14024 Edward Soil Stabilization Report 20130313

ERM NC, Inc.

8000 Corporate Center Drive
Suite 200
Charlotte, NC 28226
[phone]
[phone]
March 4, 2013

Mr. David Waggoner
Charlotte Pipe and Foundry Company
c/o Mr. Max Justice
Parker Poe Adams and Bernstein
401 South Tryon Street
Suite 3000
Charlotte, NC 28202

Subject: Stabilization of Lead Impacted Foundry Sands Report
Anne Edwards Property
Rozzelle’s Ferry Road,
Charlotte, North Carolina
Via e-mail
Dear Mr. Justice:

ERM NC, Inc (ERM) is pleased to provide Charlotte Pipe and Foundry Company
(Charlotte Pipe) with this summary report for the stabilization of lead-impacted soils
and foundry sand at the Anne Edwards property located at 10211-10311 Rozzelle’s
Ferry Road, Charlotte, North Carolina (the Site). This report summarizes the work
performed in accordance with the Voluntary Removal Action Workplan prepared by
ERM dated December 2011 as approved by North Carolina Department of
Environment and Natural Resources (NC DENR) in a letter dated August 9, 2012 . A
site location map and topographic map is presented as Figure 1.

COMPLETED SCOPE OF WORK
Health and Safety Plan
ERM developed an OSHA compliant health and safety plan (HASP) for the protection
of workers and the surrounding community at the site, compliant with EPA, OSHA,
and North Carolina regulations. ERM’s loss prevention system which consists of
behavior based health and safety practices, was implemented at the site. A summary
of the critical elements of the H&S program is provided below.
• Subsurface Utility Clearance
• Stop Work Authority
• Ambient Air Monitoring (during excavation and stabilization activities)
Full Scale Stabilization
ERM mobilized to the site on October 16, 2012 with an environmental services
subcontractor, SAEDACCO of Fort Mill, South Carolina. ERM provided one

Mr. Max Justice
4 March 2013
Page 2

environmental professional during the duration of the excavation activities to perform
dust monitoring, H&S oversight, construction quality control/quality assurance, and
confirmatory sampling activities. Site security fencing and erosion control devices
were installed around the excavation areas prior to the initiation of excavation
activities in accordance with the workplan.
The two areas of lead-impacted foundry sands identified by previous sampling and
analysis were located and staked on site by Lawrence and Associates of Monroe, NC, a
North Carolina registered land surveyor. The lead impacted areas are shown on
Figure 2.
Excavation area EH contained approximately 65 cubic yards and excavation AH
contained 431 cubic yards. The lead impacted soils were excavated using a track hoe
and transferred to two stockpiles located within a fenced area. The stockpiles were
constructed of a minimum 10-mil thick plastic under liner and top cover. Blastox 215
(solidification agent supplied by Charlotte Pipe) was mixed with the stockpiled
foundry sands/soil at a ratio of 3% by unit weight. The Blastox 215 mix ratio was
determined by J.Carpenter Environmental (Blastox 215 manufacturer’s representative)
based upon a bench scale pilot test performed by J. Carpenter Environmental from a
foundry sands/soil sample collected from the site and sample analytical data collected
from the Anne Edwards property during the 2005-2006 timeframe.
Post-excavation confirmatory samples were collected from the sidewalls and along the
base of the two excavated areas on October 19 2012 and December 10, 2012 (excavation
EH) and October 23, 2012 and December 18, 2012 (excavation AH). ERM initially
collected 15 post-excavation confirmatory samples and one duplicate quality control
sample for TCLP lead analysis between the two excavation areas. Out of the 15
confirmatory samples collected, 4 exceeded the TCLP lead remedial goal of 5
milligrams per liter (mg/L). Additional foundry sands/soils were removed from the
four areas identified by the failing TCLP samples and were subsequently added to the
stockpiles. ERM collected four additional post-excavation confirmatory samples for
TCLP lead analysis. The results of the additional confirmatory analyses indicated that
the extent of lead impacted foundry sands/soils had been excavated as the samples
indicated levels no longer exceed the TCLP levels. A summary of the excavation
confirmatory analytical results is included in Table 1. Sample location and laboratory
analytical results are summarized in Figure 3. Laboratory analytical data is presented
in Appendix A.
The Blastox 215 stabilization agent was thoroughly mixed into the stockpiled foundry
sands/soils using a backhoe at the completion of excavation activities. In order to test
the effectiveness of the stabilization process, foundry sand/soil samples were collected
from stabilized material. Based on the estimated total excavated volume of 500 cubic
yards of foundry sands requiring stabilization, approximately 6 samples were
Mr. Max Justice
4 March 2013
Page 3

collected from the excavated material for TCLP lead analysis. All 6 samples were
below the TCLP limit for lead, which is 5 mg/L. Laboratory analytical results are
summarized in Table 2. Laboratory analytical data is presented in Appendix A.
The treated material was transported to Charlotte Motor Speedway Landfill, an
approved Subtitle D landfill for disposal. Load out and transportation activities were
performed on December 17 through 20, and December 28, 2012. A total of 784.29 tons
of stabilized foundry sands were disposed of at the landfill. Documentation of the
disposal was submitted directly to Charlotte Pipe by the landfill facility.
Prior to receiving backfill material onsite, a sample of the backfill was collected and
analyzed for total metals, VOCs, and SVOCs. Laboratory analytical results for the
backfill sample are summarized in Table 3. Laboratory analytical data is presented in
Appendix A. VOCs and SVOCs were not detected in the backfill sample. Elevated
levels of metals were detected in the backfill sample; however they appear to be within
background range, as compared to background data collected from the Anne Edwards
property (multiple sampling events 2005-2006) as presented in the approved
workplan.
Prior to backfilling operations, excavation AH accumulated storm water in the
excavation. A sample of the water was collected and analyzed for total petroleum
hydrocarbons (TPH) diesel range organics (DRO) and gasoline range organics (GRO),
and total lead. The analytical data indicated no DRO or GRO, and a concentration of
lead at 0.0192 mg/L, below the NC DENR surface water quality limit of 0.025mg/L.
Therefore, the water was pumped out of the excavation and discharged onto the
ground through a sediment bag. The results of the storm water analysis are
summarized in Table 4.
Following the receipt of laboratory analytical data confirming that foundry sands
exceeding the TCLP threshold had been removed and the water had been removed,
the excavated areas were backfilled and compacted in lifts. Upon the completion of the
backfilling, load out, and offsite disposal activities, all disturbed areas were seeded
with contractor-grade grass seed and straw which was applied to minimize potential
erosion. Site security fencing and erosion and sediment control devices were then
removed from the site.

Figures
TOPOGRAPHIC SITE LOCATION MAP
ANNE EDWARDS PROPERTY
10223 ROZZELLS FERRY ROAD
CHARLOTTE, NORTH CAROLINA 1 ERM NC, Inc.
FIGURE
SOURCE: USGS 7.5 Minute Topographic Quadrangle; Mountain Island Lake, NC 1997; Contour Interval = 10 feet
SITE
LEAD IMPACTED AREAS
ANNE EDWARDS PROPERTY
10223 ROZZELLS FERRY ROAD
CHARLOTTE, NORTH CAROLINA 2 ERM NC, Inc.
FIGURE
AH
EH

70 FT 0
APPROXIMATE SCALE
Approximate Extent of Lead Impacted Soil
SOURCE: Charlotte-Mecklenburg POLARIS GIS
Approximate property boundary
LEGEND
Approximate tax parcel boundaries
EH
SAMPLE LOCATION AND ANAYTICAL RESULTS MAP
ANNE EDWARDS PROPERTY
10223 ROZZELLS FERRY ROAD
CHARLOTTE, NORTH CAROLINA 3 ERM NC, Inc.
FIGURE
35 FT 0
APPROXIMATE SCALE
Approximate Extent of Excavations
SOURCE: Charlotte-Mecklenburg POLARIS GIS
Approximate property boundary
LEGEND
Approximate tax parcel boundaries
Sample
Location Sample ID Sample Date Depth
(feet)TCLP Lead
(mg/L)
EH-1 CPAE-EH-Base-10-1 10/19/2013 10 ND
CPAE-EH-NWall -5-1 10/19/2013 5 16.2
CPAE-EH-Duplicate-EHN 10/19/2013 5 16.9
CPAE-EH-5-2 12/10/2013 5 1.8
EH-3 CPAE-EH-EWall-5-1 10/19/2013 5 1
EH-4 CPAE-EH-WWall-5-1 10/19/2013 5 1
EH-5 CPAE-EH-SWall-5-1 10/19/2013 5 1
AH-1 CPAE-AH-Base-9-1 10/23/2013 9 ND
AH-2 CPAE-AH-Base-8-2 10/23/2013 8 ND
AH-3 CPAE-AH-NWWall-5.5-1 10/23/2013 5.5 4.5
AH-4 CPAE-AH-NWall-4.5-1 10/23/2013 4.5 4.6
CPAE-AH-NEWall-6-1 10/23/2013 6 5.1
CPAE-AH-NEWall-6-2 12/18/2013 6 3
CPAE-AH-EWall-7-1 10/23/2013 7 5.4
CPAE_AH-EWall-7-2 12/18/2013 7 4.6
AH-7 CPAE-AH-SEWall-2-1 10/23/2013 2 ND
CPAE-AH-SWall-4.5-1 10/23/2013 4.5 8.1
CPAE-AH-SWall-4.5-2 12/18/2013 4.5 1.5
AH-9 CPAE-AH-SWall-5-2 10/23/2013 5 0.43
AH-10 CPAE-AH-WWall-3.5-1 10/23/2013 3.5 3.2
5
Notes:
mg/L = milligrams per liter
ND = compound not detected above method detection limit
TCLP = Toxicity Characteristic Leaching Procedure
Bold Values Exceed TCLP Limit
TCLP Limit (mg/L)
EH-2
AH-5
AH-6
AH-8
AH EXCAVATION
EH EXCAVATION
Sample Collection Locations EH-1
EH-1
EH-3
EH-2
EH-4
EH-5
AH-2
AH-1
AH-9
AH-8
AH-10
AH-4
AH-3
AH-5
AH-6
AH-7

