19034_IRC_Soil Cleanup Report and Site Closure Request_20140130

Soil Cleanup Report with
Site Closure Request
Former International Resistive Company Property
736 Greenway Road
Boone, Watauga County, North Carolina
January 30, 2014
Terracon Project No. 86127103
Prepared On Behalf of:
International Resistive Company, Inc.
Corpus Christi, Texas
Prepared by:
Terracon Consultants, Inc.
Taylors, North Carolina
Soil Cleanup Report with Site Closure Request
Former International Resistive Corporation Facility • Boone, North Carolina
January 30, 2014 • Terracon Project No. 86127103
A. Site Identification
DATE OF REPORT: January 30, 2014
lrerracon
Facility I.D.: Unknown UST Incident Number (if known): 95191
Name: International Resistive Company, Inc.
Site Location: 736 Greenway Drive
Nearest City/Town: Boone, North Carolina County: Watauga County
Latitude: N 36.1969 Longitude: W 81.6675
AST Owner: International Resistive Company, Inc.
Address: 4222 South Staples Street; Corpus Christi, Texas 78411 Phone: [phone]
AST Operator: International Resistive Company, Inc.
Address: 4222 South Staples Street; Corpus Christi, Texas 78411 Phone: [phone]
Property Owner: International Resistive Company, Inc.
Address: 4222 South Staples Street; Corpus Christi, Texas 78411 Phone: [phone]
Property Occupant: Currently not occupied
Address: NA
Consultant/Contractor: Terracon Consultants, Inc.
Phone: NA
Address: 3534 Rutherford Road; Taylors, South Carolina 29687 Phone: [phone]
Analytical Laboratory: Shealy Environmental Services, Inc. NC DENR No. 329
Address: 106 Vantage Point Drive; Columbia, South Carolina 29172 Phone: [phone]
Release Information -AST Formerly Located Along West Side of Plant
Date Discovered: November 23, 2011
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (Piping/UST): AST-formerly located along the west side of the plant
Sizes and contents of UST system(s) from which the release occurred): 275-gallon tank
containing No. 2 fuel oil.
Release Information-Hydraulic Oil ASTs Formerly Located Along East Side of Plant
Date Discovered: November 23, 2011
Estimated Quantity of Release: Unknown
Responsive • Resourceful • Reliable
Soil Cleanup Report with Site Closure Request
Former International Resistive Corporation Facility Boone, North Carolina
January 30, 2014 • Terracon Project No. 86127103
lrerracon
The results of a November 2011 assessment by SynTerra detected evidence of a release from
the fuel oil AST and hydraulic oil ASTs. At the request of the North Carolina Department of
Environment and Natural Resources (NCDENR), a Comprehensive Site Assessment (CSA) was
performed in these areas and a report, entitled Comprehensive Site Assessment Report-Fuel
Oil AST & Surface Spill Areas was submitted by S&ME, Inc. (June 22, 2012). Following its
review of the CSA, NCDENR requested that a Corrective Action Plan (CAP) be prepared to
address soil impacts from these releases. Terracon submitted the requested CAP (dated
November 21, 2012) and CAP approval followed on February 14, 2013. Following CAP
approval, Terracon mobilized to the site in July 2013 to monitor removal of petroleum-impacted
soils by excavation and removal to an off-site disposal facility. Environmental Holdings Group,
LLC (EHG) was retained by the owner to perform the soil remediation. Laboratory analyses of
post-excavation , confirmatory soil samples collected from the bottom and sidewalls of the
excavations did not detect the presence of petroleum constituents in the fuel oil and hydraulic oil
spill locations.
C. Site History and Characterization
The site formerly contained an industrial manufacturing building that was reportedly used to
manufacture electrical components from 1953 until the facility was closed in 2012. The site
formerly contained an approximate 275-gallon AST located along the west side of the building
that was used as a fuel source a humidity steam unit machine once located in that area of the
building. The building contained hydraulically-operated manufacturing equipment with oil
supplied from six integrated 1 00-gallon ASTs formerly located along the east side of the
building. Site buildings have since been razed but the concrete floor slabs remain in-place.
As part of internal due diligence requirements, IRC engaged SynTerra Corporation (SynTerra) to
conduct a Phase I Environmental Site Assessment (ESA) for the site. Based on the findings of
the Phase I ESA, SynTerra was engaged to conduct further assessment, including soil and
groundwater sampling with laboratory analysis to further evaluate previously identified
environmental concerns associated with onsite operations. A report of their findings entitled,
Report of Findings -Phase II Environmental Site Assessment, IRC, Inc., was issued on
November 21, 2011. In its report, SynTerra identified evidence of multiple releases on the IRC
property including the fuel oil AST and hydraulic oil ASTs systems; the other (non-petroleum
related) releases are being addressed separately by the NCDENR Inactive Hazardous Sites
Branch (IHSB) and will not be discussed further herein. Since the releases at the fuel oil AST
and hydraulic oil AST systems involved petroleum products, a copy of the SynTerra report was
forwarded to the NCDENR UST Section by IRC personnel. Following review of the report, the
NCDENR issued a Notice of Regulatory Requirements (NORR) on February 22 , 2012
requesting a CSA be prepared for the site.
Responsive • Resourceful • Reliable 3
Soil Cleanup Report with Site Closure Request
Former International Resistive Corporation Facility • Boone, North Carolina
January 30, 2014 • Terracon Project No. 86127103
lrerracan
In accordance with the NORR, IRC engaged S&ME to perform the GSA. S&ME issued the GSA
report, entitled Comprehensive Site Assessment Report -Fuel Oil AST & Surface Spill Areas
(Project No. 1264-11-539), on June 22, 2012. Based on the findings of the GSA report, the
NCDENR issued a NORR on September 11, 2012 requesting a CAP be prepared for the site.
As a result of the NORR, Terracon Consultants, Inc. (Terracon) was engaged to complete a CAP
for the incident. The CAP was issued as Terracon Project No. 86127103 on November 21, 2012
and was approved by letter on February 14, 2013 (Kromm to Milam).
D. Summary of Site Assessment Information
A Comprehensive Site Assessment was completed for the site by S&ME. A report of their
findings was issued to the NCDENR on June 22, 2012. As a result of an NORR issued by the
NCDENR, Terracon completed a Corrective Action Plan which was forwarded to the NCDENR
on November 21, 2012.
E. Objectives of Corrective Action at the Site
The objective of the corrective action was to reduce the concentrations of petroleum
hydrocarbons in soils. Based on the "High Risk" classification for the site, the soil cleanup goals
were the Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs) for the
respective constituents of concern.
F. Soil Remediation
Terracon mobilized to the site on July 30, 2013 to observe and document the removal of
petroleum contaminated soils from the Former AST and Surface Spill Areas by EHG. The
excavated soils were temporarily stockpiled on plastic sheeting which was placed on the
building slab pending the results of post-excavation, confirmatory soil sampling. Once the pre-
determined volume of soil had been removed from each area, Terracon screened the soils for
evidence of petroleum odors (olfactory) and organic vapor concentrations using a photo-
ionization detector (PID). Elevated organic vapor concentrations were not discernible using the
PI D.
Former AST Area-Soil Remediation
Approximately 12.8 cubic yards of petroleum-impacted soils were removed from the fuel oil spill
excavation located along the west side of the building.
Responsive • Resourceful • Reliable 4
Soil Cleanup Report with Site Closure Request
Former International Resistive Corporation Facility • Boone, North Carolina
January 30, 2014 • Terracon Project No. 86127103
Surface Spill Area-Soil Remediation
lrerracon
Approximately 41.5 cubic yards of petroleum-impacted soils were removed from the hydraulic oil
spill excavation located along the east side of the plant building. Based on review of the results
of the initial post-excavation, confirmatory soil sampling, Terracon instructed EHG to remove an
additional 15 cubic yards (approximate) of soils from the bottom of the excavation. Following
removal of the additional soil, a second post-excavation sample was collected from the base of
this excavation .
Following completion of the soil removal effort, the petroleum-impacted soils were transported to
the Foothills Environmental (Republic Services) facility located in Lenoir, North Carolina for
disposal. Copies of the disposal manifests are included in Appendix A
G. Post-Remediation Sampling
Confirmatory Soil Sampling -Former AST Area
Immediately following excavation of soils, Terracon collected five risk-based soil samples from
the fuel oil spill excavation. Samples AST-N, AST-E, AST-S, and AST-W were collected from
the excavation sidewalls. AST-B was collected from the bottom of the excavation. The
approximate soil sample locations are shown on the attached Sample Location Plan (Exhibit
2.1 ).
The soil samples were placed in laboratory-supplied glassware, labeled and stored in an ice-
packed cooler. The samples, along with chain-of-custody documentation, were delivered to
Shealy Environmental Services, Inc., in West Columbia, South Carolina for analysis of volatile
and semi-volatile organic compounds (VOCs and SVOCs) by EPA Methods 8260B and 82700,
respectively and Extractable and Volatile Petroleum Hydrocarbons (EPH and VPH) using
MAOEP methods. Based on review of the laboratory analytical results, no target analytes were
detected in the soil samples. A copy of the laboratory report is included in Appendix B.
Confirmatory Soil Sampling -Surface Spill Area
Immediately following excavation of soils, Terracon collected five risk-based soil samples from
the hydraulic oil spill excavation in accordance with NCOENR UST Section Guidelines.
Samples HO-N, HO-E, HO-S and HO-W were collected from the excavation sidewalls. HO-B
was collected from the bottom of the excavation. The approximate soil sample locations are
shown on the attached Sample Location Plan (Exhibit 2.2).
The soil samples were placed in laboratory-supplied glassware, labeled and stored in an ice-
packed cooler. The samples, along with chain-of-custody documentation, were delivered to
Shealy Environmental Services, Inc. for analysis of SVOCs by EPA Method 82700 and EPH by
MAOEP methods.
Responsive • Resourceful • Reliable 5
Soil Cleanup Report with Site Closure Request
Former International Resistive Corporation Facility • Boone, North Carolina
January 30, 2014 • Terracon Project No. 86127103
lrerracon
According to the resulting laboratory report, soil sample HO-B (collected from the bottom of the
hydraulic oil spill excavation) contained C19-C36 aliphatics at a concentration of 550 milligrams
per kilogram (mg/kg) and C11-C22 aromatics at a concentration of 38 mg/kg which exceeded
the soil-to-groundwater MSCC for C11-C22 aromatics (31 mg/kg). There is no established soil-
to-groundwater MSCC for C19-C36 aliphatics; however, the residential cleanup level is 31,000
mg/kg.
Following removal of additional soils from the bottom of the hydraulic oil spill excavation,
laboratory analysis of confirmatory soil sample HO-B-2 did not detect the presence of petroleum
constituents above their respective method detection limits. Copies of the laboratory reports are
included in Appendix B.
Groundwater Assessment
Groundwater assessment in the Former AST and Surface Spill Areas was previously performed
by S&ME as a component of the CSA. Results of this assessment did not indicate the presence
of target analytes at concentrations exceeding the applicable groundwater standard established
by 15A NCAC 2L .0202.
Groundwater was not encountered in the excavations during soil remediation. Based on the
absence of detectable concentrations of petroleum constituents in the confirmatory soil samples
collected from the bottom and sidewalls of the excavations, no further assessment of
groundwater was performed at the site.
H. Conclusions and Petition for Site Closure
Based on the results of soil cleanup activities and the absence of detectable concentrations of
petroleum constituents in the confirmatory soil samples collected from the bottom and sidewalls
of the excavations, Terracon herein petitions the NCDENR for regulatory closure of the release
incident at the former IRC facility.
I. Public Notice
Based on the absence of residual petroleum remaining on the site, public notification is not
required.
J. Exhibits
Applicable site Exhibits are provided as an attachment to this report.
Responsive • Resourceful • Reliable 6
L
Soil Cleanup Report with Site Closure Request
Former International Resistive Corporation Facility • Boone, North Carolina
January 30, 2014 .. Terracon Project No. 86127103
K. Tables
lrerracon
Based on review of the laboratory analytical reports, only two constituents were identified in one
sample (HO-B); therefore, no tables were generated. The two detected constituents are
discussed in Section G, Post-Remediation Sampling, of this report.
L. Appendices
A copy of the soil disposal documentation is included in Appendix A. Copies of the laboratory
analytical reports are included in Appendix B.
Recommendations
Based on the absence of detectable petroleum constituents above regulatory levels, Terracon
petitions the NCDENR for No Further Action status of release incident 95191.
Responsive • Resourceful • Reliable 7
Exhibits
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Appendix A
Disposal Documentation
Appendix B
laboratory Analytical Results
SC DHEC No: 32010
SHEALY ENVIRONMENTAL SERVICES, INC.
NELAC No: E87653
Case Narrative
Terracon Consultants, Inc.
Lot Number: OH01042
NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP). standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 2 of 58
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVIGES, INC.
Sample Summary
Terracon Gonsultants, lnc.
Lot Number: OH01042
Sample Number Sample lD Matrix Date Sampled Date Received
001
o02
003
004
005
AST-N
AST.E
AST-S
AST-W
AST-B
Solid 07/30/20131500
Solid 07/30/2013 1505
Solid 0713012013 1515
Solid 0713012013 1525
Solid 0713012013 1530
08101t2013
o$t01t2013
0810112013
08t0112013
0810112013
(5 samples)
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Shealy Environmental Servic€s, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 3 of 58
Lov6l'1 RoDortv2.l
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Terracon Consultants, lnc.
Lot Number: OH01042
Sample Sample lD Matrix Parameter Result O
(0 detections)
Shealy Environmental Servlces, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: tl of 58
Levol I Roportv2.l
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Client:Terracon Consultants, lnc. Laboratory lD: OH01042.001
Description: AST-N Matrix: Solid
Date Sampled:07/30/2013 1500 % Solids: 76.6 O8lO1l2O13 2203
Date Received : 08101 12013
Volatile Orqanic Compounds by GC/MS
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 08102t2013 2',151 AAC
Batch Sample Wt.(g)26418 6.44
Parameter
cAs
Number
Analytical
Marha4 Result O PQL
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Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
'l ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodiff uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
I , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T elr ae,hloroethan e
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
'r 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
't56-60-5
78-87-5
10061-01-5
10061-02-6
100-41-4
591 -78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
1 00-42-5
79-34-5
127-18-4
1 08-88-3
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
8260B
8260B
8260B
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
8260B
82608
8260B
8260B
82608
8260B
82608
82608
8260B
82608
82608
8260B
82608
82608
8260B
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.1
5.1
5.1
5.1
10
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
10
5.1
5.1
5.1
10
5.1
5.1
5.1
5.1
5.1
5.1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg I
ug/kg 1
ug/kS 1ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
uS/kS 1
ug/kg 1
PQL = Practicalquantitation limit B = Detscted in th8 method blank E = Quantitation of compound exco6ded the calibralion range H = Out of holding tim€
ND =Notdotoctad atorabovethe PQL J = Estimated rssult< PQLand: MDL P=The RPDbetwooniwo GC @lumns exc€eds40% N = Recoveryisoutofctitgria
Wh6re appllcablo, all soil sample analysis aro reportsd on a dry weight basis unless flagged with a "W"
Shealy Environmental Servic€s, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l'l www.shealylab.com
Page: 5 of 58
Levsl I Reportv2.l
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-001
Description: AST-N Matrix: Solid
Date Sampled:07/30/2013 1500 % Solids: 76.6 08101120132203
Date Received: 08I0t1201 3
Volatile Organic Compounds by GC/MS
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Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 1 0810212013 2'.151 AAC
Batch Sample Wt.(g)26418 6.44 I
Parameter
CAS Analytical
Number Marhod Result O
1,'1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-l 3-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1 330-20-7
Run 1 AcceptanceO 7o Recovery LimlG
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82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
82608 ND
5.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
129
108
118
53-142
47-138
68-124
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ISemivolatile Organic Gompounds by GC/MS
Run Prep Method1 3550C
Analytlca! Method Dilutlon Analysis Date Analyst Prep Date Batch
8270D 1 08/03/2013 0005 JRG 08102120'.13 1438 26389 I
Parametcr
cAs
Number
Analytical
Method Result O
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4€hloro-3-methyl phenol
4-Chloroaniline
bis(2-C hloroethoxy)methane
bis(2-C hloroethyl)ether
83-32-9
208-96-8
98-86-2
'120-12-7
1912-24-9
't00-52-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
92-52-4
1 01 -55-3
8s-68-7
10560-2
86-74-8
59-50-7
106-47-8
111-91-1
111-44-4
ug/kg I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
uS/kS 1ug/kg 1
ug/kg 1
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
410
410
410
4't0
410
1 000
410
410
410
410
4',to
410
410
410
1000
410
410
410
410
410
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PQL = Practical quantitation limit B = D6t6cted in the method bl€nk E = Quantitation of compound sxc€€dod lhe calibration range H = Oul of holding timo
ND = Notdotected altrabovs th6 PQL J = Estimated r€sult< PQLand: MDL P = The RPD bgtwe€n two GC columns sxceeds 407o N = Rscovory is out ofcritoria
where applicable, all soil sample analysis ars reported on a dry weight basis unless flaggsd wi$ a nv'I
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: G of 58
Level 1 Reportv2.'l I
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Client:Terracon Consultants, lnc. Laboratory lD: OH01042-001
Description:AST-N Mafix: Solid
Date Sampled:07/30/2013 1500 % Solids: 76.6 08101120132203
Date Received : 08101 12013
Semivolatile Organic Compounds bv GC/MS
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 1 08/03i2013 0005 JRG O8t0212013 1438 26389
Parameter
cAs
Number
Analytical
Methort Result O
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bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h )anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Din itro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(l,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-N itIosodi-n-propylam ine
I xiffi:i*:^"nvramine(Diphenvramine)
2-Nitroaniline
I fiIiT"il:r:
2-NitrophenolI l.I'ffi1":i",",
I
1 08-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
84-74-2
117-84-O
53-70-3
132-64-9
91-94-l
120-83-2
84-66-2
131-11-3
1 0s-67-9
534-52-',!
51-28-5
121-14-2
606-20-2
117-81-7
206-44-O
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
1 93-39-5
78-59-1
91-57-6
95-48-7
106-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
87-86-5
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
82700
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
410
410
410
410
410
4'.t0
410
410
410
1000
410
410
410
410
1 000
1000
410
410
410
410
410
410
410
1000
4't0
410
410
410
410
830
410
4'.to
410
410
410
410
410
410
1 000
1000
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
udkS 1
ug/kS 'l
ug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
uS/kS 1ug/kS I
ug/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/lq 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
uS/kS 1
ug/kS 1
ug/kg 1
uS/kS 1ug/kg 1
ug/kg 1
I PCIL = Practical quantitation limil B = Detsct8d in the method blank E = Quantitation of compound exce€dsd the calibration rango H = Out of holding tims
ND = Notdetected atorabovothe PQL J = Estimat€d result< POLandi MDL P = The RPD betweon two GC columns €xceeds40% N = Recovery is outofcdteria
Wh6re applicable, all soil sample analysis are reporled on a dry wsight basis unloss flaggod with a nV"
Shealy Environmental Services, lnc.
