13008_Pilot Mountain_PII ESA_20170410

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7011 Albert Pick Road, Suite G | Greensboro, NC 27409
t: 336.605.3009 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington

April 10, 2017

NCDEQ-DWM
Brownfields Program
610 E. Center Avenue, Suite 301
Mooresville, NC 28115

Attn: Ms. Jordan Thompson
Brownfields Project Manager

RE: Phase II Environmental Site Assessment
Former Amos & Smith Hosiery Mill Site
±8.15-Acre Site
612 East Main Street
Pilot Mountain, Surry County, North Carolina
WR Project No. 02090017.2

Ms. Thompson:

WithersRavenel (WR) is pleased to submit this report documenting Phase II Environmental Site Assessment
(ESA) activities for the above-referenced property. Assessment activities were conducted in accordance with
our Work Plan for Site Assessment of Potential Brownfields Property (Work Plan) submitted to the NCDEQ
Brownfields Program, and approved on November 10, 2016. The purpose of the assessment was to evaluate
soil and groundwater conditions relative to historic onsite property uses and findings of a Phase I ESA
conducted by WR on January 22 and 23, 2009. This report summarizes the results of WR's field activities and
presents the findings of the assessment relative to existing environmental or potential conditions at the site.

Sincerely,
WithersRavenel

Jackson S. Cates
Environmental Scientist – Environmental Professional

Mark Brown, LG, PG, RSM
Project Manager – Environmental Professional

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TABLE OF CONTENTS

1. Purpose............................................................................................................................... 1
2. Background ........................................................................................................................ 1
3. Field Activities ................................................................................................................... 4
4. Laboratory Analytical Results ......................................................................................... 6
5. findings ............................................................................................................................... 9

FIGURES
Figure 1 General Location Map
Figure 2 Site Map
Figure 3 Groundwater Assessment Results Map
Figure 4 Soil Assessment Results Map
Figure 5 Groundwater MTBE Isoconcentration Map
Figure 6 Receptor Map
Figure 7 Zoning Map (Town of Pilot Mountain)
Figure 8 Utilities Map
TABLES
Table 1A Summary of Soil Analytical Results – VOCs
Table 1B Summary of Soil Analytical Results – 8260 TICs
Table 1C Summary of Soil Analytical Results – SVOCs
Table 1D Summary of Soil Analytical Results – 8270 TICs
Table 1E Summary of Soil Analytical Results – HSL Metals/Chromium
Table 2 Summary of Groundwater Analytical Results – VOCs plus TICs, SVOCs plus TICs, HSL
Metals/Chromium
Table 3 Monitoring Well Construction Information
APPENDICES
Appendix A Boring Logs
Appendix B Well Construction Records
Appendix C Brownfields Receptor Survey Form
Appendix D Laboratory Report and Chain of Custody
Appendix E Photo Essay
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Phase II Environmental Site Assessment WithersRavenel Project #02090017.2
Former Amos & Smith Hosiery Mill Site April 2017
Page 1 of 9
1. PURPOSE
WR has performed a Phase II Environmental Site Assessment (ESA) on the Former Amos & Smith Hosiery Mill
site, a ±8.15-acre site located approximately 1,000 feet west of the intersection between East Main Street
and Old US Highway 52 Bypass in Pilot Mountain, Surry County, North Carolina (Figure 1, General Location
Map). According to the Surry County GIS records, the subject property consists of the following parcels:
Tract # Parcel # Current Owner Address Acreage
Tract 1 2044 Town of Pilot Mountain 612 Main Street ±7.27
Tract 2 2285 Otay LLC 616 Main Street ±0.88

The Phase II ESA was conducted to investigate Areas of Concern (AOCs) identified in the Phase I ESA
prepared for the property by WR on January 22 and 23, 2009. Based on the AOCs identified in the Phase I
ESA, subsurface investigation activities were performed around various portions of the site in which
environmental concerns were identified and in the building currently occupied by Otay LLC/Sports Solutions
is use as a textile manufacturing facility on the property.
The intent of the Phase II ESA was to provide a baseline soil and groundwater assessment to document the
current conditions on the site and document the presence or absence of potential contaminants arising from
the former operations conducted of the site. The Phase II ESA was performed to identify potential impacts to
soil and groundwater in specified areas and does not represent a comprehensive investigation to define the
degree and extent of contaminant migration from a known contaminant source, unless otherwise
documented. If conditions at the site change or additional information become available that would
materially affect the nature of this report, we request that we be contacted so that any change in conditions
can be properly reviewed and our report amended accordingly.
2. BACKGROUND
As indicated above, WR previously conducted a Phase I ESA for the subject site in February 2009. Following
completion of the Phase I ESA and after reviewing readily-available site information, including investigation
reports prepared by other consultants, WR concluded that additional assessment should be considered due
to possible contamination from either the initial hosiery mill operations that were not investigated during the
initial environmental study or the continued operation of the mill as a sock manufacturing facility subsequent
to the initial environmental study.

WR understands that an application for a Brownfields Agreement was submitted to the North Carolina
Department of Environment and Natural Resources (NCDENR) in June 2009 and was found eligible for entry.
In September 2009, Ms. Sharon Eckard with the NCDENR Brownfields Program sent the Town of Pilot
Mountain an “Additional Assessment Requirements” letter declaring which assessment activities should be
performed to determine how the site can be made safe for its intended use.

In December 2011, the NCDENR issued a letter that changed the status of the site from “inactive eligible” to
“No Further Interest” due to inactivity on the project.

In late 2013, Mr. Homer Dearmin, former Town Manager of Pilot Mountain, asked WR to prepare an updated
Brownfields Agreement eligibility application. The application was submitted and received in March 2014.
Mr. Dearmin, Ms. Eckard, and WR representatives participated in a conference call regarding development
of a scope of work for completing assessment activities of the property per the 2009 letter issued by Ms.
Eckard. WR understands that the Town did not pursue the assessment at that time due to anticipated costs.
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Phase II Environmental Site Assessment WithersRavenel Project #02090017.2
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It should be noted that in September 2015, NCDENR began doing business as the North Carolina Department of
Environmental Quality (NCDEQ).

On May 12, 2016, WR and representatives of the Brownfields Program, including Ms. Sharon Eckard, Mr.
Bruce Nicholson, and Ms. Joselyn Harriger, conducted a conference call to discuss the current status of the
site and the additional information needed to allow this site into the Brownfields Program. Program
representatives indicated that they wanted an evaluation of the soil, groundwater, and soil vapor in various
areas of the site. Particular areas mentioned included the areas near the current Otay, LLC/Sports Solutions
property, the former dye and wet processing areas, the former boiler room, and the existing boiler room
building. There were also discussions regarding the establishment of appropriate detection limits for target
compounds based on their “2L Standards” as defined by NCAC Title 15A, Subchapter 2L, Section .0202
(Water Quality Standards for Class GA Groundwater).

On November 1, 2016, WR submitted a Work Plan for Site Assessment of Potential Brownfields Property (Work
Plan) to the Brownfields Program, which was approved on November 10, 2016. WR began implementation
of the Work Plan on January 18, 2017. Based on conditions observed in the dry room during site assessment
activities, a Work Plan Amendment - Site Assessment of the former Amos & Smith Hosiery Mill Site was submitted
to the Brownfields Program on February 8, 2017, and approved on February 9, 2017. Below is a description
of the site assessment activities performed, the analytical results reported, and conclusions reached.
2.1. SITE CONDITIONS/USE
2.1.1. Current Area - Otay, LLC/Sports Solutions
WR has completed a recent site visit and has summarized the current processes of the present Otay,
LLC/Sports Solutions area. Sports Solutions is a textile manufacturing facility. They complete sock
manufacturing and finishing, headband and wristband manufacturing and finishing, several imprinting
applications, and screen printing. After review of the operations and facility construction, it is our opinion
that this facility does not use or produce significant volumes of chemical waste that would create any
additional subsurface contaminants.

According to Mr. Josh East, who is the Director of Operations, Sports Solutions does not dye currently nor
have they completed any dyeing operations at any time since they have occupied the building. Their “wet
processing” is actually a sock washing area used to scour, soften, and whiten socks. There was a new 6” line
installed for their waste water to go directly into the city sewer. Mr. East stated that they are not equipped
to complete dyeing at the facility as you need water heated to a certain temperature to complete the dyeing
operations. He stated that they would have to invest several thousands of dollars to acquire the equipment
in order to complete this work. The facility contains a Doming /Print Room, Finishing/Screen Printing area,
and a sock washing area (Please refer to Figure 2, Site Map for the location of structures and material).

Mr. East provided a full chemical list and comprehensive chemical use and process explanation of the onsite
operations, which were included in Appendix A of the November 2016 Work Plan. The corresponding Safety
Data Sheets (SDS) were provided in Appendix B.
2.1.2. Potential Areas of Concern
Based on review of the Phase I ESA prepared in January 2009, readily-available files, environmental
databases, representative interviews, and recent site observations, WR identified the following potential
Areas of Concerns (AOCs). (Please refer to Figure 2 for the location of structures and material.)

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Phase II Environmental Site Assessment WithersRavenel Project #02090017.2
Former Amos & Smith Hosiery Mill Site April 2017
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Chemical Storage & Air Filtration System
• Chemicals associated with dyeing operations have been used and stored on the subject property.
Signs and placards were noted on the detached boiler room and vacant warehouse exterior walls.
• An air/water filtration system to remove lint from the air was located inside the warehouse with at
least three floor drains and a possible trench.
Former Shop Areas
Two former shop areas were noted on a former site plan sketch of the building acquired during the Phase
I ESA in 2009.
Maintenance/Repair Area
The basement had been used as a maintenance and repair area for hosiery machinery.
Multiple Trench Drains and Floor Drains
Two large trench drains filled with concrete were noted in the central western portion of the site during
the Phase I ESA. Several floor drains were also noted in the building.
Boiler Rooms
The hosiery operation utilized two boiler rooms, one located within the building and another in the
detached boiler room structure, which would have utilized petroleum fuels. WR observed a large
containment basin adjacent to the detached boiler room structure. According to Mr. Harris, the former
subject property owner, a 7,500- to 10,000-gallon petroleum aboveground storage tank (AST) had been
located in this area. Obvious staining was observed near the piping inside the boiler room building.
Potential contamination associated with fueling overfills and possible leaks were investigated in these
areas during assessment activities.
Former Dye House
The Dye House formerly contained trench-style floor drains that ran along the eastern sides of the room
and discharged via piping into the sanitary sewer, after running through a lint filter. The floor drains have
been filled in with concrete by the former owner, Carolina Caro Associates, LLC. Potential contamination
associated with possible pipe leaks and the storage of chemicals in this area were investigated during
assessment activities.
Residential Heating Oil ASTs
WR observed two 250-gallon ASTs adjacent to the eastern-most residential structure. Staining and
odors typical of petroleum products were observed on the oil filter and the ground surface below the
filter. Additional petroleum staining was observed on the ground surface in close proximity to the ASTs.
Existing Groundwater Monitoring Wells
A groundwater monitoring well is located on the northern portion of the site. A second well was
discovered east of the detached boiler room, near the containment wall of the former AST. No indication
of the origin of the wells was revealed through the EDR report. It appears that three temporary wells
were installed during the UST Closure activities. The third well, located near the southwest corner of the
site, could not be located during Phase I ESA activities.

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3. FIELD ACTIVITIES
WR conducted Phase II ESA assessment activities from January 18 through March 7, 2017. The following
paragraphs describe the results of the investigation.
3.1. SUBSURFACE UTILITY LOCATION
Prior to drilling, WR mobilized to the subject property to locate and mark subsurface utilities in the
assessment areas inside and outside of the site structures. WR also notified the North Carolina One Call
Center (NC811) for the location and marking of subsurface utilities along the subject property right-of-way.
3.2. GROUNDWATER ASSESSMENT – MONITORING WELL INSTALLATIONS,
SAMPLING, AND ABANDONMENT
Between January 18 and 19, 2017, WR personnel oversaw the installation of five temporary groundwater
monitoring wells (TW-2, TW-4, TW-5, TW-6, TW-7) by a State of North Carolina-Certified Well Contractor
(Quantex, Inc.) at locations illustrated on Figure 2. Soil borings were initially advanced at these locations to
depths ranging from approximately 35 to 45 feet below land surface (BLS). Continuous soil sampling was
conducted within each boring to the termination depths to allow for soil characterization, including logging
of recovered materials, and screening of soils with a Photo-ionization detector (PID). Based on PID soil
screening results, select soil samples were transferred into laboratory-supplied containers and submitted to
a State of North Carolina-certified analytical laboratory (ESC Lab Sciences (ECS)) for analysis of the following:
 Volatile Organic Compounds (VOCs) plus Tentatively Identified Compounds (+TICs) by EPA Method
8260B;
 Semi-Volatile Organic Compounds (SVOCs) +TICs by EPA Method 8270D; and
 HSL Metals/Chromium by EPA 6020/7470A, including: antimony, arsenic, beryllium, cadmium, total
chromium, copper, lead, manganese, mercury, nickel, selenium, silver, thallium, and zinc.
After sample collection, each soil boring was converted to a temporary monitoring well. The wells were
constructed using a 15- or 20-foot section of two-inch diameter 0.010-inch machine-slotted Schedule 40 PVC
well screen placed at the base of the borehole, followed by two-inch diameter Schedule 40 PVC riser to bring
the well up to land surface. A sand pack was established around, and up to approximately two feet above, the
screen. A bentonite seal was then spread over the sand pack and hydrated. The remaining annular space was
temporarily left void up to the ground surface until a decision was made to abandon the wells or finish them
as “permanent”. Boring logs are included in Appendix A; well construction records are included in Appendix
B.
In addition to the five monitoring wells installed by WR, two existing monitoring wells were located on the
property. WR personnel returned to the site on January 25, 2017 to collect water samples from the seven
wells. Prior to sample collection, static water levels were measured in each well using an electronic water
level indicator to determine the depth to water and calculate the volume of water to be purged. The seven
monitoring wells were purged of water and fine sediment prior to sampling. The groundwater samples were
collected and submitted to ESC for analysis of the same analytical suite listed above in Section 3.2, plus aniline.
After groundwater sample results presented below in Section 4.2 were discussed with Program
representatives, the temporary wells were properly abandoned by Quantex, Inc.
3.3. SOIL BORINGS – ADVANCEMENTS, FIELD SCREENING, AND SAMPLING
Between January 24 and 25, 2017, WR personnel oversaw the advancement of sixteen shallow soil borings
at eight locations inside the building and eight locations outside facility structures. Boring locations are
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illustrated on Figure 2. Based on conditions observed during soil boring advancement at location B-10 in the
Dry Room, WR personnel oversaw the advancement of one deep (+/- 15 feet) soil boring (B-17) on February
28, 2017. The shallow borings were advanced in areas identified as Recognized Environmental Concerns
(RECs) or Historical Recognized Environmental Concerns (HRECs) in the 2009 Phase I ESA, and subdivided
by location into AOCs as presented above in Section 2.1.2. Borings were advanced in locations shown below:
Area Boring IDs
Former knitting/chemical storage B-7
Former Shop area B-8, B-9, TW-7
Former Hosiery Equipment Repair B-15, TW-6
Trench Drains B-10, B-11, B-17
Former Coal Pile B-12, B-13
Former Boiler Room B-16, TW-5
Former Dye Room
Residential ASTs
Detached Boiler Room and Former AST
Background Samples (up gradient
location)
B-14, TW-4
B-4, B-5, B-6
B-1, B-2, B-3, TW-2
BG-1, BG-2
Continuous soil sampling was conducted within each boring to depths of approximately two feet beneath
surface grade (or below the bottom of the slab-on-grade) to allow for soil characterization, including logging
of materials recovered and screening of soils with a Photo-ionization detector (PID). Based on screening of
samples with the PID, select soil samples were transferred into laboratory-supplied containers and submitted
to ESC for analysis of the same analytical suite listed above in Section 3.2, minus aniline.
Selection of samples for fixed-base laboratory analyses was generally based on the occurrence of volatile
vapors within the samples (e.g., the sample exhibiting the highest PID measurement within any given boring).
If elevated field readings were not observed, the sample was collected at the approximate boring depth in
accordance with the Work Plan. Samples collected from boring locations B-2, B-3, B-4, and B-6 were not
submitted for fixed-based laboratory analyses. Boring logs are included in Appendix A.
3.4. BROWNFIELDS PROPERTY RECEPTOR SURVEY
WR personnel performed a receptor survey on March 7, 2017 to identify any potential receptors in the area.
The receptor survey included a return visit to the Former Amos & Smith Hosiery Mill site and visits to
surrounding properties located within approximately 1,500 feet (search radius) from the property
boundaries. WR also used various online databases (i.e., Surry County GIS, SWAPInfo, and the U.S. Fish and
Wildlife Service National Wetlands Inventory, etc.) as an information source, and inquired with Town of Pilot
Mountain personnel to verify the source of the site’s water supply and any other information relating to
potential receptors surrounding the site.
WR identified the presence of several receptors (e.g., private or public water supplies) within the search
radius investigated, including one private irrigation well and several basements/crawlspaces. WR observed
a private irrigation well and a water meter located at 210 Carson Road.
WR observed 19 structures apparently with basements located within 500 feet of the site; an additional nine
structures with apparent basements were located between 500 feet and 1000 feet from the site. None of the
28 structures were entered during the receptor survey. The structure located on the project site has a
finished basement constructed beneath the western half of the building. The basement is segmented into
three rooms and, although currently unoccupied, two of the rooms are used by Surry Community College for
storage. The third room is occasionally used for private functions, reportedly including auctions.
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A Place to Grow Preschool is located approximately 500 feet west of the property boundary. However, at the
time of our survey, the preschool was found to be vacant and the property listed “For Sale”.
The First Presbyterian Church of Pilot Mountain was determined to be located approximately 1,400 feet west
of the property boundary and appears to have a basement. The church was not entered during the receptor
survey.
The nearest surface water body observed was an un-named surface water body located approximately 1,300
feet southeast of the site.
The Town of Pilot Mountain provides potable water to the entire surrounding area, obtaining their supply
from Toms Creek. While the Town maintains sanitary and storm sewer lines in the area, none of these lines
appear to intersect the area of soil impact on the site. WR was unable to determine whether these utilities
intersect the groundwater level at the location; however, due to the lower depth of groundwater at the site,
these lines are not expected to be a receptor.
WR filled out the Brownfields Property Receptor Survey form, which is presented in Appendix C.
4. LABORATORY ANALYTICAL RESULTS
4.1. SOIL ANALYTICAL RESULTS
As indicated earlier, soil samples were analyzed for VOCs+TICs by EPA Method 8260B, SVOCs+TICs by EPA
Method 8270D, and HSL Metals/Chromium by EPA 6020/7470A. Sample analyses were compared to the
NCDEQ Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) for
Unrestricted Use and Protection of Groundwater.
Volatile Organic Compounds+TICs
Data for soil samples analyzed by EPA Method 8260B+TICs indicated that one or more target compounds
were detected at concentrations above their laboratory minimum detection limits (MDLs) in samples
collected from soil borings BG-1 and BG-2; B-1 through B-17; and TW-2 and TW-5, eventually converted to
temporary monitoring wells. All target compounds were reported in concentrations below their respective
IHSB PSRGs-Unrestricted Use (PSRG-UU) and Protection of Groundwater (PSRG-PGW) standards.
Additionally, no Tentatively Identified Compounds (TICs) were reported above their respective PSRGs
standards.
A summary of the VOCs+TICs analytical results are presented in Table 1A and Table 1B, respectively. A
copy of the laboratory analytical report and chain-of-custody is included in Appendix D. Figure 4 illustrates
the locations of each soil boring and PSRG exceedances identified in each location.
Semi-Volatile Organic Compounds +TICs
Data for soil samples analyzed by EPA Method 8270D+TICs indicated that one or more target compounds
were detected at concentrations above their respective PSRG-UU or PSRG-PGW in several of the soil boring
samples.
 Concentrations of benzo(a)anthracene were detected in exceedance of its PSRG-UU (0.16 milligram
per kilogram (mg/Kg)) in boring B-16, and its PSRG-PGW (0.18 mg/Kg) in borings B-10 and B-14;
 Concentrations of benzo(b)fluoranthene were detected in exceedance of its PSRG-UU (0.16 mg/Kg)
in boring B-16, and its PSRG-PGW (0.6 mg/Kg) in borings B-10 and B-14;
 Concentrations of benzo(k)fluoranthene were detected in exceedance of its PSRG-UU (1.6 mg/Kg) in
boring B-10;
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 Concentrations of benzo(a)pyrene were detected in exceedance of its PSRG-UU (0.016 mg/Kg) in
boring B-1, and its PSRG-PGW (0.059 mg/Kg) in borings B-10, B-14 and B-16;
 Concentrations of dibenz(a,h)anthracene were detected in exceedance of its PSRG-UU (0.016 mg/Kg)
in borings B-14 and B-16, and its PSRG-PGW (0.19 mg/Kg) in boring B-10;
 Concentrations of ideno(1,2,3-cd)pyrene were detected in exceedance of its PSRG-UU (0. 16 mg/Kg)
in boring B-14, and its PSRG-PGW (2.0 mg/Kg) in boring B-10;
 A concentration of naphthalene was detected in exceedance of its PSRG-PGW (0.21 mg/Kg) in boring
B-10;
 A concentration of pentachlorophenol was detected in exceedance of its PSRG-PGW (0.0048 mg/Kg)
in boring B-14; and
 One TIC, benzo(k)fluoranthene, was detected in exceedance of its PSRG-UU (1.6 mg/Kg) in boring B-
10.
A summary of the SVOCs+TICs analytical results are presented in Table 1C and Table 1D. A copy of the
laboratory analytical report and chain-of-custody is included in Appendix D. Figure 4 illustrates the
locations of each soil boring and PSRG exceedances identified in each location
HSL Metals/Chromium
Data for soil samples analyzed by EPA Method 6020/7471A indicated the presence of one or more target
compounds in excess of their respective PSRG-UU or PSRG-PGW in all of the samples submitted for analyses
by EPA Method 6020.
 A concentration of antimony was detected in exceedance of its PSRG-PGW (0.9 mg/Kg) in boring TW-
6;
 Concentrations of arsenic were detected in exceedance of its PSRG-UU (0.68 mg/Kg) in all borings
except for boring B-17;
 Concentrations of manganese were detected in exceedance of its PSRG-PGW (65 mg/Kg) in all
borings; concentrations of manganese were detected in exceedance of its PSRG-UU (360 mg/Kg) in
borings BG-2, B-16, TW-5 and TW-6;
 A concentration of selenium was detected in exceedance of its PSRG-PGW (2.1 mg/Kg) in boring TW-
6;
 Concentrations of thallium were detected in exceedance of its respective PSRG-PGW (0.156 mg/Kg)
in borings B-1, B-9 through B-14, TW-2 and TW-4. Concentrations of thallium were detected in
exceedance of its respective PSRG-UU (0.28 mg/Kg) in borings BG-1 and BG-2, B-7, B-15 and B-16,
TW-5, TW-6, and TW-7.

Background soil samples (BG-1 and BG-2), collected from an upgradient location onsite, contained elevated
levels of arsenic, manganese and thallium in excess of their respective PSRGs. It is possible that the presence,
and/or elevated levels, of these metals may be a result of naturally-occurring concentrations in the area and
not a result of historical activities conducted at the site.
A summary of the metals analytical metals are presented in Table 1E. A copy of the laboratory analytical
report and chain-of-custody is included in Appendix D. Figure 4 illustrates the locations of each soil boring
and PSRG exceedances identified in each location.

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4.2. GROUNDWATER ANALYTICAL RESULTS
Groundwater samples were also analyzed for VOCs+TICs by EPA Method 8260B, SVOCs+TICs+aniline by
EPA Method 8270D, and HSL Metals/Chromium by EPA 6020/7470A. Sample results were compared to
their respective 2L Standards.
VOCs + TICs
Data for groundwater samples analyzed by EPA Method 8260B indicated the presence of one or more target
compounds at concentrations above their laboratory MDLs in samples collected from the temporary
monitoring wells. Only methyl-tert-butyl ether (MTBE), reported in TW-5 at a concentration of 23.8
micrograms per liter (ug/L), was detected in excess of its respective 2L Standard (20 ug/L). Data for water
samples analyzed for VOCs+TICs did not indicate the presence of any target TICs above the laboratory MDLs
in the samples collected.
SVOCs + TICs
Data for groundwater samples analyzed by EPA Method 8270D indicated the presence of one or more target
compounds at concentrations above their laboratory MDLs in samples collected from the temporary
monitoring wells. No compounds, including aniline, were detected in any of the samples in concentrations
above their respective 2L Standards. Data for water samples analyzed for SVOCs+TICs indicated the
presence of butane-2-methyoxy-2-methyl at a concentration of 1.03 ug/L. Butane-2-methyoxy-2-methyl
currently does not have an established 2L Standard.
HSL Metals/Chromium
Data for groundwater samples analyzed by EPA Method 6020/7470A indicated the presence of one or more
target compounds above their respective MDLs. However, only manganese was reported at a concentration
in excess of its respective 2L Standard, and was detected above the 2L Standard in each of the samples (TW-
1 through TW-7).
A summary of the groundwater sample analytical results is presented in Table 2. A copy of the laboratory
analytical report and chain-of-custody is included in Appendix D. Figure 3 illustrates the locations of each
monitoring well and concentrations of target analytes identified above their respective MDLs or 2L Standard
in each location.
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Phase II Environmental Site Assessment WithersRavenel Project #02090017.2
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5. FINDINGS
WithersRavenel has conducted a limited Phase II Environmental Site Assessment at the ±8.15-acre Former
Amos & Smith Hosiery Mill site located approximately 1,000 feet west of the intersection between East Main
Street and Old US Highway 52 Bypass in Pilot Mountain, Surry County, North Carolina. The findings of
assessment activities conducted at the site by WR include the following:
Soil Samples
 When analyzed by EPA Method 8260B, no VOCs were reported in concentrations above their
respective PSRGs. Additionally, no TICs were reported above their respective PSRGs.

 When analyzed by EPA Method 8270D, the following SVOCs exceeded one or more of their
respective PSRGs:
o Benzo(a)anthracene;
o Benzo(b)fluoranthene,
o Benzo(k)fluoranthene,
o Benzo(a)pyrene,
o Dibenz(a,h)anthracene;
o Ideno(1,2,3-cd)pyrene;
o Naphthalene;
o Pentachlorophenol; and
o One TIC, Benzo(k)fluoranthene.

 When analyzed by EPA Method 6020/7470A, the following HSL metals exceeded one or more of
their respective PSRGs:
o Antimony;
o Arsenic
o Manganese
o Selenium; and
o Thallium.
Groundwater Samples
 MTBE, reported at a concentration of 23.8 µg/L in the sample collected from TW-5, was the only VOC
or SVOC to exceed its respective 2L Standard (20 µg/L); and
 Manganese was the only target metal to exceed its respective 2l Standard. Concentrations of
manganese were reported in excess of its 2L Standard (50 µg/L) in each of the groundwater samples
analyzed, including the sample collected from the background well (TW-1).
Receptor Survey
 There are several sensitive receptors located within the search radius, including an on-site basement,
and several basements and other receptors located within 1,000 feet of the property boundaries; and
 There is one irrigation well located within 1,500 feet of the northern property boundary.
The findings of this assessment suggest that historical industrial operations on the property have created
areas of impacted soil and groundwater at concentrations above regulatory levels prescribed by the NCDEQ.
Given the historical industrial use of the property as a hosiery mill, the identification of these impacts is not
considered unusual. However, during implementation of this Phase II ESA, WR did not identify sources or
locations of soil or groundwater contamination that could be reasonably attributable to recent operations or
activities conducted by the current occupants.

Figures

Tables
Page 1 of 5
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Up Gradient Location on Site BG-1 0.5-2 1/24/2017 0.0172 J <0.000371 <0.000315 <0.00047 <0.000334 <0.00028 <0.00643 <0.000379 <0.000597 <0.000421 <0.000533 <0.000384 <0.000525 <0.00029
Up Gradient Location on Site BG-2 0.5-2 1/24/2017 0.0261 J <0.000372 <0.000315 <0.000471 <0.000335 <0.000281 <0.00645 <0.00038 <0.000598 <0.000422 <0.000534 <0.000384 <0.000526 <0.000291
Detached Boiler Room Building and
Former AST B-1 0.5-2 1/24/2017 0.0264 J <0.000366 <0.000311 <0.000464 <0.00033 <0.000277 <0.00635 <0.000375 <0.000589 <0.000415 <0.000527 <0.000379 <0.000518 <0.000286
Residential AST's B-5 0.5-2 1/24/2017 <0.0123 <0.000332 <0.000282 <0.000421 <0.000299 <0.000251 <0.00576 <0.00034 <0.000534 <0.000377 <0.000477 <0.000343 <0.00047 <0.00026
Former Knitting & Storage/concrete
basin/air filter system/Chemical Storage B-7 0.5-2 1/24/2017 <0.0151 <0.000408 <0.000346 <0.000517 <0.000367 <0.000309 <0.00708 <0.000417 <0.000656 <0.000463 <0.000587 <0.000421 <0.000577 <0.000319
Former Shop Areas B-8 0.5-2 1/24/2017 <0.0133 <0.000358 <0.000304 <0.000454 <0.000322 <0.000271 <0.00621 <0.000366 <0.000576 <0.000406 <0.000515 <0.00037 <0.000507 <0.00028
Former Shop Areas B-9 0.5-2 1/24/2017 0.0138 J 0.000571 J <0.000271 <0.000405 <0.000288 <0.000242 <0.00556 <0.000328 <0.000515 <0.000363 <0.000461 <0.000331 <0.000453 <0.00025
Multiple Trench Drains filled with
Concrete B-10 0.5-2 1/25/2017 0.0263 J <0.000323 <0.000274 <0.000409 <0.000291 <0.000244 <0.0056 0.000409 J <0.00052 <0.000366 <0.000464 <0.000334 <0.000457 <0.000253
Multiple Trench Drains filled with
Concrete B-11 0.5-2 1/25/2017 0.0317 J <0.000343 <0.000291 <0.000435 <0.000309 <0.000259 <0.00595 <0.000351 <0.000552 <0.000389 <0.000493 <0.000355 <0.000486 <0.000268
Former Coal Pile B-12 0.5-2 1/24/2017 0.0161 J <0.000344 <0.000291 <0.000435 <0.000309 <0.00026 <0.00596 <0.000351 <0.000552 <0.00039 <0.000494 <0.000355 <0.000486 <0.000269
Former Coal Pile B-13 0.5-2 1/24/2017 0.0152 J <0.000346 <0.000294 <0.000438 <0.000312 <0.000262 <0.006 <0.000354 <0.000556 <0.000392 <0.000497 <0.000358 <0.00049 <0.00027
Former Dye Room B-14 0.5-2 1/25/2017 0.045 J 0.000402 J <0.00029 <0.000434 <0.000308 <0.000259 0.00767 J <0.00035 <0.00055 <0.000388 <0.000492 <0.000354 <0.000484 <0.000268
Former Hosiery Equipment
Repair/Basement B-15 0.5-2 1/25/2017 <0.0141 <0.00038 <0.000322 <0.000481 <0.000342 <0.000287 <0.00659 <0.000388 <0.00061 <0.00043 <0.000546 <0.000392 <0.000538 0.00127 J
Former Boiler Room B-16 0.5-2 1/25/2017 0.0154 J <0.000356 0.000401 J <0.00045 <0.00032 <0.000269 <0.00617 <0.000363 <0.000572 <0.000403 <0.000512 <0.000367 <0.000503 <0.000278
Multiple Trench Drains filled with
Concrete B-17 14-15 2/28/2017 0.0697 <0.000364 <0.000309 <0.000461 J4 <0.000328 <0.000275 0.0488 <0.000372 <0.000586 <0.000413 J4 <0.000524 J4 <0.000376 <0.000515 <0.000285
Former Boiler Room DUP 0.5-2 1/25/2017 <0.0158 <0.000428 0.000658 J <0.000542 <0.000385 <0.000323 <0.00742 <0.000437 <0.000688 <0.000485 <0.000615 <0.000442 <0.000605 <0.000334
Detached Boiler Room Building and
Former AST TW-2 0.5-2 1/25/2017 0.066 J <0.000398 <0.000338 <0.000505 <0.000359 0.00184 0.011 J <0.000407 0.00158 J <0.000452 <0.000573 <0.000412 <0.000564 J3 J4 <0.000311
Former Dye Room TW-4 0.5-2 1/25/2017 0.0284 J <0.000354 <0.0003 <0.000449 <0.000319 <0.000268 <0.00614 <0.000362 <0.000569 <0.000401 <0.000509 <0.000366 <0.000501 J3 J4 <0.000277
Former Boiler Room TW-5 0.5-2 1/25/2017 0.0858 <0.000333 <0.000282 <0.000421 <0.000299 <0.000251 0.0141 <0.00034 <0.000535 <0.000377 <0.000478 <0.000344 <0.000471 J3 J4 <0.00026
Former Hosiery Equipment
Repair/Basement TW-6 0.5-2 1/25/2017 0.0498 J <0.000392 <0.000333 <0.000497 <0.000353 <0.000296 0.00842 J <0.000401 <0.00063 <0.000444 <0.000564 <0.000405 <0.000555 J3 J4 <0.000306
Former Shop Areas TW-7 0.5-2 1/25/2017 <0.0124 <0.000335 <0.000284 <0.000424 <0.000301 <0.000253 <0.0058 <0.000342 <0.000538 <0.00038 <0.000481 <0.000346 <0.000474 J3 J4 <0.000262
Notes:
1)
2)
3)
4)
J The identification of the analyte is acceptable; the reported value is an estimate.
Result = Result Exceeds Minimum Detection Limits J3 The associated batch QC was outside the established quality control range for precision.
Result = Result Exceeds IHSB PSRG Unrestricted Use Concentration
Result = Result Exceeds IHSB PSRG Soil-to-Groundwater
J4 The associated batch QC was outside the established quality control range for accuracy.
O1 The analyte failed the method required serial dilution test and/or subsequent post-spike criteria.
These Failures indicated matrix interference.
12,200
23
1.2
0.0073
0.32
0.34
1.2
0.0087
5,400
16
NL
0.68
268
1.3
16.2
0.005
11.6
2.2
12.6
NL5.5
818 11.6
6.7
1,230
71-43-2
24
0.82
0.018
8260B - Volatile Organic Compounds8260B - Volatile Organic Compounds
67-66-3 98-82-887-68-3 78-93-399-87-6 108-88-3127-18-4 75-69-479-01-6120-82-187-61-6
TABLE 1A
612 EAST MAIN STREET
Analytical Method
Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
Sample
Depth
(Feet BLS)
Date
Collected
All results provided in mg/kg (milligrams per kilogram) or parts per million.
PILOT MOUNTAIN, SURRY COUNTY, NORTH CAROLINA
Pilot Mountain Brownfields
IHSB PSRGs - Unrestricted Use
IHSB PSRGs - Soil-to-Groundwater
JO
SUMMARY OF SOIL ANALYTICAL RESULTS
Area Sample
ID
WR Project # 02090017.2
71-43-267-64-1
J0 Analyte exceeds %D or % Rec for Continuing Calibration per 8260C or 8270D method specific criteria. The identification of the analyte is
acceptable; the reported value is an estimate.
Qualifiers
IHSB PSRGs = Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (March 2015)
95-63-6
Page 2 of 5
Area Sample
ID
Sample
Depth
(Feet
BLS)
Date
Collected Tentatively Identified Compounds (TICs)Estimated
Concentrations
(mg/kg)
Qualifiers CAS
IHSB PSRGs -
Unrestricted
Use
IHSB PSRGs -
Industrial
IHSB PSRGs -
Soil-to-
Groundwater
Silanol, Trimethyl-0.015 J 001066-40-6 NL NA NL
Cyclotetrasiloxane, octamethyl-0.013 J 000556-67-2 NL NL NL
Silanol, Trimethyl-0.008 J 001066-40-6 NL NL NL
Cyclotetrasiloxane, octamethyl-0.017 J 000556-67-2 NL NL NL
Cyclotrisiloxane, hexamethyl-0.012 J 000541-05-9 NL NL NL
Cyclotetrasiloxane, octamethyl-0.005 J 000556-67-2 NL NL NL
Cyclotrisiloxane, hexamethyl-0.009 J 000541-05-9 NL NL NL
Cyclotrisiloxane, hexamethyl-0.010 J 000541-05-9 NL NL NL
Cyclotetrasiloxane, octamethyl-0.006 J 000556-67-2 NL NL NL
Cyclopentane 0.017 J 000287-92-3 NL NL NL
Cyclotetrasiloxane, octamethyl-0.007 J 000556-67-2 NL NL NL
Cyclopentane 0.019 J 000287-92-3 NL NL NL
Former Shop Areas B-8 0.5-2 1/24/2017 Cyclotetrasiloxane, octamethyl-0.006 J 000556-67-2 NL NL NL
Cyclotetrasiloxane, octamethyl-0.007 J 000556-67-2 NL NL NL
1-Propene, 2-methyl-0.034 J 000115-11-7 NL NL NL
Cyclotrisiloxane, hexamethyl-0.013 J 000541-05-9 NL NL NL
Multiple Trench Drains filled
with Concrete B-10 0.5-2 1/25/2017 NA NA NA NA
Multiple Trench Drains filled
with Concrete B-11 0.5-2 1/25/2017 NA NA NA NA
Cyclopentane 0.016 J 000287-92-3 NL NL NL
Cyclotetrasiloxane, octamethyl-0.004 J 000556-67-2 NL NL NL
Cyclotrisiloxane, hexamethyl-0.008 J 000541-05-9 NL NL NL
Former Coal Pile B-13 0.5-2 1/24/2017 Cyclotetrasiloxane, octamethyl-0.006 J 000556-67-2 NL NL NL
Former Dye Room B-14 0.5-2 1/25/2017 NL NL NL
Cyclotetrasiloxane, octamethyl-0.006 J 000556-67-2 NL NL NL
Cyclotrisiloxane, hexamethyl-0.010 J 000541-05-9 NL NL NL
Former Boiler Room B-16 0.5-2 1/25/2017 Octanal 0.005 J 000124-13-0 NL NL NL
Manhole/Trench Drains B-17 14-15 2/28/2017
Former Boiler Room DUP 0.5-2 1/25/2017 Cyclotrisiloxane, hexamethyl-0.011 J 000541-05-9 NL NL NL
Detached Boiler Room
Building and Former AST TW-2 0.5-2 1/25/2017 NA NA NA NA
Former Dye Room TW-4 0.5-2 1/25/2017 NA NA NA NA
Former Boiler Room TW-5 0.5-2 1/25/2017 NA NA NA NA
Former Hosiery Equipment
Repair/Basement TW-6 0.5-2 1/25/2017 NA NA NA NA
Former Shop Areas TW-7 0.5-2 1/25/2017 NA NA NA NA
Notes:
1)All results provided in mg/kg (milligrams per kilogram) or parts per million.
2)
3)IHSB PSRGs = Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (October 2016)
4)Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
5)
6)
Result = Result Exceeds Minimum Detection Limits
Result = Result Exceeds IHSB PSRG Unrestricted Use Concentration
Result = Result Exceeds IHSB PSRG Soils-to-Groundwater
QUALIFIERS:
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
V The sample concentration is too high to evaluate accurate spike recoveries.
Detached Boiler Room
Building and Former AST B-1
Former Coal Pile B-12 0.5-2 1/24/2017
Former Shop Areas B-9 0.5-2 1/24/2017
Up Gradient Location on Site BG-1 0.5-2 1/24/2017
Analytical Method
Up Gradient Location on Site BG-2 1/24/2017
Former Hosiery Equipment
Repair/Basement B-15 0.5-2 1/25/2017
NA
Residential AST's B-5 0.5-2 1/24/2017
Former Knitting &
Storage/concrete basin/air
filter system/Chemical
NA
NA
WR Project # 02090017.2
8260 TICs
B-7 0.5-2 1/24/2017
0.5-2
0.5-2 1/24/2017
SUMMARY OF SOIL ANALYTICAL RESULTS
Pilot Mountain Brownfields
612 EAST MAIN STREET
PILOT MOUNTAIN, SURRY COUNTY, NORTH CAROLINA
NA
NA
NA = Not Analyzed
NL = Not Listed
J0 J0 Analyte exceeds %D or % Rec for Continuing Calibration per 8260C or 8270D method specific criteria. The identification of the analyte is
acceptable; the reported value is an estimate.
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of
constituents.
TABLE 1B
NA
NA
NA
NA
Page 3 of 5
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Up Gradient Location on Site BG-1 0.-2 1/24/2017 <0.00882 <0.00869 <0.0876 J4 0.00785 J <0.00955 <0.008 <0.00991 <0.00753 <0.00763 <0.0113 <0.109 0.0161 J <0.00937 <0.0106 <0.0122 0.0108 J <0.0169 <0.066
Up Gradient Location on Site BG-2 0.5-2 1/24/2017 <0.00884 <0.00871 <0.0878 J4 <0.0059 <0.00957 <0.00802 <0.00993 <0.00755 <0.00765 <0.0113 <0.109 <0.00683 <0.0094 <0.0106 <0.0122 <0.00727 <0.0169 <0.0661
Detached Boiler Room Building and
Former AST B-1 0.5-2 1/24/2017 <0.00871 <0.00858 <0.0865 J4 0.022 J 0.0262 J 0.00862 J 0.0109 J 0.0185 J 0.0206 J <0.0111 <0.108 0.0405 J <0.00926 <0.0105 <0.0121 0.0246 J 0.0336 J <0.0651
Residential AST's B-5 0.5-2 1/24/2017 <0.0079 <0.00778 <0.0784 J4 <0.00527 <0.00855 <0.00716 <0.00887 <0.00674 <0.00683 <0.0101 <0.0977 <0.0061 <0.00839 <0.0095 <0.0109 <0.0065 <0.0151 <0.0591
Former Knitting & Storage/concrete
basin/air filter system/Chemical B-7 0.5-2 1/24/2017 <0.00829 <0.00817 <0.0823 J4 J6 <0.00553 <0.00898 <0.00752 <0.00931 <0.00708 <0.00717 <0.0106 <0.103 <0.00641 <0.00881 <0.00997 <0.0115 <0.00682 <0.0159 <0.062
Former Shop Areas B-8 0.5-2 1/24/2017 <0.00851 <0.00838 <0.0845 J4 0.0106 J 0.0127 J <0.00772 <0.00956 0.00788 J 0.00867 J <0.0109 <0.105 0.0105 J <0.00904 <0.0102 <0.0118 <0.007 <0.0163 <0.0637
Former Shop Areas B-9 0.5-2 1/24/2017 <0.00754 <0.00742 <0.0748 J4 <0.00503 <0.00816 <0.00684 <0.00847 <0.00644 <0.00652 <0.00964 <0.0933 <0.00583 <0.00801 <0.00907 <0.0104 <0.0062 <0.0144 <0.0564
Multiple Trench Drains filled with
Concrete B-10 0.5-2 1/25/2017 5 7.24 <1.52 J4 14.9 18.0 5.34 3.84 11.6 13.6 1.44 <1.9 37.8 3.08 4.38 0.336 J 30.9 24.5 <1.15
Multiple Trench Drains filled with
Concrete B-11 0.5-2 1/25/2017 <0.00817 <0.00804 <0.081 J4 0.0134 J 0.0203 J <0.0074 <0.00917 0.0126 J 0.0148 J <0.0104 <0.101 0.0229 J <0.00867 <0.00982 <0.0113 0.00954 J <0.0156 <0.061
Former Coal Pile B-12 0.5-2 1/24/2017 <0.00817 <0.00804 <0.0811 J4 <0.00545 <0.00885 <0.00741 <0.00918 <0.00698 <0.00706 <0.0105 <0.101 <0.00631 <0.00868 <0.00983 <0.0113 <0.00672 <0.0157 <0.0611
Former Coal Pile B-13 0.5-2 1/24/2017 <0.00823 <0.0081 <0.0817 J4 0.0103 J 0.012 J <0.00746 <0.00924 0.00826 J 0.00927 J <0.0105 <0.102 0.0173 J <0.00874 <0.0099 <0.0114 0.0131 J <0.0158 <0.0615
Former Dye Room B-14 0.5-2 1/25/2017 0.112 0.203 <0.808 J4 0.562 0.959 0.288 0.135 0.568 0.616 0.0522 <1.01 1.34 0.0727 0.165 0.0529 0.799 0.832 0.132 J
Former Hosiery Equipment
Repair/Basement B-15 0.5-2 1/25/2017 <0.00844 <0.00831 <0.0838 J4 <0.00563 <0.00914 <0.00765 <0.00948 <0.00721 <0.0073 <0.0108 <0.104 <0.00652 <0.00897 <0.0102 <0.0117 <0.00694 <0.0162 <0.0631
Former Boiler Room B-16 0.5-2 1/25/2017 <0.00822 0.0391 J <0.0815 J4 0.167 0.305 0.103 0.103 0.165 0.191 0.0365 J <0.102 0.295 <0.00873 0.108 <0.0114 0.118 0.276 <0.0614
Multiple Trench Drains filled with
Concrete B-17 14-15 2/28/2017 <0.00866 <0.00853 <0.0859 <0.00577 <0.00938 <0.00785 <0.00973 <0.00739 <0.00749 <0.0111 <0.107 J4 <0.00669 <0.0092 <0.0104 <0.012 <0.00712 <0.0166 <0.0648
Former Boiler Room DUP 0.5-2 1/25/2017 <0.00988 <0.00972 <0.098 J4 <0.00659 <0.0107 <0.00896 <0.0111 <0.00843 <0.00854 <0.0126 <0.122 <0.00763 <0.0105 <0.0119 <0.0137 <0.00812 <0.0189 <0.0739
Detached Boiler Room Building and
Former AST TW-2 0.5-2 1/25/2017 <0.00948 <0.00933 <0.094 J4 <0.00632 <0.0103 <0.00859 <0.0106 <0.00809 <0.00819 <0.0121 <0.117 0.0211 J <0.0101 <0.0114 <0.0131 <0.00779 <0.0182 <0.0708
Former Dye Room TW-4 0.5-2 1/25/2017 <0.00842 <0.00829 <0.0836 J4 0.00779 J 0.0105 J <0.00763 <0.00946 <0.00719 <0.00728 <0.0108 <0.104 0.0151 J <0.00895 <0.0101 <0.0117 0.0141 J <0.0161 <0.063
Former Boiler Room TW-5 0.5-2 1/25/2017 <0.00791 <0.00778 <0.0785 J4 0.00981 J 0.0134 J <0.00717 <0.00888 0.00805 J 0.00909 J <0.0101 <0.0978 0.0193 J <0.0084 <0.00951 <0.0109 0.0132 J 0.0159 J <0.0591
Former Hosiery Equipment
Repair/Basement TW-6 0.5-2 1/25/2017 <0.00932 <0.00918 <0.0925 J4 <0.00622 <0.0101 <0.00845 <0.0105 <0.00796 <0.00806 <0.0119 <0.115 <0.0072 <0.00991 <0.0112 <0.0129 0.0103 J <0.0179 <0.0697
Former Shop Areas TW-7 0.5-2 1/25/2017 <0.00796 <0.00784 <0.079 J4 <0.00531 <0.00862 <0.00722 <0.00894 <0.0068 <0.00688 <0.0102 <0.0985 <0.00615 <0.00846 <0.00957 <0.011 <0.00655 <0.0153 <0.0595
Notes:
1)
2)
3)
4)
J The identification of the analyte is acceptable; the reported value is an estimate.
NA J3 The associated batch QC was outside the established quality control range for precision.
Result
Result = Result Exceeds IHSB PSRG Unrestricted Use Concentration Concentration
Result J4 The associated batch QC was outside the established quality control range for accuracy.
O1
These failures indicate matrix interference.
0.016
0.19
16
187800
NL 0.016
0.059
0.16
0.18 0.6
0.16 1.6
5.9 NL
1.2720
8.4
3,600
660 NL
0.00053
330
480
56
480
2
0.16
0.21
3.8 NL
68
360
220
1
0.0048
87-86-5129-00-085-01-8193-39-5 91-20-3206-44-0 86-73-7218-01-9 53-70-3 91-94-1207-08-9 191-24-2 50-32-883-32-9 120-12-7 92-87-5 56-55-3 205-99-2
TABLE 1C
SUMMARY OF SOIL ANALYTICAL RESULTS
PILOT MOUNTAIN BROWNFIELDS
612 EAST MAIN STREET
PILOT MOUNTAIN, SURRY COUNTY, NORTH CAROLINA
Analytical Method
WR Project # 02090017.2
EPA-8270D
Area Sample
ID
Sample
Depth
(Feet BLS)
Date
Collected
IHSB PSRGs - Unrestricted Use
IHSB PSRGs - Soil-to-Groundwater
All results provided in mg/kg (milligrams per kilogram) or parts per million.
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
IHSB PSRGs = Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (October 2016)
Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
JO
Qualifiers
= Not Analyzed by Method Shown
= Result Exceeds Minimum Detection Limits
= Result Exceeds IHSB PSRG Soil-to-Groundwater
J0 Analyte exceeds %D or % Rec for Continuing Calibration per 8260C or 8270D method specific criteria. The identification of the analyte is
acceptable; the reported value is an estimate.
The analyte failed the method required serial dilution test and/or subsequent post-spike criteria.
Page 4 of 5
Area Sample
ID
Sample
Depth
(Feet
BLS)
Date
Collected Tentatively Identified Compounds (TICs)Estimated
Concentration
(mg/kg)
Qualifiers CAS
IHSB PSRGs -
Unrestricted
Use
IHSB PSRGs -
Industrial
IHSB PSRGs -
Soil-to-
Groundwater
1H-Cycloprop(e)azulene, 1a,2,3,4,4 1.040 J 000489-40-7 NL NL NL
Hexadecanoic acid 0.192 J 000057-10-3 NL NL NL
Naphthalene, 1,2,3,4,4a,5,6,8a-oct 0.070 J 030021-74-0 NL NL NL
1-Eicosanol 0.052 J 000629-96-9 NL NL NL
1-Docosene 0.134 J 001599-67-3 NL NL NL
.gamma.-Sitosterol 0.163 J 000083-47-6 NL NL NL
Oxirane, hexadecyl-0.086 J 007390-81-0 NL NL NL
Dotriacontane 0.054 J 000544-85-4 NL NL NL
13-Octadecenal 0.088 J 056554-90-6 NL NL NL
Detached Boiler Room
Building and Former AST B-1 0.5-2 1/24/2017 Hexadecanoic acid 0.076 J 000057-10-3 NL NL NL
Residential AST's B-5 0.5-2 1/24/2017 Hexadecanoic acid 0.060 J 000057-10-3 NL NL NL
Octadecanoic acid 0.036 J 000057-11-4 NL NL NL
Hexadecanoic acid 0.056 J 000057-10-3 NL NL NL
trans-Chlordane 0.055 J 005103-74-2 NL NL NL
Former Shop Areas B-8 0.5-2 1/24/2017 NA NA NA NA
Former Shop Areas B-9 0.5-2 1/24/2017 Octadecanoic acid 0.064 J 000057-11-4 NL NL NL
9,10-Anthracenedione 2.040 J 000084-65-1 14 57 NL
11H-Benzo(a)fluorene 0.813 J 000238-84-6 NL NL NL
Benzo(k)fluoranthene 7.290 J 000207-08-9 1.6 29 5.9
Dibenzothiophene 1.330 J 000132-65-0 156 2400 NL
Phenanthrene, 1-methyl-1.660 J 003674-66-9 NL NL NL
Anthracene, 9-methyl-2.280 J 000779-02-2 NL NL NL
Phenanthrene, 2,5-dimethyl-0.890 J 003674-66-6 NL NL NL
Cyclopenta(def)phenanthrenone 0.920 J 005737-13-3 NL NL NL
Benzo(k)fluoranthene 3.410 J 000207-08-9 1.6 29 5.9
2-Phenylnaphthalene 1.510 J 035465-71-5 NL NL NL
4H-Cyclopenta(def)phenanthrene 4.670 J 000203-64-5 NL NL NL
Cyclohexasiloxane, dodecamethyl-6.720 J 000540-97-6 NL NL NL
Benz(a)anthracene, 11-methyl-1.080 J 006111-78-0 NL NL NL
Hexadecanoic acid 0.223 J 000057-10-3 NL NL NL
Octadecanoic acid 0.217 J 000057-11-4 NL NL NL
Eicosane 0.042 J 000112-95-8 NL NL NL
Hexadecane,2,6,10,14-tetramethyl-0.037 J 000638-36-8 NL NL NL
28-Nor-17.alpha.(H)-hopane 0.089 J 053584-60-4 NL NL NL
Former Coal Pile B-12 0.5-2 1/24/2017 NA NA NA NA
Former Coal Pile B-13 0.5-2 1/24/2017 9-Octadecenamide, (z)-0.108 J 000301-02-0 NL NL NL
Benzo(k)fluoranthene 0.405 J 000207-08-9 1.6 29 5.9
Cyclohexasiloxane, dodecamethyl-0.470 J 000540-97-6 NL NL NL
Former Hosiery Equipment
Repair/Basement B-15 0.5-2 1/25/2017 Hexadecanoic acid 0.055 J 000057-10-3 NL NL NL
Perylene 0.145 J 000198-55-0 NL NL NL
Cyclopenta(def)phenanthrenone 0.034 J 005737-13-3 NL NL NL
Benzo(i)fluoranthene 0.035 J 000205-82-3 0.42 1.8 NL
9-Octadecenamide, (z)-0.688 J 000301-02-0 NL NL NL
Cyclypentasiloxane, decamethyl-0.032 J 000541-02-6 NL NL NL
Former Boiler Room DUP 0.5-2 1/25/2017 NA NA NA NA
Hexadecanoic acid 0.175 J 00057-10-3 NL NL NL
9-Octadecenamide, (z)-0.232 J 000301-02-0 NL NL NL
.alpha.-Pinene 0.035 J 000080-56-8 NL NL NL
Eicosane 0.061 J 000112-95-8 NL NL NL
Hexadecanoic acid 0.092 J 000057-10-3 NL NL NL
Pentacosane 0.063 J 000629-99-2 NL NL NL
Hexatriacontane 0.064 J 000630-06-8 NL NL NL
Hexadecanoic acid 0.192 J 000057-10-3 NL NL NL
Octadecanoic acid 0.240 J 000057-11-4 NL NL NL
Former Hosiery Equipment
Repair/Basement TW-6 0.5-2 1/25/2017 Hexadecanoic acid 0.024 J 000057-10-3 NL NL NL
Former Shop Areas TW-7 0.5-2 1/25/2017 NA NA NA NA
Notes:
1)All results provided in mg/kg (milligrams per kilogram) or parts per million.
2)
3)IHSB PSRGs = Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (October 2016)
4)Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
5)
6)
Result = Result Exceeds Minimum Detection Limits
Result = Result Exceeds IHSB PSRG Unrestricted Use Concentration
Result = Result Exceeds IHSB PSRG Soil-to-Groundwater
QUALIFIERS:
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
V The sample concentration is too high to evaluate accurate spike recoveries.
Former Boiler Room TW-5 0.5-2 1/25/2017
Manhole/Trench Drains B-17 14-15 2/28/2017
8270 TICs
NA
Detached Boiler Room
Building and Former AST TW-2 0.5-2
TW-4
BG-2
SUMMARY OF SOIL ANALYTICAL RESULTS
PILOT MOUNTAIN BROWNFIELDS
612 EAST MAIN STREET
PILOT MOUNTAIN, SURRY COUNTY, NORTH CAROLINA
WR Project # 02090017.2
Former Dye Room
1/25/2017
0.5-2 1/25/2017
Analytical Method
1/25/2017
1/25/2017
1/25/2017
0.5-2
B-16Former Boiler Room
Multiple Trench Drains filled
with Concrete B-11 0.5-2 1/25/2017
1/24/2017
0.5-2
B-14 0.5-2
B-10 0.5-2
NA
NA
NA
Up Gradient Location on Site BG-1 0.5-2 1/24/2017
Up Gradient Location on Site
Former Dye Room
Multiple Trench Drains filled
with Concrete
NA = Not Analyzed
NL = Not Listed
J0 Analyte exceeds %D or % Rec for Continuing Calibration per 8260C or 8270D method specific criteria. The identification of the analyte is
acceptable; the reported value is an estimate.J0
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list
of constituents.
TABLE 1D
1/24/2017
Former Knitting &
Storage/concrete basin/air
filter system/Chemical
Storage
B-7 0.5-2
Page 5 of 5
EPA-2540
TO
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Up Gradient Location on Site BG-1 0.-2 1/24/2017 72.7 0.315 J 4.71 0.382 J <0.11 24.2 11.4 19.3 77.1 3.8 1.49 <0.213 0.317 J 20.3 0.0624
Up Gradient Location on Site BG-2 0.5-2 1/24/2017 72.6 0.246 J 3.18 0.827 J <0.11 30.8 21 20.5 366 8.31 1.78 <0.214 0.367 J 43.4 0.0446
Detached Boiler Room Building and
Former AST B-1 0.5-2 1/24/2017 73.7 0.25 J 4.73 0.338 J <0.109 37.6 23 25.1 92.8 3.82 1.02 <0.21 0.225 J 28.6 0.0558
Residential AST's B-5 0.5-2 1/24/2017 81.3 <0.194 2.34 0.348 J <0.0984 12.8 24.9 20.6 70.5 2.98 0.881 <0.191 0.154 J 16.9 0.0277
Former Knitting & Storage/concrete
basin/air filter system/Chemical B-7 0.5-2 1/24/2017 77.4 0.221 J 3.97 0.31 J <0.103 43.3 33.4 22.5 139 6.01 1.08 <0.2 0.343 J 27.2 0.051
Former Shop Areas B-8 0.5-2 1/24/2017 75.4 <0.21 2.3 0.228 J <0.106 40.6 27.4 23.3 108 4.07 0.81 <0.206 <0.126 25.6 0.0436
Former Shop Areas B-9 0.5-2 1/24/2017 85.1 <0.186 2.86 0.312 J <0.094 16.2 11.7 17.9 78 4.8 0.927 <0.182 0.213 J 20.8 0.0695
Multiple Trench Drains filled with
Concrete B-10 0.5-2 1/25/2017 83.5 <0.189 3.51 0.264 J 0.281 J 18.3 27.5 23.6 99.7 3.25 0.653 <0.186 0.181 J 39 0.0483
Multiple Trench Drains filled with
Concrete B-11 0.5-2 1/25/2017 78.6 <0.201 3.08 0.394 J 0.12 J 25.5 38.6 27.8 219 4.62 1.35 <0.197 0.234 J 39.1 0.0622
Former Coal Pile B-12 0.5-2 1/24/2017 78.6 <0.201 4.02 0.289 J <0.102 20 20.9 21.5 78.4 3.38 1.14 <0.197 0.187 J 17 0.0527
Former Coal Pile B-13 0.5-2 1/24/2017 78 0.221 J 3.21 0.314 J <0.103 27 18.7 17.9 115 5.16 0.489 J <0.199 0.232 J 26.6 0.0484
Former Dye Room B-14 0.5-2 1/25/2017 78.9 0.363 J 4.72 0.531 J 0.579 J 43.4 49.4 119 163 6.72 1.91 <0.197 0.248 J 145 0.926
Former Hosiery Equipment
Repair/Basement B-15 0.5-2 1/25/2017 76.1 <0.208 4.92 0.379 J <0.105 32.9 29.8 22.6 99.9 5.05 1.65 <0.204 0.378 J 29.3 0.072
Former Boiler Room B-16 0.5-2 1/25/2017 78.1 <0.202 1.95 0.728 0.509 J 8 267 59.2 1930 4.44 0.988 <0.198 0.31 J 50.1 0.0133 J
Multiple Trench Drains filled with
Concrete B-17 14-15 2/28/2017 74.1 <0.213 0.522 J 0.221 J <0.108 6.34 57.4 29.6 189 2.73 0.525 J <0.209 <0.128 19.7 <0.00378
Former Boiler Room DUP 0.5-2 1/25/2017 65 <0.243 1.66 0.667 J <0.123 7.09 159 13.4 212 1.24 2.07 <0.239 <0.146 13.1 <0.00431
Detached Boiler Room Building and
Former AST TW-2 0.5-2 1/25/2017 67.8 <0.233 2.99 0.356 J <0.118 35.8 55.4 49.4 301 6.81 1.38 <0.229 0.242 J 49.4 0.0451
Former Dye Room TW-4 0.5-2 1/25/2017 76.2 <0.207 3.08 0.169 J <0.105 22 47.2 30.9 73.7 2.38 0.782 <0.203 0.16 J 12.4 0.0369
Former Boiler Room TW-5 0.5-2 1/25/2017 81.2 <0.195 2.14 2.14 0.21 J 42.7 37.5 18.6 974 32 <2.34 <0.191 1.43 173 <0.00345
Former Hosiery Equipment
Repair/Basement TW-6 0.5-2 1/25/2017 68.8 0.901 5.31 0.889 J 1.01 65.4 80.4 49.6 979 14 3.63 <0.225 0.729 334 0.263
Former Shop Areas TW-7 0.5-2 1/25/2017 80.6 <0.196 J6 3.21 0.233 J, O1 <0.0992 24.5 18.7 24.1 179 3.69 0.804 <0.192 0.308 J 16.8 O1 0.0475
Notes:
1)
2)
3)
4)
J The identification of the analyte is acceptable; the reported value is an estimate.
NA = Not Analyzed by Method Shown J3 The associated batch QC was outside the established quality control range for precision.
Result = Result Exceeds Minimum Detection Limits
Result = Result Exceeds IHSB PSRG Unrestricted Use Concentration
Result = Result Exceeds IHSB PSRG Soil-to-Groundwater J4 The associated batch QC was outside the established quality control range for accuracy.
3.4
0.156
0.28
NL
NL 653
JO
NL
620
700
400
270
J0 Analyte exceeds %D or % Rec for Continuing Calibration per 8260C or 8270D method specific criteria. The identification of
the analyte is acceptable; the reported value is an estimate.
300
130 11200
6.2
0.9
0.68
5.8
32
63
14.2 78
2.1
EPA-6020 EPA-7471A
2.2NL36078
7440-38-2 7440-43-9 7440-47-3
4600
7782-49-27440-02-07439-96-57439-92-1
Date
Collected
7439-97-6TSOLIDS7440-28-0
TABLE 1E
SUMMARY OF SOIL ANALYTICAL RESULTS
PILOT MOUNTAIN BROWNFIELDS
612 EAST MAIN STREET
PILOT MOUNTAIN, SURRY COUNTY, NORTH CAROLINA
7440-36-0 7440-41-7 7440-50-8 7440-66-6
WR Project # 02090017.2
Analytical Method
Area Sample
ID
IHSB PSRGs - Unrestricted Use
IHSB PSRGs - Soil-to-Groundwater
Qualifiers
Sample
Depth
(Feet BLS)
7440-22-4
All results provided in mg/kg (milligrams per kilogram) or parts per million, except total solids. Total solids is reported as a percentage.
Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents.
IHSB PSRGs = Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (October 2016)
Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected.
O1 The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. Theses failures indicate
matrix interference
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Page 1 of 1
Easting Northing
TW-1 Unknown 2 38 Unknown Unknown NM 1/25/2017 27.27 ---1571192.46 961371.82
TW-2 1/18/2017 2 36 21 21-36 NM 1/25/2017 24.18 ---1571017.40 961038.21
TW-3 Unknown 2 37 Unknown Unknown NM 1/25/2017 24.72 ---1571089.05 961036.97
TW-4 1/18/2017 2 38 23 23-38 NM 1/25/2017 29.44 ---1570950.72 961223.93
TW-5 1/18/2017 2 40 25 25-40 NM 1/25/2017 30.96 ---1571037.73 961210.94
TW-6 1/18/2017 2 35 15 15-35 NM 1/25/2017 25.94 ---1571048.85 961154.32
TW-7 1/19/2017 2 45 25 25-45 NM 1/25/2017 31.21 ---1571299.78 961166.20
1)
2)
Top-of-Casing
Elevation
Well Coordinates
(NC State Plane NAD 83 Feet)Date Water
Level
Measured
PILOT MOUNTAIN, SURRY COUNTY, NORTH CAROLINA
WR Project # 02090017.2
All measurements shown in feet, unless otherwise indicated.
Depth-to-Water
from
Below Land
Surface (BLS)
Total
Depth
Well
Casing
Depth
Notes:
Well ID Date Installed
NM Denotes "Not Measured"
Screened
Interval
TABLE 3
612 EAST MAIN STREET
MONITORING WELL CONSTRUCTION INFORMATION
Well
Casing
Diameter
(inches)
Free Product
Thickness
PILOT MOUNTAIN BROWNFIELDS

Appendix A
Soil Boring Logs
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 2.5 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
0.5 Red, brown, silty clay to clayey silt, 30-40% clay, 10-20% very fine sand, moist, no odor, mica 0.5
NC NAD83 Easting:1571599.96 NC NAD83 Northing:961275.62
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
BG-1 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 1.1 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
0.5 Red, brown, clayey silt, 20-30% clay, 10-20% very fine sand, moist, no odor, mica 0.5
NC NAD83 Easting:1571580.53 NC NAD83 Northing:961316.84
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
BG-2 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 1.2 2
Notes:
0.5
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-1 Pilot Mountain Brownfields Job #:2090017.20
NC NAD83 Easting:1571018.47 NC NAD83 Northing:961093.60
Soil Description
(Field USCS Classification)Depth(ppm)fromDepthfrom
Red, brown, silty clay, 30-40% silt, 20-30% fine-very fine sand, slightly moist, no odor, mica0.5
2.) BLS - Below Land Surface
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
3" concrete pad - coring
1.) Boring Terminated at 2' BLS

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.6 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
6" asphalt - coring
0.5 Red, brown, silty clay, 30-40% silt, 20-30% fine-very fine sand,slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571080.14 NC NAD83 Northing:961059.93
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-2 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.9 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
4" asphalt - pick axe
0.5 Red, brown, silty clay, 30-40% silt, 20-30% fine-very fine sand,slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571052.89 NC NAD83 Northing:961037.72
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-3 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.3 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
0.5 Red, brown, clayey silt, 20-30% clay, 10-20% very fine sand, moist, no odor, mica 0.5
NC NAD83 Easting:1571464.46 NC NAD83 Northing:961284.21
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-4 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.8 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
0.5 Red, brown, orange, silt, 10-20% clay, 10-20% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571483.11 NC NAD83 Northing:9615252.69
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-5 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.2 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
0.5 Red, brown, clayey silt, 30-40% clay, 10-20% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571544.06 NC NAD83 Northing:961250.54
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-6 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 1.8 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
6" concrete pad - coring
0.5 Brown, orange, clayey silt, 30-40% clay, 10-20% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571319.91 NC NAD83 Northing:961164.47
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-7 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 2.5 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
5" concrete pad - coring
0.5 Red, brown, clayey silt, 30-40% clay, 10-20% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571300.39 NC NAD83 Northing:961214.23
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-8 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 1.4 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
6" concrete pad - coring
0.5 Brown, red, clayey silt, 30-40% clay, 10-20% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571179.96 NC NAD83 Northing:961282.73
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-9 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 1.8 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
5" concrete pad - coring
0.5 Brown, red, clayey silt, 30-40% clay, trace-10% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571018.02 NC NAD83 Northing:961258.94
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 25, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-10 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.8 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
5" concrete pad - coring
0.5 Brown, red, clayey silt, 30-40% clay, 10-20% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1570953.04 NC NAD83 Northing:961330.22
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 25, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-11 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.4 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
0.5 Brown, orange, silty clay, 30-40% silt, 10-20% fine-very fine sand, slightly moist, no odor,
mica 0.5
NC NAD83 Easting:1570943.41 NC NAD83 Northing:961217.65
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-12 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.3 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
0.5 Brown, orange, silty clay, 30-40% silt, 10-20% fine-very fine sand, slightly moist, no odor,
mica 0.5
NC NAD83 Easting:1570961.53 NC NAD83 Northing:961215.07
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 24, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-13 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.6 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
5" concrete pad - coring
0.5 Brown, red, clayey silt, 30-40% clay, 10-20% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1570952.64 NC NAD83 Northing:961250.12
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 25, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-14 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.7 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
3.5" concrete pad - coring
0.5 Brown, red-orange, clayey silt, 30-40% clay, trace-10% very fine sand, dry, no odor, mica 0.5
NC NAD83 Easting:1571170.35 NC NAD83 Northing:961170.83
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 25, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-15 Pilot Mountain Brownfields Job #:2090017.20
WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.2 2
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 2' BLS
2.) BLS - Below Land Surface
Page 1 of 1
0.5 Brown, red, clayey silt, 20-30% clay, 10-20% very fine sand, slightly moist, no odor, mica 0.5
NC NAD83 Easting:1571056.41 NC NAD83 Northing:961227.52
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
January 25, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-16 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.
Boring ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
to to
2 0.2 2
4 0.5 4
6 0.1 6
8 0.2 8
10 2.2 10
12 1.5 12
14 1.0 14
15 3.3 15
Notes:
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
1.) Boring Terminated at 15' BLS
2.) BLS - Below Land Surface
Page 1 of 1
12 tan, red, silty sand, well sorted, 30-40% silt, trace-10% clays, slightly moist, no odor, mica 12
14 tan, red, silty sand,fine-very fine, well sorted, 30-40% silt, trace clays, slightly moist, no odor 14
8 red, brown, clayey silt, 30-40% clays, 20-30% fine sand, slightly moist, no odor, mica 8
10 tan, red, sandy silt, 30-40% fine sand, slighlty miost, no odor, trace clays, mica 10
4 red, brown, clayey silt, 30-40% clays, 10-20% fine sand, slightly moist, no odor, mica 4
6 red, brown, silty clay, 30-40% silt, 10-20% fine sand, slightly moist, no odor, low plasticity 6
0.5 orange, red, brown, SILT, 10-20% fine sand, 10-20% clays, dry, no odor 0.5
2 orange, red, brown, SILT, 10-20% fine sand, 20-30% clays, dry, no odor 2
NC NAD83 Easting:1571010.38 NC NAD83 Northing:961256.40
Depth Soil Description
(Field USCS Classification)Depth(ppm)from from
February 28, 2017 Pilot Mountain, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
Soil Boring Log
B-17 Pilot Mountain Brownfields Job #:2090017.20

WithersRavenel
Our People. Your Success.

Appendix B
Well Construction Records
Well ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
Notes:
0-21 ft- 2" Dia.
PVC Casing
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
3.3
brown, red, grey, clayey silt, 20-30%
clays, trace-10% very fine sand, mica,
very moist, organic odor (possible fill)
brown, red, silt, 10-20% clays, 10-20%
very fine sand, slightly moist,
micaceous, slight organic odor
From 10' to
15'
From 15' to
20'
brown, silt, trace-10% clays, 10-20%
very fine sand, moist, micaceous, slight
organic odor
From 20' to
25'
Auger refusal @ 36', saturated @ 35'
1.) Boring Terminated at 36' BLS
2.) BLS - Below Land Surface = Groundwater Level (Measured Beneath TOC)
brown, silt, trace-10% clays, trace-10%
very fine sand, moist to saturated,
micaceous, no odor
From 25' to
36'
17-19 ft Bentonite
19-36 ft Clean-Washed Torpedo SAND
0-12 ft Concrete Grout (if permanent)
From 2.5' to
5'
From 5' to
10'
33
34
35
3.) TOC - Top of Casing
36
37
38
39
40
21-36 ft 2" Dia.
0.010-Slot PVC
Well Screen
5.1
25
17
18
19
20
21
31
32
6
22.4
red, brown, silt, 10-20% clays, trace-
10% very fine sand, micaceous, slightly
moist, no odor (possible fill)
7
8
9
26
3.9
10
11
5.6
12
27
28
29
30
3.4
22
23
24
13
14
15
16
3
22.7
red, brown, silt, 10-20% clays, 10-20%
very fine sand, mica, dry - slightly
moist, piney odor (possible fill)
NC NAD83 Easting:1571017.40
1 27.7 red, brown, clayey silt, 30-40% clays,
10-20% very fine sand, dry, some fill
From 0' to
2'2
4
5
Jackson Cates Quantex, Inc.GW EL:n/a
NC NAD83 Northing:961038.21
Depth in
Feet Soil Description
(Field USCS Classification)
Well Construction
0 Ground Surface(ppm)
WELL CONSTRUCTION LOG
TW-2 Pilot Mountain Brownfields Job #:02090017.2
January 18, 2017 Pilot Mountian, NC TOC EL:n/a

WithersRavenel
Our People. Your Success.
Well ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
Notes:
2.7
3.3
1.8
1.5
0.6
3.3
2.0
32
33
34
22
23
24
25
13
14
26
15
16
17
18
19
20
21
0-19 ft Concrete Grout (if permanent)
brown, silt, trace-10% clays, trace very
fine sand, micaceous, moist to wet, no
odor
From 30' to
38'
21-38 ft Clean-Washed Torpedo SAND 23-38 ft 2" Dia.
0.010-Slot PVC
Well Screen
0-23 ft- 2" Dia.
PVC Casing
red, brown, silty clay, 30-40% silt, slight
moist, no odor, mica, low plasticity
red, brown, clayey silt, 30-40% clays,
trace very fine sand, micaceous,
slightly moist, no odor
red, brown, clayey silt, 10-20% clays,
trace very fine sand, micaceous,
slightly moist, no odor
From 0' to
2'
From 2' to
5'
From 5' to
10'
From 10' to
20'
From 20' to
30'
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
27
28
29
30
1.) Boring Terminated at 38.5' BLS
2.) BLS - Below Land Surface = Groundwater Level (Measured Beneath TOC)
3.) TOC - Top of Casing
Page 1 of 1
35
36
37
38
Auger refusal @ 38.5'
brown, red, silt, trace-10% clays, trace
very fine sand, micaceous, slightly
moist, no odor
19-21 ft Bentonite
3.1
39
40
31
8
9
10
11
12
NC NAD83 Easting:NC NAD83 Northing:961223.931570950.72
1
Depth in
Feet Soil Description
(Field USCS Classification)
Well Construction
0 Ground Surface
1.6
7
2
3
4
5
6
(ppm)
red, brown, silt, trace-10% clays, trace
very fine sand, micaceous, slightly
moist, no odor
WELL CONSTRUCTION LOG
Job #:02090017.2
GW EL:n/a
n/a
TW-4 Pilot Mountain Brownfields
January 18, 2017 Pilot Mountian, NC
Jackson Cates Quantex, Inc.
TOC EL:
WithersRavenel
Our People. Your Success.
Well ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
Notes:
21-23 ft Bentonite
0-21 ft Concrete Grout (if permanent)
0-25 ft- 2" Dia.
PVC Casing
25-40 ft 2" Dia.
0.010-Slot PVC
Well Screen
brown, silt, trace-10% clays, trace very
fine sand, micaceous, slightly moist, no
odor
From 0' to
5'
brown, red, micaceous silt, trace-10%
clays, trace very fine sand, moist, no
odor
brown, red, micaceous silt, trace-10%
clays, trace very fine sand, moist to
wet, no odor
From 10' to
15'
From 15' to
40'
From 5' to
10'
2.) BLS - Below Land Surface = Groundwater Level (Measured Beneath TOC)
3.) TOC - Top of Casing
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
40
wet @ 40'
1.) Boring Terminated at 40' BLS
23-40 ft Clean-Washed Torpedo SAND
36
3.0
37
38
39
29
30
31
3.4
32
33
34
35
22
23
24
25
26
3.2
27
28
3.7
17
18
19
20
21
3.1
16
11
3.3
12
13
14
15
6
3.6
red, brown, silt, trace-10% clays, trace
very fine sand, micaceous, slightly
moist, no odor
7
8
9
10
1 2.22
3
2.94
5
NC NAD83 Easting:1571037.73 NC NAD83 Northing:961210.94
Depth in
Feet Soil Description
(Field USCS Classification)
Well Construction
0 Ground Surface(ppm)
January 18, 2017 Pilot Mountian, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
WELL CONSTRUCTION LOG
TW-5 Pilot Mountain Brownfields Job #:02090017.2

WithersRavenel
Our People. Your Success.
Well ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
Notes:
11-13 ft Bentonite
0-11 ft Concrete Grout (if permanent)
13-35 ft Clean-Washed Torpedo SAND 15-35 ft 2" Dia.
0.010-Slot PVC
Well Screen
Page 1 of 1
39
40
27
28
29
30
31
36
3.4
32
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
red, brown, clayey silt, 20-30% clays,
10-20% very fine sand, moist, no odor
brown, red, silt, trace-10% clays, trace -
10% very fine sand, moist, no odor,
micaceous
From 0' to
2'
From 2.5' to
5'
brown, red, micaceous silt, trace-10%
clays, trace very fine sand, moist to
saturated, no odor
From 10' to
35'
saturated @ 35'
1.) Boring Terminated at 35' BLS
2.) BLS - Below Land Surface = Groundwater Level (Measured Beneath TOC)
3.) TOC - Top of Casing
37
0-15 ft- 2" Dia.
PVC Casing
38
33
34
22
23
24
25
26
0.2
35
21
1.9
11
2.6
12
13
14
15
16
2.3
17
18
19
20
6
2.5
red, brown, silt, trace-10% clays, trace
very fine sand, micaceous, slightly
moist, no odor
From 5' to
10'
7
8
9
10
1 2.52
3
2.44
5
NC NAD83 Easting:1571048.85 NC NAD83 Northing:961154.32
Depth in
Feet Soil Description
(Field USCS Classification)
Well Construction
0 Ground Surface(ppm)
WELL CONSTRUCTION LOG
TW-6 Pilot Mountain Brownfields Job #:02090017.2
January 18, 2017 Pilot Mountian, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
WithersRavenel
Our People. Your Success.
Well ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
PID
Notes:
(ppm)
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
41
42
43
44
45
2.3
23-45 ft Clean-Washed Torpedo SAND
brown, silt, trace-10% clays, 10-20%
sand, some gravel, moist, no odor,
micaceous
wet to saturated 40-45'
1.) Boring Terminated at 45' BLS
2.) BLS - Below Land Surface = Groundwater Level (Measured Beneath TOC)
3.) TOC - Top of Casing
0.5
37
38
39
40
27
23
24
25
26
2.0
35
36
16
1.5
17
18
19
20
21
1.1
28
29
30
31
1.3
32
33
34
22
11
1.2
12
13
14
15
5
6
1.1
7
8
9
10
WELL CONSTRUCTION LOG
TW-5 Pilot Mountain Brownfields Job #:02090017.2
1 1.2
0-21 ft Concrete Grout (if permanent)
0-25 ft- 2" Dia.
PVC Casing
2
3
1.64
NC NAD83 Easting:1571299.78 NC NAD83 Northing:961166.20
Depth in
Feet Soil Description
(Field USCS Classification)
Well Construction
0 Ground Surface
25-45 ft 2" Dia.
0.010-Slot PVC
Well Screen
January 19, 2017 Pilot Mountian, NC TOC EL:n/a
Jackson Cates Quantex, Inc.GW EL:n/a
21-23 ft Bentonite
From 30' to
35'
From 35' to
45'
orange, red, brown, clayey silt, 30-40%
clay, trace very fine sand, dry, no odor
orange, red, brown, clayey silt, 20-30%
clay, trace very fine sand, slightly
moist, no odor, mica
From 0' to
2'
From 2' to
5'
brown, silt, trace-10% clays, trace-10%
very fine sand, slight moist to moist, no
odor, micaceous
From 10' to
30'
light brown, orange, silt, trace-10%
clays, trace-10% very fine sand, slight
moist, no odor, micaceous
From 5' to
10'
tan, sandy silt, 20-30% very fine to fine
sand, trace-10% clays, micaceous,
moist to saturated, no odor (wet to
saturated 40'-45')

WithersRavenel
Our People. Your Success.