Tables
Sa
m
p
l
e

I
D

S
a
m
p
l
e

D
a
t
e
Sa
m
p
l
e

D
e
p
t
h

(
f
e
e
t
)
TC
L
P

L
e
a
d
(m
g
/
L
)
TCLP Cadmium (mg/L)
CP
A
E
-
E
H
-
B
a
s
e
-
1
0
-
1

1
0
/
1
9
/
2
0
1
3

1
0

N
D

N
A
CP
A
E
-
E
H
-
N
W
a
l
l

-
5
-
1

1
0
/
1
9
/
2
0
1
3

5
16
.
2
NA
CP
A
E
-
E
H
-
D
u
p
l
i
c
a
t
e
-
E
H
N

1
0
/
1
9
/
2
0
1
3

5
16
.
9
NA
CP
A
E
-
E
H
-
5
-
2

1
2
/
1
0
/
2
0
1
3

5

1
.
8

N
A
CP
A
E
-
E
H
-
E
W
a
l
l
-
5
-
1

1
0
/
1
9
/
2
0
1
3

5

1

N
A
CP
A
E
-
E
H
-
W
W
a
l
l
-
5
-
1

1
0
/
1
9
/
2
0
1
3

5

1

N
A
CP
A
E
-
E
H
-
S
W
a
l
l
-
5
-
1

1
0
/
1
9
/
2
0
1
3

5

1

N
A
CP
A
E
-
A
H
-
S
E
W
a
l
l
-
2
-
1

1
0
/
2
3
/
2
0
1
3

2

N
D

N
A
CP
A
E
-
A
H
-
B
a
s
e
-
9
-
1

1
0
/
2
3
/
2
0
1
3

9

N
D

N
A
CP
A
E
-
A
H
-
E
W
a
l
l
-
7
-
1

1
0
/
2
3
/
2
0
1
3

7
5.
4
NA
CP
A
E
_
A
H
-
E
W
a
l
l
-
7
-
2

1
2
/
1
8
/
2
0
1
3

7

4
.
6

0
.
0
5
9
CP
A
E
-
A
H
-
N
E
W
a
l
l
-
6
-
1

1
0
/
2
3
/
2
0
1
3

6
5.
1
NA
CP
A
E
-
A
H
-
N
E
W
a
l
l
-
6
-
2

1
2
/
1
8
/
2
0
1
3

6

3

0
.
1
1
CP
A
E
-
A
H
-
N
W
a
l
l
-
5
.
5
-
1

1
0
/
2
3
/
2
0
1
3

5
.
5

4
.
5

N
A
CP
A
E
-
A
H
-
N
W
a
l
l
-
4
.
5
-
1

1
0
/
2
3
/
2
0
1
3

4
.
5

4
.
6

N
A
CP
A
E
-
A
H
-
W
W
a
l
l
-
3
.
5
-
1

1
0
/
2
3
/
2
0
1
3

3
.
5

3
.
2

N
A
CP
A
E
-
A
H
-
S
W
a
l
l
-
4
.
5
-
1

1
0
/
2
3
/
2
0
1
3

4
.
5
8.
1
NA
CP
A
E
-
A
H
-
S
W
a
l
l
-
4
.
5
-
2

1
2
/
1
8
/
2
0
1
3

4
.
5

1
.
5

0
.
0
5
3
CP
A
E
-
A
H
-
S
W
a
l
l
-
5
-
2

1
0
/
2
3
/
2
0
1
3

5

0
.
4
3

N
A
CP
A
E
-
A
H
-
B
a
s
e
-
8
-
2

1
0
/
2
3
/
2
0
1
3

8

N
D

N
A
TC
L
P

L
i
m
i
t

(
m
g
/
L
)
51
No
t
e
s
:

mg
/
L

=

m
i
l
l
i
g
r
a
m
s

p
e
r

l
i
t
e
r
NA

=

S
a
m
p
l
e

N
o
t

A
n
a
l
y
z
e
d
IH
S
B

=

I
n
a
c
t
i
v
e

H
a
z
a
r
d
o
u
s

S
i
t
e
s

B
r
a
n
c
h

ND

=

c
o
m
p
o
u
n
d

n
o
t

d
e
t
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c
t
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d

a
b
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m
e
t
h
o
d

d
e
t
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c
t
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n

l
i
m
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t
TC
L
P

=

T
o
x
i
c
i
t
y

C
h
a
r
a
c
t
e
r
i
s
t
i
c

L
e
a
c
h
i
n
g

P
r
o
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d
u
r
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Bo
l
d
V
a
l
u
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s

E
x
c
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d

T
C
L
P

L
i
m
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t

TA
B
L
E

1
.

S
U
M
M
A
R
Y

O
F

E
X
C
A
V
A
T
I
O
N

C
O
N
F
I
R
M
A
T
O
R
Y

A
N
A
L
Y
T
I
C
A
L

R
E
S
U
L
T
S

-

A
n
n
e

E
d
w
a
r
d
s

P
r
o
p
e
r
t
y
NC
D
E
N
R

-

I
H
S
B

S
o
i
l

R
e
m
e
d
i
a
t
i
o
n

G
o
a
l
s

TA
B
L
E

2
.

S
U
M
M
A
R
Y

O
F

S
T
O
C
K
P
I
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C
H
A
R
A
C
T
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A
T
I
O
N

A
N
A
L
Y
T
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A
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R
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S

-

A
n
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E
d
w
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P
r
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Sa
m
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I
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S
a
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p
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D
a
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TC
L
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L
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a
d
(m
g
/
L
)
CP
A
E
-
E
H
-
S
P
-
1

1
1
/
5
/
2
0
1
2

0
.
0
7
7
CP
A
E
-
E
H
-
S
P
-
2

1
1
/
5
/
2
0
1
2

0
.
1
8
CP
A
E
-
A
H
-
S
P
-
3

1
1
/
5
/
2
0
1
2

2
.
2
CP
A
E
-
A
H
-
S
P
-
4

1
1
/
5
/
2
0
1
2

2
.
4
CP
A
E
-
A
H
-
S
P
-
5

1
1
/
5
/
2
0
1
2

1
.
6
CP
A
E
-
S
P
-
A
H
-
6

1
1
/
5
/
2
0
1
2

2
.
0
TC
L
P

L
i
m
i
t

(
m
g
/
L
)
5
No
t
e
s
:

NE

=

N
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t

E
s
t
a
b
l
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s
h
e
d
mg
/
L

=

m
i
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l
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a
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s

p
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r

l
i
t
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r
NA

=

S
a
m
p
l
e

N
o
t

A
n
a
l
y
z
e
d
IH
S
B

=

I
n
a
c
t
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e

H
a
z
a
r
d
o
u
s

S
i
t
e
s

B
r
a
n
c
h

ND

=

c
o
m
p
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n
d

n
o
t

d
e
t
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c
t
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d

a
b
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m
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t
h
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d
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t
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l
i
m
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t
TC
L
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=

T
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C
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L
e
a
c
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g

P
r
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d
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NC
D
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R

-

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H
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B

S
o
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l

R
e
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a
t
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G
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A
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A
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A
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N
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k
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P
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t
a
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m
Selenium Silver Sodium Thallium Vanadium Zinc
CP
-
S
C
S
T
-
S
P
-
1
11
/
5
/
2
0
1
2

2
'