I
106 VantaSe Point Drive W6st Columbia, SC 29172 [phone] Fax [phone]'l www.shealylab.com
Page: 7 of 58
Lovcl 1 Reportv2.'l
t
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-001
Description:AST-N Matrix: Solid
Date Sampled:07/30/2013 1500 % Solids: 76.6 08101120132203
Date Received: 08/01/2013
Semivolatile Orsanic Compounds bv GC/MS
I
I
IRun
1
Prep Method
3550c
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 0810312013 0005 JRG 0810212013 1438 26389
Parameter
cAs
Number
Analytical
Mathod Result O Units
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
85-01-8
1 08-95-2
129-00-0
95-95-4
88-06-2
Run 1 AcceptancoO % Recovery Limits
8270D
8270D
8270D
8270D
82700
410
410
410
410
410
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
I
I
I
ND
ND
ND
ND
ND
1
1
1
1
1
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
30Jt17
33-',t02
28-104
22-109
27-'.!03
41-120
MA EPH (aliphatics) - Unfractionated
73
53
64
63
71
49
I
I
Run
1
Prep Method
MADEP-EPH-
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
MADEP-EPH-o4 1 08105120131307 AMY 0810212013 0935 26616 I
Parameter
CAS Analytical
Number Method Result A
C19 - C36 Aliphatics - Unftactionated
C9 - Cl8 Aliphatics - Unfractionated
Surrogate
MADEP-EPH-O
MADEP-EPH-O
Run 1 Acceptance
% Recovery Llmits
ND
ND
13
13
mg/kg 1
mg/kg 1 I
1-Chloro-octadecane (aliphatic) - Unfractionated 81 40-140
MA EPH (aromatics) - Unfractionated
I
IRun Prep Mothod
1 MADEP.EPH-
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
MADEP-EPH-o4 1 08/05/20131307 AMY 0810212013 0935 26615
Parameter
CAS AnalyticalNumber Method Result O PQL Units I
C11 - C22 Aromatics - Unftactionated
Surrogate
MADEP.EPH.O
Run 1 Acceptancea 7o Recovery Limits
13ND mg/kg I
o - Terphenyl (aromatic) - Unfractionated
2-Fluorobiphenyl (fractionation 1 )
2-Bromonaphthalene (fractionation 2)
58
84
85
40-140
40-140
40-140 I
t
PQL = Practical quanlitation limit B = DEtected in the method blank E = Quantitation of compound exc€ed€d the calibration range
ND = Not detected at or abov6 the PQL J = Estimatsd result < PQL and: MDL P = The RPD botween two GC columns exc€eds 40%
wher6 applicablo, all soil sampls analysis are reporled on a dry weighi basis unloss flagged with a 'w"
H = Out of holding time
N = Rscovsry is out of critoria I
Shealy Environmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 8 of 58
L6vel'l Rsportv2.l I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-001
Description:AST-N Matrix: Solid
Date Sampled:07/30/2013 1500 % Solids: 76.6 08101120132203
Date Received : 08101 12013
MADEP VPH (aliphatics)
I Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 VPH MADEP-VPH-04-1.1 1 08t02t2013 2017 AWM 26434
CAS AnalyticalParameter Number Merhod Result O PQL Units RunI
I
C5 - CB Aliphatics
Cg - C12 Aliphatics
Surrogate
MADEP.VPH-O ND
MADEP-VPH-O ND
Run 1 AcceptanceO 7o Recovery Limits
3.9 mg/kg 1
3.9 mg/kg 1
2,S-Dibromotoluene (FlD) 86 70-130
t MADEP VPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 08t02t2013 2017 AWM 26436ICAS AnalyticalParameter Number Method Result O PQL Units Run
t C9 - C10 Aromatics
Surrogate
MADEP-VPH-O ND
Run 1 AcceptanceO % Recovery Limits
1.3 mg/kg 1
2,S-Dibromotoluene (PlD) 88 70-130I
I
I
I
I
I
I
I
I PQL = Prectical quantitation limit B = Detected in tha method blank E = Quantitation ofcompound exceeded thecalibralion range H = Outofholding tlmo
ND = Notdgtected atorabovethe PQL J = Estimated result< PQLand: MDL P = The RPD botween two GC columns excseds 40olo N = Recovery is outofcliteria
Whsro applicable, all soil sampls analysis are rsportod on a dry wslght basis unloss tlagged with a nV"
Shealy Environmental Services, lnc,
1
tOO VantaSe Point Driv6 West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Pcge: I of 58
Level I Roportv2.l
t
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-002
Description:AST-E Matrix: Solid
Date Sampled:07/30/2013 1505 % Solids: 77.4 0810112013 2203
Date Received: 08/01/2013
Volatile Organic Compounds by GC/MS
I
I
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 08t02t2013 2215 AAC
Batch Sample Wt.(g)
26418 6.02 I
Parameter
cAs
Number
Analytical
Mathad Result O Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-1 elra,chloroeth a ne
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-1 5-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
12448-1
106-93-4
9s-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
1 0061 -01-5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
'108-87-2
75-09-2
't0042-5
79-34-5
127-18-4
1 08-88-3
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
8260B
82608
82608
82608
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
82608
8260B
8260B
8260B
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
21
5.4
5.4
5.4
5.4
11
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
11
5.4
5.4
5.4
11
5.4
5.4
5.4
5.4
5.4
5.4
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ugftg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
I
I
I
I
I
I
I
I
I
I
I
I
I
POL = Practical quantitation limit B = DBtocted in ths melhod blank E = Quantitation of compound excssded ths calibration Enge H = Out of holding time
ND = Notdetectod atorabov6 the PQL J = EstimatBd result< PQLand: MDL P =The RPD betwesn two GC columns oxcoods 40% N = Rocovory is out ofcriteria
Where applicable, all soil sample analysis ar€ roported on a dry reight basis unless flagged with a 'W'I
Shealy Environmental S€rvic€s, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Page:10 of58
L6v€l 1 Reportv2.l
I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-002
Description: AST-E Matrix: Solid
Date Sampled:0713012013 1505 % Solids: 77.4 0810112013 2203
Date Received: 08/01/201 3
Volatile Organic Compounds by GC/MS
t Run Prep Method
1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 ',t 08t02t2013 2215 AAC
Batch Sample Wt.(g)26418 6.02
Parameter
CAS Analytical
Number Method Result O
ND
ND
ND
ND
ND
ND
ND
ND
I
I
I
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-5
79-01 -6
75-69-4
75-01-4
1330-20-7
Run I AcceptanceA % Recovery Limits
82608
8260B
82608
82608
82608
82608
82608
82608
5.4
5.4
5.4
5.4
5.4
5.4
5.4
5.4
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
I
I
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
113
92
103
53-142
47-138
68-124
Semivolatile Organic Compounds by GG/MS
t Run Prep Method1 3550C
Analytica! Method Dilution Analysis Date Analyst Prep Date Batch8270D 1 08t03t2013 003't JRG 08102t20131438 26389
Parameter
CAS Analytical
Number Method Result OI
I
t
t
I
t
I
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-C hloroethoxy)methane
bis(2-C hloroethyl)ether
83-32-9
208-96-8
98-86-2
120-12-7
't912-24-9
100-52-7
56-55-3
50-32-8
20s-99-2
191-24-2
207-08-9
92-52-4
1 01 -55-3
85-68-7
105-60-2
86-74-8
59-50-7
1 06-47-8
111-91-1
111-44-4
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
udkS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 'l
ug/kg 1
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
420
420
420
420
420
1 100
420
420
420
420
420
420
420
420
1 100
420
420
420
420
420
I PQL = Practical quanliiation limit B = Dotocted in the method blank E = Quantitation of compound 6xc6edsd the calibration range H = Out of holding timo
ND = Notdetscted atorabov9th6 PQL J = Estimated rosult< PQL and: MDL P =The RPD bstweon two GC columns exc€ods40% N = Rscovory is outofcaitoria
Where applicable, all soil sample analysis aro reportsd on a dry w€ight basis unless flagged with a .W'
Shealy Environmental Services, lnc.
I
,* Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: ll of5E
Levgl 1 Roport v2.1
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-002
Description: AST-E Matrix: Solid
Date Sampled:07/30/20131505 % Solids: 77.4 0810'1120132203
Date Received: 08/01/201 3
Semivolatile Organic Compounds by GG/MS
I
I
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 0810312013 0031 JRG 0810212013 1438 26389 I
Parameter
cAs
Number
Analytical
Math6d Result O Units Run
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenot
4,6-Diniho-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexach lorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-Nitrosodi-n-propylamine
N-Nitrosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
1 08-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
84-74-2
117-84-O
53-70-3
132-64-9
91-94-1
't20-83-2
84-66-2
1 31-1 1-3
1 05-67-9
534-52-1
51-28-5
121-14-2
606-20-2
't17-81-7
206-44-O
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
1 93-39-5
78-59-1
91-57-6
95-48-7
1 06-44-5
621$4-7
86-30-6
91-20-3
88-74-4
99-09-2
1 00-01-6
98-95-3
88-75-5
'too-02-7
87-86-5
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
420
420
420
420
420
420
420
420
420
1 100
420
420
420
420
1 100
1 100
420
420
420
420
420
420
420
1 100
420
420
420
420
420
8s0
420
420
420
420
420
420
420
420
1 100
1 100
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
USI(S 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 'l
I
I
I
I
t
I
I
I
I
I
I
I
I
PQL = Practical ouantitation limit B = Detected in the mEthod blank E = Quantitation of compound excoeded the calibration range H = Out of holding tims
ND = Not det€cted atorabove the PQL J = Estimated result< PQL and: MDL P = The RPD betw€€n two GC columns axceeds 40olo N = Recoveryisoutofcrit€ria
Where applicable, all $il sample analysis are reported on a dry wgight basis unlsss flaggsd with a nV.I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'11 www.shealylab.com
Page: 12 of 58
Lever I Roportv2.l
I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-002
Description:AST-E Matrix: Solid
Date Sampled:07/30/20131505 % Solids: 77.4 0810'1120132203
Date Received: 08/01/201 3
Semivolatile Orqanic Compounds bv GC/MS
I *1"Prep Method
3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 08t03t2013 0031 JRG 08t02t2013 1438 26389
Parameter
CAS Analytical
Number Mathad Result Ot
I
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
85-01 -8
1 08-95-2
129-00-0
95-95-4
88.06-2
Run 1 AcceptanceO % Recovery Limits
8270D
8270D
8270D
8270D
8270D
420
420
420
420
420
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
ND
,|
1
1
1
1
t
I
I
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
NitrobenzenedS
Phenol-d5
Terphenyl-d14
75 30-117
64 33-102
66 28-104
69 22-109
74 27-103
53 41-120
MA EPH (aliphatics)
I Batch
26358
Run
1
Prep ltethod
MADEP-EPH-
AnalyticalMethod Dilution
MADEP.EPH.O 'I
Analysis Date Analyst Prep Date
08t02t20132232 AMY 08/02/20130935
Parametel
CAS Analytica!
Number Method Resuh OICg - C18 Aliphatics
Cl9 - C36 Aliphatics
Surrogate
MADEP-EPH.O
MADEP-EPH-O
Run 1 AcceptanceO o/o Recovery Limits
mglkg I
mg/kg 1
ND
ND
12
12
t 1 -Chloro-octadecane (aliphatic)40-140
MA EPH (aromatics)I Run
,|
Prep Method
MADEP-EPH-
AnalyticalMethod Dilution
MADEP-EPH.O4 1
Analysis Date Analyst Prep Date Batch
08t03t20't3 1206 AMY 08t0212013 093s 26356
I Parametel
CAS AnalyticalNumber Methad Result O
C11 - C22 Aromatics
Surrogate
MADEP-EPH-O
Run ,| AcceptanceO % Recovery Limits
12 mg/kg
I
I
I
2-Bromonaphthalene (ftactionation 2)
2-Fluorobiphenyl (fractionation 1 )
o - Terphenyl (aromatic)
77
85
71
40-140
40-140
40-140
I PQL = Practical quanlitation limit B = Detecied in the mathod blank E = Quantitation of compound exceaded the calibration range
ND = Nol detected at or above ths PQL J = Estimated rssult < PQL and: MDL P = Tho RPD between two GC columns excsods 400/6
Where applicabls, all Boil sample analysis are roportsd on a dry w€ight basis unless flagg3d with a nlr
H = Out ot holding time
N = Rocovory is out of criteria
Shealy Environmental Services, lnc.
I
106 VantaSe Point Drive West Columbia, SC 29172 [phone] Fax [phone] t 1 www.shealylab.com
Page: l3 of58
Level 'l Raport v2.l
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042'002
Description:AST-E Matrix: Solid
Date Sampled:07/30/20131505 % Solids: 77.4 08101120132203
Date Received : 08101 12013
MADEP VPH (aliphatics)
t
t
IBatch
26434
Run
1
Prep Method
VPH
Analytical Method Dilution Analysis Date Analyst Prep Date
MADEP-VPH-04-1.1 ',t 0810212013 20s8 AWM
Parameter
CAS Analytical
Number Mathad Result O
C5 - C8 Aliphatics
C9 -C12 Aliphatics
Surrogate
MADEP-VPH.O
MADEP-VPH-O
Run 1 Acceptancea % Recovery Limits
ND
ND
3.6
3.6
I
I
mg/kg 1
mg/kg 'l
2,5-Dibromotoluene (FlD)70-1 30
MADEP VPH (aromatics)I
Batch
26436
Run
1
Prep Method
VPH
Analytica! Method Dilution Analysis Date Analyst Prep Date
MADEP-VPH-04-1.1 1 0810212013 2058 AWM I
Parameter
CAS Analytlcal
Number ilethod Result O
Cg - C10 Aromatics
Surogate
MADEP-VPH.O
Run 1 AcceptanceO o/o Recovery Limits
mg/kg I
2,5-Dibromotoluene (PlD)70-1 30 I
I
t
I
t
I
I
I
PQL = Practical quanftalion limit B = Dotectod in the method blank E = Quanlitation of compound sxc€sdsd the calibration rangs
ND = Not det8cted at or abov6 ths PQL J = Estimated result < PQL and: MDL P = The RPD betwoen two GC columns excosds /10%
where applicabls, all soil sample analysis ars rspolted on a dry weight basis unless flagged with a nV'
H = Out of holding time
N = Rocovory is out of criteria I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: l,t of 58
Level 1 Rsportv2.l I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-003
Description: AST-S Matrix: Solid
Date Sampled;0713012013 1515 % Solids: 70.5 0810112013 2203
Date Received : 08101 12O13
Volatile Orqanic Gompounds bv GC/MS
Run Prep Method
1 5035
Analytical Method Dilution Analysis Date Analyst82608 I 08102t20132239 AAC
Prep Date Batch Sample Wt.(g)
26418 6.47
Parameter
cAs
Number
Analytical
Marhort Result O Run
t
I
T
I
T
t
I
I
I
I
I
I
I
I
I
I
T
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-D ichloroethene
trans-1, 2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etnchloroethan e
Tetrachloroethene
Toluene
67-64-1
7',t-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
1 06-93-4
95-50-1
541-73-1
1 06-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
10061-02-6
104-41-4
591 -78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
100-42-5
79-34-5
't27-18-4
1 08-88-3
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
8260B
8260B
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
8260B
8260B
82608
82608
8260B
82608
8260B
8260B
82608
82608
82608
82608
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
us/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
22
5.5
5.5
5.5
5.5
't1
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
't1
5.5
5.5
5.5
11
5.5
5.5
5.5
5.5
5.5
5.5
PQL = Practical quantitation limit B = Detectod in tho method blank E = Quantitation of compound exceedsd the calibration range H = Out of holding time
ND = Notdotected atorabovethe PQL J = Estimatsd result< PQL and: MoL P =Tho RPD botwsen lwo cC columns excsods 40% N = Rscovery is outofclitoria
Whsre applicabls, all soil sample analysis are reporisd on a dry weight basis unless flaggod with a'W"
Shealy Envlronmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 (8O3) 791-9700 Fax [phone] www.shealylab.com
Page: l5 of58
Lovel 1 Roport v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OH01042'003
Description: AST-S Matrix: Solid
Date Sampled:07/30/20131515 % Solids: 70.5 08101120132203
Date Received : 08101 12013
Volatile Organic Compounds by GC/MS
I
I
Run Prep MethodI 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 08102120132239 AAC
Batch Sample Wt.(g)26418 6.47 I
Parameter
cAs
Number
Analytical
Marhod Result O
'1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1 ,1 , 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
75-01-4
1330-20-7
Run 1 AcceptanceO % Recovery Limits
8260B
82608
82608
82608
82608
82608
82608
8260B
ND
ND
ND
ND
ND
ND
ND
ND
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
t
I
I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-d8
121
94
109
53-142
47-138
68-124
I
ISemivolatile Organic Compounds by GC/MS
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 1 08/03/2013 0057 JRG 0810212013 1438 26389 t
Parameter
CAS Analytical
Number Method Result O Run
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
'1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
83-32-9
208-96-8
9&86-2
't20-12-7
1912-24-S
100-52-7
56-55-3
s0-32-8
205-99-2
't91-24-2
207-08-9
92-52-4
101-55-3
85-68-7
105-60-2
86-74-8
59-50-7
1 06-47-8
111-91-1
't1144-4
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
460
460
460
460
460
1200
460
460
460
460
460
460
460
460
1 200
460
460
460
460
460
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg I
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uSftS 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ug/kg 1
ug/kg 1
I
t
I
I
I
t
I
PQL = Prac,lical quantitation limit B = Detecled in the mslhod blank E = Quantitation ofcompound exc€oded the calibration range H = Out of holding time
ND = Not dstected atoraboveth6 PQL J = Estimated r€€ult< PQL and: MDL P = The RPD betw€on two GC @lumns oxc€sds 40% N = Rocovsryis out ofcriteria
Whero applimble, all soil sample analysls are roported on a dry wgight basis unloss flagged with a nV"I
Shealy Environmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shoalylab.com
Page: 16 of 58
Levol 1 Roportv2.l
I
I
t
I
Client:Terracon Consultants, lnc. Laboratory ID: OH01042-003
Description:AST-S Matrix: Solid
Date Sampled:07/30/2013 1515 % Solids: 70.5 0810112013 2203
Date Received: 08/01/2013
Semivolatile Orqanic Compounds bv GC/MS
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 08t03t20'r3 0057 JRG 08t02t20131438 26389
Parameter
cAs
Number
Analytical
Marhod Result O
I
t
I
I
I
I
t
I
T
I
I
I
I
I
I
I
I
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
460
460
460
460
460
460
460
460
460
1200
460
460
460
460
1200
1200
460
460
460
460
460
460
460
1200
460
460
460
460
460
930
460
460
460
460
460
460
460
460
1200
1200
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h )anth racene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutradiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-N itrosod i-n-propylamine
N-Nitrosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
1 08-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
84-74-2
117-84-0
53-70-3
132-64-9
91-94-1
120-83-2
84-66-2
131-11-3
105-67-9
534-52-1
51-28-5
121-14-2
606-20-2
117-81-7
206-44-0
86-73-7
1',t8-74-',1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
106-44-5
62',t-64-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-7s-5
100-02-7
87-86-5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ug/kg 1ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
udkS 1
ug/kg 1ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kS 1
uS/ks 1ug/kg 1ug/kg I
ug/kg 1uS/kS 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kS 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ug/kg 1udkS 1
ug/kg 1
PQL = Practical quantitation limil B = D6t6cied in ih6 method blank E = Quantitation of compound oxcseded the calibration rang6 H = Out of holding tlme
ND = Notdstsctsd atorabovelho POL J = Estimated r€sult< POL and: MDL P =The RPD betwsen two GC columns exceeds 40% N = Recovery is out ofcriteria
Where applicable, all soil sample analysls ars roported on a dry weight basls unless flagged with a ryV"
Shealy Environmental SeNices, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 17 of 58
Level 1 Report v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-003
Description: AST-S Matrix: Solid
Date Sampled:0713012013 1515 % Solids: 70.5 0810112013 2203
Date Received: 08/01/201 3
Semivolatile Organic Compounds by GC/MS
I
I
tRun
,|
Prep Method
3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 08/03/2013 0057 JRG 0810212013 1438 26389
Parameter
CAS Analytical
Number Method Result O
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
85-01 -8
108-95-2
129-00-0
95-95-4
88-06-2
Run 1 AcceptanceO 016 Recovery Limlts
82700
8270D
8270D
8270D
8270D
ND
ND
ND
ND
ND
460
460
460
460
460
I
I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
71
54
63
62
71
56
30-117
33-102
28-104
22-109
27-103
41-120
MA EPH (aliphatics)
I
I
I
Batch
26358
Dilution
,|
Run
1
Prep Method
MADEP-EPH.
Analytical Method
MADEP.EPH.O4
Analysis Date Analyst Prep Date
08/03/2013 1333 AMY 08/0212013 0935 I
cAs
Number
Analytical
Parameter
C9 - C18 Aliphatics
C19 - C36 Aliphatics
Surrogate
MADEP-EPH-O
MADEP-EPH.O
Run 1 AcceptanceO % Recovery Limitg
t
1 -Chloro-octadecane (aliphatic)40-140
MA EPH (aromatics)
I
IBatch
26356
Run
1
Prep Method
MADEP-EPH.
Analytical Method Dilution Analysis Date Analyst Prep Date
MADEP-EPH-o 1 08t02t20132301 AMY 08/0212013 0935
Parameter
cAs
Number
AnalyticalMaihod Result O I
Cl1 -C22Aromatics
Surrogate
MADEP-EPH-O
Run 1 AcceptanceO % Recovery Limits
14 mg/kg I
2-Bromonaphthalene (ftactionation 2)
2-Fluorobiphenyl (ftactionation'l )
o - Terphenyl (aromatic)
66
70
64
40-140
40-140
40-140 I
I
PQL = Practical quanftafon limit B = Detecled in the method blank E = Quantitation of compound excoed8d the calibmtion range
ND = Not detected at or above th6 PQL J = Estimatod result < PQL and: MDL P = Tho RPD betw€en two GC columns exceods 40olo
Whers applicabl€, all soil sampla analysis are reported on a dry weight basis unless rlagged wilh a 'W'
H = Out of holding time
N = Recovery is out of critoria I
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia,SG 29172 [phone] Fax[phone] www.shealylab.com
Page: l8 of58
Level 1 R€port v2.1 I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-003
Description:AST-S Matrix: Solid
Date Sampled:0713012013 1515 % Solids: 70.5 0810112013 2203
Date Received : 08101 12013
MADEP VPH (aliphatics)
t
I
I
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 VPH MAOEP-VPH-04-1.1 1 08t02t20't3 2139 AWM 26434
CAS AnalyticalParameter Number Marhod Result O PQL Units Run
C5 - C8 Aliphatics
C9 - C12 Aliphatics
Surrogate
MADEP.VPH.O ND
MADEP-VPH-O ND
Run 1 AcceptanceA % Recovery Limits
4.0 mglkg 1
4.0 mg/kg 1
2,S-Dibromotoluene (FlD) 77 70-130
I MADEP VPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 VPH MADEP-VPH-04-1.1 1 08t02120132139 AWM 26436I
I
CAS AnalyticalParameter Number Mcrhar{ Result a PQL Unlts Run
C9 - C10 Aromatics
Surrogate
MADEP-VPH-O ND
Run 1 AcceptanceO % Recoverv Limits
1.3 mg/kg 1
2,s-Dibromotoluene (PlD) 77 70-130I
I
T
t
I
I
t
I
I PQL ' Practical quantltation limit B = Detectod in ths method blank E = Quantitation ofcompound oxce€ded thecalibration range H = Outofholdinglimg
ND = Notdstected atorabovo the PQL J = Estimated result < POLand: MDL P = The RPD bstweon two GC mlumns exc66ds 40% N = Recov€ry is oul ofcritoria
Where applicabls, all soil sample analysis ar€ rsported on a dry reight basis unless flaggsd with a nV"
Shealy Environmental Services, lnc.
!
,06 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 19 of58
Levol 1 Reportv2.l
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-004
Description: AST-W Matrix: Solid
Date Sampled:0713012013'1525 % Solids: 74,5 0810112013 2203
Date Rec€ived: O8lO1 120'13
Volatile Organic Compounds by GC/MS
I
I
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 1 0810212013 2303 AAC
Batch Sample Wt.(g)
26418 6.'t0 I
Parameter
cAs
Number
Analytical
Method Result O Units Run
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
I ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1, 1,2,2-F et.a, chloroeth ane
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
10646-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
1 00-41-4
591-78-6
98-82-8
79-20-9
't634-04-4
108-10-1
108-87-2
75-09-2
100-42-5
79-34-5
127-18-4
108-88-3
82608
8260B
82608
82608
82608
8260B
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
8260B
82608
8260B
82608
82608
8260B
82608
8260B
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
22
5.5
5.5
5.5
5.5
11
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
11
5.5
5.5
5.5
11
5.5
5.5
5.5
5.5
5.5
5.5
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug&g 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
uglkg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
t
t
t
I
I
I
I
I
I
I
I
I
I
PQL = Practical quantitation limit B = Detectod in the method blank E = Quantiiation of compound 6xce6ded the calibration range H = Out of holding timo
ND = Notdetectod 6torabovethe PQL J = Estimatsd result< POLand: MDL P =The RPD between two GC columns oxce€ds 40% N = Recoveryisoutofcriteria
Where applicable, all soil sample analysis aro roported on a dry weight basis unless flagg6d with a'W"I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 20 of 58
Lavsl I Reportv2.l
I
I
I
I
Client:Terracon Consultants, lnc, Laboratory lD: OH01042-004
Description:AsT-W Matrix: Solid
Date Sampled:0713012013 1525 % Solids: 74.5 0810112013 2203
Date Received: 08/01/2013
Volatile Orqanic Compounds by GC/MS
t Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date82608 1 08t02t2013 2303 AAC
Batch Sample Wt.(g)26418 6.10
Parameter
CAS Analytical
Number Mathnd Result OI
I
I
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1 ,1 , 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1 82608
120-82-1 82608
71-55-6 82608
79-00-5 82608
79-01-6 82608
75-69-4 82608
75-01-4 82608
1330-20-7 82608
Run 1 AcceptanceO % Recovery Limits
5.5
5.5
5.5
5.5
5.5
5.5
5.5
5.5
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kg 1ug/kg 1
I
I
1,2-Dichloroethaned4
Bromofluorobenzene
Toluene-d8
123
90
104
53-142
47-138
68-',t24
Semivolatile Organic Gompounds by GG/MS
T
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
82700 1 08103t20130123 JRG 08102120131438 26389
Parametel
CAS Analytical
Number Method Result OI
I
I
T
t
I
I
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
83-32-9
208-96-8
98-86-2
120-12-7
1912-24-9
100-52-7
56-55-3
50-32-8
205-99-2
't91-24-2
207-08-9
92-52-4
1 01 -55-3
85-68-7
1 05-60-2
86-74-8
59-50-7
106-47-8
111-91-1
111-44-4
ug/kg 1
uS/kS 1ug/kg 1
ug/kg Iug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ug/kg 1ug/kg 1
ug/kg 1ug/lq 1
uSftS 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kg 1
uS/kS 1
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
82700
82700
82700
8270D
8270D
8270D
8270D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
440
440
440
440
440
1 100
440
440
440
440
440
440
440
440
1 100
440
440
440
440
440
I PQL = Practical quantitation limit B = Detectod in the msthod blank E = Quantitalion of compound oxceeded the calibratlon rang€
ND = Notdet6ct6d atorabovetha PQL J o Eslimated rosult< PQL and: MDL P = The RPD b6tw€€n two GC @lumns excesds 40olo
Wh6re applicable, all soil samplo analysis are reported on a dry wsight basis unless flagged with a .W'
H = Out ot holding timo
N = Recovery is out ot critsria
Shealy Envlrcnmental Servic€s, lnc.