Appendix C
Brownfields Receptor Survey
BROWNFIELDS PROPERTY RECEPTOR SURVEY
Former Amos & Smith Hosiery Mill Site
Pilot Mountain, NC
Brownfields Program Project # 13008-09-86
April 2017

Page 1 of 5
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide
the information requested below. Distances are measured from the site property boundary unless otherwise
indicated by the DEQ Brownfield’s Project Manager (PM).
Site: Former Amos & Smith Hosiery Mill Site
Address: 612 East Main Street
City: Pilot Mountain, NC
County: Surry County
Brownfields Project Number: 13008-09-86
Property and Building Characteristics
Surface Conditions Current Usage Proposed Usage
Size of Property (acres) 8.15+/- NA
% of property that is wooded/brush 31.46% 31.46%
% of property that is grassed areas 24.91% 24.91%
% of property that is agricultural crops 0.00% 0.00%
% of property that is paved 21.20% 21.20%
% of property that is covered by
buildings
22.43% 22.43%
If an existing building is on-site, please respond to the following. Information can be provided on additional
sheets as needed. If numerous buildings are on-site, consult with your PM as only information on specific
buildings may be needed.
a. Provide occupancy and use
information.

50-75 people - SCC Pilot Center, Hosiery mill, bakery, office space, and community college classrooms

BROWNFIELDS PROPERTY RECEPTOR SURVEY
Former Amos & Smith Hosiery Mill Site
Pilot Mountain, NC
Brownfields Program Project # 13008-09-86
April 2017

Page 2 of 5
b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of
openings (e.g. windows, bay doors), and height (number of stories).
Foundation - spread footing, Structural frame - steel, exterior walls- face brick, roofing structure - steel
frame or truss, roofing cover - built up tar and gravel/rubber, Interior wall - drywall/sheetrock, interior
floor cover - hardwood, No ceiling - roof insulated, average rooms per floor - 12, standard
windows/doors, loading dock with bay doors (3 on south side of building), 1 story with basement
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
6" Slab on grade construction with spread footing
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of
air return, and design considerations (e.g. positive pressure?).
There are two HVAC systems that service the onsite building. Both are rooftop units with gas/electric
heating that source outdoor air and are designed with positive pressure.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No
Surrounding Property Land Use
Please provide information on the following land uses in the vicinity of the subject site, including a map of the
surrounding areas. If specific receptors are present, please provide addresses of the facilities.
Zoning/Land Use Current Use/Occupant Proposed Usage
North Carson's Automotive and Muffler
Shop, Sanders McHone Farm
Service, and Dayton Tires and
Exxon Gas Station
Residential/Commercial/Industrial
South Railroad tracks, A Plus Carports
LLC/ Quality Commercial
Structures LLC
(industrial/manufacturing)
Residential/Commercial/Industrial/Agr
iculture
East McGill Residence (residential) Residential/Commercial/Agriculture
West Carl’s Automotive Services
(residential/commercial)
Residential/Commercial
*Note - see Figure 7 zoning map (Surry County GIS)

BROWNFIELDS PROPERTY RECEPTOR SURVEY
Former Amos & Smith Hosiery Mill Site
Pilot Mountain, NC
Brownfields Program Project # 13008-09-86
April 2017

Page 3 of 5
Specific Land Uses of Interest Y/N * Distance (ft) Direction Address
Is a school or daycare center within
1,000 ft of the Property?
Y 0, 210 on site,
west
612 E. Main St.,
522 E. Main St. (vacant)
Is there a residence within 1,000 ft of
the Property?
Y See Map See Map See Map
Is there a basement within 1,000 ft of
the Property
Y See Map See Map See Map
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing
specific addresses.
*Note - see Figure 6 - Receptor Map
Utilities
For the subject property, please provide a map of known buried utilities. If available, include depth to top,
construction material, and diameter of the utilities. In addition, please provide the following information on
utility providers. If additional assessment is required, the public utility locators should be contacted. This
information can then be added to a site map.
Is there a septic system on-site? (Y or N) ____N_____
Please provide the utility providers for the subject property
a. Natural Gas
__________________________
N/A
b. Sewer
__________________________
Town of Pilot Mountain
c. Electricity
__________________________
Duke Energy
d. Other
__________________________
Water - Town of Pilot Mountain, Propane - Otay, LLC (eastern portion of
building) G and B Energy, Surry Community College (western portion of
building) AmeriGas
For surrounding properties, please complete the following table with available information.
Utility/Potential Receptors Y/N * Distance (ft) Direction
Is a storm water pipe within 100 ft of the Property boundary? Y <20 North
Is a sanitary sewer within 100 ft of the Property boundary? Y <20 North
BROWNFIELDS PROPERTY RECEPTOR SURVEY
Former Amos & Smith Hosiery Mill Site
Pilot Mountain, NC
Brownfields Program Project # 13008-09-86
April 2017

Page 4 of 5
Is a septic system leach field within 500 ft of the Property
boundary?
N N/A N/A
Is a water line main within 100 ft of Property boundary? Y <20 North
Is a natural gas line main within 100 ft of the Property boundary? N N/A N/A
Is a buried telephone/ cable main within 100 ft of the Property
boundary?
N N/A N/A
Is a buried electrical cable main within 100 ft of Property
boundary?
N N/A N/A
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation
with the subject property.
*Note - Utilities are estimated at a depth of 1-5 feet below land surface north in the right of way of East
Main Street. See Figure 8 – Utilities Map
Water Supply
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
What is the potable water supply for the property? Public __Y____ Private ______
If Private, please provide details of the water supply source (i.e. well location, well construction, etc.). If public,
please include the water providers’ name.
Town of Pilot Mountain, Surface water, community, Toms Creek, direct stream intake
PWSID 39252
Please provide the following information regarding water supply wells in the vicinity of the Property. At a
minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if
water supply or irrigation wells may be present. Information from applicable databases can and should be
utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within
the requested radius, please provide a map of the well locations. If needed, please attach a separate table to list
all wells. Please note, the PM may opt for a more extensive water supply well survey if needed.
Water Supply Wells Y/N Distance
(ft)
Direction Address
Is a public water supply well within 1 mile of the
Property boundary?
N N/A N/A N/A
Is a private water supply well within 1,500 ft of
the Property boundary?
N N/A N/A N/A
BROWNFIELDS PROPERTY RECEPTOR SURVEY
Former Amos & Smith Hosiery Mill Site
Pilot Mountain, NC
Brownfields Program Project # 13008-09-86
April 2017

Page 5 of 5
Is an irrigation well within 1,500 ft of the
Property boundary?
Y ~1120 North 210 Carson
Road
Surface Water & Wetlands
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or
in the vicinity of the Property.
Provide Information regarding Surface
Water and Wetlands
Response/Comments
Are there surface water features on
the property? (If yes, please complete
a. to d.)
No
a. Is the water body naturally
developed or man-made?
N/A
b. List the uses of the water body. N/A
c. What is the source of the water
for the water body?
N/A
d. What is the nature of the bottom
of the water body (e.g., rocky or
concrete bottom, drainage ways or
impoundments)
N/A
e. If no on-site surface water features,
what is the nearest surface water
body?
Heatherly Creek is located approximately 430' southeast of
property boundary, which flows southwest to Toms Creek and is
part of the Ararat-Pilot Mountain local watershed, located in the
Yadkin River Basin.
f. Are there any wetlands present on
the property? If no wetlands on-site,
are wetlands suspected on adjoining
properties?
No, there are no wetlands on the subject property or adjoining
properties.

