09034_Pelton-Crane_Media Disturbance Report 20170301

Sent Via Email

March 1, 2017

Siemens Medical Solutions USA Inc.
186 Wood Avenue South
Iselin, New Jersey 08830

Attn: Mr. Robert L. Friedman

Re: Soil Disturbance Report
Former Pelton & Crane Facility
200 Clanton Road
Charlotte, NC
Brownfields Project No. 09034-06-60
H&H Project No. MPV-025

Dear Mr. Friedman:

1.0 Introduction

Hart & Hickman, PC (H&H) is pleased to present this report documenting limited soil
disturbance associated with recent building renovation activities at the former Pelton & Crane
facility located at 200 Clanton Road in Charlotte, Mecklenburg County, North Carolina (Site or
subject Site). The Site as used herein consists of the southern portion of the former Pelton &
Crane facility that was most recently occupied by Lifespan. The Site consists of one
approximately 3.1-acre parcel developed with an approximately 73,000 square foot (sq ft)
building located northwest of the Clanton Road and Pelton Street intersection. A Site location
map is provided as Figure 1, and a Site map is provided as Figure 2.

The Site and the parcel to the northwest are listed on the North Carolina Inactive Hazardous Sites
list (Pelton & Crane Site, NCD055162069). Assessment and remediation are being conducted in
accordance with an Administrative Agreement for Registered Environmental Consultant (REC)
Directed Assessment and Remedial Action between Siemens and the North Carolina Department
Robert L. Friedman
March 1, 2017
Page 2
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
of Environmental Quality (DEQ). In February 2008, a Brownfields Agreement for the Site was
completed by Clanton Partners I, LLC. The Brownfields agreement includes certain provisions
relating to disturbance of soil at the Site. In addition, the Site is subject to an Access and
Indemnity Agreement and Temporary Use Restriction between Siemens and Clanton Partners I,
LLC dated September 6, 2005. Section 10 of the Access and Indemnity Agreement and
Temporary Use Restriction includes eleven (11) terms which outline restrictions associated with
disturbance of soil or groundwater at the Site (Media Disturbance Terms).

In April 2016, FHN 200 Clanton, LLC purchased the Site and subsequently completed up-fit of
the administrative offices and warehouse portions of the Site building. The redevelopment
activities included remodeling the two-story office spaces in the southern portion of the Site
building and converting the warehouse areas in the northern portion of the Site building into a
self-storage facility. As part of the redevelopment plan, a sidewalk and handicap ramp were
installed on the western side of the Site building, a new entrance ramp was installed on the south-
central side of the Site building, and new footings were installed on the southeastern side of the
Site building. Installation of the sidewalk, entrance ramp, and footer warranted shallow soil
excavations and grading which resulted in limited soil disturbance. Additionally, limited shallow
trenching in sub-slab soil beneath the building for disconnecting existing utilities and installation
of new utilities was conducted in interior portions of the facility. Areas of soil disturbance
associated with sidewalk, entrance ramp, footer installations, and utility trenching activities are
depicted on Figure 2.

This report documents activities that H&H performed as part of the soil disturbance activities in
accordance with the Brownfields Agreement and the Access and Indemnity Agreement and
Temporary Use Restriction.

Robert L. Friedman
March 1, 2017
Page 3
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
2.0 Soil Disturbance Oversight

In accordance with the Brownfields Agreement, H&H prepared an Environmental Management
Plan (EMP) for implementation during recent Site work which received DEQ Brownfields
approval on June 20, 2016. In accordance with the Access and Indemnity Agreement and
Temporary Use Restriction and the EMP, H&H provided oversight during the redevelopment
activities to document compliance with the Media Disturbance Terms and approved EMP during
shallow excavation and grading Site work, and sub-slab trenching associated with facility
utilities. A brief discussion of the activities and our observations is provided in the following
sections.

2.1 Entrance Ramp Grading Activities

In June 2016, H&H provided oversight during grading activities for installation of an entrance
ramp to the office spaces in the southern portion of the Site building. The location of the
entrance ramp is depicted on Figure 2. Prior to grading in this area, the location of existing
groundwater monitoring well MW-8 (Figure 2) was identified and, in accordance with Media
Disturbance Term (iii), a 5 ft barricade was constructed to prevent heavy machines from coming
in contact with the well vault and potentially causing damage to the monitor well. H&H did not
observe machines coming within 5 ft of the monitor well and no damage to the well or well vault
was noted.

Grading activities for the entrance ramp included removal of surface organics and approximately
6 inches of topsoil. During excavation and grading activities for the entrance ramp, H&H
personnel field screened excavated soil for obvious evidence of staining, unusual odors, and
volatile organic vapors using a calibrated photoionization detector (PID). Field screening results
did not identify obvious evidence of impacts or elevated volatile organic vapor readings.

Robert L. Friedman
March 1, 2017
Page 4
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
Upon completion of grading activities, the excavation area was covered with plastic and secured
to prevent potential stormwater from entering the disturbed area until the concrete could be
poured for the new entrance ramp. Approximately eight (8) cubic yards (yd3) of soil and surface
organics excavated from the ramp area were stockpiled on top of plastic and covered with plastic
for use as possible fill material during construction of the handicap ramp on the western side of
the Site building. Photographs documenting the entrance ramp grading activities are provided in
Appendix A.

2.2 Footer Excavation Activities

In July and August 2016, H&H provided oversight during shallow excavation activities for
installation of a new footer on the southeastern side of the Site building. The location of the
footer excavation is depicted on Figure 2. Dimensions of the excavation were approximately 25
ft by 3 ft and approximately 2 ft below the ground surface (bgs). H&H personnel field screened
soil from the excavated area for obvious evidence of staining, unusual odors, and volatile organic
vapors with a calibrated PID. Field screening results did not identify obvious evidence of
potential impacts. No existing groundwater monitoring wells were identified in the vicinity of
the footer excavation.

Soil removed from the footer excavation was stockpiled on top of plastic and covered with
plastic in accordance with the Media Disturbance Terms and the approved EMP. Additionally,
the open excavation was secured with plastic and a temporary plastic cover was attached to the
roof of the Site building and extended to the ground surface over the excavation to prevent
potential stormwater from entering the disturbed area until concrete for the footer could be
poured. Upon completion of footer construction activities, most of the soil in the excavation
stockpile was placed back into the excavation on top of the new footer and compacted to the
ground surface. Approximately three (3) yd3 of soil from the excavation were not needed for
backfilling the excavation and remained secured in a stockpile on top of plastic and covered for
Robert L. Friedman
March 1, 2017
Page 5
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
possible use as fill beneath the handicap ramp on the western side of the Site building.
Photographs documenting the footer excavation activities are provided in Appendix A.

2.3 Western Exterior Sidewalk

Shallow excavation and grading activities for installation of a new sidewalk and handicap ramp
on the western side of the facility were conducted in July 2016. The new sidewalk extends from
the parking area south of the facility along the western side of the building to a handicap
accessible entrance located on the west side of the facility. The location of the new sidewalk is
depicted on Figure 2.

Prior to beginning excavation and grading for installation of the sidewalk, existing groundwater
monitoring well MW-18B was identified approximately 7 ft west of the work area. In
accordance with Media Disturbance Term (iii), a 5 ft barricade was constructed to prevent heavy
machines from coming in contact with the well vault and potentially causing damage to the
monitor well. H&H did not observe machines coming within 5 ft of the monitor well and no
damage to the well or well vault was noted.

Excavation activities included removal of approximately 2 inches of organics and topsoil in an
area approximately 100 ft by 5 ft for grading and installation of the new sidewalk. Additionally,
PVC stormwater drain pipes were installed at 50 ft intervals in the sidewalk excavation area
(Figure 2). Shallow trenching up to 10 inches bgs was conducted for each stormwater pipe.
During excavation and stormwater pipe trenching activities, H&H personnel field screened soil
for obvious evidence of staining, unusual odors, and elevated PID readings. Field screening
results did not identify obvious evidence of impacts.

Approximately 1 yd3 of soil and organics removed from the excavation area were staged on top
of plastic and covered with plastic in accordance with the Media Disturbance Terms and the
approved EMP. In addition, the sidewalk excavation area was covered with plastic and secured
Robert L. Friedman
March 1, 2017
Page 6
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
to prevent potential stormwater from entering the disturbed area until concrete could be poured
for the new sidewalk. Photographs documenting the sidewalk excavation and grading activities
are provided in Appendix A.

Approximately 6.5 yd3 of soil from the entrance ramp and new footer were used as backfill
beneath the handicap ramp constructed on the western side of the Site building.

2.4 Existing Utility Trenching Activities

In July 2016, two small sections of the building slab were removed to access the locations of
existing sanitary sewer pipes. One existing sanitary sewer pipe was located in the northwest
portion of the building, and one existing sanitary sewer pipe was located in the northeast portion
of the building. Locations of the sanitary sewer pipes are depicted on Figure 2.

Small amounts of soil beneath the slab of the building were removed in each location to trench
and uncover the sanitary sewer lines. Soil from each area was placed on the concrete floors of
the building adjacent to the trenches. Once uncovered, the pipes were disconnected and
permanently capped. The sanitary sewer pipe in the northwestern portion of the building was
capped approximately 12 inches beneath the slab, and the sanitary sewer pipe in the northeastern
portion of the building was capped at approximately 16 inches below the slab. During trenching
to locate the sanitary sewer lines, H&H field screened soil from each area for obvious evidence
of staining, unusual odors, and elevated PID readings. Field screening results did not identify
obvious evidence of potential impacts.

Once the sanitary sewer pipes were disconnected and permanently capped, soil removed from the
two areas was placed back into the trenches using the last out, first in principal in accordance
with the approved EMP. Concrete was then poured to replace the removed slab and seal the
Robert L. Friedman
March 1, 2017
Page 7
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
floor of the building. Photographs documenting the trenching and abandonment of the sanitary
sewer pipes are provided in Appendix A.

2.5 New Utility Trenching Activities

In July 2016, small sections of the slab were removed for installation of new utilities in the
southern portion of the building. One section of slab was removed west of the administrative
office area, and one section of slab was removed east of the administrative office area (Figure 2).
Small amounts of soil beneath the slab were removed in each location to trench and uncover
existing utilities. The soil removed from each area was placed on top of plastic on the concrete
floor of the building adjacent to each trench. During trenching activities, H&H personnel field
screened the soil for obvious evidence of staining, unusual odors, and elevated PID readings.
Field screening results did not identify obvious evidence of potential impacts.

