248 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼4-Chlorophenyl phenyl ether <0.248
0.0828 0.0457 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Chrysene <0.0457
0.823 0.140 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Cresols <0.140
0.0828 0.0395 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Dibenz(a,h)anthracene <0.0395
0.411 0.259 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Dibenzofuran <0.259
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-4Client Sample ID: SB-2 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.235 0.411 0.235 mg/Kg ☼12/08/16 11:04 12/09/16 21:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.411 0.235 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼1,3-Dichlorobenzene <0.235
0.411 0.242 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼1,4-Dichlorobenzene <0.242
0.828 0.252 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼3,3'-Dichlorobenzidine <0.252
0.411 0.216 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2,4-Dichlorophenol <0.216
0.411 0.262 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Diethyl phthalate <0.262
0.828 0.414 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2,4-Dimethylphenol <0.414
0.411 0.256 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Dimethyl phthalate <0.256
0.411 0.261 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Di-n-butyl phthalate <0.261
0.411 0.283 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼4,6-Dinitro-2-methylphenol <0.283
0.411 0.310 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2,4-Dinitrophenol <0.310
0.411 0.257 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2,4-Dinitrotoluene <0.257
0.411 0.276 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2,6-Dinitrotoluene <0.276
0.411 0.220 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Di-n-octyl phthalate <0.220
0.0828 0.0420 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Fluoranthene <0.0420
0.0828 0.0358 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Fluorene <0.0358
0.411 0.309 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Hexachlorobenzene <0.309
0.411 0.206 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Hexachlorobutadiene <0.206
0.411 0.185 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Hexachlorocyclopentadiene <0.185
0.411 0.224 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Hexachloroethane <0.224
0.0828 0.0358 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Indeno[1,2,3-cd]pyrene <0.0358
0.411 0.232 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Isophorone <0.232
0.0828 0.0346 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼1-Methylnaphthalene <0.0346
0.0828 0.0321 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2-Methylnaphthalene <0.0321
0.411 0.267 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2-Methylphenol <0.267
0.411 0.251 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼3 & 4 Methylphenol <0.251
0.0828 0.0358 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Naphthalene <0.0358
0.411 0.256 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2-Nitroaniline <0.256
0.828 0.284 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼3-Nitroaniline <0.284
0.828 0.294 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼4-Nitroaniline <0.294
0.411 0.248 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Nitrobenzene <0.248
0.411 0.300 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2-Nitrophenol <0.300
0.828 0.472 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼4-Nitrophenol <0.472
0.411 0.240 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼N-Nitrosodi-n-propylamine <0.240
0.411 0.0655 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0655
0.828 0.329 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Pentachlorophenol <0.329
0.0828 0.0420 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Phenanthrene <0.0420
0.411 0.251 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Phenol <0.251
0.0828 0.0420 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼Pyrene <0.0420
0.411 0.224 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼1,2,4-Trichlorobenzene <0.224
0.411 0.269 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2,4,5-Trichlorophenol <0.269
0.411 0.237 mg/Kg 12/08/16 11:04 12/09/16 21:21 1☼2,4,6-Trichlorophenol <0.237
2-Fluorobiphenyl (Surr)49 29-120 12/08/16 11:04 12/09/16 21:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)43 12/08/16 11:04 12/09/16 21:21 110-120
Nitrobenzene-d5 (Surr)47 12/08/16 11:04 12/09/16 21:21 127-120
Phenol-d5 (Surr)44 12/08/16 11:04 12/09/16 21:21 110-120
Terphenyl-d14 (Surr)60 12/08/16 11:04 12/09/16 21:21 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-4Client Sample ID: SB-2 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)60 10-120 12/08/16 11:04 12/09/16 21:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic 4.00 2.40 1.44 mg/Kg ☼12/08/16 12:08 12/08/16 21:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.40 1.20 mg/Kg 12/08/16 12:08 12/08/16 21:53 1☼Barium 56.2
1.20 0.120 mg/Kg 12/08/16 12:08 12/08/16 21:53 1☼Cadmium <0.120
1.20 1.08 mg/Kg 12/08/16 12:08 12/08/16 21:53 1☼Chromium 37.0
1.20 0.599 mg/Kg 12/08/16 12:08 12/08/16 21:53 1☼Lead 20.8
2.40 1.32 mg/Kg 12/08/16 12:08 12/08/16 21:53 1☼Selenium 3.95
1.22 0.489 mg/Kg 12/09/16 15:11 12/10/16 05:32 1☼Silver <0.489
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0358 0.119 0.0358 mg/Kg ☼12/09/16 08:38 12/09/16 15:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 80.6 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-5Client Sample ID: SB-3 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.286 0.0577 0.00969 mg/Kg ☼12/06/16 11:05 12/08/16 19:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Benzene <0.000773
0.00231 0.000830 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Bromobenzene <0.000830
0.00231 0.000634 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Bromochloromethane <0.000634
0.00231 0.000634 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Bromodichloromethane <0.000634
0.00231 0.000634 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Bromoform <0.000634
0.00231 0.00138 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Bromomethane 0.00199 J
0.0577 0.00588 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼2-Butanone (MEK)0.0193 J
0.00577 0.00415 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Carbon disulfide <0.00415
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Carbon tetrachloride <0.000773
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Chlorobenzene <0.000773
0.00231 0.000392 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Chlorodibromomethane <0.000392
0.00577 0.00219 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Chloroethane <0.00219
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Chloroform <0.000773
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Chloromethane <0.000773
0.00231 0.00103 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼2-Chlorotoluene <0.00103
0.00231 0.000969 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼4-Chlorotoluene <0.000969
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼cis-1,2-Dichloroethene <0.000773
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼cis-1,3-Dichloropropene <0.000773
0.00577 0.000807 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2-Dibromo-3-Chloropropane <0.000807
0.00231 0.00115 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2-Dibromoethane (EDB)<0.00115
0.00231 0.000646 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Dibromomethane <0.000646
0.00231 0.000392 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2-Dichlorobenzene <0.000392
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,3-Dichlorobenzene <0.000773
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,4-Dichlorobenzene <0.000773
0.00231 0.00115 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Dichlorodifluoromethane <0.00115
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,1-Dichloroethane <0.000773
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2-Dichloroethane <0.000773
0.00231 0.000657 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,1-Dichloroethene <0.000657
0.00231 0.000542 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2-Dichloroethene, Total <0.000542
0.00231 0.00108 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2-Dichloropropane <0.00108
0.00231 0.00108 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,3-Dichloropropane <0.00108
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼2,2-Dichloropropane <0.000773
0.00231 0.000588 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,1-Dichloropropene <0.000588
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Diisopropyl ether <0.000773
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Ethylbenzene <0.000773
0.00577 0.00131 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Hexachlorobutadiene <0.00131
0.0577 0.0193 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼2-Hexanone <0.0193
0.00231 0.000473 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Isopropylbenzene <0.000473
0.0115 0.000992 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Methylene Chloride <0.000992
0.0577 0.00219 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼4-Methyl-2-pentanone (MIBK)<0.00219
0.00231 0.00111 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Methyl tert-butyl ether <0.00111
0.00577 0.00196 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Naphthalene <0.00196
0.00231 0.00113 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼n-Butylbenzene <0.00113
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼N-Propylbenzene <0.000773
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼p-Isopropyltoluene 0.00137 J
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼sec-Butylbenzene <0.000773
0.00231 0.00127 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Styrene <0.00127
0.00231 0.00104 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼tert-Butylbenzene <0.00104
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-5Client Sample ID: SB-3 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000773 0.00231 0.000773 mg/Kg ☼12/06/16 11:05 12/08/16 19:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00231 0.00115 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,1,2,2-Tetrachloroethane <0.00115
0.00231 0.000842 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Tetrachloroethene <0.000842
0.00231 0.000853 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Toluene <0.000853
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼trans-1,2-Dichloroethene <0.000773
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼trans-1,3-Dichloropropene <0.000773
0.00231 0.000438 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2,3-Trichlorobenzene <0.000438
0.00231 0.000773 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2,4-Trichlorobenzene <0.000773
0.00231 0.00106 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,1,1-Trichloroethane <0.00106
0.00577 0.00161 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,1,2-Trichloroethane <0.00161
0.00231 0.00111 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Trichloroethene <0.00111
0.00231 0.00115 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Trichlorofluoromethane <0.00115
0.00231 0.000634 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2,3-Trichloropropane <0.000634
0.00231 0.00115 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,2,4-Trimethylbenzene 0.00198 J
0.00231 0.000865 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼1,3,5-Trimethylbenzene <0.000865
0.00231 0.00127 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Vinyl chloride <0.00127
0.00692 0.00142 mg/Kg 12/06/16 11:05 12/08/16 19:11 1☼Xylenes, Total <0.00142
4-Bromofluorobenzene (Surr)93 70-130 12/06/16 11:05 12/08/16 19:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)118 12/06/16 11:05 12/08/16 19:11 170-130
1,2-Dichloroethane-d4 (Surr)115 12/06/16 11:05 12/08/16 19:11 170-130
Toluene-d8 (Surr)89 12/06/16 11:05 12/08/16 19:11 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0380 0.0796 0.0380 mg/Kg ☼12/08/16 11:04 12/09/16 21:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0796 0.0344 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Acenaphthylene <0.0344
0.0796 0.0344 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Anthracene <0.0344
0.0796 0.0356 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Benzo[a]anthracene <0.0356
0.0796 0.0321 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Benzo[a]pyrene <0.0321
0.0796 0.0333 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Benzo[b]fluoranthene <0.0333
0.0796 0.0392 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Benzo[g,h,i]perylene <0.0392
0.0796 0.0321 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Benzo[k]fluoranthene <0.0321
0.395 0.238 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Bis(2-chloroethoxy)methane <0.238
0.395 0.253 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Bis(2-chloroethyl)ether <0.253
0.395 0.235 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼bis (2-chloroisopropyl) ether <0.235
0.395 0.246 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Bis(2-ethylhexyl) phthalate <0.246
0.395 0.243 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼4-Bromophenyl phenyl ether <0.243
0.395 0.255 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Butyl benzyl phthalate <0.255
0.395 0.246 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Carbazole <0.246
0.395 0.270 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼4-Chloroaniline <0.270
0.395 0.200 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼4-Chloro-3-methylphenol <0.200
0.395 0.248 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2-Chloronaphthalene <0.248
0.395 0.227 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2-Chlorophenol <0.227
0.395 0.239 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼4-Chlorophenyl phenyl ether <0.239
0.0796 0.0439 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Chrysene <0.0439
0.791 0.134 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Cresols <0.134
0.0796 0.0380 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Dibenz(a,h)anthracene <0.0380
0.395 0.249 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Dibenzofuran <0.249
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-5Client Sample ID: SB-3 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.226 0.395 0.226 mg/Kg ☼12/08/16 11:04 12/09/16 21:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.395 0.226 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼1,3-Dichlorobenzene <0.226
0.395 0.233 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼1,4-Dichlorobenzene <0.233
0.796 0.242 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼3,3'-Dichlorobenzidine <0.242
0.395 0.208 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2,4-Dichlorophenol <0.208
0.395 0.252 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Diethyl phthalate <0.252
0.796 0.398 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2,4-Dimethylphenol <0.398
0.395 0.246 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Dimethyl phthalate <0.246
0.395 0.251 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Di-n-butyl phthalate <0.251
0.395 0.272 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼4,6-Dinitro-2-methylphenol <0.272
0.395 0.298 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2,4-Dinitrophenol <0.298
0.395 0.247 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2,4-Dinitrotoluene <0.247
0.395 0.265 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2,6-Dinitrotoluene <0.265
0.395 0.211 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Di-n-octyl phthalate <0.211
0.0796 0.0404 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Fluoranthene <0.0404
0.0796 0.0344 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Fluorene <0.0344
0.395 0.297 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Hexachlorobenzene <0.297
0.395 0.198 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Hexachlorobutadiene <0.198
0.395 0.178 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Hexachlorocyclopentadiene <0.178
0.395 0.215 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Hexachloroethane <0.215
0.0796 0.0344 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Indeno[1,2,3-cd]pyrene <0.0344
0.395 0.223 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Isophorone <0.223
0.0796 0.0333 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼1-Methylnaphthalene <0.0333
0.0796 0.0309 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2-Methylnaphthalene <0.0309
0.395 0.257 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2-Methylphenol <0.257
0.395 0.241 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼3 & 4 Methylphenol <0.241
0.0796 0.0344 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Naphthalene <0.0344
0.395 0.246 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2-Nitroaniline <0.246
0.796 0.273 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼3-Nitroaniline <0.273
0.796 0.283 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼4-Nitroaniline <0.283
0.395 0.239 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Nitrobenzene <0.239
0.395 0.289 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2-Nitrophenol <0.289
0.796 0.454 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼4-Nitrophenol <0.454
0.395 0.230 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼N-Nitrosodi-n-propylamine <0.230
0.395 0.0629 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0629
0.796 0.316 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Pentachlorophenol <0.316
0.0796 0.0404 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Phenanthrene <0.0404
0.395 0.241 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Phenol <0.241
0.0796 0.0404 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼Pyrene <0.0404
0.395 0.215 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼1,2,4-Trichlorobenzene <0.215
0.395 0.259 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2,4,5-Trichlorophenol <0.259
0.395 0.228 mg/Kg 12/08/16 11:04 12/09/16 21:39 1☼2,4,6-Trichlorophenol <0.228
2-Fluorobiphenyl (Surr)49 29-120 12/08/16 11:04 12/09/16 21:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)43 12/08/16 11:04 12/09/16 21:39 110-120
Nitrobenzene-d5 (Surr)47 12/08/16 11:04 12/09/16 21:39 127-120
Phenol-d5 (Surr)44 12/08/16 11:04 12/09/16 21:39 110-120
Terphenyl-d14 (Surr)54 12/08/16 11:04 12/09/16 21:39 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-5Client Sample ID: SB-3 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)55 10-120 12/08/16 11:04 12/09/16 21:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic 3.75 2.37 1.42 mg/Kg ☼12/08/16 12:08 12/08/16 21:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.37 1.19 mg/Kg 12/08/16 12:08 12/08/16 21:58 1☼Barium 59.5
1.19 0.119 mg/Kg 12/08/16 12:08 12/08/16 21:58 1☼Cadmium <0.119
1.19 1.07 mg/Kg 12/08/16 12:08 12/08/16 21:58 1☼Chromium 28.6
1.19 0.594 mg/Kg 12/08/16 12:08 12/08/16 21:58 1☼Lead 17.7
2.37 1.31 mg/Kg 12/08/16 12:08 12/08/16 21:58 1☼Selenium 2.92
1.18 0.472 mg/Kg 12/09/16 15:11 12/10/16 05:38 1☼Silver <0.472
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0343 0.114 0.0343 mg/Kg ☼12/09/16 08:38 12/09/16 15:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 84.1 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-6Client Sample ID: SB-3 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0875 0.0502 0.00844 mg/Kg ☼12/06/16 11:05 12/08/16 18:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Benzene <0.000673
0.00201 0.000723 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Bromobenzene <0.000723
0.00201 0.000552 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Bromochloromethane <0.000552
0.00201 0.000552 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Bromodichloromethane <0.000552
0.00201 0.000552 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Bromoform <0.000552
0.00201 0.00121 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Bromomethane <0.00121
0.0502 0.00512 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼2-Butanone (MEK)<0.00512
0.00502 0.00362 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Carbon disulfide <0.00362
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Carbon tetrachloride <0.000673
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Chlorobenzene <0.000673
0.00201 0.000342 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Chlorodibromomethane <0.000342
0.00502 0.00191 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Chloroethane <0.00191
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Chloroform <0.000673
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Chloromethane <0.000673
0.00201 0.000894 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼2-Chlorotoluene <0.000894
0.00201 0.000844 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼4-Chlorotoluene <0.000844
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼cis-1,2-Dichloroethene <0.000673
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼cis-1,3-Dichloropropene <0.000673
0.00502 0.000703 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2-Dibromo-3-Chloropropane <0.000703
0.00201 0.00100 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2-Dibromoethane (EDB)<0.00100
0.00201 0.000563 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Dibromomethane <0.000563
0.00201 0.000342 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2-Dichlorobenzene <0.000342
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,3-Dichlorobenzene <0.000673
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,4-Dichlorobenzene <0.000673
0.00201 0.00100 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Dichlorodifluoromethane <0.00100
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,1-Dichloroethane <0.000673
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2-Dichloroethane <0.000673
0.00201 0.000573 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,1-Dichloroethene <0.000573
0.00201 0.000472 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2-Dichloroethene, Total <0.000472
0.00201 0.000944 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2-Dichloropropane <0.000944
0.00201 0.000944 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,3-Dichloropropane <0.000944
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼2,2-Dichloropropane <0.000673
0.00201 0.000512 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,1-Dichloropropene <0.000512
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Diisopropyl ether <0.000673
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Ethylbenzene <0.000673
0.00502 0.00115 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Hexachlorobutadiene <0.00115
0.0502 0.0168 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼2-Hexanone <0.0168
0.00201 0.000412 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Isopropylbenzene <0.000412
0.0100 0.000864 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Methylene Chloride <0.000864
0.0502 0.00191 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼4-Methyl-2-pentanone (MIBK)<0.00191
0.00201 0.000964 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Methyl tert-butyl ether <0.000964
0.00502 0.00171 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Naphthalene <0.00171
0.00201 0.000984 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼n-Butylbenzene <0.000984
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼N-Propylbenzene <0.000673
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼p-Isopropyltoluene 0.00954
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼sec-Butylbenzene <0.000673
0.00201 0.00110 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Styrene <0.00110
0.00201 0.000904 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼tert-Butylbenzene <0.000904
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-6Client Sample ID: SB-3 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000673 0.00201 0.000673 mg/Kg ☼12/06/16 11:05 12/08/16 18:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00201 0.00100 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,1,2,2-Tetrachloroethane <0.00100
0.00201 0.000733 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Tetrachloroethene <0.000733
0.00201 0.000743 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Toluene 0.00269
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼trans-1,2-Dichloroethene <0.000673
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼trans-1,3-Dichloropropene <0.000673
0.00201 0.000382 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2,3-Trichlorobenzene <0.000382
0.00201 0.000673 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2,4-Trichlorobenzene <0.000673
0.00201 0.000924 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,1,1-Trichloroethane <0.000924
0.00502 0.00141 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,1,2-Trichloroethane <0.00141
0.00201 0.000964 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Trichloroethene <0.000964
0.00201 0.00100 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Trichlorofluoromethane <0.00100
0.00201 0.000552 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2,3-Trichloropropane <0.000552
0.00201 0.00100 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,2,4-Trimethylbenzene <0.00100
0.00201 0.000753 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼1,3,5-Trimethylbenzene <0.000753
0.00201 0.00110 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Vinyl chloride <0.00110
0.00603 0.00124 mg/Kg 12/06/16 11:05 12/08/16 18:42 1☼Xylenes, Total <0.00124
4-Bromofluorobenzene (Surr)86 70-130 12/06/16 11:05 12/08/16 18:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)129 12/06/16 11:05 12/08/16 18:42 170-130
1,2-Dichloroethane-d4 (Surr)113 12/06/16 11:05 12/08/16 18:42 170-130
Toluene-d8 (Surr)89 12/06/16 11:05 12/08/16 18:42 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0403 0.0845 0.0403 mg/Kg ☼12/08/16 11:04 12/09/16 21:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0845 0.0366 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Acenaphthylene <0.0366
0.0845 0.0366 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Anthracene <0.0366
0.0845 0.0378 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Benzo[a]anthracene <0.0378
0.0845 0.0340 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Benzo[a]pyrene <0.0340
0.0845 0.0353 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Benzo[b]fluoranthene <0.0353
0.0845 0.0416 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Benzo[g,h,i]perylene <0.0416
0.0845 0.0340 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Benzo[k]fluoranthene <0.0340
0.420 0.252 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Bis(2-chloroethoxy)methane <0.252
0.420 0.269 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Bis(2-chloroethyl)ether <0.269
0.420 0.250 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼bis (2-chloroisopropyl) ether <0.250
0.420 0.261 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Bis(2-ethylhexyl) phthalate <0.261
0.420 0.258 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼4-Bromophenyl phenyl ether <0.258
0.420 0.271 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Butyl benzyl phthalate <0.271
0.420 0.261 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Carbazole <0.261
0.420 0.286 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼4-Chloroaniline <0.286
0.420 0.212 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼4-Chloro-3-methylphenol <0.212
0.420 0.263 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2-Chloronaphthalene <0.263
0.420 0.241 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2-Chlorophenol <0.241
0.420 0.253 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼4-Chlorophenyl phenyl ether <0.253
0.0845 0.0466 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Chrysene <0.0466
0.840 0.142 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Cresols <0.142
0.0845 0.0403 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Dibenz(a,h)anthracene <0.0403
0.420 0.265 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Dibenzofuran <0.265
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-6Client Sample ID: SB-3 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.240 0.420 0.240 mg/Kg ☼12/08/16 11:04 12/09/16 21:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.420 0.240 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼1,3-Dichlorobenzene <0.240
0.420 0.247 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼1,4-Dichlorobenzene <0.247
0.845 0.257 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼3,3'-Dichlorobenzidine <0.257
0.420 0.221 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2,4-Dichlorophenol <0.221
0.420 0.267 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Diethyl phthalate <0.267
0.845 0.422 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2,4-Dimethylphenol <0.422
0.420 0.261 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Dimethyl phthalate <0.261
0.420 0.266 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Di-n-butyl phthalate <0.266
0.420 0.289 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼4,6-Dinitro-2-methylphenol <0.289
0.420 0.316 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2,4-Dinitrophenol <0.316
0.420 0.262 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2,4-Dinitrotoluene <0.262
0.420 0.281 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2,6-Dinitrotoluene <0.281
0.420 0.224 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Di-n-octyl phthalate <0.224
0.0845 0.0429 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Fluoranthene <0.0429
0.0845 0.0366 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Fluorene <0.0366
0.420 0.315 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Hexachlorobenzene <0.315
0.420 0.211 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Hexachlorobutadiene <0.211
0.420 0.189 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Hexachlorocyclopentadiene <0.189
0.420 0.228 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Hexachloroethane <0.228
0.0845 0.0366 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Indeno[1,2,3-cd]pyrene <0.0366
0.420 0.237 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Isophorone <0.237
0.0845 0.0353 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼1-Methylnaphthalene <0.0353
0.0845 0.0328 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2-Methylnaphthalene <0.0328
0.420 0.272 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2-Methylphenol <0.272
0.420 0.256 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼3 & 4 Methylphenol <0.256
0.0845 0.0366 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Naphthalene <0.0366
0.420 0.261 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2-Nitroaniline <0.261
0.845 0.290 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼3-Nitroaniline <0.290
0.845 0.300 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼4-Nitroaniline <0.300
0.420 0.253 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Nitrobenzene <0.253
0.420 0.306 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2-Nitrophenol <0.306
0.845 0.482 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼4-Nitrophenol <0.482
0.420 0.245 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼N-Nitrosodi-n-propylamine <0.245
0.420 0.0668 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0668
0.845 0.335 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Pentachlorophenol <0.335
0.0845 0.0429 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Phenanthrene <0.0429
0.420 0.256 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Phenol <0.256
0.0845 0.0429 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼Pyrene <0.0429
0.420 0.228 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼1,2,4-Trichlorobenzene <0.228
0.420 0.275 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2,4,5-Trichlorophenol <0.275
0.420 0.242 mg/Kg 12/08/16 11:04 12/09/16 21:58 1☼2,4,6-Trichlorophenol <0.242
2-Fluorobiphenyl (Surr)70 29-120 12/08/16 11:04 12/09/16 21:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)66 12/08/16 11:04 12/09/16 21:58 110-120
Nitrobenzene-d5 (Surr)68 12/08/16 11:04 12/09/16 21:58 127-120
Phenol-d5 (Surr)66 12/08/16 11:04 12/09/16 21:58 110-120
Terphenyl-d14 (Surr)74 12/08/16 11:04 12/09/16 21:58 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-6Client Sample ID: SB-3 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)77 10-120 12/08/16 11:04 12/09/16 21:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.47 2.45 1.47 mg/Kg ☼12/09/16 09:26 12/09/16 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.45 1.23 mg/Kg 12/09/16 09:26 12/09/16 13:06 1☼Barium 13.3
1.23 0.123 mg/Kg 12/09/16 09:26 12/09/16 13:06 1☼Cadmium 2.60
1.23 1.10 mg/Kg 12/09/16 09:26 12/09/16 13:06 1☼Chromium 27.9
1.23 0.613 mg/Kg 12/09/16 09:26 12/09/16 13:06 1☼Lead 22.5
2.45 1.35 mg/Kg 12/09/16 09:26 12/09/16 13:06 1☼Selenium <1.35
1.23 0.491 mg/Kg 12/09/16 09:26 12/09/16 13:06 1☼Silver <0.491
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0369 0.123 0.0369 mg/Kg ☼12/09/16 08:38 12/09/16 15:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 78.7 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-7Client Sample ID: SB-4 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.171 0.0681 0.0114 mg/Kg ☼12/06/16 11:40 12/08/16 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Benzene <0.000912
0.00272 0.000980 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Bromobenzene <0.000980
0.00272 0.000749 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Bromochloromethane <0.000749
0.00272 0.000749 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Bromodichloromethane <0.000749
0.00272 0.000749 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Bromoform <0.000749
0.00272 0.00163 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Bromomethane 0.00239 J
0.0681 0.00694 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼2-Butanone (MEK)0.0108 J
0.00681 0.00490 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Carbon disulfide <0.00490
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Carbon tetrachloride <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Chlorobenzene <0.000912
0.00272 0.000463 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Chlorodibromomethane <0.000463
0.00681 0.00259 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Chloroethane <0.00259
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Chloroform <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Chloromethane <0.000912
0.00272 0.00121 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼2-Chlorotoluene <0.00121
0.00272 0.00114 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼4-Chlorotoluene <0.00114
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼cis-1,2-Dichloroethene <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼cis-1,3-Dichloropropene <0.000912
0.00681 0.000953 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2-Dibromo-3-Chloropropane <0.000953
0.00272 0.00136 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2-Dibromoethane (EDB)<0.00136
0.00272 0.000762 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Dibromomethane <0.000762
0.00272 0.000463 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2-Dichlorobenzene <0.000463
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,3-Dichlorobenzene <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,4-Dichlorobenzene <0.000912
0.00272 0.00136 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Dichlorodifluoromethane <0.00136
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,1-Dichloroethane <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2-Dichloroethane <0.000912
0.00272 0.000776 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,1-Dichloroethene <0.000776
0.00272 0.000640 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2-Dichloroethene, Total <0.000640
0.00272 0.00128 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2-Dichloropropane <0.00128
0.00272 0.00128 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,3-Dichloropropane <0.00128
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼2,2-Dichloropropane <0.000912
0.00272 0.000694 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,1-Dichloropropene <0.000694
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Diisopropyl ether <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Ethylbenzene <0.000912
0.00681 0.00155 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Hexachlorobutadiene <0.00155
0.0681 0.0227 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼2-Hexanone <0.0227
0.00272 0.000558 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Isopropylbenzene <0.000558
0.0136 0.00117 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Methylene Chloride <0.00117
0.0681 0.00259 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼4-Methyl-2-pentanone (MIBK)<0.00259
0.00272 0.00131 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Methyl tert-butyl ether <0.00131
0.00681 0.00231 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Naphthalene <0.00231
0.00272 0.00133 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼n-Butylbenzene <0.00133
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼N-Propylbenzene <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼p-Isopropyltoluene <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼sec-Butylbenzene <0.000912
0.00272 0.00150 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Styrene <0.00150
0.00272 0.00122 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼tert-Butylbenzene <0.00122
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-7Client Sample ID: SB-4 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000912 0.00272 0.000912 mg/Kg ☼12/06/16 11:40 12/08/16 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00272 0.00136 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,1,2,2-Tetrachloroethane <0.00136
0.00272 0.000994 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Tetrachloroethene <0.000994
0.00272 0.00101 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Toluene <0.00101
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼trans-1,2-Dichloroethene <0.000912
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼trans-1,3-Dichloropropene <0.000912
0.00272 0.000517 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2,3-Trichlorobenzene <0.000517
0.00272 0.000912 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2,4-Trichlorobenzene <0.000912
0.00272 0.00125 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,1,1-Trichloroethane <0.00125
0.00681 0.00191 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,1,2-Trichloroethane <0.00191
0.00272 0.00131 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Trichloroethene <0.00131
0.00272 0.00136 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Trichlorofluoromethane <0.00136
0.00272 0.000749 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2,3-Trichloropropane <0.000749
0.00272 0.00136 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,2,4-Trimethylbenzene 0.00193 J
0.00272 0.00102 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼1,3,5-Trimethylbenzene <0.00102
0.00272 0.00150 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Vinyl chloride <0.00150
0.00817 0.00167 mg/Kg 12/06/16 11:40 12/08/16 18:12 1☼Xylenes, Total <0.00167
4-Bromofluorobenzene (Surr)92 70-130 12/06/16 11:40 12/08/16 18:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)118 12/06/16 11:40 12/08/16 18:12 170-130
1,2-Dichloroethane-d4 (Surr)114 12/06/16 11:40 12/08/16 18:12 170-130
Toluene-d8 (Surr)90 12/06/16 11:40 12/08/16 18:12 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0400 0.0837 0.0400 mg/Kg ☼12/08/16 11:04 12/09/16 22:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0837 0.0362 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Acenaphthylene <0.0362
0.0837 0.0362 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Anthracene <0.0362
0.0837 0.0375 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Benzo[a]anthracene <0.0375
0.0837 0.0337 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Benzo[a]pyrene <0.0337
0.0837 0.0350 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Benzo[b]fluoranthene <0.0350
0.0837 0.0412 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Benzo[g,h,i]perylene <0.0412
0.0837 0.0337 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Benzo[k]fluoranthene <0.0337
0.416 0.250 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Bis(2-chloroethoxy)methane <0.250
0.416 0.266 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Bis(2-chloroethyl)ether <0.266
0.416 0.247 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼bis (2-chloroisopropyl) ether <0.247
0.416 0.259 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Bis(2-ethylhexyl) phthalate <0.259
0.416 0.256 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼4-Bromophenyl phenyl ether <0.256
0.416 0.269 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Butyl benzyl phthalate <0.269
0.416 0.259 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Carbazole <0.259
0.416 0.284 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼4-Chloroaniline <0.284
0.416 0.210 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼4-Chloro-3-methylphenol <0.210
0.416 0.261 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2-Chloronaphthalene <0.261
0.416 0.239 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2-Chlorophenol <0.239
0.416 0.251 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼4-Chlorophenyl phenyl ether <0.251
0.0837 0.0462 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Chrysene <0.0462
0.832 0.141 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Cresols <0.141
0.0837 0.0400 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Dibenz(a,h)anthracene <0.0400
0.416 0.262 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Dibenzofuran <0.262
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-7Client Sample ID: SB-4 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.237 0.416 0.237 mg/Kg ☼12/08/16 11:04 12/09/16 22:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.416 0.237 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼1,3-Dichlorobenzene <0.237
0.416 0.245 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼1,4-Dichlorobenzene <0.245
0.837 0.255 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼3,3'-Dichlorobenzidine <0.255
0.416 0.219 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2,4-Dichlorophenol <0.219
0.416 0.265 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Diethyl phthalate <0.265
0.837 0.419 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2,4-Dimethylphenol <0.419
0.416 0.259 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Dimethyl phthalate <0.259
0.416 0.264 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Di-n-butyl phthalate <0.264
0.416 0.286 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼4,6-Dinitro-2-methylphenol <0.286
0.416 0.314 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2,4-Dinitrophenol <0.314
0.416 0.260 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2,4-Dinitrotoluene <0.260
0.416 0.279 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2,6-Dinitrotoluene <0.279
0.416 0.222 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Di-n-octyl phthalate <0.222
0.0837 0.0425 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Fluoranthene <0.0425
0.0837 0.0362 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Fluorene <0.0362
0.416 0.312 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Hexachlorobenzene <0.312
0.416 0.209 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Hexachlorobutadiene <0.209
0.416 0.187 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Hexachlorocyclopentadiene <0.187
0.416 0.226 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Hexachloroethane <0.226
0.0837 0.0362 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Indeno[1,2,3-cd]pyrene <0.0362
0.416 0.235 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Isophorone <0.235
0.0837 0.0350 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼1-Methylnaphthalene <0.0350
0.0837 0.0325 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2-Methylnaphthalene <0.0325
0.416 0.270 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2-Methylphenol <0.270
0.416 0.254 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼3 & 4 Methylphenol <0.254
0.0837 0.0362 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Naphthalene <0.0362
0.416 0.259 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2-Nitroaniline <0.259
0.837 0.287 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼3-Nitroaniline <0.287
0.837 0.297 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼4-Nitroaniline <0.297
0.416 0.251 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Nitrobenzene <0.251
0.416 0.304 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2-Nitrophenol <0.304
0.837 0.477 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼4-Nitrophenol <0.477
0.416 0.242 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼N-Nitrosodi-n-propylamine <0.242
0.416 0.0662 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0662
0.837 0.332 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Pentachlorophenol <0.332
0.0837 0.0425 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Phenanthrene <0.0425
0.416 0.254 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Phenol <0.254
0.0837 0.0425 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼Pyrene <0.0425
0.416 0.226 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼1,2,4-Trichlorobenzene <0.226
0.416 0.272 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2,4,5-Trichlorophenol <0.272
0.416 0.240 mg/Kg 12/08/16 11:04 12/09/16 22:16 1☼2,4,6-Trichlorophenol <0.240
2-Fluorobiphenyl (Surr)65 29-120 12/08/16 11:04 12/09/16 22:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)60 12/08/16 11:04 12/09/16 22:16 110-120
Nitrobenzene-d5 (Surr)56 12/08/16 11:04 12/09/16 22:16 127-120
Phenol-d5 (Surr)62 12/08/16 11:04 12/09/16 22:16 110-120
Terphenyl-d14 (Surr)69 12/08/16 11:04 12/09/16 22:16 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-7Client Sample ID: SB-4 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)70 10-120 12/08/16 11:04 12/09/16 22:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.50 2.51 1.50 mg/Kg ☼12/09/16 09:26 12/09/16 14:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.51 1.25 mg/Kg 12/09/16 09:26 12/09/16 14:13 1☼Barium 70.8
1.25 0.125 mg/Kg 12/09/16 09:26 12/09/16 14:13 1☼Cadmium 1.68