Appendix D
Analytical Laboratory Reports
ANALYTICAL REPORT
February 21, 2017
Withers & Ravenel Eng. - Standard
Sample Delivery Group:L886556
Samples Received:01/27/2017
Project Number:02090017.20
Description:Pilot Mt. Brownfields
Report To:Mark Brown
115 MacKenan Drive
Cary, NC 27511
Entire Report Reviewed By:
February 21, 2017
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
February 21, 2017
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 5
⁵Sr: Sample Results 6
TW-1 L886556-01 6
TW-2 L886556-02 9
TW-3 L886556-03 12
TW-4 L886556-04 15
TW-5 L886556-05 18
TW-6 L886556-06 21
TW-7 L886556-07 24
DUP L886556-08 27
⁶Qc: Quality Control Summary 30
Mercury by Method 7470A 30
Metals (ICPMS) by Method 6020 32
Volatile Organic Compounds (GC/MS) by Method 8260B 35
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D 39
⁷Gl: Glossary of Terms 47
⁸Al: Accreditations & Locations 48
⁹Sc: Chain of Custody 49
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TW-1 L886556-01 GW J. Cates / A. Pote 01/25/17 13:15 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG947436 1 01/28/17 13:25 01/30/17 13:12 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 15:04 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/02/17 01:04 JDG
Metals (ICPMS) by Method 6020 WG948653 1 02/01/17 22:18 02/02/17 02:47 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D WG947709 1 01/30/17 08:12 01/30/17 20:15 JF
Volatile Organic Compounds (GC/MS) by Method 8260B WG948128 1 01/31/17 13:51 01/31/17 13:51 GLN
Collected by Collected date/time Received date/time
TW-2 L886556-02 GW J. Cates / A. Pote 01/25/17 14:30 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG947436 1 01/28/17 13:25 01/30/17 13:14 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 15:08 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/02/17 01:07 JDG
Metals (ICPMS) by Method 6020 WG947931 10 01/30/17 18:12 02/01/17 16:27 JDG
Metals (ICPMS) by Method 6020 WG948653 1 02/01/17 22:18 02/02/17 02:51 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D WG947709 1 01/30/17 08:12 01/30/17 20:38 JF
Volatile Organic Compounds (GC/MS) by Method 8260B WG948128 1 01/31/17 14:14 01/31/17 14:14 GLN
Collected by Collected date/time Received date/time
TW-3 L886556-03 GW J. Cates / A. Pote 01/25/17 12:30 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG947436 1 01/28/17 13:25 01/30/17 13:16 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 15:11 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/02/17 01:11 JDG
Metals (ICPMS) by Method 6020 WG947931 5 01/30/17 18:12 02/01/17 16:31 JDG
Metals (ICPMS) by Method 6020 WG948653 1 02/01/17 22:18 02/02/17 02:22 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D WG947709 1 01/30/17 08:12 01/30/17 21:02 JF
Volatile Organic Compounds (GC/MS) by Method 8260B WG948128 1 01/31/17 14:36 01/31/17 14:36 GLN
Collected by Collected date/time Received date/time
TW-4 L886556-04 GW J. Cates / A. Pote 01/25/17 13:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG947436 1 01/28/17 13:25 01/30/17 13:18 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 15:15 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/02/17 01:14 JDG
Metals (ICPMS) by Method 6020 WG948653 1 02/01/17 22:18 02/02/17 02:54 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D WG947709 1 01/30/17 08:12 01/30/17 21:25 JF
Volatile Organic Compounds (GC/MS) by Method 8260B WG948128 1 01/31/17 14:59 01/31/17 14:59 GLN
Collected by Collected date/time Received date/time
TW-5 L886556-05 GW J. Cates / A. Pote 01/25/17 13:30 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG947436 1 01/28/17 13:25 01/30/17 13:21 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 15:18 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/02/17 01:18 JDG
Metals (ICPMS) by Method 6020 WG948653 1 02/01/17 22:18 02/02/17 02:58 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D WG947709 1 01/30/17 08:12 01/30/17 21:48 JF
Volatile Organic Compounds (GC/MS) by Method 8260B WG948128 1 01/31/17 15:22 01/31/17 15:22 GLN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TW-6 L886556-06 GW J. Cates / A. Pote 01/25/17 14:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG947436 1 01/28/17 13:25 01/30/17 13:23 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 15:22 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/02/17 01:21 JDG
Metals (ICPMS) by Method 6020 WG947931 5 01/30/17 18:12 02/01/17 16:34 JDG
Metals (ICPMS) by Method 6020 WG948653 1 02/01/17 22:18 02/02/17 03:01 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D WG947709 1 01/30/17 08:12 01/30/17 22:12 JF
Volatile Organic Compounds (GC/MS) by Method 8260B WG948128 1 01/31/17 15:44 01/31/17 15:44 GLN
Collected by Collected date/time Received date/time
TW-7 L886556-07 GW J. Cates / A. Pote 01/25/17 15:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG947436 1 01/28/17 13:25 01/30/17 13:32 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 15:25 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/02/17 01:25 JDG
Metals (ICPMS) by Method 6020 WG947931 5 01/30/17 18:12 02/01/17 16:38 JDG
Metals (ICPMS) by Method 6020 WG948653 1 02/01/17 22:18 02/02/17 03:05 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D WG947709 1 01/30/17 08:12 01/30/17 22:35 JF
Volatile Organic Compounds (GC/MS) by Method 8260B WG948128 1 01/31/17 16:07 01/31/17 16:07 GLN
Collected by Collected date/time Received date/time
DUP L886556-08 GW J. Cates / A. Pote 01/25/17 12:45 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG948077 1 01/31/17 13:03 01/31/17 17:28 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 13:37 JDG
Metals (ICPMS) by Method 6020 WG947931 1 01/30/17 18:12 02/01/17 22:18 JDG
Metals (ICPMS) by Method 6020 WG947931 5 01/30/17 18:12 02/01/17 16:41 JDG
Metals (ICPMS) by Method 6020 WG948653 1 02/01/17 22:18 02/02/17 03:08 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D WG947935 1 01/30/17 18:30 01/31/17 16:48 JF
Volatile Organic Compounds (GC/MS) by Method 8260B WG948128 1 01/31/17 16:29 01/31/17 16:29 GLN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the
sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Sample Handling and Receiving
The analysis for 2-Chloroethyl Vinyl Ether was conducted from a chemically preserved container.
ESC Sample ID Project Sample ID Method
L886556-01 TW-1 8260B
L886556-02 TW-2 8260B
L886556-03 TW-3 8260B
L886556-04 TW-4 8260B
L886556-05 TW-5 8260B
L886556-06 TW-6 8260B
L886556-07 TW-7 8260B
L886556-08 DUP 8260B
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 5 of 52
Jimmy Hunt
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 5 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L886556
TW-1
Collected date/time: 01/25/17 13:15
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 01/30/2017 13:12 WG947436
Metals (ICPMS) by Method 6020
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Antimony U 0.754 2.00 1 02/02/2017 02:47 WG948653
Arsenic 0.256 J 0.250 2.00 1 02/01/2017 15:04 WG947931
Beryllium U 0.120 2.00 1 02/01/2017 15:04 WG947931
Cadmium U 0.160 1.00 1 02/01/2017 15:04 WG947931
Chromium 1.13 J 0.540 2.00 1 02/01/2017 15:04 WG947931
Copper 4.79 J 0.520 5.00 1 02/01/2017 15:04 WG947931
Lead 0.479 B J 0.240 2.00 1 02/02/2017 01:04 WG947931
Manganese 50.8 0.250 5.00 1 02/01/2017 15:04 WG947931
Nickel 1.59 B J 0.350 2.00 1 02/01/2017 15:04 WG947931
Selenium U 0.380 2.00 1 02/01/2017 15:04 WG947931
Silver U 0.310 2.00 1 02/01/2017 15:04 WG947931
Thallium U 0.190 2.00 1 02/02/2017 01:04 WG947931
Zinc 43.6 2.56 25.0 1 02/01/2017 15:04 WG947931
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 01/31/2017 13:51 WG948128
Acrolein U J4 8.87 50.0 1 01/31/2017 13:51 WG948128
Acrylonitrile U 1.87 10.0 1 01/31/2017 13:51 WG948128
Benzene U 0.331 1.00 1 01/31/2017 13:51 WG948128
Bromobenzene U 0.352 1.00 1 01/31/2017 13:51 WG948128
Bromodichloromethane U 0.380 1.00 1 01/31/2017 13:51 WG948128
Bromoform U 0.469 1.00 1 01/31/2017 13:51 WG948128
Bromomethane U 0.866 5.00 1 01/31/2017 13:51 WG948128
n-Butylbenzene U 0.361 1.00 1 01/31/2017 13:51 WG948128
sec-Butylbenzene U 0.365 1.00 1 01/31/2017 13:51 WG948128
tert-Butylbenzene U 0.399 1.00 1 01/31/2017 13:51 WG948128
Carbon tetrachloride U 0.379 1.00 1 01/31/2017 13:51 WG948128
Chlorobenzene U 0.348 1.00 1 01/31/2017 13:51 WG948128
Chlorodibromomethane U 0.327 1.00 1 01/31/2017 13:51 WG948128
Chloroethane U 0.453 5.00 1 01/31/2017 13:51 WG948128
2-Chloroethyl vinyl ether U 3.01 50.0 1 01/31/2017 13:51 WG948128
Chloroform U 0.324 5.00 1 01/31/2017 13:51 WG948128
Chloromethane U 0.276 2.50 1 01/31/2017 13:51 WG948128
2-Chlorotoluene U 0.375 1.00 1 01/31/2017 13:51 WG948128
4-Chlorotoluene U 0.351 1.00 1 01/31/2017 13:51 WG948128
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 01/31/2017 13:51 WG948128
1,2-Dibromoethane U 0.381 1.00 1 01/31/2017 13:51 WG948128
Dibromomethane U 0.346 1.00 1 01/31/2017 13:51 WG948128
1,2-Dichlorobenzene U 0.349 1.00 1 01/31/2017 13:51 WG948128
1,3-Dichlorobenzene U 0.220 1.00 1 01/31/2017 13:51 WG948128
1,4-Dichlorobenzene U 0.274 1.00 1 01/31/2017 13:51 WG948128
Dichlorodifluoromethane U 0.551 5.00 1 01/31/2017 13:51 WG948128
1,1-Dichloroethane U 0.259 1.00 1 01/31/2017 13:51 WG948128
1,2-Dichloroethane U 0.361 1.00 1 01/31/2017 13:51 WG948128
1,1-Dichloroethene U 0.398 1.00 1 01/31/2017 13:51 WG948128
cis-1,2-Dichloroethene U 0.260 1.00 1 01/31/2017 13:51 WG948128
trans-1,2-Dichloroethene U 0.396 1.00 1 01/31/2017 13:51 WG948128
1,2-Dichloropropane U 0.306 1.00 1 01/31/2017 13:51 WG948128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 6 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L886556
TW-1
Collected date/time: 01/25/17 13:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1-Dichloropropene U 0.352 1.00 1 01/31/2017 13:51 WG948128
1,3-Dichloropropane U 0.366 1.00 1 01/31/2017 13:51 WG948128
cis-1,3-Dichloropropene U 0.418 1.00 1 01/31/2017 13:51 WG948128
trans-1,3-Dichloropropene U 0.419 1.00 1 01/31/2017 13:51 WG948128
2,2-Dichloropropane U 0.321 1.00 1 01/31/2017 13:51 WG948128
Di-isopropyl ether U 0.320 1.00 1 01/31/2017 13:51 WG948128
Ethylbenzene U 0.384 1.00 1 01/31/2017 13:51 WG948128
Hexachloro-1,3-butadiene U 0.256 1.00 1 01/31/2017 13:51 WG948128
Isopropylbenzene U 0.326 1.00 1 01/31/2017 13:51 WG948128
p-Isopropyltoluene U 0.350 1.00 1 01/31/2017 13:51 WG948128
2-Butanone (MEK)U 3.93 10.0 1 01/31/2017 13:51 WG948128
Methylene Chloride U 1.00 5.00 1 01/31/2017 13:51 WG948128
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 01/31/2017 13:51 WG948128
Methyl tert-butyl ether U 0.367 1.00 1 01/31/2017 13:51 WG948128
Naphthalene U 1.00 5.00 1 01/31/2017 13:51 WG948128
n-Propylbenzene U 0.349 1.00 1 01/31/2017 13:51 WG948128
Styrene U 0.307 1.00 1 01/31/2017 13:51 WG948128
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 01/31/2017 13:51 WG948128
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 01/31/2017 13:51 WG948128
Tetrachloroethene U 0.372 1.00 1 01/31/2017 13:51 WG948128
Toluene U 0.412 1.00 1 01/31/2017 13:51 WG948128
1,2,3-Trichlorobenzene U 0.230 1.00 1 01/31/2017 13:51 WG948128
1,2,4-Trichlorobenzene U 0.355 1.00 1 01/31/2017 13:51 WG948128
1,1,1-Trichloroethane U 0.319 1.00 1 01/31/2017 13:51 WG948128
1,1,2-Trichloroethane U 0.383 1.00 1 01/31/2017 13:51 WG948128
Trichloroethene U 0.398 1.00 1 01/31/2017 13:51 WG948128
Trichlorofluoromethane U 1.20 5.00 1 01/31/2017 13:51 WG948128
1,2,3-Trichloropropane U 0.807 2.50 1 01/31/2017 13:51 WG948128
1,2,4-Trimethylbenzene U 0.373 1.00 1 01/31/2017 13:51 WG948128
1,3,5-Trimethylbenzene U 0.387 1.00 1 01/31/2017 13:51 WG948128
Vinyl chloride U 0.259 1.00 1 01/31/2017 13:51 WG948128
Xylenes, Total U 1.06 3.00 1 01/31/2017 13:51 WG948128
(S) Toluene-d8 97.5 80.0-120 01/31/2017 13:51 WG948128
(S) Dibromofluoromethane 96.1 76.0-123 01/31/2017 13:51 WG948128
(S) a,a,a-Trifluorotoluene 102 80.0-120 01/31/2017 13:51 WG948128
(S) 4-Bromofluorobenzene 100 80.0-120 01/31/2017 13:51 WG948128
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 01/30/2017 20:15 WG947709
Acenaphthylene U 0.309 1.00 1 01/30/2017 20:15 WG947709
Anthracene U 0.291 1.00 1 01/30/2017 20:15 WG947709
Benzidine U 4.32 10.0 1 01/30/2017 20:15 WG947709
Benzo(a)anthracene U 0.0975 1.00 1 01/30/2017 20:15 WG947709
Benzo(b)fluoranthene U 0.0896 1.00 1 01/30/2017 20:15 WG947709
Benzo(k)fluoranthene U 0.355 1.00 1 01/30/2017 20:15 WG947709
Benzo(g,h,i)perylene U 0.161 1.00 1 01/30/2017 20:15 WG947709
Benzo(a)pyrene U 0.340 1.00 1 01/30/2017 20:15 WG947709
Bis(2-chlorethoxy)methane U 0.329 10.0 1 01/30/2017 20:15 WG947709
Bis(2-chloroethyl)ether U 1.62 50.0 1 01/30/2017 20:15 WG947709
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 01/30/2017 20:15 WG947709
4-Bromophenyl-phenylether U 0.335 10.0 1 01/30/2017 20:15 WG947709
2-Chloronaphthalene U 0.330 1.00 1 01/30/2017 20:15 WG947709
4-Chlorophenyl-phenylether U 0.303 10.0 1 01/30/2017 20:15 WG947709
Chrysene U 0.332 1.00 1 01/30/2017 20:15 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 7 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 7 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L886556
TW-1
Collected date/time: 01/25/17 13:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Dibenz(a,h)anthracene U 0.279 1.00 1 01/30/2017 20:15 WG947709
3,3-Dichlorobenzidine U 2.02 10.0 1 01/30/2017 20:15 WG947709
2,4-Dinitrotoluene U 1.65 10.0 1 01/30/2017 20:15 WG947709
2,6-Dinitrotoluene U 0.279 10.0 1 01/30/2017 20:15 WG947709
Fluoranthene U 0.310 1.00 1 01/30/2017 20:15 WG947709
Fluorene U 0.323 1.00 1 01/30/2017 20:15 WG947709
Hexachlorobenzene U 0.341 1.00 1 01/30/2017 20:15 WG947709
Hexachloro-1,3-butadiene U 0.329 10.0 1 01/30/2017 20:15 WG947709
Hexachlorocyclopentadiene U 2.33 10.0 1 01/30/2017 20:15 WG947709
Hexachloroethane U 0.365 10.0 1 01/30/2017 20:15 WG947709
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 01/30/2017 20:15 WG947709
Isophorone U 0.272 10.0 1 01/30/2017 20:15 WG947709
Naphthalene U 0.372 1.00 1 01/30/2017 20:15 WG947709
Nitrobenzene U 0.367 10.0 1 01/30/2017 20:15 WG947709
n-Nitrosodimethylamine U 1.26 10.0 1 01/30/2017 20:15 WG947709
n-Nitrosodiphenylamine U 0.304 10.0 1 01/30/2017 20:15 WG947709
n-Nitrosodi-n-propylamine U 0.403 10.0 1 01/30/2017 20:15 WG947709
Phenanthrene U 0.366 1.00 1 01/30/2017 20:15 WG947709
Benzylbutyl phthalate U 0.275 3.00 1 01/30/2017 20:15 WG947709
Bis(2-ethylhexyl)phthalate 1.30 B J 0.709 3.00 1 01/30/2017 20:15 WG947709
Di-n-butyl phthalate 1.19 B J 0.266 3.00 1 01/30/2017 20:15 WG947709
Diethyl phthalate U 0.282 3.00 1 01/30/2017 20:15 WG947709
Dimethyl phthalate U 0.283 3.00 1 01/30/2017 20:15 WG947709
Di-n-octyl phthalate U 0.278 1.00 1 01/30/2017 20:15 WG947709
Pyrene U 0.330 1.00 1 01/30/2017 20:15 WG947709
1,2,4-Trichlorobenzene U 0.355 10.0 1 01/30/2017 20:15 WG947709
Aniline U 2.43 10.0 1 01/30/2017 20:15 WG947709
4-Chloro-3-methylphenol U 0.263 10.0 1 01/30/2017 20:15 WG947709
2-Chlorophenol U 0.283 10.0 1 01/30/2017 20:15 WG947709
2,4-Dichlorophenol U 0.284 10.0 1 01/30/2017 20:15 WG947709
2,4-Dimethylphenol U 0.264 10.0 1 01/30/2017 20:15 WG947709
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 01/30/2017 20:15 WG947709
2,4-Dinitrophenol U 3.25 10.0 1 01/30/2017 20:15 WG947709
2-Nitrophenol U 0.320 10.0 1 01/30/2017 20:15 WG947709
4-Nitrophenol U 2.01 10.0 1 01/30/2017 20:15 WG947709
Pentachlorophenol U 0.313 10.0 1 01/30/2017 20:15 WG947709
Phenol U 0.334 10.0 1 01/30/2017 20:15 WG947709
2,4,6-Trichlorophenol U 0.297 10.0 1 01/30/2017 20:15 WG947709
(S) 2-Fluorophenol 29.6 10.0-120 01/30/2017 20:15 WG947709
(S) Phenol-d5 20.0 10.0-120 01/30/2017 20:15 WG947709
(S) Nitrobenzene-d5 40.3 10.0-126 01/30/2017 20:15 WG947709
(S) 2-Fluorobiphenyl 55.0 22.0-127 01/30/2017 20:15 WG947709
(S) 2,4,6-Tribromophenol 57.5 10.0-153 01/30/2017 20:15 WG947709
(S) p-Terphenyl-d14 70.0 29.0-141 01/30/2017 20:15 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 8 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L886556
TW-2
Collected date/time: 01/25/17 14:30
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 01/30/2017 13:14 WG947436
Metals (ICPMS) by Method 6020
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Antimony U 0.754 2.00 1 02/02/2017 02:51 WG948653
Arsenic U 0.250 2.00 1 02/01/2017 15:08 WG947931
Beryllium U 0.120 2.00 1 02/01/2017 15:08 WG947931
Cadmium U 0.160 1.00 1 02/01/2017 15:08 WG947931
Chromium 0.754 J 0.540 2.00 1 02/01/2017 15:08 WG947931
Copper 5.27 0.520 5.00 1 02/01/2017 15:08 WG947931
Lead 1.54 B J 0.240 2.00 1 02/02/2017 01:07 WG947931
Manganese 1970 2.50 50.0 10 02/01/2017 16:27 WG947931
Nickel 10.9 0.350 2.00 1 02/01/2017 15:08 WG947931
Selenium U 0.380 2.00 1 02/01/2017 15:08 WG947931
Silver U 0.310 2.00 1 02/01/2017 15:08 WG947931
Thallium U 0.190 2.00 1 02/02/2017 01:07 WG947931
Zinc 18.5 J 2.56 25.0 1 02/01/2017 15:08 WG947931
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 01/31/2017 14:14 WG948128
Acrolein U J4 8.87 50.0 1 01/31/2017 14:14 WG948128
Acrylonitrile U 1.87 10.0 1 01/31/2017 14:14 WG948128
Benzene U 0.331 1.00 1 01/31/2017 14:14 WG948128
Bromobenzene U 0.352 1.00 1 01/31/2017 14:14 WG948128
Bromodichloromethane U 0.380 1.00 1 01/31/2017 14:14 WG948128
Bromoform U 0.469 1.00 1 01/31/2017 14:14 WG948128
Bromomethane U 0.866 5.00 1 01/31/2017 14:14 WG948128
n-Butylbenzene U 0.361 1.00 1 01/31/2017 14:14 WG948128
sec-Butylbenzene U 0.365 1.00 1 01/31/2017 14:14 WG948128
tert-Butylbenzene U 0.399 1.00 1 01/31/2017 14:14 WG948128
Carbon tetrachloride U 0.379 1.00 1 01/31/2017 14:14 WG948128
Chlorobenzene U 0.348 1.00 1 01/31/2017 14:14 WG948128
Chlorodibromomethane U 0.327 1.00 1 01/31/2017 14:14 WG948128
Chloroethane U 0.453 5.00 1 01/31/2017 14:14 WG948128
2-Chloroethyl vinyl ether U 3.01 50.0 1 01/31/2017 14:14 WG948128
Chloroform U 0.324 5.00 1 01/31/2017 14:14 WG948128
Chloromethane U 0.276 2.50 1 01/31/2017 14:14 WG948128
2-Chlorotoluene U 0.375 1.00 1 01/31/2017 14:14 WG948128
4-Chlorotoluene U 0.351 1.00 1 01/31/2017 14:14 WG948128
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 01/31/2017 14:14 WG948128
1,2-Dibromoethane U 0.381 1.00 1 01/31/2017 14:14 WG948128
Dibromomethane U 0.346 1.00 1 01/31/2017 14:14 WG948128
1,2-Dichlorobenzene U 0.349 1.00 1 01/31/2017 14:14 WG948128
1,3-Dichlorobenzene U 0.220 1.00 1 01/31/2017 14:14 WG948128
1,4-Dichlorobenzene U 0.274 1.00 1 01/31/2017 14:14 WG948128
Dichlorodifluoromethane U 0.551 5.00 1 01/31/2017 14:14 WG948128
1,1-Dichloroethane U 0.259 1.00 1 01/31/2017 14:14 WG948128
1,2-Dichloroethane U 0.361 1.00 1 01/31/2017 14:14 WG948128
1,1-Dichloroethene U 0.398 1.00 1 01/31/2017 14:14 WG948128
cis-1,2-Dichloroethene U 0.260 1.00 1 01/31/2017 14:14 WG948128
trans-1,2-Dichloroethene U 0.396 1.00 1 01/31/2017 14:14 WG948128
1,2-Dichloropropane U 0.306 1.00 1 01/31/2017 14:14 WG948128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 9 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 9 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L886556
TW-2
Collected date/time: 01/25/17 14:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1-Dichloropropene U 0.352 1.00 1 01/31/2017 14:14 WG948128
1,3-Dichloropropane U 0.366 1.00 1 01/31/2017 14:14 WG948128
cis-1,3-Dichloropropene U 0.418 1.00 1 01/31/2017 14:14 WG948128
trans-1,3-Dichloropropene U 0.419 1.00 1 01/31/2017 14:14 WG948128
2,2-Dichloropropane U 0.321 1.00 1 01/31/2017 14:14 WG948128
Di-isopropyl ether U 0.320 1.00 1 01/31/2017 14:14 WG948128
Ethylbenzene U 0.384 1.00 1 01/31/2017 14:14 WG948128
Hexachloro-1,3-butadiene U 0.256 1.00 1 01/31/2017 14:14 WG948128
Isopropylbenzene U 0.326 1.00 1 01/31/2017 14:14 WG948128
p-Isopropyltoluene U 0.350 1.00 1 01/31/2017 14:14 WG948128
2-Butanone (MEK)U 3.93 10.0 1 01/31/2017 14:14 WG948128
Methylene Chloride U 1.00 5.00 1 01/31/2017 14:14 WG948128
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 01/31/2017 14:14 WG948128
Methyl tert-butyl ether U 0.367 1.00 1 01/31/2017 14:14 WG948128
Naphthalene U 1.00 5.00 1 01/31/2017 14:14 WG948128
n-Propylbenzene U 0.349 1.00 1 01/31/2017 14:14 WG948128
Styrene U 0.307 1.00 1 01/31/2017 14:14 WG948128
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 01/31/2017 14:14 WG948128
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 01/31/2017 14:14 WG948128
Tetrachloroethene U 0.372 1.00 1 01/31/2017 14:14 WG948128
Toluene U 0.412 1.00 1 01/31/2017 14:14 WG948128
1,2,3-Trichlorobenzene U 0.230 1.00 1 01/31/2017 14:14 WG948128
1,2,4-Trichlorobenzene U 0.355 1.00 1 01/31/2017 14:14 WG948128
1,1,1-Trichloroethane U 0.319 1.00 1 01/31/2017 14:14 WG948128
1,1,2-Trichloroethane U 0.383 1.00 1 01/31/2017 14:14 WG948128
Trichloroethene U 0.398 1.00 1 01/31/2017 14:14 WG948128
Trichlorofluoromethane U 1.20 5.00 1 01/31/2017 14:14 WG948128
1,2,3-Trichloropropane U 0.807 2.50 1 01/31/2017 14:14 WG948128
1,2,4-Trimethylbenzene U 0.373 1.00 1 01/31/2017 14:14 WG948128
1,3,5-Trimethylbenzene U 0.387 1.00 1 01/31/2017 14:14 WG948128
Vinyl chloride U 0.259 1.00 1 01/31/2017 14:14 WG948128
Xylenes, Total U 1.06 3.00 1 01/31/2017 14:14 WG948128
(S) Toluene-d8 97.9 80.0-120 01/31/2017 14:14 WG948128
(S) Dibromofluoromethane 98.2 76.0-123 01/31/2017 14:14 WG948128
(S) a,a,a-Trifluorotoluene 102 80.0-120 01/31/2017 14:14 WG948128
(S) 4-Bromofluorobenzene 99.7 80.0-120 01/31/2017 14:14 WG948128
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 01/30/2017 20:38 WG947709
Acenaphthylene U 0.309 1.00 1 01/30/2017 20:38 WG947709
Anthracene U 0.291 1.00 1 01/30/2017 20:38 WG947709
Benzidine U 4.32 10.0 1 01/30/2017 20:38 WG947709
Benzo(a)anthracene U 0.0975 1.00 1 01/30/2017 20:38 WG947709
Benzo(b)fluoranthene U 0.0896 1.00 1 01/30/2017 20:38 WG947709
Benzo(k)fluoranthene U 0.355 1.00 1 01/30/2017 20:38 WG947709
Benzo(g,h,i)perylene U 0.161 1.00 1 01/30/2017 20:38 WG947709
Benzo(a)pyrene U 0.340 1.00 1 01/30/2017 20:38 WG947709
Bis(2-chlorethoxy)methane U 0.329 10.0 1 01/30/2017 20:38 WG947709
Bis(2-chloroethyl)ether U 1.62 50.0 1 01/30/2017 20:38 WG947709
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 01/30/2017 20:38 WG947709
4-Bromophenyl-phenylether U 0.335 10.0 1 01/30/2017 20:38 WG947709
2-Chloronaphthalene U 0.330 1.00 1 01/30/2017 20:38 WG947709
4-Chlorophenyl-phenylether U 0.303 10.0 1 01/30/2017 20:38 WG947709
Chrysene U 0.332 1.00 1 01/30/2017 20:38 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 10 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 10 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L886556
TW-2
Collected date/time: 01/25/17 14:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Dibenz(a,h)anthracene U 0.279 1.00 1 01/30/2017 20:38 WG947709
3,3-Dichlorobenzidine U 2.02 10.0 1 01/30/2017 20:38 WG947709
2,4-Dinitrotoluene U 1.65 10.0 1 01/30/2017 20:38 WG947709
2,6-Dinitrotoluene U 0.279 10.0 1 01/30/2017 20:38 WG947709
Fluoranthene U 0.310 1.00 1 01/30/2017 20:38 WG947709
Fluorene U 0.323 1.00 1 01/30/2017 20:38 WG947709
Hexachlorobenzene U 0.341 1.00 1 01/30/2017 20:38 WG947709
Hexachloro-1,3-butadiene U 0.329 10.0 1 01/30/2017 20:38 WG947709
Hexachlorocyclopentadiene U 2.33 10.0 1 01/30/2017 20:38 WG947709
Hexachloroethane U 0.365 10.0 1 01/30/2017 20:38 WG947709
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 01/30/2017 20:38 WG947709
Isophorone U 0.272 10.0 1 01/30/2017 20:38 WG947709
Naphthalene U 0.372 1.00 1 01/30/2017 20:38 WG947709
Nitrobenzene U 0.367 10.0 1 01/30/2017 20:38 WG947709
n-Nitrosodimethylamine U 1.26 10.0 1 01/30/2017 20:38 WG947709
n-Nitrosodiphenylamine U 0.304 10.0 1 01/30/2017 20:38 WG947709
n-Nitrosodi-n-propylamine U 0.403 10.0 1 01/30/2017 20:38 WG947709
Phenanthrene U 0.366 1.00 1 01/30/2017 20:38 WG947709
Benzylbutyl phthalate U 0.275 3.00 1 01/30/2017 20:38 WG947709
Bis(2-ethylhexyl)phthalate 1.25 B J 0.709 3.00 1 01/30/2017 20:38 WG947709
Di-n-butyl phthalate 1.32 B J 0.266 3.00 1 01/30/2017 20:38 WG947709
Diethyl phthalate U 0.282 3.00 1 01/30/2017 20:38 WG947709
Dimethyl phthalate U 0.283 3.00 1 01/30/2017 20:38 WG947709
Di-n-octyl phthalate U 0.278 1.00 1 01/30/2017 20:38 WG947709
Pyrene U 0.330 1.00 1 01/30/2017 20:38 WG947709
1,2,4-Trichlorobenzene U 0.355 10.0 1 01/30/2017 20:38 WG947709
Aniline U 2.43 10.0 1 01/30/2017 20:38 WG947709
4-Chloro-3-methylphenol U 0.263 10.0 1 01/30/2017 20:38 WG947709
2-Chlorophenol U 0.283 10.0 1 01/30/2017 20:38 WG947709
2,4-Dichlorophenol U 0.284 10.0 1 01/30/2017 20:38 WG947709
2,4-Dimethylphenol U 0.264 10.0 1 01/30/2017 20:38 WG947709
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 01/30/2017 20:38 WG947709
2,4-Dinitrophenol U 3.25 10.0 1 01/30/2017 20:38 WG947709
2-Nitrophenol U 0.320 10.0 1 01/30/2017 20:38 WG947709
4-Nitrophenol U 2.01 10.0 1 01/30/2017 20:38 WG947709
Pentachlorophenol U 0.313 10.0 1 01/30/2017 20:38 WG947709
Phenol U 0.334 10.0 1 01/30/2017 20:38 WG947709
2,4,6-Trichlorophenol U 0.297 10.0 1 01/30/2017 20:38 WG947709
(S) 2-Fluorophenol 21.7 10.0-120 01/30/2017 20:38 WG947709
(S) Phenol-d5 13.3 10.0-120 01/30/2017 20:38 WG947709
(S) Nitrobenzene-d5 37.8 10.0-126 01/30/2017 20:38 WG947709
(S) 2-Fluorobiphenyl 54.0 22.0-127 01/30/2017 20:38 WG947709
(S) 2,4,6-Tribromophenol 62.5 10.0-153 01/30/2017 20:38 WG947709
(S) p-Terphenyl-d14 74.8 29.0-141 01/30/2017 20:38 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 11 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 11 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L886556
TW-3
Collected date/time: 01/25/17 12:30
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 01/30/2017 13:16 WG947436
Metals (ICPMS) by Method 6020
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Antimony U 0.754 2.00 1 02/02/2017 02:22 WG948653
Arsenic U 0.250 2.00 1 02/01/2017 15:11 WG947931
Beryllium U 0.120 2.00 1 02/01/2017 15:11 WG947931
Cadmium U 0.160 1.00 1 02/01/2017 15:11 WG947931
Chromium 0.941 J 0.540 2.00 1 02/01/2017 15:11 WG947931
Copper 1.17 J 0.520 5.00 1 02/01/2017 15:11 WG947931
Lead 0.317 B J 0.240 2.00 1 02/02/2017 01:11 WG947931
Manganese 756 1.25 25.0 5 02/01/2017 16:31 WG947931
Nickel 0.495 B J 0.350 2.00 1 02/01/2017 15:11 WG947931
Selenium U 0.380 2.00 1 02/01/2017 15:11 WG947931
Silver U 0.310 2.00 1 02/01/2017 15:11 WG947931
Thallium U 0.190 2.00 1 02/02/2017 01:11 WG947931
Zinc 10.8 J 2.56 25.0 1 02/01/2017 15:11 WG947931
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 01/31/2017 14:36 WG948128
Acrolein U J4 8.87 50.0 1 01/31/2017 14:36 WG948128
Acrylonitrile U 1.87 10.0 1 01/31/2017 14:36 WG948128
Benzene U 0.331 1.00 1 01/31/2017 14:36 WG948128
Bromobenzene U 0.352 1.00 1 01/31/2017 14:36 WG948128
Bromodichloromethane U 0.380 1.00 1 01/31/2017 14:36 WG948128
Bromoform U 0.469 1.00 1 01/31/2017 14:36 WG948128
Bromomethane U 0.866 5.00 1 01/31/2017 14:36 WG948128
n-Butylbenzene U 0.361 1.00 1 01/31/2017 14:36 WG948128
sec-Butylbenzene U 0.365 1.00 1 01/31/2017 14:36 WG948128
tert-Butylbenzene U 0.399 1.00 1 01/31/2017 14:36 WG948128
Carbon tetrachloride U 0.379 1.00 1 01/31/2017 14:36 WG948128
Chlorobenzene U 0.348 1.00 1 01/31/2017 14:36 WG948128
Chlorodibromomethane U 0.327 1.00 1 01/31/2017 14:36 WG948128
Chloroethane U 0.453 5.00 1 01/31/2017 14:36 WG948128
2-Chloroethyl vinyl ether U 3.01 50.0 1 01/31/2017 14:36 WG948128
Chloroform U 0.324 5.00 1 01/31/2017 14:36 WG948128
Chloromethane U 0.276 2.50 1 01/31/2017 14:36 WG948128
2-Chlorotoluene U 0.375 1.00 1 01/31/2017 14:36 WG948128
4-Chlorotoluene U 0.351 1.00 1 01/31/2017 14:36 WG948128
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 01/31/2017 14:36 WG948128
1,2-Dibromoethane U 0.381 1.00 1 01/31/2017 14:36 WG948128
Dibromomethane U 0.346 1.00 1 01/31/2017 14:36 WG948128
1,2-Dichlorobenzene U 0.349 1.00 1 01/31/2017 14:36 WG948128
1,3-Dichlorobenzene U 0.220 1.00 1 01/31/2017 14:36 WG948128
1,4-Dichlorobenzene U 0.274 1.00 1 01/31/2017 14:36 WG948128
Dichlorodifluoromethane U 0.551 5.00 1 01/31/2017 14:36 WG948128
1,1-Dichloroethane U 0.259 1.00 1 01/31/2017 14:36 WG948128
1,2-Dichloroethane U 0.361 1.00 1 01/31/2017 14:36 WG948128
1,1-Dichloroethene U 0.398 1.00 1 01/31/2017 14:36 WG948128
cis-1,2-Dichloroethene U 0.260 1.00 1 01/31/2017 14:36 WG948128
trans-1,2-Dichloroethene U 0.396 1.00 1 01/31/2017 14:36 WG948128
1,2-Dichloropropane U 0.306 1.00 1 01/31/2017 14:36 WG948128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 12 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 12 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L886556
TW-3
Collected date/time: 01/25/17 12:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1-Dichloropropene U 0.352 1.00 1 01/31/2017 14:36 WG948128
1,3-Dichloropropane U 0.366 1.00 1 01/31/2017 14:36 WG948128
cis-1,3-Dichloropropene U 0.418 1.00 1 01/31/2017 14:36 WG948128
trans-1,3-Dichloropropene U 0.419 1.00 1 01/31/2017 14:36 WG948128
2,2-Dichloropropane U 0.321 1.00 1 01/31/2017 14:36 WG948128
Di-isopropyl ether U 0.320 1.00 1 01/31/2017 14:36 WG948128
Ethylbenzene U 0.384 1.00 1 01/31/2017 14:36 WG948128
Hexachloro-1,3-butadiene U 0.256 1.00 1 01/31/2017 14:36 WG948128
Isopropylbenzene U 0.326 1.00 1 01/31/2017 14:36 WG948128
p-Isopropyltoluene U 0.350 1.00 1 01/31/2017 14:36 WG948128
2-Butanone (MEK)U 3.93 10.0 1 01/31/2017 14:36 WG948128
Methylene Chloride U 1.00 5.00 1 01/31/2017 14:36 WG948128
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 01/31/2017 14:36 WG948128
Methyl tert-butyl ether U 0.367 1.00 1 01/31/2017 14:36 WG948128
Naphthalene U 1.00 5.00 1 01/31/2017 14:36 WG948128
n-Propylbenzene U 0.349 1.00 1 01/31/2017 14:36 WG948128
Styrene U 0.307 1.00 1 01/31/2017 14:36 WG948128
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 01/31/2017 14:36 WG948128
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 01/31/2017 14:36 WG948128
Tetrachloroethene U 0.372 1.00 1 01/31/2017 14:36 WG948128
Toluene U 0.412 1.00 1 01/31/2017 14:36 WG948128
1,2,3-Trichlorobenzene U 0.230 1.00 1 01/31/2017 14:36 WG948128
1,2,4-Trichlorobenzene U 0.355 1.00 1 01/31/2017 14:36 WG948128
1,1,1-Trichloroethane U 0.319 1.00 1 01/31/2017 14:36 WG948128
1,1,2-Trichloroethane U 0.383 1.00 1 01/31/2017 14:36 WG948128
Trichloroethene U 0.398 1.00 1 01/31/2017 14:36 WG948128
Trichlorofluoromethane U 1.20 5.00 1 01/31/2017 14:36 WG948128
1,2,3-Trichloropropane U 0.807 2.50 1 01/31/2017 14:36 WG948128
1,2,4-Trimethylbenzene U 0.373 1.00 1 01/31/2017 14:36 WG948128
1,3,5-Trimethylbenzene U 0.387 1.00 1 01/31/2017 14:36 WG948128
Vinyl chloride U 0.259 1.00 1 01/31/2017 14:36 WG948128
Xylenes, Total U 1.06 3.00 1 01/31/2017 14:36 WG948128
(S) Toluene-d8 96.9 80.0-120 01/31/2017 14:36 WG948128
(S) Dibromofluoromethane 97.4 76.0-123 01/31/2017 14:36 WG948128
(S) a,a,a-Trifluorotoluene 102 80.0-120 01/31/2017 14:36 WG948128
(S) 4-Bromofluorobenzene 101 80.0-120 01/31/2017 14:36 WG948128
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 01/30/2017 21:02 WG947709
Acenaphthylene U 0.309 1.00 1 01/30/2017 21:02 WG947709
Anthracene U 0.291 1.00 1 01/30/2017 21:02 WG947709
Benzidine U 4.32 10.0 1 01/30/2017 21:02 WG947709
Benzo(a)anthracene U 0.0975 1.00 1 01/30/2017 21:02 WG947709
Benzo(b)fluoranthene U 0.0896 1.00 1 01/30/2017 21:02 WG947709
Benzo(k)fluoranthene U 0.355 1.00 1 01/30/2017 21:02 WG947709
Benzo(g,h,i)perylene U 0.161 1.00 1 01/30/2017 21:02 WG947709
Benzo(a)pyrene U 0.340 1.00 1 01/30/2017 21:02 WG947709
Bis(2-chlorethoxy)methane U 0.329 10.0 1 01/30/2017 21:02 WG947709
Bis(2-chloroethyl)ether U 1.62 50.0 1 01/30/2017 21:02 WG947709
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 01/30/2017 21:02 WG947709
4-Bromophenyl-phenylether U 0.335 10.0 1 01/30/2017 21:02 WG947709
2-Chloronaphthalene U 0.330 1.00 1 01/30/2017 21:02 WG947709
4-Chlorophenyl-phenylether U 0.303 10.0 1 01/30/2017 21:02 WG947709
Chrysene U 0.332 1.00 1 01/30/2017 21:02 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 13 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 13 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L886556
TW-3
Collected date/time: 01/25/17 12:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Dibenz(a,h)anthracene U 0.279 1.00 1 01/30/2017 21:02 WG947709
3,3-Dichlorobenzidine U 2.02 10.0 1 01/30/2017 21:02 WG947709
2,4-Dinitrotoluene U 1.65 10.0 1 01/30/2017 21:02 WG947709
2,6-Dinitrotoluene U 0.279 10.0 1 01/30/2017 21:02 WG947709
Fluoranthene U 0.310 1.00 1 01/30/2017 21:02 WG947709
Fluorene U 0.323 1.00 1 01/30/2017 21:02 WG947709
Hexachlorobenzene U 0.341 1.00 1 01/30/2017 21:02 WG947709
Hexachloro-1,3-butadiene U 0.329 10.0 1 01/30/2017 21:02 WG947709
Hexachlorocyclopentadiene U 2.33 10.0 1 01/30/2017 21:02 WG947709
Hexachloroethane U 0.365 10.0 1 01/30/2017 21:02 WG947709
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 01/30/2017 21:02 WG947709
Isophorone U 0.272 10.0 1 01/30/2017 21:02 WG947709
Naphthalene U 0.372 1.00 1 01/30/2017 21:02 WG947709
Nitrobenzene U 0.367 10.0 1 01/30/2017 21:02 WG947709
n-Nitrosodimethylamine U 1.26 10.0 1 01/30/2017 21:02 WG947709
n-Nitrosodiphenylamine U 0.304 10.0 1 01/30/2017 21:02 WG947709
n-Nitrosodi-n-propylamine U 0.403 10.0 1 01/30/2017 21:02 WG947709
Phenanthrene U 0.366 1.00 1 01/30/2017 21:02 WG947709
Benzylbutyl phthalate U 0.275 3.00 1 01/30/2017 21:02 WG947709
Bis(2-ethylhexyl)phthalate 1.19 B J 0.709 3.00 1 01/30/2017 21:02 WG947709
Di-n-butyl phthalate 0.979 B J 0.266 3.00 1 01/30/2017 21:02 WG947709
Diethyl phthalate U 0.282 3.00 1 01/30/2017 21:02 WG947709
Dimethyl phthalate U 0.283 3.00 1 01/30/2017 21:02 WG947709
Di-n-octyl phthalate U 0.278 1.00 1 01/30/2017 21:02 WG947709
Pyrene U 0.330 1.00 1 01/30/2017 21:02 WG947709
1,2,4-Trichlorobenzene U 0.355 10.0 1 01/30/2017 21:02 WG947709
Aniline U 2.43 10.0 1 01/30/2017 21:02 WG947709
4-Chloro-3-methylphenol U 0.263 10.0 1 01/30/2017 21:02 WG947709
2-Chlorophenol U 0.283 10.0 1 01/30/2017 21:02 WG947709
2,4-Dichlorophenol U 0.284 10.0 1 01/30/2017 21:02 WG947709
2,4-Dimethylphenol U 0.264 10.0 1 01/30/2017 21:02 WG947709
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 01/30/2017 21:02 WG947709
2,4-Dinitrophenol U 3.25 10.0 1 01/30/2017 21:02 WG947709
2-Nitrophenol U 0.320 10.0 1 01/30/2017 21:02 WG947709
4-Nitrophenol U 2.01 10.0 1 01/30/2017 21:02 WG947709
Pentachlorophenol U 0.313 10.0 1 01/30/2017 21:02 WG947709
Phenol U 0.334 10.0 1 01/30/2017 21:02 WG947709
2,4,6-Trichlorophenol U 0.297 10.0 1 01/30/2017 21:02 WG947709
(S) 2-Fluorophenol 25.4 10.0-120 01/30/2017 21:02 WG947709
(S) Phenol-d5 16.4 10.0-120 01/30/2017 21:02 WG947709
(S) Nitrobenzene-d5 38.4 10.0-126 01/30/2017 21:02 WG947709
(S) 2-Fluorobiphenyl 54.0 22.0-127 01/30/2017 21:02 WG947709
(S) 2,4,6-Tribromophenol 58.6 10.0-153 01/30/2017 21:02 WG947709
(S) p-Terphenyl-d14 75.4 29.0-141 01/30/2017 21:02 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 14 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 14 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L886556
TW-4
Collected date/time: 01/25/17 13:00
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 01/30/2017 13:18 WG947436
Metals (ICPMS) by Method 6020
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Antimony U 0.754 2.00 1 02/02/2017 02:54 WG948653
Arsenic U 0.250 2.00 1 02/01/2017 15:15 WG947931
Beryllium U 0.120 2.00 1 02/01/2017 15:15 WG947931
Cadmium U 0.160 1.00 1 02/01/2017 15:15 WG947931
Chromium 0.975 J 0.540 2.00 1 02/01/2017 15:15 WG947931
Copper 1.80 J 0.520 5.00 1 02/01/2017 15:15 WG947931
Lead 0.450 B J 0.240 2.00 1 02/02/2017 01:14 WG947931
Manganese 124 0.250 5.00 1 02/01/2017 15:15 WG947931
Nickel 2.72 B 0.350 2.00 1 02/01/2017 15:15 WG947931
Selenium U 0.380 2.00 1 02/01/2017 15:15 WG947931
Silver U 0.310 2.00 1 02/01/2017 15:15 WG947931
Thallium U 0.190 2.00 1 02/02/2017 01:14 WG947931
Zinc 6.22 J 2.56 25.0 1 02/01/2017 15:15 WG947931
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 01/31/2017 14:59 WG948128
Acrolein U J4 8.87 50.0 1 01/31/2017 14:59 WG948128
Acrylonitrile U 1.87 10.0 1 01/31/2017 14:59 WG948128
Benzene U 0.331 1.00 1 01/31/2017 14:59 WG948128
Bromobenzene U 0.352 1.00 1 01/31/2017 14:59 WG948128
Bromodichloromethane 0.447 J 0.380 1.00 1 01/31/2017 14:59 WG948128
Bromoform U 0.469 1.00 1 01/31/2017 14:59 WG948128
Bromomethane U 0.866 5.00 1 01/31/2017 14:59 WG948128
n-Butylbenzene U 0.361 1.00 1 01/31/2017 14:59 WG948128
sec-Butylbenzene U 0.365 1.00 1 01/31/2017 14:59 WG948128
tert-Butylbenzene U 0.399 1.00 1 01/31/2017 14:59 WG948128
Carbon tetrachloride U 0.379 1.00 1 01/31/2017 14:59 WG948128
Chlorobenzene U 0.348 1.00 1 01/31/2017 14:59 WG948128
Chlorodibromomethane U 0.327 1.00 1 01/31/2017 14:59 WG948128
Chloroethane U 0.453 5.00 1 01/31/2017 14:59 WG948128
2-Chloroethyl vinyl ether U 3.01 50.0 1 01/31/2017 14:59 WG948128
Chloroform 7.69 0.324 5.00 1 01/31/2017 14:59 WG948128
Chloromethane U 0.276 2.50 1 01/31/2017 14:59 WG948128
2-Chlorotoluene U 0.375 1.00 1 01/31/2017 14:59 WG948128
4-Chlorotoluene U 0.351 1.00 1 01/31/2017 14:59 WG948128
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 01/31/2017 14:59 WG948128
1,2-Dibromoethane U 0.381 1.00 1 01/31/2017 14:59 WG948128
Dibromomethane U 0.346 1.00 1 01/31/2017 14:59 WG948128
1,2-Dichlorobenzene U 0.349 1.00 1 01/31/2017 14:59 WG948128
1,3-Dichlorobenzene U 0.220 1.00 1 01/31/2017 14:59 WG948128
1,4-Dichlorobenzene U 0.274 1.00 1 01/31/2017 14:59 WG948128
Dichlorodifluoromethane U 0.551 5.00 1 01/31/2017 14:59 WG948128
1,1-Dichloroethane U 0.259 1.00 1 01/31/2017 14:59 WG948128
1,2-Dichloroethane U 0.361 1.00 1 01/31/2017 14:59 WG948128
1,1-Dichloroethene U 0.398 1.00 1 01/31/2017 14:59 WG948128
cis-1,2-Dichloroethene U 0.260 1.00 1 01/31/2017 14:59 WG948128
trans-1,2-Dichloroethene U 0.396 1.00 1 01/31/2017 14:59 WG948128
1,2-Dichloropropane U 0.306 1.00 1 01/31/2017 14:59 WG948128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 15 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 15 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L886556
TW-4
Collected date/time: 01/25/17 13:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1-Dichloropropene U 0.352 1.00 1 01/31/2017 14:59 WG948128
1,3-Dichloropropane U 0.366 1.00 1 01/31/2017 14:59 WG948128
cis-1,3-Dichloropropene U 0.418 1.00 1 01/31/2017 14:59 WG948128
trans-1,3-Dichloropropene U 0.419 1.00 1 01/31/2017 14:59 WG948128
2,2-Dichloropropane U 0.321 1.00 1 01/31/2017 14:59 WG948128
Di-isopropyl ether U 0.320 1.00 1 01/31/2017 14:59 WG948128
Ethylbenzene U 0.384 1.00 1 01/31/2017 14:59 WG948128
Hexachloro-1,3-butadiene U 0.256 1.00 1 01/31/2017 14:59 WG948128
Isopropylbenzene U 0.326 1.00 1 01/31/2017 14:59 WG948128
p-Isopropyltoluene U 0.350 1.00 1 01/31/2017 14:59 WG948128
2-Butanone (MEK)U 3.93 10.0 1 01/31/2017 14:59 WG948128
Methylene Chloride U 1.00 5.00 1 01/31/2017 14:59 WG948128
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 01/31/2017 14:59 WG948128
Methyl tert-butyl ether 7.13 0.367 1.00 1 01/31/2017 14:59 WG948128
Naphthalene U 1.00 5.00 1 01/31/2017 14:59 WG948128
n-Propylbenzene U 0.349 1.00 1 01/31/2017 14:59 WG948128
Styrene U 0.307 1.00 1 01/31/2017 14:59 WG948128
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 01/31/2017 14:59 WG948128
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 01/31/2017 14:59 WG948128
Tetrachloroethene U 0.372 1.00 1 01/31/2017 14:59 WG948128
Toluene U 0.412 1.00 1 01/31/2017 14:59 WG948128
1,2,3-Trichlorobenzene U 0.230 1.00 1 01/31/2017 14:59 WG948128
1,2,4-Trichlorobenzene U 0.355 1.00 1 01/31/2017 14:59 WG948128
1,1,1-Trichloroethane U 0.319 1.00 1 01/31/2017 14:59 WG948128
1,1,2-Trichloroethane U 0.383 1.00 1 01/31/2017 14:59 WG948128
Trichloroethene U 0.398 1.00 1 01/31/2017 14:59 WG948128
Trichlorofluoromethane U 1.20 5.00 1 01/31/2017 14:59 WG948128
1,2,3-Trichloropropane U 0.807 2.50 1 01/31/2017 14:59 WG948128
1,2,4-Trimethylbenzene U 0.373 1.00 1 01/31/2017 14:59 WG948128
1,3,5-Trimethylbenzene U 0.387 1.00 1 01/31/2017 14:59 WG948128
Vinyl chloride U 0.259 1.00 1 01/31/2017 14:59 WG948128
Xylenes, Total U 1.06 3.00 1 01/31/2017 14:59 WG948128
(S) Toluene-d8 97.0 80.0-120 01/31/2017 14:59 WG948128
(S) Dibromofluoromethane 99.8 76.0-123 01/31/2017 14:59 WG948128
(S) a,a,a-Trifluorotoluene 101 80.0-120 01/31/2017 14:59 WG948128
(S) 4-Bromofluorobenzene 99.5 80.0-120 01/31/2017 14:59 WG948128
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 01/30/2017 21:25 WG947709
Acenaphthylene U 0.309 1.00 1 01/30/2017 21:25 WG947709
Anthracene U 0.291 1.00 1 01/30/2017 21:25 WG947709
Benzidine U 4.32 10.0 1 01/30/2017 21:25 WG947709
Benzo(a)anthracene U 0.0975 1.00 1 01/30/2017 21:25 WG947709
Benzo(b)fluoranthene U 0.0896 1.00 1 01/30/2017 21:25 WG947709
Benzo(k)fluoranthene U 0.355 1.00 1 01/30/2017 21:25 WG947709
Benzo(g,h,i)perylene U 0.161 1.00 1 01/30/2017 21:25 WG947709
Benzo(a)pyrene U 0.340 1.00 1 01/30/2017 21:25 WG947709
Bis(2-chlorethoxy)methane U 0.329 10.0 1 01/30/2017 21:25 WG947709
Bis(2-chloroethyl)ether U 1.62 50.0 1 01/30/2017 21:25 WG947709
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 01/30/2017 21:25 WG947709
4-Bromophenyl-phenylether U 0.335 10.0 1 01/30/2017 21:25 WG947709
2-Chloronaphthalene U 0.330 1.00 1 01/30/2017 21:25 WG947709
4-Chlorophenyl-phenylether U 0.303 10.0 1 01/30/2017 21:25 WG947709
Chrysene U 0.332 1.00 1 01/30/2017 21:25 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 16 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 16 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L886556
TW-4
Collected date/time: 01/25/17 13:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Dibenz(a,h)anthracene U 0.279 1.00 1 01/30/2017 21:25 WG947709
3,3-Dichlorobenzidine U 2.02 10.0 1 01/30/2017 21:25 WG947709
2,4-Dinitrotoluene U 1.65 10.0 1 01/30/2017 21:25 WG947709
2,6-Dinitrotoluene U 0.279 10.0 1 01/30/2017 21:25 WG947709
Fluoranthene U 0.310 1.00 1 01/30/2017 21:25 WG947709
Fluorene U 0.323 1.00 1 01/30/2017 21:25 WG947709
Hexachlorobenzene U 0.341 1.00 1 01/30/2017 21:25 WG947709
Hexachloro-1,3-butadiene U 0.329 10.0 1 01/30/2017 21:25 WG947709
Hexachlorocyclopentadiene U 2.33 10.0 1 01/30/2017 21:25 WG947709
Hexachloroethane U 0.365 10.0 1 01/30/2017 21:25 WG947709
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 01/30/2017 21:25 WG947709
Isophorone U 0.272 10.0 1 01/30/2017 21:25 WG947709
Naphthalene U 0.372 1.00 1 01/30/2017 21:25 WG947709
Nitrobenzene U 0.367 10.0 1 01/30/2017 21:25 WG947709
n-Nitrosodimethylamine U 1.26 10.0 1 01/30/2017 21:25 WG947709
n-Nitrosodiphenylamine U 0.304 10.0 1 01/30/2017 21:25 WG947709
n-Nitrosodi-n-propylamine U 0.403 10.0 1 01/30/2017 21:25 WG947709
Phenanthrene U 0.366 1.00 1 01/30/2017 21:25 WG947709
Benzylbutyl phthalate U 0.275 3.00 1 01/30/2017 21:25 WG947709
Bis(2-ethylhexyl)phthalate 1.27 B J 0.709 3.00 1 01/30/2017 21:25 WG947709
Di-n-butyl phthalate 1.01 B J 0.266 3.00 1 01/30/2017 21:25 WG947709
Diethyl phthalate U 0.282 3.00 1 01/30/2017 21:25 WG947709
Dimethyl phthalate U 0.283 3.00 1 01/30/2017 21:25 WG947709
Di-n-octyl phthalate U 0.278 1.00 1 01/30/2017 21:25 WG947709
Pyrene U 0.330 1.00 1 01/30/2017 21:25 WG947709
1,2,4-Trichlorobenzene U 0.355 10.0 1 01/30/2017 21:25 WG947709
Aniline U 2.43 10.0 1 01/30/2017 21:25 WG947709
4-Chloro-3-methylphenol U 0.263 10.0 1 01/30/2017 21:25 WG947709
2-Chlorophenol U 0.283 10.0 1 01/30/2017 21:25 WG947709
2,4-Dichlorophenol U 0.284 10.0 1 01/30/2017 21:25 WG947709
2,4-Dimethylphenol U 0.264 10.0 1 01/30/2017 21:25 WG947709
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 01/30/2017 21:25 WG947709
2,4-Dinitrophenol U 3.25 10.0 1 01/30/2017 21:25 WG947709
2-Nitrophenol U 0.320 10.0 1 01/30/2017 21:25 WG947709
4-Nitrophenol U 2.01 10.0 1 01/30/2017 21:25 WG947709
Pentachlorophenol U 0.313 10.0 1 01/30/2017 21:25 WG947709
Phenol U 0.334 10.0 1 01/30/2017 21:25 WG947709
2,4,6-Trichlorophenol U 0.297 10.0 1 01/30/2017 21:25 WG947709
(S) 2-Fluorophenol 21.0 10.0-120 01/30/2017 21:25 WG947709
(S) Phenol-d5 14.9 10.0-120 01/30/2017 21:25 WG947709
(S) Nitrobenzene-d5 31.0 10.0-126 01/30/2017 21:25 WG947709
(S) 2-Fluorobiphenyl 45.6 22.0-127 01/30/2017 21:25 WG947709
(S) 2,4,6-Tribromophenol 58.3 10.0-153 01/30/2017 21:25 WG947709
(S) p-Terphenyl-d14 69.7 29.0-141 01/30/2017 21:25 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 17 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 17 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L886556
TW-5
Collected date/time: 01/25/17 13:30
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 01/30/2017 13:21 WG947436
Metals (ICPMS) by Method 6020
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Antimony U 0.754 2.00 1 02/02/2017 02:58 WG948653
Arsenic 0.254 J 0.250 2.00 1 02/01/2017 15:18 WG947931
Beryllium 0.123 J 0.120 2.00 1 02/01/2017 15:18 WG947931
Cadmium U 0.160 1.00 1 02/01/2017 15:18 WG947931
Chromium 3.27 0.540 2.00 1 02/01/2017 15:18 WG947931
Copper 15.5 0.520 5.00 1 02/01/2017 15:18 WG947931
Lead 4.37 0.240 2.00 1 02/02/2017 01:18 WG947931
Manganese 193 0.250 5.00 1 02/01/2017 15:18 WG947931
Nickel 3.16 B 0.350 2.00 1 02/01/2017 15:18 WG947931
Selenium 0.386 J 0.380 2.00 1 02/01/2017 15:18 WG947931
Silver U 0.310 2.00 1 02/01/2017 15:18 WG947931
Thallium U 0.190 2.00 1 02/02/2017 01:18 WG947931
Zinc 24.3 J 2.56 25.0 1 02/01/2017 15:18 WG947931
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 01/31/2017 15:22 WG948128
Acrolein U J4 8.87 50.0 1 01/31/2017 15:22 WG948128
Acrylonitrile U 1.87 10.0 1 01/31/2017 15:22 WG948128
Benzene U 0.331 1.00 1 01/31/2017 15:22 WG948128
Bromobenzene U 0.352 1.00 1 01/31/2017 15:22 WG948128
Bromodichloromethane 0.467 J 0.380 1.00 1 01/31/2017 15:22 WG948128
Bromoform U 0.469 1.00 1 01/31/2017 15:22 WG948128
Bromomethane U 0.866 5.00 1 01/31/2017 15:22 WG948128
n-Butylbenzene U 0.361 1.00 1 01/31/2017 15:22 WG948128
sec-Butylbenzene U 0.365 1.00 1 01/31/2017 15:22 WG948128
tert-Butylbenzene U 0.399 1.00 1 01/31/2017 15:22 WG948128
Carbon tetrachloride U 0.379 1.00 1 01/31/2017 15:22 WG948128
Chlorobenzene U 0.348 1.00 1 01/31/2017 15:22 WG948128
Chlorodibromomethane U 0.327 1.00 1 01/31/2017 15:22 WG948128
Chloroethane U 0.453 5.00 1 01/31/2017 15:22 WG948128
2-Chloroethyl vinyl ether U 3.01 50.0 1 01/31/2017 15:22 WG948128
Chloroform 5.52 0.324 5.00 1 01/31/2017 15:22 WG948128
Chloromethane U 0.276 2.50 1 01/31/2017 15:22 WG948128
2-Chlorotoluene U 0.375 1.00 1 01/31/2017 15:22 WG948128
4-Chlorotoluene U 0.351 1.00 1 01/31/2017 15:22 WG948128
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 01/31/2017 15:22 WG948128
1,2-Dibromoethane U 0.381 1.00 1 01/31/2017 15:22 WG948128
Dibromomethane U 0.346 1.00 1 01/31/2017 15:22 WG948128
1,2-Dichlorobenzene U 0.349 1.00 1 01/31/2017 15:22 WG948128
1,3-Dichlorobenzene U 0.220 1.00 1 01/31/2017 15:22 WG948128
1,4-Dichlorobenzene U 0.274 1.00 1 01/31/2017 15:22 WG948128
Dichlorodifluoromethane U 0.551 5.00 1 01/31/2017 15:22 WG948128
1,1-Dichloroethane U 0.259 1.00 1 01/31/2017 15:22 WG948128
1,2-Dichloroethane U 0.361 1.00 1 01/31/2017 15:22 WG948128
1,1-Dichloroethene U 0.398 1.00 1 01/31/2017 15:22 WG948128
cis-1,2-Dichloroethene U 0.260 1.00 1 01/31/2017 15:22 WG948128
trans-1,2-Dichloroethene U 0.396 1.00 1 01/31/2017 15:22 WG948128
1,2-Dichloropropane U 0.306 1.00 1 01/31/2017 15:22 WG948128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 18 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 18 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L886556
TW-5
Collected date/time: 01/25/17 13:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1-Dichloropropene U 0.352 1.00 1 01/31/2017 15:22 WG948128
1,3-Dichloropropane U 0.366 1.00 1 01/31/2017 15:22 WG948128
cis-1,3-Dichloropropene U 0.418 1.00 1 01/31/2017 15:22 WG948128
trans-1,3-Dichloropropene U 0.419 1.00 1 01/31/2017 15:22 WG948128
2,2-Dichloropropane U 0.321 1.00 1 01/31/2017 15:22 WG948128
Di-isopropyl ether 0.340 J 0.320 1.00 1 01/31/2017 15:22 WG948128
Ethylbenzene U 0.384 1.00 1 01/31/2017 15:22 WG948128
Hexachloro-1,3-butadiene U 0.256 1.00 1 01/31/2017 15:22 WG948128
Isopropylbenzene U 0.326 1.00 1 01/31/2017 15:22 WG948128
p-Isopropyltoluene U 0.350 1.00 1 01/31/2017 15:22 WG948128
2-Butanone (MEK)U 3.93 10.0 1 01/31/2017 15:22 WG948128
Methylene Chloride U 1.00 5.00 1 01/31/2017 15:22 WG948128
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 01/31/2017 15:22 WG948128
Methyl tert-butyl ether 23.8 0.367 1.00 1 01/31/2017 15:22 WG948128
Naphthalene U 1.00 5.00 1 01/31/2017 15:22 WG948128
n-Propylbenzene U 0.349 1.00 1 01/31/2017 15:22 WG948128
Styrene U 0.307 1.00 1 01/31/2017 15:22 WG948128
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 01/31/2017 15:22 WG948128
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 01/31/2017 15:22 WG948128
Tetrachloroethene U 0.372 1.00 1 01/31/2017 15:22 WG948128
Toluene U 0.412 1.00 1 01/31/2017 15:22 WG948128
1,2,3-Trichlorobenzene U 0.230 1.00 1 01/31/2017 15:22 WG948128
1,2,4-Trichlorobenzene U 0.355 1.00 1 01/31/2017 15:22 WG948128
1,1,1-Trichloroethane U 0.319 1.00 1 01/31/2017 15:22 WG948128
1,1,2-Trichloroethane U 0.383 1.00 1 01/31/2017 15:22 WG948128
Trichloroethene U 0.398 1.00 1 01/31/2017 15:22 WG948128
Trichlorofluoromethane U 1.20 5.00 1 01/31/2017 15:22 WG948128
1,2,3-Trichloropropane U 0.807 2.50 1 01/31/2017 15:22 WG948128
1,2,4-Trimethylbenzene U 0.373 1.00 1 01/31/2017 15:22 WG948128
1,3,5-Trimethylbenzene U 0.387 1.00 1 01/31/2017 15:22 WG948128
Vinyl chloride U 0.259 1.00 1 01/31/2017 15:22 WG948128
Xylenes, Total U 1.06 3.00 1 01/31/2017 15:22 WG948128
(S) Toluene-d8 95.9 80.0-120 01/31/2017 15:22 WG948128
(S) Dibromofluoromethane 97.6 76.0-123 01/31/2017 15:22 WG948128
(S) a,a,a-Trifluorotoluene 103 80.0-120 01/31/2017 15:22 WG948128
(S) 4-Bromofluorobenzene 100 80.0-120 01/31/2017 15:22 WG948128
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 01/30/2017 21:48 WG947709
Acenaphthylene U 0.309 1.00 1 01/30/2017 21:48 WG947709
Anthracene U 0.291 1.00 1 01/30/2017 21:48 WG947709
Benzidine U 4.32 10.0 1 01/30/2017 21:48 WG947709
Benzo(a)anthracene U 0.0975 1.00 1 01/30/2017 21:48 WG947709
Benzo(b)fluoranthene U 0.0896 1.00 1 01/30/2017 21:48 WG947709
Benzo(k)fluoranthene U 0.355 1.00 1 01/30/2017 21:48 WG947709
Benzo(g,h,i)perylene U 0.161 1.00 1 01/30/2017 21:48 WG947709
Benzo(a)pyrene U 0.340 1.00 1 01/30/2017 21:48 WG947709
Bis(2-chlorethoxy)methane U 0.329 10.0 1 01/30/2017 21:48 WG947709
Bis(2-chloroethyl)ether U 1.62 50.0 1 01/30/2017 21:48 WG947709
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 01/30/2017 21:48 WG947709
4-Bromophenyl-phenylether U 0.335 10.0 1 01/30/2017 21:48 WG947709
2-Chloronaphthalene U 0.330 1.00 1 01/30/2017 21:48 WG947709
4-Chlorophenyl-phenylether U 0.303 10.0 1 01/30/2017 21:48 WG947709
Chrysene U 0.332 1.00 1 01/30/2017 21:48 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 19 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 19 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L886556
TW-5
Collected date/time: 01/25/17 13:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Dibenz(a,h)anthracene U 0.279 1.00 1 01/30/2017 21:48 WG947709
3,3-Dichlorobenzidine U 2.02 10.0 1 01/30/2017 21:48 WG947709
2,4-Dinitrotoluene U 1.65 10.0 1 01/30/2017 21:48 WG947709
2,6-Dinitrotoluene U 0.279 10.0 1 01/30/2017 21:48 WG947709
Fluoranthene U 0.310 1.00 1 01/30/2017 21:48 WG947709
Fluorene U 0.323 1.00 1 01/30/2017 21:48 WG947709
Hexachlorobenzene U 0.341 1.00 1 01/30/2017 21:48 WG947709
Hexachloro-1,3-butadiene U 0.329 10.0 1 01/30/2017 21:48 WG947709
Hexachlorocyclopentadiene U 2.33 10.0 1 01/30/2017 21:48 WG947709
Hexachloroethane U 0.365 10.0 1 01/30/2017 21:48 WG947709
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 01/30/2017 21:48 WG947709
Isophorone U 0.272 10.0 1 01/30/2017 21:48 WG947709
Naphthalene U 0.372 1.00 1 01/30/2017 21:48 WG947709
Nitrobenzene U 0.367 10.0 1 01/30/2017 21:48 WG947709
n-Nitrosodimethylamine U 1.26 10.0 1 01/30/2017 21:48 WG947709
n-Nitrosodiphenylamine U 0.304 10.0 1 01/30/2017 21:48 WG947709
n-Nitrosodi-n-propylamine U 0.403 10.0 1 01/30/2017 21:48 WG947709
Phenanthrene U 0.366 1.00 1 01/30/2017 21:48 WG947709
Benzylbutyl phthalate U 0.275 3.00 1 01/30/2017 21:48 WG947709
Bis(2-ethylhexyl)phthalate 1.25 B J 0.709 3.00 1 01/30/2017 21:48 WG947709
Di-n-butyl phthalate 1.14 B J 0.266 3.00 1 01/30/2017 21:48 WG947709
Diethyl phthalate U 0.282 3.00 1 01/30/2017 21:48 WG947709
Dimethyl phthalate U 0.283 3.00 1 01/30/2017 21:48 WG947709
Di-n-octyl phthalate U 0.278 1.00 1 01/30/2017 21:48 WG947709
Pyrene U 0.330 1.00 1 01/30/2017 21:48 WG947709
1,2,4-Trichlorobenzene U 0.355 10.0 1 01/30/2017 21:48 WG947709
Aniline U 2.43 10.0 1 01/30/2017 21:48 WG947709
4-Chloro-3-methylphenol U 0.263 10.0 1 01/30/2017 21:48 WG947709
2-Chlorophenol U 0.283 10.0 1 01/30/2017 21:48 WG947709
2,4-Dichlorophenol U 0.284 10.0 1 01/30/2017 21:48 WG947709
2,4-Dimethylphenol U 0.264 10.0 1 01/30/2017 21:48 WG947709
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 01/30/2017 21:48 WG947709
2,4-Dinitrophenol U 3.25 10.0 1 01/30/2017 21:48 WG947709
2-Nitrophenol U 0.320 10.0 1 01/30/2017 21:48 WG947709
4-Nitrophenol U 2.01 10.0 1 01/30/2017 21:48 WG947709
Pentachlorophenol U 0.313 10.0 1 01/30/2017 21:48 WG947709
Phenol U 0.334 10.0 1 01/30/2017 21:48 WG947709
2,4,6-Trichlorophenol U 0.297 10.0 1 01/30/2017 21:48 WG947709
(S) 2-Fluorophenol 32.9 10.0-120 01/30/2017 21:48 WG947709
(S) Phenol-d5 22.2 10.0-120 01/30/2017 21:48 WG947709
(S) Nitrobenzene-d5 43.9 10.0-126 01/30/2017 21:48 WG947709
(S) 2-Fluorobiphenyl 60.0 22.0-127 01/30/2017 21:48 WG947709
(S) 2,4,6-Tribromophenol 60.7 10.0-153 01/30/2017 21:48 WG947709
(S) p-Terphenyl-d14 75.0 29.0-141 01/30/2017 21:48 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 20 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 20 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L886556
TW-6
Collected date/time: 01/25/17 14:00
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 01/30/2017 13:23 WG947436
Metals (ICPMS) by Method 6020
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Antimony U 0.754 2.00 1 02/02/2017 03:01 WG948653
Arsenic U 0.250 2.00 1 02/01/2017 15:22 WG947931
Beryllium U 0.120 2.00 1 02/01/2017 15:22 WG947931
Cadmium U 0.160 1.00 1 02/01/2017 15:22 WG947931
Chromium 1.16 J 0.540 2.00 1 02/01/2017 15:22 WG947931
Copper 9.42 0.520 5.00 1 02/01/2017 15:22 WG947931
Lead 1.56 B J 0.240 2.00 1 02/02/2017 01:21 WG947931
Manganese 410 1.25 25.0 5 02/01/2017 16:34 WG947931
Nickel 7.32 0.350 2.00 1 02/01/2017 15:22 WG947931
Selenium 0.741 J 0.380 2.00 1 02/01/2017 15:22 WG947931
Silver U 0.310 2.00 1 02/01/2017 15:22 WG947931
Thallium U 0.190 2.00 1 02/02/2017 01:21 WG947931
Zinc 31.7 2.56 25.0 1 02/01/2017 15:22 WG947931
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 01/31/2017 15:44 WG948128
Acrolein U J4 8.87 50.0 1 01/31/2017 15:44 WG948128
Acrylonitrile U 1.87 10.0 1 01/31/2017 15:44 WG948128
Benzene U 0.331 1.00 1 01/31/2017 15:44 WG948128
Bromobenzene U 0.352 1.00 1 01/31/2017 15:44 WG948128
Bromodichloromethane U 0.380 1.00 1 01/31/2017 15:44 WG948128
Bromoform U 0.469 1.00 1 01/31/2017 15:44 WG948128
Bromomethane U 0.866 5.00 1 01/31/2017 15:44 WG948128
n-Butylbenzene U 0.361 1.00 1 01/31/2017 15:44 WG948128
sec-Butylbenzene U 0.365 1.00 1 01/31/2017 15:44 WG948128
tert-Butylbenzene U 0.399 1.00 1 01/31/2017 15:44 WG948128
Carbon tetrachloride U 0.379 1.00 1 01/31/2017 15:44 WG948128
Chlorobenzene U 0.348 1.00 1 01/31/2017 15:44 WG948128
Chlorodibromomethane U 0.327 1.00 1 01/31/2017 15:44 WG948128
Chloroethane U 0.453 5.00 1 01/31/2017 15:44 WG948128
2-Chloroethyl vinyl ether U 3.01 50.0 1 01/31/2017 15:44 WG948128
Chloroform U 0.324 5.00 1 01/31/2017 15:44 WG948128
Chloromethane U 0.276 2.50 1 01/31/2017 15:44 WG948128
2-Chlorotoluene U 0.375 1.00 1 01/31/2017 15:44 WG948128
4-Chlorotoluene U 0.351 1.00 1 01/31/2017 15:44 WG948128
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 01/31/2017 15:44 WG948128
1,2-Dibromoethane U 0.381 1.00 1 01/31/2017 15:44 WG948128
Dibromomethane U 0.346 1.00 1 01/31/2017 15:44 WG948128
1,2-Dichlorobenzene U 0.349 1.00 1 01/31/2017 15:44 WG948128
1,3-Dichlorobenzene U 0.220 1.00 1 01/31/2017 15:44 WG948128
1,4-Dichlorobenzene U 0.274 1.00 1 01/31/2017 15:44 WG948128
Dichlorodifluoromethane U 0.551 5.00 1 01/31/2017 15:44 WG948128
1,1-Dichloroethane U 0.259 1.00 1 01/31/2017 15:44 WG948128
1,2-Dichloroethane U 0.361 1.00 1 01/31/2017 15:44 WG948128
1,1-Dichloroethene U 0.398 1.00 1 01/31/2017 15:44 WG948128
cis-1,2-Dichloroethene U 0.260 1.00 1 01/31/2017 15:44 WG948128
trans-1,2-Dichloroethene U 0.396 1.00 1 01/31/2017 15:44 WG948128
1,2-Dichloropropane U 0.306 1.00 1 01/31/2017 15:44 WG948128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 21 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 21 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L886556
TW-6
Collected date/time: 01/25/17 14:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1-Dichloropropene U 0.352 1.00 1 01/31/2017 15:44 WG948128
1,3-Dichloropropane U 0.366 1.00 1 01/31/2017 15:44 WG948128
cis-1,3-Dichloropropene U 0.418 1.00 1 01/31/2017 15:44 WG948128
trans-1,3-Dichloropropene U 0.419 1.00 1 01/31/2017 15:44 WG948128
2,2-Dichloropropane U 0.321 1.00 1 01/31/2017 15:44 WG948128
Di-isopropyl ether U 0.320 1.00 1 01/31/2017 15:44 WG948128
Ethylbenzene U 0.384 1.00 1 01/31/2017 15:44 WG948128
Hexachloro-1,3-butadiene U 0.256 1.00 1 01/31/2017 15:44 WG948128
Isopropylbenzene U 0.326 1.00 1 01/31/2017 15:44 WG948128
p-Isopropyltoluene U 0.350 1.00 1 01/31/2017 15:44 WG948128
2-Butanone (MEK)U 3.93 10.0 1 01/31/2017 15:44 WG948128
Methylene Chloride U 1.00 5.00 1 01/31/2017 15:44 WG948128
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 01/31/2017 15:44 WG948128
Methyl tert-butyl ether U 0.367 1.00 1 01/31/2017 15:44 WG948128
Naphthalene U 1.00 5.00 1 01/31/2017 15:44 WG948128
n-Propylbenzene U 0.349 1.00 1 01/31/2017 15:44 WG948128
Styrene U 0.307 1.00 1 01/31/2017 15:44 WG948128
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 01/31/2017 15:44 WG948128
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 01/31/2017 15:44 WG948128
Tetrachloroethene U 0.372 1.00 1 01/31/2017 15:44 WG948128
Toluene U 0.412 1.00 1 01/31/2017 15:44 WG948128
1,2,3-Trichlorobenzene U 0.230 1.00 1 01/31/2017 15:44 WG948128
1,2,4-Trichlorobenzene U 0.355 1.00 1 01/31/2017 15:44 WG948128
1,1,1-Trichloroethane U 0.319 1.00 1 01/31/2017 15:44 WG948128
1,1,2-Trichloroethane U 0.383 1.00 1 01/31/2017 15:44 WG948128
Trichloroethene U 0.398 1.00 1 01/31/2017 15:44 WG948128
Trichlorofluoromethane U 1.20 5.00 1 01/31/2017 15:44 WG948128
1,2,3-Trichloropropane U 0.807 2.50 1 01/31/2017 15:44 WG948128
1,2,4-Trimethylbenzene U 0.373 1.00 1 01/31/2017 15:44 WG948128
1,3,5-Trimethylbenzene U 0.387 1.00 1 01/31/2017 15:44 WG948128
Vinyl chloride U 0.259 1.00 1 01/31/2017 15:44 WG948128
Xylenes, Total U 1.06 3.00 1 01/31/2017 15:44 WG948128
(S) Toluene-d8 96.6 80.0-120 01/31/2017 15:44 WG948128
(S) Dibromofluoromethane 98.5 76.0-123 01/31/2017 15:44 WG948128
(S) a,a,a-Trifluorotoluene 103 80.0-120 01/31/2017 15:44 WG948128
(S) 4-Bromofluorobenzene 99.1 80.0-120 01/31/2017 15:44 WG948128
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 01/30/2017 22:12 WG947709
Acenaphthylene U 0.309 1.00 1 01/30/2017 22:12 WG947709
Anthracene U 0.291 1.00 1 01/30/2017 22:12 WG947709
Benzidine U 4.32 10.0 1 01/30/2017 22:12 WG947709
Benzo(a)anthracene U 0.0975 1.00 1 01/30/2017 22:12 WG947709
Benzo(b)fluoranthene U 0.0896 1.00 1 01/30/2017 22:12 WG947709
Benzo(k)fluoranthene U 0.355 1.00 1 01/30/2017 22:12 WG947709
Benzo(g,h,i)perylene U 0.161 1.00 1 01/30/2017 22:12 WG947709
Benzo(a)pyrene U 0.340 1.00 1 01/30/2017 22:12 WG947709
Bis(2-chlorethoxy)methane U 0.329 10.0 1 01/30/2017 22:12 WG947709
Bis(2-chloroethyl)ether U 1.62 50.0 1 01/30/2017 22:12 WG947709
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 01/30/2017 22:12 WG947709
4-Bromophenyl-phenylether U 0.335 10.0 1 01/30/2017 22:12 WG947709
2-Chloronaphthalene U 0.330 1.00 1 01/30/2017 22:12 WG947709
4-Chlorophenyl-phenylether U 0.303 10.0 1 01/30/2017 22:12 WG947709
Chrysene U 0.332 1.00 1 01/30/2017 22:12 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 22 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 22 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L886556
TW-6
Collected date/time: 01/25/17 14:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Dibenz(a,h)anthracene U 0.279 1.00 1 01/30/2017 22:12 WG947709
3,3-Dichlorobenzidine U 2.02 10.0 1 01/30/2017 22:12 WG947709
2,4-Dinitrotoluene U 1.65 10.0 1 01/30/2017 22:12 WG947709
2,6-Dinitrotoluene U 0.279 10.0 1 01/30/2017 22:12 WG947709
Fluoranthene U 0.310 1.00 1 01/30/2017 22:12 WG947709
Fluorene U 0.323 1.00 1 01/30/2017 22:12 WG947709
Hexachlorobenzene U 0.341 1.00 1 01/30/2017 22:12 WG947709
Hexachloro-1,3-butadiene U 0.329 10.0 1 01/30/2017 22:12 WG947709
Hexachlorocyclopentadiene U 2.33 10.0 1 01/30/2017 22:12 WG947709
Hexachloroethane U 0.365 10.0 1 01/30/2017 22:12 WG947709
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 01/30/2017 22:12 WG947709
Isophorone U 0.272 10.0 1 01/30/2017 22:12 WG947709
Naphthalene U 0.372 1.00 1 01/30/2017 22:12 WG947709
Nitrobenzene U 0.367 10.0 1 01/30/2017 22:12 WG947709
n-Nitrosodimethylamine U 1.26 10.0 1 01/30/2017 22:12 WG947709
n-Nitrosodiphenylamine U 0.304 10.0 1 01/30/2017 22:12 WG947709
n-Nitrosodi-n-propylamine U 0.403 10.0 1 01/30/2017 22:12 WG947709
Phenanthrene U 0.366 1.00 1 01/30/2017 22:12 WG947709
Benzylbutyl phthalate U 0.275 3.00 1 01/30/2017 22:12 WG947709
Bis(2-ethylhexyl)phthalate 1.28 B J 0.709 3.00 1 01/30/2017 22:12 WG947709
Di-n-butyl phthalate 1.26 B J 0.266 3.00 1 01/30/2017 22:12 WG947709
Diethyl phthalate U 0.282 3.00 1 01/30/2017 22:12 WG947709
Dimethyl phthalate U 0.283 3.00 1 01/30/2017 22:12 WG947709
Di-n-octyl phthalate U 0.278 1.00 1 01/30/2017 22:12 WG947709
Pyrene U 0.330 1.00 1 01/30/2017 22:12 WG947709
1,2,4-Trichlorobenzene U 0.355 10.0 1 01/30/2017 22:12 WG947709
Aniline U 2.43 10.0 1 01/30/2017 22:12 WG947709
4-Chloro-3-methylphenol U 0.263 10.0 1 01/30/2017 22:12 WG947709
2-Chlorophenol U 0.283 10.0 1 01/30/2017 22:12 WG947709
2,4-Dichlorophenol U 0.284 10.0 1 01/30/2017 22:12 WG947709
2,4-Dimethylphenol U 0.264 10.0 1 01/30/2017 22:12 WG947709
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 01/30/2017 22:12 WG947709
2,4-Dinitrophenol U 3.25 10.0 1 01/30/2017 22:12 WG947709
2-Nitrophenol U 0.320 10.0 1 01/30/2017 22:12 WG947709
4-Nitrophenol U 2.01 10.0 1 01/30/2017 22:12 WG947709
Pentachlorophenol U 0.313 10.0 1 01/30/2017 22:12 WG947709
Phenol U 0.334 10.0 1 01/30/2017 22:12 WG947709
2,4,6-Trichlorophenol U 0.297 10.0 1 01/30/2017 22:12 WG947709
(S) 2-Fluorophenol 34.2 10.0-120 01/30/2017 22:12 WG947709
(S) Phenol-d5 20.3 10.0-120 01/30/2017 22:12 WG947709
(S) Nitrobenzene-d5 51.7 10.0-126 01/30/2017 22:12 WG947709
(S) 2-Fluorobiphenyl 69.0 22.0-127 01/30/2017 22:12 WG947709
(S) 2,4,6-Tribromophenol 64.2 10.0-153 01/30/2017 22:12 WG947709
(S) p-Terphenyl-d14 72.4 29.0-141 01/30/2017 22:12 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 23 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 23 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L886556
TW-7
Collected date/time: 01/25/17 15:00
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 01/30/2017 13:32 WG947436
Metals (ICPMS) by Method 6020
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Antimony U 0.754 2.00 1 02/02/2017 03:05 WG948653
Arsenic 1.28 J 0.250 2.00 1 02/01/2017 15:25 WG947931
Beryllium 0.775 J 0.120 2.00 1 02/01/2017 15:25 WG947931
Cadmium U 0.160 1.00 1 02/01/2017 15:25 WG947931
Chromium 3.56 0.540 2.00 1 02/01/2017 15:25 WG947931
Copper 22.1 0.520 5.00 1 02/01/2017 15:25 WG947931
Lead 6.86 0.240 2.00 1 02/02/2017 01:25 WG947931
Manganese 607 1.25 25.0 5 02/01/2017 16:38 WG947931
Nickel 9.50 0.350 2.00 1 02/01/2017 15:25 WG947931
Selenium 1.19 J 0.380 2.00 1 02/01/2017 15:25 WG947931
Silver U 0.310 2.00 1 02/01/2017 15:25 WG947931
Thallium 0.212 J 0.190 2.00 1 02/02/2017 01:25 WG947931
Zinc 65.7 2.56 25.0 1 02/01/2017 15:25 WG947931
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 01/31/2017 16:07 WG948128
Acrolein U J4 8.87 50.0 1 01/31/2017 16:07 WG948128
Acrylonitrile U 1.87 10.0 1 01/31/2017 16:07 WG948128
Benzene U 0.331 1.00 1 01/31/2017 16:07 WG948128
Bromobenzene U 0.352 1.00 1 01/31/2017 16:07 WG948128
Bromodichloromethane U 0.380 1.00 1 01/31/2017 16:07 WG948128
Bromoform U 0.469 1.00 1 01/31/2017 16:07 WG948128
Bromomethane U 0.866 5.00 1 01/31/2017 16:07 WG948128
n-Butylbenzene U 0.361 1.00 1 01/31/2017 16:07 WG948128
sec-Butylbenzene U 0.365 1.00 1 01/31/2017 16:07 WG948128
tert-Butylbenzene U 0.399 1.00 1 01/31/2017 16:07 WG948128
Carbon tetrachloride U 0.379 1.00 1 01/31/2017 16:07 WG948128
Chlorobenzene U 0.348 1.00 1 01/31/2017 16:07 WG948128
Chlorodibromomethane U 0.327 1.00 1 01/31/2017 16:07 WG948128
Chloroethane U 0.453 5.00 1 01/31/2017 16:07 WG948128
2-Chloroethyl vinyl ether U 3.01 50.0 1 01/31/2017 16:07 WG948128
Chloroform 1.56 J 0.324 5.00 1 01/31/2017 16:07 WG948128
Chloromethane U 0.276 2.50 1 01/31/2017 16:07 WG948128
2-Chlorotoluene U 0.375 1.00 1 01/31/2017 16:07 WG948128
4-Chlorotoluene U 0.351 1.00 1 01/31/2017 16:07 WG948128
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 01/31/2017 16:07 WG948128
1,2-Dibromoethane U 0.381 1.00 1 01/31/2017 16:07 WG948128
Dibromomethane U 0.346 1.00 1 01/31/2017 16:07 WG948128
1,2-Dichlorobenzene U 0.349 1.00 1 01/31/2017 16:07 WG948128
1,3-Dichlorobenzene U 0.220 1.00 1 01/31/2017 16:07 WG948128
1,4-Dichlorobenzene U 0.274 1.00 1 01/31/2017 16:07 WG948128
Dichlorodifluoromethane U 0.551 5.00 1 01/31/2017 16:07 WG948128
1,1-Dichloroethane U 0.259 1.00 1 01/31/2017 16:07 WG948128
1,2-Dichloroethane U 0.361 1.00 1 01/31/2017 16:07 WG948128
1,1-Dichloroethene U 0.398 1.00 1 01/31/2017 16:07 WG948128
cis-1,2-Dichloroethene U 0.260 1.00 1 01/31/2017 16:07 WG948128
trans-1,2-Dichloroethene U 0.396 1.00 1 01/31/2017 16:07 WG948128
1,2-Dichloropropane U 0.306 1.00 1 01/31/2017 16:07 WG948128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:06 24 of 52
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 24 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L886556
TW-7
Collected date/time: 01/25/17 15:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1-Dichloropropene U 0.352 1.00 1 01/31/2017 16:07 WG948128
1,3-Dichloropropane U 0.366 1.00 1 01/31/2017 16:07 WG948128
cis-1,3-Dichloropropene U 0.418 1.00 1 01/31/2017 16:07 WG948128