N
D

N
D

1
6
2
0
0

0
.
6
2

2
.
4

8
8
.
4

0
.
3
6

N
D

5
0
6
0

3
3
.
5
15
.
8
47
.
9
27
2
0
0
3.8

1
2
2
0
0
57
1
ND

2
1

4
5
3
0

N
D

N
D

N
D

N
D
56.6 56.8
--
15
0
0
0

6
.
2

0
.
3
9

3
,
0
0
0

3
2

1
4

N
E

2
4
0
0
0

4
.
6

6
2
0

1
1
0
0
0

4
0
0

N
E

3
6
0

1

3
0
0

N
E

7
8

7
8

N
E

0
.
1
6

7
8

4
,
6
0
0
--
NE

0
.
9

5
.
8

5
8
0

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Appendix A
October 24, 2012
LIMS USE: FR - DAVID WAGGONER
LIMS OBJECT ID: 92135929
92135929
Project:
Pace Project No.:
RE:
Mr. David Waggoner
Charlotte Pipe & Foundry Compa
1335 S. Clarkson Street
Charlotte, NC 28235
Charlotte Pipe Anne Edwards
Dear Mr. Waggoner:
Enclosed are the analytical results for sample(s) received by the laboratory on October 19, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni for
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92135929
Charlotte Pipe Anne Edwards
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
West Virginia Certification #: 356Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92135929
Charlotte Pipe Anne Edwards
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92135929001 CPAE-EH-Base-10-1 EPA 6010 1 PASI-ASH1
92135929002 CPAE-EH-NWall-5-1 EPA 6010 1 PASI-ASH1
92135929003 CPAE-EH-Duplicate-EHN EPA 6010 1 PASI-ASH1
92135929004 CPAE-EH-EWall-5-1 EPA 6010 1 PASI-ASH1
92135929005 CPAE-EH-WWall-5-1 EPA 6010 1 PASI-ASH1
92135929006 CPAE-EH-SWall-5-1 EPA 6010 1 PASI-ASH1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92135929
Charlotte Pipe Anne Edwards
Sample:CPAE-EH-Base-10-1 Lab ID:92135929001 Collected:10/19/12 14:00 Received:10/19/12 17:00 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/20/12 20:00
Lead ND mg/L 1 10/23/12 21:22 7439-92-110/23/12 11:050.025
Sample:CPAE-EH-NWall-5-1 Lab ID:92135929002 Collected:10/19/12 14:05 Received:10/19/12 17:00 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/20/12 20:00
Lead 16.2 mg/L 1 10/23/12 21:28 7439-92-110/23/12 11:050.025
Sample:CPAE-EH-Duplicate-EHN Lab ID:92135929003 Collected:10/19/12 14:05 Received:10/19/12 17:00 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/20/12 20:00
Lead 16.9 mg/L 1 10/23/12 21:44 7439-92-110/23/12 11:050.025
Sample:CPAE-EH-EWall-5-1 Lab ID:92135929004 Collected:10/19/12 14:00 Received:10/19/12 17:00 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/20/12 20:00
Lead 1.0 mg/L 1 10/23/12 21:47 7439-92-110/23/12 11:050.025
Sample:CPAE-EH-WWall-5-1 Lab ID:92135929005 Collected:10/19/12 14:10 Received:10/19/12 17:00 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/20/12 20:00
Lead 1.0 mg/L 1 10/23/12 21:50 7439-92-110/23/12 11:050.025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/24/2012 04:50 PM Page 4 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92135929
Charlotte Pipe Anne Edwards
Sample:CPAE-EH-SWall-5-1 Lab ID:92135929006 Collected:10/19/12 14:10 Received:10/19/12 17:00 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/20/12 20:00
Lead 1.0 mg/L 1 10/23/12 21:53 7439-92-110/23/12 11:050.025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/24/2012 04:50 PM Page 5 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92135929
Charlotte Pipe Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/11787
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:92135929001, 92135929002, 92135929003, 92135929004, 92135929005, 92135929006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:857852
Associated Lab Samples:92135929001, 92135929002, 92135929003, 92135929004, 92135929005, 92135929006
Matrix:Water
Analyzed
Lead mg/L ND 0.025 10/23/12 21:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
857853LABORATORY CONTROL SAMPLE:
LCSSpike
Lead mg/L 2.32.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
857854MATRIX SPIKE SAMPLE:
MSSpike
Result
92135929001
Lead mg/L 2.52.5 99 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
92135929002
857855SAMPLE DUPLICATE:
Lead mg/L 16.2 016.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/24/2012 04:50 PM Page 6 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92135929
Charlotte Pipe Anne Edwards
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/24/2012 04:50 PM Page 7 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92135929
Charlotte Pipe Anne Edwards
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92135929001 MPRP/11787 ICP/10795CPAE-EH-Base-10-1 EPA 3010 EPA 6010
92135929002 MPRP/11787 ICP/10795CPAE-EH-NWall-5-1 EPA 3010 EPA 6010
92135929003 MPRP/11787 ICP/10795CPAE-EH-Duplicate-EHN EPA 3010 EPA 6010
92135929004 MPRP/11787 ICP/10795CPAE-EH-EWall-5-1 EPA 3010 EPA 6010
92135929005 MPRP/11787 ICP/10795CPAE-EH-WWall-5-1 EPA 3010 EPA 6010
92135929006 MPRP/11787 ICP/10795CPAE-EH-SWall-5-1 EPA 3010 EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/24/2012 04:50 PM Page 8 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
November 01, 2012
LIMS USE: FR - DAVID WAGGONER
LIMS OBJECT ID: 92136218
92136218
Project:
Pace Project No.:
RE:
Mr. David Waggoner
Charlotte Pipe & Foundry Compa
1335 S. Clarkson Street
Charlotte, NC 28235
Charlotte Pipe-Anne Edwards
Dear Mr. Waggoner:
Enclosed are the analytical results for sample(s) received by the laboratory on October 23, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92136218
Charlotte Pipe-Anne Edwards
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
West Virginia Certification #: 356Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92136218
Charlotte Pipe-Anne Edwards
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92136218001 CPAE-AH-SEWALL-2-1 EPA 6010 1 PASI-AJMW
92136218002 CPAE-AH-BASE-9-1 EPA 6010 1 PASI-AJMW
92136218003 CPAE-AH-EWALL-7-1 EPA 6010 1 PASI-AJMW
92136218004 CPAE-AH-NEWALL-6-1 EPA 6010 1 PASI-AJMW
92136218005 CPAE-AH-NWALL-5.5-1 EPA 6010 1 PASI-AJMW
92136218006 CPAE-AH-NWALL-4.5-1 EPA 6010 1 PASI-AJMW
92136218007 CPAE-AH-WWALL-3.5-1 EPA 6010 1 PASI-AJMW
92136218008 CPAE-AH-SWALL-4.5-1 EPA 6010 1 PASI-AJMW
92136218009 CPAE-AH-SWALL-5-2 EPA 6010 1 PASI-AJMW
92136218010 CPAE-AH-BASE-8-2 EPA 6010 1 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92136218
Charlotte Pipe-Anne Edwards
Sample:CPAE-AH-SEWALL-2-1 Lab ID:92136218001 Collected:10/23/12 09:06 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead ND mg/L 1 10/25/12 18:42 7439-92-110/25/12 04:500.025
Sample:CPAE-AH-BASE-9-1 Lab ID:92136218002 Collected:10/23/12 09:10 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead ND mg/L 1 10/25/12 18:55 7439-92-110/25/12 04:500.025
Sample:CPAE-AH-EWALL-7-1 Lab ID:92136218003 Collected:10/23/12 09:11 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead 5.4 mg/L 1 10/25/12 18:58 7439-92-110/25/12 04:500.025
Sample:CPAE-AH-NEWALL-6-1 Lab ID:92136218004 Collected:10/23/12 09:15 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead 5.1 mg/L 1 10/25/12 19:01 7439-92-110/25/12 04:500.025
Sample:CPAE-AH-NWALL-5.5-1 Lab ID:92136218005 Collected:10/23/12 09:23 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead 4.5 mg/L 1 10/25/12 19:04 7439-92-110/25/12 04:500.025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/01/2012 04:46 PM Page 4 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92136218
Charlotte Pipe-Anne Edwards
Sample:CPAE-AH-NWALL-4.5-1 Lab ID:92136218006 Collected:10/23/12 09:27 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead 4.6 mg/L 1 10/25/12 19:07 7439-92-110/25/12 04:500.025
Sample:CPAE-AH-WWALL-3.5-1 Lab ID:92136218007 Collected:10/23/12 09:35 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead 3.2 mg/L 1 10/25/12 19:10 7439-92-110/25/12 04:500.025
Sample:CPAE-AH-SWALL-4.5-1 Lab ID:92136218008 Collected:10/23/12 09:40 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead 8.1 mg/L 1 10/25/12 19:14 7439-92-110/25/12 04:500.025
Sample:CPAE-AH-SWALL-5-2 Lab ID:92136218009 Collected:10/23/12 09:45 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/24/12 07:30
Lead 0.43 mg/L 1 10/25/12 19:17 7439-92-110/25/12 04:500.025
Sample:CPAE-AH-BASE-8-2 Lab ID:92136218010 Collected:10/23/12 09:53 Received:10/23/12 16:15 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 10/31/12 05:50
Lead ND mg/L 1 11/01/12 12:51 7439-92-111/01/12 02:450.025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/01/2012 04:46 PM Page 5 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92136218
Charlotte Pipe-Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/11803
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:92136218001, 92136218002, 92136218003, 92136218004, 92136218005, 92136218006, 92136218007,
92136218008, 92136218009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:859555
Associated Lab Samples:92136218001, 92136218002, 92136218003, 92136218004, 92136218005, 92136218006, 92136218007,
92136218008, 92136218009
Matrix:Water
Analyzed
Lead mg/L ND 0.025 10/25/12 17:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
859556LABORATORY CONTROL SAMPLE:
LCSSpike
Lead mg/L 2.22.5 90 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
859557MATRIX SPIKE SAMPLE:
MSSpike
Result
92135728002
Lead mg/L 2.42.5 95 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
92135813001
859559SAMPLE DUPLICATE:
Lead mg/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/01/2012 04:46 PM Page 6 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92136218
Charlotte Pipe-Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/11871
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:92136218010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:864255
Associated Lab Samples:92136218010
Matrix:Water
Analyzed
Lead mg/L ND 0.025 11/01/12 12:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
864256LABORATORY CONTROL SAMPLE:
LCSSpike
Lead mg/L 2.22.5 89 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
864260MATRIX SPIKE SAMPLE:
MSSpike
Result
92136651007
Lead mg/L 2.32.5 92 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
92136489001
864261SAMPLE DUPLICATE:
Lead mg/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/01/2012 04:46 PM Page 7 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92136218
Charlotte Pipe-Anne Edwards
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/01/2012 04:46 PM Page 8 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92136218
Charlotte Pipe-Anne Edwards
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92136218001 MPRP/11803 ICP/10808CPAE-AH-SEWALL-2-1 EPA 3010 EPA 6010
92136218002 MPRP/11803 ICP/10808CPAE-AH-BASE-9-1 EPA 3010 EPA 6010
92136218003 MPRP/11803 ICP/10808CPAE-AH-EWALL-7-1 EPA 3010 EPA 6010
92136218004 MPRP/11803 ICP/10808CPAE-AH-NEWALL-6-1 EPA 3010 EPA 6010
92136218005 MPRP/11803 ICP/10808CPAE-AH-NWALL-5.5-1 EPA 3010 EPA 6010
92136218006 MPRP/11803 ICP/10808CPAE-AH-NWALL-4.5-1 EPA 3010 EPA 6010
92136218007 MPRP/11803 ICP/10808CPAE-AH-WWALL-3.5-1 EPA 3010 EPA 6010
92136218008 MPRP/11803 ICP/10808CPAE-AH-SWALL-4.5-1 EPA 3010 EPA 6010
92136218009 MPRP/11803 ICP/10808CPAE-AH-SWALL-5-2 EPA 3010 EPA 6010
92136218010 MPRP/11871 ICP/10864CPAE-AH-BASE-8-2 EPA 3010 EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/01/2012 04:46 PM Page 9 of 9
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CL#
December 13, 2012
LIMS USE: FR - DAVID WAGGONER
LIMS OBJECT ID: 92141270
92141270
Project:
Pace Project No.:
RE:
Mr. David Waggoner
Charlotte Pipe & Foundry Compa
1335 S. Clarkson Street
Charlotte, NC 28235
TCLP Lead 12/10/12
Dear Mr. Waggoner:
Enclosed are the analytical results for sample(s) received by the laboratory on December 10, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92141270
TCLP Lead 12/10/12
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
West Virginia Certification #: 356Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92141270
TCLP Lead 12/10/12
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92141270001 CPAE-EH-5-2 EPA 6010 1 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92141270
TCLP Lead 12/10/12
Sample:CPAE-EH-5-2 Lab ID:92141270001 Collected:12/10/12 11:30 Received:12/10/12 14:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/11/12 16:55
Lead 1.8 mg/L 1 12/12/12 23:37 7439-92-112/12/12 11:350.025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/13/2012 02:17 PM Page 4 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92141270
TCLP Lead 12/10/12
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/12178
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:92141270001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:888670
Associated Lab Samples:92141270001
Matrix:Water
Analyzed
Lead mg/L ND 0.025 12/12/12 23:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
888671LABORATORY CONTROL SAMPLE:
LCSSpike
Lead mg/L 2.22.5 89 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
888672MATRIX SPIKE SAMPLE:
MSSpike
Result
92141270001
Lead mg/L 6.25 88 75-1251.8
Parameter Units
Dup
Result QualifiersRPDResult
92141270001
888673SAMPLE DUPLICATE:
Lead mg/L 1.7 11.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/13/2012 02:17 PM Page 5 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92141270
TCLP Lead 12/10/12
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/13/2012 02:17 PM Page 6 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92141270
TCLP Lead 12/10/12
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92141270001 MPRP/12178 ICP/11125CPAE-EH-5-2 EPA 3010 EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/13/2012 02:17 PM Page 7 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CL#
December 21, 2012
LIMS USE: FR - DAVID WAGGONER
LIMS OBJECT ID: 92142202
92142202
Project:
Pace Project No.:
RE:
Mr. David Waggoner
Charlotte Pipe & Foundry Compa
1335 S. Clarkson Street
Charlotte, NC 28235
DAILY SAMPLES 121812
Dear Mr. Waggoner:
Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92142202
DAILY SAMPLES 121812
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
West Virginia Certification #: 356Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92142202
DAILY SAMPLES 121812
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92142202001 CPAE-AH-EWALL-7-2 EPA 6010 2 PASI-AJMW
92142202002 CPAE-AH-SWALL-4.5-2 EPA 6010 2 PASI-AJMW
92142202003 CPAE-AH-NEWALL-6-2 EPA 6010 2 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92142202
DAILY SAMPLES 121812
Sample:CPAE-AH-EWALL-7-2 Lab ID:92142202001 Collected:12/18/12 11:30 Received:12/18/12 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/19/12 23:30
Cadmium 0.059 mg/L 10 12/21/12 11:30 7440-43-912/20/12 23:300.050
Lead 4.6 mg/L 10 12/21/12 11:30 7439-92-112/20/12 23:300.25
Sample:CPAE-AH-SWALL-4.5-2 Lab ID:92142202002 Collected:12/18/12 11:00 Received:12/18/12 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/19/12 23:30
Cadmium 0.053 mg/L 10 12/21/12 11:36 7440-43-912/20/12 23:300.050
Lead 1.5 mg/L 10 12/21/12 11:36 7439-92-112/20/12 23:300.25
Sample:CPAE-AH-NEWALL-6-2 Lab ID:92142202003 Collected:12/18/12 11:30 Received:12/18/12 12:40 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/19/12 23:30
Cadmium 0.11 mg/L 10 12/21/12 11:42 7440-43-912/20/12 23:300.050
Lead 3.0 mg/L 10 12/21/12 11:42 7439-92-112/20/12 23:300.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/21/2012 02:22 PM Page 4 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92142202
DAILY SAMPLES 121812
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/12246
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:92142202001, 92142202002, 92142202003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:895026
Associated Lab Samples:92142202001, 92142202002, 92142202003
Matrix:Water
Analyzed
Cadmium mg/L ND 0.0050 12/21/12 11:24
Lead mg/L ND 0.025 12/21/12 11:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
895027LABORATORY CONTROL SAMPLE:
LCSSpike
Cadmium mg/L 2.52.5 98 80-120
Lead mg/L 2.42.5 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
895028MATRIX SPIKE SAMPLE:
MSSpike
Result
92142202001
Cadmium mg/L 2.52.5 99 75-1250.059
Lead mg/L 6.92.5 94 75-1254.6
Parameter Units
Dup
Result QualifiersRPDResult
92142202002
895029SAMPLE DUPLICATE:
Cadmium mg/L 0.058 80.053
Lead mg/L 1.3 151.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/21/2012 02:22 PM Page 5 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92142202
DAILY SAMPLES 121812
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/21/2012 02:22 PM Page 6 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92142202
DAILY SAMPLES 121812
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92142202001 MPRP/12246 ICP/11184CPAE-AH-EWALL-7-2 EPA 3010 EPA 6010
92142202002 MPRP/12246 ICP/11184CPAE-AH-SWALL-4.5-2 EPA 3010 EPA 6010
92142202003 MPRP/12246 ICP/11184CPAE-AH-NEWALL-6-2 EPA 3010 EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/21/2012 02:22 PM Page 7 of 7
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
November 09, 2012
LIMS USE: FR - DAVID WAGGONER
LIMS OBJECT ID: 92137658
92137658
Project:
Pace Project No.:
RE:
Mr. David Waggoner
Charlotte Pipe & Foundry Compa
1335 S. Clarkson Street
Charlotte, NC 28235
Charlotte Pipe-Anne Edwards
Dear Mr. Waggoner:
Enclosed are the analytical results for sample(s) received by the laboratory on November 06, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92137658
Charlotte Pipe-Anne Edwards
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40South Carolina Certification #: 99030001
West Virginia Certification #: 356Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92137658
Charlotte Pipe-Anne Edwards
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92137658001 CPAE-EH-SP-1 EPA 6010 1 PASI-AJMW
92137658002 CPAE-EH-SP-2 EPA 6010 1 PASI-AJMW
92137658003 CPAE-AH-SP-3 EPA 6010 1 PASI-AJMW
92137658004 CPAE-AH-SP-4 EPA 6010 1 PASI-AJMW
92137658005 CPAE-AH-SP-5 EPA 6010 1 PASI-AJMW
92137658006 CPAE-AH-SP-6 EPA 6010 1 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92137658
Charlotte Pipe-Anne Edwards
Sample:CPAE-EH-SP-1 Lab ID:92137658001 Collected:11/05/12 13:30 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 11/08/12 06:40
Lead 0.077 mg/L 1 11/09/12 14:46 7439-92-111/09/12 03:100.025
Sample:CPAE-EH-SP-2 Lab ID:92137658002 Collected:11/05/12 13:45 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 11/08/12 06:40
Lead 0.18 mg/L 1 11/09/12 14:52 7439-92-111/09/12 03:100.025
Sample:CPAE-AH-SP-3 Lab ID:92137658003 Collected:11/05/12 14:00 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 11/08/12 06:40
Lead 2.2 mg/L 1 11/09/12 14:58 7439-92-111/09/12 03:100.025
Sample:CPAE-AH-SP-4 Lab ID:92137658004 Collected:11/05/12 14:15 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 11/08/12 06:40
Lead 2.4 mg/L 1 11/09/12 15:02 7439-92-111/09/12 03:100.025
Sample:CPAE-AH-SP-5 Lab ID:92137658005 Collected:11/05/12 14:30 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 11/08/12 06:40
Lead 1.6 mg/L 1 11/09/12 15:05 7439-92-111/09/12 03:100.025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/09/2012 04:36 PM Page 4 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92137658
Charlotte Pipe-Anne Edwards
Sample:CPAE-AH-SP-6 Lab ID:92137658006 Collected:11/05/12 14:45 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 11/08/12 06:40
Lead 2.0 mg/L 1 11/09/12 15:16 7439-92-111/09/12 03:100.025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/09/2012 04:36 PM Page 5 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137658
Charlotte Pipe-Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/11936
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:92137658001, 92137658002, 92137658003, 92137658004, 92137658005, 92137658006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:869253
Associated Lab Samples:92137658001, 92137658002, 92137658003, 92137658004, 92137658005, 92137658006
Matrix:Water
Analyzed
Lead mg/L ND 0.025 11/09/12 14:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
869254LABORATORY CONTROL SAMPLE:
LCSSpike
Lead mg/L 2.32.5 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
869255MATRIX SPIKE SAMPLE:
MSSpike
Result
92137658001