The total depth of the utility trench west of the administrative offices was approximately 22
inches below the slab. The total depth of the utility trench east of the administrative offices was
approximately 24 inches below the slab. Upon completion of the utility installation activities
and approval from the Mecklenburg County utility inspector, soil in each area was placed back
into the trenches using the last out, first in principal in accordance with the approved EMP.
Concrete was then poured to replace the removed section of slab and seal the floor of the
building. Photographs documenting new utility installation activities are provided in Appendix
A.

Robert L. Friedman
March 1, 2017
Page 8
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
3.0 Soil Sampling Activities

3.1 Soil Stockpile Sampling

The general contractor conducting the Site-work determined that some of the soil generated
during excavations for construction of the entrance ramp, footer, and sidewalk was unsuitable for
fill beneath the handicap ramp due to the presence of debris and organics. Therefore, on August
16, 2016 H&H collected a composite soil sample from the stockpiles for laboratory analysis of
volatile organic compounds (VOCs), semi-VOCs (SVOCs), and EPA Priority Pollutant List
(PPL) metals plus hexavalent chromium for disposal purposes in accordance with the approved
EMP.

The composite soil sample 10 aliquots collected from the stockpile that were combined and
homogenized to form a single sample for analysis (labeled SP-20160816). The composite soil
sample was then placed directly into laboratory supplied glassware, placed on ice in a laboratory
supplied cooler, and shipped under standard chain of custody protocols to Prism Laboratories,
Inc (Prism) for analysis of SVOCs by EPA Method 8270D and PPL metals plus hexavalent
chromium by EPA Methods 6010/7471/7196. For the VOC analysis, a single grab sample was
collected from an undisturbed portion of a representative stockpile and submitted for laboratory
analysis of VOCs by EPA Method 8260B.

3.1.1 Stockpile Soil Sample Results

Laboratory analytical results are summarized in Table 1 and the laboratory analytical report is
included as Appendix B. The analytical results were compared to IHSB Residential and
Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs). In addition to the PSRGs,
metals results were compared to published concentrations for naturally occurring metals.

Robert L. Friedman
March 1, 2017
Page 9
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
Analytical results indicate that trace levels of the VOCs acetone (0.090 mg/kg) and methyl ethyl
ketone (0.0046 J mg/kg) were detected in the soil sample at concentrations below the PSRGs.
Additionally, several metals were detected at concentrations above the laboratory reporting
limits. However, the metals detections are consistent with published concentrations for naturally
occurring metals in North Carolina soil.

Several polynuclear aromatic hydrocarbon (PAHs) were detected at concentrations above the
laboratory reporting limits in the stockpile soil sample. Benzo[a]anthracene (0.18 J mg/kg),
benzo[b]fluoranthene (0.22 J mg/kg), and benzo[a]pyrene (0.17 J mg/kg) were detected at
concentrations exceeding the Residential PSRGs of 0.16 mg/kg, 0.16 mg/kg, and 0.016 mg/kg,
respectively. The “J flag” indicates that the compound was detected above the laboratory
method detection limit, but below the laboratory reporting limit resulting in a laboratory
estimated concentration. No other PAHs were detected above the Residential PSRGs and no
compounds were detected above the Industrial/Commercial PSRGs.

Because PAHs were detected above the PSRGs in the stockpile soil sample, approximately 5.45
tons (approximately 3.6 yd3) of soil were transported to the EVO Corporation facility near
Winston-Salem, NC for treatment/disposal. Waste disposal certificates and weight tickets
documenting the disposition of the soil are provided in Appendix C.

3.2 Footer Area Soil Sampling

Soil that was disturbed during excavation and footer installation activities near the southeastern
side of the facility is exposed at the surface. Unlike the entrance ramp area and western
sidewalk, no impervious cover was placed in this area upon completion of the footer
construction. Therefore, H&H collected shallow soil samples in the disturbed area to evaluate
the potential for impacts at the surface.

Robert L. Friedman
March 1, 2017
Page 10
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
H&H advanced five shallow soil borings with a decontaminated stainless steel hand auger in 5 ft
intervals across the area where soil was placed on top of the new footer. Aliquot soil samples
were collected from the center of the hand auger bucket from each soil boring. The 5 aliquots
were combined and homogenized into a composite soil sample (labeled Footing-20160816). The
composite soil sample was then placed directly into laboratory supplied glassware, placed on ice
in a laboratory supplied cooler, and shipped under standard chain of custody protocols to Prism
for analysis of SVOCs by EPA Method 8270D and PPL metals plus hexavalent chromium by
EPA Methods 6010/7471/7196. A grab sample was collected from undisturbed portions of
aliquot soil and submitted for laboratory analysis of VOCs by EPA Method 8260B.

3.2.2 Footer Area Soil Sample Results

Laboratory analytical results for the footer area soil sample are summarized in Table 1 and the
laboratory analytical report is included as Appendix B. Similar to the stockpile soil sample, the
analytical results were compared to IHSB Residential and Industrial/Commercial PSRGs and
metals results were compared to published concentrations for naturally occurring metals.

The analytical results indicate that trace levels of the VOCs acetone (0.080 mg/kg) and methyl
ethyl ketone (0.0037 J mg/kg) were detected above the laboratory method detection level, but
well below the PSRGs. Additionally, trace levels of the SVOCs benzo[b]fluoranthene (0.12 J
mg/kg), chrysene (0.094 J mg/kg), fluoranthene (0.17 J mg/kg), and pyrene (0.15 J mg/kg) were
detected in the footer area soil sample at concentrations below the Residential and
Industrial/Commercial PSRGs. No other VOCs or SVOCs were detected above the laboratory
method detection limit.

As expected, several metals were detected at concentrations above the laboratory reporting limits
in the footer area soil sample. No detected metals concentrations exceed the
Industrial/Commercial PSRGs. Additionally, the detected metals concentrations are consistent
with naturally occurring background concentrations for North Carolina soils.
Robert L. Friedman
March 1, 2017
Page 11
S:\AAA-Master Projects\Merrifield Patrick & Vermillion - MPV\MPV-025 200 Clanton\2016 Site Work\Report\Former
Pelton&Crane_BF Proj# 09034-05-60_Media Disturbance Report .docx
3.3 Sampling Procedure

Soil samples were collected in general accordance with DEQ Inactive Hazardous Waste Sites
Program Guidelines for Assessment and Cleanup dated October 2015 and most recent versions
of the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem Support
(SESD) Field Branches Quality System and Technical Procedures guidance.

4.0 Summary and Conclusions

H&H has completed oversight and monitoring to document limited soil disturbance associated
with building renovations at the former Pelton & Crane facility located at 200 Clanton Road in
Charlotte. Site work resulting in disturbance of shallow soil at the Site included excavation and
grading for installation of a new entrance ramp, a new sidewalk, and a new footer, and trenching
activities associated with utility work. Below is a brief summary of our observations:

 Field screening of soil from each area disturbed during the redevelopment activities did
not identify evidence of potential impacts.

 An approximately 3.6 yd3 of excess soil from the entrance ramp, new footer, and western
sidewalk were transported to the EVO Corporation facility near Winston-Salem, NC for
disposal.

 Results of analyses of a composite soil sample collected from shallow exposed soil in the
disturbed area associated with the new footer excavation did not indicate compound
concentrations exceeding the Industrial/Commercial PSRGs.

Based on our observations, the recent redevelopment activities were conducted in accordance
with the Media Disturbance Terms and the DEQ approved EMP.

Ta
b
l
e

1
Su
m
m
a
r
y

o
f

S
o
i
l

A
n
a
l
y
t
i
c
a
l

D
a
t
a
Fo
r
m
e
r

P
e
l
t
o
n

C
r
a
n
e

F
a
c
i
l
i
t
y

(
B
F

P
r
o
j
e
c
t

#
0
9
0
3
4
-
0
6
-
6
0
)
20
0

C
l
a
n
t
o
n

R
o
a
d
Ch
a
r
l
o
t
t
e
,

N
o
r
t
h

C
a
r
o
l
i
n
a
H&
H

J
o
b

N
o
.

M
P
V
-
0
2
5
S
a
m
p
l
e

I
D

S
P
-
2
0
1
6
0
8
1
6

F
o
o
t
i
n
g

2
0
1
6
0
8
1
6
S
a
m
p
l
e

D
a
t
e

8
/
1
6
/
2
0
1
6

8
/
1
6
/
2
0
1
6
Range

M
e
a
n
U
n
i
t
s
VO
C
s

(82
6
0
B
)
Ac
e
t
o
n
e
0.
0
9
0

0
.
0
8
0

1
2
,
2
0
0
10
0
,
0
0
0

N
A N A
Me
t
h
y
l

E
t
h
y
l

K
e
t
o
n
e

(
2
-
B
u
t
a
n
o
n
e
)

0
.
0
0
4
6

J

0
.
0
0
3
7

J

5
,
4
0
0
28
,
4
0
0

N
A N A
SV
O
C
s

(82
7
0
)
Be
n
z
o
[
a
]
a
n
t
h
r
a
c
e
n
e
0.
1
8

J
<0
.
3
6
0.
1
6
2.
9
0

N
A N A
Be
n
z
o
[
b
]
f
l
u
o
r
a
n
t
h
e
n
e
0.
2
2

J
0.
1
2

J

0
.
1
6
2.
9
0

N
A N A
Be
n
z
o
[
g
,
h
,
i
]
p
e
r
y
l
e
n
e

0
.
1
2

J
<0
.
3
6
NE
NE

N
A N A
Be
n
z
o
[
a
]
p
y
r
e
n
e
0.
1
7

J
<0
.
3
6
0.
0
1
6
0.
2
9

N
A N A
Be
n
z
o
[
k
]
f
l
u
o
r
a
n
t
h
e
n
e

0
.
0
8
9

J
<0
.
3
6
1.
6
0
29
.
0

N
A N A
Bi
s
(
2
-
E
t
h
y
l
h
e
x
y
l
)
p
h
t
h
a
l
a
t
e

0
.
0
9
4

J
<0
.
3
6
39
16
0

N
A N A
Ch
r
y
s
e
n
e

0
.
1
7

J

0
.
0
9
4

J

1
.
6
0
29
0

N
A N A
Fl
u
o
r
a
n
t
h
e
n
e

0
.
3
6

0
.
1
7

J

4
8
6,
0
0
0

N
A N A
In
d
e
n
o
[
1
,
2
,
3
-
c
d
]
p
y
r
e
n
e

0
.
1
3

J
<0
.
3
6
0.
1
6
2.
9
0

N
A N A
Ph
e
n
a
n
t
h
r
e
n
e

0
.
1
6

J
<0
.
3
6
NE
NE

N
A N A
Py
r
e
n
e

0
.
3
0

J

0
.
1
5

J

3
6
0
4,
6
0
0

N
A N A
PP
L

M
e
t
a
l
s

(
6
0
2
0
B
/
7
4
7
1
B
/
7
1
9
6
A
)
An
t
i
m
o
n
y

0
.
4
3

0
.
4
3

6
.
2
0
94

<
1
.
0
-
8
.
8

0
.
7
6
Ar
s
e
n
i
c

2
.
7

2
.
6

0
.
6
8
0
3.
0
0

1
.
0
-
1
8

4
.
8
Be
r
y
l
l
i
u
m

0
.
5
3

0
.
5
4

3
2
.
0

4
6
0

B
R
L
-
2
.
0

0
.
1
1
Ch
r
o
m
i
u
m

2
4

2
8

N
E
NE

7
-
3
0
0

6
5
Ch
r
o
m
i
u
m

(
V
I
)
<
2
.
1
5

<

2
.
1
5
0.
3
0
0
6.
3
0

N
E

N
E
Ch
r
o
m
i
u
m

(
I
I
I
)