1.25 1.13 mg/Kg 12/09/16 09:26 12/09/16 14:13 1☼Chromium 32.9
1.25 0.626 mg/Kg 12/09/16 09:26 12/09/16 14:13 1☼Lead 20.5
2.51 1.38 mg/Kg 12/09/16 09:26 12/09/16 14:13 1☼Selenium <1.38
1.25 0.501 mg/Kg 12/09/16 09:26 12/09/16 14:13 1☼Silver <0.501
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0367 0.122 0.0367 mg/Kg ☼12/09/16 08:38 12/09/16 15:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 80.0 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-8Client Sample ID: SB-4 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0923 0.0703 0.0118 mg/Kg ☼12/06/16 11:40 12/08/16 17:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Benzene <0.000942
0.00281 0.00101 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Bromobenzene <0.00101
0.00281 0.000774 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Bromochloromethane <0.000774
0.00281 0.000774 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Bromodichloromethane <0.000774
0.00281 0.000774 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Bromoform <0.000774
0.00281 0.00169 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Bromomethane <0.00169
0.0703 0.00717 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼2-Butanone (MEK)<0.00717
0.00703 0.00506 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Carbon disulfide <0.00506
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Carbon tetrachloride <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Chlorobenzene <0.000942
0.00281 0.000478 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Chlorodibromomethane <0.000478
0.00703 0.00267 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Chloroethane <0.00267
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Chloroform <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Chloromethane <0.000942
0.00281 0.00125 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼2-Chlorotoluene <0.00125
0.00281 0.00118 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼4-Chlorotoluene <0.00118
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼cis-1,2-Dichloroethene <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼cis-1,3-Dichloropropene <0.000942
0.00703 0.000985 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2-Dibromo-3-Chloropropane <0.000985
0.00281 0.00141 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2-Dibromoethane (EDB)<0.00141
0.00281 0.000788 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Dibromomethane <0.000788
0.00281 0.000478 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2-Dichlorobenzene <0.000478
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,3-Dichlorobenzene <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,4-Dichlorobenzene <0.000942
0.00281 0.00141 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Dichlorodifluoromethane <0.00141
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,1-Dichloroethane <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2-Dichloroethane <0.000942
0.00281 0.000802 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,1-Dichloroethene <0.000802
0.00281 0.000661 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2-Dichloroethene, Total <0.000661
0.00281 0.00132 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2-Dichloropropane <0.00132
0.00281 0.00132 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,3-Dichloropropane <0.00132
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼2,2-Dichloropropane <0.000942
0.00281 0.000717 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,1-Dichloropropene <0.000717
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Diisopropyl ether <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Ethylbenzene <0.000942
0.00703 0.00160 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Hexachlorobutadiene <0.00160
0.0703 0.0235 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼2-Hexanone <0.0235
0.00281 0.000577 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Isopropylbenzene <0.000577
0.0141 0.00121 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Methylene Chloride <0.00121
0.0703 0.00267 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼4-Methyl-2-pentanone (MIBK)<0.00267
0.00281 0.00135 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Methyl tert-butyl ether <0.00135
0.00703 0.00239 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Naphthalene <0.00239
0.00281 0.00138 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼n-Butylbenzene <0.00138
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼N-Propylbenzene <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼p-Isopropyltoluene <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼sec-Butylbenzene <0.000942
0.00281 0.00155 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Styrene <0.00155
0.00281 0.00127 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼tert-Butylbenzene <0.00127
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-8Client Sample ID: SB-4 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000942 0.00281 0.000942 mg/Kg ☼12/06/16 11:40 12/08/16 17:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00281 0.00141 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,1,2,2-Tetrachloroethane <0.00141
0.00281 0.00103 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Tetrachloroethene <0.00103
0.00281 0.00104 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Toluene <0.00104
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼trans-1,2-Dichloroethene <0.000942
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼trans-1,3-Dichloropropene <0.000942
0.00281 0.000535 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2,3-Trichlorobenzene <0.000535
0.00281 0.000942 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2,4-Trichlorobenzene <0.000942
0.00281 0.00129 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,1,1-Trichloroethane <0.00129
0.00703 0.00197 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,1,2-Trichloroethane <0.00197
0.00281 0.00135 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Trichloroethene <0.00135
0.00281 0.00141 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Trichlorofluoromethane <0.00141
0.00281 0.000774 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2,3-Trichloropropane <0.000774
0.00281 0.00141 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,2,4-Trimethylbenzene <0.00141
0.00281 0.00105 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼1,3,5-Trimethylbenzene <0.00105
0.00281 0.00155 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Vinyl chloride <0.00155
0.00844 0.00173 mg/Kg 12/06/16 11:40 12/08/16 17:43 1☼Xylenes, Total <0.00173
4-Bromofluorobenzene (Surr)92 70-130 12/06/16 11:40 12/08/16 17:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)116 12/06/16 11:40 12/08/16 17:43 170-130
1,2-Dichloroethane-d4 (Surr)108 12/06/16 11:40 12/08/16 17:43 170-130
Toluene-d8 (Surr)88 12/06/16 11:40 12/08/16 17:43 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0405 0.0848 0.0405 mg/Kg ☼12/08/16 11:04 12/09/16 22:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0848 0.0367 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Acenaphthylene <0.0367
0.0848 0.0367 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Anthracene <0.0367
0.0848 0.0380 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Benzo[a]anthracene <0.0380
0.0848 0.0342 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Benzo[a]pyrene <0.0342
0.0848 0.0354 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Benzo[b]fluoranthene <0.0354
0.0848 0.0418 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Benzo[g,h,i]perylene <0.0418
0.0848 0.0342 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Benzo[k]fluoranthene <0.0342
0.422 0.253 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Bis(2-chloroethoxy)methane <0.253
0.422 0.270 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Bis(2-chloroethyl)ether <0.270
0.422 0.251 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼bis (2-chloroisopropyl) ether <0.251
0.422 0.262 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Bis(2-ethylhexyl) phthalate <0.262
0.422 0.260 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼4-Bromophenyl phenyl ether <0.260
0.422 0.272 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Butyl benzyl phthalate <0.272
0.422 0.262 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Carbazole <0.262
0.422 0.287 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼4-Chloroaniline <0.287
0.422 0.213 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼4-Chloro-3-methylphenol <0.213
0.422 0.265 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2-Chloronaphthalene <0.265
0.422 0.242 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2-Chlorophenol <0.242
0.422 0.254 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼4-Chlorophenyl phenyl ether <0.254
0.0848 0.0468 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Chrysene <0.0468
0.843 0.143 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Cresols <0.143
0.0848 0.0405 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Dibenz(a,h)anthracene <0.0405
0.422 0.266 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Dibenzofuran <0.266
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-8Client Sample ID: SB-4 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.241 0.422 0.241 mg/Kg ☼12/08/16 11:04 12/09/16 22:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.422 0.241 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼1,3-Dichlorobenzene <0.241
0.422 0.248 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼1,4-Dichlorobenzene <0.248
0.848 0.258 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼3,3'-Dichlorobenzidine <0.258
0.422 0.222 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2,4-Dichlorophenol <0.222
0.422 0.268 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Diethyl phthalate <0.268
0.848 0.424 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2,4-Dimethylphenol <0.424
0.422 0.262 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Dimethyl phthalate <0.262
0.422 0.267 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Di-n-butyl phthalate <0.267
0.422 0.290 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼4,6-Dinitro-2-methylphenol <0.290
0.422 0.318 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2,4-Dinitrophenol <0.318
0.422 0.263 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2,4-Dinitrotoluene <0.263
0.422 0.282 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2,6-Dinitrotoluene <0.282
0.422 0.225 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Di-n-octyl phthalate <0.225
0.0848 0.0430 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Fluoranthene <0.0430
0.0848 0.0367 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Fluorene <0.0367
0.422 0.316 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Hexachlorobenzene <0.316
0.422 0.211 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Hexachlorobutadiene <0.211
0.422 0.190 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Hexachlorocyclopentadiene <0.190
0.422 0.229 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Hexachloroethane <0.229
0.0848 0.0367 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Indeno[1,2,3-cd]pyrene <0.0367
0.422 0.238 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Isophorone <0.238
0.0848 0.0354 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼1-Methylnaphthalene <0.0354
0.0848 0.0329 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2-Methylnaphthalene <0.0329
0.422 0.273 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2-Methylphenol <0.273
0.422 0.257 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼3 & 4 Methylphenol <0.257
0.0848 0.0367 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Naphthalene <0.0367
0.422 0.262 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2-Nitroaniline <0.262
0.848 0.291 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼3-Nitroaniline <0.291
0.848 0.301 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼4-Nitroaniline <0.301
0.422 0.254 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Nitrobenzene <0.254
0.422 0.308 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2-Nitrophenol <0.308
0.848 0.484 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼4-Nitrophenol <0.484
0.422 0.246 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼N-Nitrosodi-n-propylamine <0.246
0.422 0.0671 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0671
0.848 0.337 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Pentachlorophenol <0.337
0.0848 0.0430 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Phenanthrene <0.0430
0.422 0.257 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Phenol <0.257
0.0848 0.0430 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼Pyrene <0.0430
0.422 0.229 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼1,2,4-Trichlorobenzene <0.229
0.422 0.276 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2,4,5-Trichlorophenol <0.276
0.422 0.243 mg/Kg 12/08/16 11:04 12/09/16 22:35 1☼2,4,6-Trichlorophenol <0.243
2-Fluorobiphenyl (Surr)60 29-120 12/08/16 11:04 12/09/16 22:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)56 12/08/16 11:04 12/09/16 22:35 110-120
Nitrobenzene-d5 (Surr)59 12/08/16 11:04 12/09/16 22:35 127-120
Phenol-d5 (Surr)58 12/08/16 11:04 12/09/16 22:35 110-120
Terphenyl-d14 (Surr)70 12/08/16 11:04 12/09/16 22:35 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-8Client Sample ID: SB-4 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)69 10-120 12/08/16 11:04 12/09/16 22:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.56 2.59 1.56 mg/Kg ☼12/09/16 09:26 12/09/16 14:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.59 1.30 mg/Kg 12/09/16 09:26 12/09/16 14:29 1☼Barium 14.9
1.30 0.130 mg/Kg 12/09/16 09:26 12/09/16 14:29 1☼Cadmium 2.13
1.30 1.17 mg/Kg 12/09/16 09:26 12/09/16 14:29 1☼Chromium 29.4
1.30 0.648 mg/Kg 12/09/16 09:26 12/09/16 14:29 1☼Lead 19.0
2.59 1.43 mg/Kg 12/09/16 09:26 12/09/16 14:29 1☼Selenium <1.43
1.30 0.519 mg/Kg 12/09/16 09:26 12/09/16 14:29 1☼Silver <0.519
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0384 0.128 0.0384 mg/Kg ☼12/09/16 08:38 12/09/16 15:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 77.9 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-9Client Sample ID: SB-5 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.161 0.0572 0.00960 mg/Kg ☼12/06/16 11:15 12/08/16 17:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Benzene <0.000766
0.00229 0.000823 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Bromobenzene <0.000823
0.00229 0.000629 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Bromochloromethane <0.000629
0.00229 0.000629 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Bromodichloromethane <0.000629
0.00229 0.000629 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Bromoform <0.000629
0.00229 0.00137 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Bromomethane <0.00137
0.0572 0.00583 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼2-Butanone (MEK)<0.00583
0.00572 0.00411 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Carbon disulfide <0.00411
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Carbon tetrachloride <0.000766
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Chlorobenzene <0.000766
0.00229 0.000389 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Chlorodibromomethane <0.000389
0.00572 0.00217 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Chloroethane <0.00217
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Chloroform <0.000766
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Chloromethane <0.000766
0.00229 0.00102 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼2-Chlorotoluene <0.00102
0.00229 0.000960 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼4-Chlorotoluene <0.000960
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼cis-1,2-Dichloroethene <0.000766
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼cis-1,3-Dichloropropene <0.000766
0.00572 0.000800 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2-Dibromo-3-Chloropropane <0.000800
0.00229 0.00114 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2-Dibromoethane (EDB)<0.00114
0.00229 0.000640 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Dibromomethane <0.000640
0.00229 0.000389 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2-Dichlorobenzene <0.000389
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,3-Dichlorobenzene <0.000766
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,4-Dichlorobenzene <0.000766
0.00229 0.00114 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Dichlorodifluoromethane <0.00114
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,1-Dichloroethane <0.000766
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2-Dichloroethane <0.000766
0.00229 0.000652 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,1-Dichloroethene <0.000652
0.00229 0.000537 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2-Dichloroethene, Total <0.000537
0.00229 0.00107 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2-Dichloropropane <0.00107
0.00229 0.00107 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,3-Dichloropropane <0.00107
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼2,2-Dichloropropane <0.000766
0.00229 0.000583 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,1-Dichloropropene <0.000583
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Diisopropyl ether <0.000766
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Ethylbenzene <0.000766
0.00572 0.00130 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Hexachlorobutadiene <0.00130
0.0572 0.0191 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼2-Hexanone <0.0191
0.00229 0.000469 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Isopropylbenzene <0.000469
0.0114 0.000983 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Methylene Chloride <0.000983
0.0572 0.00217 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼4-Methyl-2-pentanone (MIBK)<0.00217
0.00229 0.00110 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Methyl tert-butyl ether <0.00110
0.00572 0.00194 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Naphthalene <0.00194
0.00229 0.00112 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼n-Butylbenzene <0.00112
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼N-Propylbenzene <0.000766
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼p-Isopropyltoluene 0.00461
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼sec-Butylbenzene <0.000766
0.00229 0.00126 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Styrene <0.00126
0.00229 0.00103 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼tert-Butylbenzene <0.00103
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-9Client Sample ID: SB-5 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000766 0.00229 0.000766 mg/Kg ☼12/06/16 11:15 12/08/16 17:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00229 0.00114 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,1,2,2-Tetrachloroethane <0.00114
0.00229 0.000834 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Tetrachloroethene <0.000834
0.00229 0.000846 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Toluene <0.000846
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼trans-1,2-Dichloroethene <0.000766
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼trans-1,3-Dichloropropene <0.000766
0.00229 0.000434 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2,3-Trichlorobenzene <0.000434
0.00229 0.000766 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2,4-Trichlorobenzene <0.000766
0.00229 0.00105 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,1,1-Trichloroethane <0.00105
0.00572 0.00160 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,1,2-Trichloroethane <0.00160
0.00229 0.00110 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Trichloroethene <0.00110
0.00229 0.00114 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Trichlorofluoromethane <0.00114
0.00229 0.000629 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2,3-Trichloropropane <0.000629
0.00229 0.00114 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,2,4-Trimethylbenzene <0.00114
0.00229 0.000857 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼1,3,5-Trimethylbenzene <0.000857
0.00229 0.00126 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Vinyl chloride <0.00126
0.00686 0.00141 mg/Kg 12/06/16 11:15 12/08/16 17:14 1☼Xylenes, Total <0.00141
4-Bromofluorobenzene (Surr)92 70-130 12/06/16 11:15 12/08/16 17:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)115 12/06/16 11:15 12/08/16 17:14 170-130
1,2-Dichloroethane-d4 (Surr)108 12/06/16 11:15 12/08/16 17:14 170-130
Toluene-d8 (Surr)92 12/06/16 11:15 12/08/16 17:14 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0391 0.0818 0.0391 mg/Kg ☼12/08/16 12:11 12/09/16 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0818 0.0354 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Acenaphthylene <0.0354
0.0818 0.0354 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Anthracene <0.0354
0.0818 0.0366 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Benzo[a]anthracene <0.0366
0.0818 0.0330 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Benzo[a]pyrene <0.0330
0.0818 0.0342 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Benzo[b]fluoranthene <0.0342
0.0818 0.0403 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Benzo[g,h,i]perylene <0.0403
0.0818 0.0330 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Benzo[k]fluoranthene <0.0330
0.407 0.244 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Bis(2-chloroethoxy)methane <0.244
0.407 0.260 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Bis(2-chloroethyl)ether <0.260
0.407 0.242 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼bis (2-chloroisopropyl) ether <0.242
0.407 0.253 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Bis(2-ethylhexyl) phthalate <0.253
0.407 0.250 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼4-Bromophenyl phenyl ether <0.250
0.407 0.262 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Butyl benzyl phthalate <0.262
0.407 0.253 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Carbazole <0.253
0.407 0.277 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼4-Chloroaniline <0.277
0.407 0.205 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼4-Chloro-3-methylphenol <0.205
0.407 0.255 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2-Chloronaphthalene <0.255
0.407 0.233 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2-Chlorophenol <0.233
0.407 0.245 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼4-Chlorophenyl phenyl ether <0.245
0.0818 0.0452 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Chrysene <0.0452
0.813 0.138 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Cresols <0.138
0.0818 0.0391 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Dibenz(a,h)anthracene <0.0391
0.407 0.256 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Dibenzofuran <0.256
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-9Client Sample ID: SB-5 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.232 0.407 0.232 mg/Kg ☼12/08/16 12:11 12/09/16 13:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.407 0.232 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼1,3-Dichlorobenzene <0.232
0.407 0.239 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼1,4-Dichlorobenzene <0.239
0.818 0.249 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼3,3'-Dichlorobenzidine <0.249
0.407 0.214 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2,4-Dichlorophenol <0.214
0.407 0.259 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Diethyl phthalate <0.259
0.818 0.409 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2,4-Dimethylphenol <0.409
0.407 0.253 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Dimethyl phthalate <0.253
0.407 0.258 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Di-n-butyl phthalate <0.258
0.407 0.280 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼4,6-Dinitro-2-methylphenol <0.280
0.407 0.306 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2,4-Dinitrophenol <0.306
0.407 0.254 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2,4-Dinitrotoluene <0.254
0.407 0.272 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2,6-Dinitrotoluene <0.272
0.407 0.217 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Di-n-octyl phthalate <0.217
0.0818 0.0415 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Fluoranthene <0.0415
0.0818 0.0354 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Fluorene <0.0354
0.407 0.305 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Hexachlorobenzene <0.305
0.407 0.204 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Hexachlorobutadiene <0.204
0.407 0.183 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Hexachlorocyclopentadiene <0.183
0.407 0.221 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Hexachloroethane <0.221
0.0818 0.0354 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Indeno[1,2,3-cd]pyrene <0.0354
0.407 0.230 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Isophorone <0.230
0.0818 0.0342 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼1-Methylnaphthalene <0.0342
0.0818 0.0317 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2-Methylnaphthalene <0.0317
0.407 0.264 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2-Methylphenol <0.264
0.407 0.248 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼3 & 4 Methylphenol <0.248
0.0818 0.0354 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Naphthalene <0.0354
0.407 0.253 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2-Nitroaniline <0.253
0.818 0.281 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼3-Nitroaniline <0.281
0.818 0.291 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼4-Nitroaniline <0.291
0.407 0.245 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Nitrobenzene <0.245
0.407 0.297 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2-Nitrophenol <0.297
0.818 0.466 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼4-Nitrophenol <0.466
0.407 0.237 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼N-Nitrosodi-n-propylamine <0.237
0.407 0.0647 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0647
0.818 0.325 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Pentachlorophenol <0.325
0.0818 0.0415 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Phenanthrene <0.0415
0.407 0.248 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Phenol <0.248
0.0818 0.0415 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼Pyrene <0.0415
0.407 0.221 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼1,2,4-Trichlorobenzene <0.221
0.407 0.266 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2,4,5-Trichlorophenol <0.266
0.407 0.234 mg/Kg 12/08/16 12:11 12/09/16 13:12 1☼2,4,6-Trichlorophenol <0.234
2-Fluorobiphenyl (Surr)54 29-120 12/08/16 12:11 12/09/16 13:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)52 12/08/16 12:11 12/09/16 13:12 110-120
Nitrobenzene-d5 (Surr)54 12/08/16 12:11 12/09/16 13:12 127-120
Phenol-d5 (Surr)55 12/08/16 12:11 12/09/16 13:12 110-120
Terphenyl-d14 (Surr)74 12/08/16 12:11 12/09/16 13:12 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-9Client Sample ID: SB-5 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)75 10-120 12/08/16 12:11 12/09/16 13:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.42 2.36 1.42 mg/Kg ☼12/09/16 09:26 12/09/16 14:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.36 1.18 mg/Kg 12/09/16 09:26 12/09/16 14:34 1☼Barium 33.7
1.18 0.118 mg/Kg 12/09/16 09:26 12/09/16 14:34 1☼Cadmium 1.58
1.18 1.06 mg/Kg 12/09/16 09:26 12/09/16 14:34 1☼Chromium 38.9
1.18 0.590 mg/Kg 12/09/16 09:26 12/09/16 14:34 1☼Lead 18.4
2.36 1.30 mg/Kg 12/09/16 09:26 12/09/16 14:34 1☼Selenium <1.30
1.18 0.472 mg/Kg 12/09/16 09:26 12/09/16 14:34 1☼Silver <0.472
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0367 0.122 0.0367 mg/Kg ☼12/09/16 08:38 12/09/16 15:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 81.1 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-10Client Sample ID: SB-5 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0743 J 0.0784 0.0132 mg/Kg ☼12/06/16 11:15 12/08/16 16:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Benzene <0.00105
0.00314 0.00113 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Bromobenzene <0.00113
0.00314 0.000862 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Bromochloromethane <0.000862
0.00314 0.000862 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Bromodichloromethane <0.000862
0.00314 0.000862 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Bromoform <0.000862
0.00314 0.00188 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Bromomethane <0.00188
0.0784 0.00800 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼2-Butanone (MEK)<0.00800
0.00784 0.00564 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Carbon disulfide <0.00564
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Carbon tetrachloride <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Chlorobenzene <0.00105
0.00314 0.000533 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Chlorodibromomethane <0.000533
0.00784 0.00298 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Chloroethane <0.00298
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Chloroform <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Chloromethane <0.00105
0.00314 0.00140 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼2-Chlorotoluene <0.00140
0.00314 0.00132 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼4-Chlorotoluene <0.00132
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼cis-1,2-Dichloroethene <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼cis-1,3-Dichloropropene <0.00105
0.00784 0.00110 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2-Dibromo-3-Chloropropane <0.00110
0.00314 0.00157 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2-Dibromoethane (EDB)<0.00157
0.00314 0.000878 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Dibromomethane <0.000878
0.00314 0.000533 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2-Dichlorobenzene <0.000533
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,3-Dichlorobenzene <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,4-Dichlorobenzene <0.00105
0.00314 0.00157 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Dichlorodifluoromethane <0.00157
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,1-Dichloroethane <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2-Dichloroethane <0.00105
0.00314 0.000894 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,1-Dichloroethene <0.000894
0.00314 0.000737 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2-Dichloroethene, Total <0.000737
0.00314 0.00147 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2-Dichloropropane <0.00147
0.00314 0.00147 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,3-Dichloropropane <0.00147
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼2,2-Dichloropropane <0.00105
0.00314 0.000800 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,1-Dichloropropene <0.000800
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Diisopropyl ether <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Ethylbenzene <0.00105
0.00784 0.00179 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Hexachlorobutadiene <0.00179
0.0784 0.0262 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼2-Hexanone <0.0262
0.00314 0.000643 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Isopropylbenzene <0.000643
0.0157 0.00135 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Methylene Chloride <0.00135
0.0784 0.00298 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼4-Methyl-2-pentanone (MIBK)<0.00298
0.00314 0.00150 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Methyl tert-butyl ether <0.00150
0.00784 0.00267 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Naphthalene <0.00267
0.00314 0.00154 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼n-Butylbenzene <0.00154
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼N-Propylbenzene <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼p-Isopropyltoluene <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼sec-Butylbenzene <0.00105
0.00314 0.00172 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Styrene <0.00172
0.00314 0.00141 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼tert-Butylbenzene <0.00141
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-10Client Sample ID: SB-5 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.00105 0.00314 0.00105 mg/Kg ☼12/06/16 11:15 12/08/16 16:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00314 0.00157 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,1,2,2-Tetrachloroethane <0.00157
0.00314 0.00114 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Tetrachloroethene <0.00114
0.00314 0.00116 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Toluene <0.00116
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼trans-1,2-Dichloroethene <0.00105
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼trans-1,3-Dichloropropene <0.00105
0.00314 0.000596 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2,3-Trichlorobenzene <0.000596
0.00314 0.00105 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2,4-Trichlorobenzene <0.00105
0.00314 0.00144 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,1,1-Trichloroethane <0.00144
0.00784 0.00219 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,1,2-Trichloroethane <0.00219
0.00314 0.00150 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Trichloroethene <0.00150
0.00314 0.00157 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Trichlorofluoromethane <0.00157
0.00314 0.000862 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2,3-Trichloropropane <0.000862
0.00314 0.00157 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,2,4-Trimethylbenzene <0.00157
0.00314 0.00118 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼1,3,5-Trimethylbenzene <0.00118
0.00314 0.00172 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Vinyl chloride <0.00172
0.00941 0.00193 mg/Kg 12/06/16 11:15 12/08/16 16:44 1☼Xylenes, Total <0.00193
4-Bromofluorobenzene (Surr)90 70-130 12/06/16 11:15 12/08/16 16:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)111 12/06/16 11:15 12/08/16 16:44 170-130
1,2-Dichloroethane-d4 (Surr)102 12/06/16 11:15 12/08/16 16:44 170-130
Toluene-d8 (Surr)88 12/06/16 11:15 12/08/16 16:44 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0408 0.0854 0.0408 mg/Kg ☼12/08/16 12:11 12/09/16 13:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0854 0.0370 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Acenaphthylene <0.0370
0.0854 0.0370 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Anthracene <0.0370
0.0854 0.0382 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Benzo[a]anthracene <0.0382
0.0854 0.0344 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Benzo[a]pyrene <0.0344
0.0854 0.0357 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Benzo[b]fluoranthene <0.0357
0.0854 0.0421 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Benzo[g,h,i]perylene <0.0421
0.0854 0.0344 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Benzo[k]fluoranthene <0.0344
0.425 0.255 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Bis(2-chloroethoxy)methane <0.255
0.425 0.272 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Bis(2-chloroethyl)ether <0.272
0.425 0.252 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼bis (2-chloroisopropyl) ether <0.252
0.425 0.264 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Bis(2-ethylhexyl) phthalate <0.264
0.425 0.261 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼4-Bromophenyl phenyl ether <0.261
0.425 0.274 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Butyl benzyl phthalate <0.274
0.425 0.264 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Carbazole <0.264
0.425 0.289 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼4-Chloroaniline <0.289
0.425 0.214 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼4-Chloro-3-methylphenol <0.214
0.425 0.266 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2-Chloronaphthalene <0.266
0.425 0.243 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2-Chlorophenol <0.243
0.425 0.256 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼4-Chlorophenyl phenyl ether <0.256
0.0854 0.0472 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Chrysene <0.0472
0.849 0.144 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Cresols <0.144
0.0854 0.0408 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Dibenz(a,h)anthracene <0.0408
0.425 0.268 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Dibenzofuran <0.268
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-10Client Sample ID: SB-5 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.242 0.425 0.242 mg/Kg ☼12/08/16 12:11 12/09/16 13:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.425 0.242 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼1,3-Dichlorobenzene <0.242
0.425 0.250 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼1,4-Dichlorobenzene <0.250
0.854 0.260 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼3,3'-Dichlorobenzidine <0.260
0.425 0.223 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2,4-Dichlorophenol <0.223
0.425 0.270 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Diethyl phthalate <0.270
0.854 0.427 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2,4-Dimethylphenol <0.427
0.425 0.264 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Dimethyl phthalate <0.264
0.425 0.269 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Di-n-butyl phthalate <0.269
0.425 0.292 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼4,6-Dinitro-2-methylphenol <0.292
0.425 0.320 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2,4-Dinitrophenol <0.320
0.425 0.265 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2,4-Dinitrotoluene <0.265
0.425 0.284 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2,6-Dinitrotoluene <0.284
0.425 0.227 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Di-n-octyl phthalate <0.227
0.0854 0.0433 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Fluoranthene <0.0433
0.0854 0.0370 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Fluorene <0.0370
0.425 0.319 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Hexachlorobenzene <0.319
0.425 0.213 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Hexachlorobutadiene <0.213
0.425 0.191 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Hexachlorocyclopentadiene <0.191
0.425 0.231 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Hexachloroethane <0.231
0.0854 0.0370 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Indeno[1,2,3-cd]pyrene <0.0370
0.425 0.240 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Isophorone <0.240
0.0854 0.0357 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼1-Methylnaphthalene <0.0357
0.0854 0.0331 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2-Methylnaphthalene <0.0331
0.425 0.275 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2-Methylphenol <0.275
0.425 0.259 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼3 & 4 Methylphenol <0.259
0.0854 0.0370 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Naphthalene <0.0370
0.425 0.264 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2-Nitroaniline <0.264
0.854 0.293 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼3-Nitroaniline <0.293
0.854 0.303 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼4-Nitroaniline <0.303
0.425 0.256 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Nitrobenzene <0.256
0.425 0.310 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2-Nitrophenol <0.310
0.854 0.487 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼4-Nitrophenol <0.487
0.425 0.247 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼N-Nitrosodi-n-propylamine <0.247
0.425 0.0676 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0676
0.854 0.339 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Pentachlorophenol <0.339
0.0854 0.0433 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Phenanthrene <0.0433
0.425 0.259 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Phenol <0.259
0.0854 0.0433 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼Pyrene <0.0433
0.425 0.231 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼1,2,4-Trichlorobenzene <0.231
0.425 0.278 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2,4,5-Trichlorophenol <0.278
0.425 0.245 mg/Kg 12/08/16 12:11 12/09/16 13:30 1☼2,4,6-Trichlorophenol <0.245
2-Fluorobiphenyl (Surr)50 29-120 12/08/16 12:11 12/09/16 13:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)50 12/08/16 12:11 12/09/16 13:30 110-120
Nitrobenzene-d5 (Surr)49 12/08/16 12:11 12/09/16 13:30 127-120
Phenol-d5 (Surr)53 12/08/16 12:11 12/09/16 13:30 110-120
Terphenyl-d14 (Surr)72 12/08/16 12:11 12/09/16 13:30 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-10Client Sample ID: SB-5 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)72 10-120 12/08/16 12:11 12/09/16 13:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.55 2.59 1.55 mg/Kg ☼12/09/16 09:26 12/09/16 14:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.59 1.29 mg/Kg 12/09/16 09:26 12/09/16 14:40 1☼Barium 13.8
1.29 0.129 mg/Kg 12/09/16 09:26 12/09/16 14:40 1☼Cadmium 2.72
1.29 1.17 mg/Kg 12/09/16 09:26 12/09/16 14:40 1☼Chromium 75.3
1.29 0.647 mg/Kg 12/09/16 09:26 12/09/16 14:40 1☼Lead 23.7
2.59 1.42 mg/Kg 12/09/16 09:26 12/09/16 14:40 1☼Selenium <1.42
1.29 0.518 mg/Kg 12/09/16 09:26 12/09/16 14:40 1☼Silver <0.518
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0375 0.125 0.0375 mg/Kg ☼12/09/16 08:38 12/09/16 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 76.8 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-11Client Sample ID: SB-6 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.123 0.0674 0.0113 mg/Kg ☼12/06/16 11:45 12/08/16 16:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Benzene <0.000903
0.00269 0.000970 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Bromobenzene <0.000970
0.00269 0.000741 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Bromochloromethane <0.000741
0.00269 0.000741 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Bromodichloromethane <0.000741
0.00269 0.000741 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Bromoform <0.000741
0.00269 0.00162 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Bromomethane <0.00162
0.0674 0.00687 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼2-Butanone (MEK)<0.00687
0.00674 0.00485 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Carbon disulfide <0.00485
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Carbon tetrachloride <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Chlorobenzene <0.000903
0.00269 0.000458 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Chlorodibromomethane <0.000458
0.00674 0.00256 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Chloroethane <0.00256
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Chloroform <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Chloromethane <0.000903
0.00269 0.00120 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼2-Chlorotoluene <0.00120
0.00269 0.00113 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼4-Chlorotoluene <0.00113
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼cis-1,2-Dichloroethene <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼cis-1,3-Dichloropropene <0.000903
0.00674 0.000943 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2-Dibromo-3-Chloropropane <0.000943
0.00269 0.00135 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2-Dibromoethane (EDB)<0.00135
0.00269 0.000754 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Dibromomethane <0.000754
0.00269 0.000458 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2-Dichlorobenzene <0.000458
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,3-Dichlorobenzene <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,4-Dichlorobenzene <0.000903
0.00269 0.00135 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Dichlorodifluoromethane <0.00135
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,1-Dichloroethane <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2-Dichloroethane <0.000903
0.00269 0.000768 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,1-Dichloroethene <0.000768
0.00269 0.000633 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2-Dichloroethene, Total <0.000633
0.00269 0.00127 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2-Dichloropropane <0.00127
0.00269 0.00127 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,3-Dichloropropane <0.00127
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼2,2-Dichloropropane <0.000903
0.00269 0.000687 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,1-Dichloropropene <0.000687
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Diisopropyl ether <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Ethylbenzene <0.000903
0.00674 0.00154 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Hexachlorobutadiene <0.00154
0.0674 0.0225 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼2-Hexanone <0.0225
0.00269 0.000552 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Isopropylbenzene <0.000552
0.0135 0.00116 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Methylene Chloride <0.00116
0.0674 0.00256 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼4-Methyl-2-pentanone (MIBK)<0.00256
0.00269 0.00129 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Methyl tert-butyl ether <0.00129
0.00674 0.00229 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Naphthalene <0.00229
0.00269 0.00132 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼n-Butylbenzene <0.00132
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼N-Propylbenzene <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼p-Isopropyltoluene <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼sec-Butylbenzene <0.000903
0.00269 0.00148 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Styrene <0.00148
0.00269 0.00121 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼tert-Butylbenzene <0.00121
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-11Client Sample ID: SB-6 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000903 0.00269 0.000903 mg/Kg ☼12/06/16 11:45 12/08/16 16:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00269 0.00135 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,1,2,2-Tetrachloroethane <0.00135