trans-1,3-Dichloropropene U 0.419 1.00 1 01/31/2017 16:07 WG948128
2,2-Dichloropropane U 0.321 1.00 1 01/31/2017 16:07 WG948128
Di-isopropyl ether U 0.320 1.00 1 01/31/2017 16:07 WG948128
Ethylbenzene U 0.384 1.00 1 01/31/2017 16:07 WG948128
Hexachloro-1,3-butadiene U 0.256 1.00 1 01/31/2017 16:07 WG948128
Isopropylbenzene U 0.326 1.00 1 01/31/2017 16:07 WG948128
p-Isopropyltoluene U 0.350 1.00 1 01/31/2017 16:07 WG948128
2-Butanone (MEK)U 3.93 10.0 1 01/31/2017 16:07 WG948128
Methylene Chloride U 1.00 5.00 1 01/31/2017 16:07 WG948128
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 01/31/2017 16:07 WG948128
Methyl tert-butyl ether U 0.367 1.00 1 01/31/2017 16:07 WG948128
Naphthalene U 1.00 5.00 1 01/31/2017 16:07 WG948128
n-Propylbenzene U 0.349 1.00 1 01/31/2017 16:07 WG948128
Styrene U 0.307 1.00 1 01/31/2017 16:07 WG948128
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 01/31/2017 16:07 WG948128
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 01/31/2017 16:07 WG948128
Tetrachloroethene U 0.372 1.00 1 01/31/2017 16:07 WG948128
Toluene U 0.412 1.00 1 01/31/2017 16:07 WG948128
1,2,3-Trichlorobenzene U 0.230 1.00 1 01/31/2017 16:07 WG948128
1,2,4-Trichlorobenzene U 0.355 1.00 1 01/31/2017 16:07 WG948128
1,1,1-Trichloroethane U 0.319 1.00 1 01/31/2017 16:07 WG948128
1,1,2-Trichloroethane U 0.383 1.00 1 01/31/2017 16:07 WG948128
Trichloroethene U 0.398 1.00 1 01/31/2017 16:07 WG948128
Trichlorofluoromethane U 1.20 5.00 1 01/31/2017 16:07 WG948128
1,2,3-Trichloropropane U 0.807 2.50 1 01/31/2017 16:07 WG948128
1,2,4-Trimethylbenzene U 0.373 1.00 1 01/31/2017 16:07 WG948128
1,3,5-Trimethylbenzene U 0.387 1.00 1 01/31/2017 16:07 WG948128
Vinyl chloride U 0.259 1.00 1 01/31/2017 16:07 WG948128
Xylenes, Total U 1.06 3.00 1 01/31/2017 16:07 WG948128
(S) Toluene-d8 97.6 80.0-120 01/31/2017 16:07 WG948128
(S) Dibromofluoromethane 98.3 76.0-123 01/31/2017 16:07 WG948128
(S) a,a,a-Trifluorotoluene 104 80.0-120 01/31/2017 16:07 WG948128
(S) 4-Bromofluorobenzene 98.9 80.0-120 01/31/2017 16:07 WG948128
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 01/30/2017 22:35 WG947709
Acenaphthylene U 0.309 1.00 1 01/30/2017 22:35 WG947709
Anthracene U 0.291 1.00 1 01/30/2017 22:35 WG947709
Benzidine U 4.32 10.0 1 01/30/2017 22:35 WG947709
Benzo(a)anthracene U 0.0975 1.00 1 01/30/2017 22:35 WG947709
Benzo(b)fluoranthene U 0.0896 1.00 1 01/30/2017 22:35 WG947709
Benzo(k)fluoranthene U 0.355 1.00 1 01/30/2017 22:35 WG947709
Benzo(g,h,i)perylene U 0.161 1.00 1 01/30/2017 22:35 WG947709
Benzo(a)pyrene U 0.340 1.00 1 01/30/2017 22:35 WG947709
Bis(2-chlorethoxy)methane U 0.329 10.0 1 01/30/2017 22:35 WG947709
Bis(2-chloroethyl)ether U 1.62 50.0 1 01/30/2017 22:35 WG947709
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 01/30/2017 22:35 WG947709
4-Bromophenyl-phenylether U 0.335 10.0 1 01/30/2017 22:35 WG947709
2-Chloronaphthalene U 0.330 1.00 1 01/30/2017 22:35 WG947709
4-Chlorophenyl-phenylether U 0.303 10.0 1 01/30/2017 22:35 WG947709
Chrysene U 0.332 1.00 1 01/30/2017 22:35 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 25 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L886556
TW-7
Collected date/time: 01/25/17 15:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Dibenz(a,h)anthracene U 0.279 1.00 1 01/30/2017 22:35 WG947709
3,3-Dichlorobenzidine U 2.02 10.0 1 01/30/2017 22:35 WG947709
2,4-Dinitrotoluene U 1.65 10.0 1 01/30/2017 22:35 WG947709
2,6-Dinitrotoluene U 0.279 10.0 1 01/30/2017 22:35 WG947709
Fluoranthene U 0.310 1.00 1 01/30/2017 22:35 WG947709
Fluorene U 0.323 1.00 1 01/30/2017 22:35 WG947709
Hexachlorobenzene U 0.341 1.00 1 01/30/2017 22:35 WG947709
Hexachloro-1,3-butadiene U 0.329 10.0 1 01/30/2017 22:35 WG947709
Hexachlorocyclopentadiene U 2.33 10.0 1 01/30/2017 22:35 WG947709
Hexachloroethane U 0.365 10.0 1 01/30/2017 22:35 WG947709
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 01/30/2017 22:35 WG947709
Isophorone U 0.272 10.0 1 01/30/2017 22:35 WG947709
Naphthalene U 0.372 1.00 1 01/30/2017 22:35 WG947709
Nitrobenzene U 0.367 10.0 1 01/30/2017 22:35 WG947709
n-Nitrosodimethylamine U 1.26 10.0 1 01/30/2017 22:35 WG947709
n-Nitrosodiphenylamine U 0.304 10.0 1 01/30/2017 22:35 WG947709
n-Nitrosodi-n-propylamine U 0.403 10.0 1 01/30/2017 22:35 WG947709
Phenanthrene U 0.366 1.00 1 01/30/2017 22:35 WG947709
Benzylbutyl phthalate U 0.275 3.00 1 01/30/2017 22:35 WG947709
Bis(2-ethylhexyl)phthalate 1.19 B J 0.709 3.00 1 01/30/2017 22:35 WG947709
Di-n-butyl phthalate 1.11 B J 0.266 3.00 1 01/30/2017 22:35 WG947709
Diethyl phthalate 0.372 J 0.282 3.00 1 01/30/2017 22:35 WG947709
Dimethyl phthalate U 0.283 3.00 1 01/30/2017 22:35 WG947709
Di-n-octyl phthalate U 0.278 1.00 1 01/30/2017 22:35 WG947709
Pyrene U 0.330 1.00 1 01/30/2017 22:35 WG947709
1,2,4-Trichlorobenzene U 0.355 10.0 1 01/30/2017 22:35 WG947709
Aniline U 2.43 10.0 1 01/30/2017 22:35 WG947709
4-Chloro-3-methylphenol U 0.263 10.0 1 01/30/2017 22:35 WG947709
2-Chlorophenol U 0.283 10.0 1 01/30/2017 22:35 WG947709
2,4-Dichlorophenol U 0.284 10.0 1 01/30/2017 22:35 WG947709
2,4-Dimethylphenol U 0.264 10.0 1 01/30/2017 22:35 WG947709
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 01/30/2017 22:35 WG947709
2,4-Dinitrophenol U 3.25 10.0 1 01/30/2017 22:35 WG947709
2-Nitrophenol U 0.320 10.0 1 01/30/2017 22:35 WG947709
4-Nitrophenol U 2.01 10.0 1 01/30/2017 22:35 WG947709
Pentachlorophenol U 0.313 10.0 1 01/30/2017 22:35 WG947709
Phenol U 0.334 10.0 1 01/30/2017 22:35 WG947709
2,4,6-Trichlorophenol U 0.297 10.0 1 01/30/2017 22:35 WG947709
(S) 2-Fluorophenol 26.9 10.0-120 01/30/2017 22:35 WG947709
(S) Phenol-d5 16.4 10.0-120 01/30/2017 22:35 WG947709
(S) Nitrobenzene-d5 40.7 10.0-126 01/30/2017 22:35 WG947709
(S) 2-Fluorobiphenyl 56.0 22.0-127 01/30/2017 22:35 WG947709
(S) 2,4,6-Tribromophenol 52.0 10.0-153 01/30/2017 22:35 WG947709
(S) p-Terphenyl-d14 65.2 29.0-141 01/30/2017 22:35 WG947709
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 26 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L886556
DUP
Collected date/time: 01/25/17 12:45
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 01/31/2017 17:28 WG948077
Metals (ICPMS) by Method 6020
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Antimony U 0.754 2.00 1 02/02/2017 03:08 WG948653
Arsenic U 0.250 2.00 1 02/01/2017 13:37 WG947931
Beryllium U 0.120 2.00 1 02/01/2017 13:37 WG947931
Cadmium U 0.160 1.00 1 02/01/2017 13:37 WG947931
Chromium 0.791 J 0.540 2.00 1 02/01/2017 13:37 WG947931
Copper 0.611 J 0.520 5.00 1 02/01/2017 13:37 WG947931
Lead U 0.240 2.00 1 02/01/2017 22:18 WG947931
Manganese 731 1.25 25.0 5 02/01/2017 16:41 WG947931
Nickel 0.719 B J 0.350 2.00 1 02/01/2017 13:37 WG947931
Selenium U 0.380 2.00 1 02/01/2017 13:37 WG947931
Silver U 0.310 2.00 1 02/01/2017 13:37 WG947931
Thallium U 0.190 2.00 1 02/01/2017 22:18 WG947931
Zinc 9.03 J 2.56 25.0 1 02/01/2017 13:37 WG947931
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 01/31/2017 16:29 WG948128
Acrolein U J4 8.87 50.0 1 01/31/2017 16:29 WG948128
Acrylonitrile U 1.87 10.0 1 01/31/2017 16:29 WG948128
Benzene U 0.331 1.00 1 01/31/2017 16:29 WG948128
Bromobenzene U 0.352 1.00 1 01/31/2017 16:29 WG948128
Bromodichloromethane U 0.380 1.00 1 01/31/2017 16:29 WG948128
Bromoform U 0.469 1.00 1 01/31/2017 16:29 WG948128
Bromomethane U 0.866 5.00 1 01/31/2017 16:29 WG948128
n-Butylbenzene U 0.361 1.00 1 01/31/2017 16:29 WG948128
sec-Butylbenzene U 0.365 1.00 1 01/31/2017 16:29 WG948128
tert-Butylbenzene U 0.399 1.00 1 01/31/2017 16:29 WG948128
Carbon tetrachloride U 0.379 1.00 1 01/31/2017 16:29 WG948128
Chlorobenzene U 0.348 1.00 1 01/31/2017 16:29 WG948128
Chlorodibromomethane U 0.327 1.00 1 01/31/2017 16:29 WG948128
Chloroethane U 0.453 5.00 1 01/31/2017 16:29 WG948128
2-Chloroethyl vinyl ether U 3.01 50.0 1 01/31/2017 16:29 WG948128
Chloroform U 0.324 5.00 1 01/31/2017 16:29 WG948128
Chloromethane U 0.276 2.50 1 01/31/2017 16:29 WG948128
2-Chlorotoluene U 0.375 1.00 1 01/31/2017 16:29 WG948128
4-Chlorotoluene U 0.351 1.00 1 01/31/2017 16:29 WG948128
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 01/31/2017 16:29 WG948128
1,2-Dibromoethane U 0.381 1.00 1 01/31/2017 16:29 WG948128
Dibromomethane U 0.346 1.00 1 01/31/2017 16:29 WG948128
1,2-Dichlorobenzene U 0.349 1.00 1 01/31/2017 16:29 WG948128
1,3-Dichlorobenzene U 0.220 1.00 1 01/31/2017 16:29 WG948128
1,4-Dichlorobenzene U 0.274 1.00 1 01/31/2017 16:29 WG948128
Dichlorodifluoromethane U 0.551 5.00 1 01/31/2017 16:29 WG948128
1,1-Dichloroethane U 0.259 1.00 1 01/31/2017 16:29 WG948128
1,2-Dichloroethane U 0.361 1.00 1 01/31/2017 16:29 WG948128
1,1-Dichloroethene U 0.398 1.00 1 01/31/2017 16:29 WG948128
cis-1,2-Dichloroethene U 0.260 1.00 1 01/31/2017 16:29 WG948128
trans-1,2-Dichloroethene U 0.396 1.00 1 01/31/2017 16:29 WG948128
1,2-Dichloropropane U 0.306 1.00 1 01/31/2017 16:29 WG948128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 27 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L886556
DUP
Collected date/time: 01/25/17 12:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1-Dichloropropene U 0.352 1.00 1 01/31/2017 16:29 WG948128
1,3-Dichloropropane U 0.366 1.00 1 01/31/2017 16:29 WG948128
cis-1,3-Dichloropropene U 0.418 1.00 1 01/31/2017 16:29 WG948128
trans-1,3-Dichloropropene U 0.419 1.00 1 01/31/2017 16:29 WG948128
2,2-Dichloropropane U 0.321 1.00 1 01/31/2017 16:29 WG948128
Di-isopropyl ether U 0.320 1.00 1 01/31/2017 16:29 WG948128
Ethylbenzene U 0.384 1.00 1 01/31/2017 16:29 WG948128
Hexachloro-1,3-butadiene U 0.256 1.00 1 01/31/2017 16:29 WG948128
Isopropylbenzene U 0.326 1.00 1 01/31/2017 16:29 WG948128
p-Isopropyltoluene U 0.350 1.00 1 01/31/2017 16:29 WG948128
2-Butanone (MEK)U 3.93 10.0 1 01/31/2017 16:29 WG948128
Methylene Chloride U 1.00 5.00 1 01/31/2017 16:29 WG948128
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 01/31/2017 16:29 WG948128
Methyl tert-butyl ether U 0.367 1.00 1 01/31/2017 16:29 WG948128
Naphthalene U 1.00 5.00 1 01/31/2017 16:29 WG948128
n-Propylbenzene U 0.349 1.00 1 01/31/2017 16:29 WG948128
Styrene U 0.307 1.00 1 01/31/2017 16:29 WG948128
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 01/31/2017 16:29 WG948128
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 01/31/2017 16:29 WG948128
Tetrachloroethene U 0.372 1.00 1 01/31/2017 16:29 WG948128
Toluene U 0.412 1.00 1 01/31/2017 16:29 WG948128
1,2,3-Trichlorobenzene U 0.230 1.00 1 01/31/2017 16:29 WG948128
1,2,4-Trichlorobenzene U 0.355 1.00 1 01/31/2017 16:29 WG948128
1,1,1-Trichloroethane U 0.319 1.00 1 01/31/2017 16:29 WG948128
1,1,2-Trichloroethane U 0.383 1.00 1 01/31/2017 16:29 WG948128
Trichloroethene U 0.398 1.00 1 01/31/2017 16:29 WG948128
Trichlorofluoromethane U 1.20 5.00 1 01/31/2017 16:29 WG948128
1,2,3-Trichloropropane U 0.807 2.50 1 01/31/2017 16:29 WG948128
1,2,4-Trimethylbenzene U 0.373 1.00 1 01/31/2017 16:29 WG948128
1,3,5-Trimethylbenzene U 0.387 1.00 1 01/31/2017 16:29 WG948128
Vinyl chloride U 0.259 1.00 1 01/31/2017 16:29 WG948128
Xylenes, Total U 1.06 3.00 1 01/31/2017 16:29 WG948128
(S) Toluene-d8 97.3 80.0-120 01/31/2017 16:29 WG948128
(S) Dibromofluoromethane 98.5 76.0-123 01/31/2017 16:29 WG948128
(S) a,a,a-Trifluorotoluene 103 80.0-120 01/31/2017 16:29 WG948128
(S) 4-Bromofluorobenzene 100 80.0-120 01/31/2017 16:29 WG948128
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 01/31/2017 16:48 WG947935
Acenaphthylene U 0.309 1.00 1 01/31/2017 16:48 WG947935
Anthracene U 0.291 1.00 1 01/31/2017 16:48 WG947935
Benzidine U 4.32 10.0 1 01/31/2017 16:48 WG947935
Benzo(a)anthracene U 0.0975 1.00 1 01/31/2017 16:48 WG947935
Benzo(b)fluoranthene U 0.0896 1.00 1 01/31/2017 16:48 WG947935
Benzo(k)fluoranthene U 0.355 1.00 1 01/31/2017 16:48 WG947935
Benzo(g,h,i)perylene U 0.161 1.00 1 01/31/2017 16:48 WG947935
Benzo(a)pyrene U 0.340 1.00 1 01/31/2017 16:48 WG947935
Bis(2-chlorethoxy)methane U 0.329 10.0 1 01/31/2017 16:48 WG947935
Bis(2-chloroethyl)ether U 1.62 10.0 1 01/31/2017 16:48 WG947935
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 01/31/2017 16:48 WG947935
4-Bromophenyl-phenylether U 0.335 10.0 1 01/31/2017 16:48 WG947935
2-Chloronaphthalene U 0.330 1.00 1 01/31/2017 16:48 WG947935
4-Chlorophenyl-phenylether U 0.303 10.0 1 01/31/2017 16:48 WG947935
Chrysene U 0.332 1.00 1 01/31/2017 16:48 WG947935
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 28 of 52
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L886556
DUP
Collected date/time: 01/25/17 12:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Dibenz(a,h)anthracene U 0.279 1.00 1 01/31/2017 16:48 WG947935
3,3-Dichlorobenzidine U 2.02 10.0 1 01/31/2017 16:48 WG947935
2,4-Dinitrotoluene U 1.65 10.0 1 01/31/2017 16:48 WG947935
2,6-Dinitrotoluene U 0.279 10.0 1 01/31/2017 16:48 WG947935
Fluoranthene U 0.310 1.00 1 01/31/2017 16:48 WG947935
Fluorene U 0.323 1.00 1 01/31/2017 16:48 WG947935
Hexachlorobenzene U 0.341 1.00 1 01/31/2017 16:48 WG947935
Hexachloro-1,3-butadiene U 0.329 10.0 1 01/31/2017 16:48 WG947935
Hexachlorocyclopentadiene U 2.33 10.0 1 01/31/2017 16:48 WG947935
Hexachloroethane U 0.365 10.0 1 01/31/2017 16:48 WG947935
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 01/31/2017 16:48 WG947935
Isophorone U 0.272 10.0 1 01/31/2017 16:48 WG947935
Naphthalene U 0.372 1.00 1 01/31/2017 16:48 WG947935
Nitrobenzene U 0.367 10.0 1 01/31/2017 16:48 WG947935
n-Nitrosodimethylamine U 1.26 10.0 1 01/31/2017 16:48 WG947935
n-Nitrosodiphenylamine U 0.304 10.0 1 01/31/2017 16:48 WG947935
n-Nitrosodi-n-propylamine U 0.403 10.0 1 01/31/2017 16:48 WG947935
Phenanthrene U 0.366 1.00 1 01/31/2017 16:48 WG947935
Benzylbutyl phthalate U 0.275 3.00 1 01/31/2017 16:48 WG947935
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 01/31/2017 16:48 WG947935
Di-n-butyl phthalate 0.645 B J 0.266 3.00 1 01/31/2017 16:48 WG947935
Diethyl phthalate U 0.282 3.00 1 01/31/2017 16:48 WG947935
Dimethyl phthalate U 0.283 3.00 1 01/31/2017 16:48 WG947935
Di-n-octyl phthalate U 0.278 1.00 1 01/31/2017 16:48 WG947935
Pyrene U 0.330 1.00 1 01/31/2017 16:48 WG947935
1,2,4-Trichlorobenzene U 0.355 10.0 1 01/31/2017 16:48 WG947935
Aniline U 2.43 10.0 1 01/31/2017 16:48 WG947935
4-Chloro-3-methylphenol U 0.263 10.0 1 01/31/2017 16:48 WG947935
2-Chlorophenol U 0.283 10.0 1 01/31/2017 16:48 WG947935
2,4-Dichlorophenol U 0.284 10.0 1 01/31/2017 16:48 WG947935
2,4-Dimethylphenol U 0.264 10.0 1 01/31/2017 16:48 WG947935
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 01/31/2017 16:48 WG947935
2,4-Dinitrophenol U 3.25 10.0 1 01/31/2017 16:48 WG947935
2-Nitrophenol U 0.320 10.0 1 01/31/2017 16:48 WG947935
4-Nitrophenol U 2.01 10.0 1 01/31/2017 16:48 WG947935
Pentachlorophenol U 0.313 10.0 1 01/31/2017 16:48 WG947935
Phenol U 0.334 10.0 1 01/31/2017 16:48 WG947935
2,4,6-Trichlorophenol U 0.297 10.0 1 01/31/2017 16:48 WG947935
(S) 2-Fluorophenol 58.8 10.0-120 01/31/2017 16:48 WG947935
(S) Phenol-d5 40.5 10.0-120 01/31/2017 16:48 WG947935
(S) Nitrobenzene-d5 70.4 10.0-126 01/31/2017 16:48 WG947935
(S) 2-Fluorobiphenyl 91.0 22.0-127 01/31/2017 16:48 WG947935
(S) 2,4,6-Tribromophenol 87.7 10.0-153 01/31/2017 16:48 WG947935
(S) p-Terphenyl-d14 109 29.0-141 01/31/2017 16:48 WG947935
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947436
Mercury by Method 7470A L886556-01,02,03,04,05,06,07
Method Blank (MB)
(MB) R3193625-1 01/30/17 11:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.0490 0.200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3193625-2 01/30/17 11:18 • (LCSD) R3193625-4 01/30/17 11:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Mercury 3.00 3.04 2.93 101 98 80-120 4 20
L886510-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886510-03 01/30/17 11:30 • (MS) R3193625-6 01/30/17 11:35 • (MSD) R3193625-8 01/30/17 11:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 2.91 2.97 97 99 1 75-125 2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 30 of 52
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948077
Mercury by Method 7470A L886556-08
Method Blank (MB)
(MB) R3193906-1 01/31/17 17:21
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.0490 0.200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3193906-2 01/31/17 17:23 • (LCSD) R3193906-3 01/31/17 17:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Mercury 3.00 3.06 3.23 102 108 80-120 5 20
L886556-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886556-08 01/31/17 17:28 • (MS) R3193906-4 01/31/17 17:30 • (MSD) R3193906-5 01/31/17 17:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 3.11 3.03 104 101 1 75-125 3 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947931
Metals (ICPMS) by Method 6020 L886556-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3194149-1 02/01/17 13:26
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Arsenic U 0.250 2.00
Beryllium U 0.120 2.00
Cadmium U 0.160 1.00
Chromium U 0.540 2.00
Copper U 0.520 5.00
Manganese U 0.250 5.00
Nickel 0.496 J 0.350 2.00
Selenium U 0.380 2.00
Silver U 0.310 2.00
Zinc U 2.56 25.0
Method Blank (MB)
(MB) R3194149-9 02/01/17 22:07
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Lead 0.319 J 0.240 2.00
Thallium U 0.190 2.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194149-7 02/01/17 15:31 • (LCSD) R3194149-8 02/01/17 15:35
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Arsenic 50.0 42.4 42.0 85 84 80-120 1 20
Beryllium 50.0 43.7 43.9 87 88 80-120 0 20
Cadmium 50.0 47.8 47.4 96 95 80-120 1 20
Chromium 50.0 44.8 44.9 90 90 80-120 0 20
Copper 50.0 48.4 48.7 97 97 80-120 1 20
Manganese 50.0 42.2 42.0 84 84 80-120 0 20
Nickel 50.0 46.8 47.5 94 95 80-120 1 20
Selenium 50.0 42.5 43.2 85 86 80-120 2 20
Silver 50.0 44.1 44.4 88 89 80-120 1 20
Zinc 50.0 44.9 45.5 90 91 80-120 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947931
Metals (ICPMS) by Method 6020 L886556-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194149-10 02/01/17 22:11 • (LCSD) R3194149-11 02/01/17 22:14
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Lead 50.0 49.5 49.4 99 99 80-120 0 20
Thallium 50.0 48.6 48.6 97 97 80-120 0 20
L886556-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886556-08 02/01/17 13:37 • (MS) R3194149-5 02/01/17 13:44 • (MSD) R3194149-6 02/01/17 13:47
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 50.0 U 43.1 43.0 86 86 1 75-125 0 20
Beryllium 50.0 U 42.2 41.8 84 84 1 75-125 1 20
Cadmium 50.0 U 47.0 46.0 94 92 1 75-125 2 20
Chromium 50.0 0.791 45.2 44.9 89 88 1 75-125 1 20
Copper 50.0 0.611 47.9 47.0 95 93 1 75-125 2 20
Manganese 50.0 679 716 711 73 63 1 75-125 V V 1 20
Nickel 50.0 0.719 46.5 45.9 92 90 1 75-125 1 20
Selenium 50.0 U 44.7 44.9 89 90 1 75-125 0 20
Silver 50.0 U 44.7 44.7 89 89 1 75-125 0 20
Zinc 50.0 9.03 52.4 51.7 87 85 1 75-125 1 20
L886556-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886556-08 02/01/17 22:18 • (MS) R3194149-13 02/01/17 22:25 • (MSD) R3194149-14 02/01/17 22:28
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Lead 50.0 U 49.7 49.8 99 100 1 75-125 0 20
Thallium 50.0 U 49.2 49.5 98 99 1 75-125 1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948653
Metals (ICPMS) by Method 6020 L886556-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3194262-1 02/02/17 02:11
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Antimony U 0.754 2.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194262-2 02/02/17 02:15 • (LCSD) R3194262-3 02/02/17 02:18
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Antimony 57.9 54.0 53.6 93 93 80-120 1 20
L886556-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886556-03 02/02/17 02:22 • (MS) R3194262-5 02/02/17 02:29 • (MSD) R3194262-6 02/02/17 02:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Antimony 57.9 U 53.6 53.7 93 93 1 75-125 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948128
Volatile Organic Compounds (GC/MS) by Method 8260B L886556-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3194436-3 01/31/17 11:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 10.0 50.0
Acrolein U 8.87 50.0
Acrylonitrile U 1.87 10.0
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride U 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
2-Chloroethyl vinyl ether U 3.01 50.0
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
cis-1,3-Dichloropropene U 0.418 1.00
trans-1,3-Dichloropropene U 0.419 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948128
Volatile Organic Compounds (GC/MS) by Method 8260B L886556-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3194436-3 01/31/17 11:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Hexachloro-1,3-butadiene U 0.256 1.00
Isopropylbenzene U 0.326 1.00
p-Isopropyltoluene U 0.350 1.00
2-Butanone (MEK)U 3.93 10.0
Methylene Chloride U 1.00 5.00
4-Methyl-2-pentanone (MIBK) U 2.14 10.0
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.349 1.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
Trichloroethene U 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Vinyl chloride U 0.259 1.00
Xylenes, Total U 1.06 3.00
(S) Toluene-d8 97.7 80.0-120
(S) Dibromofluoromethane 100 76.0-123
(S) a,a,a-Trifluorotoluene 102 80.0-120
(S) 4-Bromofluorobenzene 103 80.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194436-1 01/31/17 10:16 • (LCSD) R3194436-2 01/31/17 10:38
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 125 129 126 103 101 10.0-160 2.68 23
Acrolein 125 226 226 181 181 10.0-160 J4 J4 0.0700 20
Acrylonitrile 125 119 111 95.2 89.0 60.0-142 6.69 20
Benzene 25.0 22.5 22.8 89.9 91.2 69.0-123 1.36 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948128
Volatile Organic Compounds (GC/MS) by Method 8260B L886556-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194436-1 01/31/17 10:16 • (LCSD) R3194436-2 01/31/17 10:38
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromobenzene 25.0 24.6 23.8 98.5 95.3 79.0-120 3.30 20
Bromodichloromethane 25.0 22.6 22.1 90.3 88.2 76.0-120 2.32 20
Bromoform 25.0 26.1 24.9 105 99.7 67.0-132 4.75 20
Bromomethane 25.0 19.3 17.6 77.1 70.4 18.0-160 9.14 20
n-Butylbenzene 25.0 23.4 23.9 93.7 95.5 72.0-126 1.82 20
sec-Butylbenzene 25.0 25.7 25.3 103 101 74.0-121 1.59 20
tert-Butylbenzene 25.0 26.3 25.5 105 102 75.0-122 2.89 20
Carbon tetrachloride 25.0 21.2 22.4 84.8 89.7 63.0-122 5.69 20
Chlorobenzene 25.0 26.8 26.5 107 106 79.0-121 1.26 20
Chlorodibromomethane 25.0 26.5 26.4 106 106 75.0-125 0.380 20
Chloroethane 25.0 18.5 18.7 73.9 75.0 47.0-152 1.50 20
2-Chloroethyl vinyl ether 125 124 119 99.2 95.0 10.0-160 4.35 22
Chloroform 25.0 22.3 22.5 89.3 89.9 72.0-121 0.730 20
Chloromethane 25.0 15.9 15.9 63.8 63.5 48.0-139 0.420 20
2-Chlorotoluene 25.0 25.9 25.3 104 101 74.0-122 2.16 20
4-Chlorotoluene 25.0 25.9 25.1 103 100 79.0-120 2.95 20
1,2-Dibromo-3-Chloropropane 25.0 20.7 20.3 82.6 81.1 64.0-127 1.84 20
1,2-Dibromoethane 25.0 25.9 25.9 104 103 77.0-123 0.170 20
Dibromomethane 25.0 23.8 24.1 95.1 96.6 78.0-120 1.56 20
1,2-Dichlorobenzene 25.0 25.0 25.3 99.9 101 80.0-120 1.19 20
1,3-Dichlorobenzene 25.0 26.2 25.1 105 100 72.0-123 4.23 20
1,4-Dichlorobenzene 25.0 23.8 24.4 95.1 97.6 77.0-120 2.61 20
Dichlorodifluoromethane 25.0 22.6 22.8 90.5 91.3 49.0-155 0.900 20
1,1-Dichloroethane 25.0 22.1 22.6 88.4 90.4 70.0-126 2.27 20
1,2-Dichloroethane 25.0 20.7 21.2 82.7 85.0 67.0-126 2.77 20
1,1-Dichloroethene 25.0 21.2 22.0 84.8 88.2 64.0-129 3.95 20
cis-1,2-Dichloroethene 25.0 22.3 23.9 89.2 95.4 73.0-120 6.73 20
trans-1,2-Dichloroethene 25.0 22.4 23.5 89.6 93.9 71.0-121 4.71 20
1,2-Dichloropropane 25.0 22.4 22.7 89.6 90.8 75.0-125 1.23 20
1,1-Dichloropropene 25.0 22.3 23.1 89.2 92.4 71.0-129 3.61 20
1,3-Dichloropropane 25.0 26.0 25.7 104 103 80.0-121 1.02 20
cis-1,3-Dichloropropene 25.0 22.3 22.7 89.2 90.8 79.0-123 1.72 20
trans-1,3-Dichloropropene 25.0 23.5 22.8 94.1 91.2 74.0-127 3.20 20
2,2-Dichloropropane 25.0 20.7 21.1 82.6 84.5 60.0-125 2.19 20
Di-isopropyl ether 25.0 19.5 20.1 78.2 80.3 59.0-133 2.67 20
Ethylbenzene 25.0 25.8 25.6 103 102 77.0-120 0.830 20
Hexachloro-1,3-butadiene 25.0 23.0 24.3 91.9 97.2 64.0-131 5.57 20
Isopropylbenzene 25.0 25.2 24.9 101 99.6 75.0-120 1.20 20
p-Isopropyltoluene 25.0 26.1 25.6 104 102 74.0-126 2.07 20
2-Butanone (MEK)125 123 119 98.1 95.4 37.0-158 2.75 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948128
Volatile Organic Compounds (GC/MS) by Method 8260B L886556-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194436-1 01/31/17 10:16 • (LCSD) R3194436-2 01/31/17 10:38
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Methylene Chloride 25.0 21.7 22.2 86.9 88.9 66.0-121 2.32 20
4-Methyl-2-pentanone (MIBK) 125 109 105 87.4 83.9 59.0-143 4.04 20
Methyl tert-butyl ether 25.0 20.8 20.8 83.3 83.1 64.0-123 0.180 20
Naphthalene 25.0 20.2 20.6 80.8 82.4 62.0-128 1.91 20
n-Propylbenzene 25.0 25.6 25.2 102 101 79.0-120 1.75 20
Styrene 25.0 26.1 25.8 105 103 78.0-124 1.18 20
1,1,1,2-Tetrachloroethane 25.0 25.8 25.4 103 102 75.0-122 1.38 20
1,1,2,2-Tetrachloroethane 25.0 24.3 23.2 97.1 92.6 71.0-122 4.65 20
Tetrachloroethene 25.0 26.9 26.9 108 108 70.0-127 0.100 20
Toluene 25.0 22.7 23.0 91.0 91.9 77.0-120 1.02 20
1,2,3-Trichlorobenzene 25.0 21.6 22.9 86.5 91.8 61.0-133 5.94 20
1,2,4-Trichlorobenzene 25.0 23.6 24.1 94.3 96.6 69.0-129 2.37 20
1,1,1-Trichloroethane 25.0 22.0 22.0 88.0 88.1 68.0-122 0.160 20
1,1,2-Trichloroethane 25.0 25.7 24.9 103 99.7 78.0-120 3.20 20
Trichloroethene 25.0 24.4 24.7 97.6 99.0 78.0-120 1.37 20
Trichlorofluoromethane 25.0 22.7 23.2 91.0 92.9 56.0-137 2.07 20
1,2,3-Trichloropropane 25.0 26.3 25.5 105 102 72.0-124 2.77 20
1,2,4-Trimethylbenzene 25.0 24.8 24.2 99.3 96.9 75.0-120 2.38 20
1,3,5-Trimethylbenzene 25.0 24.7 24.1 98.9 96.4 75.0-120 2.53 20
Vinyl chloride 25.0 20.3 20.6 81.1 82.5 64.0-133 1.80 20
Xylenes, Total 75.0 76.4 74.9 102 99.8 77.0-120 1.98 20
(S) Toluene-d8 98.1 97.6 80.0-120
(S) Dibromofluoromethane 94.3 96.4 76.0-123
(S) a,a,a-Trifluorotoluene 103 103 80.0-120
(S) 4-Bromofluorobenzene 103 100 80.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947709
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D L886556-01,02,03,04,05,06,07
Method Blank (MB)
(MB) R3193734-3 01/30/17 14:50
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Aniline U 2.43 10.0
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroethyl)ether U 1.62 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 0.304 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate 1.28 J 0.709 3.00
Di-n-butyl phthalate 1.18 J 0.266 3.00
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947709
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D L886556-01,02,03,04,05,06,07
Method Blank (MB)
(MB) R3193734-3 01/30/17 14:50
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Di-n-octyl phthalate U 0.278 1.00
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
4-Chloro-3-methylphenol U 0.263 10.0
2-Chlorophenol U 0.283 10.0
2,4-Dichlorophenol U 0.284 10.0
2,4-Dimethylphenol U 0.264 10.0
4,6-Dinitro-2-methylphenol U 2.62 10.0
2,4-Dinitrophenol U 3.25 10.0
2-Nitrophenol U 0.320 10.0
4-Nitrophenol U 2.01 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 0.334 10.0
2,4,6-Trichlorophenol U 0.297 10.0
(S) Nitrobenzene-d5 50.6 10.0-126
(S) 2-Fluorobiphenyl 64.6 22.0-127
(S) p-Terphenyl-d14 73.4 29.0-141
(S) Phenol-d5 19.2 10.0-120
(S) 2-Fluorophenol 30.4 10.0-120
(S) 2,4,6-Tribromophenol 62.8 10.0-153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3193734-1 01/30/17 14:04 • (LCSD) R3193734-2 01/30/17 14:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 32.3 34.9 64.6 69.7 42.0-120 7.58 22
Acenaphthylene 50.0 35.2 38.1 70.4 76.2 43.0-120 8.01 22
Aniline 50.0 26.6 27.4 53.2 54.8 10.0-120 2.99 25
Anthracene 50.0 34.7 37.4 69.4 74.8 44.0-120 7.52 20
Benzidine 50.0 26.4 34.2 52.9 68.5 1.00-120 25.7 36
Benzo(a)anthracene 50.0 32.8 36.1 65.6 72.1 44.0-120 9.44 20
Benzo(b)fluoranthene 50.0 33.3 34.9 66.6 69.8 40.0-120 4.79 21
Benzo(k)fluoranthene 50.0 33.3 37.7 66.5 75.4 41.0-120 12.5 22
Benzo(g,h,i)perylene 50.0 35.4 38.6 70.9 77.2 45.0-121 8.48 20
Benzo(a)pyrene 50.0 35.6 38.6 71.2 77.1 41.0-120 7.89 20
Bis(2-chlorethoxy)methane 50.0 28.0 29.8 56.0 59.6 36.0-120 6.24 25
Bis(2-chloroethyl)ether 50.0 25.4 26.3 50.8 52.6 24.0-120 3.52 29
Bis(2-chloroisopropyl)ether 50.0 30.5 31.7 61.0 63.4 32.0-120 3.89 29
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947709
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D L886556-01,02,03,04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3193734-1 01/30/17 14:04 • (LCSD) R3193734-2 01/30/17 14:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
4-Bromophenyl-phenylether 50.0 35.3 37.9 70.7 75.8 42.0-121 7.05 21
2-Chloronaphthalene 50.0 31.7 33.3 63.4 66.6 37.0-120 4.91 24
4-Chlorophenyl-phenylether 50.0 34.6 37.7 69.2 75.5 44.0-120 8.63 21
Chrysene 50.0 32.8 36.1 65.5 72.2 45.0-120 9.71 20
Dibenz(a,h)anthracene 50.0 36.0 39.4 72.0 78.8 44.0-121 9.01 21
3,3-Dichlorobenzidine 50.0 54.8 63.3 110 127 29.0-153 14.3 23
2,4-Dinitrotoluene 50.0 37.0 40.5 74.0 80.9 47.0-127 8.99 21
2,6-Dinitrotoluene 50.0 33.4 36.9 66.9 73.9 42.0-120 9.96 22
Fluoranthene 50.0 37.1 40.1 74.3 80.1 46.0-121 7.56 20
Fluorene 50.0 35.2 38.8 70.5 77.6 45.0-120 9.67 21
Hexachlorobenzene 50.0 37.5 39.3 75.0 78.6 41.0-124 4.68 21
Hexachloro-1,3-butadiene 50.0 29.3 29.5 58.7 59.0 26.0-120 0.600 31
Hexachlorocyclopentadiene 50.0 29.0 31.1 58.1 62.1 10.0-120 6.74 31
Hexachloroethane 50.0 25.9 26.9 51.9 53.9 22.0-120 3.79 34
Indeno(1,2,3-cd)pyrene 50.0 36.7 39.7 73.4 79.5 45.0-123 7.98 21
Isophorone 50.0 29.2 31.7 58.4 63.3 37.0-120 8.08 24
Naphthalene 50.0 26.9 28.2 53.7 56.3 33.0-120 4.74 28
Nitrobenzene 50.0 26.1 27.4 52.1 54.8 31.0-120 5.10 28
n-Nitrosodimethylamine 50.0 14.1 14.0 28.2 28.0 10.0-120 0.440 34
n-Nitrosodiphenylamine 50.0 34.3 36.6 68.6 73.2 44.0-120 6.48 21
n-Nitrosodi-n-propylamine 50.0 31.3 33.0 62.7 66.0 29.0-120 5.10 27
Phenanthrene 50.0 32.4 34.2 64.9 68.4 42.0-120 5.22 20
Benzylbutyl phthalate 50.0 29.8 32.9 59.6 65.8 36.0-123 9.87 22
Bis(2-ethylhexyl)phthalate 50.0 30.0 32.7 60.0 65.3 37.0-121 8.51 21
Di-n-butyl phthalate 50.0 32.6 35.6 65.2 71.2 43.0-122 8.87 21
Diethyl phthalate 50.0 36.5 39.4 72.9 78.8 48.0-123 7.76 20
Dimethyl phthalate 50.0 34.7 37.7 69.3 75.4 47.0-120 8.36 20
Di-n-octyl phthalate 50.0 29.9 32.6 59.8 65.3 38.0-120 8.83 22
Pyrene 50.0 33.0 35.6 66.0 71.2 43.0-120 7.68 21
1,2,4-Trichlorobenzene 50.0 27.4 28.8 54.8 57.6 29.0-120 5.03 29
4-Chloro-3-methylphenol 50.0 29.4 31.2 58.8 62.4 39.0-120 5.94 22
2-Chlorophenol 50.0 27.3 28.2 54.7 56.3 28.0-120 3.01 29
2,4-Dichlorophenol 50.0 30.5 32.5 61.0 65.1 37.0-120 6.54 26
2,4-Dimethylphenol 50.0 27.8 29.5 55.7 59.1 35.0-120 5.91 25
4,6-Dinitro-2-methylphenol 50.0 34.4 35.5 68.9 70.9 34.0-125 2.91 27
2,4-Dinitrophenol 50.0 19.4 18.9 38.7 37.9 10.0-120 2.26 40
2-Nitrophenol 50.0 31.1 32.4 62.1 64.8 35.0-120 4.11 28
4-Nitrophenol 50.0 12.8 13.4 25.6 26.9 10.0-120 4.92 35
Pentachlorophenol 50.0 29.0 30.5 57.9 61.0 20.0-126 5.21 32
Phenol 50.0 10.9 11.4 21.8 22.8 10.0-120 4.51 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947709
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D L886556-01,02,03,04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3193734-1 01/30/17 14:04 • (LCSD) R3193734-2 01/30/17 14:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
2,4,6-Trichlorophenol 50.0 33.5 35.7 67.0 71.4 40.0-122 6.38 24
(S) Nitrobenzene-d5 53.3 55.1 10.0-126
(S) 2-Fluorobiphenyl 70.3 75.0 22.0-127
(S) p-Terphenyl-d14 76.1 81.0 29.0-141
(S) Phenol-d5 23.9 24.8 10.0-120
(S) 2-Fluorophenol 37.5 36.8 10.0-120
(S) 2,4,6-Tribromophenol 85.8 90.8 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947935
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D L886556-08
Method Blank (MB)
(MB) R3194044-3 01/31/17 13:17
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Aniline U 2.43 10.0
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroethyl)ether U 1.62 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 0.304 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate 0.696 J 0.266 3.00
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947935
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D L886556-08
Method Blank (MB)
(MB) R3194044-3 01/31/17 13:17
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Di-n-octyl phthalate U 0.278 1.00
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
4-Chloro-3-methylphenol U 0.263 10.0
2-Chlorophenol U 0.283 10.0
2,4-Dichlorophenol U 0.284 10.0
2,4-Dimethylphenol U 0.264 10.0
4,6-Dinitro-2-methylphenol U 2.62 10.0
2,4-Dinitrophenol U 3.25 10.0
2-Nitrophenol U 0.320 10.0
4-Nitrophenol U 2.01 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 0.334 10.0
2,4,6-Trichlorophenol U 0.297 10.0
(S) Nitrobenzene-d5 72.4 10.0-126
(S) 2-Fluorobiphenyl 87.6 22.0-127
(S) p-Terphenyl-d14 113 29.0-141
(S) Phenol-d5 45.5 10.0-120
(S) 2-Fluorophenol 60.3 10.0-120
(S) 2,4,6-Tribromophenol 80.3 10.0-153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194044-1 01/31/17 12:31 • (LCSD) R3194044-2 01/31/17 12:54
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzidine 50.0 28.4 30.1 56.9 60.2 1.00-120 5.69 36
Acenaphthene 50.0 43.2 45.8 86.4 91.7 42.0-120 5.88 22
Acenaphthylene 50.0 47.0 50.8 94.0 102 43.0-120 7.64 22
Aniline 50.0 30.8 34.6 61.6 69.3 10.0-120 11.7 25
Anthracene 50.0 45.1 48.3 90.2 96.6 44.0-120 6.93 20
Benzo(a)anthracene 50.0 45.0 46.3 90.0 92.7 44.0-120 2.98 20
Benzo(b)fluoranthene 50.0 48.2 49.4 96.3 98.8 40.0-120 2.49 21
Benzo(k)fluoranthene 50.0 46.9 48.3 93.8 96.5 41.0-120 2.92 22
Benzo(g,h,i)perylene 50.0 50.7 52.4 101 105 45.0-121 3.20 20
Benzo(a)pyrene 50.0 47.9 49.3 95.7 98.7 41.0-120 3.03 20
Bis(2-chlorethoxy)methane 50.0 37.6 40.7 75.3 81.5 36.0-120 7.96 25
Bis(2-chloroethyl)ether 50.0 37.1 40.7 74.3 81.4 24.0-120 9.12 29
Bis(2-chloroisopropyl)ether 50.0 35.9 40.0 71.8 80.0 32.0-120 10.8 29
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947935
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D L886556-08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194044-1 01/31/17 12:31 • (LCSD) R3194044-2 01/31/17 12:54
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
4-Bromophenyl-phenylether 50.0 46.5 51.1 93.0 102 42.0-121 9.39 21
2-Chloronaphthalene 50.0 43.4 47.3 86.9 94.5 37.0-120 8.43 24
4-Chlorophenyl-phenylether 50.0 50.4 53.7 101 107 44.0-120 6.17 21
Chrysene 50.0 48.1 49.9 96.1 99.7 45.0-120 3.67 20
Dibenz(a,h)anthracene 50.0 49.8 51.5 99.6 103 44.0-121 3.36 21
3,3-Dichlorobenzidine 50.0 54.7 57.4 109 115 29.0-153 4.82 23
2,4-Dinitrotoluene 50.0 52.1 54.5 104 109 47.0-127 4.48 21
2,6-Dinitrotoluene 50.0 46.6 50.5 93.1 101 42.0-120 8.06 22
Fluoranthene 50.0 50.8 53.4 102 107 46.0-121 4.99 20
Fluorene 50.0 47.2 50.5 94.3 101 45.0-120 6.78 21
Hexachlorobenzene 50.0 49.1 52.2 98.2 104 41.0-124 6.24 21
Hexachloro-1,3-butadiene 50.0 39.2 42.2 78.4 84.3 26.0-120 7.34 31
Hexachlorocyclopentadiene 50.0 50.5 56.7 101 113 10.0-120 11.5 31
Hexachloroethane 50.0 34.6 37.4 69.2 74.9 22.0-120 7.82 34
Indeno(1,2,3-cd)pyrene 50.0 50.8 52.7 102 105 45.0-123 3.77 21
Isophorone 50.0 38.8 42.0 77.5 84.1 37.0-120 8.09 24
Naphthalene 50.0 33.9 36.3 67.8 72.7 33.0-120 6.91 28
Nitrobenzene 50.0 35.6 39.1 71.1 78.3 31.0-120 9.58 28
n-Nitrosodimethylamine 50.0 20.0 21.4 39.9 42.8 10.0-120 7.04 34
n-Nitrosodiphenylamine 50.0 43.7 46.8 87.3 93.6 44.0-120 6.95 21
n-Nitrosodi-n-propylamine 50.0 36.8 40.5 73.6 80.9 29.0-120 9.47 27
Phenanthrene 50.0 44.4 47.2 88.7 94.5 42.0-120 6.24 20
Benzylbutyl phthalate 50.0 43.9 45.6 87.8 91.2 36.0-123 3.80 22
Bis(2-ethylhexyl)phthalate 50.0 42.9 44.5 85.9 89.0 37.0-121 3.62 21
Di-n-butyl phthalate 50.0 47.2 49.7 94.5 99.4 43.0-122 5.05 21
Diethyl phthalate 50.0 49.9 52.7 99.7 105 48.0-123 5.50 20
Dimethyl phthalate 50.0 49.5 53.2 99.0 106 47.0-120 7.20 20
Di-n-octyl phthalate 50.0 44.7 46.3 89.5 92.5 38.0-120 3.33 22
Pyrene 50.0 45.3 46.9 90.7 93.8 43.0-120 3.37 21
1,2,4-Trichlorobenzene 50.0 36.0 39.1 72.0 78.2 29.0-120 8.27 29
4-Chloro-3-methylphenol 50.0 38.5 40.2 77.0 80.5 39.0-120 4.45 22
2-Chlorophenol 50.0 32.4 37.4 64.9 74.7 28.0-120 14.1 29
2,4-Dichlorophenol 50.0 40.2 42.7 80.4 85.4 37.0-120 6.03 26
2,4-Dimethylphenol 50.0 36.2 38.8 72.4 77.7 35.0-120 7.03 25
4,6-Dinitro-2-methylphenol 50.0 50.1 52.5 100 105 34.0-125 4.63 27
2,4-Dinitrophenol 50.0 43.9 47.7 87.8 95.3 10.0-120 8.17 40
2-Nitrophenol 50.0 38.1 41.9 76.2 83.8 35.0-120 9.48 28
4-Nitrophenol 50.0 26.1 28.4 52.1 56.9 10.0-120 8.74 35
Pentachlorophenol 50.0 39.6 41.2 79.2 82.4 20.0-126 3.91 32
Phenol 50.0 21.6 23.7 43.2 47.5 10.0-120 9.38 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947935
Semi Volatile Organic Compounds (GC/MS) by Method 8270 D L886556-08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194044-1 01/31/17 12:31 • (LCSD) R3194044-2 01/31/17 12:54
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
2,4,6-Trichlorophenol 50.0 50.8 54.9 102 110 40.0-122 7.78 24
(S) Nitrobenzene-d5 78.0 77.3 10.0-126
(S) 2-Fluorobiphenyl 104 103 22.0-127
(S) p-Terphenyl-d14 120 108 29.0-141
(S) Phenol-d5 51.0 51.2 10.0-120
(S) 2-Fluorophenol 66.6 65.1 10.0-120
(S) 2,4,6-Tribromophenol 114 113 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886556 02/21/17 17:16 48 of 52
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886556-01
Withers & Ravenel Eng. - Standard
1/25/2017
1/30/2017
WATER
0130_21
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-1
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886556-02
Withers & Ravenel Eng. - Standard
1/25/2017
1/30/2017
WATER
0130_22
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-2
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886556-03
Withers & Ravenel Eng. - Standard
1/25/2017
1/30/2017
WATER
0130_23
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-3
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886556-04
Withers & Ravenel Eng. - Standard
1/25/2017
1/30/2017
WATER
0130_24
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-4
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886556-05
Withers & Ravenel Eng. - Standard
1/25/2017
1/30/2017
WATER
0130_25
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-5
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886556-06
Withers & Ravenel Eng. - Standard
1/25/2017
1/30/2017
WATER
0130_26
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-6
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886556-07
Withers & Ravenel Eng. - Standard
1/25/2017
1/30/2017
WATER
0130_27
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-7
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886556-08
Withers & Ravenel Eng. - Standard
1/25/2017
1/31/2017
WATER
0131_22
1.00
mg/l 1
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
DUP
Project Desc.Pilot Mt. Brownfields
Butane, 2-methoxy-2-methyl-000994-05-8 2.70 J 90.001.03
Page 1 of 1SVOC TIC Report
ANALYTICAL REPORT
February 22, 2017
Withers & Ravenel Eng. - Standard
Sample Delivery Group:L886597
Samples Received:01/27/2017
Project Number:02090017.20
Description:Pilot Mt. Brownfields
Report To:Mark Brown
115 MacKenan Drive
Cary, NC 27511
Entire Report Reviewed By:
February 22, 2017
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
February 22, 2017
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 7
⁵Sr: Sample Results 8
BG-1 L886597-01 8
BG-2 L886597-02 11
B-1 L886597-03 14
B-5 L886597-04 17
B-7 L886597-05 20
B-8 L886597-06 23
B-9 L886597-07 26
B-10 L886597-08 29
B-11 L886597-09 32
B-12 L886597-10 35
B-13 L886597-11 38
B-14 L886597-12 41
B-15 L886597-13 44
B-16 L886597-14 47
DUPE L886597-15 50
TW-2 L886597-16 53
TW-4 L886597-17 56
TW-5 L886597-18 59
TW-6 L886597-19 62
TW-7 L886597-20 65
⁶Qc: Quality Control Summary 68
Total Solids by Method 2540 G-2011 68
Mercury by Method 7471A 70
Metals (ICPMS) by Method 6020 72
Volatile Organic Compounds (GC/MS) by Method 8260B 74
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 86
⁷Gl: Glossary of Terms 91
⁸Al: Accreditations & Locations 92
⁹Sc: Chain of Custody 93
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 2 of 97
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 2 of 97
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
BG-1 L886597-01 Solid Austin Pote 01/24/17 09:10 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:21 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:28 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 18:41 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/28/17 23:37 01/31/17 21:41 GLN
Collected by Collected date/time Received date/time
BG-2 L886597-02 Solid Austin Pote 01/24/17 09:20 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:24 JDG
Metals (ICPMS) by Method 6020 WG948015 20 01/31/17 22:34 02/04/17 12:55 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:31 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 19:07 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/28/17 23:37 01/31/17 22:29 GLN
Collected by Collected date/time Received date/time
B-1 L886597-03 Solid Austin Pote 01/24/17 10:10 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:26 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:35 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 19:58 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/24/17 10:10 01/31/17 22:51 GLN
Collected by Collected date/time Received date/time
B-5 L886597-04 Solid Austin Pote 01/24/17 09:30 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 11:50 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:39 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 14:49 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/24/17 09:30 01/31/17 23:13 GLN
Collected by Collected date/time Received date/time
B-7 L886597-05 Solid Austin Pote 01/24/17 15:30 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:29 JDG
Metals (ICPMS) by Method 6020 WG948015 10 01/31/17 22:34 02/04/17 12:58 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:42 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 13:31 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1.17 01/24/17 15:30 01/31/17 23:36 GLN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 3 of 97
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 3 of 97
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
B-8 L886597-06 Solid Austin Pote 01/24/17 14:45 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:31 JDG
Metals (ICPMS) by Method 6020 WG948015 10 01/31/17 22:34 02/04/17 13:02 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:46 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 15:15 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/24/17 14:45 01/31/17 23:59 GLN
Collected by Collected date/time Received date/time
B-9 L886597-07 Solid Austin Pote 01/24/17 14:10 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:34 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:49 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 17:24 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1.01 01/24/17 14:10 02/01/17 00:21 GLN
Collected by Collected date/time Received date/time
B-10 L886597-08 Solid Austin Pote 01/25/17 09:45 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:37 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:53 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 20 02/01/17 10:04 02/03/17 17:14 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/25/17 09:45 02/01/17 00:44 GLN
Collected by Collected date/time Received date/time
B-11 L886597-09 Solid Austin Pote 01/25/17 10:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:39 JDG
Metals (ICPMS) by Method 6020 WG948015 10 01/31/17 22:34 02/04/17 13:05 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 15:56 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 20:50 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/25/17 10:00 02/01/17 01:07 GLN
Collected by Collected date/time Received date/time
B-12 L886597-10 Solid Austin Pote 01/24/17 10:30 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:47 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:00 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 15:41 JF
Total Solids by Method 2540 G-2011 WG948070 1 01/31/17 10:20 01/31/17 10:31 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/24/17 10:30 02/01/17 01:30 GLN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 4 of 97
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 4 of 97
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
B-13 L886597-11 Solid Austin Pote 01/24/17 10:40 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:49 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:13 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 18:15 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/24/17 10:40 02/01/17 01:52 GLN
Collected by Collected date/time Received date/time
B-14 L886597-12 Solid Austin Pote 01/25/17 09:30 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:52 JDG
Metals (ICPMS) by Method 6020 WG948015 10 01/31/17 22:34 02/04/17 13:09 JDG
Metals (ICPMS) by Method 6020 WG948015 20 01/31/17 22:34 02/04/17 13:37 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:16 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 22:07 JF
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 10 02/01/17 10:04 02/03/17 17:40 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1 01/25/17 09:30 02/01/17 02:14 GLN
Collected by Collected date/time Received date/time
B-15 L886597-13 Solid Austin Pote 01/25/17 08:50 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:55 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:20 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 16:06 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1.07 01/25/17 08:50 02/01/17 02:37 GLN
Collected by Collected date/time Received date/time
B-16 L886597-14 Solid Austin Pote 01/25/17 08:30 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG947435 1 01/27/17 20:45 01/30/17 12:57 JDG
Metals (ICPMS) by Method 6020 WG948015 100 01/31/17 22:34 02/04/17 13:12 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:23 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 21:41 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1.03 01/25/17 08:30 01/31/17 20:33 GLN
Collected by Collected date/time Received date/time
DUPE L886597-15 Solid Austin Pote 01/25/17 08:45 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG948080 1 01/31/17 11:02 02/01/17 10:23 JDG
Metals (ICPMS) by Method 6020 WG948015 10 01/31/17 22:34 02/04/17 13:16 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:27 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 16:32 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG947760 1.03 01/25/17 08:45 02/01/17 02:59 GLN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 5 of 97
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TW-2 L886597-16 Solid Austin Pote 01/25/17 00:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG948080 1 01/31/17 11:02 02/01/17 10:25 JDG
Metals (ICPMS) by Method 6020 WG948015 20 01/31/17 22:34 02/04/17 13:19 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:30 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 20:24 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG948235 1 01/25/17 00:00 02/01/17 03:00 GLN
Collected by Collected date/time Received date/time
TW-4 L886597-17 Solid Austin Pote 01/25/17 00:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG948080 1 01/31/17 11:02 02/01/17 10:28 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:34 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 16:58 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG948235 1 01/25/17 00:00 02/01/17 03:21 GLN
Collected by Collected date/time Received date/time
TW-5 L886597-18 Solid Austin Pote 01/25/17 00:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG948080 1 01/31/17 11:02 02/01/17 10:36 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:38 JDG
Metals (ICPMS) by Method 6020 WG948015 50 01/31/17 22:34 02/04/17 13:23 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 17:49 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG948235 1 01/25/17 00:00 02/01/17 03:41 GLN
Collected by Collected date/time Received date/time
TW-6 L886597-19 Solid Austin Pote 01/25/17 00:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG948080 1 01/31/17 11:02 02/01/17 10:38 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 16:41 JDG
Metals (ICPMS) by Method 6020 WG948015 50 01/31/17 22:34 02/04/17 13:26 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 19:33 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG948235 1 01/25/17 00:00 02/01/17 04:02 GLN
Collected by Collected date/time Received date/time
TW-7 L886597-20 Solid Austin Pote 01/25/17 00:00 01/27/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7471A WG948080 1 01/31/17 11:02 02/01/17 10:13 JDG
Metals (ICPMS) by Method 6020 WG948015 10 01/31/17 22:34 02/03/17 16:45 JDG
Metals (ICPMS) by Method 6020 WG948015 5 01/31/17 22:34 02/03/17 14:17 JDG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG947910 1 02/01/17 10:04 02/02/17 21:15 JF
Total Solids by Method 2540 G-2011 WG948071 1 01/31/17 10:06 01/31/17 10:16 MEL
Volatile Organic Compounds (GC/MS) by Method 8260B WG948235 1 01/25/17 00:00 02/01/17 04:23 GLN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 7 of 97
Jimmy Hunt
Technical Service Representative
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L886597
BG-1
Collected date/time: 01/24/17 09:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 72.7 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0624 0.00385 0.0275 1 01/30/2017 12:21 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony 0.315 J 0.217 0.687 5 02/03/2017 15:28 WG948015
Arsenic 4.71 0.0172 0.687 5 02/03/2017 15:28 WG948015
Beryllium 0.382 J 0.0825 0.687 5 02/03/2017 15:28 WG948015
Cadmium U 0.110 0.687 5 02/03/2017 15:28 WG948015
Chromium 24.2 0.371 0.687 5 02/03/2017 15:28 WG948015
Copper 11.4 0.357 0.687 5 02/03/2017 15:28 WG948015
Lead 19.3 0.165 0.687 5 02/03/2017 15:28 WG948015
Manganese 77.1 0.172 1.37 5 02/03/2017 15:28 WG948015
Nickel 3.80 0.241 0.687 5 02/03/2017 15:28 WG948015
Selenium 1.49 0.261 0.687 5 02/03/2017 15:28 WG948015
Silver U 0.213 0.687 5 02/03/2017 15:28 WG948015
Thallium 0.317 J 0.131 0.687 5 02/03/2017 15:28 WG948015
Zinc 20.3 1.76 6.87 5 02/03/2017 15:28 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0172 J 0.0137 0.0687 1 01/31/2017 21:41 WG947760
Acrylonitrile U 0.00246 0.0137 1 01/31/2017 21:41 WG947760
Benzene U 0.000371 0.00137 1 01/31/2017 21:41 WG947760
Bromobenzene U 0.000390 0.00137 1 01/31/2017 21:41 WG947760
Bromodichloromethane U 0.000349 0.00137 1 01/31/2017 21:41 WG947760
Bromoform U 0.000583 0.00137 1 01/31/2017 21:41 WG947760
Bromomethane U 0.00184 0.00687 1 01/31/2017 21:41 WG947760
n-Butylbenzene U 0.000355 0.00137 1 01/31/2017 21:41 WG947760
sec-Butylbenzene U 0.000276 0.00137 1 01/31/2017 21:41 WG947760
tert-Butylbenzene U 0.000283 0.00137 1 01/31/2017 21:41 WG947760
Carbon tetrachloride U 0.000451 0.00137 1 01/31/2017 21:41 WG947760
Chlorobenzene U 0.000291 0.00137 1 01/31/2017 21:41 WG947760
Chlorodibromomethane U 0.000513 0.00137 1 01/31/2017 21:41 WG947760
Chloroethane U 0.00130 0.00687 1 01/31/2017 21:41 WG947760
2-Chloroethyl vinyl ether U 0.00322 0.0687 1 01/31/2017 21:41 WG947760
Chloroform U 0.000315 0.00687 1 01/31/2017 21:41 WG947760
Chloromethane U 0.000515 0.00344 1 01/31/2017 21:41 WG947760
2-Chlorotoluene U 0.000414 0.00137 1 01/31/2017 21:41 WG947760
4-Chlorotoluene U 0.000330 0.00137 1 01/31/2017 21:41 WG947760
1,2-Dibromo-3-Chloropropane U 0.00144 0.00687 1 01/31/2017 21:41 WG947760
1,2-Dibromoethane U 0.000471 0.00137 1 01/31/2017 21:41 WG947760
Dibromomethane U 0.000525 0.00137 1 01/31/2017 21:41 WG947760
1,2-Dichlorobenzene U 0.000419 0.00137 1 01/31/2017 21:41 WG947760
1,3-Dichlorobenzene U 0.000329 0.00137 1 01/31/2017 21:41 WG947760
1,4-Dichlorobenzene U 0.000311 0.00137 1 01/31/2017 21:41 WG947760
Dichlorodifluoromethane U 0.000980 0.00687 1 01/31/2017 21:41 WG947760
1,1-Dichloroethane U 0.000274 0.00137 1 01/31/2017 21:41 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L886597
BG-1
Collected date/time: 01/24/17 09:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000364 0.00137 1 01/31/2017 21:41 WG947760
1,1-Dichloroethene U 0.000416 0.00137 1 01/31/2017 21:41 WG947760
cis-1,2-Dichloroethene U 0.000323 0.00137 1 01/31/2017 21:41 WG947760
trans-1,2-Dichloroethene U 0.000363 0.00137 1 01/31/2017 21:41 WG947760
1,2-Dichloropropane U 0.000492 0.00137 1 01/31/2017 21:41 WG947760
1,1-Dichloropropene U 0.000436 0.00137 1 01/31/2017 21:41 WG947760
1,3-Dichloropropane U 0.000285 0.00137 1 01/31/2017 21:41 WG947760
cis-1,3-Dichloropropene U 0.000360 0.00137 1 01/31/2017 21:41 WG947760
trans-1,3-Dichloropropene U 0.000367 0.00137 1 01/31/2017 21:41 WG947760
2,2-Dichloropropane U 0.000384 0.00137 1 01/31/2017 21:41 WG947760
Di-isopropyl ether U 0.000341 0.00137 1 01/31/2017 21:41 WG947760
Ethylbenzene U 0.000408 0.00137 1 01/31/2017 21:41 WG947760
Hexachloro-1,3-butadiene U 0.000470 0.00137 1 01/31/2017 21:41 WG947760
Isopropylbenzene U 0.000334 0.00137 1 01/31/2017 21:41 WG947760
p-Isopropyltoluene U 0.000280 0.00137 1 01/31/2017 21:41 WG947760
2-Butanone (MEK)U 0.00643 0.0137 1 01/31/2017 21:41 WG947760
Methylene Chloride U 0.00137 0.00687 1 01/31/2017 21:41 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00258 0.0137 1 01/31/2017 21:41 WG947760
Methyl tert-butyl ether U 0.000291 0.00137 1 01/31/2017 21:41 WG947760
Naphthalene U 0.00137 0.00687 1 01/31/2017 21:41 WG947760
n-Propylbenzene U 0.000283 0.00137 1 01/31/2017 21:41 WG947760
Styrene U 0.000322 0.00137 1 01/31/2017 21:41 WG947760
1,1,1,2-Tetrachloroethane U 0.000363 0.00137 1 01/31/2017 21:41 WG947760
1,1,2,2-Tetrachloroethane U 0.000502 0.00137 1 01/31/2017 21:41 WG947760
Tetrachloroethene U 0.000379 0.00137 1 01/31/2017 21:41 WG947760
Toluene U 0.000597 0.00687 1 01/31/2017 21:41 WG947760
1,2,3-Trichlorobenzene U 0.000421 0.00137 1 01/31/2017 21:41 WG947760
1,2,4-Trichlorobenzene U 0.000533 0.00137 1 01/31/2017 21:41 WG947760
1,1,1-Trichloroethane U 0.000393 0.00137 1 01/31/2017 21:41 WG947760
1,1,2-Trichloroethane U 0.000381 0.00137 1 01/31/2017 21:41 WG947760
Trichloroethene U 0.000384 0.00137 1 01/31/2017 21:41 WG947760
Trichlorofluoromethane U 0.000525 0.00687 1 01/31/2017 21:41 WG947760
1,2,3-Trichloropropane U 0.00102 0.00344 1 01/31/2017 21:41 WG947760
1,2,4-Trimethylbenzene U 0.000290 0.00137 1 01/31/2017 21:41 WG947760
1,3,5-Trimethylbenzene U 0.000366 0.00137 1 01/31/2017 21:41 WG947760
Vinyl chloride U 0.000400 0.00137 1 01/31/2017 21:41 WG947760
Xylenes, Total U 0.000959 0.00412 1 01/31/2017 21:41 WG947760
(S) Toluene-d8 107 80.0-120 01/31/2017 21:41 WG947760
(S) Dibromofluoromethane 104 74.0-131 01/31/2017 21:41 WG947760
(S) a,a,a-Trifluorotoluene 103 80.0-120 01/31/2017 21:41 WG947760
(S) 4-Bromofluorobenzene 101 64.0-132 01/31/2017 21:41 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00882 0.0454 1 02/02/2017 18:41 WG947910
Acenaphthylene U 0.00922 0.0454 1 02/02/2017 18:41 WG947910
Anthracene U 0.00869 0.0454 1 02/02/2017 18:41 WG947910
Benzidine U J4 0.0876 0.458 1 02/02/2017 18:41 WG947910
Benzo(a)anthracene 0.00785 J 0.00588 0.0454 1 02/02/2017 18:41 WG947910
Benzo(b)fluoranthene U 0.00955 0.0454 1 02/02/2017 18:41 WG947910
Benzo(k)fluoranthene U 0.00800 0.0454 1 02/02/2017 18:41 WG947910
Benzo(g,h,i)perylene U 0.00991 0.0454 1 02/02/2017 18:41 WG947910
Benzo(a)pyrene U 0.00753 0.0454 1 02/02/2017 18:41 WG947910
Bis(2-chlorethoxy)methane U 0.0106 0.458 1 02/02/2017 18:41 WG947910
Bis(2-chloroethyl)ether U 0.0123 0.458 1 02/02/2017 18:41 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L886597
BG-1
Collected date/time: 01/24/17 09:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.0104 0.458 1 02/02/2017 18:41 WG947910
4-Bromophenyl-phenylether U 0.0157 0.458 1 02/02/2017 18:41 WG947910
2-Chloronaphthalene U 0.00878 0.0454 1 02/02/2017 18:41 WG947910
4-Chlorophenyl-phenylether U 0.00862 0.458 1 02/02/2017 18:41 WG947910
Chrysene U 0.00763 0.0454 1 02/02/2017 18:41 WG947910
Dibenz(a,h)anthracene U 0.0113 0.0454 1 02/02/2017 18:41 WG947910
3,3-Dichlorobenzidine U 0.109 0.458 1 02/02/2017 18:41 WG947910
2,4-Dinitrotoluene U 0.00834 0.458 1 02/02/2017 18:41 WG947910
2,6-Dinitrotoluene U 0.0101 0.458 1 02/02/2017 18:41 WG947910
Fluoranthene 0.0161 J 0.00682 0.0454 1 02/02/2017 18:41 WG947910
Fluorene U 0.00937 0.0454 1 02/02/2017 18:41 WG947910
Hexachlorobenzene U 0.0118 0.458 1 02/02/2017 18:41 WG947910
Hexachloro-1,3-butadiene U 0.0137 0.458 1 02/02/2017 18:41 WG947910
Hexachlorocyclopentadiene U 0.0807 0.458 1 02/02/2017 18:41 WG947910
Hexachloroethane U 0.0184 0.458 1 02/02/2017 18:41 WG947910
Indeno(1,2,3-cd)pyrene U 0.0106 0.0454 1 02/02/2017 18:41 WG947910
Isophorone U 0.00718 0.458 1 02/02/2017 18:41 WG947910
Naphthalene U 0.0122 0.0454 1 02/02/2017 18:41 WG947910
Nitrobenzene U 0.00955 0.458 1 02/02/2017 18:41 WG947910
n-Nitrosodimethylamine U 0.0889 0.458 1 02/02/2017 18:41 WG947910
n-Nitrosodiphenylamine U 0.00816 0.458 1 02/02/2017 18:41 WG947910
n-Nitrosodi-n-propylamine U 0.0125 0.458 1 02/02/2017 18:41 WG947910
Phenanthrene 0.0108 J 0.00726 0.0454 1 02/02/2017 18:41 WG947910
Benzylbutyl phthalate U 0.0142 0.458 1 02/02/2017 18:41 WG947910
Bis(2-ethylhexyl)phthalate U 0.0165 0.458 1 02/02/2017 18:41 WG947910
Di-n-butyl phthalate U 0.0150 0.458 1 02/02/2017 18:41 WG947910
Diethyl phthalate U 0.00950 0.458 1 02/02/2017 18:41 WG947910
Dimethyl phthalate U 0.00742 0.458 1 02/02/2017 18:41 WG947910
Di-n-octyl phthalate U 0.0125 0.458 1 02/02/2017 18:41 WG947910
Pyrene U 0.0169 0.0454 1 02/02/2017 18:41 WG947910
1,2,4-Trichlorobenzene U 0.0120 0.458 1 02/02/2017 18:41 WG947910
Aniline U 0.0440 0.458 1 02/02/2017 18:41 WG947910
4-Chloro-3-methylphenol U 0.00656 0.458 1 02/02/2017 18:41 WG947910
2-Chlorophenol U 0.0114 0.458 1 02/02/2017 18:41 WG947910
2,4-Dichlorophenol U 0.0103 0.458 1 02/02/2017 18:41 WG947910
2,4-Dimethylphenol U 0.0647 0.458 1 02/02/2017 18:41 WG947910
4,6-Dinitro-2-methylphenol U 0.170 0.458 1 02/02/2017 18:41 WG947910
2,4-Dinitrophenol U 0.135 0.458 1 02/02/2017 18:41 WG947910
2-Nitrophenol U 0.0179 0.458 1 02/02/2017 18:41 WG947910
4-Nitrophenol U 0.0722 0.458 1 02/02/2017 18:41 WG947910
Pentachlorophenol U 0.0660 0.458 1 02/02/2017 18:41 WG947910
Phenol U 0.00955 0.458 1 02/02/2017 18:41 WG947910
2,4,6-Trichlorophenol U 0.0107 0.458 1 02/02/2017 18:41 WG947910
(S) 2-Fluorophenol 61.2 20.0-120 02/02/2017 18:41 WG947910
(S) Phenol-d5 74.2 20.0-120 02/02/2017 18:41 WG947910
(S) Nitrobenzene-d5 66.9 18.0-125 02/02/2017 18:41 WG947910
(S) 2-Fluorobiphenyl 71.6 28.0-120 02/02/2017 18:41 WG947910
(S) 2,4,6-Tribromophenol 83.5 17.0-137 02/02/2017 18:41 WG947910
(S) p-Terphenyl-d14 68.8 13.0-131 02/02/2017 18:41 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L886597
BG-2
Collected date/time: 01/24/17 09:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 72.6 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0446 0.00386 0.0276 1 01/30/2017 12:24 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony 0.246 J 0.218 0.689 5 02/03/2017 15:31 WG948015
Arsenic 3.18 0.0172 0.689 5 02/03/2017 15:31 WG948015
Beryllium 0.827 J 0.331 2.76 20 02/04/2017 12:55 WG948015
Cadmium U 0.110 0.689 5 02/03/2017 15:31 WG948015
Chromium 30.8 0.372 0.689 5 02/03/2017 15:31 WG948015
Copper 21.0 0.358 0.689 5 02/03/2017 15:31 WG948015
Lead 20.5 0.165 0.689 5 02/03/2017 15:31 WG948015
Manganese 366 0.689 5.51 20 02/04/2017 12:55 WG948015
Nickel 8.31 0.241 0.689 5 02/03/2017 15:31 WG948015
Selenium 1.78 0.262 0.689 5 02/03/2017 15:31 WG948015
Silver U 0.214 0.689 5 02/03/2017 15:31 WG948015
Thallium 0.367 J 0.131 0.689 5 02/03/2017 15:31 WG948015
Zinc 43.4 1.76 6.89 5 02/03/2017 15:31 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0261 J 0.0138 0.0689 1 01/31/2017 22:29 WG947760
Acrylonitrile U 0.00247 0.0138 1 01/31/2017 22:29 WG947760
Benzene U 0.000372 0.00138 1 01/31/2017 22:29 WG947760
Bromobenzene U 0.000391 0.00138 1 01/31/2017 22:29 WG947760
Bromodichloromethane U 0.000350 0.00138 1 01/31/2017 22:29 WG947760
Bromoform U 0.000584 0.00138 1 01/31/2017 22:29 WG947760
Bromomethane U 0.00185 0.00689 1 01/31/2017 22:29 WG947760
n-Butylbenzene U 0.000355 0.00138 1 01/31/2017 22:29 WG947760
sec-Butylbenzene U 0.000277 0.00138 1 01/31/2017 22:29 WG947760
tert-Butylbenzene U 0.000284 0.00138 1 01/31/2017 22:29 WG947760
Carbon tetrachloride U 0.000452 0.00138 1 01/31/2017 22:29 WG947760
Chlorobenzene U 0.000292 0.00138 1 01/31/2017 22:29 WG947760
Chlorodibromomethane U 0.000514 0.00138 1 01/31/2017 22:29 WG947760
Chloroethane U 0.00130 0.00689 1 01/31/2017 22:29 WG947760
2-Chloroethyl vinyl ether U 0.00322 0.0689 1 01/31/2017 22:29 WG947760
Chloroform U 0.000315 0.00689 1 01/31/2017 22:29 WG947760
Chloromethane U 0.000517 0.00344 1 01/31/2017 22:29 WG947760
2-Chlorotoluene U 0.000415 0.00138 1 01/31/2017 22:29 WG947760
4-Chlorotoluene U 0.000331 0.00138 1 01/31/2017 22:29 WG947760
1,2-Dibromo-3-Chloropropane U 0.00145 0.00689 1 01/31/2017 22:29 WG947760
1,2-Dibromoethane U 0.000473 0.00138 1 01/31/2017 22:29 WG947760
Dibromomethane U 0.000526 0.00138 1 01/31/2017 22:29 WG947760
1,2-Dichlorobenzene U 0.000420 0.00138 1 01/31/2017 22:29 WG947760
1,3-Dichlorobenzene U 0.000329 0.00138 1 01/31/2017 22:29 WG947760
1,4-Dichlorobenzene U 0.000311 0.00138 1 01/31/2017 22:29 WG947760
Dichlorodifluoromethane U 0.000982 0.00689 1 01/31/2017 22:29 WG947760
1,1-Dichloroethane U 0.000274 0.00138 1 01/31/2017 22:29 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 11 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L886597
BG-2
Collected date/time: 01/24/17 09:20
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000365 0.00138 1 01/31/2017 22:29 WG947760
1,1-Dichloroethene U 0.000417 0.00138 1 01/31/2017 22:29 WG947760
cis-1,2-Dichloroethene U 0.000324 0.00138 1 01/31/2017 22:29 WG947760
trans-1,2-Dichloroethene U 0.000364 0.00138 1 01/31/2017 22:29 WG947760
1,2-Dichloropropane U 0.000493 0.00138 1 01/31/2017 22:29 WG947760
1,1-Dichloropropene U 0.000437 0.00138 1 01/31/2017 22:29 WG947760
1,3-Dichloropropane U 0.000285 0.00138 1 01/31/2017 22:29 WG947760
cis-1,3-Dichloropropene U 0.000361 0.00138 1 01/31/2017 22:29 WG947760
trans-1,3-Dichloropropene U 0.000368 0.00138 1 01/31/2017 22:29 WG947760
2,2-Dichloropropane U 0.000384 0.00138 1 01/31/2017 22:29 WG947760
Di-isopropyl ether U 0.000342 0.00138 1 01/31/2017 22:29 WG947760
Ethylbenzene U 0.000409 0.00138 1 01/31/2017 22:29 WG947760
Hexachloro-1,3-butadiene U 0.000471 0.00138 1 01/31/2017 22:29 WG947760
Isopropylbenzene U 0.000335 0.00138 1 01/31/2017 22:29 WG947760
p-Isopropyltoluene U 0.000281 0.00138 1 01/31/2017 22:29 WG947760
2-Butanone (MEK)U 0.00645 0.0138 1 01/31/2017 22:29 WG947760
Methylene Chloride U 0.00138 0.00689 1 01/31/2017 22:29 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00259 0.0138 1 01/31/2017 22:29 WG947760
Methyl tert-butyl ether U 0.000292 0.00138 1 01/31/2017 22:29 WG947760
Naphthalene U 0.00138 0.00689 1 01/31/2017 22:29 WG947760
n-Propylbenzene U 0.000284 0.00138 1 01/31/2017 22:29 WG947760
Styrene U 0.000322 0.00138 1 01/31/2017 22:29 WG947760
1,1,1,2-Tetrachloroethane U 0.000364 0.00138 1 01/31/2017 22:29 WG947760
1,1,2,2-Tetrachloroethane U 0.000503 0.00138 1 01/31/2017 22:29 WG947760
Tetrachloroethene U 0.000380 0.00138 1 01/31/2017 22:29 WG947760
Toluene U 0.000598 0.00689 1 01/31/2017 22:29 WG947760
1,2,3-Trichlorobenzene U 0.000422 0.00138 1 01/31/2017 22:29 WG947760
1,2,4-Trichlorobenzene U 0.000534 0.00138 1 01/31/2017 22:29 WG947760
1,1,1-Trichloroethane U 0.000394 0.00138 1 01/31/2017 22:29 WG947760
1,1,2-Trichloroethane U 0.000382 0.00138 1 01/31/2017 22:29 WG947760
Trichloroethene U 0.000384 0.00138 1 01/31/2017 22:29 WG947760
Trichlorofluoromethane U 0.000526 0.00689 1 01/31/2017 22:29 WG947760
1,2,3-Trichloropropane U 0.00102 0.00344 1 01/31/2017 22:29 WG947760
1,2,4-Trimethylbenzene U 0.000291 0.00138 1 01/31/2017 22:29 WG947760
1,3,5-Trimethylbenzene U 0.000366 0.00138 1 01/31/2017 22:29 WG947760
Vinyl chloride U 0.000401 0.00138 1 01/31/2017 22:29 WG947760
Xylenes, Total U 0.000962 0.00413 1 01/31/2017 22:29 WG947760
(S) Toluene-d8 105 80.0-120 01/31/2017 22:29 WG947760
(S) Dibromofluoromethane 103 74.0-131 01/31/2017 22:29 WG947760
(S) a,a,a-Trifluorotoluene 100 80.0-120 01/31/2017 22:29 WG947760
(S) 4-Bromofluorobenzene 96.1 64.0-132 01/31/2017 22:29 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00884 0.0455 1 02/02/2017 19:07 WG947910
Acenaphthylene U 0.00924 0.0455 1 02/02/2017 19:07 WG947910
Anthracene U 0.00871 0.0455 1 02/02/2017 19:07 WG947910
Benzidine U J4 0.0878 0.459 1 02/02/2017 19:07 WG947910
Benzo(a)anthracene U 0.00590 0.0455 1 02/02/2017 19:07 WG947910
Benzo(b)fluoranthene U 0.00957 0.0455 1 02/02/2017 19:07 WG947910
Benzo(k)fluoranthene U 0.00802 0.0455 1 02/02/2017 19:07 WG947910
Benzo(g,h,i)perylene U 0.00993 0.0455 1 02/02/2017 19:07 WG947910
Benzo(a)pyrene U 0.00755 0.0455 1 02/02/2017 19:07 WG947910
Bis(2-chlorethoxy)methane U 0.0106 0.459 1 02/02/2017 19:07 WG947910
Bis(2-chloroethyl)ether U 0.0123 0.459 1 02/02/2017 19:07 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 12 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L886597
BG-2
Collected date/time: 01/24/17 09:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.0105 0.459 1 02/02/2017 19:07 WG947910
4-Bromophenyl-phenylether U 0.0157 0.459 1 02/02/2017 19:07 WG947910
2-Chloronaphthalene U 0.00880 0.0455 1 02/02/2017 19:07 WG947910
4-Chlorophenyl-phenylether U 0.00864 0.459 1 02/02/2017 19:07 WG947910
Chrysene U 0.00765 0.0455 1 02/02/2017 19:07 WG947910
Dibenz(a,h)anthracene U 0.0113 0.0455 1 02/02/2017 19:07 WG947910
3,3-Dichlorobenzidine U 0.109 0.459 1 02/02/2017 19:07 WG947910
2,4-Dinitrotoluene U 0.00836 0.459 1 02/02/2017 19:07 WG947910
2,6-Dinitrotoluene U 0.0102 0.459 1 02/02/2017 19:07 WG947910
Fluoranthene U 0.00683 0.0455 1 02/02/2017 19:07 WG947910
Fluorene U 0.00940 0.0455 1 02/02/2017 19:07 WG947910
Hexachlorobenzene U 0.0118 0.459 1 02/02/2017 19:07 WG947910
Hexachloro-1,3-butadiene U 0.0138 0.459 1 02/02/2017 19:07 WG947910
Hexachlorocyclopentadiene U 0.0809 0.459 1 02/02/2017 19:07 WG947910
Hexachloroethane U 0.0185 0.459 1 02/02/2017 19:07 WG947910
Indeno(1,2,3-cd)pyrene U 0.0106 0.0455 1 02/02/2017 19:07 WG947910