2
4

2
8
24
,
0
0
0
10
0
,
0
0
0

N
E

N
E
Co
p
p
e
r
38

B

3
5

B
62
0

9
,
4
0
0

3
.
0
-
1
0
0

3
4
Le
a
d

4
8

3
3

4
0
0
80
0

B
R
L
-
5
0

1
6
Me
r
c
u
r
y

0
.
0
6
4

0
.
0
6
2

2
.
2
0

3
.
1
3

0
.
0
3
-
0
.
5
2

0
.
1
2
1
Ni
c
k
e
l

1
2

B

1
0

B

3
0
0

4
,
4
0
0

B
R
L
-
1
5
0

2
3
Zi
n
c

9
5

6
9

4
,
6
0
0
70
,
0
0
0

2
5
-
1
2
4

5
6
No
t
e
s
:
1)

N
o
r
t
h

C
a
r
o
l
i
n
a

D
e
p
a
r
t
m
e
n
t

o
f

E
n
v
i
r
o
n
m
e
n
t
a
l

Q
u
a
l
i
t
y

(
D
E
Q
)

I
n
a
c
t
i
v
e

H
a
z
a
r
d
o
u
s

S
i
t
e
s

B
r
a
n
c
h

(
I
H
S
B
)

P
r
e
l
i
m
i
n
a
r
y

S
o
i
l

R
e
m
e
d
i
a
t
i
o
n
G
o
a
l
s

(
P
S
R
G
s
)

(
O
c
t
o
b
e
r

2
0
1
6
)
.
2)

R
a
n
g
e

a
n
d

m
e
a
n

v
a
l
u
e
s

o
f

b
a
c
k
g
r
o
u
n
d

m
e
t
a
l
s

f
o
r

N
o
r
t
h

C
a
r
o
l
i
n
a

s
o
i
l
s

t
a
k
e
n

f
r
o
m

El
e
m
e
n
t
s

i
n

N
o
r
t
h

A
m
e
r
i
c
a
n

S
o
i
l
s

by

D
r
a
g
u
n

a
n
d

C
h
e
k
i
r
i
,

2
0
0
5
.
Bo
l
d
e
x
c
e
e
d
s

R
e
s
i
d
e
n
t
i
a
l

P
S
R
G
So
i
l

c
o
n
c
e
n
t
r
a
t
i
o
n
s

a
r
e

r
e
p
o
r
t
e
d

i
n

m
i
l
l
i
g
r
a
m
s

p
e
r

k
i
l
o
g
r
a
m

(
m
g
/
k
g
)
.
La
b
o
r
a
t
o
r
y

a
n
a
l
y
t
i
c
a
l

m
e
t
h
o
d
s

a
r
e

s
h
o
w
n

i
n

p
a
r
e
n
t
h
e
s
e
s
.
On
l
y

c
o
m
p
o
u
n
d
s

d
e
t
e
c
t
e
d

i
n

a
t

l
e
a
s
t

o
n
e

s
a
m
p
l
e

s
h
o
w
n

a
b
o
v
e
;

s
e
e

c
h
a
i
n

o
f

c
u
s
t
o
d
y

f
o
r
m

f
o
r

c
o
m
p
l
e
t
e

l
i
s
t

a
n
a
l
y
z
e
d
.
J
f
l
a
g

d
e
n
o
t
e
s

t
h
a
t

t
h
e

c
o
m
p
o
u
n
d

w
a
s

d
e
t
e
c
t
e
d

a
b
o
v
e

t
h
e

l
a
b
o
r
a
t
o
r
y

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t

b
u
t

b
e
l
o
w

t
h
e

l
a
b
o
r
a
t
o
r
y

r
e
p
o
r
t
i
n
g

l
i
mi
t

r
e
s
u
l
t
i
n
g

i
n

a
n

e
s
t
i
m
a
t
e
d

c
o
n
c
e
n
t
r
a
t
i
o
n
.
B
f
l
a
g

d
e
n
o
t
e
s

t
h
a
t

t
h
e

c
o
m
p
o
u
n
d

w
a
s

d
e
t
e
c
t
e
d

i
n

t
h
e

l
a
b
o
r
a
t
o
r
y

b
l
a
n
k

a
t

a

c
o
n
c
e
n
t
r
a
t
i
o
n

g
r
e
a
t
e
r

t
h
a
n

h
a
l
f

t
h
e

r
e
p
o
r
t
i
n
g

l
i
m
i
t
.
NA

=

N
o
t

A
p
p
l
i
c
a
b
l
e
;

N
E

=

n
o
t

e
s
t
a
b
l
i
s
h
e
d
;

B
R
L

=

b
e
l
o
w

r
e
p
o
r
t
i
n
g

l
i
m
i
t
Re
s
i
d
e
n
t
i
a
l

PS
R
G
s
(1
)
In
d
u
s
t
r
i
a
l
/
C
o
m
m
e
r
c
i
a
l
PS
R
G
s
(1
)
(m
g
/
k
g
)
Regional Background Metals in Soil (2)
S:\
A
A
A
-
M
a
s
t
e
r

P
r
o
j
e
c
t
s
\
M
e
r
r
i
f
i
e
l
d

P
a
t
r
i
c
k

&

V
e
r
m
i
l
l
i
o
n

-

M
P
V
\
M
P
V
-
0
2
5

2
0
0

C
l
a
n
t
o
n
\
2
0
1
6

S
i
t
e

W
o
r
k
\
T
a
b
l
e
s
\
d
a
t
a
.
x
l
s
m
2/
2
3
/
2
0
1
7
Table 1 Hart & Hickman, PC
SITE LOCATION MAP
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
02-25-2017 0
1MPV-025
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
7.5 MINUTE SERIES (TOPOGRAPHIC)
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
CHARLOTTE WEST, NORTH CAROLINA 1996
SITE
REVISION NO. 0
JOB NO. MPV-025
DATE: 2-27-17
FIGURE NO. 2
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
CAPPED PLUMBING LINE
MONITORING WELL
AREA OF SOIL DISTURBANCE
CL
A
N
T
O
N

R
O
A
D
PE
L
T
O
N

S
T
R
E
E
T
NEW FOOTER EXCAVATION
ENTRANCE RAMP
WESTERN EXTERIOR
SIDEWALK
MW-18B
MW-8
PVC STORM DRAINS
APPROXIMATE LOCATION OF NEW
SUB-SLAB UTILITY TRENCHES
PVC STORM DRAIN
OFFICES
SELF-STORAGE
NOTE:
AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY
GIS (2013).
EXISTING UTILITY TRENCH ACTIVITIES
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
S:\
A
A
A
-
M
a
s
t
e
r

P
r
o
j
e
c
t
s
\
M
e
r
r
i
f
i
e
l
d

P
a
t
r
i
c
k

&

V
e
r
m
i
l
l
i
o
n

-

M
P
V
\
M
P
V
-
0
2
5

2
0
0

C
l
a
n
t
o
n
\
B
r
o
w
n
f
i
e
l
d
s
\
F
i
g
u
r
e
s
\
S
i
t
e

M
a
p
.
d
w
g
,

F
I
G

2
,

2
/
2
7
/
2
0
1
7

2
:
2
1
:
2
2

P
M
,

z
b
a
r
l
o
w

APPENDIX A

Site Photographs
Photograph 1: Entrance ramp area located on southern side of the Site building.
Photograph 2: Monitor well MW-8 with 5 foot barrier securing the well.
MP
V
-
0
2
5
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
Photograph 3: Shallow excavation entrance ramp construction.
Photograph 4: Soil stockpile generated during excavation and grading for the entrance ramp.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 5: Entrance ramp soil stockpile secured with entrance ramp construction beyond.
Photograph 6: Entrance ramp excavation area covered with plastic until concrete could be poured.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 7: Sidewalk excavation area on the western side of the facility.
Photograph 8: Soil stockpile generated during sidewalk excavation and grading activities secured and covered.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 9: New footer excavation area on the southeastern side of the facility.
Photograph 10: Soil stockpile generated during footer excavation activities.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 11: Footer excavation soil stockpile covered and secured.
Photograph 12: Footer excavation area covered until completion of the footer construction activities.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 13: Footer excavation backfill upon completion of the footer construction activities.
Photograph 14: Footing excavation area upon completion of backfill and compaction activities.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 15: Trenching and uncovering existing sanitary sewer line in western portion of the Site building.
Photograph 16: Disconnecting and capping sanitary sewer pipe in the western portion of the facility.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 17: Section of concrete removed for installation o new utilities in the southeastern portion of the Site building.
Photograph 18: Section of concrete removed for installation o new utilities in the southeastern portion of the Site building.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 19: Trenching and installing new sub-slab utilities.
Photograph 20: Soil placed back into trench using last out, first in principal.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA
Photograph 21: Utility trench backfill and compaction activities complete.
Photograph 22: Plastic moisture barrier placed on top of utility trench area before concrete was poured.
MP
V
-
0
2
5
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
FORMER PELTON & CRANE FACILITY
200 CLANTON ROAD
CHARLOTTE, NORTH CAROLINA