0.00269 0.000983 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Tetrachloroethene <0.000983
0.00269 0.000997 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Toluene <0.000997
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼trans-1,2-Dichloroethene <0.000903
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼trans-1,3-Dichloropropene <0.000903
0.00269 0.000512 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2,3-Trichlorobenzene <0.000512
0.00269 0.000903 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2,4-Trichlorobenzene <0.000903
0.00269 0.00124 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,1,1-Trichloroethane <0.00124
0.00674 0.00189 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,1,2-Trichloroethane <0.00189
0.00269 0.00129 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Trichloroethene <0.00129
0.00269 0.00135 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Trichlorofluoromethane <0.00135
0.00269 0.000741 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2,3-Trichloropropane <0.000741
0.00269 0.00135 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,2,4-Trimethylbenzene <0.00135
0.00269 0.00101 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼1,3,5-Trimethylbenzene <0.00101
0.00269 0.00148 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Vinyl chloride <0.00148
0.00808 0.00166 mg/Kg 12/06/16 11:45 12/08/16 16:15 1☼Xylenes, Total <0.00166
4-Bromofluorobenzene (Surr)89 70-130 12/06/16 11:45 12/08/16 16:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)117 12/06/16 11:45 12/08/16 16:15 170-130
1,2-Dichloroethane-d4 (Surr)109 12/06/16 11:45 12/08/16 16:15 170-130
Toluene-d8 (Surr)91 12/06/16 11:45 12/08/16 16:15 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0393 0.0822 0.0393 mg/Kg ☼12/08/16 12:11 12/09/16 13:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0822 0.0356 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Acenaphthylene <0.0356
0.0822 0.0356 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Anthracene <0.0356
0.0822 0.0368 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Benzo[a]anthracene <0.0368
0.0822 0.0331 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Benzo[a]pyrene <0.0331
0.0822 0.0344 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Benzo[b]fluoranthene <0.0344
0.0822 0.0405 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Benzo[g,h,i]perylene <0.0405
0.0822 0.0331 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Benzo[k]fluoranthene <0.0331
0.409 0.245 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Bis(2-chloroethoxy)methane <0.245
0.409 0.261 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Bis(2-chloroethyl)ether <0.261
0.409 0.243 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼bis (2-chloroisopropyl) ether <0.243
0.409 0.254 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Bis(2-ethylhexyl) phthalate <0.254
0.409 0.252 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼4-Bromophenyl phenyl ether <0.252
0.409 0.264 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Butyl benzyl phthalate <0.264
0.409 0.254 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Carbazole <0.254
0.409 0.279 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼4-Chloroaniline <0.279
0.409 0.206 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼4-Chloro-3-methylphenol <0.206
0.409 0.256 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2-Chloronaphthalene <0.256
0.409 0.234 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2-Chlorophenol <0.234
0.409 0.247 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼4-Chlorophenyl phenyl ether <0.247
0.0822 0.0454 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Chrysene <0.0454
0.817 0.139 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Cresols <0.139
0.0822 0.0393 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Dibenz(a,h)anthracene <0.0393
0.409 0.258 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Dibenzofuran <0.258
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-11Client Sample ID: SB-6 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.233 0.409 0.233 mg/Kg ☼12/08/16 12:11 12/09/16 13:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.409 0.233 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼1,3-Dichlorobenzene <0.233
0.409 0.241 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼1,4-Dichlorobenzene <0.241
0.822 0.250 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼3,3'-Dichlorobenzidine <0.250
0.409 0.215 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2,4-Dichlorophenol <0.215
0.409 0.260 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Diethyl phthalate <0.260
0.822 0.411 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2,4-Dimethylphenol <0.411
0.409 0.254 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Dimethyl phthalate <0.254
0.409 0.259 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Di-n-butyl phthalate <0.259
0.409 0.281 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼4,6-Dinitro-2-methylphenol <0.281
0.409 0.308 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2,4-Dinitrophenol <0.308
0.409 0.255 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2,4-Dinitrotoluene <0.255
0.409 0.274 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2,6-Dinitrotoluene <0.274
0.409 0.218 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Di-n-octyl phthalate <0.218
0.0822 0.0417 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Fluoranthene <0.0417
0.0822 0.0356 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Fluorene <0.0356
0.409 0.307 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Hexachlorobenzene <0.307
0.409 0.205 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Hexachlorobutadiene <0.205
0.409 0.184 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Hexachlorocyclopentadiene <0.184
0.409 0.222 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Hexachloroethane <0.222
0.0822 0.0356 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Indeno[1,2,3-cd]pyrene <0.0356
0.409 0.231 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Isophorone <0.231
0.0822 0.0344 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼1-Methylnaphthalene <0.0344
0.0822 0.0319 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2-Methylnaphthalene <0.0319
0.409 0.265 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2-Methylphenol <0.265
0.409 0.249 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼3 & 4 Methylphenol <0.249
0.0822 0.0356 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Naphthalene <0.0356
0.409 0.254 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2-Nitroaniline <0.254
0.822 0.282 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼3-Nitroaniline <0.282
0.822 0.292 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼4-Nitroaniline <0.292
0.409 0.247 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Nitrobenzene <0.247
0.409 0.298 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2-Nitrophenol <0.298
0.822 0.469 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼4-Nitrophenol <0.469
0.409 0.238 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼N-Nitrosodi-n-propylamine <0.238
0.409 0.0650 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0650
0.822 0.326 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Pentachlorophenol <0.326
0.0822 0.0417 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Phenanthrene <0.0417
0.409 0.249 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Phenol <0.249
0.0822 0.0417 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼Pyrene <0.0417
0.409 0.222 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼1,2,4-Trichlorobenzene <0.222
0.409 0.268 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2,4,5-Trichlorophenol <0.268
0.409 0.236 mg/Kg 12/08/16 12:11 12/09/16 13:49 1☼2,4,6-Trichlorophenol <0.236
2-Fluorobiphenyl (Surr)47 29-120 12/08/16 12:11 12/09/16 13:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)44 12/08/16 12:11 12/09/16 13:49 110-120
Nitrobenzene-d5 (Surr)42 12/08/16 12:11 12/09/16 13:49 127-120
Phenol-d5 (Surr)47 12/08/16 12:11 12/09/16 13:49 110-120
Terphenyl-d14 (Surr)67 12/08/16 12:11 12/09/16 13:49 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-11Client Sample ID: SB-6 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)71 10-120 12/08/16 12:11 12/09/16 13:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.49 2.48 1.49 mg/Kg ☼12/09/16 09:26 12/09/16 14:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.48 1.24 mg/Kg 12/09/16 09:26 12/09/16 14:45 1☼Barium 14.4
1.24 0.124 mg/Kg 12/09/16 09:26 12/09/16 14:45 1☼Cadmium 2.71
1.24 1.12 mg/Kg 12/09/16 09:26 12/09/16 14:45 1☼Chromium 37.9
1.24 0.621 mg/Kg 12/09/16 09:26 12/09/16 14:45 1☼Lead 28.9
2.48 1.37 mg/Kg 12/09/16 09:26 12/09/16 14:45 1☼Selenium <1.37
1.24 0.497 mg/Kg 12/09/16 09:26 12/09/16 14:45 1☼Silver <0.497
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0382 0.127 0.0382 mg/Kg ☼12/09/16 08:38 12/09/16 16:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 79.3 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-12Client Sample ID: SB-6 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <0.0106 0.0633 0.0106 mg/Kg ☼12/06/16 11:45 12/08/16 15:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Benzene <0.000848
0.00253 0.000911 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Bromobenzene <0.000911
0.00253 0.000696 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Bromochloromethane <0.000696
0.00253 0.000696 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Bromodichloromethane <0.000696
0.00253 0.000696 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Bromoform <0.000696
0.00253 0.00152 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Bromomethane <0.00152
0.0633 0.00645 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼2-Butanone (MEK)<0.00645
0.00633 0.00456 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Carbon disulfide <0.00456
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Carbon tetrachloride <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Chlorobenzene <0.000848
0.00253 0.000430 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Chlorodibromomethane <0.000430
0.00633 0.00240 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Chloroethane <0.00240
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Chloroform <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Chloromethane <0.000848
0.00253 0.00113 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼2-Chlorotoluene <0.00113
0.00253 0.00106 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼4-Chlorotoluene <0.00106
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼cis-1,2-Dichloroethene <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼cis-1,3-Dichloropropene <0.000848
0.00633 0.000886 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2-Dibromo-3-Chloropropane <0.000886
0.00253 0.00127 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2-Dibromoethane (EDB)<0.00127
0.00253 0.000709 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Dibromomethane <0.000709
0.00253 0.000430 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2-Dichlorobenzene <0.000430
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,3-Dichlorobenzene <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,4-Dichlorobenzene <0.000848
0.00253 0.00127 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Dichlorodifluoromethane <0.00127
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,1-Dichloroethane <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2-Dichloroethane <0.000848
0.00253 0.000721 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,1-Dichloroethene <0.000721
0.00253 0.000595 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2-Dichloroethene, Total <0.000595
0.00253 0.00119 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2-Dichloropropane <0.00119
0.00253 0.00119 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,3-Dichloropropane <0.00119
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼2,2-Dichloropropane <0.000848
0.00253 0.000645 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,1-Dichloropropene <0.000645
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Diisopropyl ether <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Ethylbenzene <0.000848
0.00633 0.00144 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Hexachlorobutadiene <0.00144
0.0633 0.0211 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼2-Hexanone <0.0211
0.00253 0.000519 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Isopropylbenzene <0.000519
0.0127 0.00109 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Methylene Chloride <0.00109
0.0633 0.00240 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼4-Methyl-2-pentanone (MIBK)<0.00240
0.00253 0.00121 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Methyl tert-butyl ether <0.00121
0.00633 0.00215 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Naphthalene <0.00215
0.00253 0.00124 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼n-Butylbenzene <0.00124
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼N-Propylbenzene <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼p-Isopropyltoluene <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼sec-Butylbenzene <0.000848
0.00253 0.00139 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Styrene <0.00139
0.00253 0.00114 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼tert-Butylbenzene <0.00114
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-12Client Sample ID: SB-6 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000848 0.00253 0.000848 mg/Kg ☼12/06/16 11:45 12/08/16 15:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00253 0.00127 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,1,2,2-Tetrachloroethane <0.00127
0.00253 0.000924 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Tetrachloroethene <0.000924
0.00253 0.000936 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Toluene <0.000936
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼trans-1,2-Dichloroethene <0.000848
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼trans-1,3-Dichloropropene <0.000848
0.00253 0.000481 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2,3-Trichlorobenzene <0.000481
0.00253 0.000848 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2,4-Trichlorobenzene <0.000848
0.00253 0.00116 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,1,1-Trichloroethane <0.00116
0.00633 0.00177 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,1,2-Trichloroethane <0.00177
0.00253 0.00121 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Trichloroethene <0.00121
0.00253 0.00127 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Trichlorofluoromethane <0.00127
0.00253 0.000696 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2,3-Trichloropropane <0.000696
0.00253 0.00127 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,2,4-Trimethylbenzene <0.00127
0.00253 0.000949 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼1,3,5-Trimethylbenzene <0.000949
0.00253 0.00139 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Vinyl chloride <0.00139
0.00759 0.00156 mg/Kg 12/06/16 11:45 12/08/16 15:45 1☼Xylenes, Total <0.00156
4-Bromofluorobenzene (Surr)91 70-130 12/06/16 11:45 12/08/16 15:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)126 12/06/16 11:45 12/08/16 15:45 170-130
1,2-Dichloroethane-d4 (Surr)110 12/06/16 11:45 12/08/16 15:45 170-130
Toluene-d8 (Surr)88 12/06/16 11:45 12/08/16 15:45 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0385 0.0805 0.0385 mg/Kg ☼12/08/16 12:11 12/09/16 14:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0805 0.0349 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Acenaphthylene <0.0349
0.0805 0.0349 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Anthracene <0.0349
0.0805 0.0361 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Benzo[a]anthracene <0.0361
0.0805 0.0324 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Benzo[a]pyrene <0.0324
0.0805 0.0337 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Benzo[b]fluoranthene <0.0337
0.0805 0.0397 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Benzo[g,h,i]perylene <0.0397
0.0805 0.0324 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Benzo[k]fluoranthene <0.0324
0.400 0.240 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Bis(2-chloroethoxy)methane <0.240
0.400 0.256 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Bis(2-chloroethyl)ether <0.256
0.400 0.238 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼bis (2-chloroisopropyl) ether <0.238
0.400 0.249 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Bis(2-ethylhexyl) phthalate <0.249
0.400 0.246 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼4-Bromophenyl phenyl ether <0.246
0.400 0.258 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Butyl benzyl phthalate <0.258
0.400 0.249 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Carbazole <0.249
0.400 0.273 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼4-Chloroaniline <0.273
0.400 0.202 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼4-Chloro-3-methylphenol <0.202
0.400 0.251 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2-Chloronaphthalene <0.251
0.400 0.230 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2-Chlorophenol <0.230
0.400 0.242 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼4-Chlorophenyl phenyl ether <0.242
0.0805 0.0445 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Chrysene <0.0445
0.800 0.136 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Cresols <0.136
0.0805 0.0385 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Dibenz(a,h)anthracene <0.0385
0.400 0.252 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Dibenzofuran <0.252
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-12Client Sample ID: SB-6 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.228 0.400 0.228 mg/Kg ☼12/08/16 12:11 12/09/16 14:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.400 0.228 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼1,3-Dichlorobenzene <0.228
0.400 0.236 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼1,4-Dichlorobenzene <0.236
0.805 0.245 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼3,3'-Dichlorobenzidine <0.245
0.400 0.210 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2,4-Dichlorophenol <0.210
0.400 0.255 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Diethyl phthalate <0.255
0.805 0.403 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2,4-Dimethylphenol <0.403
0.400 0.249 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Dimethyl phthalate <0.249
0.400 0.254 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Di-n-butyl phthalate <0.254
0.400 0.275 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼4,6-Dinitro-2-methylphenol <0.275
0.400 0.302 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2,4-Dinitrophenol <0.302
0.400 0.250 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2,4-Dinitrotoluene <0.250
0.400 0.268 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2,6-Dinitrotoluene <0.268
0.400 0.214 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Di-n-octyl phthalate <0.214
0.0805 0.0409 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Fluoranthene <0.0409
0.0805 0.0349 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Fluorene <0.0349
0.400 0.300 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Hexachlorobenzene <0.300
0.400 0.201 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Hexachlorobutadiene <0.201
0.400 0.180 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Hexachlorocyclopentadiene <0.180
0.400 0.218 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Hexachloroethane <0.218
0.0805 0.0349 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Indeno[1,2,3-cd]pyrene <0.0349
0.400 0.226 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Isophorone <0.226
0.0805 0.0337 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼1-Methylnaphthalene <0.0337
0.0805 0.0312 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2-Methylnaphthalene <0.0312
0.400 0.260 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2-Methylphenol <0.260
0.400 0.244 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼3 & 4 Methylphenol <0.244
0.0805 0.0349 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Naphthalene <0.0349
0.400 0.249 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2-Nitroaniline <0.249
0.805 0.276 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼3-Nitroaniline <0.276
0.805 0.286 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼4-Nitroaniline <0.286
0.400 0.242 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Nitrobenzene <0.242
0.400 0.292 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2-Nitrophenol <0.292
0.805 0.459 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼4-Nitrophenol <0.459
0.400 0.233 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼N-Nitrosodi-n-propylamine <0.233
0.400 0.0637 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0637
0.805 0.320 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Pentachlorophenol <0.320
0.0805 0.0409 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Phenanthrene <0.0409
0.400 0.244 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Phenol <0.244
0.0805 0.0409 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼Pyrene <0.0409
0.400 0.218 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼1,2,4-Trichlorobenzene <0.218
0.400 0.262 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2,4,5-Trichlorophenol <0.262
0.400 0.231 mg/Kg 12/08/16 12:11 12/09/16 14:07 1☼2,4,6-Trichlorophenol <0.231
2-Fluorobiphenyl (Surr)46 29-120 12/08/16 12:11 12/09/16 14:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)45 12/08/16 12:11 12/09/16 14:07 110-120
Nitrobenzene-d5 (Surr)45 12/08/16 12:11 12/09/16 14:07 127-120
Phenol-d5 (Surr)45 12/08/16 12:11 12/09/16 14:07 110-120
Terphenyl-d14 (Surr)63 12/08/16 12:11 12/09/16 14:07 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-12Client Sample ID: SB-6 (3-4)
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)61 10-120 12/08/16 12:11 12/09/16 14:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.48 2.47 1.48 mg/Kg ☼12/09/16 09:26 12/09/16 14:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.47 1.24 mg/Kg 12/09/16 09:26 12/09/16 14:50 1☼Barium 5.12
1.24 0.124 mg/Kg 12/09/16 09:26 12/09/16 14:50 1☼Cadmium 1.78
1.24 1.11 mg/Kg 12/09/16 09:26 12/09/16 14:50 1☼Chromium 20.1
1.24 0.618 mg/Kg 12/09/16 09:26 12/09/16 14:50 1☼Lead 21.2
2.47 1.36 mg/Kg 12/09/16 09:26 12/09/16 14:50 1☼Selenium <1.36
1.24 0.494 mg/Kg 12/09/16 09:26 12/09/16 14:50 1☼Silver <0.494
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0367 0.122 0.0367 mg/Kg ☼12/09/16 08:38 12/09/16 16:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 80.6 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-13Client Sample ID: SB-7 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.209 0.0660 0.0111 mg/Kg ☼12/06/16 14:15 12/09/16 08:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Benzene <0.000884
0.00264 0.000950 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Bromobenzene <0.000950
0.00264 0.000726 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Bromochloromethane <0.000726
0.00264 0.000726 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Bromodichloromethane <0.000726
0.00264 0.000726 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Bromoform <0.000726
0.00264 0.00158 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Bromomethane <0.00158
0.0660 0.00673 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼2-Butanone (MEK)0.00716 J
0.00660 0.00475 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Carbon disulfide <0.00475
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Carbon tetrachloride <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Chlorobenzene <0.000884
0.00264 0.000449 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Chlorodibromomethane <0.000449
0.00660 0.00251 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Chloroethane <0.00251
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Chloroform <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Chloromethane <0.000884
0.00264 0.00117 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼2-Chlorotoluene <0.00117
0.00264 0.00111 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼4-Chlorotoluene <0.00111
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼cis-1,2-Dichloroethene <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼cis-1,3-Dichloropropene <0.000884
0.00660 0.000924 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2-Dibromo-3-Chloropropane <0.000924
0.00264 0.00132 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2-Dibromoethane (EDB)<0.00132
0.00264 0.000739 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Dibromomethane <0.000739
0.00264 0.000449 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2-Dichlorobenzene <0.000449
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,3-Dichlorobenzene <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,4-Dichlorobenzene <0.000884
0.00264 0.00132 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Dichlorodifluoromethane <0.00132
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,1-Dichloroethane <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2-Dichloroethane <0.000884
0.00264 0.000752 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,1-Dichloroethene <0.000752
0.00264 0.000620 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2-Dichloroethene, Total <0.000620
0.00264 0.00124 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2-Dichloropropane <0.00124
0.00264 0.00124 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,3-Dichloropropane <0.00124
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼2,2-Dichloropropane <0.000884
0.00264 0.000673 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,1-Dichloropropene <0.000673
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Diisopropyl ether <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Ethylbenzene <0.000884
0.00660 0.00150 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Hexachlorobutadiene <0.00150
0.0660 0.0220 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼2-Hexanone <0.0220
0.00264 0.000541 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Isopropylbenzene <0.000541
0.0132 0.00113 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Methylene Chloride <0.00113
0.0660 0.00251 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼4-Methyl-2-pentanone (MIBK)<0.00251
0.00264 0.00127 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Methyl tert-butyl ether <0.00127
0.00660 0.00224 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Naphthalene <0.00224
0.00264 0.00129 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼n-Butylbenzene <0.00129
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼N-Propylbenzene <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼p-Isopropyltoluene <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼sec-Butylbenzene <0.000884
0.00264 0.00145 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Styrene <0.00145
0.00264 0.00119 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼tert-Butylbenzene <0.00119
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-13Client Sample ID: SB-7 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000884 0.00264 0.000884 mg/Kg ☼12/06/16 14:15 12/09/16 08:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00264 0.00132 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,1,2,2-Tetrachloroethane <0.00132
0.00264 0.000963 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Tetrachloroethene <0.000963
0.00264 0.000977 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Toluene <0.000977
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼trans-1,2-Dichloroethene <0.000884
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼trans-1,3-Dichloropropene <0.000884
0.00264 0.000501 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2,3-Trichlorobenzene <0.000501
0.00264 0.000884 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2,4-Trichlorobenzene <0.000884
0.00264 0.00121 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,1,1-Trichloroethane <0.00121
0.00660 0.00185 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,1,2-Trichloroethane <0.00185
0.00264 0.00127 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Trichloroethene <0.00127
0.00264 0.00132 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Trichlorofluoromethane <0.00132
0.00264 0.000726 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2,3-Trichloropropane <0.000726
0.00264 0.00132 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,2,4-Trimethylbenzene <0.00132
0.00264 0.000990 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼1,3,5-Trimethylbenzene <0.000990
0.00264 0.00145 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Vinyl chloride <0.00145
0.00792 0.00162 mg/Kg 12/06/16 14:15 12/09/16 08:27 1☼Xylenes, Total <0.00162
4-Bromofluorobenzene (Surr)91 70-130 12/06/16 14:15 12/09/16 08:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)128 12/06/16 14:15 12/09/16 08:27 170-130
1,2-Dichloroethane-d4 (Surr)107 12/06/16 14:15 12/09/16 08:27 170-130
Toluene-d8 (Surr)92 12/06/16 14:15 12/09/16 08:27 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0418 0.0875 0.0418 mg/Kg ☼12/08/16 12:11 12/09/16 14:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0875 0.0379 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Acenaphthylene <0.0379
0.0875 0.0379 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Anthracene <0.0379
0.0875 0.0392 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Benzo[a]anthracene <0.0392
0.0875 0.0353 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Benzo[a]pyrene <0.0353
0.0875 0.0366 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Benzo[b]fluoranthene <0.0366
0.0875 0.0431 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Benzo[g,h,i]perylene <0.0431
0.0875 0.0353 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Benzo[k]fluoranthene <0.0353
0.435 0.261 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Bis(2-chloroethoxy)methane <0.261
0.435 0.278 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Bis(2-chloroethyl)ether <0.278
0.435 0.259 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼bis (2-chloroisopropyl) ether <0.259
0.435 0.270 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Bis(2-ethylhexyl) phthalate <0.270
0.435 0.268 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼4-Bromophenyl phenyl ether <0.268
0.435 0.281 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Butyl benzyl phthalate <0.281
0.435 0.270 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Carbazole <0.270
0.435 0.296 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼4-Chloroaniline <0.296
0.435 0.219 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼4-Chloro-3-methylphenol <0.219
0.435 0.273 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2-Chloronaphthalene <0.273
0.435 0.249 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2-Chlorophenol <0.249
0.435 0.262 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼4-Chlorophenyl phenyl ether <0.262
0.0875 0.0483 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Chrysene <0.0483
0.870 0.148 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Cresols <0.148
0.0875 0.0418 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Dibenz(a,h)anthracene <0.0418
0.435 0.274 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Dibenzofuran <0.274
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-13Client Sample ID: SB-7 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.248 0.435 0.248 mg/Kg ☼12/08/16 12:11 12/09/16 14:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.435 0.248 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼1,3-Dichlorobenzene <0.248
0.435 0.256 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼1,4-Dichlorobenzene <0.256
0.875 0.266 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼3,3'-Dichlorobenzidine <0.266
0.435 0.228 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2,4-Dichlorophenol <0.228
0.435 0.277 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Diethyl phthalate <0.277
0.875 0.437 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2,4-Dimethylphenol <0.437
0.435 0.270 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Dimethyl phthalate <0.270
0.435 0.275 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Di-n-butyl phthalate <0.275
0.435 0.299 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼4,6-Dinitro-2-methylphenol <0.299
0.435 0.328 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2,4-Dinitrophenol <0.328
0.435 0.272 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2,4-Dinitrotoluene <0.272
0.435 0.291 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2,6-Dinitrotoluene <0.291
0.435 0.232 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Di-n-octyl phthalate <0.232
0.0875 0.0444 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Fluoranthene <0.0444
0.0875 0.0379 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Fluorene <0.0379
0.435 0.326 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Hexachlorobenzene <0.326
0.435 0.218 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Hexachlorobutadiene <0.218
0.435 0.196 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Hexachlorocyclopentadiene <0.196
0.435 0.236 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Hexachloroethane <0.236
0.0875 0.0379 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Indeno[1,2,3-cd]pyrene <0.0379
0.435 0.245 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Isophorone <0.245
0.0875 0.0366 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼1-Methylnaphthalene <0.0366
0.0875 0.0339 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2-Methylnaphthalene <0.0339
0.435 0.282 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2-Methylphenol <0.282
0.435 0.265 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼3 & 4 Methylphenol <0.265
0.0875 0.0379 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Naphthalene <0.0379
0.435 0.270 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2-Nitroaniline <0.270
0.875 0.300 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼3-Nitroaniline <0.300
0.875 0.311 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼4-Nitroaniline <0.311
0.435 0.262 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Nitrobenzene <0.262
0.435 0.317 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2-Nitrophenol <0.317
0.875 0.499 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼4-Nitrophenol <0.499
0.435 0.253 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼N-Nitrosodi-n-propylamine <0.253
0.435 0.0692 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0692
0.875 0.347 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Pentachlorophenol <0.347
0.0875 0.0444 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Phenanthrene <0.0444
0.435 0.265 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Phenol <0.265
0.0875 0.0444 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼Pyrene <0.0444
0.435 0.236 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼1,2,4-Trichlorobenzene <0.236
0.435 0.285 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2,4,5-Trichlorophenol <0.285
0.435 0.251 mg/Kg 12/08/16 12:11 12/09/16 14:26 1☼2,4,6-Trichlorophenol <0.251
2-Fluorobiphenyl (Surr)56 29-120 12/08/16 12:11 12/09/16 14:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)54 12/08/16 12:11 12/09/16 14:26 110-120
Nitrobenzene-d5 (Surr)53 12/08/16 12:11 12/09/16 14:26 127-120
Phenol-d5 (Surr)59 12/08/16 12:11 12/09/16 14:26 110-120
Terphenyl-d14 (Surr)78 12/08/16 12:11 12/09/16 14:26 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-13Client Sample ID: SB-7 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)78 10-120 12/08/16 12:11 12/09/16 14:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.55 2.59 1.55 mg/Kg ☼12/09/16 09:26 12/09/16 15:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.59 1.29 mg/Kg 12/09/16 09:26 12/09/16 15:01 1☼Barium 20.1
1.29 0.129 mg/Kg 12/09/16 09:26 12/09/16 15:01 1☼Cadmium 2.92
1.29 1.16 mg/Kg 12/09/16 09:26 12/09/16 15:01 1☼Chromium 30.2
1.29 0.646 mg/Kg 12/09/16 09:26 12/09/16 15:01 1☼Lead 32.2
2.59 1.42 mg/Kg 12/09/16 09:26 12/09/16 15:01 1☼Selenium <1.42
1.29 0.517 mg/Kg 12/09/16 09:26 12/09/16 15:01 1☼Silver <0.517
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0484 J 0.127 0.0382 mg/Kg ☼12/09/16 08:38 12/09/16 16:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 75.4 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-14Client Sample ID: SB-7 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0520 J 0.0656 0.0110 mg/Kg ☼12/06/16 14:15 12/09/16 07:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Benzene <0.000879
0.00262 0.000945 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Bromobenzene <0.000945
0.00262 0.000722 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Bromochloromethane <0.000722
0.00262 0.000722 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Bromodichloromethane <0.000722
0.00262 0.000722 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Bromoform <0.000722
0.00262 0.00157 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Bromomethane <0.00157
0.0656 0.00669 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼2-Butanone (MEK)<0.00669
0.00656 0.00472 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Carbon disulfide <0.00472
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Carbon tetrachloride <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Chlorobenzene <0.000879
0.00262 0.000446 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Chlorodibromomethane <0.000446
0.00656 0.00249 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Chloroethane <0.00249
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Chloroform <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Chloromethane <0.000879
0.00262 0.00117 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼2-Chlorotoluene <0.00117
0.00262 0.00110 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼4-Chlorotoluene <0.00110
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼cis-1,2-Dichloroethene <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼cis-1,3-Dichloropropene <0.000879
0.00656 0.000918 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2-Dibromo-3-Chloropropane <0.000918
0.00262 0.00131 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2-Dibromoethane (EDB)<0.00131
0.00262 0.000735 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Dibromomethane <0.000735
0.00262 0.000446 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2-Dichlorobenzene <0.000446
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,3-Dichlorobenzene <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,4-Dichlorobenzene <0.000879
0.00262 0.00131 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Dichlorodifluoromethane <0.00131
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,1-Dichloroethane <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2-Dichloroethane <0.000879
0.00262 0.000748 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,1-Dichloroethene <0.000748
0.00262 0.000617 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2-Dichloroethene, Total <0.000617
0.00262 0.00123 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2-Dichloropropane <0.00123
0.00262 0.00123 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,3-Dichloropropane <0.00123
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼2,2-Dichloropropane <0.000879
0.00262 0.000669 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,1-Dichloropropene <0.000669
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Diisopropyl ether <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Ethylbenzene <0.000879
0.00656 0.00150 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Hexachlorobutadiene <0.00150
0.0656 0.0219 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼2-Hexanone <0.0219
0.00262 0.000538 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Isopropylbenzene <0.000538
0.0131 0.00113 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Methylene Chloride <0.00113
0.0656 0.00249 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼4-Methyl-2-pentanone (MIBK)<0.00249
0.00262 0.00126 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Methyl tert-butyl ether <0.00126
0.00656 0.00223 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Naphthalene <0.00223
0.00262 0.00129 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼n-Butylbenzene <0.00129
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼N-Propylbenzene <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼p-Isopropyltoluene <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼sec-Butylbenzene <0.000879
0.00262 0.00144 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Styrene <0.00144
0.00262 0.00118 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼tert-Butylbenzene <0.00118
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-14Client Sample ID: SB-7 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000879 0.00262 0.000879 mg/Kg ☼12/06/16 14:15 12/09/16 07:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00262 0.00131 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,1,2,2-Tetrachloroethane <0.00131
0.00262 0.000958 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Tetrachloroethene <0.000958
0.00262 0.000971 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Toluene <0.000971
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼trans-1,2-Dichloroethene <0.000879
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼trans-1,3-Dichloropropene <0.000879
0.00262 0.000498 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2,3-Trichlorobenzene <0.000498
0.00262 0.000879 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2,4-Trichlorobenzene <0.000879
0.00262 0.00121 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,1,1-Trichloroethane <0.00121
0.00656 0.00184 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,1,2-Trichloroethane <0.00184
0.00262 0.00126 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Trichloroethene <0.00126
0.00262 0.00131 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Trichlorofluoromethane <0.00131
0.00262 0.000722 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2,3-Trichloropropane <0.000722
0.00262 0.00131 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,2,4-Trimethylbenzene <0.00131
0.00262 0.000984 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼1,3,5-Trimethylbenzene <0.000984
0.00262 0.00144 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Vinyl chloride <0.00144
0.00787 0.00161 mg/Kg 12/06/16 14:15 12/09/16 07:58 1☼Xylenes, Total <0.00161
4-Bromofluorobenzene (Surr)92 70-130 12/06/16 14:15 12/09/16 07:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)121 12/06/16 14:15 12/09/16 07:58 170-130
1,2-Dichloroethane-d4 (Surr)113 12/06/16 14:15 12/09/16 07:58 170-130
Toluene-d8 (Surr)88 12/06/16 14:15 12/09/16 07:58 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0427 0.0894 0.0427 mg/Kg ☼12/08/16 12:11 12/09/16 14:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0894 0.0387 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Acenaphthylene <0.0387
0.0894 0.0387 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Anthracene <0.0387
0.0894 0.0400 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Benzo[a]anthracene <0.0400
0.0894 0.0360 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Benzo[a]pyrene <0.0360
0.0894 0.0374 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Benzo[b]fluoranthene <0.0374
0.0894 0.0440 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Benzo[g,h,i]perylene <0.0440
0.0894 0.0360 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Benzo[k]fluoranthene <0.0360
0.444 0.267 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Bis(2-chloroethoxy)methane <0.267
0.444 0.284 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Bis(2-chloroethyl)ether <0.284
0.444 0.264 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼bis (2-chloroisopropyl) ether <0.264
0.444 0.276 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Bis(2-ethylhexyl) phthalate <0.276
0.444 0.274 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼4-Bromophenyl phenyl ether <0.274
0.444 0.287 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Butyl benzyl phthalate <0.287
0.444 0.276 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Carbazole <0.276
0.444 0.303 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼4-Chloroaniline <0.303
0.444 0.224 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼4-Chloro-3-methylphenol <0.224
0.444 0.279 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2-Chloronaphthalene <0.279
0.444 0.255 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2-Chlorophenol <0.255
0.444 0.268 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼4-Chlorophenyl phenyl ether <0.268
0.0894 0.0494 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Chrysene <0.0494
0.889 0.151 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Cresols <0.151
0.0894 0.0427 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Dibenz(a,h)anthracene <0.0427
0.444 0.280 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Dibenzofuran <0.280
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-14Client Sample ID: SB-7 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.253 0.444 0.253 mg/Kg ☼12/08/16 12:11 12/09/16 14:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.444 0.253 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼1,3-Dichlorobenzene <0.253
0.444 0.261 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼1,4-Dichlorobenzene <0.261
0.894 0.272 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼3,3'-Dichlorobenzidine <0.272
0.444 0.233 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2,4-Dichlorophenol <0.233
0.444 0.283 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Diethyl phthalate <0.283
0.894 0.447 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2,4-Dimethylphenol <0.447
0.444 0.276 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Dimethyl phthalate <0.276
0.444 0.282 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Di-n-butyl phthalate <0.282
0.444 0.306 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼4,6-Dinitro-2-methylphenol <0.306
0.444 0.335 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2,4-Dinitrophenol <0.335
0.444 0.278 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2,4-Dinitrotoluene <0.278