Isophorone U 0.00719 0.459 1 02/02/2017 19:07 WG947910
Naphthalene U 0.0122 0.0455 1 02/02/2017 19:07 WG947910
Nitrobenzene U 0.00957 0.459 1 02/02/2017 19:07 WG947910
n-Nitrosodimethylamine U 0.0891 0.459 1 02/02/2017 19:07 WG947910
n-Nitrosodiphenylamine U 0.00818 0.459 1 02/02/2017 19:07 WG947910
n-Nitrosodi-n-propylamine U 0.0125 0.459 1 02/02/2017 19:07 WG947910
Phenanthrene U 0.00727 0.0455 1 02/02/2017 19:07 WG947910
Benzylbutyl phthalate U 0.0142 0.459 1 02/02/2017 19:07 WG947910
Bis(2-ethylhexyl)phthalate U 0.0165 0.459 1 02/02/2017 19:07 WG947910
Di-n-butyl phthalate U 0.0150 0.459 1 02/02/2017 19:07 WG947910
Diethyl phthalate U 0.00952 0.459 1 02/02/2017 19:07 WG947910
Dimethyl phthalate U 0.00744 0.459 1 02/02/2017 19:07 WG947910
Di-n-octyl phthalate U 0.0125 0.459 1 02/02/2017 19:07 WG947910
Pyrene U 0.0169 0.0455 1 02/02/2017 19:07 WG947910
1,2,4-Trichlorobenzene U 0.0121 0.459 1 02/02/2017 19:07 WG947910
Aniline U 0.0441 0.459 1 02/02/2017 19:07 WG947910
4-Chloro-3-methylphenol U 0.00657 0.459 1 02/02/2017 19:07 WG947910
2-Chlorophenol U 0.0114 0.459 1 02/02/2017 19:07 WG947910
2,4-Dichlorophenol U 0.0103 0.459 1 02/02/2017 19:07 WG947910
2,4-Dimethylphenol U 0.0649 0.459 1 02/02/2017 19:07 WG947910
4,6-Dinitro-2-methylphenol U 0.171 0.459 1 02/02/2017 19:07 WG947910
2,4-Dinitrophenol U 0.135 0.459 1 02/02/2017 19:07 WG947910
2-Nitrophenol U 0.0179 0.459 1 02/02/2017 19:07 WG947910
4-Nitrophenol U 0.0723 0.459 1 02/02/2017 19:07 WG947910
Pentachlorophenol U 0.0661 0.459 1 02/02/2017 19:07 WG947910
Phenol U 0.00957 0.459 1 02/02/2017 19:07 WG947910
2,4,6-Trichlorophenol U 0.0107 0.459 1 02/02/2017 19:07 WG947910
(S) 2-Fluorophenol 61.3 20.0-120 02/02/2017 19:07 WG947910
(S) Phenol-d5 70.1 20.0-120 02/02/2017 19:07 WG947910
(S) Nitrobenzene-d5 68.8 18.0-125 02/02/2017 19:07 WG947910
(S) 2-Fluorobiphenyl 74.2 28.0-120 02/02/2017 19:07 WG947910
(S) 2,4,6-Tribromophenol 81.9 17.0-137 02/02/2017 19:07 WG947910
(S) p-Terphenyl-d14 72.3 13.0-131 02/02/2017 19:07 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 13 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L886597
B-1
Collected date/time: 01/24/17 10:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.7 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0558 0.00380 0.0271 1 01/30/2017 12:26 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony 0.250 J 0.214 0.679 5 02/03/2017 15:35 WG948015
Arsenic 4.73 0.0170 0.679 5 02/03/2017 15:35 WG948015
Beryllium 0.338 J 0.0814 0.679 5 02/03/2017 15:35 WG948015
Cadmium U 0.109 0.679 5 02/03/2017 15:35 WG948015
Chromium 37.6 0.366 0.679 5 02/03/2017 15:35 WG948015
Copper 23.0 0.353 0.679 5 02/03/2017 15:35 WG948015
Lead 25.1 0.163 0.679 5 02/03/2017 15:35 WG948015
Manganese 92.8 0.170 1.36 5 02/03/2017 15:35 WG948015
Nickel 3.82 0.238 0.679 5 02/03/2017 15:35 WG948015
Selenium 1.02 0.258 0.679 5 02/03/2017 15:35 WG948015
Silver U 0.210 0.679 5 02/03/2017 15:35 WG948015
Thallium 0.225 J 0.129 0.679 5 02/03/2017 15:35 WG948015
Zinc 28.6 1.74 6.79 5 02/03/2017 15:35 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0264 J 0.0136 0.0679 1 01/31/2017 22:51 WG947760
Acrylonitrile U 0.00243 0.0136 1 01/31/2017 22:51 WG947760
Benzene U 0.000366 0.00136 1 01/31/2017 22:51 WG947760
Bromobenzene U 0.000385 0.00136 1 01/31/2017 22:51 WG947760
Bromodichloromethane U 0.000345 0.00136 1 01/31/2017 22:51 WG947760
Bromoform U 0.000575 0.00136 1 01/31/2017 22:51 WG947760
Bromomethane U 0.00182 0.00679 1 01/31/2017 22:51 WG947760
n-Butylbenzene U 0.000350 0.00136 1 01/31/2017 22:51 WG947760
sec-Butylbenzene U 0.000273 0.00136 1 01/31/2017 22:51 WG947760
tert-Butylbenzene U 0.000280 0.00136 1 01/31/2017 22:51 WG947760
Carbon tetrachloride U 0.000445 0.00136 1 01/31/2017 22:51 WG947760
Chlorobenzene U 0.000288 0.00136 1 01/31/2017 22:51 WG947760
Chlorodibromomethane U 0.000506 0.00136 1 01/31/2017 22:51 WG947760
Chloroethane U 0.00128 0.00679 1 01/31/2017 22:51 WG947760
2-Chloroethyl vinyl ether U 0.00318 0.0679 1 01/31/2017 22:51 WG947760
Chloroform U 0.000311 0.00679 1 01/31/2017 22:51 WG947760
Chloromethane U 0.000509 0.00339 1 01/31/2017 22:51 WG947760
2-Chlorotoluene U 0.000409 0.00136 1 01/31/2017 22:51 WG947760
4-Chlorotoluene U 0.000326 0.00136 1 01/31/2017 22:51 WG947760
1,2-Dibromo-3-Chloropropane U 0.00143 0.00679 1 01/31/2017 22:51 WG947760
1,2-Dibromoethane U 0.000466 0.00136 1 01/31/2017 22:51 WG947760
Dibromomethane U 0.000518 0.00136 1 01/31/2017 22:51 WG947760
1,2-Dichlorobenzene U 0.000414 0.00136 1 01/31/2017 22:51 WG947760
1,3-Dichlorobenzene U 0.000324 0.00136 1 01/31/2017 22:51 WG947760
1,4-Dichlorobenzene U 0.000307 0.00136 1 01/31/2017 22:51 WG947760
Dichlorodifluoromethane U 0.000968 0.00679 1 01/31/2017 22:51 WG947760
1,1-Dichloroethane U 0.000270 0.00136 1 01/31/2017 22:51 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 14 of 97
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 14 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L886597
B-1
Collected date/time: 01/24/17 10:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000360 0.00136 1 01/31/2017 22:51 WG947760
1,1-Dichloroethene U 0.000411 0.00136 1 01/31/2017 22:51 WG947760
cis-1,2-Dichloroethene U 0.000319 0.00136 1 01/31/2017 22:51 WG947760
trans-1,2-Dichloroethene U 0.000358 0.00136 1 01/31/2017 22:51 WG947760
1,2-Dichloropropane U 0.000486 0.00136 1 01/31/2017 22:51 WG947760
1,1-Dichloropropene U 0.000430 0.00136 1 01/31/2017 22:51 WG947760
1,3-Dichloropropane U 0.000281 0.00136 1 01/31/2017 22:51 WG947760
cis-1,3-Dichloropropene U 0.000356 0.00136 1 01/31/2017 22:51 WG947760
trans-1,3-Dichloropropene U 0.000362 0.00136 1 01/31/2017 22:51 WG947760
2,2-Dichloropropane U 0.000379 0.00136 1 01/31/2017 22:51 WG947760
Di-isopropyl ether U 0.000337 0.00136 1 01/31/2017 22:51 WG947760
Ethylbenzene U 0.000403 0.00136 1 01/31/2017 22:51 WG947760
Hexachloro-1,3-butadiene U 0.000464 0.00136 1 01/31/2017 22:51 WG947760
Isopropylbenzene U 0.000330 0.00136 1 01/31/2017 22:51 WG947760
p-Isopropyltoluene U 0.000277 0.00136 1 01/31/2017 22:51 WG947760
2-Butanone (MEK)U 0.00635 0.0136 1 01/31/2017 22:51 WG947760
Methylene Chloride U 0.00136 0.00679 1 01/31/2017 22:51 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00255 0.0136 1 01/31/2017 22:51 WG947760
Methyl tert-butyl ether U 0.000288 0.00136 1 01/31/2017 22:51 WG947760
Naphthalene U 0.00136 0.00679 1 01/31/2017 22:51 WG947760
n-Propylbenzene U 0.000280 0.00136 1 01/31/2017 22:51 WG947760
Styrene U 0.000318 0.00136 1 01/31/2017 22:51 WG947760
1,1,1,2-Tetrachloroethane U 0.000358 0.00136 1 01/31/2017 22:51 WG947760
1,1,2,2-Tetrachloroethane U 0.000495 0.00136 1 01/31/2017 22:51 WG947760
Tetrachloroethene U 0.000375 0.00136 1 01/31/2017 22:51 WG947760
Toluene U 0.000589 0.00679 1 01/31/2017 22:51 WG947760
1,2,3-Trichlorobenzene U 0.000415 0.00136 1 01/31/2017 22:51 WG947760
1,2,4-Trichlorobenzene U 0.000527 0.00136 1 01/31/2017 22:51 WG947760
1,1,1-Trichloroethane U 0.000388 0.00136 1 01/31/2017 22:51 WG947760
1,1,2-Trichloroethane U 0.000376 0.00136 1 01/31/2017 22:51 WG947760
Trichloroethene U 0.000379 0.00136 1 01/31/2017 22:51 WG947760
Trichlorofluoromethane U 0.000518 0.00679 1 01/31/2017 22:51 WG947760
1,2,3-Trichloropropane U 0.00101 0.00339 1 01/31/2017 22:51 WG947760
1,2,4-Trimethylbenzene U 0.000286 0.00136 1 01/31/2017 22:51 WG947760
1,3,5-Trimethylbenzene U 0.000361 0.00136 1 01/31/2017 22:51 WG947760
Vinyl chloride U 0.000395 0.00136 1 01/31/2017 22:51 WG947760
Xylenes, Total U 0.000947 0.00407 1 01/31/2017 22:51 WG947760
(S) Toluene-d8 106 80.0-120 01/31/2017 22:51 WG947760
(S) Dibromofluoromethane 104 74.0-131 01/31/2017 22:51 WG947760
(S) a,a,a-Trifluorotoluene 104 80.0-120 01/31/2017 22:51 WG947760
(S) 4-Bromofluorobenzene 99.2 64.0-132 01/31/2017 22:51 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00871 0.0448 1 02/02/2017 19:58 WG947910
Acenaphthylene U 0.00911 0.0448 1 02/02/2017 19:58 WG947910
Anthracene U 0.00858 0.0448 1 02/02/2017 19:58 WG947910
Benzidine U J4 0.0865 0.452 1 02/02/2017 19:58 WG947910
Benzo(a)anthracene 0.0220 J 0.00581 0.0448 1 02/02/2017 19:58 WG947910
Benzo(b)fluoranthene 0.0262 J 0.00943 0.0448 1 02/02/2017 19:58 WG947910
Benzo(k)fluoranthene 0.00862 J 0.00790 0.0448 1 02/02/2017 19:58 WG947910
Benzo(g,h,i)perylene 0.0109 J 0.00979 0.0448 1 02/02/2017 19:58 WG947910
Benzo(a)pyrene 0.0185 J 0.00744 0.0448 1 02/02/2017 19:58 WG947910
Bis(2-chlorethoxy)methane U 0.0105 0.452 1 02/02/2017 19:58 WG947910
Bis(2-chloroethyl)ether U 0.0122 0.452 1 02/02/2017 19:58 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L886597
B-1
Collected date/time: 01/24/17 10:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.0103 0.452 1 02/02/2017 19:58 WG947910
4-Bromophenyl-phenylether U 0.0155 0.452 1 02/02/2017 19:58 WG947910
2-Chloronaphthalene U 0.00867 0.0448 1 02/02/2017 19:58 WG947910
4-Chlorophenyl-phenylether U 0.00851 0.452 1 02/02/2017 19:58 WG947910
Chrysene 0.0206 J 0.00753 0.0448 1 02/02/2017 19:58 WG947910
Dibenz(a,h)anthracene U 0.0111 0.0448 1 02/02/2017 19:58 WG947910
3,3-Dichlorobenzidine U 0.108 0.452 1 02/02/2017 19:58 WG947910
2,4-Dinitrotoluene U 0.00824 0.452 1 02/02/2017 19:58 WG947910
2,6-Dinitrotoluene U 0.0100 0.452 1 02/02/2017 19:58 WG947910
Fluoranthene 0.0405 J 0.00673 0.0448 1 02/02/2017 19:58 WG947910
Fluorene U 0.00926 0.0448 1 02/02/2017 19:58 WG947910
Hexachlorobenzene U 0.0116 0.452 1 02/02/2017 19:58 WG947910
Hexachloro-1,3-butadiene U 0.0136 0.452 1 02/02/2017 19:58 WG947910
Hexachlorocyclopentadiene U 0.0797 0.452 1 02/02/2017 19:58 WG947910
Hexachloroethane U 0.0182 0.452 1 02/02/2017 19:58 WG947910
Indeno(1,2,3-cd)pyrene U 0.0105 0.0448 1 02/02/2017 19:58 WG947910
Isophorone U 0.00708 0.452 1 02/02/2017 19:58 WG947910
Naphthalene U 0.0121 0.0448 1 02/02/2017 19:58 WG947910
Nitrobenzene U 0.00943 0.452 1 02/02/2017 19:58 WG947910
n-Nitrosodimethylamine U 0.0878 0.452 1 02/02/2017 19:58 WG947910
n-Nitrosodiphenylamine U 0.00806 0.452 1 02/02/2017 19:58 WG947910
n-Nitrosodi-n-propylamine U 0.0123 0.452 1 02/02/2017 19:58 WG947910
Phenanthrene 0.0246 J 0.00717 0.0448 1 02/02/2017 19:58 WG947910
Benzylbutyl phthalate U 0.0140 0.452 1 02/02/2017 19:58 WG947910
Bis(2-ethylhexyl)phthalate U 0.0163 0.452 1 02/02/2017 19:58 WG947910
Di-n-butyl phthalate U 0.0148 0.452 1 02/02/2017 19:58 WG947910
Diethyl phthalate U 0.00938 0.452 1 02/02/2017 19:58 WG947910
Dimethyl phthalate U 0.00733 0.452 1 02/02/2017 19:58 WG947910
Di-n-octyl phthalate U 0.0123 0.452 1 02/02/2017 19:58 WG947910
Pyrene 0.0336 J 0.0167 0.0448 1 02/02/2017 19:58 WG947910
1,2,4-Trichlorobenzene U 0.0119 0.452 1 02/02/2017 19:58 WG947910
Aniline U 0.0434 0.452 1 02/02/2017 19:58 WG947910
4-Chloro-3-methylphenol U 0.00647 0.452 1 02/02/2017 19:58 WG947910
2-Chlorophenol U 0.0113 0.452 1 02/02/2017 19:58 WG947910
2,4-Dichlorophenol U 0.0101 0.452 1 02/02/2017 19:58 WG947910
2,4-Dimethylphenol U 0.0639 0.452 1 02/02/2017 19:58 WG947910
4,6-Dinitro-2-methylphenol U 0.168 0.452 1 02/02/2017 19:58 WG947910
2,4-Dinitrophenol U 0.133 0.452 1 02/02/2017 19:58 WG947910
2-Nitrophenol U 0.0176 0.452 1 02/02/2017 19:58 WG947910
4-Nitrophenol U 0.0713 0.452 1 02/02/2017 19:58 WG947910
Pentachlorophenol U 0.0651 0.452 1 02/02/2017 19:58 WG947910
Phenol U 0.00943 0.452 1 02/02/2017 19:58 WG947910
2,4,6-Trichlorophenol U 0.0106 0.452 1 02/02/2017 19:58 WG947910
(S) 2-Fluorophenol 71.0 20.0-120 02/02/2017 19:58 WG947910
(S) Phenol-d5 73.1 20.0-120 02/02/2017 19:58 WG947910
(S) Nitrobenzene-d5 72.4 18.0-125 02/02/2017 19:58 WG947910
(S) 2-Fluorobiphenyl 62.5 28.0-120 02/02/2017 19:58 WG947910
(S) 2,4,6-Tribromophenol 77.1 17.0-137 02/02/2017 19:58 WG947910
(S) p-Terphenyl-d14 62.4 13.0-131 02/02/2017 19:58 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 16 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L886597
B-5
Collected date/time: 01/24/17 09:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.3 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0277 0.00345 0.0246 1 01/30/2017 11:50 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.194 0.615 5 02/03/2017 15:39 WG948015
Arsenic 2.34 0.0154 0.615 5 02/03/2017 15:39 WG948015
Beryllium 0.348 J 0.0738 0.615 5 02/03/2017 15:39 WG948015
Cadmium U 0.0984 0.615 5 02/03/2017 15:39 WG948015
Chromium 12.8 0.332 0.615 5 02/03/2017 15:39 WG948015
Copper 24.9 0.320 0.615 5 02/03/2017 15:39 WG948015
Lead 20.6 0.148 0.615 5 02/03/2017 15:39 WG948015
Manganese 70.5 0.154 1.23 5 02/03/2017 15:39 WG948015
Nickel 2.98 0.215 0.615 5 02/03/2017 15:39 WG948015
Selenium 0.881 0.234 0.615 5 02/03/2017 15:39 WG948015
Silver U 0.191 0.615 5 02/03/2017 15:39 WG948015
Thallium 0.154 J 0.117 0.615 5 02/03/2017 15:39 WG948015
Zinc 16.9 1.58 6.15 5 02/03/2017 15:39 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0123 0.0615 1 01/31/2017 23:13 WG947760
Acrylonitrile U 0.00220 0.0123 1 01/31/2017 23:13 WG947760
Benzene U 0.000332 0.00123 1 01/31/2017 23:13 WG947760
Bromobenzene U 0.000349 0.00123 1 01/31/2017 23:13 WG947760
Bromodichloromethane U 0.000313 0.00123 1 01/31/2017 23:13 WG947760
Bromoform U 0.000522 0.00123 1 01/31/2017 23:13 WG947760
Bromomethane U 0.00165 0.00615 1 01/31/2017 23:13 WG947760
n-Butylbenzene U 0.000317 0.00123 1 01/31/2017 23:13 WG947760
sec-Butylbenzene U 0.000247 0.00123 1 01/31/2017 23:13 WG947760
tert-Butylbenzene U 0.000253 0.00123 1 01/31/2017 23:13 WG947760
Carbon tetrachloride U 0.000404 0.00123 1 01/31/2017 23:13 WG947760
Chlorobenzene U 0.000261 0.00123 1 01/31/2017 23:13 WG947760
Chlorodibromomethane U 0.000459 0.00123 1 01/31/2017 23:13 WG947760
Chloroethane U 0.00116 0.00615 1 01/31/2017 23:13 WG947760
2-Chloroethyl vinyl ether U 0.00288 0.0615 1 01/31/2017 23:13 WG947760
Chloroform U 0.000282 0.00615 1 01/31/2017 23:13 WG947760
Chloromethane U 0.000461 0.00308 1 01/31/2017 23:13 WG947760
2-Chlorotoluene U 0.000370 0.00123 1 01/31/2017 23:13 WG947760
4-Chlorotoluene U 0.000295 0.00123 1 01/31/2017 23:13 WG947760
1,2-Dibromo-3-Chloropropane U 0.00129 0.00615 1 01/31/2017 23:13 WG947760
1,2-Dibromoethane U 0.000422 0.00123 1 01/31/2017 23:13 WG947760
Dibromomethane U 0.000470 0.00123 1 01/31/2017 23:13 WG947760
1,2-Dichlorobenzene U 0.000375 0.00123 1 01/31/2017 23:13 WG947760
1,3-Dichlorobenzene U 0.000294 0.00123 1 01/31/2017 23:13 WG947760
1,4-Dichlorobenzene U 0.000278 0.00123 1 01/31/2017 23:13 WG947760
Dichlorodifluoromethane U 0.000877 0.00615 1 01/31/2017 23:13 WG947760
1,1-Dichloroethane U 0.000245 0.00123 1 01/31/2017 23:13 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L886597
B-5
Collected date/time: 01/24/17 09:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000326 0.00123 1 01/31/2017 23:13 WG947760
1,1-Dichloroethene U 0.000373 0.00123 1 01/31/2017 23:13 WG947760
cis-1,2-Dichloroethene U 0.000289 0.00123 1 01/31/2017 23:13 WG947760
trans-1,2-Dichloroethene U 0.000325 0.00123 1 01/31/2017 23:13 WG947760
1,2-Dichloropropane U 0.000441 0.00123 1 01/31/2017 23:13 WG947760
1,1-Dichloropropene U 0.000390 0.00123 1 01/31/2017 23:13 WG947760
1,3-Dichloropropane U 0.000255 0.00123 1 01/31/2017 23:13 WG947760
cis-1,3-Dichloropropene U 0.000322 0.00123 1 01/31/2017 23:13 WG947760
trans-1,3-Dichloropropene U 0.000329 0.00123 1 01/31/2017 23:13 WG947760
2,2-Dichloropropane U 0.000343 0.00123 1 01/31/2017 23:13 WG947760
Di-isopropyl ether U 0.000305 0.00123 1 01/31/2017 23:13 WG947760
Ethylbenzene U 0.000365 0.00123 1 01/31/2017 23:13 WG947760
Hexachloro-1,3-butadiene U 0.000421 0.00123 1 01/31/2017 23:13 WG947760
Isopropylbenzene U 0.000299 0.00123 1 01/31/2017 23:13 WG947760
p-Isopropyltoluene U 0.000251 0.00123 1 01/31/2017 23:13 WG947760
2-Butanone (MEK)U 0.00576 0.0123 1 01/31/2017 23:13 WG947760
Methylene Chloride U 0.00123 0.00615 1 01/31/2017 23:13 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00231 0.0123 1 01/31/2017 23:13 WG947760
Methyl tert-butyl ether U 0.000261 0.00123 1 01/31/2017 23:13 WG947760
Naphthalene U 0.00123 0.00615 1 01/31/2017 23:13 WG947760
n-Propylbenzene U 0.000253 0.00123 1 01/31/2017 23:13 WG947760
Styrene U 0.000288 0.00123 1 01/31/2017 23:13 WG947760
1,1,1,2-Tetrachloroethane U 0.000325 0.00123 1 01/31/2017 23:13 WG947760
1,1,2,2-Tetrachloroethane U 0.000449 0.00123 1 01/31/2017 23:13 WG947760
Tetrachloroethene U 0.000340 0.00123 1 01/31/2017 23:13 WG947760
Toluene U 0.000534 0.00615 1 01/31/2017 23:13 WG947760
1,2,3-Trichlorobenzene U 0.000377 0.00123 1 01/31/2017 23:13 WG947760
1,2,4-Trichlorobenzene U 0.000477 0.00123 1 01/31/2017 23:13 WG947760
1,1,1-Trichloroethane U 0.000352 0.00123 1 01/31/2017 23:13 WG947760
1,1,2-Trichloroethane U 0.000341 0.00123 1 01/31/2017 23:13 WG947760
Trichloroethene U 0.000343 0.00123 1 01/31/2017 23:13 WG947760
Trichlorofluoromethane U 0.000470 0.00615 1 01/31/2017 23:13 WG947760
1,2,3-Trichloropropane U 0.000912 0.00308 1 01/31/2017 23:13 WG947760
1,2,4-Trimethylbenzene U 0.000260 0.00123 1 01/31/2017 23:13 WG947760
1,3,5-Trimethylbenzene U 0.000327 0.00123 1 01/31/2017 23:13 WG947760
Vinyl chloride U 0.000358 0.00123 1 01/31/2017 23:13 WG947760
Xylenes, Total U 0.000859 0.00369 1 01/31/2017 23:13 WG947760
(S) Toluene-d8 106 80.0-120 01/31/2017 23:13 WG947760
(S) Dibromofluoromethane 105 74.0-131 01/31/2017 23:13 WG947760
(S) a,a,a-Trifluorotoluene 102 80.0-120 01/31/2017 23:13 WG947760
(S) 4-Bromofluorobenzene 97.7 64.0-132 01/31/2017 23:13 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00790 0.0406 1 02/02/2017 14:49 WG947910
Acenaphthylene U 0.00826 0.0406 1 02/02/2017 14:49 WG947910
Anthracene U 0.00778 0.0406 1 02/02/2017 14:49 WG947910
Benzidine U J4 0.0784 0.410 1 02/02/2017 14:49 WG947910
Benzo(a)anthracene U 0.00527 0.0406 1 02/02/2017 14:49 WG947910
Benzo(b)fluoranthene U 0.00855 0.0406 1 02/02/2017 14:49 WG947910
Benzo(k)fluoranthene U 0.00716 0.0406 1 02/02/2017 14:49 WG947910
Benzo(g,h,i)perylene U 0.00887 0.0406 1 02/02/2017 14:49 WG947910
Benzo(a)pyrene U 0.00674 0.0406 1 02/02/2017 14:49 WG947910
Bis(2-chlorethoxy)methane U 0.00948 0.410 1 02/02/2017 14:49 WG947910
Bis(2-chloroethyl)ether U 0.0110 0.410 1 02/02/2017 14:49 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 18 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L886597
B-5
Collected date/time: 01/24/17 09:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00935 0.410 1 02/02/2017 14:49 WG947910
4-Bromophenyl-phenylether U 0.0140 0.410 1 02/02/2017 14:49 WG947910
2-Chloronaphthalene U 0.00786 0.0406 1 02/02/2017 14:49 WG947910
4-Chlorophenyl-phenylether U 0.00772 0.410 1 02/02/2017 14:49 WG947910
Chrysene U 0.00683 0.0406 1 02/02/2017 14:49 WG947910
Dibenz(a,h)anthracene U 0.0101 0.0406 1 02/02/2017 14:49 WG947910
3,3-Dichlorobenzidine U 0.0977 0.410 1 02/02/2017 14:49 WG947910
2,4-Dinitrotoluene U 0.00747 0.410 1 02/02/2017 14:49 WG947910
2,6-Dinitrotoluene U 0.00907 0.410 1 02/02/2017 14:49 WG947910
Fluoranthene U 0.00610 0.0406 1 02/02/2017 14:49 WG947910
Fluorene U 0.00839 0.0406 1 02/02/2017 14:49 WG947910
Hexachlorobenzene U 0.0105 0.410 1 02/02/2017 14:49 WG947910
Hexachloro-1,3-butadiene U 0.0123 0.410 1 02/02/2017 14:49 WG947910
Hexachlorocyclopentadiene U 0.0722 0.410 1 02/02/2017 14:49 WG947910
Hexachloroethane U 0.0165 0.410 1 02/02/2017 14:49 WG947910
Indeno(1,2,3-cd)pyrene U 0.00950 0.0406 1 02/02/2017 14:49 WG947910
Isophorone U 0.00642 0.410 1 02/02/2017 14:49 WG947910
Naphthalene U 0.0109 0.0406 1 02/02/2017 14:49 WG947910
Nitrobenzene U 0.00855 0.410 1 02/02/2017 14:49 WG947910
n-Nitrosodimethylamine U 0.0796 0.410 1 02/02/2017 14:49 WG947910
n-Nitrosodiphenylamine U 0.00731 0.410 1 02/02/2017 14:49 WG947910
n-Nitrosodi-n-propylamine U 0.0111 0.410 1 02/02/2017 14:49 WG947910
Phenanthrene U 0.00650 0.0406 1 02/02/2017 14:49 WG947910
Benzylbutyl phthalate U 0.0127 0.410 1 02/02/2017 14:49 WG947910
Bis(2-ethylhexyl)phthalate U 0.0148 0.410 1 02/02/2017 14:49 WG947910
Di-n-butyl phthalate U 0.0134 0.410 1 02/02/2017 14:49 WG947910
Diethyl phthalate U 0.00850 0.410 1 02/02/2017 14:49 WG947910
Dimethyl phthalate U 0.00664 0.410 1 02/02/2017 14:49 WG947910
Di-n-octyl phthalate U 0.0112 0.410 1 02/02/2017 14:49 WG947910
Pyrene U 0.0151 0.0406 1 02/02/2017 14:49 WG947910
1,2,4-Trichlorobenzene U 0.0108 0.410 1 02/02/2017 14:49 WG947910
Aniline U 0.0394 0.410 1 02/02/2017 14:49 WG947910
4-Chloro-3-methylphenol U 0.00587 0.410 1 02/02/2017 14:49 WG947910
2-Chlorophenol U 0.0102 0.410 1 02/02/2017 14:49 WG947910
2,4-Dichlorophenol U 0.00918 0.410 1 02/02/2017 14:49 WG947910
2,4-Dimethylphenol U 0.0580 0.410 1 02/02/2017 14:49 WG947910
4,6-Dinitro-2-methylphenol U 0.153 0.410 1 02/02/2017 14:49 WG947910
2,4-Dinitrophenol U 0.121 0.410 1 02/02/2017 14:49 WG947910
2-Nitrophenol U 0.0160 0.410 1 02/02/2017 14:49 WG947910
4-Nitrophenol U 0.0646 0.410 1 02/02/2017 14:49 WG947910
Pentachlorophenol U 0.0591 0.410 1 02/02/2017 14:49 WG947910
Phenol U 0.00855 0.410 1 02/02/2017 14:49 WG947910
2,4,6-Trichlorophenol U 0.00959 0.410 1 02/02/2017 14:49 WG947910
(S) 2-Fluorophenol 55.0 20.0-120 02/02/2017 14:49 WG947910
(S) Phenol-d5 59.0 20.0-120 02/02/2017 14:49 WG947910
(S) Nitrobenzene-d5 56.8 18.0-125 02/02/2017 14:49 WG947910
(S) 2-Fluorobiphenyl 67.4 28.0-120 02/02/2017 14:49 WG947910
(S) 2,4,6-Tribromophenol 80.7 17.0-137 02/02/2017 14:49 WG947910
(S) p-Terphenyl-d14 81.8 13.0-131 02/02/2017 14:49 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 19 of 97
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 19 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L886597
B-7
Collected date/time: 01/24/17 15:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.4 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0510 0.00362 0.0258 1 01/30/2017 12:29 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony 0.221 J 0.204 0.646 5 02/03/2017 15:42 WG948015
Arsenic 3.97 0.0161 0.646 5 02/03/2017 15:42 WG948015
Beryllium 0.310 J 0.155 1.29 10 02/04/2017 12:58 WG948015
Cadmium U 0.103 0.646 5 02/03/2017 15:42 WG948015
Chromium 43.3 0.349 0.646 5 02/03/2017 15:42 WG948015
Copper 33.4 0.336 0.646 5 02/03/2017 15:42 WG948015
Lead 22.5 0.155 0.646 5 02/03/2017 15:42 WG948015
Manganese 139 0.323 2.58 10 02/04/2017 12:58 WG948015
Nickel 6.01 0.226 0.646 5 02/03/2017 15:42 WG948015
Selenium 1.08 0.245 0.646 5 02/03/2017 15:42 WG948015
Silver U 0.200 0.646 5 02/03/2017 15:42 WG948015
Thallium 0.343 J 0.123 0.646 5 02/03/2017 15:42 WG948015
Zinc 27.2 1.65 6.46 5 02/03/2017 15:42 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0151 0.0756 1.17 01/31/2017 23:36 WG947760
Acrylonitrile U 0.00270 0.0151 1.17 01/31/2017 23:36 WG947760
Benzene U 0.000408 0.00151 1.17 01/31/2017 23:36 WG947760
Bromobenzene U 0.000429 0.00151 1.17 01/31/2017 23:36 WG947760
Bromodichloromethane U 0.000384 0.00151 1.17 01/31/2017 23:36 WG947760
Bromoform U 0.000641 0.00151 1.17 01/31/2017 23:36 WG947760
Bromomethane U 0.00203 0.00756 1.17 01/31/2017 23:36 WG947760
n-Butylbenzene U 0.000390 0.00151 1.17 01/31/2017 23:36 WG947760
sec-Butylbenzene U 0.000304 0.00151 1.17 01/31/2017 23:36 WG947760
tert-Butylbenzene U 0.000311 0.00151 1.17 01/31/2017 23:36 WG947760
Carbon tetrachloride U 0.000496 0.00151 1.17 01/31/2017 23:36 WG947760
Chlorobenzene U 0.000320 0.00151 1.17 01/31/2017 23:36 WG947760
Chlorodibromomethane U 0.000563 0.00151 1.17 01/31/2017 23:36 WG947760
Chloroethane U 0.00143 0.00756 1.17 01/31/2017 23:36 WG947760
2-Chloroethyl vinyl ether U 0.00354 0.0756 1.17 01/31/2017 23:36 WG947760
Chloroform U 0.000346 0.00756 1.17 01/31/2017 23:36 WG947760
Chloromethane U 0.000567 0.00378 1.17 01/31/2017 23:36 WG947760
2-Chlorotoluene U 0.000455 0.00151 1.17 01/31/2017 23:36 WG947760
4-Chlorotoluene U 0.000363 0.00151 1.17 01/31/2017 23:36 WG947760
1,2-Dibromo-3-Chloropropane U 0.00159 0.00756 1.17 01/31/2017 23:36 WG947760
1,2-Dibromoethane U 0.000518 0.00151 1.17 01/31/2017 23:36 WG947760
Dibromomethane U 0.000577 0.00151 1.17 01/31/2017 23:36 WG947760
1,2-Dichlorobenzene U 0.000461 0.00151 1.17 01/31/2017 23:36 WG947760
1,3-Dichlorobenzene U 0.000362 0.00151 1.17 01/31/2017 23:36 WG947760
1,4-Dichlorobenzene U 0.000341 0.00151 1.17 01/31/2017 23:36 WG947760
Dichlorodifluoromethane U 0.00108 0.00756 1.17 01/31/2017 23:36 WG947760
1,1-Dichloroethane U 0.000301 0.00151 1.17 01/31/2017 23:36 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L886597
B-7
Collected date/time: 01/24/17 15:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000401 0.00151 1.17 01/31/2017 23:36 WG947760
1,1-Dichloroethene U 0.000457 0.00151 1.17 01/31/2017 23:36 WG947760
cis-1,2-Dichloroethene U 0.000355 0.00151 1.17 01/31/2017 23:36 WG947760
trans-1,2-Dichloroethene U 0.000399 0.00151 1.17 01/31/2017 23:36 WG947760
1,2-Dichloropropane U 0.000541 0.00151 1.17 01/31/2017 23:36 WG947760
1,1-Dichloropropene U 0.000479 0.00151 1.17 01/31/2017 23:36 WG947760
1,3-Dichloropropane U 0.000313 0.00151 1.17 01/31/2017 23:36 WG947760
cis-1,3-Dichloropropene U 0.000395 0.00151 1.17 01/31/2017 23:36 WG947760
trans-1,3-Dichloropropene U 0.000403 0.00151 1.17 01/31/2017 23:36 WG947760
2,2-Dichloropropane U 0.000421 0.00151 1.17 01/31/2017 23:36 WG947760
Di-isopropyl ether U 0.000375 0.00151 1.17 01/31/2017 23:36 WG947760
Ethylbenzene U 0.000448 0.00151 1.17 01/31/2017 23:36 WG947760
Hexachloro-1,3-butadiene U 0.000517 0.00151 1.17 01/31/2017 23:36 WG947760
Isopropylbenzene U 0.000367 0.00151 1.17 01/31/2017 23:36 WG947760
p-Isopropyltoluene U 0.000309 0.00151 1.17 01/31/2017 23:36 WG947760
2-Butanone (MEK)U 0.00708 0.0151 1.17 01/31/2017 23:36 WG947760
Methylene Chloride U 0.00151 0.00756 1.17 01/31/2017 23:36 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00284 0.0151 1.17 01/31/2017 23:36 WG947760
Methyl tert-butyl ether U 0.000320 0.00151 1.17 01/31/2017 23:36 WG947760
Naphthalene U 0.00151 0.00756 1.17 01/31/2017 23:36 WG947760
n-Propylbenzene U 0.000311 0.00151 1.17 01/31/2017 23:36 WG947760
Styrene U 0.000354 0.00151 1.17 01/31/2017 23:36 WG947760
1,1,1,2-Tetrachloroethane U 0.000399 0.00151 1.17 01/31/2017 23:36 WG947760
1,1,2,2-Tetrachloroethane U 0.000552 0.00151 1.17 01/31/2017 23:36 WG947760
Tetrachloroethene U 0.000417 0.00151 1.17 01/31/2017 23:36 WG947760
Toluene U 0.000656 0.00756 1.17 01/31/2017 23:36 WG947760
1,2,3-Trichlorobenzene U 0.000463 0.00151 1.17 01/31/2017 23:36 WG947760
1,2,4-Trichlorobenzene U 0.000587 0.00151 1.17 01/31/2017 23:36 WG947760
1,1,1-Trichloroethane U 0.000433 0.00151 1.17 01/31/2017 23:36 WG947760
1,1,2-Trichloroethane U 0.000419 0.00151 1.17 01/31/2017 23:36 WG947760
Trichloroethene U 0.000421 0.00151 1.17 01/31/2017 23:36 WG947760
Trichlorofluoromethane U 0.000577 0.00756 1.17 01/31/2017 23:36 WG947760
1,2,3-Trichloropropane U 0.00112 0.00378 1.17 01/31/2017 23:36 WG947760
1,2,4-Trimethylbenzene U 0.000319 0.00151 1.17 01/31/2017 23:36 WG947760
1,3,5-Trimethylbenzene U 0.000402 0.00151 1.17 01/31/2017 23:36 WG947760
Vinyl chloride U 0.000439 0.00151 1.17 01/31/2017 23:36 WG947760
Xylenes, Total U 0.00106 0.00453 1.17 01/31/2017 23:36 WG947760
(S) Toluene-d8 107 80.0-120 01/31/2017 23:36 WG947760
(S) Dibromofluoromethane 107 74.0-131 01/31/2017 23:36 WG947760
(S) a,a,a-Trifluorotoluene 104 80.0-120 01/31/2017 23:36 WG947760
(S) 4-Bromofluorobenzene 96.5 64.0-132 01/31/2017 23:36 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00829 0.0426 1 02/02/2017 13:31 WG947910
Acenaphthylene U 0.00867 0.0426 1 02/02/2017 13:31 WG947910
Anthracene U 0.00817 0.0426 1 02/02/2017 13:31 WG947910
Benzidine U J4 J6 0.0823 0.430 1 02/02/2017 13:31 WG947910
Benzo(a)anthracene U 0.00553 0.0426 1 02/02/2017 13:31 WG947910
Benzo(b)fluoranthene U 0.00898 0.0426 1 02/02/2017 13:31 WG947910
Benzo(k)fluoranthene U 0.00752 0.0426 1 02/02/2017 13:31 WG947910
Benzo(g,h,i)perylene U 0.00931 0.0426 1 02/02/2017 13:31 WG947910
Benzo(a)pyrene U 0.00708 0.0426 1 02/02/2017 13:31 WG947910
Bis(2-chlorethoxy)methane U 0.00995 0.430 1 02/02/2017 13:31 WG947910
Bis(2-chloroethyl)ether U 0.0116 0.430 1 02/02/2017 13:31 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 21 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L886597
B-7
Collected date/time: 01/24/17 15:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00982 0.430 1 02/02/2017 13:31 WG947910
4-Bromophenyl-phenylether U 0.0147 0.430 1 02/02/2017 13:31 WG947910
2-Chloronaphthalene U 0.00826 0.0426 1 02/02/2017 13:31 WG947910
4-Chlorophenyl-phenylether U 0.00810 0.430 1 02/02/2017 13:31 WG947910
Chrysene U 0.00717 0.0426 1 02/02/2017 13:31 WG947910
Dibenz(a,h)anthracene U 0.0106 0.0426 1 02/02/2017 13:31 WG947910
3,3-Dichlorobenzidine U 0.103 0.430 1 02/02/2017 13:31 WG947910
2,4-Dinitrotoluene U 0.00784 0.430 1 02/02/2017 13:31 WG947910
2,6-Dinitrotoluene U 0.00952 0.430 1 02/02/2017 13:31 WG947910
Fluoranthene U 0.00641 0.0426 1 02/02/2017 13:31 WG947910
Fluorene U 0.00881 0.0426 1 02/02/2017 13:31 WG947910
Hexachlorobenzene U 0.0111 0.430 1 02/02/2017 13:31 WG947910
Hexachloro-1,3-butadiene U 0.0129 0.430 1 02/02/2017 13:31 WG947910
Hexachlorocyclopentadiene U 0.0758 0.430 1 02/02/2017 13:31 WG947910
Hexachloroethane U 0.0173 0.430 1 02/02/2017 13:31 WG947910
Indeno(1,2,3-cd)pyrene U 0.00997 0.0426 1 02/02/2017 13:31 WG947910
Isophorone U 0.00674 0.430 1 02/02/2017 13:31 WG947910
Naphthalene U 0.0115 0.0426 1 02/02/2017 13:31 WG947910
Nitrobenzene U 0.00898 0.430 1 02/02/2017 13:31 WG947910
n-Nitrosodimethylamine U 0.0836 0.430 1 02/02/2017 13:31 WG947910
n-Nitrosodiphenylamine U 0.00767 0.430 1 02/02/2017 13:31 WG947910
n-Nitrosodi-n-propylamine U 0.0117 0.430 1 02/02/2017 13:31 WG947910
Phenanthrene U 0.00682 0.0426 1 02/02/2017 13:31 WG947910
Benzylbutyl phthalate U 0.0133 0.430 1 02/02/2017 13:31 WG947910
Bis(2-ethylhexyl)phthalate U 0.0155 0.430 1 02/02/2017 13:31 WG947910
Di-n-butyl phthalate U 0.0141 0.430 1 02/02/2017 13:31 WG947910
Diethyl phthalate U 0.00893 0.430 1 02/02/2017 13:31 WG947910
Dimethyl phthalate U 0.00698 0.430 1 02/02/2017 13:31 WG947910
Di-n-octyl phthalate U 0.0117 0.430 1 02/02/2017 13:31 WG947910
Pyrene U 0.0159 0.0426 1 02/02/2017 13:31 WG947910
1,2,4-Trichlorobenzene U 0.0113 0.430 1 02/02/2017 13:31 WG947910
Aniline U 0.0413 0.430 1 02/02/2017 13:31 WG947910
4-Chloro-3-methylphenol U 0.00616 0.430 1 02/02/2017 13:31 WG947910
2-Chlorophenol U 0.0107 0.430 1 02/02/2017 13:31 WG947910
2,4-Dichlorophenol U 0.00964 0.430 1 02/02/2017 13:31 WG947910
2,4-Dimethylphenol U 0.0609 0.430 1 02/02/2017 13:31 WG947910
4,6-Dinitro-2-methylphenol U 0.160 0.430 1 02/02/2017 13:31 WG947910
2,4-Dinitrophenol U 0.127 0.430 1 02/02/2017 13:31 WG947910
2-Nitrophenol U 0.0168 0.430 1 02/02/2017 13:31 WG947910
4-Nitrophenol U 0.0678 0.430 1 02/02/2017 13:31 WG947910
Pentachlorophenol U 0.0620 0.430 1 02/02/2017 13:31 WG947910
Phenol U 0.00898 0.430 1 02/02/2017 13:31 WG947910
2,4,6-Trichlorophenol U 0.0101 0.430 1 02/02/2017 13:31 WG947910
(S) 2-Fluorophenol 26.2 20.0-120 02/02/2017 13:31 WG947910
(S) Phenol-d5 33.4 20.0-120 02/02/2017 13:31 WG947910
(S) Nitrobenzene-d5 28.8 18.0-125 02/02/2017 13:31 WG947910
(S) 2-Fluorobiphenyl 50.7 28.0-120 02/02/2017 13:31 WG947910
(S) 2,4,6-Tribromophenol 80.6 17.0-137 02/02/2017 13:31 WG947910
(S) p-Terphenyl-d14 81.5 13.0-131 02/02/2017 13:31 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L886597
B-8
Collected date/time: 01/24/17 14:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 75.4 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0436 0.00371 0.0265 1 01/30/2017 12:31 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.210 0.663 5 02/03/2017 15:46 WG948015
Arsenic 2.30 0.0166 0.663 5 02/03/2017 15:46 WG948015
Beryllium 0.228 J 0.159 1.33 10 02/04/2017 13:02 WG948015
Cadmium U 0.106 0.663 5 02/03/2017 15:46 WG948015
Chromium 40.6 0.358 0.663 5 02/03/2017 15:46 WG948015
Copper 27.4 0.345 0.663 5 02/03/2017 15:46 WG948015
Lead 23.3 0.159 0.663 5 02/03/2017 15:46 WG948015
Manganese 108 0.166 1.33 5 02/03/2017 15:46 WG948015
Nickel 4.07 0.232 0.663 5 02/03/2017 15:46 WG948015
Selenium 0.810 0.252 0.663 5 02/03/2017 15:46 WG948015
Silver U 0.206 0.663 5 02/03/2017 15:46 WG948015
Thallium U 0.126 0.663 5 02/03/2017 15:46 WG948015
Zinc 25.6 1.70 6.63 5 02/03/2017 15:46 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0133 0.0663 1 01/31/2017 23:59 WG947760
Acrylonitrile U 0.00237 0.0133 1 01/31/2017 23:59 WG947760
Benzene U 0.000358 0.00133 1 01/31/2017 23:59 WG947760
Bromobenzene U 0.000377 0.00133 1 01/31/2017 23:59 WG947760
Bromodichloromethane U 0.000337 0.00133 1 01/31/2017 23:59 WG947760
Bromoform U 0.000562 0.00133 1 01/31/2017 23:59 WG947760
Bromomethane U 0.00178 0.00663 1 01/31/2017 23:59 WG947760
n-Butylbenzene U 0.000342 0.00133 1 01/31/2017 23:59 WG947760
sec-Butylbenzene U 0.000267 0.00133 1 01/31/2017 23:59 WG947760
tert-Butylbenzene U 0.000273 0.00133 1 01/31/2017 23:59 WG947760
Carbon tetrachloride U 0.000435 0.00133 1 01/31/2017 23:59 WG947760
Chlorobenzene U 0.000281 0.00133 1 01/31/2017 23:59 WG947760
Chlorodibromomethane U 0.000495 0.00133 1 01/31/2017 23:59 WG947760
Chloroethane U 0.00125 0.00663 1 01/31/2017 23:59 WG947760
2-Chloroethyl vinyl ether U 0.00310 0.0663 1 01/31/2017 23:59 WG947760
Chloroform U 0.000304 0.00663 1 01/31/2017 23:59 WG947760
Chloromethane U 0.000497 0.00332 1 01/31/2017 23:59 WG947760
2-Chlorotoluene U 0.000399 0.00133 1 01/31/2017 23:59 WG947760
4-Chlorotoluene U 0.000318 0.00133 1 01/31/2017 23:59 WG947760
1,2-Dibromo-3-Chloropropane U 0.00139 0.00663 1 01/31/2017 23:59 WG947760
1,2-Dibromoethane U 0.000455 0.00133 1 01/31/2017 23:59 WG947760
Dibromomethane U 0.000507 0.00133 1 01/31/2017 23:59 WG947760
1,2-Dichlorobenzene U 0.000404 0.00133 1 01/31/2017 23:59 WG947760
1,3-Dichlorobenzene U 0.000317 0.00133 1 01/31/2017 23:59 WG947760
1,4-Dichlorobenzene U 0.000300 0.00133 1 01/31/2017 23:59 WG947760
Dichlorodifluoromethane U 0.000946 0.00663 1 01/31/2017 23:59 WG947760
1,1-Dichloroethane U 0.000264 0.00133 1 01/31/2017 23:59 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 23 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L886597
B-8
Collected date/time: 01/24/17 14:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000351 0.00133 1 01/31/2017 23:59 WG947760
1,1-Dichloroethene U 0.000402 0.00133 1 01/31/2017 23:59 WG947760
cis-1,2-Dichloroethene U 0.000312 0.00133 1 01/31/2017 23:59 WG947760
trans-1,2-Dichloroethene U 0.000350 0.00133 1 01/31/2017 23:59 WG947760
1,2-Dichloropropane U 0.000475 0.00133 1 01/31/2017 23:59 WG947760
1,1-Dichloropropene U 0.000420 0.00133 1 01/31/2017 23:59 WG947760
1,3-Dichloropropane U 0.000275 0.00133 1 01/31/2017 23:59 WG947760
cis-1,3-Dichloropropene U 0.000347 0.00133 1 01/31/2017 23:59 WG947760
trans-1,3-Dichloropropene U 0.000354 0.00133 1 01/31/2017 23:59 WG947760
2,2-Dichloropropane U 0.000370 0.00133 1 01/31/2017 23:59 WG947760
Di-isopropyl ether U 0.000329 0.00133 1 01/31/2017 23:59 WG947760
Ethylbenzene U 0.000394 0.00133 1 01/31/2017 23:59 WG947760
Hexachloro-1,3-butadiene U 0.000454 0.00133 1 01/31/2017 23:59 WG947760
Isopropylbenzene U 0.000322 0.00133 1 01/31/2017 23:59 WG947760
p-Isopropyltoluene U 0.000271 0.00133 1 01/31/2017 23:59 WG947760
2-Butanone (MEK)U 0.00621 0.0133 1 01/31/2017 23:59 WG947760
Methylene Chloride U 0.00133 0.00663 1 01/31/2017 23:59 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00249 0.0133 1 01/31/2017 23:59 WG947760
Methyl tert-butyl ether U 0.000281 0.00133 1 01/31/2017 23:59 WG947760
Naphthalene U 0.00133 0.00663 1 01/31/2017 23:59 WG947760
n-Propylbenzene U 0.000273 0.00133 1 01/31/2017 23:59 WG947760
Styrene U 0.000310 0.00133 1 01/31/2017 23:59 WG947760
1,1,1,2-Tetrachloroethane U 0.000350 0.00133 1 01/31/2017 23:59 WG947760
1,1,2,2-Tetrachloroethane U 0.000484 0.00133 1 01/31/2017 23:59 WG947760
Tetrachloroethene U 0.000366 0.00133 1 01/31/2017 23:59 WG947760
Toluene U 0.000576 0.00663 1 01/31/2017 23:59 WG947760
1,2,3-Trichlorobenzene U 0.000406 0.00133 1 01/31/2017 23:59 WG947760
1,2,4-Trichlorobenzene U 0.000515 0.00133 1 01/31/2017 23:59 WG947760
1,1,1-Trichloroethane U 0.000379 0.00133 1 01/31/2017 23:59 WG947760
1,1,2-Trichloroethane U 0.000367 0.00133 1 01/31/2017 23:59 WG947760
Trichloroethene U 0.000370 0.00133 1 01/31/2017 23:59 WG947760
Trichlorofluoromethane U 0.000507 0.00663 1 01/31/2017 23:59 WG947760
1,2,3-Trichloropropane U 0.000983 0.00332 1 01/31/2017 23:59 WG947760
1,2,4-Trimethylbenzene U 0.000280 0.00133 1 01/31/2017 23:59 WG947760
1,3,5-Trimethylbenzene U 0.000353 0.00133 1 01/31/2017 23:59 WG947760
Vinyl chloride U 0.000386 0.00133 1 01/31/2017 23:59 WG947760
Xylenes, Total U 0.000926 0.00398 1 01/31/2017 23:59 WG947760
(S) Toluene-d8 105 80.0-120 01/31/2017 23:59 WG947760
(S) Dibromofluoromethane 106 74.0-131 01/31/2017 23:59 WG947760
(S) a,a,a-Trifluorotoluene 101 80.0-120 01/31/2017 23:59 WG947760
(S) 4-Bromofluorobenzene 98.1 64.0-132 01/31/2017 23:59 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00851 0.0438 1 02/02/2017 15:15 WG947910
Acenaphthylene U 0.00890 0.0438 1 02/02/2017 15:15 WG947910
Anthracene U 0.00838 0.0438 1 02/02/2017 15:15 WG947910
Benzidine U J4 0.0845 0.442 1 02/02/2017 15:15 WG947910
Benzo(a)anthracene 0.0106 J 0.00568 0.0438 1 02/02/2017 15:15 WG947910
Benzo(b)fluoranthene 0.0127 J 0.00922 0.0438 1 02/02/2017 15:15 WG947910
Benzo(k)fluoranthene U 0.00772 0.0438 1 02/02/2017 15:15 WG947910
Benzo(g,h,i)perylene U 0.00956 0.0438 1 02/02/2017 15:15 WG947910
Benzo(a)pyrene 0.00788 J 0.00727 0.0438 1 02/02/2017 15:15 WG947910
Bis(2-chlorethoxy)methane U 0.0102 0.442 1 02/02/2017 15:15 WG947910
Bis(2-chloroethyl)ether U 0.0119 0.442 1 02/02/2017 15:15 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L886597
B-8
Collected date/time: 01/24/17 14:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.0101 0.442 1 02/02/2017 15:15 WG947910
4-Bromophenyl-phenylether U 0.0151 0.442 1 02/02/2017 15:15 WG947910
2-Chloronaphthalene U 0.00847 0.0438 1 02/02/2017 15:15 WG947910
4-Chlorophenyl-phenylether U 0.00832 0.442 1 02/02/2017 15:15 WG947910
Chrysene 0.00867 J 0.00736 0.0438 1 02/02/2017 15:15 WG947910
Dibenz(a,h)anthracene U 0.0109 0.0438 1 02/02/2017 15:15 WG947910
3,3-Dichlorobenzidine U 0.105 0.442 1 02/02/2017 15:15 WG947910
2,4-Dinitrotoluene U 0.00805 0.442 1 02/02/2017 15:15 WG947910
2,6-Dinitrotoluene U 0.00977 0.442 1 02/02/2017 15:15 WG947910
Fluoranthene 0.0105 J 0.00658 0.0438 1 02/02/2017 15:15 WG947910
Fluorene U 0.00904 0.0438 1 02/02/2017 15:15 WG947910
Hexachlorobenzene U 0.0114 0.442 1 02/02/2017 15:15 WG947910
Hexachloro-1,3-butadiene U 0.0133 0.442 1 02/02/2017 15:15 WG947910
Hexachlorocyclopentadiene U 0.0778 0.442 1 02/02/2017 15:15 WG947910
Hexachloroethane U 0.0178 0.442 1 02/02/2017 15:15 WG947910
Indeno(1,2,3-cd)pyrene U 0.0102 0.0438 1 02/02/2017 15:15 WG947910
Isophorone U 0.00692 0.442 1 02/02/2017 15:15 WG947910
Naphthalene U 0.0118 0.0438 1 02/02/2017 15:15 WG947910
Nitrobenzene U 0.00922 0.442 1 02/02/2017 15:15 WG947910
n-Nitrosodimethylamine U 0.0858 0.442 1 02/02/2017 15:15 WG947910
n-Nitrosodiphenylamine U 0.00788 0.442 1 02/02/2017 15:15 WG947910
n-Nitrosodi-n-propylamine U 0.0120 0.442 1 02/02/2017 15:15 WG947910
Phenanthrene U 0.00700 0.0438 1 02/02/2017 15:15 WG947910
Benzylbutyl phthalate U 0.0137 0.442 1 02/02/2017 15:15 WG947910
Bis(2-ethylhexyl)phthalate U 0.0159 0.442 1 02/02/2017 15:15 WG947910
Di-n-butyl phthalate U 0.0145 0.442 1 02/02/2017 15:15 WG947910
Diethyl phthalate U 0.00916 0.442 1 02/02/2017 15:15 WG947910
Dimethyl phthalate U 0.00716 0.442 1 02/02/2017 15:15 WG947910
Di-n-octyl phthalate U 0.0120 0.442 1 02/02/2017 15:15 WG947910
Pyrene U 0.0163 0.0438 1 02/02/2017 15:15 WG947910
1,2,4-Trichlorobenzene U 0.0116 0.442 1 02/02/2017 15:15 WG947910
Aniline U 0.0424 0.442 1 02/02/2017 15:15 WG947910
4-Chloro-3-methylphenol U 0.00633 0.442 1 02/02/2017 15:15 WG947910
2-Chlorophenol U 0.0110 0.442 1 02/02/2017 15:15 WG947910
2,4-Dichlorophenol U 0.00989 0.442 1 02/02/2017 15:15 WG947910
2,4-Dimethylphenol U 0.0625 0.442 1 02/02/2017 15:15 WG947910
4,6-Dinitro-2-methylphenol U 0.164 0.442 1 02/02/2017 15:15 WG947910
2,4-Dinitrophenol U 0.130 0.442 1 02/02/2017 15:15 WG947910
2-Nitrophenol U 0.0172 0.442 1 02/02/2017 15:15 WG947910
4-Nitrophenol U 0.0696 0.442 1 02/02/2017 15:15 WG947910
Pentachlorophenol U 0.0637 0.442 1 02/02/2017 15:15 WG947910
Phenol U 0.00922 0.442 1 02/02/2017 15:15 WG947910
2,4,6-Trichlorophenol U 0.0103 0.442 1 02/02/2017 15:15 WG947910
(S) 2-Fluorophenol 31.6 20.0-120 02/02/2017 15:15 WG947910
(S) Phenol-d5 40.3 20.0-120 02/02/2017 15:15 WG947910
(S) Nitrobenzene-d5 36.8 18.0-125 02/02/2017 15:15 WG947910
(S) 2-Fluorobiphenyl 52.8 28.0-120 02/02/2017 15:15 WG947910
(S) 2,4,6-Tribromophenol 79.7 17.0-137 02/02/2017 15:15 WG947910
(S) p-Terphenyl-d14 81.2 13.0-131 02/02/2017 15:15 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 25 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L886597
B-9
Collected date/time: 01/24/17 14:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.1 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0695 0.00329 0.0235 1 01/30/2017 12:34 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.186 0.587 5 02/03/2017 15:49 WG948015
Arsenic 2.86 0.0147 0.587 5 02/03/2017 15:49 WG948015
Beryllium 0.312 J 0.0705 0.587 5 02/03/2017 15:49 WG948015
Cadmium U 0.0940 0.587 5 02/03/2017 15:49 WG948015
Chromium 16.2 0.317 0.587 5 02/03/2017 15:49 WG948015
Copper 11.7 0.305 0.587 5 02/03/2017 15:49 WG948015
Lead 17.9 0.141 0.587 5 02/03/2017 15:49 WG948015
Manganese 78.0 0.147 1.17 5 02/03/2017 15:49 WG948015
Nickel 4.80 0.206 0.587 5 02/03/2017 15:49 WG948015
Selenium 0.927 0.223 0.587 5 02/03/2017 15:49 WG948015
Silver U 0.182 0.587 5 02/03/2017 15:49 WG948015
Thallium 0.213 J 0.112 0.587 5 02/03/2017 15:49 WG948015
Zinc 20.8 1.50 5.87 5 02/03/2017 15:49 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0138 J 0.0119 0.0593 1.01 02/01/2017 00:21 WG947760
Acrylonitrile U 0.00213 0.0119 1.01 02/01/2017 00:21 WG947760
Benzene 0.000571 J 0.000321 0.00119 1.01 02/01/2017 00:21 WG947760
Bromobenzene U 0.000337 0.00119 1.01 02/01/2017 00:21 WG947760
Bromodichloromethane U 0.000301 0.00119 1.01 02/01/2017 00:21 WG947760
Bromoform U 0.000503 0.00119 1.01 02/01/2017 00:21 WG947760
Bromomethane U 0.00159 0.00593 1.01 02/01/2017 00:21 WG947760
n-Butylbenzene U 0.000305 0.00119 1.01 02/01/2017 00:21 WG947760
sec-Butylbenzene U 0.000238 0.00119 1.01 02/01/2017 00:21 WG947760
tert-Butylbenzene U 0.000244 0.00119 1.01 02/01/2017 00:21 WG947760
Carbon tetrachloride U 0.000389 0.00119 1.01 02/01/2017 00:21 WG947760
Chlorobenzene U 0.000251 0.00119 1.01 02/01/2017 00:21 WG947760
Chlorodibromomethane U 0.000443 0.00119 1.01 02/01/2017 00:21 WG947760
Chloroethane U 0.00112 0.00593 1.01 02/01/2017 00:21 WG947760
2-Chloroethyl vinyl ether U 0.00277 0.0593 1.01 02/01/2017 00:21 WG947760
Chloroform U 0.000271 0.00593 1.01 02/01/2017 00:21 WG947760
Chloromethane U 0.000445 0.00297 1.01 02/01/2017 00:21 WG947760
2-Chlorotoluene U 0.000357 0.00119 1.01 02/01/2017 00:21 WG947760
4-Chlorotoluene U 0.000284 0.00119 1.01 02/01/2017 00:21 WG947760
1,2-Dibromo-3-Chloropropane U 0.00125 0.00593 1.01 02/01/2017 00:21 WG947760
1,2-Dibromoethane U 0.000406 0.00119 1.01 02/01/2017 00:21 WG947760
Dibromomethane U 0.000453 0.00119 1.01 02/01/2017 00:21 WG947760
1,2-Dichlorobenzene U 0.000362 0.00119 1.01 02/01/2017 00:21 WG947760
1,3-Dichlorobenzene U 0.000283 0.00119 1.01 02/01/2017 00:21 WG947760
1,4-Dichlorobenzene U 0.000268 0.00119 1.01 02/01/2017 00:21 WG947760
Dichlorodifluoromethane U 0.000846 0.00593 1.01 02/01/2017 00:21 WG947760
1,1-Dichloroethane U 0.000236 0.00119 1.01 02/01/2017 00:21 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L886597
B-9
Collected date/time: 01/24/17 14:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000315 0.00119 1.01 02/01/2017 00:21 WG947760
1,1-Dichloroethene U 0.000359 0.00119 1.01 02/01/2017 00:21 WG947760
cis-1,2-Dichloroethene U 0.000278 0.00119 1.01 02/01/2017 00:21 WG947760
trans-1,2-Dichloroethene U 0.000314 0.00119 1.01 02/01/2017 00:21 WG947760
1,2-Dichloropropane U 0.000425 0.00119 1.01 02/01/2017 00:21 WG947760
1,1-Dichloropropene U 0.000376 0.00119 1.01 02/01/2017 00:21 WG947760
1,3-Dichloropropane U 0.000246 0.00119 1.01 02/01/2017 00:21 WG947760
cis-1,3-Dichloropropene U 0.000311 0.00119 1.01 02/01/2017 00:21 WG947760
trans-1,3-Dichloropropene U 0.000317 0.00119 1.01 02/01/2017 00:21 WG947760
2,2-Dichloropropane U 0.000331 0.00119 1.01 02/01/2017 00:21 WG947760
Di-isopropyl ether U 0.000294 0.00119 1.01 02/01/2017 00:21 WG947760
Ethylbenzene U 0.000352 0.00119 1.01 02/01/2017 00:21 WG947760
Hexachloro-1,3-butadiene U 0.000405 0.00119 1.01 02/01/2017 00:21 WG947760
Isopropylbenzene U 0.000288 0.00119 1.01 02/01/2017 00:21 WG947760
p-Isopropyltoluene U 0.000242 0.00119 1.01 02/01/2017 00:21 WG947760
2-Butanone (MEK)U 0.00556 0.0119 1.01 02/01/2017 00:21 WG947760
Methylene Chloride U 0.00119 0.00593 1.01 02/01/2017 00:21 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00223 0.0119 1.01 02/01/2017 00:21 WG947760
Methyl tert-butyl ether U 0.000251 0.00119 1.01 02/01/2017 00:21 WG947760
Naphthalene U 0.00119 0.00593 1.01 02/01/2017 00:21 WG947760
n-Propylbenzene U 0.000244 0.00119 1.01 02/01/2017 00:21 WG947760
Styrene U 0.000277 0.00119 1.01 02/01/2017 00:21 WG947760
1,1,1,2-Tetrachloroethane U 0.000314 0.00119 1.01 02/01/2017 00:21 WG947760
1,1,2,2-Tetrachloroethane U 0.000433 0.00119 1.01 02/01/2017 00:21 WG947760
Tetrachloroethene U 0.000328 0.00119 1.01 02/01/2017 00:21 WG947760
Toluene U 0.000515 0.00593 1.01 02/01/2017 00:21 WG947760
1,2,3-Trichlorobenzene U 0.000363 0.00119 1.01 02/01/2017 00:21 WG947760
1,2,4-Trichlorobenzene U 0.000461 0.00119 1.01 02/01/2017 00:21 WG947760
1,1,1-Trichloroethane U 0.000340 0.00119 1.01 02/01/2017 00:21 WG947760
1,1,2-Trichloroethane U 0.000329 0.00119 1.01 02/01/2017 00:21 WG947760
Trichloroethene U 0.000331 0.00119 1.01 02/01/2017 00:21 WG947760
Trichlorofluoromethane U 0.000453 0.00593 1.01 02/01/2017 00:21 WG947760
1,2,3-Trichloropropane U 0.000879 0.00297 1.01 02/01/2017 00:21 WG947760
1,2,4-Trimethylbenzene U 0.000250 0.00119 1.01 02/01/2017 00:21 WG947760
1,3,5-Trimethylbenzene U 0.000316 0.00119 1.01 02/01/2017 00:21 WG947760
Vinyl chloride U 0.000345 0.00119 1.01 02/01/2017 00:21 WG947760
Xylenes, Total U 0.000828 0.00356 1.01 02/01/2017 00:21 WG947760
(S) Toluene-d8 106 80.0-120 02/01/2017 00:21 WG947760
(S) Dibromofluoromethane 102 74.0-131 02/01/2017 00:21 WG947760
(S) a,a,a-Trifluorotoluene 102 80.0-120 02/01/2017 00:21 WG947760
(S) 4-Bromofluorobenzene 97.5 64.0-132 02/01/2017 00:21 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00754 0.0388 1 02/02/2017 17:24 WG947910
Acenaphthylene U 0.00788 0.0388 1 02/02/2017 17:24 WG947910
Anthracene U 0.00742 0.0388 1 02/02/2017 17:24 WG947910
Benzidine U J4 0.0748 0.391 1 02/02/2017 17:24 WG947910
Benzo(a)anthracene U 0.00503 0.0388 1 02/02/2017 17:24 WG947910
Benzo(b)fluoranthene U 0.00816 0.0388 1 02/02/2017 17:24 WG947910
Benzo(k)fluoranthene U 0.00684 0.0388 1 02/02/2017 17:24 WG947910
Benzo(g,h,i)perylene U 0.00847 0.0388 1 02/02/2017 17:24 WG947910
Benzo(a)pyrene U 0.00644 0.0388 1 02/02/2017 17:24 WG947910
Bis(2-chlorethoxy)methane U 0.00905 0.391 1 02/02/2017 17:24 WG947910
Bis(2-chloroethyl)ether U 0.0105 0.391 1 02/02/2017 17:24 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 27 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L886597
B-9
Collected date/time: 01/24/17 14:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00893 0.391 1 02/02/2017 17:24 WG947910
4-Bromophenyl-phenylether U 0.0134 0.391 1 02/02/2017 17:24 WG947910
2-Chloronaphthalene U 0.00751 0.0388 1 02/02/2017 17:24 WG947910
4-Chlorophenyl-phenylether U 0.00737 0.391 1 02/02/2017 17:24 WG947910
Chrysene U 0.00652 0.0388 1 02/02/2017 17:24 WG947910
Dibenz(a,h)anthracene U 0.00964 0.0388 1 02/02/2017 17:24 WG947910
3,3-Dichlorobenzidine U 0.0933 0.391 1 02/02/2017 17:24 WG947910
2,4-Dinitrotoluene U 0.00713 0.391 1 02/02/2017 17:24 WG947910
2,6-Dinitrotoluene U 0.00866 0.391 1 02/02/2017 17:24 WG947910
Fluoranthene U 0.00583 0.0388 1 02/02/2017 17:24 WG947910
Fluorene U 0.00801 0.0388 1 02/02/2017 17:24 WG947910
Hexachlorobenzene U 0.0101 0.391 1 02/02/2017 17:24 WG947910
Hexachloro-1,3-butadiene U 0.0117 0.391 1 02/02/2017 17:24 WG947910
Hexachlorocyclopentadiene U 0.0690 0.391 1 02/02/2017 17:24 WG947910
Hexachloroethane U 0.0157 0.391 1 02/02/2017 17:24 WG947910
Indeno(1,2,3-cd)pyrene U 0.00907 0.0388 1 02/02/2017 17:24 WG947910
Isophorone U 0.00613 0.391 1 02/02/2017 17:24 WG947910
Naphthalene U 0.0104 0.0388 1 02/02/2017 17:24 WG947910
Nitrobenzene U 0.00816 0.391 1 02/02/2017 17:24 WG947910
n-Nitrosodimethylamine U 0.0760 0.391 1 02/02/2017 17:24 WG947910
n-Nitrosodiphenylamine U 0.00698 0.391 1 02/02/2017 17:24 WG947910
n-Nitrosodi-n-propylamine U 0.0106 0.391 1 02/02/2017 17:24 WG947910
Phenanthrene U 0.00620 0.0388 1 02/02/2017 17:24 WG947910
Benzylbutyl phthalate U 0.0121 0.391 1 02/02/2017 17:24 WG947910
Bis(2-ethylhexyl)phthalate U 0.0141 0.391 1 02/02/2017 17:24 WG947910
Di-n-butyl phthalate U 0.0128 0.391 1 02/02/2017 17:24 WG947910
Diethyl phthalate U 0.00812 0.391 1 02/02/2017 17:24 WG947910
Dimethyl phthalate U 0.00634 0.391 1 02/02/2017 17:24 WG947910
Di-n-octyl phthalate U 0.0107 0.391 1 02/02/2017 17:24 WG947910
Pyrene U 0.0144 0.0388 1 02/02/2017 17:24 WG947910
1,2,4-Trichlorobenzene U 0.0103 0.391 1 02/02/2017 17:24 WG947910
Aniline U 0.0376 0.391 1 02/02/2017 17:24 WG947910
4-Chloro-3-methylphenol U 0.00560 0.391 1 02/02/2017 17:24 WG947910
2-Chlorophenol U 0.00976 0.391 1 02/02/2017 17:24 WG947910
2,4-Dichlorophenol U 0.00876 0.391 1 02/02/2017 17:24 WG947910
2,4-Dimethylphenol U 0.0553 0.391 1 02/02/2017 17:24 WG947910
4,6-Dinitro-2-methylphenol U 0.146 0.391 1 02/02/2017 17:24 WG947910
2,4-Dinitrophenol U 0.115 0.391 1 02/02/2017 17:24 WG947910
2-Nitrophenol U 0.0153 0.391 1 02/02/2017 17:24 WG947910
4-Nitrophenol U 0.0617 0.391 1 02/02/2017 17:24 WG947910
Pentachlorophenol U 0.0564 0.391 1 02/02/2017 17:24 WG947910
Phenol U 0.00816 0.391 1 02/02/2017 17:24 WG947910
2,4,6-Trichlorophenol U 0.00915 0.391 1 02/02/2017 17:24 WG947910
(S) 2-Fluorophenol 39.9 20.0-120 02/02/2017 17:24 WG947910
(S) Phenol-d5 49.1 20.0-120 02/02/2017 17:24 WG947910
(S) Nitrobenzene-d5 42.5 18.0-125 02/02/2017 17:24 WG947910
(S) 2-Fluorobiphenyl 61.6 28.0-120 02/02/2017 17:24 WG947910
(S) 2,4,6-Tribromophenol 78.7 17.0-137 02/02/2017 17:24 WG947910
(S) p-Terphenyl-d14 84.2 13.0-131 02/02/2017 17:24 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 28 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L886597
B-10
Collected date/time: 01/25/17 09:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.5 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0483 0.00335 0.0239 1 01/30/2017 12:37 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.189 0.599 5 02/03/2017 15:53 WG948015
Arsenic 3.51 0.0150 0.599 5 02/03/2017 15:53 WG948015
Beryllium 0.264 J 0.0718 0.599 5 02/03/2017 15:53 WG948015
Cadmium 0.281 J 0.0958 0.599 5 02/03/2017 15:53 WG948015
Chromium 18.3 0.323 0.599 5 02/03/2017 15:53 WG948015
Copper 27.5 0.311 0.599 5 02/03/2017 15:53 WG948015
Lead 23.6 0.144 0.599 5 02/03/2017 15:53 WG948015
Manganese 99.7 0.150 1.20 5 02/03/2017 15:53 WG948015
Nickel 3.25 0.209 0.599 5 02/03/2017 15:53 WG948015
Selenium 0.653 0.227 0.599 5 02/03/2017 15:53 WG948015
Silver U 0.186 0.599 5 02/03/2017 15:53 WG948015
Thallium 0.181 J 0.114 0.599 5 02/03/2017 15:53 WG948015
Zinc 39.0 1.53 5.99 5 02/03/2017 15:53 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0263 J 0.0120 0.0599 1 02/01/2017 00:44 WG947760
Acrylonitrile U 0.00214 0.0120 1 02/01/2017 00:44 WG947760
Benzene U 0.000323 0.00120 1 02/01/2017 00:44 WG947760
Bromobenzene U 0.000340 0.00120 1 02/01/2017 00:44 WG947760
Bromodichloromethane U 0.000304 0.00120 1 02/01/2017 00:44 WG947760
Bromoform U 0.000508 0.00120 1 02/01/2017 00:44 WG947760
Bromomethane U 0.00160 0.00599 1 02/01/2017 00:44 WG947760
n-Butylbenzene U 0.000309 0.00120 1 02/01/2017 00:44 WG947760
sec-Butylbenzene U 0.000241 0.00120 1 02/01/2017 00:44 WG947760
tert-Butylbenzene U 0.000247 0.00120 1 02/01/2017 00:44 WG947760
Carbon tetrachloride U 0.000393 0.00120 1 02/01/2017 00:44 WG947760
Chlorobenzene U 0.000254 0.00120 1 02/01/2017 00:44 WG947760
Chlorodibromomethane U 0.000447 0.00120 1 02/01/2017 00:44 WG947760
Chloroethane U 0.00113 0.00599 1 02/01/2017 00:44 WG947760
2-Chloroethyl vinyl ether U 0.00280 0.0599 1 02/01/2017 00:44 WG947760
Chloroform U 0.000274 0.00599 1 02/01/2017 00:44 WG947760
Chloromethane U 0.000449 0.00299 1 02/01/2017 00:44 WG947760
2-Chlorotoluene U 0.000360 0.00120 1 02/01/2017 00:44 WG947760
4-Chlorotoluene U 0.000287 0.00120 1 02/01/2017 00:44 WG947760
1,2-Dibromo-3-Chloropropane U 0.00126 0.00599 1 02/01/2017 00:44 WG947760
1,2-Dibromoethane U 0.000411 0.00120 1 02/01/2017 00:44 WG947760
Dibromomethane U 0.000457 0.00120 1 02/01/2017 00:44 WG947760
1,2-Dichlorobenzene U 0.000365 0.00120 1 02/01/2017 00:44 WG947760
1,3-Dichlorobenzene U 0.000286 0.00120 1 02/01/2017 00:44 WG947760
1,4-Dichlorobenzene U 0.000271 0.00120 1 02/01/2017 00:44 WG947760
Dichlorodifluoromethane U 0.000854 0.00599 1 02/01/2017 00:44 WG947760
1,1-Dichloroethane U 0.000238 0.00120 1 02/01/2017 00:44 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L886597
B-10
Collected date/time: 01/25/17 09:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000317 0.00120 1 02/01/2017 00:44 WG947760
1,1-Dichloroethene U 0.000363 0.00120 1 02/01/2017 00:44 WG947760
cis-1,2-Dichloroethene U 0.000281 0.00120 1 02/01/2017 00:44 WG947760
trans-1,2-Dichloroethene U 0.000316 0.00120 1 02/01/2017 00:44 WG947760
1,2-Dichloropropane U 0.000429 0.00120 1 02/01/2017 00:44 WG947760
1,1-Dichloropropene U 0.000379 0.00120 1 02/01/2017 00:44 WG947760
1,3-Dichloropropane U 0.000248 0.00120 1 02/01/2017 00:44 WG947760
cis-1,3-Dichloropropene U 0.000314 0.00120 1 02/01/2017 00:44 WG947760
trans-1,3-Dichloropropene U 0.000320 0.00120 1 02/01/2017 00:44 WG947760
2,2-Dichloropropane U 0.000334 0.00120 1 02/01/2017 00:44 WG947760
Di-isopropyl ether U 0.000297 0.00120 1 02/01/2017 00:44 WG947760
Ethylbenzene U 0.000356 0.00120 1 02/01/2017 00:44 WG947760
Hexachloro-1,3-butadiene U 0.000409 0.00120 1 02/01/2017 00:44 WG947760
Isopropylbenzene U 0.000291 0.00120 1 02/01/2017 00:44 WG947760
p-Isopropyltoluene U 0.000244 0.00120 1 02/01/2017 00:44 WG947760
2-Butanone (MEK)U 0.00560 0.0120 1 02/01/2017 00:44 WG947760
Methylene Chloride U 0.00120 0.00599 1 02/01/2017 00:44 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00225 0.0120 1 02/01/2017 00:44 WG947760
Methyl tert-butyl ether U 0.000254 0.00120 1 02/01/2017 00:44 WG947760
Naphthalene U 0.00120 0.00599 1 02/01/2017 00:44 WG947760
n-Propylbenzene U 0.000247 0.00120 1 02/01/2017 00:44 WG947760
Styrene U 0.000280 0.00120 1 02/01/2017 00:44 WG947760
1,1,1,2-Tetrachloroethane U 0.000316 0.00120 1 02/01/2017 00:44 WG947760
1,1,2,2-Tetrachloroethane U 0.000437 0.00120 1 02/01/2017 00:44 WG947760
Tetrachloroethene 0.000409 J 0.000330 0.00120 1 02/01/2017 00:44 WG947760
Toluene U 0.000520 0.00599 1 02/01/2017 00:44 WG947760
1,2,3-Trichlorobenzene U 0.000366 0.00120 1 02/01/2017 00:44 WG947760
1,2,4-Trichlorobenzene U 0.000464 0.00120 1 02/01/2017 00:44 WG947760
1,1,1-Trichloroethane U 0.000342 0.00120 1 02/01/2017 00:44 WG947760
1,1,2-Trichloroethane U 0.000332 0.00120 1 02/01/2017 00:44 WG947760
Trichloroethene U 0.000334 0.00120 1 02/01/2017 00:44 WG947760
Trichlorofluoromethane U 0.000457 0.00599 1 02/01/2017 00:44 WG947760
1,2,3-Trichloropropane U 0.000887 0.00299 1 02/01/2017 00:44 WG947760
1,2,4-Trimethylbenzene U 0.000253 0.00120 1 02/01/2017 00:44 WG947760
1,3,5-Trimethylbenzene U 0.000318 0.00120 1 02/01/2017 00:44 WG947760
Vinyl chloride U 0.000348 0.00120 1 02/01/2017 00:44 WG947760
Xylenes, Total U 0.000836 0.00359 1 02/01/2017 00:44 WG947760
(S) Toluene-d8 106 80.0-120 02/01/2017 00:44 WG947760
(S) Dibromofluoromethane 105 74.0-131 02/01/2017 00:44 WG947760
(S) a,a,a-Trifluorotoluene 104 80.0-120 02/01/2017 00:44 WG947760
(S) 4-Bromofluorobenzene 94.9 64.0-132 02/01/2017 00:44 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 5.00 0.153 0.790 20 02/03/2017 17:14 WG947910
Acenaphthylene U 0.160 0.790 20 02/03/2017 17:14 WG947910
Anthracene 7.24 0.151 0.790 20 02/03/2017 17:14 WG947910
Benzidine U J4 1.52 7.97 20 02/03/2017 17:14 WG947910
Benzo(a)anthracene 14.9 0.102 0.790 20 02/03/2017 17:14 WG947910
Benzo(b)fluoranthene 18.0 0.166 0.790 20 02/03/2017 17:14 WG947910
Benzo(k)fluoranthene 5.34 0.139 0.790 20 02/03/2017 17:14 WG947910
Benzo(g,h,i)perylene 3.84 0.172 0.790 20 02/03/2017 17:14 WG947910
Benzo(a)pyrene 11.6 0.132 0.790 20 02/03/2017 17:14 WG947910
Bis(2-chlorethoxy)methane U 0.184 7.97 20 02/03/2017 17:14 WG947910
Bis(2-chloroethyl)ether U 0.214 7.97 20 02/03/2017 17:14 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 30 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L886597
B-10
Collected date/time: 01/25/17 09:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.182 7.97 20 02/03/2017 17:14 WG947910
4-Bromophenyl-phenylether U 0.273 7.97 20 02/03/2017 17:14 WG947910
2-Chloronaphthalene U 0.153 0.790 20 02/03/2017 17:14 WG947910
4-Chlorophenyl-phenylether U 0.150 7.97 20 02/03/2017 17:14 WG947910
Chrysene 13.6 0.133 0.790 20 02/03/2017 17:14 WG947910
Dibenz(a,h)anthracene 1.44 0.196 0.790 20 02/03/2017 17:14 WG947910
3,3-Dichlorobenzidine U 1.90 7.97 20 02/03/2017 17:14 WG947910
2,4-Dinitrotoluene U 0.145 7.97 20 02/03/2017 17:14 WG947910
2,6-Dinitrotoluene U 0.176 7.97 20 02/03/2017 17:14 WG947910
Fluoranthene 37.8 0.119 0.790 20 02/03/2017 17:14 WG947910
Fluorene 3.08 0.163 0.790 20 02/03/2017 17:14 WG947910
Hexachlorobenzene U 0.205 7.97 20 02/03/2017 17:14 WG947910
Hexachloro-1,3-butadiene U 0.239 7.97 20 02/03/2017 17:14 WG947910
Hexachlorocyclopentadiene U 1.40 7.97 20 02/03/2017 17:14 WG947910
Hexachloroethane U 0.321 7.97 20 02/03/2017 17:14 WG947910
Indeno(1,2,3-cd)pyrene 4.38 0.184 0.790 20 02/03/2017 17:14 WG947910
Isophorone U 0.124 7.97 20 02/03/2017 17:14 WG947910
Naphthalene 0.336 J 0.213 0.790 20 02/03/2017 17:14 WG947910
Nitrobenzene U 0.166 7.97 20 02/03/2017 17:14 WG947910
n-Nitrosodimethylamine U 1.54 7.97 20 02/03/2017 17:14 WG947910
n-Nitrosodiphenylamine U 0.142 7.97 20 02/03/2017 17:14 WG947910
n-Nitrosodi-n-propylamine U 0.217 7.97 20 02/03/2017 17:14 WG947910
Phenanthrene 30.9 0.127 0.790 20 02/03/2017 17:14 WG947910
Benzylbutyl phthalate U 0.247 7.97 20 02/03/2017 17:14 WG947910
Bis(2-ethylhexyl)phthalate U 0.287 7.97 20 02/03/2017 17:14 WG947910
Di-n-butyl phthalate U 0.261 7.97 20 02/03/2017 17:14 WG947910
Diethyl phthalate U 0.165 7.97 20 02/03/2017 17:14 WG947910
Dimethyl phthalate U 0.129 7.97 20 02/03/2017 17:14 WG947910
Di-n-octyl phthalate U 0.217 7.97 20 02/03/2017 17:14 WG947910
Pyrene 24.5 0.294 0.790 20 02/03/2017 17:14 WG947910
1,2,4-Trichlorobenzene U 0.209 7.97 20 02/03/2017 17:14 WG947910
Aniline U 0.766 7.97 20 02/03/2017 17:14 WG947910
4-Chloro-3-methylphenol U 0.114 7.97 20 02/03/2017 17:14 WG947910
2-Chlorophenol U 0.199 7.97 20 02/03/2017 17:14 WG947910
2,4-Dichlorophenol U 0.178 7.97 20 02/03/2017 17:14 WG947910
2,4-Dimethylphenol U 1.13 7.97 20 02/03/2017 17:14 WG947910
4,6-Dinitro-2-methylphenol U 2.97 7.97 20 02/03/2017 17:14 WG947910
2,4-Dinitrophenol U 2.35 7.97 20 02/03/2017 17:14 WG947910
2-Nitrophenol U 0.311 7.97 20 02/03/2017 17:14 WG947910
4-Nitrophenol U 1.26 7.97 20 02/03/2017 17:14 WG947910
Pentachlorophenol U 1.15 7.97 20 02/03/2017 17:14 WG947910
Phenol U 0.166 7.97 20 02/03/2017 17:14 WG947910
2,4,6-Trichlorophenol U 0.187 7.97 20 02/03/2017 17:14 WG947910
(S) 2-Fluorophenol 70.3 20.0-120 02/03/2017 17:14 WG947910
(S) Phenol-d5 78.1 20.0-120 02/03/2017 17:14 WG947910
(S) Nitrobenzene-d5 75.0 18.0-125 02/03/2017 17:14 WG947910
(S) 2-Fluorobiphenyl 76.3 28.0-120 02/03/2017 17:14 WG947910
(S) 2,4,6-Tribromophenol 73.6 17.0-137 02/03/2017 17:14 WG947910
(S) p-Terphenyl-d14 61.7 13.0-131 02/03/2017 17:14 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 31 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L886597
B-11
Collected date/time: 01/25/17 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.6 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0622 0.00356 0.0254 1 01/30/2017 12:39 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.201 0.636 5 02/03/2017 15:56 WG948015
Arsenic 3.08 0.0159 0.636 5 02/03/2017 15:56 WG948015
Beryllium 0.394 J 0.0763 0.636 5 02/03/2017 15:56 WG948015
Cadmium 0.120 J 0.102 0.636 5 02/03/2017 15:56 WG948015
Chromium 25.5 0.343 0.636 5 02/03/2017 15:56 WG948015
Copper 38.6 0.331 0.636 5 02/03/2017 15:56 WG948015
Lead 27.8 0.153 0.636 5 02/03/2017 15:56 WG948015
Manganese 219 0.318 2.54 10 02/04/2017 13:05 WG948015
Nickel 4.62 0.223 0.636 5 02/03/2017 15:56 WG948015
Selenium 1.35 0.242 0.636 5 02/03/2017 15:56 WG948015
Silver U 0.197 0.636 5 02/03/2017 15:56 WG948015
Thallium 0.234 J 0.121 0.636 5 02/03/2017 15:56 WG948015
Zinc 39.1 1.63 6.36 5 02/03/2017 15:56 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0317 J 0.0127 0.0636 1 02/01/2017 01:07 WG947760
Acrylonitrile U 0.00228 0.0127 1 02/01/2017 01:07 WG947760
Benzene U 0.000343 0.00127 1 02/01/2017 01:07 WG947760
Bromobenzene U 0.000361 0.00127 1 02/01/2017 01:07 WG947760
Bromodichloromethane U 0.000323 0.00127 1 02/01/2017 01:07 WG947760
Bromoform U 0.000539 0.00127 1 02/01/2017 01:07 WG947760
Bromomethane U 0.00170 0.00636 1 02/01/2017 01:07 WG947760
n-Butylbenzene U 0.000328 0.00127 1 02/01/2017 01:07 WG947760
sec-Butylbenzene U 0.000256 0.00127 1 02/01/2017 01:07 WG947760
tert-Butylbenzene U 0.000262 0.00127 1 02/01/2017 01:07 WG947760
Carbon tetrachloride U 0.000417 0.00127 1 02/01/2017 01:07 WG947760
Chlorobenzene U 0.000270 0.00127 1 02/01/2017 01:07 WG947760
Chlorodibromomethane U 0.000474 0.00127 1 02/01/2017 01:07 WG947760
Chloroethane U 0.00120 0.00636 1 02/01/2017 01:07 WG947760
2-Chloroethyl vinyl ether U 0.00298 0.0636 1 02/01/2017 01:07 WG947760
Chloroform U 0.000291 0.00636 1 02/01/2017 01:07 WG947760
Chloromethane U 0.000477 0.00318 1 02/01/2017 01:07 WG947760
2-Chlorotoluene U 0.000383 0.00127 1 02/01/2017 01:07 WG947760
4-Chlorotoluene U 0.000305 0.00127 1 02/01/2017 01:07 WG947760
1,2-Dibromo-3-Chloropropane U 0.00134 0.00636 1 02/01/2017 01:07 WG947760
1,2-Dibromoethane U 0.000436 0.00127 1 02/01/2017 01:07 WG947760
Dibromomethane U 0.000486 0.00127 1 02/01/2017 01:07 WG947760
1,2-Dichlorobenzene U 0.000388 0.00127 1 02/01/2017 01:07 WG947760
1,3-Dichlorobenzene U 0.000304 0.00127 1 02/01/2017 01:07 WG947760
1,4-Dichlorobenzene U 0.000287 0.00127 1 02/01/2017 01:07 WG947760
Dichlorodifluoromethane U 0.000907 0.00636 1 02/01/2017 01:07 WG947760
1,1-Dichloroethane U 0.000253 0.00127 1 02/01/2017 01:07 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L886597
B-11
Collected date/time: 01/25/17 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000337 0.00127 1 02/01/2017 01:07 WG947760
1,1-Dichloroethene U 0.000385 0.00127 1 02/01/2017 01:07 WG947760
cis-1,2-Dichloroethene U 0.000299 0.00127 1 02/01/2017 01:07 WG947760
trans-1,2-Dichloroethene U 0.000336 0.00127 1 02/01/2017 01:07 WG947760
1,2-Dichloropropane U 0.000455 0.00127 1 02/01/2017 01:07 WG947760
1,1-Dichloropropene U 0.000403 0.00127 1 02/01/2017 01:07 WG947760
1,3-Dichloropropane U 0.000263 0.00127 1 02/01/2017 01:07 WG947760
cis-1,3-Dichloropropene U 0.000333 0.00127 1 02/01/2017 01:07 WG947760
trans-1,3-Dichloropropene U 0.000340 0.00127 1 02/01/2017 01:07 WG947760
2,2-Dichloropropane U 0.000355 0.00127 1 02/01/2017 01:07 WG947760
Di-isopropyl ether U 0.000315 0.00127 1 02/01/2017 01:07 WG947760
Ethylbenzene U 0.000378 0.00127 1 02/01/2017 01:07 WG947760
Hexachloro-1,3-butadiene U 0.000435 0.00127 1 02/01/2017 01:07 WG947760
Isopropylbenzene U 0.000309 0.00127 1 02/01/2017 01:07 WG947760
p-Isopropyltoluene U 0.000259 0.00127 1 02/01/2017 01:07 WG947760
2-Butanone (MEK)U 0.00595 0.0127 1 02/01/2017 01:07 WG947760
Methylene Chloride U 0.00127 0.00636 1 02/01/2017 01:07 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00239 0.0127 1 02/01/2017 01:07 WG947760
Methyl tert-butyl ether U 0.000270 0.00127 1 02/01/2017 01:07 WG947760
Naphthalene U 0.00127 0.00636 1 02/01/2017 01:07 WG947760
n-Propylbenzene U 0.000262 0.00127 1 02/01/2017 01:07 WG947760
Styrene U 0.000298 0.00127 1 02/01/2017 01:07 WG947760
1,1,1,2-Tetrachloroethane U 0.000336 0.00127 1 02/01/2017 01:07 WG947760
1,1,2,2-Tetrachloroethane U 0.000464 0.00127 1 02/01/2017 01:07 WG947760
Tetrachloroethene U 0.000351 0.00127 1 02/01/2017 01:07 WG947760
Toluene U 0.000552 0.00636 1 02/01/2017 01:07 WG947760
1,2,3-Trichlorobenzene U 0.000389 0.00127 1 02/01/2017 01:07 WG947760
1,2,4-Trichlorobenzene U 0.000493 0.00127 1 02/01/2017 01:07 WG947760
1,1,1-Trichloroethane U 0.000364 0.00127 1 02/01/2017 01:07 WG947760
1,1,2-Trichloroethane U 0.000352 0.00127 1 02/01/2017 01:07 WG947760
Trichloroethene U 0.000355 0.00127 1 02/01/2017 01:07 WG947760
Trichlorofluoromethane U 0.000486 0.00636 1 02/01/2017 01:07 WG947760
1,2,3-Trichloropropane U 0.000942 0.00318 1 02/01/2017 01:07 WG947760
1,2,4-Trimethylbenzene U 0.000268 0.00127 1 02/01/2017 01:07 WG947760
1,3,5-Trimethylbenzene U 0.000338 0.00127 1 02/01/2017 01:07 WG947760
Vinyl chloride U 0.000370 0.00127 1 02/01/2017 01:07 WG947760
Xylenes, Total U 0.000888 0.00382 1 02/01/2017 01:07 WG947760
(S) Toluene-d8 105 80.0-120 02/01/2017 01:07 WG947760
(S) Dibromofluoromethane 106 74.0-131 02/01/2017 01:07 WG947760
(S) a,a,a-Trifluorotoluene 101 80.0-120 02/01/2017 01:07 WG947760
(S) 4-Bromofluorobenzene 97.3 64.0-132 02/01/2017 01:07 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00817 0.0420 1 02/02/2017 20:50 WG947910
Acenaphthylene U 0.00853 0.0420 1 02/02/2017 20:50 WG947910
Anthracene U 0.00804 0.0420 1 02/02/2017 20:50 WG947910
Benzidine U J4 0.0810 0.424 1 02/02/2017 20:50 WG947910
Benzo(a)anthracene 0.0134 J 0.00544 0.0420 1 02/02/2017 20:50 WG947910
Benzo(b)fluoranthene 0.0203 J 0.00884 0.0420 1 02/02/2017 20:50 WG947910
Benzo(k)fluoranthene U 0.00740 0.0420 1 02/02/2017 20:50 WG947910
Benzo(g,h,i)perylene U 0.00917 0.0420 1 02/02/2017 20:50 WG947910
Benzo(a)pyrene 0.0126 J 0.00697 0.0420 1 02/02/2017 20:50 WG947910
Bis(2-chlorethoxy)methane U 0.00979 0.424 1 02/02/2017 20:50 WG947910
Bis(2-chloroethyl)ether U 0.0114 0.424 1 02/02/2017 20:50 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L886597
B-11