APPENDIX B

Laboratory Analytical Report
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
02/23/2017
Hart & Hickman (Charlotte)
Ralph McGee
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: MPV-025
Lab Submittal Date: 08/16/2016
Prism Work Order: 6080305
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
M Matrix spike outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 32
Sample Receipt Summary
02/23/2017
Prism Work Order: 6080305
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
6080305-01 08/16/16Footing 20160816 08/16/16Solid
6080305-02 08/16/16SP-20160816 08/16/16Solid
Samples were received in good condition at 5.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 32
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6080305
02/23/2017
Summary of Detections
0.12 J mg/kg dry6080305-01 Footing 20160816 Benzo(b)fluoranthene 8270D
0.094 J mg/kg dry6080305-01 Footing 20160816 Chrysene 8270D
0.17 J mg/kg dry6080305-01 Footing 20160816 Fluoranthene 8270D
0.15 J mg/kg dry6080305-01 Footing 20160816 Pyrene 8270D
0.062 mg/kg dry6080305-01 Footing 20160816 Mercury *7471B
0.43 mg/kg dry6080305-01 Footing 20160816 Antimony *6020B
2.6 mg/kg dry6080305-01 Footing 20160816 Arsenic *6020B
0.54 mg/kg dry6080305-01 Footing 20160816 Beryllium *6020B
28 mg/kg dry6080305-01 Footing 20160816 Chromium *6020B
35 B mg/kg dry6080305-01 Footing 20160816 Copper *6020B
33 mg/kg dry6080305-01 Footing 20160816 Lead *6020B
10 B mg/kg dry6080305-01 Footing 20160816 Nickel *6020B
69 mg/kg dry6080305-01 Footing 20160816 Zinc *6020B
0.080 mg/kg dry6080305-01 Footing 20160816 Acetone 8260B
0.0037 J mg/kg dry6080305-01 Footing 20160816 Methyl Ethyl Ketone (2-Butanone)8260B
0.18 J mg/kg dry6080305-02 SP-20160816 Benzo(a)anthracene 8270D
0.17 J mg/kg dry6080305-02 SP-20160816 Benzo(a)pyrene 8270D
0.22 J mg/kg dry6080305-02 SP-20160816 Benzo(b)fluoranthene 8270D
0.12 J mg/kg dry6080305-02 SP-20160816 Benzo(g,h,i)perylene 8270D
0.089 J mg/kg dry6080305-02 SP-20160816 Benzo(k)fluoranthene 8270D
0.094 J mg/kg dry6080305-02 SP-20160816 Bis(2-Ethylhexyl)phthalate 8270D
0.17 J mg/kg dry6080305-02 SP-20160816 Chrysene 8270D
0.36 mg/kg dry6080305-02 SP-20160816 Fluoranthene 8270D
0.13 J mg/kg dry6080305-02 SP-20160816 Indeno(1,2,3-cd)pyrene 8270D
0.16 J mg/kg dry6080305-02 SP-20160816 Phenanthrene 8270D
0.30 J mg/kg dry6080305-02 SP-20160816 Pyrene 8270D
0.064 mg/kg dry6080305-02 SP-20160816 Mercury *7471B
0.43 mg/kg dry6080305-02 SP-20160816 Antimony *6020B
2.7 mg/kg dry6080305-02 SP-20160816 Arsenic *6020B
0.53 mg/kg dry6080305-02 SP-20160816 Beryllium *6020B
24 mg/kg dry6080305-02 SP-20160816 Chromium *6020B
38 B mg/kg dry6080305-02 SP-20160816 Copper *6020B
48 mg/kg dry6080305-02 SP-20160816 Lead *6020B
12 B mg/kg dry6080305-02 SP-20160816 Nickel *6020B
95 mg/kg dry6080305-02 SP-20160816 Zinc *6020B
0.090 mg/kg dry6080305-02 SP-20160816 Acetone 8260B
0.0046 J mg/kg dry6080305-02 SP-20160816 Methyl Ethyl Ketone (2-Butanone)8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 32
Laboratory Report
02/23/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: Footing 20160816
Prism Sample ID: 6080305-01
Prism Work Order: 6080305
Time Collected: 08/16/16 13:45
Time Submitted: 08/16/16 15:55
General Chemistry Parameters
92.3 *SM2540 G P6H033410.100 8/18/16 15:45 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0561,2,4-Trichlorobenzene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0541,2-Dichlorobenzene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0501,3-Dichlorobenzene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0521,4-Dichlorobenzene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0691-Methylnaphthalene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0672,4,6-Trichlorophenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0692,4-Dichlorophenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0552,4-Dimethylphenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0502,4-Dinitrophenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0432,4-Dinitrotoluene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0482,6-Dinitrotoluene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0522-Chloronaphthalene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0512-Chlorophenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0572-Methylnaphthalene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0462-Methylphenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0652-Nitrophenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0713,3'-Dichlorobenzidine
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0443/4-Methylphenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0544,6-Dinitro-2-methylphenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0614-Bromophenyl phenyl ether
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0504-Chloro-3-methylphenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0434-Chloroaniline
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0464-Chlorophenyl phenyl ether
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.0554-Nitrophenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.049Acenaphthene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.052Acenaphthylene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.058Anthracene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.047Azobenzene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.047Benzo(a)anthracene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.039Benzo(a)pyrene
0.12 8270D P6H031410.36 8/18/16 21:55 JMVJmg/kg dry 0.042Benzo(b)fluoranthene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.039Benzo(g,h,i)perylene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.047Benzo(k)fluoranthene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.030Benzoic Acid
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.047Benzyl alcohol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.062bis(2-Chloroethoxy)methane
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.050Bis(2-Chloroethyl)ether
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.061Bis(2-chloroisopropyl)ether
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.053Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 32
Laboratory Report
02/23/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: Footing 20160816
Prism Sample ID: 6080305-01
Prism Work Order: 6080305
Time Collected: 08/16/16 13:45
Time Submitted: 08/16/16 15:55
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.051Butyl benzyl phthalate
0.094 8270D P6H031410.36 8/18/16 21:55 JMVJmg/kg dry 0.045Chrysene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.044Dibenzo(a,h)anthracene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.054Dibenzofuran
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.049Diethyl phthalate
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.047Dimethyl phthalate
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.051Di-n-butyl phthalate
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.044Di-n-octyl phthalate
0.17 8270D P6H031410.36 8/18/16 21:55 JMVJmg/kg dry 0.046Fluoranthene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.051Fluorene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.057Hexachlorobenzene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.064Hexachlorobutadiene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.064Hexachlorocyclopentadiene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.060Hexachloroethane
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.041Indeno(1,2,3-cd)pyrene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.048Isophorone
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.058Naphthalene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.051Nitrobenzene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.056N-Nitroso-di-n-propylamine
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.054N-Nitrosodiphenylamine
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.042Pentachlorophenol
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.046Phenanthrene
BRL 8270D P6H031410.36 8/18/16 21:55 JMVmg/kg dry 0.053Phenol
0.15 8270D P6H031410.36 8/18/16 21:55 JMVJmg/kg dry 0.047Pyrene
Surrogate Recovery Control Limits
39-13288 %2,4,6-Tribromophenol
44-11583 %2-Fluorobiphenyl
35-11582 %2-Fluorophenol
37-12278 %Nitrobenzene-d5
34-12184 %Phenol-d5
54-12778 %Terphenyl-d14
Total Metals
0.062 *7471B P6H031710.022 8/18/16 11:38 JABmg/kg dry 0.0012Mercury
0.43 *6020B P6H0348100.27 8/19/16 15:33 pfitzmg/kg dry 0.11Antimony
2.6 *6020B P6H0348101.6 8/19/16 15:33 pfitzmg/kg dry 0.14Arsenic
0.54 *6020B P6H0348100.27 8/19/16 15:33 pfitzmg/kg dry 0.12Beryllium
BRL *6020B P6H0348100.27 8/19/16 15:33 pfitzmg/kg dry 0.12Cadmium
28 *6020B P6H0348100.55 8/19/16 15:33 pfitzmg/kg dry 0.12Chromium
35 *6020B P6H0348100.55 8/19/16 15:33 pfitzBmg/kg dry 0.11Copper
33 *6020B P6H0348100.27 8/19/16 15:33 pfitzmg/kg dry 0.11Lead
10 *6020B P6H0348100.27 8/19/16 15:33 pfitzBmg/kg dry 0.092Nickel
BRL *6020B P6H0348101.1 8/19/16 15:33 pfitzmg/kg dry 0.11Selenium
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 32
Laboratory Report