I
,* Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:21 of58
Lavel 1 R@ort v2.1
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-004
Description:AsT-W Matrix: Solid
Date Sampled:0713012013 1525 % Solids: 74.5 0810112013 2203
Date Received : OBl01 12O13
Semivolatile Organic Compounds bv GC/MS
I
I
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 0810312013 0',123 JRG 0810212013 1438 26389 I
Parameter
cAs
Number
Analytical
Method Result O Units Run
bis(2-Ch loroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Din itro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutradiene
Hexach lorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenot
N-Nitrosod i-n-propylamine
N-Nitrosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentrachlorophenol
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
84-74-2
117-84-0
53-70-3
132-64-9
91-94-1
120-83-2
84-66-2
131-11-3
105-67-9
534-52-1
51-28-5
121-14-2
606-20-2
117-81-7
206-44-O
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
I 93-39-5
78-59-1
91-576
95-48-7
106-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
87-86-5
82700
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
82700
82700
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
440
440
440
440
440
440
440
440
440
1 100
440
440
440
440
1't00
1 100
440
440
440
440
440
440
440
1 100
440
440
440
440
440 I
890
440
440
440
440
440
440
440
440
1 100
1 100
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
ug/kg I
udkg 1
ug/kg 1
ugftg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
I
t
t
I
I
T
I
I
I
t
T
I
I
PQL = Practical quantitation limit B = Detecied in the method blank E = Quantitation of compound oxGeded th6 €libratim range H = Out of holding timo
ND = Notdeiocted atorabo\rolhe PQL J = Estimated result< PQLand: MDL P = The RPD betwEen two GC columns oxceeds 40% N = Recoveryis outofcriterla
Where applicable, all soil sample analysis ar€ reported on a dry wsight basis unless flaggsd with a $,.t
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 22 of 5E
Lever 1 Reportvz.l
I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-004
Description:AsT-W Matrix: Solid
Date Sampled:0713012013 1525 % Solids: 74.5 08/0112013 2203
Date Received : 08101 12013
Semivolatile Orqanic Compounds bv GC/MS
I Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 3s50C 8270D 1 08t03t20130123 JRG 08102120131438 26389
I
I
I
I
CAS AnalyticalParameter Number Marhort Result O PQL UniG Run
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
85-01-8 8270D ND
108-95-2 8270D ND
129-00-0 8270D ND
95-95-4 82700 ND
88-06-2 8270D ND
Run 1 AcceptanceO % Recovery Limits
440 ug/kg 1
440 ug/kg 1
440 ug/kg 1
440 ug/kg 1
440 ug/kg 1
2,4,6-Tribromophenol 66 30-117
2-Fluorobiphenyl 53 33-102
2-Fluorophenol 63 28-104
Nitrobenzene-ds 65 22-1Og
Phenol-d5 70 27-103
Terphenyl-d14 69 41-120
T MA EPH (aliphatics)
I Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 MADEP-EPH- MADEP-EPH-o4 ',t 08t03t20131402 AMY 08t0212013 0935 26358
CAS AnalyticatPalameter Number Method Result O PQL Units RunICg - C18 Aliphatics
C19 - C36 Aliphatics
Surrogate
MADEP-EPH-O ND
MADEP-EPH-O ND
Run 1 AcceptanceO % Recovery Limits
13 mg/kg 1
13 mS/kS 1
I
I
1-Chloro-octadecane (aliphatic) 70 40-140
MA EPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-o 1 08t02t20132330 AMY 08t02120130935 26356
I CAS AnalyticalParameter Number Marhart Result O PQL Units Run
C11 - C22 Aromatics
Surrogate
MADEP.EPH-O ND
Run I AcceptanceO % Recovery Limits
13 mg/kg 1
I
I
I
2-Bromonaphthalene (fractionation 2) 48 40-140
2-Fluorobiphenyl (ftactionation 1) 73 40-140
o - Terphenyl (aromatic) 65 40-140
I PQL = Practical quantitation limit B = D6t6cted in th6 method blank E = Quantitation ofcompound excseded the calibration range H = Outofholding time
ND = Notdetscted atoraboveth6 PQL J = Estimaled resutt< PQL and: MDL P = The RPD betweon two GC columns sxcseds 40% N = Recoveryisoutofcritoria
Where applicable, all soil sample analysis are reported on a dry woight basis unless f,agged with a "\ /"
Shealy Environmental Services, lnc.
I
106VantaSePointDrive WestColumbia, SC 29172 [phone] Fax(803)79t-9111 www.shealylab.com
Page: 23 of 58
Level 1 R€portv2.l
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042.004
Description: AST-W Matrix: Solid
Date Sampled:0713012013 1525 % Solids: 74.5 0810112013 2203
Date Received: 08/01/201 3
MADEP VPH (aliphatics)
I
I
IBatch
26434
Run
1
Prep Method
VPH
Analytical Method Dilution Analysis Date Analyst Prep Date
MADEP-VPH-04-1.1 1 0810212013 2219 AWM
Parameter
CAS Analytical
Number Method Result O
C5 - C8 Aliphatics
C9 - C12 Aliphatics
Surrogate
MADEP.VPH.O
MADEP.VPH.O
Run I AcceptanceO 06 Recovery Llmits
ND
ND
3.5
3.5
I
I
mg/kg 1
mg/kg 1
2,5-Dibromotoluene (FlD)70-130
MADEP VPH (aromatics)I
Batch
26436
Run
1
Prep Method
VPH
Analytical Method Dilution Analysis Date Analyst Prep Date
MADEP-VPH-04-1.1 1 08102120132219 AWM
Parameter
CAS AnalyticalNumber Meihod Result O
I
C9 - C10 Aromatics
Surrogate
MADEP-VPH.O
Run I AcceptanceO % Recovery Limitg T
1.2 mg/kg
2,5-Dibromotoluene (P I D)70-130 t
I
I
I
I
I
T
I
PQL = Pmclical quantitation limlt B = Detectsd in the method blank E = Quantitation of compound exc66dod ho calibraiion range
ND = Not dotected at or above the PQL J = Estimatsd result < PQL and: MOL P = The RPD betwoon two GC columns exceeds 40%
Where applicable, all soll sample analysis are roportsd on a dry wsight basis unloss flagged with a n\r"
H = Out of holding time
N = Recovery is out of criteria I
Shealy Environmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyhb.com
Page: 24 of 58
Levsl 1 Report v2.1 I
t
I
I
Client:Terracon Gonsultants, lnc. Laboratory lD: OH01042-005
Description:AsT-B Makix: Solid
Date Sampled:07/30/20131530 % Solids: 71.8 08101120132203
Date Received : 08101 12013
Volatile Organic Compounds by GC/MS
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 1 08102120132327 AAC
Batch Sample Wt.(g)
264',18 5.86
Parameter
cAs
Number
Analytical
Marhod Result A Run
I
t
I
I
I
I
I
I
T
I
I
I
I
I
I
T
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
't , 1-Dichloroethene
cis- 1,2-Dichloroethene
trans- 1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropen€
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2-T etachloroeth a ne
Tetrachloroethene
Toluene
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
110-82-7
96-12-8
124-48-1
106-93-4
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
1 0061 -01 -5
1 0061 -02-6
100-41-4
591-78-6
98-82-8
79-20-9
1634-04-4
1 08-1 0-1
108-87-2
75-09-2
1 00-42-5
79-34-5
127-18-4
108-88-3
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/(S 1
ug/kg 'lug/kg 1
ug/kg 1
ug/kg 1
ug/tg 1
ug/kg 1
uS/kg 1
ug/kg 1
ug/kg 1ug/kg 1
ug/kg 1
udkg 1
udkS 1
udks 1
uSfl(S 1
ug/kg 'lug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
ug&g 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kS I
ug/kg 'l
uS/kS 1
ug/kg 1
ug/kg 1
8260B
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
8260B
82608
82608
8260B
82608
82608
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
82608
8260B
82608
82608
82608
82608
82608
82608
82608
82608
8260B
82608
82608
82608
82608
82608
8260B
82608
82608
82608
8260B
82608
24
5.9
5.9
5.9
5.9
12
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
12
5.9
5.9
5.9
12
5.9
5.9
5.9
5.9
5.9
5.9
PQL = Practical quantitation llmii B = D6t6cted in the msthod blank E = Quantitation ofcompound exceeded the calibration range H = Out of holding time
ND = Notdotected atorabovo ths PQL J = Estimated result< PQLand: MDL P = The RPD betwesn two GC columns excoeds 40olo N ' Rocovgryisoutofcritorla
wh6re applicable, all soil sample analysis are rsporled on a dry w€ight basis unless flagged with a "W.
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 25 of 58
Levol 1 Report v2.1
Client:Terracon Consultants, lnc, Laboratory lD: OH01042-005
Description:AST-B Matrix: Solid
Date Sampled:07/30/2013 1530 % Solids: 71.8 0810112013 2203
Date Received : OBIO1 120'13
Volatile Orqanic Compounds by GC/MS
I
t
Run Prep Method1 5035
Analytical Method Dilution Analysis Date Analyst Prep Date
82608 ',t 08t0212013 2327 AAC
Batch Sample Wt.(g)
26418 5.86 I
Parameter
cAs
Number
Analytical
Method Result O POL Units Run
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
76-13-1 82608
'120-82-1 82608
71-55-6 82608
79-00-s 82608
79-0',1-6 82608
75-69-4 82608
75-01-4 82608
1330-20-7 82608
Run 1 AcceptanceO % Recovery Llmits
ND
ND
ND
ND
ND
ND
ND
ND
5.9
5.9
5.9
5.9
5.9
5.9
5.9
5.9
t
I
I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
1,2-Dichloroethane-d4
Bromofluorobenzene
Toluene-dB
53-142
47-138
68-124
Semivolatile Organic Compounds by GC/MS
I
I
130
96
105
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 1 0810312013 0149 JRG 08/0?,20131438 26389 I
Palameter
cAs
Number
Analytical
Method Result O Units Run
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
83-32-9
208-96-8
98-86-2
120-12-7
1912-24-S
100-52-7
s6-55-3
50-32-8
205-99-2
191-24-2
20748-9
92-524
101-55-3
85-68-7
105-60-2
86-74-8
59-50-7
106-47-8
1 1 1-91-1
111-44-4
8270D
8270D
82700
82700
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
82700
8270D
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg I
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
I
T
I
I
I
T
I
440
440
440
440
440
100
440
440
440
440
440
440
440
440
100
440
440
440
440
440
PQL = Practical quantitation limlt B = D6i6ciad in tho mothod blank E = Ouantltation of compound oxcosdod ths calibration range H = Out of holding time
ND=NotdatectodatorabovethePC|L J=Estimatedresult<PQLand:MDL P=TheRPDbetwesntwoGCcolumnso(ceeds40% N=Rscoveryisoutofcrileria
Wherc appllcable, all soil samDle analysis are roported on a dry weight basis unl€ss flagged with a "w"I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 26 of 58
Level'l Reportv2.l
I
t
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042.005
Description: AST-B Matrix: Solid
Date Sampled:07/30/20131530 % Solids: 71.8 08101120132203
Date Received: 08/01/2013
Semivolatile Orqanic Compounds bv GC/MS
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 08103t2013 0149 JRG 08102120',t31438 26389
Parameter
cAs
Number
Analytical
Mcthad Result O Units
I
I
I
I
I
t
I
I
I
I
I
t
I
I
I
t
I
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexach lorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-N itrosod i-n-propylam ine
N-Nitrosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
1 08-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
84-74-2
117-84-0
53-70-3
132-64-9
91-94-1
120-83-2
84-66-2
't31-1',t-3
1 05-67-9
534-52-1
51-28-5
121-14-2
606-20-2
117-8't-7
206-44-O
86-73-7
118-74-1
87-68-3
77-474
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
106-44-5
621-64-7
86-30-6
91.20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
87-86-5
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
440
440
440
440
440
440
440
440
440
1 100
440
440
440
440
1 100
1 100
440
440
440
440
440
440
440
1 100
440
440
440
440
440
890
440
440
440
440
440
440
440
440
1 100
1 100
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ug/kg 1
ug/kg 1
ug/kS 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1ug/kg 1
ug/kg 1
ug/kg 1
USI(S 1
ug/kg 1
ug/kg 1
ug/kg 1
udks 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1ug/kg 1
uglkg I
PQL = Practical quantiiation limit B = Detectsd in tha method blank E = Quantitation of compound excesded the calibralion range H = Out of holding timo
ND = Not detected atorabovethe PQL J = Estimated result< PQLand: MDL P = The RPD botween two GC columns exc66ds4070 N = Recoveryis outofcdtaila
Whers applicable, all soil sampls anaf)rsis are reporled on a dry woigil basis unless flagged witi a 'W"
Shealy Environmental Services, lnc.
106 Vantage Point Driv€ West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 27 of 58
Levol 1 RsportY2.'l
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-005
Description:AST-B Matrix: Solid
Date Sampled:07/30/2013 1530 % Solids: 71.8 08101120132203
Date Received :08101 12013
Semivolatile Organic Compounds by GC/MS
I
I
IRun
1
Prep Method
3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 1 0810312013 0149 JRG 0810212013 1438 26389
Parameter
CAS
Number
Analytical
Merhod Result O
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Sunogate
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
Run 1 AcceptanceA % Recovery Limits
82700
82700
8270D
8270D
8270D
I
I
ND
ND
ND
ND
ND
440
440
440
440
440
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
30-117
33-102
28-104
22-109
27-103
41-120
MA EPH (aliphatics) - Unfractionated
71
59
62
68
72
78
I
I
t
tRun
I
Prep Method
MADEP.EPH.
Analytica! Method Dilution Analysis Date Analyst Prep Date Batch
MADEP-EPH-o 1 08/05/2013 1406 AMY 08/02/20130935 26616
Parameter
CAS Analytical
Number Method Result O POL Units Run
C19 - C36 Aliphatics - Unfractionated
Cg - Cl8 Aliphatics - Unftactionated
Surrogate
MADEP.EPH-O
MADEP.EPH.O
Run 1 Acceptance
% Recovery Limits
mg/kg 1
mg/kg 1
ND
ND
14
14 t
1-Chloro-octadecane (aliphatic) - Unfiactionated 40-140
MA EPH (aromatics) - Unfractionated
t
tBatch
26615
Run
1
Prep Method
MADEP-EPH-
Analytical Method Dllution Analysis Date Analyst Prop Datc
MADEP-EPH-0 1 08/05/2013 1406 AMY 08/02/2013 0935
Parameter
CAS AnalyticalNumber Mathorl Result O I
C11 - C22 Aromatics - Unfractionated
Surrogate
MADEP-EPH-O
Run 1 AcceptanceO 96 Recovery Limlts
14 mg/kg I
o - Terphenyl (aromatic) - Unfractionated
2-Fluorobiphenyl (ftactionation 1 )
2-Bromonaphthalene (fractionation 2)
65
84
85
40-140
40-140
40-140 T
I
PCIL = Practical quantitation llmit B = Detected in he mathod blank E = Quantitation of compound excoedod he calibration range
ND = Not dotectsd at or abov6 th€ PQL J = Estimatod rsult < PQL and: MDL P = The RPD between two GC columns excoeds 40%
Where applicable, all soilsample analFis are reported on a dry woight basis unlcss flaggod wi$ a nv"
H = Out of holding time
N = Ro@very is out of criteria I
Shealy Environmental Services, lnc,
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] wurt,.shealylab.com
Page: 28 of 58
L6vel'l Reportv2.'l t
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01042-005
Description:AsT.B Matrix: Solid
Date Sampled:07/30/2013 1530 % Solids: 71.8 0810112013 2203
Date Received :08101 12013
MADEP VPH (aliphatics)
T
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch1 VPH MADEP-VPH-04-1.1 1 08t02t2013 2300 AWM 26434
CAS AnalyticalParameter Number Mcrhod Result O PQL Units RunI
I
C5 - C8 Aliphatics
Cg - C12 Aliphatics
Surrogate
MADEP-VPH-O ND
MADEP-VPH-O ND
Run 1 AcceptanceO o/o Recovery Limits
4.4 mg/kg 1
4.4 mg/kg 1
2,S-Dibromotoluene (FlD) 78 70-130
I MADEP VPH (aromatics)
Run Prep Method Analyrtica! Method Dilution Analysis Date Analyst Prep Date Batch1 VPH MADEP-VPH-04-1.1 1 08102t2013 2300 AWMt
t
CAS AnalyticalParameter Number Marhart Result O POL Unlts Run
C9 - C10 Aromatics
Surrogate
MADEP-VPH.O ND
Run 1 AcceptanceO % Recovery Limits
1.5 mg/kg 1
2,$Dibromotoluene (PlD) 81 70-130t
I
t
I
T
I
t
I
I PQL = Practical quantitation llmit B = Dstocted inthe mothod blank E = Quantitation ofcompound excseded the calibration range H = Outofholding tlme
ND = Notdetected at orabovethe PQL J = Estimated result< PQL and: MDL P =The RPD between two GC columns exceeds40% N = Rscovaryis outofcriterla
Whore applicable, all soil samplo analysis are reported on a dry weight basis unless llagged with a "U/'
Shealy Environm€ntal Services, lnc.
I 106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
T
Page: 20 of 58
Lovel I Roportv2.l
I
QC Summary
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 (803) 7S1-9700 Fax [phone] www.shealylab.com
Page: 30 of 58
Level I Reportv2.l
I Volatile Organic Compounds by GC/MS - MB
I Sample lD: Oe2641 8,00'1
Batch:26419
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
t Parameter a Dil PQL Units Analysis Date
t
I
I
I
t
I
I
I
I
I
I
I
I
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
Cyclohexane
1,2-Dibromo-3-chloropropane (DBCP)
Dibromochloromethane
1,2-Dibromoethane (EDB)
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Dichlorodifl uoromethane
1 ,2-Dichloroethane
1 ,'l -Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1 ,1 -Dichloroethene
'l ,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
4-Methyl-2-pentanone
Methylcyclohexane
Methylene chloride
Styrene
1,1,2,2 -T elr achloroeth ane
Tetrachloroethene
Toluene
1, 1,2-Trichloro-1,2,2-Trifl uoroethane
1,2,4-Trichlorobenzene
1,1,1 -Trichloroethane
1, 1,2-Trichloroethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10
5.0
5.0
5.0
't0
5.0
5.0
5.0
5.0
ug/kg
ug/kg
ug/kg
ugikg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
u9/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
08to2t20132113
081021201321',t3
08t02120132113
08t02120132113
08t02/2u32113
08to2120132113
o8to2l20'132113
08102120132113
08102120132113
08102120132113
08to4201321'.t3
08t02120132113
08t02t20132'.t13
08102120132113
0810?/20132113
08t02120't32113
o8t02t20132113
08to?,20132113
08t02t20132113
08102120132113
08t0?i20fi2113
08t02t20132113
08t02120132'.t13
o8t02120132113
08n,,2u32113
08102120132113
08t02120132113
08t0212013 21't3
08102120132113
o8to2120132113
08t02t20132113
08102120132113
08t02120132113
08t02t20132113
o8to2120132113
08t02120132113
08t02t201321',t3
o8t02120132113
08t02120132113
08102120132113
08/0?,20132113
o8toa20't32113
0810212013 2'.t'.t3
08t02120132113
5.0
5.0
5.0
5.0
5.0
5.0
I
T
PQL = Practical quantitation limit
ND = Not detectod at or abovs tho PQL
P = The RPD betwesn two GC @lumns excsgds 40% N = Recovery is out of criteria
J = Estimated result < PCIL and > MDL + = RPD is out of criteria
where applicable, all soil sample analysis ara reportod on a dry weight basis unloss flagged with a .w'
Note: Calculations are performed before roundlng to avoid round-off errors in calculated results
Shealy Environmential SeMces, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:3t of58
Lovel 1 Report v2.l
t
IVolatile Organic Compounds by GC/MS - MB
Sample lD: OQ26418-001
Batch:26418
Analvtica! Method: 82608
Matrix: Solid
Prep Method: 5035 I
IPalameteroDit POL Units Analysis Date
Trichloroethene
Trich lorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
I
I
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
o
1
1
1
1
AcceptanceLlmit
5.0
5.0
5.0
5.0
08t02t20't32113
08t02t20132113
08/022013 2113
oaoa2u32113
% Rec
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
109
120
112
47-138
53-142
68-124 I
t
I
I
t
I
I
I
I
T
I
PQL = Practical quantitation limit
ND = Not dotocled al or above the PQL
P = Ths RPD betwesn two GC columns excBeds 40% N = Recovery is out of criteria
J = Estimated result < PQL and : MDL + = RPD is out of ctiteria I
tWhor6 applicable, all soil sampla analysis aro roportod on a dry weight basis unless flagged with a nv"
Note: Galculatlons are performed before rounding to avoid round.off erroB in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 32 of 58
Lsvel'l Reportvz.l
I
I Volatile Organic Compounds by GC/MS - LCS
I Sample lD: Oe26418-002
Batch:264.t8
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I Parameter
SpikeAmount Result % Rec(us/ks) (us/ks) O Dit % Rec Limit Analysis Date
Acetonet 3iJii1""n,,.",",n"."