0.444 0.298 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2,6-Dinitrotoluene <0.298
0.444 0.237 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Di-n-octyl phthalate <0.237
0.0894 0.0454 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Fluoranthene <0.0454
0.0894 0.0387 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Fluorene <0.0387
0.444 0.334 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Hexachlorobenzene <0.334
0.444 0.223 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Hexachlorobutadiene <0.223
0.444 0.200 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Hexachlorocyclopentadiene <0.200
0.444 0.241 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Hexachloroethane <0.241
0.0894 0.0387 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Indeno[1,2,3-cd]pyrene <0.0387
0.444 0.251 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Isophorone <0.251
0.0894 0.0374 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼1-Methylnaphthalene <0.0374
0.0894 0.0347 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2-Methylnaphthalene <0.0347
0.444 0.288 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2-Methylphenol <0.288
0.444 0.271 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼3 & 4 Methylphenol <0.271
0.0894 0.0387 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Naphthalene <0.0387
0.444 0.276 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2-Nitroaniline <0.276
0.894 0.307 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼3-Nitroaniline <0.307
0.894 0.318 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼4-Nitroaniline <0.318
0.444 0.268 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Nitrobenzene <0.268
0.444 0.324 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2-Nitrophenol <0.324
0.894 0.510 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼4-Nitrophenol <0.510
0.444 0.259 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼N-Nitrosodi-n-propylamine <0.259
0.444 0.0707 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0707
0.894 0.355 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Pentachlorophenol <0.355
0.0894 0.0454 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Phenanthrene <0.0454
0.444 0.271 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Phenol <0.271
0.0894 0.0454 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼Pyrene <0.0454
0.444 0.241 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼1,2,4-Trichlorobenzene <0.241
0.444 0.291 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2,4,5-Trichlorophenol <0.291
0.444 0.256 mg/Kg 12/08/16 12:11 12/09/16 14:45 1☼2,4,6-Trichlorophenol <0.256
2-Fluorobiphenyl (Surr)49 29-120 12/08/16 12:11 12/09/16 14:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)44 12/08/16 12:11 12/09/16 14:45 110-120
Nitrobenzene-d5 (Surr)43 12/08/16 12:11 12/09/16 14:45 127-120
Phenol-d5 (Surr)48 12/08/16 12:11 12/09/16 14:45 110-120
Terphenyl-d14 (Surr)66 12/08/16 12:11 12/09/16 14:45 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-14Client Sample ID: SB-7 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)68 10-120 12/08/16 12:11 12/09/16 14:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.60 2.66 1.60 mg/Kg ☼12/09/16 09:26 12/09/16 15:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.66 1.33 mg/Kg 12/09/16 09:26 12/09/16 15:06 1☼Barium 12.0
1.33 0.133 mg/Kg 12/09/16 09:26 12/09/16 15:06 1☼Cadmium 7.96
1.33 1.20 mg/Kg 12/09/16 09:26 12/09/16 15:06 1☼Chromium 73.3
1.33 0.666 mg/Kg 12/09/16 09:26 12/09/16 15:06 1☼Lead 13.6
13.3 7.32 mg/Kg 12/09/16 09:26 12/12/16 12:48 5☼Selenium 8.92 J B
1.33 0.532 mg/Kg 12/09/16 09:26 12/09/16 15:06 1☼Silver <0.532
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0396 0.132 0.0396 mg/Kg ☼12/09/16 08:38 12/09/16 16:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 74.5 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-15Client Sample ID: SB-8 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.225 0.0548 0.00921 mg/Kg ☼12/06/16 14:30 12/09/16 07:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Benzene <0.000735
0.00219 0.000790 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Bromobenzene <0.000790
0.00219 0.000603 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Bromochloromethane <0.000603
0.00219 0.000603 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Bromodichloromethane <0.000603
0.00219 0.000603 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Bromoform <0.000603
0.00219 0.00132 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Bromomethane 0.00261
0.0548 0.00559 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼2-Butanone (MEK)0.0173 J
0.00548 0.00395 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Carbon disulfide <0.00395
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Carbon tetrachloride <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Chlorobenzene <0.000735
0.00219 0.000373 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Chlorodibromomethane <0.000373
0.00548 0.00208 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Chloroethane <0.00208
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Chloroform <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Chloromethane <0.000735
0.00219 0.000976 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼2-Chlorotoluene <0.000976
0.00219 0.000921 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼4-Chlorotoluene <0.000921
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼cis-1,2-Dichloroethene <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼cis-1,3-Dichloropropene <0.000735
0.00548 0.000768 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2-Dibromo-3-Chloropropane <0.000768
0.00219 0.00110 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2-Dibromoethane (EDB)<0.00110
0.00219 0.000614 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Dibromomethane <0.000614
0.00219 0.000373 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2-Dichlorobenzene <0.000373
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,3-Dichlorobenzene <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,4-Dichlorobenzene <0.000735
0.00219 0.00110 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Dichlorodifluoromethane <0.00110
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,1-Dichloroethane <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2-Dichloroethane <0.000735
0.00219 0.000625 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,1-Dichloroethene <0.000625
0.00219 0.000516 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2-Dichloroethene, Total <0.000516
0.00219 0.00103 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2-Dichloropropane <0.00103
0.00219 0.00103 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,3-Dichloropropane <0.00103
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼2,2-Dichloropropane <0.000735
0.00219 0.000559 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,1-Dichloropropene <0.000559
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Diisopropyl ether <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Ethylbenzene <0.000735
0.00548 0.00125 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Hexachlorobutadiene <0.00125
0.0548 0.0183 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼2-Hexanone <0.0183
0.00219 0.000450 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Isopropylbenzene <0.000450
0.0110 0.000943 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Methylene Chloride <0.000943
0.0548 0.00208 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼4-Methyl-2-pentanone (MIBK)<0.00208
0.00219 0.00105 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Methyl tert-butyl ether <0.00105
0.00548 0.00186 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Naphthalene <0.00186
0.00219 0.00108 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼n-Butylbenzene <0.00108
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼N-Propylbenzene <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼p-Isopropyltoluene <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼sec-Butylbenzene <0.000735
0.00219 0.00121 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Styrene <0.00121
0.00219 0.000987 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼tert-Butylbenzene <0.000987
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-15Client Sample ID: SB-8 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000735 0.00219 0.000735 mg/Kg ☼12/06/16 14:30 12/09/16 07:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00219 0.00110 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,1,2,2-Tetrachloroethane <0.00110
0.00219 0.000801 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Tetrachloroethene <0.000801
0.00219 0.000812 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Toluene <0.000812
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼trans-1,2-Dichloroethene <0.000735
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼trans-1,3-Dichloropropene <0.000735
0.00219 0.000417 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2,3-Trichlorobenzene <0.000417
0.00219 0.000735 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2,4-Trichlorobenzene <0.000735
0.00219 0.00101 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,1,1-Trichloroethane <0.00101
0.00548 0.00154 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,1,2-Trichloroethane <0.00154
0.00219 0.00105 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Trichloroethene <0.00105
0.00219 0.00110 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Trichlorofluoromethane <0.00110
0.00219 0.000603 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2,3-Trichloropropane <0.000603
0.00219 0.00110 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,2,4-Trimethylbenzene 0.00121 J
0.00219 0.000823 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼1,3,5-Trimethylbenzene <0.000823
0.00219 0.00121 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Vinyl chloride <0.00121
0.00658 0.00135 mg/Kg 12/06/16 14:30 12/09/16 07:28 1☼Xylenes, Total <0.00135
4-Bromofluorobenzene (Surr)90 70-130 12/06/16 14:30 12/09/16 07:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)130 12/06/16 14:30 12/09/16 07:28 170-130
1,2-Dichloroethane-d4 (Surr)111 12/06/16 14:30 12/09/16 07:28 170-130
Toluene-d8 (Surr)87 12/06/16 14:30 12/09/16 07:28 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0367 0.0768 0.0367 mg/Kg ☼12/08/16 12:11 12/09/16 15:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0768 0.0332 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Acenaphthylene <0.0332
0.0768 0.0332 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Anthracene <0.0332
0.0768 0.0344 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Benzo[a]anthracene <0.0344
0.0768 0.0309 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Benzo[a]pyrene <0.0309
0.0768 0.0321 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Benzo[b]fluoranthene <0.0321
0.0768 0.0378 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Benzo[g,h,i]perylene <0.0378
0.0768 0.0309 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Benzo[k]fluoranthene <0.0309
0.382 0.229 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Bis(2-chloroethoxy)methane <0.229
0.382 0.244 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Bis(2-chloroethyl)ether <0.244
0.382 0.227 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼bis (2-chloroisopropyl) ether <0.227
0.382 0.237 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Bis(2-ethylhexyl) phthalate <0.237
0.382 0.235 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼4-Bromophenyl phenyl ether <0.235
0.382 0.246 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Butyl benzyl phthalate <0.246
0.382 0.237 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Carbazole <0.237
0.382 0.260 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼4-Chloroaniline <0.260
0.382 0.193 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼4-Chloro-3-methylphenol <0.193
0.382 0.239 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2-Chloronaphthalene <0.239
0.382 0.219 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2-Chlorophenol <0.219
0.382 0.230 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼4-Chlorophenyl phenyl ether <0.230
0.0768 0.0424 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Chrysene <0.0424
0.763 0.129 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Cresols <0.129
0.0768 0.0367 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Dibenz(a,h)anthracene <0.0367
0.382 0.241 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Dibenzofuran <0.241
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-15Client Sample ID: SB-8 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.218 0.382 0.218 mg/Kg ☼12/08/16 12:11 12/09/16 15:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.382 0.218 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼1,3-Dichlorobenzene <0.218
0.382 0.225 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼1,4-Dichlorobenzene <0.225
0.768 0.234 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼3,3'-Dichlorobenzidine <0.234
0.382 0.201 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2,4-Dichlorophenol <0.201
0.382 0.243 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Diethyl phthalate <0.243
0.768 0.384 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2,4-Dimethylphenol <0.384
0.382 0.237 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Dimethyl phthalate <0.237
0.382 0.242 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Di-n-butyl phthalate <0.242
0.382 0.262 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼4,6-Dinitro-2-methylphenol <0.262
0.382 0.288 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2,4-Dinitrophenol <0.288
0.382 0.238 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2,4-Dinitrotoluene <0.238
0.382 0.256 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2,6-Dinitrotoluene <0.256
0.382 0.204 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Di-n-octyl phthalate <0.204
0.0768 0.0390 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Fluoranthene <0.0390
0.0768 0.0332 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Fluorene <0.0332
0.382 0.286 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Hexachlorobenzene <0.286
0.382 0.191 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Hexachlorobutadiene <0.191
0.382 0.172 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Hexachlorocyclopentadiene <0.172
0.382 0.207 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Hexachloroethane <0.207
0.0768 0.0332 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Indeno[1,2,3-cd]pyrene <0.0332
0.382 0.215 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Isophorone <0.215
0.0768 0.0321 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼1-Methylnaphthalene <0.0321
0.0768 0.0298 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2-Methylnaphthalene <0.0298
0.382 0.248 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2-Methylphenol <0.248
0.382 0.233 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼3 & 4 Methylphenol <0.233
0.0768 0.0332 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Naphthalene <0.0332
0.382 0.237 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2-Nitroaniline <0.237
0.768 0.264 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼3-Nitroaniline <0.264
0.768 0.273 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼4-Nitroaniline <0.273
0.382 0.230 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Nitrobenzene <0.230
0.382 0.278 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2-Nitrophenol <0.278
0.768 0.438 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼4-Nitrophenol <0.438
0.382 0.222 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼N-Nitrosodi-n-propylamine <0.222
0.382 0.0607 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0607
0.768 0.305 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Pentachlorophenol <0.305
0.0768 0.0390 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Phenanthrene <0.0390
0.382 0.233 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Phenol <0.233
0.0768 0.0390 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼Pyrene <0.0390
0.382 0.207 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼1,2,4-Trichlorobenzene <0.207
0.382 0.250 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2,4,5-Trichlorophenol <0.250
0.382 0.220 mg/Kg 12/08/16 12:11 12/09/16 15:03 1☼2,4,6-Trichlorophenol <0.220
2-Fluorobiphenyl (Surr)51 29-120 12/08/16 12:11 12/09/16 15:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)48 12/08/16 12:11 12/09/16 15:03 110-120
Nitrobenzene-d5 (Surr)42 12/08/16 12:11 12/09/16 15:03 127-120
Phenol-d5 (Surr)53 12/08/16 12:11 12/09/16 15:03 110-120
Terphenyl-d14 (Surr)72 12/08/16 12:11 12/09/16 15:03 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-15Client Sample ID: SB-8 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)70 10-120 12/08/16 12:11 12/09/16 15:03 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.38 2.30 1.38 mg/Kg ☼12/09/16 09:26 12/09/16 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.30 1.15 mg/Kg 12/09/16 09:26 12/09/16 15:17 1☼Barium 37.6
1.15 0.115 mg/Kg 12/09/16 09:26 12/09/16 15:17 1☼Cadmium 1.06 J
1.15 1.04 mg/Kg 12/09/16 09:26 12/09/16 15:17 1☼Chromium 17.4
1.15 0.576 mg/Kg 12/09/16 09:26 12/12/16 12:53 1☼Lead 17.3
2.30 1.27 mg/Kg 12/09/16 09:26 12/12/16 12:53 1☼Selenium <1.27
1.15 0.461 mg/Kg 12/09/16 09:26 12/09/16 15:17 1☼Silver <0.461
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0333 0.111 0.0333 mg/Kg ☼12/09/16 08:38 12/09/16 16:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 86.5 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-16Client Sample ID: SB-8 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.178 0.0529 0.00889 mg/Kg ☼12/06/16 14:30 12/09/16 06:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Benzene <0.000709
0.00212 0.000762 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Bromobenzene <0.000762
0.00212 0.000582 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Bromochloromethane <0.000582
0.00212 0.000582 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Bromodichloromethane <0.000582
0.00212 0.000582 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Bromoform <0.000582
0.00212 0.00127 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Bromomethane <0.00127
0.0529 0.00540 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼2-Butanone (MEK)0.0119 J
0.00529 0.00381 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Carbon disulfide <0.00381
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Carbon tetrachloride <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Chlorobenzene <0.000709
0.00212 0.000360 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Chlorodibromomethane <0.000360
0.00529 0.00201 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Chloroethane <0.00201
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Chloroform <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Chloromethane <0.000709
0.00212 0.000942 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼2-Chlorotoluene <0.000942
0.00212 0.000889 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼4-Chlorotoluene <0.000889
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼cis-1,2-Dichloroethene <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼cis-1,3-Dichloropropene <0.000709
0.00529 0.000741 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2-Dibromo-3-Chloropropane <0.000741
0.00212 0.00106 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2-Dibromoethane (EDB)<0.00106
0.00212 0.000593 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Dibromomethane <0.000593
0.00212 0.000360 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2-Dichlorobenzene <0.000360
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,3-Dichlorobenzene <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,4-Dichlorobenzene <0.000709
0.00212 0.00106 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Dichlorodifluoromethane <0.00106
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,1-Dichloroethane <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2-Dichloroethane <0.000709
0.00212 0.000603 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,1-Dichloroethene <0.000603
0.00212 0.000497 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2-Dichloroethene, Total <0.000497
0.00212 0.000995 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2-Dichloropropane <0.000995
0.00212 0.000995 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,3-Dichloropropane <0.000995
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼2,2-Dichloropropane <0.000709
0.00212 0.000540 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,1-Dichloropropene <0.000540
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Diisopropyl ether <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Ethylbenzene <0.000709
0.00529 0.00121 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Hexachlorobutadiene <0.00121
0.0529 0.0177 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼2-Hexanone <0.0177
0.00212 0.000434 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Isopropylbenzene <0.000434
0.0106 0.000910 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Methylene Chloride <0.000910
0.0529 0.00201 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼4-Methyl-2-pentanone (MIBK)<0.00201
0.00212 0.00102 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Methyl tert-butyl ether <0.00102
0.00529 0.00180 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Naphthalene <0.00180
0.00212 0.00104 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼n-Butylbenzene <0.00104
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼N-Propylbenzene <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼p-Isopropyltoluene <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼sec-Butylbenzene <0.000709
0.00212 0.00116 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Styrene <0.00116
0.00212 0.000953 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼tert-Butylbenzene <0.000953
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-16Client Sample ID: SB-8 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000709 0.00212 0.000709 mg/Kg ☼12/06/16 14:30 12/09/16 06:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00212 0.00106 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,1,2,2-Tetrachloroethane <0.00106
0.00212 0.000773 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Tetrachloroethene <0.000773
0.00212 0.000783 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Toluene <0.000783
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼trans-1,2-Dichloroethene <0.000709
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼trans-1,3-Dichloropropene <0.000709
0.00212 0.000402 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2,3-Trichlorobenzene <0.000402
0.00212 0.000709 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2,4-Trichlorobenzene <0.000709
0.00212 0.000974 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,1,1-Trichloroethane <0.000974
0.00529 0.00148 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,1,2-Trichloroethane <0.00148
0.00212 0.00102 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Trichloroethene <0.00102
0.00212 0.00106 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Trichlorofluoromethane <0.00106
0.00212 0.000582 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2,3-Trichloropropane <0.000582
0.00212 0.00106 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,2,4-Trimethylbenzene <0.00106
0.00212 0.000794 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼1,3,5-Trimethylbenzene <0.000794
0.00212 0.00116 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Vinyl chloride <0.00116
0.00635 0.00130 mg/Kg 12/06/16 14:30 12/09/16 06:59 1☼Xylenes, Total <0.00130
4-Bromofluorobenzene (Surr)88 70-130 12/06/16 14:30 12/09/16 06:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)114 12/06/16 14:30 12/09/16 06:59 170-130
1,2-Dichloroethane-d4 (Surr)105 12/06/16 14:30 12/09/16 06:59 170-130
Toluene-d8 (Surr)89 12/06/16 14:30 12/09/16 06:59 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0389 0.0814 0.0389 mg/Kg ☼12/08/16 12:11 12/09/16 15:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0814 0.0352 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Acenaphthylene <0.0352
0.0814 0.0352 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Anthracene <0.0352
0.0814 0.0365 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Benzo[a]anthracene <0.0365
0.0814 0.0328 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Benzo[a]pyrene <0.0328
0.0814 0.0340 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Benzo[b]fluoranthene <0.0340
0.0814 0.0401 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Benzo[g,h,i]perylene <0.0401
0.0814 0.0328 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Benzo[k]fluoranthene <0.0328
0.405 0.243 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Bis(2-chloroethoxy)methane <0.243
0.405 0.259 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Bis(2-chloroethyl)ether <0.259
0.405 0.241 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼bis (2-chloroisopropyl) ether <0.241
0.405 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Bis(2-ethylhexyl) phthalate <0.252
0.405 0.249 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼4-Bromophenyl phenyl ether <0.249
0.405 0.261 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Butyl benzyl phthalate <0.261
0.405 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Carbazole <0.252
0.405 0.276 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼4-Chloroaniline <0.276
0.405 0.204 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼4-Chloro-3-methylphenol <0.204
0.405 0.254 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2-Chloronaphthalene <0.254
0.405 0.232 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2-Chlorophenol <0.232
0.405 0.244 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼4-Chlorophenyl phenyl ether <0.244
0.0814 0.0450 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Chrysene <0.0450
0.809 0.137 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Cresols <0.137
0.0814 0.0389 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Dibenz(a,h)anthracene <0.0389
0.405 0.255 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Dibenzofuran <0.255
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-16Client Sample ID: SB-8 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.231 0.405 0.231 mg/Kg ☼12/08/16 12:11 12/09/16 15:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.405 0.231 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼1,3-Dichlorobenzene <0.231
0.405 0.238 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼1,4-Dichlorobenzene <0.238
0.814 0.248 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼3,3'-Dichlorobenzidine <0.248
0.405 0.213 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2,4-Dichlorophenol <0.213
0.405 0.258 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Diethyl phthalate <0.258
0.814 0.407 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2,4-Dimethylphenol <0.407
0.405 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Dimethyl phthalate <0.252
0.405 0.256 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Di-n-butyl phthalate <0.256
0.405 0.278 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼4,6-Dinitro-2-methylphenol <0.278
0.405 0.305 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2,4-Dinitrophenol <0.305
0.405 0.253 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2,4-Dinitrotoluene <0.253
0.405 0.271 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2,6-Dinitrotoluene <0.271
0.405 0.216 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Di-n-octyl phthalate <0.216
0.0814 0.0413 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Fluoranthene <0.0413
0.0814 0.0352 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Fluorene <0.0352
0.405 0.304 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Hexachlorobenzene <0.304
0.405 0.203 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Hexachlorobutadiene <0.203
0.405 0.182 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Hexachlorocyclopentadiene <0.182
0.405 0.220 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Hexachloroethane <0.220
0.0814 0.0352 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Indeno[1,2,3-cd]pyrene <0.0352
0.405 0.228 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Isophorone <0.228
0.0814 0.0340 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼1-Methylnaphthalene <0.0340
0.0814 0.0316 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2-Methylnaphthalene <0.0316
0.405 0.263 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2-Methylphenol <0.263
0.405 0.247 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼3 & 4 Methylphenol <0.247
0.0814 0.0352 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Naphthalene <0.0352
0.405 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2-Nitroaniline <0.252
0.814 0.280 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼3-Nitroaniline <0.280
0.814 0.289 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼4-Nitroaniline <0.289
0.405 0.244 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Nitrobenzene <0.244
0.405 0.295 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2-Nitrophenol <0.295
0.814 0.464 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼4-Nitrophenol <0.464
0.405 0.236 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼N-Nitrosodi-n-propylamine <0.236
0.405 0.0644 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0644
0.814 0.323 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Pentachlorophenol <0.323
0.0814 0.0413 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Phenanthrene <0.0413
0.405 0.247 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Phenol <0.247
0.0814 0.0413 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼Pyrene <0.0413
0.405 0.220 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼1,2,4-Trichlorobenzene <0.220
0.405 0.265 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2,4,5-Trichlorophenol <0.265
0.405 0.233 mg/Kg 12/08/16 12:11 12/09/16 15:22 1☼2,4,6-Trichlorophenol <0.233
2-Fluorobiphenyl (Surr)43 29-120 12/08/16 12:11 12/09/16 15:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)38 12/08/16 12:11 12/09/16 15:22 110-120
Nitrobenzene-d5 (Surr)37 12/08/16 12:11 12/09/16 15:22 127-120
Phenol-d5 (Surr)41 12/08/16 12:11 12/09/16 15:22 110-120
Terphenyl-d14 (Surr)66 12/08/16 12:11 12/09/16 15:22 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-16Client Sample ID: SB-8 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)67 10-120 12/08/16 12:11 12/09/16 15:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.47 2.45 1.47 mg/Kg ☼12/09/16 09:26 12/09/16 15:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.45 1.23 mg/Kg 12/09/16 09:26 12/09/16 15:34 1☼Barium 15.3
1.23 0.123 mg/Kg 12/09/16 09:26 12/09/16 15:34 1☼Cadmium 1.81
1.23 1.10 mg/Kg 12/09/16 09:26 12/09/16 15:34 1☼Chromium 23.5
1.23 0.613 mg/Kg 12/09/16 09:26 12/12/16 12:58 1☼Lead 22.7
2.45 1.35 mg/Kg 12/09/16 09:26 12/12/16 12:58 1☼Selenium <1.35
1.23 0.490 mg/Kg 12/09/16 09:26 12/09/16 15:34 1☼Silver <0.490
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0371 J 0.123 0.0370 mg/Kg ☼12/09/16 08:38 12/09/16 16:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 81.3 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-17Client Sample ID: SB-9 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.327 0.0775 0.0130 mg/Kg ☼12/06/16 14:50 12/09/16 06:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Benzene <0.00104
0.00310 0.00112 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Bromobenzene <0.00112
0.00310 0.000853 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Bromochloromethane <0.000853
0.00310 0.000853 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Bromodichloromethane <0.000853
0.00310 0.000853 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Bromoform <0.000853
0.00310 0.00186 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Bromomethane 0.00236 J
0.0775 0.00791 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼2-Butanone (MEK)0.0201 J
0.00775 0.00558 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Carbon disulfide <0.00558
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Carbon tetrachloride <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Chlorobenzene <0.00104
0.00310 0.000527 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Chlorodibromomethane <0.000527
0.00775 0.00295 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Chloroethane <0.00295
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Chloroform <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Chloromethane <0.00104
0.00310 0.00138 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼2-Chlorotoluene <0.00138
0.00310 0.00130 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼4-Chlorotoluene <0.00130
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼cis-1,2-Dichloroethene <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼cis-1,3-Dichloropropene <0.00104
0.00775 0.00109 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2-Dibromo-3-Chloropropane <0.00109
0.00310 0.00155 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2-Dibromoethane (EDB)<0.00155
0.00310 0.000868 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Dibromomethane <0.000868
0.00310 0.000527 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2-Dichlorobenzene <0.000527
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,3-Dichlorobenzene <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,4-Dichlorobenzene <0.00104
0.00310 0.00155 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Dichlorodifluoromethane <0.00155
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,1-Dichloroethane <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2-Dichloroethane <0.00104
0.00310 0.000884 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,1-Dichloroethene <0.000884
0.00310 0.000729 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2-Dichloroethene, Total <0.000729
0.00310 0.00146 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2-Dichloropropane <0.00146
0.00310 0.00146 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,3-Dichloropropane <0.00146
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼2,2-Dichloropropane <0.00104
0.00310 0.000791 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,1-Dichloropropene <0.000791
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Diisopropyl ether <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Ethylbenzene <0.00104
0.00775 0.00177 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Hexachlorobutadiene <0.00177
0.0775 0.0259 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼2-Hexanone <0.0259
0.00310 0.000636 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Isopropylbenzene <0.000636
0.0155 0.00133 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Methylene Chloride <0.00133
0.0775 0.00295 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼4-Methyl-2-pentanone (MIBK)<0.00295
0.00310 0.00149 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Methyl tert-butyl ether <0.00149
0.00775 0.00264 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Naphthalene <0.00264
0.00310 0.00152 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼n-Butylbenzene <0.00152
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼N-Propylbenzene <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼p-Isopropyltoluene <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼sec-Butylbenzene <0.00104
0.00310 0.00171 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Styrene <0.00171
0.00310 0.00140 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼tert-Butylbenzene <0.00140
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-17Client Sample ID: SB-9 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.00104 0.00310 0.00104 mg/Kg ☼12/06/16 14:50 12/09/16 06:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00310 0.00155 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,1,2,2-Tetrachloroethane <0.00155
0.00310 0.00113 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Tetrachloroethene <0.00113
0.00310 0.00115 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Toluene 0.00131 J
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼trans-1,2-Dichloroethene <0.00104
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼trans-1,3-Dichloropropene <0.00104
0.00310 0.000589 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2,3-Trichlorobenzene <0.000589
0.00310 0.00104 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2,4-Trichlorobenzene <0.00104
0.00310 0.00143 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,1,1-Trichloroethane <0.00143
0.00775 0.00217 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,1,2-Trichloroethane <0.00217
0.00310 0.00149 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Trichloroethene <0.00149
0.00310 0.00155 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Trichlorofluoromethane <0.00155
0.00310 0.000853 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2,3-Trichloropropane <0.000853
0.00310 0.00155 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,2,4-Trimethylbenzene <0.00155
0.00310 0.00116 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼1,3,5-Trimethylbenzene <0.00116
0.00310 0.00171 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Vinyl chloride <0.00171
0.00930 0.00191 mg/Kg 12/06/16 14:50 12/09/16 06:29 1☼Xylenes, Total <0.00191
4-Bromofluorobenzene (Surr)90 70-130 12/06/16 14:50 12/09/16 06:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)128 12/06/16 14:50 12/09/16 06:29 170-130
1,2-Dichloroethane-d4 (Surr)111 12/06/16 14:50 12/09/16 06:29 170-130
Toluene-d8 (Surr)89 12/06/16 14:50 12/09/16 06:29 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0389 0.0814 0.0389 mg/Kg ☼12/08/16 12:11 12/09/16 15:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0814 0.0353 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Acenaphthylene <0.0353
0.0814 0.0353 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Anthracene <0.0353
0.0814 0.0365 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Benzo[a]anthracene <0.0365
0.0814 0.0328 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Benzo[a]pyrene <0.0328
0.0814 0.0340 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Benzo[b]fluoranthene <0.0340
0.0814 0.0401 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Benzo[g,h,i]perylene <0.0401
0.0814 0.0328 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Benzo[k]fluoranthene <0.0328
0.405 0.243 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Bis(2-chloroethoxy)methane <0.243
0.405 0.259 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Bis(2-chloroethyl)ether <0.259
0.405 0.241 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼bis (2-chloroisopropyl) ether <0.241
0.405 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Bis(2-ethylhexyl) phthalate <0.252
0.405 0.249 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼4-Bromophenyl phenyl ether <0.249
0.405 0.261 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Butyl benzyl phthalate <0.261
0.405 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Carbazole <0.252
0.405 0.276 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼4-Chloroaniline <0.276
0.405 0.204 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼4-Chloro-3-methylphenol <0.204
0.405 0.254 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2-Chloronaphthalene <0.254
0.405 0.232 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2-Chlorophenol <0.232
0.405 0.244 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼4-Chlorophenyl phenyl ether <0.244
0.0814 0.0450 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Chrysene <0.0450
0.810 0.137 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Cresols <0.137
0.0814 0.0389 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Dibenz(a,h)anthracene <0.0389
0.405 0.255 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Dibenzofuran <0.255
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-17Client Sample ID: SB-9 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.231 0.405 0.231 mg/Kg ☼12/08/16 12:11 12/09/16 15:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.405 0.231 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼1,3-Dichlorobenzene <0.231
0.405 0.238 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼1,4-Dichlorobenzene <0.238
0.814 0.248 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼3,3'-Dichlorobenzidine <0.248
0.405 0.213 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2,4-Dichlorophenol <0.213
0.405 0.258 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Diethyl phthalate <0.258
0.814 0.407 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2,4-Dimethylphenol <0.407
0.405 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Dimethyl phthalate <0.252
0.405 0.257 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Di-n-butyl phthalate <0.257
0.405 0.278 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼4,6-Dinitro-2-methylphenol <0.278
0.405 0.305 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2,4-Dinitrophenol <0.305
0.405 0.253 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2,4-Dinitrotoluene <0.253
0.405 0.271 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2,6-Dinitrotoluene <0.271
0.405 0.216 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Di-n-octyl phthalate <0.216
0.0814 0.0413 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Fluoranthene <0.0413
0.0814 0.0353 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Fluorene <0.0353
0.405 0.304 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Hexachlorobenzene <0.304
0.405 0.203 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Hexachlorobutadiene <0.203
0.405 0.182 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Hexachlorocyclopentadiene <0.182
0.405 0.220 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Hexachloroethane <0.220
0.0814 0.0353 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Indeno[1,2,3-cd]pyrene <0.0353
0.405 0.229 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Isophorone <0.229
0.0814 0.0340 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼1-Methylnaphthalene <0.0340
0.0814 0.0316 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2-Methylnaphthalene <0.0316
0.405 0.263 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2-Methylphenol <0.263
0.405 0.247 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼3 & 4 Methylphenol <0.247
0.0814 0.0353 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Naphthalene <0.0353
0.405 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2-Nitroaniline <0.252
0.814 0.280 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼3-Nitroaniline <0.280
0.814 0.289 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼4-Nitroaniline <0.289
0.405 0.244 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Nitrobenzene <0.244
0.405 0.295 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2-Nitrophenol <0.295
0.814 0.464 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼4-Nitrophenol <0.464
0.405 0.236 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼N-Nitrosodi-n-propylamine <0.236
0.405 0.0644 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0644
0.814 0.323 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Pentachlorophenol <0.323
0.0814 0.0413 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Phenanthrene <0.0413
0.405 0.247 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Phenol <0.247
0.0814 0.0413 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼Pyrene <0.0413
0.405 0.220 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼1,2,4-Trichlorobenzene <0.220
0.405 0.265 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2,4,5-Trichlorophenol <0.265
0.405 0.233 mg/Kg 12/08/16 12:11 12/09/16 15:41 1☼2,4,6-Trichlorophenol <0.233
2-Fluorobiphenyl (Surr)49 29-120 12/08/16 12:11 12/09/16 15:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)44 12/08/16 12:11 12/09/16 15:41 110-120
Nitrobenzene-d5 (Surr)43 12/08/16 12:11 12/09/16 15:41 127-120
Phenol-d5 (Surr)49 12/08/16 12:11 12/09/16 15:41 110-120
Terphenyl-d14 (Surr)75 12/08/16 12:11 12/09/16 15:41 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-17Client Sample ID: SB-9 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)73 10-120 12/08/16 12:11 12/09/16 15:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic 1.61 J 2.41 1.44 mg/Kg ☼12/09/16 09:26 12/09/16 15:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.41 1.20 mg/Kg 12/09/16 09:26 12/09/16 15:39 1☼Barium 81.4
1.20 0.120 mg/Kg 12/09/16 09:26 12/09/16 15:39 1☼Cadmium 1.25
1.20 1.08 mg/Kg 12/09/16 09:26 12/09/16 15:39 1☼Chromium 22.0
1.20 0.601 mg/Kg 12/09/16 09:26 12/12/16 13:03 1☼Lead 16.9
2.41 1.32 mg/Kg 12/09/16 09:26 12/12/16 13:03 1☼Selenium <1.32
1.20 0.481 mg/Kg 12/09/16 09:26 12/09/16 15:39 1☼Silver <0.481
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0358 0.119 0.0358 mg/Kg ☼12/09/16 08:38 12/09/16 16:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 80.4 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-18Client Sample ID: SB-9 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.197 0.0749 0.0126 mg/Kg ☼12/06/16 14:50 12/09/16 06:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Benzene <0.00100
0.00300 0.00108 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Bromobenzene <0.00108
0.00300 0.000824 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Bromochloromethane <0.000824
0.00300 0.000824 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Bromodichloromethane <0.000824
0.00300 0.000824 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Bromoform <0.000824
0.00300 0.00180 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Bromomethane <0.00180
0.0749 0.00764 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼2-Butanone (MEK)<0.00764
0.00749 0.00539 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Carbon disulfide <0.00539
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Carbon tetrachloride <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Chlorobenzene <0.00100
0.00300 0.000509 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Chlorodibromomethane <0.000509
0.00749 0.00285 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Chloroethane <0.00285
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Chloroform <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Chloromethane <0.00100
0.00300 0.00133 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼2-Chlorotoluene <0.00133