02/23/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: Footing 20160816
Prism Sample ID: 6080305-01
Prism Work Order: 6080305
Time Collected: 08/16/16 13:45
Time Submitted: 08/16/16 15:55
BRL *6020B P6H0348100.27 8/19/16 15:33 pfitzmg/kg dry 0.12Silver
BRL *6020B P6H0348100.27 8/19/16 15:33 pfitzmg/kg dry 0.12Thallium
69 *6020B P6H034810228/19/16 15:33 pfitzmg/kg dry 1.0Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000511,1,1,2-Tetrachloroethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000301,1,1-Trichloroethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000421,1,2,2-Tetrachloroethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000551,1,2-Trichloroethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000791,2,3-Trichloropropane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000461,2,4-Trichlorobenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000471,2,4-Trimethylbenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000371,2-Dichloroethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000471,3,5-Trimethylbenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000411,3-Dichlorobenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000374-Chlorotoluene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.000304-Isopropyltoluene
0.080 8260B P6H038310.062 8/22/16 12:49 ANGmg/kg dry 0.0015Acetone
BRL 8260B P6H038310.0037 8/22/16 12:49 ANGmg/kg dry 0.00036Benzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00052Bromobenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00034Bromochloromethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00070Bromoform
BRL 8260B P6H038310.012 8/22/16 12:49 ANGmg/kg dry 0.00077Bromomethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00033Chlorobenzene
BRL 8260B P6H038310.012 8/22/16 12:49 ANGmg/kg dry 0.00052Chloroethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00045Chloroform
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00042Chloromethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00028Dichlorodifluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 32
Laboratory Report
02/23/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: Footing 20160816
Prism Sample ID: 6080305-01
Prism Work Order: 6080305
Time Collected: 08/16/16 13:45
Time Submitted: 08/16/16 15:55
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00024Ethylbenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00037Isopropylbenzene (Cumene)
BRL 8260B P6H038310.012 8/22/16 12:49 ANGmg/kg dry 0.00057m,p-Xylenes
BRL 8260B P6H038310.062 8/22/16 12:49 ANGmg/kg dry 0.00056Methyl Butyl Ketone (2-Hexanone)
0.0037 8260B P6H038310.12 8/22/16 12:49 ANGJmg/kg dry 0.00056Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6H038310.062 8/22/16 12:49 ANGmg/kg dry 0.00053Methyl Isobutyl Ketone
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00035Methylene Chloride
BRL 8260B P6H038310.012 8/22/16 12:49 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6H038310.012 8/22/16 12:49 ANGmg/kg dry 0.00020Naphthalene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00037n-Propylbenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00025o-Xylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00037Styrene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00036Toluene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00040Trichloroethylene
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00040Trichlorofluoromethane
BRL 8260B P6H038310.031 8/22/16 12:49 ANGmg/kg dry 0.00085Vinyl acetate
BRL 8260B P6H038310.0062 8/22/16 12:49 ANGmg/kg dry 0.00030Vinyl chloride
BRL 8260B P6H038310.019 8/22/16 12:49 ANGmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130105 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-129100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 32
Laboratory Report
02/23/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: SP-20160816
Prism Sample ID: 6080305-02
Prism Work Order: 6080305
Time Collected: 08/16/16 15:04
Time Submitted: 08/16/16 15:55
General Chemistry Parameters
93.3 *SM2540 G P6H033410.100 8/18/16 15:45 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0551,2,4-Trichlorobenzene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0531,2-Dichlorobenzene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0491,3-Dichlorobenzene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0511,4-Dichlorobenzene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0671-Methylnaphthalene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0662,4,6-Trichlorophenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0682,4-Dichlorophenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0542,4-Dimethylphenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0492,4-Dinitrophenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0422,4-Dinitrotoluene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0462,6-Dinitrotoluene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0512-Chloronaphthalene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0502-Chlorophenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0562-Methylnaphthalene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0452-Methylphenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0642-Nitrophenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0693,3'-Dichlorobenzidine
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0433/4-Methylphenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0534,6-Dinitro-2-methylphenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0604-Bromophenyl phenyl ether
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0494-Chloro-3-methylphenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0424-Chloroaniline
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0454-Chlorophenyl phenyl ether
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.0544-Nitrophenol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.048Acenaphthene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.051Acenaphthylene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.056Anthracene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.046Azobenzene
0.18 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.046Benzo(a)anthracene
0.17 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.038Benzo(a)pyrene
0.22 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.041Benzo(b)fluoranthene
0.12 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.038Benzo(g,h,i)perylene
0.089 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.046Benzo(k)fluoranthene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.029Benzoic Acid
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.046Benzyl alcohol
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.061bis(2-Chloroethoxy)methane
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.049Bis(2-Chloroethyl)ether
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.060Bis(2-chloroisopropyl)ether
0.094 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.052Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 32
Laboratory Report
02/23/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: SP-20160816
Prism Sample ID: 6080305-02
Prism Work Order: 6080305
Time Collected: 08/16/16 15:04
Time Submitted: 08/16/16 15:55
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.050Butyl benzyl phthalate
0.17 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.044Chrysene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.043Dibenzo(a,h)anthracene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.053Dibenzofuran
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.048Diethyl phthalate
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.046Dimethyl phthalate
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.050Di-n-butyl phthalate
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.043Di-n-octyl phthalate
0.36 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.045Fluoranthene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.050Fluorene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.055Hexachlorobenzene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.063Hexachlorobutadiene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.062Hexachlorocyclopentadiene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.059Hexachloroethane
0.13 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.040Indeno(1,2,3-cd)pyrene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.047Isophorone
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.056Naphthalene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.050Nitrobenzene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.055N-Nitroso-di-n-propylamine
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.053N-Nitrosodiphenylamine
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.041Pentachlorophenol
0.16 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.045Phenanthrene
BRL 8270D P6H031410.35 8/18/16 23:24 JMVmg/kg dry 0.052Phenol
0.30 8270D P6H031410.35 8/18/16 23:24 JMVJmg/kg dry 0.046Pyrene
Surrogate Recovery Control Limits
39-13273 %2,4,6-Tribromophenol
44-11569 %2-Fluorobiphenyl
35-11565 %2-Fluorophenol