Bromoform
t ;]3H[flilr".',X"th,
bromide)
I Carbon disulfide
Carbon tetrachlorideI :li::::r1"J"
100
50
50
50
50
100
50
50
50
50
83
44
41
43
38
93
39
40
43
38
41
39
43
45
42
44
43
44
44
40
41
41
42
43
42
42
42
42
44
87
44
47
42
90
44
41
43
46
42
41
39
44
40
43
83
88
82
85
76
93
79
79
86
76
82
77
86
91
84
87
86
88
88
80
82
83
84
86
84
85
84
84
88
87
88
93
84
90
87
82
86
92
85
83
77
87
79
86
42-149
69-1 23
69-121
61-1 1 9
1 0-168
57-148
58-122
58-136
59-129
42-163
71-125
34-1 34
53-1 39
55-125
66-1 19
74-124
52-133
51-134
57-131
10-157
67-129
71-127
68-131
70-122
69-138
72-124
70-124
70-126
59-128
54-137
50-136
59-137
70-130
60-134
41-144
70-130
54-136
69-132
45-150
61-129
49-136
34-145
63-128
55-128
08t02t20131711
0810212013 1711
08t02120131711
0810212013 1711
a810212013 1711
08102t20131711
08102120131711
08102120131711
08t02120131711
08102120131711
oaoznu!1711
08/02120131711
08t02120131711
08102120131711
o8toa2u3171'.l
08102120131711
o8nz2013171',1
o8loa20131711
08102120131711
08t02/2u31711
08102120131711
o8lo2l20't3't711
08102120131711
08t02120131711
08102t201317'.!1
0ao2l20't3 1711
0810z2u31711
08t02t201317't1
oaoa2013 1711
0810a20131711
08t0?,2013171'.
08102t20131711
0810u2013171',|
08102t2013'.t711
08102t20131711
08102t20131711
08102t201s 1711
oaoa2013 1711
08102t20't31711
08/0?J201317'.t1
0810u20131711
08t0?,20131711
08102t20131711
o8l0a2u3'1711
Chloroform 50
I Chloromethane (Methyl chloride) 50
t :::3Hil:r-chroropropane (DB.P) ::
Dibromochloromethane 50
I 1,2-Dibromoethane (EDB) 50
I 1,4-Dichlorobenzene 50'1,3-Dichlorobenzene 50
1.z-Dichlorobenzene 50
I Dichlorodifluoromethane 50
I 1,z-Dichloroethane so
1,1-Dichloroethane 50
I trans-1,2-Dichloroethene 50
I cis-1,2-Dichloroethene 50
1,1-Dichloroethene 50
1.2-DichlorooroDane 50
I trans-1,3-Dichloropropene 50
I cis-1,3-Dichloropropene 50
Ethylbenzene
I ',o.[:;;,il",=","
Methyl acetate
50
100
50
50
Methyl tertiary butyl ether (MTBE) 50
I 4-MethyF2-pentanone 1oo
I Methylcyclohexane 50
Methylene chloride 50
ll Styrene 50
t 1,1,2,2-Tetachtoroethane 50Tetrachloroethene 50Toluene 50
t l:l:i-lx*illil;,2-r'linuoroethane ;l
1 ,1,1-Trichloroethane 50
I
1,1,2-Trichloroethane s0
I
t
PQL = Practical quanlitation limit
ND = Not detected at or above the PQL
P = The RPD betwoen two GC columns ex@eds 40% N = Recovery is out of criteria
J = Estimated result < PQL and : MDL + = RPO is out of criteria
Wh6re applicable, all soil sample analysis are reported on a dry weighl basis unless flagged with a "w"
Note: Calculatlons are performed before rounding to avoid round-off errors ln calculated results
Shegly Environmental Servicos, lnc.
106 Vantage Point DrivE West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 33 of 58
Lovsl 1 Report v2.l
I
IVolatile Organic Compounds by GC/MS - LCS
Sample lD: OQ26418-002
Batch: 2641 8
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035 I
Spike
Amount
(ug/kg)
Result
(uslks)% Rec
% Rec
Limit IParameterAnalysis Date
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
Xylenes (total)
Surrogate
50
50
50
100
o
43
36
40
87
AcceptanceLimit
1
1
1
1
87
72
80
87
62-126
45-1 38
42-132
58-128
08102120131711
08t02t20131711
08102120131711
08102120131711
I
t% Rec
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
1'16
99
109
47-138
53-142
68-124 I
I
t
I
I
I
I
I
I
I
I
PQL. Practical quanlitaiion limit
ND = Not d€tect€d at or above the POL
P = The RPD betwe€n two GC columns excesds rl0% N = Recovery is out of criteria
J = Estimat6d result < PQL and : MDL + = RPD ls out of critotia I
I
wh6re applicable, all soil sample analysis are rsportod on a dry w€ight basis unloss flagged with a 'W.
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental S€rvices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'111 www.shealylab.com
Page: 34 of 58
Level 1 R@ort v2.l
I
t Volatile Organic Gompounds by GC/MS - LCSD
t Sample lD: Oe26418-003
Batch:26418
Analytical Method: 82608
Matrix: Solid
Prep Method: 5035
I parameter
Spike
Amount(ug/ks)Result(us/ks) O Dit
% Rec % RPD
% Rec % RPD Limit Limit Analysis Date
Acetone
I Benzene
I Bromodichloromethane
Bromoform
r Bromomethane (Methyl bromide)I a"TH:[:#::'
Carbon tetrachlorideI :li::::ill"J"
Chloroform
I :lffiT,"i[""
(Methvrchroride) ::I 1,2-Dibromo-3-chloropropane(DBCP) 50
42-149 20 0810212013',1735
69-123 20 08t02t20131735
69-121 20 08102120131735
61-119 20 08102120131735
10-168 20 08102120131735
57-148 20 08102120131735
58-122 20 08102120131735
58-136 20 08102120131735
59-129 20 0810?,20131735
42-163 20 08t0z2013',173571-125 20 08t0A20131735
34-134 20 08102120131735
53-139 20 0810212013 1735
5s-125 20 08tO2120131735
66-119 20 08t0212013173574-124 20 08102120'.t31735
52-133 20 08102120131735
51-134 20 08102120131735
57-131 20 08102120131735
10-157 20 08102120131735
67-129 20 08102120131735
71-127 20 08102120131735
68-131 20 08102nu3173570-'t22 20 08t02120131735
69-138 20 0810?,2u31735
72-124 20 08/0?,20131735
70:t24 20 08102120131735
70-126 20 0810?,20'.131735
59-128 20 08102120131735
s4-137 20 08102120131735
50-136 20 08102t20131735
59-137 20 08102120131735
70-130 20 08102120131735
60-134 20 08102120131735
41-144 20 0810212013',1735
70-130 20 08na2u3'1735
54-136 20 0810U20131735
69-132 20 0810?,20',131735
4s-1s0 20 0810212013173561-129 20 0A102t20131735
49-136 20 08102120131735
34-145 20 08102120131735
63-128 20 08rc2/20131735
55-128 20 08t02t20131735
100
50
50
50
50
100
50
50
50
50
50
88
44
4',!
44
38
96
41
41
44
41
43
43
45
48
43
45
43
44
44
43
43
44
44
45
44
43
44
43
45
88
44
48
44
92
45
43
44
45
44
42
40
45
41
45
88
88
82
88
76
96
82
82
88
81
86
85
90
96
85
90
86
88
88
86
85
88
88
90
88
87
87
86
90
88
87
96
88
92
89
86
89
89
87
85
81
90
82
90
5.3
0.47
0.12
3.4
0.24
3.1
3.9
3.6
3.2
6.0
4.7
9.6
5.2
6.0
2.2
3.6
0.28
0.99
0.11
7.0
4.4
6.4
4.5
5.3
4.2
2.4
4.3
2.4
1.7
1.3
1.1
2.7
4.6
2.4
2.3
5.1
3.1
2.5
2.9
2.4
4.8
2.9
4.O
4.0
Dibromochloromethane
I 1,2-Dibromoethane(EDB)
I r,+-Drcnrorooenzene
1 ,3-Dichlorobenzene
1 .2-Dichlorobenzene
I Dichlorodifluoromethane
I 1,2-Dichloroethane
1 ,1-Dichloroethane
I trans-1,2-Dichloroethene
f cis-l.2-Dichloroethene
1 ,1 -Dichloroethene
1 .2-DichlorooroDane
I trans-1,3-Dichtoropropene
I cis-l,3-Drchtoropropene
Ethylbenzene
I 2-Hexanone
I tsopropylbenzene
Methyl acetate
Methyl tertiary butyl ether (MTBE)
I 4-Methvt-2-Dentanone
I Methylcyclohexane
Methylene chloride
r Stvren€
I t,7,z,z-tetrac.ntoroethane
I eracnbroemene
Toluene
50
50
50
50
50
50
50
50
50
50
50
50
s0
50
50
100
50
50
50
100
50
50
50
50
50
50
I l:1,i.]Hllll*2'2-rrinuoroethane ::
1 ,1,1-Trichloroethane 50
I
1,1,2-Trichloroethane 50
I
I
PQL = Practical quantitatlon limlt
ND = Nol dstectsd al or above th6 PQL
P = The RPD b6tw6en two GC columns oxcoeds 40% N = Recovory is out of criterla
J = Estimated result < PQL and i MOL + = RPD is oul of criteria
Whare applicable, all soil samplg analysis are reported on a dry reight basis unl6s flagged with a "w'
Note: Calculations ars performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l'l www.shealylab.com
Page: 35 of 58
[6vel'l Rsportv2.l
I
IVolatile Organic Compounds by GC/MS - LCSD
Sample !D: OQ26418-003
Batch: 264 1 8
Analvtical Method: 82608
Matrix: Solid
Prep Method: 5035 I
SpikeAmount Result % Rec % RPD(ug/kg) (ug/kg) O Dil % Rec % RPD Limit Limit Analysis Date IParameter
Trichloroethene
Trich lorofl uorometha ne
Vinyl chloride
Xylenes (total)
Surrogate
50
50
50
100
O %Rec AcceptanceLimit
44
38
43
90
1
1
1
1
88
76
86
90
1.1 62-126 20 0810212013 1735
5.0 45-138 20 08102120131735
7.0 42-132 20 08102120131735
4.3 58-128 20 08102t20131735
t
IBromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
120
101
111
47-138
53-142
68-124 t
I
T
I
I
T
t
I
I
I
I
PQL = Practical quantitation limit
ND = Not dotoctod at or above the PQL
P = Ths RPD betreen two GC columns exceods 40% N = Rscovory is out of criteria
J = Estimated result < PQL and 2 MDL + = RPD is out of c.itsria I
I
Whero applicable, all soil sample analysis are reported on a dry w€ight basis unless flaggsd with a'W"
Note: Galculatlons are performed before rounding to avoid round-off errors in calculated results
Sh€aly Environmental Servbes, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 36 of 58
Levol 1 Repod v2.l
I
I Semivolatile Organic Compounds by GC/MS - MB
t Sample lD: Oe26389-001
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 1438
t Parameter o Dil POL Units AnalYsis Date
ugikg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
330
330
330
330
330
830
330
330
330
330
330
330
330
330
670
830
330
830
330
330
330
330
330
830
330
330
330
330
330
830
330
330
330
330
330
330
330
330
330
330
830
330
330
330
I
I
I
I
t
I
I
t
I
I
t
I
I
1 ,1 '-Biphenyl
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
2-Nitrophenol
3 & 4-Methylphenol
3,3'-Dich lorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-C hloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-C hloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Caprolactam
Carbazole
Chrysene
Di-n-butyl phthalate
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
08t02120132009
08t02120132009
08t02t20132009
08t02120132009
08t02t20132009
o8t02t20132009
08102120132009
08/022013 2009
0810,,2u32009
08102120132009
0810212013200,9
o8l0a2u32009
08102t20132009
08/02/2013 2009
08102120132009
08t02120132009
o8to2l20132A0g
08t02t20132@g
08t02120132009
08102t20132009
08t0i,2u32009
08t0?J20132009
08102t20132009
o8loa20'132009
08/02/2013 2009
o8lo2l20',t32009
08t02t20132@S
08102t20132009
oa0a2u32w9
0810?,2u32009
o810u20132009
o8lou20't32009
08t0a20fi200,9
08102t2013 2009
08102t20132009
08102120132009
08102t201320r]r9
o8lo2t20't32009
08t0u2013200s
08/022013 2009
08102t20132009
08/02/2013 2009
08/02/2013 2009
o8lo2t2013200,S
I
I
PQL = Practic€l quantitetion limit
ND = Not detectod at or above the PQL
P = Tho RPD bslweon two GC columns excseds 40olo N = Recovery is out of criteria
J = Estimated result < PQL and : MDL + = RPD is out of crileria
Whor6 applicablo, all soil sample anal!6is are reported on a dry weight basis unless flagged with a nV'
Note: Calculations are performed before rounding to avoid round.off errors in calculated results
Shealy Environmental Ssrvices, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'11 www.shealylab.com
Page: 37 of 58
Lovel I Report v2.1
I
TSemivolatile Organic Gompounds by GG/MS - MB
Sample lD: gq263g9-991
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 1438
I
IParameterResultDil PQL Units Analysis Date
Di-n-octytphthalate
Dibenzo(a,h )anth racene
Dibenzofuran
Diethylphthalate
Dimethyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexach lorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
N-N itrosodi-n-propylamine
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
A %Rec
1
1
1
1
1
1
1
,|
1
1
,|
1
1
1
1
1
1
1
1
1
1
Acceptance
Llmlt
08102120132009
081022013 2009
08/0?,2u32009
08102120132009
08to2120132009
08102120132009
o8lo2t20't32009
08102t20132009
08t02120132009
08/02/2013 2009
08102t20132009
08102t20132009
08102120132009
o8102t20132009
08102120132009
o8,lozno132009
08102t20132009
08t02t20132009
08t02t20132009
08t02t2013200s
08102120132009
330
330
330
330
330
330
330
330
330
830
330
330
330
330
330
330
330
830
330
330
330
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/k9
ug/kg
ug/kg
ug/kg
ug/kg
I
I
I
I
I
I
N-Nitrosodiphenylam ine (Diphenylamine) ND
Naphthalene
Nitrobenzene
Pentrachlorophenol
Phenanthrene
Phenol
Pyrene
Surrogate
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyldl4
87
78
80
82
89
81
30-117
33-102
28-104
22-109
27-103
41-120
I
I
t
I
I
I
t
PQL = Practical quantitation limit
ND = Noi dotsctsd at or above the PQL
P = The RPD b€twoen two GC columns oxc€eds 40% N = Rocovery is out of criteria
J = Estimat€d rosult < PQL and: MDL + = RPD is out ot critsria I
I
whsre applicabls, all soil sampls analysis are roportgd on a dry weight basis unl€ss flaggad with a 'w"
Notel Calculations are performed before rounding to avoid round-off errort in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 38 of 58
Lovel 1 Roport v2.1
I
I Semivolatile Organic Compounds by GC/MS - LCS
I Sample lD: OQ26389-002
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 '1438
t Parameter
Spike
Amount
(ug/kg)
Result
(ug/kg)
% Rec
Dil % Rec Limit Analysis Date
1 .1 '-BiohenvlI ;:i:;:l[il:,;:H:i
2,4-DichlorophenolI !:i!irffi"2,4-Dinitrotoluene
2,6-Dinitrotoluenet i.llilllrillf """
2-MethylnaphthaleneI ;,r,i*l:lf'
3 & 4-MethylphenolI ::i;:,:'Jil"i*,o',,"
4,6-Dinitro-2-methylphenol
r 4-Bromophenyl phenyl etherI ffiil]r"1,,[""J^,phenor
4-Chlorophenyl phenyl ethert i:ililffitllti
Acenaphthene
AcenaohthvleneI ffir:*""
AtrazineI ::r:ffi#;"","
Benzo(a)pyrene
Benzo(b)fluorantheneI ::Hlt;tlHflit""
bis(2-Chloroethoxy)methaneI iilllSli::n:I,l"Jlil^",
bis(2-Ethylhexyl)phthalate
Butvl benzvl DhthalateI ::rJ::l',:;
Chrysene
I
Di-n-butylphthalate
3300
3300
3300
3300
3300
1 7000
6700
6700
3300
3300
3300
3300
6700
6700
6700
6700
6700
1 7000
3300
3300
3300
3300
6700
1 7000
3300
3300
3300
3300
3300
3300
3300
3300
3300
3300
3300
3300
6700
3300
3300
3300
3300
3300
3300
3300
2200
2400
2300
2400
3000
1 6000
5100
51 00
2000
2400
2400
2700
5000
4800
4900
6000
4800
16000
2500
31 00
2900
2400
6600
1 9000
2500
2800
2600
2500
2400
2900
2600
3100
2900
2300
2800
2300
4900
2400
2900
2800
3300
2800
2400
2900
68
72
70
72
91
94
77
77
60
71
72
80
75
72
74
91
72
98
74
92
86
71
49-110
46-122
38-1 1 5
4',1-113
33-123
45-127
48-124
47-125
31-127
37-1 06
40-106
32-l07
45-123
35-108
39-108
46-1 13
24-127
40-130
46-1 1 8
49-1 18
10-125
47-',|16
48-127
18-154
46-114
44-122
48-11'.!