Lead mg/L 2.42.5 91 75-1250.077
Parameter Units
Dup
Result QualifiersRPDResult
92137658002
869257SAMPLE DUPLICATE:
Lead mg/L 0.19 70.18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/09/2012 04:36 PM Page 6 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92137658
Charlotte Pipe-Anne Edwards
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/09/2012 04:36 PM Page 7 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92137658
Charlotte Pipe-Anne Edwards
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92137658001 MPRP/11936 ICP/10922CPAE-EH-SP-1 EPA 3010 EPA 6010
92137658002 MPRP/11936 ICP/10922CPAE-EH-SP-2 EPA 3010 EPA 6010
92137658003 MPRP/11936 ICP/10922CPAE-AH-SP-3 EPA 3010 EPA 6010
92137658004 MPRP/11936 ICP/10922CPAE-AH-SP-4 EPA 3010 EPA 6010
92137658005 MPRP/11936 ICP/10922CPAE-AH-SP-5 EPA 3010 EPA 6010
92137658006 MPRP/11936 ICP/10922CPAE-AH-SP-6 EPA 3010 EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 11/09/2012 04:36 PM Page 8 of 8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CL#
December 05, 2012
LIMS USE: FR - DAVID WAGGONER
LIMS OBJECT ID: 92137653
92137653
Project:
Pace Project No.:
RE:
Mr. David Waggoner
Charlotte Pipe & Foundry Compa
1335 S. Clarkson Street
Charlotte, NC 28235
Charlotte Pipe-Anne Edwards
Dear Mr. Waggoner:
Enclosed are the analytical results for sample(s) received by the laboratory on November 06, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Metals results were added to the final report on November 28, 2012.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92137653001 CP-SCST-SP-1 EPA 6010 22 PASI-AJDA, JMW
EPA 7471 1 PASI-ASH1
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Sample:CP-SCST-SP-1 Lab ID:92137653001 Collected:11/05/12 12:10 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum 16200 mg/kg 10 11/30/12 16:47 7429-90-511/08/12 18:00109
Antimony 0.62 mg/kg 1 11/09/12 15:28 7440-36-011/08/12 18:000.54
Arsenic 2.4 mg/kg 1 11/09/12 15:28 7440-38-211/08/12 18:001.1
Barium 88.4 mg/kg 1 11/09/12 15:28 7440-39-311/08/12 18:000.54
Beryllium 0.36 mg/kg 1 11/09/12 15:28 7440-41-711/08/12 18:000.11
Cadmium ND mg/kg 1 11/09/12 15:28 7440-43-911/08/12 18:000.11
Calcium 5060 mg/kg 1 11/09/12 15:28 7440-70-211/08/12 18:0010.9
Chromium 33.5 mg/kg 1 11/09/12 15:28 7440-47-311/08/12 18:000.54
Cobalt 15.8 mg/kg 1 11/09/12 15:28 7440-48-411/08/12 18:000.54
Copper 47.9 mg/kg 1 11/09/12 15:28 7440-50-811/08/12 18:000.54
Iron 27200 mg/kg 10 11/30/12 16:47 7439-89-611/08/12 18:00109
Lead 3.8 mg/kg 1 11/09/12 15:28 7439-92-111/08/12 18:000.54
Magnesium 12200 mg/kg 10 11/30/12 16:47 7439-95-411/08/12 18:00109
Manganese 571 mg/kg 1 11/09/12 15:28 7439-96-511/08/12 18:000.54
Nickel 21.0 mg/kg 1 11/09/12 15:28 7440-02-011/08/12 18:000.54
Potassium 4530 mg/kg 1 11/09/12 15:28 7440-09-711/08/12 18:00543
Selenium ND mg/kg 1 11/09/12 15:28 7782-49-211/08/12 18:001.1
Silver ND mg/kg 1 11/09/12 15:28 7440-22-411/08/12 18:000.54
Sodium ND mg/kg 1 11/09/12 15:28 7440-23-511/08/12 18:00543
Thallium ND mg/kg 1 11/09/12 15:28 7440-28-011/08/12 18:001.1
Vanadium 56.6 mg/kg 1 11/09/12 15:28 7440-62-211/08/12 18:000.54
Zinc 56.8 mg/kg 1 11/09/12 15:28 7440-66-611/08/12 18:001.1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury ND mg/kg 1 11/08/12 15:30 7439-97-6 M111/08/12 11:500.0053
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 11/07/12 13:40 83-32-911/07/12 10:00359
Acenaphthylene ND ug/kg 1 11/07/12 13:40 208-96-811/07/12 10:00359
Aniline ND ug/kg 1 11/07/12 13:40 62-53-311/07/12 10:00359
Anthracene ND ug/kg 1 11/07/12 13:40 120-12-711/07/12 10:00359
Benzo(a)anthracene ND ug/kg 1 11/07/12 13:40 56-55-311/07/12 10:00359
Benzo(a)pyrene ND ug/kg 1 11/07/12 13:40 50-32-811/07/12 10:00359
Benzo(b)fluoranthene ND ug/kg 1 11/07/12 13:40 205-99-211/07/12 10:00359
Benzo(g,h,i)perylene ND ug/kg 1 11/07/12 13:40 191-24-211/07/12 10:00359
Benzo(k)fluoranthene ND ug/kg 1 11/07/12 13:40 207-08-911/07/12 10:00359
Benzoic Acid ND ug/kg 1 11/07/12 13:40 65-85-011/07/12 10:001790
Benzyl alcohol ND ug/kg 1 11/07/12 13:40 100-51-611/07/12 10:00717
4-Bromophenylphenyl ether ND ug/kg 1 11/07/12 13:40 101-55-311/07/12 10:00359
Butylbenzylphthalate ND ug/kg 1 11/07/12 13:40 85-68-711/07/12 10:00359
4-Chloro-3-methylphenol ND ug/kg 1 11/07/12 13:40 59-50-711/07/12 10:00717
4-Chloroaniline ND ug/kg 1 11/07/12 13:40 106-47-811/07/12 10:001790
bis(2-Chloroethoxy)methane ND ug/kg 1 11/07/12 13:40 111-91-111/07/12 10:00359
bis(2-Chloroethyl) ether ND ug/kg 1 11/07/12 13:40 111-44-411/07/12 10:00359
bis(2-Chloroisopropyl) ether ND ug/kg 1 11/07/12 13:40 108-60-111/07/12 10:00359
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 4 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Sample:CP-SCST-SP-1 Lab ID:92137653001 Collected:11/05/12 12:10 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Chloronaphthalene ND ug/kg 1 11/07/12 13:40 91-58-711/07/12 10:00359
2-Chlorophenol ND ug/kg 1 11/07/12 13:40 95-57-811/07/12 10:00359
4-Chlorophenylphenyl ether ND ug/kg 1 11/07/12 13:40 7005-72-311/07/12 10:00359
Chrysene ND ug/kg 1 11/07/12 13:40 218-01-911/07/12 10:00359
Dibenz(a,h)anthracene ND ug/kg 1 11/07/12 13:40 53-70-311/07/12 10:00359
Dibenzofuran ND ug/kg 1 11/07/12 13:40 132-64-911/07/12 10:00359
1,2-Dichlorobenzene ND ug/kg 1 11/07/12 13:40 95-50-111/07/12 10:00359
1,3-Dichlorobenzene ND ug/kg 1 11/07/12 13:40 541-73-111/07/12 10:00359
1,4-Dichlorobenzene ND ug/kg 1 11/07/12 13:40 106-46-711/07/12 10:00359
3,3'-Dichlorobenzidine ND ug/kg 1 11/07/12 13:40 91-94-111/07/12 10:001790
2,4-Dichlorophenol ND ug/kg 1 11/07/12 13:40 120-83-211/07/12 10:00359
Diethylphthalate ND ug/kg 1 11/07/12 13:40 84-66-211/07/12 10:00359
2,4-Dimethylphenol ND ug/kg 1 11/07/12 13:40 105-67-911/07/12 10:00359
Dimethylphthalate ND ug/kg 1 11/07/12 13:40 131-11-311/07/12 10:00359
Di-n-butylphthalate ND ug/kg 1 11/07/12 13:40 84-74-211/07/12 10:00359
4,6-Dinitro-2-methylphenol ND ug/kg 1 11/07/12 13:40 534-52-111/07/12 10:00717
2,4-Dinitrophenol ND ug/kg 1 11/07/12 13:40 51-28-511/07/12 10:001790
2,4-Dinitrotoluene ND ug/kg 1 11/07/12 13:40 121-14-211/07/12 10:00359
2,6-Dinitrotoluene ND ug/kg 1 11/07/12 13:40 606-20-211/07/12 10:00359
Di-n-octylphthalate ND ug/kg 1 11/07/12 13:40 117-84-011/07/12 10:00359
bis(2-Ethylhexyl)phthalate ND ug/kg 1 11/07/12 13:40 117-81-711/07/12 10:00359
Fluoranthene ND ug/kg 1 11/07/12 13:40 206-44-011/07/12 10:00359
Fluorene ND ug/kg 1 11/07/12 13:40 86-73-711/07/12 10:00359
Hexachloro-1,3-butadiene ND ug/kg 1 11/07/12 13:40 87-68-311/07/12 10:00359
Hexachlorobenzene ND ug/kg 1 11/07/12 13:40 118-74-111/07/12 10:00359
Hexachlorocyclopentadiene ND ug/kg 1 11/07/12 13:40 77-47-411/07/12 10:00359
Hexachloroethane ND ug/kg 1 11/07/12 13:40 67-72-111/07/12 10:00359
Indeno(1,2,3-cd)pyrene ND ug/kg 1 11/07/12 13:40 193-39-511/07/12 10:00359
Isophorone ND ug/kg 1 11/07/12 13:40 78-59-111/07/12 10:00359
1-Methylnaphthalene ND ug/kg 1 11/07/12 13:40 90-12-011/07/12 10:00359
2-Methylnaphthalene ND ug/kg 1 11/07/12 13:40 91-57-611/07/12 10:00359
2-Methylphenol(o-Cresol)ND ug/kg 1 11/07/12 13:40 95-48-711/07/12 10:00359
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 11/07/12 13:4011/07/12 10:00359
Naphthalene ND ug/kg 1 11/07/12 13:40 91-20-311/07/12 10:00359
2-Nitroaniline ND ug/kg 1 11/07/12 13:40 88-74-411/07/12 10:001790
3-Nitroaniline ND ug/kg 1 11/07/12 13:40 99-09-211/07/12 10:001790
4-Nitroaniline ND ug/kg 1 11/07/12 13:40 100-01-611/07/12 10:00717
Nitrobenzene ND ug/kg 1 11/07/12 13:40 98-95-311/07/12 10:00359
2-Nitrophenol ND ug/kg 1 11/07/12 13:40 88-75-511/07/12 10:00359
4-Nitrophenol ND ug/kg 1 11/07/12 13:40 100-02-711/07/12 10:001790
N-Nitrosodimethylamine ND ug/kg 1 11/07/12 13:40 62-75-911/07/12 10:00359
N-Nitroso-di-n-propylamine ND ug/kg 1 11/07/12 13:40 621-64-711/07/12 10:00359
N-Nitrosodiphenylamine ND ug/kg 1 11/07/12 13:40 86-30-611/07/12 10:00359
Pentachlorophenol ND ug/kg 1 11/07/12 13:40 87-86-511/07/12 10:001790
Phenanthrene ND ug/kg 1 11/07/12 13:40 85-01-811/07/12 10:00359
Phenol ND ug/kg 1 11/07/12 13:40 108-95-211/07/12 10:00359
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 5 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Sample:CP-SCST-SP-1 Lab ID:92137653001 Collected:11/05/12 12:10 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pyrene ND ug/kg 1 11/07/12 13:40 129-00-011/07/12 10:00359
1,2,4-Trichlorobenzene ND ug/kg 1 11/07/12 13:40 120-82-111/07/12 10:00359
2,4,5-Trichlorophenol ND ug/kg 1 11/07/12 13:40 95-95-411/07/12 10:00359
2,4,6-Trichlorophenol ND ug/kg 1 11/07/12 13:40 88-06-211/07/12 10:00359
Surrogates
Nitrobenzene-d5 (S)55 %1 11/07/12 13:40 4165-60-011/07/12 10:0023-110
2-Fluorobiphenyl (S)66 %1 11/07/12 13:40 321-60-811/07/12 10:0030-110
Terphenyl-d14 (S)81 %1 11/07/12 13:40 1718-51-011/07/12 10:0028-110
Phenol-d6 (S)54 %1 11/07/12 13:40 13127-88-311/07/12 10:0022-110
2-Fluorophenol (S)54 %1 11/07/12 13:40 367-12-411/07/12 10:0013-110
2,4,6-Tribromophenol (S)65 %1 11/07/12 13:40 118-79-611/07/12 10:0027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/07/12 16:14 67-64-149.7
Benzene ND ug/kg 1 11/07/12 16:14 71-43-22.5
Bromobenzene ND ug/kg 1 11/07/12 16:14 108-86-12.5
Bromochloromethane ND ug/kg 1 11/07/12 16:14 74-97-52.5
Bromodichloromethane ND ug/kg 1 11/07/12 16:14 75-27-42.5
Bromoform ND ug/kg 1 11/07/12 16:14 75-25-22.5
Bromomethane ND ug/kg 1 11/07/12 16:14 74-83-95.0
2-Butanone (MEK)ND ug/kg 1 11/07/12 16:14 78-93-349.7
n-Butylbenzene ND ug/kg 1 11/07/12 16:14 104-51-82.5
sec-Butylbenzene ND ug/kg 1 11/07/12 16:14 135-98-82.5
tert-Butylbenzene ND ug/kg 1 11/07/12 16:14 98-06-62.5
Carbon tetrachloride ND ug/kg 1 11/07/12 16:14 56-23-52.5
Chlorobenzene ND ug/kg 1 11/07/12 16:14 108-90-72.5
Chloroethane ND ug/kg 1 11/07/12 16:14 75-00-35.0
Chloroform ND ug/kg 1 11/07/12 16:14 67-66-32.5
Chloromethane ND ug/kg 1 11/07/12 16:14 74-87-35.0
2-Chlorotoluene ND ug/kg 1 11/07/12 16:14 95-49-82.5
4-Chlorotoluene ND ug/kg 1 11/07/12 16:14 106-43-42.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/07/12 16:14 96-12-82.5