37-12260 %Nitrobenzene-d5
34-12166 %Phenol-d5
54-12766 %Terphenyl-d14
Total Metals
0.064 *7471B P6H031710.022 8/18/16 11:52 JABmg/kg dry 0.0012Mercury
0.43 *6020B P6H0348100.27 8/19/16 15:47 pfitzmg/kg dry 0.11Antimony
2.7 *6020B P6H0348101.6 8/19/16 15:47 pfitzmg/kg dry 0.14Arsenic
0.53 *6020B P6H0348100.27 8/19/16 15:47 pfitzmg/kg dry 0.11Beryllium
BRL *6020B P6H0348100.27 8/19/16 15:47 pfitzmg/kg dry 0.12Cadmium
24 *6020B P6H0348100.53 8/19/16 15:47 pfitzmg/kg dry 0.12Chromium
38 *6020B P6H0348100.53 8/19/16 15:47 pfitzBmg/kg dry 0.11Copper
48 *6020B P6H0348100.27 8/19/16 15:47 pfitzmg/kg dry 0.11Lead
12 *6020B P6H0348100.27 8/19/16 15:47 pfitzBmg/kg dry 0.090Nickel
BRL *6020B P6H0348101.1 8/19/16 15:47 pfitzmg/kg dry 0.11Selenium
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 32
Laboratory Report
02/23/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: SP-20160816
Prism Sample ID: 6080305-02
Prism Work Order: 6080305
Time Collected: 08/16/16 15:04
Time Submitted: 08/16/16 15:55
BRL *6020B P6H0348100.27 8/19/16 15:47 pfitzmg/kg dry 0.12Silver
BRL *6020B P6H0348100.27 8/19/16 15:47 pfitzmg/kg dry 0.11Thallium
95 *6020B P6H034810218/19/16 15:47 pfitzmg/kg dry 1.0Zinc
Volatile Organic Compounds by GC/MS
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000461,1,1,2-Tetrachloroethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000271,1,1-Trichloroethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000381,1,2,2-Tetrachloroethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000501,1,2-Trichloroethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000721,2,3-Trichloropropane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000421,2,4-Trichlorobenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000431,2,4-Trimethylbenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000341,2-Dichloroethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000431,3,5-Trimethylbenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000371,3-Dichlorobenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000281,3-Dichloropropane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000344-Chlorotoluene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.000274-Isopropyltoluene
0.090 8260B P6H038310.057 8/22/16 13:17 ANGmg/kg dry 0.0014Acetone
BRL 8260B P6H038310.0034 8/22/16 13:17 ANGmg/kg dry 0.00033Benzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00047Bromobenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00031Bromochloromethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00032Bromodichloromethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00064Bromoform
BRL 8260B P6H038310.011 8/22/16 13:17 ANGmg/kg dry 0.00070Bromomethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00030Chlorobenzene
BRL 8260B P6H038310.011 8/22/16 13:17 ANGmg/kg dry 0.00047Chloroethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00041Chloroform
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00038Chloromethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00026Dichlorodifluoromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 32
Laboratory Report
02/23/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID: SP-20160816
Prism Sample ID: 6080305-02
Prism Work Order: 6080305
Time Collected: 08/16/16 15:04
Time Submitted: 08/16/16 15:55
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00022Ethylbenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00033Isopropylbenzene (Cumene)
BRL 8260B P6H038310.011 8/22/16 13:17 ANGmg/kg dry 0.00052m,p-Xylenes
BRL 8260B P6H038310.057 8/22/16 13:17 ANGmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)
0.0046 8260B P6H038310.11 8/22/16 13:17 ANGJmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6H038310.057 8/22/16 13:17 ANGmg/kg dry 0.00048Methyl Isobutyl Ketone
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00032Methylene Chloride
BRL 8260B P6H038310.011 8/22/16 13:17 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P6H038310.011 8/22/16 13:17 ANGmg/kg dry 0.00018Naphthalene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00029n-Butylbenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00034n-Propylbenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00023o-Xylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00027sec-Butylbenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00034Styrene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00032Toluene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00037Trichloroethylene
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00037Trichlorofluoromethane
BRL 8260B P6H038310.028 8/22/16 13:17 ANGmg/kg dry 0.00077Vinyl acetate
BRL 8260B P6H038310.0057 8/22/16 13:17 ANGmg/kg dry 0.00027Vinyl chloride
BRL 8260B P6H038310.017 8/22/16 13:17 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130109 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-129102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6H0383 - 5035
Blank (P6H0383-BLK1)Prepared & Analyzed: 08/22/16
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6H0383 - 5035
Blank (P6H0383-BLK1)Prepared & Analyzed: 08/22/16
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.7
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10250.9
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.4
LCS (P6H0383-BS1)Prepared & Analyzed: 08/22/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0497 0.0050 0.05000 72-11599
1,1,1-Trichloroethane mg/kg wet0.0494 0.0050 0.05000 67-13199
1,1,2,2-Tetrachloroethane mg/kg wet0.0462 0.0050 0.05000 56-12692
1,1,2-Trichloroethane mg/kg wet0.0451 0.0050 0.05000 70-13390
1,1-Dichloroethane mg/kg wet0.0466 0.0050 0.05000 74-12793
1,1-Dichloroethylene mg/kg wet0.0526 0.0050 0.05000 67-149105
1,1-Dichloropropylene mg/kg wet0.0478 0.0050 0.05000 71-13096
1,2,3-Trichlorobenzene mg/kg wet0.0501 0.0050 0.05000 68-130100
1,2,3-Trichloropropane mg/kg wet0.0480 0.0050 0.05000 60-13796
1,2,4-Trichlorobenzene mg/kg wet0.0511 0.0050 0.05000 66-125102
1,2,4-Trimethylbenzene mg/kg wet0.0494 0.0050 0.05000 69-12999
1,2-Dibromoethane mg/kg wet0.0480 0.0050 0.05000 70-13296
1,2-Dichlorobenzene mg/kg wet0.0493 0.0050 0.05000 72-12399
1,2-Dichloroethane mg/kg wet0.0498 0.0050 0.05000 68-128100
1,2-Dichloropropane mg/kg wet0.0453 0.0050 0.05000 73-13091
1,3,5-Trimethylbenzene mg/kg wet0.0498 0.0050 0.05000 69-128100
1,3-Dichlorobenzene mg/kg wet0.0498 0.0050 0.05000 71-120100
1,3-Dichloropropane mg/kg wet0.0474 0.0050 0.05000 75-12495
1,4-Dichlorobenzene mg/kg wet0.0494 0.0050 0.05000 71-12399
2,2-Dichloropropane mg/kg wet0.0520 0.0050 0.05000 50-142104
2-Chlorotoluene mg/kg wet0.0509 0.0050 0.05000 67-124102
4-Chlorotoluene mg/kg wet0.0508 0.0050 0.05000 71-126102
4-Isopropyltoluene mg/kg wet0.0496 0.0050 0.05000 68-12999
Acetone mg/kg wet0.0930 0.050 0.1000 29-19893
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6H0383 - 5035
LCS (P6H0383-BS1)Prepared & Analyzed: 08/22/16
Benzene mg/kg wet0.0461 0.0030 0.05000 74-12792
Bromobenzene mg/kg wet0.0501 0.0050 0.05000 73-125100
Bromochloromethane mg/kg wet0.0458 0.0050 0.05000 72-13492
Bromodichloromethane mg/kg wet0.0504 0.0050 0.05000 75-122101
Bromoform mg/kg wet0.0484 0.0050 0.05000 66-13597
Bromomethane mg/kg wet0.0459 0.010 0.05000 20-18092
Carbon Tetrachloride mg/kg wet0.0508 0.0050 0.05000 64-143102
Chlorobenzene mg/kg wet0.0478 0.0050 0.05000 74-11896
Chloroethane mg/kg wet0.0343 0.010 0.05000 33-14969
Chloroform mg/kg wet0.0476 0.0050 0.05000 73-12795
Chloromethane mg/kg wet0.0415 0.0050 0.05000 45-14383
cis-1,2-Dichloroethylene mg/kg wet0.0500 0.0050 0.05000 76-134100
cis-1,3-Dichloropropylene mg/kg wet0.0489 0.0050 0.05000 71-12598
Dibromochloromethane mg/kg wet0.0511 0.0050 0.05000 73-122102
Dichlorodifluoromethane mg/kg wet0.0463 0.0050 0.05000 26-14693
Ethylbenzene mg/kg wet0.0487 0.0050 0.05000 74-12897
Isopropyl Ether mg/kg wet0.0422 0.0050 0.05000 59-15984
Isopropylbenzene (Cumene)mg/kg wet0.0498 0.0050 0.05000 68-126100
m,p-Xylenes mg/kg wet0.0999 0.010 0.1000 75-124100
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0469 0.050 0.05000 J61-15794
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0438 0.10 0.05000 J63-14988
Methyl Isobutyl Ketone mg/kg wet0.0446 0.050 0.05000 J57-16289
Methylene Chloride mg/kg wet0.0469 0.0050 0.05000 74-12994
Methyl-tert-Butyl Ether mg/kg wet0.0472 0.010 0.05000 70-13094
Naphthalene mg/kg wet0.0472 0.010 0.05000 57-15794
n-Butylbenzene mg/kg wet0.0509 0.0050 0.05000 65-135102
n-Propylbenzene mg/kg wet0.0508 0.0050 0.05000 67-130102
o-Xylene mg/kg wet0.0501 0.0050 0.05000 74-126100
sec-Butylbenzene mg/kg wet0.0500 0.0050 0.05000 66-131100
Styrene mg/kg wet0.0494 0.0050 0.05000 77-12199
tert-Butylbenzene mg/kg wet0.0507 0.0050 0.05000 67-132101
Tetrachloroethylene mg/kg wet0.0464 0.0050 0.05000 68-13093
Toluene mg/kg wet0.0467 0.0050 0.05000 71-12993
trans-1,2-Dichloroethylene mg/kg wet0.0490 0.0050 0.05000 73-13298
trans-1,3-Dichloropropylene mg/kg wet0.0498 0.0050 0.05000 68-123100
Trichloroethylene mg/kg wet0.0458 0.0050 0.05000 75-13392
Trichlorofluoromethane mg/kg wet0.0523 0.0050 0.05000 44-146105
Vinyl acetate mg/kg wet0.0457 0.025 0.05000 85-16191