50-1 19
48-1't6
34-99
47-121
55-134
28-139
36-125
47-130
39-108
32-105
31-102
45-128
46-',128
43-121
47-124
45-126
51-129
08102120132035
08t02120132035
0810212013 2035
08102120132035
08t02t20132035
08102120132035
08t02t20132035
08t02t20132035
08t02t20132035
08t0u20132035
08102120132035
08t02120132035
08t02t20132035
08102120132035
08102120132035
08t02120132035
08/0?2013 2035
08t02t20132035
08102t20132035
08t02t2013 2035
o8t02t20132035
0810u20132035
08t02t20132035
08t02120132035
o8lo2l20't32035
o8to2120132035
08t0a2u32035
o8102t20132035
08t0212013203s
o8to2120132035
08t0a20132035
08to2t20132035
08t02t20132035
08t02t20132035
08t02120132035
08102t20132035
08t02t20132035
08t0?i20132035
08102120132035
08t02120'132035
08rc2/20't32035
08t02t20132035
08t02120132035
08/022013 2035
99
113
75
84
77
75
73
87
79
93
88
70
84
70
74
72
86
84
98
85
73
86
PQL = Practical quantitation limit
ND = Not delecled at or above ths PQL
P = The RPD betw6€n two GC columns excoeds 40% N = Rocov6ry is out ofcrit€ria
J = Estimated result < PQL and: MDL + = RPD is out of critsria
Where applicable, all soil sample analysis are reporlod on a dry woight basis unl€ss flagged wilh a 'W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated resultsIShealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 39 of 58
Lsvel I Reportv2.l
I
tSemivolatile Organic Compounds by GC/MS - LCS
Sample lD: Oe26389-002
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 '1438
I
SpikeAmount Result % Rec(uglkg) (uglkg) O Dit % Rec Limit Analysis Date IParameter
Di-n-octylphthalate
Dibenzo(a, h )anthrac€ne
Dibenzofuran
Diethylphthalate
Dimethyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexach lorocyclopentadiene
3300
3300
3300
3300
3300
3300
3300
3300
3300
1 7000
3300
3300
1 7000
3300
3300
3300
O %Rec
2800
2500
2400
2700
2500
27AO
2600
2800
2400
1 1000
2100
2500
2500
2700
2600
2300
2600
1 7000
2500
2700
2700
AcceptanceLimit
49-142
45-',t22
45-112
49-123
48-120
50-123
48-117
44-122
33-103
18-121
30-96
45-123
41-113
32-115
53-1 50
36-1 I 0
33-114
27-138
49-117
36-108
47-119
83
76
72
81
74
82
79
83
72
67
63
76
76
81
77
70
78
102
74
82
80
0810212013203s
08102120132035
08102t20132035
08102120132035
08102120132035
08/02/2013 2035
08102120132035
o8toa2u32095
0810?,2u32035
08102t2013203s
08/02120132035
08i0?/2u32035
08102120132035
08102120132035
08102120132035
08102120132035
08102120132035
0810212013203s
08t02t20132035
08t02t20132035
o8lo2t20't32035
t
I
I
I
T
I
Hexachloroethane 3300
lndeno(1,2,3-c,d)pyrene 3300
lsophorone 3300
N-Nitrosodi-n-propylamine 3300
N-Nitrosodiphenylamine (Diphenylamine) 3300
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Surrogate
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzened5
Phenol-d5
Terphenyl-d14
81
67
87
83
85
59
30-117
33-102
28-104
22-109
27-103
41-120
I
I
I
I
I
I
I
PQL = Practical quanlitation limit
ND = Not detscted at or above lhe PQL
P = The RPD botw66n tu/o GC @lumns excoeds 40% N = Rocovory is out of criteria
J = Estimated result < PQL and 2 MDL + = RPD is out of criioria I
IWhero applicable, all soil samplo analysis are reported on a dry \ €ight basis unless flagged with a ry\r
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Envimnmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.$healylab.com
Page: 40 of 5E
Level I R6portv2.1
I
I MA EPH (aromatics) - MB
I Sample lD: OO263s6-OO1
t Batch:263s6
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
I Parameter Result O Dil PQL Units Analysis Date
C11 - C22 Aromatics ND1
AcceptanceO % Rec Li'mit
10 mg/kg 0810312013 0842
I surrosate
2-Bromonaphthalene (fractionation 2) 72 40-140
t 2-Fluorobiphenyl (factionation 1) 73 40-140
f o - Terphenyl (aromatic) 61 40-140
I
I
I
t
t
I
I
I
t
I
I
I
'l
POL = Practical quantitation limit P = The RPD betw€en two GC columns *@eds 40% N = Recovsry is out of criteria
ND = Notdetected atorabove the PQL J = Estimated result< PQLand: MDL + = RPD is out ofcriteria
Whers applicable, all soil sample analysis are roported on a dry reight basis unless flagged with a 'W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:41 of58
Lcvel I Reportv2,l
I
IMA EPH (aromatics) - LCS
Sample lD: 9q26356-992
Batch:26356
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
t
SpikeAmount Result(ms/kq) (ms/ks)% Rec
% Rec
Limit IParameterAnalysis Date
C11 - C22 Aromatics
Surrogate I85
a
52
Acceptance
Limit
40-140 08/03/2013 091 1
% Rec
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (ftactionation 1 )
o - Terphenyl (aromatic)
81
84
70
40-140
40-140
40-140 I
I
I
I
I
I
T
I
I
I
t
I
PQL = Practical quantitation limit
ND = Not det6ct6d at il abovs the PQL
P = Th6 RPD b€t\rveen two GC columns exceeds 40% N = Recovery is out ofcriteria
J = Estimated r6ult < PQL and: MDL + = RPD is out of criteria I
I
Where applicable, all soil samplo analysis are roporbd on a dry w€ight basis unless flagged with a nV"
Note: Calculations are perfonned before rounding to avold round-off orrors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 42 of 58
Level I Report v2.l
I
t MA EPH (aromatics) - LCSD
I
sampte tD: oe263s6-oo3
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 08/0212013 935
I ^tJll"r, Resutt % Rec % RPDI Parameter (mg/kg) (mg/kg) O Dit % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics
Surrogate
85 45
AcceptanceO % Rec Liinat
1 52 16 40-140 25 08/03/2013 0940I
2-Bromonaphthalene (fractionation 2) 72 40-140
I ::i:"..',",.":fh,'llilnaton
1) ;; ii.]il
I
I
I
I
I
T
I
I
I
I
I
I
I
PQL = ftaclical quantitation limit P = The RPD belween two GC columns exeeds 40% N = Recovery is out of criteria
NO = Notdetected at orabovotho PQL J = Estimated result < PQLand: MDL + = RPD is outofcriteria
Where applicabls, all soil samplo analysis ara reported on a dry weighl basis unless flagged with a "w"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 43 of 58
Lovcl t Report vz.l
I
MA EPH (aliphatics) - MB
Sample lD: OQ26358-001
Batch:26358
Analytical Method: MADEP-EPH-o4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
t
I
IParameteroAnalysis Date
Cl9 - C36 Aliphatics
Cg - C18 Aliphatics
Surrogate
mg/kg
mg/kg
10
10
ND
ND
o
1
1
Accoptance
Limit
08/0212013 1808
08/022013 1808 I
I
% Rec
1 -Chloro-octadecane (aliphatic)40-140
I
I
I
I
I
I
I
I
I
I
I
PQL = Praclical quantitation limit
ND = Not detoctsd at or abovs ths PQL
P = The RPD betweon two GC columns excseds 40% N = Re@wry is out of crlteria
J = Estimated result < PQL and : MDL + = RPD is out of critoria I
I
Wher8 applicabls, all soil sample analysis are reportod on a dry w€ighl basis unless flaggod with a nV'
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 (803) 79'l-9700 Fax [phone] www.shealyhb.com
Page: 44 of 58
Levol 'l Report v2.1
I
t MA EPH (aliphatics) - LCS
I Sample lD: oe263s8-002
I Barcn:26358
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-O4
Prep Date: 0810212013 935
I ^tf::"", Resurt % Recr Parameter (mE/ks) (mq/ks) O Dit % Rec Limit Analysis Date
t :;:.::'fxffi::'40 35
30 15
AcceptanceO % Rec Lihit
87 40-140 0810212013 1837
51 40-140 08t02t20't3 1837
I
1-Chloro-octadecane (aliphatic) 79 4oJt4o
I
t
I
I
I
I
I
t
I
T
I
t
I
PQL = Practical quantitation limit P = Th6 RPD botw€€n two GC columns sxceeds 40oZ N = Rocovery is out of criteria
ND = Not detected ator above the PQL J = Estimated result< PQLand? MDL + = RPD is outofcriteria
Whero applicable, all soil sample anal)6is aro roported on a dry w€ight basis unl6s flagged with a w'
Note: Calculations are performed before rounding to avoad round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive west Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Page: 45 of 58
LeYel I R@ort v2.1
I
IMA EPH (aliphatics) - LCSD
Sample lD: OQ26358-003
Batch:26358
Analytical Method: MADEP-EPH-O4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
I
Spike
Amount
(mg/kg)
Result(ms/ks) O % Rec % RPD
% Rec
Limit
% RPDLimit Anatysis Date IParametel
C19 - C36 Aliphatics
C9 - C18 Aliphatics
Surrogate
32
13
Acceotance
% Rec Liinit
I25
25
40
30
o
81
42
7.1
19
40-140
40-140
08to2t2013 1907
08t0212013 1907
I
t
I
t
I
I
I
I
I
I
I
t
1 -Chloro-octadecane (aliphatic)40-'t40
PQL = Practicalquantitation limit
ND = Not det€cted at or above the PQL
P = The RPD b€tween two GC columns excesds 40% N = Rscovery is out of criteria
J = Estimated result < PQL and : MDL + = RPD is out of criteria I
I
Whor6 applicable, all soil sample analysis are roported on a dry weight basls unlsss flagged with a "W"
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Envircnmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 46 of 58
Level 1 Reportv2.l
I
I MA EPH (aromatics) - Unfractionated - MB
t '"'l':,:?,;;i6615-oo1
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 08102120'13 935
t Parameter Result O Dil PQL Units Analysis Date
C1'l - C22 Aromatics - Unfractionated ND 10 mg/kg 0810612013 1237
t surrosate AcceptanceO % Rec Lihit
2-Bromonaphthalene (fractionation 2) 83 40-140
I 2-Fluorobiphenyl (fractionation 1) 81 40-140
I o - Terphenyl (aromatic) - Unfractionated 67 40-140
I
I
I
I
I
I
I
I
I
I
I
t
I
PQL = Practical quantitafion limit P = Th6 RPD between two cC columns exceeds 40% N = Recovery is out of criteria
ND = Notdot€cted atorabovgth€ PQL J = Estimated result< PQLand: MDL + = RPD is out ofcritoria
Where applicable, all soil sample anal),ais ars rBported on a dry w€ight basis unless flagged with a "W"
Note: Calculations are performed before roundlng to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 47 of 58
Level 1 Report v2.1
I
MA EPH (aromatics) - Unfractionated - LCS
Sample lD: OQ266't5-002
Batch:2661S
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
I
t
tSpikeAmount Result % Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
1 6'lC11 - C22 Aromatics - Unfractionated 140 85
Surrogate AcceDtanceO % Rec Ltinit
40-'t40 08/06/2013 1307
I
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (fractionation 1 )
o - Terphenyl (aromatic) - Unfractionated
79
80
68
40-140
40-140
40-140 t
T
I
I
I
I
I
I
I
I
t
I
PQL = ftactical quantitatis limit
ND = Not detected at or above the POL
P = The RPD betwsen two GC columns exc€Bds 40% N = Recovery is out of criteria
J = Eslimated result < PQL and : MDL + = RPD is out of critorla I
I
wherg applicable, all soil sample analysis are reportod on a dry weight basis unless flagged with a nv'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29'|72 [phone] Fax [phone] www.shealylab.com
Page: 48 of 58
Lcv8l 1 @ortv2.1
I
T MA EPH (aromatics) - Unfractionated - LCSD
I Sample lD: 00266'15-003
I Barcn:266r5
Analytical Method : MADEP-EPH-O4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
I ^t#:"", Resurt % Rec % RPD
- Parameter (mg/kg) (mg/kg) O Dil % Rec % RPD Limit Limit Analysis Date
Cl1 - C22 Aromatics - Unfractionated 140 74 1 53 14 40-140 25 08/06/2013 1336
I Surrosate AcceDtanceO % Rec Limit
2-Bromonaphthalene (fractionation 2) 78 40-140
t 2-Fluorobiphenyl (ftactionation 1) 79 40-140
f o - Terphenyl (aromatic) - Unfractionated 61 40-140
I
I
I
I
I
t
I
I
I
I
I
I
I
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40olo N = Rscovsry is out of ffiteria
ND = Notdetscted atorabov3 th6 PQL J = Eslimaled result< PQLand: MDL + = RPD is outofcriteria
whgrs appli€ble, all soil samplo anal)6is are rgported on a dry w€lght basis unless flagged with a 'w"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Servbes, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 49 of 58
['6\rel 1 Roport v2.1
I
IMA EPH (aliphatics) - Unfractionated - MB
Sample lD: OQ26616-001
Batch:266'16
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
I
Parameter o PQL Units Analysis Date I
C19 - C36 Aliphatics - Unfractionated
Cg - C18 Aliphatics - Unfractionated
Surrogate
tmg/kg
mg/kg
ND
ND
a
1
,|
Acceptance
Limit
10
10
08106120'131237
08106t2013't237
% Rec
I
I
I
I
I
I
I
t
I
T
I
I
1 -Chloro-octadecane (aliphatic) - Unfractionated 88 40-140
PQL = P(actical quantitation limit
ND = Not det6ct6d at tr abov6 the POL
P = Th3 RPO betwtsen two GC columns exceeds 40olo N = Recovsry is out of criteria
J = Estimated result < POL and: MDL + = RPD is out of crit6ria T
Iwhsrs applicable, all soil sampl8 analysis aro reported on a dry weight basis unloss flaggod with a'w'
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Polnt Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 50 of 58
Level I Reportv2.l
!
I MA EPH (aliphatics) - Unfractionated - LCS
I '"':':,:?:*16616-002
Analytical Method: MADEP-EPH-O4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 08/02/2013 935
I ^t[f", Resutt % Rec
- Parameter (mq/ks) (mq/ks) O Dit % Rec Limit Analysis Date
r C19 - C36 Aliphatics - Unfractionated 90 79 1 88 40-140 08/06/2013 1307
I C9 - C18 Aliohatics - Unftactionated 65 47 1 72 40-'140 08/06/2013 1307
I Acceptancesurrogate o % Rec "- Li'!n-tr'--
I
1-Chloro-octadecane (aliphatic) - Unfractionated 90 40-140
I
I
T
I
I
!
I
I
I
T
I
T
I
PQL = Praclical quantilalion limil P = Ths RPD b3tween two GC columns sxcseds 40olo N = Recovery is out of criteria
NO = Not det€ctod at or above the PQL J = Estimated result < PQL and: MDL + = RPD is out of criteria
Where applicabl€, all soil sample analysis are reportBd on a dry weight basis unlBss flaggsd with a 'w"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental S€rvices, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone]'111 www.shealylab.com
Page:51 of58
L6vsl I Reportv2.l
I
IMA EPH (aliphatics) - Unfractionated - LCSD
Sample lD: OQ26616-003
Batch:26616
Analytical Method: MADEP-EPH-O4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 08/02/2013 935
T
SpikeAmount Result(ms/ks) (ms/ks) O
% Rec
% RPD Limit
% RPDLimit Analysis Date IParametel% Rec
C19 - C36 Aliphatics - Unfractionated
C9 - C18 Aliphatics - Unfractionated
Surrogate
80
57
90 72
65 37
9.4
23
40-'t40
40-140
25 08/06/2013 1336
25 08/06/2013 1336 I
O %Rec AcceptanceLimit
t
t
I
t
I
t
!
I
I
t
I
I
1-Chloro-octadecane (aliphatic) - Unfractionated 84 40-140
PQL = Practical quantitatlon limit
ND = Not d6t€cted at or above the PCIL
P = Th6 RPD betw€en two GC columns exceeds 40% N = Recov6ry is out of critsria
J = Estimated resull < FloL and : MDL + = RPD is out of critBria I
IWhor6 applicable, all soil sample analysis aro reportod on a dry weight basis unless flagged with a "w"
Note: Calculations are performed before rounding to ayoid round.off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Page: 52 of58
Level 1 Roportv2.l
I
t MADEP VPH (aliphatics) - MB
I Sampre rD: oe26434-oo1
I Batch:26434
Analytical Method: MADEP-VPH-04-1.1
Matrix: Solid
Prep Method: VPH
I Parameter Result O Dit PQL Units Analysis Date
I 3i :ilfililil.
Surrogate
3.8 mg/kg Ogl02l2o13 1922
3.8 mg/kg 08102120131922ND1
AcceptanceO % Rec Lihit
I
2,s-Dibromotoluene (FlD) 106 70-130
I
t
I
T
I
I
I
I
I
I
I
t
I
PQL = Practical quantitation limit P = The RPD betwoen two GC columns exceeds 400/6 N = Recovery is out of criteria
ND = Notdstocted Atorebovolhe PQL J = Estimated rosult< PQL andz MDL + = RPD is outofcriteria
Wh€re applicable, all sil samplo analysis aro reported on a dry weight basis unless flagged with a nV'
Note: Calculations are performed before roundlng to avoid round-off errors in calculated results
Shealy Environmental Servic€s, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Page: 53 of 58
Lavot 1Rqofiv2.1
t
MADEP VPH (aliphatics) - LCS I
ISample lD: Oe26434-002
Batch:26434
Analytical Method: MADEP-VPH-04-'1.1
Matrix: Solid
Prep Method: VPH
SpikeAmount Result % Rec(mg/kg) (mg/kg) O Dil 7o Rec Limit Analysis Date IParameter
C5 - CB Aliphatics
Cg - C12 Aliphatics
Surrogate
3.8
3.8
O %Rec
2.8
3.2
Acceptance
Limit
t
t
75
86
1
'l
70-130
70-1 30
0810212013 1801
08102120131801
2,5-Dibromotoluene (FlD)70-130
I
I
I
I
I
!
I
I
T
t
I
PQL = Praclical quantitation limit
ND = Not datectod at or above the PQL
P = The RPD b6tw68n two GC columns sxceeds 40olo N = Recovery is out of criteria
J = Estimatod rosult < POL and: MDL + = RPD is oul of critsria I
tWhors applicable, all soil sample analysis are reported on a dry w€ight basis unless flagged with a nV"
Note: Calculations are performed before rounding to ayoid round-off errors in calculated results
Shealy Environmental S6wic€s, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 54 of 58
Level I R6portv2.1
I
t MADEP VPH (aliphatics) - LCSD
I '"'l':,:?,ffi'o-'o'
Analytical Method: MADEP-VPH-O4-1.1
Matrix: Solid
Prep Method: VPH
I ^tJ:n, Resurt % Rec % RPD
" Parameter (mg/kg) (mg/kg) O Dit % Rec % RPD Limit Limit Analysis Date
C5 - CB Aliohatics 3.8 2.8 1 75 0.61 70-130 25 0810212013 1841
f Cg - C12 Atiorr",i". 3.8 3.3 1 88 2.g 70-130 25 O}to2t2o13 1841
I Acceotancesurrogate O %Rec Lihit
I
2,s-Dibromotoluene (FlD) 93 70-130
I
I
I
I
I
t
I
I
I
I
t
t
T
PQL = Practical quandtation limit P = Th€ RPD batweGn two GC columns excgsds 40% N = Recovery is out of crilgria
ND E Notdotectsd at orabovethe PQL J = Estimated rssult< PQLand: MDL + = RPD is out ofcrit€ria
Wh6re applicable, all soil sample analysis are reportsd on a dry wsight basis unless flagged with a "VV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia,SC 2S172 [phone] Fax[phone] www.shealylab.com
Page: 55 of 58
Lsvel 1 Roport v2.1
I
MADEP VPH (aromatics) - MB
Sample lD: OQ26436-001
Batch:26436
Analytical Method: MADEP-VPH-04-1.1
Matrix: Solid
Prep Method: VPH
Parameter Result Analysis Date
Cg - C10 Aromatics
Surrogate
I
I
I
I
I
I
I
ND
a
1
AcceptanceLimit
mg/kg o8t02t2013 1922
o/o Rec
2,5-Dibromotoluene (PlD)117 70-1 30
I
I
I
I
I
I
t
I
I
PQL = Practical quantitatis limit
ND = Not detscted at or above the PQL
P = Tha RPD bshd8sn two GC columns oxceeds 40o/o N = Recovsry is out of criteria
J = Estimated r6utt < PQL and Z MDL + = RPD is out of criteria I
T
Where applicablo, all soil sampls analysis aro rsported on a dry u€ight basis unloss flagged with a nV'
Note: Calculataons are performed before rounding to avoid round-off errorc an calculated results
Shealy Environm€ntal Services, lnc.
l06VantagePointDrive westColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 56 of 58
Level 1 ReDortY2.l
I
t MADEP VPH (aromatics) - LCS
I Sampte lD: OQ26436-oo2
I tsarcn:zo43b
Analytical Method: MADEP-VPH-04-1.1
Matrix: Solid
Prep Method: VPH
t ^tJ::?, Resurt % RecI Parameter (mg/kg) (mg/kg) O Dit % Rec Limit Analysis Date
Cg - C10 Aromatics 1.3 1.0
AcceptanceA % Rec Lihit
80 70-130 08102120131801
I surrosate
100 70-1302,5-Dibromotoluene (PlD)
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PQL = Practical quantitation limit P = Th6 RPD between iwo GC columns Excsods 40% N = Rs@very is out of criteria
ND = Not detocted at or above the PCIL J = Estimated result < PQL and: MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are rsporled on a dry weight basis unlsss flagged with a nV'
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 57 of 58
Levcl 1 Report v2.1
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MADEP VPH (aromatics) - LCSD I
ISample lD: OQ26436-003
Batch:26436
Analytical Method: MADEP-VPH-04-1.1
Matrix: Solid
Prep Method: VPH
Parameter
SpikeAmount Result % Rec % RPD(ms/ks) (ms/kg) O Dit % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics
Surrogate
1.3 1.0 1
AcceptanceO % Rec Lihit
0.00 70-130 25 08102t20131841
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2,5-Dibromotoluene (PlD)100 70-1 30
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PQL = Pracfcal quanlitation limit
ND = Not detsctsd at or abov8 the PQL
P = The RPD betwaen lwo GC columns exc€eds 40% N = Recovery is out of criteria
J = Estimated rosult < PQL and : MDL + = RPD is out of cribria
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I
IWhero applicable, all soil sample analy8is are roported on a dry wsight basis unless flagFd with a n\r
Note: Calculations are performed before rounding to avoid round-ofr error3 in calculated results
Shealy Environmental Services, lnc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l'l www.shealylab.com
Page: 58 of 58
L6vel 1 Reportv2.l
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SHEALY ENVIRONMENTAL SERVICES, INC.
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100 Vantag€ Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com L6rcl 1 Roport v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
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Level I Reportv2.l
I
Shealy Environmental SeNices, lnc.
106 Vantage Polnt Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
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SHEALY ENVIRONMENTAL SERVICES, INC.t
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Report of Analysis
Terracon Consultants, lnc.
3534 Rutherford Road
Taylors, SC 29687
Attention : George Flores
Project Name:lRC
Project Number:861 27 1Og
Lot Number:OHO1041
Date Completed:0810612013
*f'=*#L-
Project Manager
This report shall not be reproduced, except in its entirety, without the wriften approval of Shealy Environmental Services, lnc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
aoaoaaaaa
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: I of34
Levrl 1 R6port v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.I
ISC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329
Case Narrative
Terracon Consultants, lnc.
Lot Number: OH01041 I
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, lnc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
lf you have any questions regarding this report please crntact the Shealy Project Manager listed on the cover page.
GC/MS SVOC
Due to matrix interferences, sample -005 was analyzed at a 5X dilution. All trarget compounds were nondetect at this dilution.
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Shealy Environmsntal Services, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 2 of 34
Lavel I Reportv2.'t t
SHEALY ENVIRONMENTAL SERVIGES, INC.
Sample Summary
Terracon Consultants, lnc.
Lot Number: OHO1041
Sample Number Sample lD Matrix Date Sampled Date Received
001 Ho-N
002 Ho-E
003 Ho-s
004 Ho-w
005 Ho-B
Solid 07130120131420
Solid 0713012013 1425
Solid 07130120'13 1430
Solid 0713012013 1435
Solid 0713012013 1440
08t0112013
0810112013
08t0112013
08t0112013
o8to112013
(5 samples)
Shealy Envircnmental Services, lnc.
l06VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 3 of 34
l.evsl 1 Roportv2.'l
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Terracon Consultants, lnc.
Lot Number: OH01041
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ISample Sample lD Matrix Parameter Result O
mg/kg 19
mg/kg 19
550
38
Solid
Solid
005 Ho-B
005 Ho-B
C19 - C36 Aliphatics
C11 - C22 Aromatics
MADEP-EPH-
MADEP-EPH-
(2 detections)I
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Shealy Environmental Services, lnc.
106 Vantage Polnt Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 4 of 34
L6v6l 'l Report v2.1
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Client:Terracon Gonsultants, lnc. Laboratory lD: OH01041-001
Description: HO-N Matrix: Solid
Date Sampled:07130120'|3'1420 % Solids: 79.7 0810112013 2203
Date Received: 08/01/2013
Semivolatile Orqanic Compounds bv GC/MS
I Run PreP lrtiss AnalyticalMethod Dilution8270D 1
Analysis Date Analyst Prep Date Batch
08102t20132102 JRG 0810212013 1438 26389
Parameter
CAS Analytical
Number Method Result O
a
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Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-C hloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h )anthracene
Dibenzofuran
3,3'-Dich lorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Din itro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethy'hexyl)phthalate
Fluoranthene
83-32-9
208-96-8
98-86-2
120-12-7
1912-24-9
100-52-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
92-52-4
't01-55-3
8s-68-7
1 05-60-2
86-74-8
59-50-7
106-47-8
111-91-1
11144-4
1 08-60-1
91-58-7
95-57-8
7005-72-3
21 8-01 -9
84-74-2
117-84-O
53-70-3
1 32-64-9
91-94-1
120-83-2
84-66-2
131-'t 1-3
1 05-67-9
534-52-1
51-28-5
12'.1-14-2
606-20-2
117-81-7
206-44-O
8270D
8270D
82700
82700
8270D
8270D
8270D
8270D
8270D
8270D
827AO
8270D
8270D
8270D
8270D
8270D
82704
8270D
8270D
8270D
8270D
8270D
82704
4270D
8270D
8270D
8270D
8270D
8270D
82704
8270D
8270D
8270D
8270D
82700
82700
8270D
8270D
8270D
8270D
410
410
410
410
410
1 000
410
410
410
4',t0
410
410
410
410
1 000
410
410
410
410
410
410
410
410
410
410
410
410
410
410
1000
410
410
410
410
1000
1 000
410
410
410
410
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
uS/kS 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg I
ug/kg 1ug/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 'l
ug/kg 1ug/kg 1
us/ks 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
uS/kS 1
ug/kg 1ug/kg 1
ug/kg 1
I POL = Practcal quantitation limit B = Detected in ths method blank E = Quantitation of compound oxceedod the calibration range
ND = Not detectod at or above the PQL J i Estimated result < PQL and: MDL P = The RPD betweon two GC columns sxcaods 40%
Wh6ro applicable, all $il samplo analysls are rBporled on I dry u€ight basis unless flagged with a nV"
H = Out of holding time
N = Rscovary is out ot crlteda
Shealy Environmental Services, lnc.