Collected date/time: 01/25/17 10:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00967 0.424 1 02/02/2017 20:50 WG947910
4-Bromophenyl-phenylether U 0.0145 0.424 1 02/02/2017 20:50 WG947910
2-Chloronaphthalene U 0.00813 0.0420 1 02/02/2017 20:50 WG947910
4-Chlorophenyl-phenylether U 0.00797 0.424 1 02/02/2017 20:50 WG947910
Chrysene 0.0148 J 0.00706 0.0420 1 02/02/2017 20:50 WG947910
Dibenz(a,h)anthracene U 0.0104 0.0420 1 02/02/2017 20:50 WG947910
3,3-Dichlorobenzidine U 0.101 0.424 1 02/02/2017 20:50 WG947910
2,4-Dinitrotoluene U 0.00772 0.424 1 02/02/2017 20:50 WG947910
2,6-Dinitrotoluene U 0.00937 0.424 1 02/02/2017 20:50 WG947910
Fluoranthene 0.0229 J 0.00631 0.0420 1 02/02/2017 20:50 WG947910
Fluorene U 0.00867 0.0420 1 02/02/2017 20:50 WG947910
Hexachlorobenzene U 0.0109 0.424 1 02/02/2017 20:50 WG947910
Hexachloro-1,3-butadiene U 0.0127 0.424 1 02/02/2017 20:50 WG947910
Hexachlorocyclopentadiene U 0.0747 0.424 1 02/02/2017 20:50 WG947910
Hexachloroethane U 0.0170 0.424 1 02/02/2017 20:50 WG947910
Indeno(1,2,3-cd)pyrene U 0.00982 0.0420 1 02/02/2017 20:50 WG947910
Isophorone U 0.00664 0.424 1 02/02/2017 20:50 WG947910
Naphthalene U 0.0113 0.0420 1 02/02/2017 20:50 WG947910
Nitrobenzene U 0.00884 0.424 1 02/02/2017 20:50 WG947910
n-Nitrosodimethylamine U 0.0823 0.424 1 02/02/2017 20:50 WG947910
n-Nitrosodiphenylamine U 0.00755 0.424 1 02/02/2017 20:50 WG947910
n-Nitrosodi-n-propylamine U 0.0115 0.424 1 02/02/2017 20:50 WG947910
Phenanthrene 0.00954 J 0.00672 0.0420 1 02/02/2017 20:50 WG947910
Benzylbutyl phthalate U 0.0131 0.424 1 02/02/2017 20:50 WG947910
Bis(2-ethylhexyl)phthalate U 0.0153 0.424 1 02/02/2017 20:50 WG947910
Di-n-butyl phthalate U 0.0139 0.424 1 02/02/2017 20:50 WG947910
Diethyl phthalate U 0.00879 0.424 1 02/02/2017 20:50 WG947910
Dimethyl phthalate U 0.00687 0.424 1 02/02/2017 20:50 WG947910
Di-n-octyl phthalate U 0.0115 0.424 1 02/02/2017 20:50 WG947910
Pyrene U 0.0156 0.0420 1 02/02/2017 20:50 WG947910
1,2,4-Trichlorobenzene U 0.0111 0.424 1 02/02/2017 20:50 WG947910
Aniline U 0.0407 0.424 1 02/02/2017 20:50 WG947910
4-Chloro-3-methylphenol U 0.00607 0.424 1 02/02/2017 20:50 WG947910
2-Chlorophenol U 0.0106 0.424 1 02/02/2017 20:50 WG947910
2,4-Dichlorophenol U 0.00949 0.424 1 02/02/2017 20:50 WG947910
2,4-Dimethylphenol U 0.0599 0.424 1 02/02/2017 20:50 WG947910
4,6-Dinitro-2-methylphenol U 0.158 0.424 1 02/02/2017 20:50 WG947910
2,4-Dinitrophenol U 0.125 0.424 1 02/02/2017 20:50 WG947910
2-Nitrophenol U 0.0165 0.424 1 02/02/2017 20:50 WG947910
4-Nitrophenol U 0.0668 0.424 1 02/02/2017 20:50 WG947910
Pentachlorophenol U 0.0610 0.424 1 02/02/2017 20:50 WG947910
Phenol U 0.00884 0.424 1 02/02/2017 20:50 WG947910
2,4,6-Trichlorophenol U 0.00991 0.424 1 02/02/2017 20:50 WG947910
(S) 2-Fluorophenol 49.6 20.0-120 02/02/2017 20:50 WG947910
(S) Phenol-d5 67.6 20.0-120 02/02/2017 20:50 WG947910
(S) Nitrobenzene-d5 63.0 18.0-125 02/02/2017 20:50 WG947910
(S) 2-Fluorobiphenyl 76.8 28.0-120 02/02/2017 20:50 WG947910
(S) 2,4,6-Tribromophenol 85.3 17.0-137 02/02/2017 20:50 WG947910
(S) p-Terphenyl-d14 64.7 13.0-131 02/02/2017 20:50 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L886597
B-12
Collected date/time: 01/24/17 10:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.6 1 01/31/2017 10:31 WG948070
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0527 0.00356 0.0255 1 01/30/2017 12:47 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.201 0.636 5 02/03/2017 16:00 WG948015
Arsenic 4.02 0.0159 0.636 5 02/03/2017 16:00 WG948015
Beryllium 0.289 J 0.0764 0.636 5 02/03/2017 16:00 WG948015
Cadmium U 0.102 0.636 5 02/03/2017 16:00 WG948015
Chromium 20.0 0.344 0.636 5 02/03/2017 16:00 WG948015
Copper 20.9 0.331 0.636 5 02/03/2017 16:00 WG948015
Lead 21.5 0.153 0.636 5 02/03/2017 16:00 WG948015
Manganese 78.4 0.159 1.27 5 02/03/2017 16:00 WG948015
Nickel 3.38 0.223 0.636 5 02/03/2017 16:00 WG948015
Selenium 1.14 0.242 0.636 5 02/03/2017 16:00 WG948015
Silver U 0.197 0.636 5 02/03/2017 16:00 WG948015
Thallium 0.187 J 0.121 0.636 5 02/03/2017 16:00 WG948015
Zinc 17.0 1.63 6.36 5 02/03/2017 16:00 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0161 J 0.0127 0.0636 1 02/01/2017 01:30 WG947760
Acrylonitrile U 0.00228 0.0127 1 02/01/2017 01:30 WG947760
Benzene U 0.000344 0.00127 1 02/01/2017 01:30 WG947760
Bromobenzene U 0.000362 0.00127 1 02/01/2017 01:30 WG947760
Bromodichloromethane U 0.000323 0.00127 1 02/01/2017 01:30 WG947760
Bromoform U 0.000540 0.00127 1 02/01/2017 01:30 WG947760
Bromomethane U 0.00171 0.00636 1 02/01/2017 01:30 WG947760
n-Butylbenzene U 0.000328 0.00127 1 02/01/2017 01:30 WG947760
sec-Butylbenzene U 0.000256 0.00127 1 02/01/2017 01:30 WG947760
tert-Butylbenzene U 0.000262 0.00127 1 02/01/2017 01:30 WG947760
Carbon tetrachloride U 0.000418 0.00127 1 02/01/2017 01:30 WG947760
Chlorobenzene U 0.000270 0.00127 1 02/01/2017 01:30 WG947760
Chlorodibromomethane U 0.000475 0.00127 1 02/01/2017 01:30 WG947760
Chloroethane U 0.00120 0.00636 1 02/01/2017 01:30 WG947760
2-Chloroethyl vinyl ether U 0.00298 0.0636 1 02/01/2017 01:30 WG947760
Chloroform U 0.000291 0.00636 1 02/01/2017 01:30 WG947760
Chloromethane U 0.000477 0.00318 1 02/01/2017 01:30 WG947760
2-Chlorotoluene U 0.000383 0.00127 1 02/01/2017 01:30 WG947760
4-Chlorotoluene U 0.000305 0.00127 1 02/01/2017 01:30 WG947760
1,2-Dibromo-3-Chloropropane U 0.00134 0.00636 1 02/01/2017 01:30 WG947760
1,2-Dibromoethane U 0.000437 0.00127 1 02/01/2017 01:30 WG947760
Dibromomethane U 0.000486 0.00127 1 02/01/2017 01:30 WG947760
1,2-Dichlorobenzene U 0.000388 0.00127 1 02/01/2017 01:30 WG947760
1,3-Dichlorobenzene U 0.000304 0.00127 1 02/01/2017 01:30 WG947760
1,4-Dichlorobenzene U 0.000288 0.00127 1 02/01/2017 01:30 WG947760
Dichlorodifluoromethane U 0.000908 0.00636 1 02/01/2017 01:30 WG947760
1,1-Dichloroethane U 0.000253 0.00127 1 02/01/2017 01:30 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L886597
B-12
Collected date/time: 01/24/17 10:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000337 0.00127 1 02/01/2017 01:30 WG947760
1,1-Dichloroethene U 0.000386 0.00127 1 02/01/2017 01:30 WG947760
cis-1,2-Dichloroethene U 0.000299 0.00127 1 02/01/2017 01:30 WG947760
trans-1,2-Dichloroethene U 0.000336 0.00127 1 02/01/2017 01:30 WG947760
1,2-Dichloropropane U 0.000456 0.00127 1 02/01/2017 01:30 WG947760
1,1-Dichloropropene U 0.000404 0.00127 1 02/01/2017 01:30 WG947760
1,3-Dichloropropane U 0.000263 0.00127 1 02/01/2017 01:30 WG947760
cis-1,3-Dichloropropene U 0.000334 0.00127 1 02/01/2017 01:30 WG947760
trans-1,3-Dichloropropene U 0.000340 0.00127 1 02/01/2017 01:30 WG947760
2,2-Dichloropropane U 0.000355 0.00127 1 02/01/2017 01:30 WG947760
Di-isopropyl ether U 0.000316 0.00127 1 02/01/2017 01:30 WG947760
Ethylbenzene U 0.000378 0.00127 1 02/01/2017 01:30 WG947760
Hexachloro-1,3-butadiene U 0.000435 0.00127 1 02/01/2017 01:30 WG947760
Isopropylbenzene U 0.000309 0.00127 1 02/01/2017 01:30 WG947760
p-Isopropyltoluene U 0.000260 0.00127 1 02/01/2017 01:30 WG947760
2-Butanone (MEK)U 0.00596 0.0127 1 02/01/2017 01:30 WG947760
Methylene Chloride U 0.00127 0.00636 1 02/01/2017 01:30 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00239 0.0127 1 02/01/2017 01:30 WG947760
Methyl tert-butyl ether U 0.000270 0.00127 1 02/01/2017 01:30 WG947760
Naphthalene U 0.00127 0.00636 1 02/01/2017 01:30 WG947760
n-Propylbenzene U 0.000262 0.00127 1 02/01/2017 01:30 WG947760
Styrene U 0.000298 0.00127 1 02/01/2017 01:30 WG947760
1,1,1,2-Tetrachloroethane U 0.000336 0.00127 1 02/01/2017 01:30 WG947760
1,1,2,2-Tetrachloroethane U 0.000465 0.00127 1 02/01/2017 01:30 WG947760
Tetrachloroethene U 0.000351 0.00127 1 02/01/2017 01:30 WG947760
Toluene U 0.000552 0.00636 1 02/01/2017 01:30 WG947760
1,2,3-Trichlorobenzene U 0.000390 0.00127 1 02/01/2017 01:30 WG947760
1,2,4-Trichlorobenzene U 0.000494 0.00127 1 02/01/2017 01:30 WG947760
1,1,1-Trichloroethane U 0.000364 0.00127 1 02/01/2017 01:30 WG947760
1,1,2-Trichloroethane U 0.000353 0.00127 1 02/01/2017 01:30 WG947760
Trichloroethene U 0.000355 0.00127 1 02/01/2017 01:30 WG947760
Trichlorofluoromethane U 0.000486 0.00636 1 02/01/2017 01:30 WG947760
1,2,3-Trichloropropane U 0.000943 0.00318 1 02/01/2017 01:30 WG947760
1,2,4-Trimethylbenzene U 0.000269 0.00127 1 02/01/2017 01:30 WG947760
1,3,5-Trimethylbenzene U 0.000339 0.00127 1 02/01/2017 01:30 WG947760
Vinyl chloride U 0.000370 0.00127 1 02/01/2017 01:30 WG947760
Xylenes, Total U 0.000888 0.00382 1 02/01/2017 01:30 WG947760
(S) Toluene-d8 105 80.0-120 02/01/2017 01:30 WG947760
(S) Dibromofluoromethane 106 74.0-131 02/01/2017 01:30 WG947760
(S) a,a,a-Trifluorotoluene 102 80.0-120 02/01/2017 01:30 WG947760
(S) 4-Bromofluorobenzene 96.0 64.0-132 02/01/2017 01:30 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00817 0.0420 1 02/02/2017 15:41 WG947910
Acenaphthylene U 0.00854 0.0420 1 02/02/2017 15:41 WG947910
Anthracene U 0.00804 0.0420 1 02/02/2017 15:41 WG947910
Benzidine U J4 0.0811 0.424 1 02/02/2017 15:41 WG947910
Benzo(a)anthracene U 0.00545 0.0420 1 02/02/2017 15:41 WG947910
Benzo(b)fluoranthene U 0.00885 0.0420 1 02/02/2017 15:41 WG947910
Benzo(k)fluoranthene U 0.00741 0.0420 1 02/02/2017 15:41 WG947910
Benzo(g,h,i)perylene U 0.00918 0.0420 1 02/02/2017 15:41 WG947910
Benzo(a)pyrene U 0.00698 0.0420 1 02/02/2017 15:41 WG947910
Bis(2-chlorethoxy)methane U 0.00980 0.424 1 02/02/2017 15:41 WG947910
Bis(2-chloroethyl)ether U 0.0114 0.424 1 02/02/2017 15:41 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L886597
B-12
Collected date/time: 01/24/17 10:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00967 0.424 1 02/02/2017 15:41 WG947910
4-Bromophenyl-phenylether U 0.0145 0.424 1 02/02/2017 15:41 WG947910
2-Chloronaphthalene U 0.00813 0.0420 1 02/02/2017 15:41 WG947910
4-Chlorophenyl-phenylether U 0.00798 0.424 1 02/02/2017 15:41 WG947910
Chrysene U 0.00706 0.0420 1 02/02/2017 15:41 WG947910
Dibenz(a,h)anthracene U 0.0105 0.0420 1 02/02/2017 15:41 WG947910
3,3-Dichlorobenzidine U 0.101 0.424 1 02/02/2017 15:41 WG947910
2,4-Dinitrotoluene U 0.00773 0.424 1 02/02/2017 15:41 WG947910
2,6-Dinitrotoluene U 0.00938 0.424 1 02/02/2017 15:41 WG947910
Fluoranthene U 0.00631 0.0420 1 02/02/2017 15:41 WG947910
Fluorene U 0.00868 0.0420 1 02/02/2017 15:41 WG947910
Hexachlorobenzene U 0.0109 0.424 1 02/02/2017 15:41 WG947910
Hexachloro-1,3-butadiene U 0.0127 0.424 1 02/02/2017 15:41 WG947910
Hexachlorocyclopentadiene U 0.0747 0.424 1 02/02/2017 15:41 WG947910
Hexachloroethane U 0.0171 0.424 1 02/02/2017 15:41 WG947910
Indeno(1,2,3-cd)pyrene U 0.00983 0.0420 1 02/02/2017 15:41 WG947910
Isophorone U 0.00664 0.424 1 02/02/2017 15:41 WG947910
Naphthalene U 0.0113 0.0420 1 02/02/2017 15:41 WG947910
Nitrobenzene U 0.00885 0.424 1 02/02/2017 15:41 WG947910
n-Nitrosodimethylamine U 0.0824 0.424 1 02/02/2017 15:41 WG947910
n-Nitrosodiphenylamine U 0.00756 0.424 1 02/02/2017 15:41 WG947910
n-Nitrosodi-n-propylamine U 0.0115 0.424 1 02/02/2017 15:41 WG947910
Phenanthrene U 0.00672 0.0420 1 02/02/2017 15:41 WG947910
Benzylbutyl phthalate U 0.0131 0.424 1 02/02/2017 15:41 WG947910
Bis(2-ethylhexyl)phthalate U 0.0153 0.424 1 02/02/2017 15:41 WG947910
Di-n-butyl phthalate U 0.0139 0.424 1 02/02/2017 15:41 WG947910
Diethyl phthalate U 0.00880 0.424 1 02/02/2017 15:41 WG947910
Dimethyl phthalate U 0.00687 0.424 1 02/02/2017 15:41 WG947910
Di-n-octyl phthalate U 0.0115 0.424 1 02/02/2017 15:41 WG947910
Pyrene U 0.0157 0.0420 1 02/02/2017 15:41 WG947910
1,2,4-Trichlorobenzene U 0.0112 0.424 1 02/02/2017 15:41 WG947910
Aniline U 0.0407 0.424 1 02/02/2017 15:41 WG947910
4-Chloro-3-methylphenol U 0.00607 0.424 1 02/02/2017 15:41 WG947910
2-Chlorophenol U 0.0106 0.424 1 02/02/2017 15:41 WG947910
2,4-Dichlorophenol U 0.00950 0.424 1 02/02/2017 15:41 WG947910
2,4-Dimethylphenol U 0.0600 0.424 1 02/02/2017 15:41 WG947910
4,6-Dinitro-2-methylphenol U 0.158 0.424 1 02/02/2017 15:41 WG947910
2,4-Dinitrophenol U 0.125 0.424 1 02/02/2017 15:41 WG947910
2-Nitrophenol U 0.0165 0.424 1 02/02/2017 15:41 WG947910
4-Nitrophenol U 0.0668 0.424 1 02/02/2017 15:41 WG947910
Pentachlorophenol U 0.0611 0.424 1 02/02/2017 15:41 WG947910
Phenol U 0.00885 0.424 1 02/02/2017 15:41 WG947910
2,4,6-Trichlorophenol U 0.00992 0.424 1 02/02/2017 15:41 WG947910
(S) 2-Fluorophenol 32.5 20.0-120 02/02/2017 15:41 WG947910
(S) Phenol-d5 36.7 20.0-120 02/02/2017 15:41 WG947910
(S) Nitrobenzene-d5 35.8 18.0-125 02/02/2017 15:41 WG947910
(S) 2-Fluorobiphenyl 47.9 28.0-120 02/02/2017 15:41 WG947910
(S) 2,4,6-Tribromophenol 65.0 17.0-137 02/02/2017 15:41 WG947910
(S) p-Terphenyl-d14 71.4 13.0-131 02/02/2017 15:41 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 37 of 97
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L886597
B-13
Collected date/time: 01/24/17 10:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.0 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0484 0.00359 0.0256 1 01/30/2017 12:49 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony 0.221 J 0.203 0.641 5 02/03/2017 16:13 WG948015
Arsenic 3.21 0.0160 0.641 5 02/03/2017 16:13 WG948015
Beryllium 0.314 J 0.0769 0.641 5 02/03/2017 16:13 WG948015
Cadmium U 0.103 0.641 5 02/03/2017 16:13 WG948015
Chromium 27.0 0.346 0.641 5 02/03/2017 16:13 WG948015
Copper 18.7 0.333 0.641 5 02/03/2017 16:13 WG948015
Lead 17.9 0.154 0.641 5 02/03/2017 16:13 WG948015
Manganese 115 0.160 1.28 5 02/03/2017 16:13 WG948015
Nickel 5.16 0.224 0.641 5 02/03/2017 16:13 WG948015
Selenium 0.489 J 0.244 0.641 5 02/03/2017 16:13 WG948015
Silver U 0.199 0.641 5 02/03/2017 16:13 WG948015
Thallium 0.232 J 0.122 0.641 5 02/03/2017 16:13 WG948015
Zinc 26.6 1.64 6.41 5 02/03/2017 16:13 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0152 J 0.0128 0.0641 1 02/01/2017 01:52 WG947760
Acrylonitrile U 0.00229 0.0128 1 02/01/2017 01:52 WG947760
Benzene U 0.000346 0.00128 1 02/01/2017 01:52 WG947760
Bromobenzene U 0.000364 0.00128 1 02/01/2017 01:52 WG947760
Bromodichloromethane U 0.000326 0.00128 1 02/01/2017 01:52 WG947760
Bromoform U 0.000544 0.00128 1 02/01/2017 01:52 WG947760
Bromomethane U 0.00172 0.00641 1 02/01/2017 01:52 WG947760
n-Butylbenzene U 0.000331 0.00128 1 02/01/2017 01:52 WG947760
sec-Butylbenzene U 0.000258 0.00128 1 02/01/2017 01:52 WG947760
tert-Butylbenzene U 0.000264 0.00128 1 02/01/2017 01:52 WG947760
Carbon tetrachloride U 0.000420 0.00128 1 02/01/2017 01:52 WG947760
Chlorobenzene U 0.000272 0.00128 1 02/01/2017 01:52 WG947760
Chlorodibromomethane U 0.000478 0.00128 1 02/01/2017 01:52 WG947760
Chloroethane U 0.00121 0.00641 1 02/01/2017 01:52 WG947760
2-Chloroethyl vinyl ether U 0.00300 0.0641 1 02/01/2017 01:52 WG947760
Chloroform U 0.000294 0.00641 1 02/01/2017 01:52 WG947760
Chloromethane U 0.000481 0.00320 1 02/01/2017 01:52 WG947760
2-Chlorotoluene U 0.000386 0.00128 1 02/01/2017 01:52 WG947760
4-Chlorotoluene U 0.000308 0.00128 1 02/01/2017 01:52 WG947760
1,2-Dibromo-3-Chloropropane U 0.00135 0.00641 1 02/01/2017 01:52 WG947760
1,2-Dibromoethane U 0.000440 0.00128 1 02/01/2017 01:52 WG947760
Dibromomethane U 0.000490 0.00128 1 02/01/2017 01:52 WG947760
1,2-Dichlorobenzene U 0.000391 0.00128 1 02/01/2017 01:52 WG947760
1,3-Dichlorobenzene U 0.000306 0.00128 1 02/01/2017 01:52 WG947760
1,4-Dichlorobenzene U 0.000290 0.00128 1 02/01/2017 01:52 WG947760
Dichlorodifluoromethane U 0.000914 0.00641 1 02/01/2017 01:52 WG947760
1,1-Dichloroethane U 0.000255 0.00128 1 02/01/2017 01:52 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L886597
B-13
Collected date/time: 01/24/17 10:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000340 0.00128 1 02/01/2017 01:52 WG947760
1,1-Dichloroethene U 0.000388 0.00128 1 02/01/2017 01:52 WG947760
cis-1,2-Dichloroethene U 0.000301 0.00128 1 02/01/2017 01:52 WG947760
trans-1,2-Dichloroethene U 0.000338 0.00128 1 02/01/2017 01:52 WG947760
1,2-Dichloropropane U 0.000459 0.00128 1 02/01/2017 01:52 WG947760
1,1-Dichloropropene U 0.000406 0.00128 1 02/01/2017 01:52 WG947760
1,3-Dichloropropane U 0.000265 0.00128 1 02/01/2017 01:52 WG947760
cis-1,3-Dichloropropene U 0.000336 0.00128 1 02/01/2017 01:52 WG947760
trans-1,3-Dichloropropene U 0.000342 0.00128 1 02/01/2017 01:52 WG947760
2,2-Dichloropropane U 0.000358 0.00128 1 02/01/2017 01:52 WG947760
Di-isopropyl ether U 0.000318 0.00128 1 02/01/2017 01:52 WG947760
Ethylbenzene U 0.000381 0.00128 1 02/01/2017 01:52 WG947760
Hexachloro-1,3-butadiene U 0.000438 0.00128 1 02/01/2017 01:52 WG947760
Isopropylbenzene U 0.000312 0.00128 1 02/01/2017 01:52 WG947760
p-Isopropyltoluene U 0.000262 0.00128 1 02/01/2017 01:52 WG947760
2-Butanone (MEK)U 0.00600 0.0128 1 02/01/2017 01:52 WG947760
Methylene Chloride U 0.00128 0.00641 1 02/01/2017 01:52 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00241 0.0128 1 02/01/2017 01:52 WG947760
Methyl tert-butyl ether U 0.000272 0.00128 1 02/01/2017 01:52 WG947760
Naphthalene U 0.00128 0.00641 1 02/01/2017 01:52 WG947760
n-Propylbenzene U 0.000264 0.00128 1 02/01/2017 01:52 WG947760
Styrene U 0.000300 0.00128 1 02/01/2017 01:52 WG947760
1,1,1,2-Tetrachloroethane U 0.000338 0.00128 1 02/01/2017 01:52 WG947760
1,1,2,2-Tetrachloroethane U 0.000468 0.00128 1 02/01/2017 01:52 WG947760
Tetrachloroethene U 0.000354 0.00128 1 02/01/2017 01:52 WG947760
Toluene U 0.000556 0.00641 1 02/01/2017 01:52 WG947760
1,2,3-Trichlorobenzene U 0.000392 0.00128 1 02/01/2017 01:52 WG947760
1,2,4-Trichlorobenzene U 0.000497 0.00128 1 02/01/2017 01:52 WG947760
1,1,1-Trichloroethane U 0.000367 0.00128 1 02/01/2017 01:52 WG947760
1,1,2-Trichloroethane U 0.000355 0.00128 1 02/01/2017 01:52 WG947760
Trichloroethene U 0.000358 0.00128 1 02/01/2017 01:52 WG947760
Trichlorofluoromethane U 0.000490 0.00641 1 02/01/2017 01:52 WG947760
1,2,3-Trichloropropane U 0.000950 0.00320 1 02/01/2017 01:52 WG947760
1,2,4-Trimethylbenzene U 0.000270 0.00128 1 02/01/2017 01:52 WG947760
1,3,5-Trimethylbenzene U 0.000341 0.00128 1 02/01/2017 01:52 WG947760
Vinyl chloride U 0.000373 0.00128 1 02/01/2017 01:52 WG947760
Xylenes, Total U 0.000895 0.00385 1 02/01/2017 01:52 WG947760
(S) Toluene-d8 104 80.0-120 02/01/2017 01:52 WG947760
(S) Dibromofluoromethane 104 74.0-131 02/01/2017 01:52 WG947760
(S) a,a,a-Trifluorotoluene 102 80.0-120 02/01/2017 01:52 WG947760
(S) 4-Bromofluorobenzene 99.9 64.0-132 02/01/2017 01:52 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00823 0.0423 1 02/02/2017 18:15 WG947910
Acenaphthylene U 0.00860 0.0423 1 02/02/2017 18:15 WG947910
Anthracene U 0.00810 0.0423 1 02/02/2017 18:15 WG947910
Benzidine U J4 0.0817 0.427 1 02/02/2017 18:15 WG947910
Benzo(a)anthracene 0.0103 J 0.00549 0.0423 1 02/02/2017 18:15 WG947910
Benzo(b)fluoranthene 0.0120 J 0.00891 0.0423 1 02/02/2017 18:15 WG947910
Benzo(k)fluoranthene U 0.00746 0.0423 1 02/02/2017 18:15 WG947910
Benzo(g,h,i)perylene U 0.00924 0.0423 1 02/02/2017 18:15 WG947910
Benzo(a)pyrene 0.00826 J 0.00702 0.0423 1 02/02/2017 18:15 WG947910
Bis(2-chlorethoxy)methane U 0.00987 0.427 1 02/02/2017 18:15 WG947910
Bis(2-chloroethyl)ether U 0.0115 0.427 1 02/02/2017 18:15 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L886597
B-13
Collected date/time: 01/24/17 10:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00974 0.427 1 02/02/2017 18:15 WG947910
4-Bromophenyl-phenylether U 0.0146 0.427 1 02/02/2017 18:15 WG947910
2-Chloronaphthalene U 0.00819 0.0423 1 02/02/2017 18:15 WG947910
4-Chlorophenyl-phenylether U 0.00804 0.427 1 02/02/2017 18:15 WG947910
Chrysene 0.00927 J 0.00711 0.0423 1 02/02/2017 18:15 WG947910
Dibenz(a,h)anthracene U 0.0105 0.0423 1 02/02/2017 18:15 WG947910
3,3-Dichlorobenzidine U 0.102 0.427 1 02/02/2017 18:15 WG947910
2,4-Dinitrotoluene U 0.00778 0.427 1 02/02/2017 18:15 WG947910
2,6-Dinitrotoluene U 0.00945 0.427 1 02/02/2017 18:15 WG947910
Fluoranthene 0.0173 J 0.00636 0.0423 1 02/02/2017 18:15 WG947910
Fluorene U 0.00874 0.0423 1 02/02/2017 18:15 WG947910
Hexachlorobenzene U 0.0110 0.427 1 02/02/2017 18:15 WG947910
Hexachloro-1,3-butadiene U 0.0128 0.427 1 02/02/2017 18:15 WG947910
Hexachlorocyclopentadiene U 0.0752 0.427 1 02/02/2017 18:15 WG947910
Hexachloroethane U 0.0172 0.427 1 02/02/2017 18:15 WG947910
Indeno(1,2,3-cd)pyrene U 0.00990 0.0423 1 02/02/2017 18:15 WG947910
Isophorone U 0.00669 0.427 1 02/02/2017 18:15 WG947910
Naphthalene U 0.0114 0.0423 1 02/02/2017 18:15 WG947910
Nitrobenzene U 0.00891 0.427 1 02/02/2017 18:15 WG947910
n-Nitrosodimethylamine U 0.0829 0.427 1 02/02/2017 18:15 WG947910
n-Nitrosodiphenylamine U 0.00761 0.427 1 02/02/2017 18:15 WG947910
n-Nitrosodi-n-propylamine U 0.0116 0.427 1 02/02/2017 18:15 WG947910
Phenanthrene 0.0131 J 0.00677 0.0423 1 02/02/2017 18:15 WG947910
Benzylbutyl phthalate U 0.0132 0.427 1 02/02/2017 18:15 WG947910
Bis(2-ethylhexyl)phthalate U 0.0154 0.427 1 02/02/2017 18:15 WG947910
Di-n-butyl phthalate U 0.0140 0.427 1 02/02/2017 18:15 WG947910
Diethyl phthalate U 0.00886 0.427 1 02/02/2017 18:15 WG947910
Dimethyl phthalate U 0.00692 0.427 1 02/02/2017 18:15 WG947910
Di-n-octyl phthalate U 0.0116 0.427 1 02/02/2017 18:15 WG947910
Pyrene U 0.0158 0.0423 1 02/02/2017 18:15 WG947910
1,2,4-Trichlorobenzene U 0.0112 0.427 1 02/02/2017 18:15 WG947910
Aniline U 0.0410 0.427 1 02/02/2017 18:15 WG947910
4-Chloro-3-methylphenol U 0.00611 0.427 1 02/02/2017 18:15 WG947910
2-Chlorophenol U 0.0107 0.427 1 02/02/2017 18:15 WG947910
2,4-Dichlorophenol U 0.00956 0.427 1 02/02/2017 18:15 WG947910
2,4-Dimethylphenol U 0.0604 0.427 1 02/02/2017 18:15 WG947910
4,6-Dinitro-2-methylphenol U 0.159 0.427 1 02/02/2017 18:15 WG947910
2,4-Dinitrophenol U 0.126 0.427 1 02/02/2017 18:15 WG947910
2-Nitrophenol U 0.0167 0.427 1 02/02/2017 18:15 WG947910
4-Nitrophenol U 0.0673 0.427 1 02/02/2017 18:15 WG947910
Pentachlorophenol U 0.0615 0.427 1 02/02/2017 18:15 WG947910
Phenol U 0.00891 0.427 1 02/02/2017 18:15 WG947910
2,4,6-Trichlorophenol U 0.00999 0.427 1 02/02/2017 18:15 WG947910
(S) 2-Fluorophenol 75.6 20.0-120 02/02/2017 18:15 WG947910
(S) Phenol-d5 79.2 20.0-120 02/02/2017 18:15 WG947910
(S) Nitrobenzene-d5 75.6 18.0-125 02/02/2017 18:15 WG947910
(S) 2-Fluorobiphenyl 75.7 28.0-120 02/02/2017 18:15 WG947910
(S) 2,4,6-Tribromophenol 81.0 17.0-137 02/02/2017 18:15 WG947910
(S) p-Terphenyl-d14 60.8 13.0-131 02/02/2017 18:15 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L886597
B-14
Collected date/time: 01/25/17 09:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.9 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.926 0.00355 0.0254 1 01/30/2017 12:52 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony 0.363 J 0.200 0.634 5 02/03/2017 16:16 WG948015
Arsenic 4.72 0.0158 0.634 5 02/03/2017 16:16 WG948015
Beryllium 0.531 J 0.304 2.54 20 02/04/2017 13:37 WG948015
Cadmium 0.579 J 0.101 0.634 5 02/03/2017 16:16 WG948015
Chromium 43.4 0.342 0.634 5 02/03/2017 16:16 WG948015
Copper 49.4 0.330 0.634 5 02/03/2017 16:16 WG948015
Lead 119 0.152 0.634 5 02/03/2017 16:16 WG948015
Manganese 163 0.317 2.54 10 02/04/2017 13:09 WG948015
Nickel 6.72 0.222 0.634 5 02/03/2017 16:16 WG948015
Selenium 1.91 0.241 0.634 5 02/03/2017 16:16 WG948015
Silver U 0.197 0.634 5 02/03/2017 16:16 WG948015
Thallium 0.248 J 0.120 0.634 5 02/03/2017 16:16 WG948015
Zinc 145 1.62 6.34 5 02/03/2017 16:16 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0450 J 0.0127 0.0634 1 02/01/2017 02:14 WG947760
Acrylonitrile U 0.00227 0.0127 1 02/01/2017 02:14 WG947760
Benzene 0.000402 J 0.000342 0.00127 1 02/01/2017 02:14 WG947760
Bromobenzene U 0.000360 0.00127 1 02/01/2017 02:14 WG947760
Bromodichloromethane U 0.000322 0.00127 1 02/01/2017 02:14 WG947760
Bromoform U 0.000538 0.00127 1 02/01/2017 02:14 WG947760
Bromomethane U 0.00170 0.00634 1 02/01/2017 02:14 WG947760
n-Butylbenzene U 0.000327 0.00127 1 02/01/2017 02:14 WG947760
sec-Butylbenzene U 0.000255 0.00127 1 02/01/2017 02:14 WG947760
tert-Butylbenzene U 0.000261 0.00127 1 02/01/2017 02:14 WG947760
Carbon tetrachloride U 0.000416 0.00127 1 02/01/2017 02:14 WG947760
Chlorobenzene U 0.000269 0.00127 1 02/01/2017 02:14 WG947760
Chlorodibromomethane U 0.000473 0.00127 1 02/01/2017 02:14 WG947760
Chloroethane U 0.00120 0.00634 1 02/01/2017 02:14 WG947760
2-Chloroethyl vinyl ether U 0.00297 0.0634 1 02/01/2017 02:14 WG947760
Chloroform U 0.000290 0.00634 1 02/01/2017 02:14 WG947760
Chloromethane U 0.000475 0.00317 1 02/01/2017 02:14 WG947760
2-Chlorotoluene U 0.000382 0.00127 1 02/01/2017 02:14 WG947760
4-Chlorotoluene U 0.000304 0.00127 1 02/01/2017 02:14 WG947760
1,2-Dibromo-3-Chloropropane U 0.00133 0.00634 1 02/01/2017 02:14 WG947760
1,2-Dibromoethane U 0.000435 0.00127 1 02/01/2017 02:14 WG947760
Dibromomethane U 0.000484 0.00127 1 02/01/2017 02:14 WG947760
1,2-Dichlorobenzene U 0.000387 0.00127 1 02/01/2017 02:14 WG947760
1,3-Dichlorobenzene U 0.000303 0.00127 1 02/01/2017 02:14 WG947760
1,4-Dichlorobenzene U 0.000287 0.00127 1 02/01/2017 02:14 WG947760
Dichlorodifluoromethane U 0.000904 0.00634 1 02/01/2017 02:14 WG947760
1,1-Dichloroethane U 0.000252 0.00127 1 02/01/2017 02:14 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L886597
B-14
Collected date/time: 01/25/17 09:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000336 0.00127 1 02/01/2017 02:14 WG947760
1,1-Dichloroethene U 0.000384 0.00127 1 02/01/2017 02:14 WG947760
cis-1,2-Dichloroethene U 0.000298 0.00127 1 02/01/2017 02:14 WG947760
trans-1,2-Dichloroethene U 0.000335 0.00127 1 02/01/2017 02:14 WG947760
1,2-Dichloropropane U 0.000454 0.00127 1 02/01/2017 02:14 WG947760
1,1-Dichloropropene U 0.000402 0.00127 1 02/01/2017 02:14 WG947760
1,3-Dichloropropane U 0.000262 0.00127 1 02/01/2017 02:14 WG947760
cis-1,3-Dichloropropene U 0.000332 0.00127 1 02/01/2017 02:14 WG947760
trans-1,3-Dichloropropene U 0.000339 0.00127 1 02/01/2017 02:14 WG947760
2,2-Dichloropropane U 0.000354 0.00127 1 02/01/2017 02:14 WG947760
Di-isopropyl ether U 0.000314 0.00127 1 02/01/2017 02:14 WG947760
Ethylbenzene U 0.000377 0.00127 1 02/01/2017 02:14 WG947760
Hexachloro-1,3-butadiene U 0.000434 0.00127 1 02/01/2017 02:14 WG947760
Isopropylbenzene U 0.000308 0.00127 1 02/01/2017 02:14 WG947760
p-Isopropyltoluene U 0.000259 0.00127 1 02/01/2017 02:14 WG947760
2-Butanone (MEK)0.00767 J 0.00593 0.0127 1 02/01/2017 02:14 WG947760
Methylene Chloride U 0.00127 0.00634 1 02/01/2017 02:14 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00238 0.0127 1 02/01/2017 02:14 WG947760
Methyl tert-butyl ether U 0.000269 0.00127 1 02/01/2017 02:14 WG947760
Naphthalene U 0.00127 0.00634 1 02/01/2017 02:14 WG947760
n-Propylbenzene U 0.000261 0.00127 1 02/01/2017 02:14 WG947760
Styrene U 0.000297 0.00127 1 02/01/2017 02:14 WG947760
1,1,1,2-Tetrachloroethane U 0.000335 0.00127 1 02/01/2017 02:14 WG947760
1,1,2,2-Tetrachloroethane U 0.000463 0.00127 1 02/01/2017 02:14 WG947760
Tetrachloroethene U 0.000350 0.00127 1 02/01/2017 02:14 WG947760
Toluene U 0.000550 0.00634 1 02/01/2017 02:14 WG947760
1,2,3-Trichlorobenzene U 0.000388 0.00127 1 02/01/2017 02:14 WG947760
1,2,4-Trichlorobenzene U 0.000492 0.00127 1 02/01/2017 02:14 WG947760
1,1,1-Trichloroethane U 0.000363 0.00127 1 02/01/2017 02:14 WG947760
1,1,2-Trichloroethane U 0.000351 0.00127 1 02/01/2017 02:14 WG947760
Trichloroethene U 0.000354 0.00127 1 02/01/2017 02:14 WG947760
Trichlorofluoromethane U 0.000484 0.00634 1 02/01/2017 02:14 WG947760
1,2,3-Trichloropropane U 0.000940 0.00317 1 02/01/2017 02:14 WG947760
1,2,4-Trimethylbenzene U 0.000268 0.00127 1 02/01/2017 02:14 WG947760
1,3,5-Trimethylbenzene U 0.000337 0.00127 1 02/01/2017 02:14 WG947760
Vinyl chloride U 0.000369 0.00127 1 02/01/2017 02:14 WG947760
Xylenes, Total U 0.000885 0.00380 1 02/01/2017 02:14 WG947760
(S) Toluene-d8 106 80.0-120 02/01/2017 02:14 WG947760
(S) Dibromofluoromethane 105 74.0-131 02/01/2017 02:14 WG947760
(S) a,a,a-Trifluorotoluene 104 80.0-120 02/01/2017 02:14 WG947760
(S) 4-Bromofluorobenzene 93.5 64.0-132 02/01/2017 02:14 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.112 0.00814 0.0418 1 02/02/2017 22:07 WG947910
Acenaphthylene U 0.00851 0.0418 1 02/02/2017 22:07 WG947910
Anthracene 0.203 0.00801 0.0418 1 02/02/2017 22:07 WG947910
Benzidine U J4 0.808 4.22 10 02/03/2017 17:40 WG947910
Benzo(a)anthracene 0.562 0.0543 0.418 10 02/03/2017 17:40 WG947910
Benzo(b)fluoranthene 0.959 0.00881 0.0418 1 02/02/2017 22:07 WG947910
Benzo(k)fluoranthene 0.288 0.00738 0.0418 1 02/02/2017 22:07 WG947910
Benzo(g,h,i)perylene 0.135 0.00914 0.0418 1 02/02/2017 22:07 WG947910
Benzo(a)pyrene 0.568 0.00695 0.0418 1 02/02/2017 22:07 WG947910
Bis(2-chlorethoxy)methane U 0.00976 0.422 1 02/02/2017 22:07 WG947910
Bis(2-chloroethyl)ether U 0.0114 0.422 1 02/02/2017 22:07 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L886597
B-14
Collected date/time: 01/25/17 09:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00964 0.422 1 02/02/2017 22:07 WG947910
4-Bromophenyl-phenylether U 0.0145 0.422 1 02/02/2017 22:07 WG947910
2-Chloronaphthalene U 0.00810 0.0418 1 02/02/2017 22:07 WG947910
4-Chlorophenyl-phenylether U 0.00795 0.422 1 02/02/2017 22:07 WG947910
Chrysene 0.616 0.0704 0.418 10 02/03/2017 17:40 WG947910
Dibenz(a,h)anthracene 0.0522 0.0104 0.0418 1 02/02/2017 22:07 WG947910
3,3-Dichlorobenzidine U 1.01 4.22 10 02/03/2017 17:40 WG947910
2,4-Dinitrotoluene U 0.00770 0.422 1 02/02/2017 22:07 WG947910
2,6-Dinitrotoluene U 0.00934 0.422 1 02/02/2017 22:07 WG947910
Fluoranthene 1.34 0.00629 0.0418 1 02/02/2017 22:07 WG947910
Fluorene 0.0727 0.00865 0.0418 1 02/02/2017 22:07 WG947910
Hexachlorobenzene U 0.0109 0.422 1 02/02/2017 22:07 WG947910
Hexachloro-1,3-butadiene U 0.0127 0.422 1 02/02/2017 22:07 WG947910
Hexachlorocyclopentadiene U 0.0744 0.422 1 02/02/2017 22:07 WG947910
Hexachloroethane U 0.0170 0.422 1 02/02/2017 22:07 WG947910
Indeno(1,2,3-cd)pyrene 0.165 0.00979 0.0418 1 02/02/2017 22:07 WG947910
Isophorone U 0.00662 0.422 1 02/02/2017 22:07 WG947910
Naphthalene 0.0529 0.0113 0.0418 1 02/02/2017 22:07 WG947910
Nitrobenzene U 0.00881 0.422 1 02/02/2017 22:07 WG947910
n-Nitrosodimethylamine U 0.0820 0.422 1 02/02/2017 22:07 WG947910
n-Nitrosodiphenylamine U 0.00753 0.422 1 02/02/2017 22:07 WG947910
n-Nitrosodi-n-propylamine U 0.0115 0.422 1 02/02/2017 22:07 WG947910
Phenanthrene 0.799 0.00669 0.0418 1 02/02/2017 22:07 WG947910
Benzylbutyl phthalate U 0.131 4.22 10 02/03/2017 17:40 WG947910
Bis(2-ethylhexyl)phthalate U 0.152 4.22 10 02/03/2017 17:40 WG947910
Di-n-butyl phthalate U 0.0138 0.422 1 02/02/2017 22:07 WG947910
Diethyl phthalate U 0.00876 0.422 1 02/02/2017 22:07 WG947910
Dimethyl phthalate U 0.00685 0.422 1 02/02/2017 22:07 WG947910
Di-n-octyl phthalate U 0.115 4.22 10 02/03/2017 17:40 WG947910
Pyrene 0.832 0.156 0.418 10 02/03/2017 17:40 WG947910
1,2,4-Trichlorobenzene U 0.0111 0.422 1 02/02/2017 22:07 WG947910
Aniline U 0.0406 0.422 1 02/02/2017 22:07 WG947910
4-Chloro-3-methylphenol U 0.00605 0.422 1 02/02/2017 22:07 WG947910
2-Chlorophenol U 0.0105 0.422 1 02/02/2017 22:07 WG947910
2,4-Dichlorophenol U 0.00946 0.422 1 02/02/2017 22:07 WG947910
2,4-Dimethylphenol U 0.0597 0.422 1 02/02/2017 22:07 WG947910
4,6-Dinitro-2-methylphenol U 0.157 0.422 1 02/02/2017 22:07 WG947910
2,4-Dinitrophenol U 0.124 0.422 1 02/02/2017 22:07 WG947910
2-Nitrophenol U 0.0165 0.422 1 02/02/2017 22:07 WG947910
4-Nitrophenol U 0.0666 0.422 1 02/02/2017 22:07 WG947910
Pentachlorophenol 0.132 J 0.0609 0.422 1 02/02/2017 22:07 WG947910
Phenol U 0.00881 0.422 1 02/02/2017 22:07 WG947910
2,4,6-Trichlorophenol U 0.00988 0.422 1 02/02/2017 22:07 WG947910
(S) 2-Fluorophenol 78.4 20.0-120 02/02/2017 22:07 WG947910
(S) 2-Fluorophenol 75.7 20.0-120 02/03/2017 17:40 WG947910
(S) Phenol-d5 80.5 20.0-120 02/02/2017 22:07 WG947910
(S) Phenol-d5 83.6 20.0-120 02/03/2017 17:40 WG947910
(S) Nitrobenzene-d5 83.2 18.0-125 02/02/2017 22:07 WG947910
(S) Nitrobenzene-d5 83.7 18.0-125 02/03/2017 17:40 WG947910
(S) 2-Fluorobiphenyl 81.6 28.0-120 02/02/2017 22:07 WG947910
(S) 2-Fluorobiphenyl 84.4 28.0-120 02/03/2017 17:40 WG947910
(S) 2,4,6-Tribromophenol 73.8 17.0-137 02/03/2017 17:40 WG947910
(S) 2,4,6-Tribromophenol 90.8 17.0-137 02/02/2017 22:07 WG947910
(S) p-Terphenyl-d14 64.7 13.0-131 02/02/2017 22:07 WG947910
(S) p-Terphenyl-d14 62.6 13.0-131 02/03/2017 17:40 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L886597
B-15
Collected date/time: 01/25/17 08:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.1 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0720 0.00368 0.0263 1 01/30/2017 12:55 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.208 0.657 5 02/03/2017 16:20 WG948015
Arsenic 4.92 0.0164 0.657 5 02/03/2017 16:20 WG948015
Beryllium 0.379 J 0.0789 0.657 5 02/03/2017 16:20 WG948015
Cadmium U 0.105 0.657 5 02/03/2017 16:20 WG948015
Chromium 32.9 0.355 0.657 5 02/03/2017 16:20 WG948015
Copper 29.8 0.342 0.657 5 02/03/2017 16:20 WG948015
Lead 22.6 0.158 0.657 5 02/03/2017 16:20 WG948015
Manganese 99.9 0.164 1.31 5 02/03/2017 16:20 WG948015
Nickel 5.05 0.230 0.657 5 02/03/2017 16:20 WG948015
Selenium 1.65 0.250 0.657 5 02/03/2017 16:20 WG948015
Silver U 0.204 0.657 5 02/03/2017 16:20 WG948015
Thallium 0.378 J 0.125 0.657 5 02/03/2017 16:20 WG948015
Zinc 29.3 1.68 6.57 5 02/03/2017 16:20 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0141 0.0703 1.07 02/01/2017 02:37 WG947760
Acrylonitrile U 0.00252 0.0141 1.07 02/01/2017 02:37 WG947760
Benzene U 0.000380 0.00141 1.07 02/01/2017 02:37 WG947760
Bromobenzene U 0.000400 0.00141 1.07 02/01/2017 02:37 WG947760
Bromodichloromethane U 0.000358 0.00141 1.07 02/01/2017 02:37 WG947760
Bromoform U 0.000597 0.00141 1.07 02/01/2017 02:37 WG947760
Bromomethane U 0.00188 0.00703 1.07 02/01/2017 02:37 WG947760
n-Butylbenzene U 0.000363 0.00141 1.07 02/01/2017 02:37 WG947760
sec-Butylbenzene U 0.000283 0.00141 1.07 02/01/2017 02:37 WG947760
tert-Butylbenzene U 0.000289 0.00141 1.07 02/01/2017 02:37 WG947760
Carbon tetrachloride U 0.000462 0.00141 1.07 02/01/2017 02:37 WG947760
Chlorobenzene U 0.000298 0.00141 1.07 02/01/2017 02:37 WG947760
Chlorodibromomethane U 0.000525 0.00141 1.07 02/01/2017 02:37 WG947760
Chloroethane U 0.00133 0.00703 1.07 02/01/2017 02:37 WG947760
2-Chloroethyl vinyl ether U 0.00329 0.0703 1.07 02/01/2017 02:37 WG947760
Chloroform U 0.000322 0.00703 1.07 02/01/2017 02:37 WG947760
Chloromethane U 0.000527 0.00352 1.07 02/01/2017 02:37 WG947760
2-Chlorotoluene U 0.000423 0.00141 1.07 02/01/2017 02:37 WG947760
4-Chlorotoluene U 0.000338 0.00141 1.07 02/01/2017 02:37 WG947760
1,2-Dibromo-3-Chloropropane U 0.00147 0.00703 1.07 02/01/2017 02:37 WG947760
1,2-Dibromoethane U 0.000483 0.00141 1.07 02/01/2017 02:37 WG947760
Dibromomethane U 0.000538 0.00141 1.07 02/01/2017 02:37 WG947760
1,2-Dichlorobenzene U 0.000429 0.00141 1.07 02/01/2017 02:37 WG947760
1,3-Dichlorobenzene U 0.000337 0.00141 1.07 02/01/2017 02:37 WG947760
1,4-Dichlorobenzene U 0.000318 0.00141 1.07 02/01/2017 02:37 WG947760
Dichlorodifluoromethane U 0.00100 0.00703 1.07 02/01/2017 02:37 WG947760
1,1-Dichloroethane U 0.000280 0.00141 1.07 02/01/2017 02:37 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L886597
B-15
Collected date/time: 01/25/17 08:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000373 0.00141 1.07 02/01/2017 02:37 WG947760
1,1-Dichloroethene U 0.000426 0.00141 1.07 02/01/2017 02:37 WG947760
cis-1,2-Dichloroethene U 0.000330 0.00141 1.07 02/01/2017 02:37 WG947760
trans-1,2-Dichloroethene U 0.000371 0.00141 1.07 02/01/2017 02:37 WG947760
1,2-Dichloropropane U 0.000504 0.00141 1.07 02/01/2017 02:37 WG947760
1,1-Dichloropropene U 0.000446 0.00141 1.07 02/01/2017 02:37 WG947760
1,3-Dichloropropane U 0.000291 0.00141 1.07 02/01/2017 02:37 WG947760
cis-1,3-Dichloropropene U 0.000368 0.00141 1.07 02/01/2017 02:37 WG947760
trans-1,3-Dichloropropene U 0.000376 0.00141 1.07 02/01/2017 02:37 WG947760
2,2-Dichloropropane U 0.000392 0.00141 1.07 02/01/2017 02:37 WG947760
Di-isopropyl ether U 0.000348 0.00141 1.07 02/01/2017 02:37 WG947760
Ethylbenzene U 0.000418 0.00141 1.07 02/01/2017 02:37 WG947760
Hexachloro-1,3-butadiene U 0.000481 0.00141 1.07 02/01/2017 02:37 WG947760
Isopropylbenzene U 0.000342 0.00141 1.07 02/01/2017 02:37 WG947760
p-Isopropyltoluene U 0.000287 0.00141 1.07 02/01/2017 02:37 WG947760
2-Butanone (MEK)U 0.00659 0.0141 1.07 02/01/2017 02:37 WG947760
Methylene Chloride U 0.00141 0.00703 1.07 02/01/2017 02:37 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00264 0.0141 1.07 02/01/2017 02:37 WG947760
Methyl tert-butyl ether U 0.000298 0.00141 1.07 02/01/2017 02:37 WG947760
Naphthalene U 0.00141 0.00703 1.07 02/01/2017 02:37 WG947760
n-Propylbenzene U 0.000289 0.00141 1.07 02/01/2017 02:37 WG947760
Styrene U 0.000329 0.00141 1.07 02/01/2017 02:37 WG947760
1,1,1,2-Tetrachloroethane U 0.000371 0.00141 1.07 02/01/2017 02:37 WG947760
1,1,2,2-Tetrachloroethane U 0.000513 0.00141 1.07 02/01/2017 02:37 WG947760
Tetrachloroethene U 0.000388 0.00141 1.07 02/01/2017 02:37 WG947760
Toluene U 0.000610 0.00703 1.07 02/01/2017 02:37 WG947760
1,2,3-Trichlorobenzene U 0.000430 0.00141 1.07 02/01/2017 02:37 WG947760
1,2,4-Trichlorobenzene U 0.000546 0.00141 1.07 02/01/2017 02:37 WG947760
1,1,1-Trichloroethane U 0.000402 0.00141 1.07 02/01/2017 02:37 WG947760
1,1,2-Trichloroethane U 0.000389 0.00141 1.07 02/01/2017 02:37 WG947760
Trichloroethene U 0.000392 0.00141 1.07 02/01/2017 02:37 WG947760
Trichlorofluoromethane U 0.000538 0.00703 1.07 02/01/2017 02:37 WG947760
1,2,3-Trichloropropane U 0.00104 0.00352 1.07 02/01/2017 02:37 WG947760
1,2,4-Trimethylbenzene 0.00127 J 0.000297 0.00141 1.07 02/01/2017 02:37 WG947760
1,3,5-Trimethylbenzene 0.000501 J 0.000375 0.00141 1.07 02/01/2017 02:37 WG947760
Vinyl chloride U 0.000409 0.00141 1.07 02/01/2017 02:37 WG947760
Xylenes, Total U 0.000982 0.00422 1.07 02/01/2017 02:37 WG947760
(S) Toluene-d8 106 80.0-120 02/01/2017 02:37 WG947760
(S) Dibromofluoromethane 104 74.0-131 02/01/2017 02:37 WG947760
(S) a,a,a-Trifluorotoluene 103 80.0-120 02/01/2017 02:37 WG947760
(S) 4-Bromofluorobenzene 98.1 64.0-132 02/01/2017 02:37 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00844 0.0434 1 02/02/2017 16:06 WG947910
Acenaphthylene U 0.00882 0.0434 1 02/02/2017 16:06 WG947910
Anthracene U 0.00831 0.0434 1 02/02/2017 16:06 WG947910
Benzidine U J4 0.0838 0.438 1 02/02/2017 16:06 WG947910
Benzo(a)anthracene U 0.00563 0.0434 1 02/02/2017 16:06 WG947910
Benzo(b)fluoranthene U 0.00914 0.0434 1 02/02/2017 16:06 WG947910
Benzo(k)fluoranthene U 0.00765 0.0434 1 02/02/2017 16:06 WG947910
Benzo(g,h,i)perylene U 0.00948 0.0434 1 02/02/2017 16:06 WG947910
Benzo(a)pyrene U 0.00721 0.0434 1 02/02/2017 16:06 WG947910
Bis(2-chlorethoxy)methane U 0.0101 0.438 1 02/02/2017 16:06 WG947910
Bis(2-chloroethyl)ether U 0.0118 0.438 1 02/02/2017 16:06 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L886597
B-15
Collected date/time: 01/25/17 08:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00999 0.438 1 02/02/2017 16:06 WG947910
4-Bromophenyl-phenylether U 0.0150 0.438 1 02/02/2017 16:06 WG947910
2-Chloronaphthalene U 0.00840 0.0434 1 02/02/2017 16:06 WG947910
4-Chlorophenyl-phenylether U 0.00824 0.438 1 02/02/2017 16:06 WG947910
Chrysene U 0.00730 0.0434 1 02/02/2017 16:06 WG947910
Dibenz(a,h)anthracene U 0.0108 0.0434 1 02/02/2017 16:06 WG947910
3,3-Dichlorobenzidine U 0.104 0.438 1 02/02/2017 16:06 WG947910
2,4-Dinitrotoluene U 0.00798 0.438 1 02/02/2017 16:06 WG947910
2,6-Dinitrotoluene U 0.00969 0.438 1 02/02/2017 16:06 WG947910
Fluoranthene U 0.00652 0.0434 1 02/02/2017 16:06 WG947910
Fluorene U 0.00897 0.0434 1 02/02/2017 16:06 WG947910
Hexachlorobenzene U 0.0113 0.438 1 02/02/2017 16:06 WG947910
Hexachloro-1,3-butadiene U 0.0131 0.438 1 02/02/2017 16:06 WG947910
Hexachlorocyclopentadiene U 0.0772 0.438 1 02/02/2017 16:06 WG947910
Hexachloroethane U 0.0176 0.438 1 02/02/2017 16:06 WG947910
Indeno(1,2,3-cd)pyrene U 0.0102 0.0434 1 02/02/2017 16:06 WG947910
Isophorone U 0.00686 0.438 1 02/02/2017 16:06 WG947910
Naphthalene U 0.0117 0.0434 1 02/02/2017 16:06 WG947910
Nitrobenzene U 0.00914 0.438 1 02/02/2017 16:06 WG947910
n-Nitrosodimethylamine U 0.0851 0.438 1 02/02/2017 16:06 WG947910
n-Nitrosodiphenylamine U 0.00781 0.438 1 02/02/2017 16:06 WG947910
n-Nitrosodi-n-propylamine U 0.0119 0.438 1 02/02/2017 16:06 WG947910
Phenanthrene U 0.00694 0.0434 1 02/02/2017 16:06 WG947910
Benzylbutyl phthalate U 0.0135 0.438 1 02/02/2017 16:06 WG947910
Bis(2-ethylhexyl)phthalate U 0.0158 0.438 1 02/02/2017 16:06 WG947910
Di-n-butyl phthalate U 0.0143 0.438 1 02/02/2017 16:06 WG947910
Diethyl phthalate U 0.00909 0.438 1 02/02/2017 16:06 WG947910
Dimethyl phthalate U 0.00710 0.438 1 02/02/2017 16:06 WG947910
Di-n-octyl phthalate U 0.0119 0.438 1 02/02/2017 16:06 WG947910
Pyrene U 0.0162 0.0434 1 02/02/2017 16:06 WG947910
1,2,4-Trichlorobenzene U 0.0115 0.438 1 02/02/2017 16:06 WG947910
Aniline U 0.0421 0.438 1 02/02/2017 16:06 WG947910
4-Chloro-3-methylphenol U 0.00627 0.438 1 02/02/2017 16:06 WG947910
2-Chlorophenol U 0.0109 0.438 1 02/02/2017 16:06 WG947910
2,4-Dichlorophenol U 0.00981 0.438 1 02/02/2017 16:06 WG947910
2,4-Dimethylphenol U 0.0619 0.438 1 02/02/2017 16:06 WG947910
4,6-Dinitro-2-methylphenol U 0.163 0.438 1 02/02/2017 16:06 WG947910
2,4-Dinitrophenol U 0.129 0.438 1 02/02/2017 16:06 WG947910
2-Nitrophenol U 0.0171 0.438 1 02/02/2017 16:06 WG947910
4-Nitrophenol U 0.0690 0.438 1 02/02/2017 16:06 WG947910
Pentachlorophenol U 0.0631 0.438 1 02/02/2017 16:06 WG947910
Phenol U 0.00914 0.438 1 02/02/2017 16:06 WG947910
2,4,6-Trichlorophenol U 0.0102 0.438 1 02/02/2017 16:06 WG947910
(S) 2-Fluorophenol 72.0 20.0-120 02/02/2017 16:06 WG947910
(S) Phenol-d5 74.1 20.0-120 02/02/2017 16:06 WG947910
(S) Nitrobenzene-d5 73.6 18.0-125 02/02/2017 16:06 WG947910
(S) 2-Fluorobiphenyl 74.7 28.0-120 02/02/2017 16:06 WG947910
(S) 2,4,6-Tribromophenol 77.8 17.0-137 02/02/2017 16:06 WG947910
(S) p-Terphenyl-d14 71.0 13.0-131 02/02/2017 16:06 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L886597
B-16
Collected date/time: 01/25/17 08:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.1 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0133 J 0.00358 0.0256 1 01/30/2017 12:57 WG947435
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.202 0.640 5 02/03/2017 16:23 WG948015
Arsenic 1.95 0.0160 0.640 5 02/03/2017 16:23 WG948015
Beryllium 0.728 0.0768 0.640 5 02/03/2017 16:23 WG948015
Cadmium 0.509 J 0.102 0.640 5 02/03/2017 16:23 WG948015
Chromium 8.00 0.346 0.640 5 02/03/2017 16:23 WG948015
Copper 267 6.65 12.8 100 02/04/2017 13:12 WG948015
Lead 59.2 0.154 0.640 5 02/03/2017 16:23 WG948015
Manganese 1930 3.20 25.6 100 02/04/2017 13:12 WG948015
Nickel 4.44 0.224 0.640 5 02/03/2017 16:23 WG948015
Selenium 0.988 0.243 0.640 5 02/03/2017 16:23 WG948015
Silver U 0.198 0.640 5 02/03/2017 16:23 WG948015
Thallium 0.310 J 0.122 0.640 5 02/03/2017 16:23 WG948015
Zinc 50.1 1.64 6.40 5 02/03/2017 16:23 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0154 J 0.0132 0.0659 1.03 01/31/2017 20:33 WG947760
Acrylonitrile U 0.00235 0.0132 1.03 01/31/2017 20:33 WG947760
Benzene U 0.000356 0.00132 1.03 01/31/2017 20:33 WG947760
Bromobenzene U 0.000374 0.00132 1.03 01/31/2017 20:33 WG947760
Bromodichloromethane U 0.000335 0.00132 1.03 01/31/2017 20:33 WG947760
Bromoform U 0.000559 0.00132 1.03 01/31/2017 20:33 WG947760
Bromomethane U 0.00177 0.00659 1.03 01/31/2017 20:33 WG947760
n-Butylbenzene U 0.000340 0.00132 1.03 01/31/2017 20:33 WG947760
sec-Butylbenzene U 0.000265 0.00132 1.03 01/31/2017 20:33 WG947760
tert-Butylbenzene U 0.000271 0.00132 1.03 01/31/2017 20:33 WG947760
Carbon tetrachloride U 0.000433 0.00132 1.03 01/31/2017 20:33 WG947760
Chlorobenzene U 0.000279 0.00132 1.03 01/31/2017 20:33 WG947760
Chlorodibromomethane U 0.000491 0.00132 1.03 01/31/2017 20:33 WG947760
Chloroethane U 0.00125 0.00659 1.03 01/31/2017 20:33 WG947760
2-Chloroethyl vinyl ether U 0.00308 0.0659 1.03 01/31/2017 20:33 WG947760
Chloroform 0.000401 J 0.000302 0.00659 1.03 01/31/2017 20:33 WG947760
Chloromethane U 0.000494 0.00330 1.03 01/31/2017 20:33 WG947760
2-Chlorotoluene U 0.000397 0.00132 1.03 01/31/2017 20:33 WG947760
4-Chlorotoluene U 0.000316 0.00132 1.03 01/31/2017 20:33 WG947760
1,2-Dibromo-3-Chloropropane U 0.00138 0.00659 1.03 01/31/2017 20:33 WG947760
1,2-Dibromoethane U 0.000452 0.00132 1.03 01/31/2017 20:33 WG947760
Dibromomethane U 0.000503 0.00132 1.03 01/31/2017 20:33 WG947760
1,2-Dichlorobenzene U 0.000402 0.00132 1.03 01/31/2017 20:33 WG947760
1,3-Dichlorobenzene U 0.000315 0.00132 1.03 01/31/2017 20:33 WG947760
1,4-Dichlorobenzene U 0.000298 0.00132 1.03 01/31/2017 20:33 WG947760
Dichlorodifluoromethane U 0.000939 0.00659 1.03 01/31/2017 20:33 WG947760
1,1-Dichloroethane U 0.000262 0.00132 1.03 01/31/2017 20:33 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L886597
B-16
Collected date/time: 01/25/17 08:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000349 0.00132 1.03 01/31/2017 20:33 WG947760
1,1-Dichloroethene U 0.000399 0.00132 1.03 01/31/2017 20:33 WG947760
cis-1,2-Dichloroethene U 0.000310 0.00132 1.03 01/31/2017 20:33 WG947760
trans-1,2-Dichloroethene U 0.000348 0.00132 1.03 01/31/2017 20:33 WG947760
1,2-Dichloropropane U 0.000472 0.00132 1.03 01/31/2017 20:33 WG947760
1,1-Dichloropropene U 0.000417 0.00132 1.03 01/31/2017 20:33 WG947760
1,3-Dichloropropane U 0.000273 0.00132 1.03 01/31/2017 20:33 WG947760
cis-1,3-Dichloropropene U 0.000346 0.00132 1.03 01/31/2017 20:33 WG947760
trans-1,3-Dichloropropene U 0.000352 0.00132 1.03 01/31/2017 20:33 WG947760
2,2-Dichloropropane U 0.000367 0.00132 1.03 01/31/2017 20:33 WG947760
Di-isopropyl ether U 0.000326 0.00132 1.03 01/31/2017 20:33 WG947760
Ethylbenzene U 0.000392 0.00132 1.03 01/31/2017 20:33 WG947760
Hexachloro-1,3-butadiene U 0.000450 0.00132 1.03 01/31/2017 20:33 WG947760
Isopropylbenzene U 0.000320 0.00132 1.03 01/31/2017 20:33 WG947760
p-Isopropyltoluene U 0.000269 0.00132 1.03 01/31/2017 20:33 WG947760
2-Butanone (MEK)U 0.00617 0.0132 1.03 01/31/2017 20:33 WG947760
Methylene Chloride U 0.00132 0.00659 1.03 01/31/2017 20:33 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00248 0.0132 1.03 01/31/2017 20:33 WG947760
Methyl tert-butyl ether U 0.000279 0.00132 1.03 01/31/2017 20:33 WG947760
Naphthalene U 0.00132 0.00659 1.03 01/31/2017 20:33 WG947760
n-Propylbenzene U 0.000271 0.00132 1.03 01/31/2017 20:33 WG947760
Styrene U 0.000308 0.00132 1.03 01/31/2017 20:33 WG947760
1,1,1,2-Tetrachloroethane U 0.000348 0.00132 1.03 01/31/2017 20:33 WG947760
1,1,2,2-Tetrachloroethane U 0.000481 0.00132 1.03 01/31/2017 20:33 WG947760
Tetrachloroethene U 0.000363 0.00132 1.03 01/31/2017 20:33 WG947760
Toluene U 0.000572 0.00659 1.03 01/31/2017 20:33 WG947760
1,2,3-Trichlorobenzene U 0.000403 0.00132 1.03 01/31/2017 20:33 WG947760
1,2,4-Trichlorobenzene U 0.000512 0.00132 1.03 01/31/2017 20:33 WG947760
1,1,1-Trichloroethane U 0.000376 0.00132 1.03 01/31/2017 20:33 WG947760
1,1,2-Trichloroethane U 0.000365 0.00132 1.03 01/31/2017 20:33 WG947760
Trichloroethene U 0.000367 0.00132 1.03 01/31/2017 20:33 WG947760
Trichlorofluoromethane U 0.000503 0.00659 1.03 01/31/2017 20:33 WG947760
1,2,3-Trichloropropane U 0.000976 0.00330 1.03 01/31/2017 20:33 WG947760
1,2,4-Trimethylbenzene U 0.000278 0.00132 1.03 01/31/2017 20:33 WG947760
1,3,5-Trimethylbenzene U 0.000351 0.00132 1.03 01/31/2017 20:33 WG947760
Vinyl chloride U 0.000384 0.00132 1.03 01/31/2017 20:33 WG947760
Xylenes, Total U 0.000920 0.00395 1.03 01/31/2017 20:33 WG947760
(S) Toluene-d8 105 80.0-120 01/31/2017 20:33 WG947760
(S) Dibromofluoromethane 103 74.0-131 01/31/2017 20:33 WG947760
(S) a,a,a-Trifluorotoluene 102 80.0-120 01/31/2017 20:33 WG947760
(S) 4-Bromofluorobenzene 96.1 64.0-132 01/31/2017 20:33 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00822 0.0422 1 02/02/2017 21:41 WG947910
Acenaphthylene U 0.00859 0.0422 1 02/02/2017 21:41 WG947910
Anthracene 0.0391 J 0.00809 0.0422 1 02/02/2017 21:41 WG947910
Benzidine U J4 0.0815 0.426 1 02/02/2017 21:41 WG947910
Benzo(a)anthracene 0.167 0.00548 0.0422 1 02/02/2017 21:41 WG947910
Benzo(b)fluoranthene 0.305 0.00889 0.0422 1 02/02/2017 21:41 WG947910
Benzo(k)fluoranthene 0.103 0.00745 0.0422 1 02/02/2017 21:41 WG947910
Benzo(g,h,i)perylene 0.103 0.00923 0.0422 1 02/02/2017 21:41 WG947910
Benzo(a)pyrene 0.165 0.00701 0.0422 1 02/02/2017 21:41 WG947910
Bis(2-chlorethoxy)methane U 0.00985 0.426 1 02/02/2017 21:41 WG947910
Bis(2-chloroethyl)ether U 0.0115 0.426 1 02/02/2017 21:41 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L886597
B-16
Collected date/time: 01/25/17 08:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00973 0.426 1 02/02/2017 21:41 WG947910
4-Bromophenyl-phenylether U 0.0146 0.426 1 02/02/2017 21:41 WG947910
2-Chloronaphthalene U 0.00818 0.0422 1 02/02/2017 21:41 WG947910
4-Chlorophenyl-phenylether U 0.00802 0.426 1 02/02/2017 21:41 WG947910
Chrysene 0.191 0.00710 0.0422 1 02/02/2017 21:41 WG947910
Dibenz(a,h)anthracene 0.0365 J 0.0105 0.0422 1 02/02/2017 21:41 WG947910
3,3-Dichlorobenzidine U 0.102 0.426 1 02/02/2017 21:41 WG947910
2,4-Dinitrotoluene U 0.00777 0.426 1 02/02/2017 21:41 WG947910
2,6-Dinitrotoluene U 0.00943 0.426 1 02/02/2017 21:41 WG947910
Fluoranthene 0.295 0.00635 0.0422 1 02/02/2017 21:41 WG947910
Fluorene U 0.00873 0.0422 1 02/02/2017 21:41 WG947910
Hexachlorobenzene U 0.0110 0.426 1 02/02/2017 21:41 WG947910
Hexachloro-1,3-butadiene U 0.0128 0.426 1 02/02/2017 21:41 WG947910
Hexachlorocyclopentadiene U 0.0751 0.426 1 02/02/2017 21:41 WG947910
Hexachloroethane U 0.0171 0.426 1 02/02/2017 21:41 WG947910
Indeno(1,2,3-cd)pyrene 0.108 0.00988 0.0422 1 02/02/2017 21:41 WG947910
Isophorone U 0.00668 0.426 1 02/02/2017 21:41 WG947910
Naphthalene U 0.0114 0.0422 1 02/02/2017 21:41 WG947910
Nitrobenzene U 0.00889 0.426 1 02/02/2017 21:41 WG947910
n-Nitrosodimethylamine U 0.0828 0.426 1 02/02/2017 21:41 WG947910
n-Nitrosodiphenylamine U 0.00760 0.426 1 02/02/2017 21:41 WG947910
n-Nitrosodi-n-propylamine U 0.0116 0.426 1 02/02/2017 21:41 WG947910
Phenanthrene 0.118 0.00676 0.0422 1 02/02/2017 21:41 WG947910
Benzylbutyl phthalate U 0.0132 0.426 1 02/02/2017 21:41 WG947910
Bis(2-ethylhexyl)phthalate U 0.0154 0.426 1 02/02/2017 21:41 WG947910
Di-n-butyl phthalate U 0.0139 0.426 1 02/02/2017 21:41 WG947910
Diethyl phthalate U 0.00884 0.426 1 02/02/2017 21:41 WG947910
Dimethyl phthalate U 0.00691 0.426 1 02/02/2017 21:41 WG947910
Di-n-octyl phthalate U 0.0116 0.426 1 02/02/2017 21:41 WG947910
Pyrene 0.276 0.0157 0.0422 1 02/02/2017 21:41 WG947910
1,2,4-Trichlorobenzene U 0.0112 0.426 1 02/02/2017 21:41 WG947910
Aniline U 0.0409 0.426 1 02/02/2017 21:41 WG947910
4-Chloro-3-methylphenol U 0.00610 0.426 1 02/02/2017 21:41 WG947910
2-Chlorophenol U 0.0106 0.426 1 02/02/2017 21:41 WG947910
2,4-Dichlorophenol U 0.00955 0.426 1 02/02/2017 21:41 WG947910
2,4-Dimethylphenol U 0.0603 0.426 1 02/02/2017 21:41 WG947910
4,6-Dinitro-2-methylphenol U 0.159 0.426 1 02/02/2017 21:41 WG947910
2,4-Dinitrophenol U 0.125 0.426 1 02/02/2017 21:41 WG947910
2-Nitrophenol U 0.0166 0.426 1 02/02/2017 21:41 WG947910
4-Nitrophenol U 0.0672 0.426 1 02/02/2017 21:41 WG947910
Pentachlorophenol U 0.0614 0.426 1 02/02/2017 21:41 WG947910
Phenol U 0.00889 0.426 1 02/02/2017 21:41 WG947910
2,4,6-Trichlorophenol U 0.00997 0.426 1 02/02/2017 21:41 WG947910
(S) 2-Fluorophenol 67.9 20.0-120 02/02/2017 21:41 WG947910
(S) Phenol-d5 73.0 20.0-120 02/02/2017 21:41 WG947910
(S) Nitrobenzene-d5 73.5 18.0-125 02/02/2017 21:41 WG947910
(S) 2-Fluorobiphenyl 76.1 28.0-120 02/02/2017 21:41 WG947910
(S) 2,4,6-Tribromophenol 81.8 17.0-137 02/02/2017 21:41 WG947910
(S) p-Terphenyl-d14 72.3 13.0-131 02/02/2017 21:41 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L886597
DUPE
Collected date/time: 01/25/17 08:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 65.0 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury U 0.00431 0.0308 1 02/01/2017 10:23 WG948080
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.243 0.769 5 02/03/2017 16:27 WG948015
Arsenic 1.66 0.0192 0.769 5 02/03/2017 16:27 WG948015
Beryllium 0.667 J 0.0923 0.769 5 02/03/2017 16:27 WG948015
Cadmium U 0.123 0.769 5 02/03/2017 16:27 WG948015
Chromium 7.09 0.415 0.769 5 02/03/2017 16:27 WG948015
Copper 159 0.800 1.54 10 02/04/2017 13:16 WG948015
Lead 13.4 0.185 0.769 5 02/03/2017 16:27 WG948015
Manganese 212 0.385 3.08 10 02/04/2017 13:16 WG948015
Nickel 1.24 0.269 0.769 5 02/03/2017 16:27 WG948015
Selenium 2.07 0.292 0.769 5 02/03/2017 16:27 WG948015
Silver U 0.239 0.769 5 02/03/2017 16:27 WG948015
Thallium U 0.146 0.769 5 02/03/2017 16:27 WG948015
Zinc 13.1 1.97 7.69 5 02/03/2017 16:27 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0158 0.0792 1.03 02/01/2017 02:59 WG947760
Acrylonitrile U 0.00283 0.0158 1.03 02/01/2017 02:59 WG947760
Benzene U 0.000428 0.00158 1.03 02/01/2017 02:59 WG947760
Bromobenzene U 0.000449 0.00158 1.03 02/01/2017 02:59 WG947760
Bromodichloromethane U 0.000403 0.00158 1.03 02/01/2017 02:59 WG947760
Bromoform U 0.000672 0.00158 1.03 02/01/2017 02:59 WG947760
Bromomethane U 0.00212 0.00792 1.03 02/01/2017 02:59 WG947760
n-Butylbenzene U 0.000409 0.00158 1.03 02/01/2017 02:59 WG947760
sec-Butylbenzene U 0.000319 0.00158 1.03 02/01/2017 02:59 WG947760
tert-Butylbenzene U 0.000326 0.00158 1.03 02/01/2017 02:59 WG947760
Carbon tetrachloride U 0.000520 0.00158 1.03 02/01/2017 02:59 WG947760
Chlorobenzene U 0.000335 0.00158 1.03 02/01/2017 02:59 WG947760
Chlorodibromomethane U 0.000591 0.00158 1.03 02/01/2017 02:59 WG947760
Chloroethane U 0.00150 0.00792 1.03 02/01/2017 02:59 WG947760
2-Chloroethyl vinyl ether U 0.00371 0.0792 1.03 02/01/2017 02:59 WG947760
Chloroform 0.000658 J 0.000363 0.00792 1.03 02/01/2017 02:59 WG947760
Chloromethane U 0.000594 0.00396 1.03 02/01/2017 02:59 WG947760
2-Chlorotoluene U 0.000477 0.00158 1.03 02/01/2017 02:59 WG947760
4-Chlorotoluene U 0.000380 0.00158 1.03 02/01/2017 02:59 WG947760
1,2-Dibromo-3-Chloropropane U 0.00166 0.00792 1.03 02/01/2017 02:59 WG947760
1,2-Dibromoethane U 0.000543 0.00158 1.03 02/01/2017 02:59 WG947760
Dibromomethane U 0.000605 0.00158 1.03 02/01/2017 02:59 WG947760
1,2-Dichlorobenzene U 0.000483 0.00158 1.03 02/01/2017 02:59 WG947760
1,3-Dichlorobenzene U 0.000379 0.00158 1.03 02/01/2017 02:59 WG947760
1,4-Dichlorobenzene U 0.000359 0.00158 1.03 02/01/2017 02:59 WG947760
Dichlorodifluoromethane U 0.00113 0.00792 1.03 02/01/2017 02:59 WG947760
1,1-Dichloroethane U 0.000315 0.00158 1.03 02/01/2017 02:59 WG947760
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L886597
DUPE
Collected date/time: 01/25/17 08:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000420 0.00158 1.03 02/01/2017 02:59 WG947760
1,1-Dichloroethene U 0.000480 0.00158 1.03 02/01/2017 02:59 WG947760
cis-1,2-Dichloroethene U 0.000372 0.00158 1.03 02/01/2017 02:59 WG947760
trans-1,2-Dichloroethene U 0.000419 0.00158 1.03 02/01/2017 02:59 WG947760
1,2-Dichloropropane U 0.000568 0.00158 1.03 02/01/2017 02:59 WG947760
1,1-Dichloropropene U 0.000502 0.00158 1.03 02/01/2017 02:59 WG947760
1,3-Dichloropropane U 0.000328 0.00158 1.03 02/01/2017 02:59 WG947760
cis-1,3-Dichloropropene U 0.000415 0.00158 1.03 02/01/2017 02:59 WG947760
trans-1,3-Dichloropropene U 0.000423 0.00158 1.03 02/01/2017 02:59 WG947760
2,2-Dichloropropane U 0.000442 0.00158 1.03 02/01/2017 02:59 WG947760
Di-isopropyl ether U 0.000392 0.00158 1.03 02/01/2017 02:59 WG947760
Ethylbenzene U 0.000471 0.00158 1.03 02/01/2017 02:59 WG947760
Hexachloro-1,3-butadiene U 0.000542 0.00158 1.03 02/01/2017 02:59 WG947760
Isopropylbenzene U 0.000385 0.00158 1.03 02/01/2017 02:59 WG947760
p-Isopropyltoluene U 0.000323 0.00158 1.03 02/01/2017 02:59 WG947760
2-Butanone (MEK)U 0.00742 0.0158 1.03 02/01/2017 02:59 WG947760
Methylene Chloride U 0.00158 0.00792 1.03 02/01/2017 02:59 WG947760
4-Methyl-2-pentanone (MIBK) U 0.00299 0.0158 1.03 02/01/2017 02:59 WG947760
Methyl tert-butyl ether U 0.000335 0.00158 1.03 02/01/2017 02:59 WG947760
Naphthalene U 0.00158 0.00792 1.03 02/01/2017 02:59 WG947760
n-Propylbenzene U 0.000326 0.00158 1.03 02/01/2017 02:59 WG947760
Styrene U 0.000371 0.00158 1.03 02/01/2017 02:59 WG947760
1,1,1,2-Tetrachloroethane U 0.000419 0.00158 1.03 02/01/2017 02:59 WG947760
1,1,2,2-Tetrachloroethane U 0.000579 0.00158 1.03 02/01/2017 02:59 WG947760
Tetrachloroethene U 0.000437 0.00158 1.03 02/01/2017 02:59 WG947760
Toluene U 0.000688 0.00792 1.03 02/01/2017 02:59 WG947760
1,2,3-Trichlorobenzene U 0.000485 0.00158 1.03 02/01/2017 02:59 WG947760
1,2,4-Trichlorobenzene U 0.000615 0.00158 1.03 02/01/2017 02:59 WG947760
1,1,1-Trichloroethane U 0.000452 0.00158 1.03 02/01/2017 02:59 WG947760
1,1,2-Trichloroethane U 0.000439 0.00158 1.03 02/01/2017 02:59 WG947760
Trichloroethene U 0.000442 0.00158 1.03 02/01/2017 02:59 WG947760
Trichlorofluoromethane U 0.000605 0.00792 1.03 02/01/2017 02:59 WG947760
1,2,3-Trichloropropane U 0.00117 0.00396 1.03 02/01/2017 02:59 WG947760
1,2,4-Trimethylbenzene U 0.000334 0.00158 1.03 02/01/2017 02:59 WG947760
1,3,5-Trimethylbenzene U 0.000422 0.00158 1.03 02/01/2017 02:59 WG947760
Vinyl chloride U 0.000462 0.00158 1.03 02/01/2017 02:59 WG947760
Xylenes, Total U 0.00111 0.00475 1.03 02/01/2017 02:59 WG947760
(S) Toluene-d8 106 80.0-120 02/01/2017 02:59 WG947760
(S) Dibromofluoromethane 105 74.0-131 02/01/2017 02:59 WG947760
(S) a,a,a-Trifluorotoluene 103 80.0-120 02/01/2017 02:59 WG947760
(S) 4-Bromofluorobenzene 98.3 64.0-132 02/01/2017 02:59 WG947760
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00988 0.0508 1 02/02/2017 16:32 WG947910
Acenaphthylene U 0.0103 0.0508 1 02/02/2017 16:32 WG947910
Anthracene U 0.00972 0.0508 1 02/02/2017 16:32 WG947910
Benzidine U J4 0.0980 0.512 1 02/02/2017 16:32 WG947910
Benzo(a)anthracene U 0.00659 0.0508 1 02/02/2017 16:32 WG947910
Benzo(b)fluoranthene U 0.0107 0.0508 1 02/02/2017 16:32 WG947910
Benzo(k)fluoranthene U 0.00896 0.0508 1 02/02/2017 16:32 WG947910
Benzo(g,h,i)perylene U 0.0111 0.0508 1 02/02/2017 16:32 WG947910
Benzo(a)pyrene U 0.00843 0.0508 1 02/02/2017 16:32 WG947910
Bis(2-chlorethoxy)methane U 0.0118 0.512 1 02/02/2017 16:32 WG947910
Bis(2-chloroethyl)ether U 0.0138 0.512 1 02/02/2017 16:32 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L886597
DUPE
Collected date/time: 01/25/17 08:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.0117 0.512 1 02/02/2017 16:32 WG947910
4-Bromophenyl-phenylether U 0.0175 0.512 1 02/02/2017 16:32 WG947910
2-Chloronaphthalene U 0.00983 0.0508 1 02/02/2017 16:32 WG947910
4-Chlorophenyl-phenylether U 0.00965 0.512 1 02/02/2017 16:32 WG947910
Chrysene U 0.00854 0.0508 1 02/02/2017 16:32 WG947910
Dibenz(a,h)anthracene U 0.0126 0.0508 1 02/02/2017 16:32 WG947910
3,3-Dichlorobenzidine U 0.122 0.512 1 02/02/2017 16:32 WG947910
2,4-Dinitrotoluene U 0.00934 0.512 1 02/02/2017 16:32 WG947910
2,6-Dinitrotoluene U 0.0113 0.512 1 02/02/2017 16:32 WG947910
Fluoranthene U 0.00763 0.0508 1 02/02/2017 16:32 WG947910
Fluorene U 0.0105 0.0508 1 02/02/2017 16:32 WG947910
Hexachlorobenzene U 0.0132 0.512 1 02/02/2017 16:32 WG947910
Hexachloro-1,3-butadiene U 0.0154 0.512 1 02/02/2017 16:32 WG947910
Hexachlorocyclopentadiene U 0.0903 0.512 1 02/02/2017 16:32 WG947910
Hexachloroethane U 0.0206 0.512 1 02/02/2017 16:32 WG947910
Indeno(1,2,3-cd)pyrene U 0.0119 0.0508 1 02/02/2017 16:32 WG947910
Isophorone U 0.00803 0.512 1 02/02/2017 16:32 WG947910
Naphthalene U 0.0137 0.0508 1 02/02/2017 16:32 WG947910
Nitrobenzene U 0.0107 0.512 1 02/02/2017 16:32 WG947910
n-Nitrosodimethylamine U 0.0996 0.512 1 02/02/2017 16:32 WG947910
n-Nitrosodiphenylamine U 0.00914 0.512 1 02/02/2017 16:32 WG947910
n-Nitrosodi-n-propylamine U 0.0139 0.512 1 02/02/2017 16:32 WG947910
Phenanthrene U 0.00812 0.0508 1 02/02/2017 16:32 WG947910
Benzylbutyl phthalate U 0.0158 0.512 1 02/02/2017 16:32 WG947910
Bis(2-ethylhexyl)phthalate U 0.0185 0.512 1 02/02/2017 16:32 WG947910
Di-n-butyl phthalate U 0.0168 0.512 1 02/02/2017 16:32 WG947910
Diethyl phthalate U 0.0106 0.512 1 02/02/2017 16:32 WG947910
Dimethyl phthalate U 0.00831 0.512 1 02/02/2017 16:32 WG947910
Di-n-octyl phthalate U 0.0140 0.512 1 02/02/2017 16:32 WG947910
Pyrene U 0.0189 0.0508 1 02/02/2017 16:32 WG947910
1,2,4-Trichlorobenzene U 0.0135 0.512 1 02/02/2017 16:32 WG947910
Aniline U 0.0492 0.512 1 02/02/2017 16:32 WG947910
4-Chloro-3-methylphenol U 0.00734 0.512 1 02/02/2017 16:32 WG947910
2-Chlorophenol U 0.0128 0.512 1 02/02/2017 16:32 WG947910
2,4-Dichlorophenol U 0.0115 0.512 1 02/02/2017 16:32 WG947910
2,4-Dimethylphenol U 0.0725 0.512 1 02/02/2017 16:32 WG947910
4,6-Dinitro-2-methylphenol U 0.191 0.512 1 02/02/2017 16:32 WG947910
2,4-Dinitrophenol U 0.151 0.512 1 02/02/2017 16:32 WG947910
2-Nitrophenol U 0.0200 0.512 1 02/02/2017 16:32 WG947910
4-Nitrophenol U 0.0808 0.512 1 02/02/2017 16:32 WG947910
Pentachlorophenol U 0.0739 0.512 1 02/02/2017 16:32 WG947910
Phenol U 0.0107 0.512 1 02/02/2017 16:32 WG947910
2,4,6-Trichlorophenol U 0.0120 0.512 1 02/02/2017 16:32 WG947910
(S) 2-Fluorophenol 59.1 20.0-120 02/02/2017 16:32 WG947910
(S) Phenol-d5 61.4 20.0-120 02/02/2017 16:32 WG947910
(S) Nitrobenzene-d5 61.0 18.0-125 02/02/2017 16:32 WG947910
(S) 2-Fluorobiphenyl 64.3 28.0-120 02/02/2017 16:32 WG947910
(S) 2,4,6-Tribromophenol 73.1 17.0-137 02/02/2017 16:32 WG947910
(S) p-Terphenyl-d14 72.9 13.0-131 02/02/2017 16:32 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L886597
TW-2
Collected date/time: 01/25/17 00:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 67.8 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0451 0.00413 0.0295 1 02/01/2017 10:25 WG948080
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.233 0.738 5 02/03/2017 16:30 WG948015
Arsenic 2.99 0.0184 0.738 5 02/03/2017 16:30 WG948015
Beryllium 0.356 J 0.0886 0.738 5 02/03/2017 16:30 WG948015
Cadmium U 0.118 0.738 5 02/03/2017 16:30 WG948015
Chromium 35.8 0.398 0.738 5 02/03/2017 16:30 WG948015
Copper 55.4 0.384 0.738 5 02/03/2017 16:30 WG948015
Lead 49.4 0.177 0.738 5 02/03/2017 16:30 WG948015
Manganese 301 0.738 5.90 20 02/04/2017 13:19 WG948015
Nickel 6.81 0.258 0.738 5 02/03/2017 16:30 WG948015
Selenium 1.38 0.280 0.738 5 02/03/2017 16:30 WG948015
Silver U 0.229 0.738 5 02/03/2017 16:30 WG948015
Thallium 0.242 J 0.140 0.738 5 02/03/2017 16:30 WG948015
Zinc 49.4 1.89 7.38 5 02/03/2017 16:30 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0660 J 0.0148 0.0738 1 02/01/2017 03:00 WG948235
Acrylonitrile U 0.00264 0.0148 1 02/01/2017 03:00 WG948235
Benzene U 0.000398 0.00148 1 02/01/2017 03:00 WG948235
Bromobenzene U 0.000419 0.00148 1 02/01/2017 03:00 WG948235
Bromodichloromethane U 0.000375 0.00148 1 02/01/2017 03:00 WG948235
Bromoform U 0.000626 0.00148 1 02/01/2017 03:00 WG948235
Bromomethane U 0.00198 0.00738 1 02/01/2017 03:00 WG948235
n-Butylbenzene U 0.000381 0.00148 1 02/01/2017 03:00 WG948235
sec-Butylbenzene U 0.000297 0.00148 1 02/01/2017 03:00 WG948235
tert-Butylbenzene U 0.000304 0.00148 1 02/01/2017 03:00 WG948235
Carbon tetrachloride U 0.000484 0.00148 1 02/01/2017 03:00 WG948235
Chlorobenzene U 0.000313 0.00148 1 02/01/2017 03:00 WG948235
Chlorodibromomethane U 0.000551 0.00148 1 02/01/2017 03:00 WG948235
Chloroethane U 0.00140 0.00738 1 02/01/2017 03:00 WG948235
2-Chloroethyl vinyl ether U 0.00345 0.0738 1 02/01/2017 03:00 WG948235
Chloroform U 0.000338 0.00738 1 02/01/2017 03:00 WG948235
Chloromethane U 0.000553 0.00369 1 02/01/2017 03:00 WG948235
2-Chlorotoluene U 0.000444 0.00148 1 02/01/2017 03:00 WG948235
4-Chlorotoluene U 0.000354 0.00148 1 02/01/2017 03:00 WG948235
1,2-Dibromo-3-Chloropropane U 0.00155 0.00738 1 02/01/2017 03:00 WG948235
1,2-Dibromoethane U 0.000506 0.00148 1 02/01/2017 03:00 WG948235
Dibromomethane U 0.000564 0.00148 1 02/01/2017 03:00 WG948235
1,2-Dichlorobenzene U 0.000450 0.00148 1 02/01/2017 03:00 WG948235
1,3-Dichlorobenzene U 0.000353 0.00148 1 02/01/2017 03:00 WG948235
1,4-Dichlorobenzene U 0.000334 0.00148 1 02/01/2017 03:00 WG948235
Dichlorodifluoromethane U 0.00105 0.00738 1 02/01/2017 03:00 WG948235
1,1-Dichloroethane U 0.000294 0.00148 1 02/01/2017 03:00 WG948235
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L886597
TW-2
Collected date/time: 01/25/17 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000391 0.00148 1 02/01/2017 03:00 WG948235
1,1-Dichloroethene U 0.000447 0.00148 1 02/01/2017 03:00 WG948235
cis-1,2-Dichloroethene U 0.000347 0.00148 1 02/01/2017 03:00 WG948235
trans-1,2-Dichloroethene U 0.000390 0.00148 1 02/01/2017 03:00 WG948235
1,2-Dichloropropane U 0.000528 0.00148 1 02/01/2017 03:00 WG948235
1,1-Dichloropropene U 0.000468 0.00148 1 02/01/2017 03:00 WG948235
1,3-Dichloropropane U 0.000306 0.00148 1 02/01/2017 03:00 WG948235
cis-1,3-Dichloropropene U 0.000387 0.00148 1 02/01/2017 03:00 WG948235
trans-1,3-Dichloropropene U 0.000394 0.00148 1 02/01/2017 03:00 WG948235
2,2-Dichloropropane U 0.000412 0.00148 1 02/01/2017 03:00 WG948235
Di-isopropyl ether U 0.000366 0.00148 1 02/01/2017 03:00 WG948235
Ethylbenzene U 0.000438 0.00148 1 02/01/2017 03:00 WG948235
Hexachloro-1,3-butadiene U 0.000505 0.00148 1 02/01/2017 03:00 WG948235
Isopropylbenzene U 0.000359 0.00148 1 02/01/2017 03:00 WG948235
p-Isopropyltoluene 0.00184 0.000301 0.00148 1 02/01/2017 03:00 WG948235
2-Butanone (MEK)0.0110 J 0.00691 0.0148 1 02/01/2017 03:00 WG948235
Methylene Chloride U 0.00148 0.00738 1 02/01/2017 03:00 WG948235
4-Methyl-2-pentanone (MIBK) U 0.00277 0.0148 1 02/01/2017 03:00 WG948235
Methyl tert-butyl ether U 0.000313 0.00148 1 02/01/2017 03:00 WG948235
Naphthalene U 0.00148 0.00738 1 02/01/2017 03:00 WG948235
n-Propylbenzene U 0.000304 0.00148 1 02/01/2017 03:00 WG948235
Styrene U 0.000345 0.00148 1 02/01/2017 03:00 WG948235
1,1,1,2-Tetrachloroethane U 0.000390 0.00148 1 02/01/2017 03:00 WG948235
1,1,2,2-Tetrachloroethane U 0.000539 0.00148 1 02/01/2017 03:00 WG948235
Tetrachloroethene U 0.000407 0.00148 1 02/01/2017 03:00 WG948235
Toluene 0.00158 J 0.000641 0.00738 1 02/01/2017 03:00 WG948235
1,2,3-Trichlorobenzene U 0.000452 0.00148 1 02/01/2017 03:00 WG948235
1,2,4-Trichlorobenzene U 0.000573 0.00148 1 02/01/2017 03:00 WG948235
1,1,1-Trichloroethane U 0.000422 0.00148 1 02/01/2017 03:00 WG948235
1,1,2-Trichloroethane U 0.000409 0.00148 1 02/01/2017 03:00 WG948235
Trichloroethene U 0.000412 0.00148 1 02/01/2017 03:00 WG948235
Trichlorofluoromethane U J3 J4 0.000564 0.00738 1 02/01/2017 03:00 WG948235
1,2,3-Trichloropropane U 0.00109 0.00369 1 02/01/2017 03:00 WG948235
1,2,4-Trimethylbenzene U 0.000311 0.00148 1 02/01/2017 03:00 WG948235
1,3,5-Trimethylbenzene U 0.000393 0.00148 1 02/01/2017 03:00 WG948235
Vinyl chloride U 0.000429 0.00148 1 02/01/2017 03:00 WG948235