0.00300 0.00126 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼4-Chlorotoluene <0.00126
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼cis-1,2-Dichloroethene <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼cis-1,3-Dichloropropene <0.00100
0.00749 0.00105 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2-Dibromo-3-Chloropropane <0.00105
0.00300 0.00150 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2-Dibromoethane (EDB)<0.00150
0.00300 0.000839 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Dibromomethane <0.000839
0.00300 0.000509 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2-Dichlorobenzene <0.000509
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,3-Dichlorobenzene <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,4-Dichlorobenzene <0.00100
0.00300 0.00150 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Dichlorodifluoromethane <0.00150
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,1-Dichloroethane <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2-Dichloroethane <0.00100
0.00300 0.000854 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,1-Dichloroethene <0.000854
0.00300 0.000704 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2-Dichloroethene, Total <0.000704
0.00300 0.00141 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2-Dichloropropane <0.00141
0.00300 0.00141 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,3-Dichloropropane <0.00141
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼2,2-Dichloropropane <0.00100
0.00300 0.000764 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,1-Dichloropropene <0.000764
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Diisopropyl ether <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Ethylbenzene <0.00100
0.00749 0.00171 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Hexachlorobutadiene <0.00171
0.0749 0.0250 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼2-Hexanone <0.0250
0.00300 0.000614 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Isopropylbenzene <0.000614
0.0150 0.00129 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Methylene Chloride <0.00129
0.0749 0.00285 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼4-Methyl-2-pentanone (MIBK)<0.00285
0.00300 0.00144 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Methyl tert-butyl ether <0.00144
0.00749 0.00255 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Naphthalene <0.00255
0.00300 0.00147 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼n-Butylbenzene <0.00147
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼N-Propylbenzene <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼p-Isopropyltoluene <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼sec-Butylbenzene <0.00100
0.00300 0.00165 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Styrene <0.00165
0.00300 0.00135 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼tert-Butylbenzene <0.00135
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-18Client Sample ID: SB-9 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.00100 0.00300 0.00100 mg/Kg ☼12/06/16 14:50 12/09/16 06:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00300 0.00150 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,1,2,2-Tetrachloroethane <0.00150
0.00300 0.00109 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Tetrachloroethene <0.00109
0.00300 0.00111 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Toluene <0.00111
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼trans-1,2-Dichloroethene <0.00100
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼trans-1,3-Dichloropropene <0.00100
0.00300 0.000569 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2,3-Trichlorobenzene <0.000569
0.00300 0.00100 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2,4-Trichlorobenzene <0.00100
0.00300 0.00138 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,1,1-Trichloroethane <0.00138
0.00749 0.00210 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,1,2-Trichloroethane <0.00210
0.00300 0.00144 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Trichloroethene <0.00144
0.00300 0.00150 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Trichlorofluoromethane <0.00150
0.00300 0.000824 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2,3-Trichloropropane <0.000824
0.00300 0.00150 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,2,4-Trimethylbenzene <0.00150
0.00300 0.00112 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼1,3,5-Trimethylbenzene <0.00112
0.00300 0.00165 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Vinyl chloride <0.00165
0.00899 0.00184 mg/Kg 12/06/16 14:50 12/09/16 06:00 1☼Xylenes, Total <0.00184
4-Bromofluorobenzene (Surr)89 70-130 12/06/16 14:50 12/09/16 06:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)121 12/06/16 14:50 12/09/16 06:00 170-130
1,2-Dichloroethane-d4 (Surr)108 12/06/16 14:50 12/09/16 06:00 170-130
Toluene-d8 (Surr)89 12/06/16 14:50 12/09/16 06:00 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0401 0.0839 0.0401 mg/Kg ☼12/08/16 12:11 12/09/16 15:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0839 0.0363 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Acenaphthylene <0.0363
0.0839 0.0363 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Anthracene <0.0363
0.0839 0.0376 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Benzo[a]anthracene <0.0376
0.0839 0.0338 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Benzo[a]pyrene <0.0338
0.0839 0.0351 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Benzo[b]fluoranthene <0.0351
0.0839 0.0413 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Benzo[g,h,i]perylene <0.0413
0.0839 0.0338 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Benzo[k]fluoranthene <0.0338
0.417 0.250 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Bis(2-chloroethoxy)methane <0.250
0.417 0.267 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Bis(2-chloroethyl)ether <0.267
0.417 0.248 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼bis (2-chloroisopropyl) ether <0.248
0.417 0.259 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Bis(2-ethylhexyl) phthalate <0.259
0.417 0.257 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼4-Bromophenyl phenyl ether <0.257
0.417 0.269 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Butyl benzyl phthalate <0.269
0.417 0.259 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Carbazole <0.259
0.417 0.284 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼4-Chloroaniline <0.284
0.417 0.210 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼4-Chloro-3-methylphenol <0.210
0.417 0.262 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2-Chloronaphthalene <0.262
0.417 0.239 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2-Chlorophenol <0.239
0.417 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼4-Chlorophenyl phenyl ether <0.252
0.0839 0.0463 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Chrysene <0.0463
0.834 0.141 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Cresols <0.141
0.0839 0.0401 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Dibenz(a,h)anthracene <0.0401
0.417 0.263 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Dibenzofuran <0.263
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-18Client Sample ID: SB-9 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <0.238 0.417 0.238 mg/Kg ☼12/08/16 12:11 12/09/16 15:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.417 0.238 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼1,3-Dichlorobenzene <0.238
0.417 0.245 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼1,4-Dichlorobenzene <0.245
0.839 0.255 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼3,3'-Dichlorobenzidine <0.255
0.417 0.219 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2,4-Dichlorophenol <0.219
0.417 0.265 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Diethyl phthalate <0.265
0.839 0.419 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2,4-Dimethylphenol <0.419
0.417 0.259 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Dimethyl phthalate <0.259
0.417 0.264 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Di-n-butyl phthalate <0.264
0.417 0.287 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼4,6-Dinitro-2-methylphenol <0.287
0.417 0.314 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2,4-Dinitrophenol <0.314
0.417 0.260 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2,4-Dinitrotoluene <0.260
0.417 0.279 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2,6-Dinitrotoluene <0.279
0.417 0.223 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Di-n-octyl phthalate <0.223
0.0839 0.0426 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Fluoranthene <0.0426
0.0839 0.0363 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Fluorene <0.0363
0.417 0.313 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Hexachlorobenzene <0.313
0.417 0.209 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Hexachlorobutadiene <0.209
0.417 0.188 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Hexachlorocyclopentadiene <0.188
0.417 0.227 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Hexachloroethane <0.227
0.0839 0.0363 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Indeno[1,2,3-cd]pyrene <0.0363
0.417 0.235 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Isophorone <0.235
0.0839 0.0351 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼1-Methylnaphthalene <0.0351
0.0839 0.0325 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2-Methylnaphthalene <0.0325
0.417 0.270 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2-Methylphenol <0.270
0.417 0.254 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼3 & 4 Methylphenol <0.254
0.0839 0.0363 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Naphthalene <0.0363
0.417 0.259 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2-Nitroaniline <0.259
0.839 0.288 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼3-Nitroaniline <0.288
0.839 0.298 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼4-Nitroaniline <0.298
0.417 0.252 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Nitrobenzene <0.252
0.417 0.304 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2-Nitrophenol <0.304
0.839 0.478 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼4-Nitrophenol <0.478
0.417 0.243 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼N-Nitrosodi-n-propylamine <0.243
0.417 0.0663 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0663
0.839 0.333 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Pentachlorophenol <0.333
0.0839 0.0426 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Phenanthrene <0.0426
0.417 0.254 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Phenol <0.254
0.0839 0.0426 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼Pyrene <0.0426
0.417 0.227 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼1,2,4-Trichlorobenzene <0.227
0.417 0.273 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2,4,5-Trichlorophenol <0.273
0.417 0.240 mg/Kg 12/08/16 12:11 12/09/16 15:59 1☼2,4,6-Trichlorophenol <0.240
2-Fluorobiphenyl (Surr)48 29-120 12/08/16 12:11 12/09/16 15:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)50 12/08/16 12:11 12/09/16 15:59 110-120
Nitrobenzene-d5 (Surr)48 12/08/16 12:11 12/09/16 15:59 127-120
Phenol-d5 (Surr)49 12/08/16 12:11 12/09/16 15:59 110-120
Terphenyl-d14 (Surr)82 12/08/16 12:11 12/09/16 15:59 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-18Client Sample ID: SB-9 (3-4)
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)76 10-120 12/08/16 12:11 12/09/16 15:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <1.44 2.40 1.44 mg/Kg ☼12/09/16 09:26 12/09/16 15:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.40 1.20 mg/Kg 12/09/16 09:26 12/09/16 15:44 1☼Barium 57.5
1.20 0.120 mg/Kg 12/09/16 09:26 12/09/16 15:44 1☼Cadmium 1.99
1.20 1.08 mg/Kg 12/09/16 09:26 12/09/16 15:44 1☼Chromium 37.3
1.20 0.600 mg/Kg 12/09/16 09:26 12/12/16 13:09 1☼Lead 17.1
2.40 1.32 mg/Kg 12/09/16 09:26 12/12/16 13:09 1☼Selenium <1.32
1.20 0.480 mg/Kg 12/09/16 09:26 12/09/16 15:44 1☼Silver <0.480
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0377 0.126 0.0377 mg/Kg ☼12/09/16 08:38 12/09/16 16:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 79.5 0.1 0.1 %12/08/16 10:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-19Client Sample ID: DUP-1 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 01:01
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.233 0.0638 0.0107 mg/Kg ☼12/06/16 00:01 12/09/16 05:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Benzene <0.000855
0.00255 0.000919 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Bromobenzene <0.000919
0.00255 0.000702 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Bromochloromethane <0.000702
0.00255 0.000702 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Bromodichloromethane <0.000702
0.00255 0.000702 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Bromoform <0.000702
0.00255 0.00153 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Bromomethane <0.00153
0.0638 0.00651 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼2-Butanone (MEK)0.00859 J
0.00638 0.00460 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Carbon disulfide <0.00460
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Carbon tetrachloride <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Chlorobenzene <0.000855
0.00255 0.000434 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Chlorodibromomethane <0.000434
0.00638 0.00243 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Chloroethane <0.00243
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Chloroform <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Chloromethane <0.000855
0.00255 0.00114 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼2-Chlorotoluene <0.00114
0.00255 0.00107 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼4-Chlorotoluene <0.00107
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼cis-1,2-Dichloroethene <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼cis-1,3-Dichloropropene <0.000855
0.00638 0.000894 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2-Dibromo-3-Chloropropane <0.000894
0.00255 0.00128 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2-Dibromoethane (EDB)<0.00128
0.00255 0.000715 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Dibromomethane <0.000715
0.00255 0.000434 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2-Dichlorobenzene <0.000434
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,3-Dichlorobenzene <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,4-Dichlorobenzene <0.000855
0.00255 0.00128 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Dichlorodifluoromethane <0.00128
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,1-Dichloroethane <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2-Dichloroethane <0.000855
0.00255 0.000728 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,1-Dichloroethene <0.000728
0.00255 0.000600 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2-Dichloroethene, Total <0.000600
0.00255 0.00120 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2-Dichloropropane <0.00120
0.00255 0.00120 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,3-Dichloropropane <0.00120
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼2,2-Dichloropropane <0.000855
0.00255 0.000651 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,1-Dichloropropene <0.000651
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Diisopropyl ether <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Ethylbenzene <0.000855
0.00638 0.00146 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Hexachlorobutadiene <0.00146
0.0638 0.0213 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼2-Hexanone <0.0213
0.00255 0.000524 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Isopropylbenzene <0.000524
0.0128 0.00110 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Methylene Chloride <0.00110
0.0638 0.00243 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼4-Methyl-2-pentanone (MIBK)<0.00243
0.00255 0.00123 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Methyl tert-butyl ether <0.00123
0.00638 0.00217 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Naphthalene <0.00217
0.00255 0.00125 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼n-Butylbenzene <0.00125
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼N-Propylbenzene <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼p-Isopropyltoluene <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼sec-Butylbenzene <0.000855
0.00255 0.00140 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Styrene <0.00140
0.00255 0.00115 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼tert-Butylbenzene <0.00115
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-19Client Sample ID: DUP-1 (0.5-1.5)
Matrix: SoilDate Collected: 12/06/16 01:01
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.000855 0.00255 0.000855 mg/Kg ☼12/06/16 00:01 12/09/16 05:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00255 0.00128 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,1,2,2-Tetrachloroethane <0.00128
0.00255 0.000932 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Tetrachloroethene <0.000932
0.00255 0.000945 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Toluene <0.000945
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼trans-1,2-Dichloroethene <0.000855
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼trans-1,3-Dichloropropene <0.000855
0.00255 0.000485 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2,3-Trichlorobenzene 0.000638 J
0.00255 0.000855 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2,4-Trichlorobenzene <0.000855
0.00255 0.00117 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,1,1-Trichloroethane <0.00117
0.00638 0.00179 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,1,2-Trichloroethane <0.00179
0.00255 0.00123 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Trichloroethene <0.00123
0.00255 0.00128 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Trichlorofluoromethane <0.00128
0.00255 0.000702 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2,3-Trichloropropane <0.000702
0.00255 0.00128 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,2,4-Trimethylbenzene <0.00128
0.00255 0.000958 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼1,3,5-Trimethylbenzene <0.000958
0.00255 0.00140 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Vinyl chloride <0.00140
0.00766 0.00157 mg/Kg 12/06/16 00:01 12/09/16 05:30 1☼Xylenes, Total <0.00157
4-Bromofluorobenzene (Surr)92 70-130 12/06/16 00:01 12/09/16 05:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)119 12/06/16 00:01 12/09/16 05:30 170-130
1,2-Dichloroethane-d4 (Surr)113 12/06/16 00:01 12/09/16 05:30 170-130
Toluene-d8 (Surr)93 12/06/16 00:01 12/09/16 05:30 170-130
General Chemistry
RL RL
Percent Solids 79.2 0.1 0.1 %12/08/16 11:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-20Client Sample ID: DUP-1 (3-4)
Matrix: SoilDate Collected: 12/06/16 01:01
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0757 J 0.0759 0.0127 mg/Kg ☼12/06/16 00:01 12/09/16 05:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Benzene <0.00102
0.00303 0.00109 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Bromobenzene <0.00109
0.00303 0.000834 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Bromochloromethane <0.000834
0.00303 0.000834 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Bromodichloromethane <0.000834
0.00303 0.000834 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Bromoform <0.000834
0.00303 0.00182 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Bromomethane <0.00182
0.0759 0.00774 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼2-Butanone (MEK)<0.00774
0.00759 0.00546 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Carbon disulfide <0.00546
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Carbon tetrachloride <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Chlorobenzene <0.00102
0.00303 0.000516 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Chlorodibromomethane <0.000516
0.00759 0.00288 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Chloroethane <0.00288
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Chloroform <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Chloromethane <0.00102
0.00303 0.00135 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼2-Chlorotoluene <0.00135
0.00303 0.00127 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼4-Chlorotoluene <0.00127
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼cis-1,2-Dichloroethene <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼cis-1,3-Dichloropropene <0.00102
0.00759 0.00106 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2-Dibromo-3-Chloropropane <0.00106
0.00303 0.00152 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2-Dibromoethane (EDB)<0.00152
0.00303 0.000850 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Dibromomethane <0.000850
0.00303 0.000516 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2-Dichlorobenzene <0.000516
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,3-Dichlorobenzene <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,4-Dichlorobenzene <0.00102
0.00303 0.00152 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Dichlorodifluoromethane <0.00152
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,1-Dichloroethane <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2-Dichloroethane <0.00102
0.00303 0.000865 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,1-Dichloroethene <0.000865
0.00303 0.000713 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2-Dichloroethene, Total <0.000713
0.00303 0.00143 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2-Dichloropropane <0.00143
0.00303 0.00143 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,3-Dichloropropane <0.00143
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼2,2-Dichloropropane <0.00102
0.00303 0.000774 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,1-Dichloropropene <0.000774
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Diisopropyl ether <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Ethylbenzene <0.00102
0.00759 0.00173 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Hexachlorobutadiene <0.00173
0.0759 0.0253 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼2-Hexanone <0.0253
0.00303 0.000622 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Isopropylbenzene <0.000622
0.0152 0.00130 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Methylene Chloride <0.00130
0.0759 0.00288 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼4-Methyl-2-pentanone (MIBK)<0.00288
0.00303 0.00146 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Methyl tert-butyl ether <0.00146
0.00759 0.00258 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Naphthalene <0.00258
0.00303 0.00149 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼n-Butylbenzene <0.00149
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼N-Propylbenzene <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼p-Isopropyltoluene <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼sec-Butylbenzene <0.00102
0.00303 0.00167 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Styrene <0.00167
0.00303 0.00137 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼tert-Butylbenzene <0.00137
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-20Client Sample ID: DUP-1 (3-4)
Matrix: SoilDate Collected: 12/06/16 01:01
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.00102 0.00303 0.00102 mg/Kg ☼12/06/16 00:01 12/09/16 05:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00303 0.00152 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,1,2,2-Tetrachloroethane <0.00152
0.00303 0.00111 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Tetrachloroethene <0.00111
0.00303 0.00112 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Toluene <0.00112
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼trans-1,2-Dichloroethene <0.00102
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼trans-1,3-Dichloropropene <0.00102
0.00303 0.000577 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2,3-Trichlorobenzene 0.00123 J
0.00303 0.00102 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2,4-Trichlorobenzene <0.00102
0.00303 0.00140 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,1,1-Trichloroethane <0.00140
0.00759 0.00212 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,1,2-Trichloroethane <0.00212
0.00303 0.00146 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Trichloroethene <0.00146
0.00303 0.00152 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Trichlorofluoromethane <0.00152
0.00303 0.000834 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2,3-Trichloropropane <0.000834
0.00303 0.00152 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,2,4-Trimethylbenzene <0.00152
0.00303 0.00114 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼1,3,5-Trimethylbenzene <0.00114
0.00303 0.00167 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Vinyl chloride <0.00167
0.00910 0.00187 mg/Kg 12/06/16 00:01 12/09/16 05:01 1☼Xylenes, Total <0.00187
4-Bromofluorobenzene (Surr)87 70-130 12/06/16 00:01 12/09/16 05:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)122 12/06/16 00:01 12/09/16 05:01 170-130
1,2-Dichloroethane-d4 (Surr)108 12/06/16 00:01 12/09/16 05:01 170-130
Toluene-d8 (Surr)90 12/06/16 00:01 12/09/16 05:01 170-130
General Chemistry
RL RL
Percent Solids 60.5 0.1 0.1 %12/08/16 11:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-21Client Sample ID: DL-1
Matrix: SoilDate Collected: 12/06/16 16:55
Date Received: 12/07/16 09:40
Method: 6020B - Metals (ICP/MS)
RL MDL
Lead 23.8 0.614 0.245 mg/Kg ☼12/12/16 16:50 12/13/16 01:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 79.9 0.1 0.1 %12/08/16 11:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-22Client Sample ID: DL-2
Matrix: SoilDate Collected: 12/06/16 17:00
Date Received: 12/07/16 09:40
Method: 6020B - Metals (ICP/MS)
RL MDL
Lead 9.10 0.644 0.258 mg/Kg ☼12/12/16 16:50 12/13/16 01:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 77.1 0.1 0.1 %12/08/16 11:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-23Client Sample ID: HO-1
Matrix: OilDate Collected: 12/06/16 09:30
Date Received: 12/07/16 09:40
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <2.36 2.36 2.36 mg/Kg 12/08/16 12:37 12/08/16 23:42 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.36 2.36 mg/Kg 12/08/16 12:37 12/08/16 23:42 5PCB-1221 <2.36
2.36 2.36 mg/Kg 12/08/16 12:37 12/08/16 23:42 5PCB-1232 <2.36
2.36 2.36 mg/Kg 12/08/16 12:37 12/08/16 23:42 5PCB-1242 <2.36
2.36 2.36 mg/Kg 12/08/16 12:37 12/08/16 23:42 5PCB-1248 <2.36
2.36 2.36 mg/Kg 12/08/16 12:37 12/08/16 23:42 5PCB-1254 <2.36
2.36 2.36 mg/Kg 12/08/16 12:37 12/08/16 23:42 5PCB-1260 <2.36
DCB Decachlorobiphenyl (Surr)0 X 20-150 12/08/16 12:37 12/08/16 23:42 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 66 12/08/16 12:37 12/08/16 23:42 519-147
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-24Client Sample ID: HO-2
Matrix: OilDate Collected: 12/06/16 09:35
Date Received: 12/07/16 09:40
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <2.23 2.23 2.23 mg/Kg 12/08/16 12:37 12/08/16 23:58 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.23 2.23 mg/Kg 12/08/16 12:37 12/08/16 23:58 5PCB-1221 <2.23
2.23 2.23 mg/Kg 12/08/16 12:37 12/08/16 23:58 5PCB-1232 <2.23
2.23 2.23 mg/Kg 12/08/16 12:37 12/08/16 23:58 5PCB-1242 <2.23
2.23 2.23 mg/Kg 12/08/16 12:37 12/08/16 23:58 5PCB-1248 <2.23
2.23 2.23 mg/Kg 12/08/16 12:37 12/08/16 23:58 5PCB-1254 <2.23
2.23 2.23 mg/Kg 12/08/16 12:37 12/08/16 23:58 5PCB-1260 <2.23
DCB Decachlorobiphenyl (Surr)0 X 20-150 12/08/16 12:37 12/08/16 23:58 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 60 12/08/16 12:37 12/08/16 23:58 519-147
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-25Client Sample ID: TMW-1
Matrix: WaterDate Collected: 12/06/16 11:30
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 12/08/16 19:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 0.200 ug/L 12/08/16 19:49 1Benzene<0.200
1.00 0.210 ug/L 12/08/16 19:49 1Bromobenzene<0.210
1.00 0.150 ug/L 12/08/16 19:49 1Bromochloromethane<0.150
1.00 0.170 ug/L 12/08/16 19:49 1Bromodichloromethane<0.170
1.00 0.290 ug/L 12/08/16 19:49 1Bromoform<0.290
1.00 0.350 ug/L 12/08/16 19:49 1Bromomethane<0.350
50.0 2.64 ug/L 12/08/16 19:49 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 12/08/16 19:49 1Carbon disulfide <0.220
1.00 0.180 ug/L 12/08/16 19:49 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 12/08/16 19:49 1Chlorobenzene<0.180
1.00 0.250 ug/L 12/08/16 19:49 1Chlorodibromomethane<0.250
1.00 0.360 ug/L 12/08/16 19:49 1Chloroethane<0.360
1.00 0.230 ug/L 12/08/16 19:49 1Chloroform<0.230
1.00 0.360 ug/L 12/08/16 19:49 1Chloromethane0.501 J
1.00 0.180 ug/L 12/08/16 19:49 12-Chlorotoluene <0.180
1.00 0.170 ug/L 12/08/16 19:49 14-Chlorotoluene <0.170
1.00 0.210 ug/L 12/08/16 19:49 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 12/08/16 19:49 1cis-1,3-Dichloropropene <0.170
10.0 0.940 ug/L 12/08/16 19:49 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 12/08/16 19:49 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 12/08/16 19:49 1Dibromomethane<0.450
1.00 0.190 ug/L 12/08/16 19:49 11,2-Dichlorobenzene <0.190
1.00 0.180 ug/L 12/08/16 19:49 11,3-Dichlorobenzene <0.180
1.00 0.170 ug/L 12/08/16 19:49 11,4-Dichlorobenzene <0.170
1.00 0.170 ug/L 12/08/16 19:49 1Dichlorodifluoromethane<0.170
1.00 0.240 ug/L 12/08/16 19:49 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 12/08/16 19:49 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 12/08/16 19:49 11,1-Dichloroethene <0.250
1.00 0.210 ug/L 12/08/16 19:49 11,2-Dichloroethene, Total <0.210
1.00 0.250 ug/L 12/08/16 19:49 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 12/08/16 19:49 11,3-Dichloropropane <0.190
1.00 0.160 ug/L 12/08/16 19:49 12,2-Dichloropropane <0.160
1.00 0.200 ug/L 12/08/16 19:49 11,1-Dichloropropene <0.200
2.00 0.170 ug/L 12/08/16 19:49 1Diisopropyl ether <0.170
1.00 0.190 ug/L 12/08/16 19:49 1Ethylbenzene<0.190
2.00 0.380 ug/L 12/08/16 19:49 1Hexachlorobutadiene<0.380
10.0 1.28 ug/L 12/08/16 19:49 12-Hexanone <1.28
1.00 0.330 ug/L 12/08/16 19:49 1Isopropylbenzene<0.330
5.00 1.00 ug/L 12/08/16 19:49 1Methylene Chloride <1.00
10.0 0.810 ug/L 12/08/16 19:49 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.170 ug/L 12/08/16 19:49 1Methyl tert-butyl ether <0.170
5.00 0.210 ug/L 12/08/16 19:49 1Naphthalene<0.210
1.00 0.240 ug/L 12/08/16 19:49 1n-Butylbenzene <0.240
1.00 0.170 ug/L 12/08/16 19:49 1N-Propylbenzene <0.170
1.00 0.170 ug/L 12/08/16 19:49 1p-Isopropyltoluene <0.170
1.00 0.170 ug/L 12/08/16 19:49 1sec-Butylbenzene <0.170
1.00 0.280 ug/L 12/08/16 19:49 1Styrene<0.280
1.00 0.170 ug/L 12/08/16 19:49 1tert-Butylbenzene <0.170
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-25Client Sample ID: TMW-1
Matrix: WaterDate Collected: 12/06/16 11:30
Date Received: 12/07/16 09:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane <0.150 1.00 0.150 ug/L 12/08/16 19:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 0.190 ug/L 12/08/16 19:49 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 12/08/16 19:49 1Tetrachloroethene<0.140
1.00 0.170 ug/L 12/08/16 19:49 1Toluene<0.170
1.00 0.230 ug/L 12/08/16 19:49 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 12/08/16 19:49 1trans-1,3-Dichloropropene <0.170
1.00 0.230 ug/L 12/08/16 19:49 11,2,3-Trichlorobenzene <0.230
1.00 0.200 ug/L 12/08/16 19:49 11,2,4-Trichlorobenzene <0.200
1.00 0.190 ug/L 12/08/16 19:49 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 12/08/16 19:49 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 12/08/16 19:49 1Trichloroethene<0.200
1.00 0.210 ug/L 12/08/16 19:49 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 12/08/16 19:49 11,2,3-Trichloropropane <0.230
1.00 0.170 ug/L 12/08/16 19:49 11,2,4-Trimethylbenzene <0.170
1.00 0.170 ug/L 12/08/16 19:49 11,3,5-Trimethylbenzene <0.170
1.00 0.180 ug/L 12/08/16 19:49 1Vinyl chloride <0.180
3.00 0.580 ug/L 12/08/16 19:49 1Xylenes, Total <0.580
4-Bromofluorobenzene (Surr)85 70-130 12/08/16 19:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)94 12/08/16 19:49 170-130
1,2-Dichloroethane-d4 (Surr)84 12/08/16 19:49 170-130
Toluene-d8 (Surr)111 12/08/16 19:49 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.296 1.85 0.296 ug/L 12/08/16 10:43 12/08/16 20:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.85 0.324 ug/L 12/08/16 10:43 12/08/16 20:15 1Acenaphthylene<0.324
1.85 0.352 ug/L 12/08/16 10:43 12/08/16 20:15 1Anthracene<0.352
1.85 0.296 ug/L 12/08/16 10:43 12/08/16 20:15 1Benzo[a]anthracene <0.296
1.85 0.352 ug/L 12/08/16 10:43 12/08/16 20:15 1Benzo[a]pyrene <0.352
1.85 0.333 ug/L 12/08/16 10:43 12/08/16 20:15 1Benzo[b]fluoranthene <0.333
1.85 0.574 ug/L 12/08/16 10:43 12/08/16 20:15 1Benzo[g,h,i]perylene <0.574
1.85 0.343 ug/L 12/08/16 10:43 12/08/16 20:15 1Benzo[k]fluoranthene <0.343
9.26 1.76 ug/L 12/08/16 10:43 12/08/16 20:15 1Bis(2-chloroethoxy)methane <1.76
9.26 1.20 ug/L 12/08/16 10:43 12/08/16 20:15 1Bis(2-chloroethyl)ether <1.20
9.26 1.67 ug/L 12/08/16 10:43 12/08/16 20:15 1bis (2-chloroisopropyl) ether <1.67
9.26 1.39 ug/L 12/08/16 10:43 12/08/16 20:15 1Bis(2-ethylhexyl) phthalate <1.39
9.26 1.48 ug/L 12/08/16 10:43 12/08/16 20:15 14-Bromophenyl phenyl ether <1.48
9.26 0.926 ug/L 12/08/16 10:43 12/08/16 20:15 1Butyl benzyl phthalate <0.926
9.26 0.833 ug/L 12/08/16 10:43 12/08/16 20:15 1Carbazole<0.833
9.26 1.11 ug/L 12/08/16 10:43 12/08/16 20:15 14-Chloroaniline <1.11
9.26 1.30 ug/L 12/08/16 10:43 12/08/16 20:15 14-Chloro-3-methylphenol <1.30
9.26 1.39 ug/L 12/08/16 10:43 12/08/16 20:15 12-Chloronaphthalene <1.39
9.26 1.57 ug/L 12/08/16 10:43 12/08/16 20:15 12-Chlorophenol <1.57
9.26 1.48 ug/L 12/08/16 10:43 12/08/16 20:15 14-Chlorophenyl phenyl ether <1.48
1.85 0.306 ug/L 12/08/16 10:43 12/08/16 20:15 1Chrysene<0.306
9.26 2.78 ug/L 12/08/16 10:43 12/08/16 20:15 1Cresols<2.78
1.85 0.417 ug/L 12/08/16 10:43 12/08/16 20:15 1Dibenz(a,h)anthracene <0.417
9.26 1.20 ug/L 12/08/16 10:43 12/08/16 20:15 1Dibenzofuran<1.20
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-25Client Sample ID: TMW-1
Matrix: WaterDate Collected: 12/06/16 11:30
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene <2.04 9.26 2.04 ug/L 12/08/16 10:43 12/08/16 20:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.26 1.85 ug/L 12/08/16 10:43 12/08/16 20:15 11,3-Dichlorobenzene <1.85
9.26 1.85 ug/L 12/08/16 10:43 12/08/16 20:15 11,4-Dichlorobenzene <1.85
9.26 1.39 ug/L 12/08/16 10:43 12/08/16 20:15 13,3'-Dichlorobenzidine <1.39
9.26 2.04 ug/L 12/08/16 10:43 12/08/16 20:15 12,4-Dichlorophenol <2.04
9.26 1.11 ug/L 12/08/16 10:43 12/08/16 20:15 1Diethyl phthalate <1.11
9.26 1.48 ug/L 12/08/16 10:43 12/08/16 20:15 12,4-Dimethylphenol <1.48
9.26 1.11 ug/L 12/08/16 10:43 12/08/16 20:15 1Dimethyl phthalate <1.11
9.26 1.20 ug/L 12/08/16 10:43 12/08/16 20:15 1Di-n-butyl phthalate <1.20
23.1 2.69 ug/L 12/08/16 10:43 12/08/16 20:15 14,6-Dinitro-2-methylphenol <2.69
23.1 6.67 ug/L 12/08/16 10:43 12/08/16 20:15 12,4-Dinitrophenol <6.67
9.26 1.48 ug/L 12/08/16 10:43 12/08/16 20:15 12,4-Dinitrotoluene <1.48
9.26 1.39 ug/L 12/08/16 10:43 12/08/16 20:15 12,6-Dinitrotoluene <1.39
9.26 0.833 ug/L 12/08/16 10:43 12/08/16 20:15 1Di-n-octyl phthalate <0.833
1.85 0.296 ug/L 12/08/16 10:43 12/08/16 20:15 1Fluoranthene<0.296
1.85 0.296 ug/L 12/08/16 10:43 12/08/16 20:15 1Fluorene<0.296
9.26 1.39 ug/L 12/08/16 10:43 12/08/16 20:15 1Hexachlorobenzene<1.39
9.26 1.39 ug/L 12/08/16 10:43 12/08/16 20:15 1Hexachlorobutadiene<1.39
9.26 1.20 ug/L 12/08/16 10:43 12/08/16 20:15 1Hexachlorocyclopentadiene<1.20
9.26 2.04 ug/L 12/08/16 10:43 12/08/16 20:15 1Hexachloroethane<2.04
1.85 0.380 ug/L 12/08/16 10:43 12/08/16 20:15 1Indeno[1,2,3-cd]pyrene <0.380
9.26 2.04 ug/L 12/08/16 10:43 12/08/16 20:15 1Isophorone<2.04
1.85 0.333 ug/L 12/08/16 10:43 12/08/16 20:15 11-Methylnaphthalene <0.333
1.85 0.370 ug/L 12/08/16 10:43 12/08/16 20:15 12-Methylnaphthalene <0.370
9.26 1.48 ug/L 12/08/16 10:43 12/08/16 20:15 12-Methylphenol <1.48
9.26 1.30 ug/L 12/08/16 10:43 12/08/16 20:15 13 & 4 Methylphenol <1.30
1.85 0.343 ug/L 12/08/16 10:43 12/08/16 20:15 1Naphthalene<0.343
23.1 1.02 ug/L 12/08/16 10:43 12/08/16 20:15 12-Nitroaniline <1.02
23.1 1.48 ug/L 12/08/16 10:43 12/08/16 20:15 13-Nitroaniline <1.48
23.1 1.48 ug/L 12/08/16 10:43 12/08/16 20:15 14-Nitroaniline <1.48
9.26 2.04 ug/L 12/08/16 10:43 12/08/16 20:15 1Nitrobenzene<2.04
9.26 2.22 ug/L 12/08/16 10:43 12/08/16 20:15 12-Nitrophenol <2.22
23.1 1.85 ug/L 12/08/16 10:43 12/08/16 20:15 14-Nitrophenol <1.85
9.26 1.57 ug/L 12/08/16 10:43 12/08/16 20:15 1N-Nitrosodi-n-propylamine <1.57
9.26 3.33 ug/L 12/08/16 10:43 12/08/16 20:15 1n-Nitrosodiphenylamine(as
diphenylamine)
<3.33
23.1 3.06 ug/L 12/08/16 10:43 12/08/16 20:15 1Pentachlorophenol<3.06
1.85 0.389 ug/L 12/08/16 10:43 12/08/16 20:15 1Phenanthrene<0.389
9.26 1.39 ug/L 12/08/16 10:43 12/08/16 20:15 1Phenol<1.39
1.85 0.324 ug/L 12/08/16 10:43 12/08/16 20:15 1Pyrene<0.324
9.26 1.94 ug/L 12/08/16 10:43 12/08/16 20:15 11,2,4-Trichlorobenzene <1.94
9.26 1.20 ug/L 12/08/16 10:43 12/08/16 20:15 12,4,5-Trichlorophenol <1.20
9.26 1.76 ug/L 12/08/16 10:43 12/08/16 20:15 12,4,6-Trichlorophenol <1.76
2-Fluorobiphenyl (Surr)59 29-120 12/08/16 10:43 12/08/16 20:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)33 12/08/16 10:43 12/08/16 20:15 110-120
Nitrobenzene-d5 (Surr)60 12/08/16 10:43 12/08/16 20:15 127-120
Phenol-d5 (Surr)21 12/08/16 10:43 12/08/16 20:15 110-120
Terphenyl-d14 (Surr)80 12/08/16 10:43 12/08/16 20:15 113-120
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Client Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Lab Sample ID: 490-117643-25Client Sample ID: TMW-1
Matrix: WaterDate Collected: 12/06/16 11:30
Date Received: 12/07/16 09:40
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)80 10-120 12/08/16 10:43 12/08/16 20:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Silver <0.00300 0.00500 0.00300 mg/L 12/09/16 09:00 12/12/16 16:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00860 mg/L 12/09/16 09:00 12/12/16 16:02 1Arsenic<0.00860
0.0100 0.00500 mg/L 12/09/16 09:00 12/12/16 16:02 1Barium0.0618
0.00100 0.000500 mg/L 12/09/16 09:00 12/12/16 16:02 1Cadmium<0.000500
0.00500 0.00300 mg/L 12/09/16 09:00 12/12/16 16:02 1Chromium<0.00300
0.00500 0.00200 mg/L 12/09/16 09:00 12/12/16 16:02 1Lead<0.00200
0.0100 0.00500 mg/L 12/09/16 09:00 12/12/16 16:02 1Selenium<0.00500
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.000100 0.000200 0.000100 mg/L 12/08/16 09:10 12/08/16 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-392730/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392730
RL MDL
Acetone <0.00840 0.0500 0.00840 mg/Kg 12/08/16 14:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1Benzene
<0.000720 0.0007200.00200 mg/Kg 12/08/16 14:17 1Bromobenzene
<0.000550 0.0005500.00200 mg/Kg 12/08/16 14:17 1Bromochloromethane
<0.000550 0.0005500.00200 mg/Kg 12/08/16 14:17 1Bromodichloromethane
<0.000550 0.0005500.00200 mg/Kg 12/08/16 14:17 1Bromoform
<0.00120 0.001200.00200 mg/Kg 12/08/16 14:17 1Bromomethane
<0.00510 0.005100.0500 mg/Kg 12/08/16 14:17 12-Butanone (MEK)
<0.00360 0.003600.00500 mg/Kg 12/08/16 14:17 1Carbon disulfide
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1Carbon tetrachloride
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1Chlorobenzene
<0.000340 0.0003400.00200 mg/Kg 12/08/16 14:17 1Chlorodibromomethane
<0.00190 0.001900.00500 mg/Kg 12/08/16 14:17 1Chloroethane
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1Chloroform
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1Chloromethane
<0.000890 0.0008900.00200 mg/Kg 12/08/16 14:17 12-Chlorotoluene
<0.000840 0.0008400.00200 mg/Kg 12/08/16 14:17 14-Chlorotoluene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1cis-1,2-Dichloroethene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1cis-1,3-Dichloropropene
<0.000700 0.0007000.00500 mg/Kg 12/08/16 14:17 11,2-Dibromo-3-Chloropropane
<0.00100 0.001000.00200 mg/Kg 12/08/16 14:17 11,2-Dibromoethane (EDB)
<0.000560 0.0005600.00200 mg/Kg 12/08/16 14:17 1Dibromomethane
<0.000340 0.0003400.00200 mg/Kg 12/08/16 14:17 11,2-Dichlorobenzene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 11,3-Dichlorobenzene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 11,4-Dichlorobenzene
<0.00100 0.001000.00200 mg/Kg 12/08/16 14:17 1Dichlorodifluoromethane
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 11,1-Dichloroethane
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 11,2-Dichloroethane
<0.000570 0.0005700.00200 mg/Kg 12/08/16 14:17 11,1-Dichloroethene
<0.000470 0.0004700.00200 mg/Kg 12/08/16 14:17 11,2-Dichloroethene, Total
<0.000940 0.0009400.00200 mg/Kg 12/08/16 14:17 11,2-Dichloropropane
<0.000940 0.0009400.00200 mg/Kg 12/08/16 14:17 11,3-Dichloropropane
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 12,2-Dichloropropane
<0.000510 0.0005100.00200 mg/Kg 12/08/16 14:17 11,1-Dichloropropene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1Diisopropyl ether
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1Ethylbenzene
<0.00114 0.001140.00500 mg/Kg 12/08/16 14:17 1Hexachlorobutadiene
<0.0167 0.01670.0500 mg/Kg 12/08/16 14:17 12-Hexanone
<0.000410 0.0004100.00200 mg/Kg 12/08/16 14:17 1Isopropylbenzene
<0.000860 0.0008600.0100 mg/Kg 12/08/16 14:17 1Methylene Chloride
<0.00190 0.001900.0500 mg/Kg 12/08/16 14:17 14-Methyl-2-pentanone (MIBK)
<0.000960 0.0009600.00200 mg/Kg 12/08/16 14:17 1Methyl tert-butyl ether
<0.00170 0.001700.00500 mg/Kg 12/08/16 14:17 1Naphthalene
<0.000980 0.0009800.00200 mg/Kg 12/08/16 14:17 1n-Butylbenzene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1N-Propylbenzene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1p-Isopropyltoluene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1sec-Butylbenzene
<0.00110 0.001100.00200 mg/Kg 12/08/16 14:17 1Styrene
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392730/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392730
RL MDL
tert-Butylbenzene <0.000900 0.00200 0.000900 mg/Kg 12/08/16 14:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 11,1,1,2-Tetrachloroethane
<0.00100 0.001000.00200 mg/Kg 12/08/16 14:17 11,1,2,2-Tetrachloroethane
<0.000730 0.0007300.00200 mg/Kg 12/08/16 14:17 1Tetrachloroethene
<0.000740 0.0007400.00200 mg/Kg 12/08/16 14:17 1Toluene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1trans-1,2-Dichloroethene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 1trans-1,3-Dichloropropene
<0.000380 0.0003800.00200 mg/Kg 12/08/16 14:17 11,2,3-Trichlorobenzene
<0.000670 0.0006700.00200 mg/Kg 12/08/16 14:17 11,2,4-Trichlorobenzene
<0.000920 0.0009200.00200 mg/Kg 12/08/16 14:17 11,1,1-Trichloroethane
<0.00140 0.001400.00500 mg/Kg 12/08/16 14:17 11,1,2-Trichloroethane
<0.000960 0.0009600.00200 mg/Kg 12/08/16 14:17 1Trichloroethene
<0.00100 0.001000.00200 mg/Kg 12/08/16 14:17 1Trichlorofluoromethane
<0.000550 0.0005500.00200 mg/Kg 12/08/16 14:17 11,2,3-Trichloropropane
<0.00100 0.001000.00200 mg/Kg 12/08/16 14:17 11,2,4-Trimethylbenzene
<0.000750 0.0007500.00200 mg/Kg 12/08/16 14:17 11,3,5-Trimethylbenzene
<0.00110 0.001100.00200 mg/Kg 12/08/16 14:17 1Vinyl chloride
<0.00123 0.001230.00600 mg/Kg 12/08/16 14:17 1Xylenes, Total
4-Bromofluorobenzene (Surr)88 70-130 12/08/16 14:17 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
124 12/08/16 14:17 1Dibromofluoromethane (Surr)70-130
119 12/08/16 14:17 11,2-Dichloroethane-d4 (Surr)70-130
88 12/08/16 14:17 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392730/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392730
Acetone 0.250 0.2728 mg/Kg 109 45-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.05893 mg/Kg 118 70-130
Bromobenzene 0.0500 0.04428 mg/Kg 89 67-130
Bromochloromethane 0.0500 0.05943 mg/Kg 119 70-133
Bromodichloromethane 0.0500 0.05066 mg/Kg 101 70-130
Bromoform 0.0500 0.04618 mg/Kg 92 59-137
Bromomethane 0.0500 0.06672 mg/Kg 133 32-150
2-Butanone (MEK)0.250 0.2685 mg/Kg 107 50-149
Carbon disulfide 0.0500 0.05655 mg/Kg 113 66-138
Carbon tetrachloride 0.0500 0.05532 mg/Kg 111 70-131
Chlorobenzene 0.0500 0.05244 mg/Kg 105 70-130
Chlorodibromomethane 0.0500 0.04668 mg/Kg 93 70-130
Chloroethane 0.0500 0.05440 mg/Kg 109 37-150
Chloroform 0.0500 0.05776 mg/Kg 116 70-130
Chloromethane 0.0500 0.04718 mg/Kg 94 53-150
2-Chlorotoluene 0.0500 0.04823 mg/Kg 96 70-132
4-Chlorotoluene 0.0500 0.05061 mg/Kg 101 67-135
cis-1,2-Dichloroethene 0.0500 0.05989 mg/Kg 120 70-132
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392730/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392730
cis-1,3-Dichloropropene 0.0500 0.04645 mg/Kg 93 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.04305 mg/Kg 86 47-144
1,2-Dibromoethane (EDB)0.0500 0.05110 mg/Kg 102 69-130
Dibromomethane 0.0500 0.05615 mg/Kg 112 70-130
1,2-Dichlorobenzene 0.0500 0.05453 mg/Kg 109 70-134
1,3-Dichlorobenzene 0.0500 0.05415 mg/Kg 108 69-137
1,4-Dichlorobenzene 0.0500 0.05449 mg/Kg 109 66-134
Dichlorodifluoromethane 0.0500 0.06858 mg/Kg 137 32-150
1,1-Dichloroethane 0.0500 0.05245 mg/Kg 105 70-130
1,2-Dichloroethane 0.0500 0.05335 mg/Kg 107 65-134
1,1-Dichloroethene 0.0500 0.05522 mg/Kg 110 70-131
1,2-Dichloroethene, Total 0.100 0.1144 mg/Kg 114 70-130
1,2-Dichloropropane 0.0500 0.05049 mg/Kg 101 70-130
1,3-Dichloropropane 0.0500 0.04842 mg/Kg 97 70-130
2,2-Dichloropropane 0.0500 0.05186 mg/Kg 104 57-150
1,1-Dichloropropene 0.0500 0.05430 mg/Kg 109 70-130
Diisopropyl ether 0.0500 0.04762 mg/Kg 95 68-134
Ethylbenzene 0.0500 0.05411 mg/Kg 108 70-130
Hexachlorobutadiene 0.0500 0.05765 mg/Kg 115 64-137
2-Hexanone 0.250 0.2460 mg/Kg 98 47-148
Isopropylbenzene 0.0500 0.05489 mg/Kg 110 70-130
Methylene Chloride 0.0500 0.05731 mg/Kg 115 69-130
4-Methyl-2-pentanone (MIBK)0.250 0.2432 mg/Kg 97 48-150
Methyl tert-butyl ether 0.0500 0.05738 mg/Kg 115 54-145
Naphthalene 0.0500 0.05458 mg/Kg 109 55-149
n-Butylbenzene 0.0500 0.05124 mg/Kg 102 57-150
N-Propylbenzene 0.0500 0.04925 mg/Kg 98 62-150
p-Isopropyltoluene 0.0500 0.05380 mg/Kg 108 66-147
sec-Butylbenzene 0.0500 0.05177 mg/Kg 104 68-147
Styrene 0.0500 0.05419 mg/Kg 108 70-131
tert-Butylbenzene 0.0500 0.04958 mg/Kg 99 70-138
1,1,1,2-Tetrachloroethane 0.0500 0.04840 mg/Kg 97 70-130
1,1,2,2-Tetrachloroethane 0.0500 0.04425 mg/Kg 89 61-134
Tetrachloroethene 0.0500 0.05482 mg/Kg 110 70-130
Toluene 0.0500 0.05279 mg/Kg 106 70-130
trans-1,2-Dichloroethene 0.0500 0.05449 mg/Kg 109 70-130
trans-1,3-Dichloropropene 0.0500 0.04566 mg/Kg 91 67-130