Vinyl chloride mg/kg wet0.0448 0.0050 0.05000 48-14790
Xylenes, total mg/kg wet0.150 0.015 0.1500 74-126100
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.4
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10250.8
ug/L 50.00 76-129Surrogate: Toluene-d8 10050.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6H0383 - 5035
LCS Dup (P6H0383-BSD1)Prepared & Analyzed: 08/22/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0505 0.0050 0.05000 2072-115101 2
1,1,1-Trichloroethane mg/kg wet0.0497 0.0050 0.05000 2067-13199 0.5
1,1,2,2-Tetrachloroethane mg/kg wet0.0450 0.0050 0.05000 2056-12690 3
1,1,2-Trichloroethane mg/kg wet0.0464 0.0050 0.05000 2070-13393 3
1,1-Dichloroethane mg/kg wet0.0480 0.0050 0.05000 2074-12796 3
1,1-Dichloroethylene mg/kg wet0.0515 0.0050 0.05000 2067-149103 2
1,1-Dichloropropylene mg/kg wet0.0477 0.0050 0.05000 2071-13095 0.3
1,2,3-Trichlorobenzene mg/kg wet0.0499 0.0050 0.05000 2068-130100 0.3
1,2,3-Trichloropropane mg/kg wet0.0479 0.0050 0.05000 2060-13796 0.3
1,2,4-Trichlorobenzene mg/kg wet0.0500 0.0050 0.05000 2066-125100 2
1,2,4-Trimethylbenzene mg/kg wet0.0482 0.0050 0.05000 2069-12996 2
1,2-Dibromoethane mg/kg wet0.0492 0.0050 0.05000 2070-13298 3
1,2-Dichlorobenzene mg/kg wet0.0469 0.0050 0.05000 2072-12394 5
1,2-Dichloroethane mg/kg wet0.0506 0.0050 0.05000 2068-128101 2
1,2-Dichloropropane mg/kg wet0.0442 0.0050 0.05000 2073-13088 2
1,3,5-Trimethylbenzene mg/kg wet0.0480 0.0050 0.05000 2069-12896 4
1,3-Dichlorobenzene mg/kg wet0.0478 0.0050 0.05000 2071-12096 4
1,3-Dichloropropane mg/kg wet0.0463 0.0050 0.05000 2075-12493 2
1,4-Dichlorobenzene mg/kg wet0.0476 0.0050 0.05000 2071-12395 4
2,2-Dichloropropane mg/kg wet0.0521 0.0050 0.05000 2050-142104 0.2
2-Chlorotoluene mg/kg wet0.0495 0.0050 0.05000 2067-12499 3
4-Chlorotoluene mg/kg wet0.0490 0.0050 0.05000 2071-12698 4
4-Isopropyltoluene mg/kg wet0.0473 0.0050 0.05000 2068-12995 5
Acetone mg/kg wet0.0955 0.050 0.1000 2029-19895 3
Benzene mg/kg wet0.0466 0.0030 0.05000 2074-12793 1
Bromobenzene mg/kg wet0.0482 0.0050 0.05000 2073-12596 4
Bromochloromethane mg/kg wet0.0462 0.0050 0.05000 2072-13492 0.8
Bromodichloromethane mg/kg wet0.0510 0.0050 0.05000 2075-122102 1
Bromoform mg/kg wet0.0478 0.0050 0.05000 2066-13596 1
Bromomethane mg/kg wet0.0469 0.010 0.05000 2020-18094 2
Carbon Tetrachloride mg/kg wet0.0518 0.0050 0.05000 2064-143104 2
Chlorobenzene mg/kg wet0.0470 0.0050 0.05000 2074-11894 2
Chloroethane mg/kg wet0.0346 0.010 0.05000 2033-14969 0.6
Chloroform mg/kg wet0.0476 0.0050 0.05000 2073-12795 0.08
Chloromethane mg/kg wet0.0428 0.0050 0.05000 2045-14386 3
cis-1,2-Dichloroethylene mg/kg wet0.0502 0.0050 0.05000 2076-134100 0.5
cis-1,3-Dichloropropylene mg/kg wet0.0500 0.0050 0.05000 2071-125100 2
Dibromochloromethane mg/kg wet0.0499 0.0050 0.05000 2073-122100 3
Dichlorodifluoromethane mg/kg wet0.0452 0.0050 0.05000 2026-14690 2
Ethylbenzene mg/kg wet0.0476 0.0050 0.05000 2074-12895 2
Isopropyl Ether mg/kg wet0.0431 0.0050 0.05000 2059-15986 2
Isopropylbenzene (Cumene)mg/kg wet0.0482 0.0050 0.05000 2068-12696 3
m,p-Xylenes mg/kg wet0.0980 0.010 0.1000 2075-12498 2
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0467 0.050 0.05000 20 J61-15793 0.4
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0444 0.10 0.05000 20 J63-14989 1
Methyl Isobutyl Ketone mg/kg wet0.0455 0.050 0.05000 20 J57-16291 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6H0383 - 5035
LCS Dup (P6H0383-BSD1)Prepared & Analyzed: 08/22/16
Methylene Chloride mg/kg wet0.0467 0.0050 0.05000 2074-12993 0.4
Methyl-tert-Butyl Ether mg/kg wet0.0486 0.010 0.05000 2070-13097 3
Naphthalene mg/kg wet0.0475 0.010 0.05000 2057-15795 0.8
n-Butylbenzene mg/kg wet0.0485 0.0050 0.05000 2065-13597 5
n-Propylbenzene mg/kg wet0.0484 0.0050 0.05000 2067-13097 5
o-Xylene mg/kg wet0.0492 0.0050 0.05000 2074-12698 2
sec-Butylbenzene mg/kg wet0.0479 0.0050 0.05000 2066-13196 4
Styrene mg/kg wet0.0492 0.0050 0.05000 2077-12198 0.4
tert-Butylbenzene mg/kg wet0.0478 0.0050 0.05000 2067-13296 6
Tetrachloroethylene mg/kg wet0.0459 0.0050 0.05000 2068-13092 1
Toluene mg/kg wet0.0468 0.0050 0.05000 2071-12994 0.1
trans-1,2-Dichloroethylene mg/kg wet0.0496 0.0050 0.05000 2073-13299 1
trans-1,3-Dichloropropylene mg/kg wet0.0502 0.0050 0.05000 2068-123100 0.9
Trichloroethylene mg/kg wet0.0488 0.0050 0.05000 2075-13398 6
Trichlorofluoromethane mg/kg wet0.0510 0.0050 0.05000 2044-146102 3
Vinyl acetate mg/kg wet0.0480 0.025 0.05000 2085-16196 5
Vinyl chloride mg/kg wet0.0457 0.0050 0.05000 2048-14791 2
Xylenes, total mg/kg wet0.147 0.015 0.1500 2074-12698 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.6
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10351.4
ug/L 50.00 76-129Surrogate: Toluene-d8 10150.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6H0314 - 3546
Blank (P6H0314-BLK1)Prepared & Analyzed: 08/18/16
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3'-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6H0314 - 3546
Blank (P6H0314-BLK1)Prepared & Analyzed: 08/18/16
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.329 39-132Surrogate: 2,4,6-Tribromophenol 953.16
mg/kg wet 1.664 44-115Surrogate: 2-Fluorobiphenyl 881.46
mg/kg wet 3.329 35-115Surrogate: 2-Fluorophenol 923.07
mg/kg wet 1.664 37-122Surrogate: Nitrobenzene-d5 831.38
mg/kg wet 3.329 34-121Surrogate: Phenol-d5 943.11
mg/kg wet 1.664 54-127Surrogate: Terphenyl-d14 891.49
LCS (P6H0314-BS1)Prepared & Analyzed: 08/18/16
1,2,4-Trichlorobenzene mg/kg wet1.05 0.33 1.666 34-11863
1,2-Dichlorobenzene mg/kg wet0.952 0.33 1.666 33-11757
1,3-Dichlorobenzene mg/kg wet0.903 0.33 1.666 30-11554
1,4-Dichlorobenzene mg/kg wet0.918 0.33 1.666 31-11555
1-Methylnaphthalene mg/kg wet1.23 0.33 1.666 40-11974
2,4,6-Trichlorophenol mg/kg wet1.28 0.33 1.666 39-12677
2,4-Dichlorophenol mg/kg wet1.26 0.33 1.666 40-12276
2,4-Dimethylphenol mg/kg wet1.27 0.33 1.666 30-12776
2,4-Dinitrophenol mg/kg wet1.03 0.33 1.666 27-12962
2,4-Dinitrotoluene mg/kg wet1.46 0.33 1.666 48-12687
2,6-Dinitrotoluene mg/kg wet1.33 0.33 1.666 46-12480
2-Chloronaphthalene mg/kg wet1.62 0.33 1.666 41-11497
2-Chlorophenol mg/kg wet1.10 0.33 1.666 34-12166
2-Methylnaphthalene mg/kg wet1.18 0.33 1.666 38-12271
2-Methylphenol mg/kg wet1.16 0.33 1.666 32-12270
2-Nitrophenol mg/kg wet1.11 0.33 1.666 36-12367
3,3'-Dichlorobenzidine mg/kg wet1.37 0.33 1.666 22-12182
3/4-Methylphenol mg/kg wet1.22 0.33 1.666 34-11973
4,6-Dinitro-2-methylphenol mg/kg wet1.25 0.33 1.666 29-13275
4-Bromophenyl phenyl ether mg/kg wet1.45 0.33 1.666 46-12487
4-Chloro-3-methylphenol mg/kg wet1.32 0.33 1.666 45-12279
4-Chloroaniline mg/kg wet1.22 0.33 1.666 17-10673
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6H0314 - 3546
LCS (P6H0314-BS1)Prepared & Analyzed: 08/18/16
4-Chlorophenyl phenyl ether mg/kg wet1.43 0.33 1.666 45-12186
4-Nitrophenol mg/kg wet1.47 0.33 1.666 30-13288
Acenaphthene mg/kg wet1.36 0.33 1.666 40-12382
Acenaphthylene mg/kg wet1.38 0.33 1.666 32-13283
Anthracene mg/kg wet1.58 0.33 1.666 47-12395
Azobenzene mg/kg wet1.41 0.33 1.666 39-12584
Benzo(a)anthracene mg/kg wet1.54 0.33 1.666 49-12692
Benzo(a)pyrene mg/kg wet1.48 0.33 1.666 45-12989
Benzo(b)fluoranthene mg/kg wet1.43 0.33 1.666 45-13286
Benzo(g,h,i)perylene mg/kg wet1.41 0.33 1.666 43-13484
Benzo(k)fluoranthene mg/kg wet1.44 0.33 1.666 47-13286
Benzoic Acid mg/kg wet0.905 0.33 1.666 10-8354
Benzyl alcohol mg/kg wet1.11 0.33 1.666 29-12267
bis(2-Chloroethoxy)methane mg/kg wet1.18 0.33 1.666 36-12171
Bis(2-Chloroethyl)ether mg/kg wet1.05 0.33 1.666 31-12063
Bis(2-chloroisopropyl)ether mg/kg wet1.14 0.33 1.666 33-13168
Bis(2-Ethylhexyl)phthalate mg/kg wet1.49 0.33 1.666 51-13389
Butyl benzyl phthalate mg/kg wet1.50 0.33 1.666 48-13290
Chrysene mg/kg wet1.58 0.33 1.666 50-12495
Dibenzo(a,h)anthracene mg/kg wet1.41 0.33 1.666 45-13485
Dibenzofuran mg/kg wet1.39 0.33 1.666 44-12083
Diethyl phthalate mg/kg wet1.44 0.33 1.666 50-12486
Dimethyl phthalate mg/kg wet1.36 0.33 1.666 48-12482
Di-n-butyl phthalate mg/kg wet1.55 0.33 1.666 51-12893
Di-n-octyl phthalate mg/kg wet1.39 0.33 1.666 45-14084
Fluoranthene mg/kg wet1.52 0.33 1.666 50-12791
Fluorene mg/kg wet1.49 0.33 1.666 43-12590
Hexachlorobenzene mg/kg wet1.38 0.33 1.666 45-12283
Hexachlorobutadiene mg/kg wet1.03 0.33 1.666 32-12362
Hexachlorocyclopentadiene mg/kg wet1.03 0.33 1.666 32-11762
Hexachloroethane mg/kg wet0.911 0.33 1.666 28-11755
Indeno(1,2,3-cd)pyrene mg/kg wet1.45 0.33 1.666 45-13387
Isophorone mg/kg wet1.20 0.33 1.666 30-12272
Naphthalene mg/kg wet1.15 0.33 1.666 35-12369
Nitrobenzene mg/kg wet1.11 0.33 1.666 34-12267
N-Nitroso-di-n-propylamine mg/kg wet1.14 0.33 1.666 36-12068
N-Nitrosodiphenylamine mg/kg wet1.45 0.33 1.666 38-12787
Pentachlorophenol mg/kg wet1.39 0.33 1.666 25-13384
Phenanthrene mg/kg wet1.54 0.33 1.666 50-12192
Phenol mg/kg wet1.18 0.33 1.666 34-12171
Pyrene mg/kg wet1.52 0.33 1.666 47-12791
mg/kg wet 3.332 39-132Surrogate: 2,4,6-Tribromophenol 903.01
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 761.26
mg/kg wet 3.332 35-115Surrogate: 2-Fluorophenol 722.41
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 681.12
mg/kg wet 3.332 34-121Surrogate: Phenol-d5 752.48