Xylenes, Total U 0.00103 0.00443 1 02/01/2017 03:00 WG948235
(S) Toluene-d8 103 80.0-120 02/01/2017 03:00 WG948235
(S) Dibromofluoromethane 107 74.0-131 02/01/2017 03:00 WG948235
(S) a,a,a-Trifluorotoluene 93.7 80.0-120 02/01/2017 03:00 WG948235
(S) 4-Bromofluorobenzene 91.5 64.0-132 02/01/2017 03:00 WG948235
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00948 0.0487 1 02/02/2017 20:24 WG947910
Acenaphthylene U 0.00990 0.0487 1 02/02/2017 20:24 WG947910
Anthracene U 0.00933 0.0487 1 02/02/2017 20:24 WG947910
Benzidine U J4 0.0940 0.491 1 02/02/2017 20:24 WG947910
Benzo(a)anthracene U 0.00632 0.0487 1 02/02/2017 20:24 WG947910
Benzo(b)fluoranthene U 0.0103 0.0487 1 02/02/2017 20:24 WG947910
Benzo(k)fluoranthene U 0.00859 0.0487 1 02/02/2017 20:24 WG947910
Benzo(g,h,i)perylene U 0.0106 0.0487 1 02/02/2017 20:24 WG947910
Benzo(a)pyrene U 0.00809 0.0487 1 02/02/2017 20:24 WG947910
Bis(2-chlorethoxy)methane U 0.0114 0.491 1 02/02/2017 20:24 WG947910
Bis(2-chloroethyl)ether U 0.0132 0.491 1 02/02/2017 20:24 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L886597
TW-2
Collected date/time: 01/25/17 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.0112 0.491 1 02/02/2017 20:24 WG947910
4-Bromophenyl-phenylether U 0.0168 0.491 1 02/02/2017 20:24 WG947910
2-Chloronaphthalene U 0.00943 0.0487 1 02/02/2017 20:24 WG947910
4-Chlorophenyl-phenylether U 0.00925 0.491 1 02/02/2017 20:24 WG947910
Chrysene U 0.00819 0.0487 1 02/02/2017 20:24 WG947910
Dibenz(a,h)anthracene U 0.0121 0.0487 1 02/02/2017 20:24 WG947910
3,3-Dichlorobenzidine U 0.117 0.491 1 02/02/2017 20:24 WG947910
2,4-Dinitrotoluene U 0.00896 0.491 1 02/02/2017 20:24 WG947910
2,6-Dinitrotoluene U 0.0109 0.491 1 02/02/2017 20:24 WG947910
Fluoranthene 0.0211 J 0.00732 0.0487 1 02/02/2017 20:24 WG947910
Fluorene U 0.0101 0.0487 1 02/02/2017 20:24 WG947910
Hexachlorobenzene U 0.0126 0.491 1 02/02/2017 20:24 WG947910
Hexachloro-1,3-butadiene U 0.0148 0.491 1 02/02/2017 20:24 WG947910
Hexachlorocyclopentadiene U 0.0866 0.491 1 02/02/2017 20:24 WG947910
Hexachloroethane U 0.0198 0.491 1 02/02/2017 20:24 WG947910
Indeno(1,2,3-cd)pyrene U 0.0114 0.0487 1 02/02/2017 20:24 WG947910
Isophorone U 0.00770 0.491 1 02/02/2017 20:24 WG947910
Naphthalene U 0.0131 0.0487 1 02/02/2017 20:24 WG947910
Nitrobenzene U 0.0103 0.491 1 02/02/2017 20:24 WG947910
n-Nitrosodimethylamine U 0.0955 0.491 1 02/02/2017 20:24 WG947910
n-Nitrosodiphenylamine U 0.00877 0.491 1 02/02/2017 20:24 WG947910
n-Nitrosodi-n-propylamine U 0.0134 0.491 1 02/02/2017 20:24 WG947910
Phenanthrene U 0.00779 0.0487 1 02/02/2017 20:24 WG947910
Benzylbutyl phthalate U 0.0152 0.491 1 02/02/2017 20:24 WG947910
Bis(2-ethylhexyl)phthalate U 0.0177 0.491 1 02/02/2017 20:24 WG947910
Di-n-butyl phthalate U 0.0161 0.491 1 02/02/2017 20:24 WG947910
Diethyl phthalate U 0.0102 0.491 1 02/02/2017 20:24 WG947910
Dimethyl phthalate U 0.00797 0.491 1 02/02/2017 20:24 WG947910
Di-n-octyl phthalate U 0.0134 0.491 1 02/02/2017 20:24 WG947910
Pyrene U 0.0182 0.0487 1 02/02/2017 20:24 WG947910
1,2,4-Trichlorobenzene U 0.0129 0.491 1 02/02/2017 20:24 WG947910
Aniline U 0.0472 0.491 1 02/02/2017 20:24 WG947910
4-Chloro-3-methylphenol U 0.00704 0.491 1 02/02/2017 20:24 WG947910
2-Chlorophenol U 0.0123 0.491 1 02/02/2017 20:24 WG947910
2,4-Dichlorophenol U 0.0110 0.491 1 02/02/2017 20:24 WG947910
2,4-Dimethylphenol U 0.0695 0.491 1 02/02/2017 20:24 WG947910
4,6-Dinitro-2-methylphenol U 0.183 0.491 1 02/02/2017 20:24 WG947910
2,4-Dinitrophenol U 0.145 0.491 1 02/02/2017 20:24 WG947910
2-Nitrophenol U 0.0192 0.491 1 02/02/2017 20:24 WG947910
4-Nitrophenol U 0.0775 0.491 1 02/02/2017 20:24 WG947910
Pentachlorophenol U 0.0708 0.491 1 02/02/2017 20:24 WG947910
Phenol U 0.0103 0.491 1 02/02/2017 20:24 WG947910
2,4,6-Trichlorophenol U 0.0115 0.491 1 02/02/2017 20:24 WG947910
(S) 2-Fluorophenol 73.1 20.0-120 02/02/2017 20:24 WG947910
(S) Phenol-d5 77.1 20.0-120 02/02/2017 20:24 WG947910
(S) Nitrobenzene-d5 78.0 18.0-125 02/02/2017 20:24 WG947910
(S) 2-Fluorobiphenyl 74.6 28.0-120 02/02/2017 20:24 WG947910
(S) 2,4,6-Tribromophenol 80.2 17.0-137 02/02/2017 20:24 WG947910
(S) p-Terphenyl-d14 64.4 13.0-131 02/02/2017 20:24 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L886597
TW-4
Collected date/time: 01/25/17 00:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.2 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0369 0.00367 0.0262 1 02/01/2017 10:28 WG948080
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.207 0.656 5 02/03/2017 16:34 WG948015
Arsenic 3.08 0.0164 0.656 5 02/03/2017 16:34 WG948015
Beryllium 0.169 J 0.0787 0.656 5 02/03/2017 16:34 WG948015
Cadmium U 0.105 0.656 5 02/03/2017 16:34 WG948015
Chromium 22.0 0.354 0.656 5 02/03/2017 16:34 WG948015
Copper 47.2 0.341 0.656 5 02/03/2017 16:34 WG948015
Lead 30.9 0.157 0.656 5 02/03/2017 16:34 WG948015
Manganese 73.7 0.164 1.31 5 02/03/2017 16:34 WG948015
Nickel 2.38 0.230 0.656 5 02/03/2017 16:34 WG948015
Selenium 0.782 0.249 0.656 5 02/03/2017 16:34 WG948015
Silver U 0.203 0.656 5 02/03/2017 16:34 WG948015
Thallium 0.160 J 0.125 0.656 5 02/03/2017 16:34 WG948015
Zinc 12.4 1.68 6.56 5 02/03/2017 16:34 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0284 J 0.0131 0.0656 1 02/01/2017 03:21 WG948235
Acrylonitrile U 0.00235 0.0131 1 02/01/2017 03:21 WG948235
Benzene U 0.000354 0.00131 1 02/01/2017 03:21 WG948235
Bromobenzene U 0.000373 0.00131 1 02/01/2017 03:21 WG948235
Bromodichloromethane U 0.000333 0.00131 1 02/01/2017 03:21 WG948235
Bromoform U 0.000556 0.00131 1 02/01/2017 03:21 WG948235
Bromomethane U 0.00176 0.00656 1 02/01/2017 03:21 WG948235
n-Butylbenzene U 0.000338 0.00131 1 02/01/2017 03:21 WG948235
sec-Butylbenzene U 0.000264 0.00131 1 02/01/2017 03:21 WG948235
tert-Butylbenzene U 0.000270 0.00131 1 02/01/2017 03:21 WG948235
Carbon tetrachloride U 0.000430 0.00131 1 02/01/2017 03:21 WG948235
Chlorobenzene U 0.000278 0.00131 1 02/01/2017 03:21 WG948235
Chlorodibromomethane U 0.000489 0.00131 1 02/01/2017 03:21 WG948235
Chloroethane U 0.00124 0.00656 1 02/01/2017 03:21 WG948235
2-Chloroethyl vinyl ether U 0.00307 0.0656 1 02/01/2017 03:21 WG948235
Chloroform U 0.000300 0.00656 1 02/01/2017 03:21 WG948235
Chloromethane U 0.000492 0.00328 1 02/01/2017 03:21 WG948235
2-Chlorotoluene U 0.000395 0.00131 1 02/01/2017 03:21 WG948235
4-Chlorotoluene U 0.000315 0.00131 1 02/01/2017 03:21 WG948235
1,2-Dibromo-3-Chloropropane U 0.00138 0.00656 1 02/01/2017 03:21 WG948235
1,2-Dibromoethane U 0.000450 0.00131 1 02/01/2017 03:21 WG948235
Dibromomethane U 0.000501 0.00131 1 02/01/2017 03:21 WG948235
1,2-Dichlorobenzene U 0.000400 0.00131 1 02/01/2017 03:21 WG948235
1,3-Dichlorobenzene U 0.000314 0.00131 1 02/01/2017 03:21 WG948235
1,4-Dichlorobenzene U 0.000296 0.00131 1 02/01/2017 03:21 WG948235
Dichlorodifluoromethane U 0.000935 0.00656 1 02/01/2017 03:21 WG948235
1,1-Dichloroethane U 0.000261 0.00131 1 02/01/2017 03:21 WG948235
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L886597
TW-4
Collected date/time: 01/25/17 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000348 0.00131 1 02/01/2017 03:21 WG948235
1,1-Dichloroethene U 0.000397 0.00131 1 02/01/2017 03:21 WG948235
cis-1,2-Dichloroethene U 0.000308 0.00131 1 02/01/2017 03:21 WG948235
trans-1,2-Dichloroethene U 0.000346 0.00131 1 02/01/2017 03:21 WG948235
1,2-Dichloropropane U 0.000470 0.00131 1 02/01/2017 03:21 WG948235
1,1-Dichloropropene U 0.000416 0.00131 1 02/01/2017 03:21 WG948235
1,3-Dichloropropane U 0.000272 0.00131 1 02/01/2017 03:21 WG948235
cis-1,3-Dichloropropene U 0.000344 0.00131 1 02/01/2017 03:21 WG948235
trans-1,3-Dichloropropene U 0.000350 0.00131 1 02/01/2017 03:21 WG948235
2,2-Dichloropropane U 0.000366 0.00131 1 02/01/2017 03:21 WG948235
Di-isopropyl ether U 0.000325 0.00131 1 02/01/2017 03:21 WG948235
Ethylbenzene U 0.000390 0.00131 1 02/01/2017 03:21 WG948235
Hexachloro-1,3-butadiene U 0.000449 0.00131 1 02/01/2017 03:21 WG948235
Isopropylbenzene U 0.000319 0.00131 1 02/01/2017 03:21 WG948235
p-Isopropyltoluene U 0.000268 0.00131 1 02/01/2017 03:21 WG948235
2-Butanone (MEK)U 0.00614 0.0131 1 02/01/2017 03:21 WG948235
Methylene Chloride U 0.00131 0.00656 1 02/01/2017 03:21 WG948235
4-Methyl-2-pentanone (MIBK) U 0.00247 0.0131 1 02/01/2017 03:21 WG948235
Methyl tert-butyl ether U 0.000278 0.00131 1 02/01/2017 03:21 WG948235
Naphthalene U 0.00131 0.00656 1 02/01/2017 03:21 WG948235
n-Propylbenzene U 0.000270 0.00131 1 02/01/2017 03:21 WG948235
Styrene U 0.000307 0.00131 1 02/01/2017 03:21 WG948235
1,1,1,2-Tetrachloroethane U 0.000346 0.00131 1 02/01/2017 03:21 WG948235
1,1,2,2-Tetrachloroethane U 0.000479 0.00131 1 02/01/2017 03:21 WG948235
Tetrachloroethene U 0.000362 0.00131 1 02/01/2017 03:21 WG948235
Toluene U 0.000569 0.00656 1 02/01/2017 03:21 WG948235
1,2,3-Trichlorobenzene U 0.000401 0.00131 1 02/01/2017 03:21 WG948235
1,2,4-Trichlorobenzene U 0.000509 0.00131 1 02/01/2017 03:21 WG948235
1,1,1-Trichloroethane U 0.000375 0.00131 1 02/01/2017 03:21 WG948235
1,1,2-Trichloroethane U 0.000363 0.00131 1 02/01/2017 03:21 WG948235
Trichloroethene U 0.000366 0.00131 1 02/01/2017 03:21 WG948235
Trichlorofluoromethane U J3 J4 0.000501 0.00656 1 02/01/2017 03:21 WG948235
1,2,3-Trichloropropane U 0.000972 0.00328 1 02/01/2017 03:21 WG948235
1,2,4-Trimethylbenzene U 0.000277 0.00131 1 02/01/2017 03:21 WG948235
1,3,5-Trimethylbenzene U 0.000349 0.00131 1 02/01/2017 03:21 WG948235
Vinyl chloride U 0.000382 0.00131 1 02/01/2017 03:21 WG948235
Xylenes, Total U 0.000916 0.00394 1 02/01/2017 03:21 WG948235
(S) Toluene-d8 102 80.0-120 02/01/2017 03:21 WG948235
(S) Dibromofluoromethane 108 74.0-131 02/01/2017 03:21 WG948235
(S) a,a,a-Trifluorotoluene 93.0 80.0-120 02/01/2017 03:21 WG948235
(S) 4-Bromofluorobenzene 88.1 64.0-132 02/01/2017 03:21 WG948235
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00842 0.0433 1 02/02/2017 16:58 WG947910
Acenaphthylene U 0.00880 0.0433 1 02/02/2017 16:58 WG947910
Anthracene U 0.00829 0.0433 1 02/02/2017 16:58 WG947910
Benzidine U J4 0.0836 0.437 1 02/02/2017 16:58 WG947910
Benzo(a)anthracene 0.00779 J 0.00561 0.0433 1 02/02/2017 16:58 WG947910
Benzo(b)fluoranthene 0.0105 J 0.00912 0.0433 1 02/02/2017 16:58 WG947910
Benzo(k)fluoranthene U 0.00763 0.0433 1 02/02/2017 16:58 WG947910
Benzo(g,h,i)perylene U 0.00946 0.0433 1 02/02/2017 16:58 WG947910
Benzo(a)pyrene U 0.00719 0.0433 1 02/02/2017 16:58 WG947910
Bis(2-chlorethoxy)methane U 0.0101 0.437 1 02/02/2017 16:58 WG947910
Bis(2-chloroethyl)ether U 0.0118 0.437 1 02/02/2017 16:58 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L886597
TW-4
Collected date/time: 01/25/17 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00997 0.437 1 02/02/2017 16:58 WG947910
4-Bromophenyl-phenylether U 0.0150 0.437 1 02/02/2017 16:58 WG947910
2-Chloronaphthalene U 0.00838 0.0433 1 02/02/2017 16:58 WG947910
4-Chlorophenyl-phenylether U 0.00822 0.437 1 02/02/2017 16:58 WG947910
Chrysene U 0.00728 0.0433 1 02/02/2017 16:58 WG947910
Dibenz(a,h)anthracene U 0.0108 0.0433 1 02/02/2017 16:58 WG947910
3,3-Dichlorobenzidine U 0.104 0.437 1 02/02/2017 16:58 WG947910
2,4-Dinitrotoluene U 0.00796 0.437 1 02/02/2017 16:58 WG947910
2,6-Dinitrotoluene U 0.00967 0.437 1 02/02/2017 16:58 WG947910
Fluoranthene 0.0151 J 0.00651 0.0433 1 02/02/2017 16:58 WG947910
Fluorene U 0.00895 0.0433 1 02/02/2017 16:58 WG947910
Hexachlorobenzene U 0.0112 0.437 1 02/02/2017 16:58 WG947910
Hexachloro-1,3-butadiene U 0.0131 0.437 1 02/02/2017 16:58 WG947910
Hexachlorocyclopentadiene U 0.0770 0.437 1 02/02/2017 16:58 WG947910
Hexachloroethane U 0.0176 0.437 1 02/02/2017 16:58 WG947910
Indeno(1,2,3-cd)pyrene U 0.0101 0.0433 1 02/02/2017 16:58 WG947910
Isophorone U 0.00685 0.437 1 02/02/2017 16:58 WG947910
Naphthalene U 0.0117 0.0433 1 02/02/2017 16:58 WG947910
Nitrobenzene U 0.00912 0.437 1 02/02/2017 16:58 WG947910
n-Nitrosodimethylamine U 0.0849 0.437 1 02/02/2017 16:58 WG947910
n-Nitrosodiphenylamine U 0.00779 0.437 1 02/02/2017 16:58 WG947910
n-Nitrosodi-n-propylamine U 0.0119 0.437 1 02/02/2017 16:58 WG947910
Phenanthrene 0.0141 J 0.00693 0.0433 1 02/02/2017 16:58 WG947910
Benzylbutyl phthalate U 0.0135 0.437 1 02/02/2017 16:58 WG947910
Bis(2-ethylhexyl)phthalate U 0.0157 0.437 1 02/02/2017 16:58 WG947910
Di-n-butyl phthalate U 0.0143 0.437 1 02/02/2017 16:58 WG947910
Diethyl phthalate U 0.00906 0.437 1 02/02/2017 16:58 WG947910
Dimethyl phthalate U 0.00708 0.437 1 02/02/2017 16:58 WG947910
Di-n-octyl phthalate U 0.0119 0.437 1 02/02/2017 16:58 WG947910
Pyrene U 0.0161 0.0433 1 02/02/2017 16:58 WG947910
1,2,4-Trichlorobenzene U 0.0115 0.437 1 02/02/2017 16:58 WG947910
Aniline U 0.0420 0.437 1 02/02/2017 16:58 WG947910
4-Chloro-3-methylphenol U 0.00626 0.437 1 02/02/2017 16:58 WG947910
2-Chlorophenol U 0.0109 0.437 1 02/02/2017 16:58 WG947910
2,4-Dichlorophenol U 0.00979 0.437 1 02/02/2017 16:58 WG947910
2,4-Dimethylphenol U 0.0618 0.437 1 02/02/2017 16:58 WG947910
4,6-Dinitro-2-methylphenol U 0.163 0.437 1 02/02/2017 16:58 WG947910
2,4-Dinitrophenol U 0.129 0.437 1 02/02/2017 16:58 WG947910
2-Nitrophenol U 0.0171 0.437 1 02/02/2017 16:58 WG947910
4-Nitrophenol U 0.0689 0.437 1 02/02/2017 16:58 WG947910
Pentachlorophenol U 0.0630 0.437 1 02/02/2017 16:58 WG947910
Phenol U 0.00912 0.437 1 02/02/2017 16:58 WG947910
2,4,6-Trichlorophenol U 0.0102 0.437 1 02/02/2017 16:58 WG947910
(S) 2-Fluorophenol 72.4 20.0-120 02/02/2017 16:58 WG947910
(S) Phenol-d5 75.4 20.0-120 02/02/2017 16:58 WG947910
(S) Nitrobenzene-d5 73.8 18.0-125 02/02/2017 16:58 WG947910
(S) 2-Fluorobiphenyl 77.1 28.0-120 02/02/2017 16:58 WG947910
(S) 2,4,6-Tribromophenol 81.0 17.0-137 02/02/2017 16:58 WG947910
(S) p-Terphenyl-d14 74.6 13.0-131 02/02/2017 16:58 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L886597
TW-5
Collected date/time: 01/25/17 00:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.2 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury U 0.00345 0.0246 1 02/01/2017 10:36 WG948080
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.195 0.616 5 02/03/2017 16:38 WG948015
Arsenic 2.14 0.0154 0.616 5 02/03/2017 16:38 WG948015
Beryllium 2.14 0.0739 0.616 5 02/03/2017 16:38 WG948015
Cadmium 0.210 J 0.0985 0.616 5 02/03/2017 16:38 WG948015
Chromium 42.7 0.333 0.616 5 02/03/2017 16:38 WG948015
Copper 37.5 0.320 0.616 5 02/03/2017 16:38 WG948015
Lead 18.6 0.148 0.616 5 02/03/2017 16:38 WG948015
Manganese 974 1.54 12.3 50 02/04/2017 13:23 WG948015
Nickel 32.0 0.216 0.616 5 02/03/2017 16:38 WG948015
Selenium U 2.34 6.16 50 02/04/2017 13:23 WG948015
Silver U 0.191 0.616 5 02/03/2017 16:38 WG948015
Thallium 1.43 0.117 0.616 5 02/03/2017 16:38 WG948015
Zinc 173 15.8 61.6 50 02/04/2017 13:23 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0858 0.0123 0.0616 1 02/01/2017 03:41 WG948235
Acrylonitrile U 0.00220 0.0123 1 02/01/2017 03:41 WG948235
Benzene U 0.000333 0.00123 1 02/01/2017 03:41 WG948235
Bromobenzene U 0.000350 0.00123 1 02/01/2017 03:41 WG948235
Bromodichloromethane U 0.000313 0.00123 1 02/01/2017 03:41 WG948235
Bromoform U 0.000522 0.00123 1 02/01/2017 03:41 WG948235
Bromomethane U 0.00165 0.00616 1 02/01/2017 03:41 WG948235
n-Butylbenzene U 0.000318 0.00123 1 02/01/2017 03:41 WG948235
sec-Butylbenzene U 0.000248 0.00123 1 02/01/2017 03:41 WG948235
tert-Butylbenzene U 0.000254 0.00123 1 02/01/2017 03:41 WG948235
Carbon tetrachloride U 0.000404 0.00123 1 02/01/2017 03:41 WG948235
Chlorobenzene U 0.000261 0.00123 1 02/01/2017 03:41 WG948235
Chlorodibromomethane U 0.000459 0.00123 1 02/01/2017 03:41 WG948235
Chloroethane U 0.00117 0.00616 1 02/01/2017 03:41 WG948235
2-Chloroethyl vinyl ether U 0.00288 0.0616 1 02/01/2017 03:41 WG948235
Chloroform U 0.000282 0.00616 1 02/01/2017 03:41 WG948235
Chloromethane U 0.000462 0.00308 1 02/01/2017 03:41 WG948235
2-Chlorotoluene U 0.000371 0.00123 1 02/01/2017 03:41 WG948235
4-Chlorotoluene U 0.000296 0.00123 1 02/01/2017 03:41 WG948235
1,2-Dibromo-3-Chloropropane U 0.00129 0.00616 1 02/01/2017 03:41 WG948235
1,2-Dibromoethane U 0.000422 0.00123 1 02/01/2017 03:41 WG948235
Dibromomethane U 0.000471 0.00123 1 02/01/2017 03:41 WG948235
1,2-Dichlorobenzene U 0.000376 0.00123 1 02/01/2017 03:41 WG948235
1,3-Dichlorobenzene U 0.000294 0.00123 1 02/01/2017 03:41 WG948235
1,4-Dichlorobenzene U 0.000278 0.00123 1 02/01/2017 03:41 WG948235
Dichlorodifluoromethane U 0.000878 0.00616 1 02/01/2017 03:41 WG948235
1,1-Dichloroethane U 0.000245 0.00123 1 02/01/2017 03:41 WG948235
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L886597
TW-5
Collected date/time: 01/25/17 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000326 0.00123 1 02/01/2017 03:41 WG948235
1,1-Dichloroethene U 0.000373 0.00123 1 02/01/2017 03:41 WG948235
cis-1,2-Dichloroethene U 0.000289 0.00123 1 02/01/2017 03:41 WG948235
trans-1,2-Dichloroethene U 0.000325 0.00123 1 02/01/2017 03:41 WG948235
1,2-Dichloropropane U 0.000441 0.00123 1 02/01/2017 03:41 WG948235
1,1-Dichloropropene U 0.000390 0.00123 1 02/01/2017 03:41 WG948235
1,3-Dichloropropane U 0.000255 0.00123 1 02/01/2017 03:41 WG948235
cis-1,3-Dichloropropene U 0.000323 0.00123 1 02/01/2017 03:41 WG948235
trans-1,3-Dichloropropene U 0.000329 0.00123 1 02/01/2017 03:41 WG948235
2,2-Dichloropropane U 0.000344 0.00123 1 02/01/2017 03:41 WG948235
Di-isopropyl ether U 0.000305 0.00123 1 02/01/2017 03:41 WG948235
Ethylbenzene U 0.000366 0.00123 1 02/01/2017 03:41 WG948235
Hexachloro-1,3-butadiene U 0.000421 0.00123 1 02/01/2017 03:41 WG948235
Isopropylbenzene U 0.000299 0.00123 1 02/01/2017 03:41 WG948235
p-Isopropyltoluene U 0.000251 0.00123 1 02/01/2017 03:41 WG948235
2-Butanone (MEK)0.0141 0.00576 0.0123 1 02/01/2017 03:41 WG948235
Methylene Chloride U 0.00123 0.00616 1 02/01/2017 03:41 WG948235
4-Methyl-2-pentanone (MIBK) U 0.00232 0.0123 1 02/01/2017 03:41 WG948235
Methyl tert-butyl ether U 0.000261 0.00123 1 02/01/2017 03:41 WG948235
Naphthalene U 0.00123 0.00616 1 02/01/2017 03:41 WG948235
n-Propylbenzene U 0.000254 0.00123 1 02/01/2017 03:41 WG948235
Styrene U 0.000288 0.00123 1 02/01/2017 03:41 WG948235
1,1,1,2-Tetrachloroethane U 0.000325 0.00123 1 02/01/2017 03:41 WG948235
1,1,2,2-Tetrachloroethane U 0.000450 0.00123 1 02/01/2017 03:41 WG948235
Tetrachloroethene U 0.000340 0.00123 1 02/01/2017 03:41 WG948235
Toluene U 0.000535 0.00616 1 02/01/2017 03:41 WG948235
1,2,3-Trichlorobenzene U 0.000377 0.00123 1 02/01/2017 03:41 WG948235
1,2,4-Trichlorobenzene U 0.000478 0.00123 1 02/01/2017 03:41 WG948235
1,1,1-Trichloroethane U 0.000352 0.00123 1 02/01/2017 03:41 WG948235
1,1,2-Trichloroethane U 0.000341 0.00123 1 02/01/2017 03:41 WG948235
Trichloroethene U 0.000344 0.00123 1 02/01/2017 03:41 WG948235
Trichlorofluoromethane U J3 J4 0.000471 0.00616 1 02/01/2017 03:41 WG948235
1,2,3-Trichloropropane U 0.000913 0.00308 1 02/01/2017 03:41 WG948235
1,2,4-Trimethylbenzene U 0.000260 0.00123 1 02/01/2017 03:41 WG948235
1,3,5-Trimethylbenzene U 0.000328 0.00123 1 02/01/2017 03:41 WG948235
Vinyl chloride U 0.000358 0.00123 1 02/01/2017 03:41 WG948235
Xylenes, Total U 0.000860 0.00370 1 02/01/2017 03:41 WG948235
(S) Toluene-d8 102 80.0-120 02/01/2017 03:41 WG948235
(S) Dibromofluoromethane 102 74.0-131 02/01/2017 03:41 WG948235
(S) a,a,a-Trifluorotoluene 96.1 80.0-120 02/01/2017 03:41 WG948235
(S) 4-Bromofluorobenzene 91.2 64.0-132 02/01/2017 03:41 WG948235
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00791 0.0406 1 02/02/2017 17:49 WG947910
Acenaphthylene U 0.00826 0.0406 1 02/02/2017 17:49 WG947910
Anthracene U 0.00778 0.0406 1 02/02/2017 17:49 WG947910
Benzidine U J4 0.0785 0.410 1 02/02/2017 17:49 WG947910
Benzo(a)anthracene 0.00981 J 0.00527 0.0406 1 02/02/2017 17:49 WG947910
Benzo(b)fluoranthene 0.0134 J 0.00856 0.0406 1 02/02/2017 17:49 WG947910
Benzo(k)fluoranthene U 0.00717 0.0406 1 02/02/2017 17:49 WG947910
Benzo(g,h,i)perylene U 0.00888 0.0406 1 02/02/2017 17:49 WG947910
Benzo(a)pyrene 0.00805 J 0.00675 0.0406 1 02/02/2017 17:49 WG947910
Bis(2-chlorethoxy)methane U 0.00948 0.410 1 02/02/2017 17:49 WG947910
Bis(2-chloroethyl)ether U 0.0110 0.410 1 02/02/2017 17:49 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L886597
TW-5
Collected date/time: 01/25/17 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00936 0.410 1 02/02/2017 17:49 WG947910
4-Bromophenyl-phenylether U 0.0140 0.410 1 02/02/2017 17:49 WG947910
2-Chloronaphthalene U 0.00787 0.0406 1 02/02/2017 17:49 WG947910
4-Chlorophenyl-phenylether U 0.00772 0.410 1 02/02/2017 17:49 WG947910
Chrysene 0.00909 J 0.00684 0.0406 1 02/02/2017 17:49 WG947910
Dibenz(a,h)anthracene U 0.0101 0.0406 1 02/02/2017 17:49 WG947910
3,3-Dichlorobenzidine U 0.0978 0.410 1 02/02/2017 17:49 WG947910
2,4-Dinitrotoluene U 0.00748 0.410 1 02/02/2017 17:49 WG947910
2,6-Dinitrotoluene U 0.00908 0.410 1 02/02/2017 17:49 WG947910
Fluoranthene 0.0193 J 0.00611 0.0406 1 02/02/2017 17:49 WG947910
Fluorene U 0.00840 0.0406 1 02/02/2017 17:49 WG947910
Hexachlorobenzene U 0.0105 0.410 1 02/02/2017 17:49 WG947910
Hexachloro-1,3-butadiene U 0.0123 0.410 1 02/02/2017 17:49 WG947910
Hexachlorocyclopentadiene U 0.0723 0.410 1 02/02/2017 17:49 WG947910
Hexachloroethane U 0.0165 0.410 1 02/02/2017 17:49 WG947910
Indeno(1,2,3-cd)pyrene U 0.00951 0.0406 1 02/02/2017 17:49 WG947910
Isophorone U 0.00643 0.410 1 02/02/2017 17:49 WG947910
Naphthalene U 0.0109 0.0406 1 02/02/2017 17:49 WG947910
Nitrobenzene U 0.00856 0.410 1 02/02/2017 17:49 WG947910
n-Nitrosodimethylamine U 0.0797 0.410 1 02/02/2017 17:49 WG947910
n-Nitrosodiphenylamine U 0.00732 0.410 1 02/02/2017 17:49 WG947910
n-Nitrosodi-n-propylamine U 0.0112 0.410 1 02/02/2017 17:49 WG947910
Phenanthrene 0.0132 J 0.00650 0.0406 1 02/02/2017 17:49 WG947910
Benzylbutyl phthalate U 0.0127 0.410 1 02/02/2017 17:49 WG947910
Bis(2-ethylhexyl)phthalate U 0.0148 0.410 1 02/02/2017 17:49 WG947910
Di-n-butyl phthalate U 0.0134 0.410 1 02/02/2017 17:49 WG947910
Diethyl phthalate U 0.00851 0.410 1 02/02/2017 17:49 WG947910
Dimethyl phthalate U 0.00665 0.410 1 02/02/2017 17:49 WG947910
Di-n-octyl phthalate U 0.0112 0.410 1 02/02/2017 17:49 WG947910
Pyrene 0.0159 J 0.0152 0.0406 1 02/02/2017 17:49 WG947910
1,2,4-Trichlorobenzene U 0.0108 0.410 1 02/02/2017 17:49 WG947910
Aniline U 0.0394 0.410 1 02/02/2017 17:49 WG947910
4-Chloro-3-methylphenol U 0.00588 0.410 1 02/02/2017 17:49 WG947910
2-Chlorophenol U 0.0102 0.410 1 02/02/2017 17:49 WG947910
2,4-Dichlorophenol U 0.00919 0.410 1 02/02/2017 17:49 WG947910
2,4-Dimethylphenol U 0.0580 0.410 1 02/02/2017 17:49 WG947910
4,6-Dinitro-2-methylphenol U 0.153 0.410 1 02/02/2017 17:49 WG947910
2,4-Dinitrophenol U 0.121 0.410 1 02/02/2017 17:49 WG947910
2-Nitrophenol U 0.0160 0.410 1 02/02/2017 17:49 WG947910
4-Nitrophenol U 0.0647 0.410 1 02/02/2017 17:49 WG947910
Pentachlorophenol U 0.0591 0.410 1 02/02/2017 17:49 WG947910
Phenol U 0.00856 0.410 1 02/02/2017 17:49 WG947910
2,4,6-Trichlorophenol U 0.00960 0.410 1 02/02/2017 17:49 WG947910
(S) 2-Fluorophenol 64.8 20.0-120 02/02/2017 17:49 WG947910
(S) Phenol-d5 70.2 20.0-120 02/02/2017 17:49 WG947910
(S) Nitrobenzene-d5 64.8 18.0-125 02/02/2017 17:49 WG947910
(S) 2-Fluorobiphenyl 73.7 28.0-120 02/02/2017 17:49 WG947910
(S) 2,4,6-Tribromophenol 80.6 17.0-137 02/02/2017 17:49 WG947910
(S) p-Terphenyl-d14 82.4 13.0-131 02/02/2017 17:49 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L886597
TW-6
Collected date/time: 01/25/17 00:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 68.8 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.263 0.00407 0.0290 1 02/01/2017 10:38 WG948080
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony 0.901 0.229 0.726 5 02/03/2017 16:41 WG948015
Arsenic 5.31 0.0182 0.726 5 02/03/2017 16:41 WG948015
Beryllium 0.889 J 0.871 7.26 50 02/04/2017 13:26 WG948015
Cadmium 1.01 0.116 0.726 5 02/03/2017 16:41 WG948015
Chromium 65.4 0.392 0.726 5 02/03/2017 16:41 WG948015
Copper 80.4 0.378 0.726 5 02/03/2017 16:41 WG948015
Lead 49.6 0.174 0.726 5 02/03/2017 16:41 WG948015
Manganese 979 1.82 14.5 50 02/04/2017 13:26 WG948015
Nickel 14.0 0.254 0.726 5 02/03/2017 16:41 WG948015
Selenium 3.63 0.276 0.726 5 02/03/2017 16:41 WG948015
Silver U 0.225 0.726 5 02/03/2017 16:41 WG948015
Thallium 0.729 0.138 0.726 5 02/03/2017 16:41 WG948015
Zinc 334 18.6 72.6 50 02/04/2017 13:26 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0498 J 0.0145 0.0726 1 02/01/2017 04:02 WG948235
Acrylonitrile U 0.00260 0.0145 1 02/01/2017 04:02 WG948235
Benzene U 0.000392 0.00145 1 02/01/2017 04:02 WG948235
Bromobenzene U 0.000413 0.00145 1 02/01/2017 04:02 WG948235
Bromodichloromethane U 0.000369 0.00145 1 02/01/2017 04:02 WG948235
Bromoform U 0.000616 0.00145 1 02/01/2017 04:02 WG948235
Bromomethane U 0.00195 0.00726 1 02/01/2017 04:02 WG948235
n-Butylbenzene U 0.000375 0.00145 1 02/01/2017 04:02 WG948235
sec-Butylbenzene U 0.000292 0.00145 1 02/01/2017 04:02 WG948235
tert-Butylbenzene U 0.000299 0.00145 1 02/01/2017 04:02 WG948235
Carbon tetrachloride U 0.000476 0.00145 1 02/01/2017 04:02 WG948235
Chlorobenzene U 0.000308 0.00145 1 02/01/2017 04:02 WG948235
Chlorodibromomethane U 0.000542 0.00145 1 02/01/2017 04:02 WG948235
Chloroethane U 0.00137 0.00726 1 02/01/2017 04:02 WG948235
2-Chloroethyl vinyl ether U 0.00340 0.0726 1 02/01/2017 04:02 WG948235
Chloroform U 0.000333 0.00726 1 02/01/2017 04:02 WG948235
Chloromethane U 0.000545 0.00363 1 02/01/2017 04:02 WG948235
2-Chlorotoluene U 0.000437 0.00145 1 02/01/2017 04:02 WG948235
4-Chlorotoluene U 0.000349 0.00145 1 02/01/2017 04:02 WG948235
1,2-Dibromo-3-Chloropropane U 0.00153 0.00726 1 02/01/2017 04:02 WG948235
1,2-Dibromoethane U 0.000498 0.00145 1 02/01/2017 04:02 WG948235
Dibromomethane U 0.000555 0.00145 1 02/01/2017 04:02 WG948235
1,2-Dichlorobenzene U 0.000443 0.00145 1 02/01/2017 04:02 WG948235
1,3-Dichlorobenzene U 0.000347 0.00145 1 02/01/2017 04:02 WG948235
1,4-Dichlorobenzene U 0.000328 0.00145 1 02/01/2017 04:02 WG948235
Dichlorodifluoromethane U 0.00104 0.00726 1 02/01/2017 04:02 WG948235
1,1-Dichloroethane U 0.000289 0.00145 1 02/01/2017 04:02 WG948235
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L886597
TW-6
Collected date/time: 01/25/17 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000385 0.00145 1 02/01/2017 04:02 WG948235
1,1-Dichloroethene U 0.000440 0.00145 1 02/01/2017 04:02 WG948235
cis-1,2-Dichloroethene U 0.000341 0.00145 1 02/01/2017 04:02 WG948235
trans-1,2-Dichloroethene U 0.000383 0.00145 1 02/01/2017 04:02 WG948235
1,2-Dichloropropane U 0.000520 0.00145 1 02/01/2017 04:02 WG948235
1,1-Dichloropropene U 0.000460 0.00145 1 02/01/2017 04:02 WG948235
1,3-Dichloropropane U 0.000301 0.00145 1 02/01/2017 04:02 WG948235
cis-1,3-Dichloropropene U 0.000381 0.00145 1 02/01/2017 04:02 WG948235
trans-1,3-Dichloropropene U 0.000388 0.00145 1 02/01/2017 04:02 WG948235
2,2-Dichloropropane U 0.000405 0.00145 1 02/01/2017 04:02 WG948235
Di-isopropyl ether U 0.000360 0.00145 1 02/01/2017 04:02 WG948235
Ethylbenzene U 0.000431 0.00145 1 02/01/2017 04:02 WG948235
Hexachloro-1,3-butadiene U 0.000497 0.00145 1 02/01/2017 04:02 WG948235
Isopropylbenzene U 0.000353 0.00145 1 02/01/2017 04:02 WG948235
p-Isopropyltoluene U 0.000296 0.00145 1 02/01/2017 04:02 WG948235
2-Butanone (MEK)0.00842 J 0.00680 0.0145 1 02/01/2017 04:02 WG948235
Methylene Chloride U 0.00145 0.00726 1 02/01/2017 04:02 WG948235
4-Methyl-2-pentanone (MIBK) U 0.00273 0.0145 1 02/01/2017 04:02 WG948235
Methyl tert-butyl ether U 0.000308 0.00145 1 02/01/2017 04:02 WG948235
Naphthalene U 0.00145 0.00726 1 02/01/2017 04:02 WG948235
n-Propylbenzene U 0.000299 0.00145 1 02/01/2017 04:02 WG948235
Styrene U 0.000340 0.00145 1 02/01/2017 04:02 WG948235
1,1,1,2-Tetrachloroethane U 0.000383 0.00145 1 02/01/2017 04:02 WG948235
1,1,2,2-Tetrachloroethane U 0.000530 0.00145 1 02/01/2017 04:02 WG948235
Tetrachloroethene U 0.000401 0.00145 1 02/01/2017 04:02 WG948235
Toluene U 0.000630 0.00726 1 02/01/2017 04:02 WG948235
1,2,3-Trichlorobenzene U 0.000444 0.00145 1 02/01/2017 04:02 WG948235
1,2,4-Trichlorobenzene U 0.000564 0.00145 1 02/01/2017 04:02 WG948235
1,1,1-Trichloroethane U 0.000415 0.00145 1 02/01/2017 04:02 WG948235
1,1,2-Trichloroethane U 0.000402 0.00145 1 02/01/2017 04:02 WG948235
Trichloroethene U 0.000405 0.00145 1 02/01/2017 04:02 WG948235
Trichlorofluoromethane U J3 J4 0.000555 0.00726 1 02/01/2017 04:02 WG948235
1,2,3-Trichloropropane U 0.00108 0.00363 1 02/01/2017 04:02 WG948235
1,2,4-Trimethylbenzene U 0.000306 0.00145 1 02/01/2017 04:02 WG948235
1,3,5-Trimethylbenzene U 0.000386 0.00145 1 02/01/2017 04:02 WG948235
Vinyl chloride U 0.000423 0.00145 1 02/01/2017 04:02 WG948235
Xylenes, Total U 0.00101 0.00436 1 02/01/2017 04:02 WG948235
(S) Toluene-d8 101 80.0-120 02/01/2017 04:02 WG948235
(S) Dibromofluoromethane 100 74.0-131 02/01/2017 04:02 WG948235
(S) a,a,a-Trifluorotoluene 98.0 80.0-120 02/01/2017 04:02 WG948235
(S) 4-Bromofluorobenzene 89.8 64.0-132 02/01/2017 04:02 WG948235
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00932 0.0479 1 02/02/2017 19:33 WG947910
Acenaphthylene U 0.00975 0.0479 1 02/02/2017 19:33 WG947910
Anthracene U 0.00918 0.0479 1 02/02/2017 19:33 WG947910
Benzidine U J4 0.0925 0.484 1 02/02/2017 19:33 WG947910
Benzo(a)anthracene U 0.00622 0.0479 1 02/02/2017 19:33 WG947910
Benzo(b)fluoranthene U 0.0101 0.0479 1 02/02/2017 19:33 WG947910
Benzo(k)fluoranthene U 0.00845 0.0479 1 02/02/2017 19:33 WG947910
Benzo(g,h,i)perylene U 0.0105 0.0479 1 02/02/2017 19:33 WG947910
Benzo(a)pyrene U 0.00796 0.0479 1 02/02/2017 19:33 WG947910
Bis(2-chlorethoxy)methane U 0.0112 0.484 1 02/02/2017 19:33 WG947910
Bis(2-chloroethyl)ether U 0.0130 0.484 1 02/02/2017 19:33 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L886597
TW-6
Collected date/time: 01/25/17 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.0110 0.484 1 02/02/2017 19:33 WG947910
4-Bromophenyl-phenylether U 0.0166 0.484 1 02/02/2017 19:33 WG947910
2-Chloronaphthalene U 0.00928 0.0479 1 02/02/2017 19:33 WG947910
4-Chlorophenyl-phenylether U 0.00911 0.484 1 02/02/2017 19:33 WG947910
Chrysene U 0.00806 0.0479 1 02/02/2017 19:33 WG947910
Dibenz(a,h)anthracene U 0.0119 0.0479 1 02/02/2017 19:33 WG947910
3,3-Dichlorobenzidine U 0.115 0.484 1 02/02/2017 19:33 WG947910
2,4-Dinitrotoluene U 0.00882 0.484 1 02/02/2017 19:33 WG947910
2,6-Dinitrotoluene U 0.0107 0.484 1 02/02/2017 19:33 WG947910
Fluoranthene U 0.00720 0.0479 1 02/02/2017 19:33 WG947910
Fluorene U 0.00991 0.0479 1 02/02/2017 19:33 WG947910
Hexachlorobenzene U 0.0124 0.484 1 02/02/2017 19:33 WG947910
Hexachloro-1,3-butadiene U 0.0145 0.484 1 02/02/2017 19:33 WG947910
Hexachlorocyclopentadiene U 0.0853 0.484 1 02/02/2017 19:33 WG947910
Hexachloroethane U 0.0195 0.484 1 02/02/2017 19:33 WG947910
Indeno(1,2,3-cd)pyrene U 0.0112 0.0479 1 02/02/2017 19:33 WG947910
Isophorone U 0.00758 0.484 1 02/02/2017 19:33 WG947910
Naphthalene U 0.0129 0.0479 1 02/02/2017 19:33 WG947910
Nitrobenzene U 0.0101 0.484 1 02/02/2017 19:33 WG947910
n-Nitrosodimethylamine U 0.0940 0.484 1 02/02/2017 19:33 WG947910
n-Nitrosodiphenylamine U 0.00863 0.484 1 02/02/2017 19:33 WG947910
n-Nitrosodi-n-propylamine U 0.0132 0.484 1 02/02/2017 19:33 WG947910
Phenanthrene 0.0103 J 0.00767 0.0479 1 02/02/2017 19:33 WG947910
Benzylbutyl phthalate U 0.0150 0.484 1 02/02/2017 19:33 WG947910
Bis(2-ethylhexyl)phthalate U 0.0174 0.484 1 02/02/2017 19:33 WG947910
Di-n-butyl phthalate U 0.0158 0.484 1 02/02/2017 19:33 WG947910
Diethyl phthalate U 0.0100 0.484 1 02/02/2017 19:33 WG947910
Dimethyl phthalate U 0.00784 0.484 1 02/02/2017 19:33 WG947910
Di-n-octyl phthalate U 0.0132 0.484 1 02/02/2017 19:33 WG947910
Pyrene U 0.0179 0.0479 1 02/02/2017 19:33 WG947910
1,2,4-Trichlorobenzene U 0.0127 0.484 1 02/02/2017 19:33 WG947910
Aniline U 0.0465 0.484 1 02/02/2017 19:33 WG947910
4-Chloro-3-methylphenol U 0.00693 0.484 1 02/02/2017 19:33 WG947910
2-Chlorophenol U 0.0121 0.484 1 02/02/2017 19:33 WG947910
2,4-Dichlorophenol U 0.0108 0.484 1 02/02/2017 19:33 WG947910
2,4-Dimethylphenol U 0.0684 0.484 1 02/02/2017 19:33 WG947910
4,6-Dinitro-2-methylphenol U 0.180 0.484 1 02/02/2017 19:33 WG947910
2,4-Dinitrophenol U 0.142 0.484 1 02/02/2017 19:33 WG947910
2-Nitrophenol U 0.0189 0.484 1 02/02/2017 19:33 WG947910
4-Nitrophenol U 0.0763 0.484 1 02/02/2017 19:33 WG947910
Pentachlorophenol U 0.0697 0.484 1 02/02/2017 19:33 WG947910
Phenol U 0.0101 0.484 1 02/02/2017 19:33 WG947910
2,4,6-Trichlorophenol U 0.0113 0.484 1 02/02/2017 19:33 WG947910
(S) 2-Fluorophenol 47.7 20.0-120 02/02/2017 19:33 WG947910
(S) Phenol-d5 45.7 20.0-120 02/02/2017 19:33 WG947910
(S) Nitrobenzene-d5 51.7 18.0-125 02/02/2017 19:33 WG947910
(S) 2-Fluorobiphenyl 57.3 28.0-120 02/02/2017 19:33 WG947910
(S) 2,4,6-Tribromophenol 55.4 17.0-137 02/02/2017 19:33 WG947910
(S) p-Terphenyl-d14 43.6 13.0-131 02/02/2017 19:33 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L886597
TW-7
Collected date/time: 01/25/17 00:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.6 1 01/31/2017 10:16 WG948071
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0475 0.00347 0.0248 1 02/01/2017 10:13 WG948080
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U J6 0.196 0.620 5 02/03/2017 14:17 WG948015
Arsenic 3.21 0.0155 0.620 5 02/03/2017 14:17 WG948015
Beryllium 0.233 J O1 0.0744 0.620 5 02/03/2017 14:17 WG948015
Cadmium U 0.0992 0.620 5 02/03/2017 14:17 WG948015
Chromium 24.5 0.335 0.620 5 02/03/2017 14:17 WG948015
Copper 18.7 0.322 0.620 5 02/03/2017 14:17 WG948015
Lead 24.1 0.149 0.620 5 02/03/2017 14:17 WG948015
Manganese 179 0.0310 0.200 10 02/03/2017 16:45 WG948015
Nickel 3.69 0.217 0.620 5 02/03/2017 14:17 WG948015
Selenium 0.804 0.236 0.620 5 02/03/2017 14:17 WG948015
Silver U 0.192 0.620 5 02/03/2017 14:17 WG948015
Thallium 0.308 J 0.118 0.620 5 02/03/2017 14:17 WG948015
Zinc 16.8 O1 1.59 6.20 5 02/03/2017 14:17 WG948015
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0124 0.0620 1 02/01/2017 04:23 WG948235
Acrylonitrile U 0.00222 0.0124 1 02/01/2017 04:23 WG948235
Benzene U 0.000335 0.00124 1 02/01/2017 04:23 WG948235
Bromobenzene U 0.000352 0.00124 1 02/01/2017 04:23 WG948235
Bromodichloromethane U 0.000315 0.00124 1 02/01/2017 04:23 WG948235
Bromoform U 0.000526 0.00124 1 02/01/2017 04:23 WG948235
Bromomethane U 0.00166 0.00620 1 02/01/2017 04:23 WG948235
n-Butylbenzene U 0.000320 0.00124 1 02/01/2017 04:23 WG948235
sec-Butylbenzene U 0.000249 0.00124 1 02/01/2017 04:23 WG948235
tert-Butylbenzene U 0.000255 0.00124 1 02/01/2017 04:23 WG948235
Carbon tetrachloride U 0.000407 0.00124 1 02/01/2017 04:23 WG948235
Chlorobenzene U 0.000263 0.00124 1 02/01/2017 04:23 WG948235
Chlorodibromomethane U 0.000463 0.00124 1 02/01/2017 04:23 WG948235
Chloroethane U 0.00117 0.00620 1 02/01/2017 04:23 WG948235
2-Chloroethyl vinyl ether U 0.00290 0.0620 1 02/01/2017 04:23 WG948235
Chloroform U 0.000284 0.00620 1 02/01/2017 04:23 WG948235
Chloromethane U 0.000465 0.00310 1 02/01/2017 04:23 WG948235
2-Chlorotoluene U 0.000373 0.00124 1 02/01/2017 04:23 WG948235
4-Chlorotoluene U 0.000298 0.00124 1 02/01/2017 04:23 WG948235
1,2-Dibromo-3-Chloropropane U 0.00130 0.00620 1 02/01/2017 04:23 WG948235
1,2-Dibromoethane U 0.000425 0.00124 1 02/01/2017 04:23 WG948235
Dibromomethane U 0.000474 0.00124 1 02/01/2017 04:23 WG948235
1,2-Dichlorobenzene U 0.000378 0.00124 1 02/01/2017 04:23 WG948235
1,3-Dichlorobenzene U 0.000296 0.00124 1 02/01/2017 04:23 WG948235
1,4-Dichlorobenzene U 0.000280 0.00124 1 02/01/2017 04:23 WG948235
Dichlorodifluoromethane U 0.000884 0.00620 1 02/01/2017 04:23 WG948235
1,1-Dichloroethane U 0.000247 0.00124 1 02/01/2017 04:23 WG948235
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L886597
TW-7
Collected date/time: 01/25/17 00:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000329 0.00124 1 02/01/2017 04:23 WG948235
1,1-Dichloroethene U 0.000376 0.00124 1 02/01/2017 04:23 WG948235
cis-1,2-Dichloroethene U 0.000291 0.00124 1 02/01/2017 04:23 WG948235
trans-1,2-Dichloroethene U 0.000327 0.00124 1 02/01/2017 04:23 WG948235
1,2-Dichloropropane U 0.000444 0.00124 1 02/01/2017 04:23 WG948235
1,1-Dichloropropene U 0.000393 0.00124 1 02/01/2017 04:23 WG948235
1,3-Dichloropropane U 0.000257 0.00124 1 02/01/2017 04:23 WG948235
cis-1,3-Dichloropropene U 0.000325 0.00124 1 02/01/2017 04:23 WG948235
trans-1,3-Dichloropropene U 0.000331 0.00124 1 02/01/2017 04:23 WG948235
2,2-Dichloropropane U 0.000346 0.00124 1 02/01/2017 04:23 WG948235
Di-isopropyl ether U 0.000308 0.00124 1 02/01/2017 04:23 WG948235
Ethylbenzene U 0.000368 0.00124 1 02/01/2017 04:23 WG948235
Hexachloro-1,3-butadiene U 0.000424 0.00124 1 02/01/2017 04:23 WG948235
Isopropylbenzene U 0.000301 0.00124 1 02/01/2017 04:23 WG948235
p-Isopropyltoluene U 0.000253 0.00124 1 02/01/2017 04:23 WG948235
2-Butanone (MEK)U 0.00580 0.0124 1 02/01/2017 04:23 WG948235
Methylene Chloride U 0.00124 0.00620 1 02/01/2017 04:23 WG948235
4-Methyl-2-pentanone (MIBK) U 0.00233 0.0124 1 02/01/2017 04:23 WG948235
Methyl tert-butyl ether U 0.000263 0.00124 1 02/01/2017 04:23 WG948235
Naphthalene U 0.00124 0.00620 1 02/01/2017 04:23 WG948235
n-Propylbenzene U 0.000255 0.00124 1 02/01/2017 04:23 WG948235
Styrene U 0.000290 0.00124 1 02/01/2017 04:23 WG948235
1,1,1,2-Tetrachloroethane U 0.000327 0.00124 1 02/01/2017 04:23 WG948235
1,1,2,2-Tetrachloroethane U 0.000453 0.00124 1 02/01/2017 04:23 WG948235
Tetrachloroethene U 0.000342 0.00124 1 02/01/2017 04:23 WG948235
Toluene U 0.000538 0.00620 1 02/01/2017 04:23 WG948235
1,2,3-Trichlorobenzene U 0.000380 0.00124 1 02/01/2017 04:23 WG948235
1,2,4-Trichlorobenzene U 0.000481 0.00124 1 02/01/2017 04:23 WG948235
1,1,1-Trichloroethane U 0.000355 0.00124 1 02/01/2017 04:23 WG948235
1,1,2-Trichloroethane U 0.000344 0.00124 1 02/01/2017 04:23 WG948235
Trichloroethene U 0.000346 0.00124 1 02/01/2017 04:23 WG948235
Trichlorofluoromethane U J3 J4 0.000474 0.00620 1 02/01/2017 04:23 WG948235
1,2,3-Trichloropropane U 0.000919 0.00310 1 02/01/2017 04:23 WG948235
1,2,4-Trimethylbenzene U 0.000262 0.00124 1 02/01/2017 04:23 WG948235
1,3,5-Trimethylbenzene U 0.000330 0.00124 1 02/01/2017 04:23 WG948235
Vinyl chloride U 0.000361 0.00124 1 02/01/2017 04:23 WG948235
Xylenes, Total U 0.000866 0.00372 1 02/01/2017 04:23 WG948235
(S) Toluene-d8 99.5 80.0-120 02/01/2017 04:23 WG948235
(S) Dibromofluoromethane 99.5 74.0-131 02/01/2017 04:23 WG948235
(S) a,a,a-Trifluorotoluene 97.1 80.0-120 02/01/2017 04:23 WG948235
(S) 4-Bromofluorobenzene 89.8 64.0-132 02/01/2017 04:23 WG948235
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00796 0.0409 1 02/02/2017 21:15 WG947910
Acenaphthylene U 0.00832 0.0409 1 02/02/2017 21:15 WG947910
Anthracene U 0.00784 0.0409 1 02/02/2017 21:15 WG947910
Benzidine U J4 0.0790 0.413 1 02/02/2017 21:15 WG947910
Benzo(a)anthracene U 0.00531 0.0409 1 02/02/2017 21:15 WG947910
Benzo(b)fluoranthene U 0.00862 0.0409 1 02/02/2017 21:15 WG947910
Benzo(k)fluoranthene U 0.00722 0.0409 1 02/02/2017 21:15 WG947910
Benzo(g,h,i)perylene U 0.00894 0.0409 1 02/02/2017 21:15 WG947910
Benzo(a)pyrene U 0.00680 0.0409 1 02/02/2017 21:15 WG947910
Bis(2-chlorethoxy)methane U 0.00955 0.413 1 02/02/2017 21:15 WG947910
Bis(2-chloroethyl)ether U 0.0111 0.413 1 02/02/2017 21:15 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L886597
TW-7
Collected date/time: 01/25/17 00:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00943 0.413 1 02/02/2017 21:15 WG947910
4-Bromophenyl-phenylether U 0.0141 0.413 1 02/02/2017 21:15 WG947910
2-Chloronaphthalene U 0.00793 0.0409 1 02/02/2017 21:15 WG947910
4-Chlorophenyl-phenylether U 0.00778 0.413 1 02/02/2017 21:15 WG947910
Chrysene U 0.00688 0.0409 1 02/02/2017 21:15 WG947910
Dibenz(a,h)anthracene U 0.0102 0.0409 1 02/02/2017 21:15 WG947910
3,3-Dichlorobenzidine U 0.0985 0.413 1 02/02/2017 21:15 WG947910
2,4-Dinitrotoluene U 0.00753 0.413 1 02/02/2017 21:15 WG947910
2,6-Dinitrotoluene U 0.00914 0.413 1 02/02/2017 21:15 WG947910
Fluoranthene U 0.00615 0.0409 1 02/02/2017 21:15 WG947910
Fluorene U 0.00846 0.0409 1 02/02/2017 21:15 WG947910
Hexachlorobenzene U 0.0106 0.413 1 02/02/2017 21:15 WG947910
Hexachloro-1,3-butadiene U 0.0124 0.413 1 02/02/2017 21:15 WG947910
Hexachlorocyclopentadiene U 0.0728 0.413 1 02/02/2017 21:15 WG947910
Hexachloroethane U 0.0166 0.413 1 02/02/2017 21:15 WG947910
Indeno(1,2,3-cd)pyrene U 0.00957 0.0409 1 02/02/2017 21:15 WG947910
Isophorone U 0.00647 0.413 1 02/02/2017 21:15 WG947910
Naphthalene U 0.0110 0.0409 1 02/02/2017 21:15 WG947910
Nitrobenzene U 0.00862 0.413 1 02/02/2017 21:15 WG947910
n-Nitrosodimethylamine U 0.0802 0.413 1 02/02/2017 21:15 WG947910
n-Nitrosodiphenylamine U 0.00737 0.413 1 02/02/2017 21:15 WG947910
n-Nitrosodi-n-propylamine U 0.0112 0.413 1 02/02/2017 21:15 WG947910
Phenanthrene U 0.00655 0.0409 1 02/02/2017 21:15 WG947910
Benzylbutyl phthalate U 0.0128 0.413 1 02/02/2017 21:15 WG947910
Bis(2-ethylhexyl)phthalate U 0.0149 0.413 1 02/02/2017 21:15 WG947910
Di-n-butyl phthalate U 0.0135 0.413 1 02/02/2017 21:15 WG947910
Diethyl phthalate U 0.00857 0.413 1 02/02/2017 21:15 WG947910
Dimethyl phthalate U 0.00670 0.413 1 02/02/2017 21:15 WG947910
Di-n-octyl phthalate U 0.0112 0.413 1 02/02/2017 21:15 WG947910
Pyrene U 0.0153 0.0409 1 02/02/2017 21:15 WG947910
1,2,4-Trichlorobenzene U 0.0109 0.413 1 02/02/2017 21:15 WG947910
Aniline U 0.0397 0.413 1 02/02/2017 21:15 WG947910
4-Chloro-3-methylphenol U 0.00592 0.413 1 02/02/2017 21:15 WG947910
2-Chlorophenol U 0.0103 0.413 1 02/02/2017 21:15 WG947910
2,4-Dichlorophenol U 0.00925 0.413 1 02/02/2017 21:15 WG947910
2,4-Dimethylphenol U 0.0584 0.413 1 02/02/2017 21:15 WG947910
4,6-Dinitro-2-methylphenol U 0.154 0.413 1 02/02/2017 21:15 WG947910
2,4-Dinitrophenol U 0.122 0.413 1 02/02/2017 21:15 WG947910
2-Nitrophenol U 0.0161 0.413 1 02/02/2017 21:15 WG947910
4-Nitrophenol U 0.0651 0.413 1 02/02/2017 21:15 WG947910
Pentachlorophenol U 0.0595 0.413 1 02/02/2017 21:15 WG947910
Phenol U 0.00862 0.413 1 02/02/2017 21:15 WG947910
2,4,6-Trichlorophenol U 0.00966 0.413 1 02/02/2017 21:15 WG947910
(S) 2-Fluorophenol 67.2 20.0-120 02/02/2017 21:15 WG947910
(S) Phenol-d5 78.2 20.0-120 02/02/2017 21:15 WG947910
(S) Nitrobenzene-d5 72.2 18.0-125 02/02/2017 21:15 WG947910
(S) 2-Fluorobiphenyl 79.5 28.0-120 02/02/2017 21:15 WG947910
(S) 2,4,6-Tribromophenol 88.2 17.0-137 02/02/2017 21:15 WG947910
(S) p-Terphenyl-d14 75.2 13.0-131 02/02/2017 21:15 WG947910
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948070
Total Solids by Method 2540 G-2011 L886597-01,02,03,04,05,06,07,08,09,10
Method Blank (MB)
(MB) R3193952-1 01/31/17 10:31
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000300
L886597-01 Original Sample (OS) • Duplicate (DUP)
(OS) L886597-01 01/31/17 10:31 • (DUP) R3193952-3 01/31/17 10:31
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 72.7 73.1 1 0.518 5
Laboratory Control Sample (LCS)
(LCS) R3193952-2 01/31/17 10:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948071
Total Solids by Method 2540 G-2011 L886597-11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3193951-1 01/31/17 10:16
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000500
L886597-11 Original Sample (OS) • Duplicate (DUP)
(OS) L886597-11 01/31/17 10:16 • (DUP) R3193951-3 01/31/17 10:16
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 78.0 77.3 1 0.971 5
Laboratory Control Sample (LCS)
(LCS) R3193951-2 01/31/17 10:16
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947435
Mercury by Method 7471A L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14
Method Blank (MB)
(MB) R3193584-1 01/30/17 11:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0028 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3193584-2 01/30/17 11:45 • (LCSD) R3193584-3 01/30/17 11:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.278 0.275 93 92 80-120 1 20
L886597-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886597-04 01/30/17 11:50 • (MS) R3193584-4 01/30/17 11:53 • (MSD) R3193584-5 01/30/17 11:55
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.369 0.0277 0.365 0.386 91 97 1 75-125 5 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948080
Mercury by Method 7471A L886597-15,16,17,18,19,20
Method Blank (MB)
(MB) R3194078-1 02/01/17 10:05
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0028 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194078-2 02/01/17 10:07 • (LCSD) R3194078-3 02/01/17 10:10
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.297 0.279 99 93 80-120 6 20
L886597-20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886597-20 02/01/17 10:13 • (MS) R3194078-4 02/01/17 10:15 • (MSD) R3194078-5 02/01/17 10:18
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.372 0.0475 0.405 0.423 96 101 1 75-125 4 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948015
Metals (ICPMS) by Method 6020 L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3194817-1 02/03/17 14:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.158 0.500
Arsenic U 0.0125 0.500
Beryllium U 0.06 0.500
Cadmium U 0.08 0.500
Chromium U 0.27 0.500
Copper U 0.26 0.500
Lead U 0.12 0.500
Manganese 0.133 J 0.125 1.00
Nickel U 0.175 0.500
Selenium U 0.19 0.500
Silver U 0.155 0.500
Thallium U 0.095 0.500
Zinc U 1.28 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194817-2 02/03/17 14:10 • (LCSD) R3194817-3 02/03/17 14:13
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Antimony 116 106 99.8 91 86 80-120 6 20
Arsenic 100 100 101 100 101 80-120 0 20
Beryllium 100 103 97.3 103 97 80-120 5 20
Cadmium 100 109 106 109 106 80-120 3 20
Chromium 100 103 103 103 103 80-120 0 20
Copper 100 105 106 105 106 80-120 0 20
Lead 100 109 104 109 104 80-120 4 20
Manganese 100 103 101 103 101 80-120 2 20
Nickel 100 105 105 105 105 80-120 1 20
Selenium 100 109 105 109 105 80-120 4 20
Silver 20.0 21.8 21.1 109 106 80-120 3 20
Thallium 100 106 103 106 103 80-120 4 20
Zinc 100 101 101 101 101 80-120 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948015
Metals (ICPMS) by Method 6020 L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
L886597-20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886597-20 02/03/17 14:17 • (MS) R3194817-6 02/03/17 14:27 • (MSD) R3194817-7 02/03/17 14:31
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 28.8 U 46.4 43.9 32 31 5 75-125 J6 J6 5 20
Arsenic 24.8 3.21 125 120 98 94 5 75-125 4 20
Beryllium 24.8 0.233 101 99.9 81 80 5 75-125 1 20
Cadmium 24.8 U 139 136 112 109 5 75-125 3 20
Chromium 24.8 24.5 159 154 108 104 5 75-125 3 20
Copper 24.8 18.7 157 153 111 108 5 75-125 2 20
Lead 24.8 24.1 156 154 106 105 5 75-125 1 20
Manganese 24.8 169 287 301 95 106 5 75-125 5 20
Nickel 24.8 3.69 135 129 106 101 5 75-125 5 20
Selenium 24.8 0.804 127 126 102 101 5 75-125 1 20
Silver 4.96 U 26.9 26.1 108 105 5 75-125 3 20
Thallium 24.8 0.308 132 124 106 100 5 75-125 6 20
Zinc 24.8 16.8 150 150 107 107 5 75-125 0 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947760
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Method Blank (MB)
(MB) R3194440-3 01/31/17 17:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947760
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Method Blank (MB)
(MB) R3194440-3 01/31/17 17:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK) U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 104 80.0-120
(S) Dibromofluoromethane 101 74.0-131
(S) a,a,a-Trifluorotoluene 103 80.0-120
(S) 4-Bromofluorobenzene 98.4 64.0-132
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194440-1 01/31/17 16:43 • (LCSD) R3194440-2 01/31/17 17:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.102 0.103 81.9 82.1 11.0-160 0.320 23
Acrylonitrile 0.125 0.114 0.116 91.4 93.2 61.0-143 1.90 20
Benzene 0.0250 0.0238 0.0255 95.3 102 71.0-124 6.78 20
Bromobenzene 0.0250 0.0218 0.0247 87.3 98.6 78.0-120 12.1 20
Bromodichloromethane 0.0250 0.0239 0.0249 95.5 99.5 75.0-120 4.11 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947760
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194440-1 01/31/17 16:43 • (LCSD) R3194440-2 01/31/17 17:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.0250 0.0232 0.0260 92.7 104 65.0-133 11.5 20
Bromomethane 0.0250 0.0217 0.0224 86.6 89.5 26.0-160 3.26 20
n-Butylbenzene 0.0250 0.0231 0.0255 92.5 102 73.0-126 9.82 20
sec-Butylbenzene 0.0250 0.0219 0.0239 87.6 95.5 75.0-121 8.64 20
tert-Butylbenzene 0.0250 0.0226 0.0254 90.5 102 74.0-122 11.6 20
Carbon tetrachloride 0.0250 0.0239 0.0253 95.5 101 66.0-123 5.65 20
Chlorobenzene 0.0250 0.0227 0.0254 90.8 102 79.0-121 11.2 20
Chlorodibromomethane 0.0250 0.0241 0.0271 96.2 108 74.0-128 11.9 20
Chloroethane 0.0250 0.0240 0.0261 96.2 104 51.0-147 8.02 20
2-Chloroethyl vinyl ether 0.125 0.0559 0.0635 44.7 50.8 10.0-160 12.6 22
Chloroform 0.0250 0.0227 0.0240 91.0 95.9 73.0-123 5.29 20
Chloromethane 0.0250 0.0220 0.0227 88.1 90.7 51.0-138 2.83 20
2-Chlorotoluene 0.0250 0.0241 0.0265 96.4 106 72.0-124 9.49 20
4-Chlorotoluene 0.0250 0.0226 0.0252 90.3 101 78.0-120 10.9 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0200 0.0195 80.2 78.1 65.0-126 2.70 20
1,2-Dibromoethane 0.0250 0.0224 0.0248 89.4 99.1 78.0-122 10.2 20
Dibromomethane 0.0250 0.0239 0.0252 95.4 101 79.0-120 5.46 20
1,2-Dichlorobenzene 0.0250 0.0235 0.0253 94.2 101 80.0-120 7.37 20
1,3-Dichlorobenzene 0.0250 0.0217 0.0236 86.7 94.2 72.0-123 8.39 20
1,4-Dichlorobenzene 0.0250 0.0215 0.0236 85.9 94.2 77.0-120 9.20 20
Dichlorodifluoromethane 0.0250 0.0244 0.0248 97.6 99.2 49.0-155 1.62 20
1,1-Dichloroethane 0.0250 0.0238 0.0255 95.4 102 70.0-128 6.57 20
1,2-Dichloroethane 0.0250 0.0234 0.0251 93.8 100 69.0-128 6.69 20
1,1-Dichloroethene 0.0250 0.0245 0.0260 98.2 104 63.0-131 5.71 20
cis-1,2-Dichloroethene 0.0250 0.0222 0.0239 88.7 95.6 74.0-123 7.57 20
trans-1,2-Dichloroethene 0.0250 0.0248 0.0265 99.2 106 72.0-122 6.43 20
1,2-Dichloropropane 0.0250 0.0240 0.0253 96.1 101 75.0-126 5.37 20
1,1-Dichloropropene 0.0250 0.0255 0.0268 102 107 72.0-130 4.99 20
1,3-Dichloropropane 0.0250 0.0231 0.0254 92.6 102 80.0-121 9.30 20
cis-1,3-Dichloropropene 0.0250 0.0255 0.0271 102 109 80.0-125 6.20 20
trans-1,3-Dichloropropene 0.0250 0.0252 0.0262 101 105 75.0-129 3.91 20
2,2-Dichloropropane 0.0250 0.0207 0.0219 82.7 87.4 60.0-129 5.54 20
Di-isopropyl ether 0.0250 0.0231 0.0245 92.2 98.0 62.0-133 6.05 20
Ethylbenzene 0.0250 0.0217 0.0245 86.9 98.0 77.0-120 12.0 20
Hexachloro-1,3-butadiene 0.0250 0.0236 0.0256 94.3 102 68.0-128 8.10 20
Isopropylbenzene 0.0250 0.0221 0.0251 88.2 100 75.0-120 12.7 20
p-Isopropyltoluene 0.0250 0.0226 0.0253 90.3 101 74.0-125 11.4 20
2-Butanone (MEK)0.125 0.106 0.112 85.2 89.8 37.0-159 5.24 20
Methylene Chloride 0.0250 0.0223 0.0232 89.3 92.8 67.0-123 3.81 20
4-Methyl-2-pentanone (MIBK) 0.125 0.116 0.117 92.4 93.5 60.0-144 1.15 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947760
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194440-1 01/31/17 16:43 • (LCSD) R3194440-2 01/31/17 17:06
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Methyl tert-butyl ether 0.0250 0.0222 0.0237 88.8 94.7 66.0-125 6.40 20
Naphthalene 0.0250 0.0224 0.0237 89.5 94.9 64.0-125 5.87 20
n-Propylbenzene 0.0250 0.0224 0.0250 89.4 99.9 78.0-120 11.0 20
Styrene 0.0250 0.0240 0.0267 96.0 107 78.0-124 10.7 20
1,1,1,2-Tetrachloroethane 0.0250 0.0232 0.0261 93.0 104 74.0-124 11.4 20
1,1,2,2-Tetrachloroethane 0.0250 0.0207 0.0227 83.0 91.0 73.0-120 9.19 20
Tetrachloroethene 0.0250 0.0229 0.0259 91.7 104 70.0-127 12.1 20
Toluene 0.0250 0.0232 0.0240 93.0 96.1 77.0-120 3.35 20
1,2,3-Trichlorobenzene 0.0250 0.0230 0.0252 92.1 101 68.0-126 8.80 20
1,2,4-Trichlorobenzene 0.0250 0.0227 0.0257 90.7 103 70.0-127 12.4 20
1,1,1-Trichloroethane 0.0250 0.0244 0.0250 97.7 99.9 69.0-125 2.19 20
1,1,2-Trichloroethane 0.0250 0.0216 0.0241 86.4 96.5 78.0-120 11.0 20
Trichloroethene 0.0250 0.0242 0.0255 96.7 102 79.0-120 5.34 20
Trichlorofluoromethane 0.0250 0.0249 0.0256 99.7 102 59.0-136 2.57 20
1,2,3-Trichloropropane 0.0250 0.0217 0.0242 86.7 96.8 73.0-124 11.1 20
1,2,4-Trimethylbenzene 0.0250 0.0222 0.0244 88.8 97.7 75.0-120 9.54 20
1,3,5-Trimethylbenzene 0.0250 0.0218 0.0244 87.0 97.5 75.0-120 11.4 20
Vinyl chloride 0.0250 0.0247 0.0254 98.7 102 63.0-134 2.89 20
Xylenes, Total 0.0750 0.0663 0.0730 88.4 97.3 77.0-120 9.54 20
(S) Toluene-d8 106 104 80.0-120
(S) Dibromofluoromethane 102 101 74.0-131
(S) a,a,a-Trifluorotoluene 103 102 80.0-120
(S) 4-Bromofluorobenzene 98.3 99.8 64.0-132
L886597-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886597-14 01/31/17 20:33 • (MS) R3194440-4 01/31/17 19:26 • (MSD) R3194440-5 01/31/17 19:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.160 0.0154 0.180 0.183 99.6 102 1.03 10.0-160 1.93 36
Acrylonitrile 0.160 U 0.159 0.135 96.7 81.7 1.03 14.0-160 16.8 33
Benzene 0.0320 U 0.0329 0.0310 99.9 94.1 1.03 13.0-146 6.02 27
Bromobenzene 0.0320 U 0.0310 0.0289 94.2 87.7 1.03 10.0-149 7.09 33
Bromodichloromethane 0.0320 U 0.0334 0.0307 101 93.1 1.03 15.0-142 8.39 28
Bromoform 0.0320 U 0.0337 0.0317 102 96.3 1.03 10.0-147 6.11 31
Bromomethane 0.0320 U 0.0299 0.0272 90.7 82.5 1.03 10.0-160 9.45 32
n-Butylbenzene 0.0320 U 0.0329 0.0285 100 86.5 1.03 10.0-154 14.5 37
sec-Butylbenzene 0.0320 U 0.0304 0.0267 92.3 81.2 1.03 10.0-151 12.9 36
tert-Butylbenzene 0.0320 U 0.0308 0.0287 93.6 87.0 1.03 10.0-152 7.38 35
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947760
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
L886597-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886597-14 01/31/17 20:33 • (MS) R3194440-4 01/31/17 19:26 • (MSD) R3194440-5 01/31/17 19:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.0320 U 0.0323 0.0301 98.0 91.3 1.03 13.0-140 7.02 30
Chlorobenzene 0.0320 U 0.0321 0.0295 97.4 89.5 1.03 10.0-149 8.41 31
Chlorodibromomethane 0.0320 U 0.0333 0.0317 101 96.2 1.03 12.0-147 4.89 29
Chloroethane 0.0320 U 0.0320 0.0302 97.2 91.6 1.03 10.0-159 5.95 33
2-Chloroethyl vinyl ether 0.160 U 0.0963 0.105 58.5 64.0 1.03 10.0-160 9.10 32
Chloroform 0.0320 0.000401 0.0322 0.0293 96.4 87.6 1.03 18.0-148 9.43 28
Chloromethane 0.0320 U 0.0298 0.0279 90.6 84.8 1.03 10.0-146 6.56 29
2-Chlorotoluene 0.0320 U 0.0334 0.0297 101 90.2 1.03 10.0-151 11.6 35
4-Chlorotoluene 0.0320 U 0.0317 0.0290 96.3 88.1 1.03 10.0-150 8.79 35
1,2-Dibromo-3-Chloropropane 0.0320 U 0.0296 0.0272 89.9 82.5 1.03 10.0-149 8.61 34
1,2-Dibromoethane 0.0320 U 0.0323 0.0308 97.9 93.5 1.03 14.0-145 4.56 28
Dibromomethane 0.0320 U 0.0336 0.0311 102 94.5 1.03 18.0-144 7.65 27
1,2-Dichlorobenzene 0.0320 U 0.0338 0.0307 103 93.1 1.03 10.0-153 9.71 34
1,3-Dichlorobenzene 0.0320 U 0.0324 0.0285 98.5 86.5 1.03 10.0-150 12.9 35
1,4-Dichlorobenzene 0.0320 U 0.0326 0.0293 99.0 89.0 1.03 10.0-148 10.6 34
Dichlorodifluoromethane 0.0320 U 0.0322 0.0306 97.8 92.8 1.03 10.0-160 5.30 30
1,1-Dichloroethane 0.0320 U 0.0328 0.0313 99.5 94.9 1.03 19.0-148 4.73 28
1,2-Dichloroethane 0.0320 U 0.0338 0.0313 103 95.0 1.03 17.0-147 7.64 27
1,1-Dichloroethene 0.0320 U 0.0333 0.0305 101 92.5 1.03 10.0-150 8.79 31
cis-1,2-Dichloroethene 0.0320 U 0.0312 0.0282 94.6 85.6 1.03 16.0-145 9.94 28
trans-1,2-Dichloroethene 0.0320 U 0.0326 0.0312 99.0 94.7 1.03 11.0-142 4.44 29
1,2-Dichloropropane 0.0320 U 0.0341 0.0325 103 98.6 1.03 17.0-148 4.70 28
1,1-Dichloropropene 0.0320 U 0.0323 0.0300 97.9 91.1 1.03 10.0-150 7.15 30
1,3-Dichloropropane 0.0320 U 0.0329 0.0310 99.9 94.0 1.03 16.0-148 6.18 27
cis-1,3-Dichloropropene 0.0320 U 0.0327 0.0303 99.2 91.8 1.03 13.0-150 7.69 28
trans-1,3-Dichloropropene 0.0320 U 0.0349 0.0327 106 99.2 1.03 10.0-152 6.70 29
2,2-Dichloropropane 0.0320 U 0.0314 0.0281 95.4 85.4 1.03 16.0-143 11.0 30
Di-isopropyl ether 0.0320 U 0.0336 0.0314 102 95.2 1.03 16.0-149 6.97 28
Ethylbenzene 0.0320 U 0.0302 0.0279 91.5 84.7 1.03 10.0-147 7.78 31
Hexachloro-1,3-butadiene 0.0320 U 0.0292 0.0229 88.7 69.5 1.03 10.0-154 24.2 40
Isopropylbenzene 0.0320 U 0.0312 0.0283 94.5 85.9 1.03 10.0-147 9.61 33
p-Isopropyltoluene 0.0320 U 0.0311 0.0272 94.4 82.7 1.03 10.0-156 13.2 37
2-Butanone (MEK)0.160 U 0.199 0.192 121 117 1.03 10.0-160 3.29 33
Methylene Chloride 0.0320 U 0.0312 0.0299 94.6 90.7 1.03 16.0-139 4.17 29
4-Methyl-2-pentanone (MIBK) 0.160 U 0.169 0.160 103 97.1 1.03 12.0-160 5.50 32
Methyl tert-butyl ether 0.0320 U 0.0331 0.0311 100 94.3 1.03 21.0-145 6.29 29
Naphthalene 0.0320 U 0.0326 0.0298 98.8 90.3 1.03 10.0-153 8.99 36
n-Propylbenzene 0.0320 U 0.0311 0.0280 94.3 85.0 1.03 10.0-151 10.4 34
Styrene 0.0320 U 0.0325 0.0297 98.7 90.0 1.03 10.0-155 9.15 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947760
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
L886597-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886597-14 01/31/17 20:33 • (MS) R3194440-4 01/31/17 19:26 • (MSD) R3194440-5 01/31/17 19:49
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,1,2-Tetrachloroethane 0.0320 U 0.0330 0.0301 100 91.5 1.03 10.0-147 9.04 30
1,1,2,2-Tetrachloroethane 0.0320 U 0.0329 0.0316 99.7 96.0 1.03 10.0-155 3.79 31
Tetrachloroethene 0.0320 U 0.0314 0.0290 95.2 88.0 1.03 10.0-144 7.87 32
Toluene 0.0320 U 0.0314 0.0288 95.2 87.5 1.03 10.0-144 8.38 28
1,2,3-Trichlorobenzene 0.0320 U 0.0342 0.0290 104 88.0 1.03 10.0-153 16.4 40
1,2,4-Trichlorobenzene 0.0320 U 0.0339 0.0285 103 86.6 1.03 10.0-156 17.1 40
1,1,1-Trichloroethane 0.0320 U 0.0328 0.0301 99.7 91.2 1.03 18.0-145 8.87 29
1,1,2-Trichloroethane 0.0320 U 0.0323 0.0300 98.0 90.9 1.03 12.0-151 7.46 28
Trichloroethene 0.0320 U 0.0308 0.0289 93.4 87.6 1.03 11.0-148 6.36 29
Trichlorofluoromethane 0.0320 U 0.0328 0.0308 99.6 93.4 1.03 10.0-157 6.36 34
1,2,3-Trichloropropane 0.0320 U 0.0309 0.0304 93.9 92.2 1.03 10.0-154 1.85 32
1,2,4-Trimethylbenzene 0.0320 U 0.0302 0.0273 91.6 82.7 1.03 10.0-151 10.2 34
1,3,5-Trimethylbenzene 0.0320 U 0.0311 0.0279 94.5 84.8 1.03 10.0-150 10.9 33
Vinyl chloride 0.0320 U 0.0315 0.0304 95.6 92.4 1.03 10.0-150 3.48 29
Xylenes, Total 0.0960 U 0.0916 0.0844 92.6 85.4 1.03 10.0-150 8.12 31
(S) Toluene-d8 105 104 80.0-120
(S) Dibromofluoromethane 101 103 74.0-131
(S) a,a,a-Trifluorotoluene 101 101 80.0-120
(S) 4-Bromofluorobenzene 99.1 97.0 64.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948235
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-16,17,18,19,20
Method Blank (MB)
(MB) R3194064-4 02/01/17 01:15
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948235
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-16,17,18,19,20
Method Blank (MB)
(MB) R3194064-4 02/01/17 01:15
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK) U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 103 80.0-120
(S) Dibromofluoromethane 107 74.0-131
(S) a,a,a-Trifluorotoluene 93.2 80.0-120
(S) 4-Bromofluorobenzene 91.8 64.0-132
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194064-1 01/31/17 23:31 • (LCSD) R3194064-2 01/31/17 23:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.118 0.118 94.6 94.6 11.0-160 0.0500 23
Acrylonitrile 0.125 0.133 0.129 106 103 61.0-143 2.81 20
Benzene 0.0250 0.0264 0.0259 105 104 71.0-124 1.72 20
Bromobenzene 0.0250 0.0229 0.0227 91.5 90.6 78.0-120 0.900 20
Bromodichloromethane 0.0250 0.0243 0.0239 97.0 95.5 75.0-120 1.58 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948235
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-16,17,18,19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194064-1 01/31/17 23:31 • (LCSD) R3194064-2 01/31/17 23:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.0250 0.0228 0.0232 91.4 92.9 65.0-133 1.68 20
Bromomethane 0.0250 0.0307 0.0286 123 114 26.0-160 7.07 20
n-Butylbenzene 0.0250 0.0264 0.0264 106 106 73.0-126 0.130 20
sec-Butylbenzene 0.0250 0.0224 0.0222 89.7 88.8 75.0-121 0.960 20
tert-Butylbenzene 0.0250 0.0220 0.0219 87.8 87.4 74.0-122 0.420 20
Carbon tetrachloride 0.0250 0.0233 0.0232 93.1 92.6 66.0-123 0.560 20
Chlorobenzene 0.0250 0.0242 0.0243 96.8 97.2 79.0-121 0.480 20
Chlorodibromomethane 0.0250 0.0242 0.0249 96.8 99.5 74.0-128 2.72 20
Chloroethane 0.0250 0.0262 0.0250 105 100 51.0-147 4.38 20
2-Chloroethyl vinyl ether 0.125 0.0598 0.0606 47.9 48.5 10.0-160 1.34 22
Chloroform 0.0250 0.0259 0.0252 104 101 73.0-123 2.84 20
Chloromethane 0.0250 0.0214 0.0210 85.7 84.0 51.0-138 2.06 20
2-Chlorotoluene 0.0250 0.0235 0.0230 93.9 91.9 72.0-124 2.18 20
4-Chlorotoluene 0.0250 0.0230 0.0230 92.0 92.0 78.0-120 0.000 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0241 0.0242 96.4 96.8 65.0-126 0.450 20
1,2-Dibromoethane 0.0250 0.0260 0.0264 104 106 78.0-122 1.76 20
Dibromomethane 0.0250 0.0248 0.0246 99.1 98.3 79.0-120 0.860 20
1,2-Dichlorobenzene 0.0250 0.0259 0.0262 104 105 80.0-120 0.980 20
1,3-Dichlorobenzene 0.0250 0.0218 0.0219 87.1 87.7 72.0-123 0.670 20
1,4-Dichlorobenzene 0.0250 0.0257 0.0255 103 102 77.0-120 0.780 20
Dichlorodifluoromethane 0.0250 0.0281 0.0270 113 108 49.0-155 4.23 20
1,1-Dichloroethane 0.0250 0.0258 0.0252 103 101 70.0-128 2.49 20
1,2-Dichloroethane 0.0250 0.0250 0.0247 100 98.9 69.0-128 1.27 20
1,1-Dichloroethene 0.0250 0.0261 0.0233 104 93.3 63.0-131 11.1 20
cis-1,2-Dichloroethene 0.0250 0.0273 0.0260 109 104 74.0-123 5.02 20
trans-1,2-Dichloroethene 0.0250 0.0259 0.0247 104 98.8 72.0-122 4.93 20
1,2-Dichloropropane 0.0250 0.0243 0.0243 97.2 97.4 75.0-126 0.140 20
1,1-Dichloropropene 0.0250 0.0258 0.0253 103 101 72.0-130 1.82 20
1,3-Dichloropropane 0.0250 0.0253 0.0259 101 104 80.0-121 2.50 20
cis-1,3-Dichloropropene 0.0250 0.0235 0.0234 94.0 93.8 80.0-125 0.200 20
trans-1,3-Dichloropropene 0.0250 0.0255 0.0255 102 102 75.0-129 0.0200 20
2,2-Dichloropropane 0.0250 0.0219 0.0230 87.7 92.1 60.0-129 4.84 20
Di-isopropyl ether 0.0250 0.0236 0.0231 94.5 92.3 62.0-133 2.31 20
Ethylbenzene 0.0250 0.0241 0.0242 96.4 96.7 77.0-120 0.270 20
Hexachloro-1,3-butadiene 0.0250 0.0209 0.0216 83.6 86.3 68.0-128 3.24 20
Isopropylbenzene 0.0250 0.0233 0.0231 93.0 92.2 75.0-120 0.860 20
p-Isopropyltoluene 0.0250 0.0215 0.0213 86.0 85.3 74.0-125 0.820 20
2-Butanone (MEK)0.125 0.139 0.136 111 109 37.0-159 2.23 20
Methylene Chloride 0.0250 0.0263 0.0253 105 101 67.0-123 3.71 20
4-Methyl-2-pentanone (MIBK) 0.125 0.112 0.111 89.9 89.1 60.0-144 0.900 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948235
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-16,17,18,19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194064-1 01/31/17 23:31 • (LCSD) R3194064-2 01/31/17 23:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Methyl tert-butyl ether 0.0250 0.0240 0.0232 95.8 92.7 66.0-125 3.34 20
Naphthalene 0.0250 0.0233 0.0247 93.1 98.7 64.0-125 5.79 20
n-Propylbenzene 0.0250 0.0232 0.0232 92.9 92.7 78.0-120 0.250 20
Styrene 0.0250 0.0235 0.0235 94.0 94.2 78.0-124 0.230 20
1,1,1,2-Tetrachloroethane 0.0250 0.0237 0.0232 94.7 92.9 74.0-124 1.91 20
1,1,2,2-Tetrachloroethane 0.0250 0.0243 0.0247 97.2 98.7 73.0-120 1.46 20
Tetrachloroethene 0.0250 0.0229 0.0234 91.8 93.7 70.0-127 2.07 20
Toluene 0.0250 0.0239 0.0239 95.6 95.5 77.0-120 0.0800 20
1,2,3-Trichlorobenzene 0.0250 0.0208 0.0218 83.2 87.4 68.0-126 4.89 20
1,2,4-Trichlorobenzene 0.0250 0.0219 0.0223 87.6 89.4 70.0-127 1.96 20
1,1,1-Trichloroethane 0.0250 0.0252 0.0249 101 99.6 69.0-125 1.14 20
1,1,2-Trichloroethane 0.0250 0.0258 0.0262 103 105 78.0-120 1.60 20
Trichloroethene 0.0250 0.0238 0.0238 95.4 95.1 79.0-120 0.270 20
Trichlorofluoromethane 0.0250 0.0255 0.00839 102 33.6 59.0-136 J3 J4 101 20
1,2,3-Trichloropropane 0.0250 0.0245 0.0245 98.1 98.0 73.0-124 0.170 20
1,2,4-Trimethylbenzene 0.0250 0.0220 0.0218 88.1 87.3 75.0-120 0.920 20
1,3,5-Trimethylbenzene 0.0250 0.0223 0.0221 89.1 88.3 75.0-120 0.810 20
Vinyl chloride 0.0250 0.0261 0.0248 104 99.4 63.0-134 4.90 20
Xylenes, Total 0.0750 0.0702 0.0699 93.6 93.2 77.0-120 0.360 20
(S) Toluene-d8 98.8 99.0 80.0-120
(S) Dibromofluoromethane 104 102 74.0-131
(S) a,a,a-Trifluorotoluene 93.5 93.2 80.0-120
(S) 4-Bromofluorobenzene 92.1 91.3 64.0-132
L886750-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886750-02 02/01/17 06:08 • (MS) R3194064-5 02/01/17 01:57 • (MSD) R3194064-6 02/01/17 02:18
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.175 ND 32.9 26.0 151 119 125 10.0-160 23.5 36
Acrylonitrile 0.175 ND 27.3 24.9 125 114 125 14.0-160 9.14 33
Benzene 0.0349 0.277 4.99 4.88 108 105 125 13.0-146 2.28 27
Bromobenzene 0.0349 ND 4.39 4.40 97.1 97.3 125 10.0-149 0.180 33
Bromodichloromethane 0.0349 ND 4.04 4.15 92.6 95.1 125 15.0-142 2.67 28
Bromoform 0.0349 ND 4.12 4.25 94.3 97.3 125 10.0-147 3.10 31
Bromomethane 0.0349 ND 3.55 3.61 81.4 82.6 125 10.0-160 1.44 32
n-Butylbenzene 0.0349 0.405 4.97 5.21 104 110 125 10.0-154 4.73 37
sec-Butylbenzene 0.0349 ND 4.37 4.32 96.3 95.1 125 10.0-151 1.20 36
tert-Butylbenzene 0.0349 ND 4.18 4.21 95.6 96.4 125 10.0-152 0.850 35
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 83 of 97
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948235
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-16,17,18,19,20
L886750-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886750-02 02/01/17 06:08 • (MS) R3194064-5 02/01/17 01:57 • (MSD) R3194064-6 02/01/17 02:18
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.0349 ND 4.12 4.07 94.3 93.3 125 13.0-140 1.10 30
Chlorobenzene 0.0349 ND 4.52 4.68 103 107 125 10.0-149 3.50 31
Chlorodibromomethane 0.0349 ND 4.34 4.34 99.5 99.3 125 12.0-147 0.150 29
Chloroethane 0.0349 ND 0.761 1.22 17.4 27.9 125 10.0-159 J3 46.3 33
2-Chloroethyl vinyl ether 0.175 ND 11.7 11.8 53.7 54.1 125 10.0-160 0.800 32
Chloroform 0.0349 ND 4.60 4.46 105 102 125 18.0-148 3.05 28
Chloromethane 0.0349 ND 3.97 3.90 91.0 89.3 125 10.0-146 1.87 29
2-Chlorotoluene 0.0349 ND 4.62 4.64 106 106 125 10.0-151 0.560 35
4-Chlorotoluene 0.0349 ND 4.25 4.23 97.3 96.9 125 10.0-150 0.440 35
1,2-Dibromo-3-Chloropropane 0.0349 ND 4.97 5.17 114 118 125 10.0-149 4.04 34
1,2-Dibromoethane 0.0349 ND 4.85 4.91 111 112 125 14.0-145 1.22 28
Dibromomethane 0.0349 ND 4.37 4.33 100 99.2 125 18.0-144 0.910 27
1,2-Dichlorobenzene 0.0349 ND 4.68 4.78 107 109 125 10.0-153 2.05 34
1,3-Dichlorobenzene 0.0349 ND 4.14 4.05 94.8 92.8 125 10.0-150 2.19 35
1,4-Dichlorobenzene 0.0349 ND 4.52 4.66 104 107 125 10.0-148 2.89 34
Dichlorodifluoromethane 0.0349 ND 4.79 5.04 110 115 125 10.0-160 5.03 30
1,1-Dichloroethane 0.0349 ND 4.67 4.52 107 103 125 19.0-148 3.26 28
1,2-Dichloroethane 0.0349 ND 4.52 4.41 103 101 125 17.0-147 2.48 27
1,1-Dichloroethene 0.0349 14.2 18.2 13.0 92.5 0.000 125 10.0-150 J3 J6 33.4 31
cis-1,2-Dichloroethene 0.0349 ND 4.84 4.65 111 106 125 16.0-145 4.10 28
trans-1,2-Dichloroethene 0.0349 ND 5.56 4.53 127 104 125 11.0-142 20.5 29
1,2-Dichloropropane 0.0349 ND 4.35 4.43 99.5 101 125 17.0-148 1.91 28