1,2,3-Trichlorobenzene 0.0500 0.05711 mg/Kg 114 57-146
1,2,4-Trichlorobenzene 0.0500 0.05902 mg/Kg 118 47-150
1,1,1-Trichloroethane 0.0500 0.05716 mg/Kg 114 70-130
1,1,2-Trichloroethane 0.0500 0.05144 mg/Kg 103 70-130
Trichloroethene 0.0500 0.05835 mg/Kg 117 70-130
Trichlorofluoromethane 0.0500 0.05859 mg/Kg 117 53-150
1,2,3-Trichloropropane 0.0500 0.04696 mg/Kg 94 60-139
1,2,4-Trimethylbenzene 0.0500 0.05239 mg/Kg 105 70-140
1,3,5-Trimethylbenzene 0.0500 0.05744 mg/Kg 115 69-141
Vinyl chloride 0.0500 0.05369 mg/Kg 107 63-150
Xylenes, Total 0.100 0.1074 mg/Kg 107 70-130
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392730/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392730
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
LCS LCS
Qualifier Limits%Recovery
99Dibromofluoromethane (Surr)70 -130
961,2-Dichloroethane-d4 (Surr)70 -130
93Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392730/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392730
Acetone 0.250 0.2877 mg/Kg 115 45-145 5 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05967 mg/Kg 119 70-130 1 37
Bromobenzene 0.0500 0.04510 mg/Kg 90 67-130 2 40
Bromochloromethane 0.0500 0.06133 mg/Kg 123 70-133 3 15
Bromodichloromethane 0.0500 0.05269 mg/Kg 105 70-130 4 20
Bromoform 0.0500 0.04654 mg/Kg 93 59-137 1 17
Bromomethane 0.0500 0.06799 mg/Kg 136 32-150 2 45
2-Butanone (MEK)0.250 0.2706 mg/Kg 108 50-149 1 39
Carbon disulfide 0.0500 0.05798 mg/Kg 116 66-138 3 41
Carbon tetrachloride 0.0500 0.05601 mg/Kg 112 70-131 1 41
Chlorobenzene 0.0500 0.05261 mg/Kg 105 70-130 0 40
Chlorodibromomethane 0.0500 0.04772 mg/Kg 95 70-130 2 14
Chloroethane 0.0500 0.05625 mg/Kg 112 37-150 3 50
Chloroform 0.0500 0.05909 mg/Kg 118 70-130 2 15
Chloromethane 0.0500 0.04764 mg/Kg 95 53-150 1 47
2-Chlorotoluene 0.0500 0.04909 mg/Kg 98 70-132 2 41
4-Chlorotoluene 0.0500 0.05026 mg/Kg 101 67-135 1 41
cis-1,2-Dichloroethene 0.0500 0.05618 mg/Kg 112 70-132 6 18
cis-1,3-Dichloropropene 0.0500 0.04809 mg/Kg 96 70-130 3 42
1,2-Dibromo-3-Chloropropane 0.0500 0.04634 mg/Kg 93 47-144 7 38
1,2-Dibromoethane (EDB)0.0500 0.05245 mg/Kg 105 69-130 3 17
Dibromomethane 0.0500 0.05728 mg/Kg 115 70-130 2 19
1,2-Dichlorobenzene 0.0500 0.05578 mg/Kg 112 70-134 2 40
1,3-Dichlorobenzene 0.0500 0.05436 mg/Kg 109 69-137 0 41
1,4-Dichlorobenzene 0.0500 0.05412 mg/Kg 108 66-134 1 41
Dichlorodifluoromethane 0.0500 0.06786 mg/Kg 136 32-150 1 50
1,1-Dichloroethane 0.0500 0.05336 mg/Kg 107 70-130 2 42
1,2-Dichloroethane 0.0500 0.05436 mg/Kg 109 65-134 2 16
1,1-Dichloroethene 0.0500 0.05749 mg/Kg 115 70-131 4 43
1,2-Dichloroethene, Total 0.100 0.1108 mg/Kg 111 70-130 3 41
1,2-Dichloropropane 0.0500 0.05136 mg/Kg 103 70-130 2 15
1,3-Dichloropropane 0.0500 0.05009 mg/Kg 100 70-130 3 15
2,2-Dichloropropane 0.0500 0.05225 mg/Kg 105 57-150 1 42
1,1-Dichloropropene 0.0500 0.05520 mg/Kg 110 70-130 2 41
Diisopropyl ether 0.0500 0.04847 mg/Kg 97 68-134 2 36
Ethylbenzene 0.0500 0.05463 mg/Kg 109 70-130 1 38
Hexachlorobutadiene 0.0500 0.06014 mg/Kg 120 64-137 4 44
2-Hexanone 0.250 0.2504 mg/Kg 100 47-148 2 38
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392730/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392730
Isopropylbenzene 0.0500 0.05527 mg/Kg 111 70-130 1 39
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 0.0500 0.05735 mg/Kg 115 69-130 0 19
4-Methyl-2-pentanone (MIBK)0.250 0.2524 mg/Kg 101 48-150 4 41
Methyl tert-butyl ether 0.0500 0.05803 mg/Kg 116 54-145 1 36
Naphthalene 0.0500 0.05537 mg/Kg 111 55-149 1 37
n-Butylbenzene 0.0500 0.05256 mg/Kg 105 57-150 3 39
N-Propylbenzene 0.0500 0.05101 mg/Kg 102 62-150 4 38
p-Isopropyltoluene 0.0500 0.05506 mg/Kg 110 66-147 2 38
sec-Butylbenzene 0.0500 0.05294 mg/Kg 106 68-147 2 38
Styrene 0.0500 0.05487 mg/Kg 110 70-131 1 40
tert-Butylbenzene 0.0500 0.05099 mg/Kg 102 70-138 3 38
1,1,1,2-Tetrachloroethane 0.0500 0.04960 mg/Kg 99 70-130 2 41
1,1,2,2-Tetrachloroethane 0.0500 0.04510 mg/Kg 90 61-134 2 16
Tetrachloroethene 0.0500 0.05614 mg/Kg 112 70-130 2 41
Toluene 0.0500 0.05443 mg/Kg 109 70-130 3 40
trans-1,2-Dichloroethene 0.0500 0.05458 mg/Kg 109 70-130 0 41
trans-1,3-Dichloropropene 0.0500 0.04669 mg/Kg 93 67-130 2 41
1,2,3-Trichlorobenzene 0.0500 0.05776 mg/Kg 116 57-146 1 42
1,2,4-Trichlorobenzene 0.0500 0.05947 mg/Kg 119 47-150 1 43
1,1,1-Trichloroethane 0.0500 0.05746 mg/Kg 115 70-130 1 41
1,1,2-Trichloroethane 0.0500 0.05308 mg/Kg 106 70-130 3 17
Trichloroethene 0.0500 0.05911 mg/Kg 118 70-130 1 41
Trichlorofluoromethane 0.0500 0.05861 mg/Kg 117 53-150 0 49
1,2,3-Trichloropropane 0.0500 0.04881 mg/Kg 98 60-139 4 16
1,2,4-Trimethylbenzene 0.0500 0.05340 mg/Kg 107 70-140 2 38
1,3,5-Trimethylbenzene 0.0500 0.05756 mg/Kg 115 69-141 0 38
Vinyl chloride 0.0500 0.05335 mg/Kg 107 63-150 1 46
Xylenes, Total 0.100 0.1081 mg/Kg 108 70-130 1 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
87
LCSD LCSD
Qualifier Limits%Recovery
99Dibromofluoromethane (Surr)70 -130
1011,2-Dichloroethane-d4 (Surr)70 -130
94Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-392810/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
RL MDL
Acetone <2.66 25.0 2.66 ug/L 12/08/16 15:36 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.200 0.2001.00 ug/L 12/08/16 15:36 1Benzene
<0.210 0.2101.00 ug/L 12/08/16 15:36 1Bromobenzene
<0.150 0.1501.00 ug/L 12/08/16 15:36 1Bromochloromethane
<0.170 0.1701.00 ug/L 12/08/16 15:36 1Bromodichloromethane
<0.290 0.2901.00 ug/L 12/08/16 15:36 1Bromoform
<0.350 0.3501.00 ug/L 12/08/16 15:36 1Bromomethane
<2.64 2.6450.0 ug/L 12/08/16 15:36 12-Butanone (MEK)
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392810/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
RL MDL
Carbon disulfide <0.220 1.00 0.220 ug/L 12/08/16 15:36 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.180 0.1801.00 ug/L 12/08/16 15:36 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 12/08/16 15:36 1Chlorobenzene
<0.250 0.2501.00 ug/L 12/08/16 15:36 1Chlorodibromomethane
<0.360 0.3601.00 ug/L 12/08/16 15:36 1Chloroethane
<0.230 0.2301.00 ug/L 12/08/16 15:36 1Chloroform
<0.360 0.3601.00 ug/L 12/08/16 15:36 1Chloromethane
<0.180 0.1801.00 ug/L 12/08/16 15:36 12-Chlorotoluene
<0.170 0.1701.00 ug/L 12/08/16 15:36 14-Chlorotoluene
<0.210 0.2101.00 ug/L 12/08/16 15:36 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 12/08/16 15:36 1cis-1,3-Dichloropropene
<0.940 0.94010.0 ug/L 12/08/16 15:36 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 12/08/16 15:36 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 12/08/16 15:36 1Dibromomethane
<0.190 0.1901.00 ug/L 12/08/16 15:36 11,2-Dichlorobenzene
<0.180 0.1801.00 ug/L 12/08/16 15:36 11,3-Dichlorobenzene
<0.170 0.1701.00 ug/L 12/08/16 15:36 11,4-Dichlorobenzene
<0.170 0.1701.00 ug/L 12/08/16 15:36 1Dichlorodifluoromethane
<0.240 0.2401.00 ug/L 12/08/16 15:36 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 12/08/16 15:36 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 12/08/16 15:36 11,1-Dichloroethene
<0.210 0.2101.00 ug/L 12/08/16 15:36 11,2-Dichloroethene, Total
<0.250 0.2501.00 ug/L 12/08/16 15:36 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 12/08/16 15:36 11,3-Dichloropropane
<0.160 0.1601.00 ug/L 12/08/16 15:36 12,2-Dichloropropane
<0.200 0.2001.00 ug/L 12/08/16 15:36 11,1-Dichloropropene
<0.170 0.1702.00 ug/L 12/08/16 15:36 1Diisopropyl ether
<0.190 0.1901.00 ug/L 12/08/16 15:36 1Ethylbenzene
<0.380 0.3802.00 ug/L 12/08/16 15:36 1Hexachlorobutadiene
<1.28 1.2810.0 ug/L 12/08/16 15:36 12-Hexanone
<0.330 0.3301.00 ug/L 12/08/16 15:36 1Isopropylbenzene
<1.00 1.005.00 ug/L 12/08/16 15:36 1Methylene Chloride
<0.810 0.81010.0 ug/L 12/08/16 15:36 14-Methyl-2-pentanone (MIBK)
<0.170 0.1701.00 ug/L 12/08/16 15:36 1Methyl tert-butyl ether
<0.210 0.2105.00 ug/L 12/08/16 15:36 1Naphthalene
<0.240 0.2401.00 ug/L 12/08/16 15:36 1n-Butylbenzene
<0.170 0.1701.00 ug/L 12/08/16 15:36 1N-Propylbenzene
<0.170 0.1701.00 ug/L 12/08/16 15:36 1p-Isopropyltoluene
<0.170 0.1701.00 ug/L 12/08/16 15:36 1sec-Butylbenzene
<0.280 0.2801.00 ug/L 12/08/16 15:36 1Styrene
<0.170 0.1701.00 ug/L 12/08/16 15:36 1tert-Butylbenzene
<0.150 0.1501.00 ug/L 12/08/16 15:36 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 12/08/16 15:36 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 12/08/16 15:36 1Tetrachloroethene
<0.170 0.1701.00 ug/L 12/08/16 15:36 1Toluene
<0.230 0.2301.00 ug/L 12/08/16 15:36 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 12/08/16 15:36 1trans-1,3-Dichloropropene
<0.230 0.2301.00 ug/L 12/08/16 15:36 11,2,3-Trichlorobenzene
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392810/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
RL MDL
1,2,4-Trichlorobenzene <0.200 1.00 0.200 ug/L 12/08/16 15:36 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.190 0.1901.00 ug/L 12/08/16 15:36 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 12/08/16 15:36 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 12/08/16 15:36 1Trichloroethene
<0.210 0.2101.00 ug/L 12/08/16 15:36 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 12/08/16 15:36 11,2,3-Trichloropropane
<0.170 0.1701.00 ug/L 12/08/16 15:36 11,2,4-Trimethylbenzene
<0.170 0.1701.00 ug/L 12/08/16 15:36 11,3,5-Trimethylbenzene
<0.180 0.1801.00 ug/L 12/08/16 15:36 1Vinyl chloride
<0.580 0.5803.00 ug/L 12/08/16 15:36 1Xylenes, Total
4-Bromofluorobenzene (Surr)87 70-130 12/08/16 15:36 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 12/08/16 15:36 1Dibromofluoromethane (Surr)70-130
83 12/08/16 15:36 11,2-Dichloroethane-d4 (Surr)70-130
111 12/08/16 15:36 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392810/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
Acetone 100 90.09 ug/L 90 39-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 20.0 18.55 ug/L 93 70-130
Bromobenzene 20.0 20.20 ug/L 101 70-130
Bromochloromethane 20.0 19.30 ug/L 96 70-130
Bromodichloromethane 20.0 19.31 ug/L 97 70-130
Bromoform 20.0 17.71 ug/L 89 70-137
Bromomethane 20.0 12.07 ug/L 60 53-150
2-Butanone (MEK)100 97.45 ug/L 97 55-143
Carbon disulfide 20.0 15.28 ug/L 76 64-135
Carbon tetrachloride 20.0 19.27 ug/L 96 70-147
Chlorobenzene 20.0 19.60 ug/L 98 70-130
Chlorodibromomethane 20.0 20.58 ug/L 103 70-133
Chloroethane 20.0 19.89 ug/L 99 60-138
Chloroform 20.0 19.27 ug/L 96 70-130
Chloromethane 20.0 17.11 ug/L 86 33-150
2-Chlorotoluene 20.0 18.47 ug/L 92 70-130
4-Chlorotoluene 20.0 18.58 ug/L 93 70-130
cis-1,2-Dichloroethene 20.0 18.09 ug/L 90 70-130
cis-1,3-Dichloropropene 20.0 20.67 ug/L 103 70-133
1,2-Dibromo-3-Chloropropane 20.0 20.59 ug/L 103 45-138
1,2-Dibromoethane (EDB)20.0 20.08 ug/L 100 70-130
Dibromomethane 20.0 19.67 ug/L 98 70-130
1,2-Dichlorobenzene 20.0 19.87 ug/L 99 70-130
1,3-Dichlorobenzene 20.0 19.04 ug/L 95 70-130
1,4-Dichlorobenzene 20.0 19.46 ug/L 97 70-130
Dichlorodifluoromethane 20.0 24.40 ug/L 122 48-150
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392810/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
1,1-Dichloroethane 20.0 19.03 ug/L 95 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane 20.0 21.93 ug/L 110 70-130
1,1-Dichloroethene 20.0 17.80 ug/L 89 70-132
1,2-Dichloroethene, Total 40.0 36.26 ug/L 91 70-130
1,2-Dichloropropane 20.0 18.64 ug/L 93 70-130
1,3-Dichloropropane 20.0 19.74 ug/L 99 70-130
2,2-Dichloropropane 20.0 22.56 ug/L 113 60-143
1,1-Dichloropropene 20.0 18.12 ug/L 91 70-130
Diisopropyl ether 20.0 20.00 ug/L 100 66-142
Ethylbenzene 20.0 18.66 ug/L 93 70-130
Hexachlorobutadiene 20.0 17.50 ug/L 88 70-138
2-Hexanone 100 98.38 ug/L 98 54-142
Isopropylbenzene 20.0 18.63 ug/L 93 70-131
Methylene Chloride 20.0 19.69 ug/L 98 70-130
4-Methyl-2-pentanone (MIBK)100 95.74 ug/L 96 60-137
Methyl tert-butyl ether 20.0 20.60 ug/L 103 70-130
Naphthalene 20.0 22.79 ug/L 114 54-150
n-Butylbenzene 20.0 16.75 ug/L 84 68-137
N-Propylbenzene 20.0 17.67 ug/L 88 70-134
p-Isopropyltoluene 20.0 17.39 ug/L 87 66-130
sec-Butylbenzene 20.0 16.80 ug/L 84 70-135
Styrene 20.0 19.67 ug/L 98 70-130
tert-Butylbenzene 20.0 17.29 ug/L 86 70-130
1,1,1,2-Tetrachloroethane 20.0 18.99 ug/L 95 70-130
1,1,2,2-Tetrachloroethane 20.0 21.38 ug/L 107 69-131
Tetrachloroethene 20.0 18.28 ug/L 91 70-130
Toluene 20.0 18.43 ug/L 92 70-130
trans-1,2-Dichloroethene 20.0 18.17 ug/L 91 70-130
trans-1,3-Dichloropropene 20.0 21.08 ug/L 105 63-142
1,2,3-Trichlorobenzene 20.0 21.46 ug/L 107 46-150
1,2,4-Trichlorobenzene 20.0 20.81 ug/L 104 58-147
1,1,1-Trichloroethane 20.0 19.16 ug/L 96 70-135
1,1,2-Trichloroethane 20.0 18.94 ug/L 95 70-130
Trichloroethene 20.0 17.61 ug/L 88 70-130
Trichlorofluoromethane 20.0 18.71 ug/L 94 59-150
1,2,3-Trichloropropane 20.0 19.44 ug/L 97 70-131
1,2,4-Trimethylbenzene 20.0 17.92 ug/L 90 70-130
1,3,5-Trimethylbenzene 20.0 17.79 ug/L 89 70-130
Vinyl chloride 20.0 19.87 ug/L 99 57-137
Xylenes, Total 40.0 36.95 ug/L 92 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
LCS LCS
Qualifier Limits%Recovery
93Dibromofluoromethane (Surr)70 -130
861,2-Dichloroethane-d4 (Surr)70 -130
112Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392810/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
Acetone 100 98.16 ug/L 98 39-150 9 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 20.0 19.20 ug/L 96 70-130 3 12
Bromobenzene 20.0 20.34 ug/L 102 70-130 1 16
Bromochloromethane 20.0 19.57 ug/L 98 70-130 1 16
Bromodichloromethane 20.0 19.88 ug/L 99 70-130 3 14
Bromoform 20.0 18.20 ug/L 91 70-137 3 14
Bromomethane 20.0 12.84 ug/L 64 53-150 6 19
2-Butanone (MEK)100 104.0 ug/L 104 55-143 7 19
Carbon disulfide 20.0 15.44 ug/L 77 64-135 1 16
Carbon tetrachloride 20.0 20.24 ug/L 101 70-147 5 16
Chlorobenzene 20.0 19.82 ug/L 99 70-130 1 12
Chlorodibromomethane 20.0 20.08 ug/L 100 70-133 2 13
Chloroethane 20.0 20.67 ug/L 103 60-138 4 15
Chloroform 20.0 19.79 ug/L 99 70-130 3 14
Chloromethane 20.0 17.71 ug/L 89 33-150 3 20
2-Chlorotoluene 20.0 18.81 ug/L 94 70-130 2 15
4-Chlorotoluene 20.0 19.32 ug/L 97 70-130 4 15
cis-1,2-Dichloroethene 20.0 19.10 ug/L 96 70-130 5 15
cis-1,3-Dichloropropene 20.0 21.13 ug/L 106 70-133 2 15
1,2-Dibromo-3-Chloropropane 20.0 20.86 ug/L 104 45-138 1 19
1,2-Dibromoethane (EDB)20.0 20.24 ug/L 101 70-130 1 13
Dibromomethane 20.0 20.42 ug/L 102 70-130 4 14
1,2-Dichlorobenzene 20.0 20.07 ug/L 100 70-130 1 12
1,3-Dichlorobenzene 20.0 19.44 ug/L 97 70-130 2 13
1,4-Dichlorobenzene 20.0 19.44 ug/L 97 70-130 0 12
Dichlorodifluoromethane 20.0 24.97 ug/L 125 48-150 2 16
1,1-Dichloroethane 20.0 19.78 ug/L 99 70-130 4 17
1,2-Dichloroethane 20.0 22.72 ug/L 114 70-130 4 13
1,1-Dichloroethene 20.0 17.96 ug/L 90 70-132 1 20
1,2-Dichloroethene, Total 40.0 38.31 ug/L 96 70-130 5 14
1,2-Dichloropropane 20.0 18.82 ug/L 94 70-130 1 15
1,3-Dichloropropane 20.0 19.88 ug/L 99 70-130 1 12
2,2-Dichloropropane 20.0 22.95 ug/L 115 60-143 2 20
1,1-Dichloropropene 20.0 19.10 ug/L 96 70-130 5 16
Diisopropyl ether 20.0 19.83 ug/L 99 66-142 1 14
Ethylbenzene 20.0 19.09 ug/L 95 70-130 2 12
Hexachlorobutadiene 20.0 17.84 ug/L 89 70-138 2 16
2-Hexanone 100 100.8 ug/L 101 54-142 2 17
Isopropylbenzene 20.0 19.10 ug/L 95 70-131 2 13
Methylene Chloride 20.0 20.36 ug/L 102 70-130 3 15
4-Methyl-2-pentanone (MIBK)100 96.14 ug/L 96 60-137 0 21
Methyl tert-butyl ether 20.0 21.12 ug/L 106 70-130 2 16
Naphthalene 20.0 23.29 ug/L 116 54-150 2 15
n-Butylbenzene 20.0 17.31 ug/L 87 68-137 3 14
N-Propylbenzene 20.0 18.19 ug/L 91 70-134 3 14
p-Isopropyltoluene 20.0 18.07 ug/L 90 66-130 4 13
sec-Butylbenzene 20.0 17.63 ug/L 88 70-135 5 14
Styrene 20.0 19.94 ug/L 100 70-130 1 12
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392810/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
tert-Butylbenzene 20.0 18.19 ug/L 91 70-130 5 14
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,1,2-Tetrachloroethane 20.0 19.47 ug/L 97 70-130 2 13
1,1,2,2-Tetrachloroethane 20.0 21.37 ug/L 107 69-131 0 15
Tetrachloroethene 20.0 19.32 ug/L 97 70-130 6 17
Toluene 20.0 18.95 ug/L 95 70-130 3 13
trans-1,2-Dichloroethene 20.0 19.21 ug/L 96 70-130 6 15
trans-1,3-Dichloropropene 20.0 21.29 ug/L 106 63-142 1 13
1,2,3-Trichlorobenzene 20.0 21.57 ug/L 108 46-150 1 16
1,2,4-Trichlorobenzene 20.0 20.91 ug/L 105 58-147 0 15
1,1,1-Trichloroethane 20.0 20.10 ug/L 101 70-135 5 15
1,1,2-Trichloroethane 20.0 19.28 ug/L 96 70-130 2 13
Trichloroethene 20.0 18.54 ug/L 93 70-130 5 14
Trichlorofluoromethane 20.0 18.44 ug/L 92 59-150 1 22
1,2,3-Trichloropropane 20.0 19.01 ug/L 95 70-131 2 14
1,2,4-Trimethylbenzene 20.0 18.45 ug/L 92 70-130 3 13
1,3,5-Trimethylbenzene 20.0 18.11 ug/L 91 70-130 2 14
Vinyl chloride 20.0 21.10 ug/L 105 57-137 6 15
Xylenes, Total 40.0 37.90 ug/L 95 70-132 3 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
LCSD LCSD
Qualifier Limits%Recovery
94Dibromofluoromethane (Surr)70 -130
881,2-Dichloroethane-d4 (Surr)70 -130
110Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-117167-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
Acetone <13.3 1250 1183 ug/L 95 39-150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzene <1.00 250 242.4 ug/L 97 55-147
Bromobenzene <1.05 250 259.9 ug/L 104 60-133
Bromochloromethane <0.750 250 249.3 ug/L 100 59-132
Bromodichloromethane <0.850 250 256.9 ug/L 103 70-140
Bromoform <1.45 250 238.8 ug/L 96 53-150
Bromomethane <1.75 250 172.2 ug/L 69 30-150
2-Butanone (MEK)<13.2 1250 1202 ug/L 96 50-143
Carbon disulfide <1.10 250 192.6 ug/L 77 35-150
Carbon tetrachloride <0.900 250 261.5 ug/L 105 56-150
Chlorobenzene <0.900 250 255.0 ug/L 102 70-130
Chlorodibromomethane <1.25 250 265.8 ug/L 106 66-140
Chloroethane <1.80 250 266.1 ug/L 106 58-141
Chloroform <1.15 250 255.9 ug/L 102 66-138
Chloromethane <1.80 250 232.9 ug/L 93 10-150
2-Chlorotoluene <0.900 250 246.3 ug/L 99 67-138
4-Chlorotoluene <0.850 250 250.3 ug/L 100 69-138
cis-1,2-Dichloroethene <1.05 250 249.3 ug/L 100 68-131
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-117167-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
cis-1,3-Dichloropropene <0.850 250 265.7 ug/L 106 70-133
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane <4.70 250 278.0 ug/L 111 38-138
1,2-Dibromoethane (EDB)<1.05 250 258.8 ug/L 104 65-137
Dibromomethane <2.25 250 251.5 ug/L 101 70-130
1,2-Dichlorobenzene <0.950 250 259.0 ug/L 104 70-130
1,3-Dichlorobenzene <0.900 250 251.5 ug/L 101 68-131
1,4-Dichlorobenzene <0.850 250 251.1 ug/L 100 70-130
Dichlorodifluoromethane <0.850 250 338.5 ug/L 135 10-150
1,1-Dichloroethane <1.20 250 244.0 ug/L 98 61-139
1,2-Dichloroethane <1.00 250 285.4 ug/L 114 64-136
1,1-Dichloroethene <1.25 250 245.4 ug/L 98 54-150
1,2-Dichloroethene, Total <1.05 500 482.5 ug/L 97 60-134
1,2-Dichloropropane <1.25 250 236.7 ug/L 95 67-130
1,3-Dichloropropane <0.950 250 245.4 ug/L 98 70-130
2,2-Dichloropropane <0.800 250 287.4 ug/L 115 50-146
1,1-Dichloropropene <1.00 250 240.4 ug/L 96 54-150
Diisopropyl ether 1.31 J 250 245.6 ug/L 98 56-142
Ethylbenzene <0.950 250 242.3 ug/L 97 65-139
Hexachlorobutadiene <1.90 250 211.1 ug/L 84 61-141
2-Hexanone <6.40 1250 1166 ug/L 93 44-150
Isopropylbenzene <1.65 250 245.0 ug/L 98 70-137
Methylene Chloride <5.00 250 257.8 ug/L 103 64-130
4-Methyl-2-pentanone (MIBK)<4.05 1250 1157 ug/L 93 50-140
Methyl tert-butyl ether 358 250 608.3 ug/L 100 55-141
Naphthalene <1.05 250 276.9 ug/L 111 32-150
n-Butylbenzene <1.20 250 223.3 ug/L 89 61-141
N-Propylbenzene <0.850 250 236.4 ug/L 95 53-150
p-Isopropyltoluene <0.850 250 229.5 ug/L 92 66-137
sec-Butylbenzene <0.850 250 225.5 ug/L 90 55-136
Styrene <1.40 250 257.5 ug/L 103 70-130
tert-Butylbenzene <0.850 250 235.4 ug/L 94 70-138
1,1,1,2-Tetrachloroethane <0.750 250 255.3 ug/L 102 70-131
1,1,2,2-Tetrachloroethane <0.950 250 270.6 ug/L 108 56-145
Tetrachloroethene <0.700 250 238.9 ug/L 96 57-138
Toluene <0.850 250 240.1 ug/L 96 64-136
trans-1,2-Dichloroethene <1.15 250 233.2 ug/L 93 59-143
trans-1,3-Dichloropropene <0.850 250 266.5 ug/L 107 63-142
1,2,3-Trichlorobenzene <1.15 250 255.8 ug/L 102 36-150
1,2,4-Trichlorobenzene <1.00 250 260.7 ug/L 104 47-147
1,1,1-Trichloroethane <0.950 250 260.1 ug/L 104 68-144
1,1,2-Trichloroethane <0.950 250 239.2 ug/L 96 70-130
Trichloroethene <1.00 250 237.5 ug/L 95 63-135
Trichlorofluoromethane <1.05 250 228.5 ug/L 91 44-150
1,2,3-Trichloropropane <1.15 250 246.4 ug/L 99 65-131
1,2,4-Trimethylbenzene <0.850 250 239.9 ug/L 96 64-136
1,3,5-Trimethylbenzene <0.850 250 238.1 ug/L 95 69-139
Vinyl chloride <0.900 250 266.6 ug/L 107 57-150
Xylenes, Total <2.90 500 483.1 ug/L 97 69-132
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-117167-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
4-Bromofluorobenzene (Surr)70 -130
Surrogate
87
MS MS
Qualifier Limits%Recovery
93Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
110Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117167-B-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
Acetone <13.3 1250 984.6 ug/L 79 39-150 18 28
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Benzene <1.00 250 234.9 ug/L 94 55-147 3 22
Bromobenzene <1.05 250 251.0 ug/L 100 60-133 3 18
Bromochloromethane <0.750 250 241.7 ug/L 97 59-132 3 21
Bromodichloromethane <0.850 250 246.8 ug/L 99 70-140 4 196
Bromoform <1.45 250 224.0 ug/L 90 53-150 6 20
Bromomethane <1.75 250 204.6 ug/L 82 30-150 17 44
2-Butanone (MEK)<13.2 1250 1112 ug/L 89 50-143 8 28
Carbon disulfide <1.10 250 197.0 ug/L 79 35-150 2 34
Carbon tetrachloride <0.900 250 254.1 ug/L 102 56-150 3 18
Chlorobenzene <0.900 250 246.7 ug/L 99 70-130 3 15
Chlorodibromomethane <1.25 250 257.8 ug/L 103 66-140 3 19
Chloroethane <1.80 250 263.1 ug/L 105 58-141 1 31
Chloroform <1.15 250 246.1 ug/L 98 66-138 4 21
Chloromethane <1.80 250 225.4 ug/L 90 10-150 3 43
2-Chlorotoluene <0.900 250 240.4 ug/L 96 67-138 2 17
4-Chlorotoluene <0.850 250 243.4 ug/L 97 69-138 3 15
cis-1,2-Dichloroethene <1.05 250 242.5 ug/L 97 68-131 3 21
cis-1,3-Dichloropropene <0.850 250 256.0 ug/L 102 70-133 4 19
1,2-Dibromo-3-Chloropropane <4.70 250 261.5 ug/L 105 38-138 6 26
1,2-Dibromoethane (EDB)<1.05 250 244.8 ug/L 98 65-137 6 21
Dibromomethane <2.25 250 238.2 ug/L 95 70-130 5 19
1,2-Dichlorobenzene <0.950 250 244.7 ug/L 98 70-130 6 15
1,3-Dichlorobenzene <0.900 250 242.2 ug/L 97 68-131 4 14
1,4-Dichlorobenzene <0.850 250 238.9 ug/L 96 70-130 5 14
Dichlorodifluoromethane <0.850 250 335.0 ug/L 134 10-150 1 50
1,1-Dichloroethane <1.20 250 237.6 ug/L 95 61-139 3 23
1,2-Dichloroethane <1.00 250 273.7 ug/L 109 64-136 4 22
1,1-Dichloroethene <1.25 250 244.4 ug/L 98 54-150 0 24
1,2-Dichloroethene, Total <1.05 500 476.3 ug/L 95 60-134 1 22
1,2-Dichloropropane <1.25 250 228.1 ug/L 91 67-130 4 19
1,3-Dichloropropane <0.950 250 231.4 ug/L 93 70-130 6 17
2,2-Dichloropropane <0.800 250 279.7 ug/L 112 50-146 3 20
1,1-Dichloropropene <1.00 250 234.0 ug/L 94 54-150 3 24
Diisopropyl ether 1.31 J 250 240.5 ug/L 96 56-142 2 22
Ethylbenzene <0.950 250 236.8 ug/L 95 65-139 2 18
Hexachlorobutadiene <1.90 250 225.0 ug/L 90 61-141 6 26
2-Hexanone <6.40 1250 1066 ug/L 85 44-150 9 21
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117167-B-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392810
Isopropylbenzene <1.65 250 238.8 ug/L 96 70-137 3 17
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Methylene Chloride <5.00 250 254.3 ug/L 102 64-130 1 22
4-Methyl-2-pentanone (MIBK)<4.05 1250 1073 ug/L 86 50-140 8 24
Methyl tert-butyl ether 358 250 580.6 ug/L 89 55-141 5 24
Naphthalene <1.05 250 274.0 ug/L 110 32-150 1 40
n-Butylbenzene <1.20 250 219.1 ug/L 88 61-141 2 17
N-Propylbenzene <0.850 250 230.8 ug/L 92 53-150 2 18
p-Isopropyltoluene <0.850 250 227.2 ug/L 91 66-137 1 16
sec-Butylbenzene <0.850 250 222.3 ug/L 89 55-136 1 50
Styrene <1.40 250 245.7 ug/L 98 70-130 5 16
tert-Butylbenzene <0.850 250 231.2 ug/L 92 70-138 2 17
1,1,1,2-Tetrachloroethane <0.750 250 246.6 ug/L 99 70-131 3 16
1,1,2,2-Tetrachloroethane <0.950 250 255.3 ug/L 102 56-145 6 19
Tetrachloroethene <0.700 250 234.9 ug/L 94 57-138 2 17
Toluene <0.850 250 234.3 ug/L 94 64-136 2 18
trans-1,2-Dichloroethene <1.15 250 233.8 ug/L 94 59-143 0 25
trans-1,3-Dichloropropene <0.850 250 259.3 ug/L 104 63-142 3 18
1,2,3-Trichlorobenzene <1.15 250 258.4 ug/L 103 36-150 1 43
1,2,4-Trichlorobenzene <1.00 250 255.1 ug/L 102 47-147 2 24
1,1,1-Trichloroethane <0.950 250 253.8 ug/L 102 68-144 2 17
1,1,2-Trichloroethane <0.950 250 224.8 ug/L 90 70-130 6 18
Trichloroethene <1.00 250 229.3 ug/L 92 63-135 4 17
Trichlorofluoromethane <1.05 250 238.3 ug/L 95 44-150 4 32
1,2,3-Trichloropropane <1.15 250 237.3 ug/L 95 65-131 4 19
1,2,4-Trimethylbenzene <0.850 250 234.4 ug/L 94 64-136 2 18
1,3,5-Trimethylbenzene <0.850 250 234.3 ug/L 94 69-139 2 17
Vinyl chloride <0.900 250 270.4 ug/L 108 57-150 1 37
Xylenes, Total <2.90 500 465.5 ug/L 93 69-132 4 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
MSD MSD
Qualifier Limits%Recovery
93Dibromofluoromethane (Surr)70 -130
921,2-Dichloroethane-d4 (Surr)70 -130
110Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-392895/10
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392895
RL MDL
Acetone <0.00840 0.0500 0.00840 mg/Kg 12/09/16 02:33 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1Benzene
<0.000720 0.0007200.00200 mg/Kg 12/09/16 02:33 1Bromobenzene
<0.000550 0.0005500.00200 mg/Kg 12/09/16 02:33 1Bromochloromethane
<0.000550 0.0005500.00200 mg/Kg 12/09/16 02:33 1Bromodichloromethane
<0.000550 0.0005500.00200 mg/Kg 12/09/16 02:33 1Bromoform
<0.00120 0.001200.00200 mg/Kg 12/09/16 02:33 1Bromomethane
<0.00510 0.005100.0500 mg/Kg 12/09/16 02:33 12-Butanone (MEK)
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392895/10
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392895
RL MDL
Carbon disulfide <0.00360 0.00500 0.00360 mg/Kg 12/09/16 02:33 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1Carbon tetrachloride
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1Chlorobenzene
<0.000340 0.0003400.00200 mg/Kg 12/09/16 02:33 1Chlorodibromomethane
<0.00190 0.001900.00500 mg/Kg 12/09/16 02:33 1Chloroethane
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1Chloroform
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1Chloromethane
<0.000890 0.0008900.00200 mg/Kg 12/09/16 02:33 12-Chlorotoluene
<0.000840 0.0008400.00200 mg/Kg 12/09/16 02:33 14-Chlorotoluene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1cis-1,2-Dichloroethene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1cis-1,3-Dichloropropene
<0.000700 0.0007000.00500 mg/Kg 12/09/16 02:33 11,2-Dibromo-3-Chloropropane
<0.00100 0.001000.00200 mg/Kg 12/09/16 02:33 11,2-Dibromoethane (EDB)
<0.000560 0.0005600.00200 mg/Kg 12/09/16 02:33 1Dibromomethane
<0.000340 0.0003400.00200 mg/Kg 12/09/16 02:33 11,2-Dichlorobenzene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 11,3-Dichlorobenzene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 11,4-Dichlorobenzene
<0.00100 0.001000.00200 mg/Kg 12/09/16 02:33 1Dichlorodifluoromethane
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 11,1-Dichloroethane
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 11,2-Dichloroethane
<0.000570 0.0005700.00200 mg/Kg 12/09/16 02:33 11,1-Dichloroethene
<0.000470 0.0004700.00200 mg/Kg 12/09/16 02:33 11,2-Dichloroethene, Total
<0.000940 0.0009400.00200 mg/Kg 12/09/16 02:33 11,2-Dichloropropane
<0.000940 0.0009400.00200 mg/Kg 12/09/16 02:33 11,3-Dichloropropane
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 12,2-Dichloropropane
<0.000510 0.0005100.00200 mg/Kg 12/09/16 02:33 11,1-Dichloropropene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1Diisopropyl ether
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1Ethylbenzene
<0.00114 0.001140.00500 mg/Kg 12/09/16 02:33 1Hexachlorobutadiene
<0.0167 0.01670.0500 mg/Kg 12/09/16 02:33 12-Hexanone
<0.000410 0.0004100.00200 mg/Kg 12/09/16 02:33 1Isopropylbenzene
<0.000860 0.0008600.0100 mg/Kg 12/09/16 02:33 1Methylene Chloride
<0.00190 0.001900.0500 mg/Kg 12/09/16 02:33 14-Methyl-2-pentanone (MIBK)
<0.000960 0.0009600.00200 mg/Kg 12/09/16 02:33 1Methyl tert-butyl ether
<0.00170 0.001700.00500 mg/Kg 12/09/16 02:33 1Naphthalene
<0.000980 0.0009800.00200 mg/Kg 12/09/16 02:33 1n-Butylbenzene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1N-Propylbenzene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1p-Isopropyltoluene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1sec-Butylbenzene
<0.00110 0.001100.00200 mg/Kg 12/09/16 02:33 1Styrene
<0.000900 0.0009000.00200 mg/Kg 12/09/16 02:33 1tert-Butylbenzene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 11,1,1,2-Tetrachloroethane
<0.00100 0.001000.00200 mg/Kg 12/09/16 02:33 11,1,2,2-Tetrachloroethane
<0.000730 0.0007300.00200 mg/Kg 12/09/16 02:33 1Tetrachloroethene
<0.000740 0.0007400.00200 mg/Kg 12/09/16 02:33 1Toluene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1trans-1,2-Dichloroethene
<0.000670 0.0006700.00200 mg/Kg 12/09/16 02:33 1trans-1,3-Dichloropropene
<0.000380 0.0003800.00200 mg/Kg 12/09/16 02:33 11,2,3-Trichlorobenzene
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392895/10
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392895
RL MDL
1,2,4-Trichlorobenzene <0.000670 0.00200 0.000670 mg/Kg 12/09/16 02:33 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000920 0.0009200.00200 mg/Kg 12/09/16 02:33 11,1,1-Trichloroethane
<0.00140 0.001400.00500 mg/Kg 12/09/16 02:33 11,1,2-Trichloroethane
<0.000960 0.0009600.00200 mg/Kg 12/09/16 02:33 1Trichloroethene
<0.00100 0.001000.00200 mg/Kg 12/09/16 02:33 1Trichlorofluoromethane
<0.000550 0.0005500.00200 mg/Kg 12/09/16 02:33 11,2,3-Trichloropropane
<0.00100 0.001000.00200 mg/Kg 12/09/16 02:33 11,2,4-Trimethylbenzene
<0.000750 0.0007500.00200 mg/Kg 12/09/16 02:33 11,3,5-Trimethylbenzene
<0.00110 0.001100.00200 mg/Kg 12/09/16 02:33 1Vinyl chloride
<0.00123 0.001230.00600 mg/Kg 12/09/16 02:33 1Xylenes, Total
4-Bromofluorobenzene (Surr)88 70-130 12/09/16 02:33 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
126 12/09/16 02:33 1Dibromofluoromethane (Surr)70-130
117 12/09/16 02:33 11,2-Dichloroethane-d4 (Surr)70-130
86 12/09/16 02:33 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392895/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392895
Acetone 0.250 0.2825 mg/Kg 113 45-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.05765 mg/Kg 115 70-130
Bromobenzene 0.0500 0.04311 mg/Kg 86 67-130
Bromochloromethane 0.0500 0.05944 mg/Kg 119 70-133
Bromodichloromethane 0.0500 0.05056 mg/Kg 101 70-130
Bromoform 0.0500 0.04452 mg/Kg 89 59-137
Bromomethane 0.0500 0.06824 mg/Kg 136 32-150
2-Butanone (MEK)0.250 0.2816 mg/Kg 113 50-149
Carbon disulfide 0.0500 0.05695 mg/Kg 114 66-138
Carbon tetrachloride 0.0500 0.05700 mg/Kg 114 70-131
Chlorobenzene 0.0500 0.05220 mg/Kg 104 70-130
Chlorodibromomethane 0.0500 0.04694 mg/Kg 94 70-130
Chloroethane 0.0500 0.05668 mg/Kg 113 37-150
Chloroform 0.0500 0.05933 mg/Kg 119 70-130
Chloromethane 0.0500 0.04711 mg/Kg 94 53-150
2-Chlorotoluene 0.0500 0.04792 mg/Kg 96 70-132
4-Chlorotoluene 0.0500 0.05007 mg/Kg 100 67-135
cis-1,2-Dichloroethene 0.0500 0.05544 mg/Kg 111 70-132
cis-1,3-Dichloropropene 0.0500 0.04613 mg/Kg 92 70-130
1,2-Dibromo-3-Chloropropane 0.0500 0.04686 mg/Kg 94 47-144
1,2-Dibromoethane (EDB)0.0500 0.05190 mg/Kg 104 69-130
Dibromomethane 0.0500 0.05497 mg/Kg 110 70-130
1,2-Dichlorobenzene 0.0500 0.05131 mg/Kg 103 70-134
1,3-Dichlorobenzene 0.0500 0.05078 mg/Kg 102 69-137
1,4-Dichlorobenzene 0.0500 0.04945 mg/Kg 99 66-134
Dichlorodifluoromethane 0.0500 0.07159 mg/Kg 143 32-150
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392895/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392895
1,1-Dichloroethane 0.0500 0.05473 mg/Kg 109 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane 0.0500 0.05408 mg/Kg 108 65-134
1,1-Dichloroethene 0.0500 0.05887 mg/Kg 118 70-131
1,2-Dichloroethene, Total 0.100 0.1109 mg/Kg 111 70-130
1,2-Dichloropropane 0.0500 0.05111 mg/Kg 102 70-130
1,3-Dichloropropane 0.0500 0.04971 mg/Kg 99 70-130
2,2-Dichloropropane 0.0500 0.05357 mg/Kg 107 57-150
1,1-Dichloropropene 0.0500 0.05555 mg/Kg 111 70-130
Diisopropyl ether 0.0500 0.05029 mg/Kg 101 68-134
Ethylbenzene 0.0500 0.05481 mg/Kg 110 70-130
Hexachlorobutadiene 0.0500 0.06326 mg/Kg 127 64-137
2-Hexanone 0.250 0.2628 mg/Kg 105 47-148
Isopropylbenzene 0.0500 0.05678 mg/Kg 114 70-130
Methylene Chloride 0.0500 0.05800 mg/Kg 116 69-130
4-Methyl-2-pentanone (MIBK)0.250 0.2602 mg/Kg 104 48-150
Methyl tert-butyl ether 0.0500 0.05810 mg/Kg 116 54-145
Naphthalene 0.0500 0.05064 mg/Kg 101 55-149
n-Butylbenzene 0.0500 0.05271 mg/Kg 105 57-150
N-Propylbenzene 0.0500 0.05102 mg/Kg 102 62-150
p-Isopropyltoluene 0.0500 0.05531 mg/Kg 111 66-147
sec-Butylbenzene 0.0500 0.05464 mg/Kg 109 68-147
Styrene 0.0500 0.05216 mg/Kg 104 70-131
tert-Butylbenzene 0.0500 0.05335 mg/Kg 107 70-138
1,1,1,2-Tetrachloroethane 0.0500 0.05012 mg/Kg 100 70-130
1,1,2,2-Tetrachloroethane 0.0500 0.04647 mg/Kg 93 61-134
Tetrachloroethene 0.0500 0.05626 mg/Kg 113 70-130
Toluene 0.0500 0.05557 mg/Kg 111 70-130
trans-1,2-Dichloroethene 0.0500 0.05542 mg/Kg 111 70-130
trans-1,3-Dichloropropene 0.0500 0.04431 mg/Kg 89 67-130
1,2,3-Trichlorobenzene 0.0500 0.04944 mg/Kg 99 57-146
1,2,4-Trichlorobenzene 0.0500 0.04817 mg/Kg 96 47-150
1,1,1-Trichloroethane 0.0500 0.05905 mg/Kg 118 70-130
1,1,2-Trichloroethane 0.0500 0.05359 mg/Kg 107 70-130
Trichloroethene 0.0500 0.05655 mg/Kg 113 70-130
Trichlorofluoromethane 0.0500 0.06132 mg/Kg 123 53-150
1,2,3-Trichloropropane 0.0500 0.04883 mg/Kg 98 60-139
1,2,4-Trimethylbenzene 0.0500 0.05190 mg/Kg 104 70-140
1,3,5-Trimethylbenzene 0.0500 0.06093 mg/Kg 122 69-141
Vinyl chloride 0.0500 0.05505 mg/Kg 110 63-150
Xylenes, Total 0.100 0.1079 mg/Kg 108 70-130
4-Bromofluorobenzene (Surr)70 -130
Surrogate
87
LCS LCS
Qualifier Limits%Recovery
96Dibromofluoromethane (Surr)70 -130
951,2-Dichloroethane-d4 (Surr)70 -130
93Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392895/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392895
Acetone 0.250 0.2570 mg/Kg 103 45-145 9 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.05653 mg/Kg 113 70-130 2 37
Bromobenzene 0.0500 0.04051 mg/Kg 81 67-130 6 40
Bromochloromethane 0.0500 0.05721 mg/Kg 114 70-133 4 15
Bromodichloromethane 0.0500 0.04850 mg/Kg 97 70-130 4 20
Bromoform 0.0500 0.04132 mg/Kg 83 59-137 7 17
Bromomethane 0.0500 0.06272 mg/Kg 125 32-150 8 45
2-Butanone (MEK)0.250 0.2613 mg/Kg 105 50-149 7 39
Carbon disulfide 0.0500 0.05399 mg/Kg 108 66-138 5 41
Carbon tetrachloride 0.0500 0.05388 mg/Kg 108 70-131 6 41
Chlorobenzene 0.0500 0.04853 mg/Kg 97 70-130 7 40
Chlorodibromomethane 0.0500 0.04342 mg/Kg 87 70-130 8 14
Chloroethane 0.0500 0.05292 mg/Kg 106 37-150 7 50
Chloroform 0.0500 0.05608 mg/Kg 112 70-130 6 15
Chloromethane 0.0500 0.04470 mg/Kg 89 53-150 5 47
2-Chlorotoluene 0.0500 0.04504 mg/Kg 90 70-132 6 41
4-Chlorotoluene 0.0500 0.04562 mg/Kg 91 67-135 9 41
cis-1,2-Dichloroethene 0.0500 0.05755 mg/Kg 115 70-132 4 18
cis-1,3-Dichloropropene 0.0500 0.04261 mg/Kg 85 70-130 8 42
1,2-Dibromo-3-Chloropropane 0.0500 0.04207 mg/Kg 84 47-144 11 38
1,2-Dibromoethane (EDB)0.0500 0.04882 mg/Kg 98 69-130 6 17
Dibromomethane 0.0500 0.05261 mg/Kg 105 70-130 4 19
1,2-Dichlorobenzene 0.0500 0.04879 mg/Kg 98 70-134 5 40
1,3-Dichlorobenzene 0.0500 0.04747 mg/Kg 95 69-137 7 41
1,4-Dichlorobenzene 0.0500 0.04660 mg/Kg 93 66-134 6 41
Dichlorodifluoromethane 0.0500 0.06505 mg/Kg 130 32-150 10 50
1,1-Dichloroethane 0.0500 0.05102 mg/Kg 102 70-130 7 42
1,2-Dichloroethane 0.0500 0.05113 mg/Kg 102 65-134 6 16
1,1-Dichloroethene 0.0500 0.05537 mg/Kg 111 70-131 6 43
1,2-Dichloroethene, Total 0.100 0.1101 mg/Kg 110 70-130 1 41
1,2-Dichloropropane 0.0500 0.04877 mg/Kg 98 70-130 5 15
1,3-Dichloropropane 0.0500 0.04614 mg/Kg 92 70-130 7 15
2,2-Dichloropropane 0.0500 0.04961 mg/Kg 99 57-150 8 42
1,1-Dichloropropene 0.0500 0.05206 mg/Kg 104 70-130 6 41
Diisopropyl ether 0.0500 0.04638 mg/Kg 93 68-134 8 36
Ethylbenzene 0.0500 0.05106 mg/Kg 102 70-130 7 38
Hexachlorobutadiene 0.0500 0.05983 mg/Kg 120 64-137 6 44
2-Hexanone 0.250 0.2470 mg/Kg 99 47-148 6 38
Isopropylbenzene 0.0500 0.05213 mg/Kg 104 70-130 9 39
Methylene Chloride 0.0500 0.05407 mg/Kg 108 69-130 7 19
4-Methyl-2-pentanone (MIBK)0.250 0.2427 mg/Kg 97 48-150 7 41
Methyl tert-butyl ether 0.0500 0.05376 mg/Kg 108 54-145 8 36
Naphthalene 0.0500 0.04840 mg/Kg 97 55-149 5 37
n-Butylbenzene 0.0500 0.04992 mg/Kg 100 57-150 5 39
N-Propylbenzene 0.0500 0.04734 mg/Kg 95 62-150 7 38
p-Isopropyltoluene 0.0500 0.05207 mg/Kg 104 66-147 6 38
sec-Butylbenzene 0.0500 0.05145 mg/Kg 103 68-147 6 38
Styrene 0.0500 0.04946 mg/Kg 99 70-131 5 40
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392895/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 392895
tert-Butylbenzene 0.0500 0.04877 mg/Kg 98 70-138 9 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,1,2-Tetrachloroethane 0.0500 0.04599 mg/Kg 92 70-130 9 41
1,1,2,2-Tetrachloroethane 0.0500 0.04219 mg/Kg 84 61-134 10 16
Tetrachloroethene 0.0500 0.05179 mg/Kg 104 70-130 8 41
Toluene 0.0500 0.05114 mg/Kg 102 70-130 8 40
trans-1,2-Dichloroethene 0.0500 0.05253 mg/Kg 105 70-130 5 41
trans-1,3-Dichloropropene 0.0500 0.04060 mg/Kg 81 67-130 9 41
1,2,3-Trichlorobenzene 0.0500 0.04719 mg/Kg 94 57-146 5 42
1,2,4-Trichlorobenzene 0.0500 0.04586 mg/Kg 92 47-150 5 43
1,1,1-Trichloroethane 0.0500 0.05599 mg/Kg 112 70-130 5 41
1,1,2-Trichloroethane 0.0500 0.04969 mg/Kg 99 70-130 8 17
Trichloroethene 0.0500 0.05401 mg/Kg 108 70-130 5 41
Trichlorofluoromethane 0.0500 0.05731 mg/Kg 115 53-150 7 49
1,2,3-Trichloropropane 0.0500 0.04644 mg/Kg 93 60-139 5 16
1,2,4-Trimethylbenzene 0.0500 0.04886 mg/Kg 98 70-140 6 38
1,3,5-Trimethylbenzene 0.0500 0.05719 mg/Kg 114 69-141 6 38
Vinyl chloride 0.0500 0.05066 mg/Kg 101 63-150 8 46
Xylenes, Total 0.100 0.1003 mg/Kg 100 70-130 7 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
85
LCSD LCSD
Qualifier Limits%Recovery
98Dibromofluoromethane (Surr)70 -130
941,2-Dichloroethane-d4 (Surr)70 -130
93Toluene-d8 (Surr)70 -130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-392749/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392931 Prep Batch: 392749
RL MDL
Acenaphthene <0.320 2.00 0.320 ug/L 12/08/16 10:43 12/08/16 18:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.350 0.3502.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Acenaphthylene
<0.380 0.3802.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Anthracene
<0.320 0.3202.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Benzo[a]anthracene
<0.380 0.3802.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Benzo[a]pyrene
<0.360 0.3602.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Benzo[b]fluoranthene
<0.620 0.6202.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Benzo[g,h,i]perylene
<0.370 0.3702.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Benzo[k]fluoranthene
<1.90 1.9010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Bis(2-chloroethoxy)methane
<1.30 1.3010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Bis(2-chloroethyl)ether
<1.80 1.8010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1bis (2-chloroisopropyl) ether
<1.50 1.5010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Bis(2-ethylhexyl) phthalate
<1.60 1.6010.0 ug/L 12/08/16 10:43 12/08/16 18:18 14-Bromophenyl phenyl ether
<1.00 1.0010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Butyl benzyl phthalate
<0.900 0.90010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Carbazole
<1.20 1.2010.0 ug/L 12/08/16 10:43 12/08/16 18:18 14-Chloroaniline
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392749/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392931 Prep Batch: 392749
RL MDL
4-Chloro-3-methylphenol <1.40 10.0 1.40 ug/L 12/08/16 10:43 12/08/16 18:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.50 1.5010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12-Chloronaphthalene
<1.70 1.7010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12-Chlorophenol
<1.60 1.6010.0 ug/L 12/08/16 10:43 12/08/16 18:18 14-Chlorophenyl phenyl ether
<0.330 0.3302.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Chrysene
<3.00 3.0010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Cresols
<0.450 0.4502.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Dibenz(a,h)anthracene
<1.30 1.3010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Dibenzofuran
<2.20 2.2010.0 ug/L 12/08/16 10:43 12/08/16 18:18 11,2-Dichlorobenzene
<2.00 2.0010.0 ug/L 12/08/16 10:43 12/08/16 18:18 11,3-Dichlorobenzene
<2.00 2.0010.0 ug/L 12/08/16 10:43 12/08/16 18:18 11,4-Dichlorobenzene
<1.50 1.5010.0 ug/L 12/08/16 10:43 12/08/16 18:18 13,3'-Dichlorobenzidine
<2.20 2.2010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12,4-Dichlorophenol
<1.20 1.2010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Diethyl phthalate
<1.60 1.6010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12,4-Dimethylphenol
<1.20 1.2010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Dimethyl phthalate
<1.30 1.3010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Di-n-butyl phthalate
<2.90 2.9025.0 ug/L 12/08/16 10:43 12/08/16 18:18 14,6-Dinitro-2-methylphenol
<7.20 7.2025.0 ug/L 12/08/16 10:43 12/08/16 18:18 12,4-Dinitrophenol
<1.60 1.6010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12,4-Dinitrotoluene
<1.50 1.5010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12,6-Dinitrotoluene
<0.900 0.90010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Di-n-octyl phthalate
<0.320 0.3202.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Fluoranthene
<0.320 0.3202.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Fluorene
<1.50 1.5010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Hexachlorobenzene
<1.50 1.5010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Hexachlorobutadiene
<1.30 1.3010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Hexachlorocyclopentadiene
<2.20 2.2010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Hexachloroethane
<0.410 0.4102.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Indeno[1,2,3-cd]pyrene
<2.20 2.2010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Isophorone
<0.360 0.3602.00 ug/L 12/08/16 10:43 12/08/16 18:18 11-Methylnaphthalene
<0.400 0.4002.00 ug/L 12/08/16 10:43 12/08/16 18:18 12-Methylnaphthalene
<1.60 1.6010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12-Methylphenol
<1.40 1.4010.0 ug/L 12/08/16 10:43 12/08/16 18:18 13 & 4 Methylphenol
<0.370 0.3702.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Naphthalene
<1.10 1.1025.0 ug/L 12/08/16 10:43 12/08/16 18:18 12-Nitroaniline
<1.60 1.6025.0 ug/L 12/08/16 10:43 12/08/16 18:18 13-Nitroaniline
<1.60 1.6025.0 ug/L 12/08/16 10:43 12/08/16 18:18 14-Nitroaniline
<2.20 2.2010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Nitrobenzene
<2.40 2.4010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12-Nitrophenol
<2.00 2.0025.0 ug/L 12/08/16 10:43 12/08/16 18:18 14-Nitrophenol
<1.70 1.7010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1N-Nitrosodi-n-propylamine
<3.60 3.6010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1n-Nitrosodiphenylamine(as
diphenylamine)
<3.30 3.3025.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Pentachlorophenol
<0.420 0.4202.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Phenanthrene
<1.50 1.5010.0 ug/L 12/08/16 10:43 12/08/16 18:18 1Phenol
<0.350 0.3502.00 ug/L 12/08/16 10:43 12/08/16 18:18 1Pyrene
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392749/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392931 Prep Batch: 392749
RL MDL
1,2,4-Trichlorobenzene <2.10 10.0 2.10 ug/L 12/08/16 10:43 12/08/16 18:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.30 1.3010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12,4,5-Trichlorophenol
<1.90 1.9010.0 ug/L 12/08/16 10:43 12/08/16 18:18 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)88 29-120 12/08/16 18:18 1
MB MB
Surrogate
12/08/16 10:43
Dil FacPreparedAnalyzedQualifierLimits%Recovery
53 12/08/16 10:43 12/08/16 18:18 12-Fluorophenol (Surr)10-120
92 12/08/16 10:43 12/08/16 18:18 1Nitrobenzene-d5 (Surr)27-120
34 12/08/16 10:43 12/08/16 18:18 1Phenol-d5 (Surr)10-120
92 12/08/16 10:43 12/08/16 18:18 1Terphenyl-d14 (Surr)13-120
92 12/08/16 10:43 12/08/16 18:18 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392749/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392931 Prep Batch: 392749
Acenaphthene 40.0 32.20 ug/L 80 36-129
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 40.0 32.21 ug/L 81 36-120
Anthracene 40.0 32.24 ug/L 81 42-130
Benzo[a]anthracene 40.0 32.82 ug/L 82 41-131
Benzo[a]pyrene 40.0 30.86 ug/L 77 45-131
Benzo[b]fluoranthene 40.0 33.01 ug/L 83 43-132
Benzo[g,h,i]perylene 40.0 31.42 ug/L 79 38-138
Benzo[k]fluoranthene 40.0 32.64 ug/L 82 44-129
Bis(2-chloroethoxy)methane 40.0 32.72 ug/L 82 35-127
Bis(2-chloroethyl)ether 40.0 30.37 ug/L 76 27-132
bis (2-chloroisopropyl) ether 40.0 33.37 ug/L 83 24-136
Bis(2-ethylhexyl) phthalate 40.0 34.78 ug/L 87 41-147
4-Bromophenyl phenyl ether 40.0 31.76 ug/L 79 36-135
Butyl benzyl phthalate 40.0 35.29 ug/L 88 34-146
Carbazole 40.0 33.79 ug/L 84 42-130
4-Chloroaniline 40.0 30.66 ug/L 77 27-131
4-Chloro-3-methylphenol 40.0 33.68 ug/L 84 10-150
2-Chloronaphthalene 40.0 29.98 ug/L 75 32-127
2-Chlorophenol 40.0 27.79 ug/L 69 10-150
4-Chlorophenyl phenyl ether 40.0 31.45 ug/L 79 36-131
Chrysene 40.0 32.14 ug/L 80 39-130
Cresols 80.0 53.12 ug/L 66 10-132
Dibenz(a,h)anthracene 40.0 30.98 ug/L 77 43-140
Dibenzofuran 40.0 31.48 ug/L 79 35-127
1,2-Dichlorobenzene 40.0 27.68 ug/L 69 27-120
1,3-Dichlorobenzene 40.0 26.65 ug/L 67 22-120
1,4-Dichlorobenzene 40.0 27.56 ug/L 69 24-120
3,3'-Dichlorobenzidine 40.0 35.56 ug/L 89 46-143
2,4-Dichlorophenol 40.0 30.89 ug/L 77 10-150
Diethyl phthalate 40.0 34.64 ug/L 87 31-136
2,4-Dimethylphenol 40.0 30.47 ug/L 76 10-150
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392749/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392931 Prep Batch: 392749
Dimethyl phthalate 40.0 33.69 ug/L 84 34-134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Di-n-butyl phthalate 40.0 35.33 ug/L 88 42-140
4,6-Dinitro-2-methylphenol 80.0 65.65 ug/L 82 10-150
2,4-Dinitrophenol 80.0 58.78 ug/L 73 10-150
2,4-Dinitrotoluene 40.0 36.93 ug/L 92 36-138
2,6-Dinitrotoluene 40.0 35.77 ug/L 89 41-137
Di-n-octyl phthalate 40.0 36.36 ug/L 91 42-142
Fluoranthene 40.0 34.00 ug/L 85 31-132
Fluorene 40.0 32.29 ug/L 81 37-130
Hexachlorobenzene 40.0 33.36 ug/L 83 36-140
Hexachlorobutadiene 40.0 28.67 ug/L 72 18-136
Hexachlorocyclopentadiene 40.0 20.39 ug/L 51 17-128
Hexachloroethane 40.0 27.49 ug/L 69 23-120
Indeno[1,2,3-cd]pyrene 40.0 30.10 ug/L 75 40-136
Isophorone 40.0 29.81 ug/L 75 39-120
1-Methylnaphthalene 40.0 31.37 ug/L 78 36-131
2-Methylnaphthalene 40.0 30.81 ug/L 77 31-120
2-Methylphenol 40.0 28.32 ug/L 71 10-133
3 & 4 Methylphenol 40.0 24.80 ug/L 62 10-135
Naphthalene 40.0 30.02 ug/L 75 32-120
2-Nitroaniline 40.0 35.01 ug/L 88 35-147
3-Nitroaniline 40.0 34.31 ug/L 86 36-128
4-Nitroaniline 40.0 36.38 ug/L 91 38-139
Nitrobenzene 40.0 31.43 ug/L 79 10-150
2-Nitrophenol 40.0 32.08 ug/L 80 10-150
4-Nitrophenol 80.0 27.66 ug/L 35 10-110
N-Nitrosodi-n-propylamine 40.0 33.33 ug/L 83 32-136
n-Nitrosodiphenylamine(as