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6H0314 - 3546
LCS (P6H0314-BS1)Prepared & Analyzed: 08/18/16
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 771.28
LCS Dup (P6H0314-BSD1)Prepared & Analyzed: 08/18/16
1,2,4-Trichlorobenzene mg/kg wet0.984 0.33 1.666 2034-11859 6
1,2-Dichlorobenzene mg/kg wet0.867 0.33 1.666 2033-11752 9
1,3-Dichlorobenzene mg/kg wet0.834 0.33 1.666 2030-11550 8
1,4-Dichlorobenzene mg/kg wet0.857 0.33 1.666 2031-11551 7
1-Methylnaphthalene mg/kg wet1.20 0.33 1.666 2040-11972 2
2,4,6-Trichlorophenol mg/kg wet1.29 0.33 1.666 2039-12678 1
2,4-Dichlorophenol mg/kg wet1.25 0.33 1.666 2040-12275 0.3
2,4-Dimethylphenol mg/kg wet1.26 0.33 1.666 2030-12776 0.8
2,4-Dinitrophenol mg/kg wet1.10 0.33 1.666 2027-12966 7
2,4-Dinitrotoluene mg/kg wet1.49 0.33 1.666 2048-12689 2
2,6-Dinitrotoluene mg/kg wet1.36 0.33 1.666 2046-12481 2
2-Chloronaphthalene mg/kg wet1.60 0.33 1.666 2041-11496 2
2-Chlorophenol mg/kg wet1.05 0.33 1.666 2034-12163 5
2-Methylnaphthalene mg/kg wet1.14 0.33 1.666 2038-12269 3
2-Methylphenol mg/kg wet1.13 0.33 1.666 2032-12268 3
2-Nitrophenol mg/kg wet1.06 0.33 1.666 2036-12364 5
3,3'-Dichlorobenzidine mg/kg wet1.47 0.33 1.666 2022-12188 7
3/4-Methylphenol mg/kg wet1.22 0.33 1.666 2034-11974 0.4
4,6-Dinitro-2-methylphenol mg/kg wet1.33 0.33 1.666 2029-13280 6
4-Bromophenyl phenyl ether mg/kg wet1.46 0.33 1.666 2046-12488 0.5
4-Chloro-3-methylphenol mg/kg wet1.35 0.33 1.666 2045-12281 2
4-Chloroaniline mg/kg wet1.22 0.33 1.666 2017-10674 0.02
4-Chlorophenyl phenyl ether mg/kg wet1.42 0.33 1.666 2045-12185 0.8
4-Nitrophenol mg/kg wet1.51 0.33 1.666 2030-13291 2
Acenaphthene mg/kg wet1.33 0.33 1.666 2040-12380 2
Acenaphthylene mg/kg wet1.39 0.33 1.666 2032-13283 0.6
Anthracene mg/kg wet1.61 0.33 1.666 2047-12396 1
Azobenzene mg/kg wet1.41 0.33 1.666 2039-12584 0.08
Benzo(a)anthracene mg/kg wet1.60 0.33 1.666 2049-12696 4
Benzo(a)pyrene mg/kg wet1.51 0.33 1.666 2045-12991 2
Benzo(b)fluoranthene mg/kg wet1.47 0.33 1.666 2045-13288 3
Benzo(g,h,i)perylene mg/kg wet1.43 0.33 1.666 2043-13486 2
Benzo(k)fluoranthene mg/kg wet1.51 0.33 1.666 2047-13291 5
Benzoic Acid mg/kg wet0.954 0.33 1.666 2010-8357 5
Benzyl alcohol mg/kg wet1.06 0.33 1.666 2029-12264 4
bis(2-Chloroethoxy)methane mg/kg wet1.14 0.33 1.666 2036-12168 3
Bis(2-Chloroethyl)ether mg/kg wet0.959 0.33 1.666 2031-12058 9
Bis(2-chloroisopropyl)ether mg/kg wet1.07 0.33 1.666 2033-13164 6
Bis(2-Ethylhexyl)phthalate mg/kg wet1.56 0.33 1.666 2051-13394 5
Butyl benzyl phthalate mg/kg wet1.55 0.33 1.666 2048-13293 4
Chrysene mg/kg wet1.65 0.33 1.666 2050-12499 4
Dibenzo(a,h)anthracene mg/kg wet1.45 0.33 1.666 2045-13487 3
Dibenzofuran mg/kg wet1.37 0.33 1.666 2044-12082 1
Diethyl phthalate mg/kg wet1.48 0.33 1.666 2050-12489 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6H0314 - 3546
LCS Dup (P6H0314-BSD1)Prepared & Analyzed: 08/18/16
Dimethyl phthalate mg/kg wet1.38 0.33 1.666 2048-12483 2
Di-n-butyl phthalate mg/kg wet1.59 0.33 1.666 2051-12895 2
Di-n-octyl phthalate mg/kg wet1.42 0.33 1.666 2045-14085 2
Fluoranthene mg/kg wet1.55 0.33 1.666 2050-12793 2
Fluorene mg/kg wet1.49 0.33 1.666 2043-12589 0.3
Hexachlorobenzene mg/kg wet1.42 0.33 1.666 2045-12285 3
Hexachlorobutadiene mg/kg wet0.951 0.33 1.666 2032-12357 8
Hexachlorocyclopentadiene mg/kg wet0.936 0.33 1.666 2032-11756 9
Hexachloroethane mg/kg wet0.854 0.33 1.666 2028-11751 6
Indeno(1,2,3-cd)pyrene mg/kg wet1.49 0.33 1.666 2045-13389 3
Isophorone mg/kg wet1.19 0.33 1.666 2030-12271 0.6
Naphthalene mg/kg wet1.11 0.33 1.666 2035-12367 3
Nitrobenzene mg/kg wet1.04 0.33 1.666 2034-12263 6
N-Nitroso-di-n-propylamine mg/kg wet1.13 0.33 1.666 2036-12068 1
N-Nitrosodiphenylamine mg/kg wet1.47 0.33 1.666 2038-12788 1
Pentachlorophenol mg/kg wet1.44 0.33 1.666 2025-13386 3
Phenanthrene mg/kg wet1.60 0.33 1.666 2050-12196 4
Phenol mg/kg wet1.16 0.33 1.666 2034-12169 2
Pyrene mg/kg wet1.56 0.33 1.666 2047-12794 3
mg/kg wet 3.331 39-132Surrogate: 2,4,6-Tribromophenol 913.03
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 741.23
mg/kg wet 3.331 35-115Surrogate: 2-Fluorophenol 682.28
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 641.07
mg/kg wet 3.331 34-121Surrogate: Phenol-d5 722.39
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 781.30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6H0317 - 7471B
Blank (P6H0317-BLK1)Prepared & Analyzed: 08/18/16
Mercury mg/kg wetBRL0.020
LCS (P6H0317-BS1)Prepared & Analyzed: 08/18/16
Mercury mg/kg wet0.442 0.020 0.4167 80-120106
Matrix Spike (P6H0317-MS1)Prepared & Analyzed: 08/18/16 Source: 6080305-01
Mercury mg/kg dry0.496 0.021 0.4300 0.0622 80-120101
Matrix Spike Dup (P6H0317-MSD1)Prepared & Analyzed: 08/18/16 Source: 6080305-01
Mercury mg/kg dry0.536 0.022 0.4671 0.0622 2080-120101 8
Batch P6H0348 - 3050B
Blank (P6H0348-BLK1)Prepared & Analyzed: 08/19/16
Antimony mg/kg wetBRL0.25
Arsenic mg/kg wetBRL1.5
Beryllium mg/kg wetBRL0.25
Cadmium mg/kg wetBRL0.25
Chromium mg/kg wetBRL0.50
Copper mg/kg wet2.74 0.50 BH
Lead mg/kg wetBRL0.25
Nickel mg/kg wet1.52 0.25 B
Selenium mg/kg wetBRL1.0
Silver mg/kg wetBRL0.25
Thallium mg/kg wetBRL0.25
Zinc mg/kg wetBRL20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6H0348 - 3050B
LCS (P6H0348-BS1)Prepared & Analyzed: 08/19/16
Antimony mg/kg wet24.3 0.25 25.00 80-12097
Arsenic mg/kg wet23.5 1.5 25.00 80-12094
Beryllium mg/kg wet23.1 0.25 25.00 80-12092
Cadmium mg/kg wet24.7 0.25 25.00 80-12099
Chromium mg/kg wet23.3 0.50 25.00 80-12093
Copper mg/kg wet24.4 0.50 25.00 B80-12098
Lead mg/kg wet25.5 0.25 25.00 80-120102
Nickel mg/kg wet23.7 0.25 25.00 B80-12095
Selenium mg/kg wet22.9 1.0 25.00 80-12091
Silver mg/kg wet10.3 0.25 10.00 80-120103
Thallium mg/kg wet25.1 0.25 25.00 80-120100
Zinc mg/kg wet23.5 20 25.00 80-12094
Matrix Spike (P6H0348-MS1)Prepared & Analyzed: 08/19/16 Source: 6080305-01
Antimony mg/kg dry6.81 0.27 26.56 0.431 MI75-12524
Arsenic mg/kg dry25.9 1.6 26.56 2.60 75-12588
Beryllium mg/kg dry24.2 0.27 26.56 0.536 75-12589
Cadmium mg/kg dry25.5 0.27 26.56 0.156 75-12595
Chromium mg/kg dry60.9 0.53 26.56 28.2 75-125123
Copper mg/kg dry61.9 0.53 26.56 34.9 B75-125102
Lead mg/kg dry62.9 0.27 26.56 33.2 75-125112
Nickel mg/kg dry38.3 0.27 26.56 10.1 B75-125106
Selenium mg/kg dry22.8 1.1 26.56 0.213 75-12585
Silver mg/kg dry10.7 0.27 10.62 BRL 75-125101
Thallium mg/kg dry25.0 0.27 26.56 0.125 75-12594
Zinc mg/kg dry98.1 21 26.56 69.2 75-125109
Matrix Spike Dup (P6H0348-MSD1)Prepared & Analyzed: 08/19/16 Source: 6080305-01
Antimony mg/kg dry3.81 0.27 27.23 0.431 20 D, MI75-12512 56
Arsenic mg/kg dry24.3 1.6 27.23 2.60 2075-12580 6
Beryllium mg/kg dry25.4 0.27 27.23 0.536 2075-12591 5
Cadmium mg/kg dry26.0 0.27 27.23 0.156 2075-12595 2
Chromium mg/kg dry51.9 0.54 27.23 28.2 2075-12587 16
Copper mg/kg dry65.8 0.54 27.23 34.9 20 B75-125113 6
Lead mg/kg dry65.2 0.27 27.23 33.2 2075-125117 4
Nickel mg/kg dry40.1 0.27 27.23 10.1 20 B75-125110 5
Selenium mg/kg dry22.8 1.1 27.23 0.213 2075-12583 0.2
Silver mg/kg dry10.8 0.27 10.89 BRL 2075-12599 1
Thallium mg/kg dry25.2 0.27 27.23 0.125 2075-12592 0.8
Zinc mg/kg dry99.7 22 27.23 69.2 2075-125112 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6H0348 - 3050B
Post Spike (P6H0348-PS1)Prepared & Analyzed: 08/19/16 Source: 6080305-01
Antimony ug/L171 200.0 1.57 80-12085
Arsenic ug/L179 200.0 9.49 80-12085
Beryllium ug/L178 200.0 1.96 80-12088
Cadmium ug/L172 200.0 0.571 80-12086
Chromium ug/L267 200.0 103 80-12082
Copper ug/L300 200.0 128 B80-12086
Lead ug/L281 200.0 121 80-12080
Nickel ug/L210 200.0 36.9 B80-12087
Selenium ug/L165 200.0 0.779 80-12082
Silver ug/L181 200.0 0.276 80-12090
Thallium ug/L167 200.0 0.455 80-12083
Zinc ug/L406 200.0 253 M80-12077
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 32
2/23/17
Level II QC Report
2923 South Tryon St. Ste 100
Project: MPV-025Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Prism Work Order: 6080305
Time Submitted: 8/16/2016 3:55:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P6H0334 - Solids, Dry Weight
Duplicate (P6H0334-DUP6)Prepared: 08/17/16 Analyzed: 08/18/16 Source: 6080305-01
% Solids % by Weight91.9 0.100 92.3 200.4
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P6H03346080305-01 08/17/16 14:3930 30g g
P6H03346080305-02 08/17/16 14:3930 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P6H03146080305-01 08/18/16 8:5830 1g mL
P6H03146080305-02 08/18/16 8:5830.36 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P6H03486080305-01 08/19/16 9:501.98 50g mL
P6H03486080305-02 08/19/16 9:502.01 50g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P6H03176080305-01 08/18/16 9:300.58 50g mL
P6H03176080305-02 08/18/16 9:300.59 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P6H03836080305-01 08/22/16 9:204.37 5g mL
P6H03836080305-02 08/22/16 9:204.74 5g mL
Subcontracted Analyses
Lab Number
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Analysis
6080305-01 Hexavalent Chromium (Sub)
6080305-02 Hexavalent Chromium (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 32
Page 26 of 32
Page 27 of 32
Page 28 of 32
Page 29 of 32
Page 30 of 32
Page 31 of 32
Page 32 of 32

APPENDIX C

Waste Disposal Documents