Dibromochloromethane ND ug/kg 1 11/07/12 16:14 124-48-12.5
1,2-Dibromoethane (EDB)ND ug/kg 1 11/07/12 16:14 106-93-42.5
Dibromomethane ND ug/kg 1 11/07/12 16:14 74-95-32.5
1,2-Dichlorobenzene ND ug/kg 1 11/07/12 16:14 95-50-12.5
1,3-Dichlorobenzene ND ug/kg 1 11/07/12 16:14 541-73-12.5
1,4-Dichlorobenzene ND ug/kg 1 11/07/12 16:14 106-46-72.5
Dichlorodifluoromethane ND ug/kg 1 11/07/12 16:14 75-71-85.0
1,1-Dichloroethane ND ug/kg 1 11/07/12 16:14 75-34-32.5
1,2-Dichloroethane ND ug/kg 1 11/07/12 16:14 107-06-22.5
1,1-Dichloroethene ND ug/kg 1 11/07/12 16:14 75-35-42.5
cis-1,2-Dichloroethene ND ug/kg 1 11/07/12 16:14 156-59-22.5
trans-1,2-Dichloroethene ND ug/kg 1 11/07/12 16:14 156-60-52.5
1,2-Dichloropropane ND ug/kg 1 11/07/12 16:14 78-87-52.5
1,3-Dichloropropane ND ug/kg 1 11/07/12 16:14 142-28-92.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 6 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Sample:CP-SCST-SP-1 Lab ID:92137653001 Collected:11/05/12 12:10 Received:11/06/12 16:05 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
2,2-Dichloropropane ND ug/kg 1 11/07/12 16:14 594-20-72.5
1,1-Dichloropropene ND ug/kg 1 11/07/12 16:14 563-58-62.5
cis-1,3-Dichloropropene ND ug/kg 1 11/07/12 16:14 10061-01-52.5
trans-1,3-Dichloropropene ND ug/kg 1 11/07/12 16:14 10061-02-62.5
Diisopropyl ether ND ug/kg 1 11/07/12 16:14 108-20-32.5
Ethylbenzene ND ug/kg 1 11/07/12 16:14 100-41-42.5
Hexachloro-1,3-butadiene ND ug/kg 1 11/07/12 16:14 87-68-32.5
2-Hexanone ND ug/kg 1 11/07/12 16:14 591-78-624.8
Isopropylbenzene (Cumene)ND ug/kg 1 11/07/12 16:14 98-82-82.5
p-Isopropyltoluene ND ug/kg 1 11/07/12 16:14 99-87-62.5
Methylene Chloride ND ug/kg 1 11/07/12 16:14 75-09-29.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/07/12 16:14 108-10-124.8
Methyl-tert-butyl ether ND ug/kg 1 11/07/12 16:14 1634-04-42.5
Naphthalene ND ug/kg 1 11/07/12 16:14 91-20-32.5
n-Propylbenzene ND ug/kg 1 11/07/12 16:14 103-65-12.5
Styrene ND ug/kg 1 11/07/12 16:14 100-42-52.5
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/07/12 16:14 630-20-62.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/07/12 16:14 79-34-52.5
Tetrachloroethene ND ug/kg 1 11/07/12 16:14 127-18-42.5
Toluene ND ug/kg 1 11/07/12 16:14 108-88-32.5
1,2,3-Trichlorobenzene ND ug/kg 1 11/07/12 16:14 87-61-62.5
1,2,4-Trichlorobenzene ND ug/kg 1 11/07/12 16:14 120-82-12.5
1,1,1-Trichloroethane ND ug/kg 1 11/07/12 16:14 71-55-62.5
1,1,2-Trichloroethane ND ug/kg 1 11/07/12 16:14 79-00-52.5
Trichloroethene ND ug/kg 1 11/07/12 16:14 79-01-62.5
Trichlorofluoromethane ND ug/kg 1 11/07/12 16:14 75-69-42.5
1,2,3-Trichloropropane ND ug/kg 1 11/07/12 16:14 96-18-42.5
1,2,4-Trimethylbenzene ND ug/kg 1 11/07/12 16:14 95-63-62.5
1,3,5-Trimethylbenzene ND ug/kg 1 11/07/12 16:14 108-67-82.5
Vinyl acetate ND ug/kg 1 11/07/12 16:14 108-05-424.8
Vinyl chloride ND ug/kg 1 11/07/12 16:14 75-01-45.0
Xylene (Total)ND ug/kg 1 11/07/12 16:14 1330-20-75.0
m&p-Xylene ND ug/kg 1 11/07/12 16:14 179601-23-15.0
o-Xylene ND ug/kg 1 11/07/12 16:14 95-47-62.5
Surrogates
Dibromofluoromethane (S)144 %1 11/07/12 16:14 1868-53-7 S370-130
Toluene-d8 (S)101 %1 11/07/12 16:14 2037-26-570-130
4-Bromofluorobenzene (S)91 %1 11/07/12 16:14 460-00-470-130
1,2-Dichloroethane-d4 (S)141 %1 11/07/12 16:14 17060-07-0 S370-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 8.0 %1 11/09/12 09:230.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 7 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/4659
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92137653001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:868501
Associated Lab Samples:92137653001
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 11/08/12 15:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
868502LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.065.067 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
868503MATRIX SPIKE SAMPLE:
MSSpike
Result
92137653001
Mercury mg/kg 0.028 M1.061 45 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
92137704001
868504SAMPLE DUPLICATE:
Mercury mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 8 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/11929
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92137653001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:868522
Associated Lab Samples:92137653001
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 11/09/12 15:22
Arsenic mg/kg ND 1.0 11/09/12 15:22
Barium mg/kg ND 0.50 11/09/12 15:22
Beryllium mg/kg ND 0.10 11/09/12 15:22
Cadmium mg/kg ND 0.10 11/09/12 15:22
Chromium mg/kg ND 0.50 11/09/12 15:22
Cobalt mg/kg ND 0.50 11/09/12 15:22
Copper mg/kg ND 0.50 11/09/12 15:22
Lead mg/kg ND 0.50 11/09/12 15:22
Manganese mg/kg ND 0.50 11/09/12 15:22
Nickel mg/kg ND 0.50 11/09/12 15:22
Selenium mg/kg ND 1.0 11/09/12 15:22
Silver mg/kg ND 0.50 11/09/12 15:22
Thallium mg/kg ND 1.0 11/09/12 15:22
Zinc mg/kg ND 1.0 11/09/12 15:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
868523LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 49.650 99 80-120
Arsenic mg/kg 48.650 97 80-120
Barium mg/kg 49.050 98 80-120
Beryllium mg/kg 49.150 98 80-120
Cadmium mg/kg 49.250 98 80-120
Chromium mg/kg 48.250 96 80-120
Cobalt mg/kg 48.450 97 80-120
Copper mg/kg 50.050 100 80-120
Lead mg/kg 48.650 97 80-120
Manganese mg/kg 47.950 96 80-120
Nickel mg/kg 49.150 98 80-120
Selenium mg/kg 49.450 99 80-120
Silver mg/kg 24.325 97 80-120
Thallium mg/kg 48.350 97 80-120
Zinc mg/kg 47.450 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
868524MATRIX SPIKE SAMPLE:
MSSpike
Result
92137653001
Antimony mg/kg 35.6 M151.3 68 75-1250.62
Arsenic mg/kg 47.951.3 89 75-1252.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 9 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
868524MATRIX SPIKE SAMPLE:
MSSpike
Result
92137653001
Barium mg/kg 124 M151.3 69 75-12588.4
Beryllium mg/kg 49.351.3 95 75-1250.36
Cadmium mg/kg 48.451.3 94 75-125ND
Chromium mg/kg 79.551.3 90 75-12533.5
Cobalt mg/kg 60.151.3 86 75-12515.8
Copper mg/kg 10351.3 107 75-12547.9
Lead mg/kg 49.451.3 89 75-1253.8
Manganese mg/kg 608 M151.3 72 75-125571
Nickel mg/kg 66.251.3 88 75-12521.0
Selenium mg/kg 45.851.3 88 75-125ND
Silver mg/kg 24.125.6 94 75-125ND
Thallium mg/kg 43.051.3 84 75-125ND
Zinc mg/kg 93.8 M151.3 72 75-12556.8
Parameter Units
Dup
Result QualifiersRPDResult
92137704001
868525SAMPLE DUPLICATE:
Antimony mg/kg .35JND
Arsenic mg/kg 1.3 161.12 ug/g
Barium mg/kg NDND
Beryllium mg/kg NDND
Cadmium mg/kg NDND
Chromium mg/kg .034JND
Cobalt mg/kg NDND
Copper mg/kg .048JND
Lead mg/kg NDND
Manganese mg/kg .098JND
Nickel mg/kg NDND
Selenium mg/kg 1.8 31.91 ug/g
Silver mg/kg NDND
Thallium mg/kg NDND
Zinc mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 10 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/21021
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92137653001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:867612
Associated Lab Samples:92137653001
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.8 11/07/12 15:19
1,1,1-Trichloroethane ug/kg ND 5.8 11/07/12 15:19
1,1,2,2-Tetrachloroethane ug/kg ND 5.8 11/07/12 15:19
1,1,2-Trichloroethane ug/kg ND 5.8 11/07/12 15:19
1,1-Dichloroethane ug/kg ND 5.8 11/07/12 15:19
1,1-Dichloroethene ug/kg ND 5.8 11/07/12 15:19
1,1-Dichloropropene ug/kg ND 5.8 11/07/12 15:19
1,2,3-Trichlorobenzene ug/kg ND 5.8 11/07/12 15:19
1,2,3-Trichloropropane ug/kg ND 5.8 11/07/12 15:19
1,2,4-Trichlorobenzene ug/kg ND 5.8 11/07/12 15:19
1,2,4-Trimethylbenzene ug/kg ND 5.8 11/07/12 15:19
1,2-Dibromo-3-chloropropane ug/kg ND 5.8 11/07/12 15:19
1,2-Dibromoethane (EDB)ug/kg ND 5.8 11/07/12 15:19
1,2-Dichlorobenzene ug/kg ND 5.8 11/07/12 15:19
1,2-Dichloroethane ug/kg ND 5.8 11/07/12 15:19
1,2-Dichloropropane ug/kg ND 5.8 11/07/12 15:19
1,3,5-Trimethylbenzene ug/kg ND 5.8 11/07/12 15:19
1,3-Dichlorobenzene ug/kg ND 5.8 11/07/12 15:19
1,3-Dichloropropane ug/kg ND 5.8 11/07/12 15:19
1,4-Dichlorobenzene ug/kg ND 5.8 11/07/12 15:19
2,2-Dichloropropane ug/kg ND 5.8 11/07/12 15:19
2-Butanone (MEK)ug/kg ND 117 11/07/12 15:19
2-Chlorotoluene ug/kg ND 5.8 11/07/12 15:19
2-Hexanone ug/kg ND 58.4 11/07/12 15:19
4-Chlorotoluene ug/kg ND 5.8 11/07/12 15:19
4-Methyl-2-pentanone (MIBK)ug/kg ND 58.4 11/07/12 15:19
Acetone ug/kg ND 117 11/07/12 15:19
Benzene ug/kg ND 5.8 11/07/12 15:19
Bromobenzene ug/kg ND 5.8 11/07/12 15:19
Bromochloromethane ug/kg ND 5.8 11/07/12 15:19
Bromodichloromethane ug/kg ND 5.8 11/07/12 15:19
Bromoform ug/kg ND 5.8 11/07/12 15:19
Bromomethane ug/kg ND 11.7 11/07/12 15:19
Carbon tetrachloride ug/kg ND 5.8 11/07/12 15:19
Chlorobenzene ug/kg ND 5.8 11/07/12 15:19
Chloroethane ug/kg ND 11.7 11/07/12 15:19
Chloroform ug/kg ND 5.8 11/07/12 15:19
Chloromethane ug/kg ND 11.7 11/07/12 15:19
cis-1,2-Dichloroethene ug/kg ND 5.8 11/07/12 15:19
cis-1,3-Dichloropropene ug/kg ND 5.8 11/07/12 15:19
Dibromochloromethane ug/kg ND 5.8 11/07/12 15:19
Dibromomethane ug/kg ND 5.8 11/07/12 15:19
Dichlorodifluoromethane ug/kg ND 11.7 11/07/12 15:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 11 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:867612
Associated Lab Samples:92137653001
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.8 11/07/12 15:19
Ethylbenzene ug/kg ND 5.8 11/07/12 15:19
Hexachloro-1,3-butadiene ug/kg ND 5.8 11/07/12 15:19
Isopropylbenzene (Cumene)ug/kg ND 5.8 11/07/12 15:19
m&p-Xylene ug/kg ND 11.7 11/07/12 15:19
Methyl-tert-butyl ether ug/kg ND 5.8 11/07/12 15:19
Methylene Chloride ug/kg ND 23.4 11/07/12 15:19
n-Butylbenzene ug/kg ND 5.8 11/07/12 15:19
n-Propylbenzene ug/kg ND 5.8 11/07/12 15:19
Naphthalene ug/kg ND 5.8 11/07/12 15:19
o-Xylene ug/kg ND 5.8 11/07/12 15:19
p-Isopropyltoluene ug/kg ND 5.8 11/07/12 15:19
sec-Butylbenzene ug/kg ND 5.8 11/07/12 15:19
Styrene ug/kg ND 5.8 11/07/12 15:19
tert-Butylbenzene ug/kg ND 5.8 11/07/12 15:19
Tetrachloroethene ug/kg ND 5.8 11/07/12 15:19