diphenylamine)
34.0 32.49 ug/L 96 44-123
Pentachlorophenol 80.0 67.83 ug/L 85 10-150
Phenanthrene 40.0 32.26 ug/L 81 39-126
Phenol 40.0 13.85 ug/L 35 10-110
Pyrene 40.0 32.54 ug/L 81 37-129
1,2,4-Trichlorobenzene 40.0 27.81 ug/L 70 24-127
2,4,5-Trichlorophenol 40.0 30.95 ug/L 77 10-150
2,4,6-Trichlorophenol 40.0 35.45 ug/L 89 10-150
2-Fluorobiphenyl (Surr)29 -120
Surrogate
74
LCS LCS
Qualifier Limits%Recovery
422-Fluorophenol (Surr)10 -120
77Nitrobenzene-d5 (Surr)27 -120
30Phenol-d5 (Surr)10 -120
81Terphenyl-d14 (Surr)13 -120
862,4,6-Tribromophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392749/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392931 Prep Batch: 392749
Acenaphthene 40.0 33.54 ug/L 84 36-129 4 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 40.0 33.84 ug/L 85 36-120 5 50
Anthracene 40.0 33.75 ug/L 84 42-130 5 50
Benzo[a]anthracene 40.0 34.37 ug/L 86 41-131 5 50
Benzo[a]pyrene 40.0 33.01 ug/L 83 45-131 7 50
Benzo[b]fluoranthene 40.0 37.13 ug/L 93 43-132 12 50
Benzo[g,h,i]perylene 40.0 33.57 ug/L 84 38-138 7 50
Benzo[k]fluoranthene 40.0 33.16 ug/L 83 44-129 2 50
Bis(2-chloroethoxy)methane 40.0 33.61 ug/L 84 35-127 3 50
Bis(2-chloroethyl)ether 40.0 32.18 ug/L 80 27-132 6 50
bis (2-chloroisopropyl) ether 40.0 34.55 ug/L 86 24-136 3 50
Bis(2-ethylhexyl) phthalate 40.0 37.08 ug/L 93 41-147 6 47
4-Bromophenyl phenyl ether 40.0 33.93 ug/L 85 36-135 7 50
Butyl benzyl phthalate 40.0 37.72 ug/L 94 34-146 7 50
Carbazole 40.0 35.41 ug/L 89 42-130 5 50
4-Chloroaniline 40.0 31.27 ug/L 78 27-131 2 34
4-Chloro-3-methylphenol 40.0 35.00 ug/L 88 10-150 4 50
2-Chloronaphthalene 40.0 31.55 ug/L 79 32-127 5 50
2-Chlorophenol 40.0 29.89 ug/L 75 10-150 7 49
4-Chlorophenyl phenyl ether 40.0 33.32 ug/L 83 36-131 6 50
Chrysene 40.0 34.40 ug/L 86 39-130 7 50
Cresols 80.0 54.37 ug/L 68 10-132 2 50
Dibenz(a,h)anthracene 40.0 33.38 ug/L 83 43-140 7 50
Dibenzofuran 40.0 33.05 ug/L 83 35-127 5 50
1,2-Dichlorobenzene 40.0 29.52 ug/L 74 27-120 6 50
1,3-Dichlorobenzene 40.0 29.10 ug/L 73 22-120 9 50
1,4-Dichlorobenzene 40.0 29.44 ug/L 74 24-120 7 50
3,3'-Dichlorobenzidine 40.0 37.51 ug/L 94 46-143 5 50
2,4-Dichlorophenol 40.0 32.13 ug/L 80 10-150 4 50
Diethyl phthalate 40.0 36.03 ug/L 90 31-136 4 50
2,4-Dimethylphenol 40.0 31.12 ug/L 78 10-150 2 50
Dimethyl phthalate 40.0 35.11 ug/L 88 34-134 4 50
Di-n-butyl phthalate 40.0 37.07 ug/L 93 42-140 5 50
4,6-Dinitro-2-methylphenol 80.0 68.48 ug/L 86 10-150 4 50
2,4-Dinitrophenol 80.0 63.59 ug/L 79 10-150 8 50
2,4-Dinitrotoluene 40.0 39.87 ug/L 100 36-138 8 50
2,6-Dinitrotoluene 40.0 37.14 ug/L 93 41-137 4 50
Di-n-octyl phthalate 40.0 38.70 ug/L 97 42-142 6 49
Fluoranthene 40.0 35.98 ug/L 90 31-132 6 50
Fluorene 40.0 33.59 ug/L 84 37-130 4 50
Hexachlorobenzene 40.0 34.73 ug/L 87 36-140 4 50
Hexachlorobutadiene 40.0 30.33 ug/L 76 18-136 6 50
Hexachlorocyclopentadiene 40.0 21.77 ug/L 54 17-128 7 50
Hexachloroethane 40.0 30.03 ug/L 75 23-120 9 50
Indeno[1,2,3-cd]pyrene 40.0 32.43 ug/L 81 40-136 7 50
Isophorone 40.0 30.11 ug/L 75 39-120 1 50
1-Methylnaphthalene 40.0 32.13 ug/L 80 36-131 2 50
2-Methylnaphthalene 40.0 32.36 ug/L 81 31-120 5 50
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392749/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 392931 Prep Batch: 392749
2-Methylphenol 40.0 28.90 ug/L 72 10-133 2 45
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
3 & 4 Methylphenol 40.0 25.47 ug/L 64 10-135 3 46
Naphthalene 40.0 31.15 ug/L 78 32-120 4 50
2-Nitroaniline 40.0 35.91 ug/L 90 35-147 3 50
3-Nitroaniline 40.0 36.77 ug/L 92 36-128 7 27
4-Nitroaniline 40.0 38.22 ug/L 96 38-139 5 42
Nitrobenzene 40.0 32.68 ug/L 82 10-150 4 50
2-Nitrophenol 40.0 34.04 ug/L 85 10-150 6 50
4-Nitrophenol 80.0 28.44 ug/L 36 10-110 3 40
N-Nitrosodi-n-propylamine 40.0 34.49 ug/L 86 32-136 3 50
n-Nitrosodiphenylamine(as
diphenylamine)
34.0 33.73 ug/L 99 44-123 4 50
Pentachlorophenol 80.0 71.62 ug/L 90 10-150 5 50
Phenanthrene 40.0 33.47 ug/L 84 39-126 4 50
Phenol 40.0 14.54 ug/L 36 10-110 5 36
Pyrene 40.0 34.11 ug/L 85 37-129 5 50
1,2,4-Trichlorobenzene 40.0 29.20 ug/L 73 24-127 5 50
2,4,5-Trichlorophenol 40.0 31.32 ug/L 78 10-150 1 50
2,4,6-Trichlorophenol 40.0 37.63 ug/L 94 10-150 6 50
2-Fluorobiphenyl (Surr)29 -120
Surrogate
84
LCSD LCSD
Qualifier Limits%Recovery
482-Fluorophenol (Surr)10 -120
86Nitrobenzene-d5 (Surr)27 -120
34Phenol-d5 (Surr)10 -120
93Terphenyl-d14 (Surr)13 -120
1002,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Method BlankLab Sample ID: MB 490-392774/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
RL MDL
Acenaphthene <0.0320 0.0670 0.0320 mg/Kg 12/08/16 11:03 12/09/16 19:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.0290 0.02900.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Acenaphthylene
<0.0290 0.02900.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Anthracene
<0.0300 0.03000.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Benzo[a]anthracene
<0.0270 0.02700.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Benzo[a]pyrene
<0.0280 0.02800.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Benzo[b]fluoranthene
<0.0330 0.03300.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Benzo[g,h,i]perylene
<0.0270 0.02700.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Benzo[k]fluoranthene
<0.200 0.2000.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Bis(2-chloroethoxy)methane
<0.213 0.2130.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Bis(2-chloroethyl)ether
<0.198 0.1980.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1bis (2-chloroisopropyl) ether
<0.207 0.2070.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Bis(2-ethylhexyl) phthalate
<0.205 0.2050.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 14-Bromophenyl phenyl ether
<0.215 0.2150.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Butyl benzyl phthalate
<0.207 0.2070.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Carbazole
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392774/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
RL MDL
4-Chloroaniline <0.227 0.333 0.227 mg/Kg 12/08/16 11:03 12/09/16 19:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.168 0.1680.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 14-Chloro-3-methylphenol
<0.209 0.2090.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12-Chloronaphthalene
<0.191 0.1910.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12-Chlorophenol
<0.201 0.2010.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 14-Chlorophenyl phenyl ether
<0.0370 0.03700.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Chrysene
<0.113 0.1130.666 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Cresols
<0.0320 0.03200.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Dibenz(a,h)anthracene
<0.210 0.2100.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Dibenzofuran
<0.190 0.1900.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 11,2-Dichlorobenzene
<0.190 0.1900.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 11,3-Dichlorobenzene
<0.196 0.1960.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 11,4-Dichlorobenzene
<0.204 0.2040.670 mg/Kg 12/08/16 11:03 12/09/16 19:48 13,3'-Dichlorobenzidine
<0.175 0.1750.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12,4-Dichlorophenol
<0.212 0.2120.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Diethyl phthalate
<0.335 0.3350.670 mg/Kg 12/08/16 11:03 12/09/16 19:48 12,4-Dimethylphenol
<0.207 0.2070.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Dimethyl phthalate
<0.211 0.2110.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Di-n-butyl phthalate
<0.229 0.2290.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 14,6-Dinitro-2-methylphenol
<0.251 0.2510.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12,4-Dinitrophenol
<0.208 0.2080.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12,4-Dinitrotoluene
<0.223 0.2230.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12,6-Dinitrotoluene
<0.178 0.1780.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Di-n-octyl phthalate
<0.0340 0.03400.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Fluoranthene
<0.0290 0.02900.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Fluorene
<0.250 0.2500.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Hexachlorobenzene
<0.167 0.1670.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Hexachlorobutadiene
<0.150 0.1500.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Hexachlorocyclopentadiene
<0.181 0.1810.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Hexachloroethane
<0.0290 0.02900.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Indeno[1,2,3-cd]pyrene
<0.188 0.1880.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Isophorone
<0.0280 0.02800.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 11-Methylnaphthalene
<0.0260 0.02600.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 12-Methylnaphthalene
<0.216 0.2160.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12-Methylphenol
<0.203 0.2030.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 13 & 4 Methylphenol
<0.0290 0.02900.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Naphthalene
<0.207 0.2070.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12-Nitroaniline
<0.230 0.2300.670 mg/Kg 12/08/16 11:03 12/09/16 19:48 13-Nitroaniline
<0.238 0.2380.670 mg/Kg 12/08/16 11:03 12/09/16 19:48 14-Nitroaniline
<0.201 0.2010.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Nitrobenzene
<0.243 0.2430.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12-Nitrophenol
<0.382 0.3820.670 mg/Kg 12/08/16 11:03 12/09/16 19:48 14-Nitrophenol
<0.194 0.1940.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1N-Nitrosodi-n-propylamine
<0.0530 0.05300.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1n-Nitrosodiphenylamine(as
diphenylamine)
<0.266 0.2660.670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Pentachlorophenol
<0.0340 0.03400.0670 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Phenanthrene
<0.203 0.2030.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 1Phenol
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392774/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
RL MDL
Pyrene <0.0340 0.0670 0.0340 mg/Kg 12/08/16 11:03 12/09/16 19:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.181 0.1810.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 11,2,4-Trichlorobenzene
<0.218 0.2180.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12,4,5-Trichlorophenol
<0.192 0.1920.333 mg/Kg 12/08/16 11:03 12/09/16 19:48 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)77 29-120 12/09/16 19:48 1
MB MB
Surrogate
12/08/16 11:03
Dil FacPreparedAnalyzedQualifierLimits%Recovery
61 12/08/16 11:03 12/09/16 19:48 12-Fluorophenol (Surr)10-120
81 12/08/16 11:03 12/09/16 19:48 1Nitrobenzene-d5 (Surr)27-120
68 12/08/16 11:03 12/09/16 19:48 1Phenol-d5 (Surr)10-120
83 12/08/16 11:03 12/09/16 19:48 1Terphenyl-d14 (Surr)13-120
55 12/08/16 11:03 12/09/16 19:48 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392774/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
Acenaphthene 1.67 1.228 mg/Kg 74 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.234 mg/Kg 74 38-120
Anthracene 1.67 1.285 mg/Kg 77 46-124
Benzo[a]anthracene 1.67 1.286 mg/Kg 77 45-120
Benzo[a]pyrene 1.67 1.253 mg/Kg 75 45-120
Benzo[b]fluoranthene 1.67 1.303 mg/Kg 78 42-120
Benzo[g,h,i]perylene 1.67 1.323 mg/Kg 79 38-120
Benzo[k]fluoranthene 1.67 1.319 mg/Kg 79 42-120
Bis(2-chloroethoxy)methane 1.67 1.178 mg/Kg 71 32-120
Bis(2-chloroethyl)ether 1.67 1.203 mg/Kg 72 31-120
bis (2-chloroisopropyl) ether 1.67 0.9288 mg/Kg 56 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.214 mg/Kg 73 43-120
4-Bromophenyl phenyl ether 1.67 1.270 mg/Kg 76 40-120
Butyl benzyl phthalate 1.67 1.226 mg/Kg 74 43-133
Carbazole 1.67 1.330 mg/Kg 80 44-120
4-Chloroaniline 1.67 1.246 mg/Kg 75 35-120
4-Chloro-3-methylphenol 1.67 1.305 mg/Kg 78 38-120
2-Chloronaphthalene 1.67 1.228 mg/Kg 74 34-120
2-Chlorophenol 1.67 1.169 mg/Kg 70 32-120
4-Chlorophenyl phenyl ether 1.67 1.291 mg/Kg 77 42-120
Chrysene 1.67 1.314 mg/Kg 79 43-120
Cresols 3.33 2.331 mg/Kg 70 36-129
Dibenz(a,h)anthracene 1.67 1.274 mg/Kg 76 32-128
Dibenzofuran 1.67 1.241 mg/Kg 74 41-120
1,2-Dichlorobenzene 1.67 1.120 mg/Kg 67 33-120
1,3-Dichlorobenzene 1.67 1.091 mg/Kg 65 32-120
1,4-Dichlorobenzene 1.67 1.106 mg/Kg 66 32-120
3,3'-Dichlorobenzidine 1.67 1.122 mg/Kg 67 39-120
2,4-Dichlorophenol 1.67 1.211 mg/Kg 73 32-120
Diethyl phthalate 1.67 1.314 mg/Kg 79 41-122
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392774/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
2,4-Dimethylphenol 1.67 1.195 mg/Kg 72 32-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Dimethyl phthalate 1.67 1.285 mg/Kg 77 55-120
Di-n-butyl phthalate 1.67 1.299 mg/Kg 78 46-127
4,6-Dinitro-2-methylphenol 3.33 2.606 mg/Kg 78 27-134
2,4-Dinitrophenol 3.33 1.968 mg/Kg 59 10-142
2,4-Dinitrotoluene 1.67 1.348 mg/Kg 81 43-120
2,6-Dinitrotoluene 1.67 1.287 mg/Kg 77 43-120
Di-n-octyl phthalate 1.67 1.245 mg/Kg 75 40-130
Fluoranthene 1.67 1.355 mg/Kg 81 46-120
Fluorene 1.67 1.239 mg/Kg 74 42-120
Hexachlorobenzene 1.67 1.354 mg/Kg 81 44-120
Hexachlorobutadiene 1.67 1.138 mg/Kg 68 31-120
Hexachlorocyclopentadiene 1.67 0.8965 mg/Kg 54 24-120
Hexachloroethane 1.67 1.106 mg/Kg 66 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.249 mg/Kg 75 41-121
Isophorone 1.67 1.163 mg/Kg 70 33-120
1-Methylnaphthalene 1.67 1.210 mg/Kg 73 32-120
2-Methylnaphthalene 1.67 1.220 mg/Kg 73 28-120
2-Methylphenol 1.67 1.179 mg/Kg 71 36-120
3 & 4 Methylphenol 1.67 1.152 mg/Kg 69 37-120
Naphthalene 1.67 1.138 mg/Kg 68 32-120
2-Nitroaniline 1.67 1.305 mg/Kg 78 40-120
3-Nitroaniline 1.67 1.255 mg/Kg 75 42-120
4-Nitroaniline 1.67 1.271 mg/Kg 76 43-120
Nitrobenzene 1.67 1.156 mg/Kg 69 26-120
2-Nitrophenol 1.67 1.203 mg/Kg 72 29-120
4-Nitrophenol 3.33 2.171 mg/Kg 65 32-136
N-Nitrosodi-n-propylamine 1.67 1.110 mg/Kg 67 35-120
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.295 mg/Kg 91 52-140
Pentachlorophenol 3.33 2.210 mg/Kg 66 44-134
Phenanthrene 1.67 1.303 mg/Kg 78 45-120
Phenol 1.67 1.220 mg/Kg 73 30-120
Pyrene 1.67 1.253 mg/Kg 75 43-120
1,2,4-Trichlorobenzene 1.67 1.134 mg/Kg 68 29-120
2,4,5-Trichlorophenol 1.67 1.350 mg/Kg 81 39-120
2,4,6-Trichlorophenol 1.67 1.275 mg/Kg 76 39-120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
77
LCS LCS
Qualifier Limits%Recovery
722-Fluorophenol (Surr)10 -120
73Nitrobenzene-d5 (Surr)27 -120
76Phenol-d5 (Surr)10 -120
81Terphenyl-d14 (Surr)13 -120
852,4,6-Tribromophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-117419-D-11-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
Acenaphthene <0.0383 2.01 1.232 mg/Kg 61 19-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene <0.0347 2.01 1.187 mg/Kg 59 25-120☼
Anthracene <0.0347 2.01 1.275 mg/Kg 63 28-125☼
Benzo[a]anthracene <0.0359 2.01 1.331 mg/Kg 66 23-120☼
Benzo[a]pyrene <0.0323 2.01 1.254 mg/Kg 62 15-128☼
Benzo[b]fluoranthene <0.0335 2.01 1.270 mg/Kg 63 12-133☼
Benzo[g,h,i]perylene <0.0395 2.01 1.356 mg/Kg 67 22-120☼
Benzo[k]fluoranthene <0.0323 2.01 1.418 mg/Kg 70 28-120☼
Bis(2-chloroethoxy)methane <0.239 2.01 1.073 mg/Kg 53 24-120☼
Bis(2-chloroethyl)ether <0.255 2.01 1.177 mg/Kg 59 22-120☼
bis (2-chloroisopropyl) ether <0.237 2.01 1.011 mg/Kg 50 20-120☼
Bis(2-ethylhexyl) phthalate <0.248 2.01 1.315 mg/Kg 65 26-120☼
4-Bromophenyl phenyl ether <0.245 2.01 1.264 mg/Kg 63 31-120☼
Butyl benzyl phthalate <0.257 2.01 1.332 mg/Kg 66 24-133☼
Carbazole <0.248 2.01 1.293 mg/Kg 64 25-123☼
4-Chloroaniline <0.272 2.01 1.179 mg/Kg 59 26-120☼
4-Chloro-3-methylphenol <0.201 2.01 1.253 mg/Kg 62 21-120☼
2-Chloronaphthalene <0.250 2.01 1.202 mg/Kg 60 24-120☼
2-Chlorophenol <0.229 2.01 1.123 mg/Kg 56 25-120☼
4-Chlorophenyl phenyl ether <0.241 2.01 1.274 mg/Kg 63 26-120☼
Chrysene <0.0443 2.01 1.348 mg/Kg 67 20-120☼
Cresols <0.135 4.02 2.247 mg/Kg 56 10-200☼
Dibenz(a,h)anthracene <0.0383 2.01 1.307 mg/Kg 65 12-128☼
Dibenzofuran <0.251 2.01 1.229 mg/Kg 61 21-120☼
1,2-Dichlorobenzene <0.228 2.01 1.119 mg/Kg 56 10-120☼
1,3-Dichlorobenzene <0.228 2.01 1.076 mg/Kg 53 10-120☼
1,4-Dichlorobenzene <0.235 2.01 1.086 mg/Kg 54 10-120☼
3,3'-Dichlorobenzidine <0.244 2.01 1.196 mg/Kg 59 10-120☼
2,4-Dichlorophenol <0.210 2.01 1.203 mg/Kg 60 17-120☼
Diethyl phthalate <0.254 2.01 1.240 mg/Kg 62 29-122☼
2,4-Dimethylphenol <0.401 2.01 1.149 mg/Kg 57 17-120☼
Dimethyl phthalate <0.248 2.01 1.180 mg/Kg 59 30-120☼
Di-n-butyl phthalate <0.253 2.01 1.258 mg/Kg 63 29-126☼
4,6-Dinitro-2-methylphenol <0.274 F1 4.02 <0.276 F1 mg/Kg 0 10-134☼
2,4-Dinitrophenol <0.301 F1 4.02 <0.303 F1 mg/Kg 0 10-150☼
2,4-Dinitrotoluene <0.249 2.01 1.128 mg/Kg 56 24-121☼
2,6-Dinitrotoluene <0.267 2.01 1.132 mg/Kg 56 24-120☼
Di-n-octyl phthalate <0.213 2.01 1.353 mg/Kg 67 27-130☼
Fluoranthene <0.0407 2.01 1.307 mg/Kg 65 10-143☼
Fluorene <0.0347 2.01 1.250 mg/Kg 62 20-120☼
Hexachlorobenzene <0.299 2.01 1.428 mg/Kg 71 25-120☼
Hexachlorobutadiene <0.200 2.01 1.181 mg/Kg 59 10-120☼
Hexachlorocyclopentadiene <0.180 F1 2.01 <0.181 F1 mg/Kg 0 10-120☼
Hexachloroethane <0.217 2.01 0.9933 mg/Kg 49 10-120☼
Indeno[1,2,3-cd]pyrene <0.0347 2.01 1.265 mg/Kg 63 22-121☼
Isophorone <0.225 2.01 1.078 mg/Kg 54 24-120☼
1-Methylnaphthalene <0.0335 2.01 1.143 mg/Kg 57 10-120☼
2-Methylnaphthalene <0.0311 2.01 1.130 mg/Kg 56 13-120☼
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-117419-D-11-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
2-Methylphenol <0.259 2.01 1.139 mg/Kg 57 23-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
3 & 4 Methylphenol <0.243 2.01 1.108 mg/Kg 55 19-120☼
Naphthalene <0.0347 2.01 1.109 mg/Kg 55 10-120☼
2-Nitroaniline <0.248 2.01 1.230 mg/Kg 61 31-120☼
3-Nitroaniline <0.275 2.01 1.383 mg/Kg 69 31-120☼
4-Nitroaniline <0.285 2.01 1.250 mg/Kg 62 28-120☼
Nitrobenzene <0.241 2.01 1.091 mg/Kg 54 19-120☼
2-Nitrophenol <0.291 2.01 0.7787 mg/Kg 39 23-120☼
4-Nitrophenol <0.457 4.02 2.360 mg/Kg 59 16-139☼
N-Nitrosodi-n-propylamine <0.232 2.01 1.020 mg/Kg 51 24-120☼
n-Nitrosodiphenylamine(as
diphenylamine)
<0.0635 1.71 1.235 mg/Kg 72 26-150☼
Pentachlorophenol <0.319 4.02 2.545 mg/Kg 63 19-145☼
Phenanthrene <0.0407 2.01 1.300 mg/Kg 65 21-122☼
Phenol <0.243 2.01 1.209 mg/Kg 60 15-120☼
Pyrene <0.0407 2.01 1.381 mg/Kg 69 20-123☼
1,2,4-Trichlorobenzene <0.217 2.01 1.116 mg/Kg 56 14-120☼
2,4,5-Trichlorophenol <0.261 2.01 1.434 mg/Kg 71 27-120☼
2,4,6-Trichlorophenol <0.230 2.01 1.273 mg/Kg 63 24-122☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
63
MS MS
Qualifier Limits%Recovery
582-Fluorophenol (Surr)10 -120
61Nitrobenzene-d5 (Surr)27 -120
63Phenol-d5 (Surr)10 -120
76Terphenyl-d14 (Surr)13 -120
752,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117419-D-11-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
Acenaphthene <0.0383 2.01 1.212 mg/Kg 60 19-120 2 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene <0.0347 2.01 1.157 mg/Kg 58 25-120 3 50☼
Anthracene <0.0347 2.01 1.255 mg/Kg 63 28-125 2 49☼
Benzo[a]anthracene <0.0359 2.01 1.271 mg/Kg 63 23-120 5 50☼
Benzo[a]pyrene <0.0323 2.01 1.195 mg/Kg 60 15-128 5 50☼
Benzo[b]fluoranthene <0.0335 2.01 1.302 mg/Kg 65 12-133 2 50☼
Benzo[g,h,i]perylene <0.0395 2.01 1.301 mg/Kg 65 22-120 4 50☼
Benzo[k]fluoranthene <0.0323 2.01 1.251 mg/Kg 62 28-120 12 45☼
Bis(2-chloroethoxy)methane <0.239 2.01 1.061 mg/Kg 53 24-120 1 50☼
Bis(2-chloroethyl)ether <0.255 2.01 1.254 mg/Kg 62 22-120 6 50☼
bis (2-chloroisopropyl) ether <0.237 2.01 0.9995 mg/Kg 50 20-120 1 50☼
Bis(2-ethylhexyl) phthalate <0.248 2.01 1.278 mg/Kg 64 26-120 3 50☼
4-Bromophenyl phenyl ether <0.245 2.01 1.226 mg/Kg 61 31-120 3 37☼
Butyl benzyl phthalate <0.257 2.01 1.258 mg/Kg 63 24-133 6 50☼
Carbazole <0.248 2.01 1.228 mg/Kg 61 25-123 5 46☼
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117419-D-11-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
4-Chloroaniline <0.272 2.01 1.155 mg/Kg 58 26-120 2 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Chloro-3-methylphenol <0.201 2.01 1.217 mg/Kg 61 21-120 3 49☼
2-Chloronaphthalene <0.250 2.01 1.160 mg/Kg 58 24-120 4 50☼
2-Chlorophenol <0.229 2.01 1.132 mg/Kg 56 25-120 1 50☼
4-Chlorophenyl phenyl ether <0.241 2.01 1.245 mg/Kg 62 26-120 2 50☼
Chrysene <0.0443 2.01 1.281 mg/Kg 64 20-120 5 49☼
Cresols <0.135 4.01 2.190 mg/Kg 55 10-200 3 50☼
Dibenz(a,h)anthracene <0.0383 2.01 1.253 mg/Kg 62 12-128 4 50☼
Dibenzofuran <0.251 2.01 1.192 mg/Kg 59 21-120 3 50☼
1,2-Dichlorobenzene <0.228 2.01 1.123 mg/Kg 56 10-120 0 50☼
1,3-Dichlorobenzene <0.228 2.01 1.099 mg/Kg 55 10-120 2 50☼
1,4-Dichlorobenzene <0.235 2.01 1.090 mg/Kg 54 10-120 0 50☼
3,3'-Dichlorobenzidine <0.244 2.01 1.105 mg/Kg 55 10-120 8 50☼
2,4-Dichlorophenol <0.210 2.01 1.183 mg/Kg 59 17-120 2 50☼
Diethyl phthalate <0.254 2.01 1.167 mg/Kg 58 29-122 6 45☼
2,4-Dimethylphenol <0.401 2.01 1.107 mg/Kg 55 17-120 4 50☼
Dimethyl phthalate <0.248 2.01 1.138 mg/Kg 57 30-120 4 46☼
Di-n-butyl phthalate <0.253 2.01 1.213 mg/Kg 60 29-126 4 49☼
4,6-Dinitro-2-methylphenol <0.274 F1 4.01 <0.276 F1 mg/Kg 0 10-134 NC 50☼
2,4-Dinitrophenol <0.301 F1 4.01 <0.302 F1 mg/Kg 0 10-150 NC 50☼
2,4-Dinitrotoluene <0.249 2.01 1.149 mg/Kg 57 24-121 2 50☼
2,6-Dinitrotoluene <0.267 2.01 1.090 mg/Kg 54 24-120 4 50☼
Di-n-octyl phthalate <0.213 2.01 1.308 mg/Kg 65 27-130 3 50☼
Fluoranthene <0.0407 2.01 1.249 mg/Kg 62 10-143 4 50☼
Fluorene <0.0347 2.01 1.210 mg/Kg 60 20-120 3 50☼
Hexachlorobenzene <0.299 2.01 1.352 mg/Kg 67 25-120 6 50☼
Hexachlorobutadiene <0.200 2.01 1.191 mg/Kg 59 10-120 1 50☼
Hexachlorocyclopentadiene <0.180 F1 2.01 <0.181 F1 mg/Kg 0 10-120 NC 50☼
Hexachloroethane <0.217 2.01 1.052 mg/Kg 52 10-120 6 50☼
Indeno[1,2,3-cd]pyrene <0.0347 2.01 1.222 mg/Kg 61 22-121 3 50☼
Isophorone <0.225 2.01 1.063 mg/Kg 53 24-120 1 50☼
1-Methylnaphthalene <0.0335 2.01 1.133 mg/Kg 56 10-120 1 50☼
2-Methylnaphthalene <0.0311 2.01 1.151 mg/Kg 57 13-120 2 50☼
2-Methylphenol <0.259 2.01 1.112 mg/Kg 55 23-120 2 50☼
3 & 4 Methylphenol <0.243 2.01 1.078 mg/Kg 54 19-120 3 50☼
Naphthalene <0.0347 2.01 1.109 mg/Kg 55 10-120 0 50☼
2-Nitroaniline <0.248 2.01 1.176 mg/Kg 59 31-120 4 50☼
3-Nitroaniline <0.275 2.01 1.257 mg/Kg 63 31-120 10 49☼
4-Nitroaniline <0.285 2.01 1.191 mg/Kg 59 28-120 5 49☼
Nitrobenzene <0.241 2.01 1.103 mg/Kg 55 19-120 1 50☼
2-Nitrophenol <0.291 2.01 0.8194 mg/Kg 41 23-120 5 50☼
4-Nitrophenol <0.457 4.01 2.263 mg/Kg 56 16-139 4 45☼
N-Nitrosodi-n-propylamine <0.232 2.01 1.036 mg/Kg 52 24-120 2 50☼
n-Nitrosodiphenylamine(as
diphenylamine)
<0.0635 1.71 1.210 mg/Kg 71 26-150 2 50☼
Pentachlorophenol <0.319 4.01 2.298 mg/Kg 57 19-145 10 50☼
Phenanthrene <0.0407 2.01 1.258 mg/Kg 63 21-122 3 50☼
Phenol <0.243 2.01 1.201 mg/Kg 60 15-120 1 50☼
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117419-D-11-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393298 Prep Batch: 392774
Pyrene <0.0407 2.01 1.315 mg/Kg 66 20-123 5 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2,4-Trichlorobenzene <0.217 2.01 1.146 mg/Kg 57 14-120 3 50☼
2,4,5-Trichlorophenol <0.261 2.01 1.348 mg/Kg 67 27-120 6 50☼
2,4,6-Trichlorophenol <0.230 2.01 1.202 mg/Kg 60 24-122 6 50☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
57
MSD MSD
Qualifier Limits%Recovery
562-Fluorophenol (Surr)10 -120
56Nitrobenzene-d5 (Surr)27 -120
59Phenol-d5 (Surr)10 -120
67Terphenyl-d14 (Surr)13 -120
682,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Method BlankLab Sample ID: MB 490-392804/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
RL MDL
Acenaphthene <0.0320 0.0670 0.0320 mg/Kg 12/08/16 12:11 12/09/16 12:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.0290 0.02900.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Acenaphthylene
<0.0290 0.02900.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Anthracene
<0.0300 0.03000.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Benzo[a]anthracene
<0.0270 0.02700.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Benzo[a]pyrene
<0.0280 0.02800.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Benzo[b]fluoranthene
<0.0330 0.03300.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Benzo[g,h,i]perylene
<0.0270 0.02700.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Benzo[k]fluoranthene
<0.200 0.2000.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Bis(2-chloroethoxy)methane
<0.213 0.2130.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Bis(2-chloroethyl)ether
<0.198 0.1980.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1bis (2-chloroisopropyl) ether
<0.207 0.2070.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Bis(2-ethylhexyl) phthalate
<0.205 0.2050.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 14-Bromophenyl phenyl ether
<0.215 0.2150.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Butyl benzyl phthalate
<0.207 0.2070.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Carbazole
<0.227 0.2270.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 14-Chloroaniline
<0.168 0.1680.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 14-Chloro-3-methylphenol
<0.209 0.2090.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12-Chloronaphthalene
<0.191 0.1910.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12-Chlorophenol
<0.201 0.2010.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 14-Chlorophenyl phenyl ether
<0.0370 0.03700.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Chrysene
<0.113 0.1130.666 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Cresols
<0.0320 0.03200.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Dibenz(a,h)anthracene
<0.210 0.2100.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Dibenzofuran
<0.190 0.1900.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 11,2-Dichlorobenzene
<0.190 0.1900.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 11,3-Dichlorobenzene
<0.196 0.1960.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 11,4-Dichlorobenzene
<0.204 0.2040.670 mg/Kg 12/08/16 12:11 12/09/16 12:16 13,3'-Dichlorobenzidine
<0.175 0.1750.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12,4-Dichlorophenol
<0.212 0.2120.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Diethyl phthalate
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-392804/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
RL MDL
2,4-Dimethylphenol <0.335 0.670 0.335 mg/Kg 12/08/16 12:11 12/09/16 12:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.207 0.2070.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Dimethyl phthalate
<0.211 0.2110.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Di-n-butyl phthalate
<0.229 0.2290.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 14,6-Dinitro-2-methylphenol
<0.251 0.2510.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12,4-Dinitrophenol
<0.208 0.2080.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12,4-Dinitrotoluene
<0.223 0.2230.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12,6-Dinitrotoluene
<0.178 0.1780.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Di-n-octyl phthalate
<0.0340 0.03400.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Fluoranthene
<0.0290 0.02900.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Fluorene
<0.250 0.2500.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Hexachlorobenzene
<0.167 0.1670.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Hexachlorobutadiene
<0.150 0.1500.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Hexachlorocyclopentadiene
<0.181 0.1810.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Hexachloroethane
<0.0290 0.02900.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Indeno[1,2,3-cd]pyrene
<0.188 0.1880.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Isophorone
<0.0280 0.02800.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 11-Methylnaphthalene
<0.0260 0.02600.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 12-Methylnaphthalene
<0.216 0.2160.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12-Methylphenol
<0.203 0.2030.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 13 & 4 Methylphenol
<0.0290 0.02900.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Naphthalene
<0.207 0.2070.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12-Nitroaniline
<0.230 0.2300.670 mg/Kg 12/08/16 12:11 12/09/16 12:16 13-Nitroaniline
<0.238 0.2380.670 mg/Kg 12/08/16 12:11 12/09/16 12:16 14-Nitroaniline
<0.201 0.2010.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Nitrobenzene
<0.243 0.2430.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12-Nitrophenol
<0.382 0.3820.670 mg/Kg 12/08/16 12:11 12/09/16 12:16 14-Nitrophenol
<0.194 0.1940.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1N-Nitrosodi-n-propylamine
<0.0530 0.05300.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1n-Nitrosodiphenylamine(as
diphenylamine)
<0.266 0.2660.670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Pentachlorophenol
<0.0340 0.03400.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Phenanthrene
<0.203 0.2030.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Phenol
<0.0340 0.03400.0670 mg/Kg 12/08/16 12:11 12/09/16 12:16 1Pyrene
<0.181 0.1810.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 11,2,4-Trichlorobenzene
<0.218 0.2180.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12,4,5-Trichlorophenol
<0.192 0.1920.333 mg/Kg 12/08/16 12:11 12/09/16 12:16 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)74 29-120 12/09/16 12:16 1
MB MB
Surrogate
12/08/16 12:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
74 12/08/16 12:11 12/09/16 12:16 12-Fluorophenol (Surr)10-120
78 12/08/16 12:11 12/09/16 12:16 1Nitrobenzene-d5 (Surr)27-120
74 12/08/16 12:11 12/09/16 12:16 1Phenol-d5 (Surr)10-120
84 12/08/16 12:11 12/09/16 12:16 1Terphenyl-d14 (Surr)13-120
76 12/08/16 12:11 12/09/16 12:16 12,4,6-Tribromophenol (Surr)10-120
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392804/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
Acenaphthene 1.67 1.332 mg/Kg 80 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.249 mg/Kg 75 38-120
Anthracene 1.67 1.341 mg/Kg 80 46-124
Benzo[a]anthracene 1.67 1.360 mg/Kg 82 45-120
Benzo[a]pyrene 1.67 1.333 mg/Kg 80 45-120
Benzo[b]fluoranthene 1.67 1.378 mg/Kg 83 42-120
Benzo[g,h,i]perylene 1.67 1.428 mg/Kg 86 38-120
Benzo[k]fluoranthene 1.67 1.416 mg/Kg 85 42-120
Bis(2-chloroethoxy)methane 1.67 1.178 mg/Kg 71 32-120
Bis(2-chloroethyl)ether 1.67 1.276 mg/Kg 77 31-120
bis (2-chloroisopropyl) ether 1.67 0.9601 mg/Kg 58 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.320 mg/Kg 79 43-120
4-Bromophenyl phenyl ether 1.67 1.328 mg/Kg 80 40-120
Butyl benzyl phthalate 1.67 1.310 mg/Kg 79 43-133
Carbazole 1.67 1.346 mg/Kg 81 44-120
4-Chloroaniline 1.67 1.280 mg/Kg 77 35-120
4-Chloro-3-methylphenol 1.67 1.307 mg/Kg 78 38-120
2-Chloronaphthalene 1.67 1.255 mg/Kg 75 34-120
2-Chlorophenol 1.67 1.117 mg/Kg 67 32-120
4-Chlorophenyl phenyl ether 1.67 1.371 mg/Kg 82 42-120
Chrysene 1.67 1.411 mg/Kg 85 43-120
Cresols 3.33 2.280 mg/Kg 68 36-129
Dibenz(a,h)anthracene 1.67 1.399 mg/Kg 84 32-128
Dibenzofuran 1.67 1.292 mg/Kg 77 41-120
1,2-Dichlorobenzene 1.67 1.115 mg/Kg 67 33-120
1,3-Dichlorobenzene 1.67 1.069 mg/Kg 64 32-120
1,4-Dichlorobenzene 1.67 1.066 mg/Kg 64 32-120
3,3'-Dichlorobenzidine 1.67 1.089 mg/Kg 65 39-120
2,4-Dichlorophenol 1.67 1.223 mg/Kg 73 32-120
Diethyl phthalate 1.67 1.385 mg/Kg 83 41-122
2,4-Dimethylphenol 1.67 1.209 mg/Kg 73 32-120
Dimethyl phthalate 1.67 1.341 mg/Kg 80 55-120
Di-n-butyl phthalate 1.67 1.359 mg/Kg 82 46-127
4,6-Dinitro-2-methylphenol 3.33 2.449 mg/Kg 73 27-134
2,4-Dinitrophenol 3.33 1.996 mg/Kg 60 10-142
2,4-Dinitrotoluene 1.67 1.423 mg/Kg 85 43-120
2,6-Dinitrotoluene 1.67 1.366 mg/Kg 82 43-120
Di-n-octyl phthalate 1.67 1.367 mg/Kg 82 40-130
Fluoranthene 1.67 1.379 mg/Kg 83 46-120
Fluorene 1.67 1.320 mg/Kg 79 42-120
Hexachlorobenzene 1.67 1.405 mg/Kg 84 44-120
Hexachlorobutadiene 1.67 1.170 mg/Kg 70 31-120
Hexachlorocyclopentadiene 1.67 0.9145 mg/Kg 55 24-120
Hexachloroethane 1.67 1.120 mg/Kg 67 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.341 mg/Kg 80 41-121
Isophorone 1.67 1.206 mg/Kg 72 33-120
1-Methylnaphthalene 1.67 1.195 mg/Kg 72 32-120
2-Methylnaphthalene 1.67 1.174 mg/Kg 70 28-120
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392804/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
2-Methylphenol 1.67 1.147 mg/Kg 69 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
3 & 4 Methylphenol 1.67 1.133 mg/Kg 68 37-120
Naphthalene 1.67 1.115 mg/Kg 67 32-120
2-Nitroaniline 1.67 1.354 mg/Kg 81 40-120
3-Nitroaniline 1.67 1.346 mg/Kg 81 42-120
4-Nitroaniline 1.67 1.304 mg/Kg 78 43-120
Nitrobenzene 1.67 1.160 mg/Kg 70 26-120
2-Nitrophenol 1.67 1.181 mg/Kg 71 29-120
4-Nitrophenol 3.33 2.484 mg/Kg 75 32-136
N-Nitrosodi-n-propylamine 1.67 1.135 mg/Kg 68 35-120
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.321 mg/Kg 93 52-140
Pentachlorophenol 3.33 1.915 mg/Kg 57 44-134
Phenanthrene 1.67 1.348 mg/Kg 81 45-120
Phenol 1.67 1.220 mg/Kg 73 30-120
Pyrene 1.67 1.357 mg/Kg 81 43-120
1,2,4-Trichlorobenzene 1.67 1.120 mg/Kg 67 29-120
2,4,5-Trichlorophenol 1.67 1.369 mg/Kg 82 39-120
2,4,6-Trichlorophenol 1.67 1.309 mg/Kg 79 39-120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
74
LCS LCS
Qualifier Limits%Recovery
652-Fluorophenol (Surr)10 -120
70Nitrobenzene-d5 (Surr)27 -120
71Phenol-d5 (Surr)10 -120
84Terphenyl-d14 (Surr)13 -120
822,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix SpikeLab Sample ID: 490-117346-A-29-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
Acenaphthene <0.0349 1.81 1.298 mg/Kg 72 19-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene <0.0317 1.81 1.231 mg/Kg 68 25-120☼
Anthracene <0.0317 1.81 1.342 mg/Kg 74 28-125☼
Benzo[a]anthracene <0.0327 1.81 1.403 mg/Kg 77 23-120☼
Benzo[a]pyrene <0.0295 1.81 1.324 mg/Kg 73 15-128☼
Benzo[b]fluoranthene <0.0306 1.81 1.444 mg/Kg 80 12-133☼
Benzo[g,h,i]perylene <0.0360 1.81 1.419 mg/Kg 78 22-120☼
Benzo[k]fluoranthene <0.0295 1.81 1.379 mg/Kg 76 28-120☼
Bis(2-chloroethoxy)methane <0.218 1.81 0.9931 mg/Kg 55 24-120☼
Bis(2-chloroethyl)ether <0.232 1.81 1.124 mg/Kg 62 22-120☼
bis (2-chloroisopropyl) ether <0.216 1.81 0.9273 mg/Kg 51 20-120☼
Bis(2-ethylhexyl) phthalate <0.226 1.81 1.367 mg/Kg 75 26-120☼
4-Bromophenyl phenyl ether <0.224 1.81 1.438 mg/Kg 79 31-120☼
Butyl benzyl phthalate <0.235 1.81 1.293 mg/Kg 71 24-133☼
Carbazole <0.226 1.81 1.226 mg/Kg 68 25-123☼
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-117346-A-29-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
4-Chloroaniline <0.248 1.81 1.115 mg/Kg 62 26-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4-Chloro-3-methylphenol <0.183 1.81 1.325 mg/Kg 73 21-120☼
2-Chloronaphthalene <0.228 1.81 1.232 mg/Kg 68 24-120☼
2-Chlorophenol <0.208 1.81 1.039 mg/Kg 57 25-120☼
4-Chlorophenyl phenyl ether <0.219 1.81 1.371 mg/Kg 76 26-120☼
Chrysene <0.0404 1.81 1.401 mg/Kg 77 20-120☼
Cresols <0.123 3.62 2.138 mg/Kg 59 10-200☼
Dibenz(a,h)anthracene <0.0349 1.81 1.363 mg/Kg 75 12-128☼
Dibenzofuran <0.229 1.81 1.280 mg/Kg 71 21-120☼
1,2-Dichlorobenzene <0.207 1.81 1.012 mg/Kg 56 10-120☼
1,3-Dichlorobenzene <0.207 1.81 0.9807 mg/Kg 54 10-120☼
1,4-Dichlorobenzene <0.214 1.81 0.9891 mg/Kg 55 10-120☼
3,3'-Dichlorobenzidine <0.223 1.81 0.9409 mg/Kg 52 10-120☼
2,4-Dichlorophenol <0.191 1.81 1.169 mg/Kg 64 17-120☼
Diethyl phthalate <0.231 1.81 1.309 mg/Kg 72 29-122☼
2,4-Dimethylphenol <0.366 1.81 1.147 mg/Kg 63 17-120☼
Dimethyl phthalate <0.226 1.81 1.240 mg/Kg 68 30-120☼
Di-n-butyl phthalate <0.230 1.81 1.316 mg/Kg 73 29-126☼
4,6-Dinitro-2-methylphenol <0.250 3.62 0.9761 mg/Kg 27 10-134☼
2,4-Dinitrophenol <0.274 3.62 0.6830 mg/Kg 19 10-150☼
2,4-Dinitrotoluene <0.227 1.81 1.316 mg/Kg 73 24-121☼
2,6-Dinitrotoluene <0.243 1.81 1.248 mg/Kg 69 24-120☼
Di-n-octyl phthalate <0.194 1.81 1.440 mg/Kg 79 27-130☼
Fluoranthene <0.0371 1.81 1.330 mg/Kg 73 10-143☼
Fluorene <0.0317 1.81 1.298 mg/Kg 72 20-120☼
Hexachlorobenzene <0.273 1.81 1.435 mg/Kg 79 25-120☼
Hexachlorobutadiene <0.182 1.81 1.117 mg/Kg 62 10-120☼
Hexachlorocyclopentadiene <0.164 1.81 0.5994 mg/Kg 33 10-120☼
Hexachloroethane <0.198 1.81 1.010 mg/Kg 56 10-120☼
Indeno[1,2,3-cd]pyrene <0.0317 1.81 1.325 mg/Kg 73 22-121☼
Isophorone <0.205 1.81 1.011 mg/Kg 56 24-120☼
1-Methylnaphthalene <0.0306 1.81 1.138 mg/Kg 63 10-120☼
2-Methylnaphthalene <0.0284 1.81 1.129 mg/Kg 62 13-120☼
2-Methylphenol <0.236 1.81 1.095 mg/Kg 60 23-120☼
3 & 4 Methylphenol <0.222 1.81 1.043 mg/Kg 58 19-120☼
Naphthalene <0.0317 1.81 1.037 mg/Kg 57 10-120☼
2-Nitroaniline <0.226 1.81 1.260 mg/Kg 70 31-120☼
3-Nitroaniline <0.251 1.81 1.230 mg/Kg 68 31-120☼
4-Nitroaniline <0.260 1.81 1.196 mg/Kg 66 28-120☼
Nitrobenzene <0.219 1.81 1.029 mg/Kg 57 19-120☼
2-Nitrophenol <0.265 1.81 1.018 mg/Kg 56 23-120☼
4-Nitrophenol <0.417 3.62 2.469 mg/Kg 68 16-139☼
N-Nitrosodi-n-propylamine <0.212 1.81 0.9519 mg/Kg 53 24-120☼
n-Nitrosodiphenylamine(as
diphenylamine)
<0.0578 1.54 1.371 mg/Kg 89 26-150☼
Pentachlorophenol <0.290 3.62 2.669 mg/Kg 74 19-145☼
Phenanthrene <0.0371 1.81 1.291 mg/Kg 71 21-122☼
Phenol <0.222 1.81 1.092 mg/Kg 60 15-120☼
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-117346-A-29-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
Pyrene <0.0371 1.81 1.307 mg/Kg 72 20-123☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2,4-Trichlorobenzene <0.198 1.81 1.050 mg/Kg 58 14-120☼
2,4,5-Trichlorophenol <0.238 1.81 1.486 mg/Kg 82 27-120☼
2,4,6-Trichlorophenol <0.210 1.81 1.340 mg/Kg 74 24-122☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
67
MS MS
Qualifier Limits%Recovery
562-Fluorophenol (Surr)10 -120
58Nitrobenzene-d5 (Surr)27 -120
63Phenol-d5 (Surr)10 -120
78Terphenyl-d14 (Surr)13 -120
852,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117346-A-29-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
Acenaphthene <0.0349 1.79 1.272 mg/Kg 71 19-120 2 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene <0.0317 1.79 1.207 mg/Kg 68 25-120 2 50☼
Anthracene <0.0317 1.79 1.278 mg/Kg 72 28-125 5 49☼
Benzo[a]anthracene <0.0327 1.79 1.274 mg/Kg 71 23-120 10 50☼
Benzo[a]pyrene <0.0295 1.79 1.252 mg/Kg 70 15-128 6 50☼
Benzo[b]fluoranthene <0.0306 1.79 1.223 mg/Kg 68 12-133 17 50☼
Benzo[g,h,i]perylene <0.0360 1.79 1.370 mg/Kg 77 22-120 4 50☼
Benzo[k]fluoranthene <0.0295 1.79 1.302 mg/Kg 73 28-120 6 45☼
Bis(2-chloroethoxy)methane <0.218 1.79 1.103 mg/Kg 62 24-120 11 50☼
Bis(2-chloroethyl)ether <0.232 1.79 1.249 mg/Kg 70 22-120 10 50☼
bis (2-chloroisopropyl) ether <0.216 1.79 1.011 mg/Kg 57 20-120 9 50☼
Bis(2-ethylhexyl) phthalate <0.226 1.79 1.171 mg/Kg 66 26-120 15 50☼
4-Bromophenyl phenyl ether <0.224 1.79 1.305 mg/Kg 73 31-120 10 37☼
Butyl benzyl phthalate <0.235 1.79 1.371 mg/Kg 77 24-133 6 50☼
Carbazole <0.226 1.79 1.228 mg/Kg 69 25-123 0 46☼
4-Chloroaniline <0.248 1.79 1.151 mg/Kg 64 26-120 3 50☼
4-Chloro-3-methylphenol <0.183 1.79 1.297 mg/Kg 73 21-120 2 49☼
2-Chloronaphthalene <0.228 1.79 1.225 mg/Kg 69 24-120 1 50☼
2-Chlorophenol <0.208 1.79 1.145 mg/Kg 64 25-120 10 50☼
4-Chlorophenyl phenyl ether <0.219 1.79 1.305 mg/Kg 73 26-120 5 50☼
Chrysene <0.0404 1.79 1.306 mg/Kg 73 20-120 7 49☼
Cresols <0.123 3.57 2.249 mg/Kg 63 10-200 5 50☼
Dibenz(a,h)anthracene <0.0349 1.79 1.337 mg/Kg 75 12-128 2 50☼
Dibenzofuran <0.229 1.79 1.244 mg/Kg 70 21-120 3 50☼
1,2-Dichlorobenzene <0.207 1.79 1.115 mg/Kg 62 10-120 10 50☼
1,3-Dichlorobenzene <0.207 1.79 1.077 mg/Kg 60 10-120 9 50☼
1,4-Dichlorobenzene <0.214 1.79 1.099 mg/Kg 62 10-120 11 50☼
3,3'-Dichlorobenzidine <0.223 1.79 0.8374 mg/Kg 47 10-120 12 50☼
2,4-Dichlorophenol <0.191 1.79 1.242 mg/Kg 70 17-120 6 50☼
Diethyl phthalate <0.231 1.79 1.250 mg/Kg 70 29-122 5 45☼
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117346-A-29-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393095 Prep Batch: 392804
2,4-Dimethylphenol <0.366 1.79 1.168 mg/Kg 65 17-120 2 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Dimethyl phthalate <0.226 1.79 1.201 mg/Kg 67 30-120 3 46☼
Di-n-butyl phthalate <0.230 1.79 1.266 mg/Kg 71 29-126 4 49☼
4,6-Dinitro-2-methylphenol <0.250 3.57 0.6544 mg/Kg 18 10-134 39 50☼
2,4-Dinitrophenol <0.274 3.57 0.4990 mg/Kg 14 10-150 31 50☼
2,4-Dinitrotoluene <0.227 1.79 1.255 mg/Kg 70 24-121 5 50☼
2,6-Dinitrotoluene <0.243 1.79 1.220 mg/Kg 68 24-120 2 50☼
Di-n-octyl phthalate <0.194 1.79 1.209 mg/Kg 68 27-130 17 50☼
Fluoranthene <0.0371 1.79 1.175 mg/Kg 66 10-143 12 50☼
Fluorene <0.0317 1.79 1.249 mg/Kg 70 20-120 4 50☼
Hexachlorobenzene <0.273 1.79 1.397 mg/Kg 78 25-120 3 50☼
Hexachlorobutadiene <0.182 1.79 1.205 mg/Kg 67 10-120 8 50☼
Hexachlorocyclopentadiene <0.164 1.79 0.5628 mg/Kg 32 10-120 6 50☼
Hexachloroethane <0.198 1.79 1.105 mg/Kg 62 10-120 9 50☼
Indeno[1,2,3-cd]pyrene <0.0317 1.79 1.279 mg/Kg 72 22-121 4 50☼
Isophorone <0.205 1.79 1.082 mg/Kg 61 24-120 7 50☼
1-Methylnaphthalene <0.0306 1.79 1.201 mg/Kg 67 10-120 5 50☼
2-Methylnaphthalene <0.0284 1.79 1.209 mg/Kg 68 13-120 7 50☼
2-Methylphenol <0.236 1.79 1.146 mg/Kg 64 23-120 5 50☼
3 & 4 Methylphenol <0.222 1.79 1.103 mg/Kg 62 19-120 6 50☼
Naphthalene <0.0317 1.79 1.135 mg/Kg 64 10-120 9 50☼
2-Nitroaniline <0.226 1.79 1.244 mg/Kg 70 31-120 1 50☼
3-Nitroaniline <0.251 1.79 1.172 mg/Kg 66 31-120 5 49☼
4-Nitroaniline <0.260 1.79 1.093 mg/Kg 61 28-120 9 49☼
Nitrobenzene <0.219 1.79 1.112 mg/Kg 62 19-120 8 50☼
2-Nitrophenol <0.265 1.79 1.077 mg/Kg 60 23-120 6 50☼
4-Nitrophenol <0.417 3.57 2.373 mg/Kg 66 16-139 4 45☼
N-Nitrosodi-n-propylamine <0.212 1.79 1.058 mg/Kg 59 24-120 11 50☼
n-Nitrosodiphenylamine(as
diphenylamine)
<0.0578 1.52 1.288 mg/Kg 85 26-150 6 50☼
Pentachlorophenol <0.290 3.57 2.512 mg/Kg 70 19-145 6 50☼
Phenanthrene <0.0371 1.79 1.290 mg/Kg 72 21-122 0 50☼
Phenol <0.222 1.79 1.203 mg/Kg 67 15-120 10 50☼
Pyrene <0.0371 1.79 1.334 mg/Kg 75 20-123 2 50☼
1,2,4-Trichlorobenzene <0.198 1.79 1.161 mg/Kg 65 14-120 10 50☼
2,4,5-Trichlorophenol <0.238 1.79 1.446 mg/Kg 81 27-120 3 50☼
2,4,6-Trichlorophenol <0.210 1.79 1.300 mg/Kg 73 24-122 3 50☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
69
MSD MSD
Qualifier Limits%Recovery
622-Fluorophenol (Surr)10 -120
65Nitrobenzene-d5 (Surr)27 -120
67Phenol-d5 (Surr)10 -120
81Terphenyl-d14 (Surr)13 -120
802,4,6-Tribromophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 490-392824/1-A
Matrix: Waste Prep Type: Total/NA
Analysis Batch: 392908 Prep Batch: 392824
RL MDL
PCB-1016 <0.500 0.500 0.500 mg/Kg 12/08/16 12:37 12/08/16 23:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.5000.500 mg/Kg 12/08/16 12:37 12/08/16 23:12 1PCB-1221
<0.500 0.5000.500 mg/Kg 12/08/16 12:37 12/08/16 23:12 1PCB-1232
<0.500 0.5000.500 mg/Kg 12/08/16 12:37 12/08/16 23:12 1PCB-1242
<0.500 0.5000.500 mg/Kg 12/08/16 12:37 12/08/16 23:12 1PCB-1248
<0.500 0.5000.500 mg/Kg 12/08/16 12:37 12/08/16 23:12 1PCB-1254
<0.500 0.5000.500 mg/Kg 12/08/16 12:37 12/08/16 23:12 1PCB-1260
DCB Decachlorobiphenyl (Surr)107 p 20-150 12/08/16 23:12 1
MB MB
Surrogate
12/08/16 12:37
Dil FacPreparedAnalyzedQualifierLimits%Recovery
104 12/08/16 12:37 12/08/16 23:12 1Tetrachloro-m-xylene 19-147
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392824/2-A
Matrix: Waste Prep Type: Total/NA
Analysis Batch: 392908 Prep Batch: 392824
PCB-1248 5.00 4.778 mg/Kg 96 56-141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
DCB Decachlorobiphenyl (Surr)20 -150
Surrogate
119
LCS LCS
Qualifier Limits%Recovery
104Tetrachloro-m-xylene 19 -147
Client Sample ID: HO-2Lab Sample ID: 490-117643-24 DU
Matrix: Oil Prep Type: Total/NA
Analysis Batch: 392908 Prep Batch: 392824
PCB-1016 <2.23 <2.40 mg/Kg NC 50
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
PCB-1221 <2.23 <2.40 mg/Kg NC
PCB-1232 <2.23 <2.40 mg/Kg NC
PCB-1242 <2.23 <2.40 mg/Kg NC
PCB-1248 <2.23 <2.40 mg/Kg NC
PCB-1254 <2.23 <2.40 mg/Kg NC
PCB-1260 <2.23 <2.40 mg/Kg NC 50
DCB Decachlorobiphenyl (Surr)X 20 -150
Surrogate
0
DU DU
Qualifier Limits%Recovery
64Tetrachloro-m-xylene 19 -147
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-392796/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393176 Prep Batch: 392796
RL MDL
Arsenic <1.18 1.97 1.18 mg/Kg 12/08/16 12:08 12/08/16 19:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.984 0.9841.97 mg/Kg 12/08/16 12:08 12/08/16 19:25 1Barium
<0.0984 0.09840.984 mg/Kg 12/08/16 12:08 12/08/16 19:25 1Cadmium
<0.886 0.8860.984 mg/Kg 12/08/16 12:08 12/08/16 19:25 1Chromium
<0.492 0.4920.984 mg/Kg 12/08/16 12:08 12/08/16 19:25 1Lead
<1.08 1.081.97 mg/Kg 12/08/16 12:08 12/08/16 19:25 1Selenium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392796/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393176 Prep Batch: 392796
Arsenic 19.0 17.45 mg/Kg 92 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 762 756.6 mg/Kg 99 80-120
Cadmium 19.0 19.10 mg/Kg 100 80-120
Chromium 76.2 80.51 mg/Kg 106 80-120
Lead 19.0 17.89 mg/Kg 94 80-120
Selenium 19.0 17.31 mg/Kg 91 80-120
Client Sample ID: Matrix SpikeLab Sample ID: 320-24082-B-1-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393176 Prep Batch: 392796
Arsenic 1.50 J 19.4 19.34 mg/Kg 92 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 51.1 775 800.6 mg/Kg 97 75-125
Cadmium 0.198 J 19.4 19.48 mg/Kg 99 75-125
Chromium 11.4 77.5 87.38 mg/Kg 98 75-125
Lead 4.60 19.4 21.34 mg/Kg 86 75-125
Selenium 1.38 J 19.4 17.79 mg/Kg 85 75-125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-24082-B-1-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393176 Prep Batch: 392796
Arsenic 1.50 J 19.3 19.59 mg/Kg 94 75-125 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 51.1 774 796.9 mg/Kg 96 75-125 0 20
Cadmium 0.198 J 19.3 18.97 mg/Kg 97 75-125 3 20
Chromium 11.4 77.4 92.50 mg/Kg 105 75-125 6 20
Lead 4.60 19.3 23.79 mg/Kg 99 75-125 11 20
Selenium 1.38 J 19.3 19.03 mg/Kg 91 75-125 7 20
Client Sample ID: Method BlankLab Sample ID: MB 490-393053/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393847 Prep Batch: 393053
RL MDL
Arsenic <0.00860 ^0.0100 0.00860 mg/L 12/09/16 09:00 12/12/16 15:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-393053/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393847 Prep Batch: 393053
RL MDL
Barium <0.00500 0.0100 0.00500 mg/L 12/09/16 09:00 12/12/16 15:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000500 0.0005000.00100 mg/L 12/09/16 09:00 12/12/16 15:35 1Cadmium
<0.00300 0.003000.00500 mg/L 12/09/16 09:00 12/12/16 15:35 1Chromium
<0.00200 0.002000.00500 mg/L 12/09/16 09:00 12/12/16 15:35 1Lead
<0.00500 0.005000.0100 mg/L 12/09/16 09:00 12/12/16 15:35 1Selenium
<0.00300 0.003000.00500 mg/L 12/09/16 09:00 12/12/16 15:35 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-393053/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393847 Prep Batch: 393053
Arsenic 0.0500 0.05610 ^mg/L 112 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 2.084 mg/L 104 80-120
Cadmium 0.0500 0.04860 mg/L 97 80-120
Chromium 0.200 0.2012 mg/L 101 80-120
Lead 0.0500 0.05090 mg/L 102 80-120
Selenium 0.0500 0.05300 mg/L 106 80-120
Silver 0.0500 0.04190 mg/L 84 80-120
Client Sample ID: TMW-1Lab Sample ID: 490-117643-25 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393847 Prep Batch: 393053