1,1-Dichloropropene 0.0349 ND 4.67 4.53 107 104 125 10.0-150 3.14 30
1,3-Dichloropropane 0.0349 ND 4.72 4.81 108 110 125 16.0-148 2.03 27
cis-1,3-Dichloropropene 0.0349 ND 4.11 4.11 94.1 94.2 125 13.0-150 0.0400 28
trans-1,3-Dichloropropene 0.0349 ND 4.43 4.42 101 101 125 10.0-152 0.290 29
2,2-Dichloropropane 0.0349 ND 3.71 3.63 85.0 83.2 125 16.0-143 2.14 30
Di-isopropyl ether 0.0349 ND 4.48 4.14 103 94.7 125 16.0-149 8.07 28
Ethylbenzene 0.0349 4.77 8.36 9.13 82.4 99.9 125 10.0-147 8.77 31
Hexachloro-1,3-butadiene 0.0349 ND 3.40 3.70 77.8 84.8 125 10.0-154 8.53 40
Isopropylbenzene 0.0349 0.584 4.85 4.95 97.7 100 125 10.0-147 2.01 33
p-Isopropyltoluene 0.0349 0.261 4.48 4.48 96.7 96.5 125 10.0-156 0.190 37
2-Butanone (MEK)0.175 ND 29.6 27.4 135 125 125 10.0-160 7.68 33
Methylene Chloride 0.0349 ND 6.10 6.78 140 155 125 16.0-139 J5 J5 10.5 29
4-Methyl-2-pentanone (MIBK) 0.175 ND 23.6 22.8 108 105 125 12.0-160 3.24 32
Methyl tert-butyl ether 0.0349 ND 5.22 4.32 120 98.9 125 21.0-145 18.9 29
Naphthalene 0.0349 3.11 7.56 8.09 102 114 125 10.0-153 6.80 36
n-Propylbenzene 0.0349 1.45 5.54 5.70 93.5 97.4 125 10.0-151 3.01 34
Styrene 0.0349 7.35 10.4 11.4 69.8 93.2 125 10.0-155 9.38 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG948235
Volatile Organic Compounds (GC/MS) by Method 8260B L886597-16,17,18,19,20
L886750-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886750-02 02/01/17 06:08 • (MS) R3194064-5 02/01/17 01:57 • (MSD) R3194064-6 02/01/17 02:18
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,1,2-Tetrachloroethane 0.0349 ND 4.18 4.26 95.6 97.5 125 10.0-147 1.89 30
1,1,2,2-Tetrachloroethane 0.0349 ND 1.53 2.62 35.1 59.9 125 10.0-155 J3 52.2 31
Tetrachloroethene 0.0349 1.09 5.14 5.53 92.6 102 125 10.0-144 7.26 32
Toluene 0.0349 4.84 8.11 8.73 75.0 89.2 125 10.0-144 7.35 28
1,2,3-Trichlorobenzene 0.0349 ND 4.05 4.27 92.7 97.8 125 10.0-153 5.29 40
1,2,4-Trichlorobenzene 0.0349 ND 4.25 4.39 97.3 101 125 10.0-156 3.31 40
1,1,1-Trichloroethane 0.0349 ND 4.58 4.44 105 102 125 18.0-145 3.16 29
1,1,2-Trichloroethane 0.0349 ND 4.69 4.80 107 110 125 12.0-151 2.13 28
Trichloroethene 0.0349 ND 6.73 6.08 154 139 125 11.0-148 J5 10.1 29
Trichlorofluoromethane 0.0349 2.87 8.84 14.3 137 263 125 10.0-157 J3 J5 47.4 34
1,2,3-Trichloropropane 0.0349 ND 4.91 4.62 112 106 125 10.0-154 6.09 32
1,2,4-Trimethylbenzene 0.0349 9.64 11.8 12.7 49.1 69.0 125 10.0-151 7.14 34
1,3,5-Trimethylbenzene 0.0349 2.40 6.12 6.31 85.1 89.5 125 10.0-150 3.10 33
Vinyl chloride 0.0349 ND 4.38 4.32 100 98.8 125 10.0-150 1.51 29
Xylenes, Total 0.105 13.7 24.1 26.2 79.8 95.2 125 10.0-150 7.98 31
(S) Toluene-d8 98.1 97.9 80.0-120
(S) Dibromofluoromethane 101 97.1 74.0-131
(S) a,a,a-Trifluorotoluene 93.8 95.6 80.0-120
(S) 4-Bromofluorobenzene 95.7 94.4 64.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947910
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3194753-3 02/02/17 13:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0330
Acenaphthylene U 0.00671 0.0330
Aniline U 0.0320 0.333
Anthracene U 0.00632 0.0330
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0330
Benzo(b)fluoranthene U 0.00695 0.0330
Benzo(k)fluoranthene U 0.00582 0.0330
Benzo(g,h,i)perylene U 0.00721 0.0330
Benzo(a)pyrene U 0.00548 0.0330
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0330
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0330
Dibenz(a,h)anthracene U 0.00821 0.0330
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0330
Fluorene U 0.00682 0.0330
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0330
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0330
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.00594 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0330
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947910
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Method Blank (MB)
(MB) R3194753-3 02/02/17 13:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Di-n-octyl phthalate U 0.00907 0.333
Pyrene U 0.0123 0.0330
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 75.3 18.0-125
(S) 2-Fluorobiphenyl 75.6 28.0-120
(S) p-Terphenyl-d14 83.8 13.0-131
(S) Phenol-d5 74.9 20.0-120
(S) 2-Fluorophenol 72.3 20.0-120
(S) 2,4,6-Tribromophenol 73.0 17.0-137
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194753-1 02/02/17 12:14 • (LCSD) R3194753-2 02/02/17 12:40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.667 0.577 0.553 86.5 82.8 47.0-120 4.34 21
Acenaphthylene 0.667 0.599 0.566 89.8 84.8 48.0-120 5.77 21
Aniline 0.667 0.456 0.412 68.4 61.8 27.0-120 10.2 28
Anthracene 0.667 0.593 0.544 88.9 81.6 46.0-120 8.57 20
Benzidine 0.667 ND ND 0.000 0.000 1.00-120 J4 J4 0.000 36
Benzo(a)anthracene 0.667 0.569 0.540 85.3 80.9 46.0-120 5.33 20
Benzo(b)fluoranthene 0.667 0.584 0.567 87.5 85.0 45.0-120 2.87 22
Benzo(k)fluoranthene 0.667 0.573 0.533 85.9 79.9 45.0-120 7.29 23
Benzo(g,h,i)perylene 0.667 0.538 0.540 80.7 80.9 48.0-120 0.310 21
Benzo(a)pyrene 0.667 0.585 0.561 87.7 84.2 46.0-120 4.18 21
Bis(2-chlorethoxy)methane 0.667 0.460 0.437 69.0 65.5 41.0-120 5.07 22
Bis(2-chloroethyl)ether 0.667 0.547 0.506 82.0 75.8 28.0-120 7.78 28
Bis(2-chloroisopropyl)ether 0.667 0.531 0.508 79.7 76.2 40.0-120 4.43 27
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947910
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194753-1 02/02/17 12:14 • (LCSD) R3194753-2 02/02/17 12:40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
4-Bromophenyl-phenylether 0.667 0.544 0.513 81.6 76.9 45.0-120 5.96 20
2-Chloronaphthalene 0.667 0.542 0.523 81.2 78.5 43.0-120 3.44 22
4-Chlorophenyl-phenylether 0.667 0.541 0.500 81.1 74.9 46.0-120 7.94 21
Chrysene 0.667 0.579 0.555 86.9 83.2 46.0-120 4.27 20
Dibenz(a,h)anthracene 0.667 0.549 0.544 82.3 81.5 47.0-120 0.940 22
3,3-Dichlorobenzidine 0.667 0.587 0.580 88.0 86.9 20.0-130 1.27 24
2,4-Dinitrotoluene 0.667 0.650 0.602 97.5 90.3 48.0-122 7.59 21
2,6-Dinitrotoluene 0.667 0.607 0.569 91.0 85.3 46.0-120 6.47 21
Fluoranthene 0.667 0.574 0.534 86.0 80.1 46.0-120 7.15 20
Fluorene 0.667 0.584 0.547 87.6 82.0 47.0-120 6.63 20
Hexachlorobenzene 0.667 0.532 0.502 79.7 75.3 42.0-120 5.77 20
Hexachloro-1,3-butadiene 0.667 0.375 0.362 56.2 54.3 36.0-120 3.44 26
Hexachlorocyclopentadiene 0.667 0.566 0.536 84.9 80.4 20.0-124 5.48 26
Hexachloroethane 0.667 0.480 0.450 71.9 67.4 32.0-120 6.48 31
Indeno(1,2,3-cd)pyrene 0.667 0.550 0.542 82.4 81.3 48.0-120 1.45 21
Isophorone 0.667 0.510 0.478 76.5 71.6 42.0-120 6.61 21
Naphthalene 0.667 0.405 0.393 60.7 58.9 41.0-120 2.99 24
Nitrobenzene 0.667 0.461 0.438 69.1 65.6 36.0-120 5.16 24
n-Nitrosodimethylamine 0.667 0.506 0.448 75.9 67.1 20.0-120 12.2 31
n-Nitrosodiphenylamine 0.667 0.536 0.515 80.4 77.2 42.0-120 4.04 20
n-Nitrosodi-n-propylamine 0.667 0.600 0.558 90.0 83.7 39.0-120 7.26 23
Phenanthrene 0.667 0.578 0.539 86.6 80.8 45.0-120 6.91 20
Benzylbutyl phthalate 0.667 0.629 0.603 94.3 90.4 41.0-123 4.14 20
Bis(2-ethylhexyl)phthalate 0.667 0.611 0.583 91.6 87.4 41.0-124 4.69 20
Di-n-butyl phthalate 0.667 0.623 0.577 93.5 86.6 44.0-120 7.66 20
Diethyl phthalate 0.667 0.604 0.556 90.6 83.4 46.0-120 8.22 20
Dimethyl phthalate 0.667 0.584 0.555 87.6 83.3 47.0-120 5.09 21
Di-n-octyl phthalate 0.667 0.646 0.605 96.8 90.6 40.0-123 6.62 21
Pyrene 0.667 0.564 0.542 84.6 81.3 45.0-120 4.00 21
1,2,4-Trichlorobenzene 0.667 0.378 0.361 56.7 54.1 40.0-120 4.69 25
4-Chloro-3-methylphenol 0.667 0.474 0.455 71.0 68.3 46.0-120 3.98 20
2-Chlorophenol 0.667 0.501 0.468 75.1 70.1 37.0-120 6.91 27
2,4-Dichlorophenol 0.667 0.426 0.405 63.9 60.7 45.0-120 5.02 21
2,4-Dimethylphenol 0.667 0.435 0.411 65.2 61.6 40.0-120 5.71 22
4,6-Dinitro-2-methylphenol 0.667 0.633 0.592 94.9 88.7 34.0-120 6.75 23
2,4-Dinitrophenol 0.667 0.493 0.481 73.9 72.1 10.0-120 2.47 30
2-Nitrophenol 0.667 0.454 0.439 68.1 65.8 42.0-120 3.43 24
4-Nitrophenol 0.667 0.679 0.639 102 95.9 40.0-120 6.04 21
Pentachlorophenol 0.667 0.604 0.572 90.6 85.8 33.0-122 5.46 22
Phenol 0.667 0.536 0.503 80.3 75.4 38.0-120 6.27 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947910
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3194753-1 02/02/17 12:14 • (LCSD) R3194753-2 02/02/17 12:40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2,4,6-Trichlorophenol 0.667 0.576 0.562 86.3 84.2 47.0-120 2.47 22
(S) Nitrobenzene-d5 65.4 63.3 18.0-125
(S) 2-Fluorobiphenyl 83.4 80.5 28.0-120
(S) p-Terphenyl-d14 79.6 77.4 13.0-131
(S) Phenol-d5 81.4 78.6 20.0-120
(S) 2-Fluorophenol 78.4 74.0 20.0-120
(S) 2,4,6-Tribromophenol 85.8 81.0 17.0-137
L886597-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886597-05 02/02/17 13:31 • (MS) R3194753-4 02/02/17 13:57 • (MSD) R3194753-5 02/02/17 14:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.862 U 0.736 0.610 85.4 70.7 1 37.0-120 18.8 23
Acenaphthylene 0.862 U 0.775 0.630 89.9 73.2 1 41.0-120 20.5 22
Aniline 0.862 U 0.653 0.551 75.8 64.0 1 10.0-120 17.0 31
Anthracene 0.862 U 0.725 0.597 84.1 69.3 1 30.0-123 19.3 25
Benzidine 0.862 U ND ND 0.000 0.000 1 1.00-120 J6 J6 0.000 36
Benzo(a)anthracene 0.862 U 0.660 0.560 76.6 65.0 1 21.0-123 16.4 26
Benzo(b)fluoranthene 0.862 U 0.673 0.584 78.1 67.8 1 20.0-127 14.1 29
Benzo(k)fluoranthene 0.862 U 0.672 0.558 78.0 64.8 1 22.0-123 18.5 28
Benzo(g,h,i)perylene 0.862 U 0.633 0.563 73.4 65.3 1 10.0-120 11.8 32
Benzo(a)pyrene 0.862 U 0.680 0.576 78.9 66.8 1 23.0-120 16.6 27
Bis(2-chlorethoxy)methane 0.862 U 0.595 0.521 69.1 60.4 1 37.0-120 13.4 22
Bis(2-chloroethyl)ether 0.862 U 0.690 0.594 80.1 68.9 1 26.0-120 15.0 27
Bis(2-chloroisopropyl)ether 0.862 U 0.688 0.593 79.9 68.8 1 35.0-120 14.9 25
4-Bromophenyl-phenylether 0.862 U 0.663 0.547 77.0 63.5 1 34.0-120 19.2 23
2-Chloronaphthalene 0.862 U 0.705 0.591 81.8 68.6 1 40.0-120 17.6 22
4-Chlorophenyl-phenylether 0.862 U 0.674 0.547 78.3 63.5 1 37.0-120 20.9 23
Chrysene 0.862 U 0.690 0.583 80.1 67.7 1 19.0-127 16.8 27
Dibenz(a,h)anthracene 0.862 U 0.654 0.569 75.9 66.0 1 10.0-120 13.9 28
3,3-Dichlorobenzidine 0.862 U 1.06 0.920 123 107 1 10.0-142 13.8 30
2,4-Dinitrotoluene 0.862 U 0.846 0.677 98.2 78.6 1 37.0-129 22.2 24
2,6-Dinitrotoluene 0.862 U 0.796 0.654 92.3 75.9 1 40.0-120 19.5 23
Fluoranthene 0.862 U 0.695 0.575 80.6 66.8 1 20.0-133 18.8 28
Fluorene 0.862 U 0.746 0.611 86.5 70.9 1 35.0-120 19.9 23
Hexachlorobenzene 0.862 U 0.649 0.536 75.3 62.2 1 33.0-120 19.0 24
Hexachloro-1,3-butadiene 0.862 U 0.468 0.400 54.4 46.5 1 33.0-120 15.6 25
Hexachlorocyclopentadiene 0.862 U 0.687 0.566 79.8 65.7 1 10.0-120 19.4 33
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 89 of 97
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG947910
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L886597-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20
L886597-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L886597-05 02/02/17 13:31 • (MS) R3194753-4 02/02/17 13:57 • (MSD) R3194753-5 02/02/17 14:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexachloroethane 0.862 U 0.592 0.500 68.7 58.0 1 21.0-120 16.9 30
Indeno(1,2,3-cd)pyrene 0.862 U 0.641 0.563 74.4 65.3 1 10.0-120 12.9 30
Isophorone 0.862 U 0.647 0.562 75.1 65.2 1 38.0-120 14.1 22
Naphthalene 0.862 U 0.525 0.459 61.0 53.3 1 37.0-120 13.5 25
Nitrobenzene 0.862 U 0.596 0.514 69.1 59.7 1 32.0-120 14.7 24
n-Nitrosodimethylamine 0.862 U 0.606 0.513 70.3 59.6 1 18.0-120 16.5 27
n-Nitrosodiphenylamine 0.862 U 0.707 0.581 82.1 67.4 1 20.0-125 19.6 25
n-Nitrosodi-n-propylamine 0.862 U 0.759 0.646 88.1 74.9 1 34.0-120 16.2 23
Phenanthrene 0.862 U 0.712 0.583 82.6 67.7 1 24.0-124 19.9 25
Benzylbutyl phthalate 0.862 U 0.693 0.600 80.5 69.6 1 18.0-130 14.5 27
Bis(2-ethylhexyl)phthalate 0.862 U 0.680 0.585 78.9 67.9 1 19.0-127 14.9 28
Di-n-butyl phthalate 0.862 U 0.695 0.564 80.7 65.5 1 29.0-120 20.8 26
Diethyl phthalate 0.862 U 0.777 0.626 90.1 72.6 1 42.0-121 21.6 23
Dimethyl phthalate 0.862 U 0.767 0.625 89.0 72.5 1 42.0-120 20.5 23
Di-n-octyl phthalate 0.862 U 0.712 0.608 82.7 70.6 1 21.0-122 15.8 27
Pyrene 0.862 U 0.681 0.590 79.1 68.5 1 19.0-127 14.3 29
1,2,4-Trichlorobenzene 0.862 U 0.484 0.417 56.2 48.3 1 39.0-120 15.0 25
4-Chloro-3-methylphenol 0.862 U 0.627 0.541 72.8 62.8 1 37.0-121 14.7 23
2-Chlorophenol 0.862 U 0.652 0.554 75.6 64.3 1 34.0-120 16.2 25
2,4-Dichlorophenol 0.862 U 0.564 0.493 65.5 57.2 1 41.0-120 13.4 22
2,4-Dimethylphenol 0.862 U 0.593 0.521 68.9 60.4 1 27.0-120 13.0 25
4,6-Dinitro-2-methylphenol 0.862 U 0.862 0.716 100 83.1 1 10.0-131 18.5 29
2,4-Dinitrophenol 0.862 U 0.738 0.600 85.6 69.6 1 10.0-142 20.7 30
2-Nitrophenol 0.862 U 0.613 0.537 71.1 62.3 1 34.0-124 13.1 27
4-Nitrophenol 0.862 U 0.871 0.723 101 84.0 1 26.0-133 18.5 25
Pentachlorophenol 0.862 U 0.831 0.671 96.4 77.9 1 15.0-152 21.2 26
Phenol 0.862 U 0.684 0.582 79.4 67.5 1 33.0-120 16.2 24
2,4,6-Trichlorophenol 0.862 U 0.782 0.642 90.8 74.5 1 40.0-125 19.7 24
(S) Nitrobenzene-d5 66.0 57.0 18.0-125
(S) 2-Fluorobiphenyl 82.8 69.4 28.0-120
(S) p-Terphenyl-d14 67.7 59.2 13.0-131
(S) Phenol-d5 80.3 66.6 20.0-120
(S) 2-Fluorophenol 77.3 66.2 20.0-120
(S) 2,4,6-Tribromophenol 88.6 70.7 17.0-137
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 90 of 97
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 90 of 97
ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is
high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
O1 The analyte failed the method required serial dilution test and/or subsequent post-spike criteria.
These failures indicate matrix interference.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 91 of 97
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 91 of 97
ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:26 92 of 97
Our Locations
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State Accreditations
Third Party & Federal Accreditations
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our “one location” design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
1. Drinking Water 2. Underground Storage Tanks 3. Aquatic Toxicity 4. Chemical/Microbiological 5. Mold n/a Accreditation not applicable
1461.02A2LA – ISO 170255
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.20 L886597 02/22/17 08:40 92 of 97
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-16
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_47
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-2
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-17
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_48
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-4
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-18
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_49
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-5
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-19
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_50
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-6
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-20
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_51
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-7
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-01
Withers & Ravenel Eng. - Standard
1/24/2017
1/31/2017
SOIL
0131_17
1.00
mg/kg 2
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
BG-1
Project Desc.Pilot Mt. Brownfields
Silanol, trimethyl-001066-40-6 3.73 J 91.000.015
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 91.000.013
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-02
Withers & Ravenel Eng. - Standard
1/24/2017
1/31/2017
SOIL
0131_19
1.00
mg/kg 3
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
BG-2
Project Desc.Pilot Mt. Brownfields
Silanol, trimethyl-001066-40-6 3.73 J 83.000.008
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 83.000.017
Cyclotrisiloxane, hexamethyl-000541-05-9 5.42 J 80.000.012
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-03
Withers & Ravenel Eng. - Standard
1/24/2017
1/31/2017
SOIL
0131_20
1.00
mg/kg 2
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-1
Project Desc.Pilot Mt. Brownfields
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 90.000.005
Cyclotrisiloxane, hexamethyl-000541-05-9 5.42 J 80.000.009
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-04
Withers & Ravenel Eng. - Standard
1/24/2017
1/31/2017
SOIL
0131_21
1.00
mg/kg 3
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-5
Project Desc.Pilot Mt. Brownfields
Cyclotrisiloxane, hexamethyl-000541-05-9 5.42 J 90.000.010
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 90.000.006
Cyclopentane000287-92-3 2.87 J 86.000.017
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-05
Withers & Ravenel Eng. - Standard
1/24/2017
1/31/2017
SOIL
0131_22
1.17
mg/kg 2
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-7
Project Desc.Pilot Mt. Brownfields
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 91.000.007
Cyclopentane000287-92-3 2.87 J 86.000.019
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-06
Withers & Ravenel Eng. - Standard
1/24/2017
1/31/2017
SOIL
0131_23
1.00
mg/kg 1
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-8
Project Desc.Pilot Mt. Brownfields
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 91.000.006
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-07
Withers & Ravenel Eng. - Standard
1/24/2017
2/1/2017
SOIL
0131_24
1.01
mg/kg 3
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-9
Project Desc.Pilot Mt. Brownfields
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 90.000.007
1-Propene, 2-methyl-000115-11-7 1.84 J 87.000.034
Cyclotrisiloxane, hexamethyl-000541-05-9 5.42 J 80.000.013
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-08
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_25
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-10
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-09
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_26
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-11
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-10
Withers & Ravenel Eng. - Standard
1/24/2017
2/1/2017
SOIL
0131_27
1.00
mg/kg 3
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-12
Project Desc.Pilot Mt. Brownfields
Cyclopentane000287-92-3 2.87 J 86.000.016
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 83.000.004
Cyclotrisiloxane, hexamethyl-000541-05-9 5.42 J 80.000.008
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-11
Withers & Ravenel Eng. - Standard
1/24/2017
2/1/2017
SOIL
0131_28
1.00
mg/kg 1
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-13
Project Desc.Pilot Mt. Brownfields
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 87.000.006
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-12
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_29
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-14
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-13
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_30
1.07
mg/kg 2
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-15
Project Desc.Pilot Mt. Brownfields
Cyclotetrasiloxane, octamethyl-000556-67-2 7.06 J 87.000.006
Cyclotrisiloxane, hexamethyl-000541-05-9 5.42 J 80.000.010
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-14
Withers & Ravenel Eng. - Standard
1/25/2017
1/31/2017
SOIL
0131_14
1.03
mg/kg 1
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-16
Project Desc.Pilot Mt. Brownfields
Octanal000124-13-0 8.12 J 90.000.005
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-15
Withers & Ravenel Eng. - Standard
1/25/2017
2/1/2017
SOIL
0131_31
1.03
mg/kg 1
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
DUPE
Project Desc.Pilot Mt. Brownfields
Cyclotrisiloxane, hexamethyl-000541-05-9 5.42 J 90.000.011
Page 1 of 1VOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-01
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_19
1.00
mg/kg 3
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
BG-1
Project Desc.Pilot Mt. Brownfields
1H-Cycloprop[e]azulene, 1a,2,3,4,4000489-40-7 8.11 J 99.001.04
Hexadecanoic acid000057-10-3 10.71 J 99.000.192
Naphthalene, 1,2,3,4,4a,5,6,8a-oct030021-74-0 8.47 J 96.000.070
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-02
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_20
1.00
mg/kg 6
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
BG-2
Project Desc.Pilot Mt. Brownfields
1-Eicosanol000629-96-9 15.40 J 94.000.052
1-Docosene001599-67-3 13.52 J 93.000.134
.gamma.-Sitosterol000083-47-6 17.44 J 93.000.163
Oxirane, hexadecyl-007390-81-0 15.05 J 91.000.086
Dotriacontane000544-85-4 15.34 J 91.000.054
13-Octadecenal056554-90-6 14.08 J 90.000.088
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-03
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_22
1.00
mg/kg 1
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-1
Project Desc.Pilot Mt. Brownfields
Hexadecanoic acid000057-10-3 10.70 J 98.000.076
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-04
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_10
1.00
mg/kg 1
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-5
Project Desc.Pilot Mt. Brownfields
Hexadecanoic acid000057-10-3 10.70 J 97.000.060
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-05
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_07
1.00
mg/kg 3
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-7
Project Desc.Pilot Mt. Brownfields
Octadecanoic acid000057-11-4 11.55 J 98.000.036
Hexadecanoic acid000057-10-3 10.71 J 97.000.056
trans-Chlordane005103-74-2 11.72 J 90.000.055
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-06
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_11
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-8
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-07
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_16
1.00
mg/kg 1
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-9
Project Desc.Pilot Mt. Brownfields
Octadecanoic acid000057-11-4 11.55 J 98.000.064
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-09
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_24
1.00
mg/kg 5
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-11
Project Desc.Pilot Mt. Brownfields
Hexadecanoic acid000057-10-3 10.71 J 99.000.223
Octadecanoic acid000057-11-4 11.55 J 98.000.217
Eicosane000112-95-8 9.52 J 91.000.042
Hexadecane, 2,6,10,14-tetramethyl-000638-36-8 10.04 J 90.000.037
28-Nor-17.alpha.(H)-hopane053584-60-4 15.79 J 86.000.089
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-10
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_12
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-12
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-11
Withers & Ravenel Eng. - Standard
1/24/2017
2/2/2017
SOIL
0202_18
1.00
mg/kg 1
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-13
Project Desc.Pilot Mt. Brownfields
9-Octadecenamide, (Z)-000301-02-0 12.37 J 93.000.108
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-12
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_27
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-14
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-13
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_13
1.00
mg/kg 1
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-15
Project Desc.Pilot Mt. Brownfields
Hexadecanoic acid000057-10-3 10.70 J 98.000.055
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-14
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_26
1.00
mg/kg 3
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-16
Project Desc.Pilot Mt. Brownfields
Perylene000198-55-0 14.74 J 98.000.145
Cyclopenta(def)phenanthrenone005737-13-3 11.41 J 95.000.034
Benzo[j]fluoranthene000205-82-3 14.48 J 93.000.035
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-15
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_14
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
DUPE
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-16
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_23
1.00
mg/kg 4
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-2
Project Desc.Pilot Mt. Brownfields
Hexadecanoic acid000057-10-3 10.71 J 99.000.175
9-Octadecenamide, (Z)-000301-02-0 12.38 J 94.000.232
.alpha.-Pinene000080-56-8 4.81 J 91.000.035
Eicosane000112-95-8 10.00 J 91.000.061
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-17
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_15
1.00
mg/kg 3
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-4
Project Desc.Pilot Mt. Brownfields
Hexadecanoic acid000057-10-3 10.71 J 99.000.092
Pentacosane000629-99-2 15.33 J 91.000.063
Hexatriacontane000630-06-8 16.70 J 90.000.064
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-18
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_17
1.00
mg/kg 2
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-5
Project Desc.Pilot Mt. Brownfields
Hexadecanoic acid000057-10-3 10.71 J 99.000.192
Octadecanoic acid000057-11-4 11.55 J 99.000.240
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-19
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_21
1.00
mg/kg 1
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-6
Project Desc.Pilot Mt. Brownfields
Hexadecanoic acid000057-10-3 10.70 J 97.000.024
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-20
Withers & Ravenel Eng. - Standard
1/25/2017
2/2/2017
SOIL
0202_25
1.00
0
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
TW-7
Project Desc.Pilot Mt. Brownfields
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-08
Withers & Ravenel Eng. - Standard
1/25/2017
2/3/2017
SOIL
0203A_14
20.00
mg/kg 13
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-10
Project Desc.Pilot Mt. Brownfields
9,10-Anthracenedione000084-65-1 11.07 J 99.002.04
11H-Benzo[a]fluorene000238-84-6 12.11 J 98.000.813
Benzo[k]fluoranthene000207-08-9 14.74 J 98.007.29
Dibenzothiophene000132-65-0 10.07 J 96.001.33
Phenanthrene, 1-methyl-000832-69-9 10.72 J 96.001.66
Anthracene, 9-methyl-000779-02-2 10.75 J 96.002.28
Phenanthrene, 2,5-dimethyl-003674-66-6 11.32 J 96.000.890
Cyclopenta(def)phenanthrenone005737-13-3 11.42 J 95.000.920
Benzo[k]fluoranthene000207-08-9 14.48 J 94.003.41
2-Phenylnaphthalene035465-71-5 11.04 J 93.001.51
Page 1 of 2SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-08
Withers & Ravenel Eng. - Standard
1/25/2017
2/3/2017
SOIL
0203A_14
20.00
mg/kg 13
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-10
Project Desc.Pilot Mt. Brownfields
4H-Cyclopenta[def]phenanthrene000203-64-5 10.85 J 92.004.67
Cyclohexasiloxane, dodecamethyl-000540-97-6 7.21 J 91.006.72
Benz[a]anthracene, 11-methyl-006111-78-0 13.49 J 90.001.08
Page 2 of 2SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L886597-12
Withers & Ravenel Eng. - Standard
1/25/2017
2/3/2017
SOIL
0203A_15
10.00
mg/kg 2
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-14
Project Desc.Pilot Mt. Brownfields
Benzo[k]fluoranthene000207-08-9 14.73 J 97.000.405
Cyclohexasiloxane, dodecamethyl-000540-97-6 7.21 J 91.000.470
Page 1 of 1SVOC TIC Report
ANALYTICAL REPORT
March 15, 2017
Withers & Ravenel Eng. - Standard
Sample Delivery Group:L893336
Samples Received:03/02/2017
Project Number:02090017.2
Description:Pilot Mt. Brownfields
Report To:Mark Brown
115 MacKenan Drive
Cary, NC 27511
Entire Report Reviewed By:
March 15, 2017
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
March 15, 2017
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 4
⁵Sr: Sample Results 5
B-17 L893336-01 5
⁶Qc: Quality Control Summary 8
Total Solids by Method 2540 G-2011 8
Mercury by Method 7471A 9
Metals (ICPMS) by Method 6020 10
Volatile Organic Compounds (GC/MS) by Method 8260B 13
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 19
⁷Gl: Glossary of Terms 24
⁸Al: Accreditations & Locations 25
⁹Sc: Chain of Custody 26
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
B-17 L893336-01 Solid J. Cates 02/28/17 11:00 03/02/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG958171 1 03/08/17 14:55 03/08/17 15:05 KDW
Mercury by Method 7471A WG957460 1 03/03/17 06:14 03/06/17 11:46 NJB
Metals (ICPMS) by Method 6020 WG958145 5 03/06/17 12:33 03/08/17 01:38 LAT
Metals (ICPMS) by Method 6020 WG958145 5 03/06/17 12:33 03/09/17 20:06 VSS
Metals (ICPMS) by Method 6020 WG960719 5 03/14/17 10:07 03/14/17 17:12 JPD
Volatile Organic Compounds (GC/MS) by Method 8260B WG958930 1 02/28/17 11:00 03/08/17 11:28 JAH
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG957618 1 03/03/17 12:13 03/06/17 11:48 KMP
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.2 L893336 03/15/17 14:32 4 of 27
Jimmy Hunt
Technical Service Representative
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.2 L893336 03/15/17 14:38 4 of 27
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L893336
B-17
Collected date/time: 02/28/17 11:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.1 1 03/08/2017 15:05 WG958171
Mercury by Method 7471A
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury U 0.00378 0.0270 1 03/06/2017 11:46 WG957460
Metals (ICPMS) by Method 6020
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Antimony U 0.213 0.675 5 03/08/2017 01:38 WG958145
Arsenic 0.522 J 0.0169 0.675 5 03/08/2017 01:38 WG958145
Beryllium 0.221 J 0.0810 0.675 5 03/09/2017 20:06 WG958145
Cadmium U 0.108 0.675 5 03/08/2017 01:38 WG958145
Chromium 6.34 0.364 0.675 5 03/08/2017 01:38 WG958145
Copper 57.4 0.351 0.675 5 03/08/2017 01:38 WG958145
Lead 29.6 0.162 0.675 5 03/08/2017 01:38 WG958145
Manganese 189 0.169 1.35 5 03/08/2017 01:38 WG958145
Nickel 2.73 0.236 0.675 5 03/08/2017 01:38 WG958145
Selenium 0.525 J 0.256 0.675 5 03/08/2017 01:38 WG958145
Silver U 0.209 0.675 5 03/08/2017 01:38 WG958145
Thallium U 0.128 0.675 5 03/08/2017 01:38 WG958145
Zinc 19.7 1.73 6.75 5 03/14/2017 17:12 WG960719
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0697 0.0135 0.0675 1 03/08/2017 11:28 WG958930
Acrylonitrile U 0.00242 0.0135 1 03/08/2017 11:28 WG958930
Benzene U 0.000364 0.00135 1 03/08/2017 11:28 WG958930
Bromobenzene U 0.000383 0.00135 1 03/08/2017 11:28 WG958930
Bromodichloromethane U 0.000343 0.00135 1 03/08/2017 11:28 WG958930
Bromoform U 0.000572 0.00135 1 03/08/2017 11:28 WG958930
Bromomethane U 0.00181 0.00675 1 03/08/2017 11:28 WG958930
n-Butylbenzene U 0.000348 0.00135 1 03/08/2017 11:28 WG958930
sec-Butylbenzene U 0.000271 0.00135 1 03/08/2017 11:28 WG958930
tert-Butylbenzene U 0.000278 0.00135 1 03/08/2017 11:28 WG958930
Carbon tetrachloride U 0.000443 0.00135 1 03/08/2017 11:28 WG958930
Chlorobenzene U 0.000286 0.00135 1 03/08/2017 11:28 WG958930
Chlorodibromomethane U 0.000503 0.00135 1 03/08/2017 11:28 WG958930
Chloroethane U 0.00128 0.00675 1 03/08/2017 11:28 WG958930
2-Chloroethyl vinyl ether U 0.00316 0.0675 1 03/08/2017 11:28 WG958930
Chloroform U 0.000309 0.00675 1 03/08/2017 11:28 WG958930
Chloromethane U 0.000506 0.00337 1 03/08/2017 11:28 WG958930
2-Chlorotoluene U 0.000406 0.00135 1 03/08/2017 11:28 WG958930
4-Chlorotoluene U 0.000324 0.00135 1 03/08/2017 11:28 WG958930
1,2-Dibromo-3-Chloropropane U 0.00142 0.00675 1 03/08/2017 11:28 WG958930
1,2-Dibromoethane U 0.000463 0.00135 1 03/08/2017 11:28 WG958930
Dibromomethane U 0.000515 0.00135 1 03/08/2017 11:28 WG958930
1,2-Dichlorobenzene U 0.000412 0.00135 1 03/08/2017 11:28 WG958930
1,3-Dichlorobenzene U 0.000322 0.00135 1 03/08/2017 11:28 WG958930
1,4-Dichlorobenzene U 0.000305 0.00135 1 03/08/2017 11:28 WG958930
Dichlorodifluoromethane U 0.000962 0.00675 1 03/08/2017 11:28 WG958930
1,1-Dichloroethane U 0.000269 0.00135 1 03/08/2017 11:28 WG958930
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L893336
B-17
Collected date/time: 02/28/17 11:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,2-Dichloroethane U 0.000358 0.00135 1 03/08/2017 11:28 WG958930
1,1-Dichloroethene U 0.000409 0.00135 1 03/08/2017 11:28 WG958930
cis-1,2-Dichloroethene U 0.000317 0.00135 1 03/08/2017 11:28 WG958930
trans-1,2-Dichloroethene U 0.000356 0.00135 1 03/08/2017 11:28 WG958930
1,2-Dichloropropane U 0.000483 0.00135 1 03/08/2017 11:28 WG958930
1,1-Dichloropropene U 0.000428 0.00135 1 03/08/2017 11:28 WG958930
1,3-Dichloropropane U 0.000279 0.00135 1 03/08/2017 11:28 WG958930
cis-1,3-Dichloropropene U 0.000354 0.00135 1 03/08/2017 11:28 WG958930
trans-1,3-Dichloropropene U 0.000360 0.00135 1 03/08/2017 11:28 WG958930
2,2-Dichloropropane U 0.000376 0.00135 1 03/08/2017 11:28 WG958930
Di-isopropyl ether U 0.000335 0.00135 1 03/08/2017 11:28 WG958930
Ethylbenzene U 0.000401 0.00135 1 03/08/2017 11:28 WG958930
Hexachloro-1,3-butadiene U J4 0.000461 0.00135 1 03/08/2017 11:28 WG958930
Isopropylbenzene U 0.000328 0.00135 1 03/08/2017 11:28 WG958930
p-Isopropyltoluene U 0.000275 0.00135 1 03/08/2017 11:28 WG958930
2-Butanone (MEK)0.0488 0.00631 0.0135 1 03/08/2017 11:28 WG958930
Methylene Chloride U 0.00135 0.00675 1 03/08/2017 11:28 WG958930
4-Methyl-2-pentanone (MIBK) U 0.00254 0.0135 1 03/08/2017 11:28 WG958930
Methyl tert-butyl ether U 0.000286 0.00135 1 03/08/2017 11:28 WG958930
Naphthalene U 0.00135 0.00675 1 03/08/2017 11:28 WG958930
n-Propylbenzene U 0.000278 0.00135 1 03/08/2017 11:28 WG958930
Styrene U 0.000316 0.00135 1 03/08/2017 11:28 WG958930
1,1,1,2-Tetrachloroethane U 0.000356 0.00135 1 03/08/2017 11:28 WG958930
1,1,2,2-Tetrachloroethane U 0.000492 0.00135 1 03/08/2017 11:28 WG958930
Tetrachloroethene U 0.000372 0.00135 1 03/08/2017 11:28 WG958930
Toluene U 0.000586 0.00675 1 03/08/2017 11:28 WG958930
1,2,3-Trichlorobenzene U J4 0.000413 0.00135 1 03/08/2017 11:28 WG958930
1,2,4-Trichlorobenzene U J4 0.000524 0.00135 1 03/08/2017 11:28 WG958930
1,1,1-Trichloroethane U 0.000386 0.00135 1 03/08/2017 11:28 WG958930
1,1,2-Trichloroethane U 0.000374 0.00135 1 03/08/2017 11:28 WG958930
Trichloroethene U 0.000376 0.00135 1 03/08/2017 11:28 WG958930
Trichlorofluoromethane U 0.000515 0.00675 1 03/08/2017 11:28 WG958930
1,2,3-Trichloropropane U 0.00100 0.00337 1 03/08/2017 11:28 WG958930
1,2,4-Trimethylbenzene U 0.000285 0.00135 1 03/08/2017 11:28 WG958930
1,3,5-Trimethylbenzene U 0.000359 0.00135 1 03/08/2017 11:28 WG958930
Vinyl chloride U 0.000393 0.00135 1 03/08/2017 11:28 WG958930
Xylenes, Total U 0.000942 0.00405 1 03/08/2017 11:28 WG958930
(S) Toluene-d8 103 80.0-120 03/08/2017 11:28 WG958930
(S) Dibromofluoromethane 105 74.0-131 03/08/2017 11:28 WG958930
(S) a,a,a-Trifluorotoluene 98.3 80.0-120 03/08/2017 11:28 WG958930
(S) 4-Bromofluorobenzene 92.1 64.0-132 03/08/2017 11:28 WG958930
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00866 0.0445 1 03/06/2017 11:48 WG957618
Acenaphthylene U 0.00905 0.0445 1 03/06/2017 11:48 WG957618
Anthracene U 0.00853 0.0445 1 03/06/2017 11:48 WG957618
Benzidine U 0.0859 0.449 1 03/06/2017 11:48 WG957618
Benzo(a)anthracene U 0.00577 0.0445 1 03/06/2017 11:48 WG957618
Benzo(b)fluoranthene U 0.00938 0.0445 1 03/06/2017 11:48 WG957618
Benzo(k)fluoranthene U 0.00785 0.0445 1 03/06/2017 11:48 WG957618
Benzo(g,h,i)perylene U 0.00973 0.0445 1 03/06/2017 11:48 WG957618
Benzo(a)pyrene U 0.00739 0.0445 1 03/06/2017 11:48 WG957618
Bis(2-chlorethoxy)methane U 0.0104 0.449 1 03/06/2017 11:48 WG957618
Bis(2-chloroethyl)ether U 0.0121 0.449 1 03/06/2017 11:48 WG957618
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L893336
B-17
Collected date/time: 02/28/17 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.0103 0.449 1 03/06/2017 11:48 WG957618
4-Bromophenyl-phenylether U 0.0154 0.449 1 03/06/2017 11:48 WG957618
2-Chloronaphthalene U 0.00862 0.0445 1 03/06/2017 11:48 WG957618
4-Chlorophenyl-phenylether U 0.00846 0.449 1 03/06/2017 11:48 WG957618
Chrysene U 0.00749 0.0445 1 03/06/2017 11:48 WG957618
Dibenz(a,h)anthracene U 0.0111 0.0445 1 03/06/2017 11:48 WG957618
3,3-Dichlorobenzidine U J4 0.107 0.449 1 03/06/2017 11:48 WG957618
2,4-Dinitrotoluene U 0.00819 0.449 1 03/06/2017 11:48 WG957618
2,6-Dinitrotoluene U 0.00994 0.449 1 03/06/2017 11:48 WG957618
Fluoranthene U 0.00669 0.0445 1 03/06/2017 11:48 WG957618
Fluorene U 0.00920 0.0445 1 03/06/2017 11:48 WG957618
Hexachlorobenzene U 0.0115 0.449 1 03/06/2017 11:48 WG957618
Hexachloro-1,3-butadiene U 0.0135 0.449 1 03/06/2017 11:48 WG957618
Hexachlorocyclopentadiene U 0.0792 0.449 1 03/06/2017 11:48 WG957618
Hexachloroethane U 0.0181 0.449 1 03/06/2017 11:48 WG957618
Indeno(1,2,3-cd)pyrene U 0.0104 0.0445 1 03/06/2017 11:48 WG957618
Isophorone U 0.00704 0.449 1 03/06/2017 11:48 WG957618
Naphthalene U 0.0120 0.0445 1 03/06/2017 11:48 WG957618
Nitrobenzene U 0.00938 0.449 1 03/06/2017 11:48 WG957618
n-Nitrosodimethylamine U 0.0873 0.449 1 03/06/2017 11:48 WG957618
n-Nitrosodiphenylamine U 0.00801 0.449 1 03/06/2017 11:48 WG957618
n-Nitrosodi-n-propylamine U 0.0122 0.449 1 03/06/2017 11:48 WG957618
Phenanthrene U 0.00712 0.0445 1 03/06/2017 11:48 WG957618
Benzylbutyl phthalate U 0.0139 0.449 1 03/06/2017 11:48 WG957618
Bis(2-ethylhexyl)phthalate U 0.0162 0.449 1 03/06/2017 11:48 WG957618
Di-n-butyl phthalate U 0.0147 0.449 1 03/06/2017 11:48 WG957618
Diethyl phthalate U 0.00932 0.449 1 03/06/2017 11:48 WG957618
Dimethyl phthalate U 0.00729 0.449 1 03/06/2017 11:48 WG957618
Di-n-octyl phthalate U 0.0122 0.449 1 03/06/2017 11:48 WG957618
Pyrene U 0.0166 0.0445 1 03/06/2017 11:48 WG957618
1,2,4-Trichlorobenzene U 0.0118 0.449 1 03/06/2017 11:48 WG957618
Aniline U 0.0432 0.449 1 03/06/2017 11:48 WG957618
4-Chloro-3-methylphenol U 0.00644 0.449 1 03/06/2017 11:48 WG957618
2-Chlorophenol U 0.0112 0.449 1 03/06/2017 11:48 WG957618
2,4-Dichlorophenol U 0.0101 0.449 1 03/06/2017 11:48 WG957618
2,4-Dimethylphenol U 0.0635 0.449 1 03/06/2017 11:48 WG957618
4,6-Dinitro-2-methylphenol U 0.167 0.449 1 03/06/2017 11:48 WG957618
2,4-Dinitrophenol U 0.132 0.449 1 03/06/2017 11:48 WG957618
2-Nitrophenol U 0.0175 0.449 1 03/06/2017 11:48 WG957618
4-Nitrophenol U 0.0708 0.449 1 03/06/2017 11:48 WG957618
Pentachlorophenol U 0.0648 0.449 1 03/06/2017 11:48 WG957618
Phenol U 0.00938 0.449 1 03/06/2017 11:48 WG957618
2,4,6-Trichlorophenol U 0.0105 0.449 1 03/06/2017 11:48 WG957618
(S) 2-Fluorophenol 40.0 20.0-120 03/06/2017 11:48 WG957618
(S) Phenol-d5 59.7 20.0-120 03/06/2017 11:48 WG957618
(S) Nitrobenzene-d5 66.1 18.0-125 03/06/2017 11:48 WG957618
(S) 2-Fluorobiphenyl 69.4 28.0-120 03/06/2017 11:48 WG957618
(S) 2,4,6-Tribromophenol 61.3 17.0-137 03/06/2017 11:48 WG957618
(S) p-Terphenyl-d14 85.9 13.0-131 03/06/2017 11:48 WG957618
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958171
Total Solids by Method 2540 G-2011 L893336-01
Method Blank (MB)
(MB) R3201978-1 03/08/17 15:05
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00150
L893342-03 Original Sample (OS) • Duplicate (DUP)
(OS) L893342-03 03/08/17 15:05 • (DUP) R3201978-3 03/08/17 15:05
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 83.8 83.9 1 0.136 5
Laboratory Control Sample (LCS)
(LCS) R3201978-2 03/08/17 15:05
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 99.9 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG957460
Mercury by Method 7471A L893336-01
Method Blank (MB)
(MB) R3201256-1 03/06/17 11:21
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0028 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3201256-2 03/06/17 11:23 • (LCSD) R3201256-3 03/06/17 11:26
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.273 0.274 91 91 80-120 0 20
L893308-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L893308-04 03/06/17 11:28 • (MS) R3201256-4 03/06/17 11:31 • (MSD) R3201256-5 03/06/17 11:33
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.323 0.00670 0.301 0.288 91 87 1 75-125 5 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958145
Metals (ICPMS) by Method 6020 L893336-01
Method Blank (MB)
(MB) R3202030-1 03/07/17 21:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Antimony U 0.158 0.500
Arsenic U 0.0125 0.500
Beryllium U 0.06 0.500
Cadmium U 0.08 0.500
Chromium U 0.27 0.500
Copper U 0.26 0.500
Lead U 0.12 0.500
Manganese 0.306 J 0.125 1.00
Nickel U 0.175 0.500
Selenium U 0.19 0.500
Silver U 0.155 0.500
Thallium U 0.095 0.500
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3202030-2 03/07/17 21:38 • (LCSD) R3202030-3 03/07/17 21:42
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Antimony 100 105 106 105 106 80-120 0 20
Arsenic 100 103 104 103 104 80-120 1 20
Beryllium 100 89.0 88.4 89 88 80-120 1 20
Cadmium 100 111 112 111 112 80-120 1 20
Chromium 100 104 106 104 106 80-120 1 20
Copper 100 107 108 107 108 80-120 1 20
Lead 100 106 107 106 107 80-120 0 20
Manganese 100 103 103 103 103 80-120 0 20
Nickel 100 107 108 107 108 80-120 1 20
Selenium 100 102 102 102 102 80-120 0 20
Silver 20.0 20.9 21.3 105 107 80-120 2 20
Thallium 100 104 107 104 107 80-120 3 20
L893281-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L893281-07 03/07/17 21:45 • (MS) R3202030-6 03/07/17 21:56 • (MSD) R3202030-7 03/07/17 21:59
Spike Amount (dry)Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Antimony 24.6 0.224 71.1 67.2 58 54 5 75-125 J6 J6 6 20
Arsenic 24.6 3.30 125 122 98 96 5 75-125 2 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958145
Metals (ICPMS) by Method 6020 L893336-01
L893281-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L893281-07 03/07/17 21:45 • (MS) R3202030-6 03/07/17 21:56 • (MSD) R3202030-7 03/07/17 21:59
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Beryllium 24.6 0.641 98.8 93.3 80 75 5 75-125 6 20
Cadmium 24.6 0.175 135 130 110 105 5 75-125 4 20
Chromium 24.6 16.1 141 140 102 101 5 75-125 1 20
Copper 24.6 7.82 133 131 102 100 5 75-125 2 20
Lead 24.6 24.0 141 138 95 93 5 75-125 2 20
Manganese 24.6 341 336 382 0 33 5 75-125 J6 J6 13 20
Nickel 24.6 10.1 134 135 100 101 5 75-125 1 20
Selenium 24.6 1.03 129 125 104 100 5 75-125 3 20
Silver 4.93 U 25.4 24.5 103 100 5 75-125 3 20
Thallium 24.6 0.265 127 121 103 98 5 75-125 5 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG960719
Metals (ICPMS) by Method 6020 L893336-01
Method Blank (MB)
(MB) R3203285-1 03/14/17 16:56
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Zinc U 1.28 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3203285-2 03/14/17 17:00 • (LCSD) R3203285-3 03/14/17 17:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Zinc 100 102 84.7 102 85 80-120 18 20
L893336-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L893336-01 03/14/17 17:12 • (MS) R3203285-6 03/14/17 17:23 • (MSD) R3203285-7 03/14/17 17:26
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Zinc 27.0 19.7 182 187 120 124 5 75-125 3 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958930
Volatile Organic Compounds (GC/MS) by Method 8260B L893336-01
Method Blank (MB)
(MB) R3202143-3 03/08/17 10:03
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958930
Volatile Organic Compounds (GC/MS) by Method 8260B L893336-01
Method Blank (MB)
(MB) R3202143-3 03/08/17 10:03
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK) U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene U 0.000434 0.00500
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 106 80.0-120
(S) Dibromofluoromethane 105 74.0-131
(S) a,a,a-Trifluorotoluene 103 80.0-120
(S) 4-Bromofluorobenzene 96.9 64.0-132
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3202143-1 03/08/17 09:02 • (LCSD) R3202143-2 03/08/17 09:23
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.112 0.119 89.8 95.3 11.0-160 5.96 23
Acrylonitrile 0.125 0.113 0.124 90.7 99.3 61.0-143 9.03 20
Benzene 0.0250 0.0221 0.0223 88.4 89.1 71.0-124 0.770 20
Bromobenzene 0.0250 0.0211 0.0203 84.6 81.3 78.0-120 3.97 20
Bromodichloromethane 0.0250 0.0222 0.0223 88.9 89.2 75.0-120 0.380 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958930
Volatile Organic Compounds (GC/MS) by Method 8260B L893336-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3202143-1 03/08/17 09:02 • (LCSD) R3202143-2 03/08/17 09:23
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.0250 0.0223 0.0221 89.0 88.3 65.0-133 0.780 20
Bromomethane 0.0250 0.0226 0.0223 90.2 89.4 26.0-160 0.930 20
n-Butylbenzene 0.0250 0.0216 0.0210 86.3 83.9 73.0-126 2.83 20
sec-Butylbenzene 0.0250 0.0195 0.0190 78.0 75.8 75.0-121 2.89 20
tert-Butylbenzene 0.0250 0.0202 0.0193 80.8 77.3 74.0-122 4.43 20
Carbon tetrachloride 0.0250 0.0230 0.0226 91.9 90.3 66.0-123 1.78 20
Chlorobenzene 0.0250 0.0212 0.0212 84.9 84.8 79.0-121 0.0600 20
Chlorodibromomethane 0.0250 0.0227 0.0225 90.7 90.2 74.0-128 0.600 20
Chloroethane 0.0250 0.0218 0.0216 87.0 86.3 51.0-147 0.830 20
2-Chloroethyl vinyl ether 0.125 0.160 0.166 128 133 10.0-160 3.62 22
Chloroform 0.0250 0.0225 0.0225 90.1 89.9 73.0-123 0.190 20
Chloromethane 0.0250 0.0198 0.0198 79.2 79.1 51.0-138 0.180 20
2-Chlorotoluene 0.0250 0.0215 0.0212 86.2 84.8 72.0-124 1.60 20
4-Chlorotoluene 0.0250 0.0214 0.0210 85.8 84.1 78.0-120 1.98 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0214 0.0218 85.7 87.4 65.0-126 1.91 20
1,2-Dibromoethane 0.0250 0.0222 0.0222 88.7 88.6 78.0-122 0.120 20
Dibromomethane 0.0250 0.0225 0.0226 90.0 90.5 79.0-120 0.490 20
1,2-Dichlorobenzene 0.0250 0.0219 0.0217 87.8 86.8 80.0-120 1.15 20
1,3-Dichlorobenzene 0.0250 0.0198 0.0190 79.3 76.1 72.0-123 4.14 20
1,4-Dichlorobenzene 0.0250 0.0213 0.0213 85.2 85.3 77.0-120 0.150 20
Dichlorodifluoromethane 0.0250 0.0201 0.0201 80.5 80.5 49.0-155 0.0300 20
1,1-Dichloroethane 0.0250 0.0223 0.0225 89.3 90.2 70.0-128 1.02 20
1,2-Dichloroethane 0.0250 0.0237 0.0237 94.9 94.8 69.0-128 0.0600 20
1,1-Dichloroethene 0.0250 0.0215 0.0217 86.1 86.9 63.0-131 0.950 20
cis-1,2-Dichloroethene 0.0250 0.0227 0.0227 90.9 90.7 74.0-123 0.230 20
trans-1,2-Dichloroethene 0.0250 0.0217 0.0212 86.7 84.7 72.0-122 2.34 20
1,2-Dichloropropane 0.0250 0.0223 0.0222 89.2 88.8 75.0-126 0.380 20
1,1-Dichloropropene 0.0250 0.0232 0.0233 92.8 93.2 72.0-130 0.450 20
1,3-Dichloropropane 0.0250 0.0224 0.0226 89.7 90.2 80.0-121 0.580 20
cis-1,3-Dichloropropene 0.0250 0.0249 0.0250 99.5 100 80.0-125 0.640 20
trans-1,3-Dichloropropene 0.0250 0.0251 0.0253 100 101 75.0-129 0.600 20
2,2-Dichloropropane 0.0250 0.0213 0.0220 85.4 87.8 60.0-129 2.81 20
Di-isopropyl ether 0.0250 0.0211 0.0212 84.5 85.0 62.0-133 0.610 20
Ethylbenzene 0.0250 0.0205 0.0205 82.2 81.9 77.0-120 0.340 20
Hexachloro-1,3-butadiene 0.0250 0.0166 0.0159 66.2 63.5 68.0-128 J4 J4 4.27 20
Isopropylbenzene 0.0250 0.0204 0.0202 81.8 80.8 75.0-120 1.20 20
p-Isopropyltoluene 0.0250 0.0196 0.0188 78.4 75.3 74.0-125 3.94 20
2-Butanone (MEK)0.125 0.127 0.146 102 116 37.0-159 13.5 20
Methylene Chloride 0.0250 0.0211 0.0212 84.3 84.9 67.0-123 0.780 20
4-Methyl-2-pentanone (MIBK) 0.125 0.140 0.147 112 117 60.0-144 4.78 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958930
Volatile Organic Compounds (GC/MS) by Method 8260B L893336-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3202143-1 03/08/17 09:02 • (LCSD) R3202143-2 03/08/17 09:23
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Methyl tert-butyl ether 0.0250 0.0217 0.0220 86.9 88.0 66.0-125 1.16 20
Naphthalene 0.0250 0.0172 0.0171 68.7 68.4 64.0-125 0.430 20
n-Propylbenzene 0.0250 0.0210 0.0205 83.8 82.1 78.0-120 2.07 20
Styrene 0.0250 0.0225 0.0222 89.8 89.0 78.0-124 0.950 20
1,1,1,2-Tetrachloroethane 0.0250 0.0217 0.0214 86.8 85.6 74.0-124 1.33 20
1,1,2,2-Tetrachloroethane 0.0250 0.0198 0.0196 79.2 78.5 73.0-120 0.880 20
Tetrachloroethene 0.0250 0.0212 0.0212 84.9 84.7 70.0-127 0.200 20
Toluene 0.0250 0.0225 0.0225 89.9 90.2 77.0-120 0.310 20
1,2,3-Trichlorobenzene 0.0250 0.0165 0.0158 66.0 63.3 68.0-126 J4 J4 4.18 20
1,2,4-Trichlorobenzene 0.0250 0.0172 0.0164 68.9 65.5 70.0-127 J4 J4 5.15 20
1,1,1-Trichloroethane 0.0250 0.0219 0.0219 87.5 87.6 69.0-125 0.130 20
1,1,2-Trichloroethane 0.0250 0.0201 0.0206 80.2 82.3 78.0-120 2.56 20
Trichloroethene 0.0250 0.0219 0.0220 87.7 87.8 79.0-120 0.160 20
Trichlorofluoromethane 0.0250 0.0241 0.0245 96.3 97.9 59.0-136 1.63 20
1,2,3-Trichloropropane 0.0250 0.0216 0.0210 86.4 84.0 73.0-124 2.78 20
1,2,4-Trimethylbenzene 0.0250 0.0203 0.0193 81.1 77.3 75.0-120 4.76 20
1,3,5-Trimethylbenzene 0.0250 0.0201 0.0194 80.3 77.7 75.0-120 3.25 20
Vinyl chloride 0.0250 0.0222 0.0220 89.0 88.1 63.0-134 0.960 20
Xylenes, Total 0.0750 0.0618 0.0610 82.4 81.3 77.0-120 1.30 20
(S) Toluene-d8 103 103 80.0-120
(S) Dibromofluoromethane 104 105 74.0-131
(S) a,a,a-Trifluorotoluene 98.0 99.2 80.0-120
(S) 4-Bromofluorobenzene 97.0 94.9 64.0-132
L894042-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L894042-07 03/08/17 13:12 • (MS) R3202143-5 03/08/17 13:53 • (MSD) R3202143-4 03/08/17 13:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.186 ND 0.133 0.0947 33.6 12.8 1 10.0-160 33.9 36
Acrylonitrile 0.186 ND 0.148 0.105 79.9 56.8 1 14.0-160 J3 33.9 33
Benzene 0.0371 0.00247 0.0213 0.0232 50.7 55.8 1 13.0-146 8.48 27
Bromobenzene 0.0371 ND 0.0174 0.0207 46.9 55.7 1 10.0-149 17.2 33
Bromodichloromethane 0.0371 ND 0.0221 0.0238 59.5 64.2 1 15.0-142 7.54 28
Bromoform 0.0371 ND 0.0219 0.0214 58.9 57.5 1 10.0-147 2.46 31
Bromomethane 0.0371 ND 0.0196 0.0197 52.7 53.0 1 10.0-160 0.510 32
n-Butylbenzene 0.0371 ND 0.0156 0.0241 39.3 62.1 1 10.0-154 J3 42.7 37
sec-Butylbenzene 0.0371 ND 0.0147 0.0225 38.6 59.6 1 10.0-151 J3 42.0 36
tert-Butylbenzene 0.0371 ND 0.0158 0.0229 42.5 61.6 1 10.0-152 J3 36.8 35
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958930
Volatile Organic Compounds (GC/MS) by Method 8260B L893336-01
L894042-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L894042-07 03/08/17 13:12 • (MS) R3202143-5 03/08/17 13:53 • (MSD) R3202143-4 03/08/17 13:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.0371 ND 0.0201 0.0239 54.1 64.3 1 13.0-140 17.2 30
Chlorobenzene 0.0371 ND 0.0175 0.0210 47.2 56.6 1 10.0-149 18.0 31
Chlorodibromomethane 0.0371 ND 0.0217 0.0226 58.3 60.8 1 12.0-147 4.16 29
Chloroethane 0.0371 ND 0.0194 0.0204 52.3 55.0 1 10.0-159 5.06 33
2-Chloroethyl vinyl ether 0.186 ND ND ND 0.000 0.000 1 10.0-160 J6 J6 0.000 32
Chloroform 0.0371 ND 0.0221 0.0240 59.4 64.7 1 18.0-148 8.45 28
Chloromethane 0.0371 ND 0.0155 0.0158 41.6 42.6 1 10.0-146 2.30 29
2-Chlorotoluene 0.0371 ND 0.0170 0.0228 45.7 61.4 1 10.0-151 29.3 35
4-Chlorotoluene 0.0371 ND 0.0163 0.0213 44.0 57.4 1 10.0-150 26.5 35
1,2-Dibromo-3-Chloropropane 0.0371 ND 0.0294 0.0226 79.2 60.9 1 10.0-149 26.1 34
1,2-Dibromoethane 0.0371 ND 0.0218 0.0215 58.6 58.0 1 14.0-145 1.13 28
Dibromomethane 0.0371 ND 0.0227 0.0223 61.1 59.9 1 18.0-144 1.86 27
1,2-Dichlorobenzene 0.0371 ND 0.0182 0.0223 49.0 59.9 1 10.0-153 20.1 34
1,3-Dichlorobenzene 0.0371 ND 0.0154 0.0195 41.3 52.6 1 10.0-150 24.0 35
1,4-Dichlorobenzene 0.0371 ND 0.0162 0.0203 43.5 54.7 1 10.0-148 22.8 34
Dichlorodifluoromethane 0.0371 ND 0.0190 0.0213 51.3 57.4 1 10.0-160 11.3 30
1,1-Dichloroethane 0.0371 ND 0.0217 0.0235 58.4 63.2 1 19.0-148 7.78 28
1,2-Dichloroethane 0.0371 ND 0.0247 0.0240 66.5 64.5 1 17.0-147 3.09 27
1,1-Dichloroethene 0.0371 ND 0.0178 0.0206 47.9 55.5 1 10.0-150 14.8 31
cis-1,2-Dichloroethene 0.0371 ND 0.0212 0.0227 57.1 61.0 1 16.0-145 6.54 28
trans-1,2-Dichloroethene 0.0371 ND 0.0175 0.0195 47.1 52.6 1 11.0-142 11.0 29
1,2-Dichloropropane 0.0371 ND 0.0215 0.0244 58.0 65.8 1 17.0-148 12.6 28
1,1-Dichloropropene 0.0371 ND 0.0190 0.0232 51.1 62.5 1 10.0-150 20.0 30
1,3-Dichloropropane 0.0371 ND 0.0225 0.0233 60.6 62.7 1 16.0-148 3.37 27
cis-1,3-Dichloropropene 0.0371 ND 0.0232 0.0256 62.5 68.9 1 13.0-150 9.71 28
trans-1,3-Dichloropropene 0.0371 ND 0.0246 0.0258 66.3 69.5 1 10.0-152 4.63 29
2,2-Dichloropropane 0.0371 ND 0.0212 0.0239 57.0 64.4 1 16.0-143 12.2 30
Di-isopropyl ether 0.0371 ND 0.0218 0.0236 58.8 63.6 1 16.0-149 7.75 28
Ethylbenzene 0.0371 0.00203 0.0172 0.0212 40.9 51.7 1 10.0-147 20.8 31
Hexachloro-1,3-butadiene 0.0371 ND 0.0138 0.0250 37.3 67.2 1 10.0-154 J3 57.3 40
Isopropylbenzene 0.0371 ND 0.0160 0.0219 43.1 58.8 1 10.0-147 31.0 33
p-Isopropyltoluene 0.0371 ND 0.0150 0.0224 40.4 60.4 1 10.0-156 J3 39.7 37
2-Butanone (MEK)0.186 0.152 0.197 0.156 24.1 2.37 1 10.0-160 J6 22.8 33
Methylene Chloride 0.0371 ND 0.0201 0.0202 54.0 54.3 1 16.0-139 0.470 29
4-Methyl-2-pentanone (MIBK) 0.186 ND 0.198 0.158 107 84.8 1 12.0-160 22.7 32
Methyl tert-butyl ether 0.0371 ND 0.0242 0.0232 65.2 62.4 1 21.0-145 4.35 29
Naphthalene 0.0371 ND 0.0304 0.0280 77.4 70.9 1 10.0-153 8.15 36
n-Propylbenzene 0.0371 0.00155 0.0157 0.0221 38.2 55.2 1 10.0-151 33.6 34
Styrene 0.0371 ND 0.0109 0.0190 29.4 51.2 1 10.0-155 J3 53.9 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG958930
Volatile Organic Compounds (GC/MS) by Method 8260B L893336-01
L894042-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L894042-07 03/08/17 13:12 • (MS) R3202143-5 03/08/17 13:53 • (MSD) R3202143-4 03/08/17 13:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,1,2-Tetrachloroethane 0.0371 ND 0.0196 0.0222 52.8 59.8 1 10.0-147 12.5 30
1,1,2,2-Tetrachloroethane 0.0371 ND 0.0227 0.0205 61.2 55.1 1 10.0-155 10.6 31
Tetrachloroethene 0.0371 ND 0.0151 0.0198 40.7 53.4 1 10.0-144 27.0 32
Toluene 0.0371 0.0120 0.0262 0.0258 38.2 37.2 1 10.0-144 1.46 28
1,2,3-Trichlorobenzene 0.0371 ND 0.0150 0.0193 40.3 51.8 1 10.0-153 25.2 40
1,2,4-Trichlorobenzene 0.0371 ND 0.0147 0.0194 39.5 52.2 1 10.0-156 27.7 40
1,1,1-Trichloroethane 0.0371 ND 0.0208 0.0238 56.0 64.0 1 18.0-145 13.4 29
1,1,2-Trichloroethane 0.0371 ND 0.0211 0.0215 56.9 57.8 1 12.0-151 1.52 28
Trichloroethene 0.0371 ND 0.0183 0.0221 49.2 59.5 1 11.0-148 18.9 29
Trichlorofluoromethane 0.0371 ND 0.0216 0.0241 58.2 64.9 1 10.0-157 10.8 34
1,2,3-Trichloropropane 0.0371 ND 0.0256 0.0224 69.0 60.3 1 10.0-154 13.4 32
1,2,4-Trimethylbenzene 0.0371 0.00760 0.0179 0.0229 27.6 41.3 1 10.0-151 24.8 34
1,3,5-Trimethylbenzene 0.0371 0.00262 0.0160 0.0221 36.1 52.5 1 10.0-150 31.9 33
Vinyl chloride 0.0371 ND 0.0183 0.0198 49.3 53.2 1 10.0-150 7.66 29
Xylenes, Total 0.111 0.0119 0.0544 0.0643 38.1 47.0 1 10.0-150 16.8 31
(S) Toluene-d8 101 102 80.0-120
(S) Dibromofluoromethane 110 104 74.0-131
(S) a,a,a-Trifluorotoluene 97.0 97.1 80.0-120
(S) 4-Bromofluorobenzene 93.4 92.0 64.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02090017.2 L893336 03/15/17 14:38 18 of 27
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG957618
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L893336-01
Method Blank (MB)
(MB) R3201111-3 03/06/17 09:04
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0330
Acenaphthylene U 0.00671 0.0330
Aniline U 0.0320 0.333
Anthracene U 0.00632 0.0330
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0330
Benzo(b)fluoranthene U 0.00695 0.0330
Benzo(k)fluoranthene U 0.00582 0.0330
Benzo(g,h,i)perylene U 0.00721 0.0330
Benzo(a)pyrene U 0.00548 0.0330
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0330
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0330
Dibenz(a,h)anthracene U 0.00821 0.0330
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0330
Fluorene U 0.00682 0.0330
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0330
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0330
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.00594 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0330
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02090017.2 L893336 03/15/17 14:38 19 of 27
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG957618
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L893336-01
Method Blank (MB)
(MB) R3201111-3 03/06/17 09:04
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Di-n-octyl phthalate U 0.00907 0.333
Pyrene U 0.0123 0.0330
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 81.9 18.0-125
(S) 2-Fluorobiphenyl 79.8 28.0-120
(S) p-Terphenyl-d14 90.5 13.0-131
(S) Phenol-d5 74.9 20.0-120
(S) 2-Fluorophenol 68.7 20.0-120
(S) 2,4,6-Tribromophenol 74.6 17.0-137
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3201111-1 03/06/17 08:18 • (LCSD) R3201111-2 03/06/17 08:41
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Aniline 0.667 0.578 0.533 86.7 79.8 27.0-120 8.25 28
Acenaphthene 0.667 0.659 0.653 98.9 97.9 47.0-120 1.01 21
Acenaphthylene 0.667 0.695 0.681 104 102 48.0-120 1.96 21
Anthracene 0.667 0.661 0.691 99.1 104 46.0-120 4.52 20
Benzidine 0.667 0.261 0.219 39.1 32.9 1.00-120 17.3 36
Benzo(a)anthracene 0.667 0.652 0.657 97.8 98.5 46.0-120 0.720 20
Benzo(b)fluoranthene 0.667 0.677 0.684 102 103 45.0-120 0.960 22
Benzo(k)fluoranthene 0.667 0.630 0.648 94.4 97.1 45.0-120 2.76 23
Benzo(g,h,i)perylene 0.667 0.682 0.682 102 102 48.0-120 0.0300 21
Benzo(a)pyrene 0.667 0.661 0.673 99.1 101 46.0-120 1.80 21
Bis(2-chlorethoxy)methane 0.667 0.494 0.495 74.0 74.2 41.0-120 0.290 22
Bis(2-chloroethyl)ether 0.667 0.609 0.574 91.3 86.1 28.0-120 5.85 28
Bis(2-chloroisopropyl)ether 0.667 0.624 0.600 93.5 89.9 40.0-120 3.91 27
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.2 L893336 03/15/17 14:38 20 of 27
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG957618
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L893336-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3201111-1 03/06/17 08:18 • (LCSD) R3201111-2 03/06/17 08:41
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
4-Bromophenyl-phenylether 0.667 0.648 0.668 97.1 100 45.0-120 3.08 20
2-Chloronaphthalene 0.667 0.639 0.630 95.8 94.5 43.0-120 1.47 22
4-Chlorophenyl-phenylether 0.667 0.704 0.705 106 106 46.0-120 0.140 21
Chrysene 0.667 0.664 0.674 99.6 101 46.0-120 1.37 20
Dibenz(a,h)anthracene 0.667 0.674 0.676 101 101 47.0-120 0.260 22
3,3-Dichlorobenzidine 0.667 0.961 0.922 144 138 20.0-130 J4 J4 4.21 24
2,4-Dinitrotoluene 0.667 0.759 0.767 114 115 48.0-122 0.990 21
2,6-Dinitrotoluene 0.667 0.696 0.696 104 104 46.0-120 0.0600 21
Fluoranthene 0.667 0.696 0.716 104 107 46.0-120 2.79 20
Fluorene 0.667 0.692 0.694 104 104 47.0-120 0.240 20
Hexachlorobenzene 0.667 0.650 0.679 97.4 102 42.0-120 4.34 20
Hexachloro-1,3-butadiene 0.667 0.561 0.520 84.1 78.0 36.0-120 7.48 26
Hexachlorocyclopentadiene 0.667 0.566 0.553 84.9 82.9 20.0-124 2.28 26
Hexachloroethane 0.667 0.602 0.551 90.3 82.6 32.0-120 8.92 31
Indeno(1,2,3-cd)pyrene 0.667 0.672 0.672 101 101 48.0-120 0.0300 21
Isophorone 0.667 0.536 0.532 80.4 79.7 42.0-120 0.800 21
Naphthalene 0.667 0.482 0.460 72.2 69.0 41.0-120 4.57 24
Nitrobenzene 0.667 0.511 0.493 76.6 73.9 36.0-120 3.62 24
n-Nitrosodimethylamine 0.667 0.604 0.535 90.5 80.2 20.0-120 12.0 31
n-Nitrosodiphenylamine 0.667 0.626 0.650 93.8 97.4 42.0-120 3.76 20
n-Nitrosodi-n-propylamine 0.667 0.647 0.632 97.1 94.8 39.0-120 2.37 23
Phenanthrene 0.667 0.648 0.670 97.1 100 45.0-120 3.44 20
Benzylbutyl phthalate 0.667 0.693 0.686 104 103 41.0-123 0.910 20
Bis(2-ethylhexyl)phthalate 0.667 0.686 0.694 103 104 41.0-124 1.20 20
Di-n-butyl phthalate 0.667 0.671 0.704 101 106 44.0-120 4.75 20
Diethyl phthalate 0.667 0.696 0.702 104 105 46.0-120 0.840 20
Dimethyl phthalate 0.667 0.688 0.699 103 105 47.0-120 1.69 21
Di-n-octyl phthalate 0.667 0.656 0.659 98.4 98.9 40.0-123 0.480 21
Pyrene 0.667 0.659 0.655 98.7 98.2 45.0-120 0.580 21
1,2,4-Trichlorobenzene 0.667 0.504 0.482 75.5 72.3 40.0-120 4.41 25
4-Chloro-3-methylphenol 0.667 0.544 0.548 81.6 82.2 46.0-120 0.790 20
2-Chlorophenol 0.667 0.580 0.553 87.0 82.9 37.0-120 4.83 27
2,4-Dichlorophenol 0.667 0.527 0.512 79.1 76.8 45.0-120 2.97 21
2,4-Dimethylphenol 0.667 0.521 0.503 78.1 75.5 40.0-120 3.37 22
4,6-Dinitro-2-methylphenol 0.667 0.542 0.535 81.2 80.2 34.0-120 1.22 23
2,4-Dinitrophenol 0.667 0.302 0.291 45.3 43.6 10.0-120 3.83 30
2-Nitrophenol 0.667 0.517 0.502 77.5 75.3 42.0-120 2.88 24
4-Nitrophenol 0.667 0.618 0.620 92.6 92.9 40.0-120 0.360 21
Pentachlorophenol 0.667 0.480 0.469 71.9 70.3 33.0-122 2.29 22
Phenol 0.667 0.591 0.570 88.6 85.5 38.0-120 3.51 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG957618
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L893336-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3201111-1 03/06/17 08:18 • (LCSD) R3201111-2 03/06/17 08:41
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2,4,6-Trichlorophenol 0.667 0.672 0.665 101 99.7 47.0-120 1.07 22
(S) Nitrobenzene-d5 76.6 73.8 18.0-125
(S) 2-Fluorobiphenyl 93.0 92.7 28.0-120
(S) p-Terphenyl-d14 98.6 99.8 13.0-131
(S) Phenol-d5 87.0 83.9 20.0-120
(S) 2-Fluorophenol 82.5 76.7 20.0-120
(S) 2,4,6-Tribromophenol 93.1 99.2 17.0-137
L893308-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L893308-03 03/06/17 13:44 • (MS) R3201111-4 03/06/17 14:08 • (MSD) R3201111-5 03/06/17 14:31
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Aniline 0.721 0.0715 0.568 0.584 68.8 71.1 1 10.0-120 2.76 31
Acenaphthene 0.721 U 0.676 0.631 93.7 87.5 1 37.0-120 6.84 23
Acenaphthylene 0.721 U 0.713 0.664 99.0 92.1 1 41.0-120 7.14 22
Anthracene 0.721 U 0.713 0.688 98.8 95.4 1 30.0-123 3.53 25
Benzidine 0.721 U 0.568 0.559 78.7 77.5 1 1.00-120 1.62 36
Benzo(a)anthracene 0.721 U 0.679 0.673 94.2 93.4 1 21.0-123 0.900 26
Benzo(b)fluoranthene 0.721 U 0.710 0.708 98.5 98.2 1 20.0-127 0.290 29
Benzo(k)fluoranthene 0.721 U 0.682 0.672 94.6 93.3 1 22.0-123 1.44 28
Benzo(g,h,i)perylene 0.721 U 0.637 0.609 88.3 84.5 1 10.0-120 4.40 32
Benzo(a)pyrene 0.721 U 0.710 0.697 98.5 96.6 1 23.0-120 1.89 27
Bis(2-chlorethoxy)methane 0.721 U 0.503 0.502 69.7 69.7 1 37.0-120 0.0400 22
Bis(2-chloroethyl)ether 0.721 U 0.563 0.576 78.1 79.9 1 26.0-120 2.28 27
Bis(2-chloroisopropyl)ether 0.721 U 0.609 0.610 84.5 84.7 1 35.0-120 0.160 25
4-Bromophenyl-phenylether 0.721 U 0.676 0.676 93.7 93.8 1 34.0-120 0.0500 23
2-Chloronaphthalene 0.721 U 0.645 0.609 89.5 84.5 1 40.0-120 5.73 22
4-Chlorophenyl-phenylether 0.721 U 0.736 0.682 102 94.6 1 37.0-120 7.62 23
Chrysene 0.721 U 0.705 0.685 97.8 95.1 1 19.0-127 2.77 27
Dibenz(a,h)anthracene 0.721 U 0.664 0.644 92.2 89.3 1 10.0-120 3.11 28
3,3-Dichlorobenzidine 0.721 U 1.03 1.02 142 141 1 10.0-142 1.10 30
2,4-Dinitrotoluene 0.721 U 0.822 0.756 114 105 1 37.0-129 8.30 24
2,6-Dinitrotoluene 0.721 U 0.734 0.679 102 94.2 1 40.0-120 7.79 23
Fluoranthene 0.721 0.00962 0.747 0.735 102 101 1 20.0-133 1.66 28
Fluorene 0.721 U 0.721 0.680 100 94.4 1 35.0-120 5.87 23
Hexachlorobenzene 0.721 U 0.690 0.675 95.7 93.6 1 33.0-120 2.20 24
Hexachloro-1,3-butadiene 0.721 U 0.534 0.555 74.0 77.0 1 33.0-120 3.98 25
Hexachlorocyclopentadiene 0.721 U 0.271 0.271 37.6 37.6 1 10.0-120 0.170 33
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG957618
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L893336-01
L893308-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L893308-03 03/06/17 13:44 • (MS) R3201111-4 03/06/17 14:08 • (MSD) R3201111-5 03/06/17 14:31
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexachloroethane 0.721 U 0.530 0.552 73.5 76.5 1 21.0-120 4.02 30
Indeno(1,2,3-cd)pyrene 0.721 U 0.663 0.637 92.0 88.4 1 10.0-120 4.06 30
Isophorone 0.721 U 0.554 0.545 76.8 75.6 1 38.0-120 1.62 22
Naphthalene 0.721 U 0.471 0.483 65.4 67.0 1 37.0-120 2.42 25
Nitrobenzene 0.721 U 0.495 0.505 68.7 70.1 1 32.0-120 1.99 24
n-Nitrosodimethylamine 0.721 U 0.515 0.543 71.4 75.3 1 18.0-120 5.30 27
n-Nitrosodiphenylamine 0.721 U 0.674 0.664 93.5 92.1 1 20.0-125 1.52 25
n-Nitrosodi-n-propylamine 0.721 U 0.656 0.635 91.0 88.1 1 34.0-120 3.27 23
Phenanthrene 0.721 U 0.693 0.677 96.2 93.9 1 24.0-124 2.35 25
Benzylbutyl phthalate 0.721 U 0.694 0.677 96.3 93.9 1 18.0-130 2.47 27
Bis(2-ethylhexyl)phthalate 0.721 U 0.702 0.693 97.3 96.1 1 19.0-127 1.22 28
Di-n-butyl phthalate 0.721 U 0.718 0.710 99.6 98.5 1 29.0-120 1.16 26
Diethyl phthalate 0.721 U 0.752 0.686 104 95.2 1 42.0-121 9.14 23
Dimethyl phthalate 0.721 U 0.731 0.680 101 94.3 1 42.0-120 7.23 23
Di-n-octyl phthalate 0.721 U 0.693 0.684 96.2 94.9 1 21.0-122 1.37 27
Pyrene 0.721 U 0.678 0.669 94.0 92.7 1 19.0-127 1.37 29
1,2,4-Trichlorobenzene 0.721 U 0.491 0.508 68.1 70.5 1 39.0-120 3.40 25
4-Chloro-3-methylphenol 0.721 U 0.598 0.577 83.0 80.1 1 37.0-121 3.53 23
2-Chlorophenol 0.721 U 0.568 0.587 78.8 81.4 1 34.0-120 3.26 25
2,4-Dichlorophenol 0.721 U 0.564 0.559 78.3 77.5 1 41.0-120 1.03 22
2,4-Dimethylphenol 0.721 U 0.553 0.550 76.7 76.3 1 27.0-120 0.520 25
4,6-Dinitro-2-methylphenol 0.721 U 0.350 0.363 48.6 50.3 1 10.0-131 3.53 29
2,4-Dinitrophenol 0.721 U 0.164 0.168 22.7 23.3 1 10.0-142 2.45 30
2-Nitrophenol 0.721 U 0.523 0.536 72.6 74.3 1 34.0-124 2.34 27
4-Nitrophenol 0.721 U 0.615 0.589 85.3 81.6 1 26.0-133 4.43 25
Pentachlorophenol 0.721 U 0.552 0.563 76.6 78.2 1 15.0-152 1.98 26
Phenol 0.721 U 0.593 0.588 82.3 81.6 1 33.0-120 0.860 24
2,4,6-Trichlorophenol 0.721 U 0.714 0.683 99.1 94.8 1 40.0-125 4.48 24
(S) Nitrobenzene-d5 67.8 70.6 18.0-125
(S) 2-Fluorobiphenyl 89.3 82.6 28.0-120
(S) p-Terphenyl-d14 95.2 92.0 13.0-131
(S) Phenol-d5 81.0 79.5 20.0-120
(S) 2-Fluorophenol 75.4 76.1 20.0-120
(S) 2,4,6-Tribromophenol 100 99.0 17.0-137
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02090017.2 L893336 03/15/17 14:38 25 of 27
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L893336-01
Withers & Ravenel Eng. - Standard
2/28/2017
3/6/2017
SOIL
0306_14
1.00
mg/kg 2
SEMI-VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-17
Project Desc.Pilot Mt. Brownfields
9-Octadecenamide, (Z)-000301-02-0 12.36 J 91.000.688
Cyclopentasiloxane, decamethyl-000541-02-6 6.06 J 90.000.032
Page 1 of 1SVOC TIC Report
Client ID:
ESC Sample No:
Client Name:
Matrix:
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds.
Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are
prepared utilizing a computerized library search routine of electron impact mass spectral data and
evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard from the total ion
chromatogram. TIC's are identified and quantitated only if the peak area is 10% or more of that of the
nearest internal standard.
Dilution Factor:
Lab File ID:
Date Analyzed:
Date Collected:
QAQFEST. CONC.RTCOMPOUNDCAS NO.
Concentration units:
Number of TICs Found:
L893336-01
Withers & Ravenel Eng. - Standard
2/28/2017
3/8/2017
SOIL
0308_10
1.00
0
VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Laboratory ServicesEnvironmental Science Corp.
B-17
Project Desc.Pilot Mt. Brownfields
Page 1 of 1VOC TIC Report

Appendix E
Photo Essay

Photo 1
The Pilot Center (subject property)

Photo 2
TW-1 (existing monitoring well)

Photo 3
Mobilizing Drill Rig

Photo 4
Soil Boring (B-2)

Photo 5
Soil Boring (B-4)

Photo 6
Sub-Slab Soil Boring (B-15)

Photo 7
Soil Boring (B-17)

Photo 8
Patched Sub-Slab Soil Boring

Photo 9
Temporary Well Location (TW-4)

Photo 10
Temporary Well Locations (TW-5)

Photo 11
Temporary Well Location (TW-6)

Photo 12
Temporary Well Location (TW-2)

Photo 13
Temporary Well Location (TW-7)

Photo 14
Abandoned Temporary Well (TW-6)

Photo 15
Water Supply Well and Water Meter Located at 210 Carson Street

Photo 16
Basement (typical) Located at 203 Academy Street