Toluene ug/kg ND 5.8 11/07/12 15:19
trans-1,2-Dichloroethene ug/kg ND 5.8 11/07/12 15:19
trans-1,3-Dichloropropene ug/kg ND 5.8 11/07/12 15:19
Trichloroethene ug/kg ND 5.8 11/07/12 15:19
Trichlorofluoromethane ug/kg ND 5.8 11/07/12 15:19
Vinyl acetate ug/kg ND 58.4 11/07/12 15:19
Vinyl chloride ug/kg ND 11.7 11/07/12 15:19
Xylene (Total)ug/kg ND 11.7 11/07/12 15:19
1,2-Dichloroethane-d4 (S)%152 70-132 S011/07/12 15:19
4-Bromofluorobenzene (S)%95 70-130 11/07/12 15:19
Dibromofluoromethane (S)%155 70-130 S011/07/12 15:19
Toluene-d8 (S)%101 70-130 11/07/12 15:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
867613LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 61.054.9 111 70-131
1,1,1-Trichloroethane ug/kg 62.854.9 114 70-141
1,1,2,2-Tetrachloroethane ug/kg 66.954.9 122 70-130
1,1,2-Trichloroethane ug/kg 68.754.9 125 70-132
1,1-Dichloroethane ug/kg 61.754.9 112 70-143
1,1-Dichloroethene ug/kg 61.354.9 112 70-137
1,1-Dichloropropene ug/kg 56.554.9 103 70-135
1,2,3-Trichlorobenzene ug/kg 66.754.9 121 69-153
1,2,3-Trichloropropane ug/kg 66.054.9 120 70-130
1,2,4-Trichlorobenzene ug/kg 64.254.9 117 55-171
1,2,4-Trimethylbenzene ug/kg 61.054.9 111 70-149
1,2-Dibromo-3-chloropropane ug/kg 67.554.9 123 68-141
1,2-Dibromoethane (EDB)ug/kg 66.754.9 121 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 12 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
867613LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 62.654.9 114 70-140
1,2-Dichloroethane ug/kg 65.754.9 120 70-137
1,2-Dichloropropane ug/kg 62.654.9 114 70-133
1,3,5-Trimethylbenzene ug/kg 61.454.9 112 70-143
1,3-Dichlorobenzene ug/kg 60.454.9 110 70-144
1,3-Dichloropropane ug/kg 65.654.9 119 70-132
1,4-Dichlorobenzene ug/kg 60.954.9 111 70-142
2,2-Dichloropropane ug/kg 57.354.9 104 68-152
2-Butanone (MEK)ug/kg 129110 118 70-149
2-Chlorotoluene ug/kg 62.054.9 113 70-141
2-Hexanone ug/kg 155 F311014170-149
4-Chlorotoluene ug/kg 63.154.9 115 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 153 F311013970-153
Acetone ug/kg 133110 121 70-157
Benzene ug/kg 63.354.9 115 70-130
Bromobenzene ug/kg 64.254.9 117 70-141
Bromochloromethane ug/kg 68.354.9 124 70-149
Bromodichloromethane ug/kg 62.054.9 113 70-130
Bromoform ug/kg 72.9 F3,L354.9 133 70-131
Bromomethane ug/kg 80.2 F3,L354.9 146 64-136
Carbon tetrachloride ug/kg 59.354.9 108 70-154
Chlorobenzene ug/kg 62.854.9 114 70-135
Chloroethane ug/kg 70.654.9 128 68-151
Chloroform ug/kg 61.054.9 111 70-130
Chloromethane ug/kg 86.2 F3,L354.9 157 70-132
cis-1,2-Dichloroethene ug/kg 60.954.9 111 70-140
cis-1,3-Dichloropropene ug/kg 66.354.9 121 70-137
Dibromochloromethane ug/kg 65.954.9 120 70-130
Dibromomethane ug/kg 63.454.9 115 70-136
Dichlorodifluoromethane ug/kg 146 F3,L354.9 265 36-148
Diisopropyl ether ug/kg 61.054.9 111 70-139
Ethylbenzene ug/kg 61.154.9 111 70-137
Hexachloro-1,3-butadiene ug/kg 60.254.9 110 70-145
Isopropylbenzene (Cumene)ug/kg 58.954.9 107 70-141
m&p-Xylene ug/kg 122110 111 70-140
Methyl-tert-butyl ether ug/kg 67.454.9 123 45-150
Methylene Chloride ug/kg 70.954.9 129 70-133
n-Butylbenzene ug/kg 61.054.9 111 65-155
n-Propylbenzene ug/kg 60.654.9 110 70-148
Naphthalene ug/kg 71.354.9 130 70-148
o-Xylene ug/kg 60.754.9 110 70-141
p-Isopropyltoluene ug/kg 62.854.9 114 70-148
sec-Butylbenzene ug/kg 61.154.9 111 70-145
Styrene ug/kg 63.954.9 116 70-138
tert-Butylbenzene ug/kg 61.354.9 112 70-143
Tetrachloroethene ug/kg 57.554.9 105 70-140
Toluene ug/kg 60.654.9 110 70-130
trans-1,2-Dichloroethene ug/kg 59.654.9 109 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 13 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
867613LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 66.654.9 121 70-138
Trichloroethene ug/kg 57.854.9 105 70-132
Trichlorofluoromethane ug/kg 63.654.9 116 69-134
Vinyl acetate ug/kg 96.0110 87 24-161
Vinyl chloride ug/kg 71.054.9 129 55-140
Xylene (Total)ug/kg 183165 111 70-141
1,2-Dichloroethane-d4 (S)%105 70-132
4-Bromofluorobenzene (S)%99 70-130
Dibromofluoromethane (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
868559MATRIX SPIKE SAMPLE:
MSSpike
Result
92137673003
1,1-Dichloroethene ug/kg 42.946 93 49-180ND
Benzene ug/kg 37.346 81 50-166ND
Chlorobenzene ug/kg 43.446 94 43-169ND
Toluene ug/kg 43.746 95 52-163ND
Trichloroethene ug/kg 43.046 94 49-167ND
1,2-Dichloroethane-d4 (S)%97 70-132
4-Bromofluorobenzene (S)%96 70-130
Dibromofluoromethane (S)%92 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92137635005
868558SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 14 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
Dup
Result QualifiersRPDResult
92137635005
868558SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 54.7JND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 15 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
Dup
Result QualifiersRPDResult
92137635005
868558SAMPLE DUPLICATE:
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%102 59129
4-Bromofluorobenzene (S)%95 3593
Dibromofluoromethane (S)%100 56121
Toluene-d8 (S)%98 39100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 16 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/19613
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92137653001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:867525
Associated Lab Samples:92137653001
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 11/07/12 11:21
1,2-Dichlorobenzene ug/kg ND 330 11/07/12 11:21
1,3-Dichlorobenzene ug/kg ND 330 11/07/12 11:21
1,4-Dichlorobenzene ug/kg ND 330 11/07/12 11:21
1-Methylnaphthalene ug/kg ND 330 11/07/12 11:21
2,4,5-Trichlorophenol ug/kg ND 330 11/07/12 11:21
2,4,6-Trichlorophenol ug/kg ND 330 11/07/12 11:21
2,4-Dichlorophenol ug/kg ND 330 11/07/12 11:21
2,4-Dimethylphenol ug/kg ND 330 11/07/12 11:21
2,4-Dinitrophenol ug/kg ND 1650 11/07/12 11:21
2,4-Dinitrotoluene ug/kg ND 330 11/07/12 11:21
2,6-Dinitrotoluene ug/kg ND 330 11/07/12 11:21
2-Chloronaphthalene ug/kg ND 330 11/07/12 11:21
2-Chlorophenol ug/kg ND 330 11/07/12 11:21
2-Methylnaphthalene ug/kg ND 330 11/07/12 11:21
2-Methylphenol(o-Cresol)ug/kg ND 330 11/07/12 11:21
2-Nitroaniline ug/kg ND 1650 11/07/12 11:21
2-Nitrophenol ug/kg ND 330 11/07/12 11:21
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 11/07/12 11:21
3,3'-Dichlorobenzidine ug/kg ND 1650 11/07/12 11:21
3-Nitroaniline ug/kg ND 1650 11/07/12 11:21
4,6-Dinitro-2-methylphenol ug/kg ND 660 11/07/12 11:21
4-Bromophenylphenyl ether ug/kg ND 330 11/07/12 11:21
4-Chloro-3-methylphenol ug/kg ND 660 11/07/12 11:21
4-Chloroaniline ug/kg ND 1650 11/07/12 11:21
4-Chlorophenylphenyl ether ug/kg ND 330 11/07/12 11:21
4-Nitroaniline ug/kg ND 660 11/07/12 11:21
4-Nitrophenol ug/kg ND 1650 11/07/12 11:21
Acenaphthene ug/kg ND 330 11/07/12 11:21
Acenaphthylene ug/kg ND 330 11/07/12 11:21
Aniline ug/kg ND 330 11/07/12 11:21
Anthracene ug/kg ND 330 11/07/12 11:21
Benzo(a)anthracene ug/kg ND 330 11/07/12 11:21
Benzo(a)pyrene ug/kg ND 330 11/07/12 11:21
Benzo(b)fluoranthene ug/kg ND 330 11/07/12 11:21
Benzo(g,h,i)perylene ug/kg ND 330 11/07/12 11:21
Benzo(k)fluoranthene ug/kg ND 330 11/07/12 11:21
Benzoic Acid ug/kg ND 1650 11/07/12 11:21
Benzyl alcohol ug/kg ND 660 11/07/12 11:21
bis(2-Chloroethoxy)methane ug/kg ND 330 11/07/12 11:21
bis(2-Chloroethyl) ether ug/kg ND 330 11/07/12 11:21
bis(2-Chloroisopropyl) ether ug/kg ND 330 11/07/12 11:21
bis(2-Ethylhexyl)phthalate ug/kg ND 330 11/07/12 11:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 17 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:867525
Associated Lab Samples:92137653001
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 11/07/12 11:21
Chrysene ug/kg ND 330 11/07/12 11:21
Di-n-butylphthalate ug/kg ND 330 11/07/12 11:21
Di-n-octylphthalate ug/kg ND 330 11/07/12 11:21
Dibenz(a,h)anthracene ug/kg ND 330 11/07/12 11:21
Dibenzofuran ug/kg ND 330 11/07/12 11:21
Diethylphthalate ug/kg ND 330 11/07/12 11:21
Dimethylphthalate ug/kg ND 330 11/07/12 11:21
Fluoranthene ug/kg ND 330 11/07/12 11:21
Fluorene ug/kg ND 330 11/07/12 11:21
Hexachloro-1,3-butadiene ug/kg ND 330 11/07/12 11:21
Hexachlorobenzene ug/kg ND 330 11/07/12 11:21
Hexachlorocyclopentadiene ug/kg ND 330 11/07/12 11:21
Hexachloroethane ug/kg ND 330 11/07/12 11:21
Indeno(1,2,3-cd)pyrene ug/kg ND 330 11/07/12 11:21
Isophorone ug/kg ND 330 11/07/12 11:21
N-Nitroso-di-n-propylamine ug/kg ND 330 11/07/12 11:21
N-Nitrosodimethylamine ug/kg ND 330 11/07/12 11:21
N-Nitrosodiphenylamine ug/kg ND 330 11/07/12 11:21
Naphthalene ug/kg ND 330 11/07/12 11:21
Nitrobenzene ug/kg ND 330 11/07/12 11:21
Pentachlorophenol ug/kg ND 1650 11/07/12 11:21
Phenanthrene ug/kg ND 330 11/07/12 11:21
Phenol ug/kg ND 330 11/07/12 11:21
Pyrene ug/kg ND 330 11/07/12 11:21
2,4,6-Tribromophenol (S)%64 27-110 11/07/12 11:21
2-Fluorobiphenyl (S)%73 30-110 11/07/12 11:21
2-Fluorophenol (S)%62 13-110 11/07/12 11:21
Nitrobenzene-d5 (S)%63 23-110 11/07/12 11:21
Phenol-d6 (S)%66 22-110 11/07/12 11:21
Terphenyl-d14 (S)%93 28-110 11/07/12 11:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
867526LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
867531
1,2,4-Trichlorobenzene ug/kg 13701670 82 39-101791310 4 30
1,2-Dichlorobenzene ug/kg 13101670 79 36-110761270 3 30
1,3-Dichlorobenzene ug/kg 12801670 77 35-110751250 2 30
1,4-Dichlorobenzene ug/kg 13001670 78 35-110761260 3 30
1-Methylnaphthalene ug/kg 13401670 81 45-105761270 6 30
2,4,5-Trichlorophenol ug/kg 14101670 85 48-109851410 0 30
2,4,6-Trichlorophenol ug/kg 13501670 81 45-111811350 0 30
2,4-Dichlorophenol ug/kg 13301670 80 51-116771280 4 30
2,4-Dimethylphenol ug/kg 13501670 81 42-103771290 5 30
2,4-Dinitrophenol ug/kg 83308330 100 28-1031018410 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 18 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
867526LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
867531
2,4-Dinitrotoluene ug/kg 12401670 75 46-114701160 7 30
2,6-Dinitrotoluene ug/kg 11401670 68 48-112671120 2 30
2-Chloronaphthalene ug/kg 13501670 81 44-105781310 3 30