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106 VantaSe Point Drive West Columbia, SC 29172 (803) 791-S700 Fax [phone]'11 www.shealylab.com
Page: 5 of 3tt
Lovel I Rcport v2.1
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Client:Terracon Consultants, lnc. Laboratory lD: OH0'1041.001
Description: HO.N Matrix: Solid
Date Sampled:0713012013 1420 % Solids: 79.7 0810112013 2203
Date Received : 08101 12013
Semivolatile Orsanic Gompounds by GC/MS
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Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 1 08102120',t3 2102 JRG 0810212013 1438 26389 I
Analytical
Parameter
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-N itrosodi-n-propylamine
N-Nitrosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
86-73-7
1',|8-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48'7
106-44-5
621$4-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
87-86-5
85-01-8
108-9s-2
129-00-0
95-95-4
88-06-2
Run I Acceptancea % Recovery Limits
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
Result O
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4'10
410
410
1 000
410
4't0
410
410
410
840
410
4't0
410
4'10
410
410
410
410
1000
1000
410
410
410
410
410
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
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2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
78
75
68
72
79
61
30-1 1 7
33-102
28-104
22-109
27-103
41-120
MA EPH (aliphatics)
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IRun Prep Method
1 MADEP-EPH-
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
MADEP-EPH-0 1 08/02/2013 1936 AMY 08/02/20130935 26358
cAs
Number
AnalyticalMeihod Result a TParameterPQLRun
t
POL = ftactical quantitation limit B = Det€ciod in the m€thod blank E = Quantitation of compound oxceedod ths calibration range H = Out of holding tims
ND = Notdetoctod atoraboveths POL J = Estimatsd result< PQL and: MDL P =Ths RPD between two GC columns excesds 40% N = Recovery is out ofcrlteria
Wherc applicable, all soil samplo anal)€is are roported on a dry w€ighl basis unless flaggod with a 1W I
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealyhb.com
Page: 6 of 34
L6vel 1 Reportv2.l
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Client:Terracon Consultants, lnc. Laboratory lD: OH01041-001
Description: HO-N Matrix: Solid
Date Sampled:0713012013 1420 % Solids: 79.7 0810112013 2203
Date Received : 08101 12013
MA EPH (aliphatics)
I Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
t 1 MADEP-EPH- MADEP-EPH-0 1 08/02/20131936 AMy 0a102t2013 0935 26358
CAS AnalyticalParameter Number Marh^.{ Result O PQL Units Run
T
I
Cg - C18 Aliphatics
C19 - C36 Aliphatics
Surrogate
MADEP-EPH-O ND
MADEP-EPH-O ND
Run 1 AcceptanceO % Recovery Limits
12 mg/kg 1
12 mg/kg 1
1-Chloro-octadecane (aliphatic) 79 40-140
I MA EPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Dat6 Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-o 1 08/03/2013'1009 AMy 08t0212013 093s 26356I
t
CAS AnatyticalParameter Number Marhar{ Result O PQL Unlts Run
C11 -Cz2Aromatics
Surrogate
MADEP-EPH-O ND
Run 1 AcceptanceO % Recovery Limits
12 mg/kg 1
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2-Bromonaphthalene (fractionation 2) 49 40-'140
2-Fluorobiphenyl (fractionation 1) 91 40-140
o - Terphenyl (aromatic) 79 40-140
I PQL= Practicalquantitation limii B = D€tsted in ths method blank E = Quantitation of compound exce6d€d tho calibration rangs H = Outof holdingtime
ND=NotdetoctBdatorabovethePQL J=Estimatodresult<PQLand:MDL P=TheRPDbetwBentwoGCcolumnsexcosds40% N=Recoveryisoutolctiteria
Whsre applicabl€, all soil sample anal)6is are reporled on a dry w€ight basis unlass flagged with a 'W"
Shealy Environmental Services, lnc.
!
106 VantaSe Point Drive West Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Page: 7 of 34
Lsv€l 1 Report t2.,
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Client:Terracon Consultants, lnc, Laboratory lD: OH01041-002
Description: HO-E Matrix: Solid
Date Sampled:0713012013 1425 % Solids: 83.7 0810112013 2203
Date Received: 08101I201 3
Semivolatile Organic Compounds by GC/MS
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Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 08102120132220 JRG 08102120131438 26389 I
Parameter
cAs
Number
Analytical
Method Result A PQL Units Run
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-&methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h )anth racene
Dibenzofuran
3,3'-Dichlorobenzid ine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
83-32-9
208-96-8
98-86-2
120-12-7
1912-24-9
100-52-7
56-55-3
50-32-8
205-99-2
191-24-2
207-O8-9
92-52-4
101-5s-3
85-68-7
10560-2
86-74-8
59-50-7
1 06-47-8
1 1 1-91-1
't11-44-4
108€0-1
91-58-7
95-57-8
7005-72-3
218-O',t-9
84-74-2
117-84-0
53-70-3
132-64-9
91-94-1
't20-83-2
84-66-2
131-1 1-3
10567-9
534-52-1
51-28-5
121-14-2
606,-20-2
117-81-7
206-44-O
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
udkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uS/kS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
I
I
I
I
I
I
I
I
I
I
I
T
I
380
380
380
380
380
960
380
380
380
380
380
380
380
380
960
380
380
380
380
380
380
380
380
380
380
380
380
380
380
960
380
380
380
380
960
960
380
380
380
380
PQL = Practical quantitation limit B = Det€ctod in the method blank E = Quantitation of compound excesded tls calibration rango H = Out of holding tim6
ND = Notdetected atorabove the PQL J = Estimated result< PQLand: MOL P =The RPD betw6en two GC columns exce€ds 40% N = Rocoveryisoutofcritoria
Where applicable, all soil sampls anal)rsis are reportod on a dry weighl basis unloss flaggod with a'w't
Shealy Environmental Services, lnc.
106VantagePointDrive westColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 8 of 34
L€vel't Rsportv2.'l
I
I
I
t
Client:Terracon Consultants, lnc. Laboratory lD: OH01041-002
Description: HO-E Matrix: Solid
Date Sampled:0713012013 1425 % Solids: 83.7 0810112013 2203
Date Received: 08/01/2013
Semivolatile Organic Compounds by GC/MS
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 08t02t20132220 JRG 08t02t20131438 26389
Parameter
CAS
Number
Analytical
Mathod Result O
I
I
I
I
I
I
t
I
I
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexach lorocyclopentad iene
Hexachloroethane
lndeno( 1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-N itrosodi-n-propylamine
N-Nitosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4, 5-Trichlorophenol
2,4,6-Trich lorophenol
Surrogate
86-73-7
118-74-1
87.68-3
77-47-4
67-72-1
1 93-39-5
78-59-1
91-57-6
95-48-7
106-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
,t00-01-6
98-95-3
88-75-5
100-02-7
87-86-5
85-01 -8
1 08-95-2
129_00_0
95-95-4
88-06-2
Run 1 AcceptanceO % Recovery Limits
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
380
380
380
960
380
380
380
380
380
770
380
380
380
380
380
380
380
380
960
960
380
380
380
380
380
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1uS/kS 1
ug/kg 1uS/kS 1
ug/kg 1
ug/kg 1
uSIq 1
ugftS I
ug/kg 1ug/kg 1
ug/kS 1
ug/lq 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1ug/kg 1ug/l(g 1
ug/kg 1
I
T
I
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
TerphenyFdl4
77
60
67
66
71
53
30-117
33-102
28-104
22-109
27-103
41-120
MA EPH (aliphatics)
Run Prep Method1 MADEP.EPH.
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
MADEP-EPH-o4 1 08t02t20132005 AMY 08102120130935 26358IParameter
cAs
Number
AnalyticalMerhod Result O PQL Units
T
I POL = Practical quantitation limit B = Detected in th6 method blank E = Quantitation of compound exceoded the calibration range H = Out of holding time
ND = Not detectod at orabovsthe PQL J = Estimated rssult< PQL and: MDL P = The RPD between two GC columns excoeds 40% N = Rocoveryisoutofcriteria
Where applicable, all soil sampls analysis are reportsd on a dry wBight basis unless flagged with a nV"
Shealy Environmental Services, lnc.
t
106 Vantage Point Drive Wsst Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 9 of 34
Levol 1 Roport v2.1
t
Client:Terracon Consultants, lnc, Laboratory lD: OH01041-002
Description: HO.E Matrix: Solid
Date Sampled:0713012013 1425 % Solids: 83.7 0810112013 2203
Date Received : 08101 120'13
MA EPH (aliphatics)
I
I
IBatch
26358
Run
1
Prep Method
MADEP-EPH.
AnalyticalMethod Dilution
MADEP.EPH-o4 1
Analysis Date Analyst Prep Date
08102120132005 AMY 08/02/20130935
Parameter
cAs
Number
Analytical
Mathod Result O Units
C9 - C18 Aliphatics
C19 - C36 Aliphatics
Surrogate
MADEP-EPH-O
MADEP-EPH-O
Run 1 AcceptanceO % Recovery Limits
I
I
mg/kg 1
mg/kg 1
ND
ND
12
12
1 -Chloro-octadecane (aliphatic)40-140
MA EPH (aromatics)I
Run
1
Prep Method
MADEP.EPH.
Analytlcal Method
MADEP-EPH-04
Dilution Analysis Date Analyst Prep Date Batch
1 0810312013 1038 AMY 0810212013 0935 26356 I
Parameter
CAS AnalyticalNumber Method Result O
C1l - C22 Aromatics
Surrogate
MADEP.EPH-O
Run'l AcceptanceO c6 Recoyery Limits
mg/kg I
2-Bromonaphthalene (ftactionation 2)
2-Fluorobiphenyl (fractionation 1 )
o - Terphenyl (aromatic)
78
80
65
40-140
40-140
40-140 I
I
I
I
I
I
I
I
PQL = Practical quantitation limit B = Detected in lhs mothod blank E = Quantitation of compound sxcseded tho calibration range
ND = Notdet€ct6d atorabovetho PCIL J = Estimatod rosult< PCILsnd: MDL P =The RPD bet\rvoen two GC columns exceeds 40%
Whers applicable, all soil sample analysis are roported on a dry wsight basis unless flagged with a "VV'
H = Out of holding timo
N = Rgcovery is oul of criteria I
Shealy Environmental Services, lnc.
1OO vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: t0 of 3,t
LsvBl I Report v2.1 I
I
I
T
Client:Terracon Consultants, lnc, Laboratory lD:OH01041-003
Description: HO-S Matrix: Solid
Date Sampled:0713012013 1430 % Solids: 82.5 0810112013 2203
Date Received: 08/01/2013
Semivolatile Orsanic Compounds bv GC/MS
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 1 08102t20132247 JRG 08102120131438 26389
Parameter
cAs
Number
Analytical
Mathod Result O Units Run
I
I
t
I
I
I
I
I
I
I
I
I
I
I
I
I
t
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h )anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
83-32-9
208-96-8
98-86-2
120-12-7
1912-24-9
100-52-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
92-52-4
1 01 -55-3
85-68-7
1 05-60-2
86-74-8
59-50-7
1 06-47-8
11',t-91-1
't11-44-4
108.60-1
91-58-7
95-57-8
7005-72-3
218-01-9
84-74-2
117-84-0
53-70-3
1 32-64-9
91-94-1
120-83-2
84-66-2
1 31 -1 1-3
105-67-9
534-52-1
51-28-5
'121-14-2
606-20-2
117-81-7
206-44-O
8270D
8270D
8270D
8270D
8270D
82700
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82704
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
390
390
390
390
390
990
390
390
390
390
390
390
390
390
990
390
390
390
390
390
390
390
390
390
390
390
390
390
390
990
390
390
390
390
990
990
390
390
390
390
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1uS/kS 1
ug/kg 1
ug/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1uS/kg 1
uSfl(g 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kS 1
ug/kg 1
us/kg 1
ug/kg 1
uglkg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1uS/kS I
ug/kg 1
PQL = Prac,ticalquan0tation l,mit B = Detoctsd in th€ method blank E = Quantitation of compound oxceedsd trle calibration range H = Out of holding tlme
ND = Noldetocted atorabovo ths PQL J = Estimated rssull< PQLand: MDL P = The RPD between two GC columns exceods 40% N. Recovery isoutotcritsria
Wh6re applicablo, all soil sampls analysis are roportod on a dry u€ight basis unless flagged with a nV'
Shealy Environm€ntal Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: ll of34
Lsvel '1 Report v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OH01041-003
Description: HO-S Matrix: Solid
Date Sampled:0713012013 1430 % Solids: 82.5 0810112013 2203
Date Received: 08/01/2013
Semivolatile Organic Compounds by GG/MS
I
I
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
8270D 1 08102120132247 JRG 08102120131438 26389 I
Parameter
cAs
Number
Analytical
Method Result O PQL Units Run
Fluorene
Hexachlorobenzene
Hexachlorobutradiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-N itrosod i-n-propylamine
N-Nitrosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
86-73-7
'118-74-1
87-68-3
77-47-4
67-72-1
1 93-39-5
78-59-1
91-57-6
95-48-7
1 06-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
't00-02-7
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
Run 1 Acceptancea % Recovery Limits
8270D
8270D
8270D
8270D
82700
82700
8270D
8270D
82700
82700
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1
uS/kS 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
390
390
390
990
390
390
390
390
390
800
390
390
390
390
390
390
390
390
990
990
390
390
390
390
390
I
I
I
I
I
I
I
t
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
I
I
I
80
64
68
69
75
53
30-117
33-102
28-104
22-109
27-103
41-120
MA EPH (aliphatics)
Run Prep Method
1 MADEP.EPH-
Analytical Method Dilution Analysls Date Analyst Prep Date Batch
MADEP-EPH-o 1 08102120'.t32035 AMY 0810212013093s 26358
Parameter
cAs
Number
Analytlcal
Method Result O IPQLUnits Run
I
PQL = Practical quantitation limit B = Dotsted in th€ m€thod blenk E = Quantitation of compound *c66ded the calibration rangs H = Out of holding tims
NO = Notdstsctsd atorabove the POL J = Estimatod result< PQLand: MDL P = The RPD botw€en two GC columns oxc6eds40% N = Recovory is outofctitoria
Wh6re applicable, all soil sample analysis aro roported on a dry wsight basis unless ilagged with a nV"I
Sh€aly Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 25172 [phone] Fax [phone] www.shealylab.com
Page: 12 of34
Lovsl'l Repoftv2.l
I
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01041-003
Description: HO-S Matrix: Solid
Date Sampled:0713012013 1430 % Solids: 82.5 0810112013 2203
Date Received: 08/01 /201 3
MA EPH (aliphatics)
I Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
r 1 MADEP-EPH- MADEP-EPH-oA 1 08t02t20132035 AMY 08102120130935 263s8
CAS AnalyticalParameter Number Method Result O POL Units Runt
t
C9 - C18 Aliphatics
C19 - C36 Aliphatics
Surrogate
MADEP-EPH.O ND
MADEP-EPH-O ND
Run 1 Acceptancea % Recovery Limits
12 mg/kg 1
12 mg/kg 1
I-Chloro-octadecane (aliphatic) 75 40-140
I MA EPH (aromatics)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-o ',t 08103t20',t31107 AMY 0810212013 0935 26356I
I
CAS AnalyttcalParameter Number Morhart Result O PQL Unlts Run
Cl'l -C22 Aromatics
Surrogate
MADEP.EPH-O ND
Run 1 AcceptanceO % Recovery Limits
12 mg/kg 1
I
I
I
I
I
I
I
I
2-Bromonaphthalene (fractionation 2) 57 40-140
2-Fluorobiphenyl (ftactionation 1) 76 40-140
o - Terphenyl (aromatic) 60 40-140
t PQL=Practicalquantitationlimit B=Detectadinlhemethodblank E=Quantitationofcompoundexce€dedthecallbrationrange H=Outofholdingtimo
ND = Notdetoctod storabove $le PQL J = Estimated result< PQL and: MDL P =The RPD betwoen two GC columns sxceeds 40% N = Recovsryis outofcriteria
where applicable, all soil sample analysis ars reported on a dry weighl basis unless flagged with a "w'
Shealy Environmental Services, lnc.
t
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 13 of34
Lovsl 1 Report v2.l
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01041-004
Description: HO-W Matrix: Solid
Date Sampled:0713012013 1435 % Solids: 75.1 0810112013 2203
Date Received : 08101 12013
Semivolatile Orqanic Compounds bv GC/MS
I
I
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 1 08t02t20132313 JRG 08t02120131438 26389 I
Parameter
cAs
Number
Analytical
Mathod Result O Units Run
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h )anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
83-32-9
208-96-8
98-86-2
120-12-7
1q',t2-24-9
100-52-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
92-52-4
1 01 -5s-3
8$68-7
10560-2
86-74-8
s$50-7
106.47-8
I 1 1-91-1
1't1-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
84-74-2
't17-84-0
53-70-3
132-64-9
91-94-1
120-83-2
84-66-2
131-11-3
105-67-9
534-52-1
51-28-5
121-14-2
606-20-2
117-81-7
206-44-0
8270D
8270D
8270D
8270D
82700
82700
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
82700
8270D
82700
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
430
430
430
430
430
1 100
430
430
430
430
430
430
430
430
1 100
430
430
430
430
430
430
430
430
430
430
430
430
430
430
1 100
430
430
430
430
1 100
1 100
430
430
430
430
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
uglkg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
t
I
I
I
I
I
I
I
I
I
I
I
t
PQL = Practical quantitation limit B = D8lectsd in the method blank E = Quantltalion of compound excoeded th6 calibEtion range H = Out of hotding tim6
ND = Notdotected atorabovetho PQL J = Eslimatod rssult< PQL and: MDL P = The RPD beiw€on two GC columns exceods 40olo N = Recoveryis outofcritorla
Where applicablo, all soil sample anallrsis are reported on a dry w€ight basis unloss flagged with a nV"I
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] t www.shealylab.com
Page: ltl of 34
Lovsl't Reportv2.l
I
I
I
t
Client:Terracon Consultants, lnc. Laboratory lD: OH01041-004
Description: HO-W Matrix: Solid
Date Sampled:0713012013 1435 % Solids: 75.1 0810112013 2203
Date Received: 08/01/2013
Semivolatile Orsanic Compounds bv GC/MS
I Run Prep Method
1 35s0C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
82700 1 08t02t20132313 JRG 08t02120131438 26389
Parameter
CAS
Number
Analytical
Merhod Result Ot
I
I
I
t
I
I
I
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-N itrosodi-n-propylam ine
N-N itrosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
86-73-7
1',t8-74-1
87-68-3
77-47-4
67-72-1
1 93-39-5
78-59-1
91-57-6
95-48-7
1 06-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
1 00-01 -6
98-95-3
88-7s-5
100-02-7
87-86-5
85-01-8
1 08-95-2
1 29-00-0
95-95-4
88-06-2
Run 1 AcceptanceO % Recovery Limits
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
82700
8270D
8270D
8270D
8270D
82700
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
430
430
430
1 100
430
430
430
430
430
870
430
430
430
430
430
430
430
430
1 100
1 100
430
430
430
430
430
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uS/kg
ug/kg
ug/kg
ug/kg
ug/kS
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uslks
ug/kg
usfts
uS/kg
ug/kg
uS/ks
uS/kS
ug/kg
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
I
I
I
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene{5
Phenol-d5
Terphenyl-d14
74
75
64
67
73
56
30-1 1 7
33-1 02
28-104
22-109
27-103
41-120
MA EPH (aliphatics)
Run Prep Method1 MADEP-EPH.
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
MADEP-EPH-oA 1 08t02t20132104 AMy 08102120130935 26358ICAS
Number
Analytical
Method Result OParameter PQL Unlts Run
I
I PQL = Practical quantitation limit B = Detectod in th6 msthod blank E = Quantitation of compound excsedsd the calibration range H = Out of holding time
ND = Notdotectsd atorabovethe PQL J = Estimated result< PQL andi MDL P = The RPD between two GC columns excosds40o/o N = Recoveryis outofcriteria
Whers applicable, all soil sampl8 analysis aro reporlgd on a dry w€ight basis unless flagged with a nV"
Shealy Environmental SeMces, lnc.
I 106 Vantase Point Ddve West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.comI Page: 15 of 34
Lovel 1 ReDort vz.l
I
Client:Terracon Consultants, lnc. Laboratory lD: OH0'1041-004
Description: HO-W Matrix: Solid
Date Sampled:0713012013 1435 % Solids: 75.1 0810112013 2203
Date Received: 08/01/2013
MA EPH (aliphatics)
I
T
IBatch
263s8
Run
1
Prep Method
MADEP-EPH-
Analytical Method Dilution
MADEP-EPH.OA 1
Analysis Date Analyst Prep Date
08t02t2013 2104 AMy 08/0212013 0935
Parametel
CAS
Number
Analytical
Method Result O Units
C9 - Cl8 Aliphatics
C19 - C36 Aliphatics
Surrogate
MADEP-EPH-O
MADEP-EPH.O
Run 1 AcceptanceA % Recovery Limits
mg/kg 1
mg/kg 1
ND
ND
13
13
I
I
1 -Chloro-octadecane (aliphatic)40-140
MA EPH (aromatics)t
Batch
26356
Run
1
Prep Method
MADEP-EPH-
Analytical Method Dilution Analysis Date Analyst Prep Date
MADEP-EPH-o4 1 08/03/2013 1136 AMy 08/0212013 0935 I
Parametel
CAS AnalyticalNumber ilathod Result O
C11 -C2zAromatics
Surrogate
MADEP-EPH-O
Run 1 AcceptanceO % Recovery Limits I13mg/kg
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (fractionation 1 )
o - Terphenyl (aromatic)
49
86
75
40-140
40-140
40-140 t
I
I
I
I
t
I
t
PCIL = Practical quantiiation limit B = Datected in lhe method blank E = Quantitation of compound exc66ded the calibration range
ND=NotdetoctodalorabovathsPOL J=Estimatedresult<PQLandiMDL P=TheRPDbetweentwoGCcolumnsexcseds/t0%
Whoro applicablo, all soil sample analyEis ars reported on a dry weight basis unless flagged with a "w'
H = Out of hotdlng time
N = Recovgry is out of criteria I
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 16 of 34
Lav6l 1 Rsport v2.1 t
I
I
I
Client:Terracon Consultants, lnc. Laboratory lD: OH01041-005
Description: HO-B Matrix: Solid
Date Sampled:0713012013 1440 % Solids: 83.3 0810112013 2203
Date Received: 08/01/2013
Semivolatile Orsanic Compounds bv GC/MS
Run Prep Method1 3550C
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 5 08i05/20131211 JRG 08t02t20131438 26389
Parameter
CAS
Number
Analytical
Methad Result O Units Run
t
I
I
I
I
I
I
I
t
I
I
t
I
I
I
T
t
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
1,1'-Biphenyl
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-C hloroethyl)ether
bis(2-Chloroisopropyl)ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Di-n-butyl phthalate
Di-n-octylphthalate
Dibenzo(a,h)anth racene
Dibenzofuran
3, 3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
Dimethyl phthalate
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluoranthene
83-32-9
208-96-8
98-86-2
'120-12-7
1912-24-9
100-52-7
56-55-3
50-32-8
20s-99-2
1g',t-24-2
207-08-9
92-52-4
1 01 -55-3
85-68-7
105-60-2
86-74-8
59-50-7
1 06-47-8
1 1 1-91-1
111-44-4
1 08-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
84-74-2
117-84-O
53-70-3
132-64-9
91-94-1
120-83-2
84-66-2
1 3't -1 1-3
10567-9
534-52-1
51-28-5
121-14-2
606-20-2
1'.17-g',t-7
206-44-0
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
82700
8270D
1 900
1900
't900
1 900
1 900
4800
1900
1900
1900
1900
1900
1 900
1 900
1 900
4800
1900
1900
1900
1900
1900
1 900
1 900
1 900
1900
1900
1 900
1 900
1 900
1 900
4800
1900
1900
1900
1900
4800
4800
1900
1900
1900
1900
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kS
udkg
us/kg
uS/kg
usfts
ug/kg
ug/kg
ug/kg
us/kg
ug/kg
uS/kS
ug/kg
ug/kg
ug/lq
ug/kg
ug/kg
ug/kg
uS/kS
ug/kg
ug/kg
ug/kg
ug/kg
uS/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PQL = Practical quantitatlon limit B = Dstected in the method blank E = Quantitalion of compound sxceeded the calibration range H = Out of holding tlme
ND = Notdetect€d atorabovethe PQL J = Estimated rosult< PQL and: MDL P = The RPD between two GC columns exceeds 40% N = Rocoveryi6outofctilerla
lryher€ applicablg, all soil sample analysis are reportgd on a dry reight basis unloss flagged with a "W'
Shealy Environmental S€rvices, lnc.