Arsenic <0.00860 0.0500 0.05930 mg/L 119 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0618 2.00 2.123 mg/L 103 75-125
Cadmium <0.000500 0.0500 0.04780 mg/L 96 75-125
Chromium <0.00300 0.200 0.2005 mg/L 100 75-125
Lead <0.00200 0.0500 0.05170 mg/L 103 75-125
Selenium <0.00500 0.0500 0.05440 mg/L 109 75-125
Silver <0.00300 0.0500 0.04090 mg/L 82 75-125
Client Sample ID: TMW-1Lab Sample ID: 490-117643-25 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393847 Prep Batch: 393053
Arsenic <0.00860 0.0500 0.06240 mg/L 125 75-125 5 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0618 2.00 2.112 mg/L 103 75-125 1 20
Cadmium <0.000500 0.0500 0.04780 mg/L 96 75-125 0 20
Chromium <0.00300 0.200 0.1989 mg/L 99 75-125 1 20
Lead <0.00200 0.0500 0.05330 mg/L 107 75-125 3 20
Selenium <0.00500 0.0500 0.05270 mg/L 105 75-125 3 20
Silver <0.00300 0.0500 0.04060 mg/L 81 75-125 1 20
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-393063/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393240 Prep Batch: 393063
RL MDL
Arsenic <1.18 1.96 1.18 mg/Kg 12/09/16 09:26 12/09/16 12:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.18 1.181.96 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Arsenic
<0.982 0.9821.96 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Barium
<0.982 0.9821.96 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Barium
<0.0982 0.09820.982 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Cadmium
<0.0982 0.09820.982 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Cadmium
<0.884 0.8840.982 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Chromium
<0.884 0.8840.982 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Chromium
<0.491 0.4910.982 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Lead
<0.491 0.4910.982 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Lead
1.120 J 1.081.96 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Selenium
<1.08 1.081.96 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Selenium
<0.393 0.3930.982 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Silver
<0.393 0.3930.982 mg/Kg 12/09/16 09:26 12/09/16 12:25 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-393063/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393240 Prep Batch: 393063
Arsenic 19.4 18.33 mg/Kg 95 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 19.4 17.09 mg/Kg 88 80-120
Barium 775 755.6 mg/Kg 97 80-120
Barium 775 755.6 mg/Kg 97 80-120
Cadmium 19.4 18.53 mg/Kg 96 80-120
Cadmium 19.4 18.53 mg/Kg 96 80-120
Chromium 77.5 75.56 mg/Kg 97 80-120
Chromium 77.5 75.56 mg/Kg 97 80-120
Lead 19.4 18.47 mg/Kg 95 80-120
Lead 19.4 18.47 mg/Kg 95 80-120
Selenium 19.4 18.26 mg/Kg 94 80-120
Selenium 19.4 17.83 mg/Kg 92 80-120
Silver 19.4 16.88 mg/Kg 87 80-120
Silver 19.4 16.88 mg/Kg 87 80-120
Client Sample ID: Matrix SpikeLab Sample ID: 490-116866-B-2-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393240 Prep Batch: 393063
Arsenic 3.27 22.9 24.19 mg/Kg 91 75-125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 3.01 22.9 23.27 mg/Kg 88 75-125☼
Barium 17.0 917 900.4 mg/Kg 96 75-125☼
Barium 17.0 917 900.4 mg/Kg 96 75-125☼
Cadmium 0.165 J 22.9 21.55 mg/Kg 93 75-125☼
Cadmium 0.165 J 22.9 21.55 mg/Kg 93 75-125☼
Chromium 6.02 91.7 96.64 mg/Kg 99 75-125☼
Chromium 6.02 91.7 96.64 mg/Kg 99 75-125☼
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-116866-B-2-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393240 Prep Batch: 393063
Lead 15.5 22.9 34.64 mg/Kg 83 75-125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Lead 15.5 22.9 34.64 mg/Kg 83 75-125☼
Selenium 1.74 J B 22.9 22.68 mg/Kg 91 75-125☼
Selenium <1.29 22.9 22.19 mg/Kg 97 75-125☼
Silver <0.470 22.9 19.83 mg/Kg 86 75-125☼
Silver <0.470 22.9 19.83 mg/Kg 86 75-125☼
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-116866-B-2-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393240 Prep Batch: 393063
Arsenic 3.27 23.0 26.69 mg/Kg 102 75-125 10 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 3.01 23.0 24.81 mg/Kg 95 75-125 6 20☼
Barium 17.0 919 906.2 mg/Kg 97 75-125 1 20☼
Barium 17.0 919 906.2 mg/Kg 97 75-125 1 20☼
Cadmium 0.165 J 23.0 21.62 mg/Kg 93 75-125 0 20☼
Cadmium 0.165 J 23.0 21.62 mg/Kg 93 75-125 0 20☼
Chromium 6.02 91.9 97.22 mg/Kg 99 75-125 1 20☼
Chromium 6.02 91.9 97.22 mg/Kg 99 75-125 1 20☼
Lead 15.5 23.0 36.66 mg/Kg 92 75-125 6 20☼
Lead 15.5 23.0 36.66 mg/Kg 92 75-125 6 20☼
Selenium 1.74 J B 23.0 22.81 mg/Kg 92 75-125 1 20☼
Selenium <1.29 23.0 22.31 mg/Kg 97 75-125 1 20☼
Silver <0.470 23.0 19.96 mg/Kg 87 75-125 1 20☼
Silver <0.470 23.0 19.96 mg/Kg 87 75-125 1 20☼
Client Sample ID: Method BlankLab Sample ID: MB 490-393258/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393435 Prep Batch: 393258
RL MDL
Silver <0.402 1.00 0.402 mg/Kg 12/09/16 15:11 12/10/16 02:56 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-393258/25-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393435 Prep Batch: 393258
Silver 19.7 20.53 mg/Kg 104 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-117730-A-5-C MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393435 Prep Batch: 393258
Silver <0.413 F1 20.6 13.73 F1 mg/Kg 67 75-125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117730-A-5-D MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393435 Prep Batch: 393258
Silver <0.413 F1 19.8 15.65 mg/Kg 79 75-125 13 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-393746/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393880 Prep Batch: 393746
RL MDL
Lead <0.200 0.501 0.200 mg/Kg 12/12/16 16:50 12/13/16 00:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-393746/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393880 Prep Batch: 393746
Lead 19.4 17.94 mg/Kg 92 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-117525-A-1-N MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393880 Prep Batch: 393746
Lead 54.0 20.3 69.76 mg/Kg 78 75-125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117525-A-1-O MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393880 Prep Batch: 393746
Lead 54.0 20.1 72.88 mg/Kg 94 75-125 4 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-392663/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393156 Prep Batch: 392663
RL MDL
Mercury <0.000100 0.000200 0.000100 mg/L 12/08/16 09:10 12/08/16 16:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392663/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393156 Prep Batch: 392663
Mercury 0.00100 0.001046 mg/L 105 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392663/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393156 Prep Batch: 392663
Mercury 0.00100 0.001049 mg/L 105 80-120 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-117449-D-1-D MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393156 Prep Batch: 392663
Mercury <0.000100 0.00100 0.001050 mg/L 105 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117449-D-1-E MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 393156 Prep Batch: 392663
Mercury <0.000100 0.00100 0.001070 mg/L 107 75-125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-392794/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393123 Prep Batch: 392794
RL MDL
Mercury <0.0288 0.0960 0.0288 mg/Kg 12/08/16 12:01 12/09/16 08:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-392794/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393123 Prep Batch: 392794
Mercury 0.165 0.1593 mg/Kg 97 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-392794/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393123 Prep Batch: 392794
Mercury 0.168 0.1576 mg/Kg 94 80-120 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 560-65333-B-1-F MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393123 Prep Batch: 392794
Mercury <0.0301 0.168 0.1664 mg/Kg 99 80-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method: 7471B - Mercury (CVAA) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 560-65333-B-1-G MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393123 Prep Batch: 392794
Mercury <0.0301 0.161 0.1524 mg/Kg 94 80-120 9 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 490-393035/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393480 Prep Batch: 393035
RL MDL
Mercury <0.0293 0.0977 0.0293 mg/Kg 12/09/16 08:38 12/09/16 15:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-393035/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393602 Prep Batch: 393035
Mercury 0.160 0.1586 mg/Kg 99 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-393035/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393602 Prep Batch: 393035
Mercury 0.167 0.1690 mg/Kg 101 80-120 6 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-117137-B-3-C MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393480 Prep Batch: 393035
Mercury <0.0383 0.220 0.1858 mg/Kg 85 80-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-117137-B-3-D MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 393480 Prep Batch: 393035
Mercury <0.0383 0.222 0.1958 mg/Kg 88 80-120 5 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: Moisture - Percent Moisture
Client Sample ID: SB-5 (0.5-1.5)Lab Sample ID: 490-117643-9 DU
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 392752
Percent Solids 81.1 76.9 %5 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
GC/MS VOA
Analysis Batch: 392730
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260B 392807490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-2 SB-1 (3-4)Total/NA
Soil 8260B 392807490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-4 SB-2 (3-4)Total/NA
Soil 8260B 392807490-117643-5 SB-3 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-6 SB-3 (3-4)Total/NA
Soil 8260B 392807490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-8 SB-4 (3-4)Total/NA
Soil 8260B 392807490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-10 SB-5 (3-4)Total/NA
Soil 8260B 392807490-117643-11 SB-6 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-12 SB-6 (3-4)Total/NA
Solid 8260BMB 490-392730/8 Method Blank Total/NA
Solid 8260BLCS 490-392730/4 Lab Control Sample Total/NA
Solid 8260BLCSD 490-392730/5 Lab Control Sample Dup Total/NA
Prep Batch: 392807
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 5035490-117643-2 SB-1 (3-4)Total/NA
Soil 5035490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil 5035490-117643-4 SB-2 (3-4)Total/NA
Soil 5035490-117643-5 SB-3 (0.5-1.5)Total/NA
Soil 5035490-117643-6 SB-3 (3-4)Total/NA
Soil 5035490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil 5035490-117643-8 SB-4 (3-4)Total/NA
Soil 5035490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil 5035490-117643-10 SB-5 (3-4)Total/NA
Soil 5035490-117643-11 SB-6 (0.5-1.5)Total/NA
Soil 5035490-117643-12 SB-6 (3-4)Total/NA
Soil 5035490-117643-13 SB-7 (0.5-1.5)Total/NA
Soil 5035490-117643-14 SB-7 (3-4)Total/NA
Soil 5035490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 5035490-117643-16 SB-8 (3-4)Total/NA
Soil 5035490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 5035490-117643-18 SB-9 (3-4)Total/NA
Soil 5035490-117643-19 DUP-1 (0.5-1.5)Total/NA
Soil 5035490-117643-20 DUP-1 (3-4)Total/NA
Analysis Batch: 392810
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-117643-25 TMW-1 Total/NA
Water 8260BMB 490-392810/7 Method Blank Total/NA
Water 8260BLCS 490-392810/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-392810/4 Lab Control Sample Dup Total/NA
Water 8260B490-117167-B-1 MS Matrix Spike Total/NA
Water 8260B490-117167-B-1 MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 392895
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260B 392807490-117643-13 SB-7 (0.5-1.5)Total/NA
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QC Association Summary
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
GC/MS VOA (Continued)
Analysis Batch: 392895 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260B 392807490-117643-14 SB-7 (3-4)Total/NA
Soil 8260B 392807490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-16 SB-8 (3-4)Total/NA
Soil 8260B 392807490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-18 SB-9 (3-4)Total/NA
Soil 8260B 392807490-117643-19 DUP-1 (0.5-1.5)Total/NA
Soil 8260B 392807490-117643-20 DUP-1 (3-4)Total/NA
Solid 8260BMB 490-392895/10 Method Blank Total/NA
Solid 8260BLCS 490-392895/4 Lab Control Sample Total/NA
Solid 8260BLCSD 490-392895/5 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 392749
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C490-117643-25 TMW-1 Total/NA
Water 3510CMB 490-392749/1-A Method Blank Total/NA
Water 3510CLCS 490-392749/2-A Lab Control Sample Total/NA
Water 3510CLCSD 490-392749/3-A Lab Control Sample Dup Total/NA
Prep Batch: 392774
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3550C490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 3550C490-117643-2 SB-1 (3-4)Total/NA
Soil 3550C490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil 3550C490-117643-4 SB-2 (3-4)Total/NA
Soil 3550C490-117643-5 SB-3 (0.5-1.5)Total/NA
Soil 3550C490-117643-6 SB-3 (3-4)Total/NA
Soil 3550C490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil 3550C490-117643-8 SB-4 (3-4)Total/NA
Solid 3550CMB 490-392774/1-A Method Blank Total/NA
Solid 3550CLCS 490-392774/2-A Lab Control Sample Total/NA
Solid 3550C490-117419-D-11-B MS Matrix Spike Total/NA
Solid 3550C490-117419-D-11-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 392804
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3550C490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil 3550C490-117643-10 SB-5 (3-4)Total/NA
Soil 3550C490-117643-11 SB-6 (0.5-1.5)Total/NA
Soil 3550C490-117643-12 SB-6 (3-4)Total/NA
Soil 3550C490-117643-13 SB-7 (0.5-1.5)Total/NA
Soil 3550C490-117643-14 SB-7 (3-4)Total/NA
Soil 3550C490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 3550C490-117643-16 SB-8 (3-4)Total/NA
Soil 3550C490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 3550C490-117643-18 SB-9 (3-4)Total/NA
Solid 3550CMB 490-392804/1-A Method Blank Total/NA
Solid 3550CLCS 490-392804/2-A Lab Control Sample Total/NA
Solid 3550C490-117346-A-29-E MS Matrix Spike Total/NA
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TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
GC/MS Semi VOA (Continued)
Prep Batch: 392804 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C490-117346-A-29-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 392931
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 392749490-117643-25 TMW-1 Total/NA
Water 8270D 392749MB 490-392749/1-A Method Blank Total/NA
Water 8270D 392749LCS 490-392749/2-A Lab Control Sample Total/NA
Water 8270D 392749LCSD 490-392749/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 393095
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270D 392804490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil 8270D 392804490-117643-10 SB-5 (3-4)Total/NA
Soil 8270D 392804490-117643-11 SB-6 (0.5-1.5)Total/NA
Soil 8270D 392804490-117643-12 SB-6 (3-4)Total/NA
Soil 8270D 392804490-117643-13 SB-7 (0.5-1.5)Total/NA
Soil 8270D 392804490-117643-14 SB-7 (3-4)Total/NA
Soil 8270D 392804490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 8270D 392804490-117643-16 SB-8 (3-4)Total/NA
Soil 8270D 392804490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 8270D 392804490-117643-18 SB-9 (3-4)Total/NA
Solid 8270D 392804MB 490-392804/1-A Method Blank Total/NA
Solid 8270D 392804LCS 490-392804/2-A Lab Control Sample Total/NA
Solid 8270D 392804490-117346-A-29-E MS Matrix Spike Total/NA
Solid 8270D 392804490-117346-A-29-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 393298
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270D 392774490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 8270D 392774490-117643-2 SB-1 (3-4)Total/NA
Soil 8270D 392774490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil 8270D 392774490-117643-4 SB-2 (3-4)Total/NA
Soil 8270D 392774490-117643-5 SB-3 (0.5-1.5)Total/NA
Soil 8270D 392774490-117643-6 SB-3 (3-4)Total/NA
Soil 8270D 392774490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil 8270D 392774490-117643-8 SB-4 (3-4)Total/NA
Solid 8270D 392774MB 490-392774/1-A Method Blank Total/NA
Solid 8270D 392774LCS 490-392774/2-A Lab Control Sample Total/NA
Solid 8270D 392774490-117419-D-11-B MS Matrix Spike Total/NA
Solid 8270D 392774490-117419-D-11-C MSD Matrix Spike Duplicate Total/NA
GC Semi VOA
Prep Batch: 392824
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Oil 3580A490-117643-23 HO-1 Total/NA
Oil 3580A490-117643-24 HO-2 Total/NA
Waste 3580AMB 490-392824/1-A Method Blank Total/NA
Waste 3580ALCS 490-392824/2-A Lab Control Sample Total/NA
Oil 3580A490-117643-24 DU HO-2 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
GC Semi VOA (Continued)
Analysis Batch: 392908
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Oil 8082A 392824490-117643-23 HO-1 Total/NA
Oil 8082A 392824490-117643-24 HO-2 Total/NA
Waste 8082A 392824MB 490-392824/1-A Method Blank Total/NA
Waste 8082A 392824LCS 490-392824/2-A Lab Control Sample Total/NA
Oil 8082A 392824490-117643-24 DU HO-2 Total/NA
Metals
Prep Batch: 392663
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-117643-25 TMW-1 Total/NA
Water 7470AMB 490-392663/1-A Method Blank Total/NA
Water 7470ALCS 490-392663/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-392663/3-A Lab Control Sample Dup Total/NA
Water 7470A490-117449-D-1-D MS Matrix Spike Total/NA
Water 7470A490-117449-D-1-E MSD Matrix Spike Duplicate Total/NA
Prep Batch: 392794
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 7471B490-117643-2 SB-1 (3-4)Total/NA
Soil 7471B490-117643-3 SB-2 (0.5-1.5)Total/NA
Solid 7471BMB 490-392794/1-A Method Blank Total/NA
Solid 7471BLCS 490-392794/2-A Lab Control Sample Total/NA
Solid 7471BLCSD 490-392794/3-A Lab Control Sample Dup Total/NA
Solid 7471B560-65333-B-1-F MS Matrix Spike Total/NA
Solid 7471B560-65333-B-1-G MSD Matrix Spike Duplicate Total/NA
Prep Batch: 392796
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3051A490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 3051A490-117643-2 SB-1 (3-4)Total/NA
Soil 3051A490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil 3051A490-117643-4 SB-2 (3-4)Total/NA
Soil 3051A490-117643-5 SB-3 (0.5-1.5)Total/NA
Solid 3051AMB 490-392796/1-A Method Blank Total/NA
Solid 3051ALCS 490-392796/2-A Lab Control Sample Total/NA
Solid 3051A320-24082-B-1-B MS Matrix Spike Total/NA
Solid 3051A320-24082-B-1-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 393035
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B490-117643-4 SB-2 (3-4)Total/NA
Soil 7471B490-117643-5 SB-3 (0.5-1.5)Total/NA
Soil 7471B490-117643-6 SB-3 (3-4)Total/NA
Soil 7471B490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil 7471B490-117643-8 SB-4 (3-4)Total/NA
Soil 7471B490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil 7471B490-117643-10 SB-5 (3-4)Total/NA
Soil 7471B490-117643-11 SB-6 (0.5-1.5)Total/NA
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TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Metals (Continued)
Prep Batch: 393035 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B490-117643-12 SB-6 (3-4)Total/NA
Soil 7471B490-117643-13 SB-7 (0.5-1.5)Total/NA
Soil 7471B490-117643-14 SB-7 (3-4)Total/NA
Soil 7471B490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 7471B490-117643-16 SB-8 (3-4)Total/NA
Soil 7471B490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 7471B490-117643-18 SB-9 (3-4)Total/NA
Solid 7471BMB 490-393035/1-A Method Blank Total/NA
Solid 7471BLCS 490-393035/2-A Lab Control Sample Total/NA
Solid 7471BLCSD 490-393035/3-A Lab Control Sample Dup Total/NA
Solid 7471B490-117137-B-3-C MS Matrix Spike Total/NA
Solid 7471B490-117137-B-3-D MSD Matrix Spike Duplicate Total/NA
Prep Batch: 393053
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-117643-25 TMW-1 Total/NA
Water 3010AMB 490-393053/1-A Method Blank Total/NA
Water 3010ALCS 490-393053/2-A Lab Control Sample Total/NA
Water 3010A490-117643-25 MS TMW-1 Total/NA
Water 3010A490-117643-25 MSD TMW-1 Total/NA
Prep Batch: 393063
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3051A490-117643-6 SB-3 (3-4)Total/NA
Soil 3051A490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil 3051A490-117643-8 SB-4 (3-4)Total/NA
Soil 3051A490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil 3051A490-117643-10 SB-5 (3-4)Total/NA
Soil 3051A490-117643-11 SB-6 (0.5-1.5)Total/NA
Soil 3051A490-117643-12 SB-6 (3-4)Total/NA
Soil 3051A490-117643-13 SB-7 (0.5-1.5)Total/NA
Soil 3051A490-117643-14 SB-7 (3-4)Total/NA
Soil 3051A490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 3051A490-117643-16 SB-8 (3-4)Total/NA
Soil 3051A490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 3051A490-117643-18 SB-9 (3-4)Total/NA
Solid 3051AMB 490-393063/1-A Method Blank Total/NA
Solid 3051ALCS 490-393063/2-A Lab Control Sample Total/NA
Solid 3051A490-116866-B-2-E MS Matrix Spike Total/NA
Solid 3051A490-116866-B-2-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 393123
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B 392794490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 7471B 392794490-117643-2 SB-1 (3-4)Total/NA
Soil 7471B 392794490-117643-3 SB-2 (0.5-1.5)Total/NA
Solid 7471B 392794MB 490-392794/1-A Method Blank Total/NA
Solid 7471B 392794LCS 490-392794/2-A Lab Control Sample Total/NA
Solid 7471B 392794LCSD 490-392794/3-A Lab Control Sample Dup Total/NA
Solid 7471B 392794560-65333-B-1-F MS Matrix Spike Total/NA
Solid 7471B 392794560-65333-B-1-G MSD Matrix Spike Duplicate Total/NA
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TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Analysis Batch: 393156
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 392663490-117643-25 TMW-1 Total/NA
Water 7470A 392663MB 490-392663/1-A Method Blank Total/NA
Water 7470A 392663LCS 490-392663/2-A Lab Control Sample Total/NA
Water 7470A 392663LCSD 490-392663/3-A Lab Control Sample Dup Total/NA
Water 7470A 392663490-117449-D-1-D MS Matrix Spike Total/NA
Water 7470A 392663490-117449-D-1-E MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 393176
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 392796490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 6010D 392796490-117643-2 SB-1 (3-4)Total/NA
Soil 6010D 392796490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil 6010D 392796490-117643-4 SB-2 (3-4)Total/NA
Soil 6010D 392796490-117643-5 SB-3 (0.5-1.5)Total/NA
Solid 6010D 392796MB 490-392796/1-A Method Blank Total/NA
Solid 6010D 392796LCS 490-392796/2-A Lab Control Sample Total/NA
Solid 6010D 392796320-24082-B-1-B MS Matrix Spike Total/NA
Solid 6010D 392796320-24082-B-1-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 393240
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 393063MB 490-393063/1-A Method Blank Total/NA
Solid 6010D 393063LCS 490-393063/2-A Lab Control Sample Total/NA
Solid 6010D 393063490-116866-B-2-E MS Matrix Spike Total/NA
Solid 6010D 393063490-116866-B-2-F MSD Matrix Spike Duplicate Total/NA
Prep Batch: 393258
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3051A490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 3051A490-117643-2 SB-1 (3-4)Total/NA
Soil 3051A490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil 3051A490-117643-4 SB-2 (3-4)Total/NA
Soil 3051A490-117643-5 SB-3 (0.5-1.5)Total/NA
Solid 3051AMB 490-393258/1-A Method Blank Total/NA
Solid 3051ALCS 490-393258/25-A Lab Control Sample Total/NA
Solid 3051A490-117730-A-5-C MS Matrix Spike Total/NA
Solid 3051A490-117730-A-5-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 393435
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 393258490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil 6010D 393258490-117643-2 SB-1 (3-4)Total/NA
Soil 6010D 393258490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil 6010D 393258490-117643-4 SB-2 (3-4)Total/NA
Soil 6010D 393258490-117643-5 SB-3 (0.5-1.5)Total/NA
Solid 6010D 393258MB 490-393258/1-A Method Blank Total/NA
Solid 6010D 393258LCS 490-393258/25-A Lab Control Sample Total/NA
Solid 6010D 393258490-117730-A-5-C MS Matrix Spike Total/NA
Solid 6010D 393258490-117730-A-5-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 393446
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 393063490-117643-6 SB-3 (3-4)Total/NA
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QC Association Summary
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Metals (Continued)
Analysis Batch: 393446 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 393063490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil 6010D 393063490-117643-8 SB-4 (3-4)Total/NA
Soil 6010D 393063490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil 6010D 393063490-117643-10 SB-5 (3-4)Total/NA
Soil 6010D 393063490-117643-11 SB-6 (0.5-1.5)Total/NA
Soil 6010D 393063490-117643-12 SB-6 (3-4)Total/NA
Soil 6010D 393063490-117643-13 SB-7 (0.5-1.5)Total/NA
Soil 6010D 393063490-117643-14 SB-7 (3-4)Total/NA
Soil 6010D 393063490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 6010D 393063490-117643-16 SB-8 (3-4)Total/NA
Soil 6010D 393063490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 6010D 393063490-117643-18 SB-9 (3-4)Total/NA
Solid 6010D 393063MB 490-393063/1-A Method Blank Total/NA
Solid 6010D 393063LCS 490-393063/2-A Lab Control Sample Total/NA
Solid 6010D 393063490-116866-B-2-E MS Matrix Spike Total/NA
Solid 6010D 393063490-116866-B-2-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 393480
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B 393035490-117643-4 SB-2 (3-4)Total/NA
Soil 7471B 393035490-117643-5 SB-3 (0.5-1.5)Total/NA
Soil 7471B 393035490-117643-6 SB-3 (3-4)Total/NA
Soil 7471B 393035490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil 7471B 393035490-117643-8 SB-4 (3-4)Total/NA
Soil 7471B 393035490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil 7471B 393035490-117643-10 SB-5 (3-4)Total/NA
Soil 7471B 393035490-117643-11 SB-6 (0.5-1.5)Total/NA
Soil 7471B 393035490-117643-12 SB-6 (3-4)Total/NA
Soil 7471B 393035490-117643-13 SB-7 (0.5-1.5)Total/NA
Soil 7471B 393035490-117643-14 SB-7 (3-4)Total/NA
Soil 7471B 393035490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 7471B 393035490-117643-16 SB-8 (3-4)Total/NA
Soil 7471B 393035490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 7471B 393035490-117643-18 SB-9 (3-4)Total/NA
Solid 7471B 393035MB 490-393035/1-A Method Blank Total/NA
Solid 7471B 393035490-117137-B-3-C MS Matrix Spike Total/NA
Solid 7471B 393035490-117137-B-3-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 393602
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 393035LCS 490-393035/2-A Lab Control Sample Total/NA
Solid 7471B 393035LCSD 490-393035/3-A Lab Control Sample Dup Total/NA
Prep Batch: 393746
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3051A490-117643-21 DL-1 Total/NA
Soil 3051A490-117643-22 DL-2 Total/NA
Solid 3051AMB 490-393746/1-A Method Blank Total/NA
Solid 3051ALCS 490-393746/2-A Lab Control Sample Total/NA
Solid 3051A490-117525-A-1-N MS Matrix Spike Total/NA
Solid 3051A490-117525-A-1-O MSD Matrix Spike Duplicate Total/NA
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TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Analysis Batch: 393752
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 393063490-117643-14 SB-7 (3-4)Total/NA
Soil 6010D 393063490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil 6010D 393063490-117643-16 SB-8 (3-4)Total/NA
Soil 6010D 393063490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil 6010D 393063490-117643-18 SB-9 (3-4)Total/NA
Analysis Batch: 393847
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 393053490-117643-25 TMW-1 Total/NA
Water 6010D 393053MB 490-393053/1-A Method Blank Total/NA
Water 6010D 393053LCS 490-393053/2-A Lab Control Sample Total/NA
Water 6010D 393053490-117643-25 MS TMW-1 Total/NA
Water 6010D 393053490-117643-25 MSD TMW-1 Total/NA
Analysis Batch: 393880
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6020B 393746490-117643-21 DL-1 Total/NA
Soil 6020B 393746490-117643-22 DL-2 Total/NA
Solid 6020B 393746MB 490-393746/1-A Method Blank Total/NA
Solid 6020B 393746LCS 490-393746/2-A Lab Control Sample Total/NA
Solid 6020B 393746490-117525-A-1-N MS Matrix Spike Total/NA
Solid 6020B 393746490-117525-A-1-O MSD Matrix Spike Duplicate Total/NA
General Chemistry
Analysis Batch: 392752
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture490-117643-1 SB-1 (0.5-1.5)Total/NA
Soil Moisture490-117643-2 SB-1 (3-4)Total/NA
Soil Moisture490-117643-3 SB-2 (0.5-1.5)Total/NA
Soil Moisture490-117643-4 SB-2 (3-4)Total/NA
Soil Moisture490-117643-5 SB-3 (0.5-1.5)Total/NA
Soil Moisture490-117643-6 SB-3 (3-4)Total/NA
Soil Moisture490-117643-7 SB-4 (0.5-1.5)Total/NA
Soil Moisture490-117643-8 SB-4 (3-4)Total/NA
Soil Moisture490-117643-9 SB-5 (0.5-1.5)Total/NA
Soil Moisture490-117643-10 SB-5 (3-4)Total/NA
Soil Moisture490-117643-11 SB-6 (0.5-1.5)Total/NA
Soil Moisture490-117643-12 SB-6 (3-4)Total/NA
Soil Moisture490-117643-13 SB-7 (0.5-1.5)Total/NA
Soil Moisture490-117643-14 SB-7 (3-4)Total/NA
Soil Moisture490-117643-15 SB-8 (0.5-1.5)Total/NA
Soil Moisture490-117643-16 SB-8 (3-4)Total/NA
Soil Moisture490-117643-17 SB-9 (0.5-1.5)Total/NA
Soil Moisture490-117643-18 SB-9 (3-4)Total/NA
Soil Moisture490-117643-19 DUP-1 (0.5-1.5)Total/NA
Soil Moisture490-117643-20 DUP-1 (3-4)Total/NA
Soil Moisture490-117643-21 DL-1 Total/NA
Soil Moisture490-117643-22 DL-2 Total/NA
Solid Moisture490-117602-G-19 MS Matrix Spike Total/NA
Solid Moisture490-117602-G-19 MSD Matrix Spike Duplicate Total/NA
Soil Moisture490-117643-9 DU SB-5 (0.5-1.5)Total/NA
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Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Client Sample ID: SB-1 (0.5-1.5)Lab Sample ID: 490-117643-1
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 08:55 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.619 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 21:09 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392774 12/08/16 11:04 MNM TAL NSHTotal/NA 30.77 g 1.00 mL
Analysis 8270D 1 393298 12/09/16 20:25 T1C TAL NSHTotal/NA
Prep 3051A 392796 12/08/16 12:08 JSF TAL NSHTotal/NA .511 g 100 mL
Analysis 6010D 1 393176 12/08/16 21:37 RDF TAL NSHTotal/NA
Prep 3051A 393258 12/09/16 15:11 PG1 TAL NSHTotal/NA 0.501 g 100 mL
Analysis 6010D 1 393435 12/10/16 05:17 KKK TAL NSHTotal/NA
Prep 7471B 392794 12/08/16 12:01 LCS TAL NSHTotal/NA 0.625 g 100 mL
Analysis 7471B 1 393123 12/09/16 09:05 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-1 (3-4)Lab Sample ID: 490-117643-2
Matrix: SoilDate Collected: 12/06/16 09:55
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 08:55 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.669 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 20:40 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392774 12/08/16 11:04 MNM TAL NSHTotal/NA 30.16 g 1.00 mL
Analysis 8270D 1 393298 12/09/16 20:43 T1C TAL NSHTotal/NA
Prep 3051A 392796 12/08/16 12:08 JSF TAL NSHTotal/NA .499 g 100 mL
Analysis 6010D 1 393176 12/08/16 21:43 RDF TAL NSHTotal/NA
Prep 3051A 393258 12/09/16 15:11 PG1 TAL NSHTotal/NA 0.513 g 100 mL
Analysis 6010D 1 393435 12/10/16 05:22 KKK TAL NSHTotal/NA
Prep 7471B 392794 12/08/16 12:01 LCS TAL NSHTotal/NA 0.622 g 100 mL
Analysis 7471B 1 393123 12/09/16 09:07 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-2 (0.5-1.5)Lab Sample ID: 490-117643-3
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:00 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.849 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 20:10 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392774 12/08/16 11:04 MNM TAL NSHTotal/NA 30.34 g 1.00 mL
Analysis 8270D 1 393298 12/09/16 21:02 T1C TAL NSHTotal/NA
Prep 3051A 392796 12/08/16 12:08 JSF TAL NSHTotal/NA .517 g 100 mL
Analysis 6010D 1 393176 12/08/16 21:48 RDF TAL NSHTotal/NA
Prep 3051A 393258 12/09/16 15:11 PG1 TAL NSHTotal/NA 0.504 g 100 mL
Analysis 6010D 1 393435 12/10/16 05:27 KKK TAL NSHTotal/NA
Prep 7471B 392794 12/08/16 12:01 LCS TAL NSHTotal/NA 0.610 g 100 mL
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Client Sample ID: SB-2 (0.5-1.5)Lab Sample ID: 490-117643-3
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Analysis 7471B LCS12/09/16 09:101 TAL NSH393123
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-2 (3-4)Lab Sample ID: 490-117643-4
Matrix: SoilDate Collected: 12/06/16 12:00
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:00 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.017 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 19:41 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392774 12/08/16 11:04 MNM TAL NSHTotal/NA 30.13 g 1.00 mL
Analysis 8270D 1 393298 12/09/16 21:21 T1C TAL NSHTotal/NA
Prep 3051A 392796 12/08/16 12:08 JSF TAL NSHTotal/NA .518 g 100 mL
Analysis 6010D 1 393176 12/08/16 21:53 RDF TAL NSHTotal/NA
Prep 3051A 393258 12/09/16 15:11 PG1 TAL NSHTotal/NA 0.507 g 100 mL
Analysis 6010D 1 393435 12/10/16 05:32 KKK TAL NSHTotal/NA
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.624 g 100 mL
Analysis 7471B 1 393480 12/09/16 15:43 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-3 (0.5-1.5)Lab Sample ID: 490-117643-5
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:05 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.158 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 19:11 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392774 12/08/16 11:04 MNM TAL NSHTotal/NA 30.05 g 1.00 mL
Analysis 8270D 1 393298 12/09/16 21:39 T1C TAL NSHTotal/NA
Prep 3051A 392796 12/08/16 12:08 JSF TAL NSHTotal/NA .501 g 100 mL
Analysis 6010D 1 393176 12/08/16 21:58 RDF TAL NSHTotal/NA
Prep 3051A 393258 12/09/16 15:11 PG1 TAL NSHTotal/NA 0.504 g 100 mL
Analysis 6010D 1 393435 12/10/16 05:38 KKK TAL NSHTotal/NA
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.624 g 100 mL
Analysis 7471B 1 393480 12/09/16 15:46 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-3 (3-4)Lab Sample ID: 490-117643-6
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:05 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.327 g 5.0 mL
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Client Sample ID: SB-3 (3-4)Lab Sample ID: 490-117643-6
Matrix: SoilDate Collected: 12/06/16 12:05
Date Received: 12/07/16 09:40
Analysis 8260B TSC12/08/16 18:421 TAL NSH392730
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 g 5 mL
Prep 3550C 392774 12/08/16 11:04 MNM TAL NSHTotal/NA 30.25 g 1.00 mL
Analysis 8270D 1 393298 12/09/16 21:58 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.518 g 100 mL
Analysis 6010D 1 393446 12/09/16 13:06 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.620 g 100 mL
Analysis 7471B 1 393480 12/09/16 15:49 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-4 (0.5-1.5)Lab Sample ID: 490-117643-7
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:40 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.593 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 18:12 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392774 12/08/16 11:04 MNM TAL NSHTotal/NA 30.01 g 1.00 mL
Analysis 8270D 1 393298 12/09/16 22:16 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.499 g 100 mL
Analysis 6010D 1 393446 12/09/16 14:13 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.613 g 100 mL
Analysis 7471B 1 393480 12/09/16 15:52 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-4 (3-4)Lab Sample ID: 490-117643-8
Matrix: SoilDate Collected: 12/06/16 12:40
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:40 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.563 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 17:43 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392774 12/08/16 11:04 MNM TAL NSHTotal/NA 30.42 g 1.00 mL
Analysis 8270D 1 393298 12/09/16 22:35 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.495 g 100 mL
Analysis 6010D 1 393446 12/09/16 14:29 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.602 g 100 mL
Analysis 7471B 1 393480 12/09/16 15:54 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Client Sample ID: SB-5 (0.5-1.5)Lab Sample ID: 490-117643-9
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:15 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.392 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 17:14 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.29 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 13:12 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.522 g 100 mL
Analysis 6010D 1 393446 12/09/16 14:34 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.605 g 100 mL
Analysis 7471B 1 393480 12/09/16 15:57 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-5 (3-4)Lab Sample ID: 490-117643-10
Matrix: SoilDate Collected: 12/06/16 12:15
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:15 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.154 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 16:44 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.65 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 13:30 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.503 g 100 mL
Analysis 6010D 1 393446 12/09/16 14:40 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.625 g 100 mL
Analysis 7471B 1 393480 12/09/16 16:00 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-6 (0.5-1.5)Lab Sample ID: 490-117643-11
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:45 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.682 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 16:15 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.84 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 13:49 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.508 g 100 mL
Analysis 6010D 1 393446 12/09/16 14:45 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.595 g 100 mL
Analysis 7471B 1 393480 12/09/16 16:03 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Client Sample ID: SB-6 (3-4)Lab Sample ID: 490-117643-12
Matrix: SoilDate Collected: 12/06/16 12:45
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 11:45 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.902 g 5.0 mL
Analysis 8260B 1 392730 12/08/16 15:45 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.97 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 14:07 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.502 g 100 mL
Analysis 6010D 1 393446 12/09/16 14:50 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.608 g 100 mL
Analysis 7471B 1 393480 12/09/16 16:05 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-7 (0.5-1.5)Lab Sample ID: 490-117643-13
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 14:15 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.026 g 5.0 mL
Analysis 8260B 1 392895 12/09/16 08:27 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.48 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 14:26 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.513 g 100 mL
Analysis 6010D 1 393446 12/09/16 15:01 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.625 g 100 mL
Analysis 7471B 1 393480 12/09/16 16:08 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-7 (3-4)Lab Sample ID: 490-117643-14
Matrix: SoilDate Collected: 12/06/16 15:15
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 14:15 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.114 g 5.0 mL
Analysis 8260B 1 392895 12/09/16 07:58 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.17 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 14:45 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.504 g 100 mL
Analysis 6010D 1 393446 12/09/16 15:06 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.504 g 100 mL
Analysis 6010D 5 393752 12/12/16 12:48 KKK TAL NSHTotal/NA
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.610 g 100 mL
Analysis 7471B 1 393480 12/09/16 16:16 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
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Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Client Sample ID: SB-8 (0.5-1.5)Lab Sample ID: 490-117643-15
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 14:30 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.272 g 5.0 mL
Analysis 8260B 1 392895 12/09/16 07:28 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.28 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 15:03 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.502 g 100 mL
Analysis 6010D 1 393446 12/09/16 15:17 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.502 g 100 mL
Analysis 6010D 1 393752 12/12/16 12:53 KKK TAL NSHTotal/NA
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.625 g 100 mL
Analysis 7471B 1 393480 12/09/16 16:19 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-8 (3-4)Lab Sample ID: 490-117643-16
Matrix: SoilDate Collected: 12/06/16 15:30
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 14:30 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.814 g 5.0 mL
Analysis 8260B 1 392895 12/09/16 06:59 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.38 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 15:22 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.502 g 100 mL
Analysis 6010D 1 393446 12/09/16 15:34 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.502 g 100 mL
Analysis 6010D 1 393752 12/12/16 12:58 KKK TAL NSHTotal/NA
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.599 g 100 mL
Analysis 7471B 1 393480 12/09/16 16:22 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-9 (0.5-1.5)Lab Sample ID: 490-117643-17
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 14:50 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.011 g 5.0 mL
Analysis 8260B 1 392895 12/09/16 06:29 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.69 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 15:41 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.517 g 100 mL
Analysis 6010D 1 393446 12/09/16 15:39 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.517 g 100 mL
Analysis 6010D 1 393752 12/12/16 13:03 KKK TAL NSHTotal/NA
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.625 g 100 mL
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Client Sample ID: SB-9 (0.5-1.5)Lab Sample ID: 490-117643-17
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Analysis 7471B LCS12/09/16 16:241 TAL NSH393480
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: SB-9 (3-4)Lab Sample ID: 490-117643-18
Matrix: SoilDate Collected: 12/06/16 15:50
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 14:50 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.2 g 5.0 mL
Analysis 8260B 1 392895 12/09/16 06:00 TSC TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 392804 12/08/16 12:11 MNM TAL NSHTotal/NA 30.15 g 1.00 mL
Analysis 8270D 1 393095 12/09/16 15:59 T1C TAL NSHTotal/NA
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.524 g 100 mL
Analysis 6010D 1 393446 12/09/16 15:44 KKK TAL NSHTotal/NA 1.0 mL 1.0 mL
Prep 3051A 393063 12/09/16 09:26 PG1 TAL NSHTotal/NA 0.524 g 100 mL
Analysis 6010D 1 393752 12/12/16 13:09 KKK TAL NSHTotal/NA
Prep 7471B 393035 12/09/16 08:38 LCS TAL NSHTotal/NA 0.601 g 100 mL
Analysis 7471B 1 393480 12/09/16 16:27 LCS TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 10:50 BAA TAL NSHTotal/NA
Client Sample ID: DUP-1 (0.5-1.5)Lab Sample ID: 490-117643-19
Matrix: SoilDate Collected: 12/06/16 01:01
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 00:01 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.942 g 5.0 mL
Analysis 8260B 1 392895 12/09/16 05:30 TSC TAL NSHTotal/NA 5 g 5 mL
Analysis Moisture 1 392752 12/08/16 11:20 BAA TAL NSHTotal/NA
Client Sample ID: DUP-1 (3-4)Lab Sample ID: 490-117643-20
Matrix: SoilDate Collected: 12/06/16 01:01
Date Received: 12/07/16 09:40
Prep 5035 JLP12/06/16 00:01 TAL NSH392807
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.443 g 5.0 mL
Analysis 8260B 1 392895 12/09/16 05:01 TSC TAL NSHTotal/NA 5 g 5 mL
Analysis Moisture 1 392752 12/08/16 11:20 BAA TAL NSHTotal/NA
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Client Sample ID: DL-1 Lab Sample ID: 490-117643-21
Matrix: SoilDate Collected: 12/06/16 16:55
Date Received: 12/07/16 09:40
Prep 3051A PG112/12/16 16:50 TAL NSH393746
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 0.510 g 100 mL
Analysis 6020B 1 393880 12/13/16 01:20 BLG TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 11:20 BAA TAL NSHTotal/NA
Client Sample ID: DL-2 Lab Sample ID: 490-117643-22
Matrix: SoilDate Collected: 12/06/16 17:00
Date Received: 12/07/16 09:40
Prep 3051A PG112/12/16 16:50 TAL NSH393746
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 0.503 g 100 mL
Analysis 6020B 1 393880 12/13/16 01:25 BLG TAL NSHTotal/NA
Analysis Moisture 1 392752 12/08/16 11:20 BAA TAL NSHTotal/NA
Client Sample ID: HO-1 Lab Sample ID: 490-117643-23
Matrix: OilDate Collected: 12/06/16 09:30
Date Received: 12/07/16 09:40
Prep 3580A MNM12/08/16 12:37 TAL NSH392824
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.06 g 10 mL
Analysis 8082A 5 392908 12/08/16 23:42 LEG TAL NSHTotal/NA
Client Sample ID: HO-2 Lab Sample ID: 490-117643-24
Matrix: OilDate Collected: 12/06/16 09:35
Date Received: 12/07/16 09:40
Prep 3580A MNM12/08/16 12:37 TAL NSH392824
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.12 g 10 mL
Analysis 8082A 5 392908 12/08/16 23:58 LEG TAL NSHTotal/NA
Client Sample ID: TMW-1 Lab Sample ID: 490-117643-25
Matrix: WaterDate Collected: 12/06/16 11:30
Date Received: 12/07/16 09:40
Analysis 8260B AK112/08/16 19:491 TAL NSH392810
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3510C 392749 12/08/16 10:43 KB TAL NSHTotal/NA 270 mL 1 mL
Analysis 8270D 1 392931 12/08/16 20:15 T1C TAL NSHTotal/NA
Prep 3010A 393053 12/09/16 09:00 CAH TAL NSHTotal/NA 50.0 mL 50.0 mL
Analysis 6010D 1 393847 12/12/16 16:02 KKK TAL NSHTotal/NA
Prep 7470A 392663 12/08/16 09:10 LCS TAL NSHTotal/NA 30.0 mL 30.0 mL
Analysis 7470A 1 393156 12/08/16 16:48 LCS TAL NSHTotal/NA
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-117643-1Client: Hart & Hickman, PC
SDG: GSL-002Project/Site: Scottish Rite Temple
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8468082APolychlorinated Biphenyls (PCBs) by Gas Chromatography TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
SW8467471BMercury (CVAA)TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-117643-1
Project/Site: Scottish Rite Temple SDG: GSL-002
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-16 *
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:
Moisture Soil Percent Solids
TestAmerica Nashville
* Certification renewal pending - certification considered valid.
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Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-117643-1
SDG Number: GSL-002
Login Number: 117643
Question Answer Comment
Creator: McBride, Mike
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueResidual Chlorine Checked.
TestAmerica Nashville
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