2-Chlorophenol ug/kg 12701670 76 36-110761260 1 30
2-Methylnaphthalene ug/kg 13501670 81 39-112781300 4 30
2-Methylphenol(o-Cresol)ug/kg 13101670 79 39-101761270 3 30
2-Nitroaniline ug/kg 25903330 78 44-111762530 2 30
2-Nitrophenol ug/kg 12901670 77 41-100761270 2 30
3&4-Methylphenol(m&p Cresol)ug/kg 12301670 74 43-103731220 1 30
3,3'-Dichlorobenzidine ug/kg 26903330 81 10-150832750 2 30
3-Nitroaniline ug/kg 28003330 84 35-110812700 4 30
4,6-Dinitro-2-methylphenol ug/kg 30803330 92 38-118963210 4 30
4-Bromophenylphenyl ether ug/kg 13701670 82 47-115841400 2 30
4-Chloro-3-methylphenol ug/kg 26203330 78 43-127772560 2 30
4-Chloroaniline ug/kg 24703330 74 34-109712380 4 30
4-Chlorophenylphenyl ether ug/kg 14501670 87 44-115851410 2 30
4-Nitroaniline ug/kg 32603330 98 37-111923080 6 30
4-Nitrophenol ug/kg 78108330 94 21-152917620 2 30
Acenaphthene ug/kg 14401670 86 38-117851420 1 30
Acenaphthylene ug/kg 14101670 85 46-107831380 3 30
Aniline ug/kg 11801670 71 29-110701170 0 30
Anthracene ug/kg 14601670 87 50-110861440 1 30
Benzo(a)anthracene ug/kg 14801670 89 47-116871450 2 30
Benzo(a)pyrene ug/kg 15301670 92 47-106891490 3 30
Benzo(b)fluoranthene ug/kg 14101670 85 47-109851410 0 30
Benzo(g,h,i)perylene ug/kg 15201670 91 39-115881470 3 30
Benzo(k)fluoranthene ug/kg 15101670 91 45-117871460 4 30
Benzoic Acid ug/kg 55008330 66 16-110685650 3 30
Benzyl alcohol ug/kg 26003330 78 38-105772570 1 30
bis(2-Chloroethoxy)methane ug/kg 12801670 77 39-110741230 4 30
bis(2-Chloroethyl) ether ug/kg 13101670 79 19-119761270 3 30
bis(2-Chloroisopropyl) ether ug/kg 12201670 73 21-110701170 4 30
bis(2-Ethylhexyl)phthalate ug/kg 12401670 75 35-116721190 4 30
Butylbenzylphthalate ug/kg 12401670 74 38-110711180 5 30
Chrysene ug/kg 14601670 87 49-110861430 2 30
Di-n-butylphthalate ug/kg 13301670 80 43-109761270 4 30
Di-n-octylphthalate ug/kg 12101670 73 37-109701170 3 30
Dibenz(a,h)anthracene ug/kg 14801670 89 43-116861440 3 30
Dibenzofuran ug/kg 14401670 87 45-106851420 2 30
Diethylphthalate ug/kg 13401670 80 41-114771280 5 30
Dimethylphthalate ug/kg 13301670 80 43-110771280 3 30
Fluoranthene ug/kg 16501670 99 50-114961600 3 30
Fluorene ug/kg 14501670 87 46-114841400 3 30
Hexachloro-1,3-butadiene ug/kg 13501670 81 28-111771290 5 30
Hexachlorobenzene ug/kg 13701670 82 46-120841390 2 30
Hexachlorocyclopentadiene ug/kg 16301670 98 18-119991640 1 30
Hexachloroethane ug/kg 12401670 75 33-110711190 4 30
Indeno(1,2,3-cd)pyrene ug/kg 15201670 91 42-115881470 3 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 19 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
867526LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
867531
Isophorone ug/kg 9881670 59 44-10957948 4 30
N-Nitroso-di-n-propylamine ug/kg 11801670 71 43-104721190 1 30
N-Nitrosodimethylamine ug/kg 11901670 71 29-110721200 1 30
N-Nitrosodiphenylamine ug/kg 14101670 84 48-113861430 2 30
Naphthalene ug/kg 13501670 81 41-110791310 3 30
Nitrobenzene ug/kg 9681670 58 38-11055924 5 30
Pentachlorophenol ug/kg 29203330 88 32-128923060 5 30
Phenanthrene ug/kg 14401670 86 50-110851410 2 30
Phenol ug/kg 12601670 75 28-106741240 2 30
Pyrene ug/kg 14001670 84 45-114811360 3 30
2,4,6-Tribromophenol (S)%83 27-11084
2-Fluorobiphenyl (S)%81 30-11077
2-Fluorophenol (S)%71 13-11067
Nitrobenzene-d5 (S)%71 23-11065
Phenol-d6 (S)%72 22-11068
Terphenyl-d14 (S)%86 28-11081
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 20 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/5116
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92137653001
Parameter Units
Dup
Result QualifiersRPDResult
92137774011
868597SAMPLE DUPLICATE:
Percent Moisture %9.7 59.3
Parameter Units
Dup
Result QualifiersRPDResult
92137774010
868598SAMPLE DUPLICATE:
Percent Moisture %9.6 29.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 21 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.
Results unaffected by high bias.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 22 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92137653
Charlotte Pipe-Anne Edwards
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92137653001 MPRP/11929 ICP/10915CP-SCST-SP-1 EPA 3050 EPA 6010
92137653001 MERP/4659 MERC/4558CP-SCST-SP-1 EPA 7471 EPA 7471
92137653001 OEXT/19613 MSSV/6965CP-SCST-SP-1 EPA 3546 EPA 8270
92137653001 MSV/21021CP-SCST-SP-1 EPA 8260
92137653001 PMST/5116CP-SCST-SP-1 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/05/2012 03:58 PM Page 23 of 23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CL#
December 12, 2012
LIMS USE: FR - SCOTT ROBINSON
LIMS OBJECT ID: 92141268
92141268
Project:
Pace Project No.:
RE:
Scott Robinson
ERM
8000 Corporate Center
Suite 200
Charlotte, NC 28226
CPAE 12/10/12
Dear Scott Robinson:
Enclosed are the analytical results for sample(s) received by the laboratory on December 10, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92141268
CPAE 12/10/12
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92141268
CPAE 12/10/12
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92141268001 CPAE-AH-Water-1 EPA 8015 Modified 2 PASI-CMEJ
EPA 5030/8015 Mod.2 PASI-CRGF
EPA 6010 1 PASI-AJMW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92141268
CPAE 12/10/12
Method:
Client:ERM NC/SC/TN
EPA 8015 Modified
Date:December 12, 2012
Description:8015 GCS THC-Diesel
General Information:
1 sample was analyzed for EPA 8015 Modified. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3510 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92141268
CPAE 12/10/12
Method:
Client:ERM NC/SC/TN
EPA 5030/8015 Mod.
Date:December 12, 2012
Description:Gasoline Range Organics
General Information:
1 sample was analyzed for EPA 5030/8015 Mod.. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92141268
CPAE 12/10/12
Method:
Client:ERM NC/SC/TN
EPA 6010
Date:December 12, 2012
Description:6010 MET ICP
General Information:
1 sample was analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3010 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92141268
CPAE 12/10/12
Sample:CPAE-AH-Water-1 Lab ID:92141268001 Collected:12/10/12 13:30 Received:12/10/12 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3510
Diesel Components ND mg/L 1 12/11/12 18:53 68334-30-512/11/12 08:500.50
Surrogates
n-Pentacosane (S)85 %1 12/11/12 18:53 629-99-212/11/12 08:5048-110
Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod.
Gasoline Range Organics ND mg/L 1 12/11/12 14:25 8006-61-90.080
Surrogates
4-Bromofluorobenzene (S)101 %1 12/11/12 14:25 460-00-470-145
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead 19.2 ug/L 1 12/12/12 02:08 7439-92-112/11/12 12:005.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2012 05:23 PM Page 7 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92141268
CPAE 12/10/12
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/6480
EPA 5030/8015 Mod.
EPA 5030/8015 Mod.
Gasoline Range Organics
Associated Lab Samples:92141268001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:887501
Associated Lab Samples:92141268001
Matrix:Water
Analyzed
Gasoline Range Organics mg/L ND 0.080 12/11/12 11:45
4-Bromofluorobenzene (S)%96 70-145 12/11/12 11:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
887502LABORATORY CONTROL SAMPLE:
LCSSpike
Gasoline Range Organics mg/L 0.59.5 119 70-150
4-Bromofluorobenzene (S)%100 70-145
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
887503MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92141112007
887504
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Gasoline Range Organics mg/L .5 130 70-150120 7.50.085 0.73 0.68
4-Bromofluorobenzene (S)%100 70-14597
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2012 05:23 PM Page 8 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92141268
CPAE 12/10/12
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/12167
EPA 3010
EPA 6010
6010 MET
Associated Lab Samples:92141268001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:887723
Associated Lab Samples:92141268001
Matrix:Water
Analyzed
Lead ug/L ND 5.0 12/12/12 02:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
887724LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 480500 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
887725MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92141268001
887726
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 500 92 75-12593 150019.2 481 484
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2012 05:23 PM Page 9 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92141268
CPAE 12/10/12
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/20039
EPA 3510
EPA 8015 Modified
8015 GCS
Associated Lab Samples:92141268001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:887277
Associated Lab Samples:92141268001
Matrix:Water
Analyzed
Diesel Components mg/L ND 0.50 12/11/12 16:54
n-Pentacosane (S)%107 48-110 12/11/12 16:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
887278LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Components mg/L 9.510 95 41-114
n-Pentacosane (S)%101 48-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
887279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92141161001
887280
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Components mg/L 20 73 41-11485 1520ND14.7 17.0
n-Pentacosane (S)%95 48-110109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2012 05:23 PM Page 10 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92141268
CPAE 12/10/12
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2012 05:23 PM Page 11 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92141268
CPAE 12/10/12
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92141268001 OEXT/20039 GCSV/13514CPAE-AH-Water-1 EPA 3510 EPA 8015 Modified
92141268001 GCV/6480CPAE-AH-Water-1 EPA 5030/8015 Mod.
92141268001 MPRP/12167 ICP/11121CPAE-AH-Water-1 EPA 3010 EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2012 05:23 PM Page 12 of 12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]