106 Vantage Point Drive West Columbla, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: l7 of34
Lsvol I Roport v2.1
Client:Terracon Consultants, lnc. Laboratory lD: OH01041-005
Description: HO-B Matrix: Solid
Date Sampled:0713012013 1440 % Solids: 83.3 0810112013 2203
Date Received: 08/01/201 3
Semivolatile Organic Gompounds by GC/MS
I
I
Run Prep Method1 3550c
Analytical Method Dilution Analysis Date Analyst Prep Date Batch8270D 5 08/05/20',t31211 JRG 08102120131438 26389 I
Parameter
cAs
Number
Analytical
Method Result O Units Run
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentradiene
Hexachloroethane
lndeno( 1,2,3-c,d)pyrene
lsophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4-Methylphenol
N-N itrosodi-n-propylam ine
N-Nitrosodiphenylamine (Diphenylamine)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nihobenzene
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,$Trichlorophenol
2,4,6-Trich lorophenol
Surrogate
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
1 93-39-5
78-59-1
91-57-6
95-48-7
1 06-44-5
621-64-7
86-30-6
91-20-3
88-74-4
99-09-2
1 00-01-6
98-9s-3
88-75-5
100-02-7
87-86-5
85-01-8
1 08-95-2
129-00-0
95-95-4
88-06-2
Run 1 AcceptanceO 96 Recovery Limits
8270D
8270D
8270D
8270D
8270D
8270D
8270D
82700
8270D
8270D
8270D
8270D
82700
8270D
8270D
82700
82700
8270D
8270D
8270D
82700
8270D
82700
82704
82700
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1 900
1 900
1 900
4800
1900
1900
1900
1900
1900
3900
1900
1900
1900
1900
1900
1900
1900
1900
4800
4800
1900
1900
1900
1900
1900
I
I
I
I
I
I
I
I
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 'l
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 'l
ug/kg 1
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
NitrobenzenedS
Phenol-d5
Tcrphenyl-d14
70
76
74
76
81
58
30-117
33-102
28-104
22-109
27-103
41-120
MA EPH (aliphatics)
I
I
IRun Prep ll/lethod
1 MADEP-EPH-
Analytical Method Dilutaon Analysis Date Analyst Prep Date Batch
MADEP-EPH-o4 1 08/05/2013 1435 AMY 0810212013 0935 26358
Parameter
CAS
Number
AnalyticalMethod Result O IPQLRun
I
PQL = Practical quantitation limit B = Dotected in the m€thod blank E = Quantitation of compound €xc€sded ths calibralion rango H = Out of holding timo
ND = Not dstocted atorabovethe PQL J = Estimated result< PQL and: MDL P = The RPD betw€€n two GC columns exce€ds 40% N = Recoveryis outofctitoria
Wherg applicabla, all soil sample analysis are reported on a dry r,voight basls unless flagged with a nV'I
Shealy Environmental Services, lnc.
l06VantagePointDrive W€stColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 18 of34
L6vel'l Raportv2.l
I
I
I
T
Client:Terracon Consultants, lnc. Laboratory lD: OH01041-005
Description: HO-B Matrix: Solid
Date Sampled:0713012013 1440 % Solids: 83.3 0810112013 2203
Date Received: 08/01/201 3
MA EPH (aliphatics)
I Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
r 1 MADEP-EPH- MADEP-EPH-o 1 08/05/2013143s AMY 08102t2013 0935 26358
I
I
CAS AnalyticalParameter Number Marhart Result O PQL Units Run
C9 - C18 Aliphatics
G19 ' C36 Aliphatics
Surrogate
MADEP-EPH-O ND
MADEP-EPH.O 550
Run 1 AcceptanceO % Recovery Limits
12 mg/kg 1
12 mg/kg 1
1-Chloro-octadecane (aliphatic) 75 40-140
I MA EPH (aromatics)
Run Prep Method Analytica! Method Dalution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-oA ',t 08/05/20131534 AMY 0810212013 0935 26356I
I
CAS AnalyticalParameter Number Marhar{ Result O PQL Unitt Run
Cl1 -C22Aromatics
Surrogate
12 mglkg IMADEP.EPH.O 38
Run 1 AcceptanceO % Recovery Limits
t
I
I
T
I
I
I
I
2-Bromonaphthalene (fractionation 2) 59 40-140
2-Fluorobiphenyl (fractionation 1) 82 40-140
o - Terphenyl (aromatic) 75 40-140
I PQL = Practical quantitation limit B = Detectsd inthe method blank E = Quantitation ofcompound exc€€dod ths calibretion range H = Out ofholding time
ND = Notdetectod at orabov6 the PQL J = Estimatod rssult< PQL and: MDL P =The RPD between two GC columns sxc€eds 40% N = Recoveryisoutofc.itStia
Whers applicablo, all soil sample analysls are reported on a dry w€ight basis unloss flaggsd with a'W'
Shealy Environmental Servlces, lnc.
I
106 VantaSe Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 19 of34
L6v€l I Roport v2.1
I
QG Summary
Shealy Environmental Sorvices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sh€alylab.com
Pager 20 of 34
Levsl I Report v2.l
I Semivolatile Organic Compounds by GC/MS - MB
I Sample lD: OQ26389-001
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 1438
I Parameter Result Analysis Date
I
t
I
I
I
t
I
T
t
T
I
I
T
1 ,1 '-Biphenyl
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
2-Nitrophenol
3 & 4-Methylphenol
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Din itro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitroaniline
4'Nitrophenol
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Caprolactam
Carbazole
Chrysene
Di-n-butyl phthalate
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
330
330
330
330
330
830
330
330
330
330
330
330
330
330
670
830
330
830
330
330
330
330
330
830
330
330
330
330
330
830
330
330
330
330
330
330
330
330
330
330
830
330
330
330
ug/kg
ugikg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
08102120132009
08t0212013200s
08t02t20132009
08102120132009
oaoa2u32009
08102120132009
08102120132009
0810212u32a09
o8to2l201320og
08/02/2013 2009
o8to2l20't32009
08102120132009
08t02t20132009
08t02t20132009
08to?i2013200s
08t02120132009
08t02/2u32009
08rca20't32009
08t02t20132009
08t02120132009
o8toa2u32009
08t0u20132009
08t02120132009
oaoa20132w9
08t0u20132009
o8t0u2013200s
08t02i20132009
08t02t2013200s
08/022013 2000
08t02120132009
08t02t20132009
o8t02t2u3zaog
o8t02120132009
o8t02120132009
08t02120132009
081w20132009
o8to2t20rc2049
08t0z2u32004
08t02120132009
0810212013200,9
08/02/2013 2009
o81o2t20132009
08102120132009
o8to2t20132009
POL = ftactical quantitatlon limit
ND = Not detocted at or abovo the PQL
P = Ths RPD betwsen two GC columns exceeds 40olo N = Rocovery is out of criteria
J = Estimatod rssult < PQL and: MDL + = RPD is out of criteria
t
Where applicablo, all soil sample anal)rsis are reported on a dry woight basis unless flagged with a 'W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:21 of 3,1
Lewl 1 R.port v2.l
I
ISemivolatile Organic Compounds by GG/MS - MB
Sample lD: OQ26389-001
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 1438
I
Parameter a IAnalysis Date
Di-n-octylphthalate
Dibenzo(a,h )anthracene
Dibenzofuran
Diethylphthalate
Dimethyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
N-N itrosodi-n-propylamine
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
I
I
I
I
I
t
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
330
330
330
330
330
330
330
330
330
830
330
330
330
330
330
330
330
830
330
330
330
ND
ND
ND
ND
ND
ND
o
08102t20132009
08t02t20't32009
08/021201 3 2009
08102120132009
08102120132009
08/02/2013 2009
08t0?,20132009
08/02y2013 2009
08t02t20132009
08/02/2013 2009
08t02t20132009
0u02t20132009
08to2120132009
08t02t2013200s
08102120132009
08102120132009
oaoa2u32009
08t02t20132009
08t02t20132009
08t02t20132009
08t02t20132009
N-Nitrosodiphenylamine (Diphenylamine) ND
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Sunogate % Rec Acceptance
Limit
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
87
78
80
82
89
81
30-1 1 7
33-102
28-104
22-109
27-103
41-120
I
I
I
I
I
I
t
PQL = Practical quantitatlon limit
ND = Not d6t6cted at or above ths PQL
P = The RPD betwo€n two GC columns sxceeds 40% N = Rocovory is out of criteria
J = Estimatod rosutt < PQL and 2 MDL + = RPO is out of giteria I
1
Wh6re applicabls, all soil sample analysis ar€ reported on a dry w€ight basis unless flagged with a "w.
Note: Calculations are performed before rounding to avoid round-off errors in calculated resuhs
Shealy Environmental Services, lnc.
l06VantagePointDriv€ WostColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 2!l of 34
Level 1 R60ort v2.1
I
I Semivolatile Organic Compounds by GC/MS - LCS
t Sample lD: Oe26389-002
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 '1438
I Parameter
SpikeAmount Result % Rec(uslks) (us/kg) O Dil % Rec Limit Analysis Date
I
I
t
I
I
T
I
I
I
T
I
I
I
1,1'-Biphenyl
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
2-Nitrophenol
3 & 4-Methylphenol
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-Chloro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Atrazine
Benzaldehyde
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Caprolactam
Carbazole
Chrysene
Di-n-butyl phthalate
3300
3300
3300
3300
3300
1 7000
6700
6700
3300
3300
3300
3300
6700
6700
6700
6700
6700
1 7000
3300
3300
3300
3300
6700
1 7000
3300
3300
3300
3300
3300
3300
3300
3300
3300
3300
3300
3300
6700
3300
3300
3300
3300
3300
3300
3300
2200
2400
2300
2400
3000
16000
5100
5100
2000
2400
2400
2700
5000
4800
4900
6000
4800
16000
2500
31 00
2900
2400
6600
1 9000
2500
2800
2600
2500
2400
2900
2600
3't 00
2900
2300
2800
2300
4900
2400
2900
2800
3300
2800
2400
2900
68
72
70
72
9'l
94
77
77
60
71
72
80
75
72
74
91
72
98
74
92
86
71
99
113
75
84
77
75
73
87
79
93
88
70
84
70
74
72
86
84
98
85
73
86
49-1 1 0
46-122
3B-1 1 5
41-113
33-123
45-127
48-124
47-125
31-127
37-106
40-106
32-107
45-123
35-108
39-108
46-113
24-127
40-1 30
46-1 1 8
49-1 18
10-125
47-116
48-127
1 8-1 54
46-114
44-122
48-111
50-1 1 I
48-1 16
34-99
47-121
55-134
28-139
36-125
47-130
39-108
32-105
31-102
45-128
46-128
43-121
47-128
45-126
51-129
08t02t20132035
08t02120132035
08t02120132035
08t02t2afi2035
08t02120132035
08t02t20132035
o8to2120132035
08t02t20132035
08t02t20132035
08t02t20132035
08t02t20132035
o8to2l20't32015
08t02t20132035
08t02t20132035
08t0?/2u32035
08102120132035
o8toa2u320s5
08t02120132035
08102120132035
08102t20132035
0810u20132035
o8to2120132035
08/02/2013 2035
o8to2l20't32035
08n2J20132035
08/022013 2035
08102120132035
08t0u20132035
0810u20132035
o8to2t20132035
08/02/2013 2035
08t02t20132095
08t02t20132035
0810u20132035
08n?,20132035
0810?,2u32035
08102120132035
08102120132035
08t02120132035
08t02120132035
o8lo2l20't32035
08t02t20132035
08102120132035
08102120132035
I
I
PQL = Practical quantitation limit
ND = Not dBtocted at or above th6 PQL
P = The RPD bstween two GC columns exceeds 40% N = Re@very is out of criteria
J = Estimated result < PQL and: MDL + = RPO is out of criteria
Wher6 applicable, all soil sample analysis aro reportsd on a dry wEight basis unless flagged with a "w"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'111 www.shealylab.com
Page: 23 of 3,1
L6vel 1 Rcpod v2.1
I
ISemivolatile Organic Compounds by GG/MS - LCS
Sample lD: OQ26389-002
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 '1438
t
Spike
Amount(us/ks)Result(us/ks)o/o Rec
% Rec
Limit IParameterAnalysis Date
Di-n-octylphthalate
Dibenzo(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutradiene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-c,d)pyrene
lsophorone
N-N itrosodi-n-propylam ine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Surrogate
2800
2500
2400
2700
2500
2700
2600
2800
2400
11000
2',t00
2500
2s00
2700
2600
2300
2600
1 7000
2500
2700
2700
Acceptance
Limit
08t02120132035
08t02t20132035
08102t20132035
08t02t20132035
08102120132035
08102120132035
08102120132035
0u02120132035
08102t20132035
08t02120132035
08102120132035
08102t20132035
08102120132035
08i0?,2u32035
08102120132035
08t02t20132035
08102120132035
08/02t20132035
o8rc?,2u32035
08102120132035
08t0?,2u32035
N-Nitrosodiphenylamine (Diphenylamine) 3300
3300
3300
3300
3300
3300
3300
3300
3300
3300
1 7000
3300
3300
3300
3300
3300
3300
1 7000
3300
3300
3300
O %Rec
83
76
72
81
74
82
79
83
72
67
63
76
76
81
77
70
78
102
74
82
80
49-142
45-122
45-112
49-123
48-120
50-123
48-117
44-122
33-103
18-121
30-96
45-123
41-113
32-115
53-150
36-1 1 0
33-',114
27-138
49-117
36-108
47-119
I
t
t
I
I
I
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyldl4
81
67
87
83
85
59
30-117
33-102
28-104
22-109
27-103
41-120
I
I
T
t
I
I
t
PQL = Practical quantitation limit
ND = Not detsctsd at or abov€ th8 PQL
P = Ths RPD betw€en two GC columns excesds 407o N = Recov€ry is out of criteria
J = Estimated result < PQL and : MDL + = RPD is out of critgria t
I
Wh6re applicablo, all soil sampls analysB aro roportod on a dry w€ight basis unless flagged with a ry\r
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
'106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 24 of 34
Lovsl 1 Rsport v2.l
I
I Semivolatile Organic Compounds by GC/MS - MS
t Sample lD: OH01041-001 MS
Batch:26399
Analvtical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 1438
I Parameter
Sample SPike
Amount Amount(us/ks) (uq/kq)
Result
(us/ks)Dilo % Rec
% Rec
Limit Analysis Date
AcenaohtheneI il:[T#[:"J"
Anthracene
t ffiLn*"
Benzo(a)anthracene
Benzo(a)pyreneI t::::HfJ:;'H:
Benzo(k)fluoranthene
t 1,1'-Biphenylr rTi},lli,i;Il,lliJl' "'n"'
Caprolactram
I ;:ffi::-,"thy,pheno,
4-Chloroaniline
I bis(2-Chloroethoxy)methaner iilli 3lilff.l,lllf",Til.",
2-Chloronaphthalene
t ?.3lilffilllilpheny,erher
Chrysene
I Di-n-butyl phthalateI 3:#:Illffi',"':""."
DibenzofuranI l:lSiTJIii#''"
Diethylphthalate
Dimethvl ohthalateI i:IBiI-",1',lJ!["J,*"*,
2,4-DinitrophenolI l:l.3ilillfllll!
bis(2-Ethylhexyl)phthalate
Fluoranthene
t Frliiilio,oo"n,"n"
Hexachlorobutadiene
t
Hexachlorocyclopentadiene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4200
4200
4200
4200
4200
4200
4200
4200
4200
4200
4200
4100
4200
4200
4200
4200
4200
4200
4200
8400
4200
4200
4200
4200
4200
4200
4200
4200
4200
8400
4200
4200
4200
4200
21000
21000
8400
8400
4200
4200
4200
4200
4204
21000
3000
3300
3200
3100
3100
3't00
3300
3800
3700
3000
3700
3100
3200
3300
4200
3500
3800
3300
3000
s200
2700
2800
3000
3000
3000
3500
3900
2800
2900
6700
3200
3300
3000
3800
20000
1 9000
6300
6200
3500
3400
3200
3500
2900
1 5000
72
79
76
74
75
75
78
91
90
7',!
88
74
76
80
101
84
91
79
71
62
64
66
71
71
72
85
93
67
69
80
76
78
71
91
96
91
75
74
84
81
78
84
70
72
30-130 08102t20132',128
30-130 08t02120132128
30-130 08t02120132128
30-130 08102120132128
30-130 08102120132128
30-130 08t02120132128
30-130 08102120132128
30-130 08102120132128
30-130 08/0i,2u32128
30-130 08/0?,20132128
30-130 08t02t20132128
30-130 08102120132128
30-130 08i0?,20132128
30-130 08nz20132128
30-130 08/0a20132128
30-130 08/0?,20132128
30-130 08102t20132128
10-130 08102t20132128
30-130 08102t20132128
30-130 08102t20132128
30-130 08102t20132128
30-130 08/0,J20132128
30-130 081o2t20132128
30-130 08102t20132128
30-130 08102t20132128
30-130 08to?,20132128
30-130 0810?J20132128
30-130 08n?J20132128
30-130 081o2t20132128
30-130 08102t20132128
3G.130 08102t20132128
30-130 08/02t20132',t28
30-130 08/02t20132128
30-130 08/0a20132128
30-130 08na20132128
30-130 08t02t20132128
30-130 0u02t20132128
30-130 0810a20132',|.28
30-130 08/0u20132128
30-130 08102120132128
30-130 08102120132128
30-130 08t02120132128
30-130 0810a20132128
30-130 081oa20132128
t
I
PCIL = ftactical quantitation limit
ND = Not dotected at or above lhe PQL
P = The RPD betwesn two GC columns excsods 40% N = Recovery is out of criieria
J = Estimated result < PQL and : MDL + = RPD is out of dteria
wher6 applicable, all soil sample analyEis ars report€d on a dry weight basis unless flagged with a nv'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealyhb.com
Page: 25 of 34
Level 1 Rcport v2.1
I
ISemivolatile Organic Gompounds by GC/MS - MS
Sample lD: OHO1041-001MS
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 08102120'13 1438
I
Sample
Amount(us/kg)
Spike
Amount(us/ks)
Result
(us/ks)
% Rec
Dil % Rec Limit Analysis Date IParameter
Hexachloroethane ND
lndeno(1,2,3-c,d)pyrene ND
lsophorone ND
2-Methylnaphthalene ND
2-Methylphenol ND
3 & 4-Methylphenol ND
N-Nitrosodi-n-propylamine ND
N-Nitrosodiphenylamine (Diphenylamine) ND
Naphthalene ND
2-Nitroaniline ND
3-Nitroaniline ND
4-Nitroaniline ND
Nitrobenzene ND
2-Nitrophenol ND
4-Nitrophenol ND
Pentachlorophenol ND
Phenanthrene ND
Phenol ND
Pyrene ND
2,4,5-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Surrogate
30-130 08102t20132128
30-130 08102120'132128
30-130 08102120132128
30-130 08102t20132128
30-130 08102120132128
30-130 08102120132128
30-130 08102120132128
30-130 08102t20't32128
30-130 08t02t20't32128
30-130 08102120132128
30-130 08102120132128
30-130 08102120132128
30-130 08t02120'.t32128
30-130 08102120132128
30-130 08t02120132128
30-130 08102t20132128
30-130 08to2t20132128
30-130 08102120132128
30-130 08102120132128
30-130 08n?,2u32128
30-130 08n2/20132128
4200
4200
4200
4200
4200
8400
4200
4200
4200
8400
8400
8400
4200
8400
2'1000
2'1000
4200
4200
4200
4200
4200
2400
2900
3200
2900
3300
6300
3200
3100
2900
6800
5500
7800
3100
6000
23000
22000
3000
3100
3200
3400
3300
58
69
76
70
79
75
78
75
69
82
66
93
74
72
110
103
73
74
76
82
79
t
I
I
I
I
I
AcceDtanceO % Rec Lihir
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzened5
Phenol-d5
Terphenyl-d14
I
I
I
I
I
I
I
84
72
72
77
75
58
30-117
33-102
28-104
22-109
27-103
41-120
PQL = Practical quantitation limit
ND = Not d€isctod at or above ihs PQL
P = The RPD bstweon two GC columns exceeds 407o N = Rocovary is out of critaria
J = Estimated r€sutt < PQL and: MDL + = RPD is out of crikria I
tWhere applicable, all soil sample analysis are roported on a dry woight basis unless flag$d with a \rlr'
Note: Calculations are performed before rounding to ayoid round-off errors in calculated re3ults
Shealy Environmental Services, lnc.
106VantagePointDrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Pago: 26 of 34
Lov6l I Ropon v2.'l
I
I Semivolatile Organic Compounds by GG/MS - MSD
I Sample lD: OHo1 041-001 MD
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 0810212013 1438
t Parameter
Sample SPike
Amount Amount Result o/o Rec % RPD(us/ks) (us/ks) (us/ks) A Dil % Rec % RPD Limit Limit Analysis Date
- AcenaohtheneI ffirT#:::"J"
Anthracene
I llffin,o"
Benzo(a)anthracene
Benzo(a)ovreneI :::::HffiJilH:"
Benzo(k)fluoranthene
I 1,1'-Biphenylr ffifi#l};lll,lli"t'"'n"'
Caprolactam
! ;fliffi:-.",hyrpheno,
4-Chloroaniline
I bis(2-Chloroethoxy)methaneI ill[;:3lilff.ll,l",'lil"",
2-Chloronaphthalene
I i:3lilffillliipheny,ether
Chrysene
I Di-n-butyl phthalateT il;flTfi5i1::*,"
DibenzofuranI i:l.i,i"Xi"l""JfJ"'"1''"
Diethylphthalate
Dimethvl DhthalateI i:Il:ffil.f,l!iloJ,on"no,
2,4-DinitrophenolI 3:I3ilixllliffii
bis(2-Ethylhexyl)phthalate. FluorantheneI Ftuorene
I Hexachlorobenzene
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4200
4200
4200
4200
4200
4200
4200
4200
4200
4200
4200
4100
4200
4200
4200
4200
4200
4200
4200
8400
4200
4200
4200
4200
4200
4200
4200
4200
4200
8400
4200
4200
4200
4200
21000
21000
8400
8400
4200
4200
4200
4200
4200
21000
2800
3100
2900
3000
3000
2700
3200
3900
4000
2200
3900
2500
3000
3200
3700
3400
3600
2900
3000
4500
2300
2300
2600
2800
3000
3500
4400
2400
2700
6500
3100
3200
2900
4100
1 9000
1 8000
6100
6000
3400
3300
3100
3400
2400
1 1000
167
174
169
173
171
165
177
193
195
152
193
160
't 72
177
189
182
185
169
1 71
154
156
154
163
167
1 71
183
't 104
't 57
165
177
174
175
169
199
192
187
173
172
't 82
180
174
180
157
155
6.'1 30-130 40 08102120132154
5.9 30-130 40 08102120132154
8.6 30-130 40 081042u32154
1.8 30-130 40 08102120132154
5.9 30-130 40 08102120132154
13 30-130 40 081021201321s4
1.1 30-130 40 08102J201321542.1 30-130 40 08/02120132154
5.7 30-130 40 08102120132154
32 30-130 40 081021201s2154
5.6 30-130 40 0810?/2u32'.154
21 30-130 40 08102120132154
5.3 30-130 40 08102120132154
2.9 30-130 40 08102120132154
12 30-130 40 08102120192'.t542.5 30-130 40 08102120132154
7.O 30-130 40 0810u20132154
13 10-130 40 08102120'.132154
0.042 30-130 40 08102120132154
14 30-130 40 08102120132154
14 30-130 40 081021201321s4
20 30-130 40 08102120132154
11 30-130 40 081021201321545.6 30-130 40 08102120132154
0.95 30-130 40 08102120132154
2.1 30-130 40 08102120132154
12 30-130 40 08102120',132154'r5 30-130 40 08102120132154
4.8 30-130 40 08na20132154
3.4 30-130 40 08102120132154
2.1 30-130 40 08102120132154
3.8 30-130 40 08102120132154
3.1 30-130 40 0u0a20132154
8.5 30-130 40 0uoa20'132154
5.0 30-130 40 08102120132154
4.6 30-130 40 08102120132154
3.7 30-130 40 08/0?20132154
3.4 30-130 40 0uoa20't32154
2.5 30-130 40 081021201321541.7 30-130 40 08102120132154
4.7 30-130 40 0u0420132154
4.s 30-130 40 08n42u32154
20 30-130 40 0u0?,20't32154
26 30-130 40 08102120132154
I
Hexachlorocyclopentadiene
t
t
PQL = Practical quanfiation limit
ND = Not dgtected at tr ebove the POL
P = The RPD betwe€n two GC columns excoeds 40% N = Recovery is out of critoria
J = Estimated result < PQL and 2 MDL + = RPD is out of criteria
Whero applicable, all soil sample analysis are reporled on a dry w€ight basis unless flagged with a nV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Orive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 27 of 34
l€vel 1 Raportv2.l
I
ISemivolatile Organic Compounds by GC/MS - MSD
Sample lD: OHo1041 -001 MD
Batch:26389
Analytical Method: 8270D
Matrix: Solid
Prep Method: 3550C
Prep Date: 08102120'13 1438
I
Sample SPike
Amount Amount Result(uq/kE) (uq/ks) (us/ks) O Dil % Rec
% Rec
o/o RPD Limit
% RPDLimit Analysis Date IParameter
Hexachloroethane ND
lndeno(1,2,3-c,d)pyrene ND
lsophorone ND
2-Methylnaphthalene ND
2-Methylphenol ND
3 & 4-Methylphenol ND
N-Nitrosodi-n-propylamine ND
N-Nitrosodiphenylamine (Diphenylamine) ND
Naphthalene ND
2-Nitroaniline ND
3-Nitroaniline ND
4-Nitroaniline ND
Nitrobenzene ND
2-Nitrophenol ND
4-Nitrophenol ND
Pentachlorophenol ND
Phenanthrene ND
Phenol ND
Pyrene ND
2,4,5-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Sunogate AcceotanceO % Rec Liinit
4200
4200
4200
4200
4200
8400
4200
4200
4200
8400
8400
8400
4200
8400
21000
21000
4200
4200
4200
4200
4200
2000
2400
3200
2700
3100
6000
3100
3100
2500
5700
5400
7500
2800
s900
23000
21000
3000
2800
3100
2900
2700
47
58
76
64
73
72
74
73
59
69
64
90
67
70
108
101
71
68
74
69
65
20 30-130
17 30-130
0.23 30-130
8.5 30-1308.3 30-130
3.5 30-130
5.3 30-1302.2 30-13016 30-130
17 30-130
1.9 30-130
2.9 30-130
9.2 30-130
2.3 30-130
1.4 30-1302.8 30-1302.9 30-130
8.1 30-130
1.6 30-130
'17 30-13019 30-130
40 08102120132',t54
40 08102120132154
40 08102t20132154
40 081o2t2013215440 08102120132154
40 0810212013215440 08102t2013215440 08/0?,2013215440 08102120132154
40 08102t2013215440 08102t20132154
40 08t02t20132154
40 08t02t20132154
40 08t02t20132154
40 08t02t2013215440 08t0a2u3215440 08t0a20132154
40 08t02t2013215440 08102120132154
40 08102120132154
40 08t02t20132154
I
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2,4,6-Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
79
58
62
69
69
54
30-1 1 7
33-102
28-104
22-109
27-103
41-120
I
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I
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I
I
IPQL = Practical quantitation limit
ND = Not d€tocted at or abov6 tho PQL
P = Ths RPD bstweon lwo GC columns exceeds 407o N = R6covory is out ofcritgria
J = Estimated result < PQL and 2 MDL + . RPD is out of critsria
Whers applicable, all soil sample analysis ars reported on a dry w6ight basis unlsss flaggBd with a "v\f
Note: Calculations are performed before rounding to avoid round-off errors in calculated results TShealy Envircnmental Services, lnc.
'106VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page: 28 of 34
Lovel 1 Roport v2.l
I
I MA EPH (aromatics) - MB
f Sample lD: OQ263S6-OO1
I Batcn:26356
Analytical Method: MADEP-EPH-O4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
t Parameter Result O Dit PQL Units Analysis Date
C11 - C22 Aromatics
I surrosate
ND1
AcceptanceO % Rec Lihit
10 mg/kg 0810312013 0842
2-Bromonaphthalene (fractionation 2) 72 40-140
t :-:i:**'*nationl) Ii ii:"',,ii
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PCIL = Praciical quantitation limit P = The RPO betw€en two GC columns exceeds 40% N = Rocovsry is out of criteria
ND = Not detoctEd at or abovs ths PQL J = Estimatod result < PQL and: MDL + = RPD is out of criteria
Whorc applicable, all soilsample analysis aro reported on a dry wsight basls unloss flagged with a "W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environm€ntal Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 29 of 34
Levcl I Rsportv2.l
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MA EPH (aromatics) - LCS
Sample lD: 9q26356-gg2
Batch:26356
Analytical Method: MADEP-EPH-o4
Matrix: Solid
Prep Method: MADEP-EPH-O4
Prep Date: 08/02/2013 935
t
I
TParameter
Spike
Amount
(mslks)Result(ms/ks)% Rec
% Rec
Limit Analysis Date
C1'l -C22Aromatics
Surrogate
85
o
52
AcceptanceLimit
40-140 08/03/2013 091 1
% Rec
2-Bromonaphthalene (ftactionation 2)
2-Fluorobiphenyl (fractionation'l )
o - Terphenyl (aromatic)
81
84
70
40-140
40-140
40-140
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IPQL = Practical quanlitation limit
ND = Not dotocted at or above the PQL
P = The RPD b3lreen two GC columns exceeds 4oolo N = Rocovory is out of criteria
J = Estimatod result < PQL and: MDL + = RPD is out of crilsria
Wher€ applieblB, all soil samplo analysis are r6porlsd on a dry weight basis unless flaggsd wilh a nV"
Note: Calculations are perfomed before rounding to avoid round-off errors in calculated results IShealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'l www.shealylab.com
Page: 30 of 34
Lovel 1 Report v2.1
I
I MA EPH (aromatics) - LCSD
I
sampte tD: oe26356-003
Analytical Method: MADEP-EPH-O4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810212013 935
I ^trl:tl"r, Resurt % Rec % RPDr Parameter (ms/ks) (ms/ks) O Dit % Rec % RPD Limit Limit Analysis Date
85 45 1 52 16 40-140 25 08/03/2013 0940
AcceDtanceO % Rec LihittC11 - C22 Aromatics
Surrogate
2-Bromonaphthalene (fractionation 2) 72 40-140
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PQL = Praclical quantitation limit P = Th6 RPD botwsen two GC columns oxceeds 400/6 N = Recovery is out of criteria
ND = Notdet€ctod atorabovethe F{lL J = Estimated rsult< PQL and > MDL + = RPD is outof criteria
Whors applicablo, all soil samplo analysis ar€ reported on a dry woight basis unloss flagged with a "VV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 [phone] Fax [phone] www.shealylab.com
Page:31 of34
Lerol 1 R@ort v2.1
I
MA EPH (aliphatics) - MB
Sample lD: OQ26358-001
Batch:26358
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-o4
Prep Date: 08/02/2013 935
Parameter Dito Analysis Date
C19 - C36 Aliphatics
Cg - C18 Aliphatics
Surrogate
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mg/kg
mg/kg
10
10
ND
ND
o
1
1
AcceptanceLimft
08/02/2013 1808
08/02/2013 1808
% Rec
1 -Chloro-octadecane (aliphatic)40-140
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t
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PQL = Practical quantitation limit
ND = Not dstec-tod at or above lhe POL
P = Thg RPD belwoen two GC columns excoeds 40% N = Rscovsry is out of critsria
J = Estimated result < PQL and : MDL + = RPD is out d cribria
I
I
IWhere applicable, all soil sample analysis aro reported on a dry weight basis unless flaggsd with a "l/lf,
Note: Calculations are performed before roundlng to avoid round-off errors in calculated results
Shealy Envircnmental Services, lnc.
106 Vantage Point Drive W€st Columbia, SC 29172 [phone] Fax [phone]'111 www.shealylab.com
Page: 32 of 3tt
Levsl I Roportv2.'l
I
I MA EPH (aliphatics) - LCS
I Sample lD: 0026358-002
I Barcn:26356
Analytical Method: MADEP-EPH-o4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 08102120'13 935
I ^t#in, Resurt % Recr Parameter (ms/ks) (mq/ks) O Dit % Rec Limit Analysis Date
40 3530 15
AcceptanceO % Rec LihitI :;:"::'ix#::'87 40-140 08t02t2013'.t837
51 40-140 0810212013',t837
I
1-Chloro-octadecane (aliphatic) 79 40-140
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PCIL = Practical quantitation limit P = Tho RPD botwoen two GC columns 6xce6ds 40% N = Rscovory is out of criteria
ND = Notdetoctod atorabovetho PCIL J = Estimated result< PQL and: MDL + = RPD is @t of criteria
Where applicable, all soil samplo analysis aro reported on a dry wsight basis unloss flagged with a "W"
Note: Calculatlons are performed before rounding to avoid round-off errors in calculated results
Shealy Environm€ntal Services, lnc.
106 Vantage Point Drive West Columbla, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 33 of 34
Lewl I Roportv2.l
MA EPH (aliphatics) - LGSD
Sample lD: OQ26358-003
Batch:26358
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: O8lO2l2O13 935
I
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Parameter
Spike
Amount
(mg/kg)
Result(msrks) O
% Rec % RPDDil % Rec % RPD Limit Limit Analysis Date
C19 - C36 Aliphatics
Cg - C18 Aliphatics
Surrogate
32
13
40
30
o
181
142
7.1 40-140 25 08102t2013',t907
19 40-140 25 08102120131907
7o Rec AcceptanceLimit
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1 -Chloro-octadecane (aliphatic)40-140
PQL = Practical quantitation limit
ND = Not dotected at or abov6 the PQL
P = The RPD betwo€n two GC @lumns oxceeds 40% N = Recovery is out of critgria
J = Estimated rosult < PQL and: MDL + = RPO is out of crltoria
I
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IWh6re spplicable, all soil sample analysis are rsportsd on a dry w€ight basis unlass flagg6d with a "VV"
Note: Calculations are performed before rounding to ayoid round-off errors in calculated results
Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]'11 www.shealylab.com
Page: 34 of 34
Lovsl 1 Rgportv2.l
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t€Yel 1 R.port Y2.1
ISHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com ILevel I Roport v2.'l
SHEALY ENVIRONMENTAL SERVICES, INC.I
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Report of Analysis
Terracon Consultants, lnc.
3534 Rutherford Road
Taylors, SC 29687
Attention: George Flores
Project Name:lRC
Project Number:861 27 103
Lot Number:OH09037
Date Completed :08/1 3/201 3
s_*fu*
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, lnc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checkllst,
aoaooaoaa
Shealy Environmental Seruices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page:1 of12
Lovol 1 Rsportv2.l
SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No:32010
I
I
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NC DENR No: 329NELAC No: E87653
Case Narrative
Terracon Consultants, lnc.
Lot Number: OH09037
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, lnc. ("Shealy") Quality Assurance Management Plan (OAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
lfyou have any questions regarding this report please contactthe Shealy Project Manager listed on the cover page.
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Shealy Environmental Services, lnc.
106 Vantage Point Driv6 West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Pagez 2 ol 12
Level 'l Roport v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, lnc.
Lot Number: OH09037
Sample Number Sample lD Matrix Date Sampled Date Received
001 Ho-B-2 Solid 08/08/2013 1835 08/09/2013
(1 sample)
Shealy Environmental Services, lnc. Page: 3 of 12
106 Vantage Point Drive West Columbia, SC 29172 (S03) 791-9700 Fax [phone] www.shealylab.com Lowl 1 Rgportv2'1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Terracon Consultants, lnc.
Lot Number: OH09037
Sample Sample lD Matrix Parameter Result O Units
(0 detections)
Shealy Environmontal Sewices, lnc.
106VantagePointOrive WestColumbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page:4 ol 12
Level I Roport v2.l
t
I
Client:Terracon Consultants, lnc. Laboratory lD: OH09037-001
Description: HO-B-2 Matrix: Solid
Date Sampled:08/08/2013 1835 % Solids: 81.4 08112120132137
Date Received: 08/09/2013
MA EPH (aliphatics)
f Run Prep Method Analytical Method Dilution Analysis Date Anatyst Prep Date Batch
r 1 MADEP-EPH- MADEP-EPH-oA 1 08t12t20131134 AMy 08/09/20't3 2145 26923
CAS AnalyticalParameter Number Method Result O PQL Units RunI
I
Cg - C18 Aliphatics
C19 - C36 Aliphatics
Surrogate
MADEP-EPH.O ND
MADEP-EPH.O ND
Run 1 AcceptanceO % Recovery Limits
12 mg/kg 1
12 mg/kg 1
l-Chloro-octadecane (aliphatic) 68 40-140
I MA EPH (aromatics)
Run Prep illethod Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-0 1 08t12t2013 1401 AMy O8t09l20',l3 2145 26924I
I
CAS AnalyticalParameter Number Marhar{ Result O PQL Unlt6 Run
C1'l -C22Aromatics
Surrogate
MADEP.EPH.O ND
Run I AcceptanceO % Recovery Limits
12 mg/kg 1
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2-Bromonaphthalene (fractionation 2) 74 40-140
2-Fluorobiphenyl (fractionation 1) 77 4O-14O
o - Terphenyl (aromatic) 61 40-140
I PQL = Pracucal quantitation limit B = Detsted in tho mothod blank E = Quantitation of compound oxceded ths calibration rango H = Outof holdingtime
ND=Notdetectedatorabov6thePQL J=Estimatodrosult<PCILand:MDL P:TheRPDbetweenlwoGCcolumnsexceeds40To N=Rocovoryisoutofcrilorie
Wher6 applicablo, all soil sample analysis are reported on a dry w€ight basis unless flaggsd with a 'W"
Shealy Environm€ntal Servic€s, lnc.
I
106 Vantase Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 5 of 12
L3vel 1 Roportv2.l
I
QC Summary
Shealy Environmental SeNices, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 6 of 12
LEvsl 'l Report v2.1
I MA EPH (aliphatics) - MB
I Sample lD: oe26923-oo1
I Batcn:26923
Analytical Method: MADEP-EPH-O4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810912013 2145
t Parameter Result O Dit PQL Units Analysis Date
I :;:"T'^txffi::"10
10
mg/kg 0811212013 1006
mg/kg 0811212013 1006ND1
AcceptanceO % Rec Lihit
I
'l-Chloro-octadecane (aliphatic) 72 40-140
t
T
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t
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T
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PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 407o N = Racovery is out of criteria
ND = Nol dst€cl€d ator abovetho PQL J = Estimated r6sult< PQLand: MDL + = RPD is outofcritoria
Whsre applicabls, all soil sample analysis ar6 roported on a dry waight basis unloss flagged with a n1/'
Note: Calculations are performed before rounding to avoid round-off errors In calculated results
Shealy Environmental Seruices, lnc. Prge : 7 of 12
lOGVantagePointDrivg WestColumbia, SC 29172 (S03)791-9700 Fax[phone]'l www.shealylab.com Lovel lRs9ortv2'1
IMA EPH (aliphatics) - LCS
Sample ]D: OQ26923-002
Batch:26923
Analytica! Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810912013 2145
I
Spike
Amount(mg/ks)
Result
(mg/ks)
% Rec
Dil % Rec Limit Analysis Date IParameter
C19 - C36 Aliphatics
Cg - C18 Aliphatics
Surrogate
I40
30
o
31
't7
AcceptanceLimit
1
1
77
55
40-140
40-140
o8112t2013 1035
0811212013 1035
% Rec
I
t
I
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I
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t
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1 -Chloro-octadecane (aliphatic)40-140
POL = Practicalquantitation limit
ND = Not detectod at or abovs ths PQL
P = The RPD bgtw€sn two GC columns exceeds 40% N = Racovery ls out ofcritsria
J = Estimatod result < PQL and : MDL + = RPD is out of critoria t
IWhore applicable, all soil samplo analysis are rsported on a dry w€ight basis unless flagged with a "W"
Note: Calculations are parformed before rounding to avoid round-off erlors in calculated results
Shealy Environmental Services, lnc,
106 Vantag€ Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 8 of t2
Lavol 1 R€port v2.l
I
t MA EPH (aliphatics) - LCSD
t
t.'l':,:i,oo26e23-oo3
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 08109120'13 2145
I ^tnl:n, Resurt % Rec % RPD! Parameter (ms/ks) (ms/ks) A Dit % Rec % RPD Limit Limit Analysis Date
C19 - C36 AliphaticsI ll;""J"',1"""''"'
40 29
30 15
AcceptanceO % Rec Lihit
1 73 4.9 40-140 25 08112120131105
1 52 6.6 40-140 25 08112120131105
I
l-Chloro-octadecane (aliphatic) 71 4o-14o
I
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t
t
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PQL = Ractical quanlitation limit P = Tho RPD betwe€n two GC columns oxceods 40% N = Recovery is out of critsria
ND = Not detected at or above the PCIL J = Estimatod result < PQL and: MDL + = RPD is out of criteria
wh6re applicable, all soil Bample analysis are reported on a dry w€ight basis unl€ss flagged with a nV"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmentral Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: I of 12
Lsvel 'l R6port v2.l
I
MA EPH (aromatics) - MB
Sample lD: OQ26924-001
Batch:26924
Analytical Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810912013 2145
T
I
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I
Parameter o Analysis Date
C11 -C22 Aromatics
Surrogate
10ND
a
1
AcceptanceLimit
mg/kg 08112120131233
% Rec
2-Bromonaphthalene (factionation 2)
2-Fluorobiphenyl (fractionation 1 )
o - Terphenyl (aromatic)
81
83
71
40-140
40-140
40-140 I
t
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I
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IPQL = ftactical quanlitation limit
ND = Not deiectod at or above lhe PQL
P = The RPD b6tween two GC columns exceeds 40% N = Rocovory is out of criteria
J = Estimated r€sult < PQL and : MDL + = RPD is out of criteria
wher6 applicablo, all soil sample analysis are reported on a dry weight ba6is unless flaggsd with a "W"
Note: Calculations are performed before rounding to avoid round-off errors In calculated results IShealy Envircnmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29'172 (803) 7S1-9700 Fax [phone] www.shealylab.com
Page: 10 of 12
Lgvel 1 Reportv2.l
I
I MA EPH (aromatics) - LCS
I
t'-l':,:'.,7}%e24-oo2
Analytical Method: MADEP-EPH-O4
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 08109120'13 2145
t ^t#:l"", Resurt % Recr Parameter (mq/kq) (mq/kg) O Oit % Rec Limit Analysis Date
C11 - C22 Aromatics
Surrogate
85 46
AcceptanceO % Rec Lihit
55 40-',140 0811212013 1302I
2-Bromonaphthalene (ftactionation 2) 74 40-140
I :l#,"il:liL:lilna'[on
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PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Rscovery is out of critsria
ND = Notdetectod atorabovgthe PQL J = Estimated.esult< PQL and: MDL + = RPD is out ofcriteria
Whoro applicable, all soil sampl€ analysls are ropoded on a dry weight basis unl€ss llagged with a .W'
Note: Calculations are performed before roundlng to avoid round-off errors in calculated results
Shealy Environmental Services, lnc.
l06VantagePointDrive WestColumbia, SC 29172 [phone] Fax[phone] www.shealylab.com
Page:11 ol 12
L€vel 1 Roport v2.l
TMA EPH (aromatics) - LCSD
Sample lD: Oe26924-003
Batch:26924
Analytica! Method: MADEP-EPH-04
Matrix: Solid
Prep Method: MADEP-EPH-04
Prep Date: 0810912013 2145
I
SpikeAmount Result % Rec % RPD(mg/kg) (mg/kg) O Dit % Rec % RPD Limit Limit Analysis Date IParameter
C11 - C22 Aromatics
Surrogate I85
a
8.1 40-140 25 08t12t20131332
% Rec Acceptance
Limat
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (fractionation 1 )
o - Terphenyl (aromatic)
74
86
66
40-'.t40
40-140
40-140 t
T
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PQL = Practical quantitaiion limii
ND = Not dotectod at or above the PQL
P = The RPO betw66n two GC columns oxceeds 40% N = Recovsry is out of criteria
J = Estimated r€sult < PQL and : MDL + = RPD is out of crilarla t
t
Where applicable, all soil samplo analysls ar3 reportod on a dry w€ight basis unloss flagged with a 1Ir
Note: Calculatlons are porformed before rounding to avoid round-off errors In calculated results
Shealy Environmental Services, lnc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: l2 of 12
Lovel'l Rsportv2.l
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